Nuclear resonant inelastic X-ray scattering at high pressure and low temperature
Abstract
In this study, a new synchrotron radiation experimental capability of coupling nuclear resonant inelastic X-ray scattering with the cryogenically cooled high-pressure diamond anvil cell technique is presented. The new technique permits measurements of phonon density of states at low temperature and high pressure simultaneously, and can be applied to studies of phonon contribution to pressure- and temperature-induced magnetic, superconducting and metal–insulator transitions in resonant isotope-bearing materials. In this report, a pnictide sample, EuFe2As2, is used as an example to demonstrate this new capability at beamline 3-ID of the Advanced Photon Source, Argonne National Laboratory. A detailed description of the technical development is given. The Fe-specific phonon density of states and magnetism from the Fe sublattice in Eu57Fe2As2 at high pressure and low temperature were derived by using this new capability.
- Authors:
-
- Univ. of Illinois at Urbana-Champaign, Urbana, IL (United States); Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)
- Univ. of Texas at Austin, Austin, TX (United States); Center for High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai (China)
- Chinese Academy of Sciences (CAS), Beijing (China). Inst. of High Energy Physics (IHEP)
- Chinese Academy of Sciences (CAS), Beijing (China). Inst. of Physics
- Carnegie Inst. of Washington, Argonne, IL (United States). HPSynC
- Carnegie Inst. of Washington, Argonne, IL (United States). HPSynC; Center for High Pressure Science and Technology Advanced Research (HPSTAR), Shanghai (China)
- Carnegie Inst. of Washington, Argonne, IL (United States). Geophysical Lab.
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC); National Science Foundation (NSF); National Natural Science Foundation of China (NSFC)
- OSTI Identifier:
- 1241005
- Grant/Contract Number:
- AC02-06CH11357; EAR- 0838221; FG02- 99ER45775; 11220101003
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Synchrotron Radiation (Online)
- Additional Journal Information:
- Journal Name: Journal of Synchrotron Radiation (Online); Journal Volume: 22; Journal Issue: 3; Journal ID: ISSN 1600-5775
- Publisher:
- International Union of Crystallography
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; nuclear resonant scattering; phonon density of states; high pressure; low temperature; iron-pnictides
Citation Formats
Bi, Wenli, Zhao, Jiyong, Lin, Jung -Fu, Jia, Quanjie, Hu, Michael Y., Jin, Changqing, Ferry, Richard, Yang, Wenge, Struzhkin, Viktor, and Alp, E. Ercan. Nuclear resonant inelastic X-ray scattering at high pressure and low temperature. United States: N. p., 2015.
Web. doi:10.1107/S1600577515003586.
Bi, Wenli, Zhao, Jiyong, Lin, Jung -Fu, Jia, Quanjie, Hu, Michael Y., Jin, Changqing, Ferry, Richard, Yang, Wenge, Struzhkin, Viktor, & Alp, E. Ercan. Nuclear resonant inelastic X-ray scattering at high pressure and low temperature. United States. https://doi.org/10.1107/S1600577515003586
Bi, Wenli, Zhao, Jiyong, Lin, Jung -Fu, Jia, Quanjie, Hu, Michael Y., Jin, Changqing, Ferry, Richard, Yang, Wenge, Struzhkin, Viktor, and Alp, E. Ercan. Thu .
"Nuclear resonant inelastic X-ray scattering at high pressure and low temperature". United States. https://doi.org/10.1107/S1600577515003586. https://www.osti.gov/servlets/purl/1241005.
@article{osti_1241005,
title = {Nuclear resonant inelastic X-ray scattering at high pressure and low temperature},
author = {Bi, Wenli and Zhao, Jiyong and Lin, Jung -Fu and Jia, Quanjie and Hu, Michael Y. and Jin, Changqing and Ferry, Richard and Yang, Wenge and Struzhkin, Viktor and Alp, E. Ercan},
abstractNote = {In this study, a new synchrotron radiation experimental capability of coupling nuclear resonant inelastic X-ray scattering with the cryogenically cooled high-pressure diamond anvil cell technique is presented. The new technique permits measurements of phonon density of states at low temperature and high pressure simultaneously, and can be applied to studies of phonon contribution to pressure- and temperature-induced magnetic, superconducting and metal–insulator transitions in resonant isotope-bearing materials. In this report, a pnictide sample, EuFe2As2, is used as an example to demonstrate this new capability at beamline 3-ID of the Advanced Photon Source, Argonne National Laboratory. A detailed description of the technical development is given. The Fe-specific phonon density of states and magnetism from the Fe sublattice in Eu57Fe2As2 at high pressure and low temperature were derived by using this new capability.},
doi = {10.1107/S1600577515003586},
journal = {Journal of Synchrotron Radiation (Online)},
number = 3,
volume = 22,
place = {United States},
year = {Thu Jan 01 00:00:00 EST 2015},
month = {Thu Jan 01 00:00:00 EST 2015}
}
Web of Science
Works referenced in this record:
Nuclear resonant scattering beamline at the Advanced Photon Source
journal, December 1994
- Alp, E. E.; Mooney, T. M.; Toellner, T.
- Hyperfine Interactions, Vol. 90, Issue 1
Lattice dynamics and inelastic nuclear resonant x-ray scattering
journal, August 2001
- Alp, E. E.; Sturhahn, W.; Toellner, T. S.
- Journal of Physics: Condensed Matter, Vol. 13, Issue 34
Avalanche photodiodes as large dynamic range detectors for synchrotron radiation
journal, November 1994
- Toellner, T. S.; Sturhahn, W.; Alp, E. E.
- Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 350, Issue 3
Is an Electron-Phonon Superconductor?
journal, July 2008
- Boeri, L.; Dolgov, O. V.; Golubov, A. A.
- Physical Review Letters, Vol. 101, Issue 2
The ruby pressure standard to 150GPa
journal, December 2005
- Chijioke, Akobuije D.; Nellis, W. J.; Soldatov, A.
- Journal of Applied Physics, Vol. 98, Issue 11
Magnetism, superconductivity, and pairing symmetry in iron-based superconductors
journal, October 2008
- Chubukov, A. V.; Efremov, D. V.; Eremin, I.
- Physical Review B, Vol. 78, Issue 13
Sound velocities of compressed Fe 3 C from simultaneous synchrotron X-ray diffraction and nuclear resonant scattering measurements
journal, September 2009
- Gao, Lili; Chen, Bin; Lerche, Michael
- Journal of Synchrotron Radiation, Vol. 16, Issue 6
Raman Spectroscopy at High Pressures
journal, January 2012
- Goncharov, Alexander F.
- International Journal of Spectroscopy, Vol. 2012
Mössbauer Spectroscopy and Transition Metal Chemistry
book, January 1978
- Gütlich, Philipp; Link, Rainer; Trautwein, Alfred X.
- Inorganic Chemistry Concepts
Influence of magnetism on phonons in as seen via inelastic x-ray scattering
journal, June 2009
- Hahn, S. E.; Lee, Y.; Ni, N.
- Physical Review B, Vol. 79, Issue 22
Magnetic Interactions on Single-Crystal EuFe 2 As 2 Studied by 57 Fe Mössbauer Spectroscopy
journal, March 2012
- Ikeda, Shugo; Yoshida, Kazuki; Kobayashi, Hisao
- Journal of the Physical Society of Japan, Vol. 81, Issue 3
X-ray absorption spectroscopy and high pressure
journal, May 1992
- Itiéf Baudelet, J.; Dartyge, E.; Fontaine, A.
- High Pressure Research, Vol. 8, Issue 5-6
Melting of compressed iron by monitoring atomic dynamics
journal, January 2013
- Jackson, Jennifer M.; Sturhahn, Wolfgang; Lerche, Michael
- Earth and Planetary Science Letters, Vol. 362
High time resolution x‐ray measurements with an avalanche photodiode detector
journal, January 1992
- Kishimoto, Shunji
- Review of Scientific Instruments, Vol. 63, Issue 1
Observation of a pressure-induced As–As hybridization associated with a change in the electronic state of Fe in the tetragonal phase of EuFe 2 As 2
journal, December 2012
- Kobayashi, Hisao; Ikeda, Shugo; Sakaguchi, Yui
- Journal of Physics: Condensed Matter, Vol. 25, Issue 2
Phase diagram of pressure-induced superconductivity in EuFe As probed by high-pressure resistivity up to 3.2 GPa
journal, June 2011
- Kurita, Nobuyuki; Kimata, Motoi; Kodama, Kota
- Physical Review B, Vol. 83, Issue 21
Unconventional Pairing Originating from the Disconnected Fermi Surfaces of Superconducting
journal, August 2008
- Kuroki, Kazuhiko; Onari, Seiichiro; Arita, Ryotaro
- Physical Review Letters, Vol. 101, Issue 8
Phonon density of states of Fe O across high-pressure structural and electronic transitions
journal, August 2011
- Lin, Jung-Fu; Tse, John S.; Alp, Esen E.
- Physical Review B, Vol. 84, Issue 6
Phonon Density of States of Iron up to 153 Gigapascals
journal, May 2001
- Mao, H. K.
- Science, Vol. 292, Issue 5518
Pressure-induced changes in the magnetic and valence state of EuFe As
journal, July 2011
- Matsubayashi, K.; Munakata, K.; Isobe, M.
- Physical Review B, Vol. 84, Issue 2
Unconventional Superconductivity with a Sign Reversal in the Order Parameter of
journal, July 2008
- Mazin, I. I.; Singh, D. J.; Johannes, M. D.
- Physical Review Letters, Vol. 101, Issue 5
Evidence for a reentrant superconducting state in under pressure
journal, June 2009
- Miclea, C. F.; Nicklas, M.; Jeevan, H. S.
- Physical Review B, Vol. 79, Issue 21
57 Fe and 151 Eu Mössbauer spectroscopy and magnetization studies of Eu(Fe 0.89 Co 0.11 ) 2 As 2 and Eu(Fe 0.9 Ni 0.1 ) 2 As 2
journal, February 2011
- Nowik, I.; Felner, I.; Ren, Z.
- New Journal of Physics, Vol. 13, Issue 2
High-temperature superconductivity in iron-based materials
journal, August 2010
- Paglione, Johnpierre; Greene, Richard L.
- Nature Physics, Vol. 6, Issue 9
Pressure-Induced High-Spin to Low-Spin Transition in FeS Evidenced by X-Ray Emission Spectroscopy
journal, April 1999
- Rueff, J. -P.; Kao, C. -C.; Struzhkin, V. V.
- Physical Review Letters, Vol. 82, Issue 16
Inelastic x-ray scattering by electronic excitations under high pressure
journal, March 2010
- Rueff, Jean-Pascal; Shukla, Abhay
- Reviews of Modern Physics, Vol. 82, Issue 1
Effect of pressure, temperature, fluorine doping, and rare earth elements on the phonon density of states of FeAsO studied by nuclear inelastic scattering
journal, February 2013
- Sergueev, I.; Hermann, R. P.; Bessas, D.
- Physical Review B, Vol. 87, Issue 6
Observation of Nuclear Resonant Scattering Accompanied by Phonon Excitation Using Synchrotron Radiation
journal, May 1995
- Seto, M.; Yoda, Y.; Kikuta, S.
- Physical Review Letters, Vol. 74, Issue 19
Phonons in iron monolayers
journal, March 2010
- Stankov, S.; Sladecek, M.; Ślezak, T.
- Journal of Physics: Conference Series, Vol. 217
CONUSS and PHOENIX: Evaluation of nuclear resonant scattering data
journal, March 2000
- Sturhahn, W.
- Hyperfine Interactions, Vol. 125, Issue 1/4, p. 149-172
Nuclear resonant spectroscopy
journal, January 2004
- Sturhahn, Wolfgang
- Journal of Physics: Condensed Matter, Vol. 16, Issue 5
Phonon Density of States Measured by Inelastic Nuclear Resonant Scattering
journal, May 1995
- Sturhahn, W.; Toellner, T. S.; Alp, E. E.
- Physical Review Letters, Vol. 74, Issue 19
EuFe 2 As 2 under High Pressure: An Antiferromagnetic Bulk Superconductor
journal, August 2009
- Terashima, Taichi; Kimata, Motoi; Satsukawa, Hidetaka
- Journal of the Physical Society of Japan, Vol. 78, Issue 8
Monochromatization of synchrotron radiation for nuclear resonant scattering experiments
journal, January 2000
- Toellner, T. S.
- Hyperfine Interactions, Vol. 125, Issue 1/4, p. 3-28
A cryogenically stabilized meV-monochromator for hard X-rays
journal, February 2006
- Toellner, T. S.; Alatas, A.; Said, A.
- Journal of Synchrotron Radiation, Vol. 13, Issue 2
Structural phase transitions in EuFe 2 As 2 superconductor at low temperatures and high pressures
journal, August 2011
- Uhoya, Walter O.; Tsoi, Georgiy M.; Vohra, Yogesh K.
- Journal of Physics: Condensed Matter, Vol. 23, Issue 36
Pressure-decoupled magnetic and structural transitions of the parent compound of iron-based 122 superconductors BaFe2As2
journal, October 2013
- Wu, J. J.; Lin, J. -F.; Wang, X. C.
- Proceedings of the National Academy of Sciences, Vol. 110, Issue 43
Magnetic and structural transitions of SrFe2As2 at high pressure and low temperature
journal, January 2014
- Wu, J. J.; Lin, J. F.; Wang, X. C.
- Scientific Reports, Vol. 4, Issue 1
Nuclear resonant scattering at high pressure and high temperature
journal, December 2004
- Zhao, Jiyong; Sturhahn, Wolfgang; Lin, Jung-fu
- High Pressure Research, Vol. 24, Issue 4
Works referencing / citing this record:
Magnetic phase diagram of -FeH
journal, January 2020
- Ying, Jianjun; Zhao, Jiyong; Bi, Wenli
- Physical Review B, Vol. 101, Issue 2
Microscopic phase diagram of LaFeAsO single crystals under pressure
journal, November 2018
- Materne, Philipp; Bi, Wenli; Zhao, Jiyong
- Physical Review B, Vol. 98, Issue 17
High-pressure nuclear inelastic scattering with backscattering monochromatization
journal, August 2019
- Sergueev, Ilya; Glazyrin, Konstantin; Herrmann, Markus G.
- Journal of Synchrotron Radiation, Vol. 26, Issue 5
High-pressure nuclear inelastic scattering with backscattering monochromatization
text, January 2019
- Sergueev, Ilya; Glazyrin, Konstantin; Herrmann, Markus G.
- Deutsches Elektronen-Synchrotron, DESY, Hamburg
Microscopic phase diagram of LaFeAsO single crystals under pressure
text, January 2018
- Materne, Philipp; Bi, Wenli; Zhao, Jiyong
- Unpublished