A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources

Steinke, I.; Walther, M.; Lehmkühler, F.; Wochner, P.; Valerio, J.; Mager, R.; Schroer, M. A.; Lee, S.; Roseker, W.; Jain, A.; Sikorski, M.; Song, S.; Hartmann, R.; Huth, M.; Strüder, L.; Sprung, M.; Robert, A.; Fuoss, P. H.; Stephenson, G. B.; Grübel, G.

doi:10.1063/1.4953921

Title: A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources

Full Record
Other Related Research

Abstract

In this study we describe a setup for x-ray scattering experiments on complex fluids using a liquid jet. The setup supports Small and Wide Angle X-ray Scattering (SAXS/WAXS) geometries. The jet is formed by a gas-dynamic virtual nozzle (GDVN) allowing for diameters ranging between 1 μm and 20 μm at a jet length of several hundred μm. To control jet properties such as jet length, diameter, or flow rate, the instrument is equipped with several diagnostic tools. Three microscopes are installed to quantify jet dimensions and stability in situ. The setup has been used at several beamlines performing both SAXS and WAXS experiments. Finally, as a typical example we show an experiment on a colloidal dispersion in a liquid jet at the X-ray Correlation Spectroscopy instrument at the Linac Coherent Light Source free-electron laser.

Authors:

Steinke, I. ^[1]; Walther, M. ^[2]; Lehmkühler, F. ^[1]; Wochner, P. ^[3]; Valerio, J. ^[2]; Mager, R. ^[4];

^[1]; Lee, S. ^[5]; Roseker, W. ^[2]; Jain, A. ^[2]; Sikorski, M. ^[6]; Song, S. ^[6];

^[7]; Huth, M. ^[7]; Strüder, L. ^[7]; Sprung, M. ^[2]; Robert, A. ^[6]; Fuoss, P. H. ^[8]; Stephenson, G. B. ^[8]; Grübel, G. ^[1]

German Electron Synchrotron (DESY), Hamburg (Germany); The Hamburg Centre for Ultrafast Imaging (CUI) (Germany)
German Electron Synchrotron (DESY), Hamburg (Germany)
Max Planck Inst. for Solid State Research, Stuttgart (Germany)
Max Planck Inst. for Intelligent Systems, Stuttgart (Germany)
Korea Research Inst. of Standards and Science (KRISS), Daejeon (Korea, Republic of). Frontier in Extreme Physics
SLAC National Accelerator Lab., Menlo Park, CA (United States). Linac Coherent Light Source (LCLS)
PNSensor GmbH, Munich (Germany)
Argonne National Lab. (ANL), Argonne, IL (United States)

Publication Date:: Fri Jun 17 00:00:00 EDT 2016

Research Org.:: SLAC National Accelerator Lab., Menlo Park, CA (United States); Argonne National Lab. (ANL), Argonne, IL (United States); German Electron Synchrotron (DESY), Hamburg (Germany); Korea Research Inst. of Standards and Science (KRISS), Daejeon (Korea, Republic of)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES); German Research Foundation (DFG); Hamburg Centre for Ultrafast Imaging (CUI) (Germany); Ministry of Science, ICT and Future Planning (Korea, Republic of)

Contributing Org.:: The Hamburg Centre for Ultrafast Imaging (CUI) (Germany); Max Planck Inst. for Solid State Research, Stuttgart (Germany); Max Planck Inst. for Intelligent Systems, Stuttgart (Germany); PNSensor GmbH, Munich (Germany)

OSTI Identifier:: 1352668

Alternate Identifier(s):: OSTI ID: 1257659; OSTI ID: 1352666

Grant/Contract Number:: AC02-76SF00515; NRF-2014M3C1A8048818; NRF-2014M1A7A1A01030128; AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Review of Scientific Instruments

Additional Journal Information:: Journal Volume: 87; Journal Issue: 6; Journal ID: ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: English

Subject:: 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; Fluid jets; Nozzle jets; Fluid drops; Light emitting diodes; X-ray scattering

Citation Formats


                    Steinke, I., Walther, M., Lehmkühler, F., Wochner, P., Valerio, J., Mager, R., Schroer, M. A., Lee, S., Roseker, W., Jain, A., Sikorski, M., Song, S., Hartmann, R., Huth, M., Strüder, L., Sprung, M., Robert, A., Fuoss, P. H., Stephenson, G. B., and Grübel, G. A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources.  United States: N. p., 2016. 
Web.  doi:10.1063/1.4953921.

Copy to clipboard


                    Steinke, I., Walther, M., Lehmkühler, F., Wochner, P., Valerio, J., Mager, R., Schroer, M. A., Lee, S., Roseker, W., Jain, A., Sikorski, M., Song, S., Hartmann, R., Huth, M., Strüder, L., Sprung, M., Robert, A., Fuoss, P. H., Stephenson, G. B., & Grübel, G. A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources.  United States.  https://doi.org/10.1063/1.4953921

Copy to clipboard


                    Steinke, I., Walther, M., Lehmkühler, F., Wochner, P., Valerio, J., Mager, R., Schroer, M. A., Lee, S., Roseker, W., Jain, A., Sikorski, M., Song, S., Hartmann, R., Huth, M., Strüder, L., Sprung, M., Robert, A., Fuoss, P. H., Stephenson, G. B., and Grübel, G. Fri .  
"A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources".  United States.  https://doi.org/10.1063/1.4953921.  https://www.osti.gov/servlets/purl/1352668.

Copy to clipboard


                    
@article{osti_1352668,

  title        = {A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources},

  author       = {Steinke, I. and Walther, M. and Lehmkühler, F. and Wochner, P. and Valerio, J. and Mager, R. and Schroer, M. A. and Lee, S. and Roseker, W. and Jain, A. and Sikorski, M. and Song, S. and Hartmann, R. and Huth, M. and Strüder, L. and Sprung, M. and Robert, A. and Fuoss, P. H. and Stephenson, G. B. and Grübel, G.},

  abstractNote = {In this study we describe a setup for x-ray scattering experiments on complex fluids using a liquid jet. The setup supports Small and Wide Angle X-ray Scattering (SAXS/WAXS) geometries. The jet is formed by a gas-dynamic virtual nozzle (GDVN) allowing for diameters ranging between 1 μm and 20 μm at a jet length of several hundred μm. To control jet properties such as jet length, diameter, or flow rate, the instrument is equipped with several diagnostic tools. Three microscopes are installed to quantify jet dimensions and stability in situ. The setup has been used at several beamlines performing both SAXS and WAXS experiments. Finally, as a typical example we show an experiment on a colloidal dispersion in a liquid jet at the X-ray Correlation Spectroscopy instrument at the Linac Coherent Light Source free-electron laser.},

  doi          = {10.1063/1.4953921},

  journal      = {Review of Scientific Instruments},

  number       = 6,

  volume       = 87,

  place        = {United States},

  year         = {Fri Jun 17 00:00:00 EDT 2016},

  month        = {Fri Jun 17 00:00:00 EDT 2016}

}

Copy to clipboard

Journal Article:

Free Publicly Available Full Text

Accepted Manuscript (Publisher)

Accepted Manuscript (DOE)

Publisher's Version of Record

https://doi.org/10.1063/1.4953921

Other availability

Search WorldCat to find libraries that may hold this journal

Citation Metrics:

Cited by: 9 works

Citation information provided by
Web of Science

Save / Share:

Export Metadata

Save to My Library

Similar Records in DOE PAGES and OSTI.GOV collections:

A liquid jet setup for x-ray scattering experiments on complex liquids at free-electron laser sources

Journal Article Steinke, I. ; Lehmkühler, F., E-mail: felix.lehmkuehler@desy.de ; Schroer, M. A. ; ... - Review of Scientific Instruments

In this paper we describe a setup for x-ray scattering experiments on complex fluids using a liquid jet. The setup supports Small and Wide Angle X-ray Scattering (SAXS/WAXS) geometries. The jet is formed by a gas-dynamic virtual nozzle (GDVN) allowing for diameters ranging between 1 μm and 20 μm at a jet length of several hundred μm. To control jet properties such as jet length, diameter, or flow rate, the instrument is equipped with several diagnostic tools. Three microscopes are installed to quantify jet dimensions and stability in situ. The setup has been used at several beamlines performing both SAXSmore »« less
https://doi.org/10.1063/1.4953921
Injector for scattering measurements on fully solvated biospecies

Journal Article Weierstall, U ; Spence, J C. H. ; Doak, R B - Review of Scientific Instruments

We describe a liquid jet injector system developed to deliver fully solvated microscopic target species into a probe beam under either vacuum or ambient conditions. The injector was designed specifically for x-ray scattering studies of biological nanospecies using x-ray free electron lasers and third generation synchrotrons, but is of interest to any application in which microscopic samples must be delivered in a fully solvated state and with microscopic precision. By utilizing a gas dynamic virtual nozzle (GDVN) to generate a sample-containing liquid jet of diameter ranging from 300 nm to 20 {mu}m, the injector avoids the clogging problems associated inmore »« less
https://doi.org/10.1063/1.3693040
3D Volumetric Structural Hierarchy Induced by Colloidal Polymerization of a Quantum-Dot Ionic Liquid Monomer Conjugate

Journal Article Welch, Paul M. ; Dreier, Timothy A. ; Magurudeniya, Harsha D. ; ... - Macromolecules

Hierarchically structured emissive quantum dot (CdS/CdSe) poly(ionic liquid) composites are synthesized through colloidal polymerization within a lyotropic liquid crystal, yielding a solvent-responsive nanoparticle (NP) composite possessing four ordered structural motifs. The composite is prepared by coassembling an amphiphilic ionic liquid (IL) monomer, 3-decyl-1-vinylimidazolium chloride, [C₁₀VIm⁺][Cl^-], and IL monomer, 3-(10-mercaptodecyl)-1-vinylimidazolium bromide surface-functionalized quantum dots, QD-[SC₁₀VIm⁺][Br^-], in 30 wt % water. Photo (UV)-initiated free radical polymerization serves to form a colloidal copolymer that collimates pairs of QDs within the core of large cylinders (average diameter = 21 nm and length = 422 nm), as evidenced by ultrasmall-angle X-ray scattering (USAXS). As revealedmore »« less
Cited by 2
https://doi.org/10.1021/acs.macromol.0c00011

Full Text Available
Inelastic x-ray scattering study of supercooled liquid and solid silicon.

Conference Alatas, A ; Said, A ; Sinn, H ; ...

Momentum-resolved inelastic x-ray scattering (IXS) technique is one of the powerful methods for the study of dynamical properties of a given system even in extreme conditions like high temperature and high pressure. At the same time, experimental studies of physical and structural properties of liquids have multiplied in recent years with the advent of containerless techniques. These methods reduce the possibility of contamination of specimens and remove external nucleation sites. Therefore, by combining the IXS method with the levitation method, the dynamical properties of stable liquids up to 3000 K and supercooled phase of liquids can be studied. Silicon ismore »« less
A setup for resonant inelastic soft x-ray scattering on liquids at free electron laser light sources

Journal Article Kunnus, Kristjan ; Schreck, Simon ; Foehlisch, Alexander ; ... - Review of Scientific Instruments

We present a flexible and compact experimental setup that combines an in vacuum liquid jet with an x-ray emission spectrometer to enable static and femtosecond time-resolved resonant inelastic soft x-ray scattering (RIXS) measurements from liquids at free electron laser (FEL) light sources. We demonstrate the feasibility of this type of experiments with the measurements performed at the Linac Coherent Light Source FEL facility. At the FEL we observed changes in the RIXS spectra at high peak fluences which currently sets a limit to maximum attainable count rate at FELs. The setup presented here opens up new possibilities to study themore » structure and dynamics in liquids.« less
https://doi.org/10.1063/1.4772685

Similar Records