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Title: Frontiers of in situ electron microscopy

Journal Article · · MRS Bulletin
DOI:https://doi.org/10.1557/mrs.2014.305· OSTI ID:1193214
 [1];  [2];  [3]
  1. Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States)
  2. Brookhaven National Lab. (BNL), Upton, NY (United States)
  3. Univ. of California-San Diego, San Diego, CA (United States)

In situ transmission electron microscopy (TEM) has become an increasingly important tool for materials characterization. It provides key information on the structural dynamics of a material during transformations and the correlation between structure and properties of materials. With the recent advances in instrumentation, including aberration corrected optics, sample environment control, the sample stage, and fast and sensitive data acquisition, in situ TEM characterization has become more and more powerful. In this article, a brief review of the current status and future opportunities of in situ TEM is included. It also provides an introduction to the six articles covered by in this issue of MRS Bulletin explore the frontiers of in situ electron microscopy, including liquid and gas environmental TEM, dynamic four-dimensional TEM, nanomechanics, ferroelectric domain switching studied by in situ TEM, and state-of-the-art atomic imaging of light elements (i.e., carbon atoms) and individual defects.

Research Organization:
Brookhaven National Laboratory (BNL), Upton, NY (United States)
Sponsoring Organization:
USDOE Office of Science (SC), Basic Energy Sciences (BES)
Grant/Contract Number:
SC00112704
OSTI ID:
1193214
Report Number(s):
BNL-108005-2015-JA; R&D Project: MA015MACA; KC0201010
Journal Information:
MRS Bulletin, Vol. 40, Issue 01; ISSN 0883-7694
Publisher:
Materials Research SocietyCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 95 works
Citation information provided by
Web of Science

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Mechanical Properties of Si Nanowires as Revealed by in Situ Transmission Electron Microscopy and Molecular Dynamics Simulations journal January 2012
Revealing Correlation of Valence State with Nanoporous Structure in Cobalt Catalyst Nanoparticles by In Situ Environmental TEM journal April 2012
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Dipolar Magnetism in Ordered and Disordered Low-Dimensional Nanoparticle Assemblies journal February 2013
Coherence and modality of driven interlayer-coupled magnetic vortices journal April 2014
Interface-induced nonswitchable domains in ferroelectric thin films journal August 2014
Reaction-Driven Restructuring of Rh-Pd and Pt-Pd Core-Shell Nanoparticles journal November 2008
Demonstration of an Electrochemical Liquid Cell for Operando Transmission Electron Microscopy Observation of the Lithiation/Delithiation Behavior of Si Nanowire Battery Anodes journal November 2013
Design and Applications of Environmental Cell Transmission Electron Microscope for In Situ Observations of Gas–Solid Reactions journal November 2001
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Novel microchip for in situ TEM imaging of living organisms and bio-reactions in aqueous conditions journal January 2008
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Developments in in situ Environmental Cell High-Resolution Electron Microscopy and Applications to Catalysis journal January 2002
In Situ Studies of Chemistry and Structure of Materials in Reactive Environments journal January 2011
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Direct Observations of Oxygen-induced Platinum Nanoparticle Ripening Studied by In Situ TEM journal June 2010
Environmental electron microscopy (ETEM) for catalysts with a closed E-cell with carbon windows journal April 2006
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Direct observation of stick-slip movements of water nanodroplets induced by an electron beam journal April 2012
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Nanocrystal Diffusion in a Liquid Thin Film Observed by in Situ Transmission Electron Microscopy journal June 2009
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Single-donor ionization energies in a nanoscale CMOS channel journal December 2009
Strong crystal size effect on deformation twinning journal January 2010
Visualization of Electrode–Electrolyte Interfaces in LiPF 6 /EC/DEC Electrolyte for Lithium Ion Batteries via in Situ TEM journal March 2014
Atomic origins of the high catalytic activity of nanoporous gold journal August 2012

Cited By (13)

Electrochemical and Structural Analysis in All‐Solid‐State Lithium Batteries by Analytical Electron Microscopy: Progress and Perspectives journal October 2019
The Mechanical Properties of Nanowires journal January 2017
Direct observation of oxygen vacancy-driven structural and resistive phase transitions in La2/3Sr1/3MnO3 journal February 2017
The chemistry of nucleation journal January 2016
Pitfalls and reproducibility of in situ synchrotron powder X-ray diffraction studies of solvothermal nanoparticle formation journal March 2018
In situ study of nucleation and growth dynamics of Au nanoparticles on MoS 2 nanoflakes journal January 2018
Direct Visualization of Li Dendrite Effect on LiCoO 2 Cathode by In Situ TEM journal November 2018
Bimetallic synergy in cobalt–palladium nanocatalysts for CO oxidation journal December 2018
Automating material image analysis for material discovery journal April 2019
Advanced tomography techniques for inorganic, organic, and biological materials journal July 2016
Developments of cation-exchange by in situ electron microscopy journal January 2019
Reversible superdense ordering of lithium between two graphene sheets journal November 2018
Tip-enhanced Raman spectroscopy for surfaces and interfaces journal January 2017