Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography

Meirer, F.; Kalirai, S.; Weker, J. Nelson; Liu, Y.; Andrews, J. C.; Weckhuysen, B. M.

doi:10.1039/C5CC00401B

Title: Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography

Abstract

Metal accumulation at the catalyst particle surface plays a role in particle agglutination during fluid catalytic cracking.

Authors:

Meirer, F. ^[1]; Kalirai, S. ^[1]; Weker, J. Nelson ^[2]; Liu, Y. ^[2]; Andrews, J. C. ^[2]; Weckhuysen, B. M. ^[1]

Utrecht Univ., Utrecht (The Netherlands)
SLAC National Accelerator Laboratory (SLAC), Menlo Park, CA (United States)

Publication Date:: Tue Apr 14 00:00:00 EDT 2015

Research Org.:: SLAC National Accelerator Lab., Menlo Park, CA (United States)

Sponsoring Org.:: USDOE Office of Science (SC)

OSTI Identifier:: 1215407

Grant/Contract Number:: 321140

Resource Type:: Accepted Manuscript

Journal Name:: ChemComm

Additional Journal Information:: Journal Volume: 51; Journal Issue: 38; Journal ID: ISSN 1359-7345

Publisher:: Royal Society of Chemistry

Country of Publication:: United States

Language:: English

Subject:: 02 PETROLEUM

Citation Formats


                    Meirer, F., Kalirai, S., Weker, J. Nelson, Liu, Y., Andrews, J. C., and Weckhuysen, B. M. Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography.  United States: N. p., 2015. 
Web.  doi:10.1039/C5CC00401B.

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                    Meirer, F., Kalirai, S., Weker, J. Nelson, Liu, Y., Andrews, J. C., & Weckhuysen, B. M. Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography.  United States.  https://doi.org/10.1039/C5CC00401B

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                    Meirer, F., Kalirai, S., Weker, J. Nelson, Liu, Y., Andrews, J. C., and Weckhuysen, B. M. Tue .  
"Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography".  United States.  https://doi.org/10.1039/C5CC00401B.  https://www.osti.gov/servlets/purl/1215407.

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@article{osti_1215407,

  title        = {Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography},

  author       = {Meirer, F. and Kalirai, S. and Weker, J. Nelson and Liu, Y. and Andrews, J. C. and Weckhuysen, B. M.},

  abstractNote = {Metal accumulation at the catalyst particle surface plays a role in particle agglutination during fluid catalytic cracking.},

  doi          = {10.1039/C5CC00401B},

  journal      = {ChemComm},

  number       = 38,

  volume       = 51,

  place        = {United States},

  year         = {Tue Apr 14 00:00:00 EDT 2015},

  month        = {Tue Apr 14 00:00:00 EDT 2015}

}

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Works referencing / citing this record:

Nickel Poisoning of a Cracking Catalyst Unravelled by Single‐Particle X‐ray Fluorescence‐Diffraction‐Absorption Tomography
journal, January 2020

Gambino, Marianna; Veselý, Martin; Filez, Matthias
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Similar Records

Title: Agglutination of single catalyst particles during fluid catalytic cracking as observed by X-ray nanotomography

Abstract

Citation Formats

Designing FCC catalysts with high-silica Y zeolites journal, August 1991

Heterogeneities of individual catalyst particles in space and time as monitored by spectroscopy journal, October 2012

Hard and soft X-ray microscopy and tomography in catalysis: bridging the different time and length scales journal, January 2010

Imaging Catalysts at Work: A Hierarchical Approach from the Macro- to the Meso- and Nano-scale journal, November 2012

On the interaction of vanadium and nickel compounds with cracking catalyst journal, December 1984

Vanadium passivation of cracking catalysts by imaging secondary ion mass spectrometry journal, January 1995

Nickel and vanadium on equilibrium cracking catalysts by imaging secondary ion mass spectrometry journal, February 1988

Mapping Metals Incorporation of a Whole Single Catalyst Particle Using Element Specific X-ray Nanotomography journal, January 2015

Life and death of a single catalytic cracking particle journal, April 2015

Assessment of the 3 D Pore Structure and Individual Components of Preshaped Catalyst Bodies by X-Ray Imaging journal, December 2014

Back Cover: Characterization of a Fluidized Catalytic Cracking Catalyst on Ensemble and Individual Particle Level by X-ray Micro- and Nanotomography, Micro-X-ray Fluorescence, and Micro-X-ray Diffraction (ChemCatChem 5/2014) journal, May 2014

Chemical imaging of catalytic solids with synchrotron radiation journal, January 2010

Phase retrieval using polychromatic illumination for transmission X-ray microscopy journal, January 2011

Hard X-ray Spectroscopic Nano-Imaging of Hierarchical Functional Materials at Work journal, September 2013

TXM-Wizard : a program for advanced data collection and evaluation in full-field transmission X-ray microscopy journal, January 2012

X-ray ptychographic computed tomography at 16 nm isotropic 3D resolution journal, January 2014

Fourier ring correlation as a resolution criterion for super-resolution microscopy journal, September 2013

3D elemental sensitive imaging using transmission X-ray microscopy journal, February 2012

Nanoscale elemental sensitivity study of Nd 2 Fe 14 B using absorption correlation tomography : Nanoscale Elemental Sensitivity Study of N journal, August 2013

Study of the accessibility effect on the irreversible deactivation of FCC catalysts from contaminant feed metals journal, September 2007

Visualization of the Equilibrium FCC Catalyst Surface by AFM and SEM–EDS journal, October 2003

Nanoscale Morphological and Chemical Changes of High Voltage Lithium–Manganese Rich NMC Composite Cathodes with Cycling journal, July 2014

Hydrodynamics of a gas–solid fluidized bed with thermally induced interparticle forces journal, January 2015

High-speed tracking of rupture and clustering in freely falling granular streams journal, June 2009

Particle cluster dynamics during fluidization journal, August 2013

The influence of interparticle forces on the fluidization behaviour of some industrial materials at high temperature journal, May 2000

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Magnetophoretic Sorting of Single Catalyst Particles journal, August 2018

Nickel Poisoning of a Cracking Catalyst Unravelled by Single‐Particle X‐ray Fluorescence‐Diffraction‐Absorption Tomography journal, January 2020

Accurate 3D Characterization of Catalytic Bodies Surface by Scanning Electron Microscopy journal, June 2019

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Fluid catalytic cracking technology: current status and recent discoveries on catalyst contamination journal, December 2018

Chemical imaging of Fischer-Tropsch catalysts under operating conditions journal, March 2017

Magnetophoretic Sorting of Single Catalyst Particles journal, August 2018

Designing FCC catalysts with high-silica Y zeolites
journal, August 1991

Heterogeneities of individual catalyst particles in space and time as monitored by spectroscopy
journal, October 2012

Hard and soft X-ray microscopy and tomography in catalysis: bridging the different time and length scales
journal, January 2010

Imaging Catalysts at Work: A Hierarchical Approach from the Macro- to the Meso- and Nano-scale
journal, November 2012

On the interaction of vanadium and nickel compounds with cracking catalyst
journal, December 1984

Vanadium passivation of cracking catalysts by imaging secondary ion mass spectrometry
journal, January 1995

Nickel and vanadium on equilibrium cracking catalysts by imaging secondary ion mass spectrometry
journal, February 1988

Mapping Metals Incorporation of a Whole Single Catalyst Particle Using Element Specific X-ray Nanotomography
journal, January 2015

Life and death of a single catalytic cracking particle
journal, April 2015

Assessment of the 3 D Pore Structure and Individual Components of Preshaped Catalyst Bodies by X-Ray Imaging
journal, December 2014

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Chemical imaging of catalytic solids with synchrotron radiation
journal, January 2010

Phase retrieval using polychromatic illumination for transmission X-ray microscopy
journal, January 2011

Hard X-ray Spectroscopic Nano-Imaging of Hierarchical Functional Materials at Work
journal, September 2013

TXM-Wizard : a program for advanced data collection and evaluation in full-field transmission X-ray microscopy
journal, January 2012

X-ray ptychographic computed tomography at 16 nm isotropic 3D resolution
journal, January 2014

Fourier ring correlation as a resolution criterion for super-resolution microscopy
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3D elemental sensitive imaging using transmission X-ray microscopy
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Nanoscale elemental sensitivity study of Nd ₂ Fe ₁₄ B using absorption correlation tomography : Nanoscale Elemental Sensitivity Study of N
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Study of the accessibility effect on the irreversible deactivation of FCC catalysts from contaminant feed metals
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Visualization of the Equilibrium FCC Catalyst Surface by AFM and SEM–EDS
journal, October 2003

Nanoscale Morphological and Chemical Changes of High Voltage Lithium–Manganese Rich NMC Composite Cathodes with Cycling
journal, July 2014

Hydrodynamics of a gas–solid fluidized bed with thermally induced interparticle forces
journal, January 2015

High-speed tracking of rupture and clustering in freely falling granular streams
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Particle cluster dynamics during fluidization
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