Superelasticity by reversible variant reorientation in a Ni-Mn-Ga microwire with bamboo grains
Abstract
The link between microstructure and mechanical properties is investigated for a superelastic Ni–Mn–Ga microwire with 226 μm diameter, created by solidification via the Taylor method. The wire, which consists of bamboo grains with tetragonal martensite matrix and coarse γ precipitates, exhibits fully reversible superelastic behavior up to 4% tensile strain. Upon multiple tensile load–unload cycles, reproducible stress fluctuations of ~3 MPa are measured on the loading superelastic stress plateau of ~50 MPa. During cycles at various temperatures spanning -70 to 55 °C, the plateau stress decreases from 58 to 48 MPa near linearly with increasing temperature. Based on in situ synchrotron X-ray diffraction measurements, we conclude that this superelastic behavior is due to reversible martensite variants reorientation (i.e., reversible twinning) with lattice rotation of ~13°. The reproducible stress plateau fluctuations are assigned to reversible twinning at well-defined locations along the wire. The strain recovery during unloading is attributed to reverse twinning, driven by the internal stress generated on loading between the elastic γ precipitates and the twinning martensite matrix. Lastly, the temperature dependence of the twining stress on loading is related to the change in tetragonality of the martensite, as measured by X-ray diffraction.
- Authors:
-
- Northwestern Univ., Evanston, IL (United States); Beijing Inst. of Technology, Beijing (China)
- Northwestern Univ., Evanston, IL (United States)
- Beijing Inst. of Technology, Beijing (China)
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Univ. of Science and Technology, Beijing (China)
- Boise State Univ., ID (United States)
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- National Science Foundation (NSF); National Key Basic Research Program of China; USDOE Office of Science (SC), Basic Energy Sciences (BES)
- OSTI Identifier:
- 1245144
- Alternate Identifier(s):
- OSTI ID: 1251455
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Acta Materialia
- Additional Journal Information:
- Journal Volume: 99; Journal ID: ISSN 1359-6454
- Publisher:
- Elsevier
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Ni2MnGa; oligocrystalline materials; shape-memory effect; size effect; superelasticity; twinning
Citation Formats
Wang, Z. L., Zheng, P., Nie, Z. H., Ren, Y., Wang, Y. D., Mullner, P., and Dunand, D. C. Superelasticity by reversible variant reorientation in a Ni-Mn-Ga microwire with bamboo grains. United States: N. p., 2015.
Web. doi:10.1016/j.actamat.2015.08.002.
Wang, Z. L., Zheng, P., Nie, Z. H., Ren, Y., Wang, Y. D., Mullner, P., & Dunand, D. C. Superelasticity by reversible variant reorientation in a Ni-Mn-Ga microwire with bamboo grains. United States. https://doi.org/10.1016/j.actamat.2015.08.002
Wang, Z. L., Zheng, P., Nie, Z. H., Ren, Y., Wang, Y. D., Mullner, P., and Dunand, D. C. Wed .
"Superelasticity by reversible variant reorientation in a Ni-Mn-Ga microwire with bamboo grains". United States. https://doi.org/10.1016/j.actamat.2015.08.002. https://www.osti.gov/servlets/purl/1245144.
@article{osti_1245144,
title = {Superelasticity by reversible variant reorientation in a Ni-Mn-Ga microwire with bamboo grains},
author = {Wang, Z. L. and Zheng, P. and Nie, Z. H. and Ren, Y. and Wang, Y. D. and Mullner, P. and Dunand, D. C.},
abstractNote = {The link between microstructure and mechanical properties is investigated for a superelastic Ni–Mn–Ga microwire with 226 μm diameter, created by solidification via the Taylor method. The wire, which consists of bamboo grains with tetragonal martensite matrix and coarse γ precipitates, exhibits fully reversible superelastic behavior up to 4% tensile strain. Upon multiple tensile load–unload cycles, reproducible stress fluctuations of ~3 MPa are measured on the loading superelastic stress plateau of ~50 MPa. During cycles at various temperatures spanning -70 to 55 °C, the plateau stress decreases from 58 to 48 MPa near linearly with increasing temperature. Based on in situ synchrotron X-ray diffraction measurements, we conclude that this superelastic behavior is due to reversible martensite variants reorientation (i.e., reversible twinning) with lattice rotation of ~13°. The reproducible stress plateau fluctuations are assigned to reversible twinning at well-defined locations along the wire. The strain recovery during unloading is attributed to reverse twinning, driven by the internal stress generated on loading between the elastic γ precipitates and the twinning martensite matrix. Lastly, the temperature dependence of the twining stress on loading is related to the change in tetragonality of the martensite, as measured by X-ray diffraction.},
doi = {10.1016/j.actamat.2015.08.002},
journal = {Acta Materialia},
number = ,
volume = 99,
place = {United States},
year = {Wed Aug 26 00:00:00 EDT 2015},
month = {Wed Aug 26 00:00:00 EDT 2015}
}
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