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Title: A Flow-Through Reaction Cell that Couples Time - Resolved Analysis

Abstract

A non-metallic flow-through reaction cell is described, designed for in situ time-resolved X-ray diffraction coupled with stable isotope analysis. The experimental setup allows the correlation of Cu isotope fractionation with changes in crystal structure during copper sulfide dissolution. This flow-through cell can be applied to many classes of fluid-mineral reactions that involve dissolution or ion exchange.

Authors:
; ; ; ; ;
Publication Date:
Research Org.:
Brookhaven National Lab. (BNL), Upton, NY (United States)
Sponsoring Org.:
USDOE SC OFFICE OF SCIENCE (SC)
OSTI Identifier:
1041721
Report Number(s):
BNL-97399-2012-JA
Journal ID: ISSN 0021-8898; JACGAR; TRN: US201212%%133
DOE Contract Number:  
DE-AC02-98CH10886
Resource Type:
Journal Article
Journal Name:
Journal of Applied Crystallography
Additional Journal Information:
Journal Volume: 44; Journal Issue: 2; Journal ID: ISSN 0021-8898
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; COPPER ISOTOPES; COPPER SULFIDES; CORRELATIONS; CRYSTAL STRUCTURE; DISSOLUTION; FRACTIONATION; ION EXCHANGE; ISOTOPES; STABLE ISOTOPES; X-RAY DIFFRACTION

Citation Formats

Wall, A, Heaney, P, Mathur, R, Post, J, Hanson, J, and Eng, P. A Flow-Through Reaction Cell that Couples Time - Resolved Analysis. United States: N. p., 2011. Web. doi:10.1107/S0021889811000525.
Wall, A, Heaney, P, Mathur, R, Post, J, Hanson, J, & Eng, P. A Flow-Through Reaction Cell that Couples Time - Resolved Analysis. United States. https://doi.org/10.1107/S0021889811000525
Wall, A, Heaney, P, Mathur, R, Post, J, Hanson, J, and Eng, P. 2011. "A Flow-Through Reaction Cell that Couples Time - Resolved Analysis". United States. https://doi.org/10.1107/S0021889811000525.
@article{osti_1041721,
title = {A Flow-Through Reaction Cell that Couples Time - Resolved Analysis},
author = {Wall, A and Heaney, P and Mathur, R and Post, J and Hanson, J and Eng, P},
abstractNote = {A non-metallic flow-through reaction cell is described, designed for in situ time-resolved X-ray diffraction coupled with stable isotope analysis. The experimental setup allows the correlation of Cu isotope fractionation with changes in crystal structure during copper sulfide dissolution. This flow-through cell can be applied to many classes of fluid-mineral reactions that involve dissolution or ion exchange.},
doi = {10.1107/S0021889811000525},
url = {https://www.osti.gov/biblio/1041721}, journal = {Journal of Applied Crystallography},
issn = {0021-8898},
number = 2,
volume = 44,
place = {United States},
year = {Sat Dec 31 00:00:00 EST 2011},
month = {Sat Dec 31 00:00:00 EST 2011}
}