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Title: Evaluation of plasma sprayed crucible coatings for melt processing copper-refractory metal alloys

Conference ·
OSTI ID:10136747

A study was made to access the suitability of several plasma arc sprayed coatings applied to graphite for application as containment crucibles for melt processing copper-refractory metal alloys. Coatings of Ta, TaC, TaB{sub 2} and ZrO{sub 2}{center_dot}8w/o Y{sub 2}O{sub 3} were evaluated and compared to uncoated graphite. The ZrO{sub 2}{center_dot}8w/pY{sub 2}O{sub 3} coating was sprayed over a tungsten bond coat. Prealloyed samples of Cu-15v/o Cr and Cu-15v/o Nb were placed within the crucibles and heated inductively to 1800{degree}C and 2100{degree}C, respectively. Compatibility of the coating-alloy system was evaluated by optical and scanning electron microscopy, EDS, XRD and combustion chromatography.

Research Organization:
Ames Lab., IA (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
W-7405-ENG-82
OSTI ID:
10136747
Report Number(s):
IS-M-700; CONF-9206135-2; ON: DE92010871
Resource Relation:
Conference: 1992 international thermal spray conference,Orlando, FL (United States),1-5 Jun 1992; Other Information: PBD: [1992]
Country of Publication:
United States
Language:
English