Rational design of efficient electrode–electrolyte interfaces for solid-state energy storage using ion soft landing

Prabhakaran, Venkateshkumar; Mehdi, B. Layla; Ditto, Jeffrey J.; Engelhard, Mark H.; Wang, Bingbing; Gunaratne, K. Don D.; Johnson, David C.; Browning, Nigel D.; Johnson, Grant E.; Laskin, Julia

doi:10.1038/ncomms11399

Title: Rational design of efficient electrode–electrolyte interfaces for solid-state energy storage using ion soft landing

Journal Article · Thu Apr 21 00:00:00 EDT 2016 · Nature Communications

DOI:https://doi.org/10.1038/ncomms11399· OSTI ID:1253857

Prabhakaran, Venkateshkumar ^[1]; Mehdi, B. Layla ^[1]; Ditto, Jeffrey J. ^[2]; Engelhard, Mark H. ^[1]; Wang, Bingbing ^[1]; Gunaratne, K. Don D. ^[1]; Johnson, David C. ^[2]; Browning, Nigel D. ^[1]; Johnson, Grant E. ^[1]; Laskin, Julia ^[1]

Pacific Northwest National Lab. (PNNL), Richland, WA (United States)
Univ. of Oregon, Eugene, OR (United States)

Here, the rational design of improved electrode-electrolyte interfaces (EEI) for energy storage is critically dependent on a molecular-level understanding of ionic interactions and nanoscale phenomena. The presence of non-redox active species at EEI has been shown to strongly influence Faradaic efficiency and long-term operational stability during energy storage processes. Herein, we achieve substantially higher performance and long-term stability of EEI prepared with highly-dispersed discrete redox-active cluster anions (50 ng of pure ~0.7 nm size molybdenum polyoxometalate anions (POM) anions on 25 mg (≈ 0.2 wt%) carbon nanotube (CNT) electrodes) by complete elimination of strongly coordinating non-redox species through ion soft-landing (SL). For the first time, electron microscopy provides atomically-resolved images of individual POM species directly on complex technologically relevant CNT electrodes. In this context, SL is established as a versatile approach for the controlled design of novel surfaces for both fundamental and applied research in energy storage.

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Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Organization:: USDOE

Grant/Contract Number:: AC05-76RL01830

OSTI ID:: 1253857

Report Number(s):: PNNL-SA-113159; ncomms11399

Journal Information:: Nature Communications, Vol. 7; ISSN 2041-1723

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 71 works

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