Advanced grazing-incidence techniques for modern soft-matter materials analysis

Hexemer, Alexander; Müller-Buschbaum, Peter

doi:10.1107/S2052252514024178

Title: Advanced grazing-incidence techniques for modern soft-matter materials analysis

Abstract

The complex nano-morphology of modern soft-matter materials is successfully probed with advanced grazing-incidence techniques. Based on grazing-incidence small- and wide-angle X-ray and neutron scattering (GISAXS, GIWAXS, GISANS and GIWANS), new possibilities arise which are discussed with selected examples. Due to instrumental progress, highly interesting possibilities for local structure analysis in this material class arise from the use of micro- and nanometer-sized X-ray beams in micro- or nanofocused GISAXS and GIWAXS experiments. The feasibility of very short data acquisition times down to milliseconds creates exciting possibilities forin situandin operandoGISAXS and GIWAXS studies. Tuning the energy of GISAXS and GIWAXS in the soft X-ray regime and in time-of flight GISANS allows the tailoring of contrast conditions and thereby the probing of more complex morphologies. In addition, recent progress in software packages, useful for data analysis for advanced grazing-incidence techniques, is discussed.

Authors:

Hexemer, Alexander ^[1]; Müller-Buschbaum, Peter ^[2]

Lawrence Berkeley National Lab., CA (United States)
Physik-Department, Lehrstuhl für Funktionelle Materialien, Technische Universität München, Garching (Germany); cNanosystems Initiative Munich,, Munchen (Germany)

Publication Date:: Thu Jan 01 00:00:00 EST 2015

Research Org.:: Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1209548

Grant/Contract Number:: AC02-05CH11231

Resource Type:: Accepted Manuscript

Journal Name:: IUCrJ

Additional Journal Information:: Journal Volume: 2; Journal Issue: 1; Journal ID: ISSN 2052-2525

Publisher:: International Union of Crystallography

Country of Publication:: United States

Language:: English

Subject:: 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; grazing-incidence techniques; GISAXS; GIWAXS; resonant soft X-ray scattering; GISANS; morphology; soft matter

Citation Formats


                    Hexemer, Alexander, and Müller-Buschbaum, Peter. Advanced grazing-incidence techniques for modern soft-matter materials analysis.  United States: N. p., 2015. 
Web.  doi:10.1107/S2052252514024178.

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                    Hexemer, Alexander, & Müller-Buschbaum, Peter. Advanced grazing-incidence techniques for modern soft-matter materials analysis.  United States.  https://doi.org/10.1107/S2052252514024178

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                    Hexemer, Alexander, and Müller-Buschbaum, Peter. Thu .  
"Advanced grazing-incidence techniques for modern soft-matter materials analysis".  United States.  https://doi.org/10.1107/S2052252514024178.  https://www.osti.gov/servlets/purl/1209548.

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@article{osti_1209548,

  title        = {Advanced grazing-incidence techniques for modern soft-matter materials analysis},

  author       = {Hexemer, Alexander and Müller-Buschbaum, Peter},

  abstractNote = {The complex nano-morphology of modern soft-matter materials is successfully probed with advanced grazing-incidence techniques. Based on grazing-incidence small- and wide-angle X-ray and neutron scattering (GISAXS, GIWAXS, GISANS and GIWANS), new possibilities arise which are discussed with selected examples. Due to instrumental progress, highly interesting possibilities for local structure analysis in this material class arise from the use of micro- and nanometer-sized X-ray beams in micro- or nanofocused GISAXS and GIWAXS experiments. The feasibility of very short data acquisition times down to milliseconds creates exciting possibilities forin situandin operandoGISAXS and GIWAXS studies. Tuning the energy of GISAXS and GIWAXS in the soft X-ray regime and in time-of flight GISANS allows the tailoring of contrast conditions and thereby the probing of more complex morphologies. In addition, recent progress in software packages, useful for data analysis for advanced grazing-incidence techniques, is discussed.},

  doi          = {10.1107/S2052252514024178},

  journal      = {IUCrJ},

  number       = 1,

  volume       = 2,

  place        = {United States},

  year         = {Thu Jan 01 00:00:00 EST 2015},

  month        = {Thu Jan 01 00:00:00 EST 2015}

}

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Title: Advanced grazing-incidence techniques for modern soft-matter materials analysis

Abstract

Citation Formats

Substrate‐Dependent Molecular and Nanostructural Orientation of Nafion Thin Films journal, July 2019

The Crystallization of PEDOT:PSS Polymeric Electrodes Probed In Situ during Printing journal, April 2015

Structure of Organometal Halide Perovskite Films as Determined with Grazing-Incidence X-Ray Scattering Methods journal, March 2017

Energy Losses in Small-Molecule Organic Photovoltaics journal, June 2017

An in situ GISAXS study of selective solvent vapor annealing in thin block copolymer films: Symmetry breaking of in-plane sphere order upon deswelling journal, October 2015

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Morphological properties of airbrush spray-deposited enzymatic cellulose thin films journal, May 2018

In situ grazing-incidence small-angle X-ray scattering observation of block-copolymer templated formation of magnetic nanodot arrays and their magnetic properties journal, November 2016

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In operando morphology investigation of inverted bulk heterojunction organic solar cells by GISAXS journal, January 2015

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HEKATE—A novel grazing incidence neutron scattering concept for the European Spallation Source journal, March 2018

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Drying of electrically conductive hybrid polymer–gold nanorods studied with in situ microbeam GISAXS collection, January 2019

Morphological properties of airbrush spray-deposited enzymatic cellulose thin films text, January 2018

Distortion analysis of crystalline and locally quasicrystalline 2D photonic structures with grazing-incidence small-angle X-ray scattering text, January 2019

Investigating Polymer–Metal Interfaces by Grazing Incidence Small-Angle X-Ray Scattering from Gradients to Real-Time Studies text, January 2016

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Drying of electrically conductive hybrid polymer–gold nanorods studied with in situ microbeam GISAXS text, January 2019

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Substrate‐Dependent Molecular and Nanostructural Orientation of Nafion Thin Films
journal, July 2019

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journal, April 2015

Structure of Organometal Halide Perovskite Films as Determined with Grazing-Incidence X-Ray Scattering Methods
journal, March 2017

Energy Losses in Small-Molecule Organic Photovoltaics
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An in situ GISAXS study of selective solvent vapor annealing in thin block copolymer films: Symmetry breaking of in-plane sphere order upon deswelling
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journal, March 2018

Morphological properties of airbrush spray-deposited enzymatic cellulose thin films
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In situ grazing-incidence small-angle X-ray scattering observation of block-copolymer templated formation of magnetic nanodot arrays and their magnetic properties
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journal, January 2015

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journal, January 2018

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journal, January 2019

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journal, January 2019

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journal, January 2018

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journal, January 2019

Determining order-to-disorder transitions in block copolymer thin films using a self-referencing fluorescent probe
journal, January 2020

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journal, March 2018

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journal, November 2016

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journal, September 2016

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journal, March 2019

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journal, May 2019

Grazing-incidence small-angle X-ray scattering (GISAXS) on small periodic targets using large beams
journal, May 2017

Hybrid perovskite solar cells: In situ investigation of solution-processed PbI ₂ reveals metastable precursors and a pathway to producing porous thin films
journal, April 2017

Morphological characterization of fullerene and fullerene-free organic photovoltaics by combined real and reciprocal space techniques
journal, May 2017

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journal, March 2019

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text, January 2019

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journal, December 2016

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journal, September 2019

Distortion analysis of crystalline and locally quasicrystalline 2D photonic structures with grazing-incidence small-angle X-ray scattering
text, January 2019

Unravelling the structural rearrangement of polymer colloidal crystals under dry sintering conditions
text, January 2018

Structure-function correlations in sputter deposited gold/fluorocarbon multilayers for tuning optical response
text, January 2019

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journal, April 2019

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collection, January 2019

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text, January 2018

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text, January 2019

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text, January 2016

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text, January 2019

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text, January 2019

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