DOE PAGES title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Characterizing the recovery of a solid surface after tungsten nano-tendril formation

Abstract

Here, recovery of a flat tungsten surface from a nano-tendril surface is attempted through three techniques; a mechanical wipe, a 1673 K annealing, and laser-induced thermal transients. Results were determined through SEM imaging and elastic recoil detection to assess the helium content in the surface. The mechanical wipe leaves a ~0.5 μm deep layer of nano-tendrils on the surface post-wipe regardless of the initial nano-tendril layer depth. Laser-induced thermal transients only significantly impact the surface morphology at heat loads of 35.2 MJ/m2 s1/2 or above, however a fully flat or recovered surface was not achieved for 100 transients at this heat load despite reducing the helium content by a factor of ~7. A 1673 K annealing removes all detectable levels of helium but sub-surface voids/bubbles remain intact. The surface is recovered to a nearly flat state with only some remnants of nano-tendrils re-integrating into the surface remaining.

Authors:
 [1];  [2];  [1];  [2];  [1];  [1]
  1. Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States). Plasma Science and Fusion Center
  2. Dutch Institute For Fundamental Energy Research (DIFFER), Nieuwegein (Netherlands). EURATOM-FOM
Publication Date:
Research Org.:
Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States). Plasma Science and Fusion Center
Sponsoring Org.:
USDOE Office of Science (SC), Fusion Energy Sciences (FES); National Science Foundation (NSF)
OSTI Identifier:
1897977
Alternate Identifier(s):
OSTI ID: 1252236
Grant/Contract Number:  
SC0002060; DMR-0819762; SC00-02060
Resource Type:
Accepted Manuscript
Journal Name:
Journal of Nuclear Materials
Additional Journal Information:
Journal Volume: 463; Journal ID: ISSN 0022-3115
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
11 NUCLEAR FUEL CYCLE AND FUEL MATERIALS; Helium; Ion-surface interactions; Thermal shock; Tungsten fuzz

Citation Formats

Wright, G. M., van Eden, G. G., Kesler, L. A., De Temmerman, G., Whyte, D. G., and Woller, K. B. Characterizing the recovery of a solid surface after tungsten nano-tendril formation. United States: N. p., 2014. Web. doi:10.1016/j.jnucmat.2014.11.083.
Wright, G. M., van Eden, G. G., Kesler, L. A., De Temmerman, G., Whyte, D. G., & Woller, K. B. Characterizing the recovery of a solid surface after tungsten nano-tendril formation. United States. https://doi.org/10.1016/j.jnucmat.2014.11.083
Wright, G. M., van Eden, G. G., Kesler, L. A., De Temmerman, G., Whyte, D. G., and Woller, K. B. Thu . "Characterizing the recovery of a solid surface after tungsten nano-tendril formation". United States. https://doi.org/10.1016/j.jnucmat.2014.11.083. https://www.osti.gov/servlets/purl/1897977.
@article{osti_1897977,
title = {Characterizing the recovery of a solid surface after tungsten nano-tendril formation},
author = {Wright, G. M. and van Eden, G. G. and Kesler, L. A. and De Temmerman, G. and Whyte, D. G. and Woller, K. B.},
abstractNote = {Here, recovery of a flat tungsten surface from a nano-tendril surface is attempted through three techniques; a mechanical wipe, a 1673 K annealing, and laser-induced thermal transients. Results were determined through SEM imaging and elastic recoil detection to assess the helium content in the surface. The mechanical wipe leaves a ~0.5 μm deep layer of nano-tendrils on the surface post-wipe regardless of the initial nano-tendril layer depth. Laser-induced thermal transients only significantly impact the surface morphology at heat loads of 35.2 MJ/m2 s1/2 or above, however a fully flat or recovered surface was not achieved for 100 transients at this heat load despite reducing the helium content by a factor of ~7. A 1673 K annealing removes all detectable levels of helium but sub-surface voids/bubbles remain intact. The surface is recovered to a nearly flat state with only some remnants of nano-tendrils re-integrating into the surface remaining.},
doi = {10.1016/j.jnucmat.2014.11.083},
journal = {Journal of Nuclear Materials},
number = ,
volume = 463,
place = {United States},
year = {Thu Nov 27 00:00:00 EST 2014},
month = {Thu Nov 27 00:00:00 EST 2014}
}

Journal Article:

Citation Metrics:
Cited by: 10 works
Citation information provided by
Web of Science

Save / Share:

Works referenced in this record:

Formation of helium induced nanostructure ‘fuzz’ on various tungsten grades
journal, September 2010


Sputtering properties of tungsten ‘fuzzy’ surfaces
journal, August 2011


Helium concentration in tungsten nano-tendril surface morphology using Elastic Recoil Detection
journal, July 2013


Helium effects on tungsten under fusion-relevant plasma loading conditions
journal, July 2013


Visualized Blow-off from Helium Irradiated Tungsten in Response to ELM-like Heat Load
journal, January 2009

  • Kajita, Shin; Ohno, Noriyasu; Sakaguchi, Wataru
  • Plasma and Fusion Research, Vol. 4
  • DOI: 10.1585/pfr.4.004

An experiment on the dynamics of ion implantation and sputtering of surfaces
journal, February 2014

  • Wright, G. M.; Barnard, H. A.; Kesler, L. A.
  • Review of Scientific Instruments, Vol. 85, Issue 2
  • DOI: 10.1063/1.4861917

Sub-ms laser pulse irradiation on tungsten target damaged by exposure to helium plasma
journal, September 2007


Thermal response of nanostructured tungsten
journal, February 2014


Recovery of Tungsten Surface with Fiber-Form Nanostructure by Plasmas Exposures
journal, February 2013

  • Miyamoto, Takanori; Takamura, Shuichi; Kurishita, Hiroaki
  • Plasma Science and Technology, Vol. 15, Issue 2
  • DOI: 10.1088/1009-0630/15/2/17

Tungsten nano-tendril growth in the Alcator C-Mod divertor
journal, March 2012


The effect of high-flux H plasma exposure with simultaneous transient heat loads on tungsten surface damage and power handling
journal, November 2014


In situ observation of structural change of nanostructured tungsten during annealing
journal, June 2014


Helium induced nanoscopic morphology on tungsten under fusion relevant plasma conditions
journal, January 2008


TEM analysis of high temperature annealed W nanostructure surfaces
journal, February 2012