The solidification products of levitated Fe83B17 studied by high-energy x-ray diffraction

Quirinale, D. G.; Rustan, G. E.; Kreyssig, A.; Lapidus, S. H.; Kramer, M. J.; Goldman, A. I.

doi:10.1063/1.4966596

Title: The solidification products of levitated Fe83B17 studied by high-energy x-ray diffraction

Abstract

Detailed high-energy x-ray diffraction studies were performed to gain insight into the evolution of phase formation in undercooled Fe₈₃B₁₇ and the mechanism for the stabilization of face-centered cubic (fcc) Fe in the presence of Fe₂₃B₆. Fe₈₃B₁₇ solidifies directly into either the equilibrium Fe₂B + Fe phases or the metastable Fe₂₃B₆ + Fe phases. When formed, the metastable Fe₂₃B₆ phase either rapidly transforms into the equilibrium Fe₂B phase within the solidification plateau or can persist down to ambient temperature. Here, we detail these different solidification behaviors in a set of thermal cycles taken from one sample and demonstrate the absence of a direct correlation with cooling rate and thermal history. We show that the coherent growth of Fe₂₃B₆ and fcc Fe suppresses the allotropic transition from fcc Fe to bcc Fe. The temperature evolution of the phase fractions and lattice parameters is also presented.

Authors:

Quirinale, D. G. ^[1]; Rustan, G. E. ^[1]; Kreyssig, A. ^[1]; Lapidus, S. H. ^[2]; Kramer, M. J. ^[1]; Goldman, A. I. ^[1]

Iowa State Univ., Ames, IA (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)

Publication Date:: Thu Nov 03 00:00:00 EDT 2016

Research Org.:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science - Office of Basic Energy Sciences - Materials Sciences and Engineering Division; National Science Foundation (NSF); Pennsylvania State Univ., University Park, PA (United States). Materials Research Science and Engineering Center (MRSEC); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

OSTI Identifier:: 1411023

Alternate Identifier(s):: OSTI ID: 1330909

Grant/Contract Number:: AC02-06CH11357; AC02-07CH11358; DMR-1308099

Resource Type:: Accepted Manuscript

Journal Name:: Journal of Applied Physics

Additional Journal Information:: Journal Volume: 120; Journal Issue: 17; Journal ID: ISSN 0021-8979

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; Crystallography; Thermal instruments; Crystal lattices; Crystal structure; High-energy X rays; Supercooling; X-ray diffraction; Bragg peak; Epitaxy; Phase transitions

Citation Formats


                    Quirinale, D. G., Rustan, G. E., Kreyssig, A., Lapidus, S. H., Kramer, M. J., and Goldman, A. I. The solidification products of levitated Fe83B17 studied by high-energy x-ray diffraction.  United States: N. p., 2016. 
Web.  doi:10.1063/1.4966596.

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                    Quirinale, D. G., Rustan, G. E., Kreyssig, A., Lapidus, S. H., Kramer, M. J., & Goldman, A. I. The solidification products of levitated Fe83B17 studied by high-energy x-ray diffraction.  United States.  https://doi.org/10.1063/1.4966596

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                    Quirinale, D. G., Rustan, G. E., Kreyssig, A., Lapidus, S. H., Kramer, M. J., and Goldman, A. I. Thu .  
"The solidification products of levitated Fe83B17 studied by high-energy x-ray diffraction".  United States.  https://doi.org/10.1063/1.4966596.  https://www.osti.gov/servlets/purl/1411023.

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@article{osti_1411023,

  title        = {The solidification products of levitated Fe83B17 studied by high-energy x-ray diffraction},

  author       = {Quirinale, D. G. and Rustan, G. E. and Kreyssig, A. and Lapidus, S. H. and Kramer, M. J. and Goldman, A. I.},

  abstractNote = {Detailed high-energy x-ray diffraction studies were performed to gain insight into the evolution of phase formation in undercooled Fe83B17 and the mechanism for the stabilization of face-centered cubic (fcc) Fe in the presence of Fe23B6. Fe83B17 solidifies directly into either the equilibrium Fe2B + Fe phases or the metastable Fe23B6 + Fe phases. When formed, the metastable Fe23B6 phase either rapidly transforms into the equilibrium Fe2B phase within the solidification plateau or can persist down to ambient temperature. Here, we detail these different solidification behaviors in a set of thermal cycles taken from one sample and demonstrate the absence of a direct correlation with cooling rate and thermal history. We show that the coherent growth of Fe23B6 and fcc Fe suppresses the allotropic transition from fcc Fe to bcc Fe. The temperature evolution of the phase fractions and lattice parameters is also presented.},

  doi          = {10.1063/1.4966596},

  journal      = {Journal of Applied Physics},

  number       = 17,

  volume       = 120,

  place        = {United States},

  year         = {Thu Nov 03 00:00:00 EDT 2016},

  month        = {Thu Nov 03 00:00:00 EDT 2016}

}

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Title: The solidification products of levitated Fe83B17 studied by high-energy x-ray diffraction

Abstract

Citation Formats

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Crystallization of the amorphous alloys Fe50Ni30B20and Fe80oB20
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