Flexible and conductive MXene films and nanocomposites with high capacitance
Abstract
MXenes, a new family of 2D materials, combine hydrophilic surfaces with metallic conductivity. Delamination of MXene produces single-layer nanosheets with thickness of about a nanometer and lateral size of the order of micrometers. The high aspect ratio of delaminated MXene renders it promising nanofiller in multifunctional polymer nanocomposites. In this study, Ti3C2Tx MXene was mixed with either a charged polydiallyldimethylammonium chloride (PDDA) or an electrically neutral polyvinyl alcohol (PVA) to produce Ti3C2Tx/polymer composites. The as-fabricated composites are flexible and have electrical conductivities as high as 2.2 × 104 S/m in the case of the Ti3C2Tx/PVA composite film and 2.4 × 105 S/m for pure Ti3C2Tx films. The tensile strength of the Ti3C2Tx/PVA composites was significantly enhanced compared with pure Ti3C2Tx or PVA films. The intercalation and confinement of the polymer between the MXene flakes not only increased flexibility but also enhanced cationic intercalation, offering an impressive volumetric capacitance of ~530 F/cm3 for MXene/PVA-KOH composite film at 2 mV/s. Finally, to our knowledge, this study is a first, but crucial, step in exploring the potential of using MXenes in polymer-based multifunctional nanocomposites for a host of applications, such as structural components, energy storage devices, wearable electronics, electrochemical actuators, and radiofrequency shielding,more »
- Authors:
-
- Drexel Univ., Philadelphia, PA (United States); Dalian University of Technology (China)
- Drexel Univ., Philadelphia, PA (United States)
- Drexel Univ., Philadelphia, PA (United States); Nanjing Univ. (China)
- Dalian University of Technology (China)
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC)
- OSTI Identifier:
- 1286810
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Proceedings of the National Academy of Sciences of the United States of America (Online)
- Additional Journal Information:
- Journal Name: Proceedings of the National Academy of Sciences of the United States of America (Online); Journal Volume: 111; Journal Issue: 47; Journal ID: ISSN 1091-6490
- Publisher:
- National Academy of Sciences
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; 25 ENERGY STORAGE
Citation Formats
Ling, Zheng, Ren, Chang E., Zhao, Meng-Qiang, Yang, Jian, Giammarco, James M., Qiu, Jieshan, Barsoum, Michel W., and Gogotsi, Yury. Flexible and conductive MXene films and nanocomposites with high capacitance. United States: N. p., 2014.
Web. doi:10.1073/pnas.1414215111.
Ling, Zheng, Ren, Chang E., Zhao, Meng-Qiang, Yang, Jian, Giammarco, James M., Qiu, Jieshan, Barsoum, Michel W., & Gogotsi, Yury. Flexible and conductive MXene films and nanocomposites with high capacitance. United States. https://doi.org/10.1073/pnas.1414215111
Ling, Zheng, Ren, Chang E., Zhao, Meng-Qiang, Yang, Jian, Giammarco, James M., Qiu, Jieshan, Barsoum, Michel W., and Gogotsi, Yury. Tue .
"Flexible and conductive MXene films and nanocomposites with high capacitance". United States. https://doi.org/10.1073/pnas.1414215111. https://www.osti.gov/servlets/purl/1286810.
@article{osti_1286810,
title = {Flexible and conductive MXene films and nanocomposites with high capacitance},
author = {Ling, Zheng and Ren, Chang E. and Zhao, Meng-Qiang and Yang, Jian and Giammarco, James M. and Qiu, Jieshan and Barsoum, Michel W. and Gogotsi, Yury},
abstractNote = {MXenes, a new family of 2D materials, combine hydrophilic surfaces with metallic conductivity. Delamination of MXene produces single-layer nanosheets with thickness of about a nanometer and lateral size of the order of micrometers. The high aspect ratio of delaminated MXene renders it promising nanofiller in multifunctional polymer nanocomposites. In this study, Ti3C2Tx MXene was mixed with either a charged polydiallyldimethylammonium chloride (PDDA) or an electrically neutral polyvinyl alcohol (PVA) to produce Ti3C2Tx/polymer composites. The as-fabricated composites are flexible and have electrical conductivities as high as 2.2 × 104 S/m in the case of the Ti3C2Tx/PVA composite film and 2.4 × 105 S/m for pure Ti3C2Tx films. The tensile strength of the Ti3C2Tx/PVA composites was significantly enhanced compared with pure Ti3C2Tx or PVA films. The intercalation and confinement of the polymer between the MXene flakes not only increased flexibility but also enhanced cationic intercalation, offering an impressive volumetric capacitance of ~530 F/cm3 for MXene/PVA-KOH composite film at 2 mV/s. Finally, to our knowledge, this study is a first, but crucial, step in exploring the potential of using MXenes in polymer-based multifunctional nanocomposites for a host of applications, such as structural components, energy storage devices, wearable electronics, electrochemical actuators, and radiofrequency shielding, to name a few.},
doi = {10.1073/pnas.1414215111},
journal = {Proceedings of the National Academy of Sciences of the United States of America (Online)},
number = 47,
volume = 111,
place = {United States},
year = {Tue Nov 11 00:00:00 EST 2014},
month = {Tue Nov 11 00:00:00 EST 2014}
}
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Leaf-inspired multiresponsive MXene-based actuator for programmable smart devices
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Near-Infrared Light and Solar Light Activated Self-Healing Epoxy Coating having Enhanced Properties Using MXene Flakes as Multifunctional Fillers
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High-Voltage Symmetric Supercapacitor Based on 2D Titanium Carbide (MXene, Ti 2 CT x )/Carbon Nanosphere Composites in a Neutral Aqueous Electrolyte
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Adhesion of two-dimensional titanium carbides (MXenes) and graphene to silicon
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Two-dimensional MXene-reinforced robust surface superhydrophobicity with self-cleaning and photothermal-actuating binary effects
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Interrogating the impact of onion-like carbons on the supercapacitive properties of MXene (Ti 2 CT X )
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A highly flexible and sensitive piezoresistive sensor based on MXene with greatly changed interlayer distances
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Electromagnetic Shielding by MXene-Graphene-PVDF Composite with Hydrophobic, Lightweight and Flexible Graphene Coated Fabric
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Dynamic charge acceptance and hydrogen evolution of a new MXene additive in advanced lead-acid batteries via a rapid screening three-electrode method
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A nanoporous MXene film enables flexible supercapacitors with high energy storage
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Enhanced thermal properties of poly(vinylidene fluoride) composites with ultrathin nanosheets of MXene
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A wearable, self-adhesive, long-lastingly moist and healable epidermal sensor assembled from conductive MXene nanocomposites
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A synergetic stabilization and strengthening strategy for two-dimensional ordered hybrid transition metal carbides
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Knittable and Washable Multifunctional MXene‐Coated Cellulose Yarns
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A safe and fast-charging lithium-ion battery anode using MXene supported Li 3 VO 4
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Synergistic Effects between MXenes and Ni Chains in Flexible and Ultrathin Electromagnetic Interference Shielding Films
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Interface Schottky barrier in Hf 2 NT 2 /MSSe (T = F, O, OH; M = Mo, W) heterostructures
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Magazine‐Bending‐Inspired Architecting Anti‐T of MXene Flakes with Vertical Ion Transport for High‐Performance Supercapacitors
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Photoluminescent Ti 3 C 2 MXene Quantum Dots for Multicolor Cellular Imaging
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The effect of two‐dimensional d‐Ti 3 C 2 on the mechanical and thermal conductivity properties of thermoplastic polyurethane composites
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Alkali-induced 3D crinkled porous Ti 3 C 2 MXene architectures coupled with NiCoP bimetallic phosphide nanoparticles as anodes for high-performance sodium-ion batteries
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Biomimetic MXene Textures with Enhanced Light‐to‐Heat Conversion for Solar Steam Generation and Wearable Thermal Management
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Highly Conductive Ti 3 C 2 T x MXene Hybrid Fibers for Flexible and Elastic Fiber-Shaped Supercapacitors
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Solution-processed titanium carbide MXene films examined as highly transparent conductors
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Mechanically strong MXene/Kevlar nanofiber composite membranes as high-performance nanofluidic osmotic power generators
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Silver nanowires intercalating Ti 3 C 2 T x MXene composite films with excellent flexibility for electromagnetic interference shielding
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Controllable magnitude and anisotropy of the electrical conductivity of Hf 3 C 2 O 2 MXene
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MXene-supported Co 3 O 4 quantum dots for superior lithium storage and oxygen evolution activities
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Ultrathin MXene-Micropattern-Based Field-Effect Transistor for Probing Neural Activity
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Alternative electrodes for HTMs and noble-metal-free perovskite solar cells: 2D MXenes electrodes
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Highly Flexible, Freestanding Supercapacitor Electrode with Enhanced Performance Obtained by Hybridizing Polypyrrole Chains with MXene
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Facile Solution Processing of Stable MXene Dispersions towards Conductive Composite Fibers
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Ti 3 C 2 T x (MXene)‐Silicon Heterojunction for Efficient Photovoltaic Cells
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Advances in Two-Dimensional MXenes for Nitrogen Electrocatalytic Reduction to Ammonia
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MXenes for Plasmonic Photodetection
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Tailoring Electrocatalytic Properties of Pt Nanoparticles Grown on Ti 3 C 2 T X MXene Surface
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Two-dimensional semiconducting Lu 2 CT 2 (T = F, OH) MXene with low work function and high carrier mobility
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Heterostructures of MXenes and N-doped graphene as highly active bifunctional electrocatalysts
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Review of MXenes as new nanomaterials for energy storage/delivery and selected environmental applications
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Ti 3 C 2 MXene as a new nanofiller for robust and conductive elastomer composites
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Wearable Electronics Based on 2D Materials for Human Physiological Information Detection
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2D MXene-containing polymer electrolytes for all-solid-state lithium metal batteries
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Unleashing the potential of Ti 2 CT x MXene as a pulse modulator for mid-infrared fiber lasers
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Conductive Inks Based on a Lithium Titanate Nanotube Gel for High-Rate Lithium-Ion Batteries with Customized Configuration
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Flexible Ti 3 C 2 T x /PEDOT:PSS films with outstanding volumetric capacitance for asymmetric supercapacitors
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Preparation of a new 2D MXene/PES composite membrane with excellent hydrophilicity and high flux
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Polyoxometalate-coupled MXene nanohybrid via poly(ionic liquid) linkers and its electrode for enhanced supercapacitive performance
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Lightweight and flexible MXene/CNF/silver composite membranes with a brick-like structure and high-performance electromagnetic-interference shielding
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MXene Aerogel Scaffolds for High‐Rate Lithium Metal Anodes
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In situ formation of NaTi 2 (PO 4 ) 3 cubes on Ti 3 C 2 MXene for dual-mode sodium storage
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Preparation and electrochemical performance of modified Ti 3 C 2 T x /polypyrrole composites
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Titanium carbide MXene: Synthesis, electrical and optical properties and their applications in sensors and energy storage devices
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Thickness-independent capacitance of vertically aligned liquid-crystalline MXenes
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Mechanically strong and electrically conductive multilayer MXene nanocomposites
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Hollow MXene Spheres and 3D Macroporous MXene Frameworks for Na-Ion Storage
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Ternary Manganese Oxide Composite Electrodes to Harvest Enhanced Capacitive Performances via Successive Reaction Mechanism
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Ultrastrong and Highly Conductive MXene‐Based Films for High‐Performance Electromagnetic Interference Shielding
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Electromagnetic interference shielding with 2D transition metal carbides (MXenes)
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Ultrafast Flash Energy Conductance at MXene‐Surfactant Interface and Its Molecular Origins
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Highly Conductive Optical Quality Solution-Processed Films of 2D Titanium Carbide
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Flexible MXene/Graphene Films for Ultrafast Supercapacitors with Outstanding Volumetric Capacitance
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Inkjet Printing of Self-Assembled 2D Titanium Carbide and Protein Electrodes for Stimuli-Responsive Electromagnetic Shielding
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The Rise of 2D Photothermal Materials beyond Graphene for Clean Water Production
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Foldable Conductive Cellulose Fiber Networks Modified by Graphene Nanoplatelet-Bio-Based Composites
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MXene-Silicon Van Der Waals Heterostructures for High-Speed Self-Driven Photodetectors
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MoS 2 -on-MXene Heterostructures as Highly Reversible Anode Materials for Lithium-Ion Batteries
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Superior electronic structure of two-dimensional 3d transition metal dicarbides for applications in spintronics
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Applications of 2D MXenes in energy conversion and storage systems
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Titanium carbide MXenes combined with red-emitting carbon dots as a unique turn-on fluorescent nanosensor for label-free determination of glucose
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Functionalization of MXene Nanosheets for Polystyrene towards High Thermal Stability and Flame Retardant Properties
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2D Black Phosphorus: from Preparation to Applications for Electrochemical Energy Storage
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Modified MXene/Holey Graphene Films for Advanced Supercapacitor Electrodes with Superior Energy Storage
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The Rise of 2D Photothermal Materials beyond Graphene for Clean Water Production
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Facile Solution Processing of Stable MXene Dispersions towards Conductive Composite Fibers
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Mechanically strong MXene/Kevlar nanofiber composite membranes as high-performance nanofluidic osmotic power generators
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Adhesion of two-dimensional titanium carbides (MXenes) and graphene to silicon
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Enhanced Thermal Conductivity of Epoxy Composites Filled with 2D Transition Metal Carbides (MXenes) with Ultralow Loading
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Heating of Ti3C2Tx MXene/polymer composites in response to Radio Frequency fields
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One-step Solution Processing of Ag, Au and Pd@MXene Hybrids for SERS
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Leaf-inspired multiresponsive MXene-based actuator for programmable smart devices
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Chemical Stability of Ti3C2 MXene with Al in the Temperature Range 500–700 °C
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Nitrogen Doped Intercalation TiO2/TiN/Ti3C2Tx Nanocomposite Electrodes with Enhanced Pseudocapacitance
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Synthesis and Electrochemical Properties of Two-Dimensional RGO/Ti3C2Tx Nanocomposites
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