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Title: Transmission and fluorescence X-ray absorption spectroscopy cell/flow reactor for powder samples under vacuum or in reactive atmospheres

Authors:
 [1]; ORCiD logo [1];  [2]; ORCiD logo [2];  [3];  [2];  [1]
  1. Department of Chemical Engineering, University of California at Davis, Davis, California 95616, USA
  2. KAUST Catalysis Center (KCC), King Abdullah University of Science and Technology (KAUST), 23955-6900 Thuwal, Saudi Arabia
  3. SLAC National Accelerator Laboratory, SSRL, Menlo Park, California 94025, USA
Publication Date:
Sponsoring Org.:
USDOE
OSTI Identifier:
1272643
Grant/Contract Number:  
AC02-76500515; FG02-04ER15513
Resource Type:
Publisher's Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Name: Review of Scientific Instruments Journal Volume: 87 Journal Issue: 7; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics
Country of Publication:
United States
Language:
English

Citation Formats

Hoffman, A. S., Debefve, L. M., Bendjeriou-Sedjerari, A., Ould-Chikh, S., Bare, Simon R., Basset, J. -M., and Gates, B. C. Transmission and fluorescence X-ray absorption spectroscopy cell/flow reactor for powder samples under vacuum or in reactive atmospheres. United States: N. p., 2016. Web. doi:10.1063/1.4958824.
Hoffman, A. S., Debefve, L. M., Bendjeriou-Sedjerari, A., Ould-Chikh, S., Bare, Simon R., Basset, J. -M., & Gates, B. C. Transmission and fluorescence X-ray absorption spectroscopy cell/flow reactor for powder samples under vacuum or in reactive atmospheres. United States. https://doi.org/10.1063/1.4958824
Hoffman, A. S., Debefve, L. M., Bendjeriou-Sedjerari, A., Ould-Chikh, S., Bare, Simon R., Basset, J. -M., and Gates, B. C. Tue . "Transmission and fluorescence X-ray absorption spectroscopy cell/flow reactor for powder samples under vacuum or in reactive atmospheres". United States. https://doi.org/10.1063/1.4958824.
@article{osti_1272643,
title = {Transmission and fluorescence X-ray absorption spectroscopy cell/flow reactor for powder samples under vacuum or in reactive atmospheres},
author = {Hoffman, A. S. and Debefve, L. M. and Bendjeriou-Sedjerari, A. and Ould-Chikh, S. and Bare, Simon R. and Basset, J. -M. and Gates, B. C.},
abstractNote = {},
doi = {10.1063/1.4958824},
journal = {Review of Scientific Instruments},
number = 7,
volume = 87,
place = {United States},
year = {Tue Jul 26 00:00:00 EDT 2016},
month = {Tue Jul 26 00:00:00 EDT 2016}
}

Journal Article:
Free Publicly Available Full Text
Publisher's Version of Record
https://doi.org/10.1063/1.4958824

Citation Metrics:
Cited by: 26 works
Citation information provided by
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Works referenced in this record:

An infrared spectroscopic study of water-related species in silica glasses
journal, June 1996


An in situ and operando X-ray absorption spectroscopy setup for measuring sub-monolayer model and powder catalysts
journal, August 2005

  • Weiher, Norbert; Bus, Eveline; Gorzolnik, Blazej
  • Journal of Synchrotron Radiation, Vol. 12, Issue 5
  • DOI: 10.1107/S0909049505020261

Low‐cost, heated, and/or cooled flow‐through cell for transmission x‐ray absorption spectroscopy
journal, June 1996

  • Jentoft, R. E.; Deutsch, S. E.; Gates, B. C.
  • Review of Scientific Instruments, Vol. 67, Issue 6
  • DOI: 10.1063/1.1147023

A versatile in situ spectroscopic cell for fluorescence/transmission EXAFS and X-ray diffraction of heterogeneous catalysts in gas and liquid phase
journal, June 2007

  • Hannemann, Stefan; Casapu, Maria; Grunwaldt, Jan-Dierk
  • Journal of Synchrotron Radiation, Vol. 14, Issue 4
  • DOI: 10.1107/S0909049507024466

Controlling the hydrogenolysis of silica-supported tungsten pentamethyl leads to a class of highly electron deficient partially alkylated metal hydrides
journal, January 2016

  • Maity, Niladri; Barman, Samir; Callens, Emmanuel
  • Chemical Science, Vol. 7, Issue 2
  • DOI: 10.1039/C5SC03490F

A new X-ray absorption experimental set-up dedicated to DeNOx catalysis
journal, July 1999

  • Revel, R.; Bazin, D.; Seigneurin, A.
  • Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 155, Issue 1-2
  • DOI: 10.1016/S0168-583X(99)00253-0

Transmission and fluorescence X-ray absorption spectroscopy cell/flow reactor for powder samples under vacuum or in reactive atmospheres
journal, July 2016

  • Hoffman, A. S.; Debefve, L. M.; Bendjeriou-Sedjerari, A.
  • Review of Scientific Instruments, Vol. 87, Issue 7
  • DOI: 10.1063/1.4958824

An i n s i t u cell for transmission EXAFS measurements on catalytic samples
journal, August 1989

  • Kampers, F. W. H.; Maas, T. M. J.; van Grondelle, J.
  • Review of Scientific Instruments, Vol. 60, Issue 8
  • DOI: 10.1063/1.1140684

Single-atom catalysis of CO oxidation using Pt1/FeOx
journal, July 2011

  • Qiao, Botao; Wang, Aiqin; Yang, Xiaofeng
  • Nature Chemistry, Vol. 3, Issue 8
  • DOI: 10.1038/nchem.1095

Single-Site Zeolite-Anchored Organoiridium Carbonyl Complexes: Characterization of Structure and Reactivity by Spectroscopy and Computational Chemistry
journal, July 2015

  • Martinez-Macias, Claudia; Chen, Mingyang; Dixon, David A.
  • Chemistry - A European Journal, Vol. 21, Issue 33
  • DOI: 10.1002/chem.201501277

Chapter 6 Characterization of Catalysts in Reactive Atmospheres by X‐ray Absorption Spectroscopy
book, February 2009


XAFS spectroscopy; fundamental principles and data analysis
journal, May 2000

  • Koningsberger, D. C.; Mojet, B. L.; van Dorssen, G. E.
  • Topics in Catalysis, Vol. 10, Issue 3/4, p. 143-155
  • DOI: 10.1023/A:1019105310221

A flow-through x-ray absorption spectroscopy cell for characterization of powder catalysts in the working state
journal, October 2001

  • Odzak, J. F.; Argo, A. M.; Lai, F. S.
  • Review of Scientific Instruments, Vol. 72, Issue 10
  • DOI: 10.1063/1.1403011

The surface chemistry of amorphous silica. Zhuravlev model
journal, November 2000


Bipodal Surface Organometallic Complexes with Surface N-Donor Ligands and Application to the Catalytic Cleavage of C–H and C–C Bonds in n -Butane
journal, November 2013

  • Bendjeriou-Sedjerari, Anissa; Azzi, Joachim M.; Abou-Hamad, Edy
  • Journal of the American Chemical Society, Vol. 135, Issue 47
  • DOI: 10.1021/ja407902g

Silica-supported catalysts get a new breath of life
journal, December 2015


Effect of chemical environment on magnitude of x‐ray absorption resonance at L I I I edges. Studies on metallic elements, compounds, and catalysts
journal, June 1979

  • Lytle, F. W.; Wei, P. S. P.; Greegor, R. B.
  • The Journal of Chemical Physics, Vol. 70, Issue 11
  • DOI: 10.1063/1.437376

X-ray absorption spectroscopy, x-ray photoelectron spectroscopy, and analytical electron microscopy studies of cobalt catalysts. 2. Hydrogen reduction properties
journal, January 1990

  • Castner, David G.; Watson, Philip R.; Chan, Ignatius Y.
  • The Journal of Physical Chemistry, Vol. 94, Issue 2
  • DOI: 10.1021/j100365a057