On the scaling of multicrystal data sets collected at high-intensity X-ray and electron sources
Abstract
Here, the need for data-scaling has become increasingly evident as time-resolved pump-probe photocrystallography is rapidly developing at high intensity X-ray sources. Several aspects of the scaling of data sets collected at synchrotrons, XFELs (X-ray Free Electron Lasers) and high-intensity pulsed electron sources are discussed. They include laser-ON/laser-OFF data scaling, inter- and intra-data set scaling. (C) 2015 Author(s). All article content, except where otherwise noted, is licensed under a Creative Commons Attribution 3.0 Unported License.
- Authors:
-
- Univ. at Buffalo, State Univ. of New York, Buffalo, NY (United States)
- Univ. at Buffalo, State Univ. of New York, Buffalo, NY (United States); Univ. de Lorraine, Vandoeuvre-les-Nancy Cedex (France)
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1323136
- Grant/Contract Number:
- W-31-109-ENG-38
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Structural Dynamics
- Additional Journal Information:
- Journal Volume: 2; Journal Issue: 6; Journal ID: ISSN 2329-7778
- Publisher:
- American Crystallographic Association/AIP
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; resolved laue diffraction; photochemistry; complexes; data sets; anisotropy; electron sources; X-ray lasers; free electron lasers
Citation Formats
Coppens, Philip, and Fournier, Bertrand. On the scaling of multicrystal data sets collected at high-intensity X-ray and electron sources. United States: N. p., 2015.
Web. doi:10.1063/1.4935526.
Coppens, Philip, & Fournier, Bertrand. On the scaling of multicrystal data sets collected at high-intensity X-ray and electron sources. United States. https://doi.org/10.1063/1.4935526
Coppens, Philip, and Fournier, Bertrand. Wed .
"On the scaling of multicrystal data sets collected at high-intensity X-ray and electron sources". United States. https://doi.org/10.1063/1.4935526. https://www.osti.gov/servlets/purl/1323136.
@article{osti_1323136,
title = {On the scaling of multicrystal data sets collected at high-intensity X-ray and electron sources},
author = {Coppens, Philip and Fournier, Bertrand},
abstractNote = {Here, the need for data-scaling has become increasingly evident as time-resolved pump-probe photocrystallography is rapidly developing at high intensity X-ray sources. Several aspects of the scaling of data sets collected at synchrotrons, XFELs (X-ray Free Electron Lasers) and high-intensity pulsed electron sources are discussed. They include laser-ON/laser-OFF data scaling, inter- and intra-data set scaling. (C) 2015 Author(s). All article content, except where otherwise noted, is licensed under a Creative Commons Attribution 3.0 Unported License.},
doi = {10.1063/1.4935526},
journal = {Structural Dynamics},
number = 6,
volume = 2,
place = {United States},
year = {Wed Nov 11 00:00:00 EST 2015},
month = {Wed Nov 11 00:00:00 EST 2015}
}
Free Publicly Available Full Text
Publisher's Version of Record
Other availability
Cited by: 3 works
Citation information provided by
Web of Science
Web of Science
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
On the assessment of time-resolved diffraction results
journal, August 2014
- Fournier, Bertrand; Coppens, Philip
- Acta Crystallographica Section A Foundations and Advances, Vol. 70, Issue a1
An alternative method of solving the layer scaling equations of Hamilton, Rollett and Sparks
journal, November 1966
- Fox, G. C.; Holmes, K. C.
- Acta Crystallographica, Vol. 20, Issue 6
On the relative scaling of X-ray photographs
journal, January 1965
- Hamilton, W. C.; Rollett, J. S.; Sparks, R. A.
- Acta Crystallographica, Vol. 18, Issue 1
Accurate macromolecular structures using minimal measurements from X-ray free-electron lasers
journal, March 2014
- Hattne, Johan; Echols, Nathaniel; Tran, Rosalie
- Nature Methods, Vol. 11, Issue 5
Shedding Light on the Photochemistry of Coinage-Metal Phosphorescent Materials: A Time-Resolved Laue Diffraction Study of an Ag I –Cu I Tetranuclear Complex
journal, September 2014
- Jarzembska, Katarzyna N.; Kamiński, Radosław; Fournier, Bertrand
- Inorganic Chemistry, Vol. 53, Issue 19
Structure-factor analysis of femtosecond microdiffraction patterns from protein nanocrystals
journal, February 2011
- Kirian, Richard A.; White, Thomas A.; Holton, James M.
- Acta Crystallographica Section A Foundations of Crystallography, Vol. 67, Issue 2
Restricted Photochemistry in the Molecular Solid State: Structural Changes on Photoexcitation of Cu(I) Phenanthroline Metal-to-Ligand Charge Transfer (MLCT) Complexes by Time-Resolved Diffraction
journal, March 2012
- Makal, Anna; Benedict, Jason; Trzop, Elzbieta
- The Journal of Physical Chemistry A, Vol. 116, Issue 13
The development of Laue techniques for single-pulse diffraction of chemical complexes: time-resolved Laue diffraction on a binuclear rhodium metal-organic complex
journal, May 2011
- Makal, Anna; Trzop, Elzbieta; Sokolow, Jesse
- Acta Crystallographica Section A Foundations of Crystallography, Vol. 67, Issue 4
Fixed target matrix for femtosecond time-resolved and in situ serial micro-crystallography
journal, August 2015
- Mueller, C.; Marx, A.; Epp, S. W.
- Structural Dynamics, Vol. 2, Issue 5
Data scaling and temperature calibration in time-resolved photocrystallographic experiments
journal, September 2010
- Schmøkel, Mette S.; Kamiński, Radosław; Benedict, Jason B.
- Acta Crystallographica Section A Foundations of Crystallography, Vol. 66, Issue 6
X-ray lasers for structural and dynamic biology
journal, September 2012
- Spence, J. C. H.; Weierstall, U.; Chapman, H. N.
- Reports on Progress in Physics, Vol. 75, Issue 10
LASER – a program for response-ratio refinement of time-resolved diffraction data
journal, August 2010
- Vorontsov, Ivan; Pillet, Sébastien; Kamiński, Radosław
- Journal of Applied Crystallography, Vol. 43, Issue 5
Single-crystal-to-single-crystal E → Z isomerization of tiglic acid in a supramolecular framework
journal, July 2007
- Zheng, Shao-Liang; Messerschmidt, Marc; Coppens, Philip
- Acta Crystallographica Section B Structural Science, Vol. 63, Issue 4
Shedding Light on the Photochemistry of Coinage-Metal Phosphorescent Materials: A Time-Resolved Laue Diffraction Study of an Ag I –Cu I Tetranuclear Complex
journal, September 2014
- Jarzembska, Katarzyna N.; Kamiński, Radosław; Fournier, Bertrand
- Inorganic Chemistry, Vol. 53, Issue 19
Restricted Photochemistry in the Molecular Solid State: Structural Changes on Photoexcitation of Cu(I) Phenanthroline Metal-to-Ligand Charge Transfer (MLCT) Complexes by Time-Resolved Diffraction
journal, March 2012
- Makal, Anna; Benedict, Jason; Trzop, Elzbieta
- The Journal of Physical Chemistry A, Vol. 116, Issue 13
X-ray lasers for structural and dynamic biology
journal, September 2012
- Spence, J. C. H.; Weierstall, U.; Chapman, H. N.
- Reports on Progress in Physics, Vol. 75, Issue 10
The RATIO method for time-resolved Laue crystallography
journal, January 2009
- Coppens, Philip; Pitak, Mateusz; Gembicky, Milan
- Journal of Synchrotron Radiation, Vol. 16, Issue 2
Analysis of multicrystal pump–probe data sets. I. Expressions for the RATIO model
journal, August 2014
- Fournier, Bertrand; Coppens, Philip
- Acta Crystallographica Section A Foundations and Advances, Vol. 70, Issue 5
Works referencing / citing this record:
On the Nature of Luminescence Thermochromism of Multinuclear Copper(I) Benzoate Complexes in the Crystalline State
journal, January 2019
- Jarzembska, Katarzyna; Hapka, Michał; Kamiński, Radosław
- Crystals, Vol. 9, Issue 1