Time-resolved x-ray diffraction and electrical resistance measurements of structural phase transitions in zirconium

Velisavljevic, Nenad; Sinogeikin, Stanislav; Saavedra, Ramon A.; Chellappa, Raja S.; Rothkirch, Andre; Dattelbaum, Dana M.; Konopkova, Zuzana; Liermann, Hans-Peter; Bishop, Matthew M.; Tsoi, Georgiy M.; Vohra, Yogesh K.

doi:10.1088/1742-6596/500/3/032020

Title: Time-resolved x-ray diffraction and electrical resistance measurements of structural phase transitions in zirconium

Journal Article · Wed May 07 00:00:00 EDT 2014 · Journal of Physics. Conference Series (Online)

DOI:https://doi.org/10.1088/1742-6596/500/3/032020· OSTI ID:1764194

^[1]; Sinogeikin, Stanislav ^[2];

^[1]; Chellappa, Raja S. ^[1]; Rothkirch, Andre ^[3];

^[1]; Konopkova, Zuzana ^[3]; Liermann, Hans-Peter ^[3]; Bishop, Matthew M. ^[4]; Tsoi, Georgiy M. ^[4]; Vohra, Yogesh K. ^[4]

Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Carnegie Inst. of Washington, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT)
Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
Univ. of Alabama, Birmingham, AL (United States)

Here, we have designed a portable pressure controller module to tune compression rates and maximum pressures attainable in a standard gas-membrane diamond anvil cell (DAC). During preliminary experiments, performed on zirconium (Zr) metal sample, pressure jumps of up to 80 GPa were systematically obtained in less than 0.2s (resulting in compression rate of few GPa/s up to more than 400 GPa/s). In-situ x-ray diffraction and electrical resistance measurements were performed simultaneously during this rapid pressure increase to provide the first time resolved data on α → ω → β structural evolution in Zr at high pressures. Direct control of compression rates and peak pressures, which can be held for prolonged time, allows for investigation of structural evolution and kinetics of structural phase transitions of materials under previously unexplored compression rate-pressure conditions that bridge traditional static and shock/dynamic experimental platforms.

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Research Organization:: Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS); Univ. of Alabama, Birmingham, AL (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES); German Federal Ministry of Education and Research (BMBF); National Science Foundation (NSF)

Grant/Contract Number:: 89233218CNA000001; NA0002014; AC52-06NA25396; NA0001974; FG02-99ER45775; AC02-06CH11357; 05KS7RF1

OSTI ID:: 1764194

Alternate ID(s):: OSTI ID: 1251164

Report Number(s):: LA-UR-13-28748

Journal Information:: Journal of Physics. Conference Series (Online), Vol. 500, Issue 3; ISSN 1742-6596

Publisher:: Institute of Physics (IOP)Copyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 9 works

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References (10)

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Cited By (4)

Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression Smith, Jesse S.; Sinogeikin, Stanislav V.; Lin, Chuanlong Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926887	journal	July 2015
Online remote control systems for static and dynamic compression and decompression using diamond anvil cells Sinogeikin, Stanislav V.; Smith, Jesse S.; Rod, Eric Review of Scientific Instruments, Vol. 86, Issue 7 https://doi.org/10.1063/1.4926892	journal	July 2015
Room-temperature compression and equation of state of body-centered cubic zirconium Pigott, Jeffrey S.; Velisavljevic, Nenad; Moss, Eric K. Journal of Physics: Condensed Matter, Vol. 32, Issue 12 https://doi.org/10.1088/1361-648x/ab5e6e	journal	December 2019
The Extreme Conditions Beamline P02.2 and the Extreme Conditions Science Infrastructure at PETRA III Liermann, H. -P.; Konôpková, Z.; Morgenroth, W. Journal of Synchrotron Radiation, Vol. 22, Issue 4 https://doi.org/10.1107/s1600577515005937	journal	June 2015

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36 MATERIALS SCIENCE
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