Ultra-stable sub-meV monochromator for hard X-rays

Toellner, T. S.; Collins, J.; Goetze, K.; Hu, M. Y.; Preissner, C.; Trakhtenberg, E.; Yan, L.

doi:10.1107/S1600577515012230

Title: Ultra-stable sub-meV monochromator for hard X-rays

Journal Article · Fri Jul 17 00:00:00 EDT 2015 · Journal of Synchrotron Radiation (Online)

DOI:https://doi.org/10.1107/S1600577515012230· OSTI ID:1212710

Toellner, T. S. ^[1]; Collins, J. ^[1]; Goetze, K. ^[1]; Hu, M. Y. ^[1]; Preissner, C. ^[1]; Trakhtenberg, E. ^[1]; Yan, L. ^[1]

Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source.

A high-resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in ¹⁵¹Eu. The first-of-its-kind, fully cryogenic design achieves an energy-alignment stability of 0.017 meV r.m.s. per day, or a 100-fold improvement over other meV-monochromators, and can tolerate higher X-ray power loads than room-temperature designs of comparable resolution. This offers the potential for significantly more accurate measurements of lattice excitation energies using nuclear resonant vibrational spectroscopy if combined with accurate energy calibration using, for example, high-speed Doppler shifting. The design of the monochromator along with its performance and impact on transmitted beam properties are presented.

View Accepted Manuscript (DOE)

Cite

Export

Save

Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source.

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: AC02-06CH11357; FC52-06NA27684

OSTI ID:: 1212710

Journal Information:: Journal of Synchrotron Radiation (Online), Vol. 22, Issue 5; ISSN 1600-5775

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 3 works

Citation information provided by
Web of Science

References (19)

Measuring wavelengths and lattice constants with the Mössbauer wavelength standard Shvyd'ko, Yu. V.; Lucht, M.; Gerdau, E. Journal of Synchrotron Radiation, Vol. 9, Issue 1 https://doi.org/10.1107/S0909049501019203	journal	December 2001
Dispersive spread of virtual sources by asymmetric X-ray monochromators Huang, X. R.; Macrander, A. T.; Honnicke, M. G. Journal of Applied Crystallography, Vol. 45, Issue 2 https://doi.org/10.1107/S0021889812003366	journal	March 2012
Milli-electronvolt monochromatization of hard X-rays with a sapphire backscattering monochromator Sergueev, I.; Wille, H. -C.; Hermann, R. P. Journal of Synchrotron Radiation, Vol. 18, Issue 5 https://doi.org/10.1107/S090904951102485X	journal	July 2011
Interplay between structural instability and lattice dynamics in ${EuRh}_{2} (P_{x} {As}_{1 - x})_{2}$ Barla, A.; Chefki, M.; Huhnt, C. Physical Review B, Vol. 69, Issue 10 https://doi.org/10.1103/PhysRevB.69.100102	journal	March 2004
A refractive collimator for synchrotron radiation Baron, A. Q. R.; Kohmura, Y.; Ohishi, Y. Applied Physics Letters, Vol. 74, Issue 10 https://doi.org/10.1063/1.123591	journal	March 1999
Dependence of the silicon lattice constant on isotopic mass Herrero, C. P. Solid State Communications, Vol. 110, Issue 5 https://doi.org/10.1016/S0038-1098(99)00082-4	journal	April 1999
Construction of a precision diffractometer for nuclear Bragg scattering at the Photon Factory Ishikawa, Tetsuya; Yoda, Yoshitaka; Izumi, Koichi Review of Scientific Instruments, Vol. 63, Issue 1 https://doi.org/10.1063/1.1143188	journal	January 1992
Nuclear resonance scattering of synchrotron radiation at the 21.5 keV resonance of ¹⁵¹ Eu Leupold, O.; Pollmann, J.; Gerdau, E. Europhysics Letters (EPL), Vol. 35, Issue 9 https://doi.org/10.1209/epl/i1996-00169-0	journal	September 1996
Anomalous Isotopic Effect on the Lattice Parameter of Silicon Wille, H. -C.; Shvyd’ko, Yu. V.; Gerdau, E. Physical Review Letters, Vol. 89, Issue 28 https://doi.org/10.1103/PhysRevLett.89.285901	journal	December 2002
X-ray monochromator with an energy resolution of 8×10−9 at 14.41 keV Yabashi, Makina; Tamasaku, Kenji; Kikuta, Seishi Review of Scientific Instruments, Vol. 72, Issue 11 https://doi.org/10.1063/1.1406925	journal	November 2001
High-energy-resolution x-ray optics with refractive collimators Chumakov, A. I.; Rüffer, R.; Leupold, O. Applied Physics Letters, Vol. 77, Issue 1 https://doi.org/10.1063/1.126867	journal	July 2000
Crystal monochromator with a resolution beyond 10 ⁸ Toellner, T. S.; Hu, M. Y.; Sturhahn, W. Journal of Synchrotron Radiation, Vol. 8, Issue 4 https://doi.org/10.1107/S0909049501007257	journal	June 2001
A cryogenically stabilized meV-monochromator for hard X-rays Toellner, T. S.; Alatas, A.; Said, A. Journal of Synchrotron Radiation, Vol. 13, Issue 2 https://doi.org/10.1107/S0909049505042664	journal	February 2006
An X-ray monochromator with 1.65 meV energy resolution Chumakov, A. I.; Metge, J.; Baron, A. Q. R. Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 383, Issue 2-3 https://doi.org/10.1016/S0168-9002(96)00924-2	journal	December 1996
High-Resolution Monochromators for Nuclear Resonant Scattering Developed at BL09XU, SPring-8 Yoda, Yoshitaka; Zhang, Xiaowei; Kikuta, Seishi SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings https://doi.org/10.1063/1.2436213	conference	January 2007
Phonon spectroscopy by inelastic x-ray scattering Burkel, Eberhard Reports on Progress in Physics, Vol. 63, Issue 2 https://doi.org/10.1088/0034-4885/63/2/203	journal	January 2000
Wave theory of focusing monochromator of synchrotron radiation Kohn, V. G.; Chumakov, A. I.; Rüffer, R. Journal of Synchrotron Radiation, Vol. 16, Issue 5 https://doi.org/10.1107/S090904950902319X	journal	July 2009
Dependence of the crystal lattice constant on isotopic composition: Theory and ab initio calculations for C, Si, and Ge Pavone, Pasquale; Baroni, Stefano Solid State Communications, Vol. 90, Issue 5 https://doi.org/10.1016/0038-1098(94)90154-6	journal	May 1994
Six-reflection meV-monochromator for synchrotron radiation Toellner, T. S.; Alatas, A.; Said, A. H. Journal of Synchrotron Radiation, Vol. 18, Issue 4 https://doi.org/10.1107/S0909049511017535	journal	May 2011

Cited By (2)

Rocking curve imaging of high quality sapphire crystals in backscattering geometry Jafari, A.; Sergueev, I.; Bessas, D. Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/pubdb-2017-00751	text	January 2017
Rocking curve imaging of high quality sapphire crystals in backscattering geometry Jafari, A.; Sergueev, I.; Bessas, D. Journal of Applied Physics, Vol. 121, Issue 4 https://doi.org/10.1063/1.4974106	journal	January 2017

Similar Records

Ultra-stable sub-meV monochromator for hard X-rays

Journal Article · Fri Jul 17 00:00:00 EDT 2015 · Journal of Synchrotron Radiation (Online) · OSTI ID:1212710

Toellner, T. S.; Collins, J.; Goetze, K.; +4 more

Milli-electronvolt monochromatization of hard X-rays with a sapphire backscattering monochromator

Journal Article · Wed Jul 20 00:00:00 EDT 2011 · Journal of Synchrotron Radiation · OSTI ID:1212710

Sergueev, I.; Wille, H.-C.; Hermann, R. P.; +4 more

The sapphire backscattering monochromator at the Dynamics beamline P01 of PETRA III

Journal Article · Tue Feb 23 00:00:00 EST 2016 · Hyperfine Interactions · OSTI ID:1212710

Alexeev, P.; Asadchikov, V.; Bessas, D.; +14 more

Related Subjects

71 CLASSICAL AND QUANTUM MECHANICS
GENERAL PHYSICS
high energy-resolution
monochromator
europium
nuclear resonance
cryostat

Title: Ultra-stable sub-meV monochromator for hard X-rays

Citation Formats

References (19)

Cited By (2)

Similar Records

Related Subjects