Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water

Bruemmer, S. M.; Olszta, M. J.; Toloczko, M. B.; Schreiber, D. K.

doi:10.1016/J.CORSCI.2017.11.024

Title: Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water

Abstract

The effects of alloying elements in Ni-5at%X binary alloys on intergranular (IG) corrosion and stress corrosion cracking (SCC) have been assessed in 300–360 °C hydrogenated water at the Ni/NiO stability line. Alloys with Cr or Al additions exhibited grain boundary oxidation and IGSCC, while localized degradation was not observed for pure Ni, Ni-Cu or Ni-Fe alloys. Environment-enhanced crack growth was determined by comparing the response in water and N₂ gas. Lastly, results demonstrate that selective grain boundary oxidation of Cr and Al promoted IGSCC of these Ni alloys in hydrogenated water.

Authors:

Bruemmer, S. M. ^[1]; Olszta, M. J. ^[1]; Toloczko, M. B. ^[1]; Schreiber, D. K. ^[1]

Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

Publication Date:: Sun Nov 26 00:00:00 EST 2017

Research Org.:: Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE Office of Science (SC), Biological and Environmental Research (BER)

OSTI Identifier:: 1413459

Report Number(s):: PNNL-SA-129070
Journal ID: ISSN 0010-938X; PII: S0010938X17317997; TRN: US1800431

Grant/Contract Number:: AC05-76RL01830

Resource Type:: Accepted Manuscript

Journal Name:: Corrosion Science

Additional Journal Information:: Journal Volume: 131; Journal ID: ISSN 0010-938X

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; A. Nickel; Alloy; B. TEM; C. Intergranular corrosion; Stress corrosion; Selective oxidation

Citation Formats


                    Bruemmer, S. M., Olszta, M. J., Toloczko, M. B., and Schreiber, D. K. Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water.  United States: N. p., 2017. 
Web.  doi:10.1016/J.CORSCI.2017.11.024.

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                    Bruemmer, S. M., Olszta, M. J., Toloczko, M. B., & Schreiber, D. K. Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water.  United States.  https://doi.org/10.1016/J.CORSCI.2017.11.024

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                    Bruemmer, S. M., Olszta, M. J., Toloczko, M. B., and Schreiber, D. K. Sun .  
"Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water".  United States.  https://doi.org/10.1016/J.CORSCI.2017.11.024.  https://www.osti.gov/servlets/purl/1413459.

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@article{osti_1413459,

  title        = {Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water},

  author       = {Bruemmer, S. M. and Olszta, M. J. and Toloczko, M. B. and Schreiber, D. K.},

  abstractNote = {The effects of alloying elements in Ni-5at%X binary alloys on intergranular (IG) corrosion and stress corrosion cracking (SCC) have been assessed in 300–360 °C hydrogenated water at the Ni/NiO stability line. Alloys with Cr or Al additions exhibited grain boundary oxidation and IGSCC, while localized degradation was not observed for pure Ni, Ni-Cu or Ni-Fe alloys. Environment-enhanced crack growth was determined by comparing the response in water and N2 gas. Lastly, results demonstrate that selective grain boundary oxidation of Cr and Al promoted IGSCC of these Ni alloys in hydrogenated water.},

  doi          = {10.1016/J.CORSCI.2017.11.024},

  journal      = {Corrosion Science},

  number       = ,

  volume       = 131,

  place        = {United States},

  year         = {Sun Nov 26 00:00:00 EST 2017},

  month        = {Sun Nov 26 00:00:00 EST 2017}

}

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https://doi.org/10.1016/J.CORSCI.2017.11.024

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Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water

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Title: Grain boundary selective oxidation and intergranular stress corrosion crack growth of high-purity nickel binary alloys in high-temperature hydrogenated water

Abstract

Citation Formats

Emerging Issues and Fundamental Processes in Environmental Cracking in Hot Water journal, May 2008

Microstructural and microchemical mechanisms controlling intergranular stress corrosion cracking in light-water-reactor systems journal, October 1994

Equilibrium aspects of hydrogen-induced cracking of steels journal, September 1974

The effects of segregated impurities on intergranular fracture energy journal, April 1979

A Quantitative Model of Hydrogen Induced Grain Boundary Cracking journal, May 1973

Stress corrosion cracking mechanisms of alloy 600 polycrystals and single crystals in primary water—Influence of hydrogen journal, August 2000

Stress Corrosion Cracking of Stainless Steels and Nickel Alloys in High-Temperature Water journal, January 2008

Life prediction by mechanistic modeling and system monitoring of environmental cracking of iron and nickel alloys in aqueous systems journal, August 1988

IGSCC Behavior of Alloy 600 Steam Generator Tubing in Water or Steam Tests Above 360 C journal, December 1987

High-Resolution Characterization of Intergranular Attack and Stress Corrosion Cracking of Alloy 600 in High-Temperature Primary Water journal, June 2000

TEM investigations of intergranular stress corrosion cracking in austenitic alloys in PWR environmental conditions journal, January 2003

Advanced TEM characterization of stress corrosion cracking of Alloy 600 in pressurized water reactor primary water environment journal, September 2009

Examinations of Oxidation and Sulfidation of Grain Boundaries in Alloy 600 Exposed to Simulated Pressurized Water Reactor Primary Water journal, April 2013

Internal oxidation journal, December 1988

Enhanced diffusion of oxygen during internal oxidation of nickel-base alloys journal, December 1982

The high-temperature internal oxidation and intergranular oxidation of nickel-chromium alloys journal, January 1983

Influence of oxide films on primary water stress corrosion cracking initiation of alloy 600 journal, January 2006

Advanced microstructural characterization of the intergranular oxidation of Alloy 600 journal, November 2015

Internal oxidation of alloy 690 in hydrogenated steam journal, January 2015

An atom probe tomography study of internal oxidation processes in Alloy 600 journal, May 2016

In situ site-specific specimen preparation for atom probe tomography journal, February 2007

TEM Sample Preparation and FIB-Induced Damage journal, May 2007

Directly correlated transmission electron microscopy and atom probe tomography of grain boundary oxidation in a Ni–Al binary alloy exposed to high-temperature water journal, October 2013

Grain boundary depletion and migration during selective oxidation of Cr in a Ni–5Cr binary alloy exposed to high-temperature hydrogenated water journal, October 2014

Effects of boundary migration and pinning particles on intergranular oxidation revealed by 2D and 3D analytical electron microscopy journal, June 2017

Three-dimensional characterization of stress corrosion cracks journal, January 2011

Potential-pH diagrams for alloy-water systems under LWR conditions journal, May 1993

Pourbaix diagrams for chromium, aluminum and titanium extended to high-subcritical and low-supercritical conditions journal, May 2012

Revised Pourbaix Diagrams for Copper at 25 to 300°C journal, January 1997

Pourbaix diagrams for the iron–water system extended to high-subcritical and low-supercritical conditions journal, February 2012

Pourbaix diagrams for the nickel-water system extended to high-subcritical and low-supercritical conditions journal, May 2012

Selective Internal Oxidation as a Mechanism for Intergranular Stress Corrosion Cracking of Ni-Cr-Fe Alloys journal, June 2007

Ab Initio Modeling of Bulk and Intragranular Diffusion in Ni Alloys journal, April 2015

The mechanism of oxidation of dilute NiAl alloys at 800–1200°C journal, January 1977

Mechanism of Oxidation of Dilute Nickel–Chromium Alloys journal, September 1966

Creep and intergranular cracking of Ni-Cr-Fe-C in 360 °C argon journal, June 1994

Development of an Oxidation Method for Prior Austenite Grain Boundary Revelation journal, August 2018

Chemo-mechanical coupling effect on high temperature oxidation: A review journal, July 2019

Emerging Issues and Fundamental Processes in Environmental Cracking in Hot Water
journal, May 2008

Microstructural and microchemical mechanisms controlling intergranular stress corrosion cracking in light-water-reactor systems
journal, October 1994

Equilibrium aspects of hydrogen-induced cracking of steels
journal, September 1974

The effects of segregated impurities on intergranular fracture energy
journal, April 1979

A Quantitative Model of Hydrogen Induced Grain Boundary Cracking
journal, May 1973

Stress corrosion cracking mechanisms of alloy 600 polycrystals and single crystals in primary water—Influence of hydrogen
journal, August 2000

Stress Corrosion Cracking of Stainless Steels and Nickel Alloys in High-Temperature Water
journal, January 2008

Life prediction by mechanistic modeling and system monitoring of environmental cracking of iron and nickel alloys in aqueous systems
journal, August 1988

IGSCC Behavior of Alloy 600 Steam Generator Tubing in Water or Steam Tests Above 360 C
journal, December 1987

High-Resolution Characterization of Intergranular Attack and Stress Corrosion Cracking of Alloy 600 in High-Temperature Primary Water
journal, June 2000

TEM investigations of intergranular stress corrosion cracking in austenitic alloys in PWR environmental conditions
journal, January 2003

Advanced TEM characterization of stress corrosion cracking of Alloy 600 in pressurized water reactor primary water environment
journal, September 2009

Examinations of Oxidation and Sulfidation of Grain Boundaries in Alloy 600 Exposed to Simulated Pressurized Water Reactor Primary Water
journal, April 2013

Internal oxidation
journal, December 1988

Enhanced diffusion of oxygen during internal oxidation of nickel-base alloys
journal, December 1982

The high-temperature internal oxidation and intergranular oxidation of nickel-chromium alloys
journal, January 1983

Influence of oxide films on primary water stress corrosion cracking initiation of alloy 600
journal, January 2006

Advanced microstructural characterization of the intergranular oxidation of Alloy 600
journal, November 2015

Internal oxidation of alloy 690 in hydrogenated steam
journal, January 2015

An atom probe tomography study of internal oxidation processes in Alloy 600
journal, May 2016

In situ site-specific specimen preparation for atom probe tomography
journal, February 2007

TEM Sample Preparation and FIB-Induced Damage
journal, May 2007

Directly correlated transmission electron microscopy and atom probe tomography of grain boundary oxidation in a Ni–Al binary alloy exposed to high-temperature water
journal, October 2013

Grain boundary depletion and migration during selective oxidation of Cr in a Ni–5Cr binary alloy exposed to high-temperature hydrogenated water
journal, October 2014

Effects of boundary migration and pinning particles on intergranular oxidation revealed by 2D and 3D analytical electron microscopy
journal, June 2017

Three-dimensional characterization of stress corrosion cracks
journal, January 2011

Potential-pH diagrams for alloy-water systems under LWR conditions
journal, May 1993

Pourbaix diagrams for chromium, aluminum and titanium extended to high-subcritical and low-supercritical conditions
journal, May 2012

Revised Pourbaix Diagrams for Copper at 25 to 300°C
journal, January 1997

Pourbaix diagrams for the iron–water system extended to high-subcritical and low-supercritical conditions
journal, February 2012

Pourbaix diagrams for the nickel-water system extended to high-subcritical and low-supercritical conditions
journal, May 2012

Selective Internal Oxidation as a Mechanism for Intergranular Stress Corrosion Cracking of Ni-Cr-Fe Alloys
journal, June 2007

Ab Initio Modeling of Bulk and Intragranular Diffusion in Ni Alloys
journal, April 2015

The mechanism of oxidation of dilute NiAl alloys at 800–1200°C
journal, January 1977

Mechanism of Oxidation of Dilute Nickel–Chromium Alloys
journal, September 1966

Creep and intergranular cracking of Ni-Cr-Fe-C in 360 °C argon
journal, June 1994

Development of an Oxidation Method for Prior Austenite Grain Boundary Revelation
journal, August 2018

Chemo-mechanical coupling effect on high temperature oxidation: A review
journal, July 2019