New developments in high pressure x-ray spectroscopy beamline at High Pressure Collaborative Access Team
Abstract
The 16 ID-D (Insertion Device - D station) beamline of the High Pressure Collaborative Access Team at the Advanced Photon Source is dedicated to high pressure research using X-ray spectroscopy techniques typically integrated with diamond anvil cells. The beamline provides X-rays of 4.5-37 keV, and current available techniques include X-ray emission spectroscopy, inelastic X-ray scattering, and nuclear resonant scattering. Here, the recent developments include a canted undulator upgrade, 17-element analyzer array for inelastic X-ray scattering, and an emission spectrometer using a polycapillary half-lens. Recent development projects and future prospects are also discussed.
- Authors:
-
- Carnegie Inst. of Washington, Argonne, IL (United States)
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division; USDOE National Nuclear Security Administration (NNSA)
- OSTI Identifier:
- 1212197
- Alternate Identifier(s):
- OSTI ID: 1228696
- Grant/Contract Number:
- AC02-06CH11357; NA0001974; FG02-99ER45775
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Review of Scientific Instruments
- Additional Journal Information:
- Journal Volume: 86; Journal Issue: 7; Journal ID: ISSN 0034-6748
- Publisher:
- American Institute of Physics (AIP)
- Country of Publication:
- United States
- Language:
- ENGLISH
- Subject:
- 47 OTHER INSTRUMENTATION
Citation Formats
Xiao, Y. M., Chow, P., Boman, G., Bai, L. G., Rod, E., Bommannavar, A., Kenney-Benson, C., Sinogeikin, S., and Shen, G. Y. New developments in high pressure x-ray spectroscopy beamline at High Pressure Collaborative Access Team. United States: N. p., 2015.
Web. doi:10.1063/1.4926888.
Xiao, Y. M., Chow, P., Boman, G., Bai, L. G., Rod, E., Bommannavar, A., Kenney-Benson, C., Sinogeikin, S., & Shen, G. Y. New developments in high pressure x-ray spectroscopy beamline at High Pressure Collaborative Access Team. United States. https://doi.org/10.1063/1.4926888
Xiao, Y. M., Chow, P., Boman, G., Bai, L. G., Rod, E., Bommannavar, A., Kenney-Benson, C., Sinogeikin, S., and Shen, G. Y. Wed .
"New developments in high pressure x-ray spectroscopy beamline at High Pressure Collaborative Access Team". United States. https://doi.org/10.1063/1.4926888. https://www.osti.gov/servlets/purl/1212197.
@article{osti_1212197,
title = {New developments in high pressure x-ray spectroscopy beamline at High Pressure Collaborative Access Team},
author = {Xiao, Y. M. and Chow, P. and Boman, G. and Bai, L. G. and Rod, E. and Bommannavar, A. and Kenney-Benson, C. and Sinogeikin, S. and Shen, G. Y.},
abstractNote = {The 16 ID-D (Insertion Device - D station) beamline of the High Pressure Collaborative Access Team at the Advanced Photon Source is dedicated to high pressure research using X-ray spectroscopy techniques typically integrated with diamond anvil cells. The beamline provides X-rays of 4.5-37 keV, and current available techniques include X-ray emission spectroscopy, inelastic X-ray scattering, and nuclear resonant scattering. Here, the recent developments include a canted undulator upgrade, 17-element analyzer array for inelastic X-ray scattering, and an emission spectrometer using a polycapillary half-lens. Recent development projects and future prospects are also discussed.},
doi = {10.1063/1.4926888},
journal = {Review of Scientific Instruments},
number = 7,
volume = 86,
place = {United States},
year = {Wed Jul 22 00:00:00 EDT 2015},
month = {Wed Jul 22 00:00:00 EDT 2015}
}
Web of Science
Works referenced in this record:
The 57 Fe Synchrotron Mössbauer Source at the ESRF
journal, May 2012
- Potapkin, Vasily; Chumakov, Aleksandr I.; Smirnov, Gennadii V.
- Journal of Synchrotron Radiation, Vol. 19, Issue 4
Vibrational spectroscopy at high pressures—LVI. A Raman study of some alkali metal halates, and the X-ray compressibility of KClO3
journal, January 1991
- Adams, David M.; Heath, Andrew E.; Pogson, Mark
- Spectrochimica Acta Part A: Molecular Spectroscopy, Vol. 47, Issue 8
Pressure-Induced High-Spin to Low-Spin Transition in FeS Evidenced by X-Ray Emission Spectroscopy
journal, April 1999
- Rueff, J. -P.; Kao, C. -C.; Struzhkin, V. V.
- Physical Review Letters, Vol. 82, Issue 16
Pressure induced valence change of Eu in EuFe 2 As 2 at low temperature and high pressures probed by resonant inelastic x-ray scattering
journal, January 2014
- Kumar, Ravhi S.; Zhang, Yi; Thamizhavel, Arumugam
- Applied Physics Letters, Vol. 104, Issue 4
Experimental aspects of inelastic X-ray scattering studies on liquids under extreme conditions (P-T)
journal, September 2008
- Alatas, Ahmet; Sinn, Harald; Zhao, Jiyong
- High Pressure Research, Vol. 28, Issue 3
Synchrotron radiation and high pressure: new light on materials under extreme conditions
journal, February 2005
- Hemley, Russell J.; Mao, Ho-kwang; Struzhkin, Viktor V.
- Journal of Synchrotron Radiation, Vol. 12, Issue 2
Inelastic x-ray scattering at ultrahigh pressures
journal, August 2001
- Mao, Ho-kwang; Kao, Chichang; Hemley, Russell J.
- Journal of Physics: Condensed Matter, Vol. 13, Issue 34
High-pressure Apparatus Integrated with Synchrotron Radiation
journal, January 2014
- Shen, G.; Wang, Y.
- Reviews in Mineralogy and Geochemistry, Vol. 78, Issue 1
Probing of bonding changes in B2O3 glasses at high pressure with inelastic X-ray scattering
journal, October 2005
- Lee, Sung Keun; Eng, Peter J.; Mao, Ho-kwang
- Nature Materials, Vol. 4, Issue 11
Nuclear resonant scattering at high pressure and high temperature
journal, December 2004
- Zhao, Jiyong; Sturhahn, Wolfgang; Lin, Jung-fu
- High Pressure Research, Vol. 24, Issue 4
Pressure-induced valence change in : A combined high-pressure inelastic x-ray scattering and theoretical investigation
journal, August 2008
- Kumar, Ravhi S.; Svane, Axel; Vaitheeswaran, G.
- Physical Review B, Vol. 78, Issue 7
Electronic dynamics and plasmons of sodium under compression
journal, December 2011
- Mao, H. -K.; Ding, Y.; Xiao, Y.
- Proceedings of the National Academy of Sciences, Vol. 108, Issue 51
Crystal and Electronic Structure of FeSe at High Pressure and Low Temperature
journal, October 2010
- Kumar, Ravhi S.; Zhang, Yi; Sinogeikin, Stanislav
- The Journal of Physical Chemistry B, Vol. 114, Issue 39
Resonant X-ray emission study of the lower-mantle ferropericlase at high pressures
journal, August 2010
- Lin, J. -F.; Mao, Z.; Jarrige, I.
- American Mineralogist, Vol. 95, Issue 8-9
Synchrotron Mössbauer spectroscopy using high-speed shutters
journal, November 2010
- Toellner, T. S.; Alp, E. E.; Graber, T.
- Journal of Synchrotron Radiation, Vol. 18, Issue 2
Lattice design challenges for fourth-generation storage-ring light sources
journal, August 2014
- Borland, Michael; Decker, Glenn; Emery, Louis
- Journal of Synchrotron Radiation, Vol. 21, Issue 5
Synchrotron facilities and the study of the Earth's deep interior
journal, July 2005
- Duffy, Thomas S.
- Reports on Progress in Physics, Vol. 68, Issue 8
X-ray Raman scattering studies on C60 fullerenes and multi-walled carbon nanotubes under pressure
journal, April 2007
- Kumar, Ravhi S.; Pravica, Michael G.; Cornelius, Andrew L.
- Diamond and Related Materials, Vol. 16, Issue 4-7
Electronic and magnetic studies of materials to megabar pressures
journal, January 2000
- Struzhkin, Viktor V.; Hemley, Russell J.; Mao, Ho‐kwang
- Hyperfine Interactions, Vol. 128, Issue 1/3, p. 323-343
Sound velocities for hexagonally close-packed iron compressed hydrostatically to 136 GPa from phonon density of states: SOUND VELOCITIES FOR HCP-IRON
journal, June 2013
- Gleason, A. E.; Mao, W. L.; Zhao, J. Y.
- Geophysical Research Letters, Vol. 40, Issue 12
HPCAT: an integrated high-pressure synchrotron facility at the Advanced Photon Source
journal, September 2008
- Shen, Guoyin; Chow, Paul; Xiao, Yuming
- High Pressure Research, Vol. 28, Issue 3
Electronic Structure of Crystalline at High Pressures
journal, October 2010
- Mao, Ho Kwang; Shirley, Eric L.; Ding, Yang
- Physical Review Letters, Vol. 105, Issue 18
Pressure induced high spin-low spin transition in FeSe superconductor studied by x-ray emission spectroscopy and ab initio calculations
journal, August 2011
- Kumar, Ravhi S.; Zhang, Yi; Xiao, Yuming
- Applied Physics Letters, Vol. 99, Issue 6
Bonding Changes in Compressed Superhard Graphite
journal, October 2003
- Mao, W. L.
- Science, Vol. 302, Issue 5644
The formation of sp3 bonding in compressed BN
journal, January 2004
- Meng, Yue; Mao, Ho-kwang; Eng, Peter J.
- Nature Materials, Vol. 3, Issue 2
Focusing polycapillary to reduce parasitic scattering for inelastic x-ray measurements at high pressure
journal, July 2015
- Chow, P.; Xiao, Y. M.; Rod, E.
- Review of Scientific Instruments, Vol. 86, Issue 7
A versatile medium-resolution x-ray emission spectrometer for diamond anvil cell applications
journal, August 2013
- Mortensen, D. R.; Seidler, G. T.; Bradley, J. A.
- Review of Scientific Instruments, Vol. 84, Issue 8
Solubility of xenotime in a 2 M HCl aqueous fluid from 1.2 to 2.6 GPa and 300 to 500 C
journal, September 2012
- Tanis, E. A.; Simon, A.; Tschauner, O.
- American Mineralogist, Vol. 97, Issue 10
Electronic Phase Transitions in F-electron Metals at High Pressures: Synchrotron X-ray Spectroscopic Studies on GD to 100 GPa
journal, January 2008
- Yoo, Choong-Shik; Maddox, Brian; Iota, Valentin
- MRS Proceedings, Vol. 1104
X-ray Emission Spectroscopy of Cerium Across the Volume Collapse Transition
journal, November 2012
- Lipp, M. J.; Sorini, A. P.; Bradley, J.
- Physical Review Letters, Vol. 109, Issue 19
Synchrotron radiation, an intense x-ray source for high pressure diffraction studies
journal, December 1980
- Bassett, William A.
- Physics of the Earth and Planetary Interiors, Vol. 23, Issue 4
Iron-rich perovskite in the Earth's lower mantle
journal, September 2011
- Mao, Z.; Lin, J. F.; Scott, H. P.
- Earth and Planetary Science Letters, Vol. 309, Issue 3-4
Magnetic spectroscopy at high pressures using X-ray magnetic circular dichroism
journal, September 2008
- Haskel, Daniel; Tseng, Y. C.; Souza-Neto, N. M.
- High Pressure Research, Vol. 28, Issue 3
Nuclear resonant spectroscopy
journal, January 2004
- Sturhahn, Wolfgang
- Journal of Physics: Condensed Matter, Vol. 16, Issue 5
Chemistry at high pressure
journal, January 2006
- McMillan, Paul F.
- Chemical Society Reviews, Vol. 35, Issue 10
DLSR design and plans: an international overview
journal, August 2014
- Hettel, Robert
- Journal of Synchrotron Radiation, Vol. 21, Issue 5
Inelastic x-ray scattering of dense solid oxygen: Evidence for intermolecular bonding
journal, August 2008
- Meng, Y.; Eng, P. J.; Tse, J. S.
- Proceedings of the National Academy of Sciences, Vol. 105, Issue 33
Works referencing / citing this record:
Valence and spin states of iron are invisible in Earth’s lower mantle
journal, March 2018
- Liu, Jiachao; Dorfman, Susannah M.; Zhu, Feng
- Nature Communications, Vol. 9, Issue 1
Pressure-induced changes in the electron density distribution in α-Ge near the α-β transition
journal, August 2015
- Li, Rui; Liu, Jing; Bai, Ligang
- Applied Physics Letters, Vol. 107, Issue 7
Spectroscopy of low and intermediate Z elements at extreme conditions: in situ studies of Earth materials at pressure and temperature via X-ray Raman scattering
journal, July 2016
- Sternemann, C.; Wilke, M.
- High Pressure Research, Vol. 36, Issue 3
High pressure effects on U L 3 x-ray absorption in partial fluorescence yield mode and single crystal x-ray diffraction in the heavy fermion compound UCd 11
journal, February 2016
- Nasreen, Farzana; Antonio, Daniel; VanGennep, Derrick
- Journal of Physics: Condensed Matter, Vol. 28, Issue 10
High-pressure studies with x-rays using diamond anvil cells
journal, November 2016
- Shen, Guoyin; Mao, Ho Kwang
- Reports on Progress in Physics, Vol. 80, Issue 1