Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials

Huang, X. J.; Yang, W. G.; Harder, R.; Sun, Y.; Lu, M.; Chu, Y. S.; Robinson, I. K.; Mao, H. K.

doi:10.1021/acs.nanolett.5b03568

Title: Deformation twinning of a silver nanocrystal under high pressure. Supplementary materials

Journal Article · Tue Oct 20 00:00:00 EDT 2015 · Nano Letters

DOI:https://doi.org/10.1021/acs.nanolett.5b03568· OSTI ID:1237176

Huang, X. J. ^[1]; Yang, W. G. ^[2]; Harder, R. ^[3]; Sun, Y. ^[3]; Lu, M. ^[4]; Chu, Y. S. ^[4]; Robinson, I. K. ^[5]; Mao, H. K. ^[6]

Brookhaven National Lab. (BNL), Upton, NY (United States); Argonne National Lab. (ANL), Argonne, IL (United States)
Argonne National Lab. (ANL), Argonne, IL (United States); Center for High Pressure Science and Technology Advanced Research, Shanghai (China)
Argonne National Lab. (ANL), Argonne, IL (United States)
Brookhaven National Lab. (BNL), Upton, NY (United States)
Univ. College London, Bloomsbury (United Kingdom); Research Complex at Harwell, Didcot (United Kingdom)
Center for High Pressure Science and Technology Advanced Research, Shanghai (China)

Within a high-pressure environment, crystal deformation is controlled by complex processes such as dislocation motion, twinning, and phase transitions, which change materials’ microscopic morphology and alter their properties. Understanding a crystal’s response to external stress provides a unique opportunity for rational tailoring of its functionalities. It is very challenging to track the strain evolution and physical deformation from a single nanoscale crystal under high-pressure stress. Here, we report an in situ three-dimensional mapping of morphology and strain evolutions in a single-crystal silver nanocube within a high-pressure environment using the Bragg Coherent Diffractive Imaging (CDI) method. We observed a continuous lattice distortion, followed by a deformation twining process at a constant pressure. As a result, the ability to visualize stress-introduced deformation of nanocrystals with high spatial resolution and prominent strain sensitivity provides an important route for interpreting and engineering novel properties of nanomaterials.

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Research Organization:: Brookhaven National Laboratory (BNL), Upton, NY (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: SC00112704

OSTI ID:: 1237176

Alternate ID(s):: OSTI ID: 1237177; OSTI ID: 1340331

Report Number(s):: BNL-108436-2015-JA; BNL-108437-2015-JA; BNL-111705-2016-JA; R&D Project: LS001

Journal Information:: Nano Letters, Vol. 15, Issue 11; ISSN 1530-6984

Publisher:: American Chemical SocietyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 23 works

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