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Title: First experimental feasibility study of VIPIC: a custom-made detector for X-ray speckle measurements

Journal Article · · Journal of Synchrotron Radiation (Online)
 [1];  [1];  [2];  [3];  [1];  [4];  [5];  [5];  [5];  [5];  [1];  [6]
  1. Brookhaven National Lab. (BNL), Upton, NY (United States)
  2. Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States)
  3. AGH Univ. of Science and Technology, Krakow (Poland). Dept. of Metrology and Electronics
  4. SLAC National Accelerator Lab., Menlo Park, CA (United States)
  5. Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS), X-ray Science Division
  6. McGill Univ., Montreal, QC (Canada). Dept of Physics

The Vertically Integrated Photon Imaging Chip (VIPIC) was custom-designed for X-ray photon correlation spectroscopy, an application in which occupancy per pixel is low but high time resolution is needed. VIPIC operates in a sparsified streaming mode in which each detected photon is immediately read out as a time- and position-stamped event. This event stream can be fed directly to an autocorrelation engine or accumulated to form a conventional image. The detector only delivers non-zero data (sparsified readout), greatly reducing the communications overhead typical of conventional frame-oriented detectors such as charge-coupled devices or conventional hybrid pixel detectors. This feature allowscontinuousacquisition of data with timescales from microseconds to hours. In this work VIPIC has been used to measure X-ray photon correlation spectroscopy data on polystyrene latex nano-colliodal suspensions in glycerol and on colloidal suspensions of silica spheres in water. Relaxation times of the nano-colloids have been measured for different temperatures. These results demonstrate that VIPIC can operatecontinuouslyin the microsecond time frame, while at the same time probing longer timescales.

Research Organization:
SLAC National Accelerator Lab., Menlo Park, CA (United States); Fermi National Accelerator Lab. (FNAL), Batavia, IL (United States); Argonne National Lab. (ANL), Argonne, IL (United States); Brookhaven National Lab. (BNL), Upton, NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
AC02-76SF00515; AC02-06CH11357; SC0012704; SC00112704
OSTI ID:
1256705
Alternate ID(s):
OSTI ID: 1331594; OSTI ID: 1354368
Report Number(s):
BNL-112884-2016-JA; JSYRES; PII: S1600577516000114
Journal Information:
Journal of Synchrotron Radiation (Online), Vol. 23, Issue 2; ISSN 1600-5775
Publisher:
International Union of CrystallographyCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 6 works
Citation information provided by
Web of Science

References (14)

X-ray imaging detectors for synchrotron and XFEL sources journal April 2015
Photon Correlation Spectroscopy of Colloidal Palladium Using a Coherent X-Ray Beam journal December 1996
X-Ray Photon Correlation Spectroscopy Study of Brownian Motion of Gold Colloids in Glycerol journal July 1995
Dynamics and rheology under continuous shear flow studied by x-ray photon correlation spectroscopy journal March 2010
Through-silicon-via aware interconnect prediction and optimization for 3D stacked ICs conference January 2009
Dynamics in shear flow studied by X-ray Photon Correlation Spectroscopy journal April 2008
Mean and variance of single photon counting with deadtime journal June 2000
A theoretical framework for the Vogel-Fulcher-Tammann equation for covalent network glasses derived by the stochastic matrix method journal October 2000
Temperature-dependent structural arrest of silica colloids in a water–lutidine binary mixture journal January 2010
Test Challenges for 3D Integrated Circuits journal September 2009
Relationship between Structural and Stress Relaxation in a Block-Copolymer Melt journal June 2006
Jamming Behavior of Domains in a Spiral Antiferromagnetic System journal May 2013
X-ray photon correlation spectroscopy under flow journal May 2008
Measurement of the velocity difference by photon correlation spectroscopy: an improved scheme journal January 1997

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