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Title: Characterization of ZnO nanoparticle suspension in water: Effectiveness of ultrasonic dispersion

Journal Article · · Powder Technology
 [1];  [1];  [1];  [2];  [3];  [3];  [1]
  1. Univ. of Pittsburgh, PA (United States); National Energy Technology Lab. (NETL), Pittsburgh, PA, (United States)
  2. Univ. of Pittsburgh, PA (United States)
  3. National Energy Technology Lab. (NETL), Pittsburgh, PA, (United States)

Suspensions of ZnO nanoparticles in water were prepared with the two-step powder dispersion process using several methods of ultrasonication. The dispersion of ZnO was found to proceed by a fragmentation process. with minimum achievable particle size in the range 50 to 300 nm. This is consistent with other oxide nanopowder systems, in which most primary particulates still remain in hardened aggregates that cannot be further reduced. A submersible accelerometer probe was developed and used to measure the relative ultrasonic energy held in the liquid for the various ultrasonication methods. oscillation at the expected frequencies was identified in each case, with strong variability at different locations in the liquid volume.

Research Organization:
National Energy Technology Laboratory (NETL), Pittsburgh, PA, Morgantown, WV, and Albany, OR (United States)
Sponsoring Organization:
USDOE Assistant Secretary for Fossil Energy (FE)
OSTI ID:
1014930
Report Number(s):
NETL-TPR-2639
Journal Information:
Powder Technology, Vol. 194, Issue 1-2; ISSN 0032-5910
Publisher:
Elsevier
Country of Publication:
United States
Language:
English