Conductive two-dimensional titanium carbide ‘clay’ with high volumetric capacitance
Abstract
Safe and powerful energy storage devices are becoming increasingly important. Charging times of seconds to minutes, with power densities exceeding those of batteries, can in principle be provided by electrochemical capacitors—in particular, pseudocapacitors. Recent research has focused mainly on improving the gravimetric performance of the electrodes of such systems, but for portable electronics and vehicles volume is at a premium. The best volumetric capacitances of carbon-based electrodes are around 300 farads per cubic centimetre; hydrated ruthenium oxide can reach capacitances of 1,000 to 1,500 farads per cubic centimetre with great cyclability, but only in thin films. Recently, electrodes made of two-dimensional titanium carbide (Ti3C2, a member of the ‘MXene’ family), produced by etching aluminium from titanium aluminium carbide (Ti3AlC2, a ‘MAX’ phase) in concentrated hydrofluoric acid, have been shown to have volumetric capacitances of over 300 farads per cubic centimetre. In this paper, we report a method of producing this material using a solution of lithium fluoride and hydrochloric acid. The resulting hydrophilic material swells in volume when hydrated, and can be shaped like clay and dried into a highly conductive solid or rolled into films tens of micrometres thick. Additive-free films of this titanium carbide ‘clay’ have volumetric capacitancesmore »
- Authors:
-
- Drexel Univ., Philadelphia, PA (United States). Department of Materials Science and Engineering, and A. J. Drexel Nanomaterials Institute
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC)
- OSTI Identifier:
- 1286827
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Nature (London)
- Additional Journal Information:
- Journal Name: Nature (London); Journal Volume: 516; Journal Issue: 7529; Journal ID: ISSN 0028-0836
- Publisher:
- Nature Publishing Group
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 25 ENERGY STORAGE; Batteries; Two-dimensional materials Design; synthesis and processing
Citation Formats
Ghidiu, Michael, Lukatskaya, Maria R., Zhao, Meng-Qiang, Gogotsi, Yury G., and Barsoum, Michel W. Conductive two-dimensional titanium carbide ‘clay’ with high volumetric capacitance. United States: N. p., 2014.
Web. doi:10.1038/nature13970.
Ghidiu, Michael, Lukatskaya, Maria R., Zhao, Meng-Qiang, Gogotsi, Yury G., & Barsoum, Michel W. Conductive two-dimensional titanium carbide ‘clay’ with high volumetric capacitance. United States. https://doi.org/10.1038/nature13970
Ghidiu, Michael, Lukatskaya, Maria R., Zhao, Meng-Qiang, Gogotsi, Yury G., and Barsoum, Michel W. Wed .
"Conductive two-dimensional titanium carbide ‘clay’ with high volumetric capacitance". United States. https://doi.org/10.1038/nature13970. https://www.osti.gov/servlets/purl/1286827.
@article{osti_1286827,
title = {Conductive two-dimensional titanium carbide ‘clay’ with high volumetric capacitance},
author = {Ghidiu, Michael and Lukatskaya, Maria R. and Zhao, Meng-Qiang and Gogotsi, Yury G. and Barsoum, Michel W.},
abstractNote = {Safe and powerful energy storage devices are becoming increasingly important. Charging times of seconds to minutes, with power densities exceeding those of batteries, can in principle be provided by electrochemical capacitors—in particular, pseudocapacitors. Recent research has focused mainly on improving the gravimetric performance of the electrodes of such systems, but for portable electronics and vehicles volume is at a premium. The best volumetric capacitances of carbon-based electrodes are around 300 farads per cubic centimetre; hydrated ruthenium oxide can reach capacitances of 1,000 to 1,500 farads per cubic centimetre with great cyclability, but only in thin films. Recently, electrodes made of two-dimensional titanium carbide (Ti3C2, a member of the ‘MXene’ family), produced by etching aluminium from titanium aluminium carbide (Ti3AlC2, a ‘MAX’ phase) in concentrated hydrofluoric acid, have been shown to have volumetric capacitances of over 300 farads per cubic centimetre. In this paper, we report a method of producing this material using a solution of lithium fluoride and hydrochloric acid. The resulting hydrophilic material swells in volume when hydrated, and can be shaped like clay and dried into a highly conductive solid or rolled into films tens of micrometres thick. Additive-free films of this titanium carbide ‘clay’ have volumetric capacitances of up to 900 farads per cubic centimetre, with excellent cyclability and rate performances. In addition, this capacitance is almost twice that of our previous report, and our synthetic method also offers a much faster route to film production as well as the avoidance of handling hazardous concentrated hydrofluoric acid.},
doi = {10.1038/nature13970},
journal = {Nature (London)},
number = 7529,
volume = 516,
place = {United States},
year = {Wed Nov 26 00:00:00 EST 2014},
month = {Wed Nov 26 00:00:00 EST 2014}
}
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A Solid-State Fibriform Supercapacitor Boosted by Host-Guest Hybridization between the Carbon Nanotube Scaffold and MXene Nanosheets
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Room‐Temperature Liquid Metal Confined in MXene Paper as a Flexible, Freestanding, and Binder‐Free Anode for Next‐Generation Lithium‐Ion Batteries
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Ti 3 C 2 MXene Paper for the Effective Adsorption and Controllable Release of Aroma Molecules
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Mechanical Exfoliation of Select MAX Phases and Mo 4 Ce 4 Al 7 C 3 Single Crystals to Produce MAXenes
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The thermal and electrical properties of the promising semiconductor MXene Hf2CO2
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Dynamic charge acceptance and hydrogen evolution of a new MXene additive in advanced lead-acid batteries via a rapid screening three-electrode method
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A novel lithium-ion hybrid capacitor based on an aerogel-like MXene wrapped Fe 2 O 3 nanosphere anode and a 3D nitrogen sulphur dual-doped porous carbon cathode
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Concisely modularized assembling of graphene-based thin films with promising electrode performance
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Binder-free bonding of modularized MXene thin films into thick film electrodes for on-chip micro-supercapacitors with enhanced areal performance metrics
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Recent progress in flexible non-lithium based rechargeable batteries
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A high-performance trace level acetone sensor using an indispensable V 4 C 3 T x MXene
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Titanium carbide MXenes combined with red-emitting carbon dots as a unique turn-on fluorescent nanosensor for label-free determination of glucose
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- Science Advances, Vol. 4, Issue 1
Surface-agnostic highly stretchable and bendable conductive MXene multilayers
journal, March 2018
- An, Hyosung; Habib, Touseef; Shah, Smit
- Science Advances, Vol. 4, Issue 3
In Situ High-Pressure X-ray Diffraction and Raman Spectroscopy Study of Ti3C2Tx MXene
journal, October 2018
- Zhang, Luxi; Su, Weitao; Huang, Yanwei
- Nanoscale Research Letters, Vol. 13, Issue 1
Photodynamic Therapy Based on Graphene and MXene in Cancer Theranostics
journal, October 2019
- Gazzi, Arianna; Fusco, Laura; Khan, Anooshay
- Frontiers in Bioengineering and Biotechnology, Vol. 7
Three-Dimensional Architectures in Electrochemical Capacitor Applications – Insights, Opinions, and Perspectives
journal, September 2020
- Galek, Przemyslaw; Mackowiak, Adam; Bujewska, Paulina
- Frontiers in Energy Research, Vol. 8
Environmental Stability of MXenes as Energy Storage Materials
journal, December 2019
- Li, Xinliang; Huang, Zhaodong; Zhi, Chunyi
- Frontiers in Materials, Vol. 6
Fabrication of a Novel Antifouling Polysulfone Membrane with in Situ Embedment of Mxene Nanosheets
journal, November 2019
- Shen, Zhen; Chen, Wei; Xu, Hang
- International Journal of Environmental Research and Public Health, Vol. 16, Issue 23
First-Principles Study of Vacancies in Ti3SiC2 and Ti3AlC2
journal, January 2017
- Wang, Hui; Han, Han; Yin, Gen
- Materials, Vol. 10, Issue 2
A Semimetal-Like Molybdenum Carbide Quantum Dots Photoacoustic Imaging and Photothermal Agent with High Photothermal Conversion Efficiency
journal, September 2018
- Dai, Wenhao; Dong, Haifeng; Zhang, Xueji
- Materials, Vol. 11, Issue 9
First-Principles Studies of Adsorptive Remediation of Water and Air Pollutants Using Two-Dimensional MXene Materials
journal, November 2018
- Zhang, Yujuan; Zhang, Ningning; Ge, Changchun
- Materials, Vol. 11, Issue 11
A Facile Method to Construct MXene/CuO Nanocomposite with Enhanced Catalytic Activity of CuO on Thermal Decomposition of Ammonium Perchlorate
journal, December 2018
- Zhao, Haifeng; Lv, Jing; Sang, Junshan
- Materials, Vol. 11, Issue 12
Preparation of Ti3C2Tx/NiZn Ferrite Hybrids with Improved Electromagnetic Properties
journal, February 2020
- Zhou, Xiaobing; Li, Youbing; Huang, Qing
- Materials, Vol. 13, Issue 4
Deformation and Failure of MXene Nanosheets
journal, March 2020
- Zeleniakiene, Daiva; Monastyreckis, Gediminas; Aniskevich, Andrey
- Materials, Vol. 13, Issue 5
Investigation of Fumed Silica/Aqueous NaCl Superdielectric Material
journal, February 2016
- Jenkins, Natalie; Petty, Clayton; Phillips, Jonathan
- Materials, Vol. 9, Issue 2
Printable Nanomaterials for the Fabrication of High-Performance Supercapacitors
journal, July 2018
- Sun, Jiazhen; Cui, Bo; Chu, Fuqiang
- Nanomaterials, Vol. 8, Issue 7
A New Model to Predict Optimum Conditions for Growth of 2D Materials on a Substrate
journal, July 2019
- Liu, Yu-Peng; Ning, Bo-Yuan; Gong, Le-Cheng
- Nanomaterials, Vol. 9, Issue 7
Highly Efficient Catalytic Performances of Nitro Compounds and Morin via Self-Assembled MXene-Pd Nanocomposites Synthesized through Self-Reduction Strategy
journal, July 2019
- Yin, Juanjuan; Zhang, Lun; Jiao, Tifeng
- Nanomaterials, Vol. 9, Issue 7
Synergistic Effects of Two-Dimensional MXene and Ammonium Polyphosphate on Enhancing the Fire Safety of Polyvinyl Alcohol Composite Aerogels
journal, November 2019
- Sheng, Xinxin; Li, Sihao; Zhao, Yanfeng
- Polymers, Vol. 11, Issue 12
Calculating the free energy of 2D materials on substrates
text, January 2019
- Liu, Yu-Peng; Ning, Bo-Yuan; Gong, Le-Cheng
- arXiv
Local chemical bonding and structural properties in Ti3AlC2 MAX phase and Ti3C2Tx MXene probed by Ti 1s X-ray absorption spectroscopy
text, January 2020
- Magnuson, Martin; Näslund, Lars-Åke
- arXiv
2D Superparamagnetic Tantalum Carbide Composite MXenes for Efficient Breast-Cancer Theranostics
journal, January 2018
- Liu, Zhuang; Lin, Han; Zhao, Menglong
- Theranostics, Vol. 8, Issue 6