High pressure Laue diffraction and its application to study microstructural changes during the α → β phase transition in Si

Popov, D.; Park, C.; Kenney-Benson, C.; Shen, G.

doi:10.1063/1.4926894

Title: High pressure Laue diffraction and its application to study microstructural changes during the α → β phase transition in Si

Journal Article · Mon Jul 20 00:00:00 EDT 2015 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.4926894· OSTI ID:1203736

^[1];

^[1]; Kenney-Benson, C. ^[1]; Shen, G. ^[1]

Carnegie Inst. of Washington, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT)

Here, an approach using polychromatic x-ray Laue diffraction is described for studying pressure induced microstructural changes of materials under pressure. The advantages of this approach with respect to application of monochromatic x-ray diffraction and other techniques are discussed. Experiments to demonstrate the applications of the method have been performed on the α → β phase transition in Si at high pressures using a diamond anvil cell. We present the characterization of microstructures across the α–β phase transition, such as morphology of both the parent and product phases, relative orientation of single-crystals, and deviatoric strains. Subtle inhomogeneous strain of the single-crystal sample caused by lattice rotations becomes detectable with the approach.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF)

Grant/Contract Number:: NA0001974; FG02-99ER45775; AC02-06CH11357

OSTI ID:: 1203736

Alternate ID(s):: OSTI ID: 1228683

Journal Information:: Review of Scientific Instruments, Vol. 86, Issue 7; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: ENGLISH

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Cited by: 8 works

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References (23)

A superbend X-ray microdiffraction beamline at the advanced light source Tamura, N.; Kunz, M.; Chen, K. Materials Science and Engineering: A, Vol. 524, Issue 1-2 https://doi.org/10.1016/j.msea.2009.03.062	journal	October 2009
High Pressure Raman Spectroscopy of Single Crystals of Hexahydro-1,3,5-trinitro-1,3,5-triazine (RDX) Dreger, Zbigniew A.; Gupta, Yogendra M. The Journal of Physical Chemistry B, Vol. 111, Issue 15 https://doi.org/10.1021/jp0681092	journal	April 2007
Pressure dependence of the Imma phase of silicon McMahon, M. I.; Nelmes, R. J.; Wright, N. G. Physical Review B, Vol. 50, Issue 2 https://doi.org/10.1103/PhysRevB.50.739	journal	July 1994
Kinetics of pressure induced structural phase transitions—A review Chandra Shekar, N. V.; Rajan, K. Govinda Bulletin of Materials Science, Vol. 24, Issue 1 https://doi.org/10.1007/BF02704834	journal	February 2001
Adapting polychromatic X-ray microdiffraction techniques to high-pressure research: energy scan approach Ice, Gene E.; Dera, Przemyslaw; Liu, Wenjun Journal of Synchrotron Radiation, Vol. 12, Issue 5 https://doi.org/10.1107/S0909049505024684	journal	August 2005
Microscope Observation of the Process of the Pressure-Induced Phase Transition of RbCl by Means of a Diamond Anvil Okano, Yoji; Nomura, Motoyuki Japanese Journal of Applied Physics, Vol. 28, Issue Part 1, No. 4 https://doi.org/10.1143/JJAP.28.696	journal	April 1989
Raman scattering and phonon dispersion in Si and GaP at very high pressure Weinstein, Bernard A.; Piermarini, G. J. Physical Review B, Vol. 12, Issue 4 https://doi.org/10.1103/PhysRevB.12.1172	journal	August 1975
In situ X-ray microdiffraction study of deformation-induced phase transformation in 304 austenitic stainless steel Li, N.; Wang, Y. D.; Liu, W. J. Acta Materialia, Vol. 64 https://doi.org/10.1016/j.actamat.2013.11.001	journal	February 2014
Pressure induced phase transitions in silicon, germanium and some III–V compounds Minomura, S.; Drickamer, H. G. Journal of Physics and Chemistry of Solids, Vol. 23, Issue 5 https://doi.org/10.1016/0022-3697(62)90085-9	journal	May 1962
Kinetics of intracrystalline olivine–ringwoodite transformation Kerschhofer, L.; Rubie, D. C.; Sharp, T. G. Physics of the Earth and Planetary Interiors, Vol. 121, Issue 1-2 https://doi.org/10.1016/S0031-9201(00)00160-6	journal	September 2000
Ultrahigh pressure diamond‐anvil cell and several semiconductor phase transition pressures in relation to the fixed point pressure scale Piermarini, G. J.; Block, S. Review of Scientific Instruments, Vol. 46, Issue 8 https://doi.org/10.1063/1.1134381	journal	August 1975
Tutorial on x-ray microLaue diffraction Ice, Gene E.; Pang, Judy W. L. Materials Characterization, Vol. 60, Issue 11 https://doi.org/10.1016/j.matchar.2009.07.006	journal	November 2009
Raman and X-Ray Scattering Studies of High-Pressure Phases of Urea Lamelas, F. J.; Dreger, Z. A.; Gupta, Y. M. The Journal of Physical Chemistry B, Vol. 109, Issue 16 https://doi.org/10.1021/jp040760m	journal	April 2005
Crystal data for high-pressure phases of silicon Hu, Jing Zhu; Merkle, Larry D.; Menoni, Carmen S. Physical Review B, Vol. 34, Issue 7 https://doi.org/10.1103/PhysRevB.34.4679	journal	October 1986
Characterization of three-dimensional crystallographic distributions using polychromatic X-ray microdiffraction Ice, G. E.; Pang, J. W. L.; Barabash, R. I. Scripta Materialia, Vol. 55, Issue 1 https://doi.org/10.1016/j.scriptamat.2006.02.046	journal	July 2006
Automated indexing for texture and strain measurement with broad-bandpass x-ray microbeams Chung, Jin-Seok; Ice, Gene E. Journal of Applied Physics, Vol. 86, Issue 9 https://doi.org/10.1063/1.371507	journal	November 1999
The kinetics of cubic boron nitride formation in the system BN-Mg2N2 Lorenz, Helmar; Lorenz, Bernd; K�hne, Ulrich Journal of Materials Science, Vol. 23, Issue 9 https://doi.org/10.1007/BF00551302	journal	September 1988
Calibration of the ruby pressure gauge to 800 kbar under quasi-hydrostatic conditions Mao, H. K.; Xu, J.; Bell, P. M. Journal of Geophysical Research, Vol. 91, Issue B5, p. 4673-4676 https://doi.org/10.1029/JB091iB05p04673	journal	January 1986
Angle calculations for 3- and 4-circle X-ray and neutron diffractometers Busing, W. R.; Levy, H. A. Acta Crystallographica, Vol. 22, Issue 4 https://doi.org/10.1107/S0365110X67000970	journal	April 1967
High resolution three-dimensional X-ray diffraction study of dislocations in grains of MgGeO ₃ post-perovskite at 90 GPa : DISLOCATIONS IN GRAINS OF MgGeO Nisr, Carole; Ribárik, Gábor; Ungár, Tamás Journal of Geophysical Research: Solid Earth, Vol. 117, Issue B3 https://doi.org/10.1029/2011JB008401	journal	March 2012
Mechanisms of transformation and deformation in Mg1.8Fe0.2SiO4 olivine and wadsleyite under non-hydrostatic stress Dupas-Bruzek, Catherine; Sharp, Thomas G.; Rubie, David C. Physics of the Earth and Planetary Interiors, Vol. 108, Issue 1 https://doi.org/10.1016/S0031-9201(98)00086-7	journal	May 1998
Two-dimensional detector software: From real detector to idealised image or two-theta scan Hammersley, A. P.; Svensson, S. O.; Hanfland, M. High Pressure Research, Vol. 14, Issue 4-6, p. 235-248 https://doi.org/10.1080/08957959608201408	journal	January 1996
Crystal Structures at High Pressures of Metallic Modifications of Silicon and Germanium Jamieson, J. C. Science, Vol. 139, Issue 3556 https://doi.org/10.1126/science.139.3556.762	journal	February 1963

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Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments Hrubiak, Rostislav; Smith, Jesse S.; Shen, Guoyin Review of Scientific Instruments, Vol. 90, Issue 2 https://doi.org/10.1063/1.5057518	journal	February 2019
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