National Library of Energy BETA

Sample records for x-ray method shows

  1. X-ray phase-contrast methods

    SciTech Connect (OSTI)

    Lider, V. V., E-mail: lider@ns.crys.ras.ru; Kovalchuk, M. V. [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)] [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)

    2013-11-15

    This review is devoted to a comparative description of the methods for forming X-ray phase-contrast images of weakly absorbing (phase) objects. These include the crystal interferometer method, the Talbot interferometer method, diffraction-enhanced X-ray imaging, and the in-line method. The potential of their practical application in various fields of science and technology is discussed. The publications on the development and optimization of X-ray phase-contrast methods and the experimental study of phase objects are analyzed.

  2. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Instruments and Methods X-Ray Nanoimaging: Instruments and Methods Print To be held as part of SPIE. http:spie.orgOP318 August 28-29, 2013; San Diego, California, USA...

  3. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservationBio-Inspired SolarAbout /Two0PhotosPresentationsWorld's largestX-RayX-RayX-RayX-Ray

  4. Systems and methods for detecting x-rays

    DOE Patents [OSTI]

    Bross, Alan D.; Mellott, Kerry L.; Pla-Dalmau, Anna

    2006-05-02

    Systems and methods for detecting x-rays are disclosed herein. One or more x-ray-sensitive scintillators can be configured from a plurality of heavy element nano-sized particles and a plastic material, such as polystyrene. As will be explained in greater detail herein, the heavy element nano-sized particles (e.g., PbWO4) can be compounded into the plastic material with at least one dopant that permits the plastic material to scintillate. X-rays interact with the heavy element nano-sized particles to produce electrons that can deposit energy in the x-ray sensitive scintillator, which in turn can produce light.

  5. Archaeometrical studies using X-ray fluorescence methods

    SciTech Connect (OSTI)

    Pauna, Catalina; Constantinescu, B.; Constantin, F.; Bugoi, R.; Stan, D.; Vasilescu, A. [National Institute of Nuclear Physics and Engineering, POB MG-6, 077125, Bucharest (Romania)

    2010-04-26

    Elemental analysis contributes to authentication (knowing the elemental composition and considering the information about the usual composition of the objects in different historical periods it can be established if the item is original or fake), provenance studies (minor and trace elements indicates ores origin and 'consequently' mines location), (relative) dating of archaeological objects (e.g. for painted items--the chemical recipes for pigments can offer information about the age of objects). The paper gives a general layout for the NIPNE Archaeometry Laboratory's applications using X-Ray Fluorescence (XRF), micro--Proton Induced X-Ray Emission (micro-PIXE), micro-Synchrotron Radiation Induced X-Ray Fluorescence (micro--SR-XRF) methods.

  6. X-RAY METHODS FOR THE CHEMICAL CHARACTERIZATION OF ATMOSPHERIC AEROSOLS

    E-Print Network [OSTI]

    Jaklevic, J.M.

    2010-01-01

    for the routine analysis of air pollution samples, itof x-ray methods to the analysis of air particulate samples.

  7. SU-E-I-01: A Fast, Analytical Pencil Beam Based Method for First Order X-Ray Scatter Estimation of Kilovoltage Cone Beam X-Rays

    SciTech Connect (OSTI)

    Liu, J; Bourland, J [Wake Forest University, Winston-salem, NC (United States)

    2014-06-01

    Purpose: To analytically estimate first-order x-ray scatter for kV cone beam x-ray imaging with high computational efficiency. Methods: In calculating first-order scatter using the Klein-Nishina formula, we found that by integrating the point-to-point scatter along an interaction line, a “pencil-beam” scatter kernel (BSK) can be approximated to a quartic expression when the imaging field is small. This BSK model for monoenergetic, 100keV x-rays has been verified on homogeneous cube and cylinder water phantoms by comparing with the exact implementation of KN formula. For heterogeneous medium, the water-equivalent length of a BSK was acquired with an improved Siddon's ray-tracing algorithm, which was also used in calculating pre- and post- scattering attenuation. To include the electron binding effect for scattering of low-kV photons, the mean corresponding scattering angle is determined from the effective point of scattered photons of a BSK. The behavior of polyenergetic x-rays was also investigated for 120kV x-rays incident to a sandwiched infinite heterogeneous slab phantom, with the electron binding effect incorporated. Exact computation and Monte Carlo simulations were performed for comparisons, using the EGSnrc code package. Results: By reducing the 3D volumetric target (o(n{sup 3})) to 2D pencil-beams (o(n{sup 2})), the computation expense can be generally lowered by n times, which our experience verifies. The scatter distribution on a flat detector shows high agreement between the analytic BSK model and exact calculations. The pixel-to-pixel differences are within (-2%, 2%) for the homogeneous cube and cylinder phantoms and within (0, 6%) for the heterogeneous slab phantom. However, the Monte Carlo simulation shows increased deviation of the BSK model toward detector periphery. Conclusion: The proposed BSK model, accommodating polyenergetic x-rays and electron binding effect at low kV, shows great potential in efficiently estimating the first-order scatter from small imaging fields. We are investigating more thoroughly to improve performance and explore applications.

  8. Method and apparatus for micromachining using hard X-rays

    DOE Patents [OSTI]

    Siddons, D.P.; Johnson, E.D.; Guckel, H.; Klein, J.L.

    1997-10-21

    An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures. 21 figs.

  9. Method and apparatus for micromachining using hard X-rays

    DOE Patents [OSTI]

    Siddons, David Peter (Shoreham, NY); Johnson, Erik D. (Ridge, NY); Guckel, Henry (Madison, WI); Klein, Jonathan L. (Madison, WI)

    1997-10-21

    An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures.

  10. A method of measuring gold nanoparticle concentrations by x-ray fluorescence for biomedical applications

    SciTech Connect (OSTI)

    Wu Di; Li Yuhua; Wong, Molly D.; Liu Hong [Center for Bioengineering and School of Electrical and Computer Engineering, University of Oklahoma, Norman, Oklahoma 73019 (United States)

    2013-05-15

    Purpose: This paper reports a technique that enables the quantitative determination of the concentration of gold nanoparticles (GNPs) through the accurate detection of their fluorescence radiation in the diagnostic x-ray spectrum. Methods: Experimentally, x-ray fluorescence spectra of 1.9 and 15 nm GNP solutions are measured using an x-ray spectrometer, individually and within chicken breast tissue samples. An optimal combination of excitation and emission filters is determined to segregate the fluorescence spectra at 66.99 and 68.80 keV from the background scattering. A roadmap method is developed that subtracts the scattered radiation (acquired before the insertion of GNP solutions) from the signal radiation acquired after the GNP solutions are inserted. Results: The methods effectively minimize the background scattering in the spectrum measurements, showing linear relationships between GNP solutions from 0.1% to 10% weight concentration and from 0.1% to 1.0% weight concentration inside a chicken breast tissue sample. Conclusions: The investigation demonstrated the potential of imaging gold nanoparticles quantitatively in vivo for in-tissue studies, but future studies will be needed to investigate the ability to apply this method to clinical applications.

  11. X-ray microtomography shows pore structure and tortuosity in alkali-activated binders

    SciTech Connect (OSTI)

    Provis, John L.; Myers, Rupert J.; White, Claire E.; Rose, Volker; Deventer, Jannie S.J. van

    2012-06-15

    Durability of alkali-activated binders is of vital importance in their commercial application, and depends strongly on microstructure and pore network characteristics. X-ray microtomography ({mu}CT) offers, for the first time, direct insight into microstructural and pore structure characteristics in three dimensions. Here, {mu}CT is performed on a set of sodium metasilicate-activated fly ash/slag blends, using a synchrotron beamline instrument. Segmentation of the samples into pore and solid regions is then conducted, and pore tortuosity is calculated by a random walker method. Segmented porosity and diffusion tortuosity are correlated, and vary as a function of slag content (slag addition reduces porosity and increases tortuosity), and sample age (extended curing gives lower porosity and higher tortuosity). This is particularly notable for samples with {>=} 50% slag content, where a space-filling calcium (alumino)silicate hydrate gel provides porosity reductions which are not observed for the sodium aluminosilicate ('geopolymer') gels which do not chemically bind water of hydration.

  12. Comment on 'Dirac R-matrix method for the calculation of x-ray...

    Office of Scientific and Technical Information (OSTI)

    Comment on 'Dirac R-matrix method for the calculation of x-ray line polarization' Citation Details In-Document Search Title: Comment on 'Dirac R-matrix method for the calculation...

  13. A new background correction method in X-ray phase contrast imaging with Talbot-Lau interferometer

    E-Print Network [OSTI]

    Wang, Shenghao; Momose, Atsushi; Gao, Kun; Wang, Zhili; Zhang, Can; Han, Huajie; Yang, Meng; Zhang, Kai; Zhu, Peiping; Wu, Ziyu

    2015-01-01

    X-ray Talbot-Lau interferometer has been used widely to conduct X-ray phase contrast imaging with a conventional low-brilliance X-ray source. Typically, in this X-ray phase contrast imaging technique, a background correction process has to be performed in order to obtain the pure signal of the sample. In this manuscript, we reported on an experimental research on the background correction strategies within this X-ray imaging technique, especially we introduced a new way to perform background correction, the key point of this new method is changing the initial phase of each pixel by a cyclic shift operation on the raw images collected by phase stepping scan. Experimental result and numerical analysis show that this new method could successfully realize background correction without error, moreover, a potential advantage of this new method is that its effective phase measuring range could be tuned flexibly in some degree for example to (-{\\pi}+3, {\\pi}+3], thus it would find potential advantage in certain case ...

  14. Method for detecting binding events using micro-X-ray fluorescence spectrometry

    DOE Patents [OSTI]

    Warner, Benjamin P. (Los Alamos, NM); Havrilla, George J. (Los Alamos, NM); Mann, Grace (Hong Kong, HK)

    2010-12-28

    Method for detecting binding events using micro-X-ray fluorescence spectrometry. Receptors are exposed to at least one potential binder and arrayed on a substrate support. Each member of the array is exposed to X-ray radiation. The magnitude of a detectable X-ray fluorescence signal for at least one element can be used to determine whether a binding event between a binder and a receptor has occurred, and can provide information related to the extent of binding between the binder and receptor.

  15. Method and apparatus for producing durationally short ultraviolet or x-ray laser pulses

    DOE Patents [OSTI]

    MacGowan, B.J.; Matthews, D.L.; Trebes, J.E.

    1987-05-05

    A method and apparatus is disclosed for producing ultraviolet or x- ray laser pulses of short duration. An ultraviolet or x-ray laser pulse of long duration is progressively refracted, across the surface of an opaque barrier, by a streaming plasma that is produced by illuminating a solid target with a pulse of conventional line focused high power laser radiation. The short pulse of ultraviolet or x-ray laser radiation, which may be amplified to high power, is separated out by passage through a slit aperture in the opaque barrier.

  16. High efficiency replicated x-ray optics and fabrication method

    DOE Patents [OSTI]

    Barbee, Jr., Troy W. (Palo Alto, CA); Lane, Stephen M. (Oakland, CA); Hoffman, Donald E. (Fremont, CA)

    2001-01-01

    Replicated x-ray optics are fabricated by sputter deposition of reflecting layers on a super-polished reusable mandrel. The reflecting layers are strengthened by a supporting multilayer that results in stronger stress-relieved reflecting surfaces that do not deform during separation from the mandrel. The supporting multilayer enhances the ability to part the replica from the mandrel without degradation in surface roughness. The reflecting surfaces are comparable in smoothness to the mandrel surface. An outer layer is electrodeposited on the supporting multilayer. A parting layer may be deposited directly on the mandrel before the reflecting surface to facilitate removal of the layered, tubular optic device from the mandrel without deformation. The inner reflecting surface of the shell can be a single layer grazing reflection mirror or a resonant multilayer mirror. The resulting optics can be used in a wide variety of applications, including lithography, microscopy, radiography, tomography, and crystallography.

  17. Multilayer graphene stacks grown by different methods-thickness measurements by X-ray diffraction, Raman spectroscopy and optical transmission

    SciTech Connect (OSTI)

    Tokarczyk, M., E-mail: mateusz.tokarczyk@fuw.edu.pl; Kowalski, G.; K?pa, H.; Grodecki, K.; Drabi?ska, A. [University of Warsaw, Institute of Experimental Physics, Faculty of Physics (Poland); Strupi?ski, W. [Institute of Electronic Materials Technology (Poland)

    2013-12-15

    X-ray diffraction, Raman spectroscopy and Optical absorption estimates of the thickness of graphene multi layer stacks (number of graphene layers) are presented for three different growth techniques. The objective of this work was focused on comparison and reconciliation of the two already widely used methods for thickness estimates (Raman and Absorption) with the calibration of the X-ray method as far as Scherer constant K is concerned and X-ray based Wagner-Aqua extrapolation method.

  18. X-ray photon-in/photon-out methods for chemical imaging

    SciTech Connect (OSTI)

    Marcus, Matthew A.

    2010-03-24

    Most interesting materials in nature are heterogeneous, so it is useful to have analytical techniques with spatial resolution sufficient to resolve these heterogeneities.This article presents the basics of X-ray photon-in/photon-out chemical imaging. This family of methods allows one to derive images reflectingthe chemical state of a given element in a complex sample, at micron or deep sub-micron scale. X-ray chemical imaging is relatively non-destructiveand element-selective, and requires minimal sample preparation. The article presents the basic concepts and some considerations of data takingand data analysis, along with some examples.

  19. X-ray survival characteristics and genetic analysis for nine saccharomyces deletion mutants that show altered radiation sensitivity

    SciTech Connect (OSTI)

    Game, John C.; Williamson, Marsha S.; Baccari, Clelia

    2004-01-07

    The availability of a genome-wide set of Saccharomyces deletion mutants provides a chance to identify all the yeast genes involved in DNA repair. Using X-rays, we are screening these mutants to identify additional genes that show increased sensitivity to the lethal effects of ionizing radiation. For each mutant identified as sensitive, we are confirming that the sensitivity phenotype co-segregates with the deletion allele and are obtaining multipoint survival-versus-dose assays in at least two haploid and one homozygous diploid strains. We present data for deletion mutants involving the genes DOT1, MDM20, NAT3, SPT7, SPT20, GCN5, HFI1, DCC1 and VID21/EAF1, and discuss their potential roles in repair. Eight of these genes have a clear radiation-sensitive phenotype when deleted, but the ninth, GCN5, has at most a borderline phenotype. None of the deletions confer substantial sensitivity to ultra-violet radiation, although one or two may confer marginal sensitivity. The DOT1 gene is of interest because its only known function is to methylate one lysine residue in the core of the histone H3 protein. We find that histone H3 mutants (supplied by K. Struhl) in which this residue is replaced by other amino-acids are also X-ray sensitive, seeming to confirm that methylation of the lysine-79 residue is required for effective repair of radiation damage.

  20. Comparison of two x-ray phase-contrast imaging methods with a microfocus source

    E-Print Network [OSTI]

    and experiments using a liquid-metal-jet x-ray microfocus source. Radiation doses required for detection radiation, simulations show a lower dose requirement for PBI for small object features and a lower dose and implementation of a compact low-dose diffraction enhanced medical imaging system," Acad. Radiol. 16(8), 911

  1. HEW simulations and quantification of the microroughness requirements for X-ray telescopes by means of numerical and analytical methods

    E-Print Network [OSTI]

    Spiga, D; Pareschi, G

    2015-01-01

    Future X-ray telescopes like SIMBOL-X will operate in a wide band of the X-ray spectrum (from 0.1 to 80 keV); these telescopes will extend the optical performances of the existing soft X-ray telescopes to the hard X-ray band, and in particular they will be characterized by a angular resolution (conveniently expressed in terms of HEW, Half-Energy- Width) less than 20 arcsec. However, it is well known that the microroughness of the reflecting surfaces of the optics causes the scattering of X-rays. As a consequence, the imaging quality can be severely degraded. Moreover, the X-ray scattering can be the dominant problem in hard X-rays because its relevance is an increasing function of the photon energy. In this work we consistently apply a numerical method and an analytical one to evaluate the X-ray scattering impact on the HEW of an X-ray optic, as a function of the photon energy: both methods can also include the effects of figure errors in determining the final HEW. A comparison of the results obtained with th...

  2. Method for the fabrication of three-dimensional microstructures by deep X-ray lithography

    DOE Patents [OSTI]

    Sweatt, William C.; Christenson, Todd R.

    2005-04-05

    A method for the fabrication of three-dimensional microstructures by deep X-ray lithography (DXRL) comprises a masking process that uses a patterned mask with inclined mask holes and off-normal exposures with a DXRL beam aligned with the inclined mask holes. Microstructural features that are oriented in different directions can be obtained by using multiple off-normal exposures through additional mask holes having different orientations. Various methods can be used to block the non-aligned mask holes from the beam when using multiple exposures. A method for fabricating a precision 3D X-ray mask comprises forming an intermediate mask and a master mask on a common support membrane.

  3. Precise orientation of single crystals by a simple x-ray diffraction rocking curve method

    SciTech Connect (OSTI)

    Doucette, L.D.; Pereira da Cunha, M.; Lad, R.J.

    2005-03-01

    A simple method has been developed for accurately measuring the crystallographic orientation of a single crystal boule, employing a conventional four-circle x-ray diffraction arrangement in the rocking curve mode which relaxes the need for precise instrument and/or reference alignment. By acquiring a total of eight rocking curve measurements at specific orientations about the specimen azimuth, the absolute miscut angle between a crystal surface and the desired crystallographic plane can be resolved to within {+-}0.01 deg.

  4. Mapping Strain in Nanocrystalline Nitinol: an X-ray Diffraction Method (SULI paper)

    SciTech Connect (OSTI)

    Bibee, Mathew; /SLAC, SSRL

    2006-01-04

    Understanding the mechanical properties of biomedical devices is critical in predicting and preventing their failure in the body. Such knowledge is essential, for example, in the design of biomedical stents, which must undergo repeated strain over their ten year lifetimes without breaking. Computational models are used to predict mechanical response of a device, but these models are not complete; there are significant deviations from the predictions, especially when devices are subjected to repeated multi-axial loads. Improving these models requires comparisons with actual measurements of strained nitinol. Local measurements of the full strain tensor can be made using X-ray diffraction techniques, but they are currently limited to materials whose grain size is larger than the X-ray beam size or require several diffraction patterns produced by rotation of the sample. Nitinol stents are nanocrystalline, with grains smaller than any available X-ray beam. We present a method for measuring the local strain in a nanocrystalline material from a single X-ray diffraction pattern by extending current powder diffraction techniques. The components of the strain tensor are mapped onto a displacement ellipsoid, which is then reconstructed from diffraction data through Bragg's law and least-squares fitting. Using simulated diffraction data, we performed sensitivity tests to examine how the accuracy of the method depends on how much of the diffraction pattern is measured. We found that strain can be accurately calculated from measurements of at least three diffraction arcs of at least 20{sup o} in length. Thus we believe that our method is a viable approach to calculating strain provided a sufficient amount of diffraction pattern is recorded.

  5. Following the dynamics of matter with femtosecond precision using the X-ray streaking method

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    David, C.; Karvinen, P.; Sikorski, M.; Song, S.; Vartiainen, I.; Milne, C. J.; Mozzanica, A.; Kayser, Y.; Diaz, A.; Mohacsi, I.; et al

    2015-01-06

    X-ray Free Electron Lasers (FELs) can produce extremely intense and very short pulses, down to below 10 femtoseconds (fs). Among the key applications are ultrafast time-resolved studies of dynamics of matter by observing responses to fast excitation pulses in a pump-probe manner. Detectors with sufficient time resolution for observing these processes are not available. Therefore, such experiments typically measure a sample's full dynamics by repeating multiple pump-probe cycles at different delay times. This conventional method assumes that the sample returns to an identical or very similar state after each cycle. Here we describe a novel approach that can provide amore »time trace of responses following a single excitation pulse, jitter-free, with fs timing precision. We demonstrate, in an X-ray diffraction experiment, how it can be applied to the investigation of ultrafast irreversible processes.« less

  6. Dual x-ray fluorescence spectrometer and method for fluid analysis

    DOE Patents [OSTI]

    Wilson, Bary W.; Shepard, Chester L.

    2005-02-22

    Disclosed are an X-ray fluorescence (SRF) spectrometer and method for on-site and in-line determination of contaminant elements in lubricating oils and in fuel oils on board a marine vessel. An XRF source block 13 contains two radionuclide sources 16, 17 (e.g. Cd 109 and Fe 55), each oriented 180 degrees from the other to excite separate targets. The Cd 109 source 16 excites sample lube oil flowing through a low molecular weight sample line 18. The Fe 55 source 17 excites fuel oil manually presented to the source beam inside a low molecular weight vial 26 or other container. Two separate detectors A and B are arranged to detect the fluorescent x-rays from the targets, photons from the analyte atoms in the lube oil for example, and sulfur identifying x-rays from bunker fuel oil for example. The system allows both automated in-line and manual on-site analysis using one set of signal processing and multi-channel analyzer electronics 34, 37 as well as one computer 39 and user interface 43.

  7. A practical global distortion correction method for an image intensifier based x-ray fluoroscopy system

    SciTech Connect (OSTI)

    Gutierrez, Luis F.; Ozturk, Cengizhan; McVeigh, Elliot R.; Lederman, Robert J. [Department of Biomedical Engineering, Johns Hopkins University, Baltimore, Maryland 21205 and Lab of Cardiac Energetics, National Institutes of Health, Bethesda, Maryland 20892 (United States); Cardiovascular Branch, Division of Intramural Research, National Heart, Lung, and Blood Institute, National Institutes of Health, Bethesda, Maryland 20892 and Biomedical Engineering Institute, Bogazici University, Istanbul (Turkey); Lab of Cardiac Energetics, National Institutes of Health, Bethesda, Maryland 20892 and Department of Biomedical Engineering, Johns Hopkins University, Baltimore, Maryland 21205 (United States); Cardiovascular Branch, Division of Intramural Research, National Heart, Lung, and Blood Institute, National Institutes of Health, Bethesda, Maryland 20892 (United States)

    2008-03-15

    X-ray images acquired on systems with image intensifiers (II) exhibit characteristic distortion which is due to both external and internal factors. The distortion is dependent on the orientation of the II, a fact particularly relevant to II's mounted on C arms which have several degrees of freedom of motion. Previous descriptions of distortion correction strategies have relied on a dense sampling of the C-arm orientation space, and as such have been limited mostly to a single arc of the primary angle, {alpha}. We present a new method which smooths the trajectories of the segmented vertices of the grid phantom as a function of {alpha} prior to solving the two-dimensional warping problem. It also shows that the same residual errors of distortion correction could be achieved without fitting the trajectories of the grid vertices, but instead applying the previously described global method of distortion correction, followed by directly smoothing the values of the polynomial coefficients as functions of the C-arm orientation parameters. When this technique was applied to a series of test images at arbitrary {alpha}, the root-mean-square (RMS) residual error was 0.22 pixels. The new method was extended to three degrees of freedom of the C-arm motion: the primary angle, {alpha}; the secondary angle, {beta}; and the source-to-intensifier distance, {lambda}. Only 75 images were used to characterize the distortion for the following ranges: {alpha}, {+-}45 deg. ({delta}{alpha}=22.5 deg.); {beta}, {+-}36 deg. ({delta}{beta}=18 deg.); {lambda}, 98-118 cm ({delta}{lambda}=10 cm). When evaluated on a series of test images acquired at arbitrary ({alpha},{beta},{lambda}), the RMS residual error was 0.33 pixels. This method is targeted at applications such as guidance of catheter-based interventions and treatment planning for brachytherapy, which require distortion-corrected images over a large range of C-arm orientations.

  8. Vertical dispersion methods in x-ray spectroscopy of high temperature plasmas

    SciTech Connect (OSTI)

    Renner, O.; Missalla, T.; Foerster, E.

    1995-12-31

    General formulae for the applying the vertical dispersion principle in x-ray spectroscopy of multiple charged ions are summarized, the characteristics of the experimental schemes based on flat and bent crystals are discussed. The unique properties of the novel spectroscopic methods, i.e., their extremely high dispersion, high spectral and 1-D spatial resolution and good collection efficiency, make them very attractive for ultrahigh-resolution spectroscopy. The examples of successful use of the vertical dispersion modifications of the double-crystal and the Johann spectrometer in diagnostics of several types of laser-generated plasma are presented.

  9. Imaging method based on attenuation, refraction and ultra-small-angle-scattering of x-rays

    DOE Patents [OSTI]

    Wernick, Miles N.; Chapman, Leroy Dean; Oltulu, Oral; Zhong, Zhong

    2005-09-20

    A method for detecting an image of an object by measuring the intensity at a plurality of positions of a transmitted beam of x-ray radiation emitted from the object as a function of angle within the transmitted beam. The intensity measurements of the transmitted beam are obtained by a crystal analyzer positioned at a plurality of angular positions. The plurality of intensity measurements are used to determine the angular intensity spectrum of the transmitted beam. One or more parameters, such as an attenuation property, a refraction property and a scatter property, can be obtained from the angular intensity spectrum and used to display an image of the object.

  10. Method and apparatus for molecular imaging using X-rays at resonance wavelengths

    DOE Patents [OSTI]

    Chapline, Jr., George F. (Alamo, CA)

    1985-01-01

    Holographic X-ray images are produced representing the molecular structure of a microscopic object, such as a living cell, by directing a beam of coherent X-rays upon the object to produce scattering of the X-rays by the object, producing interference on a recording medium between the scattered X-rays from the object and unscattered coherent X-rays and thereby producing holograms on the recording surface, and establishing the wavelength of the coherent X-rays to correspond with a molecular resonance of a constituent of such object and thereby greatly improving the contrast, sensitivity and resolution of the holograms as representations of molecular structures involving such constituent. For example, the coherent X-rays may be adjusted to the molecular resonant absorption line of nitrogen at about 401.3 eV to produce holographic images featuring molecular structures involving nitrogen.

  11. A real-time regional adaptive exposure method for saving dose-area product in x-ray fluoroscopy

    SciTech Connect (OSTI)

    Burion, Steve; Funk, Tobias; Speidel, Michael A.

    2013-05-15

    Purpose: Reduction of radiation dose in x-ray imaging has been recognized as a high priority in the medical community. Here the authors show that a regional adaptive exposure method can reduce dose-area product (DAP) in x-ray fluoroscopy. The authors' method is particularly geared toward providing dose savings for the pediatric population. Methods: The scanning beam digital x-ray system uses a large-area x-ray source with 8000 focal spots in combination with a small photon-counting detector. An imaging frame is obtained by acquiring and reconstructing up to 8000 detector images, each viewing only a small portion of the patient. Regional adaptive exposure was implemented by varying the exposure of the detector images depending on the local opacity of the object. A family of phantoms ranging in size from infant to obese adult was imaged in anteroposterior view with and without adaptive exposure. The DAP delivered to each phantom was measured in each case, and noise performance was compared by generating noise arrays to represent regional noise in the images. These noise arrays were generated by dividing the image into regions of about 6 mm{sup 2}, calculating the relative noise in each region, and placing the relative noise value of each region in a one-dimensional array (noise array) sorted from highest to lowest. Dose-area product savings were calculated as the difference between the ratio of DAP with adaptive exposure to DAP without adaptive exposure. The authors modified this value by a correction factor that matches the noise arrays where relative noise is the highest to report a final dose-area product savings. Results: The average dose-area product saving across the phantom family was (42 {+-} 8)% with the highest dose-area product saving in the child-sized phantom (50%) and the lowest in the phantom mimicking an obese adult (23%). Conclusions: Phantom measurements indicate that a regional adaptive exposure method can produce large DAP savings without compromising the noise performance in the image regions with highest noise.

  12. Fluctuation X-Ray Scattering

    SciTech Connect (OSTI)

    Saldin, PI: D. K.; Co-I's: J. C. H. Spence and P. Fromme

    2013-01-25

    The work supported by the grant was aimed at developing novel methods of finding the structures of biomolecules using x-rays from novel sources such as the x-ray free electron laser and modern synchrotrons

  13. Tunable X-ray source

    DOE Patents [OSTI]

    Boyce, James R. (Williamsburg, VA)

    2011-02-08

    A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

  14. Determination of Diffusion Profiles in Altered Wellbore Cement Using X-ray Computed Tomography Methods

    SciTech Connect (OSTI)

    Mason, Harris E. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Walsh, Stuart D. C. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); DuFrane, Wyatt L. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States); Carroll, Susan A. [Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

    2014-06-17

    The development of accurate, predictive models for use in determining wellbore integrity requires detailed information about the chemical and mechanical changes occurring in hardened Portland cements. X-ray computed tomography (XRCT) provides a method that can nondestructively probe these changes in three dimensions. Here, we describe a method for extracting subvoxel mineralogical and chemical information from synchrotron XRCT images by combining advanced image segmentation with geochemical models of cement alteration. The method relies on determining “effective linear activity coefficients” (ELAC) for the white light source to generate calibration curves that relate the image grayscales to material composition. The resulting data set supports the modeling of cement alteration by CO2-rich brine with discrete increases in calcium concentration at reaction boundaries. The results of these XRCT analyses can be used to further improve coupled geochemical and mechanical models of cement alteration in the wellbore environment.

  15. A scaled gradient projection method for the X-ray imaging of solar flares

    E-Print Network [OSTI]

    Bonettini, S

    2013-01-01

    In this paper we present a new optimization algorithm for the reconstruction of X-ray images of solar flares by means of the data collected by the Reuven Ramaty High Energy Solar Spectroscopic Imager (RHESSI). The imaging concept of the satellite is based of rotating modulation collimator instruments, which allow the use of both Fourier imaging approaches and reconstruction techniques based on the straightforward inversion of the modulated count profiles. Although in the last decade a greater attention has been devoted to the former strategies due to their very limited computational cost, here we consider the latter model and investigate the effectiveness of a scaled gradient projection method for the solution of the corresponding constrained minimization problem. Moreover, regularization is introduced through either an early stopping of the iterative procedure, or a Tikhonov term added to the discrepancy function, by means of a discrepancy principle accounting for the Poisson nature of the noise affecting th...

  16. Karyotyping human chromosomes by optical and x-ray ptychography methods

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Shemilt, Laura; Verbanis, Ephanielle; Schwenke, Joerg; Estandarte, Ana  K.; Xiong, Gang; Harder, Ross; Parmar, Neha; Yusuf, Mohammed; Zhang, Fucai; Robinson, Ian  K.

    2015-02-01

    Sorting and identifying chromosomes, a process known as karyotyping, is widely used to detect changes in chromosome shapes and gene positions. In a karyotype the chromosomes are identified by their size and therefore this process can be performed by measuring macroscopic structural variables. Chromosomes contain a specific number of basepairs that linearly correlate with their size; therefore, it is possible to perform a karyotype on chromosomes using their mass as an identifying factor. Here, we obtain the first images, to our knowledge, of chromosomes using the novel imaging method of ptychography. We can use the images to measure the massmore »of chromosomes and perform a partial karyotype from the results. We also obtain high spatial resolution using this technique with synchrotron source x-rays.« less

  17. Method for improving x-ray diffraction determinations of residual stress in nickel-base alloys

    DOE Patents [OSTI]

    Berman, R.M.; Cohen, I.

    1988-04-26

    A process for improving the technique of measuring residual stress by x-ray diffraction in pieces of nickel-base alloys is discussed. Part of a predetermined area of the surface of a nickel-base alloy is covered with a dispersion. This exposes the covered and uncovered portions of the surface of the alloy to x-rays by way of an x-ray diffractometry apparatus, making x-ray diffraction determinations of the exposed surface, and measuring the residual stress in the alloy based on these determinations. The dispersion is opaque to x-rays and serves a dual purpose, since it masks off unsatisfactory signals such that only a small portion of the surface is measured, and it supplies an internal standard by providing diffractogram peaks comparable to the peaks of the nickel alloy so that the alloy peaks can be very accurately located regardless of any sources of error external to the sample. 2 figs.

  18. Method for improve x-ray diffraction determinations of residual stress in nickel-base alloys

    DOE Patents [OSTI]

    Berman, Robert M. (Pittsburgh, PA); Cohen, Isadore (Pittsburgh, PA)

    1990-01-01

    A process for improving the technique of measuring residual stress by x-ray diffraction in pieces of nickel-base alloys which comprises covering part of a predetermined area of the surface of a nickel-base alloy with a dispersion, exposing the covered and uncovered portions of the surface of the alloy to x-rays by way of an x-ray diffractometry apparatus, making x-ray diffraction determinations of the exposed surface, and measuring the residual stress in the alloy based on these determinations. The dispersion is opaque to x-rays and serves a dual purpose since it masks off unsatisfactory signals such that only a small portion of the surface is measured, and it supplies an internal standard by providing diffractogram peaks comparable to the peaks of the nickel alloy so that the alloy peaks can be very accurately located regardless of any sources of error external to the sample.

  19. X-ray lithography source

    DOE Patents [OSTI]

    Piestrup, Melvin A. (Woodside, CA); Boyers, David G. (Mountain View, CA); Pincus, Cary (Sunnyvale, CA)

    1991-01-01

    A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and elminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an exellent moderate-priced X-ray source for lithography.

  20. Standard test method for determination of uranium or gadolinium (or both) in gadolinium oxide-uranium oxide pellets or by X-ray fluorescence (XRF)

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2008-01-01

    Standard test method for determination of uranium or gadolinium (or both) in gadolinium oxide-uranium oxide pellets or by X-ray fluorescence (XRF)

  1. Spectral encoding method for measuring the relative arrival time between x-ray/optical pulses

    SciTech Connect (OSTI)

    Bionta, M. R.; Hartmann, N.; Weaver, M.; French, D.; Glownia, J. M.; Bostedt, C.; Chollet, M.; Ding, Y.; Fritz, D. M.; Fry, A. R.; Krzywinski, J.; Lemke, H. T.; Messerschmidt, M.; Schorb, S.; Zhu, D.; White, W. E.; Nicholson, D. J.; Cryan, J. P.; Baker, K.; Kane, D. J.; and others

    2014-08-15

    The advent of few femtosecond x-ray light sources brings promise of x-ray/optical pump-probe experiments that can measure chemical and structural changes in the 10–100 fs time regime. Widely distributed timing systems used at x-ray Free-Electron Laser facilities are typically limited to above 50 fs fwhm jitter in active x-ray/optical synchronization. The approach of single-shot timing measurements is used to sort results in the event processing stage. This has seen wide use to accommodate the insufficient precision of active stabilization schemes. In this article, we review the current technique for “measure-and-sort” at the Linac Coherent Light Source at the SLAC National Accelerator Laboratory. The relative arrival time between an x-ray pulse and an optical pulse is measured near the experimental interaction region as a spectrally encoded cross-correlation signal. The cross-correlation provides a time-stamp for filter-and-sort algorithms used for real-time sorting. Sub-10 fs rms resolution is common in this technique, placing timing precision at the same scale as the duration of the shortest achievable x-ray pulses.

  2. Method and apparatus for analog signal conditioner for high speed, digital x-ray spectrometer

    DOE Patents [OSTI]

    Warburton, W.K.; Hubbard, B.

    1999-02-09

    A signal processing system which accepts input from an x-ray detector-preamplifier and produces a signal of reduced dynamic range for subsequent analog-to-digital conversion is disclosed. The system conditions the input signal to reduce the number of bits required in the analog-to-digital converter by removing that part of the input signal which varies only slowly in time and retaining the amplitude of the pulses which carry information about the x-rays absorbed by the detector. The parameters controlling the signal conditioner`s operation can be readily supplied in digital form, allowing it to be integrated into a feedback loop as part of a larger digital x-ray spectroscopy system. 13 figs.

  3. Method and apparatus for analog signal conditioner for high speed, digital x-ray spectrometer

    DOE Patents [OSTI]

    Warburton, William K. (1300 Mills St., Menlo Park, CA 94025); Hubbard, Bradley (Santa Cruz, CA)

    1999-01-01

    A signal processing system which accepts input from an x-ray detector-preamplifier and produces a signal of reduced dynamic range for subsequent analog-to-digital conversion. The system conditions the input signal to reduce the number of bits required in the analog-to-digital converter by removing that part of the input signal which varies only slowly in time and retaining the amplitude of the pulses which carry information about the x-rays absorbed by the detector. The parameters controlling the signal conditioner's operation can be readily supplied in digital form, allowing it to be integrated into a feedback loop as part of a larger digital x-ray spectroscopy system.

  4. Resonant Soft X-Ray Contrast Variation Methods as Composition-Specific Probes of Thin Polymer Film Structure

    E-Print Network [OSTI]

    Welch, Cynthia F.

    2008-01-01

    traditional x-ray and neutron scattering techniques is oftentechniques used in neutron scattering, which requiretraditional x-ray and neutron scattering techniques. 16, 32

  5. Spectral Resolution for Five-Element, Filtered, X-Ray Detector (XRD) Arrays Using the Methods of Backus and Gilbert

    SciTech Connect (OSTI)

    FEHL,DAVID LEE; BIGGS,F.; CHANDLER,GORDON A.; STYGAR,WILLIAM A.

    2000-01-17

    The generalized method of Backus and Gilbert (BG) is described and applied to the inverse problem of obtaining spectra from a 5-channel, filtered array of x-ray detectors (XRD's). This diagnostic is routinely fielded on the Z facility at Sandia National Laboratories to study soft x-ray photons ({le}2300 eV), emitted by high density Z-pinch plasmas. The BG method defines spectral resolution limits on the system of response functions that are in good agreement with the unfold method currently in use. The resolution so defined is independent of the source spectrum. For noise-free, simulated data the BG approximating function is also in reasonable agreement with the source spectrum (150 eV black-body) and the unfold. This function may be used as an initial trial function for iterative methods or a regularization model.

  6. Systems and methods for detecting an image of an object by use of an X-ray beam having a polychromatic distribution

    DOE Patents [OSTI]

    Parham, Christopher; Zhong, Zhong; Pisano, Etta; Connor, Dean; Chapman, Leroy D.

    2010-06-22

    Systems and methods for detecting an image of an object using an X-ray beam having a polychromatic energy distribution are disclosed. According to one aspect, a method can include detecting an image of an object. The method can include generating a first X-ray beam having a polychromatic energy distribution. Further, the method can include positioning a single monochromator crystal in a predetermined position to directly intercept the first X-ray beam such that a second X-ray beam having a predetermined energy level is produced. Further, an object can be positioned in the path of the second X-ray beam for transmission of the second X-ray beam through the object and emission from the object as a transmitted X-ray beam. The transmitted X-ray beam can be directed at an angle of incidence upon a crystal analyzer. Further, an image of the object can be detected from a beam diffracted from the analyzer crystal.

  7. Method for characterizing mask defects using image reconstruction from X-ray diffraction patterns

    DOE Patents [OSTI]

    Hau-Riege, Stefan Peter (Fremont, CA)

    2007-05-01

    The invention applies techniques for image reconstruction from X-ray diffraction patterns on the three-dimensional imaging of defects in EUVL multilayer films. The reconstructed image gives information about the out-of-plane position and the diffraction strength of the defect. The positional information can be used to select the correct defect repair technique. This invention enables the fabrication of defect-free (since repaired) X-ray Mo--Si multilayer mirrors. Repairing Mo--Si multilayer-film defects on mask blanks is a key for the commercial success of EUVL. It is known that particles are added to the Mo--Si multilayer film during the fabrication process. There is a large effort to reduce this contamination, but results are not sufficient, and defects continue to be a major mask yield limiter. All suggested repair strategies need to know the out-of-plane position of the defects in the multilayer.

  8. Method and apparatus for digitally based high speed x-ray spectrometer

    DOE Patents [OSTI]

    Warburton, W.K.; Hubbard, B.

    1997-11-04

    A high speed, digitally based, signal processing system which accepts input data from a detector-preamplifier and produces a spectral analysis of the x-rays illuminating the detector. The system achieves high throughputs at low cost by dividing the required digital processing steps between a ``hardwired`` processor implemented in combinatorial digital logic, which detects the presence of the x-ray signals in the digitized data stream and extracts filtered estimates of their amplitudes, and a programmable digital signal processing computer, which refines the filtered amplitude estimates and bins them to produce the desired spectral analysis. One set of algorithms allow this hybrid system to match the resolution of analog systems while operating at much higher data rates. A second set of algorithms implemented in the processor allow the system to be self calibrating as well. The same processor also handles the interface to an external control computer. 19 figs.

  9. Method and apparatus for digitally based high speed x-ray spectrometer

    DOE Patents [OSTI]

    Warburton, William K. (1300 Mills St., Menlo Park, CA 94025); Hubbard, Bradley (Santa Cruz, CA)

    1997-01-01

    A high speed, digitally based, signal processing system which accepts input data from a detector-preamplifier and produces a spectral analysis of the x-rays illuminating the detector. The system achieves high throughputs at low cost by dividing the required digital processing steps between a "hardwired" processor implemented in combinatorial digital logic, which detects the presence of the x-ray signals in the digitized data stream and extracts filtered estimates of their amplitudes, and a programmable digital signal processing computer, which refines the filtered amplitude estimates and bins them to produce the desired spectral analysis. One set of algorithms allow this hybrid system to match the resolution of analog systems while operating at much higher data rates. A second set of algorithms implemented in the processor allow the system to be self calibrating as well. The same processor also handles the interface to an external control computer.

  10. A theoretical comparison of x-ray angiographic image quality using energy-dependent and conventional subtraction methods

    SciTech Connect (OSTI)

    Tanguay, Jesse; Kim, Ho Kyung; Cunningham, Ian A.

    2012-01-15

    Purpose: X-ray digital subtraction angiography (DSA) is widely used for vascular imaging. However, the need to subtract a mask image can result in motion artifacts and compromised image quality. The current interest in energy-resolving photon-counting (EPC) detectors offers the promise of eliminating motion artifacts and other advanced applications using a single exposure. The authors describe a method of assessing the iodine signal-to-noise ratio (SNR) that may be achieved with energy-resolved angiography (ERA) to enable a direct comparison with other approaches including DSA and dual-energy angiography for the same patient exposure. Methods: A linearized noise-propagation approach, combined with linear expressions of dual-energy and energy-resolved imaging, is used to describe the iodine SNR. The results were validated by a Monte Carlo calculation for all three approaches and compared visually for dual-energy and DSA imaging using a simple angiographic phantom with a CsI-based flat-panel detector. Results: The linearized SNR calculations show excellent agreement with Monte Carlo results. While dual-energy methods require an increased tube heat load of 2x to 4x compared to DSA, and photon-counting detectors are not yet ready for angiographic imaging, the available iodine SNR for both methods as tested is within 10% of that of conventional DSA for the same patient exposure over a wide range of patient thicknesses and iodine concentrations. Conclusions: While the energy-based methods are not necessarily optimized and further improvements are likely, the linearized noise-propagation analysis provides the theoretical framework of a level playing field for optimization studies and comparison with conventional DSA. It is concluded that both dual-energy and photon-counting approaches have the potential to provide similar angiographic image quality to DSA.

  11. Phase-based x-ray scattering—A possible method to detect cancer cells in a very early stage

    SciTech Connect (OSTI)

    Feye-Treimer, U. Treimer, W.

    2014-05-15

    Purpose: This theoretical work contains a detailed investigation of the potential and sensitivity of phase-based x-ray scattering for cancer detection in biopsies if cancer is in a very early stage of development. Methods: Cancer cells in their early stage of development differ from healthy ones mainly due to their faster growing cell nuclei and the enlargement of their densities. This growth is accompanied by an altered nucleus–plasma relation for the benefit of the cell nuclei, that changes the physical properties especially the index of refraction of the cell and the one of the cell nuclei. Interaction of radiation with matter is known to be highly sensitive to small changes of the index of refraction of matter; therefore a detection of such changes of volume and density of cell nuclei by means of high angular resolved phase-based scattering of x rays might provide a technique to distinguish malignant cells from healthy ones ifthe cell–cell nucleus system is considered as a coherent phase shifting object. Then one can observe from a thin biopsy which represents a monolayer of cells (no multiple scattering) that phase-based x-ray scattering curves from healthy cells differ from those of cancer cells in their early stage of development. Results: Detailed calculations of x-ray scattering patterns from healthy and cancer cell nuclei yield graphs and numbers with which one can distinguish healthy cells from cancer ones, taking into account that both kinds of cells occur in a tissue within a range of size and density. One important result is the role and the influence of the (lateral) coherence width of the radiation on the scattering curves and the sensitivity of phase-based scattering for cancer detection. A major result is that a larger coherence width yields a larger sensitivity for cancer detection. Further import results are calculated limits for critical sizes and densities of cell nuclei in order to attribute the investigated tissue to be healthy or diseased. Conclusions: With this proposed method it should be in principle possible to detect cancer cells in apparently healthy tissues in biopsies and/or in samples of the far border region of abscised or excised tissues. Thus this method could support established methods in diagnostics of cancer-suspicious samples.

  12. High speed optical and X-ray methods for evaluating laser-generated shock-wave in materials

    SciTech Connect (OSTI)

    Paisley, D.; Swift, D.

    2000-11-01

    Optical diagnostic techniques including interferometry, electronic streak photography, and transient x-ray diffraction are used to study the dynamic material response to shock loading by direct laser irradiation and impact by laser-launched plates. The Los Alamos Trident laser is one of several lasers that have been used to generate shocks of 10 Kbar to several Mbar in single crystal and polycrystalline materials. Incorporating optical velocity interferometry (line-VISAR and point-VISAR) with transient x-ray diffraction can provide a complete understanding of the dynamic material response to shock compression and release. Laser-launched flyer plates provide an ideal method to generate one-dimensional shocks in materials. The quality of the one-dimensionality of the launch and acceleration of plates is evaluated by line-imaging VISA.R. The line-imaging VISAR images the fringes along a line across the diameter of the plate. Each fringe maxima and minima provide acceleration and velocity information at the specific point on the plate. By varying the fringe constant number of fringes and fringe spacing on the plate, detailed experimental data can be obtained. For our experiments, most plates are 3-mm diameter and accelerated to 0.2-->6 km/sec.

  13. Methods for assisting recovery of damaged brain and spinal cord using arrays of X-Ray microplanar beams

    DOE Patents [OSTI]

    Dilmanian, F. Avraham (Yaphank, NY); McDonald, III, John W. (Baltimore, MD)

    2007-12-04

    A method of assisting recovery of an injury site of brain or spinal cord injury includes providing a therapeutic dose of X-ray radiation to the injury site through an array of parallel microplanar beams. The dose at least temporarily removes regeneration inhibitors from the irradiated regions. Substantially unirradiated cells surviving between the microplanar beams migrate to the in-beam irradiated portion and assist in recovery. The dose may be administered in dose fractions over several sessions, separated in time, using angle-variable intersecting microbeam arrays (AVIMA). Additional doses may be administered by varying the orientation of the microplanar beams. The method may be enhanced by injecting stem cells into the injury site.

  14. Methods for assisting recovery of damaged brain and spinal cord using arrays of X-ray microplanar beams

    DOE Patents [OSTI]

    Dilmanian, F. Avraham; McDonald, III, John W.

    2007-01-02

    A method of assisting recovery of an injury site of brain or spinal cord injury includes providing a therapeutic dose of X-ray radiation to the injury site through an array of parallel microplanar beams. The dose at least temporarily removes regeneration inhibitors from the irradiated regions. Substantially unirradiated cells surviving between the microplanar beams migrate to the in-beam irradiated portion and assist in recovery. The dose may be administered in dose fractions over several sessions, separated in time, using angle-variable intersecting microbeam arrays (AVIMA). Additional doses may be administered by varying the orientation of the microplanar beams. The method may be enhanced by injecting stem cells into the injury site.

  15. Toward an organ based dose prescription method for the improved accuracy of murine dose in orthovoltage x-ray irradiators

    SciTech Connect (OSTI)

    Belley, Matthew D.; Wang, Chu [Medical Physics Graduate Program, Duke University Medical Center, Durham, North Carolina 27705 (United States)] [Medical Physics Graduate Program, Duke University Medical Center, Durham, North Carolina 27705 (United States); Nguyen, Giao; Gunasingha, Rathnayaka [Duke Radiation Dosimetry Laboratory, Duke University Medical Center, Durham, North Carolina 27710 (United States)] [Duke Radiation Dosimetry Laboratory, Duke University Medical Center, Durham, North Carolina 27710 (United States); Chao, Nelson J. [Department of Medicine, Duke University Medical Center, Durham, North Carolina 27710 and Department of Immunology, Duke University Medical Center, Durham, North Carolina 27710 (United States)] [Department of Medicine, Duke University Medical Center, Durham, North Carolina 27710 and Department of Immunology, Duke University Medical Center, Durham, North Carolina 27710 (United States); Chen, Benny J. [Department of Medicine, Duke University Medical Center, Durham, North Carolina 27710 (United States)] [Department of Medicine, Duke University Medical Center, Durham, North Carolina 27710 (United States); Dewhirst, Mark W. [Department of Radiation Oncology, Duke University Medical Center, Durham, North Carolina 27710 (United States)] [Department of Radiation Oncology, Duke University Medical Center, Durham, North Carolina 27710 (United States); Yoshizumi, Terry T., E-mail: terry.yoshizumi@duke.edu [Duke Radiation Dosimetry Laboratory, Duke University Medical Center, Durham, North Carolina 27710 (United States); Department of Radiology, Duke University Medical Center, Durham, North Carolina 27710 (United States); Department of Radiation Oncology, Duke University Medical Center, Durham, North Carolina 27710 (United States)

    2014-03-15

    Purpose: Accurate dosimetry is essential when irradiating mice to ensure that functional and molecular endpoints are well understood for the radiation dose delivered. Conventional methods of prescribing dose in mice involve the use of a single dose rate measurement and assume a uniform average dose throughout all organs of the entire mouse. Here, the authors report the individual average organ dose values for the irradiation of a 12, 23, and 33 g mouse on a 320 kVp x-ray irradiator and calculate the resulting error from using conventional dose prescription methods. Methods: Organ doses were simulated in the Geant4 application for tomographic emission toolkit using the MOBY mouse whole-body phantom. Dosimetry was performed for three beams utilizing filters A (1.65 mm Al), B (2.0 mm Al), and C (0.1 mm Cu + 2.5 mm Al), respectively. In addition, simulated x-ray spectra were validated with physical half-value layer measurements. Results: Average doses in soft-tissue organs were found to vary by as much as 23%–32% depending on the filter. Compared to filters A and B, filter C provided the hardest beam and had the lowest variation in soft-tissue average organ doses across all mouse sizes, with a difference of 23% for the median mouse size of 23 g. Conclusions: This work suggests a new dose prescription method in small animal dosimetry: it presents a departure from the conventional approach of assigninga single dose value for irradiation of mice to a more comprehensive approach of characterizing individual organ doses to minimize the error and uncertainty. In human radiation therapy, clinical treatment planning establishes the target dose as well as the dose distribution, however, this has generally not been done in small animal research. These results suggest that organ dose errors will be minimized by calibrating the dose rates for all filters, and using different dose rates for different organs.

  16. Absolute x-ray energy calibration over a wide energy range using a diffraction-based iterative method

    E-Print Network [OSTI]

    Duffy, Thomas S.

    Mineral Physics Institute, Stony Brook University, Stony Brook, New York 11794, USA 2 DepartmentAbsolute x-ray energy calibration over a wide energy range using a diffraction-based iterative;REVIEW OF SCIENTIFIC INSTRUMENTS 83, 063901 (2012) Absolute x-ray energy calibration over a wide energy

  17. Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Miaja-Avila, L.; O'Neil, G. C.; Uhlig, J.; Cromer, C. L.; Dowell, M. L.; Jimenez, R.; Hoover, A. S.; Silverman, K. L.; Ullom, J. N.

    2015-03-02

    We describe a laser-driven x-ray plasma source designed for ultrafast x-ray absorption spectroscopy. The source is comprised of a 1 kHz, 20 W, femtosecond pulsed infrared laser and a water target. We present the x-ray spectra as a function of laser energy and pulse duration. Additionally, we investigate the plasma temperature and photon flux as we vary the laser energy. We obtain a 75 ?m FWHM x-ray spot size, containing ~106 photons/s, by focusing the produced x-rays with a polycapillary optic. Since the acquisition of x-ray absorption spectra requires the averaging of measurements from >107 laser pulses, we also presentmore »data on the source stability, including single pulse measurements of the x-ray yield and the x-ray spectral shape. In single pulse measurements, the x-ray flux has a measured standard deviation of 8%, where the laser pointing is the main cause of variability. Further, we show that the variability in x-ray spectral shape from single pulses is low, thus justifying the combining of x-rays obtained from different laser pulses into a single spectrum. Finally, we show a static x-ray absorption spectrum of a ferrioxalate solution as detected by a microcalorimeter array. Altogether, our results demonstrate that this water-jet based plasma source is a suitable candidate for laboratory-based time-resolved x-ray absorption spectroscopy experiments.« less

  18. X-ray emission from O stars

    E-Print Network [OSTI]

    David H. Cohen

    2008-02-01

    Young O stars are strong, hard, and variable X-ray sources, properties which strongly affect their circumstellar and galactic environments. After ~1 Myr, these stars settle down to become steady sources of soft X-rays. I use high-resolution X-ray spectroscopy and MHD modeling to show that young O stars like theta-1 Ori C are well explained by the magnetically channeled wind shock scenario. After their magnetic fields dissipate, older O stars produce X-rays via shock heating in their unstable stellar winds. Here too I use X-ray spectroscopy and numerical modeling to confirm this scenario. In addition to elucidating the nature and cause of the O star X-ray emission, modeling of the high-resolution X-ray spectra of O supergiants provides strong evidence that mass-loss rates of these O stars have been overestimated.

  19. X-ray microscopy. Beyond ensemble averages

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ice, Gene E.; Budai, John D.

    2015-06-23

    This work exemplifies emerging tools to characterize local materials structure and dynamics, made possible by powerful X-ray synchrotron and transmission electron microscopy methods.

  20. Method and apparatus for enhanced sensitivity filmless medical x-ray imaging, including three-dimensional imaging

    DOE Patents [OSTI]

    Parker, Sherwood (Berkeley, CA)

    1995-01-01

    A filmless X-ray imaging system includes at least one X-ray source, upper and lower collimators, and a solid-state detector array, and can provide three-dimensional imaging capability. The X-ray source plane is distance z.sub.1 above upper collimator plane, distance z.sub.2 above the lower collimator plane, and distance z.sub.3 above the plane of the detector array. The object to be X-rayed is located between the upper and lower collimator planes. The upper and lower collimators and the detector array are moved horizontally with scanning velocities v.sub.1, v.sub.2, v.sub.3 proportional to z.sub.1, z.sub.2 and z.sub.3, respectively. The pattern and size of openings in the collimators, and between detector positions is proportional such that similar triangles are always defined relative to the location of the X-ray source. X-rays that pass through openings in the upper collimator will always pass through corresponding and similar openings in the lower collimator, and thence to a corresponding detector in the underlying detector array. Substantially 100% of the X-rays irradiating the object (and neither absorbed nor scattered) pass through the lower collimator openings and are detected, which promotes enhanced sensitivity. A computer system coordinates repositioning of the collimators and detector array, and X-ray source locations. The computer system can store detector array output, and can associate a known X-ray source location with detector array output data, to provide three-dimensional imaging. Detector output may be viewed instantly, stored digitally, and/or transmitted electronically for image viewing at a remote site.

  1. Method and apparatus for enhanced sensitivity filmless medical x-ray imaging, including three-dimensional imaging

    DOE Patents [OSTI]

    Parker, S.

    1995-10-24

    A filmless X-ray imaging system includes at least one X-ray source, upper and lower collimators, and a solid-state detector array, and can provide three-dimensional imaging capability. The X-ray source plane is distance z{sub 1} above upper collimator plane, distance z{sub 2} above the lower collimator plane, and distance z{sub 3} above the plane of the detector array. The object to be X-rayed is located between the upper and lower collimator planes. The upper and lower collimators and the detector array are moved horizontally with scanning velocities v{sub 1}, v{sub 2}, v{sub 3} proportional to z{sub 1}, z{sub 2} and z{sub 3}, respectively. The pattern and size of openings in the collimators, and between detector positions is proportional such that similar triangles are always defined relative to the location of the X-ray source. X-rays that pass through openings in the upper collimator will always pass through corresponding and similar openings in the lower collimator, and thence to a corresponding detector in the underlying detector array. Substantially 100% of the X-rays irradiating the object (and neither absorbed nor scattered) pass through the lower collimator openings and are detected, which promotes enhanced sensitivity. A computer system coordinates repositioning of the collimators and detector array, and X-ray source locations. The computer system can store detector array output, and can associate a known X-ray source location with detector array output data, to provide three-dimensional imaging. Detector output may be viewed instantly, stored digitally, and/or transmitted electronically for image viewing at a remote site. 5 figs.

  2. X-ray Observations of Mrk 231

    E-Print Network [OSTI]

    T. J. Turner

    1998-08-10

    This paper presents new X-ray observations of Mrk 231, an active galaxy of particular interest due to its large infrared luminosity and the presence of several blueshifted broad absorption line (BAL) systems, a phenomenon observed in a small fraction of QSOs. A ROSAT HRI image of Mrk 231 is presented, this shows an extended region of soft X-ray emission, covering several tens of kpc, consistent with the extent of the host galaxy. An ASCA observation of Mrk 231 is also presented. Hard X-rays are detected but the data show no significant variability in X-ray flux. The hard X-ray continuum is heavily attenuated and X-ray column estimates range from ~ 2 x 10^{22} - 10^{23} cm^{-2} depending on whether the material is assumed to be neutral or ionized, and on the model assumed for the extended X-ray component. These ASCA data provide only the second hard X-ray spectrum of a BAL AGN presented to date. The broad-band spectral-energy-distribution of the source is discussed. While Mrk 231 is X-ray weak compared to Seyfert 1 galaxies, it has an optical-to-X-ray spectrum typical of a QSO.

  3. Standard test method for uranium analysis in natural and waste water by X-ray fluorescence

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2004-01-01

    1.1 This test method applies for the determination of trace uranium content in waste water. It covers concentrations of U between 0.05 mg/L and 2 mg/L. 1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  4. Hard x-ray broad band Laue lenses (80 - 600 keV): building methods and performances

    E-Print Network [OSTI]

    Virgilli, E; Rosati, P; Liccardo, V; Squerzanti, S; Carassiti, V; Caroli, E; Auricchio, N; Stephen, J B

    2015-01-01

    We present the status of the laue project devoted to develop a technology for building a 20 meter long focal length Laue lens for hard x-/soft gamma-ray astronomy (80 - 600 keV). The Laue lens is composed of bent crystals of Gallium Arsenide (GaAs, 220) and Germanium (Ge, 111), and, for the first time, the focusing property of bent crystals has been exploited for this field of applications. We show the preliminary results concerning the adhesive employed to fix the crystal tiles over the lens support, the positioning accuracy obtained and possible further improvements. The Laue lens petal that will be completed in a few months has a pass band of 80 - 300 keV and is a fraction of an entire Laue lens capable of focusing X-rays up to 600 keV, possibly extendable down to 20 - 30 keV with suitable low absorption crystal materials and focal length. The final goal is to develop a focusing optics that can improve the sensitivity over current telescopes in this energy band by 2 orders of magnitude.

  5. Spatiotemporal Monte Carlo transport methods in x-ray semiconductor detectors: Application to pulse-height spectroscopy in a-Se

    SciTech Connect (OSTI)

    Fang Yuan; Badal, Andreu; Allec, Nicholas; Karim, Karim S.; Badano, Aldo

    2012-01-15

    Purpose: The authors describe a detailed Monte Carlo (MC) method for the coupled transport of ionizing particles and charge carriers in amorphous selenium (a-Se) semiconductor x-ray detectors, and model the effect of statistical variations on the detected signal. Methods: A detailed transport code was developed for modeling the signal formation process in semiconductor x-ray detectors. The charge transport routines include three-dimensional spatial and temporal models of electron-hole pair transport taking into account recombination and trapping. Many electron-hole pairs are created simultaneously in bursts from energy deposition events. Carrier transport processes include drift due to external field and Coulombic interactions, and diffusion due to Brownian motion. Results: Pulse-height spectra (PHS) have been simulated with different transport conditions for a range of monoenergetic incident x-ray energies and mammography radiation beam qualities. Two methods for calculating Swank factors from simulated PHS are shown, one using the entire PHS distribution, and the other using the photopeak. The latter ignores contributions from Compton scattering and K-fluorescence. Comparisons differ by approximately 2% between experimental measurements and simulations. Conclusions: The a-Se x-ray detector PHS responses simulated in this work include three-dimensional spatial and temporal transport of electron-hole pairs. These PHS were used to calculate the Swank factor and compare it with experimental measurements. The Swank factor was shown to be a function of x-ray energy and applied electric field. Trapping and recombination models are all shown to affect the Swank factor.

  6. Chest x-Rays

    Broader source: Energy.gov [DOE]

    The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica.

  7. X-ray beamsplitter

    DOE Patents [OSTI]

    Ceglio, Natale M. (Livermore, CA); Stearns, Daniel S. (Mountain View, CA); Hawryluk, Andrew M. (Modesto, CA); Barbee, Jr., Troy W. (Palo Alto, CA)

    1989-01-01

    An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

  8. X-ray beamsplitter

    DOE Patents [OSTI]

    Ceglio, N.M.; Stearns, D.G.; Hawryluk, A.M.; Barbee, T.W. Jr.

    1987-08-07

    An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5--50 pairs of alternate Mo/Si layers with a period of 20--250 A. The support membrane is 10--200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window. 6 figs.

  9. Compound refractive X-ray lens

    DOE Patents [OSTI]

    Nygren, David R. (Berkeley, CA); Cahn, Robert (Walnut Creek, CA); Cederstrom, Bjorn (Traellborg, SE); Danielsson, Mats (Stocksund, SE); Vestlund, Jonas (Stockholm, SE)

    2000-01-01

    An apparatus and method for focusing X-rays. In one embodiment, his invention is a commercial-grade compound refractive X-ray lens. The commercial-grade compound refractive X-ray lens includes a volume of low-Z material. The volume of low-Z material has a first surface which is adapted to receive X-rays of commercially-applicable power emitted from a commercial-grade X-ray source. The volume of low-Z material also has a second surface from which emerge the X-rays of commercially-applicable power which were received at the first surface. Additionally, the commercial-grade compound refractive X-ray lens includes a plurality of openings which are disposed between the first surface and the second surface. The plurality of openings are oriented such that the X-rays of commercially-applicable power which are received at the first surface, pass through the volume of low-Z material and through the plurality openings. In so doing, the X-rays which emerge from the second surface are refracted to a focal point.

  10. X-ray laser

    DOE Patents [OSTI]

    Nilsen, Joseph (Livermore, CA)

    1991-01-01

    An X-ray laser (10) that lases between the K edges of carbon and oxygen, i.e. between 44 and 23 Angstroms, is provided. The laser comprises a silicon (12) and dysprosium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state nickel-like dysprosium ions (34) are resonantly photo-pumped to their upper X-ray laser state by line emission from hydrogen-like silicon ions (32). The novel X-ray laser should prove especially useful for the microscopy of biological specimens.

  11. Quantitative characterization of the protein contents of the exocrine pancreatic acinar cell by soft x-ray microscopy and advanced digital imaging methods

    SciTech Connect (OSTI)

    Loo Jr., Billy W.

    2000-06-09

    The study of the exocrine pancreatic acinar cell has been central to the development of models of many cellular processes, especially of protein transport and secretion. Traditional methods used to examine this system have provided a wealth of qualitative information from which mechanistic models have been inferred. However they have lacked the ability to make quantitative measurements, particularly of the distribution of protein in the cell, information critical for grounding of models in terms of magnitude and relative significance. This dissertation describes the development and application of new tools that were used to measure the protein content of the major intracellular compartments in the acinar cell, particularly the zymogen granule. Soft x-ray microscopy permits image formation with high resolution and contrast determined by the underlying protein content of tissue rather than staining avidity. A sample preparation method compatible with x-ray microscopy was developed and its properties evaluated. Automatic computerized methods were developed to acquire, calibrate, and analyze large volumes of x-ray microscopic images of exocrine pancreatic tissue sections. Statistics were compiled on the protein density of several organelles, and on the protein density, size, and spatial distribution of tens of thousands of zymogen granules. The results of these measurements, and how they compare to predictions of different models of protein transport, are discussed.

  12. Transient x-ray diffraction and its application to materials science and x-ray optics

    SciTech Connect (OSTI)

    Hauer, A.A.; Kopp, R.; Cobble, J.; Kyrala, G.; Springer, R.

    1997-12-01

    Time resolved x-ray diffraction and scattering have been applied to the measurement of a wide variety of physical phenomena from chemical reactions to shock wave physics. Interest in this method has heightened in recent years with the advent of versatile, high power, pulsed x-ray sources utilizing laser plasmas, electron beams and other methods. In this article, we will describe some of the fundamentals involved in time resolved x-ray diffraction, review some of the history of its development, and describe some recent progress in the field. In this article we will emphasize the use of laser-plasmas as the x-ray source for transient diffraction.

  13. System for phase-contrast x-ray radiography using X pinch radiation and a method thereof

    DOE Patents [OSTI]

    Chandler, Katherine (Ithaca, NY); Chelkovenko, Tatiana (Moscow, RU); Hammer, David (Ithaca, NY); Pikuz, Sergei (Moscow, RU); Sinars, Daniel (Albuquerque, NM); Song, Byungmoo (Ithaca, NY)

    2007-11-06

    A radiograph system with an anode plate, a cathode plate, and a power source coupled to said anode plate and the cathode plate. At least two wires coupled between the anode plate and the cathode plate provide a configuration to form an X-pinch having a photon source size of less than five microns at energies above 2.5 keV. Material at the configuration forming the X-pinch vaporizes upon application of a suitable current to the wires forming a dense hot plasma and emitting a single x-ray pulse with sufficient photons having energies in the range of from about 2.5 keV to about 20 keV to provide a phase contrast image of an object in the path of the photons. Multiple simultaneous images may be formed of a plurality of objects. Suitable filters and x-ray detectors are provided.

  14. Analysis of Order Formation in Block Copolymer Thin Films Using Resonant Soft X-Ray Scattering

    E-Print Network [OSTI]

    Virgili, Justin M.; Tao, Yuefei; Kortright, Jeffrey B.; Balsara, Nitash P.; Segalman, Rachel A.

    2006-01-01

    Methods of X-Ray and Neutron Scattering in Polymer Science.µ t for X-ray and neutron scattering experiments is unity;18 In classical scattering of light, X-rays or neutrons the

  15. X-ray scattering studies of structure and dynamics of surfaces and interfaces of polymeric liquids

    E-Print Network [OSTI]

    Jiang, Zhang

    2007-01-01

    Evanescent X-ray and Neutron Scattering. Springer-Verlag,Methods of X-ray and neutron scattering in polymer science.Stanley. X-ray and neutron scattering from rough surfaces.

  16. COMBINING CLASSIFIERS FOR BONE FRACTURE DETECTION IN X-RAY IMAGES Vineta Lai Fun Lum, Wee Kheng Leow, Ying Chen,

    E-Print Network [OSTI]

    Leow, Wee Kheng

    COMBINING CLASSIFIERS FOR BONE FRACTURE DETECTION IN X-RAY IMAGES Vineta Lai Fun Lum, Wee Kheng combination methods ap- plied to the detection of bone fractures in x-ray images. Test results show, only about 12% of them contained fractured femurs. For radius images, about 30% of 145 consecu- tive

  17. X-ray microtomography

    SciTech Connect (OSTI)

    Landis, Eric N.; Keane, Denis T.

    2010-12-15

    In this tutorial, we describe X-ray microtomography as a technique to nondestructively characterize material microstructure in three dimensions at a micron level spatial resolution. While commercially available laboratory scale instrumentation is available, we focus our attention on synchrotron-based systems, where we can exploit a high flux, monochromatic X-ray beam to produce high fidelity three-dimensional images. A brief description of the physics and the mathematical analysis behind the technique is followed by example applications to specific materials characterization problems, with a particular focus on the utilization of three-dimensional image processing that can be used to extract a wide range of useful information.

  18. X-Ray Data Booklet X-RAY DATA BOOKLET

    E-Print Network [OSTI]

    X-Ray Data Booklet X-RAY DATA BOOKLET Center for X-ray Optics and Advanced Light Source Lawrence Electromagnetic Relations Radioactivity and Radiation Protection Useful Formulas CXRO Home | ALS Home | LBL Home in PDF format Data Booklet Authors CXRO Home | ALS Home | LBL Home Privacy and Security Notice Please

  19. Crystal defect studies using x-ray diffuse scattering

    SciTech Connect (OSTI)

    Larson, B.C.

    1980-01-01

    Microscopic lattice defects such as point (single atom) defects, dislocation loops, and solute precipitates are characterized by local electronic density changes at the defect sites and by distortions of the lattice structure surrounding the defects. The effect of these interruptions of the crystal lattice on the scattering of x-rays is considered in this paper, and examples are presented of the use of the diffuse scattering to study the defects. X-ray studies of self-interstitials in electron irradiated aluminum and copper are discussed in terms of the identification of the interstitial configuration. Methods for detecting the onset of point defect aggregation into dislocation loops are considered and new techniques for the determination of separate size distributions for vacancy loops and interstitial loops are presented. Direct comparisons of dislocation loop measurements by x-rays with existing electron microscopy studies of dislocation loops indicate agreement for larger size loops, but x-ray measurements report higher concentrations in the smaller loop range. Methods for distinguishing between loops and three-dimensional precipitates are discussed and possibilities for detailed studies considered. A comparison of dislocation loop size distributions obtained from integral diffuse scattering measurements with those from TEM show a discrepancy in the smaller sizes similar to that described above.

  20. Coherent x-ray diffraction imaging of paint pigmentparticles by scanning a phase plate modulator

    SciTech Connect (OSTI)

    Chu Y. S.; Chen B.; Zhang F.; Berenguer F.; Bean R.; Kewish C.; Vila-Comamala J.; Rodenburg J.; Robinson I.

    2011-10-19

    We have implemented a coherent x-ray diffraction imaging technique that scans a phase plate to modulate wave-fronts of the x-ray beam transmitted by samples. The method was applied to measure a decorative alkyd paint containing iron oxide red pigment particles. By employing an iterative algorithm for wave-front modulation phase retrieval, we obtained an image of the paint sample that shows the distribution of the pigment particles and is consistent with the result obtained from a transmission x-ray microscope. The technique has been experimentally proven to be a feasible coherent x-ray imaging method with about 120 nm spatial resolution and was shown to work well with industrially relevant specimens.

  1. TV-based conjugate gradient method and discrete L-curve for few-view CT reconstruction of X-ray in vivo data

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Yang, Xiaoli; Hofmann, Ralf; Dapp, Robin; van de Kamp, Thomas; Rolo, Tomy dos Santos; Xiao, Xianghui; Moosmann, Julian; Kashef, Jubin; Stotzka, Rainer

    2015-01-01

    High-resolution, three-dimensional (3D) imaging of soft tissues requires the solution of two inverse problems: phase retrieval and the reconstruction of the 3D image from a tomographic stack of two-dimensional (2D) projections. The number of projections per stack should be small to accommodate fast tomography of rapid processes and to constrain X-ray radiation dose to optimal levels to either increase the duration o fin vivo time-lapse series at a given goal for spatial resolution and/or the conservation of structure under X-ray irradiation. In pursuing the 3D reconstruction problem in the sense of compressive sampling theory, we propose to reduce the numbermore »of projections by applying an advanced algebraic technique subject to the minimisation of the total variation (TV) in the reconstructed slice. This problem is formulated in a Lagrangian multiplier fashion with the parameter value determined by appealing to a discrete L-curve in conjunction with a conjugate gradient method. The usefulness of this reconstruction modality is demonstrated for simulated and in vivo data, the latter acquired in parallel-beam imaging experiments using synchrotron radiation.« less

  2. Methods for assisting recovery of damaged brain and spinal cord and treating various diseases using arrays of x-ray microplanar beams

    DOE Patents [OSTI]

    Dilmanian, F. Avraham (Yaphank, NY); Anchel, David J. (Rocky Point, NY); Gaudette, Glenn (Holden, MA); Romanelli, Pantaleo (Monteroduni, IT); Hainfeld, James (Shoreham, NY)

    2010-06-29

    A method of assisting recovery of an injury site of the central nervous system (CNS) or treating a disease includes providing a therapeutic dose of X-ray radiation to a target volume through an array of parallel microplanar beams. The dose to treat CNS injury temporarily removes regeneration inhibitors from the irradiated site. Substantially unirradiated cells surviving between beams migrate to the in-beam portion and assist recovery. The dose may be staggered in fractions over sessions using angle-variable intersecting microbeam arrays (AVIMA). Additional doses are administered by varying the orientation of the beams. The method is enhanced by injecting stem cells into the injury site. One array or the AVIMA method is applied to ablate selected cells in a target volume associated with disease for palliative or curative effect. Atrial fibrillation is treated by irradiating the atrial wall to destroy myocardial cells while continuously rotating the subject.

  3. X-Ray Diagnostics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservationBio-Inspired SolarAbout /Two0PhotosPresentationsWorld's largest singleX-Ray

  4. Fat to muscle ratio measurements with dual energy x-ray absorbtiometry

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Chen, A.; Luo, J.; Wang, A.; Broadbent, C.; Zhong, J.; Dilmanian, F. A.; Zafonte, F.; Zhong, Z.

    2015-03-14

    Accurate measurement of the fat-to-muscle ratio in animal model is important for obesity research. In addition, an efficient way to measure the fat to muscle ratio in animal model using dual-energy absorptiometry is presented in this paper. A radioactive source exciting x-ray fluorescence from a target material is used to provide the two x-ray energies needed. The x-rays, after transmitting through the sample, are measured with an energy-sensitive Ge detector. Phantoms and specimens were measured. The results showed that the method was sensitive to the fat to muscle ratios with good linearity. A standard deviation of a few percent inmore »the fat to muscle ratio could be observed with the x-ray dose of 0.001 mGy.« less

  5. Fat to Muscle Ratio Measurements with Dual Energy X Ray Absorbtiometry

    E-Print Network [OSTI]

    Chen, A; Broadbent, C; Zhong, J; Dilmanian, A; Zafonte, F; Zhong, Z

    2014-01-01

    Accurate measurement of the fat-to-muscle ratio in animal model is important for obesity research. An efficient way to measure the fat to muscle ratio in animal model using dual-energy absorptiometry is presented in this paper. A radioactive source exciting x-ray fluorescence from a target material is used to provide the two x-ray energies needed. The x-rays, after transmitting through the sample, are measured with an energy-sensitive Ge detector. Phantoms and specimens were measured. The results showed that the method was sensitive to the fat to muscle ratios with good linearity. A standard deviation of a few percent in the fat to muscle ratio could be observed with the x-ray dose of 0.001 mGy.

  6. X-ray spectrometry

    SciTech Connect (OSTI)

    Markowicz, A.A.; Van Grieken, R.E.

    1986-04-01

    In the period under review, i.e, through 1984 and 1985, some 600 articles on XRS (X-ray spectrometry) were published; most of these have been scanned and the most fundamental ones are discussed. All references will refer to English-language articles, unless states otherwise. Also general books have appeared on quantitative EPXMA (electron-probe X-ray microanalysis) and analytical electron microscopy (AEM) as well as an extensive review on the application of XRS to trace analysis of environmental samples. In the period under review no radically new developments have been seen in XRS. However, significant improvements have been made. Gain in intensities has been achieved by more efficient excitation, higher reflectivity of dispersing media, and better geometry. Better understanding of the physical process of photon- and electron-specimen interactions led to complex but more accurate equations for correction of various interelement effects. Extensive use of micro- and minicomputers now enables fully automatic operation, including qualitative analysis. However, sample preparation and presentation still put a limit to further progress. Although some authors find XRS in the phase of stabilization or even stagnation, further gradual developments are expected, particularly toward more dedicated equipment, advanced automation, and image analysis systems. Ways are outlined in which XRS has been improved in the 2 last years by excitation, detection, instrumental, methodological, and theoretical advances. 340 references.

  7. Spatially resolved energy dispersive x-ray spectroscopic method for in-situ evaluation of mechanical properties during the growth of a C - Pt composite nanowire

    SciTech Connect (OSTI)

    Banerjee, Amit; Banerjee, S. S., E-mail: satyajit@iitk.ac.in [Department of Physics, Indian Institute of Technology Kanpur, Kanpur, 208016 (India)

    2014-05-15

    A core-shell type C-Pt composite nanowire is fabricated using focused ion and electron beam induced chemical vapor deposition techniques. Using information from spatially resolved energy dispersive x-ray spectra, we detect the resonance vibration in the C-Pt composite nanowire. We use this method to measure the Young's moduli of the constituents (C, Pt) of the composite nanowire and also estimate the density of the FEB CVD grown Pt shell surrounding the C core. By measuring the resonance characteristics of the composite nanowire we estimate a Pt shell growth rate of ?0.9 nms{sup ?1}. The study is analyzed to suggest that the Pt shell growth mechanism is primarily governed by the sticking coefficient of the organometallic vapor on the C nanowire core.

  8. X-ray lithography using holographic images

    DOE Patents [OSTI]

    Howells, M.S.; Jacobsen, C.

    1997-03-18

    Methods for forming X-ray images having 0.25 {micro}m minimum line widths on X-ray sensitive material are presented. A holographic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required. 15 figs.

  9. Miniature x-ray source

    DOE Patents [OSTI]

    Trebes, James E. (Livermore, CA); Stone, Gary F. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA); Chornenky, Victor I. (Minnetonka, MN)

    2002-01-01

    A miniature x-ray source capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature x-ray source comprises a compact vacuum tube assembly containing a cathode, an anode, a high voltage feedthru for delivering high voltage to the anode, a getter for maintaining high vacuum, a connection for an initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is highly x-ray transparent and made, for example, from boron nitride. The compact size and potential for remote operation allows the x-ray source, for example, to be placed adjacent to a material sample undergoing analysis or in proximity to the region to be treated for medical applications.

  10. X-ray transmission movies of spontaneous dynamic events

    SciTech Connect (OSTI)

    Smilowitz, L.; Henson, B. F.; Holmes, M.; Novak, A.; Oschwald, D.; Dolgonos, P.; Qualls, B.

    2014-11-15

    We describe a new x-ray radiographic imaging system which allows for continuous x-ray transmission imaging of spontaneous dynamic events. We demonstrate this method on thermal explosions in three plastic bonded formulations of the energetic material octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine. We describe the x-ray imaging system and triggering developed to enable the continuous imaging of a thermal explosion.

  11. Ultra-short wavelength x-ray system

    DOE Patents [OSTI]

    Umstadter, Donald (Ann Arbor, MI); He, Fei (Ann Arbor, MI); Lau, Yue-Ying (Potomac, MD)

    2008-01-22

    A method and apparatus to generate a beam of coherent light including x-rays or XUV by colliding a high-intensity laser pulse with an electron beam that is accelerated by a synchronized laser pulse. Applications include x-ray and EUV lithography, protein structural analysis, plasma diagnostics, x-ray diffraction, crack analysis, non-destructive testing, surface science and ultrafast science.

  12. Towards phasing using high X-ray intensity

    SciTech Connect (OSTI)

    Galli, Lorenzo; Son, Sang -Kil; Barends, Thomas R. M.; White, Thomas A.; Barty, Anton; Botha, Sabine; Boutet, Sébastien; Caleman, Carl; Doak, R. Bruce; Nanao, Max H.; Nass, Karol; Shoeman, Robert L.; Timneanu, Nicusor; Santra, Robin; Schlichting, Ilme; Chapman, Henry N.

    2015-09-30

    X-ray free-electron lasers (XFELs) show great promise for macromolecular structure determination from sub-micrometre-sized crystals, using the emerging method of serial femtosecond crystallography. The extreme brightness of the XFEL radiation can multiply ionize most, if not all, atoms in a protein, causing their scattering factors to change during the pulse, with a preferential `bleaching' of heavy atoms. This paper investigates the effects of electronic damage on experimental data collected from a Gd derivative of lysozyme microcrystals at different X-ray intensities, and the degree of ionization of Gd atoms is quantified from phased difference Fourier maps. In conclusion, a pattern sorting scheme is proposed to maximize the ionization contrast and the way in which the local electronic damage can be used for a new experimental phasing method is discussed.

  13. Towards phasing using high X-ray intensity

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Galli, Lorenzo; Son, Sang -Kil; Barends, Thomas R. M.; White, Thomas A.; Barty, Anton; Botha, Sabine; Boutet, Sébastien; Caleman, Carl; Doak, R. Bruce; Nanao, Max H.; et al

    2015-09-30

    X-ray free-electron lasers (XFELs) show great promise for macromolecular structure determination from sub-micrometre-sized crystals, using the emerging method of serial femtosecond crystallography. The extreme brightness of the XFEL radiation can multiply ionize most, if not all, atoms in a protein, causing their scattering factors to change during the pulse, with a preferential `bleaching' of heavy atoms. This paper investigates the effects of electronic damage on experimental data collected from a Gd derivative of lysozyme microcrystals at different X-ray intensities, and the degree of ionization of Gd atoms is quantified from phased difference Fourier maps. In conclusion, a pattern sorting schememore »is proposed to maximize the ionization contrast and the way in which the local electronic damage can be used for a new experimental phasing method is discussed.« less

  14. X-ray Emission from Isolated Be Stars

    E-Print Network [OSTI]

    David H. Cohen

    2000-08-22

    I discuss the X-ray observations of Be stars, and how their properties compare to non-emission B stars. I focus on several specific stars that show high flux levels and variability but also report on several interesting survey results. The Be X-ray properties are discussed in the context of wind-shock X-ray emission from normal OB stars as well as in the context of general mechanisms that have been proposed to explain the Be phenomenon. Finally, I conclude with a discussion of the spectral diagnostics that will be available from the new generation of X-ray telescopes.

  15. X-ray shearing interferometer

    DOE Patents [OSTI]

    Koch, Jeffrey A. (Livermore, CA)

    2003-07-08

    An x-ray interferometer for analyzing high density plasmas and optically opaque materials includes a point-like x-ray source for providing a broadband x-ray source. The x-rays are directed through a target material and then are reflected by a high-quality ellipsoidally-bent imaging crystal to a diffraction grating disposed at 1.times. magnification. A spherically-bent imaging crystal is employed when the x-rays that are incident on the crystal surface are normal to that surface. The diffraction grating produces multiple beams which interfere with one another to produce an interference pattern which contains information about the target. A detector is disposed at the position of the image of the target produced by the interfering beams.

  16. X-ray compass for determining device orientation

    DOE Patents [OSTI]

    Da Silva, L.B.; Matthews, D.L.; Fitch, J.P.; Everett, M.J.; Colston, B.W.; Stone, G.F.

    1999-06-15

    An apparatus and method for determining the orientation of a device with respect to an x-ray source are disclosed. In one embodiment, the present invention is coupled to a medical device in order to determine the rotational orientation of the medical device with respect to the x-ray source. In such an embodiment, the present invention is comprised of a scintillator portion which is adapted to emit photons upon the absorption of x-rays emitted from the x-ray source. An x-ray blocking portion is coupled to the scintillator portion. The x-ray blocking portion is disposed so as to vary the quantity of x-rays which penetrate the scintillator portion based upon the particular rotational orientation of the medical device with respect to the x-ray source. A photon transport mechanism is also coupled to the scintillator portion. The photon transport mechanism is adapted to pass the photons emitted from the scintillator portion to an electronics portion. By analyzing the quantity of the photons, the electronics portion determines the rotational orientation of the medical device with respect to the x-ray source. 25 figs.

  17. X-ray compass for determining device orientation

    DOE Patents [OSTI]

    Da Silva, Luiz B. (Danville, CA); Matthews, Dennis L. (Moss Beach, CA); Fitch, Joseph P. (Livermore, CA); Everett, Matthew J. (Pleasanton, CA); Colston, Billy W. (Livermore, CA); Stone, Gary F. (Livermore, CA)

    1999-01-01

    An apparatus and method for determining the orientation of a device with respect to an x-ray source. In one embodiment, the present invention is coupled to a medical device in order to determine the rotational orientation of the medical device with respect to the x-ray source. In such an embodiment, the present invention is comprised of a scintillator portion which is adapted to emit photons upon the absorption of x-rays emitted from the x-ray source. An x-ray blocking portion is coupled to the scintillator portion. The x-ray blocking portion is disposed so as to vary the quantity of x-rays which penetrate the scintillator portion based upon the particular rotational orientation of the medical device with respect to the x-ray source. A photon transport mechanism is also coupled to the scintillator portion. The photon transport mechanism is adapted to pass the photons emitted from the scintillator portion to an electronics portion. By analyzing the quantity of the photons, the electronics portion determines the rotational orientation of the medical device with respect to the x-ray source.

  18. X-ray fluorescence mapping

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorkingLos Alamos verifies largest single goldWindX-RayX-Ray ScienceX-Ray

  19. A general framework and review of scatter correction methods in x-ray cone-beam computerized tomography. Part 1: Scatter compensation approaches

    SciTech Connect (OSTI)

    Ruehrnschopf, Ernst-Peter; Klingenbeck, Klaus

    2011-07-15

    Since scattered radiation in cone-beam volume CT implies severe degradation of CT images by quantification errors, artifacts, and noise increase, scatter suppression is one of the main issues related to image quality in CBCT imaging. The aim of this review is to structurize the variety of scatter suppression methods, to analyze the common structure, and to develop a general framework for scatter correction procedures. In general, scatter suppression combines hardware techniques of scatter rejection and software methods of scatter correction. The authors emphasize that scatter correction procedures consist of the main components scatter estimation (by measurement or mathematical modeling) and scatter compensation (deterministic or statistical methods). The framework comprises most scatter correction approaches and its validity also goes beyond transmission CT. Before the advent of cone-beam CT, a lot of papers on scatter correction approaches in x-ray radiography, mammography, emission tomography, and in Megavolt CT had been published. The opportunity to avail from research in those other fields of medical imaging has not yet been sufficiently exploited. Therefore additional references are included when ever it seems pertinent. Scatter estimation and scatter compensation are typically intertwined in iterative procedures. It makes sense to recognize iterative approaches in the light of the concept of self-consistency. The importance of incorporating scatter compensation approaches into a statistical framework for noise minimization has to be underscored. Signal and noise propagation analysis is presented. A main result is the preservation of differential-signal-to-noise-ratio (dSNR) in CT projection data by ideal scatter correction. The objective of scatter compensation methods is the restoration of quantitative accuracy and a balance between low-contrast restoration and noise reduction. In a synopsis section, the different deterministic and statistical methods are discussed with respect to their properties and applications. The current paper is focused on scatter compensation algorithms. The multitude of scatter estimation models will be dealt with in a separate paper.

  20. In-situ energy dispersive x-ray diffraction study of the growth of CuO nanowires by annealing method

    SciTech Connect (OSTI)

    Srivastava, Himanshu; Ganguli, Tapas; Deb, S. K.; Sant, Tushar; Poswal, H. K.; Sharma, Surinder M.

    2013-10-14

    The in-situ growth of CuO nanowires was studied by Energy Dispersive X-ray Diffraction (EDXRD) to observe the mechanism of growth. The study was carried out for comparison at two temperatures—at 500 °C, the optimum temperature of the nanowires growth, and at 300 °C just below the temperature range of the growth. The in situ observation revealed the successive oxidation of Cu foil to Cu{sub 2}O layer and finally to CuO layer. Further analysis showed the presence of a compressive stress in CuO layer due to interface at CuO and Cu{sub 2}O layers. The compressive stress was found to increase with the growth of the nanowires at 500 °C while it relaxed with the growth of CuO layer at 300 °C. The present results do not support the existing model of stress relaxation induced growth of nanowires. Based on the detailed Transmission Electron Microscope, Scanning Electron Microscope, and EDXRD results, a microstructure based growth model has been suggested.

  1. Center for X-Ray Optics, 1992

    SciTech Connect (OSTI)

    Not Available

    1993-08-01

    This report discusses the following topics: Center for X-Ray Optics; Soft X-Ray Imaging wit Zone Plate Lenses; Biological X-Ray microscopy; Extreme Ultraviolet Lithography for Nanoelectronic Pattern Transfer; Multilayer Reflective Optics; EUV/Soft X-ray Reflectometer; Photoemission Microscopy with Reflective Optics; Spectroscopy with Soft X-Rays; Hard X-Ray Microprobe; Coronary Angiography; and Atomic Scattering Factors.

  2. Method and apparatus for combinatorial logic signal processor in a digitally based high speed x-ray spectrometer

    DOE Patents [OSTI]

    Warburton, William K. (1300 Mills St., Menlo Park, CA 94025); Zhou, Zhiquing (Carl) (Fremont, CA)

    1999-01-01

    A high speed, digitally based, signal processing system which accepts a digitized input signal and detects the presence of step-like pulses in the this data stream, extracts filtered estimates of their amplitudes, inspects for pulse pileup, and records input pulse rates and system livetime. The system has two parallel processing channels: a slow channel, which filters the data stream with a long time constant trapezoidal filter for good energy resolution; and a fast channel which filters the data stream with a short time constant trapezoidal filter, detects pulses, inspects for pileups, and captures peak values from the slow channel for good events. The presence of a simple digital interface allows the system to be easily integrated with a digital processor to produce accurate spectra at high count rates and allow all spectrometer functions to be fully automated. Because the method is digitally based, it allows pulses to be binned based on time related values, as well as on their amplitudes, if desired.

  3. Multiple wavelength X-ray monochromators

    DOE Patents [OSTI]

    Steinmeyer, P.A.

    1992-11-17

    An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focusing the separate first and second output x-ray radiation wavelengths into separate focal points. 3 figs.

  4. Multiple wavelength X-ray monochromators

    DOE Patents [OSTI]

    Steinmeyer, Peter A. (Arvada, CO)

    1992-11-17

    An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focussing the separate first and second output x-ray radiation wavelengths into separate focal points.

  5. Miniature x-ray source

    DOE Patents [OSTI]

    Trebes, James E. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA)

    2000-01-01

    A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

  6. Automated suppression of errors in LTP-II slope measurements with x-ray optics

    E-Print Network [OSTI]

    Ali, Zulfiqar

    2012-01-01

    precise reflective X-ray optics,” Nucl. Instrum. and Methods70 (2001). [2] P. Z. Takacs, “X- ray optics metrology,” in [Handbook of Optics], 3rd ed. , Vol. V, M. Bass, Ed. ,

  7. X-ray lasers and methods utilizing two component driving illumination provided by optical laser means of relatively low energy and small physical size

    DOE Patents [OSTI]

    Rosen, Mordecai D. (Berkeley, CA); Matthews, Dennis L. (El Granada, CA)

    1991-01-01

    An X-ray laser (10), and related methodology, are disclosed wherein an X-ray laser target (12) is illuminated with a first pulse of optical laser radiation (14) of relatively long duration having scarcely enough energy to produce a narrow and linear cool plasma of uniform composition (38). A second, relatively short pulse of optical laser radiation (18) is uniformly swept across the length, from end to end, of the plasma (38), at about the speed of light, to consecutively illuminate continuously succeeding portions of the plasma (38) with optical laser radiation having scarcely enough energy to heat, ionize, and invert them into the continuously succeeding portions of an X-ray gain medium. This inventive double pulse technique results in a saving of more than two orders of magnitude in driving optical laser energy, when compared to the conventional single pulse approach.

  8. Use of soft x-ray diagnostic on the COMPASS tokamak for investigations of sawteeth crash neighborhood and of plasma position using fast inversion methods

    SciTech Connect (OSTI)

    Imrisek, M. [Institute of Plasma Physics ASCR, Prague (Czech Republic); Faculty of Mathematics and Physics, Charles University in Prague, Prague (Czech Republic); Weinzettl, V.; Mlynar, J.; Panek, R.; Hron, M. [Institute of Plasma Physics ASCR, Prague (Czech Republic); Odstrcil, T. [Max-Planck-Institut für Plasmaphysik, Garching (Germany); Odstrcil, M. [Faculty of Nuclear Sciences and Physical Engineering, Czech Technical University in Prague, Prague (Czech Republic); Optical Research Center, University of Southampton, Southampton (United Kingdom); Ficker, O. [Faculty of Nuclear Sciences and Physical Engineering, Czech Technical University in Prague, Prague (Czech Republic); Pinzon, J. R. [Institue Jean Lamour, Université de Lorraine, Nancy (France); Ehrlacher, C. [ENS Cachan, Paris (France)

    2014-11-15

    The soft x-ray diagnostic is suitable for monitoring plasma activity in the tokamak core, e.g., sawtooth instability. Moreover, spatially resolved measurements can provide information about plasma position and shape, which can supplement magnetic measurements. In this contribution, fast algorithms with the potential for a real-time use are tested on the data from the COMPASS tokamak. In addition, the soft x-ray data are compared with data from other diagnostics in order to discuss possible connection between sawtooth instability on one side and the transition to higher confinement mode, edge localized modes and productions of runaway electrons on the other side.

  9. Nuclear Instruments and Methods in Physics Research A 514 (2003) 206214 A silicon strip detector coupled to the RX64 ASIC for X-ray

    E-Print Network [OSTI]

    Ramello, Luciano

    2003-01-01

    , such as mammography and angiography at the iodine K-edge, the dual energy technique [3] makes it possible to isolate. The system is capable of single photon counting in digital X-ray imaging, with possible applications to dual energy mammography and angiography. The main features of the detecting system are low noise, good spatial

  10. High-Resolution Soft X-Ray Spectral Analysis in the CK Region of Titanium Carbide (TiC) using the DV-X alpha Molecular Orbital Method

    E-Print Network [OSTI]

    Shimomura, Kenta

    2010-01-01

    1 XRD pattern of the measured TiC powder sample. Figure 2XAS. Intensity (arb. units) TiC X-ray: Cu K? voltage: 40 kVintensity (arb. units) CK-XES TiC b a c HOPG e f CK-XAS TiC

  11. Noise variance analysis using a flat panel x-ray detector: A method for additive noise assessment with application to breast CT applications

    SciTech Connect (OSTI)

    Yang Kai; Huang, Shih-Ying; Packard, Nathan J.; Boone, John M. [Department of Radiology, University of California, Davis Medical Center, 4860 Y Street, Suite 3100 Ellison Building, Sacramento, California 95817 (United States); Department of Radiology, University of California, Davis Medical Center, 4860 Y Street, Suite 3100 Ellison Building, Sacramento, California 95817 (United States) and Department of Biomedical Engineering, University of California, Davis, Davis, California, 95616 (United States)

    2010-07-15

    Purpose: A simplified linear model approach was proposed to accurately model the response of a flat panel detector used for breast CT (bCT). Methods: Individual detector pixel mean and variance were measured from bCT projection images acquired both in air and with a polyethylene cylinder, with the detector operating in both fixed low gain and dynamic gain mode. Once the coefficients of the linear model are determined, the fractional additive noise can be used as a quantitative metric to evaluate the system's efficiency in utilizing x-ray photons, including the performance of different gain modes of the detector. Results: Fractional additive noise increases as the object thickness increases or as the radiation dose to the detector decreases. For bCT scan techniques on the UC Davis prototype scanner (80 kVp, 500 views total, 30 frames/s), in the low gain mode, additive noise contributes 21% of the total pixel noise variance for a 10 cm object and 44% for a 17 cm object. With the dynamic gain mode, additive noise only represents approximately 2.6% of the total pixel noise variance for a 10 cm object and 7.3% for a 17 cm object. Conclusions: The existence of the signal-independent additive noise is the primary cause for a quadratic relationship between bCT noise variance and the inverse of radiation dose at the detector. With the knowledge of the additive noise contribution to experimentally acquired images, system modifications can be made to reduce the impact of additive noise and improve the quantum noise efficiency of the bCT system.

  12. Ultrafast X-ray Sources

    SciTech Connect (OSTI)

    George Neil

    2010-04-19

    Since before the scattering of X-rays off of DNA led to the first understanding of the double helix structure, sources of X-rays have been an essential tool for scientists examining the structure and interactions of matter. The resolution of a microscope is proportional to the wavelength of light so x-rays can see much finer structures than visible light, down to single atoms. In addition, the energy of X-rays is resonant with the core atomic levels of atoms so with appropriate wavelengths the placement of specific atoms in a large molecule can be determined. Over 10,000 scientists use synchrotron sources, storage rings of high energy electrons, each year worldwide. As an example of such use, virtually every picture of a protein or drug molecule that one sees in the scientific press is a reconstruction based on X-ray scattering of synchrotron light from the crystallized form of that molecule. Unfortunately those pictures are static and proteins work through configuration (shape) changes in response to energy transfer. To understand how biological systems work requires following the energy flow to these molecules and tracking how shape changes drive their interaction with other molecules. We'd like to be able to freeze the action of these molecules at various steps along the way with an X-ray strobe light. How fast does it have to be? To actually get a picture of a molecule in a fixed configuration requires X-ray pulses as short as 30 femtoseconds (1/30 of a millionth of a millionth of a second). To capture the energy flow through changes in electronic levels requires a faster strobe, less than 1 femtosecond! And to acquire such information in smaller samples with higher accuracy demands brighter and brighter X-rays. Unfortunately modern synchrotrons (dubbed 3rd Generation Light Sources) cannot deliver such short bright pulses of X-rays. An entirely new approach is required, linear-accelerator (linac-)-based light sources termed 4th or Next Generation Light Sources (NGLSs). Although NGLSs will not displace synchrotrons from their role they do offer exciting new capabilities which can be understood from the physics of the light production in each device.

  13. Study of runaway electrons using dosimetry of hard x-ray radiations in Damavand tokamak

    SciTech Connect (OSTI)

    Rasouli, C.; Pourshahab, B.; Rasouli, H.; Hosseini Pooya, S. M.; Orouji, T.

    2014-05-15

    In this work several studies have been conducted on hard x-ray emissions of Damavand tokamak based on radiation dosimetry using the Thermoluminescence method. The goal was to understand interactions of runaway electrons with plasma particles, vessel wall, and plasma facing components. Total of 354 GR-200 (LiF:Mg,Cu,P) thermoluminescence dosimeter (TLD) crystals have been placed on 118 points – three TLDs per point – to map hard x-ray radiation doses on the exterior of the vacuum vessel. Results show two distinctive levels of x-ray radiations doses on the exterior of the vessel. The low-dose area on which measured dose is about 0.5 mSv/shot. In the low-dose area there is no particular component inside the vessel. On the contrary, on high-dose area of the vessel, x-ray radiations dose exceeds 30 mSv/shot. The high-dose area coincides with the position of limiters, magnetic probe ducts, and vacuum vessel intersections. Among the high-dose areas, the highest level of dose is measured in the position of the limiter, which could be due to its direct contact with the plasma column and with runaway electrons. Direct collisions of runaway electrons with the vessel wall and plasma facing components make a major contribution for production of hard x-ray photons in Damavand tokamak.

  14. Compact x-ray source and panel

    DOE Patents [OSTI]

    Sampayon, Stephen E. (Manteca, CA)

    2008-02-12

    A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

  15. High-rate x-ray spectroscopy in mammography with a CdTe detector: A digital pulse processing approach

    SciTech Connect (OSTI)

    Abbene, L.; Gerardi, G.; Principato, F.; Del Sordo, S.; Ienzi, R.; Raso, G. [Dipartimento di Fisica e Tecnologie Relative, Universita di Palermo, Viale delle Scienze, Edificio 18, Palermo 90128 (Italy) and INAF/IASF Palermo, Via Ugo La Malfa 153, 90146 Palermo (Italy); Dipartimento di Fisica e Tecnologie Relative, Universita di Palermo, Viale delle Scienze, Edificio 18, Palermo 90128 (Italy); INAF/IASF Palermo, Via Ugo La Malfa 153, 90146 Palermo (Italy); Istituto di Radiologia, Policlinico, 90100 Palermo (Italy); Dipartimento di Fisica e Tecnologie Relative, Universita di Palermo, Viale delle Scienze, Edificio 18, Palermo 90128 (Italy)

    2010-12-15

    Purpose:Direct measurement of mammographic x-ray spectra under clinical conditions is a difficult task due to the high fluence rate of the x-ray beams as well as the limits in the development of high resolution detection systems in a high counting rate environment. In this work we present a detection system, based on a CdTe detector and an innovative digital pulse processing (DPP) system, for high-rate x-ray spectroscopy in mammography. Methods: The DPP system performs a digital pile-up inspection and a digital pulse height analysis of the detector signals, digitized through a 14-bit, 100 MHz digitizer, for x-ray spectroscopy even at high photon counting rates. We investigated on the response of the digital detection system both at low (150 cps) and at high photon counting rates (up to 500 kcps) by using monoenergetic x-ray sources and a nonclinical molybdenum anode x-ray tube. Clinical molybdenum x-ray spectrum measurements were also performed by using a pinhole collimator and a custom alignment device. Results: The detection system shows excellent performance up to 512 kcps with an energy resolution of 4.08% FWHM at 22.1 keV. Despite the high photon counting rate (up to 453 kcps), the molybdenum x-ray spectra, measured under clinical conditions, are characterized by a low number of pile-up events. The agreement between the attenuation curves and the half value layer values, obtained from the measured spectra, simulated spectra, and from the exposure values directly measured with an ionization chamber, also shows the accuracy of the measurements. Conclusions: These results make the proposed detection system a very attractive tool for both laboratory research and advanced quality controls in mammography.

  16. X-ray radiography for container inspection

    DOE Patents [OSTI]

    Katz, Jonathan I. (Clayton, MO); Morris, Christopher L. (Los Alamos, NM)

    2011-06-07

    Arrangements of X-ray inspection systems are described for inspecting high-z materials in voluminous objects such as containers. Inspection methods may involve generating a radiographic image based on detected attenuation corresponding to a pulsed beams of radiation transmitted through a voluminous object. The pulsed beams of radiation are generated by a high-energy source and transmitted substantially downward along an incident angle, of approximately 1.degree. to 30.degree., to a vertical axis extending through the voluminous object. The generated radiographic image may be analyzed to detect on localized high attenuation representative of high-z materials and to discriminate high-z materials from lower and intermediate-z materials on the basis of the high density and greater attenuation of high-z material for higher energy (3-10 MeV) X-rays, and the compact nature of threatening masses of fissionable materials.

  17. Characterization of X-ray generator beam profiles.

    SciTech Connect (OSTI)

    Mitchell, Dean J; Harding, Lee T.; Thoreson, Gregory G.; Theisen, Lisa Anne; Parmeter, John Ethan; Thompson, Kyle Richard

    2013-07-01

    T to compute the radiography properties of various materials, the flux profiles of X-ray sources must be characterized. This report describes the characterization of X-ray beam profiles from a Kimtron industrial 450 kVp radiography system with a Comet MXC-45 HP/11 bipolar oil-cooled X-ray tube. The empirical method described here uses a detector response function to derive photon flux profiles based on data collected with a small cadmium telluride detector. The flux profiles are then reduced to a simple parametric form that enables computation of beam profiles for arbitrary accelerator energies.

  18. X-ray mammography with synchrotron radiation

    SciTech Connect (OSTI)

    Burattini, E. (CNR and INFN-Laboratori Nazionali di Frascati, Frascati, Rome (Italy)); Gambaccini, M.; Marziani, M.; Rimondi, O. (Dipartimento di Fisica dell'Universita and Sezione INFN di Ferrara, Ferrara (Italy)); Indovina, P.L. (Dipartimento di Scienze Fisiche dell'Universita and Sezione INFN di Napoli, Naples (Italy)); Pocek, M.; Simonetti, G. (Istituto di Radiologia, Ospedale Sant'Eugenio, Universita di Tor Vergata, Rome (Italy)); Benassi, M.; Tirelli, C. (Istituto Nazionale del Cancro, Regina Elena, Rome (Italy)); Passariello, R. (Cattedra di Radiologia, Universita dell'Aquila, L'Aquila (Italy))

    1992-01-01

    For the first time in the literature, radiographs of breast phantoms were obtained using several monochromatic synchrotron radiation x-ray beams of selected energy in the range from 14 to 26 keV. In addition, after optimization of the photon energy as a function of the phantom thickness, several mammographs were obtained on surgically removed human breast specimens containing cancer nodules. Comparison between radiographs using a conventional x-ray unit and those obtained of the same specimens utilizing synchrotron monochromatic beams clearly shows that higher contrast and better resolution can be achieved with synchrotron radiation. These results demonstrate the possibility of obtaining radiographs of excised human breast tissue containing a greater amount of radiological information using synchrotron radiation.

  19. X-ray afterglows from gamma-ray bursts

    E-Print Network [OSTI]

    M. Tavani

    1997-03-24

    We consider possible interpretations of the recently detected X- ray afterglow from the gamma-ray burst source GRB 970228. Cosmological and Galactic models of gamma-ray bursts predict different flux and spectral evolution of X-ray afterglows. We show that models based on adiabatic expansion of relativistic forward shocks require very efficient particle energization or post-burst re-acceleration during the expansion. Cooling neutron star models predict a very distinctive spectral and flux evolution that can be tested in current X-ray data.

  20. Soft-x-ray spectroscopy study of nanoscale materials

    SciTech Connect (OSTI)

    Guo, J.-H.

    2005-07-30

    The ability to control the particle size and morphology of nanoparticles is of crucial importance nowadays both from a fundamental and industrial point of view considering the tremendous amount of high-tech applications. Controlling the crystallographic structure and the arrangement of atoms along the surface of nanostructured material will determine most of its physical properties. In general, electronic structure ultimately determines the properties of matter. Soft X-ray spectroscopy has some basic features that are important to consider. X-ray is originating from an electronic transition between a localized core state and a valence state. As a core state is involved, elemental selectivity is obtained because the core levels of different elements are well separated in energy, meaning that the involvement of the inner level makes this probe localized to one specific atomic site around which the electronic structure is reflected as a partial density-of-states contribution. The participation of valence electrons gives the method chemical state sensitivity and further, the dipole nature of the transitions gives particular symmetry information. The new generation synchrotron radiation sources producing intensive tunable monochromatized soft X-ray beams have opened up new possibilities for soft X-ray spectroscopy. The introduction of selectively excited soft X-ray emission has opened a new field of study by disclosing many new possibilities of soft X-ray resonant inelastic scattering. In this paper, some recent findings regarding soft X-ray absorption and emission studies of various nanostructured systems are presented.

  1. NEW X-RAY DETECTIONS OF WNL STARS

    SciTech Connect (OSTI)

    Skinner, Stephen L.; Zhekov, Svetozar A.; Guedel, Manuel; Schmutz, Werner; Sokal, Kimberly R.

    2012-05-15

    Previous studies have demonstrated that putatively single nitrogen-type Wolf-Rayet stars (WN stars) without known companions are X-ray sources. However, almost all WN star X-ray detections so far have been of earlier WN2-WN6 spectral subtypes. Later WN7-WN9 subtypes (also known as WNL stars) have proved more difficult to detect, an important exception being WR 79a (WN9ha). We present here new X-ray detections of the WNL stars WR 16 (WN8h) and WR 78 (WN7h). These new results, when combined with previous detections, demonstrate that X-ray emission is present in WN stars across the full range of spectral types, including later WNL stars. The two WN8 stars observed to date (WR 16 and WR 40) show unusually low X-ray luminosities (L{sub x} ) compared to other WN stars, and it is noteworthy that they also have the lowest terminal wind speeds (v{sub {infinity}}). Existing X-ray detections of about a dozen WN stars reveal a trend of increasing L{sub x} with wind luminosity L{sub wind} = (1/2)M-dot v{sup 2}{sub {infinity}}, suggesting that wind kinetic energy may play a key role in establishing X-ray luminosity levels in WN stars.

  2. Focused X-ray source

    DOE Patents [OSTI]

    Piestrup, Melvin A. (Woodside, CA); Boyers, David G. (Mountain View, CA); Pincus, Cary I. (Sunnyvale, CA); Maccagno, Pierre (Stanford, CA)

    1990-01-01

    An intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator.

  3. Soft X-ray microflares

    E-Print Network [OSTI]

    Mirzoeva, I K

    2015-01-01

    Soft X-ray solar bursts are studied. Weak bursts with powers up to 10-8 W/m2 were detected. All the events were confirmed by GOES observations. Parameters of these microflares are determined. A physical mechanism for the low-intensity solar events is discussed.

  4. Focused X-ray source

    DOE Patents [OSTI]

    Piestrup, M.A.; Boyers, D.G.; Pincus, C.I.; Maccagno, P.

    1990-08-21

    Disclosed is an intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator. 8 figs.

  5. Three New Long Period X-ray Pulsars Discovered in the Small Magellanic Cloud

    E-Print Network [OSTI]

    D. J. Macomb; D. W. Fox; R. C. Lamb; T. A. Prince

    2003-01-04

    The Small Magellanic Cloud is increasingly an invaluable laboratory for studying accreting and isolated X-ray pulsars. We add to the class of compact SMC objects by reporting the discovery of three new long period X-ray pulsars detected with the {\\it Chandra X-ray Observatory}. The pulsars, with periods of 152, 304 and 565 seconds, all show hard X-ray spectra over the range from 0.6 - 7.5 keV. The source positions of the three pulsars are consistent with known H-alpha emission sources, indicating they are likely to be Be type X-ray binary star systems.

  6. High performance x-ray anti-scatter grid

    DOE Patents [OSTI]

    Logan, C.M.

    1995-05-23

    Disclosed are an x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury. 4 Figs.

  7. Three-dimensional x-ray fluorescence mapping of a gold nanoparticle-loaded phantom

    SciTech Connect (OSTI)

    Ren, Liqiang; Wu, Di; Li, Yuhua; Liu, Hong, E-mail: liu@ou.edu [Center for Bioengineering and School of Electrical and Computer Engineering, University of Oklahoma, Norman, Oklahoma 73019 (United States)] [Center for Bioengineering and School of Electrical and Computer Engineering, University of Oklahoma, Norman, Oklahoma 73019 (United States); Wang, Ge [Biomedical Imaging Cluster and Department of Biomedical Engineering, Rensselaer Polytechnic Institute, Troy, New York 12180 (United States)] [Biomedical Imaging Cluster and Department of Biomedical Engineering, Rensselaer Polytechnic Institute, Troy, New York 12180 (United States); Wu, Xizeng [Department of Radiology, University of Alabama, Birmingham, Alabama 35233 (United States)] [Department of Radiology, University of Alabama, Birmingham, Alabama 35233 (United States)

    2014-03-15

    Purpose : X-ray fluorescence (XRF) is a promising technique with sufficient specificity and sensitivity for identifying and quantifying features in small samples containing high atomic number (Z) materials such as iodine, gadolinium, and gold. In this study, the feasibility of applying XRF to early breast cancer diagnosis and treatment is studied using a novel approach for three-dimensional (3D) x-ray fluorescence mapping (XFM) of gold nanoparticle (GNP)-loaded objects in a physical phantom at the technical level. Methods : All the theoretical analysis and experiments are conducted under the condition of using x-ray pencil beam and a compactly integrated x-ray spectrometer. The penetrability of the fluorescence x-rays from GNPs is first investigated by adopting a combination of BR12 with 70 mm/50 mm in thickness on the excitation/emission path to mimic the possible position of tumor goldin vivo. Then, a physical phantom made of BR12 is designed to translate in 3D space with three precise linear stages and subsequently the step by step XFM scanning is performed. The experimental technique named as background subtraction is applied to isolate the gold fluorescence from each spectrum obtained by the spectrometer. Afterwards, the attenuations of both the incident primary x-ray beam with energies beyond the gold K-edge energy (80.725 keV) and the isolated gold K{sub ?} fluorescence x-rays (65.99 –69.80 keV) acquired after background subtraction are well calibrated, and finally the unattenuated K{sub ?} fluorescence counts are used to realize mapping reconstruction and to describe the linear relationship between gold fluorescence counts and corresponding concentration of gold solutions. Results : The penetration results show that the goldK{sub ?} fluorescence x-rays have sufficient penetrability for this phantom study, and the reconstructed mapping results indicate that both the spatial distribution and relative concentration of GNPs within the designed BR12 phantom can be well identified and quantified. Conclusions : Although the XFM method in this investigation is still studied at the technical level and is not yet practical for routinein vivo mapping tasks with GNPs, the current penetrability measurements and phantom study strongly suggest the feasibility to establish and develop a 3D XFM system.

  8. Producing X-rays at the APS

    ScienceCinema (OSTI)

    None

    2013-04-19

    An introduction and overview of the Advanced Photon Source at Argonne National Laboratory, the technology that produces the brightest X-ray beams in the Western Hemisphere, and the research carried out by scientists using those X-rays.

  9. Microgap x-ray detector

    DOE Patents [OSTI]

    Wuest, Craig R. (Danville, CA); Bionta, Richard M. (Livermore, CA); Ables, Elden (Livermore, CA)

    1994-01-01

    An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

  10. Microgap x-ray detector

    DOE Patents [OSTI]

    Wuest, C.R.; Bionta, R.M.; Ables, E.

    1994-05-03

    An x-ray detector is disclosed which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope. 3 figures.

  11. Phase-sensitive X-ray imager

    DOE Patents [OSTI]

    Baker, Kevin Louis

    2013-01-08

    X-ray phase sensitive wave-front sensor techniques are detailed that are capable of measuring the entire two-dimensional x-ray electric field, both the amplitude and phase, with a single measurement. These Hartmann sensing and 2-D Shear interferometry wave-front sensors do not require a temporally coherent source and are therefore compatible with x-ray tubes and also with laser-produced or x-pinch x-ray sources.

  12. A high-transparency, micro-patternable chip for X-ray diffraction analysis of microcrystals under native growth conditions

    SciTech Connect (OSTI)

    Murray, Thomas D.; Lyubimov, Artem Y.; Ogata, Craig M.; Vo, Huy; Uervirojnangkoorn, Monarin; Brunger, Axel T.; Berger, James M.

    2015-08-11

    Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2 µl) of microcrystals grown under common laboratory formats and delivering them to an X-ray beam source under native growth conditions. One approach that shows promise in overcoming the challenges intrinsic to microcrystal analysis is to pair so-called `fixed-target' sample-delivery devices with microbeam-based X-ray diffraction methods. However, to record weak diffraction patterns it is necessary to fabricate devices from X-ray-transparent materials that minimize background scattering. Presented here is the design of a new micro-diffraction device consisting of three layers fabricated from silicon nitride, photoresist and polyimide film. The chip features low X-ray scattering and X-ray absorption properties, and uses a customizable blend of hydrophobic and hydrophilic surface patterns to help localize microcrystals to defined regions. Microcrystals in their native growth conditions can be loaded into the chips with a standard pipette, allowing data collection at room temperature. Diffraction data collected from hen egg-white lysozyme microcrystals (10–15 µm) loaded into the chips yielded a complete, high-resolution (<1.6 Å) data set sufficient to determine a high-quality structure by molecular replacement. In addition, the features of the chip allow the rapid and user-friendly analysis of microcrystals grown under virtually any laboratory format at microfocus synchrotron beamlines and XFELs.

  13. Improving the Raster Scanning Methods used with X-ray Fluorescence to See the Ancient Greek Text of Archimedes (SULI Paper)

    SciTech Connect (OSTI)

    Griffin, Isabella B.; /Norfolk State U. /SLAC, SSRL

    2006-01-04

    X-ray fluorescence is being used to detect the ancient Greek copy of Archimedes work. The copy of Archimedes text was erased with a weak acid and written over to make a prayer book in the Middle Ages. The ancient parchment, made of goat skin, has on it some of Archimedes most valuable writings. The ink in the text contains iron which will fluoresce under x-ray radiation. My research project deals with the scanning and imaging process. The palimpsest is put in a stage that moves in a raster format. As the beam hits the parchment, a germanium detector detects the iron atoms and discriminates against other elements. Since the computer scans in both forwards and backwards directions, it is imperative that each row of data lines up exactly on top of the next row. There are several parameters to consider when scanning the parchment. These parameters include: speed, count time, shutter time, x-number of points, and acceleration. Formulas were made to relate these parameters together. During the actual beam time of this project, the scanning was very slow going; it took 30 hours to scan 1/2 of a page. Using the formulas, the scientists doubled distance and speed to scan the parchment faster; however, the grey scaled data was not lined up properly causing the images to look blurred. My project was is to find out why doubling the parameters caused blurred images, and to fix the problem if it is fixable.

  14. Dose optimization in cardiac x-ray imaging

    SciTech Connect (OSTI)

    Gislason-Lee, Amber J.; McMillan, Catherine; Cowen, Arnold R.; Davies, Andrew G.

    2013-09-15

    Purpose: The aim of this research was to optimize x-ray image quality to dose ratios in the cardiac catheterization laboratory. This study examined independently the effects of peak x-ray tube voltage (kVp), copper (Cu), and gadolinium (Gd) x-ray beam filtration on the image quality to radiation dose balance for adult patient sizes.Methods: Image sequences of polymethyl methacrylate (PMMA) phantoms representing two adult patient sizes were captured using a modern flat panel detector based x-ray imaging system. Tin and copper test details were used to simulate iodine-based contrast medium and stents/guide wires respectively, which are used in clinical procedures. Noise measurement for a flat field image and test detail contrast were used to calculate the contrast to noise ratio (CNR). Entrance surface dose (ESD) and effective dose measurements were obtained to calculate the figure of merit (FOM), CNR{sup 2}/dose. This FOM determined the dose efficiency of x-ray spectra investigated. Images were captured with 0.0, 0.1, 0.25, 0.4, and 0.9 mm Cu filtration and with a range of gadolinium oxysulphide (Gd{sub 2}O{sub 2}S) filtration.Results: Optimum x-ray spectra were the same for the tin and copper test details. Lower peak tube voltages were generally favored. For the 20 cm phantom, using 2 Lanex Fast Back Gd{sub 2}O{sub 2}S screens as x-ray filtration at 65 kVp provided the highest FOM considering ESD and effective dose. Considering ESD, this FOM was only marginally larger than that from using 0.4 mm Cu at 65 kVp. For the 30 cm phantom, using 0.25 mm copper filtration at 80 kVp was most optimal; considering effective dose the FOM was highest with no filtration at 65 kVp.Conclusions: These settings, adjusted for x-ray tube loading limits and clinically acceptable image quality, should provide a useful option for optimizing patient dose to image quality in cardiac x-ray imaging. The same optimal x-ray beam spectra were found for both the tin and copper details, suggesting that iodine contrast based imaging and visualization of interventional devices could potentially be optimized for dose using similar x-ray beam spectra.

  15. Spectral Formation in X-Ray Pulsar Accretion Columns

    E-Print Network [OSTI]

    Peter A. Becker; Michael T. Wolff

    2005-03-03

    We present the first self-consistent model for the dynamics and the radiative transfer occurring in bright X-ray pulsar accretion columns, with a special focus on the role of the shock in energizing the emerging X-rays. The pressure inside the accretion column of a luminous X-ray pulsar is dominated by the photons, and consequently the equations describing the coupled radiative-dynamical structure must be solved simultaneously. Spectral formation in these sources is therefore a complex, nonlinear phenomenon. We obtain the analytical solution for the Green's function describing the upscattering of monochromatic radiation injected into the column from the thermal mound located near the base of the flow. The Green's function is convolved with a Planck distribution to model the X-ray spectrum resulting from the reprocessing of blackbody photons produced in the thermal mound. These photons diffuse through the infalling gas and eventually escape out the walls of the column, forming the observed X-ray spectrum. We show that the resulting column-integrated, phase-averaged spectrum has a power-law shape at high energies and a blackbody shape at low energies, in agreement with the observational data for many X-ray pulsars.

  16. Constraints on jet X-ray emission in low/hard state X-ray binaries

    E-Print Network [OSTI]

    Thomas J. Maccarone

    2005-03-31

    We show that the combination of the similarities between the X-ray properties of low luminosity accreting black holes and accreting neutron stars, combined with the differences in their radio properties argues that the X-rays from these systems are unlikely to be formed in the relativistic jets. Specifically, the spectra of extreme island state neutron stars and low/hard state black holes are known to be indistinguishable, while the power spectra from these systems are known to show only minor differences beyond what would be expected from scaling the characteristic variability frequencies by the mass of the compact object. The spectral and temporal similarities thus imply a common emission mechanism that has only minor deviations from having all key parameters scaling linearly with the mass of the compact object, while we show that this is inconsistent with the observations that the radio powers of neutron stars are typically about 30 times lower than those of black holes at the same X-ray luminosity. We also show that an abrupt luminosity change would be expected when a system makes a spectral state transition from a radiatively inefficient jet dominated accretion flow to a thin disk dominated flow, but that such a change is not seen.

  17. Intermolecular triple proton and deuteron transfer in crystalline 3,5-dimethylpyrazole studied by NMR, NQR, and x-ray methods

    SciTech Connect (OSTI)

    Wehrle, B.; Aguilar-Parrilla, F.; Limbach, H.H. ); de la Concepcion Foces-Foces, M.; Cano, F.H. ); Elguero, J. ); Baldy, A.; Pierrot, M. ); Khurshid, M.M.T.; Larcombe-McDouall, J.B.; Smith, J.A.S. )

    1989-09-13

    A combination of {sup 13}C, {sup 15}N magnetic resonance, {sup 14}N quadrupole double resonance, and x-ray studies of solid 3,5-dimethylpyrazole between 270 and 350 K has shown that the NH...N hydrogen bond units present in the crystal are dynamically disordered, so that each nitrogen atom is on average attached to half a hydrogen atom. The molecules form discrete hydrogen-bonded cyclic trimers, in which the hydrogen atoms move in a double minimum potential energy surface which is symmetrical, to within experimental error. The experimental evidence in this temperature range is consistent with disorder by means of correlated triple hydrogen jumps with an activation energy of 45 kJ mol{sup {minus}1}. There is a large kinetic hydrogen (HHH)/deuterium (DDD) isotope effort of >20 at 299 K and equal to 8 at 347 K.

  18. Reliable before-fabrication forecasting of expected surface slope distributions for x-ray optics

    E-Print Network [OSTI]

    Yashchuk, Yekaterina V.

    2013-01-01

    of x-ray optics for the LCLS free-electron laser,” Proc.beamlines and diagnostics at LCLS,” Nucl. Instrum. Methods A

  19. X-ray Moiré deflectometry using synthetic reference images

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Stutman, Dan; Valdivia, Maria Pia; Finkenthal, Michael

    2015-06-25

    Moiré fringe deflectometry with grating interferometers is a technique that enables refraction-based x-ray imaging using a single exposure of an object. To obtain the refraction image, the method requires a reference fringe pattern (without the object). Our study shows that, in order to avoid artifacts, the reference pattern must be exactly matched in phase with the object fringe pattern. In experiments, however, it is difficult to produce a perfectly matched reference pattern due to unavoidable interferometer drifts. We present a simple method to obtain matched reference patterns using a phase-scan procedure to generate synthetic Moiré images. As a result, themore »method will enable deflectometric diagnostics of transient phenomena such as laser-produced plasmas and could improve the sensitivity and accuracy of medical phase-contrast imaging.« less

  20. X-ray Emission from Ionized Wind-Bubbles around Wolf-Rayet Stars

    E-Print Network [OSTI]

    Dwarkadas, Vikram V

    2015-01-01

    Using a code that employs a self-consistent method for computing the effects of photoionization on circumstellar gas dynamics, we model the formation of wind-driven nebulae around massive Wolf-Rayet (W-R) stars. Our algorithm incorporates a simplified model of the photo-ionization source, computes the fractional ionization of hydrogen due to the photoionizing flux and recombination, and determines self-consistently the energy balance due to ionization, photo-heating and radiative cooling. We take into account changes in stellar properties and mass-loss over the star's evolution. Our multi-dimensional simulations clearly reveal the presence of strong ionization front instabilities. Using various X-ray emission models, and abundances consistent with those derived for W-R nebulae, we compute the X-ray flux and spectra from our wind bubble models. We show the evolution of the X-ray spectral features with time over the evolution of the star, taking the absorption of the X-rays by the ionized bubble into account. O...

  1. Comptonization and the Spectra of Accretion-Powered X-Ray Pulsars

    E-Print Network [OSTI]

    Michael T. Wolff; Peter A. Becker; Kenneth D. Wolfram

    2007-04-17

    Accretion-powered X-ray pulsars are among the most luminous X-ray sources in the Galaxy. However, despite decades of theoretical and observational work since their discovery, no satisfactory model for the formation of the observed X-ray spectra has emerged. In this paper, we report on a self-consistent calculation of the spectrum emerging from a pulsar accretion column that includes an explicit treatment of the bulk and thermal Comptonization occurring in the radiation-dominated shocks that form in the accretion flows. Using a rigorous eigenfunction expansion method, we obtain a closed-form expression for the Green's function describing the upscattering of monochromatic radiation injected into the column. The Green's function is convolved with bremsstrahlung, cyclotron, and blackbody source terms to calculate the emergent photon spectrum. We show that energization of photons in the shock naturally produces an X-ray spectrum with a relatively flat continuum and a high-energy exponential cutoff. Finally, we demonstrate that our model yields good agreement with the spectra of the bright pulsar Her X-1 and the low luminosity pulsar X Per.

  2. X-ray Imaging Workshop

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorkingLos Alamos verifies largest single goldWindX-Ray ImagingInImaging and

  3. Femtosecond x-ray absorption spectroscopy with hard x-ray free electron laser

    SciTech Connect (OSTI)

    Katayama, Tetsuo; Togashi, Tadashi; Tono, Kensuke; Kameshima, Takashi; Inubushi, Yuichi; Sato, Takahiro; Hatsui, Takaki; Yabashi, Makina; Obara, Yuki; Misawa, Kazuhiko; Bhattacharya, Atanu; Kurahashi, Naoya; Ogi, Yoshihiro; Suzuki, Toshinori; Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198

    2013-09-23

    We have developed a method of dispersive x-ray absorption spectroscopy with a hard x-ray free electron laser (XFEL), generated by a self-amplified spontaneous emission (SASE) mechanism. A transmission grating was utilized for splitting SASE-XFEL light, which has a relatively large bandwidth (?E/E ? 5 × 10{sup ?3}), into several branches. Two primary split beams were introduced into a dispersive spectrometer for measuring signal and reference spectra simultaneously. After normalization, we obtained a Zn K-edge absorption spectrum with a photon-energy range of 210 eV, which is in excellent agreement with that measured by a conventional wavelength-scanning method. From the analysis of the difference spectra, the noise ratio was evaluated to be ?3 × 10{sup ?3}, which is sufficiently small to trace minute changes in transient spectra induced by an ultrafast optical laser. This scheme enables us to perform single-shot, high-accuracy x-ray absorption spectroscopy with femtosecond time resolution.

  4. Soft X-ray techniques to study mesoscale magnetism

    E-Print Network [OSTI]

    Kortright, Jeffrey B.

    2003-01-01

    X-Ray Techniques to Study Mesoscale Magnetism Jeffrey B.X-Ray Techniques to Study Mesoscale Magnetism Jeffrey B.

  5. Controlling X-rays With Light

    SciTech Connect (OSTI)

    Glover, Ernie; Hertlein, Marcus; Southworth, Steve; Allison, Tom; van Tilborg, Jeroen; Kanter, Elliot; Krassig, B.; Varma, H.; Rude, Bruce; Santra, Robin; Belkacem, Ali; Young, Linda

    2010-08-02

    Ultrafast x-ray science is an exciting frontier that promises the visualization of electronic, atomic and molecular dynamics on atomic time and length scales. A largelyunexplored area of ultrafast x-ray science is the use of light to control how x-rays interact with matter. In order to extend control concepts established for long wavelengthprobes to the x-ray regime, the optical control field must drive a coherent electronic response on a timescale comparable to femtosecond core-hole lifetimes. An intense field is required to achieve this rapid response. Here an intense optical control pulse isobserved to efficiently modulate photoelectric absorption for x-rays and to create an ultrafast transparency window. We demonstrate an application of x-ray transparencyrelevant to ultrafast x-ray sources: an all-photonic temporal cross-correlation measurement of a femtosecond x-ray pulse. The ability to control x-ray/matterinteractions with light will create new opportunities at current and next-generation x-ray light sources.

  6. X-RAY EMISSION FROM MAGNETIC MASSIVE STARS

    SciTech Connect (OSTI)

    Nazé, Yaël; Petit, Véronique; Rinbrand, Melanie; Owocki, Stan; Cohen, David; Ud-Doula, Asif; Wade, Gregg A.

    2014-11-01

    Magnetically confined winds of early-type stars are expected to be sources of bright and hard X-rays. To clarify the systematics of the observed X-ray properties, we have analyzed a large series of Chandra and XMM-Newton observations, corresponding to all available exposures of known massive magnetic stars (over 100 exposures covering ?60% of stars compiled in the catalog of Petit et al.). We show that the X-ray luminosity is strongly correlated with the stellar wind mass-loss rate, with a power-law form that is slightly steeper than linear for the majority of the less luminous, lower- M-dot B stars and flattens for the more luminous, higher- M-dot O stars. As the winds are radiatively driven, these scalings can be equivalently written as relations with the bolometric luminosity. The observed X-ray luminosities, and their trend with mass-loss rates, are well reproduced by new MHD models, although a few overluminous stars (mostly rapidly rotating objects) exist. No relation is found between other X-ray properties (plasma temperature, absorption) and stellar or magnetic parameters, contrary to expectations (e.g., higher temperature for stronger mass-loss rate). This suggests that the main driver for the plasma properties is different from the main determinant of the X-ray luminosity. Finally, variations of the X-ray hardnesses and luminosities, in phase with the stellar rotation period, are detected for some objects and they suggest that some temperature stratification exists in massive stars' magnetospheres.

  7. X-ray emitting young stars in the Orion Nebula

    E-Print Network [OSTI]

    Eric D. Feigelson; Patrick Broos; James A. Gaffney III; Gordon Garmire; Lynne A. Hillenbrand; Steven H. Pravdo; Leisa Townsley; Yohko Tsuboi

    2002-03-19

    The Orion Nebula Cluster and the molecular cloud in its vicinity have been observed with the ACIS-I detector on board the Chandra X-ray Observatory with 23 hours exposure. We detect 1075 X-ray sources: 91% are spatially associated with known stellar members of the cluster, and 7% are newly identified deeply embedded cloud members. This provides the largest X-ray study of a pre-main sequence stellar population. We examine here the X-ray properties of Orion young stars as a function of mass. Results include: (a) the discovery of rapid variability in the O9.5 31 M_o star \\theta^2A Ori, and several early B stars, inconsistent with the standard model of X-ray production in small wind shocks; (b) support for the hypothesis that intermediate-mass mid-B through A type stars do not themselves produce significant X-ray emission; (c) confirmation that low-mass G- through M-type T Tauri stars exhibit powerful flaring but typically at luminosities considerably below the `saturation' level; (d) confirmation that the presence or absence of a circumstellar disk has no discernable effect on X-ray emission; (e) evidence that T Tauri plasma temperatures are often very high with T >= 100 MK, even when luminosities are modest and flaring is not evident; and (f) detection of the largest sample of pre-main sequence very low mass objects showing high flaring levels and a decline in magnetic activity as they evolve into L- and T-type brown dwarfs.

  8. ON THE X-RAY OUTBURSTS OF TRANSIENT ANOMALOUS X-RAY PULSARS AND SOFT GAMMA-RAY REPEATERS

    SciTech Connect (OSTI)

    Cal Latin-Small-Letter-Dotless-I skan, Sirin; Ertan, Uenal [Sabanc Latin-Small-Letter-Dotless-I University, Orhanl Latin-Small-Letter-Dotless-I -Tuzla, Istanbul, 34956 (Turkey)

    2012-10-20

    We show that the X-ray outburst light curves of four transient anomalous X-ray pulsars (AXPs) and soft gamma-ray repeaters (SGRs), namely, XTE J1810-197, SGR 0501+4516, SGR 1627-41, and CXOU J164710.2-455216, can be produced by the fallback disk model that was also applied to the outburst light curves of persistent AXPs and SGRs in our earlier work. The model solves the diffusion equation for the relaxation of a disk that has been pushed back by a soft gamma-ray burst. The sets of main disk parameters used for these transient sources are very similar to each other and to those employed in our earlier models of persistent AXPs and SGRs. There is a characteristic difference between the X-ray outburst light curves of transient and persistent sources. This can be explained by the differences in the disk surface density profiles of the transient and persistent sources in quiescence indicated by their quiescent X-ray luminosities. Our results imply that a viscous disk instability operating at a critical temperature in the range of {approx}1300-2800 K is a common property of all fallback disks around AXPs and SGRs. The effect of the instability is more pronounced and starts earlier for the sources with lower quiescent luminosities, which leads to the observable differences in the X-ray enhancement light curves of transient and persistent sources. A single active disk model with the same basic disk parameters can account for the enhancement phases of both transient and persistent AXPs and SGRs. We also present a detailed parameter study to show the effects of disk parameters on the evolution of the X-ray luminosity of AXPs and SGRs in the X-ray enhancement phases.

  9. Dimensionality and noise in energy selective x-ray imaging

    SciTech Connect (OSTI)

    Alvarez, Robert E.

    2013-11-15

    Purpose: To develop and test a method to quantify the effect of dimensionality on the noise in energy selective x-ray imaging.Methods: The Cramèr-Rao lower bound (CRLB), a universal lower limit of the covariance of any unbiased estimator, is used to quantify the noise. It is shown that increasing dimensionality always increases, or at best leaves the same, the variance. An analytic formula for the increase in variance in an energy selective x-ray system is derived. The formula is used to gain insight into the dependence of the increase in variance on the properties of the additional basis functions, the measurement noise covariance, and the source spectrum. The formula is also used with computer simulations to quantify the dependence of the additional variance on these factors. Simulated images of an object with three materials are used to demonstrate the trade-off of increased information with dimensionality and noise. The images are computed from energy selective data with a maximum likelihood estimator.Results: The increase in variance depends most importantly on the dimension and on the properties of the additional basis functions. With the attenuation coefficients of cortical bone, soft tissue, and adipose tissue as the basis functions, the increase in variance of the bone component from two to three dimensions is 1.4 × 10{sup 3}. With the soft tissue component, it is 2.7 × 10{sup 4}. If the attenuation coefficient of a high atomic number contrast agent is used as the third basis function, there is only a slight increase in the variance from two to three basis functions, 1.03 and 7.4 for the bone and soft tissue components, respectively. The changes in spectrum shape with beam hardening also have a substantial effect. They increase the variance by a factor of approximately 200 for the bone component and 220 for the soft tissue component as the soft tissue object thickness increases from 1 to 30 cm. Decreasing the energy resolution of the detectors increases the variance of the bone component markedly with three dimension processing, approximately a factor of 25 as the resolution decreases from 100 to 3 bins. The increase with two dimension processing for adipose tissue is a factor of two and with the contrast agent as the third material for two or three dimensions is also a factor of two for both components. The simulated images show that a maximum likelihood estimator can be used to process energy selective x-ray data to produce images with noise close to the CRLB.Conclusions: The method presented can be used to compute the effects of the object attenuation coefficients and the x-ray system properties on the relationship of dimensionality and noise in energy selective x-ray imaging systems.

  10. X-Ray Spectroscopy: An Experimental Technique to Measure Charge State Distribution Right at the Ion-Solid Interaction

    E-Print Network [OSTI]

    Sharma, Prashant

    2015-01-01

    Charge state distributions of $^{56}$Fe and $^{58}$Ni projectile ions passing through thin carbon foils have been studied in the energy range of 1.44 - 2.69 MeV/u using a novel method from the x-ray spectroscopy technique. Interestingly the charge state distribution in the bulk show Lorentzian behavior instead of usual Gaussian distribution. Further, different parameters of charge state distribution like mean charge state, distribution width and asymmetric parameter are determined and compared with the empirical calculations and ETACHA predictions. It is found that the x-ray measurement technique is appropriate to determine the mean charge state right at the interaction zone or in the bulk. Interestingly, empirical formalism predicts much lower projectile mean charge states compare to x-ray measurements which clearly indicate multi-electron capture from the target surface. The ETACHA predictions and experimental results are found to be comparable for energies $\\geq$ 2 MeV/u.

  11. Biological imaging by soft x-ray diffraction microscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Shapiro, D.; Thibault, P.; Beetz, T.; Elser, V.; Howells, M.; Jacobsen, C.; Kirz, J.; Lima, E.; Miao, H.; Neiman, A. M.; et al

    2005-10-25

    We have used the method of x-ray diffraction microscopy to image the complex-valued exit wave of an intact and unstained yeast cell. The images of the freeze-dried cell, obtained by using 750-eV x-rays from different angular orientations, portray several of the cell's major internal components to 30-nm resolution. The good agreement among the independently recovered structures demonstrates the accuracy of the imaging technique. To obtain the best possible reconstructions, we have implemented procedures for handling noisy and incomplete diffraction data, and we propose a method for determining the reconstructed resolution. This work represents a previously uncharacterized application of x-ray diffractionmore »microscopy to a specimen of this complexity and provides confidence in the feasibility of the ultimate goal of imaging biological specimens at 10-nm resolution in three dimensions.« less

  12. X-ray transmissive debris shield

    DOE Patents [OSTI]

    Spielman, Rick B. (Albuquerque, NM)

    1994-01-01

    A composite window structure is described for transmitting x-ray radiation and for shielding radiation generated debris. In particular, separate layers of different x-ray transmissive materials are laminated together to form a high strength, x-ray transmissive debris shield which is particularly suited for use in high energy fluences. In one embodiment, the composite window comprises alternating layers of beryllium and a thermoset polymer.

  13. X-ray laser microscope apparatus

    DOE Patents [OSTI]

    Suckewer, Szymon (Princeton, NJ); DiCicco, Darrell S. (Plainsboro, NJ); Hirschberg, Joseph G. (Coral Gables, FL); Meixler, Lewis D. (East Windsor, NJ); Sathre, Robert (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ)

    1990-01-01

    A microscope consisting of an x-ray contact microscope and an optical microscope. The optical, phase contrast, microscope is used to align a target with respect to a source of soft x-rays. The source of soft x-rays preferably comprises an x-ray laser but could comprise a synchrotron or other pulse source of x-rays. Transparent resist material is used to support the target. The optical microscope is located on the opposite side of the transparent resist material from the target and is employed to align the target with respect to the anticipated soft x-ray laser beam. After alignment with the use of the optical microscope, the target is exposed to the soft x-ray laser beam. The x-ray sensitive transparent resist material whose chemical bonds are altered by the x-ray beam passing through the target mater GOVERNMENT LICENSE RIGHTS This invention was made with government support under Contract No. De-FG02-86ER13609 awarded by the Department of Energy. The Government has certain rights in this invention.

  14. Lensless imaging of nanoporous glass with soft X-rays

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Turner, Joshua J.; Nelson, Johanna; Huang, Xiaojing; Steinbrener, Jan; Jacobsen, Chris

    2013-06-01

    Coherent soft X-ray diffraction has been used to image nanoporous glass structure in two dimensions using different methods. The merit of the reconstructions was judged using a new method of Fourier phase correlation with a final, refined image. The porous structure was found to have a much larger average size then previously believed.

  15. X-ray characterization of solid small molecule organic materials

    SciTech Connect (OSTI)

    Billinge, Simon; Shankland, Kenneth; Shankland, Norman; Florence, Alastair

    2014-06-10

    The present invention provides, inter alia, methods of characterizing a small molecule organic material, e.g., a drug or a drug product. This method includes subjecting the solid small molecule organic material to x-ray total scattering analysis at a short wavelength, collecting data generated thereby, and mathematically transforming the data to provide a refined set of data.

  16. DISCOVERY OF X-RAY PULSATIONS FROM THE NEXT GEMINGA, PSR J1836+5925

    SciTech Connect (OSTI)

    Lin, L. C. C.; Kong, A. K. H. [Institute of Astronomy, National Tsing-Hua University, Hsinchu 30013, Taiwan (China); Hui, C. Y. [Department of Astronomy and Space Science, Chungnam National University, Daejeon (Korea, Republic of); Li, K. T. [Department of Biological Science and Technology, China Medical University, Taichung 40402, Taiwan (China); Takata, J. [Department of Physics, University of Hong Kong, Pokfulam Road, Hong Kong (China); Hu, C. P.; Chou, Y. [Graduate Institute of Astronomy, National Central University, Jhongli 32001, Taiwan (China); Yen, D. C. C., E-mail: cyhui@cnu.ac.kr [Department of Mathematics, Fu Jen Catholic University, New Taipei City 24205, Taiwan (China)

    2014-09-20

    We report recent XMM-Newton investigations of PSR J1836+5925, the ''next Geminga'', which determined an X-ray pulsation of ?173.3 ms. Its X-ray periodicity is consistent with the ?-ray ephemeris at the same epoch. The X-ray folded light curve has a sinusoidal structure that is different from the double-peaked ?-ray pulse profile. We have also analyzed the X-ray phase-averaged spectra which shows that the X-ray emission from PSR J1836+5925 is thermal dominant. This suggests that the X-ray pulsation mainly originates from the modulated hot spot on the stellar surface.

  17. Hyperspectral image reconstruction for x-ray fluorescence tomography

    SciTech Connect (OSTI)

    Gürsoy, Do?a; Biçer, Tekin; Lanzirotti, Antonio; Newville, Matthew G.; De Carlo, Francesco

    2015-01-01

    A penalized maximum-likelihood estimation is proposed to perform hyperspectral (spatio-spectral) image reconstruction for X-ray fluorescence tomography. The approach minimizes a Poisson-based negative log-likelihood of the observed photon counts, and uses a penalty term that has the effect of encouraging local continuity of model parameter estimates in both spatial and spectral dimensions simultaneously. The performance of the reconstruction method is demonstrated with experimental data acquired from a seed of arabidopsis thaliana collected at the 13-ID-E microprobe beamline at the Advanced Photon Source. The resulting element distribution estimates with the proposed approach show significantly better reconstruction quality than the conventional analytical inversion approaches, and allows for a high data compression factor which can reduce data acquisition times remarkably. In particular, this technique provides the capability to tomographically reconstruct full energy dispersive spectra without compromising reconstruction artifacts that impact the interpretation of results.

  18. Hyperspectral image reconstruction for x-ray fluorescence tomography

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Gürsoy, Do?a; Biçer, Tekin; Lanzirotti, Antonio; Newville, Matthew G.; De Carlo, Francesco

    2015-01-01

    A penalized maximum-likelihood estimation is proposed to perform hyperspectral (spatio-spectral) image reconstruction for X-ray fluorescence tomography. The approach minimizes a Poisson-based negative log-likelihood of the observed photon counts, and uses a penalty term that has the effect of encouraging local continuity of model parameter estimates in both spatial and spectral dimensions simultaneously. The performance of the reconstruction method is demonstrated with experimental data acquired from a seed of arabidopsis thaliana collected at the 13-ID-E microprobe beamline at the Advanced Photon Source. The resulting element distribution estimates with the proposed approach show significantly better reconstruction quality than the conventional analytical inversionmore »approaches, and allows for a high data compression factor which can reduce data acquisition times remarkably. In particular, this technique provides the capability to tomographically reconstruct full energy dispersive spectra without compromising reconstruction artifacts that impact the interpretation of results.« less

  19. X-ray spectroscopy of neutron star low-mass X-ray binaries

    E-Print Network [OSTI]

    Krauss, Miriam Ilana

    2007-01-01

    In this thesis, I present work spanning a variety of topics relating to neutron star lowmass X-ray binaries (LMXBs) and utilize spectral information from X-ray observations to further our understanding of these sources. ...

  20. X-ray radiography with highly charged ions

    DOE Patents [OSTI]

    Marrs, Roscoe E. (Livermore, CA)

    2000-01-01

    An extremely small (1-250 micron FWHM) beam of slow highly charged ions deexciting on an x-ray production target generates x-ray monochromatic radiation that is passed through a specimen and detected for imaging. The resolution of the x-ray radiograms is improved and such detection is achieved with relatively low dosages of radiation passing through the specimen. An apparatus containing an electron beam ion trap (and modifications thereof) equipped with a focusing column serves as a source of ions that generate radiation projected onto an image detector. Electronic and other detectors are able to detect an increased amount of radiation per pixel than achieved by previous methods and apparati.

  1. Data fusion in neutron and X-ray computed tomography

    SciTech Connect (OSTI)

    Schrapp, Michael J.; Goldammer, Matthias; Schulz, Michael; Issani, Siraj; Bhamidipati, Suryanarayana; Böni, Peter

    2014-10-28

    We present a fusion methodology between neutron and X-ray computed tomography (CT). On the one hand, the inspection by X-ray CT of a wide class of multimaterials in non-destructive testing applications suffers from limited information of object features. On the other hand, neutron imaging can provide complementary data in such a way that the combination of both data sets fully characterizes the object. In this contribution, a novel data fusion procedure, called Fusion Regularized Simultaneous Algebraic Reconstruction Technique, is developed where the X-ray reconstruction is modified to fulfill the available data from the imaging with neutrons. The experiments, which were obtained from an aluminum profile containing a steel screw, and attached carbon fiber plates demonstrate that the image quality in CT can be significantly improved when the proposed fusion method is used.

  2. Application of a PWFA to an X-ray FEL

    E-Print Network [OSTI]

    Israeli, Yasmine; Reiche, Sven; Pedrozzi, Marco; Muggli, Patric

    2016-01-01

    There is a growing demand for X-ray Free-electron lasers (FELs) in various science fields, in particular for those with short pulses, larger photon fluxes and shorter wavelengths. The level of X-ray power and the pulse energy depend on the amount of electron bunch energy. Increasing the latter will increase the power of the radiating X-rays. Using numerical simulations we explore the possibility of using a plasma wakefield accelerator (PWFA) scheme to increase the electron beam energy of an existing FEL facility without significantly increasing the accelerator length. In this paper we use parameters of the SwissFEL beam. The simulations are carried out in 2D cylindrical symmetry using the code OSIRIS. Initial results show an energy gain of ~2 GeV after propagation of 0.5 m in the plasma with a relative energy spread of ~1%.

  3. Absolute timing measurements of the Ni-like Pd and Sn soft-x-ray lasers

    SciTech Connect (OSTI)

    Staub, F.; Braud, M.; Balmer, J.E.; Nilsen, J.

    2005-10-15

    The absolute time of emission of the x-ray laser output with respect to the arrival of a 100-ps pump pulse has been measured with the aid of a calibrated timing fiducial. The results show the x-ray laser to appear up to 60 ps (80 ps) before the peak of the pump pulse in the case of the Sn (Pd) x-ray laser, which is in good agreement with simulations obtained from the LASNEX and CRETIN codes. The pulse duration was found to be {approx}45 ps for both the Sn and the Pd x-ray lasers.

  4. The cool component and the dichotomy, lateral expansion, and axial rotation of solar X-ray jets

    SciTech Connect (OSTI)

    Moore, Ronald L.; Sterling, Alphonse C.; Falconer, David A.; Robe, Dominic

    2013-06-01

    We present results from a study of 54 polar X-ray jets that were observed in coronal X-ray movies from the X-ray Telescope on Hinode and had simultaneous coverage in movies of the cooler transition region (T ? 10{sup 5} K) taken in the He II 304 Å band of the Atmospheric Imaging Assembly (AIA) on Solar Dynamics Observatory. These dual observations verify the standard-jet/blowout-jet dichotomy of polar X-ray jets previously found primarily from XRT movies alone. In accord with models of blowout jets and standard jets, the AIA 304 Å movies show a cool (T ? 10{sup 5} K) component in nearly all blowout X-ray jets and in a small minority of standard X-ray jets, obvious lateral expansion in blowout X-ray jets but none in standard X-ray jets, and obvious axial rotation in both blowout X-ray jets and standard X-ray jets. In our sample, the number of turns of axial rotation in the cool-component standard X-ray jets is typical of that in the blowout X-ray jets, suggesting that the closed bipolar magnetic field in the jet base has substantial twist not only in all blowout X-ray jets but also in many standard X-ray jets. We point out that our results for the dichotomy, lateral expansion, and axial rotation of X-ray jets add credence to published speculation that type-II spicules are miniature analogs of X-ray jets, are generated by granule-size emerging bipoles, and thereby carry enough energy to power the corona and solar wind.

  5. Confusion of Diffuse Objects in the X-ray Sky

    E-Print Network [OSTI]

    G. Mark Voit; August E. Evrard; Greg L. Bryan

    2000-12-08

    Most of the baryons in the present-day universe are thought to reside in intergalactic space at temperatures of 10^5-10^7 K. X-ray emission from these baryons contributes a modest (~10%) fraction of the ~ 1 keV background whose prominence within the large-scale cosmic web depends on the amount of non-gravitational energy injected into intergalactic space by supernovae and AGNs. Here we show that the virialized regions of groups and clusters cover over a third of the sky, creating a source-confusion problem that may hinder X-ray searches for individual intercluster filaments and contaminate observations of distant groups.

  6. A 0535+26: an X-ray/Optical Tour

    E-Print Network [OSTI]

    Camero-Arranz, A; Wilson-Hodge, C A; Jenke, P; Coe, M J; Steele, I; Caballero, I; Gutierrez-Soto, J; Kretschmar, P; Suso, J; McBride, V A; Rodriguez, J

    2011-01-01

    We compiled X-ray and Optical observations of the accreting X-ray binary system A 0535+262 since its discovery in 1975, that will allow us to shed light on the unpredictable behavior of this binary system. We present the data in terms of the Be-disk interaction with the neutron star companion. In addition, we show recent results from the continuous monitoring of this source by the Gamma-ray Burst Monitor(GBM), on board the Fermi observatory, since its launch in 2008 June 11.

  7. Bragg x-ray survey spectrometer for ITER

    SciTech Connect (OSTI)

    Varshney, S. K.; Jakhar, S. [ITER-India, Institute for Plasma Research, Bhat, Gandhinagar, Gujarat 382428 (India); Barnsley, R. [ITER Organization, Route de Vinon sur Verdon, 13115 Saint Paul Lez Durance (France); O'Mullane, M. G. [Department of Physics, University of Strathclyde, Glasgow G4 0NG (United Kingdom)

    2012-10-15

    Several potential impurity ions in the ITER plasmas will lead to loss of confined energy through line and continuum emission. For real time monitoring of impurities, a seven channel Bragg x-ray spectrometer (XRCS survey) is considered. This paper presents design and analysis of the spectrometer, including x-ray tracing by the Shadow-XOP code, sensitivity calculations for reference H-mode plasma and neutronics assessment. The XRCS survey performance analysis shows that the ITER measurement requirements of impurity monitoring in 10 ms integration time at the minimum levels for low-Z to high-Z impurity ions can largely be met.

  8. Accuracy evaluation of a Compton X-ray spectrometer with bremsstrahlung X-rays generated by a 6 MeV electron bunch

    SciTech Connect (OSTI)

    Kojima, Sadaoki Arikawa, Yasunobu; Zhang, Zhe; Ikenouchi, Takahito; Morace, Alessio; Nagai, Takahiro; Abe, Yuki; Sakata, Shouhei; Inoue, Hiroaki; Utsugi, Masaru; Nakai, Mitsuo; Nishimura, Hiroaki; Shiraga, Hiroyuki; Fujioka, Shinsuke; Azechi, Hiroshi; Nishimura, Yasuhiko; Togawa, Hiromi; Ozaki, Tetsuo; Kato, Ryukou

    2014-11-15

    A Compton-scattering-based X-ray spectrometer is developed to obtain the energy distribution of fast electrons produced by intense laser and matter interactions. Bremsstrahlung X-rays generated by fast electrons in a material are used to measure fast electrons’ energy distribution in matter. In the Compton X-ray spectrometer, X-rays are converted into recoil electrons by Compton scattering in a converter made from fused silica glass, and a magnet-based electron energy analyzer is used to measure the energy distribution of the electrons that recoil in the direction of the incident X-rays. The spectrum of the incident X-rays is reconstructed from the energy distribution of the recoil electrons. The accuracy of this spectrometer is evaluated using a quasi-monoenergetic 6 MeV electron bunch that emanates from a linear accelerator. An electron bunch is injected into a 1.5 mm thick tungsten plate to produce bremsstrahlung X-rays. The spectrum of these bremsstrahlung X-rays is obtained in the range from 1 to 9 MeV. The energy of the electrons in the bunch is estimated using a Monte Carlo simulation of particle-matter interactions. The result shows that the spectrometer's energy accuracy is ±0.5 MeV for 6.0 MeV electrons.

  9. Phased Contrast X-Ray Imaging

    ScienceCinema (OSTI)

    Erin Miller

    2012-12-31

    The Pacific Northwest National Laboratory is developing a range of technologies to broaden the field of explosives detection. Phased contrast X-ray imaging, which uses silicon gratings to detect distortions in the X-ray wave front, may be applicable to mail or luggage scanning for explosives; it can also be used in detecting other contraband, small-parts inspection, or materials characterization.

  10. X-rays from Hot Subdwarfs

    E-Print Network [OSTI]

    Mereghetti, Sandro

    2015-01-01

    Thanks to the high sensitivity of the instruments on board the XMM-Newton and Chandra satellites, it has become possible to explore the properties of the X-ray emission from hot subdwarfs. The small but growing sample of hot subdwarfs detected in X-rays includes binary systems, in which the X-rays result from wind accretion onto a compact companion (white dwarf or neutron star), as well as isolated sdO stars in which X-rays are probably due to shock instabilities in the wind. X-ray observations of these low mass stars provide information which can be useful also for our understanding of the winds of more luminous and massive early-type stars and can lead to the discovery of particularly interesting binary systems.

  11. High Energy Vision: Processing X-rays

    E-Print Network [OSTI]

    DePasquale, Joseph; Edmonds, Peter

    2015-01-01

    Astronomy is by nature a visual science. The high quality imagery produced by the world's observatories can be a key to effectively engaging with the public and helping to inspire the next generation of scientists. Creating compelling astronomical imagery can, however, be particularly challenging in the non-optical wavelength regimes. In the case of X-ray astronomy, where the amount of light available to create an image is severely limited, it is necessary to employ sophisticated image processing algorithms to translate light beyond human vision into imagery that is aesthetically pleasing while still being scientifically accurate. This paper provides a brief overview of the history of X-ray astronomy leading to the deployment of NASA's Chandra X-ray Observatory, followed by an examination of the specific challenges posed by processing X-ray imagery. The authors then explore image processing techniques used to mitigate such processing challenges in order to create effective public imagery for X-ray astronomy. ...

  12. High-resolution X-ray spectroscopy of Theta Car

    E-Print Network [OSTI]

    Yael Naze; Gregor Rauw

    2008-08-25

    Context : The peculiar hot star Theta Car in the open cluster IC2602 is a blue straggler as well as a single-line binary of short period (2.2d). Aims : Its high-energy properties are not well known, though X-rays can provide useful constraints on the energetic processes at work in binaries as well as in peculiar, single objects. Methods : We present the analysis of a 50ks exposure taken with the XMM-Newton observatory. It provides medium as well as high-resolution spectroscopy. Results : Our high-resolution spectroscopy analysis reveals a very soft spectrum with multiple temperature components (1--6MK) and an X-ray flux slightly below the `canonical' value (log[L_X(0.1-10.)/L_{BOL}] ~ -7). The X-ray lines appear surprisingly narrow and unshifted, reminiscent of those of beta Cru and tau Sco. Their relative intensities confirm the anomalous abundances detected in the optical domain (C strongly depleted, N strongly enriched, O slightly depleted). In addition, the X-ray data favor a slight depletion in neon and iron, but they are less conclusive for the magnesium abundance (solar-like?). While no significant changes occur during the XMM-Newton observation, variability in the X-ray domain is detected on the long-term range. The formation radius of the X-ray emission is loosely constrained to <5 R_sol, which allows for a range of models (wind-shock, corona, magnetic confinement,...) though not all of them can be reconciled with the softness of the spectrum and the narrowness of the lines.

  13. Sampling-based Uncertainty Quantification in Deconvolution of X-ray Radiographs

    SciTech Connect (OSTI)

    Howard, M. [NSTec; Luttman, A. [NSTec; Fowler, M. [NSTec

    2014-11-01

    In imaging applications that focus on quantitative analysis{such as X-ray radiography in the security sciences--it is necessary to be able to reliably estimate the uncertainties in the processing algorithms applied to the image data, and deconvolving the system blur out of the image is usually an essential step. In this work we solve the deconvolution problem within a Bayesian framework for edge-enhancing reconstruction with uncertainty quantification. The likelihood is a normal approximation to the Poisson likelihood, and the prior is generated from a classical total variation regularized Poisson deconvolution. Samples from the corresponding posterior distribution are computed using a Markov chain Monte Carlo approach, giving a pointwise measure of uncertainty in the final, deconvolved signal. We demonstrate the results on real data used to calibrate a high-energy X-ray source and show that this approach gives reconstructions as good as classical regularization methods, while mitigating many of their drawbacks.

  14. Data Selection Criteria for Spectroscopic Measurements of Neutron Star Radii with X-ray Bursts

    E-Print Network [OSTI]

    Ozel, Feryal; Guver, Tolga

    2015-01-01

    Data selection and the determination of systematic uncertainties in the spectroscopic measurements of neutron star radii from thermonuclear X-ray bursts have been the subject of numerous recent studies. In one approach, the uncertainties and outliers were determined by a data-driven Bayesian mixture model, whereas in a second approach, data selection was performed by requiring that the observations follow theoretical expectations. We show here that, due to inherent limitations in the data, the theoretically expected trends are not discernible in the majority of X-ray bursts even if they are present. Therefore, the proposed theoretical selection criteria are not practical with the current data for distinguishing clean data sets from outliers. Furthermore, when the data limitations are not taken into account, the theoretically motivated approach selects a small subset of bursts with properties that are in fact inconsistent with the underlying assumptions of the method. We conclude that the data-driven selection...

  15. X-ray Mass Estimates at $z\\sim0.3$ for the CNOC Cluster Sample

    E-Print Network [OSTI]

    Aaron D. Lewis; E. Ellingson; Simon L. Morris; R. G. Carlberg

    1999-01-06

    Results are presented from the analysis of ROSAT HRI and PSPC observations of the CNOC subsample of the EMSS high redshift galaxy clusters. X-ray surface brightness profiles of 14 clusters with $0.17 < z < 0.55$ are constructed and fit to isothermal $\\beta$ models. Where possible, we use both the HRI and PSPC data to constrain the fit. Under the assumptions of isothermality, hydrostatic equilibrium, and spherical symmetry, we derive total X-ray masses within a range of radii from 141 to $526 h^{-1}_{100}$ kpc. These masses are compared with both the dynamical masses obtained from galaxy velocities and the projected masses from published gravitational lensing studies. We find no systematic bias between X-ray and dynamical methods across the sample, with an average $M_{Dyn}/M_X=1.04\\pm0.07$, although individual clusters exhibit mass discrepancies up to a factor of 2. We estimate that the systematic effects due to cooling flows, non-equilibrium systems and temperature gradients affect the average mass ratio by no more than $15-20%$. Weak gravitational lensing masses appear to be systematically higher than X-ray results by factors of $\\sim50%$, while strong lensing estimates show larger discrepancies (factors of $\\sim2.5$). However, these comparisons are complicated by the need to extrapolate the X-ray data to larger or smaller radii. X-ray derived cluster gas masses are calculated, from which we obtain a cluster baryon fraction of $\\sim5%h^{-3/2}_{100}$, yielding $\\Omega_0 \\sim0.3h^{-1/2}_{100}$.

  16. Micellar structure from comparison of X-ray and neutron small-angle scattering

    E-Print Network [OSTI]

    Boyer, Edmond

    249 Micellar structure from comparison of X-ray and neutron small-angle scattering T. Zemb and P according to the method developed by Hayter and Penfold. Both X-ray and neutron scattering signals, or by a combination of both. It has been shown recent- ly [1, 2] that it is possible in neutron scattering studies

  17. Imaging Performance of the XMM-Newton X-ray telescopes

    E-Print Network [OSTI]

    B. Aschenbach; U. Briel; F. Haberl; H. Braeuninger; W. Burkert; A. Oppitz; P. Gondoin; D. Lumb

    2000-07-18

    The in-orbit imaging performance of the three X-ray telescopes on board of the X-ray astronomy observatory XMM-Newton is presented and compared with the performance measured on ground at the MPE PANTER test facility. The comparison shows an excellent agreement between the on ground and in-orbit performance.

  18. Flat Quartz-Crystal X-ray Spectrometer for Nuclear Forensics Applications 

    E-Print Network [OSTI]

    Goodsell, Alison

    2012-10-19

    and U. Using the flat quartz-crystal x-ray spectrometer and customized collimation system, the Monte Carlo N-Particle (MCNP) simulations showed the 103.7 keV Pu x-ray peak signal-to-noise ratio improved by a factor of 13 and decreased the percent error...

  19. X-ray imaging and controlled solidification of Al-Cu alloys toward microstructures by design

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Clarke, Amy J.; Tourret, Damien; Imhoff, Seth D.; Gibbs, Paul J.; Fezzaa, Kamel; Cooley, Jason C.; Lee, Wah -Keat; Deriy, Alex; Patterson, Brian M.; Papin, Pallas A.; et al

    2015-01-30

    X-ray imaging, which permits the microscopic visualization of metal alloy solidification dynamics, can be coupled with controlled solidification to create microstructures by design. This x-ray image shows a process-derived composite microstructure being made from a eutectic Al-17.1 at.%Cu alloy by successive solidification and remelting steps.

  20. Metal binding in proteins: machine learning complements X-ray absorption spectroscopy

    E-Print Network [OSTI]

    Passerini, Andrea

    Metal binding in proteins: machine learning complements X-ray absorption spectroscopy Marco Lippi1 for the identification of metalloproteins and metal binding sites on a genome scale. An extensive evaluation conducted in combination with X- ray absorption spectroscopy shows the great potentiality of the approach. 1 Metal binding

  1. Relations between concurrent hard X-ray sources in solar flares

    E-Print Network [OSTI]

    Marina Battaglia; Arnold O. Benz

    2006-06-14

    Context: Solar flares release a large fraction of their energy into non-thermal electrons, but it is not clear where and how. Bremsstrahlung X-rays are observed from the corona and chromosphere. Aims: We aim to characterize the acceleration process by the coronal source and its leakage toward the footpoints in the chromosphere. The relations between the sources reflect the geometry and constrict the configuration of the flare. Methods: We studied solar flares of GOES class larger than M1 with three or more hard X-ray sources observed simultaneously in the course of the flare. The events were observed with the X-ray satellite RHESSI from February 2002 until July 2005. We used imaging spectroscopy methods to determine the spectral evolution of each source in each event. The images of all of the five events show two sources visible only at high energies (footpoints) and one source only visible at low energies (coronal or looptop source, in two cases situated over the limb). Results: We find soft-hard-soft behavior in both, coronal source and footpoints. The coronal source is nearly always softer than the footpoints. The footpoint spectra differ significantly only in one event out of five. Conclusions: The observations are consistent with acceleration in the coronal source and an intricate connection between the corona and chromosphere.

  2. X-rays Illuminate Ancient Archimedes Text

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorkingLos Alamos verifies largest single goldWindX-RayX-RayX-ray

  3. High power x-ray welding of metal-matrix composites

    DOE Patents [OSTI]

    Rosenberg, Richard A. (Naperville, IL); Goeppner, George A. (Orland Park, IL); Noonan, John R. (Naperville, IL); Farrell, William J. (Flossmoor, IL); Ma, Qing (Westmont, IL)

    1999-01-01

    A method for joining metal-matrix composites (MMCs) by using high power x-rays as a volumetric heat source is provided. The method involves directing an x-ray to the weld line between two adjacent MMCs materials to create an irradiated region or melt zone. The x-rays have a power density greater than about 10.sup.4 watts/cm.sup.2 and provide the volumetric heat required to join the MMC materials. Importantly, the reinforcing material of the metal-matrix composites remains uniformly distributed in the melt zone, and the strength of the MMCs are not diminished. In an alternate embodiment, high power x-rays are used to provide the volumetric heat required to weld metal elements, including metal elements comprised of metal alloys. In an alternate embodiment, high power x-rays are used to provide the volumetric heat required to weld metal elements, including metal elements comprised of metal alloys.

  4. Investigation of the signature of lung tissue in X-ray grating-based phase-contrast imaging

    E-Print Network [OSTI]

    Weber, Thomas; Haas, Wilhelm; Pelzer, Georg; Rieger, Jens; Ritter, André; Wucherer, Lukas; Braun, Jan Matthias; Durst, Jürgen; Michel, Thilo; Anton, Gisela

    2012-01-01

    Purpose: Grating-based X-ray phase-contrast imaging is a promising modality increasing the soft tissue contrast in medical imaging. In this work, the signature of lung tissue in X-ray grating-based physe-contrast imaging is investigated. Methods: We used a Talbot-Lau interferometer for our investigations of two C57BL/6 mice. Both underwent projection imaging and computed tomography. Results: The results show that the three images obtained by X-ray phase-contrast imaging show complementary anatomical structures. Especially the dark field image allows a more-exact determination of the position of the lung in the chest cavity. Conclusion: Due to its sensitivity to granular structures, the dark field image may be used for the diagnosis of lung diseases in earlier stages or without a CT scan. Furthermore, X-ray phase-contrast imaging may also have great potential in the application of animal laboratory sciences to reduce the number of required animals used in long-term translational, toxicity, and regenerative med...

  5. X-ray Imaging Shows Feather Patterns of First Birds

    Broader source: Energy.gov [DOE]

    One-hundred million years ago, what did birds look like? Scientists have taken a huge step towards finding the answer, leaving the creative imaginations behind such classics as Jurassic Park, The Land Before Time and Dinotopic to contend with science.

  6. X-ray Spectral Properties of the BAT AGN Sample

    E-Print Network [OSTI]

    L. M. Winter; R. Mushotzky; C. S. Reynolds; J. Tueller

    2008-08-04

    The 9-month Swift Burst Alert Telescope (BAT) catalog provides the first unbiased (log N_H = 0.03) AGN. In this paper, we present the collected X-ray properties (0.3 - 12keV) for the 153 AGN detected. In addition, we examine the X-ray properties for a complete sample of non-beamed sources, above the Galactic plane. Of these, 45% are best fit by simple power law models while 55% require the more complex partial covering model. One of our goals was to determine the fraction of "hidden" AGN, which we define as sources with scattering fractions Marshall et al. 1980). From the log N-log S relationship, we show that we are complete to log S < -11 in the 2-10 keV band. Both the collected X-ray properties of our uniform sample and the log N-log S relationship will now provide valuable input to X-ray background models for z ~ 0. (abridged)

  7. The X-ray emission of the gamma Cassiopiae stars

    E-Print Network [OSTI]

    Smith, Myron A; Motch, C

    2015-01-01

    Long considered as the "odd man out" among X-ray emitting Be stars, \\gamma Cas (B0.5e\\,IV) is now recognized as the prototype of a class of stars that emit hard thermal X-rays. Our classification differs from the historical use of the term "gamma Cas stars" defined from optical properties alone. The luminosity output of this class contributes significantly to the hard X-ray production of massive stars in the Galaxy. The gamma Cas stars have light curves showing variability on a few broadly-defined timescales and spectra indicative of an optically thin plasma consisting of one or more hot thermal components. By now 9--13 Galactic \\approx B0-1.5e main sequence stars are judged to be members or candidate members of the \\gc\\ class. Conservative criteria for this designation are for a \\approxB0-1.5e III-V star to have an X-ray luminosity of 10^{32}--10^{33} ergs s^{-1}, a hot thermal spectrum containing the short wavelength Ly \\alpha FeXXV and FeXXVI lines and the fluorescence FeK feature all in emission. If therm...

  8. X-rays at Solid-Liquid Surfaces

    SciTech Connect (OSTI)

    Dosch, Helmut (Max Planck Institute for Metals Research) [Max Planck Institute for Metals Research

    2007-05-02

    Solid-liquid interfaces play an important role in many areas of current and future technologies, and in our biosphere. They play a key role in the development of nanofluidics and nanotribology, which sensitively depend on our knowledge of the microscopic structures and phenomena at the solid-liquid interface. The detailed understanding of how a fluid meets a wall is also a theoretical challenge. In particular, the phenomena at repulsive walls are of interest, since they affect many different phenomena, such as water-repellent surfaces or the role of the hydrophobic interaction in protein folding. Recent x-ray reflectivity studies of various solid-liquid interfaces have disclosed rather intriguiing phenomena, which will be discussed in this lecture: premelting of ice in contact with silica; liquid Pb in contact with Si; water in contact with hydrophobic surfaces. These experiments, carried out with high-energy x-ray microbeams, reveal detailed insight into the liquid density profile closest to the wall. A detailed insight into atomistic phenomena at solid-liquid interfaces is also a prerequisite in the microscopic control of electrochemical reactions at interfaces. Recent x-ray studies show the enormous future potential of such non-destructive analytical tools for the in situ observation of (electro-)chemical surface reactions. This lecture will review recent x-ray experiments on solid-liquid interfaces.

  9. Small Angle X-Ray Scattering Detector

    DOE Patents [OSTI]

    Hessler, Jan P.

    2004-06-15

    A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

  10. X-ray source for mammography

    DOE Patents [OSTI]

    Logan, Clinton M. (Pleasanton, CA)

    1994-01-01

    An x-ray source utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms.

  11. X-ray source for mammography

    DOE Patents [OSTI]

    Logan, C.M.

    1994-12-20

    An x-ray source is described utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms. 6 figures.

  12. Compton backscattered collmated X-ray source

    DOE Patents [OSTI]

    Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

    2000-01-01

    A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

  13. Compton backscattered collimated x-ray source

    DOE Patents [OSTI]

    Ruth, R.D.; Huang, Z.

    1998-10-20

    A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

  14. Compton backscattered collimated x-ray source

    DOE Patents [OSTI]

    Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

    1998-01-01

    A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

  15. X-ray laser driven gold targets

    SciTech Connect (OSTI)

    Petrova, Tz. B., E-mail: lina.petrova@nrl.navy.mil; Whitney, K. G.; Davis, J. [Plasma Physics Division, Naval Research Laboratory, 4555 Overlook Ave. SW, Washington, DC 20375 (United States)] [Plasma Physics Division, Naval Research Laboratory, 4555 Overlook Ave. SW, Washington, DC 20375 (United States)

    2014-03-15

    The femtosecond population dynamics of gold irradiated by a coherent high-intensity (>10{sup 17}?W/cm{sup 2}) x-ray laser pulse is investigated theoretically. There are two aspects to the assembled model. One is the construction of a detailed model of platinum-like gold inclusive of all inner-shell states that are created by photoionization of atomic gold and decay either by radiative or Auger processes. Second is the computation of the population dynamics that ensues when an x-ray pulse is absorbed in gold. The hole state generation depends on the intensity and wavelength of the driving x-ray pulse. The excited state populations reached during a few femtosecond timescales are high enough to generate population inversions, whose gain coefficients are calculated. These amplified lines in the emitted x-ray spectrum provide important diagnostics of the radiation dynamics and also suggest a nonlinear way to increase the frequency of the coherent output x-ray pulses relative to the frequency of the driver input x-ray pulse.

  16. Some new schemes for producing high-accuracy elliptical X-ray mirrors by elastic bending

    SciTech Connect (OSTI)

    Padmore, H.A.; Howells, M.R.; Irick, S.; Renner, T.; Sandler, R.; Koo, Y.-M.

    1996-08-01

    Although x-ray micro-foci can be produced by a variety of diffractive methods, grazing incidence mirrors are the only route to an achromatic focus. In this paper we describe our efforts to produce elliptically shaped mirrors with the very high figure accuracy necessary for producing a micro-focus. The motivation for this work is provided by the need to produce achromatic foci for a range of applications ranging from tunable micro-focus x-ray photoelectron spectroscopy ({mu}-XPS) at soft x-ray energies to micro-focus white beam x-ray diffraction ({mu}-XRD) at hard x-ray energies. We describe the methodology of beam bending, a practical example of a system we have produced for {mu}-XRD, and results demonstrating the production of a surface with micro-radian figure accuracy.

  17. An X-ray Reprocessing Model of Disk Thermal Emission in Type 1 Seyfert Galaxies

    E-Print Network [OSTI]

    James Chiang

    2002-02-12

    Using a geometry consisting of a hot central Comptonizing plasma surrounded by a thin accretion disk, we model the optical through hard X-ray spectral energy distributions of the type 1 Seyfert galaxies NGC 3516 and NGC 7469. As in the model proposed by Poutanen, Krolik, & Ryde for the X-ray binary Cygnus X-1 and later applied to Seyfert galaxies by Zdziarski, Lubi\\'nski, & Smith, feedback between the radiation reprocessed by the disk and the thermal Comptonization emission from the hot central plasma plays a pivotal role in determining the X-ray spectrum, and as we show, the optical and ultraviolet spectra as well. Seemingly uncorrelated optical/UV and X-ray light curves, similar to those which have been observed from these objects can be explained by variations in the size, shape, and temperature of the Comptonizing plasma. Furthermore, by positing a disk mass accretion rate which satisfies a condition for global energy balance between the thermal Comptonization luminosity and the power available from accretion, one can predict the spectral properties of the hard X-ray continuum above $\\sim 50$ keV in type 1 Seyfert galaxies. Forthcoming measurements of the hard X-ray continuum by more sensitive hard X-ray and soft $\\gamma$-ray telescopes, in conjunction with simultaneous optical, UV, and soft X-ray monitoring, will allow the mass accretion rates to be directly constrained for these sources in the context of this model.

  18. SWIFT X-RAY OBSERVATIONS OF CLASSICAL NOVAE. II. THE SUPER SOFT SOURCE SAMPLE

    SciTech Connect (OSTI)

    Schwarz, Greg J.; Ness, Jan-Uwe; Osborne, J. P.; Page, K. L.; Evans, P. A.; Beardmore, A. P.; Walter, Frederick M.; Andrew Helton, L.; Woodward, Charles E.; Bode, Mike; Starrfield, Sumner; Drake, Jeremy J.

    2011-12-01

    The Swift gamma-ray burst satellite is an excellent facility for studying novae. Its rapid response time and sensitive X-ray detector provides an unparalleled opportunity to investigate the previously poorly sampled evolution of novae in the X-ray regime. This paper presents Swift observations of 52 Galactic/Magellanic Cloud novae. We included the X-Ray Telescope (0.3-10 keV) instrument count rates and the UltraViolet and Optical Telescope (1700-8000 A) filter photometry. Also included in the analysis are the publicly available pointed observations of 10 additional novae the X-ray archives. This is the largest X-ray sample of Galactic/Magellanic Cloud novae yet assembled and consists of 26 novae with Super Soft X-ray emission, 19 from Swift observations. The data set shows that the faster novae have an early hard X-ray phase that is usually missing in slower novae. The Super Soft X-ray phase occurs earlier and does not last as long in fast novae compared to slower novae. All the Swift novae with sufficient observations show that novae are highly variable with rapid variability and different periodicities. In the majority of cases, nuclear burning ceases less than three years after the outburst begins. Previous relationships, such as the nuclear burning duration versus t{sub 2} or the expansion velocity of the eject and nuclear burning duration versus the orbital period, are shown to be poorly correlated with the full sample indicating that additional factors beyond the white dwarf mass and binary separation play important roles in the evolution of a nova outburst. Finally, we confirm two optical phenomena that are correlated with strong, soft X-ray emission which can be used to further increase the efficiency of X-ray campaigns.

  19. Electron Acceleration for X-ray Production Using Paired Pyroelectric Crystals Jeffrey Geuther, Yaron Danon, Frank Saglime, Bryndol Sones

    E-Print Network [OSTI]

    Danon, Yaron

    crystal was also tested. The counts per thermal cycle and maximum energy of the x-ray spectra were shown-ray generator, and to suggest innovative methods to improve the x-ray yield and increase the endpoint energy-vacuum conditions has been shown to be a viable method of producing x-rays. The z-negative face of the crystal forms

  20. New Homogeneous Standards by Atomic Layer Deposition for Synchrotron X-ray Fluorescence and Absorption Spectroscopies.

    SciTech Connect (OSTI)

    Butterworth, A.L.; Becker, N.; Gainsforth, Z.; Lanzirotti, A.; Newville, M.; Proslier, T.; Stodolna, J.; Sutton, S.; Tyliszczak, T.; Westphal, A.J.; Zasadzinski, J. (UCB)

    2012-03-13

    Quantification of synchrotron XRF analyses is typically done through comparisons with measurements on the NIST SRM 1832/1833 thin film standards. Unfortunately, these standards are inhomogeneous on small scales at the tens of percent level. We are synthesizing new homogeneous multilayer standards using the Atomic Layer Deposition technique and characterizing them using multiple analytical methods, including ellipsometry, Rutherford Back Scattering at Evans Analytical, Synchrotron X-ray Fluorescence (SXRF) at Advanced Photon Source (APS) Beamline 13-ID, Synchrotron X-ray Absorption Spectroscopy (XAS) at Advanced Light Source (ALS) Beamlines 11.0.2 and 5.3.2.1 and by electron microscopy techniques. Our motivation for developing much-needed cross-calibration of synchrotron techniques is borne from coordinated analyses of particles captured in the aerogel of the NASA Stardust Interstellar Dust Collector (SIDC). The Stardust Interstellar Dust Preliminary Examination (ISPE) team have characterized three sub-nanogram, {approx}1{micro}m-sized fragments considered as candidates to be the first contemporary interstellar dust ever collected, based on their chemistries and trajectories. The candidates were analyzed in small wedges of aerogel in which they were extracted from the larger collector, using high sensitivity, high spatial resolution >3 keV synchrotron x-ray fluorescence spectroscopy (SXRF) and <2 keV synchrotron x-ray transmission microscopy (STXM) during Stardust ISPE. The ISPE synchrotron techniques have complementary capabilities. Hard X-ray SXRF is sensitive to sub-fg mass of elements Z {ge} 20 (calcium) and has a spatial resolution as low as 90nm. X-ray Diffraction data were collected simultaneously with SXRF data. Soft X-ray STXM at ALS beamline 11.0.2 can detect fg-mass of most elements, including cosmochemically important oxygen, magnesium, aluminum and silicon, which are invisible to SXRF in this application. ALS beamline 11.0.2 has spatial resolution better than 25 nm. Limiting factors for Stardust STXM analyses were self-imposed limits of photon dose due to radiation damage concerns, and significant attenuation of <1500 eV X-rays by {approx}80{micro}m thick, {approx}25 mg/cm{sup 3} density silica aerogel capture medium. In practice, the ISPE team characterized the major, light elements using STXM (O, Mg, Al, Si) and the heavier minor and trace elements using SXRF. The two data sets overlapped only with minor Fe and Ni ({approx}1% mass abundance), providing few quantitative cross-checks. New improved standards for cross calibration are essential for consortium-based analyses of Stardust interstellar and cometary particles, IDPs. Indeed, they have far reaching application across the whole synchrotron-based analytical community. We have synthesized three ALD multilayers simultaneously on silicon nitride membranes and silicon and characterized them using RBS (on Si), XRF (on Si{sub 3}N{sub 4}) and STXM/XAS (holey Si{sub 3}N{sub 4}). The systems we have started to work with are Al-Zn-Fe and Y-Mg-Er. We have found these ALD multi-layers to be uniform at {micro}m- to nm scales, and have found excellent consistency between four analytical techniques so far. The ALD films can also be used as a standard for e-beam instruments, eg., TEM EELS or EDX. After some early issues with the consistency of coatings to the back-side of the membrane windows, we are confident to be able to show multi-analytical agreement to within 10%. As the precision improves, we can use the new standards to verify or improve the tabulated cross-sections.

  1. Standard test method for determination of bromine and chlorine in UF6 and uranyl nitrate by X-Ray fluorescence (XRF) spectroscopy

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2001-01-01

    1.1 This method covers the determination of bromine (Br) and chlorine (Cl) in uranium hexafluoride (UF6) and uranyl nitrate solution. The method as written covers the determination of bromine in UF6 over the concentration range of 0.2 to 8 ?g/g, uranium basis. The chlorine in UF6 can be determined over the range of 4 to 160 ?g/g, uranium basis. Higher concentrations may be covered by appropriate dilutions. The detection limit for Br is 0.2 ?g/g uranium basis and for Cl is 4 ?g/g uranium basis. 1.2 This standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  2. Project Title: Radiochemical Analysis by High Sensitivity Dual-Optic Micro X-ray Fluorescence

    SciTech Connect (OSTI)

    Havrilla, George J.; Gao, Ning

    2002-06-01

    A novel dual-optic micro X-ray fluorescence instrument will be developed to do radiochemical analysis of high-level radioactive wastes at DOE sites such as Savannah River Site and Hanford. This concept incorporates new X-ray optical elements such as monolithic polycapillaries and double bent crystals, which focus X-rays. The polycapillary optic can be used to focus X-rays emitted by the X-ray tube thereby increasing the X-ray flux on the sample over 1000 times. Polycapillaries will also be used to collect the X-rays from the excitation site and screen the radiation background from the radioactive species in the specimen. This dual-optic approach significantly reduces the background and increases the analyte signal thereby increasing the sensitivity of the analysis. A doubly bent crystal used as the focusing optic produces focused monochromatic X-ray excitation, which eliminates the bremsstrahlung background from the X-ray source. The coupling of the doubly bent crystal for monochromatic excitation with a polycapillary for signal collection can effectively eliminate the noise background and radiation background from the specimen. The integration of these X-ray optics increases the signal-to-noise and thereby increases the sensitivity of the analysis for low-level analytes. This work will address a key need for radiochemical analysis of high-level waste using a non-destructive, multi-element, and rapid method in a radiation environment. There is significant potential that this instrumentation could be capable of on-line analysis for process waste stream characterization at DOE sites.

  3. Development of an X-ray pixel detector with multi-port charge-coupled device for X-ray free-electron laser experiments

    SciTech Connect (OSTI)

    Kameshima, Takashi; Ono, Shun; Kudo, Togo; Ozaki, Kyosuke; Kirihara, Yoichi; Kobayashi, Kazuo; Inubushi, Yuichi; Yabashi, Makina; Hatsui, Takaki; RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5148 ; Horigome, Toshio; Holland, Andrew; Holland, Karen; Burt, David; Murao, Hajime

    2014-03-15

    This paper presents development of an X-ray pixel detector with a multi-port charge-coupled device (MPCCD) for X-ray Free-Electron laser experiments. The fabrication process of the CCD was selected based on the X-ray radiation hardness against the estimated annual dose of 1.6 × 10{sup 14} photon/mm{sup 2}. The sensor device was optimized by maximizing the full well capacity as high as 5 Me- within 50 ?m square pixels while keeping the single photon detection capability for X-ray photons higher than 6 keV and a readout speed of 60 frames/s. The system development also included a detector system for the MPCCD sensor. This paper summarizes the performance, calibration methods, and operation status.

  4. Differential phase contrast X-ray imaging system and components

    DOE Patents [OSTI]

    Stutman, Daniel; Finkenthal, Michael

    2014-07-01

    A differential phase contrast X-ray imaging system includes an X-ray illumination system, a beam splitter arranged in an optical path of the X-ray illumination system, and a detection system arranged in an optical path to detect X-rays after passing through the beam splitter.

  5. Pyroelectric crystal-based X-ray diffractometer

    E-Print Network [OSTI]

    Fernandes, Louis Edward

    2007-01-01

    We investigate the use of an Amptek Cool-X X-ray Generator for an instructional tool in the physics of x-rays, as well as a source for x-rays for crystal diffraction experiments. The x-ray source is a solid-state two-phase ...

  6. Deep x-ray lithography for micromechanics

    SciTech Connect (OSTI)

    Christenson, T.R. [Sandia National Labs., Albuquerque, NM (United States); Guckel, H. [Wisconsin Univ., Madison, WI (United States). Dept. of Electrical and Computer Engineering

    1995-08-01

    Extensions of the German LIGA process have brought about fabrication capability suitable for cost effective production of precision engineered components. The process attributes allow fabrication of mechanical components which are not capable of being made via conventional subtractive machining methods. Two process improvements have been responsible for this extended capability which involve the areas of thick photoresist application and planarization via precision lapping. Application of low-stress x-ray photoresist has been achieved using room temperature solvent bonding of a preformed photoresist sheet. Precision diamond lapping and polishing has provided a flexible process for the planarization of a wide variety of electroplated metals in the presence of photoresist. Exposure results from the 2.5 GeV National Synchrotron Light Source storage ring at Brookhaven National Laboratory have shown that structural heights of several millimeter and above are possible. The process capabilities are also well suited for microactuator fabrication. Linear and rotational magnetic microactuators have been constructed which use coil winding technology with LIGA fabricated coil forms. Actuator output forces of 1 milliNewton have been obtained with power dissipation on the order of milliWatts. A rotational microdynamometer system which is capable of measuring torque-speed data is also discussed.

  7. Phase Effects on Mesoscale Object X-ray Absorption Images

    SciTech Connect (OSTI)

    Martz, Jr., H E; Aufderheide, M B; Barty, A; Lehman, S K; Kozioziemski, B J; Schneberk, D J

    2004-09-24

    At Lawrence Livermore National Laboratory particular emphasis is being placed on the nondestructive characterization (NDC) of 'mesoscale' objects.[Martz and Albrecht 2003] We define mesoscale objects as objects that have mm extent with {micro}m features. Here we confine our discussions to x-ray imaging methods applicable to mesoscale object characterization. The goal is object recovery algorithms including phase to enable emerging high-spatial resolution x-ray imaging methods to ''see'' inside or image mesoscale-size materials and objects. To be successful our imaging characterization effort must be able to recover the object function to one micrometer or better spatial resolution over a few millimeters field-of-view with very high contrast.

  8. X-ray spectral states of microquasars

    E-Print Network [OSTI]

    Julien Malzac; Renaud Belmont

    2008-10-25

    We discuss the origin of the dramatically different X-ray spectral shapes observed in the Low Hard State (LHS: dominated by thermal comptonisation) and the High Soft State (HSS: dominated by the accretion disc thermal emission and non-thermal comptonisation in the corona). We present numerical simulations using a new code accounting for the so-called synchrotron boiler effect. These numerical simulations when compared to the data allow us to constrain the magnetic field and temperature of the hot protons in the corona. For the hard state of Cygnus X-1 we find a magnetic field below equipartition with radiation, suggesting that the corona is not powered through magnetic field dissipation (as assumed in most accretion disc corona models). On the other hand, our results also point toward proton temperatures that are substantially lower than typical temperatures of the ADAF models. Finally, we show that in both spectral states Comptonising plasma could be powered essentially through power-law acceleration of non-thermal electrons, which are then partly thermalised by the synchrotron and Coulomb boiler. This suggests that, contrary to current beliefs, the corona of the HSS and that of the LHS could be of very similar nature. The differences between the LHS and HSS coronal spectra would then be predominantly caused by the strong disc soft cooling emission which is present in the HSS and absent in the LHS.

  9. Ultrafast X-Ray Coherent Control

    SciTech Connect (OSTI)

    Reis, David

    2009-05-01

    This main purpose of this grant was to develop the nascent #12;eld of ultrafast x-ray science using accelerator-based sources, and originally developed from an idea that a laser could modulate the di#11;racting properties of a x-ray di#11;racting crystal on a fast enough time scale to switch out in time a shorter slice from the already short x-ray pulses from a synchrotron. The research was carried out primarily at the Advanced Photon Source (APS) sector 7 at Argonne National Laboratory and the Sub-Picosecond Pulse Source (SPPS) at SLAC; in anticipation of the Linac Coherent Light Source (LCLS) x-ray free electron laser that became operational in 2009 at SLAC (all National User Facilities operated by BES). The research centered on the generation, control and measurement of atomic-scale dynamics in atomic, molecular optical and condensed matter systems with temporal and spatial resolution . It helped develop the ultrafast physics, techniques and scienti#12;c case for using the unprecedented characteristics of the LCLS. The project has been very successful with results have been disseminated widely and in top journals, have been well cited in the #12;eld, and have laid the foundation for many experiments being performed on the LCLS, the world's #12;rst hard x-ray free electron laser.

  10. Oscillations During Thermonuclear X-ray Bursts

    E-Print Network [OSTI]

    Tod E. Strohmayer

    2001-01-12

    High amplitude, nearly coherent X-ray brightness oscillations during thermonuclear X-ray bursts were discovered with the Rossi X-ray Timing Explorer (RXTE) in early 1996. Spectral and timing evidence strongly supports the conclusion that these oscillations are caused by rotational modulation of the burst emission and that they reveal the spin frequency of neutron stars in low mass X-ray binaries, a long sought goal of X-ray astronomy. Studies carried out over the past year have led to the discovery of burst oscillations in four new sources, bringing to ten the number with confirmed burst oscillations. I review the status of our knowledge of these oscillations and indicate how they can be used to probe the physics of neutron stars. For a few burst oscillation sources it has been proposed that the strongest and most ubiquitous frequency is actually the first overtone of the spin frequency and hence that two nearly antipodal hot spots are present on the neutron star. This inference has important implications for both the physics of thermonuclear burning as well as the mass - radius relation for neutron stars, so its confirmation is crucial. I discuss recent attempts to confirm this hypothesis for 4U 1636-53, the source for which a signal at the putative fundamental (290 Hz) has been claimed.

  11. In Operando X-ray Diffraction and Transmission X-ray Microscopy of Lithium Sulfur Batteries

    E-Print Network [OSTI]

    Cui, Yi

    In Operando X-ray Diffraction and Transmission X-ray Microscopy of Lithium Sulfur Batteries Johanna Information ABSTRACT: Rechargeable lithium-sulfur (Li-S) batteries hold great potential for high not well understood. In this Article, these changes in Li-S batteries are studied in operando by X

  12. X-Ray Data from the X-Ray Data Booklet Online

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Thompson, Albert C.; Attwood, David T.; Gullikson, Eric M.; Howells, Malcolm R.; Kortright, Jeffrey B.; Robinson, Arthur L.; Underwood, James H.; Kim, Kwang-Je; Kirz, Janos; Lindau, Ingolf; Pianetta, Piero; Winick, Herman; Williams, Gwyn P.; Scofield, James H.

    The original X-Ray Data Booklet, published in 1985, became a classic reference source. The online version has been significantly revised and updated to reflect today's science. Hundreds of pages of authoritative data provide the x-ray properties of elements, information on synchrotron radiation, scattering processes, optics and detectors, and other related calculations, formulas, and data tables.

  13. X-ray Point Source Populations Constituting the Galactic Ridge X-ray Emission

    E-Print Network [OSTI]

    Morihana, Kumiko; Yoshida, Tessei; Ebisawa, Ken

    2013-01-01

    Apparently diffuse X-ray emission has been known to exist along the central quarter of the Galactic Plane since the beginning of the X-ray astronomy, which is referred to as the Galactic Ridge X-ray emission (GRXE). Recent deep X-ray observations have shown that numerous X-ray point sources account for a large fraction of the GRXE in the hard band (2-8 keV). However, the nature of these sources is poorly understood. Using the deepest X-ray observations made in the Chandra Bulge Field (Revnivtsev et al., 2009,2011), we present the result of a coherent photometric and spectroscopic analysis of individual X-ray point sources for the purpose of constraining their nature and deriving their fractional contributions to the hard band continuum and Fe K\\alpha line emission of the GRXE. Based on the X-ray color-color diagram, we divided the point sources into three groups: A (hard), B (soft and broad spectrum), and C (soft and peaked spectrum). The group A sources are further decomposed spectrally into thermal and non-...

  14. PUBLISHED ONLINE: 2 JULY 2013 | DOI: 10.1038/NPHYS2670 Self-organized criticality in X-ray flares of

    E-Print Network [OSTI]

    Loss, Daniel

    statistical results of X-ray flares of GRBs with known redshifts, and show that X-ray flares and solar flares-organized criticality (SOC) system. The statistical properties of X-ray flares of GRBs are similar to solar flares for the first time. On the other hand, it is well known that solar flares with a timescale of hours

  15. ELECTRON FLUX SPECTRAL IMAGING OF SOLAR FLARES THROUGH REGULARIZED ANALYSIS OF HARD X-RAY SOURCE VISIBILITIES

    E-Print Network [OSTI]

    Piana, Michele

    ELECTRON FLUX SPECTRAL IMAGING OF SOLAR FLARES THROUGH REGULARIZED ANALYSIS OF HARD X-RAY SOURCE a new method for imaging spectroscopy analysis of hard X-ray emission during solar flares. The method the method to a solar flare observed on 2002 February 20 by the RHESSI instrument. The event is characterized

  16. Modelling the radio to X-ray SED of galaxies

    E-Print Network [OSTI]

    Laura Silva; Alessandro Bressan; Gian Luigi Granato; Pasquale Panuzzo

    2001-06-07

    We present our model to interpret the SED of galaxies. The model for the UV to sub-mm SED is already well established (Silva et al 1998). We remind here its main features and show some applications. Recently we have extended the model to the radio range (Bressan et al 2001), and we have started to include the X-ray emission from the stellar component.

  17. X-ray Clusters at High Redshift

    E-Print Network [OSTI]

    I. M. Gioia

    1997-11-30

    As the largest gravitationally bound structures known, clusters provide clear constraints on the formation of structure and on the composition of the universe. Despite their extreme importance for cosmology the number of clusters at high redshift (z > 0.75) is rather small. There are only a few X-ray emitting examples reported and a handful of optically-selected ones. These clusters can provide stringent constrains on theories of large scale structure formation, if they are massive enough. I will review the status of these distant X-ray selected clusters. These objects are of special importance because their X-ray emission implies that they are massive, comparable to low redshift examples, and their existence is problematic for some theories of structure formation.

  18. Characterization of nuclear physics targets using Rutherford backscattering and particle induced x-ray emission

    E-Print Network [OSTI]

    Th. Rubehn; G. J. Wozniak; L. Phair; L. G. Moretto; Kin M. Yu

    1996-09-23

    Rutherford backscattering and particle induced x-ray emission have been utilized to precisely characterize targets used in nuclear fission experiments. The method allows for a fast and non destructive determination of target thickness, homogeneity and element composition.

  19. Thin optic surface analysis for high resolution X-ray telescopes

    E-Print Network [OSTI]

    Akilian, Mireille

    2004-01-01

    The art of glass developed throughout the years has covered artifacts ranging from crude ornaments to high precision optics used in flat panel displays, hard disk drives, and x-ray telescopes. Methods for manufacturing ...

  20. EVIDENCE OF NON-THERMAL X-RAY EMISSION FROM HH 80

    SciTech Connect (OSTI)

    López-Santiago, J.; Peri, C. S.; Benaglia, P.; Bonito, R.; Miceli, M.; Albacete-Colombo, J. F.; De Castro, E.

    2013-10-20

    Protostellar jets appear at all stages of star formation when the accretion process is still at work. Jets travel at velocities of hundreds of km s{sup –1}, creating strong shocks when interacting with the interstellar medium. Several cases of jets have been detected in X-rays, typically showing soft emission. For the first time, we report evidence of hard X-ray emission possibly related to non-thermal processes not explained by previous models of the post-shock emission predicted in the jet/ambient interaction scenario. HH 80 is located at the south head of the jet associated with the massive protostar IRAS 18162-2048. It shows soft and hard X-ray emission in regions that are spatially separated, with the soft X-ray emission region situated behind the region of hard X-ray emission. We propose a scenario for HH 80 where soft X-ray emission is associated with thermal processes from the interaction of the jet with denser ambient matter and hard X-ray emission is produced by synchrotron radiation at the front shock.

  1. Evidence Against BALS in the X-ray Bright QSO PG1416-129

    E-Print Network [OSTI]

    Paul J. Green; Thomas L. Aldcroft; Smita Mathur; Norbert Schartel

    1997-02-24

    Recent results from the ROSAT All Sky Survey, and from deep ROSAT pointings reveal that broad absorption line quasars (BALQSOs) are weak in the soft X-ray bandpass (with optical-to-X-ray spectral slope alpha_{ox}>1.8) in comparison to QSOs with normal OUV spectra (mean alpha_{ox}=1.4). One glaring exception appeared to be the nearby BALQSO PG1416-129, which is a bright ROSAT source showing no evidence for intrinsic soft X-ray absorption. We present here our new HST FOS spectrum of PG1416-129, in which we find no evidence for BALs. We show that the features resulting in the original BAL classification, based on IUE spectra, were probably spurious. On the basis of UV, X-ray and optical evidence, we conclude that PG1416-129, is not now, and has never been a BALQSO. Our result suggests that weak soft X-ray emission is a defining characteristic of true BALQSOs. If BALQSOs indeed harbor normal intrinsic spectral energy distributions, their observed soft X-ray weakness is most likely the result of absorption. The ubiquitous occurrence of weak soft X-ray emission with UV absorption (BALs) thus suggests absorbers in each energy regime that are physically associated, if not identical.

  2. X-ray diffraction study of Penicillium Vitale catalase in the complex with aminotriazole

    SciTech Connect (OSTI)

    Borovik, A. A.; Grebenko, A. I.; Melik-Adamyan, V. R.

    2011-07-15

    The three-dimensional structure of the enzyme catalase from Penicillium vitale in a complex with the inhibitor aminotriazole was solved and refined by protein X-ray crystallography methods. An analysis of the three-dimensional structure of the complex showed that the inhibition of the enzyme occurs as a result of the covalent binding of aminotriazole to the amino-acid residue His64 in the active site of the enzyme. An investigation of the three-dimensional structure of the complex resulted in the amino-acid residues being more precisely identified. The binding sites of saccharide residues and calcium ions in the protein molecule were found.

  3. Radiobiological studies using gamma and x rays.

    SciTech Connect (OSTI)

    Potter, Charles Augustus; Longley, Susan W.; Scott, Bobby R. [Lovelace Respiratory Research Institute, Albuquerque, NM; Lin, Yong [Lovelace Respiratory Research Institute, Albuquerque, NM; Wilder, Julie [Lovelace Respiratory Research Institute, Albuquerque, NM; Hutt, Julie A. [Lovelace Respiratory Research Institute, Albuquerque, NM; Padilla, Mabel T. [Lovelace Respiratory Research Institute, Albuquerque, NM; Gott, Katherine M. [Lovelace Respiratory Research Institute, Albuquerque, NM

    2013-02-01

    There are approximately 500 self-shielded research irradiators used in various facilities throughout the U.S. These facilities use radioactive sources containing either 137Cs or 60Co for a variety of biological investigations. A report from the National Academy of Sciences[1] described the issues with security of particular radiation sources and the desire for their replacement. The participants in this effort prepared two peer-reviewed publications to document the results of radiobiological studies performed using photons from 320-kV x rays and 137Cs on cell cultures and mice. The effectiveness of X rays was shown to vary with cell type.

  4. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformationJesse Bergkamp GraduateResidentialLensless Imaging of WholeX-Ray Imaging inX-Ray

  5. X-ray reflection spectra from ionized slabs

    E-Print Network [OSTI]

    R. R. Ross; A. C. Fabian; A. J. Young

    1999-02-23

    X-ray reflection spectra are an important component in the X-ray spectra of many active galactic nuclei and Galactic black hole candidates. It is likely that reflection takes place from highly ionized surfaces of the accretion disc in some cases. This can lead to strong Comptonization of the emergent iron, and other, absorption and emission features. We present such reflection spectra here, computed in a self-consistent manner with the method described by Ross and Fabian. In particular we emphasise the range where the ionization parameter (the flux to density ratio) \\xi is around and above 10^4. Such spectra may be relevant to the observed spectral features found in black hole candidates such as Cygnus X-1 in the low/hard state.

  6. Quantitative determination of mineral composition by powder x-ray diffraction

    DOE Patents [OSTI]

    Pawloski, G.A.

    1984-08-10

    An external standard intensity ratio method is used for quantitatively determining mineralogic compositions of samples by x-ray diffraction. The method uses ratios of x-ray intensity peaks from a single run. Constants are previously determined for each mineral which is to be quantitatively measured. Ratios of the highest intensity peak of each mineral to be quantified in the sample and the highest intensity peak of a reference mineral contained in the sample are used to calculate sample composition.

  7. Efficient electronic structure calculation for molecular ionization dynamics at high x-ray intensity

    E-Print Network [OSTI]

    Hao, Yajiang; Hanasaki, Kota; Son, Sang-Kil; Santra, Robin

    2015-01-01

    We present the implementation of an electronic-structure approach dedicated to ionization dynamics of molecules interacting with x-ray free-electron laser (XFEL) pulses. In our scheme, molecular orbitals for molecular core-hole states are represented by linear combination of numerical atomic orbitals that are solutions of corresponding atomic core-hole states. We demonstrate that our scheme efficiently calculates all possible multiple-hole configurations of molecules formed during XFEL pulses. The present method is suitable to investigate x-ray multiphoton multiple ionization dynamics and accompanying nuclear dynamics, providing essential information on the chemical dynamics relevant for high-intensity x-ray imaging.

  8. Streak cameras for soft x-ray and optical radiation

    SciTech Connect (OSTI)

    Medecki, H.

    1983-09-01

    The principal component of a streak camera is the image converter tube. A slit-shaped photocathode transforms the radiation into a proportional emission of electrons. An electron - optics arrangement accelerates the electrons and projects them into a phosphor screen creating the image of the slit. A pair of deflection plates deflects the electronic beam along a direction perpendicular to the main dimension of the slit. Different portions of the phosphor screen show the instantaneous image of the slit with brightness proportional to the number of emitted electrons and, consequently, to the intensity of the radiation. For our x-ray streak cameras, we use the RCA C73435A image conventer tube intended for the measurement of the radiation of light and modified to have an x-ray sensitive photocathode. Practical considerations lead to the use of transparent rather than reflecting photocathodes. Several of these camera tubes are briefly described.

  9. Optical Klystron Enhancement to SASE X-ray FELs

    SciTech Connect (OSTI)

    Ding, Yuantao; Emma, Paul; Huang, Zhirong; Kumar, Vinit

    2006-04-07

    The optical klystron enhancement to self-amplified spontaneous emission (SASE) free electron lasers (FELs) is studied in theory and in simulations. In contrast to a seeded FEL, the optical klystron gain in a SASE FEL is not sensitive to any phase mismatch between the radiation and the microbunched electron beam. The FEL performance with the addition of four optical klystrons located at the undulator long breaks in the Linac Coherent Light Source (LCLS) shows significant improvement if the uncorrelated energy spread at the undulator entrance can be controlled to a very small level. In addition, FEL saturation at shorter x-ray wavelengths (around 1.0 A) within the LCLS undulator length becomes possible. We also discuss the application of the optical klystron in a compact x-ray FEL design that employs relatively low electron beam energy together with a shorter-period undulator.

  10. First-Principles Calculation of Principal Hugoniot and K-Shell X-ray Absorption Spectra for Warm Dense KCl

    E-Print Network [OSTI]

    Zhao, Shijun; Kang, Wei; Li, Zi; Zhang, Ping; He, Xian-Tu

    2015-01-01

    Principal Hugoniot and K-shell X-ray absorption spectra of warm dense KCl are calculated using the first-principles molecular dynamics method. Evolution of electronic structures as well as the influence of the approximate description of ionization on pressure (caused by the underestimation of the energy gap between conduction bands and valence bands) in the first-principles method are illustrated by the calculation. Pressure ionization and thermal smearing are shown as the major factors to prevent the deviation of pressure from global accumulation along the Hugoniot. In addition, cancellation between electronic kinetic pressure and virial pressure further reduces the deviation. The calculation of X-ray absorption spectra shows that the band gap of KCl persists after the pressure ionization of the $3p$ electrons of Cl and K taking place at lower energy, which provides a detailed understanding to the evolution of electronic structures of warm dense matter.

  11. Anti-contamination device for cryogenic soft X-ray diffraction microscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Huang, Xiaojing; Miao, Huijie; Nelson, Johanna; Turner, Joshua; Steinbrener, Jan; Shapiro, David; Kirz, Janos; Jacobsen, Chris

    2011-05-01

    Cryogenic microscopy allows one to view frozen hydrated biological and soft matter specimens with good structural preservation and a high degree of stability against radiation damage. We describe a liquid nitrogen-cooled anti-contamination device for cryogenic X-ray diffraction microscopy. The anti-contaminator greatly reduces the buildup of ice layers on the specimen due to condensation of residual water vapor in the experimental vacuum chamber. We show by coherent X-ray diffraction measurements that this leads to fivefold reduction of background scattering, which is important for far-field X-ray diffraction microscopy of biological specimens.

  12. The TESIS project: Are type 2 QSO hidden in X-ray emitting EROs?

    E-Print Network [OSTI]

    Severgnini, P; Braito, V; Saracco, P; Longhetti, M; Bender, R; Drory, N; Feulner, G; Hopp, U; Mannucci, F; Maraston, C

    2003-01-01

    Here we present the results obtained from the analysis of 75 ksec of XMM-Newton observations of a sample of EROs selected from one MUNICS field (K'<19.5 mag). We find 6 EROs with a X-ray counterpart down to a 2--10 keV flux limit of ~10^{-15} cgs. For all of them the X-ray--to--optical flux ratios and the 2--10 keV luminosities suggest the presence of AGN. In particular, a complete X-ray spectral analysis shows that high luminosity, obscured AGNs (i.e. QSO2 candidates) are present in 3 of them.

  13. The TESIS project: Are type 2 QSO hidden in X-ray emitting EROs?

    E-Print Network [OSTI]

    P. Severgnini; R. Della Ceca; V. Braito; P. Saracco; M. Longhetti; R. Bender; N. Drory; G. Feulner; U. Hopp; F. Mannucci; C. Maraston

    2003-12-03

    Here we present the results obtained from the analysis of 75 ksec of XMM-Newton observations of a sample of EROs selected from one MUNICS field (K'<19.5 mag). We find 6 EROs with a X-ray counterpart down to a 2--10 keV flux limit of ~10^{-15} cgs. For all of them the X-ray--to--optical flux ratios and the 2--10 keV luminosities suggest the presence of AGN. In particular, a complete X-ray spectral analysis shows that high luminosity, obscured AGNs (i.e. QSO2 candidates) are present in 3 of them.

  14. Resonantly excited betatron hard X-Rays from Ionization Injected Electron Beam in a Laser Plasma Accelerator

    E-Print Network [OSTI]

    Huang, K; Li, Y F; Li, D Z; Tao, M Z; Mirzaie, M; Ma, Y; Zhao, J R; Li, M H; Chen, M; Hafz, N; Sokollik, T; Sheng, Z M; Zhang, J

    2015-01-01

    A new scheme for bright hard x-ray emission from laser wakefield electron accelerator is reported, where pure nitrogen gas is adopted. Intense Betatron x-ray beams are generated from ionization injected K-shell electrons of nitrogen into the accelerating wave bucket. The x-ray radiation shows synchrotron-like spectrum with total photon yield 8$\\times$10$^8$/shot and $10^8$ over 110keV. In particular, the betatron hard x-ray photon yield is 10 times higher compared to the case of helium gas under the same laser parameters. Particle-in-cell simulation suggests that the enhancement of the x-ray yield results from ionization injection, which enables the electrons to be quickly accelerated to the driving laser region for subsequent betatron resonance. Employing the present scheme,the single stage nitrogen gas target could be used to generate stable high brightness betatron hard x-ray beams.

  15. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservationBio-Inspired SolarAbout /Two0PhotosPresentationsWorld's

  16. Optical Identification of the Hardest X-ray Source in the ASCA Large Sky Survey

    E-Print Network [OSTI]

    M. Akiyama; K. Ohta; T. Yamada; M. Eracleous; J. P. Halpern; N. Kashikawa; M. Yagi; W. Kawasaki; M. Sakano; T. Tsuru; Y. Ueda; T. Takahashi

    1998-01-18

    We report the optical identification of the hardest X-ray source (AX J131501+3141) detected in an unbiased wide-area survey in the 0.5--10 keV band, the ASCA Large Sky Survey. The X-ray spectrum of the source is very hard and is well reproduced by a power-law component (Gamma = 1.5^+0.7_-0.6) with N_H = 6^+4_-2 *10^22 cm^-2 (Sakano et al. 1998). We have found a galaxy with R=15.62 mag near the center of the error circle for the X-ray source. The optical spectrum of the galaxy shows only narrow emission lines whose ratios correspond to those of a type 2 Seyfert galaxy at z = 0.072, implying an absorption-corrected X-ray luminosity of 2*10^43 erg sec^-1 (2--10 keV) and M_B = -20.93 mag. A radio point source is also associated with the center of the galaxy. We thus identify the X-ray source with this galaxy as an obscured AGN. The hidden nature of the nucleus of the galaxy in the optical band is consistent with the X-ray spectrum. These results support the idea that the obscured AGNs/QSOs contribute significantly to the cosmic X-ray background in the hard band at the faint flux level.

  17. DISCOVERY OF AN EXTENDED X-RAY JET IN AP LIBRAE

    SciTech Connect (OSTI)

    Kaufmann, S.; Wagner, S. J.; Tibolla, O.

    2013-10-20

    Chandra observations of the low-energy-peaked BL Lac object (LBL) AP Librae (AP Lib) revealed the clear discovery of a non-thermal X-ray jet. AP Lib is the first LBL with an extended non-thermal X-ray jet that shows emission into the very high energy range. The X-ray jet has an extension of ?15''(? 14 kpc). The X-ray jet morphology is similar to the radio jet observed with Very Large Array at 1.36 GHz emerging in the southeast direction and bends by 50° at a distance of 12'' toward the northeast. The intensity profiles of the X-ray emission studied are consistent with those found in the radio range. The spectral analysis reveals that the X-ray spectra of the core and jet region are both inverse-Compton-(IC)-dominated. This adds to a still small sample of BL Lac objects whose X-ray jets are IC-dominated and thus more similar to the high-luminosity Fanaroff-Riley II sources than to the low-luminosity Fanaroff-Riley I objects, which are usually considered to be the parent population of BL Lac objects.

  18. Phase-contrast imaging using ultrafast x-rays in laser-shocked materials

    SciTech Connect (OSTI)

    Workman, Jonathan B; Cobble, James A; Flippo, Kirk; Gautier, Donald C; Montgomery, David S; Offermann, Dustin T

    2010-01-01

    High-energy x-rays, > 10-keV, can be efficiently produced from ultrafast laser target interactions with many applications to dense target materials in Inertial Confinement Fusion (ICF) and High-Energy Density Physics (HEDP). These same x-rays can also be applied to measurements of low-density materials inside high-density hohlraum environments. In the experiments presented, high-energy x-ray images of laser-shocked polystyrene are produced through phase contrast imaging. The plastic targets are nominally transparent to traditional x-ray absorption but show detailed features in regions of high density gradients due to refractive effects often called phase contrast imaging. The 200-TW Trident laser is used both to produce the x-ray source and to shock the polystyrene target. X-rays at 17-keV produced from 2-ps, 100-J laser interactions with a 12-micron molybdenum wire are used to produce a small source size, required for optimizing refractive effects. Shocks are driven in the 1-mm thick polystyrene target using 2-ns, 250-J, 532-nm laser drive with phase plates. X-ray images of shocks compare well to 1-D hydro calculations, HELIOS-CR.

  19. Catalog of supersoft X-ray sources

    E-Print Network [OSTI]

    J. Greiner

    2000-05-11

    This catalog comprises an up-to-date (December 1999) list of luminous (>10^36 erg/s), binary supersoft X-ray sources. This electronic version (including the accompannying Web-pages) supersedes the printed version of Greiner (1996).

  20. SLAC All Access: X-ray Microscope

    ScienceCinema (OSTI)

    Nelson, Johanna; Liu, Yijin

    2014-06-13

    SLAC physicists Johanna Nelson and Yijin Liu give a brief overview of the X-ray microscope at the Stanford Synchrotron Radiation Lightsource (SSRL) that is helping improve rechargeable-battery technology by letting researchers peek into the inner workings of batteries as they operate.

  1. The Long Term Stability of Oscillations During Thermonuclear X-ray Bursts: Constraining the Binary X-ray Mass Function

    E-Print Network [OSTI]

    Tod E. Strohmayer; William Zhang; Jean H. Swank; Iosif Lapidus

    1998-06-18

    We report on the long term stability of the millisecond oscillations observed with the Rossi X-ray Timing Explorer (RXTE) during thermonuclear X-ray bursts from the low mass X-ray binaries (LMXB) 4U 1728-34 and 4U 1636-53. We show that bursts from 4U 1728-34 spanning more than 1.5 years have observed asymptotic oscillation periods which are within 0.2 microsec. of each other, well within the magnitude which could be produced by the orbital motion of the neutron star in a typical LMXB. This stability implies a timescale to change the oscillation period of > 23,000 years, suggesting a highly stable process such as stellar rotation as the oscillation mechanism. We show that period offsets in three distinct bursts from 4U 1636-53 can be plausibly interpreted as due to orbital motion of the neutron star in this 3.8 hour binary system. We discuss the constraints on the mass function which can in principle be derived using this technique.

  2. SIMULTANEOUS X-RAY AND ULTRAVIOLET OBSERVATIONS OF THE SW SEXTANTIS STAR DW URSAE MAJORIS

    SciTech Connect (OSTI)

    Hoard, D. W.; Wachter, S. [Spitzer Science Center, California Institute of Technology, MS 220-6, 1200 E. California Blvd., Pasadena, CA 91125 (United States); Lu, Ting-Ni [Institute of Astronomy, National Tsing Hua University, Hsinchu 30013, Taiwan (China); Knigge, Christian [School of Physics and Astronomy, University of Southampton, Highfield, Southampton SO17 1BJ (United Kingdom); Homer, Lee; Szkody, Paula [Department of Astronomy, University of Washington, Box 351580, Seattle, WA 98195-1580 (United States); Still, M. [NASA Ames Research Center, Moffett Field, CA 94035 (United States); Long, Knox S. [Space Telescope Science Institute, 3700 San Martin Drive, Baltimore, MD 21218 (United States); Dhillon, V. S., E-mail: hoard@ipac.caltech.ed [Department of Physics and Astronomy, University of Sheffield, Sheffield S3 7RH (United Kingdom)

    2010-11-15

    We present the first pointed X-ray observation of DW Ursae Majoris, a novalike cataclysmic variable (CV) and one of the archetype members of the SW Sextantis class, obtained with the XMM-Newton satellite. These data provide the first detailed look at an SW Sex star in the X-ray regime (with previous X-ray knowledge of the SW Sex stars limited primarily to weak or non-detections in the ROSAT All Sky Survey). It is also one of only a few XMM-Newton observations (to date) of any high mass transfer rate novalike CV, and the only one in the evolutionarily important 3-4 hr orbital period range. The observed X-ray spectrum of DW UMa is very soft, with {approx}95% of the detected X-ray photons at energies <2 keV. The spectrum can be fit equally well by a one-component cooling flow model, with a temperature range of 0.2-3.5 keV, or a two-component, two-temperature thermal plasma model, containing hard ({approx}5-6 keV) and soft ({approx}0.8 keV) components. The X-ray light curve of DW UMa shows a likely partial eclipse, implying X-ray reprocessing in a vertically extended region, and an orbital modulation, implying a structural asymmetry in the X-ray reprocessing site (e.g., it cannot be a uniform corona). We also obtained a simultaneous near-ultraviolet light curve of DW UMa using the Optical Monitor on XMM-Newton. This light curve is similar in appearance to published optical-UV light curves of DW UMa and shows a prominent deep eclipse. Regardless of the exact nature of the X-ray reprocessing site in DW UMa, the lack of a prominent hard X-ray total eclipse and very low fraction of high energy X-rays point to the presence of an optically and geometrically thick accretion disk that obscures the boundary layer and modifies the X-ray spectrum emitted near the white dwarf.

  3. Beam based calibration of X-ray pinhole camera in SSRF

    E-Print Network [OSTI]

    Yong-Bin Leng; Guo-Qing Huang; Man-Zhou Zhang; Zhi-Chu Chen; Jie Chen; Kai-Rong Ye

    2011-03-25

    The Shanghai Synchrotron Radiation Facility (SSRF) contains a 3.5-GeV storage ring serving as a national X-ray synchrotron radiation user facility characterized by a low emittance and a low coupling. The stability and quality of the electron beams are monitored continuously by an array of diagnostics. In particular, an X-ray pinhole camera is employed in the diagnostics beamline of the ring to characterize the position, size, and emittance of the beam. The performance of the measurement of the transverse electron beam size is given by the width of the point spread function (PSF) of the X-ray pinhole camera. Typically the point spread function of the X-ray pinhole camera is calculated via analytical or numerical method. In this paper we will introduce a new beam based calibration method to derive the width of the PSF online.

  4. High-resolution ab initio three-dimensional x-ray diffraction microscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Chapman, Henry N.; Barty, Anton; Marchesini, Stefano; Noy, Aleksandr; Hau-Riege, Stefan P.; Cui, Congwu; Howells, Malcolm R.; Rosen, Rachel; He, Haifeng; Spence, John C. H.; et al

    2006-01-01

    Coherent x-ray diffraction microscopy is a method of imaging nonperiodic isolated objects at resolutions limited, in principle, by only the wavelength and largest scattering angles recorded. We demonstrate x-ray diffraction imaging with high resolution in all three dimensions, as determined by a quantitative analysis of the reconstructed volume images. These images are retrieved from the three-dimensional diffraction data using no a priori knowledge about the shape or composition of the object, which has never before been demonstrated on a nonperiodic object. We also construct two-dimensional images of thick objects with greatly increased depth of focus (without loss of transverse spatialmore »resolution). These methods can be used to image biological and materials science samples at high resolution with x-ray undulator radiation and establishes the techniques to be used in atomic-resolution ultrafast imaging at x-ray free-electron laser sources.« less

  5. The hidden X-ray breaks in afterglow light curves

    SciTech Connect (OSTI)

    Curran, P. A.; Wijers, R. A. M. J.; Horst, A. J. van der; Starling, R. L. C.

    2008-05-22

    Gamma-Ray Burst (GRB) afterglow observations in the Swift era have a perceived lack of achromatic jet breaks compared to the BeppoSAX, or pre-Swift era. Specifically, relatively few breaks, consistent with jet breaks, are observed in the X-ray light curves of these bursts. If these breaks are truly missing, it has serious consequences for the interpretation of GRB jet collimation and energy requirements, and the use of GRBs as standard candles.Here we address the issue of X-ray breaks which are possibly 'hidden' and hence the light curves are misinterpreted as being single power-laws. We show how a number of precedents, including GRB 990510 and GRB 060206, exist for such hidden breaks and how, even with the well sampled light curves of the Swift era, these breaks may be left misidentified. We do so by synthesising X-ray light curves and finding general trends via Monte Carlo analysis. Furthermore, in light of these simulations, we discuss how to best identify achromatic breaks in afterglow light curves via multi-wavelength analysis.

  6. Rise Time Measurement for Ultrafast X-Ray Pulses

    DOE Patents [OSTI]

    Celliers, Peter M.; Weber, Franz A.; Moon, Stephen J.

    2005-04-05

    A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

  7. X-ray small-angle scattering from sputtered CeO{sub 2}/C bilayers

    SciTech Connect (OSTI)

    Haviar, S.; Dubau, M.; Khalakhan, I.; Vorokhta, M.; Matolinova, I.; Matolin, V.; Vales, V.; Endres, J.; Holy, V.; Buljan, M.; Bernstorff, S.

    2013-01-14

    Surface and interface morphology of cerium oxide/carbon bilayers used as thin-film catalysts is studied by grazing-incidence small-angle x-ray scattering, scanning electron microscopy, and atomic-force microscopy, and the dependence of the structural parameters on the thicknesses of the constituting layers is investigated. The applicability of x-ray scattering and its advantages over standard analytical methods are discussed.

  8. X-ray imaging crystal spectrometer for extended X-ray sources

    DOE Patents [OSTI]

    Bitter, Manfred L. (Princeton, NJ); Fraenkel, Ben (Jerusalem, IL); Gorman, James L. (Bordentown, NJ); Hill, Kenneth W. (Lawrenceville, NJ); Roquemore, A. Lane (Cranbury, NJ); Stodiek, Wolfgang (Princeton, NJ); von Goeler, Schweickhard E. (Princeton, NJ)

    2001-01-01

    Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

  9. X-RAY POINT-SOURCE POPULATIONS CONSTITUTING THE GALACTIC RIDGE X-RAY EMISSION

    SciTech Connect (OSTI)

    Morihana, Kumiko [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan)] [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Tsujimoto, Masahiro; Ebisawa, Ken [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan)] [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan); Yoshida, Tessei, E-mail: morihana@crab.riken.jp [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)] [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)

    2013-03-20

    Apparently diffuse X-ray emission has been known to exist along the central quarter of the Galactic Plane since the beginning of X-ray astronomy; this is referred to as the Galactic Ridge X-ray emission (GRXE). Recent deep X-ray observations have shown that numerous X-ray point sources account for a large fraction of the GRXE in the hard band (2-8 keV). However, the nature of these sources is poorly understood. Using the deepest X-ray observations made in the Chandra bulge field, we present the result of a coherent photometric and spectroscopic analysis of individual X-ray point sources for the purpose of constraining their nature and deriving their fractional contributions to the hard-band continuum and Fe K line emission of the GRXE. Based on the X-ray color-color diagram, we divided the point sources into three groups: A (hard), B (soft and broad spectrum), and C (soft and peaked spectrum). The group A sources are further decomposed spectrally into thermal and non-thermal sources with different fractions in different flux ranges. From their X-ray properties, we speculate that the group A non-thermal sources are mostly active galactic nuclei and the thermal sources are mostly white dwarf (WD) binaries such as magnetic and non-magnetic cataclysmic variables (CVs), pre-CVs, and symbiotic stars, whereas the group B and C sources are X-ray active stars in flares and quiescence, respectively. In the log N-log S curve of the 2-8 keV band, the group A non-thermal sources are dominant above Almost-Equal-To 10{sup -14} erg cm{sup -2} s{sup -1}, which is gradually taken over by Galactic sources in the fainter flux ranges. The Fe K{alpha} emission is mostly from the group A thermal (WD binaries) and the group B (X-ray active stars) sources.

  10. A Chandra X-ray Study of NGC 1068: II. The Luminous X-ray Source Population

    E-Print Network [OSTI]

    David A. Smith; Andrew S. Wilson

    2003-03-17

    We present an analysis of the compact X-ray source population in the Seyfert~2 galaxy NGC 1068, imaged with Chandra. We find a total of 84 compact sources, of which 66 are projected onto the galactic disk of NGC 1068. Spectra of the brightest sources have been modeled with both multi-color disk blackbody and power-law models. The power-law model provides the better description of the spectrum for most of these sources. Five sources have 0.4-8 keV intrinsic luminosities greater than 10^{39} erg/s, assuming that their emission is isotropic and that they are associated with NGC 1068. We refer to these sources as Intermediate Luminosity X-ray Objects (IXOs). If these five sources are X-ray binaries accreting with luminosities that are both sub-Eddington and isotropic, then the implied source masses are >7 solar masses, and so they are inferred to be black holes. The brightest source has a much harder spectrum (Gamma = 0.9\\pm0.1) than that found in Galactic black hole candidates and other IXOs. It also shows large-amplitude variability on both short-term and long-term timescales. The ratio of the number of sources with luminosities greater than 2.1 x 10^{38} erg/s in the 0.4-8 keV band to the rate of massive star formation is the same, to within a factor of two, for NGC 1068, the Antennae, NGC 5194 (the main galaxy in M51), and the Circinus galaxy. This suggests that the rate of production of X-ray binaries per massive star is approximately the same for galaxies with currently active star formation, including ``starbursts''.

  11. X-ray/UV variability and the origin of soft X-ray excess emission from II Zw 177

    E-Print Network [OSTI]

    Pal, Main; Misra, Ranjeev; Pawar, Pramod K

    2016-01-01

    We study X-ray and UV emission from the narrow-line Seyfert 1 galaxy II~Zw~177 using a $137\\ks$ long and another $13\\ks$ short \\xmm{} observation performed in 2012 and 2001, respectively. Both observations show soft X-ray excess emission contributing $76.9\\pm4.9\\%$ in 2012 and $58.8\\pm10.2\\%$ in 2001 in the $0.3-2\\kev$ band. We find that both blurred reflection from an ionized disc and Comptonized disc emission describe the observed soft excess well. Time-resolved spectroscopy on scales of $\\sim20\\ks$ reveals strong correlation between the soft excess and the powerlaw components. The fractional variability amplitude $F_{var}$ derived from EPIC-pn lightcurves at different energy bands is nearly constant ($F_{var} \\sim20\\%$). This is in contrast to other AGNs where the lack of short term variation in soft X-ray excess emission has been attributed to intense light bending in the framework of the "lamppost" model. Thus, the variations in powerlaw emission are most likely intrinsic to corona rather than just due t...

  12. Low-level determination of plutonium by gamma and L x-ray spectroscopy

    SciTech Connect (OSTI)

    Nitsche, H.; Gatti, R.C.; Lee, S.C.

    1991-04-01

    we have developed an analytical method for detection of {sup 239}Pu in aqueous samples at concentrations as low as 10{sup {minus}10} M. This nuclear counting technique utilizes the uranium L X-rays, which follow the alpha decay of plutonium. Because L X-rays are specific for the element and not for the individual isotopes, the isotopic composition of the plutonium sample must be known. The counting efficiency in the 11--23 keV range is determined from a plutonium standard, and the concentration of the sample is then calculated from the L X-ray count and the isotopic composition. The total L X-ray count is corrected for possible contributions from other radionuclides present as impurities by measuring the low-energy gamma spectrum for each contaminant to establish specific photon/X-ray ratios. The ratios are important when {sup 241}Pu and {sup 242}Pu are measured, because the respective decay chain members produce non-U L X-rays. This new method can replace the use of labor-intensive radiochemical separation techniques and elaborate activation methods for analysis of {sup 239}Pu in aqueous samples. It is also applicable for assaying plutonium in liquid wastes that pose possible hazards to the environment.

  13. Molecular orientation in soft matter thin films studied by resonant soft x-ray reflectivity

    SciTech Connect (OSTI)

    Mezger, Markus; Jerome, Blandine; Kortright, Jeffrey B; Valvidares, Manuel; Gullikson, Eric M; Giglia, Angelo; Mahne, Nicola; Nannarone, Stefano

    2011-04-05

    We present a technique to study depth profiles of molecular orientation in soft matter thin films with nanometer resolution. The method is based on dichroism in resonant soft x-ray reflectivity using linear s and p polarization. It combines the chemical sensitivity of near-edge x-ray absorption fine structure spectroscopy to specific molecular bonds and their orientation relative to the polarization of the incident beam with the precise depth profiling capability of x-ray reflectivity. We demonstrate these capabilities on side chain liquid crystalline polymer thin films with soft x-ray reflectivity data at the carbon K edge. Optical constants of the anisotropic refractive index ellipsoid were obtained from a quantitative analysis using the Berreman formalism. For films up to 50 nm thickness we find that the degree of orientation of the long axis exhibits no depth variation and is independent of the film thickness.

  14. High-resolution x-ray diffraction microscopy of specifically labeled yeast cells

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Nelson, Johanna; Huang, Xiaojing; Steinbrener, Jan; Shapiro, David; Kirz, Janos; Marchesini, Stephano; Neiman, Aaron M.; Turner, Joshua J.; Jacobsen, Chris

    2010-04-20

    X-ray diffraction microscopy complements other x-ray microscopy methods by being free of lens-imposed radiation dose and resolution limits, and it allows for high-resolution imaging of biological specimens too thick to be viewed by electron microscopy. We report here the highest resolution (11-13 nm) x-ray diffraction micrograph of biological specimens, and a demonstration of molecular-specific gold labeling at different depths within cells via through-focus propagation of the reconstructed wavefield. The lectin concanavalin A conjugated to colloidal gold particles was used to label the ?-mannan sugar in the cell wall of the yeast Saccharomyces cerevisiae. Cells were plunge-frozen in liquid ethane andmore »freeze-dried, after which they were imaged whole using x-ray diffraction microscopy at 750 eV photon energy.« less

  15. Molecular orientation in soft matter thin films studied by resonant soft X-ray reflectivity

    SciTech Connect (OSTI)

    Mezger, Markus; Jerome, Blandine; Kortright, Jeffrey B.; Valvidares, Manuel; Gullikson, Eric; Giglia, Angelo; Mahne, Nicola; Nannarone, Stefano

    2011-01-12

    We present a technique to study depth profiles of molecular orientation in soft matter thin films with nanometer resolution. The method is based on dichroism in resonant soft X-ray reflectivity using linear s- and p-polarization. It combines the chemical sensitivity of Near-Edge X-ray Absorption Fine Structure spectroscopy to specific molecular bonds and their orientation relative to the polarization of the incident beam with the precise depth profiling capability of X-ray reflectivity. We demonstrate these capabilities on side chain liquid crystalline polymer thin films with soft X-ray reflectivity data at the carbon K edge. Optical constants of the anisotropic refractive index ellipsoid were obtained from a quantitative analysis using the Berreman formalism. For films up to 50 nm thickness we find that the degree of orientation of the long axis exhibits no depth variation and isindependent of the film thickness.

  16. Temporal structure of X-ray radiation pulses of picosecond laser plasma

    SciTech Connect (OSTI)

    Belyaev, V S; Kovkov, D V; Matafonov, A P; Karabadzhak, G F; Raikunov, G G [Central Research Institute of Machine Building, Korolev, Moscow region (Russian Federation); Faenov, A Ya; Pikuz, S A; Skobelev, I Yu; Pikuz, T A; Fokin, D A; Fortov, V E [Joint Institute for High Temperatures, Russian Academy of Sciences, Moscow (Russian Federation); Ignat'ev, G N; Kapitanov, S V; Krapiva, P S; Korotkov, K E [All-Russian Institute of Automatics, Moscow (Russian Federation)

    2013-09-30

    The shape of the X-ray pulse generated by picosecond laser plasma is experimentally studied. The unusual phenomenon was experimentally observed for the first time for targets made of moderate-heavy chemical elements, namely, the pulse of hard X-ray radiation generated by laser plasma at the laser radiation flux of ?10{sup 18} W cm{sup -2} had a longer duration than the pulse of softer X-ray radiation. A simple kinetic model is suggested for explaining this fact. We have suggested a method for controlling the temporal shape of X-ray pulse emitted by laser plasma by varying the contrast of laser pulse. (interaction of laser radiation with matter)

  17. Note: Dynamic strain field mapping with synchrotron X-ray digital image correlation

    SciTech Connect (OSTI)

    Lu, L. [CAS Key Laboratory of Mechanical Behavior and Design of Materials, Department of Modern Mechanics, University of Science and Technology of China, Hefei, Anhui 230027 (China); The Peac Institute of Multiscale Sciences, Chengdu, Sichuan 610207 (China); Fan, D.; Luo, S. N., E-mail: sluo@pims.ac.cn [The Peac Institute of Multiscale Sciences, Chengdu, Sichuan 610207 (China); Bie, B. X. [The Peac Institute of Multiscale Sciences, Chengdu, Sichuan 610207 (China); School of Science, Wuhan University of Technology, Wuhan, Hubei 430070 (China); Ran, X. X.; Qi, M. L., E-mail: qiml@whut.edu.cn [School of Science, Wuhan University of Technology, Wuhan, Hubei 430070 (China); Parab, N.; Sun, J. Z.; Liao, H. J.; Hudspeth, M. C.; Claus, B. [School of Aeronautics and Astronautics, Purdue University, West Lafayette, Indiana 47907 (United States); Fezzaa, K.; Sun, T. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Chen, W. [School of Aeronautics and Astronautics, Purdue University, West Lafayette, Indiana 47907 (United States); School of Material Science Engineering, Purdue University, West Lafayette, Indiana 47907 (United States); Gong, X. L., E-mail: gongxl@ustc.edu.cn [CAS Key Laboratory of Mechanical Behavior and Design of Materials, Department of Modern Mechanics, University of Science and Technology of China, Hefei, Anhui 230027 (China)

    2014-07-15

    We present a dynamic strain field mapping method based on synchrotron X-ray digital image correlation (XDIC). Synchrotron X-ray sources are advantageous for imaging with exceptional spatial and temporal resolutions, and X-ray speckles can be produced either from surface roughness or internal inhomogeneities. Combining speckled X-ray imaging with DIC allows one to map strain fields with high resolutions. Based on experiments on void growth in Al and deformation of a granular material during Kolsky bar/gas gun loading at the Advanced Photon Source beamline 32ID, we demonstrate the feasibility of dynamic XDIC. XDIC is particularly useful for dynamic, in-volume, measurements on opaque materials under high strain-rate, large, deformation.

  18. High-resolution x-ray diffraction microscopy of specifically labeled yeast cells

    SciTech Connect (OSTI)

    Nelson, Johanna; Huang, Xiaojing; Steinbrener, Jan; Shapiro, David; Kirz, Janos; Marchesini, Stephano; Neiman, Aaron M.; Turner, Joshua J.; Jacobsen, Chris

    2010-04-20

    X-ray diffraction microscopy complements other x-ray microscopy methods by being free of lens-imposed radiation dose and resolution limits, and it allows for high-resolution imaging of biological specimens too thick to be viewed by electron microscopy. We report here the highest resolution (11-13 nm) x-ray diffraction micrograph of biological specimens, and a demonstration of molecular-specific gold labeling at different depths within cells via through-focus propagation of the reconstructed wavefield. The lectin concanavalin A conjugated to colloidal gold particles was used to label the ?-mannan sugar in the cell wall of the yeast Saccharomyces cerevisiae. Cells were plunge-frozen in liquid ethane and freeze-dried, after which they were imaged whole using x-ray diffraction microscopy at 750 eV photon energy.

  19. X-ray temperature distribution function of clusters in presence of large non-radial motions

    E-Print Network [OSTI]

    A. Del Popolo; M. Gambera

    2004-01-29

    We consider the non-radial motions, originating in the outskirts of clusters of galaxies and we show how it may reduce the discrepancy between Cold Dark Matter (CDM) predicted X-ray temperature distribution function of clusters of galaxies and that really observed, so resolving the problem of the X-ray clusters abundance over-production predicted by the CDM model. We construct the X-ray temperature distribution function using Press-Schechter's (1974) theory and Evrard's (1990) prescriptions for the mass-temperature relation, taking also account of the non-radial motions originating from the gravitational interaction of the quadrupole moment of the protocluster. Then, we compare our X-ray temperature distribution function with the tidal field of the matter of the neighboring protostructures. We find that the model produces a reasonable cluster temperature distribution.

  20. Evidence of Bulk Acceleration of the GRB X-ray Flare Emission Region

    E-Print Network [OSTI]

    Uhm, Z Lucas

    2015-01-01

    Gamma-ray bursts (GRBs), the most luminous explosions in the universe, invoke relativistic jets beaming towards Earth with the highest velocities for bulk motion in the universe. Some of them are followed by softer, less energetic, X-ray flares, which also move with relativistic velocities towards Earth. Observations and theoretical modeling suggest that X-ray flares share a similar physical mechanism as GRB prompt emission itself. Here we show a clear observational evidence that the X-ray flare emission region is undergoing rapid acceleration as the photons are emitted. The observed X-ray flare light curves and photon index evolution can be interpreted within a simple toy model invoking synchrotron radiation in an accelerating emission region far from the GRB central engine. Such an acceleration process demands an additional energy dissipation source other than kinetic energy, which points towards a significant Poynting-flux in the emission region.

  1. Achieving hard X-ray nanofocusing using a wedged multilayer Laue lens

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Huang, Xiaojing; Conley, Raymond; Bouet, Nathalie; Zhou, Juan; Macrander, Albert; Maser, Jorg; Yan, Hanfei; Nazaretski, Evgeny; Lauer, Kenneth; Harder, Ross; et al

    2015-05-04

    We report on the fabrication and the characterization of a wedged multilayer Laue lens for x-ray nanofocusing. The lens was fabricated using a sputtering deposition technique, in which a specially designed mask was employed to introduce a thickness gradient in the lateral direction of the multilayer. X-ray characterization shows an efficiency of 27% and a focus size of 26 nm at 14.6 keV, in a good agreement with theoretical calculations. These results indicate that the desired wedging is achieved in the fabricated structure. We anticipate that continuous development on wedged MLLs will advance x-ray nanofocusing optics to new frontiers andmore »enrich capabilities and opportunities for hard X-ray microscopy.« less

  2. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing...

  3. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    times science has used high-brilliance x-rays to look so closely at these reactions. Lead author Dr. David Mueller at the ALS using x-rays to characterize working fuel cells....

  4. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Using Light to Control How X Rays Interact with Matter Print Wednesday, 27 January 2010 00:00 Schemes that use one light...

  5. A World's Top-10 X-ray Crystal Structure

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    A World's Top-10 X-ray Crystal Structure October 7, 2014 Bookmark and Share Philip Coppens An x-ray crystal structure solved by Philip Coppens has been chosen as one of the world's...

  6. Dawn of x-ray nonlinear optics | Stanford Synchrotron Radiation...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Dawn of x-ray nonlinear optics Wednesday, July 8, 2015 - 3:00pm SLAC, Redtail Hawk Conference Room 108A Speaker: David Reis, PULSE Program Description X-ray free electron lasers...

  7. Staff Research Physicist (X-Ray Spectroscopy) | Princeton Plasma...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    position to work on X-ray spectroscopy, atomic physics, X-ray instrumentation, and high energy density physics. Near-term research goals include participating in the design,...

  8. Synchrotron X-ray Diffraction Study of Microtubules Buckling and Bundling under Osmotic Stress: A Probe of Interprotofilament Interactions

    E-Print Network [OSTI]

    Weeks, Eric R.

    Synchrotron X-ray Diffraction Study of Microtubules Buckling and Bundling under Osmotic Stress the microtubule wall. Synchrotron x-ray diffraction of microtubules under increasing osmotic stress shows (SAXRD) study of MTs subjected to osmotic stress [5] and depletion attraction [6] due to added poly

  9. A Chandra X-ray Study of NGC 1068 - I. Observations of Extended Emission

    E-Print Network [OSTI]

    A. J. Young; A. S. Wilson; P. L. Shopbell

    2001-04-02

    We report sub arc-second resolution X-ray imaging-spectroscopy of the archetypal type 2 Seyfert galaxy NGC 1068 with the Chandra X-ray Observatory. The observations reveal the detailed structure and spectra of the 13 kpc-extent nebulosity previously imaged at lower resolution with ROSAT. The Chandra image shows a bright, compact source coincident with the brightest radio and optical emission; this source is extended by \\simeq 1.5 arcsec (165 pc) in the same direction as the nuclear optical line and radio continuum emission. Bright X-ray emission extends \\simeq 5 arcsec (550 pc) to the NE and coincides with the NE radio lobe and gas in the narrow line region. The large-scale emission shows trailing spiral arms and other structures. Numerous point sources associated with NGC 1068 are seen. There is a very strong correlation between the X-ray emission and the high excitation ionized gas seen in HST and ground-based [O III] \\lambda 5007 images. The X-rays to the NE of the nucleus are absorbed by only the Galactic column density and thus originate from the near side of the disk of NGC 1068. In contrast the X-rays to the SW are more highly absorbed and must come from gas in the disk or on the far side of it. This geometry is similar to that inferred for the narrow line region and radio lobes. (Abstract truncated).

  10. HARD X-RAY OBSERVATIONS OF A JET AND ACCELERATED ELECTRONS IN THE CORONA

    SciTech Connect (OSTI)

    Glesener, Lindsay; Lin, R. P.; Krucker, Saem, E-mail: glesener@ssl.berkeley.edu [Space Science Laboratory, UC Berkeley, 7 Gauss Way, Berkeley, CA 94720 (United States)

    2012-07-20

    We report the first hard X-ray observation of a solar jet on the limb with flare footpoints occulted, so that faint emission from accelerated electrons in the corona can be studied in detail. In this event on 2003 August 21, RHESSI observed a double coronal hard X-ray source in the pre-impulsive phase at both thermal and nonthermal energies. In the impulsive phase, the first of two hard X-ray bursts consists of a single thermal/nonthermal source coinciding with the lower of the two earlier sources, and the second burst shows an additional nonthermal, elongated source, spatially and temporally coincident with the coronal jet. Analysis of the jet hard X-ray source shows that collisional losses by accelerated electrons can deposit enough energy to generate the jet. The hard X-ray time profile above 20 keV matches that of the accompanying Type III and broadband gyrosynchrotron radio emission, indicating both accelerated electrons escaping outward along the jet path and electrons trapped in the flare loop. The double coronal hard X-ray source, the open field lines indicated by Type III bursts, and the presence of a small post-flare loop are consistent with significant electron acceleration in an interchange reconnection geometry.

  11. X-rays from Supernova Remnants

    E-Print Network [OSTI]

    B. Aschenbach

    2002-08-28

    A summary of X-ray observations of supernova remnants is presented including the explosion fragment A of the Vela SNR, Tycho, N132D, RX J0852-4622, the Crab Nebula and the 'bulls eye', and SN 1987A, high-lighting the progress made with Chandra and XMM-Newton and touching upon the questions which arise from these observations and which might inspire future research.

  12. The X-ray Telescope of CAST

    E-Print Network [OSTI]

    M. Kuster; H. Bräuninger; S. Cébrian; M. Davenport; C. Elefteriadis; J. Englhauser; H. Fischer; J. Franz; P. Friedrich; R. Hartmann; F. H. Heinsius; D. H. H. Hoffmann; G. Hoffmeister; J. N. Joux; D. Kang; K. Königsmann; R. Kotthaus; T. Papaevangelou; C. Lasseur; A. Lippitsch; G. Lutz; J. Morales; A. Rodríguez; L. Strüder; J. Vogel; K. Zioutas

    2007-05-10

    The Cern Axion Solar Telescope (CAST) is in operation and taking data since 2003. The main objective of the CAST experiment is to search for a hypothetical pseudoscalar boson, the axion, which might be produced in the core of the sun. The basic physics process CAST is based on is the time inverted Primakoff effect, by which an axion can be converted into a detectable photon in an external electromagnetic field. The resulting X-ray photons are expected to be thermally distributed between 1 and 7 keV. The most sensitive detector system of CAST is a pn-CCD detector combined with a Wolter I type X-ray mirror system. With the X-ray telescope of CAST a background reduction of more than 2 orders off magnitude is achieved, such that for the first time the axion photon coupling constant g_agg can be probed beyond the best astrophysical constraints g_agg < 1 x 10^-10 GeV^-1.

  13. Portable Parallel Beam X-Ray Diffraction System | Department...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    than 50 pounds, and uses about 50 watts of power. The X-Beam uses polycapillary x-ray optics to collect x-rays over a large solid angle from a low-power x-ray source and to form...

  14. Small Angle X-ray Scattering (SAXS) Laboratory Learning Experiences

    E-Print Network [OSTI]

    Meagher, Mary

    .A. & Svergun D.I. (1987). Structure Analysis by Small-Angle X-Ray and Neutron Scattering. NY: Plenum PressSmall Angle X-ray Scattering (SAXS) Laboratory Learning Experiences o - Use of small angle X-ray scattering instrumentation o - Programs that you will use SAXS (BRUKER AXS) PRIMUS (Konarev, Volkov, Koch

  15. Femtosecond laser-electron x-ray source

    DOE Patents [OSTI]

    Hartemann, Frederic V.; Baldis, Hector A.; Barty, Chris P.; Gibson, David J.; Rupp, Bernhard

    2004-04-20

    A femtosecond laser-electron X-ray source. A high-brightness relativistic electron injector produces an electron beam pulse train. A system accelerates the electron beam pulse train. The femtosecond laser-electron X-ray source includes a high intra-cavity power, mode-locked laser and an x-ray optics system.

  16. Monitoring x-ray beam damage on lipid films by an integrated Brewster angle microscope/x-ray diffractometer

    E-Print Network [OSTI]

    Lee, Ka Yee C.

    Polyunsaturated lipids with conjugated tails are easily dam- aged by x-ray irradiation in the presence of oxygen samples and thin films has been detected since the beginning of x-ray studies. Dam- age to lipid samples

  17. X-ray Spectral Survey of WGACAT Quasars, II: Optical and Radio Properties of Quasars with Low Energy X-ray Cut-offs

    E-Print Network [OSTI]

    Martin Elvis; Fabrizio Fiore; Paolo Giommi; Paolo Padovani

    1997-08-05

    We have selected quasars with X-ray colors suggestive of a low energy cut-off, from the ROSAT PSPC pointed archive. We examine the radio and optical properties of these 13 quasars. Five out of the seven quasars with good optical spectra show associated optical absorption lines, with two having high delta-v candidate systems. Two other cut-off quasars show reddening associated with the quasar. We conclude that absorption is highly likely to be the cause of the X-ray cut-offs, and that the absorbing material associated with the quasars, not intervening along the line-of-sight. The suggestion that Gigahertz Peaked Sources are associated with X-ray cut-offs remains unclear with this expanded sample.

  18. The prospects for constraining dark energy with future X-ray cluster gas mass fraction measurements

    E-Print Network [OSTI]

    David Rapetti; Steven W. Allen; Adam Mantz

    2008-06-25

    We examine the ability of a future X-ray observatory to constrain dark energy via measurements of the cluster X-ray gas mass fraction, fgas. We find that fgas measurements for a sample of ~500 hot, X-ray bright, dynamically relaxed clusters, to a precision of ~5 per cent, can be used to constrain dark energy with a Dark Energy Task Force (DETF) figure of merit of 15-40, with the possibility of boosting these values by 40 per cent or more by optimizing the redshift distribution of target clusters. Such constraints are comparable to those predicted by the DETF for other leading, planned dark energy experiments. A future fgas experiment will be preceded by a large X-ray or SZ survey that will find hot, X-ray luminous clusters out to high redshifts. Short `snapshot' observations with the new X-ray observatory should then be able to identify a sample of ~500 suitably relaxed systems. The redshift, temperature and X-ray luminosity range of interest has already been partially probed by existing X-ray cluster surveys which allow reasonable estimates of the fraction of clusters that will be suitably relaxed for fgas work. Our analysis uses a Markov Chain Monte Carlo method which fully captures the relevant degeneracies between parameters and facilitates the incorporation of priors and systematic uncertainties in the analysis. We explore the effects of such uncertainties for scenarios ranging from optimistic to pessimistic. We conclude that the fgas experiment will provide tight constraints on the mean matter and dark energy densities, with a peak sensitivity for dark energy work at redshifts midway between those of supernovae and baryon acoustic oscillation/weak lensing/cluster number counts experiments. In combination, these experiments should enable a precise measurement of the evolution of dark energy. (Abridged)

  19. Template-based CTA to x-ray angio rigid registration of coronary arteries in frequency domain with automatic x-ray segmentation

    SciTech Connect (OSTI)

    Aksoy, Timur; Unal, Gozde; Demirci, Stefanie; Navab, Nassir; Degertekin, Muzaffer

    2013-10-15

    Purpose: A key challenge for image guided coronary interventions is accurate and absolutely robust image registration bringing together preinterventional information extracted from a three-dimensional (3D) patient scan and live interventional image information. In this paper, the authors present a novel scheme for 3D to two-dimensional (2D) rigid registration of coronary arteries extracted from preoperative image scan (3D) and a single segmented intraoperative x-ray angio frame in frequency and spatial domains for real-time angiography interventions by C-arm fluoroscopy.Methods: Most existing rigid registration approaches require a close initialization due to the abundance of local minima and high complexity of search algorithms. The authors' method eliminates this requirement by transforming the projections into translation-invariant Fourier domain for estimating the 3D pose. For 3D rotation recovery, template Digitally Reconstructed Radiographs (DRR) as candidate poses of 3D vessels of segmented computed tomography angiography are produced by rotating the camera (image intensifier) around the DICOM angle values with a specific range as in C-arm setup. The authors have compared the 3D poses of template DRRs with the segmented x-ray after equalizing the scales in three domains, namely, Fourier magnitude, Fourier phase, and Fourier polar. The best rotation pose candidate was chosen by one of the highest similarity measures returned by the methods in these domains. It has been noted in literature that frequency domain methods are robust against noise and occlusion which was also validated by the authors' results. 3D translation of the volume was then recovered by distance-map based BFGS optimization well suited to convex structure of the authors' objective function without local minima due to distance maps. A novel automatic x-ray vessel segmentation was also performed in this study.Results: Final results were evaluated in 2D projection space for patient data; and with ground truth values and landmark distances for the images acquired with a solid phantom vessel. Results validate that rotation recovery in frequency domain is robust against differences in segmentations in two modalities. Distance-map translation is successful in aligning coronary trees with highest possible overlap.Conclusions: Numerical and qualitative results show that single view rigid alignment in projection space is successful. This work can be extended with multiple views to resolve depth ambiguity and with deformable registration to account for nonrigid motion in patient data.

  20. The evolution of planetary nebulae. V. The diffuse X-ray emission

    E-Print Network [OSTI]

    M. Steffen; D. Schoenberner; A. Warmuth

    2008-09-05

    Observations with space-borne X-ray telescopes revealed the existence of soft, diffuse X-ray emission from the inner regions of planetary nebulae. Although the existing images support the idea that this emission arises from the hot shocked central-star wind which fills the inner cavity of a planetary nebula, existing models have difficulties to explain the observations consistently. We investigate how the inclusion of thermal conduction changes the physical parameters of the hot shocked wind gas and the amount of X-ray emission predicted by time-dependent hydrodynamical models of planetary nebulae with central stars of normal, hydrogen-rich surface composition. The radiation hydrodynamical models show that heat conduction leads to lower temperatures and higher densities within a bubble and brings the physical properties of the X-ray emitting domain into close agreement with the values derived from observations. Depending on the central-star mass and the evolutionary phase, our models predict X-ray [0.45--2.5 keV] luminosities between $10^{-8}$ and $10^{-4}$ of the stellar bolometric luminosities, in good agreement with the observations. Less than 1% of the wind power is radiated away in this X-ray band. Although temperature, density, and also the mass of the hot bubble is significantly altered by heat conduction, the dynamics of the whole system remains practically the same. Heat conduction allows the construction of nebular models which predict the correct amount of X-ray emission and at the same time are fully consistent with the observed mass-loss rate and wind speed. Thermal conduction must be considered as a viable physical process for explaining the diffuse X-ray emission from planetary nebulae with closed inner cavities. Magnetic fields must then be absent or extremely weak.

  1. Magnetic circular dichroism in x-ray absorption and core-level photoemission

    SciTech Connect (OSTI)

    Tobin, J.G.; Waddill, G.D.; Gouder, T.H.; Colmenares, C.A.; Pappas, D.P.

    1993-03-17

    Here is reported observation of magnetic circular dichroism in both x-ray absorption and core-level photoemission of ultra thin magnetic films using circularly polarized x-rays. Iron films (1--4 ML) grown on a Cu(001) substrate at 150 K and magnetized perpendicular to the surface show dramatic changes in the L{sub 2,3} branching ratio for different x-ray polarizations. For linearly-polarized x-rays perpendicular to the magnetic axis of the sample the branching ratio was 0.75. For films {ge} 2 ML, this ratio varied from 0.64 to 0.85 for photon spin parallel and anti-parallel, respectively, to the magnetic axis. This effect was observed either by changing the x-ray helicity for a fixed magnetic axis, or by reversing the magnetic axis for a fixed x-ray helicity. Our observation can be analyzed within a simple one-electron picture, if the raw branching ratios are no so that the linear value becomes statistical Furthermore, warming the films to {approximately}300 K eliminated this effect, indicating a loss of magnetization in the film over a temperature range of {approximately}30 K. Finally, reversing the relative orientation of the photon spin and the magnetic axis from parallel to anti-parallel allowed measurement of the exchange splitting of the Fe 2p and 3p core levels which were found to be 0.3 eV and 0.2 eV. respectively. These results are consistent with earlier studies, but the use of off-plane circularly-polarized x-rays from a bending magnet monochromator offers {approximately}2 orders of magnitude greater intensity than typical spin-polarization measurements. Finally, we have performed preliminary x-ray absorption studies of UFe{sub 2}, demonstrating the feasibilty of MCD measurements in 5f as well as 3d materials.

  2. Continuous motion scan ptychography: Characterization for increased speed in coherent x-ray imaging

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Deng, Junjing; Nashed, Youssef S. G.; Chen, Si; Phillips, Nicholas W.; Peterka, Tom; Ross, Rob; Vogt, Stefan; Jacobsen, Chris; Vine, David J.

    2015-02-23

    Ptychography is a coherent diffraction imaging (CDI) method for extended objects in which diffraction patterns are acquired sequentially from overlapping coherent illumination spots. The object’s complex transmission function can be reconstructed from those diffraction patterns at a spatial resolution limited only by the scattering strength of the object and the detector geometry. Most experiments to date have positioned the illumination spots on the sample using a move-settle-measure sequence in which the move and settle steps can take longer to complete than the measure step. We describe here the use of a continuous “fly-scan” mode for ptychographic data collection in whichmore »the sample is moved continuously, so that the experiment resembles one of integrating the diffraction patterns from multiple probe positions. This allows one to use multiple probe mode reconstruction methods to obtain an image of the object and also of the illumination function. We show in simulations, and in x-ray imaging experiments, some of the characteristics of fly-scan ptychography, including a factor of 25 reduction in the data acquisition time. This approach will become increasingly important as brighter x-ray sources are developed, such as diffraction limited storage rings.« less

  3. Data Selection Criteria for Spectroscopic Measurements of Neutron Star Radii with X-ray Bursts

    E-Print Network [OSTI]

    Feryal Ozel; Dimitrios Psaltis; Tolga Guver

    2015-09-09

    Data selection and the determination of systematic uncertainties in the spectroscopic measurements of neutron star radii from thermonuclear X-ray bursts have been the subject of numerous recent studies. In one approach, the uncertainties and outliers were determined by a data-driven Bayesian mixture model, whereas in a second approach, data selection was performed by requiring that the observations follow theoretical expectations. We show here that, due to inherent limitations in the data, the theoretically expected trends are not discernible in the majority of X-ray bursts even if they are present. Therefore, the proposed theoretical selection criteria are not practical with the current data for distinguishing clean data sets from outliers. Furthermore, when the data limitations are not taken into account, the theoretically motivated approach selects a small subset of bursts with properties that are in fact inconsistent with the underlying assumptions of the method. We conclude that the data-driven selection methods do not suffer from the limitations of this theoretically motivated one.

  4. X-Ray Emission from the Pre-Planetary Nebula Henize 3-1475

    E-Print Network [OSTI]

    Sahai, R; Frank, A; Morris, M; Blackman, E G; Sahai, Raghvendra; Kastner, Joel H.; Frank, Adam; Morris, Mark; Blackman, Eric G.

    2003-01-01

    We report the first detection of X-ray emission in a pre-planetary nebula, Hen 3-1475. Pre-planetary nebulae are rare objects in the short transition stage between the Asymptotic Giant Branch and planetary nebula evolutionary phases, and Hen 3-1475, characterised by a remarkable S-shaped chain of optical knots, is one of the most noteworthy members of this class. Observations with the Advanced CCD Imaging Spectrometer (ACIS) onboard the Chandra X-Ray observatory show the presence of compact emission coincident with the brightest optical knot in this bipolar object, which is displaced from the central star by 2.7 arcsec along the polar axis. Model fits to the X-ray spectrum indicate an X-ray temperature and luminosity, respectively, of (4.3-5.7) 10^6 K and (4+/-1.4) 10^{31} (D/5 kpc)^2 erg s^{-1}, respectively. Our 3-sigma upper limit on the luminosity of compact X-ray emission from the central star in Hen 3-1475 is ~5 10^{31} (D/5 kpc)^2 erg s^{-1}. The detection of X-rays in Hen 3-1475 is consistent with mod...

  5. MULTI-KEV X-RAY YIELDS FROM HIGH-Z GAS TARGETS FIELDED AT OMEGA

    SciTech Connect (OSTI)

    Kane, J O; Fournier, K B; May, M J; Colvin, J D; Thomas, C A; Marrs, R E; Compton, S M; Moody, J D; Bond, E J; Davis, J F

    2010-11-04

    The authors report on modeling of x-ray yield from gas-filled targets shot at the OMEGA laser facility. The OMEGA targets were 1.8 mm long, 1.95 mm in diameter Be cans filled with either a 50:50 Ar:Xe mixture, pure Ar, pure Kr or pure Xe at {approx} 1 atm. The OMEGA experiments heated the gas with 20 kJ of 3{omega} ({approx} 350 nm) laser energy delivered in a 1 ns square pulse. the emitted x-ray flux was monitored with the x-ray diode based DANTE instruments in the sub-keV range. Two-dimensional x-ray images (for energies 3-5 keV) of the targets were recorded with gated x-ray detectors. The x-ray spectra were recorded with the HENWAY crystal spectrometer at OMEGA. Predictions are 2D r-z cylindrical with DCA NLTE atomic physics. Models generally: (1) underpredict the Xe L-shell yields; (2) overpredict the Ar K-shell yields; (3) correctly predict the Xe thermal yields; and (4) greatly underpredict the Ar thermal yields. However, there are spreads within the data, e.g. the DMX Ar K-shell yields are correctly predicted. The predicted thermal yields show strong angular dependence.

  6. Observation of solar high energy gamma and X-ray emission and solar energetic particles

    E-Print Network [OSTI]

    Struminsky, Alexei

    2015-01-01

    We considered 18 solar flares observed between June 2010 and July 2012, in which high energy >100 MeV {\\gamma}-emission was registered by the Large Area Telescope (LAT) aboard FermiGRO. We examined for these {\\gamma}-events soft X-ray observations by GOES, hard X-ray observations by the Anti-Coincidence Shield of the SPectrometer aboard INTEGRAL (ACS SPI) and the Gamma-Ray burst Monitor (GBM) aboard FermiGRO. Hard X-ray and {\\pi}0-decay {\\gamma}-ray emissions are used as tracers of electron and proton acceleration, respectively. Bursts of hard X-ray were observed by ACS SPI during impulsive phase of 13 events. Bursts of hard X-ray >100 keV were not found during time intervals, when prolonged hard {\\gamma}-emission was registered by LAT/FermiGRO. Those events showing prolonged high-energy gamma-ray emission not accompanied by >100 keV hard X-ray emission are interpreted as an indication of either different acceleration processes for protons and electrons or as the presence of a proton population accelerated du...

  7. X-ray power and yield measurements at the refurbished Z machine

    SciTech Connect (OSTI)

    Jones, M. C., E-mail: micjone@sandia.gov; Ampleford, D. J.; Cuneo, M. E.; Hohlfelder, R.; Jennings, C. A.; Johnson, D. W.; Jones, B.; Lopez, M. R.; MacArthur, J.; Mills, J. A.; Preston, T.; Rochau, G. A.; Savage, M.; Spencer, D.; Sinars, D. B.; Porter, J. L. [Sandia National Laboratories, Albuquerque, New Mexico 87185 (United States)

    2014-08-15

    Advancements have been made in the diagnostic techniques to measure accurately the total radiated x-ray yield and power from z-pinch implosion experiments at the Z machine with high accuracy. The Z machine is capable of outputting 2 MJ and 330 TW of x-ray yield and power, and accurately measuring these quantities is imperative. We will describe work over the past several years which include the development of new diagnostics, improvements to existing diagnostics, and implementation of automated data analysis routines. A set of experiments on the Z machine were conducted in which the load and machine configuration were held constant. During this shot series, it was observed that the total z-pinch x-ray emission power determined from the two common techniques for inferring the x-ray power, a Kimfol filtered x-ray diode diagnostic and the total power and energy diagnostic, gave 449 TW and 323 TW, respectively. Our analysis shows the latter to be the more accurate interpretation. More broadly, the comparison demonstrates the necessity to consider spectral response and field of view when inferring x-ray powers from z-pinch sources.

  8. Prospects for measuring neutron-star masses and radii with X-ray pulse profile modeling

    SciTech Connect (OSTI)

    Psaltis, Dimitrios; Özel, Feryal [Astronomy Department, University of Arizona, 933 North Cherry Avenue, Tucson, AZ 85721 (United States); Chakrabarty, Deepto, E-mail: dpsaltis@email.arizona.edu, E-mail: fozel@email.arizona.edu, E-mail: deepto@mit.edu [Department of Physics and Kavli Institute for Astrophysics and Space Research, Massachusetts Institute of Technology, Cambridge, MA 02139 (United States)

    2014-06-01

    Modeling the amplitudes and shapes of the X-ray pulsations observed from hot, rotating neutron stars provides a direct method for measuring neutron-star properties. This technique constitutes an important part of the science case for the forthcoming NICER and proposed LOFT X-ray missions. In this paper, we determine the number of distinct observables that can be derived from pulse profile modeling and show that using only bolometric pulse profiles is insufficient for breaking the degeneracy between inferred neutron-star radius and mass. However, we also show that for moderately spinning (300-800 Hz) neutron stars, analysis of pulse profiles in two different energy bands provides additional constraints that allow a unique determination of the neutron-star properties. Using the fractional amplitudes of the fundamental and the second harmonic of the pulse profile in addition to the amplitude and phase difference of the spectral color oscillations, we quantify the signal-to-noise ratio necessary to achieve a specified measurement precision for neutron star radius. We find that accumulating 10{sup 6} counts in a pulse profile is sufficient to achieve a ? 5% uncertainty in the neutron star radius, which is the level of accuracy required to determine the equation of state of neutron-star matter. Finally, we formally derive the background limits that can be tolerated in the measurements of the various pulsation amplitudes as a function of the system parameters.

  9. X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO)

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Henke, B. L.; Gullikson, E. M.; Davis, J. C.

    The primary interactions of low-energy x-rays within condensed matter, viz. photoabsorption and coherent scattering, are described for photon energies outside the absorption threshold regions by using atomic scattering factors. The atomic scattering factors may be accurately determined from the atomic photoabsorption cross sections using modified Kramers-Kronig dispersion relations. From a synthesis of the currently available experimental data and recent theoretical calculations for photoabsorption, the angle-independent, forward-scattering components of the atomic scattering factors have been thus semiempirically determined and tabulated here for 92 elements and for the region 50-30,000 eV. Atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction. The incoherent scattering contributions that become significant for the light elements at the higher photon energies are similarly determined. The basic x-ray interaction relations that are used in applied x-ray physics are presented here in terms of the atomic scattering factors. The bulk optical constants are also related to the atomic scattering factors. These atomic and optical relations are applied to the detailed calculation of the reflectivity characteristics of a series of practical x-ray mirror, multilayer, and crystal monochromators. Comparisons of the results of this semiempirical,"atom-like", description of x-ray interactions for the low-energy region with those of experiment and ab initio theory are presented.

  10. Experimental investigation of beam heating in a soft X-ray scanning transmission X-ray microscope

    E-Print Network [OSTI]

    Hitchcock, Adam P.

    Experimental investigation of beam heating in a soft X-ray scanning transmission X-ray microscope and an accuracy of Æ1 C has been fabricated for scanning transmission X-ray microscopes (STXM). Here we describe at temperatures near their respective melting points as a means of checking for possible sample heating caused

  11. Supersymmetric Higgs-portal and X-ray lines

    E-Print Network [OSTI]

    Hyun Min Lee; Chan Beom Park; Myeonghun Park

    2015-01-29

    We consider a Dirac singlet fermion as thermal dark matter for explaining the X-ray line in the context of a supersymmetric Higgs-portal model or a generalized Dirac NMSSM. The Dirac singlet fermion gets a mass splitting due to their Yukawa couplings to two Higgs doublets and their superpartners, Higgsinos, after electroweak symmetry breaking. We show that a correct relic density can be obtained from thermal freeze-out, due to the co-annihilation with Higgsinos for the same Yukawa couplings. We discuss the phenomenology of the Higgsinos in this model such as displaced vertices at the LHC.

  12. Installation of soft X-ray array diagnostics and its application to tomography reconstruction using synthetic KSTAR X-ray images

    SciTech Connect (OSTI)

    Lee, Seung Hun; Jang, Juhyeok; Hong, Joohwan; Jang, Siwon; Choe, Wonho; Pacella, D.; Romano, A.; Gabellieri, L.; Kim, Junghee

    2014-11-15

    Four-array system of soft X-ray diagnostics was installed on KSTAR tokamak. Each array has 32 viewing chords of two photo-diode array detectors with spatial resolution of 2 cm. To estimate signals from the soft X-ray radiation power, typical n{sub e}, T{sub e}, and argon impurity line radiation profiles in KSTAR are chosen. The photo-diodes were absolutely calibrated as a function of the incident photon energy in 2–40 keV range with a portable X-ray tube. Two-dimensional T{sub e} image properties by multi-energy method were simulated and visualized with six combinations of beryllium filter sets within the dynamic range of signal ratio.

  13. Quality indexes based on water measurements for low and medium energy x-ray beams: A theoretical study with PENELOPE

    SciTech Connect (OSTI)

    Chica, U.; Anguiano, M.; Lallena, A. M.; Vilches, M.

    2014-01-15

    Purpose : To study the use of quality indexes based on ratios of absorbed doses in water at two different depths to characterize x-ray beams of low and medium energies. Methods : A total of 55 x-ray beam spectra were generated with the codes XCOMP5R and SPEKCALC and used as input of a series of Monte Carlo simulations performed with PENELOPE, in which the percentage depth doses in water and thek{sub Q,Q{sub 0}} factors, defined in the TRS-398 protocol, were determined for each beam. Some of these calculations were performed by simulating the ionization chamber PTW 30010. Results : The authors found that the relation betweenk{sub Q,Q{sub 0}} and the ratios of absorbed doses at two depths is almost linear. A set of ratios statistically compatible with that showing the best fit has been determined. Conclusions : The results of this study point out which of these ratios of absorbed doses in water could be used to better characterize x-ray beams of low and medium energies.

  14. Do X-ray Binary Spectral State Transition Luminosities Vary?

    E-Print Network [OSTI]

    Thomas J. Maccarone

    2003-08-02

    We tabulate the luminosities of the soft-to-hard state transitions of all X-ray binaries for which there exist good X-ray flux measurements at the time of the transition, good distance estimates, and good mass estimates for the compact star. We show that the state transition luminosities are at about 1-4% of the Eddington rate, markedly smaller than those typically quoted in the literature, with a mean value of 2%. Only the black hole candidate GRO J~1655-40 and the neutron star systems Aql X-1 and 4U 1728-34 have measured state transition luminosities inconsistent with this value at the 1$\\sigma$ level. GRO J~1655-40, in particular, shows a state transition luminosity below the mean value for the other sources at the $4\\sigma$ level. This result, combined with the known inner disk inclination angle (the disk is nearly parallel to the line of sight) from GRO J~1655-40's relativistic jets suggest that the hard X-ray emitting region in GRO J~1655-40 can have a velocity of no more than about $\\beta=0.68$, with a most likely value of about $\\beta=0.52$, and a minimum speed of $\\beta=0.45$, assuming that the variations in state transition luminosities are solely due to relativistic beaming effects. The variance in the state transition luminosities suggests an emission region with a velocity of $\\sim0.2c$. The results are discussed in terms of different emission models for the low/hard state. We also discuss the implications for measuring the dimensionless viscosity parameter $\\alpha$. We also find that if its state transitions occur at typical luminosities, then GX 339-4 is likely to be at a distance of at least 7.6 kpc, much further than typically quoted estimates.

  15. Apparatus for monitoring X-ray beam alignment

    DOE Patents [OSTI]

    Steinmeyer, P.A.

    1991-10-08

    A self-contained, hand-held apparatus is provided for monitoring alignment of an X-ray beam in an instrument employing an X-ray source. The apparatus includes a transducer assembly containing a photoresistor for providing a range of electrical signals responsive to a range of X-ray beam intensities from the X-ray beam being aligned. A circuit, powered by a 7.5 VDC power supply and containing an audio frequency pulse generator whose frequency varies with the resistance of the photoresistor, is provided for generating a range of audible sounds. A portion of the audible range corresponds to low X-ray beam intensity. Another portion of the audible range corresponds to high X-ray beam intensity. The transducer assembly may include an a photoresistor, a thin layer of X-ray fluorescent material, and a filter layer transparent to X-rays but opaque to visible light. X-rays from the beam undergoing alignment penetrate the filter layer and excite the layer of fluorescent material. The light emitted from the fluorescent material alters the resistance of the photoresistor which is in the electrical circuit including the audio pulse generator and a speaker. In employing the apparatus, the X-ray beam is aligned to a complete alignment by adjusting the X-ray beam to produce an audible sound of the maximum frequency. 2 figures.

  16. HgMn Stars as apparent X-ray emitters

    E-Print Network [OSTI]

    Hubrig, S; Mathys, G

    1998-01-01

    In the ROSAT all-sky survey 11 HgMn stars were detected as soft X-ray emitters (Berghoefer, Schmitt & Cassinelli 1996). Prior to ROSAT, X-ray observations with the Einstein Observatory had suggested that stars in the spectral range B5-A7 are devoid of X-ray emission. Since there is no X-ray emitting mechanism available for these stars (also not for HgMn stars), the usual argument in the case of an X-ray detected star of this spectral type is the existence of an unseen low-mass companion which is responsible for the X-ray emission. The purpose of the present work is to use all available data for our sample of X-ray detected HgMn stars and conclude on the nature of possible companions.

  17. X-Ray Imaging Crystal Spectrometer for Extended X-Ray Sources

    SciTech Connect (OSTI)

    Bitter, Manfred L.; Fraekel, Benjamin; Gorman, James L.; Hill, Kenneth W.; Roquemore, Lane A.; Stodiek, Wolfgang; Goeler, Schweickhard von

    1999-05-01

    Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokamak fusion experiment to provide spatially and temporally resolved data on plasma parameters such as ion temperature, toroidal and poloidal rotation, electron temperature, impurity ion charge-state distributions, and impurity transport. The imaging properties of these spherically or toroidally curved crystals provide both spectrally and spatially resolved X-ray data from the plasma using only one small spherically or toroidally curved crystal, thus eliminating the requirement for a large array of crystal spectrometers and the need to cross-calibrate the various crystals.

  18. Two-Bunch Self-Seeding for Narrow-Bandwidth Hard X-Ray Free-Electron...

    Office of Scientific and Technical Information (OSTI)

    one of the most promising methods to accomplish this. In the hard x-ray regime with high- energy electrons, this method requires a large magnetic chicane to match the path length...

  19. X-ray emission from a nanosecond-pulse discharge in an inhomogeneous electric field at atmospheric pressure

    SciTech Connect (OSTI)

    Zhang Cheng; Shao Tao; Ren Chengyan; Zhang Dongdong; Tarasenko, Victor; Kostyrya, Igor D.; Ma Hao; Yan Ping

    2012-12-15

    This paper describes experimental studies of the dependence of the X-ray intensity on the anode material in nanosecond high-voltage discharges. The discharges were generated by two nanosecond-pulse generators in atmospheric air with a highly inhomogeneous electric field by a tube-plate gap. The output pulse of the first generator (repetitive pulse generator) has a rise time of about 15 ns and a full width at half maximum of 30-40 ns. The output of the second generator (single pulse generator) has a rise time of about 0.3 ns and a full width at half maximum of 1 ns. The electrical characteristics and the X-ray emission of nanosecond-pulse discharge in atmospheric air are studied by the measurement of voltage-current waveforms, discharge images, X-ray count and dose. Our experimental results showed that the anode material rarely affects electrical characteristics, but it can significantly affect the X-ray density. Comparing the density of X-rays, it was shown that the highest x-rays density occurred in the diffuse discharge in repetitive pulse mode, then the spark discharge with a small air gap, and then the corona discharge with a large air gap, in which the X-ray density was the lowest. Therefore, it could be confirmed that the bremsstrahlung at the anode contributes to the X-ray emission from nanosecond-pulse discharges.

  20. SPEC application for achieving inelastic X-ray scattering experiment in the SSRF

    E-Print Network [OSTI]

    Lan, Xuying; Liang, Dongxu; Yan, Shuai; Mao, Chengwen; Li, Aiguo; Wang, Jie

    2015-01-01

    In order to carry out inelastic X-ray scattering (IXS) experiment at BL15U1 beamline of Shanghai Synchrotron Radiation Facility (SSRF), the data acquisition and control system based on SPEC software has been developed. The IXS experimental method needs linkage control of monochromator, silicon drift detector (SDD) and ionization chamber on continuous segment-scan mode with variable step size, and gains the data of energy, spectrum and light intensity synchronously. A method is presented for achieving this function which was not realized only by using SSCAN of Experimental Physics and Industrial Control System (EPICS). This paper shows work details including control system description, SPEC configurations for EPICS devices, macro definitions and applications in the BL15U1. An IXS experiment was executed by using the SPEC control system, its results prove that the method is feasible to perform the experiment.

  1. X-ray emission properties of galaxies in Abell 3128

    E-Print Network [OSTI]

    Russell J. Smith

    2003-07-15

    We use archival Chandra X-ray Observatory data to investigate X-ray emission from early-type galaxies in the rich z=0.06 cluster Abell 3128. By combining the X-ray count-rates from an input list of optically-selected galaxies, we obtain a statistical detection of X-ray flux, unbiased by X-ray selection limits. Using 87 galaxies with reliable Chandra data, X-ray emission is detected for galaxies down to M_B ~ -19.0, with only an upper limit determined for galaxies at M_B ~ -18.3. The ratio of X-ray to optical luminosities is consistent with recent determinations of the low-mass X-ray binary content of nearby elliptical galaxies. Taken individually, in contrast, we detect significant (3sigma) flux for only six galaxies. Of these, one is a foreground galaxy, while two are optically-faint galaxies with X-ray hardness ratios characteristic of active galactic nuclei. The remaining three detected galaxies are amongst the optically-brightest cluster members, and have softer X-ray spectra. Their X-ray flux is higher than that expected from X-ray binaries, by a factor 2-10; the excess suggests these galaxies have retained their hot gaseous haloes. The source with the highest L_X / L_B ratio is of unusual optical morphology with prominent sharp-edged shells. Notwithstanding these few exceptions, the cluster population overall exhibits X-ray properties consistent with their emission being dominated by X-ray binaries. We conclude that in rich cluster environments, interaction with the ambient intra-cluster medium acts to strip most galaxies of their hot halo gas.

  2. Metrology for the advancement of x-ray optics at the ALS

    E-Print Network [OSTI]

    Goldberg, Kenneth

    2014-01-01

    S. Yuan et al. , X-ray Optics and Instrumentation 2010,in X-ray and Neutron Optics, Springer, Berlin S. G. AlcockX-ray beam metrology and X-ray optic alignment by Hartmann

  3. X-Ray Synchrotron Emitting Fe-Rich Ejecta in SNR RCW 86

    E-Print Network [OSTI]

    Jeonghee Rho; Kristy K. Dyer; Kazimierz J. Borkowski; Stephen P. Reynolds

    2002-07-31

    Supernova remnants may exhibit both thermal and nonthermal X-ray emission. We present Chandra observations of RCW 86. Striking differences in the morphology of X-rays below 1 keV and above 2 keV point to a different physical origin. Hard X-ray emission is correlated fairly well with the edges of regions of radio emission, suggesting that these are the locations of shock waves at which both short-lived X-ray emitting electrons, and longer-lived radio-emitting electrons, are accelerated. Soft X-rays are spatially well-correlated with optical emission from nonradiative shocks, which are almost certainly portions of the outer blast wave. These soft X-rays are well fit with simple thermal plane-shock models. Harder X-rays show Fe K alpha emission and are well described with a similar soft thermal component, but a much stronger synchrotron continuum dominating above 2 keV, and a strong Fe K alpha line. Quantitative analysis of this line and the surrounding continuum shows that it cannot be produced by thermal emission from a cosmic-abundance plasma; the ionization time is too short, as shown both by the low centroid energy (6.4 keV) and the absence of oxygen lines below 1 keV. Instead, a model of a plane shock into Fe-rich ejecta, with a synchrotron continuum, provides a natural explanation. This requires that reverse shocks into ejecta be accelerating electrons to energies of order 50 TeV. We show that maximum energies of this order can be produced by radiation-limited diffusive shock acceleration at the reverse shocks.

  4. Characterization of the Electronic Structure of Silicon Nanoparticles Using X-ray Absorption and Emission

    SciTech Connect (OSTI)

    Vaverka, A M

    2008-07-15

    Resolving open questions regarding transport in nanostructures can have a huge impact on a broad range of future technologies such as light harvesting for energy. Silicon has potential to be used in many of these applications. Understanding how the band edges of nanostructures move as a function of size, surface termination and assembly is of fundamental importance in understanding the transport properties of these materials. In this thesis work I have investigated the change in the electronic structure of silicon nanoparticle assemblies as the surface termination is changed. Nanoparticles are synthesized using a thermal evaporation technique and sizes are determined using atomic force microscopy (AFM). By passivating the particles with molecules containing alcohol groups we are able to modify the size dependent band edge shifts. Both the valence and conduction bands are measured using synchrotron based x-ray absorption spectroscopy (XAS) and soft x-ray fluorescence (SXF) techniques. Particles synthesized via recrystallization of amorphous silicon/SiO{sub 2} multilayers of thicknesses below 10 nm are also investigated using the synchrotron techniques. These samples also show quantum confinement effects but the electronic structure is different from those synthesized via evaporation methods. The total bandgap is determined for all samples measured. The origins of these differences in the electronic structures are discussed.

  5. X-ray Selected Clusters of Galaxies

    E-Print Network [OSTI]

    Isabella M. Gioia

    1996-01-21

    This paper given at the meeting on "Mapping, Measuring and Modelling the Universe" presents three topics: 1) the study of the clusters and groups of galaxies found serendipitously in the North Ecliptic Pole (NEP) region of the ROSAT all-sky survey; 2) the highest redshift clusters found in the EMSS (up to z=0.82) and the cosmological implications of their very existence; 3) the gravitational lensing in the EMSS X-ray selected clusters of galaxies observed by the Hubble Space Telescope.

  6. SMB, Small Angle X-Ray Scattering

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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  7. SMB, X-ray Absorption Spectroscopy

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  8. SMB, X-ray Emission Spectroscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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  9. SMB, X-ray Fluorescence Imaging

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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  10. X-Ray Microscopy | Argonne National Laboratory

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  11. X-ray Microscopy and Imaging: FAQs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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  12. Lensless X-Ray Imaging in Reflection

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  13. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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  14. Lensless X-Ray Imaging in Reflection

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  15. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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  16. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would likeUniverseIMPACTThousand CubicResourcelogo and-E C H N I CLensless X-Ray ImagingLensless

  17. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would likeUniverseIMPACTThousand CubicResourcelogo and-E C H N I CLensless X-Ray

  18. An X-ray, IR, and Submillimeter Flare of Sagittarius A*

    E-Print Network [OSTI]

    D. P. Marrone; F. K. Baganoff; M. R. Morris; J. M. Moran; A. M. Ghez; S. D. Hornstein; C. D. Dowell; D. J. Munoz; M. W. Bautz; G. R. Ricker; W. N. Brandt; G. P. Garmire; J. R. Lu; K. Matthews; J. -H. Zhao; R. Rao; G. C. Bower

    2008-07-14

    Energetic flares are observed in the Galactic supermassive black hole Sagittarius A* from radio to X-ray wavelengths. On a few occasions, simultaneous flares have been detected in IR and X-ray observations, but clear counterparts at longer wavelengths have not been seen. We present a flare observed over several hours on 2006 July 17 with the Chandra X-Ray Observatory, the Keck II telescope, the Caltech Submillimeter Observatory, and the Submillimeter Array. All telescopes observed strong flare events, but the submillimeter peak is found to occur nearly 100 minutes after the X-ray peak. Submillimeter polarization data show linear polarization in the excess flare emission, increasing from 9% to 17% as the flare passes through its peak, consistent with a transition from optically thick to thin synchrotron emission. The temporal and spectral behavior of the flare require that the energetic electrons responsible for the emission cool faster than expected from their radiative output. This is consistent with adiabatic cooling in an expanding emission region, with X-rays produced through self-Compton scattering, although not consistent with the simplest model of such expansion. We also present a submillimeter flare that followed a bright IR flare on 2005 July 31. Compared to 2006, this event had a larger peak IR flux and similar submillimeter flux, but it lacked measurable X-ray emission. It also showed a shorter delay between the IR and submillimeter peaks. Based on these events we propose a synchrotron and self-Compton model to relate the submillimeter lag and the variable IR/X-ray luminosity ratio.

  19. Constraints on the Bulk Lorentz Factors of GRB X-Ray Flares

    E-Print Network [OSTI]

    Yi, Shuang-Xi; Wang, Fa-Yin; Dai, Zi-Gao

    2015-01-01

    X-ray flares were discovered in the afterglow phase of gamma-ray bursts (GRBs) by the {\\em Swift} satellite a decade ago and known as a canonical component in GRB X-ray afterglows. In this paper, we constrain the Lorentz factors of GRB X-ray flares using two different methods. For the first method, we estimate the lower limit on the bulk Lorentz factor with the flare duration and jet break time. In the second method, the upper limit on the Lorentz factor is derived by assuming that the X-ray flare jet has undergone saturated acceleration. We also re-estimate the initial Lorentz factor with GRB afterglow onsets, and find the coefficient of the theoretical Lorentz factor is 1.67 rather than the commonly used 2 for interstellar medium (ISM) and 1.44 for the wind case. We find that the correlation between the limited Lorentz factor and the isotropic radiation energy of X-ray flares in the ISM case is more consistent with that of prompt emission than the wind case in a statistical sense. For a comparison, the lowe...

  20. A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

    SciTech Connect (OSTI)

    Seidler, G. T. Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R.

    2014-11-15

    We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ?5 keV to ?10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}–10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

  1. X-ray K-edge analysis of drain lines in Wilhelm Hall, Ames Laboratory

    SciTech Connect (OSTI)

    Jensen, T.; Whitmore, C. |

    1999-01-05

    From August 12--27, 1998 X-ray K-edge measurements were made on drain lines in seven rooms in Wilhelm Hall, Ames Laboratory. The purpose of these measurements was to determine the extent of thorium (and other heavy metal) contamination inside these pipes. The K-edge method is a noninvasive inspection technique that can provide accurate quantification of heavy metal contamination interior to an object. Of the seven drain lines inspected, one was found to have no significant contamination, three showed significant thorium deposits, two showed mercury contamination, and one line was found to contain mercury, thorium and uranium. The K-edge measurements were found to be consistent with readings from hand-held survey meters, and provided much greater detail on the location and amount of heavy metal contamination.

  2. A semiempirical linear model of indirect, flat-panel x-ray detectors

    SciTech Connect (OSTI)

    Huang, Shih-Ying; Yang Kai; Abbey, Craig K.; Boone, John M. [Department of Biomedical Engineering, University of California, Davis, California, One Shields Avenue, Davis, California 95616 (United States) and Department of Radiology, University of California, Davis, Medical Center, 4860 Y Street, Ambulatory Care Center Suite 0505, Sacramento, California 95817 (United States); Department of Radiology, University of California, Davis, Medical Center, 4860 Y Street, Ambulatory Care Center Suite 0505, Sacramento, California 95817 (United States); Department of Psychological and Brain Sciences, University of California, Santa Barbara, California 92106 (United States); Department of Biomedical Engineering, University of California, Davis, California, One Shields Avenue, Davis, California 95616 (United States) and Department of Radiology, University of California, Davis, Medical Center, 4860 Y Street, Ambulatory Care Center Suite 3100, Sacramento, California 95817 (United States)

    2012-04-15

    Purpose: It is important to understand signal and noise transfer in the indirect, flat-panel x-ray detector when developing and optimizing imaging systems. For optimization where simulating images is necessary, this study introduces a semiempirical model to simulate projection images with user-defined x-ray fluence interaction. Methods: The signal and noise transfer in the indirect, flat-panel x-ray detectors is characterized by statistics consistent with energy-integration of x-ray photons. For an incident x-ray spectrum, x-ray photons are attenuated and absorbed in the x-ray scintillator to produce light photons, which are coupled to photodiodes for signal readout. The signal mean and variance are linearly related to the energy-integrated x-ray spectrum by empirically determined factors. With the known first- and second-order statistics, images can be simulated by incorporating multipixel signal statistics and the modulation transfer function of the imaging system. To estimate the semiempirical input to this model, 500 projection images (using an indirect, flat-panel x-ray detector in the breast CT system) were acquired with 50-100 kilovolt (kV) x-ray spectra filtered with 0.1-mm tin (Sn), 0.2-mm copper (Cu), 1.5-mm aluminum (Al), or 0.05-mm silver (Ag). The signal mean and variance of each detector element and the noise power spectra (NPS) were calculated and incorporated into this model for accuracy. Additionally, the modulation transfer function of the detector system was physically measured and incorporated in the image simulation steps. For validation purposes, simulated and measured projection images of air scans were compared using 40 kV/0.1-mm Sn, 65 kV/0.2-mm Cu, 85 kV/1.5-mm Al, and 95 kV/0.05-mm Ag. Results: The linear relationship between the measured signal statistics and the energy-integrated x-ray spectrum was confirmed and incorporated into the model. The signal mean and variance factors were linearly related to kV for each filter material (r{sup 2} of signal mean to kV: 0.91, 0.93, 0.86, and 0.99 for 0.1-mm Sn, 0.2-mm Cu, 1.5-mm Al, and 0.05-mm Ag, respectively; r{sup 2} of signal variance to kV: 0.99 for all four filters). The comparison of the signal and noise (mean, variance, and NPS) between the simulated and measured air scan images suggested that this model was reasonable in predicting accurate signal statistics of air scan images using absolute percent error. Overall, the model was found to be accurate in estimating signal statistics and spatial correlation between the detector elements of the images acquired with indirect, flat-panel x-ray detectors. Conclusions: The semiempirical linear model of the indirect, flat-panel x-ray detectors was described and validated with images of air scans. The model was found to be a useful tool in understanding the signal and noise transfer within indirect, flat-panel x-ray detector systems.

  3. High-Resolution Structure of the Photosynthetic Mn4Ca Catalyst from X-ray Spectroscopy

    SciTech Connect (OSTI)

    Yachandra, Vittal; Yano, Junko; Kern, Jan; Pushkar, Yulia; Sauer, Kenneth; Glatzel, Pieter; Bergmann, Uwe; Messinger, Johannes; Zouni, Athina; Yachandra, Vittal K.

    2007-08-01

    The application of high-resolution X-ray spectroscopy methods to study the photosynthetic water oxidizing complex, which contains a unique hetero-nuclear catalytic Mn4Ca cluster, are described. Issues of X-ray damage especially at the metal sites in the Mn4Ca cluster are discussed. The structure of the Mn4Ca catalyst at high-resolution which has so far eluded attempts of determination by X-ray diffraction, EXAFS and other spectroscopic techniques has been addressed using polarized EXAFS techniques applied to oriented PS II membrane preparations and PS II single crystals. A review of how the resolution of traditional EXAFS techniques can be improved, using methods such as range-extended EXAFS is presented, and the changes that occur in the structure of the cluster as it advances through the catalytic cycle are described. X-ray absorption and emission techniques (XANES and K? emission) have been used earlier to determine the oxidation states of the Mn4Ca cluster, and in this report we review the use of X-ray resonant Raman spectroscopy to understand the electronic structure of the Mn4Ca cluster as it cycles through the intermediate S-states.

  4. Wide band focusing x-ray spectrograph with spatial resolution

    SciTech Connect (OSTI)

    Pikuz, S. A.; Douglass, J. D.; Shelkovenko, T. A.; Sinars, D. B.; Hammer, D. A.

    2008-01-15

    A new, wide spectral bandwidth x-ray spectrograph, the wide-bandwidth focusing spectrograph with spatial resolution (WB-FSSR), based on spherically bent mica crystals, is described. The wide bandwidth is achieved by combining three crystals to form a large aperture dispersive element. Since the WB-FSSR covers a wide spectral band, it is very convenient for application as a routine diagnostic tool in experiments in which the desired spectral coverage is different from one test to the next. The WB-FSSR has been tested in imploding wire-array experiments on a 1 MA pulsed power machine, and x-ray spectra were recorded in the 1-20 A spectral band using different orders of mica crystal reflection. Using a two mirror-symmetrically placed WB-FSSR configuration, it was also possible to distinguish between a real spectral shift and a shift of recorded spectral lines caused by the spatial distribution of the radiating plasma. A spectral resolution of about 2000 was demonstrated and a spatial resolution of {approx}100 {mu}m was achieved in the spectral band of 5-10 A in second order of mica reflection. A simple method of numerical analysis of spectrograph capability is proposed.

  5. Experimental validation of a kilovoltage x-ray source model for computing imaging dose

    SciTech Connect (OSTI)

    Poirier, Yannick, E-mail: yannick.poirier@cancercare.mb.ca [CancerCare Manitoba, 675 McDermot Ave, Winnipeg, Manitoba R3E 0V9 (Canada)] [CancerCare Manitoba, 675 McDermot Ave, Winnipeg, Manitoba R3E 0V9 (Canada); Kouznetsov, Alexei; Koger, Brandon [Department of Physics and Astronomy, University of Calgary, Calgary, Alberta T2N 1N4 (Canada)] [Department of Physics and Astronomy, University of Calgary, Calgary, Alberta T2N 1N4 (Canada); Tambasco, Mauro, E-mail: mtambasco@mail.sdsu.edu [Department of Physics, San Diego State University, San Diego, California 92182-1233 and Department of Physics and Astronomy and Department of Oncology, University of Calgary, Calgary, Alberta T2N 1N4 (Canada)] [Department of Physics, San Diego State University, San Diego, California 92182-1233 and Department of Physics and Astronomy and Department of Oncology, University of Calgary, Calgary, Alberta T2N 1N4 (Canada)

    2014-04-15

    Purpose: To introduce and validate a kilovoltage (kV) x-ray source model and characterization method to compute absorbed dose accrued from kV x-rays. Methods: The authors propose a simplified virtual point source model and characterization method for a kV x-ray source. The source is modeled by: (1) characterizing the spatial spectral and fluence distributions of the photons at a plane at the isocenter, and (2) creating a virtual point source from which photons are generated to yield the derived spatial spectral and fluence distribution at isocenter of an imaging system. The spatial photon distribution is determined by in-air relative dose measurements along the transverse (x) and radial (y) directions. The spectrum is characterized using transverse axis half-value layer measurements and the nominal peak potential (kVp). This source modeling approach is used to characterize a Varian{sup ®} on-board-imager (OBI{sup ®}) for four default cone-beam CT beam qualities: beams using a half bowtie filter (HBT) with 110 and 125 kVp, and a full bowtie filter (FBT) with 100 and 125 kVp. The source model and characterization method was validated by comparing dose computed by the authors’ inhouse software (kVDoseCalc) to relative dose measurements in a homogeneous and a heterogeneous block phantom comprised of tissue, bone, and lung-equivalent materials. Results: The characterized beam qualities and spatial photon distributions are comparable to reported values in the literature. Agreement between computed and measured percent depth-dose curves is ?2% in the homogeneous block phantom and ?2.5% in the heterogeneous block phantom. Transverse axis profiles taken at depths of 2 and 6 cm in the homogeneous block phantom show an agreement within 4%. All transverse axis dose profiles in water, in bone, and lung-equivalent materials for beams using a HBT, have an agreement within 5%. Measured profiles of FBT beams in bone and lung-equivalent materials were higher than their computed counterparts resulting in an agreement within 2.5%, 5%, and 8% within solid water, bone, and lung, respectively. Conclusions: The proposed virtual point source model and characterization method can be used to compute absorbed dose in both the homogeneous and heterogeneous block phantoms within of 2%–8% of measured values, depending on the phantom and the beam quality. The authors’ results also provide experimental validation for their kV dose computation software, kVDoseCalc.

  6. X-ray spectral variability of type 2 Seyfert galaxies

    E-Print Network [OSTI]

    Hernández-García, L; González-Martín, O; Márquez, I

    2015-01-01

    Variability across the electromagnetic spectrum is a property of AGN that can help constraining the physical properties of these galaxies. This is the third of a serie of papers with the aim of studying the X-ray variability of different families of AGN. The main purpose of this work is to investigate the variability pattern in a sample of optically selected type 2 Seyfert galaxies. We use the 26 Seyferts in the Veron-Cetty and Veron catalogue with data available from Chandra and/or XMM-Newton public archives at different epochs, with timescales ranging from a few hours to years. All the spectra of the same source are simultaneously fitted and we let different parameters to vary in the model. Whenever possible, short-term variations and/or long-term UV flux variations are studied. We divide the sample in Compton-thick, Compton-thin, and changing-look candidates. Short-term variability at X-rays is not found. From the 25 analyzed sources, 11 show long-term variations; eight (out of 11) are Compton-thin, one (o...

  7. Soft x-ray reduction camera for submicron lithography

    DOE Patents [OSTI]

    Hawryluk, Andrew M. (2708 Rembrandt Pl., Modesto, CA 95356); Seppala, Lynn G. (7911 Mines Rd., Livermore, CA 94550)

    1991-01-01

    Soft x-ray projection lithography can be performed using x-ray optical components and spherical imaging lenses (mirrors), which form an x-ray reduction camera. The x-ray reduction is capable of projecting a 5x demagnified image of a mask onto a resist coated wafer using 4.5 nm radiation. The diffraction limited resolution of this design is about 135 nm with a depth of field of about 2.8 microns and a field of view of 0.2 cm.sup.2. X-ray reflecting masks (patterned x-ray multilayer mirrors) which are fabricated on thick substrates and can be made relatively distortion free are used, with a laser produced plasma for the source. Higher resolution and/or larger areas are possible by varying the optic figures of the components and source characteristics.

  8. Fabrication process for a gradient index x-ray lens

    DOE Patents [OSTI]

    Bionta, Richard M. (Livermore, CA); Makowiecki, Daniel M. (Livermore, CA); Skulina, Kenneth M. (Livermore, CA)

    1995-01-01

    A process for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments m the soft x-ray region.

  9. Fabrication process for a gradient index x-ray lens

    DOE Patents [OSTI]

    Bionta, R.M.; Makowiecki, D.M.; Skulina, K.M.

    1995-01-17

    A process is disclosed for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments in the soft x-ray region. 13 figures.

  10. Density gradient free electron collisionally excited x-ray laser

    DOE Patents [OSTI]

    Campbell, E.M.; Rosen, M.D.

    1984-11-29

    An operational x-ray laser is provided that amplifies 3p-3s transition x-ray radiation along an approximately linear path. The x-ray laser is driven by a high power optical laser. The driving line focused optical laser beam illuminates a free-standing thin foil that may be associated with a substrate for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the x-ray laser gain medium. The x-ray laser may be driven by more than one optical laser beam. The x-ray laser has been successfully demonstrated to function in a series of experimental tests.

  11. Density gradient free electron collisionally excited X-ray laser

    DOE Patents [OSTI]

    Campbell, Edward M. (Pleasanton, CA); Rosen, Mordecai D. (Berkeley, CA)

    1989-01-01

    An operational X-ray laser (30) is provided that amplifies 3p-3s transition X-ray radiation along an approximately linear path. The X-ray laser (30) is driven by a high power optical laser. The driving line focused optical laser beam (32) illuminates a free-standing thin foil (34) that may be associated with a substrate (36) for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the X-ray laser gain medium. The X-ray laser (30) may be driven by more than one optical laser beam (32, 44). The X-ray laser (30) has been successfully demonstrated to function in a series of experimental tests.

  12. Thickness Measurements from Single X-ray Phase-contrast Speckle Projection

    E-Print Network [OSTI]

    Xi, Yan; Ma, Jingchen; Zhao, Jun

    2015-01-01

    We propose a one-shot thickness measurement method for sponge-like structures using a propagation-based X-ray phase-contrast imaging (P-PCI) method. In P-PCI, the air-material interface refracts the incident X-ray. Refracted many times along their paths by such a structure, incident X-rays propagate randomly within a small divergent angle range, resulting in a speckle pattern in the captured image. We found structure thickness and contrast of a phase-contrast projection are directly related in images. This relationship can be described by a natural logarithm equation. Thus, from the one phase-contrast view, depth information can be retrieved from its contrast. Our preliminary biological experiments indicate promise in its application to measurements requiring in vivo and ongoing assessment of lung tumor progression.

  13. ISOCAM Photometry of Narrow-Line X-ray Galaxies

    E-Print Network [OSTI]

    J. D. Law-Green; A. Zezas; M. J. Ward; C. Boisson

    1998-12-23

    Mid-infrared photometry of the hosts of Narrow-Line X-ray Galaxies at 6 microns and 12 microns has been attempted with ISOCAM. No conclusive detections have been made. This implies that these are quiescent objects with little or no active star-formation. Neither X-ray binaries nor starburst-driven superwinds are consistent explanations for the X-ray emission in these objects. We conclude that these NLXGs are predominantly AGN-powered.

  14. X-ray interferometry with spherically bent crystals (abstract)

    SciTech Connect (OSTI)

    Koch, Jeffrey A.

    2001-01-01

    Recent progress in manufacturing high-quality spherically bent crystals allows highly monochromatic x-ray beams to be produced, and allows efficient x-ray imaging with {mu}m-scale resolution. This article explores some of the constraints for x-ray interferometry utilizing spherically bent crystals and laser-produced plasma sources, and discusses several shearing interferometer concepts that might be experimentally investigated.

  15. Legacy of the X-Ray Laser Program

    SciTech Connect (OSTI)

    Nilsen, J.

    1993-08-06

    The X-Ray Laser Program has evolved from a design effort focusing on developing a Strategic Defense Initiative weapon that protects against Soviet ICBMs to a scientific project that is producing new technologies for industrial and medical research. While the great technical successes and failures of the X-ray laser itself cannot be discussed, this article presents the many significant achievements made as part of the X-ray laser effort that are now being used for other applications at LLNL.

  16. The X-ray synchrotron emission of RCW 86 and the implications for its age

    E-Print Network [OSTI]

    Jacco Vink; Johan Bleeker; Kurt van der Heyden; Andrei Bykov; Aya Bamba; Ryo Yamazaki

    2006-07-13

    We report here X-ray imaging spectroscopy observations of the northeastern shell of the supernova remnant RCW 86 with Chandra and XMM-Newton. Along this part of the shell the dominant X-ray radiation mechanism changes from thermal to synchrotron emission. We argue that both the presence of X-ray synchrotron radiation and the width of the synchrotron emitting region suggest a locally higher shock velocity of V_s = 2700 km/s and a magnetic field of B = 24+/-5 microGauss. Moreover, we also show that a simple power law cosmic ray electron spectrum with an exponential cut-off cannot explain the broad band synchrotron emission. Instead a concave electron spectrum is needed, as predicted by non-linear shock acceleration models. Finally, we show that the derived shock velocity strengthens the case that RCW 86 is the remnant of SN 185.

  17. X-ray micromodulated luminescence tomography in dual-cone ...

    E-Print Network [OSTI]

    2014-07-01

    Jul 16, 2014 ... source, a polycapillary lens, and an electron multiplying charge coupled device ... sources generate x-rays by accelerating electrons into high-z.

  18. X-Ray Characterization of Diesel Sprays | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Sprays X-Ray Characterization of Diesel Sprays 2005 Diesel Engine Emissions Reduction (DEER) Conference Presentations and Posters 2005deerpowell.pdf More Documents & Publications...

  19. Probing Spatial, Electronic Structures with X-ray Scattering...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Techniques Wednesday, September 5, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Gang Chen Seminar:...

  20. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of...

  1. In situ X-ray Characterization of Energy Storage Materials |...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Scholar, SSRL MSD Hard X-ray Department A key factor in the global move towards clean, renewable energy is the electrification of the automobile. Current battery technology...

  2. Dissociation of strong acid revisited: X-ray photoelectron spectroscop...

    Office of Scientific and Technical Information (OSTI)

    X-ray photoelectron spectroscopy and molecular dynamics simulations of HNO3 in water Citation Details In-Document Search Title: Dissociation of strong acid revisited:...

  3. Simulating Wavefront Correction via Deformable Mirrors at X-Ray...

    Office of Scientific and Technical Information (OSTI)

    Resource Type: Conference Resource Relation: Conference: Presented at: X-ray Adaptive Optics, San Diego, CA, United States, Aug 14 - Aug 14, 2012 Research Org: Lawrence Livermore...

  4. Resonant Soft X-Ray Scattering - Combining Structural with Spectroscop...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    spectroscopy has become an important tool in understanding the electronic structure of materials. Resonant absorption edges in the soft x-ray regime are especially interesting...

  5. A Record Run for the APS X-ray Source

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    signals that comprise radiation interlock systems protecting personnel and equipment; * Beam diagnostics controlling multiple x-ray beams simultaneously while utilizing more than...

  6. Insight into obscure transition uncovered by X-rays | Argonne...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of X-ray techniques. This transition has ramifications for material design for electronics and sensors. The transition between being electrically conductive (metallic) at...

  7. Advances in X-Ray Diagnostics of Diesel Fuel Sprays

    Broader source: Energy.gov [DOE]

    Recent advances in high-speed X-ray imaging has shown several distinct behaviors of commercial fuel injectors that cannot be seen with more conventional techniques.

  8. X-ray image reconstruction from a diffraction pattern alone

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Marchesini, Stefano

    X-ray diffraction pattern of a sample of 50 nm colloidal gold particles, recorded at a wavelength of 2.1 nm.

  9. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    were able to directly observe redox processes in thin-film iron and cobalt perovskite oxide electrocatalysts using surface-sensitive, x-ray absorption spectroscopy while...

  10. Electronic structure of titania aerogels: Soft x-ray absorption...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Electronic structure of titania aerogels: Soft x-ray absorption study Citation Details In-Document Search Title: Electronic structure of titania aerogels: Soft...

  11. Characterization of spatially resolved high resolution x-ray...

    Office of Scientific and Technical Information (OSTI)

    Characterization of spatially resolved high resolution x-ray spectrometers for high energy density physics and light source experiments Citation Details In-Document Search Title:...

  12. X-ray microscopy at CNM | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorkingLos Alamos verifies largest single goldWindX-RayX-Ray ScienceX-RayX-ray

  13. A concept for Z-dependent microbunching measurements with coherent X-ray transition radiation in a sase FEL

    E-Print Network [OSTI]

    Lumpkin, A.H.; Fawley, W.M.; Rule, D.W.

    2004-01-01

    Model to Data from a SASE FEL at 540, 265, and 157 nm,”simulation of the x-ray SASE FEL showing the SASE radiationTRANSITION RADIATION IN A SASE FEL* A.H. Lumpkin # , W.M.

  14. On the Cooling Tails of Thermonuclear X-ray Bursts: The IGR J17480–2446 Link

    E-Print Network [OSTI]

    Linares, Manuel

    The neutron star transient and 11 Hz X-ray pulsar IGR J17480–2446, recently discovered in the globular cluster Terzan 5, showed unprecedented bursting activity during its 2010 October-November outburst. We analyzed all ...

  15. Spectral Formation in X-Ray Pulsars: Bulk Comptonization in the Accretion Shock

    E-Print Network [OSTI]

    Peter A. Becker; Michael T. Wolff

    2005-05-06

    Accretion-powered X-ray pulsars are among the most luminous X-ray sources in the Galaxy. However, despite decades of theoretical and observational work since their discovery, no satisfactory model for the formation of the observed X-ray spectra has emerged. In particular, the previously available theories are unable to reproduce the power-law variation observed at high energies in many sources. In this paper, we present the first self-consistent calculation of the spectrum emerging from a pulsar accretion column that includes an explicit treatment of the energization occurring in the shock. Using a rigorous eigenfunction expansion method based on the exact dynamical solution for the velocity profile in the column, we obtain a closed-form expression for the Green's function describing the upscattering of radiation injected into the column from a monochromatic source located at the top of the thermal mound, near the base of the flow. The Green's function is convolved with a Planck distribution to calculate the radiation spectrum resulting from the reprocessing of blackbody photons emitted by the thermal mound. We demonstrate that the energization of the photons in the shock naturally produces an X-ray spectrum with a power-law shape at high energies and a blackbody shape at low energies, in agreement with many observations of accreting X-ray pulsars.

  16. IKT 16: the first X-ray confirmed composite SNR in the SMC

    E-Print Network [OSTI]

    Maitra, Chandreyee; Filipovic, Miroslav; Haberl, Frank; Tiengo, Andrea; Grieve, Kevin; Roper, Quentin

    2015-01-01

    Aims: IKT 16 is an X-ray and radio-faint supernova remnant (SNR) in the Small Magellanic Cloud (SMC). A detailed X-ray study of this SNR with XMM-Newton confirmed the presence of a hard X-ray source near its centre, indicating the detection of the first composite SNR in the SMC. With a dedicated Chandra observation we aim to resolve the point source and confirm its nature. We also acquire new ATCA observations of the source at 2.1 GHz with improved flux density estimates and resolution. Methods: We perform detailed spatial and spectral analysis of the source. With the highest resolution X-ray and radio image of the centre of the SNR available today, we resolve the source and confirm its pulsar wind nebula (PWN) nature. Further, we constrain the geometrical parameters of the PWN and perform spectral analysis for the point source and the PWN separately. We also test for the radial variations of the PWN spectrum and its possible east west asymmetry. Results: The X-ray source at the centre of IKT 16 can be resolv...

  17. X-ray tests of a two-dimensional stigmatic imaging scheme with variable magnifications

    SciTech Connect (OSTI)

    Lu, J.; Bitter, M.; Hill, K. W.; Delgado-Aparicio, L. F.; Efthimion, P. C.; Pablant, N. A.; Beiersdorfer, P.; Caughey, T. A.; Brunner, J.

    2014-11-15

    A two-dimensional stigmatic x-ray imaging scheme, consisting of two spherically bent crystals, one concave and one convex, was recently proposed [M. Bitter et al., Rev. Sci. Instrum. 83, 10E527 (2012)]. The Bragg angles and the radii of curvature of the two crystals of this imaging scheme are matched to eliminate the astigmatism and to satisfy the Bragg condition across both crystal surfaces for a given x-ray energy. In this paper, we consider more general configurations of this imaging scheme, which allow us to vary the magnification for a given pair of crystals and x-ray energy. The stigmatic imaging scheme has been validated for the first time by imaging x-rays generated by a micro-focus x-ray source with source size of 8.4 ?m validated by knife-edge measurements. Results are presented from imaging the tungsten L?1 emission at 8.3976 keV, using a convex Si-422 crystal and a concave Si-533 crystal with 2d-spacings of 2.21707 Å and 1.65635 Å and radii of curvature of 500 ± 1 mm and 823 ± 1 mm, respectively, showing a spatial resolution of 54.9 ?m. This imaging scheme is expected to be of interest for the two-dimensional imaging of laser produced plasmas.

  18. Attenuation of super-soft X-ray sources by circumstellar material

    E-Print Network [OSTI]

    Nielsen, Mikkel

    2015-01-01

    Recent studies have suggested the possibility of significantly obscuring super-soft X-ray sources in relatively modest amounts of local matter lost from the binaries themselves. If correct, then this would have explained the paucity of observed super-soft X-ray sources and would have significance for the search for single-degenerate type Ia supernova progenitors. We point out that earlier studies of circumbinary obscuration ignored photo-ionisations of the gas by the emission from the super-soft X-ray source. We revisit the problem using a full, self-consistent calculation of the ionisation state of the circumbinary material photo-ionised by the radiation of the central source. Our results show that the circumstellar mass-loss rates required for obcuration of super-soft X-ray sources is about an order of magnitude larger than those reported in earlier studies, for comparable model parameters. While this does not entrirely rule out the possibility of circumstellar material obscuring super-soft X-ray sources, i...

  19. X-Ray and Optical Observations of A 0535+26

    E-Print Network [OSTI]

    Camero-Arranz, A; Wilson-Hodge, C A; Jenke, P; Steele, I; Coe, M J; Gutierrez-Soto, J; Kretschmar, P; Caballero, I; Case, G; Cherry, M L; Yan, J; Suso, J; Rodríguez, J; Guiriec, S; McBride, V A

    2011-01-01

    We present recent contemporaneous X-ray and optical observations of the Be/X-ray binary system A 0535+26 with the Fermi/Gamma-ray Burst Monitor (GBM) and several ground-based observatories. These new observations are put into the context of the rich historical data and discussed in terms of the neutron star Be-disk interaction. The Be circumstellar disk was exceptionally large just before the 2009 December giant outburst, which may explain the origin of the unusual recent X-ray activity of this source. We found a peculiar evolution of the pulse profile during this giant outburst, with the two main components evolving in opposite ways with energy. A hard 30-70 mHz X-ray QPO was detected with GBM during this 2009 December giant outburst. It becomes stronger with increasing energy and disappears at energies below 25 keV. In the long-term a strong optical/X-ray correlation was found for this system, however in the medium-term the H{\\alpha} EW and the V-band brightness showed an anti-correlation after \\sim2002 Aug...

  20. Swift observations of GRB 070110: an extraordinary X-ray afterglow powered by the central engine

    E-Print Network [OSTI]

    Troja, E; O'Brien, P; Zhang, B; Sbarufatti, B; Mangano, V; Willingale, R; Chincarini, G; Osborne, J P; Marshall, F E; Burrows, D N; Campana, S; Gehrels, N; Guidorzi, C; Krimm, H A; La Parola, V; Liang, E W; Mineo, T; Moretti, A; Page, K L; Romano, P; Tagliaferri, G; Zhang, B B

    2007-01-01

    We present a detailed analysis of Swift multi-wavelength observations of GRB 070110 and its remarkable afterglow. The early X-ray light curve, interpreted as the tail of the prompt emission, displays a spectral evolution already seen in other gamma-ray bursts. The optical afterglow shows a shallow decay up to ~2 d after the burst, which is not consistent with standard afterglow models. The most intriguing feature is a very steep decay in the X-ray flux at ~20 ks after the burst, ending an apparent plateau. The abrupt drop of the X-ray light curve rules out an external shock as the origin of the plateau in this burst and implies long-lasting activity of the central engine. The temporal and spectral properties of the plateau phase point towards a continuous central engine emission rather than the episodic emission of X-ray flares. We suggest that the observed X-ray plateau is powered by a spinning down central engine, possibly a millisecond pulsar, which dissipates energy at an internal radius before depositing...

  1. Swift observations of GRB 070110: an extraordinary X-ray afterglow powered by the central engine

    E-Print Network [OSTI]

    E. Troja; G. Cusumano; P. O'Brien; B. Zhang; B. Sbarufatti; V. Mangano; R. Willingale; G. Chincarini; J. P. Osborne; F. E. Marshall; D. N. Burrows; S. Campana; N. Gehrels; C. Guidorzi; H. A. Krimm; V. La Parola; E. W. Liang; T. Mineo; A. Moretti; K. L. Page; P. Romano; G. Tagliaferri; B. B. Zhang; M. J. Page; P. Schady

    2007-05-01

    We present a detailed analysis of Swift multi-wavelength observations of GRB 070110 and its remarkable afterglow. The early X-ray light curve, interpreted as the tail of the prompt emission, displays a spectral evolution already seen in other gamma-ray bursts. The optical afterglow shows a shallow decay up to ~2 d after the burst, which is not consistent with standard afterglow models. The most intriguing feature is a very steep decay in the X-ray flux at ~20 ks after the burst, ending an apparent plateau. The abrupt drop of the X-ray light curve rules out an external shock as the origin of the plateau in this burst and implies long-lasting activity of the central engine. The temporal and spectral properties of the plateau phase point towards a continuous central engine emission rather than the episodic emission of X-ray flares. We suggest that the observed X-ray plateau is powered by a spinning down central engine, possibly a millisecond pulsar, which dissipates energy at an internal radius before depositing energy into the external shock.

  2. A NEW COSMOLOGICAL DISTANCE MEASURE USING ACTIVE GALACTIC NUCLEUS X-RAY VARIABILITY

    SciTech Connect (OSTI)

    Franca, Fabio La; Bianchi, Stefano; Branchini, Enzo; Matt, Giorgio [Dipartimento di Matematica e Fisica, Università Roma Tre, Via della Vasca Navale 84, I-00146, Roma (Italy); Ponti, Gabriele, E-mail: lafranca@fis.uniroma3.it [Max-Planck-Institut für Extraterrestrische Physik, Giessenbachstrasse 1, D-85748 Garching bei München (Germany)

    2014-05-20

    We report the discovery of a luminosity distance estimator using active galactic nuclei (AGNs). We combine the correlation between the X-ray variability amplitude and the black hole (BH) mass with the single-epoch spectra BH mass estimates which depend on the AGN luminosity and the line width emitted by the broad-line region. We demonstrate that significant correlations do exist that allow one to predict the AGN (optical or X-ray) luminosity as a function of the AGN X-ray variability and either the H? or the Pa? line widths. In the best case, when the Pa? is used, the relationship has an intrinsic dispersion of ?0.6 dex. Although intrinsically more disperse than supernovae Ia, this relation constitutes an alternative distance indicator potentially able to probe, in an independent way, the expansion history of the universe. With respect to this, we show that the new mission concept Athena should be able to measure the X-ray variability of hundreds of AGNs and then constrain the distance modulus with uncertainties of 0.1 mag up to z ? 0.6. We also discuss how our estimator has the prospect of becoming a cosmological probe even more sensitive than the current supernovae Ia samples by using a new dedicated wide-field X-ray telescope able to measure the variability of thousands of AGNs.

  3. X-Ray Spectroscopy of the Classical Nova V458 Vulpeculae with Suzaku

    E-Print Network [OSTI]

    Tsujimoto, Masahiro; Drake, Jeremy J; Ness, Jan-Uwe; Kitamoto, Shunji

    2008-01-01

    We conducted a target of opportunity X-ray observation of the classical nova V458 Vulpeculae 88 days after the explosion using the Suzaku satellite. With a 20 ks exposure, the X-ray Imaging Spectrometer detected X-ray emission significantly harder than typical super-soft source emission. The X-ray spectrum shows K lines from N, Ne, Mg, Si, and S, and L-series emission from Fe in highly ionized states. The spectrum can be described by a single temperature (0.64 keV) thin thermal plasma model in collisional equilibrium with a hydrogen-equivalent extinction column density of ~3e21/cm2, a flux of ~1e-12 erg/s/cm2, and a luminosity of ~6e34 erg/s in the 0.3-3.0 keV band at an assumed distance of 13 kpc. We found a hint of an enhancement of N and deficiencies of O and Fe relative to other metals. The observed X-ray properties can be interpreted as the emission arising from shocks of ejecta from an ONe-type nova.

  4. X-Ray Spectroscopy of the Classical Nova V458 Vulpeculae with Suzaku

    E-Print Network [OSTI]

    Masahiro Tsujimoto; Dai Takei; Jeremy J. Drake; Jan-Uwe Ness; Shunji Kitamoto

    2008-10-17

    We conducted a target of opportunity X-ray observation of the classical nova V458 Vulpeculae 88 days after the explosion using the Suzaku satellite. With a 20 ks exposure, the X-ray Imaging Spectrometer detected X-ray emission significantly harder than typical super-soft source emission. The X-ray spectrum shows K lines from N, Ne, Mg, Si, and S, and L-series emission from Fe in highly ionized states. The spectrum can be described by a single temperature (0.64 keV) thin thermal plasma model in collisional equilibrium with a hydrogen-equivalent extinction column density of ~3e21/cm2, a flux of ~1e-12 erg/s/cm2, and a luminosity of ~6e34 erg/s in the 0.3-3.0 keV band at an assumed distance of 13 kpc. We found a hint of an enhancement of N and deficiencies of O and Fe relative to other metals. The observed X-ray properties can be interpreted as the emission arising from shocks of ejecta from an ONe-type nova.

  5. UNIVERSAL BEHAVIOR OF X-RAY FLARES FROM BLACK HOLE SYSTEMS

    SciTech Connect (OSTI)

    Wang, F. Y.; Dai, Z. G.; Yi, S. X.; Xi, S. Q. E-mail: dzg@nju.edu.cn

    2015-01-01

    X-ray flares have been discovered in black hole systems such as gamma-ray bursts, the tidal disruption event Swift J1644+57, the supermassive black hole Sagittarius A* at the center of our Galaxy, and some active galactic nuclei. Occurrences of X-ray flares are always accompanied by relativistic jets. However, it is still unknown whether or not there is a physical analogy among such X-ray flares produced in black hole systems spanning nine orders of magnitude in mass. Here, we report observed data of X-ray flares and show that they have three statistical properties similar to solar flares, including power-law distributions of their energies, durations, and waiting times, which can be explained by a fractal-diffusive, self-organized criticality model. These statistical similarities, together with the fact that solar flares are triggered by a magnetic reconnection process, suggest that all of the X-ray flares are consistent with magnetic reconnection events, implying that their concomitant relativistic jets may be magnetically dominated.

  6. Recollimation boundary layers as X-ray sources in young stellar jets

    SciTech Connect (OSTI)

    Günther, Hans Moritz; Li, Zhi-Yun; Schneider, P. C.

    2014-11-01

    Young stars accrete mass from circumstellar disks and, in many cases, the accretion coincides with a phase of massive outflows, which can be highly collimated. Those jets emit predominantly in the optical and IR wavelength range. However, in several cases, X-ray and UV observations reveal a weak but highly energetic component in those jets. X-rays are observed both from stationary regions close to the star and from knots in the jet several hundred AU from the star. In this article, we show semianalytically that a fast stellar wind that is recollimated by the pressure from a slower, more massive disk wind can have the right properties to power stationary X-ray emission. The size of the shocked regions is compatible with observational constraints. Our calculations support a wind-wind interaction scenario for the high-energy emission near the base of young stellar object jets. For the specific case of DG Tau, a stellar wind with a mass-loss rate of 5 × 10{sup –10} M {sub ?} yr{sup –1} and a wind speed of 800 km s{sup –1} reproduces the observed X-ray spectrum. We conclude that a stellar wind recollimation shock is a viable scenario to power stationary X-ray emission close to the jet launching point.

  7. X-ray Spectroscopy for Quality Control of Chemotherapy Drugs

    SciTech Connect (OSTI)

    Greaves, E. D.; Barros, H.; Bermudez, J.; Sajo-Bohus, L.; Angeli-Greaves, M.

    2007-10-26

    We develop a method, employing Compton peak standardization and the use of matrix-matched spiked samples with Total Reflection X-ray Fluorescence (TXRF), for the determination of platinum plasma concentrations of patients undergoing chemotherapy with Pt-bearing drugs. Direct blood plasma analysis attains Pt detection limits of 70 ng/ml. Measurement results of prescribed drug doses are compared to achieved blood Pt concentrations indicating a lack of expected correlations. Direct analysis of Pt-containing infused drugs from a variety of suppliers indicates cases of abnormal concentrations which raises quality control issues. We demonstrate the potential usefulness of the method for pharmacokinetic studies or for routine optimization and quality control of Pt chemotherapy treatments.

  8. High counting rates of x-ray photon detection using APD detectors on synchrotron machines

    SciTech Connect (OSTI)

    Kakuno, E. M.; Giacomolli, B. A.; Scorzato, C. R. [Universidade Federal do Pampa - UNIPAMPA-Bage, 96413-170 (Brazil); Laboratorio Nacional de Luz Sincrotron - LNLS, 13086-100 (Brazil)

    2012-05-17

    In this work we show the results of 10 x 10 mm{sup 2} Si-APD detector's test with guard ring detecting x-rays. The result of mapping surface is also exhibited. We show and discuss the difficulty of single photon detection in high counting rate experiments in synchrotrons machines.

  9. Determination of the polarization state of x rays with the help of anomalous transmission

    SciTech Connect (OSTI)

    Schulze, K. S. Uschmann, I.; Förster, E.; Marx, B.; Paulus, G. G.; Stöhlker, T.

    2014-04-14

    Besides intensity and direction, the polarization of an electromagnetic wave provides characteristic information on the crossed medium. Here, we present two methods for the determination of the polarization state of x rays by polarizers based on anomalous transmission (Borrmann effect). Using a polarizer-analyzer setup, we have measured a polarization purity of less than 1.5?×?10{sup ?5}, three orders of magnitude better than obtained in earlier work. Using the analyzer crystal in multiple-beam case with slightly detuned azimuth, we show how the first three Stokes parameters can be determined with a single angular scan. Thus, polarization analyzers based on anomalous transmission make it possible to detect changes of the polarization in a range from degrees down to arcseconds.

  10. Optical and X-ray variability of two Small Magellanic Cloud X-ray binary pulsars - SXP46.6 and SXP6.85

    E-Print Network [OSTI]

    K. E. McGowan; M. J. Coe; M. P. E. Schurch; R. H. D. Corbet; J. L. Galache; A. Udalski

    2007-11-26

    We present long-term optical and RXTE data of two X-ray binary pulsars in the Small Magellanic Cloud, SXP46.6 and SXP6.85. The optical light curves of both sources show substantial (~0.5-0.8 mag) changes over the time span of the observations. While the optical data for SXP6.85 do not reveal any periodic behaviour, by detrending the optical measurements for SXP46.6 we find an orbital period of ~137 days, consistent with results from the X-ray data. The detection of Type I X-ray outbursts from SXP46.6, combined with the fact that we also see optical outbursts at these times, implies that SXP46.6 is a high orbital eccentricity system. Using contemporaneous optical spectra of SXP46.6 we find that the equivalent width of the H_alpha emission line changes over time indicating that the size of the circumstellar disc varies. By studying the history of the colour variations for SXP6.85 we find that the source gets redder as it brightens which can also be attributed to changes in the circumstellar disc. We do not find any correlation between the X-ray and optical data for SXP6.85. The results for SXP6.85 suggest that it is a low eccentricity binary and that the optical modulations are due to the Be phenomenon.

  11. Compact 'diode-based' multi-energy soft x-ray diagnostic for NSTX

    SciTech Connect (OSTI)

    Tritz, K.; Clayton, D. J.; Stutman, D.; Finkenthal, M. [Johns Hopkins University, Baltimore, Maryland 21218 (United States)

    2012-10-15

    A novel and compact, diode-based, multi-energy soft x-ray (ME-SXR) diagnostic has been developed for the National Spherical Tokamak Experiment. The new edge ME-SXR system tested on NSTX consists of a set of vertically stacked diode arrays, each viewing the plasma tangentially through independent pinholes and filters providing an overlapping view of the plasma midplane which allows simultaneous SXR measurements with coarse sub-sampling of the x-ray spectrum. Using computed x-ray spectral emission data, combinations of filters can provide fast (>10 kHz) measurements of changes in the electron temperature and density profiles providing a method to 'fill-in' the gaps of the multi-point Thomson scattering system.

  12. Time-delayed beam splitting with energy separation of x-ray channels

    SciTech Connect (OSTI)

    Stetsko, Yuri P.; Shvyd'ko, Yuri V.; Brian Stephenson, G. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)] [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)

    2013-10-21

    We introduce a time-delayed beam splitting method based on the energy separation of x-ray photon beams. It is implemented and theoretically substantiated on an example of an x-ray optical scheme similar to that of the classical Michelson interferometer. The splitter/mixer uses Bragg-case diffraction from a thin diamond crystal. Another two diamond crystals are used as back-reflectors. Because of energy separation and a minimal number (three) of optical elements, the split-delay line has high efficiency and is simple to operate. Due to the high transparency of diamond crystal, the split-delay line can be used in a beam sharing mode at x-ray free-electron laser facilities.

  13. Sensitivity Analysis of X-ray Spectra from Scanning Electron Microscopes

    SciTech Connect (OSTI)

    Miller, Thomas Martin; Patton, Bruce W.; Weber, Charles F.; Bekar, Kursat B.

    2014-10-01

    The primary goal of this project is to evaluate x-ray spectra generated within a scanning electron microscope (SEM) to determine elemental composition of small samples. This will be accomplished by performing Monte Carlo simulations of the electron and photon interactions in the sample and in the x-ray detector. The elemental inventories will be determined by an inverse process that progressively reduces the difference between the measured and simulated x-ray spectra by iteratively adjusting composition and geometric variables in the computational model. The intended benefit of this work will be to develop a method to perform quantitative analysis on substandard samples (heterogeneous phases, rough surfaces, small sizes, etc.) without involving standard elemental samples or empirical matrix corrections (i.e., true standardless quantitative analysis).

  14. Development of all-solid-state flash x-ray generator with photoconductive semiconductor switches

    SciTech Connect (OSTI)

    Xun, Ma; Jianjun, Deng; Hongwei, Liu; Jianqiang, Yuan; Jinfeng, Liu; Bing, Wei; Yanling, Qing; Wenhui, Han; Lingyun, Wang; Pin, Jiang; Hongtao, Li

    2014-09-15

    A compact, low-jitter, and high repetitive rate all-solid-state flash x-ray generator making use of photo conductive semiconductor switches was developed recently for the diagnostic purpose of some hydrokinetical experiments. The generator consisted of twelve stages of Blumlein pulse forming networks, and an industrial cold cathode diode was used to generate intense x-ray radiations with photon energy up to 220 keV. Test experiments showed that the generator could produce >1 kA electron beam currents and x-ray pulses with ?40 ns duration under 100 Hz repetitive rates at least (limited by the triggering laser on hand), also found was that the delay time of the cathode explosive emission is crucial to the energy transfer efficiency of the whole system. In addition, factors affecting the diode impedance, how the switching synchronization and diode impedance determining the allowable operation voltage were discussed.

  15. Sagittarius A* Rivaled the Sun in the Ancient X-ray Sky

    E-Print Network [OSTI]

    Xian Chen; Pau Amaro-Seoane

    2014-12-17

    Sagittarius A*, lying the Galactic Center $8$ kpc from Earth, hosts the closest supermassive black hole known to us. It is now inactive, but there are evidences indicating that about six million years ago it underwent a powerful outburst where the luminosity could have approached the Eddington limit. Motivated by the fact that in extragalaxies the supermassive black holes with similar masses and near-Eddington luminosities are usually strong X-ray emitters, we calculate here the X-ray luminosity of Sagittarius A*, assuming that the outburst was due to accretion of gas or tidal disruption of stars, both scenarios having been considered to trigger the previous outburst. We show that in both cases Sagittarius A* could precipitate on Earth an X-ray ($h\

  16. Spectrometer for Hard X-Ray Free Electron Laser Based on Diffraction Focusing

    E-Print Network [OSTI]

    Kohn, V G; Vartanyants, I A

    2012-01-01

    X-ray free electron lasers (XFELs) generate sequences of ultra-short, spatially coherent pulses of x-ray radiation. We propose the diffraction focusing spectrometer (DFS), which is able to measure the whole energy spectrum of the radiation of a single XFEL pulse with an energy resolution of $\\Delta E/E\\approx 2\\times 10^{-6}$. This is much better than for most modern x-ray spectrometers. Such resolution allows one to resolve the fine spectral structure of the XFEL pulse. The effect of diffraction focusing occurs in a single crystal plate due to dynamical scattering, and is similar to focusing in a Pendry lens made from the metamaterial with a negative refraction index. Such a spectrometer is easier to operate than those based on bent crystals. We show that the DFS can be used in a wide energy range from 5 keV to 20 keV.

  17. High Efficiency, Multi-Terawatt X-ray free electron lasers

    E-Print Network [OSTI]

    Emma, Claudio; Wu, Juhao; Pellegrini, Claudio

    2015-01-01

    We study high efficiency, multi-terawatt peak power, few angstrom wavelength, X-ray Free Electron Lasers (X-ray FELs). To obtain these characteristics we consider an optimized undulator design: superconducting, helical, with short period and built-in strong focusing. This design reduces the length of the breaks between modules, decreasing diffraction effects, and allows using a stronger transverse electron focusing. Both effects reduce the gain length and the overall undulator length. The peak power and efficiency depend on the transverse electron beam distribution and on time dependent effects, like synchrotron sideband growth. The last effect is identified as the main cause for reduction of electron beam microbunching and FEL peak power. We show that the optimal functional form for the undulator magnetic field tapering profile, yielding the maximum output power, depends significantly on these effects. The output power achieved when neglecting time dependent effects for an LCLS-like X-ray FEL with a 100 m lo...

  18. X-ray quantum optics with Mössbauer nuclei embedded in thin film cavities

    E-Print Network [OSTI]

    K. P. Heeg; J. Evers

    2013-05-18

    A promising platform for the emerging field of x-ray quantum optics are M\\"ossbauer nuclei embedded in thin film cavities probed by near-resonant x-ray light, as used in a number of recent experiments. Here, we develop a quantum optical framework for the description of experimentally relevant settings involving nuclei embedded in x-ray waveguides. We apply our formalism to two settings of current experimental interest based on the archetype M\\"ossbauer isotope 57Fe. For present experimental conditions, we derive compact analytical expressions and show that the alignment of medium magnetization as well as incident and detection polarization enable the engineering advanced quantum optical level schemes. The model encompasses non-linear and quantum effects which could become accessible in future experiments.

  19. X-ray flares from dense shells formed in gamma-ray burst explosions

    E-Print Network [OSTI]

    Hascoet, R; Daigne, F; Mochkovitch, R

    2015-01-01

    Bright X-ray flares are routinely detected by the Swift satellite during the early afterglow of gamma-ray bursts, when the explosion ejecta drives a blast wave into the external medium. We suggest that the flares are produced as the reverse shock propagates into the tail of the ejecta. The ejecta is expected to contain a few dense shells formed at an earlier stage of the explosion. We show an example of how such dense shells form and describe how the reverse shock interacts with them. A new reflected shock is generated in this interaction, which produces a short-lived X-ray flare. The model provides a natural explanation for the main observed features of the X-ray flares --- the fast rise, the steep power-law decline, and the characteristic peak duration \\Delta t /t= (0.1-0.3).

  20. High Mass X-ray Binaries: Progenitors of double neutron star systems

    E-Print Network [OSTI]

    Chaty, Sylvain

    2015-01-01

    In this review I briefly describe the nature of the three kinds of High-Mass X-ray Binaries (HMXBs), accreting through: (i) Be circumstellar disc, (ii) supergiant stellar wind, and (iii) Roche lobe filling supergiants. A previously unknown population of HMXBs hosting supergiant stars has been revealed in the last years, with multi-wavelength campaigns including high energy (INTEGRAL, Swift, XMM, Chandra) and optical/infrared (mainly ESO) observations. This population is divided between obscured supergiant HMXBs, and supergiant fast X-ray transients (SFXTs), characterized by short and intense X-ray flares. I discuss the characteristics of these types of supergiant HMXBs, propose a scenario describing the properties of these high-energy sources, and finally show how the observations can constrain the accretion models (e.g. clumpy winds, magneto-centrifugal barrier, transitory accretion disc, etc). Because they are the likely progenitors of Luminous Blue Variables (LBVs), and also of double neutron star systems,...

  1. In Situ X-Ray Probing Reveals Fingerprints of Surface Platinum Oxide

    SciTech Connect (OSTI)

    Friebel, Daniel

    2011-08-24

    In situ x-ray absorption spectroscopy (XAS) at the Pt L{sub 3} edge is a useful probe for Pt-O interactions at polymer electrolyte membrane fuel cell (PEMFC) cathodes. We show that XAS using the high energy resolution fluorescence detection (HERFD) mode, applied to a well-defined monolayer Pt/Rh(111) sample where the bulk penetrating hard x-rays probe only surface Pt atoms, provides a unique sensitivity to structure and chemical bonding at the Pt-electrolyte interface. Ab initio multiple-scattering calculations using the FEFF8 code and complementary extended x-ray absorption fine structure (EXAFS) results indicate that the commonly observed large increase of the white-line at high electrochemical potentials on PEMFC cathodes originates from platinum oxide formation, whereas previously proposed chemisorbed oxygen-containing species merely give rise to subtle spectral changes.

  2. Demonstration of x-ray fluorescence imaging of a high-energy-density plasma

    SciTech Connect (OSTI)

    MacDonald, M. J., E-mail: macdonm@umich.edu; Gamboa, E. J. [Department of Atmospheric, Oceanic, and Space Sciences, University of Michigan, Ann Arbor, Michigan 48109 (United States); SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Keiter, P. A.; Fein, J. R.; Klein, S. R.; Kuranz, C. C.; LeFevre, H. J.; Manuel, M. J.-E.; Wan, W. C.; Drake, R. P. [Department of Atmospheric, Oceanic, and Space Sciences, University of Michigan, Ann Arbor, Michigan 48109 (United States); Montgomery, D. S. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Biener, M. M.; Fournier, K. B. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Streit, J. [Schafer Corporation, Livermore, California 94551 (United States)

    2014-11-15

    Experiments at the Trident Laser Facility have successfully demonstrated the use of x-ray fluorescence imaging (XRFI) to diagnose shocked carbonized resorcinol formaldehyde (CRF) foams doped with Ti. One laser beam created a shock wave in the doped foam. A second laser beam produced a flux of vanadium He-? x-rays, which in turn induced Ti K-shell fluorescence within the foam. Spectrally resolved 1D imaging of the x-ray fluorescence provided shock location and compression measurements. Additionally, experiments using a collimator demonstrated that one can probe specific regions within a target. These results show that XRFI is a capable alternative to path-integrated measurements for diagnosing hydrodynamic experiments at high energy density.

  3. X-ray source assembly having enhanced output stability, and fluid stream analysis applications thereof

    DOE Patents [OSTI]

    Radley, Ian; Bievenue, Thomas J.; Burdett Jr., John H.; Gallagher, Brian W.; Shakshober, Stuart M.; Chen, Zewu; Moore, Michael D.

    2007-04-24

    An x-ray source assembly (2700) and method of operation are provided having enhanced output stability. The assembly includes an anode (2125) having a source spot upon which electrons (2120) impinge and a control system (2715/2720) for controlling position of the anode source spot relative to an output structure. The control system can maintain the anode source spot location relative to the output structure (2710) notwithstanding a change in one or more operating conditions of the x-ray source assembly. One aspect of the disclosed invention is most amenable to the analysis of sulfur in petroleum-based fuels.

  4. An x-ray setup to investigate the atomic order of confined liquids in slit geometry

    SciTech Connect (OSTI)

    Lippmann, M.; Ehnes, A.; Seeck, O. H.

    2014-01-15

    A setup has been designed to investigate thin films of confined liquids with the use of X-ray scattering methods. The confinement is realized between the flat culets of a pair of diamonds by positioning and orienting the lower diamond with nanometer and micro radian accuracy. We routinely achieve gaps between 5 and 50 nm at culet diameters of 200 ?m. With this setup and a micro focused X-ray beam we have investigated the in-plane and the out-off-plane atomic order of benzene with atomic resolution.

  5. Pulse energy measurement at the hard x-ray laser in Japan

    SciTech Connect (OSTI)

    Kato, M.; Tanaka, T.; Saito, N.; Kurosawa, T.; Richter, M.; Sorokin, A. A.; Tiedtke, K.; Kudo, T.; Yabashi, M.; Tono, K.; Ishikawa, T.

    2012-07-09

    The pulse energies of a free electron laser have accurately been measured in the hard x-ray spectral range. In the photon energy regime from 4.4 keV to 16.8 keV, pulse energies up to 100 {mu}J were obtained at the hard x-ray laser facility SACLA (SPring-8 Angstrom Compact free-electron LAser). Two independent methods, using a cryogenic radiometer and a gas monitor detector, were applied and agreement within 3.3% was achieved. Based on our validated pulse energy measurement, a SACLA online monitor detector could be calibrated for all future experiments.

  6. Digital real time radiography and X-ray computed tomography development at AWE plc

    SciTech Connect (OSTI)

    Tatum, Paul J. [Metallic Materials Business Area AWE plc, Reading Berkshire England RG7 4PR (United Kingdom)

    1999-12-02

    Digital X-ray imaging promises many advantages over conventional film radiography. The technique collects images electronically thus eliminating X-ray film, chemicals and chemical waste. Many radiographs can be stored on an optical disk or CD ROM and can be retrieved quickly and repeatedly using modern data archiving methods. Data can be transmitted electronically over local networks or the Internet for remote consultations. This paper discusses the development of a lens coupled digital radiography system currently being developed at AWE plc to examine high-density weapon components and sub-assemblies.

  7. X-ray source assembly having enhanced output stability, and fluid stream analysis applications thereof

    DOE Patents [OSTI]

    Radley, Ian (Glenmont, NY); Bievenue, Thomas J. (Delmar, NY); Burdett, John H. (Charlton, NY); Gallagher, Brian W. (Guilderland, NY); Shakshober, Stuart M. (Hudson, NY); Chen, Zewu (Schenectady, NY); Moore, Michael D. (Alplaus, NY)

    2008-06-08

    An x-ray source assembly and method of operation are provided having enhanced output stability. The assembly includes an anode having a source spot upon which electrons impinge and a control system for controlling position of the anode source spot relative to an output structure. The control system can maintain the anode source spot location relative to the output structure notwithstanding a change in one or more operating conditions of the x-ray source assembly. One aspect of the disclosed invention is most amenable to the analysis of sulfur in petroleum-based fuels.

  8. The X-ray Pump–Probe instrument at the Linac Coherent Light Source

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Chollet, Matthieu; Alonso-Mori, Roberto; Cammarata, Marco; Damiani, Daniel; Defever, Jim; Delor, James T.; Feng, Yiping; Glownia, James M.; Langton, J. Brian; Nelson, Silke; et al

    2015-04-21

    The X-ray Pump–Probe instrument achieves femtosecond time-resolution with hard X-ray methods using a free-electron laser source. It covers a photon energy range of 4–24 keV. A femtosecond optical laser system is available across a broad spectrum of wavelengths for generating transient states of matter. The instrument is designed to emphasize versatility and the scientific goals encompass ultrafast physical, chemical and biological processes involved in the transformation of matter and transfer of energy at the atomic scale.

  9. Hard X-ray spatial array diagnostics on Joint Texas Experimental Tokamak

    SciTech Connect (OSTI)

    Huang, D. W.; Chen, Z. Y. Luo, Y. H.; Tong, R. H.; Yan, W.; Jin, W.; Zhuang, G.

    2014-11-15

    A spatially distributed hard X-ray detection array has been developed to diagnose the loss of runaway electron with toroidal and poloidal resolution. The hard X-ray radiation in the energy ranges of 0.3–1 MeV resulted from runaway electrons can be measured. The detection array consists of 12 CdTe detectors which are arranged surrounding the tokamak. It is found that most runaway electrons which transport to plasma boundary tend to loss on limiters. The application of electrode biasing probe resulted in enhancement of local runaway loss. Resonant magnetic perturbations enhanced the runaway electrons diffusion and showed an asymmetric poloidal loss rate.

  10. Hexakis(4-phormylphenoxy)cyclotriphosphazene: X-ray and DFT-calculated structures

    SciTech Connect (OSTI)

    Albayrak, Cigdem Kosar, Basak; Odabasoglu, Mustafa; Bueyuekguengoer, Orhan

    2010-12-15

    The crystal structure of hexakis(4-phormylphenoxy)cyclotriphosphazene is determined by using X-ray diffraction and then the molecular structure is investigated with density functional theory (DFT). X-Ray study shows that the title compound has C-H-{pi} interaction with phosphazene ring. The molecules in the unit cell are packed with Van der Waals and dipole-dipole interactions and the molecules are packed in zigzag shaped. Optimized molecular geometry is calculated with DFT at B3LYP/6-311G(d,p) level. The results from both experimental and theoretical calculations are compared in this study.

  11. Evidence for Centrifugal Barrier in X-ray Pulsar GRO J1744-28

    E-Print Network [OSTI]

    Wei Cui

    1997-12-13

    We present further observational evidence of the effects of a centrifugal barrier in GRO J1744-28, based on continued monitoring of the source with RXTE. For X-ray pulsars, the centrifugal barrier manifests itself in the cessation of pulsed emission when the source becomes faint. We show that such phenomenon occurred repeatedly for GRO J1744-28, following the decay of two X-ray outbursts. This has allowed a direct measurement of the dipole field strength for this pulsar. Here we argue that some of the other peculiar properties observed of this source may also be related to an active centrifugal barrier.

  12. Demonstration of 12 nm resolution Fresnel zone plate lens based soft x-ray microscopy

    SciTech Connect (OSTI)

    Chao, W.; Kim, J.; Rekawa, S.; Fischer, P.; Anderson, E. H.

    2009-06-05

    To extend soft x-ray microscopy to a resolution of order 10 nm or better, we developed a new nanofabrication process for Fresnel zone plate lenses. The new process, based on the double patterning technique, has enabled us to fabricate high quality gold zone plates with 12 nm outer zones. Testing of the zone plate with the full-field transmission x-ray microscope, XM-1, in Berkeley, showed that the lens clearly resolved 12 nm lines and spaces. This result represents a significant step towards 10 nm resolution and beyond.

  13. Measurements of Ionic Structure in Shock Compressed Lithium Hydride from Ultrafast X-Ray Thomson Scattering

    SciTech Connect (OSTI)

    Kritcher, A. L. [L-399, Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551 (United States); Department of Nuclear Engineering, University of California Berkeley, Berkeley, California 94709 (United States); Neumayer, P.; Doeppner, T.; Landen, O. L.; Glenzer, S. H. [L-399, Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551 (United States); Brown, C. R. D. [Department of Physics, Imperial College, London SW7 2AZ (United Kingdom); AWE plc., Aldermaston, Reading, RG7 4PR (United Kingdom); Davis, P. [L-399, Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551 (United States); Department of Physics, University of California Berkeley, Berkeley, California 94709 (United States); Falcone, R. W.; Lee, H. J. [Department of Physics, University of California Berkeley, Berkeley, California 94709 (United States); Gericke, D. O.; Vorberger, J.; Wuensch, K. [CFSA, Department of Physics, University of Warwick, Coventry CV4 7AL (United Kingdom); Gregori, G. [Department of Physics, Oxford University, Oxford OX1 3PU (United Kingdom); Holst, B.; Redmer, R. [Universitaet Rostock, Institut fuer Physik, D-18051 Rostock (Germany); Morse, E. C. [Department of Nuclear Engineering, University of California Berkeley, Berkeley, California 94709 (United States); Pelka, A.; Roth, M. [Institut fuer Kernphysik, Technische Universitaet Darmstadt, Darmstadt (Germany)

    2009-12-11

    We present the first ultrafast temporally, spectrally, and angularly resolved x-ray scattering measurements from shock-compressed matter. The experimental spectra yield the absolute elastic and inelastic scattering intensities from the measured density of free electrons. Laser-compressed lithium-hydride samples are well characterized by inelastic Compton and plasmon scattering of a K-alpha x-ray probe providing independent measurements of temperature and density. The data show excellent agreement with the total intensity and structure when using the two-species form factor and accounting for the screening of ion-ion interactions.

  14. X-ray outburst of CI Cam/XTE J0421+560: RXTE observations

    E-Print Network [OSTI]

    M. Revnivtsev; A. Emelyanov; K. Borozdin

    1999-05-05

    We present the results of observations of XTE J0421+560 X-ray transient with Rossi X-ray Timing Explorer in the beginning of April 1998. Lightcurve, obtained by ASM all-sky monitor, shows unusually fast decrease in the object's luminosity. Spectra from series of observations by PCA and HEXTE experiments were studied in detail. Two emission line regions with energies around 6.5 keV and around 8 keV have been mentioned in the spectra. The possibility of generation of the observed emission in relativistic plasma jet has been discussed. Some analogy is found with known Galactic jet source SS433.

  15. Optical identification of hard X-ray source IGRJ18257-0707

    E-Print Network [OSTI]

    R. A. Burenin; I. F. Bikmaev; M. G. Revnivtsev; J. A. Tomsick; S. Yu. Sazonov; M. N. Pavlinskiy; R. A. Sunyaev

    2008-10-14

    We present the results of the optical identification of hard X-ray source IGRJ18257-0707 trough the spectroscopic observations of its optical counterpart with RTT150 telescope. Accurate position of the X-ray source, determined using Chandra observations, allowed us to associate this source with the faint optical object (m_R=~20.4), which shows broad H_\\alpha emission line in its optical spectrum. Therefore we conclude that the source IGRJ18257-0707 is a type 1 Seyfert galaxy at redshift z=0.037.

  16. Logical operations with single x-ray photons via dynamically-controlled nuclear resonances

    E-Print Network [OSTI]

    Jonas Gunst; Christoph H. Keitel; Adriana Pálffy

    2015-06-01

    The implementation of logical operations on polarization-encoded x-rays via resonant light-nucleus interactions is theoretically investigated. We show that by means of resonant scattering off nuclei and fast rotations of the nuclear hyperfine magnetic field to control the polarization of the output photon, single-qubit logical gates can be simulated. A second control qubit may be employed to trigger the magnetic field rotation, thus allowing several implementation choices for a controlled NOT gate for x-ray photons.

  17. Bessel spatial profile of a soft x-ray laser beam

    SciTech Connect (OSTI)

    Tissandier, F.; Sebban, S.; Ribiere, M.; Gautier, J.; Zeitoun, Ph.; Lambert, G.; Goddet, J.-Ph.; Burgy, F.; Valentin, C.; Rousse, A. [Laboratoire d'Optique Appliquee, ENSTA Paristech/Ecole Polytechnique/CNRS, UMR 7639, F-91761 Palaiseau Cedex (France); Nejdl, J.; Mocek, T. [Institute of Physics, ASCR, Na Slovance 2, CZ-182 21 Prague 8 (Czech Republic); Maynard, G. [Laboratoire de Physique des Gaz et des Plasmas, Universite Paris Sud/CNRS, UMR 8578, F-91405 Orsay Cedex (France)

    2010-12-06

    We report far-field profile measurements of an optical-field-ionized high-order harmonic-seeded soft x-ray laser. We show that the beam transverse profile can be controlled between a regular Gaussian shape and a Bessel profile exhibiting several rings via the infrared laser pump intensity. These experimental data are supported by a complete numerical modeling including a two-dimensional plasma amplifier simulation and a two-level soft x-ray amplification using a Maxwell-Bloch treatment. This model takes into account the experimental high-order harmonic wavefront and intensity before it is numerically amplified.

  18. Maskelynite formation via solid-state transformation: Evidence of infrared and x-ray anisotropy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Jaret, Steven J.; Ehm, Lars; Woerner, William R.; Phillips, Brian L.; Nekvasil, Hanna; Wright, Shawn P.; Glotch, Timothy D.

    2015-03-24

    We present optical microscopy, micro-Raman spectroscopy, nuclear magnetic resonance (NMR) spectroscopy, high-energy X-ray total scattering experiments, and micro-Fourier transform infrared (micro-FTIR) spectroscopy on shocked labradorite from the Lonar Crater, India. We show that maskelynite of shock class 2 is structurally more similar to fused glass than to crystalline plagioclase. However, there are slight but significant differences – preservation of original pre-impact igneous zoning, anisotropy at Infrared wavelengths, X-ray anisotropy, and preservation of some intermediate range order – which are all consistent with a solid-state transformation formation of maskelynite.

  19. Chandra Imaging of the X-ray Core of the Virgo Cluster

    E-Print Network [OSTI]

    A. J. Young; A. S. Wilson; C. G. Mundell

    2002-07-15

    We report sub-arcsecond X-ray imaging spectroscopy of M87 and the core of the Virgo cluster with the Chandra X-ray Observatory. The X-ray morphology shows structure on arcsecond (~100 pc) to ten arcminute (~50 kpc) scales, the most prominent feature being an "arc" running from the east, across the central region of M87 and off to the southwest. A ridge in the radio map, ending in an "ear"-shaped structure, follows the arc to the east. Depressions in the X-ray surface brightness correspond to the inner radio lobes and there is no evidence of shock-heated gas surrounding them. There are also at least two approximately circular (centered near the nucleus) "edges" in the X-ray brightness distribution, the radii of which are slightly larger than the nuclear distances of the inner radio lobes and intermediate radio ridges, respectively. We speculate that these discontinuities may be spherical pulses or "fronts" driven by the same jet activity as is responsible for the radio structure; such pulses are found in recent numerical simulations. All these results provide good evidence that the nuclear activity affects the intra-cluster medium. We present a temperature map of the intra-cluster medium, and obtain the temperature, pressure and cooling time as a function of nuclear distance for the arcs and the ambient intra-cluster medium. We show that the gas in the arcs is cooler than, and probably over-pressured with respect to, the ambient intra-cluster medium. The metal abundances of the cooler gas in the arc are somewhat enhanced relative to the ambient intra-cluster medium, favoring a ``buoyant plume'' origin for the X-ray arc, in which ambient gas near the nucleus is entrained by buoyant radio plasma and carried to larger nuclear distances. (Abstract truncated).

  20. Hard x-ray tomographic studies of the destruction of an energetic electron ring

    SciTech Connect (OSTI)

    Wang, Y.; Gekelman, W.; Pribyl, P.

    2013-05-15

    A tomography system was designed and built at the Large Plasma Device to measure the spatial distribution of hard x-ray (100 KeV-3 MeV) emissivity. The x-rays were generated when a hot electron ring was significantly disrupted by a shear Alfven wave. The plasma is pulsed at 1 Hz (1 shot/s). A lead shielded scintillator detector with an acceptance angle defined by a lead pinhole is mounted on a rotary gimbal and used to detect the x-rays. The system measures one chord per plasma shot using only one detector. A data plane usually consists of several hundred chords. A novel Dot by Dot Reconstruction (DDR) method is introduced to calculate the emissivity profile from the line integrated data. In the experiments, there are often physical obstructions, which make measurements at certain angles impossible. The DDR method works well even in this situation. The method was tested with simulated data, and was found to be more effective than previously published methods for the specific geometry of this experiment. The reconstructed x-ray emissivity from experimental data by this method is shown.

  1. X-rays from magnetically channeled winds of OB stars

    E-Print Network [OSTI]

    David H. Cohen

    2008-01-30

    OB stars with strong radiation-driven stellar winds and large-scale magnetic fields generate strong and hard X-ray emission via the Magnetically Channeled Wind Shock (MCWS) mechanism. In this brief paper, I describe four separate X-ray diagnostics of the MCWS mechanism in OB stars, with applications to the prototype young O star, theta-1 Ori C.

  2. Electromagnetic Application: X-RAY Alawi H. Ba-Surrah

    E-Print Network [OSTI]

    Masoudi, Husain M.

    , Pulyui published high-quality x-ray images in journals in Paris and London. · Nikola Tesla In April 1887, Nikola Tesla began to investigate X-rays using high voltages and tubes of his own design, as well. The principle behind Tesla's device is called the Bremsstrahlung process, in which a high-energy secondary X

  3. HIGH-RESOLUTION X-RAY SPECTROSCOPY OF CRUCIS: A

    E-Print Network [OSTI]

    Cohen, David

    a corona; clear presence of UV driven wind at moderate temperatures; lack of wind X-ray absorption edges the years, consen- sus has thus instead favored an Intrinsic Wind Shock (IWS) model, in which the X-ray emission comes from shocks distributed throughout the wind, most likely arising from the strong, intrinsic

  4. X-rays from Hot Stars: Stellar Astronomy Research with

    E-Print Network [OSTI]

    Cohen, David

    emission lines Hot stars*: massive outflows ("stellar winds") ­ are the x-rays associated with these winds can actually take an image of its "wind nebula" ­ in all other cases, we infer the presence of a wind a model for fitting the detailed shapes of x-ray emission line profiles from hot star winds The very hot

  5. National School on Neutron and X-ray Scattering

    E-Print Network [OSTI]

    15th National School on Neutron and X-ray Scattering August 10 - 24, 2013 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

  6. Thirteenth National School on Neutron and X-ray Scattering

    E-Print Network [OSTI]

    Thirteenth National School on Neutron and X-ray Scattering June 11 ­ June 25, 2011 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

  7. Sixteenth National School on Neutron and X-ray Scattering

    E-Print Network [OSTI]

    Pennycook, Steve

    Sixteenth National School on Neutron and X-ray Scattering June 14-28, 2014 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major's Neutron Scattering Science Division. Scientific Directors: Suzanne G.E. te Velthuis, Esen Ercan Alp

  8. Neutron and X-ray Scattering Study of Magnetic Manganites

    E-Print Network [OSTI]

    Boothroyd, Andrew

    Neutron and X-ray Scattering Study of Magnetic Manganites Graeme Eoin Johnstone A Thesis submitted are performed using a variety of neutron scattering and x-ray scattering techniques. The electronic ground for analysing the results of the polarised neutron scattering experiment. There are a large number of people who

  9. National School on Neutron and X-ray Scattering

    E-Print Network [OSTI]

    Pennycook, Steve

    National School on Neutron and X-ray Scattering May 30 ­ June 13, 2009 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

  10. Fourteenth National School on Neutron and X-ray Scattering

    E-Print Network [OSTI]

    Pennycook, Steve

    Fourteenth National School on Neutron and X-ray Scattering August 12 - 25, 2012 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

  11. Twelfth National School on Neutron and X-ray Scattering

    E-Print Network [OSTI]

    Pennycook, Steve

    Twelfth National School on Neutron and X-ray Scattering June 12 ­ June 26, 2010 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

  12. Tenth National School on Neutron and X-ray Scattering

    E-Print Network [OSTI]

    Pennycook, Steve

    Tenth National School on Neutron and X-ray Scattering September 24 - October 11, 2008 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

  13. Millisecond oscillations during thermonuclear X-ray bursts

    E-Print Network [OSTI]

    Muno, Michael Patrick, 1975-

    2002-01-01

    I analyze 68 oscillation trains detected in a search of 159 thermonuclear bursts from eight neutron star X-ray binaries observed with the Rossi X-ray Timing Explorer. I use all data that were public as of September 2001. ...

  14. Microwave and hard X-ray imaging observations of

    E-Print Network [OSTI]

    White, Stephen

    Microwave and hard X-ray imaging observations of energetic electrons in solar flares: event of 2003 to nonthermal energies are seen via microwave and hard X-ray emission from the solar corona. Imaging sophisticated and fully dedicated solar radio telescope operating at microwave frequencies (17 & 34 GHz) capable

  15. Advances in x-ray computed microtomography at the NSLS

    SciTech Connect (OSTI)

    Dowd, B.A.; Andrews, A.B.; Marr, R.B.; Siddons, D.P.; Jones, K.W.; Peskin, A.M.

    1998-08-01

    The X-Ray Computed Microtomography workstation at beamline X27A at the NSLS has been utilized by scientists from a broad range of disciplines from industrial materials processing to environmental science. The most recent applications are presented here as well as a description of the facility that has evolved to accommodate a wide variety of materials and sample sizes. One of the most exciting new developments reported here resulted from a pursuit of faster reconstruction techniques. A Fast Filtered Back Transform (FFBT) reconstruction program has been developed and implemented, that is based on a refinement of the gridding algorithm first developed for use with radio astronomical data. This program has reduced the reconstruction time to 8.5 sec for a 929 x 929 pixel{sup 2} slice on an R10,000 CPU, more than 8x reduction compared with the Filtered Back-Projection method.

  16. X-ray studies of concentrated aqueous solutions

    SciTech Connect (OSTI)

    Ludwig, K.F. Jr.; Warburton, W.K.; Fontaine, A.

    1987-07-01

    Concentrated aqueous solutions of three transition metal bromides (ZnBr/sub 2/, CuBr/sub 2/, and NiBr/sub 2/) and an alkali bromide (RbBr) have been studied with differential anomalous scattering (DAS) and extended x-ray absorption fine structure (EXAFS). The aq-ZnBr/sub 2/ solutions exhibit considerable inner-shell ion complexing with the formation of tetrahedral complexes about the Zn/sup 2 +/. In aq-CuBr/sub 2/, the Cu/sup 2 +/ has an octahedral coordination shell. Most of the anions are bound directly to the cations in both solutions. In contrast, there are only a few Ni--Br nearest neighbors in aq-NiBr/sub 2/. Instead, cations and anions share hydrating water molecules. Preliminary data show that any ion complexing in aq-RbBr must be weak. These results are in good agreement with published thermodynamic studies.

  17. Near Infrared observations of Soft X-ray selected AGN

    E-Print Network [OSTI]

    D. Grupe; H. -C Thomas

    2002-02-21

    We report the results of near infrared observations of 19 soft X-ray selected AGN. The goal of the observations was to search for strong, narrow Paschen-alpha or Brackett-gamma emission lines, as a sign of nuclear starbursts. We found Pa-alpha emission in the spectra of 11 sources and Br-gamma in at least five. Strong NIR emission has been found in two sources, CBS 126 and Mkn 766, both objects with strong [OIII]5007 emission, weak FeII emission and wavelength dependent degree of polarization in the optical. Classical Narrow Line Seyfert 1 galaxies do not show exceptionally strong NIR emission lines. We present the results of our study and discuss how our findings fit into an evolutionary scheme of AGN.

  18. Broadband high resolution X-ray spectral analyzer

    DOE Patents [OSTI]

    Silver, E.H.; Legros, M.; Madden, N.W.; Goulding, F.; Landis, D.

    1998-07-07

    A broad bandwidth high resolution X-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces X-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available X-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for X-ray microanalysis or in research applications such as laboratory and astrophysical X-ray and particle spectroscopy. 6 figs.

  19. ZAP! The X-Ray Laser is Born

    SciTech Connect (OSTI)

    Ratner, Daniel

    2009-11-17

    SLAC has converted its giant particle accelerator into the world's first X-ray laser. By a billion fold the world's brightest X-ray source, the laser packs a trillion photons into pulses as short as a millionth of a billionth of a second. The ultra-bright, ultra-short X-ray pulses will drive a wide range of new experiments, as scientists strip electrons from atoms, photograph single molecules and make movies of chemical reactions. How has SLAC accomplished such feats of X-ray wizardry? Attend this public lecture to learn about the basics of an X-ray laser, the technologies at SLAC that make it possible, and the exciting new experiments now underway.

  20. High spatial resolution X-ray and gamma ray imaging system using diffraction crystals

    DOE Patents [OSTI]

    Smither, Robert K. (Hinsdale, IL)

    2011-05-17

    A method and a device for high spatial resolution imaging of a plurality of sources of x-ray and gamma-ray radiation are provided. The device comprises a plurality of arrays, with each array comprising a plurality of elements comprising a first collimator, a diffracting crystal, a second collimator, and a detector.

  1. Faint X-ray binaries and their optical counterparts in M31

    SciTech Connect (OSTI)

    Vulic, N.; Gallagher, S. C.; Barmby, P., E-mail: nvulic@uwo.ca [Department of Physics and Astronomy, Western University, London, ON, N6A 3K7 (Canada)

    2014-08-01

    X-ray binaries (XRBs) are probes of both star formation and stellar mass, but more importantly remain one of the only direct tracers of the compact object population. To investigate the XRB population in M31, we utilized all 121 publicly available observations of M31 totalling over 1 Ms from Chandra's ACIS instrument. We studied 83 star clusters in the bulge using the year 1 star cluster catalogue from the Panchromatic Hubble Andromeda Treasury Survey. We found 15 unique star clusters that matched to 17 X-ray point sources within 1'' (3.8 pc). This population is composed predominantly of globular cluster low-mass XRBs, with one previously unidentified star cluster X-ray source. Star clusters that were brighter and more compact preferentially hosted an X-ray source. Specifically, logistic regression showed that the F475W magnitude was the most important predictor followed by the effective radius, while color (F475W–F814W) was not statistically significant. We also completed a matching analysis of 1566 H II regions and found 10 unique matches to 9 X-ray point sources within 3'' (11 pc). The H II regions hosting X-ray point sources were on average more compact than unmatched H II regions, but logistic regression concluded that neither the radius nor H? luminosity was a significant predictor. Four matches have no previous classification and thus are high-mass XRB candidates. A stacking analysis of both star clusters and H II regions resulted in non-detections, giving typical upper limits of ?10{sup 32} erg s{sup –1}, which probes the quiescent XRB regime.

  2. High-order multilayer coated blazed gratings for high resolution soft x-ray spectroscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Voronov, Dmitriy L.; Goray, Leonid I.; Warwick, Tony; Yashchuk, Valeriy V.; Padmore, Howard A.

    2015-02-17

    A grand challenge in soft x-ray spectroscopy is to drive the resolving power of monochromators and spectrometers from the 104 achieved routinely today to well above 105. This need is driven mainly by the requirements of a new technique that is set to have enormous impact in condensed matter physics, Resonant Inelastic X-ray Scattering (RIXS). Unlike x-ray absorption spectroscopy, RIXS is not limited by an energy resolution dictated by the core-hole lifetime in the excitation process. Using much higher resolving power than used for normal x-ray absorption spectroscopy enables access to the energy scale of soft excitations in matter. Thesemore »excitations such as magnons and phonons drive the collective phenomena seen in correlated electronic materials such as high temperature superconductors. RIXS opens a new path to study these excitations at a level of detail not formerly possible. However, as the process involves resonant excitation at an energy of around 1 keV, and the energy scale of the excitations one would like to see are at the meV level, to fully utilize the technique requires the development of monochromators and spectrometers with one to two orders of magnitude higher energy resolution than has been conventionally possible. Here we investigate the detailed diffraction characteristics of multilayer blazed gratings. These elements offer potentially revolutionary performance as the dispersive element in ultra-high resolution x-ray spectroscopy. In doing so, we have established a roadmap for the complete optimization of the grating design. Traditionally 1st order gratings are used in the soft x-ray region, but we show that as in the optical domain, one can work in very high spectral orders and thus dramatically improve resolution without significant loss in efficiency.« less

  3. Single mimivirus particles intercepted and imaged with an X-ray laser (CXIDB ID 2)

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Seibert, M. Marvin; Ekeberg, Tomas

    These are the files used to reconstruct the images in the paper "Single Mimivirus particles intercepted and imaged with an X-ray laser". Besides the diffracted intensities, the Hawk configuration files used for the reconstructions are also provided. The files from CXIDB ID 2 are the pattern and configuration files for the pattern showed in Figure 2b in the paper.

  4. Resonance scattering in X-ray line profiles of Pup Clumping in Hot Star Winds

    E-Print Network [OSTI]

    Cohen, David

    Resonance scattering in X-ray line profiles of Pup Clumping in Hot Star Winds W.-R. Hamann, A the same wind parameters. We show that the differences in profile shape can be accounted for in a model its effect is difficult to distinguish from a low effective continuum optical depth in the wind. Thus

  5. Single mimivirus particles intercepted and imaged with an X-ray laser (CXIDB ID 2)

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Seibert, M. Marvin; Ekeberg, Tomas

    2011-02-02

    These are the files used to reconstruct the images in the paper "Single Mimivirus particles intercepted and imaged with an X-ray laser". Besides the diffracted intensities, the Hawk configuration files used for the reconstructions are also provided. The files from CXIDB ID 2 are the pattern and configuration files for the pattern showed in Figure 2b in the paper.

  6. Single mimivirus particles intercepted and imaged with an X-ray laser (CXIDB ID 1)

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Seibert, M. Marvin; Ekeberg, Tomas; Maia, Filipe R.N.C.

    2011-02-02

    These are the files used to reconstruct the images in the paper "Single Mimivirus particles intercepted and imaged with an X-ray laser". Besides the diffracted intensities, the Hawk configuration files used for the reconstructions are also provided. The files from CXIDB ID 1 are the pattern and configuration files for the pattern showed in Figure 2a in the paper.

  7. Single mimivirus particles intercepted and imaged with an X-ray laser (CXIDB ID 1)

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Seibert, M. Marvin; Ekeberg, Tomas; Maia, Filipe R.N.C.

    These are the files used to reconstruct the images in the paper "Single Mimivirus particles intercepted and imaged with an X-ray laser". Besides the diffracted intensities, the Hawk configuration files used for the reconstructions are also provided. The files from CXIDB ID 1 are the pattern and configuration files for the pattern showed in Figure 2a in the paper.

  8. Bent Crystal X-Ray Mirrors for Time-Resolved Experiments with Femtosecond Laser-Produced X-ray Pulses

    E-Print Network [OSTI]

    von der Linde, D.

    Bent Crystal X-Ray Mirrors for Time-Resolved Experiments with Femtosecond Laser-Produced X@iep.physik.uni-essen.de Abstract. In the last few years, bent crystal X-ray mirrors have played an important role in time, for example, with the help of toroidally bent crystals which allow a monochromatic point-to-point imaging

  9. X-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND

    E-Print Network [OSTI]

    Bergen, Universitetet i

    X-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND ANIL BHARDWAJ extraterrestrische Physik, Garching, Germany 6 Applied Physics Laboratory, John Hopkins University, Laurel, MD 20723 planets Jupiter and Saturn in the energy range of 0.2-2 keV. These flares are found to occur in tandem

  10. Millimeter, Microwave, Hard X--ray and Soft X--ray Observations of Energetic Electron Populations in Solar Flares

    E-Print Network [OSTI]

    White, Stephen

    Millimeter, Microwave, Hard X--ray and Soft X--ray Observations of Energetic Electron Populations in Solar Flares M. R. Kundu 1 , S. M. White 1 , N. Gopalswamy 1 and J. Lim 1,2 1 Dept. of Astronomy, Univ. of Maryland, College Park MD 20742 2 Solar Astronomy 264--33, Caltech, Pasadena CA 91125 Submitted

  11. Efficacy of fixed filtration for rapid kVp-switching dual energy x-ray systems

    SciTech Connect (OSTI)

    Yao, Yuan; Wang, Adam S.; Pelc, Norbert J.; Department of Radiology, Stanford University, Stanford, California 94305; Department of Electrical Engineering, Stanford University, Stanford, California 94305

    2014-03-15

    Purpose: Dose efficiency of dual kVp imaging can be improved if the two beams are filtered to remove photons in the common part of their spectra, thereby increasing spectral separation. While there are a number of advantages to rapid kVp-switching for dual energy, it may not be feasible to have two different filters for the two spectra. Therefore, the authors are interested in whether a fixed added filter can improve the dose efficiency of kVp-switching dual energy x-ray systems. Methods: The authors hypothesized that a K-edge filter would provide the energy selectivity needed to remove overlap of the spectra and hence increase the precision of material separation at constant dose. Preliminary simulations were done using calcium and water basis materials and 80 and 140 kVp x-ray spectra. Precision of the decomposition was evaluated based on the propagation of the Poisson noise through the decomposition function. Considering availability and cost, the authors chose a commercial Gd{sub 2}O{sub 2}S screen as the filter for their experimental validation. Experiments were conducted on a table-top system using a phantom with various thicknesses of acrylic and copper and 70 and 125 kVp x-ray spectra. The authors kept the phantom exposure roughly constant with and without filtration by adjusting the tube current. The filtered and unfiltered raw data of both low and high energy were decomposed into basis material and the variance of the decomposition for each thickness pair was calculated. To evaluate the filtration performance, the authors measured the ratio of material decomposition variance with and without filtration. Results: Simulation results show that the ideal filter material depends on the object composition and thickness, and ranges across the lanthanide series, with higher atomic number filters being preferred for more attenuating objects. Variance reduction increases with filter thickness, and substantial reductions (40%) can be achieved with a 2× loss in intensity. The authors’ experimental results validate the simulations, yet were overall slightly worse than expectation. For large objects, conventional (non-K-edge) beam hardening filters perform well. Conclusions: This study demonstrates the potential of fixed K-edge filtration to improve the dose efficiency and material decomposition precision for rapid kVp-switching dual energy systems.

  12. ESTIMATE OF SOLAR MAXIMUM USING THE 1-8 Å GEOSTATIONARY OPERATIONAL ENVIRONMENTAL SATELLITES X-RAY MEASUREMENTS

    SciTech Connect (OSTI)

    Winter, L. M.; Balasubramaniam, K. S.

    2014-10-01

    We present an alternate method of determining the progression of the solar cycle through an analysis of the solar X-ray background. Our results are based on the NOAA Geostationary Operational Environmental Satellites (GOES) X-ray data in the 1-8 Å band from 1986 to the present, covering solar cycles 22, 23, and 24. The X-ray background level tracks the progression of the solar cycle through its maximum and minimum. Using the X-ray data, we can therefore make estimates of the solar cycle progression and the date of solar maximum. Based upon our analysis, we conclude that the Sun reached its hemisphere-averaged maximum in solar cycle 24 in late 2013. This is within six months of the NOAA prediction of a maximum in spring 2013.

  13. Estimate of Solar Maximum using the 1-8 \\AA$\\,$Geostationary Operational Environmental Satellites X-ray Measurements

    E-Print Network [OSTI]

    Winter, L M

    2014-01-01

    We present an alternate method of determining the progression of the solar cycle through an analysis of the solar X-ray background. Our results are based on the NOAA Geostationary Operational Environmental Satellites (GOES) X-ray data in the 1-8 \\AA$\\,$band from 1986 - present, covering solar cycles 22, 23, and 24. The X-ray background level tracks the progression of the solar cycle through its maximum and minimum. Using the X-ray data, we can therefore make estimates of the solar cycle progression and date of solar maximum. Based upon our analysis, we conclude that the Sun reached its hemisphere-averaged maximum in Solar Cycle 24 in late 2013. This is within six months of the NOAA prediction of a maximum in Spring 2013.

  14. Comparison of SOFC Cathode Microstructure Quantified using X-ray Nanotomography and Focused Ioni Beam-scanning Electron Microscopy

    SciTech Connect (OSTI)

    G Nelson; W Harris; J Lombardo; J Izzo Jr.; W Chiu; P Tanasini; M Cantoni; J Van herle; C Comninellis; et al.

    2011-12-31

    X-ray nanotomography and focused ion beam scanning electron microscopy (FIB-SEM) have been applied to investigate the complex 3D microstructure of solid oxide fuel cell (SOFC) electrodes at spatial resolutions of 45 nm and below. The application of near edge differential absorption for x-ray nanotomography and energy selected backscatter detection for FIB-SEM enable elemental mapping within the microstructure. Using these methods, non-destructive 3D x-ray imaging and FIB-SEM serial sectioning have been applied to compare three-dimensional elemental mapping of the LSM, YSZ, and pore phases in the SOFC cathode microstructure. The microstructural characterization of an SOFC cathode is reported based on these measurements. The results presented demonstrate the viability of x-ray nanotomography as a quantitative characterization technique and provide key insights into the SOFC cathode microstructure.

  15. Comparison of SOFC Cathode Microstructure Quantified using X-ray Nanotomography and Focused Ion Beam - Scanning Electron Microscopy

    SciTech Connect (OSTI)

    Nelson, George J.; Harris, William H.; Lombardo, Jeffrey J.; Izzo, Jr., John R.; Chiu, W. K. S.; Tanasini, Pietro; Cantoni, Marco; Van herle, Jan; Comninellis, Christos; Andrews, Joy C.; Liu, Yijin; Pianetta, Piero; Chu, Yong

    2011-03-24

    X-ray nanotomography and focused ion beam scanning electron microscopy (FIB-SEM) have been applied to investigate the complex 3D microstructure of solid oxide fuel cell (SOFC) electrodes at spatial resolutions of 45 nm and below. The application of near edge differential absorption for x-ray nanotomography and energy selected backscatter detection for FIB–SEM enable elemental mapping within the microstructure. Using these methods, non-destructive 3D x-ray imaging and FIB–SEM serial sectioning have been applied to compare three-dimensional elemental mapping of the LSM, YSZ, and pore phases in the SOFC cathode microstructure. The microstructural characterization of an SOFC cathode is reported based on these measurements. The results presented demonstrate the viability of x-ray nanotomography as a quantitative characterization technique and provide key insights into the SOFC cathode microstructure.

  16. X-ray Computed Tomography of coal: Final report

    SciTech Connect (OSTI)

    Maylotte, D.H.; Spiro, C.L.; Kosky, P.G.; Lamby, E.J.

    1986-12-01

    X-ray Computed Tomography (CT) is a method of mapping with x-rays the internal structures of coal. The technique normally produces 2-D images of the internal structures of an object. These images can be recast to create pseudo 3-D representations. CT of coal has been explored for a variety of different applications to coal and coal processing technology. In a comparison of CT data with conventional coal analyses and petrography, CT was found to offer a good indication of the total ash content of the coal. The spatial distribution of the coal mineral matter as seen with CT has been suggested as an indicator of coal washability. Studies of gas flow through coal using xenon gas as a tracer have shown the extremely complicated nature of the modes of penetration of gas through coal, with significant differences in the rates at which the gas can pass along and across the bedding planes of coal. In a special furnace designed to allow CT images to be taken while the coal was being heated, the pyrolysis and gasification of coal have been studied. Gasification rates with steam and CO/sub 2/ for a range of coal ranks have been obtained, and the location of the gasification reactions within the piece of coal can be seen. Coal drying and the progress of the pyrolysis wave into coal have been examined when the coal was subjected to the kind of sudden temperature jump that it might experience in fixed bed gasifier applications. CT has also been used to examine stable flow structures within model fluidized beds and the accessibility of lump coal to microbial desulfurization. 53 refs., 242 figs., 26 tabs.

  17. Constraining Black Hole Spin Via X-ray Spectroscopy

    E-Print Network [OSTI]

    Laura W. Brenneman; Christopher S. Reynolds

    2006-08-23

    We present an analysis of the observed broad iron line feature and putative warm absorber in the long 2001 XMM-Newton observation of the Seyfert-1.2 galaxy MCG-6-30-15. The new "kerrdisk" model we have designed for simulating line emission from accretion disk systems allows black hole spin to be a free parameter in the fit, enabling the user to formally constrain the angular momentum of a black hole, among other physical parameters of the system. In an important extension of previous work, we derive constraints on the black hole spin in MCG-6-30-15 using a self-consistent model for X-ray reflection from the surface of the accretion disk while simultaneously accounting for absorption by dusty photoionized material along the line of sight (the warm absorber). Even including these complications, the XMM-Newton/EPIC-pn data require extreme relativistic broadening of the X-ray reflection spectrum; assuming no emission from within the radius of marginal stability, we derive a formal constraint on the dimensionless black hole spin parameter of a > 0.987 at 90% confidence. The principal unmodeled effect that can significantly reduce the inferred black hole spin is powerful emission from within the radius of marginal stability. Although significant theoretical developments are required to fully understand this region, we argue that the need for a rapidly spinning black hole is robust to physically plausible levels of emission from within the radius of marginal stability. In particular, we show that a non-rotating black hole is strongly ruled out.

  18. NSLS-II X-Ray Diagnostics Development

    SciTech Connect (OSTI)

    ILINSKI, P.

    2011-03-28

    NSLS-II x-ray diagnostics will provide continuous online data of electron beam dimensions, which will be used to derive electron beam emittance and energy spread. It will also provide information of electron beam tilt for coupling evaluation. X-ray diagnostics will be based on imaging of bending magnet and three-pole wiggler synchrotron radiation sources. Diagnostics from three-pole wiggler source will be used to derive particles energy spread. Beta and dispersion functions will have to be evaluated for emittance and particles energy spread calculations. Due to small vertical source sizes imaging need to be performed in x-ray energy range. X-ray optics with high numerical aperture, such as compound refractive lens, will be used to achieve required spatial resolution. Optical setups with different magnifications in horizontal and vertical directions fill be employed to deal with large aspect ratio of the source. X-ray diagnostics setup will include x-ray imaging optics, monochromatization, x-ray imaging and recording components.

  19. A remarkable recurrent nova in M 31: The predicted 2014 outburst in X-rays with Swift

    E-Print Network [OSTI]

    Henze, M; Darnley, M J; Bode, M F; Williams, S C; Shafter, A W; Sala, G; Kato, M; Hachisu, I; Hernanz, M

    2015-01-01

    The M 31 nova M31N 2008-12a was recently found to be a recurrent nova (RN) with a recurrence time of about 1 year. This is by far the fastest recurrence time scale of any known RNe. Our optical monitoring programme detected the predicted 2014 outburst of M31N 2008-12a in early October. We immediately initiated an X-ray/UV monitoring campaign with Swift to study the multiwavelength evolution of the outburst. We monitored M31N 2008-12a with daily Swift observations for 20 days after discovery, covering the entire supersoft X-ray source (SSS) phase. We detected SSS emission around day six after outburst. The SSS state lasted for approximately two weeks until about day 19. M31N 2008-12a was a bright X-ray source with a high blackbody temperature. The X-ray properties of this outburst were very similar to the 2013 eruption. Combined X-ray spectra show a fast rise and decline of the effective blackbody temperature. The short-term X-ray light curve showed strong, aperiodic variability which decreased significantly a...

  20. Complete multiwavelength evolution of galactic black hole transients during outburst decay. II. Compact jets and X-ray variability properties

    SciTech Connect (OSTI)

    Dinçer, T.; Kalemci, E.; Tomsick, J. A.; Buxton, M. M.; Bailyn, C. D.

    2014-11-01

    We investigated the relation between compact jet emission and X-ray variability properties of all black hole transients with multiwavelength coverage during their outburst decays. We studied the evolution of all power spectral components (including low-frequency quasi-periodic oscillations; QPOs), and related this evolution to changes in jet properties tracked by radio and infrared observations. We grouped sources according to their tracks in the radio/X-ray luminosity relation and show that the standards show stronger broadband X-ray variability than outliers at a given X-ray luminosity when the compact jet turns on. This trend is consistent with the internal shock model and can be important for the understanding of the presence of tracks in the radio/X-ray luminosity relation. We also observed that the total and the QPO rms amplitudes increase together during the earlier part of the outburst decay, but after the compact jet turns, either the QPO disappears or its rms amplitude decreases significantly while the total rms amplitudes remain high. We discuss these results with a scenario including a variable corona and a non-variable disk with a mechanism for the QPO separate from the mechanism that creates broad components. Finally, we evaluated the timing predictions of the magnetically dominated accretion flow model that can explain the presence of tracks in the radio/X-ray luminosity relation.

  1. Deep Near Infrared Observations of the X-ray Emitting Class 0 Protostar Candidates in the Orion Molecular Cloud-3

    E-Print Network [OSTI]

    M. Tsujimoto; K. Koyama; Y. Tsuboi; G. Chartas; M. Goto; N. Kobayashi; H. Terada; A. T. Tokunaga

    2002-03-09

    We obtained near infrared (NIR) imaging with the Subaru Telescope of the class 0 protostar candidates in the Orion Molecular Cloud-3, two of which were discovered to have X-ray emission by the Chandra X-ray Observatory. We found strong evidence for the class~0 nature of the X-ray sources. First, our deep K-band image shows no emission brighter than 19.6 mag from both of these X-ray sources. Since class I protostars or class II T Tauri stars should be easily detected in the NIR with this sensitivity, the lack of K-band detection suggests that they are likely much more obscured than class I protostars. Second, our H2 v=1-0 S(1) image shows a bubble-like feature from one of the X-ray class 0 protostar candidates, which reinforces the idea that this is a class 0 protostar. We also discuss the nature of nine NIR sources found in our deep image based on their colors, spatial coincidence with millimeter cores, and the properties of their X-ray counterparts.

  2. Protein crystallography: From X-ray diffraction spots to a three dimensional image

    SciTech Connect (OSTI)

    Terwilliger, T.C.; Berendzen, J.

    1998-02-25

    Proteins are remarkable molecular machines that are essential for life. They can do many things ranging from the precise control of blood clotting to synthesizing complex organic compounds. Pictures of protein molecules are in high demand in biotechnology because they are important for applications such as drug discovery and for engineering enzymes for commercial use. X-ray crystallography is the most common method for determining the three-dimensional structures of protein molecules. When a crystal of a protein is placed in an X-ray beam, scattering of X-rays off the ordered molecules produces a diffraction pattern that can be measured on a position-sensitive CCD or image-plate detector. Protein crystals typically contain thousands of atoms and the diffraction data are generally measured to relatively low resolution. Consequently the direct methods approaches generally cannot be applied. Instead, if the crystal is modified by adding metal atoms at specific sites or by tuning the wavelength of the X-rays to cross an absorption edge of a metal atom in the crystal, then the information from these additional measurements is sufficient to first identify the /locations of the metal atoms. This information is then used along with the diffraction data to make a three-dimensional picture of electron densities. This picture can be used to determine the position of most or all of the atoms in the protein.

  3. Apparatus for generating x-ray holograms

    DOE Patents [OSTI]

    Rhodes, C.K.; Boyer, K.; Solem, J.C.; Haddad, W.S.

    1990-09-11

    Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced. 7 figs.

  4. Apparatus for generating x-ray holograms

    DOE Patents [OSTI]

    Rhodes, Charles K. (Chicago, IL); Boyer, Keith (Los Alamos, NM); Solem, Johndale C. (Los Alamos, NM); Haddad, Waleed S. (Chicago, IL)

    1990-01-01

    Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced.

  5. Simultaneous cryo X-ray ptychographic and fluorescence microscopy of green algae

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Deng, Junjing; Vine, David J.; Chen, Si; Nashed, Youssef S. G.; Jin, Qiaoling; Phillips, Nicholas W.; Peterka, Tom; Ross, Rob; Vogt, Stefan; Jacobsen, Chris J.

    2015-02-24

    Trace metals play important roles in normal and in disease-causing biological functions. X-ray fluorescence microscopy reveals trace elements with no dependence on binding affinities (unlike with visible light fluorophores) and with improved sensitivity relative to electron probes. However, X-ray fluorescence is not very sensitive for showing the light elements that comprise the majority of cellular material. Here we show that X-ray ptychography can be combined with fluorescence to image both cellular structure and trace element distribution in frozen-hydrated cells at cryogenic temperatures, with high structural and chemical fidelity. Ptychographic reconstruction algorithms deliver phase and absorption contrast images at a resolutionmore »beyond that of the illuminating lens or beam size. Using 5.2-keV X-rays, we have obtained sub–30-nm resolution structural images and ~90-nm–resolution fluorescence images of several elements in frozen-hydrated green algae. This combined approach offers a way to study the role of trace elements in their structural context.« less

  6. Resonant x-ray magnetic scattering in holmium

    SciTech Connect (OSTI)

    Gibbs, D.

    1991-01-01

    We review the results of resonant x-ray magnetic scattering experiments on the rare earth metal holmium. When the incident incident x-ray energy is tuned near the L{sub III} absorption edge, large resonant enhancements of the magnetic scattering and resonant integer harmonics are observed. These results are analyzed within the theory of x-ray resonance exchange scattering assuming electric dipole (2p {yields} 5d) and quadrupole (2p {yields} 4f) transitions among atomic orbitals. 30 refs., 5 figs.

  7. X-ray backscatter imaging of nuclear materials

    DOE Patents [OSTI]

    Chapman, Jeffrey Allen; Gunning, John E; Hollenbach, Daniel F; Ott, Larry J; Shedlock, Daniel

    2014-09-30

    The energy of an X-ray beam and critical depth are selected to detect structural discontinuities in a material having an atomic number Z of 57 or greater. The critical depth is selected by adjusting the geometry of a collimator that blocks backscattered radiation so that backscattered X-ray originating from a depth less than the critical depth is not detected. Structures of Lanthanides and Actinides, including nuclear fuel rod materials, can be inspected for structural discontinuities such as gaps, cracks, and chipping employing the backscattered X-ray.

  8. Optical and X-ray Variability of Blazars

    E-Print Network [OSTI]

    Gupta, A C

    2015-01-01

    Here we report our recent results of variability studies in optical and X-ray bands of three blazars namely 3C 273, PKS 2155 - 304 and BL Lacertae with XMM-Newton. We found large amplitude optical to X-rays variability in 3C 273, and PKS 2155 - 304 on year time scale. In 3C 273, we noticed that synchrotron cooling and particle acceleration are at work at different epoch of observations. In PKS 2155 - 304, spectral energy distribution from optical to X-ray is fitted with LPPL (log parabolic + power law) model. In BL Lacertae, optical flux and degree of polarization were anti-correlated.

  9. Spatiotemporal focusing dynamics in plasmas at X-ray wavelength

    SciTech Connect (OSTI)

    Sharma, A., E-mail: a-physics2001@yahoo.com; Tibai, Z. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary)] [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Hebling, J. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary) [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Szentagothai Research Centre, University of Pecs, Pecs-7624 (Hungary); Mishra, S. K. [Institute for Plasma Research, Gandhinagar (India)] [Institute for Plasma Research, Gandhinagar (India)

    2014-03-15

    Using a finite curvature beam, we investigate here the spatiotemporal focusing dynamics of a laser pulse in plasmas at X-ray wavelength. We trace the dependence of curvature parameter on the focusing of laser pulse and recognize that the self-focusing in plasma is more intense for the X-ray laser pulse with curved wavefront than with flat wavefront. The simulation results demonstrate that spatiotemporal focusing dynamics in plasmas can be controlled with the appropriate choice of beam-plasma parameters to explore the high intensity effects in X-ray regime.

  10. Laser-Produced Coherent X-Ray Sources

    SciTech Connect (OSTI)

    Donald Umstadter

    2007-01-31

    We study the generation of x-rays from the interaction of relativistic electrons with ultra-intense laser pulse either directly or via laser generated ion channels. The laser pulse acts as the accelerator and wiggler leading to an all-optical synchrotron-like x-ray source. The mm sized accelerator and micron-sized wiggler leads to a compact source of high brightness, ultrafast x-rays with applications in relativistic nonlinear optics, ultrafast chemistry, biology, inner-shell electronic processes and phase transitions.

  11. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorkingLos Alamos verifies largest single goldWind Power >X-RayX-RayX-Ray

  12. Radiation exposure in X-ray-based imaging techniques used in osteoporosis

    E-Print Network [OSTI]

    Damilakis, John; Adams, Judith E.; Guglielmi, Giuseppe; Link, Thomas M.

    2010-01-01

    and nonradiologists in dual-energy X-ray absorptiometrymorphometry studies using dual-energy X-ray absorptiometry.dose measurements in dual energy X-ray absorptiometry (DXA).

  13. X-ray optics metrology limited by random noise, instrumental drifts, and systematic errors

    E-Print Network [OSTI]

    Yashchuk, Valeriy V.

    2010-01-01

    X-ray optics metrology limited by random noise, instrumentalUSA Center for X-ray Optics, Lawrence Berkeley Nationaland reflecting x-ray optics suitable for micro- and nano-

  14. Beyond 3-D X-ray Imaging: Methodology Development and Applications...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    to the availability of the new generation of X-ray sources and the advanced X-ray optics. The advanced X-ray Optics along with novel methodology has made it possible to...

  15. Automated suppression of errors in LTP-II slope measurements with x-ray optics

    E-Print Network [OSTI]

    Ali, Zulfiqar

    2011-01-01

    slope measurements with x-ray optics Zulfiqar Ali, Curtis L.with state-of-the-art x-ray optics. Significant suppressionscanning, metrology of x-ray optics, deflectometry Abstract

  16. Synchrotron X-ray Scattering Studies of Rapidly Evolving Nanoscale Interfacial Systems /

    E-Print Network [OSTI]

    Dai, Yeling

    2013-01-01

    Stanley. X-ray and neutron scattering from rough surfaces.Stanley. X-ray and neutron scattering from rough surfaces.grazing incidence x-ray and neutron scattering from ordered

  17. Imaging nanoscale magnetic structures with polarized soft x-ray photons

    E-Print Network [OSTI]

    Fischer, P.

    2010-01-01

    with polarized soft X-ray photons Peter Fischer and Mi -polarized soft X-ray photons which provide a strong X-rayhigh intense soft X-ray photon pulses hold the promise of

  18. A New Scheme for Stigmatic X-ray Imaging with Large Magnification...

    Office of Scientific and Technical Information (OSTI)

    F; Beiersdorfer, P; Wang, E; Sanchez del Rio, M; Caughey, T A 70 PLASMA PHYSICS AND FUSION TECHNOLOGY X-ray Imaging X-ray Imaging This paper describes a new x-ray scheme for...

  19. Spectral softening in the X-RAY afterglow of GRB 130925A as predicted by the dust scattering model

    SciTech Connect (OSTI)

    Zhao, Yi-Nan; Shao, Lang, E-mail: lshao@hebtu.edu.cn [Department of Space Science and Astronomy, Hebei Normal University, Shijiazhuang 050024 (China)

    2014-07-01

    Gamma-ray bursts (GRBs) usually occur in a dense star-forming region with a massive circumburst medium. The small-angle scattering of intense prompt X-ray emission off the surrounding dust grains will have observable consequences and sometimes can dominate the X-ray afterglow. In most of the previous studies, only the Rayleigh-Gans (RG) approximation is employed for describing the scattering process, which works accurately for the typical size of grains (with radius of a ? 0.1 ?m) in the diffuse interstellar medium. When the size of the grains may significantly increase, as in a more dense region where GRBs would occur, the RG approximation may not be valid enough for modeling detailed observational data. In order to study the temporal and spectral properties of the scattered X-ray emission more accurately with potentially larger dust grains, we provide a practical approach using the series expansions of anomalous diffraction (AD) approximation based on the complicated Mie theory. We apply our calculations to understand the puzzling X-ray afterglow of recently observed GRB 130925A that showed a significant spectral softening. We find that the X-ray scattering scenarios with either AD or RG approximation adopted could well reproduce both the temporal and spectral profile simultaneously. Given the plateau present in the early X-ray light curve, a typical distribution of smaller grains as in the interstellar medium would be suggested for GRB 130925A.

  20. On the Lack of Type I X-ray Bursts in Black Hole X-ray Binaries: Evidence for the Event Horizon?

    E-Print Network [OSTI]

    Ramesh Narayan; Jeremy S. Heyl

    2002-06-28

    Type I X-ray bursts are very common in neutron star X-ray binaries, but no Type I burst has been seen in the dozen or so binaries in which the accreting compact star is too massive to be a neutron star and therefore is identified as a black hole candidate. We have carried out a global linear stability analysis of the accumulating fuel on the surface of a compact star to identify the conditions under which thermonuclear bursts are triggered. Our analysis, which improves on previous calculations, reproduces the gross observational trends of bursts in neutron star systems. It further shows that, if black hole candidates have surfaces, they would very likely exhibit instabilities similar to those that lead to Type I bursts on neutron stars. The lack of bursts in black hole candidates is thus significant, and indicates that these objects have event horizons. We discuss possible caveats to this conclusion.

  1. Combining X-ray Absorption and X-ray Diffraction Techniques for in Situ Studies of Chemical Transformations in Heterogeneous Catalysis: Advantages and Limitations

    SciTech Connect (OSTI)

    Frenkel, A.I.; Hanson, J.; Wang, Q.; Marinkovic, N.; Chen, J.G.; Barrio, L.; Si, R.; Lopez Camara, A.; Estrella, A.M.; Rodriguez, J.A.

    2011-08-05

    Recent advances in catalysis instrumentations include synchrotron-based facilities where time-resolved X-ray scattering and absorption techniques are combined in the same in situ or operando experiment to study catalysts at work. To evaluate the advances and limitations of this method, we performed a series of experiments at the new XAFS/XRD instrument in the National Synchrotron Light Source. Nearly simultaneous X-ray diffraction (XRD) and X-ray absorption fine-structure (XAFS) measurements of structure and kinetics of several catalysts under reducing or oxidizing conditions have been performed and carefully analyzed. For CuFe{sub 2}O{sub 4} under reducing conditions, the combined use of the two techniques allowed us to obtain accurate data on kinetics of nucleation and growth of metallic Cu. For the inverse catalyst CuO/CeO{sub 2} that underwent isothermal reduction (with CO) and oxidation (with O{sub 2}), the XAFS data measured in the same experiment with XRD revealed strongly disordered Cu species that went undetected by diffraction. These and other examples emphasize the unique sensitivity of these two complementary methods to follow catalytic processes in the broad ranges of length and time scales.

  2. Combining X-ray Absorption and X-ray Diffraction Techniques for in Situ Studies of Chemical Transformations in Heterogeneous Catalysis:Advantages and Limitations

    SciTech Connect (OSTI)

    A Frenkel; Q Wang; N Marinkovic; J Chen; L Barrio; R Si; A Lopez Camara; A Estella; J Rodriquez; J Hanson

    2011-12-31

    Recent advances in catalysis instrumentations include synchrotron-based facilities where time-resolved X-ray scattering and absorption techniques are combined in the same in situ or operando experiment to study catalysts at work. To evaluate the advances and limitations of this method, we performed a series of experiments at the new XAFS/XRD instrument in the National Synchrotron Light Source. Nearly simultaneous X-ray diffraction (XRD) and X-ray absorption fine-structure (XAFS) measurements of structure and kinetics of several catalysts under reducing or oxidizing conditions have been performed and carefully analyzed. For CuFe{sub 2}O{sub 4} under reducing conditions, the combined use of the two techniques allowed us to obtain accurate data on kinetics of nucleation and growth of metallic Cu. For the inverse catalyst CuO/CeO{sub 2} that underwent isothermal reduction (with CO) and oxidation (with O{sub 2}), the XAFS data measured in the same experiment with XRD revealed strongly disordered Cu species that went undetected by diffraction. These and other examples emphasize the unique sensitivity of these two complementary methods to follow catalytic processes in the broad ranges of length and time scales.

  3. Achieving hard X-ray nanofocusing using a wedged multilayer Laue...

    Office of Scientific and Technical Information (OSTI)

    anticipate that continuous development on wedged MLLs will advance x-ray nanofocusing optics to new frontiers and enrich capabilities and opportunities for hard X-ray microscopy....

  4. Luminosity function of binary X-ray sources calculated using the Scenario Machine

    E-Print Network [OSTI]

    A. I. Bogomazov; V. M. Lipunov

    2007-05-20

    Using the ``Scenario Machine'' we have carried out a population synthesis of X-ray binaries for the purpose of modelling of X-ray luminosity functions (XLFs) in different types of galaxies: star burst, spiral, and elliptical. This computer code allows to calculate, by using Monte Carlo simulations, the evolution of a large ensemble of binary systems, with proper accounting for the spin evolution of magnetized neutron stars. We show that the XLF has no universal type. It depends on the star formation rate in the galaxy. Also it is of importance to take into account the evolution of binary systems and life times of X-ray stages in theoretical models of such functions. We have calculated cumulative and differential XLFs for the galaxy with the constant star formation rate. Also we have calculated cumulative luminosity functions for different intervals of time after the star formation burst in the galaxy and curves depicting the evolution of the X-ray luminosity after the star formation burst in the galaxy.

  5. X-ray and radio emission from Type In supernova SN 2010jl

    E-Print Network [OSTI]

    Chandra, Poonam; Chugai, Nikolai; Fransson, Claes; Soderberg, Alicia M

    2015-01-01

    We present all X-ray and radio observations of the Type IIn supernova SN 2010jl. The X-ray observations cover a period up to day 1500 with Chandra, XMM-Newton, NuSTAR and Swift-XRT. The Chandra observations after 2012 June, the XMM-Newton observation in 2013 November, and most of the Swift-XRT observations until 2014 December are presented for the first time. All the spectra can be fitted by an absorbed hot thermal model except for \\chandra spectra on 2011 October and 2012 June when an additional component is needed. Although the origin of this component is uncertain, it is spatially coincident with the supernova and occurs when there are changes to the supernova spectrum in the energy range close to that of the extra component, indicating that the emission is related to the supernova. The X-ray light curve shows an initial plateau followed by a steep drop starting at day $\\sim 300$. We attribute the drop to a decrease in the circumstellar density. The column density to the X-ray emission drops rapidly with t...

  6. Development of high-repetition-rate laser pump/x-ray probe methodologies for synchrotron facilities

    SciTech Connect (OSTI)

    March, Anne Marie; Doumy, Gilles; Kanter, Elliot P.; Kraessig, Bertold; Southworth, Stephen H.; Attenkofer, Klaus; Kurtz, Charles A.; Young, Linda [X-ray Science Division, Advanced Photon Source, Argonne National Laboratory, 9700 S. Cass Ave., Argonne, Illinois 60439 (United States); Stickrath, Andrew [Chemical Sciences and Engineering Division, Argonne National Laboratory, 9700 S. Cass Ave., Argonne, Illinois 60439 (United States); Chen, Lin X. [Chemical Sciences and Engineering Division, Argonne National Laboratory, 9700 S. Cass Ave., Argonne, Illinois 60439 (United States); Department of Chemistry, Northwestern University, 2145 Sheridan Road, Evanston, Illinois 60208 (United States)

    2011-07-15

    We describe our implementation of a high repetition rate (54 kHz-6.5 MHz), high power (>10 W), laser system at the 7ID beamline at the Advanced Photon Source for laser pump/x-ray probe studies of optically driven molecular processes. Laser pulses at 1.06 {mu}m wavelength and variable duration (10 or 130 ps) are synchronized to the storage ring rf signal to a precision of {approx}250 fs rms. Frequency doubling and tripling of the laser radiation using nonlinear optical techniques have been applied to generate 532 and 355 nm light. We demonstrate that by combining a microfocused x-ray probe with focused optical laser radiation the requisite fluence (with <10 {mu}J/pulse) for efficient optical excitation can be readily achieved with a compact and commercial laser system at megahertz repetition rates. We present results showing the time-evolution of near-edge x-ray spectra of a well-studied, laser-excited metalloporphyrin, Ni(II)-tetramesitylporphyrin. The use of high repetition rate, short pulse lasers as pump sources will dramatically enhance the duty cycle and efficiency in data acquisition and hence capabilities for laser-pump/x-ray probe studies of ultrafast structural dynamics at synchrotron sources.

  7. X-ray Burst Oscillations: From Flame Spreading to the Cooling Wake

    E-Print Network [OSTI]

    Simin Mahmoodifar; Tod Strohmayer

    2015-10-16

    Type I X-ray bursts are thermonuclear flashes observed from the surface of accreting neutron stars in Low Mass X-ray Binaries. Oscillations have been observed during the rise and/or decay of some of these X-ray bursts. Those seen during the rise can be well explained by a spreading hot spot model, but to date there haven't been any quantitative studies that consistently track the oscillation amplitude both during the rise and decay (tail) of bursts. Here we compute the light curves and amplitudes of oscillations in X-ray burst models that realistically account for both flame spreading and subsequent cooling. We present results for two such "cooling wake" models, a "canonical" cooling model where each patch on the neutron star surface heats and cools identically, and an "asymmetric" model where parts of the star cool at different rates. We show that while canonical cooling models can generate oscillations in the tails of bursts, they cannot easily produce the highest observed modulation amplitudes. Alternatively, a simple model with asymmetric cooling can achieve higher amplitudes consistent with the observations.

  8. X-Ray Emitting Blast Wave from the Recurrent Nova RS Ophiuchi

    E-Print Network [OSTI]

    J. L. Sokoloski; G. J. M. Luna; K. Mukai; Scott J. Kenyon

    2006-05-30

    Stellar explosions such as novae and supernovae produce most of the heavy elements in the Universe. Although the onset of novae from runaway thermonuclear fusion reactions on the surface of a white dwarf in a binary star system is understood[1], the structure, dynamics, and mass of the ejecta are not well known. In rare cases, the white dwarf is embedded in the wind nebula of a red-giant companion; the explosion products plow through the nebula and produce X-ray emission. Early this year, an eruption of the recurrent nova RS Ophiuchi[2,3] provided the first opportunity to perform comprehensive X-ray observations of such an event and diagnose conditions within the ejecta. Here we show that the hard X-ray emission from RS Ophiuchi early in the eruption emanates from behind a blast wave, or outward-moving shock wave, that expanded freely for less than 2 days and then decelerated due to interaction with the nebula. The X-rays faded rapidly, suggesting that the blast wave deviates from the standard spherical shell structure[4-6]. The early onset of deceleration indicates that the ejected shell had a low mass, the white dwarf has a high mass[7], and that RS Ophiuchi is a progenitor of the type of supernova integral to studies of the expansion of the universe.

  9. X-ray Thomson scattering measurements of temperature and density from multi-shocked CH capsules

    SciTech Connect (OSTI)

    Fletcher, L. B. [Department of Physics, University of California, Berkeley, California 94720 (United States)] [Department of Physics, University of California, Berkeley, California 94720 (United States); Kritcher, A.; Pak, A.; Ma, T.; Döppner, T.; Divol, L.; Landen, O. L.; Glenzer, S. H. [Lawrence Livermore National Laboratory, 7000 East Av., Livermore, California 94550 (United States)] [Lawrence Livermore National Laboratory, 7000 East Av., Livermore, California 94550 (United States); Fortmann, C. [Lawrence Livermore National Laboratory, 7000 East Av., Livermore, California 94550 (United States) [Lawrence Livermore National Laboratory, 7000 East Av., Livermore, California 94550 (United States); University of California, Los Angeles, California 90095 (United States); Vorberger, J.; Gericke, D. O. [Department of Physics, Centre for Fusion, Space, and Astrophysics, University of Warwick, Coventry CV4 7AL (United Kingdom)] [Department of Physics, Centre for Fusion, Space, and Astrophysics, University of Warwick, Coventry CV4 7AL (United Kingdom); Chapman, D. A. [Department of Physics, Centre for Fusion, Space, and Astrophysics, University of Warwick, Coventry CV4 7AL (United Kingdom) [Department of Physics, Centre for Fusion, Space, and Astrophysics, University of Warwick, Coventry CV4 7AL (United Kingdom); Plasma Physics Department, AWE plc, Aldermaston (United Kingdom); Falcone, R. W. [Department of Physics, University of California, Berkeley, California 94720 (United States) [Department of Physics, University of California, Berkeley, California 94720 (United States); Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States)

    2013-05-15

    Proof-of-principle measurements of the electron densities, temperatures, and ionization states of spherically compressed multi-shocked CH (polystyrene) capsules have been achieved using spectrally resolved x-ray Thomson scattering. A total energy of 13.5 kJ incident on target is used to compress a 70 ?m thick CH shell above solid-mass density using three coalescing shocks. Separately, a laser-produced zinc He-? x-ray source at 9 keV delayed 200 ps-800 ps after maximum compression is used to probe the plasma in the non-collective scattering regime. The data show that x-ray Thomson scattering enables a complete description of the time-dependent hydrodynamic evolution of shock-compressed CH capsules, with a maximum measured density of ? > 6 g cm{sup ?3}. In addition, the results demonstrate that accurate measurements of x-ray scattering from bound-free transitions in the CH plasma demonstrate strong evidence that continuum lowering is the primary ionization mechanism of carbon L-shell electrons.

  10. Suzaku Spectroscopy of the Extended X-Ray Emission in M17

    E-Print Network [OSTI]

    Yoshiaki Hyodo; Masahiro Tsujimoto; Kenji Hamaguchi; Katsuji Koyama; Shunji Kitamoto; Yoshitomo Maeda; Yohko Tsuboi; Yuichiro Ezoe

    2007-07-27

    We present the results of a Suzaku spectroscopic study of the soft extended X-ray emission in the HII region M17. The spectrum of the extended emission was obtained with a high signal-to-noise ratio in a spatially-resolved manner using the X-ray Imaging Spectrometer (XIS). We established that the contamination by unresolved point sources, the Galactic Ridge X-ray emission, the cosmic X-ray background, and the local hot bubble emission is negligible in the background-subtracted XIS spectrum of the diffuse emission. Half a dozen of emission lines were resolved clearly for the first time, including K lines of highly ionized O, Ne, and Mg as well as L series complex of Fe at 0.5--1.5 keV. Based on the diagnosis of these lines, we obtained the following results: (1) the extended emission is an optically-thin thermal plasma represented well by a single temperature of 3.0 +/- 0.4 MK, (2) the abundances of elements with emission lines in the diffuse spectrum are 0.1--0.3 solar, while those of bright discrete sources are 0.3--1.5 solar, (3) the metal abundances relative to each other in the diffuse emission are consistent with solar except for a Ne enhancement of a factor of 2, (4) both the plasma temperature and the chemical composition of the diffuse emission show no spatial variation across the studied spatial scale of about 5 pc.

  11. Phase Tomography Using X-ray Talbot Interferometer

    SciTech Connect (OSTI)

    Momose, A.; Yashiro, W.; Moritake, M. [Graduate School of Frontier Sciences, University of Tokyo, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan); Takeda, Y. [Graduate School of Pure and Applied Sciences, University of Tsukuba, 1-1-1 Tennodai, Tsukuba, Ibaraki 305-8573 (Japan); Uesugi, K.; Suzuki, Y. [SPring-8/JASRI, 1-1-1 Kouto, Mikazuki, Hyogo 679-5198 (Japan); Hattori, T. [Laboratory of Advanced Science and Technology for Industry, University of Hyogo, 3-1-2 Kouto, Kamigori, Hyogo 678-1205 (Japan)

    2007-01-19

    A biological tomography result obtained with an X-ray Talbot interferometer is reported. An X-ray Talbot interferometer was constructed using an amplitude grating fabricated by X-ray lithography at the LIGA beamline of NewSUBARU and gold electroplating. The pitch and pattern thickness of the grating were 8 {mu}m and 30 {mu}m, respectively. The effective area was 20 x 20 mm2, which was entirely illuminated with a wide beam available at the medium-length beamline 20B2 of SPring-8, allowing the acquisition of a three-dimensional tomogram of almost the whole body of a fish. The resulting image obtained with 17.7 keV X-rays revealed organs with bones in the same view.

  12. Performance enhancement approaches for a dual energy x-ray

    E-Print Network [OSTI]

    Fu, Kenneth

    2010-01-01

    Evans, J.P.O. , “Stereoscopic dual energy imaging for targetCrawford, C.R. , “Dual Energy Volumetric X-ray Tomographicimages in 4–10 MeV Dual- energy customs system for material

  13. X-ray emission from the terrestrial magnetosheath

    E-Print Network [OSTI]

    Robertson, Ina Picket; Cravens, Thomas Edward

    2003-04-29

    [1] X-rays are generated throughout the terrestrial magnetosheath as a consequence of charge transfer collisions between heavy solar wind ions and geocoronal neutrals. The solar wind ions resulting from these collisions are left in highly excited...

  14. Active pixel sensors for X-ray astronomy

    E-Print Network [OSTI]

    Cohen, Matthew (Matthew L.)

    2005-01-01

    An active pixel sensor array, APS-1, has been fabricated for the purpose of scientific x-ray detection. This thesis presents the results of testing the device. Alternate design architectures are explored. Recommendations ...

  15. Accreting X-ray millisecond pulsars observed with INTEGRAL

    E-Print Network [OSTI]

    Maurizio Falanga

    2007-11-07

    I review the properties of three X-ray accreting millisecond pulsars observed with INTEGRAL. Out of seven recently discovered accretion-powered pulsars (one discovered by INTEGRAL), three were observed with the INTEGRAL satellite up to 300 keV. Detailed timing and spectral results will be presented, including data obtained during the most recent outburst of the pulsar HETE J1900.1-2455. Accreting X-ray millisecond pulsars are key systems to understand the spin and accretion history of neutron stars. They are also a good laboratory in which to study the source spectra, pulse profile, and phase shift between X-ray pulses in different energy ranges which give additional information of the X-ray production processes and emission environment.

  16. Magnetically Confined Wind Shocks in X-rays - a Review

    E-Print Network [OSTI]

    ud-Doula, Asif

    2015-01-01

    A subset (~ 10%) of massive stars present strong, globally ordered (mostly dipolar) magnetic fields. The trapping and channeling of their stellar winds in closed magnetic loops leads to magnetically confined wind shocks (MCWS), with pre-shock flow speeds that are some fraction of the wind terminal speed. These shocks generate hot plasma, a source of X-rays. In the last decade, several developments took place, notably the determination of the hot plasma properties for a large sample of objects using XMM-Newton and Chandra, as well as fully self-consistent MHD modelling and the identification of shock retreat effects in weak winds. Despite a few exceptions, the combination of magnetic confinement, shock retreat and rotation effects seems to be able to account for X-ray emission in massive OB stars. Here we review these new observational and theoretical aspects of this X-ray emission and envisage some perspectives for the next generation of X-ray observatories.

  17. X-ray obscuration in local Universe AGN

    E-Print Network [OSTI]

    Matteo Guainazzi

    2006-10-31

    I review the constraints that X-ray observations impose on the physical properties and the geometrical distribution of cold absorbing gas in nearby obscured Active Galactic Nuclei (AGN), as well as their implications for AGN structure models.

  18. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    interpretation of XMLD data. Magnetism and X Rays The ancient Greeks and also the Chinese knew about strange and rare stones with the power to attract iron. Moreover, when...

  19. The Ulysses Catalog of Solar Hard X-Ray Flares

    E-Print Network [OSTI]

    Tranquille, C.; Hurley, K.; Hudson, H. S.

    2009-01-01

    Sturrock, P.A. (ed. ) Solar Flares: A Monograph from SkylabSmith E.V.P. : 1963, Solar Flares, Macmillan, New York.Catalog of Solar Hard X-Ray Flares Table 1 (Continued. )

  20. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the...

  1. X-Ray Propagation in Tapered Waveguides: Simulation and Optimization

    E-Print Network [OSTI]

    Peinke, Joachim

    [1,2]. X-ray waveguides (WG) have been designed and fabricated as planar layered systems (1D-WG) [3. The propagation in the stuctures is studied by numerical solution of the parabolic wave equation (PWE), as used

  2. Generation of Coherent X-Ray Radiation through Modulation Compression...

    Office of Scientific and Technical Information (OSTI)

    In this paper, we propose a scheme to generate tunable coherent X-ray radiation for future light source applications. This scheme uses an energy chirped electron beam, a laser...

  3. Towards attosecond X-ray pulses from the FEL

    E-Print Network [OSTI]

    Zholents, Alexander A.; Fawley, William M.

    2004-01-01

    can be used instead of HC FEL. In the following illustra-UM is now tuned for resonant FEL interaction with the 32-nmAttosecond X-Ray Pulses from the FEL Alexander A. Zholents,

  4. Vitreous carbon mask substrate for X-ray lithography

    DOE Patents [OSTI]

    Aigeldinger, Georg (Livermore, CA); Skala, Dawn M. (Fremont, CA); Griffiths, Stewart K. (Livermore, CA); Talin, Albert Alec (Livermore, CA); Losey, Matthew W. (Livermore, CA); Yang, Chu-Yeu Peter (Dublin, CA)

    2009-10-27

    The present invention is directed to the use of vitreous carbon as a substrate material for providing masks for X-ray lithography. The new substrate also enables a small thickness of the mask absorber used to pattern the resist, and this enables improved mask accuracy. An alternative embodiment comprised the use of vitreous carbon as a LIGA substrate wherein the VC wafer blank is etched in a reactive ion plasma after which an X-ray resist is bonded. This surface treatment provides a surface enabling good adhesion of the X-ray photoresist and subsequent nucleation and adhesion of the electrodeposited metal for LIGA mold-making while the VC substrate practically eliminates secondary radiation effects that lead to delamination of the X-ray resist form the substrate, the loss of isolated resist features, and the formation of a resist layer adjacent to the substrate that is insoluble in the developer.

  5. High order reflectivity of graphite (HOPG) crystals for x ray...

    Office of Scientific and Technical Information (OSTI)

    (22.1 keV) x-rays, produced by petawatt class laser pulses interacting with a Kr gas jet and a silver foil, to measure the integrated crystal reflectivity of flat Highly...

  6. X-ray imaging reveals secrets in battery materials | Argonne...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-ray imaging reveals secrets in battery materials June 22, 2015 Tweet EmailPrint Imaging and data analysis techniques offer new approach to probing material properties In a new...

  7. Monochromatic wavelength dispersive x-ray fluorescence providing sensitive and selective detection of uranium

    SciTech Connect (OSTI)

    Havrilla, George J [Los Alamos National Laboratory; Collins, Michael L [Los Alamos National Laboratory; Montoya, Velma M [Los Alamos National Laboratory; Chen, Zewu [XOS; Wei, Fuzhong [XOS

    2010-01-01

    Monochromatic wavelength dispersive X-ray fluorescence (MWDXRF) is a sensitive and selective method for elemental compositional analyses. The basis for this instrumental advance is the doubly curved crystal (DCC) optic. Previous work has demonstrated the feasibility of sensitive trace element detection for yttrium as a surrogate for curium in aqueous solutions. Additional measurements have demonstrated similar sensitivity in several different matrix environments which attests to the selectivity of the DCC optic as well as the capabilities of the MWDXRF concept. The objective of this effort is to develop an improved Pu characterization method for nuclear fuel reprocessing plants. The MWDXRF prototype instrument is the second step in a multi-year effort to achieve an improved Pu assay. This work will describe a prototype MWDXRF instrument designed for uranium detection and characterization. The prototype consists of an X-ray tube with a rhodium anode and a DCC excitation optic incorporated into the source. The DCC optic passes the RhK{alpha} line at 20.214 keV for monochromatic excitation of the sample. The source is capable of 50 W power at 50 kV and 1.0 mA operation. The x-ray emission from the sample is collected by a DCC optic set at the UL{alpha} line of 13.613 keV. The collection optic transmits the UL{alpha} x-rays to the silicon drift detector. The x-ray source, sample, collection optic and detector are all mounted on motion controlled stages for the critical alignment of these components. The sensitivity and selectivity of the instrument is obtained through the monochromatic excitation and the monochromatic detection. The prototype instrument performance has a demonstrated for sensitivity for uranium detection of around 2 ppm at the current state of development. Further improvement in sensitivity is expected with more detailed alignment.

  8. Novel opportunities for sub-meV inelastic X-ray scattering at high-repetition rate self-seeded X-ray free-electron lasers

    E-Print Network [OSTI]

    Chubar, Oleg; Kocharyan, Vitali; Madsen, Anders; Saldin, Evgeni; Serkez, Svitozar; Shvyd'ko, Yuri; Sutter, John

    2015-01-01

    Inelastic X-ray scattering (IXS) is an important tool for studies of equilibrium dynamics in condensed matter. A new spectrometer recently proposed for ultra-high-resolution IXS (UHRIX) has achieved 0.6~meV and 0.25~nm$^{-1}$ spectral and momentum transfer resolutions, respectively. However, further improvements down to 0.1~meV and 0.02~nm$^{-1}$ are required to close the gap in energy-momentum space between high and low frequency probes. We show that this goal can be achieved by further optimizing the X-ray optics and by increasing the spectral flux of the incident X-ray pulses. UHRIX performs best at energies from 5 to 10 keV, where a combination of self-seeding and undulator tapering at the SASE-2 beamline of the European XFEL promises up to a hundred-fold increase in average spectral flux compared with nominal SASE pulses at saturation, or three orders of magnitude more than possible with storage-ring based radiation sources. Wave-optics propagation shows that about $7\\times 10^{12}$~ph/s in a $90$-$\\mu$e...

  9. High-pressure X-ray diffraction and X-ray emission studies on iron-bearing silicate perovskite under high pressures

    SciTech Connect (OSTI)

    Lin, Jung-Fu; Speciale, Sergio; Prakapenka, Vitali B.; Dera, Przemek; Lavina, Babara; Watson, Heather C.

    2010-06-22

    Iron-bearing silicate perovskite is believed to be the most abundant mineral of the Earth's lower mantle. Recent studies have shown that Fe{sup 2+} exists predominantly in the intermediate-spin state with a total spin number of 1 in silicate perovskite in the lower part of the lower mantle. Here we have measured the spin states of iron and the pressure-volume relation in silicate perovskite [(Mg{sub 0.6},Fe{sub 0.4})SiO{sub 3}] at pressure conditions relevant to the lowermost mantle using in situ X-ray emission and X-ray diffraction in a diamond cell. Our results showed that the intermediate-spin Fe{sup 2+} is stable in the silicate perovskite up to {approx} 125 GPa but starts to transition to the low-spin state at approximately 135 GPa. Concurrent X-ray diffraction measurements showed a decrease of approximately 1% in the unit cell volume in the silicate perovskite [(Mg{sub 0.6},Fe{sub 0.4})SiO{sub 3}], which is attributed to the intermediate-spin to the low-spin transition. The transition pressure coincides with the pressure conditions of the lowermost mantle, raising the possibility of the existence of the silicate perovskite phase with the low-spin Fe{sup 2+} across the transition from the post-perovskite to the perovskite phases in the bottom of the D{double_prime} layer.

  10. Probing Martensitic Transition in Nitinol Wire: A Comparison of X-ray Diffraction and Other Techniques

    SciTech Connect (OSTI)

    Butler, J.; Tiernan, P.; Tofail, S. A. M.; Ghandi, A. A. [Materials and Surface Science Institute, University of Limerick, Limerick (Ireland)

    2011-01-17

    Martensitic to austenite transformation in Nitinol wire can be measured by a number of techniques such as XRD (X-Ray Diffraction), DSC (Differential Scanning Calorimetry), BFR (Bend and Free Recovery) and Vickers indentation recovery. A comparison of results from these varied characterisation techniques is reported here to obtain a greater understanding of the thermal-elastic-structural changes associated with martensitic transformation. The transformation temperatures measured by DSC were found to correspond well with the structural and mechanical information obtained from XRD, BFR and Vickers indent recovery methods. Indent recovery is a relatively new and accurate method of monitoring stress induced martensitic transformations in NiTi and is one of only a few methods of stress inducing martensitic transformation in large scale samples. It is especially useful for NiTi in the as-cast billet form, where tensile testing is impossible. BFR is uniquely popular in the NiTi wire manufacturing sector and is recognised as the most accurate method of measuring the transformation temperature. Here the material is stressed to a representative in-service stress level during the test. No other test uses the shape memory effect for measuring the transformation temperature of NiTi. The results show that the DSC thermogram and XRD diffractogram have a peak overlap which is a common occurrence in NiTi that has been extensively processed. The XRD method further explains the observations in the DSC thermogram and in combination they confirm the transformation temperature.

  11. X-ray tube with magnetic electron steering

    DOE Patents [OSTI]

    Reed, Kim W. (Albuquerque, NM); Turman, Bobby N. (Albuquerque, NM); Kaye, Ronald J. (Albuquerque, NM); Schneider, Larry X. (Albuquerque, NM)

    2000-01-01

    An X-ray tube uses a magnetic field to steer electrons. The magnetic field urges electrons toward the anode, increasing the proportion of electrons emitted from the cathode that reach desired portions of the anode and consequently contribute to X-ray production. The magnetic field also urges electrons reflected from the anode back to the anode, further increasing the efficiency of the tube.

  12. New Directions in X-Ray Light Sources

    ScienceCinema (OSTI)

    Falcone, Roger

    2010-01-08

    July 15, 2008 Berkeley Lab lecture: Molecular movies of chemical reactions and material phase transformations need a strobe of x-rays, the penetrating light that reveals how atoms and molecules assemble in chemical and biological systems and complex materials. Roger Falcone, Director of the Advanced Light Source,will discuss a new generation of x ray sources that will enable a new science of atomic dynamics on ultrafast timescales.

  13. New focusing multilayer structures for X-ray plasma spectroscopy

    SciTech Connect (OSTI)

    Bibishkin, M S; Luchin, V I; Salashchenko, N N; Chernov, V V; Chkhalo, N I; Kazakov, E D; Shevelko, A P

    2008-02-28

    New focusing short-period multilayer structures are developed which opens up wide possibilities for X-ray and VUV spectroscopy. Multilayer structures are deposited on a flat surface of a mica crystal which is then bent to a small-radius cylinder. The use of this structure in a von Hamos spectrometer for X-ray laser plasma diagnostics is demonstrated. (interaction of laser radiation with matter. laser plasma)

  14. Evaluation of partial coherence correction in X-ray ptychography

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Burdet, Nicolas; Shi, Xiaowen; Parks, Daniel; Clark, Jesse N.; Huang, Xiaojing; Kevan, Stephen D.; Robinson, Ian K.

    2015-02-23

    Coherent X-ray Diffraction Imaging (CDI) and X-ray ptychography both heavily rely on the high degree of spatial coherence of the X-ray illumination for sufficient experimental data quality for reconstruction convergence. Nevertheless, the majority of the available synchrotron undulator sources have a limited degree of partial coherence, leading to reduced data quality and a lower speckle contrast in the coherent diffraction patterns. It is still an open question whether experimentalists should compromise the coherence properties of an X-ray source in exchange for a higher flux density at a sample, especially when some materials of scientific interest are relatively weak scatterers. Amore »previous study has suggested that in CDI, the best strategy for the study of strong phase objects is to maintain a high degree of coherence of the illuminating X-rays because of the broadening of solution space resulting from the strong phase structures. In this article, we demonstrate the first systematic analysis of the effectiveness of partial coherence correction in ptychography as a function of the coherence properties, degree of complexity of illumination (degree of phase diversity of the probe) and sample phase complexity. We have also performed analysis of how well ptychographic algorithms refine X-ray probe and complex coherence functions when those variables are unknown at the start of reconstructions, for noise-free simulated data, in the case of both real-valued and highly-complex objects.« less

  15. A short working distance multiple crystal x-ray spectrometer

    SciTech Connect (OSTI)

    Dickinson, B.; Seidler, G. T.; Webb, Z. W.; Bradley, J. A.; Nagle, K. P. [Department of Physics, University of Washington, Seattle, Washington 98195 (United States); Heald, S. M. [Advanced Photon Source, Argonne National Laboratories, Argonne, Illinois 60439 (United States); Gordon, R. A. [Department of Physics, Simon Fraser University, Burnaby, British Columbia V5A 1S6 (Canada); Chou, I. M. [U.S. Geological Survey, Reston, Virginia 20192 (United States)

    2008-12-15

    For x-ray spot sizes of a few tens of microns or smaller, a millimeter-sized flat analyzer crystal placed {approx}1 cm from the sample will exhibit high energy resolution while subtending a collection solid angle comparable to that of a typical spherically bent crystal analyzer (SBCA) at much larger working distances. Based on this observation and a nonfocusing geometry for the analyzer optic, we have constructed and tested a short working distance (SWD) multicrystal x-ray spectrometer. This prototype instrument has a maximum effective collection solid angle of 0.14 sr, comparable to that of 17 SBCA at 1 m working distance. We find good agreement with prior work for measurements of the Mn K{beta} x-ray emission and resonant inelastic x-ray scattering for MnO, and also for measurements of the x-ray absorption near-edge structure for Dy metal using L{alpha}{sub 2} partial-fluorescence yield detection. We discuss future applications at third- and fourth-generation light sources. For concentrated samples, the extremely large collection angle of SWD spectrometers will permit collection of high-resolution x-ray emission spectra with a single pulse of the Linac Coherent Light Source. The range of applications of SWD spectrometers and traditional multi-SBCA instruments has some overlap, but also is significantly complementary.

  16. The ASTRO-H X-ray Observatory

    E-Print Network [OSTI]

    Takahashi, Tadayuki; Kelley, Richard; Aharonian, Henri AartsFelix; Akamatsu, Hiroki; Akimoto, Fumie; Allen, Steve; Anabuki, Naohisa; Angelini, Lorella; Arnaud, Keith; Asai, Makoto; Audard, Marc; Awaki, Hisamitsu; Azzarello, Philipp; Baluta, Chris; Bamba, Aya; Bando, Nobutaka; Bautz, Mark; Blandford, Roger; Boyce, Kevin; Brown, Greg; Cackett, Ed; Chernyakova, Maria; Coppi, Paolo; Costantini, Elisa; de Plaa, Jelle; Herder, Jan-Willem den; DiPirro, Michael; Done, Chris; Dotani, Tadayasu; Doty, John; Ebisawa, Ken; Eckart, Megan; Enoto, Teruaki; Ezoe, Yuichiro; Fabian, Andrew; Ferrigno, Carlo; Foster, Adam; Fujimoto, Ryuichi; Fukazawa, Yasushi; Funk, Stefan; Furuzawa, Akihiro; Galeazzi, Massimiliano; Gallo, Luigi; Gandhi, Poshak; Gendreau, Keith; Gilmore, Kirk; Haas, Daniel; Haba, Yoshito; Hamaguchi, Kenji; Hatsukade, Isamu; Hayashi, Takayuki; Hayashida, Kiyoshi; Hiraga, Junko; Hirose, Kazuyuki; Hornschemeier, Ann; Hoshino, Akio; Hughes, John; Hwang, Una; Iizuka, Ryo; Inoue, Yoshiyuki; Ishibashi, Kazunori; Ishida, Manabu; Ishimura, Kosei; Ishisaki, Yoshitaka; Ito, Masayuki; Iwata, Naoko; Iyomoto, Naoko; Kaastra, Jelle; Kallman, Timothy; Kamae, Tuneyoshi; Kataoka, Jun; Katsuda, Satoru; Kawahara, Hajime; Kawaharada, Madoka; Kawai, Nobuyuki; Kawasaki, Shigeo; Khangaluyan, Dmitry; Kilbourne, Caroline; Kimura, Masashi; Kinugasa, Kenzo; Kitamoto, Shunji; Kitayama, Tetsu; Kohmura, Takayoshi; Kokubun, Motohide; Kosaka, Tatsuro; Koujelev, Alex; Koyama, Katsuji; Krimm, Hans; Kubota, Aya; Kunieda, Hideyo; LaMassa, Stephanie; Laurent, Philippe; Lebrun, Francois; Leutenegger, Maurice; Limousin, Olivier; Loewenstein, Michael; Long, Knox; Lumb, David; Madejski, Grzegorz; Maeda, Yoshitomo; Makishima, Kazuo; Marchand, Genevieve; Markevitch, Maxim; Matsumoto, Hironori; Matsushita, Kyoko; McCammon, Dan; McNamara, Brian; Miller, Jon; Miller, Eric; Mineshige, Shin; Minesugi, Kenji; Mitsuishi, Ikuyuki; Miyazawa, Takuya; Mizuno, Tsunefumi; Mori, Hideyuki; Mori, Koji; Mukai, Koji; Murakami, Toshio; Murakami, Hiroshi; Mushotzky, Richard; Nagano, Housei; Nagino, Ryo; Nakagawa, Takao; Nakajima, Hiroshi; Nakamori, Takeshi; Nakazawa, Kazuhiro; Namba, Yoshiharu; Natsukari, Chikara; Nishioka, Yusuke; Nobukawa, Masayoshi; Nomachi, Masaharu; Dell, Steve O'; Odaka, Hirokazu; Ogawa, Hiroyuki; Ogawa, Mina; Ogi, Keiji; Ohashi, Takaya; Ohno, Masanori; Ohta, Masayuki; Okajima, Takashi; Okamoto, Atsushi; Okazaki, Tsuyoshi; Ota, Naomi; Ozaki, Masanobu; Paerels, Frits; Paltani, Stephane; Parmar, Arvind; Petre, Robert; Pohl, Martin; Porter, F Scott; Ramsey, Brian; Reis, Rubens; Reynolds, Christopher; Russell, Helen; Safi-Harb, Samar; Sakai, Shin-ichiro; Sameshima, Hiroaki; Sanders, Jeremy; Sato, Goro; Sato, Rie; Sato, Yoichi; Sato, Kosuke; Sawada, Makoto; Serlemitsos, Peter; Seta, Hiromi; Shibano, Yasuko; Shida, Maki; Shimada, Takanobu; Shinozaki, Keisuke; Shirron, Peter; Simionescu, Aurora; Simmons, Cynthia; Smith, Randall; Sneiderman, Gary; Soong, Yang; Stawarz, Lukasz; Sugawara, Yasuharu; Sugita, Hiroyuki; Sugita, Satoshi; Szymkowiak, Andrew; Tajima, Hiroyasu; Takahashi, Hiromitsu; Takeda, Shin-ichiro; Takei, Yoh; Tamagawa, Toru; Tamura, Takayuki; Tamura, Keisuke; Tanaka, Takaaki; Tanaka, Yasuo; Tashiro, Makoto; Tawara, Yuzuru; Terada, Yukikatsu; Terashima, Yuichi; Tombesi, Francesco; Tomida, Hiroshi; Tsuboi, Yoko; Tsujimoto, Masahiro; Tsunemi, Hiroshi; Tsuru, Takeshi; Uchida, Hiroyuki; Uchiyama, Yasunobu; Uchiyama, Hideki; Ueda, Yoshihiro; Ueno, Shiro; Uno, Shinichiro; Urry, Meg; Ursino, Eugenio; de Vries, Cor; Wada, Atsushi; Watanabe, Shin; Werner, Norbert; White, Nicholas; Yamada, Takahiro; Yamada, Shinya; Yamaguchi, Hiroya; Yamasaki, Noriko; Yamauchi, Shigeo; Yamauchi, Makoto; Yatsu, Yoichi; Yonetoku, Daisuke; Yoshida, Atsumasa; Yuasa, Takayuki

    2012-01-01

    The joint JAXA/NASA ASTRO-H mission is the sixth in a series of highly successful X-ray missions initiated by the Institute of Space and Astronautical Science (ISAS). ASTRO-H will investigate the physics of the high-energy universe via a suite of four instruments, covering a very wide energy range, from 0.3 keV to 600 keV. These instruments include a high-resolution, high-throughput spectrometer sensitive over 0.3-2 keV with high spectral resolution of Delta E < 7 eV, enabled by a micro-calorimeter array located in the focal plane of thin-foil X-ray optics; hard X-ray imaging spectrometers covering 5-80 keV, located in the focal plane of multilayer-coated, focusing hard X-ray mirrors; a wide-field imaging spectrometer sensitive over 0.4-12 keV, with an X-ray CCD camera in the focal plane of a soft X-ray telescope; and a non-focusing Compton-camera type soft gamma-ray detector, sensitive in the 40-600 keV band. The simultaneous broad bandpass, coupled with high spectral resolution, will enable the pursuit o...

  17. X-rays from protostellar jets: emission from continuous flows

    E-Print Network [OSTI]

    R. Bonito; S. Orlando; G. Peres; F. Favata; R. Rosner

    2006-10-17

    Recently X-ray emission from protostellar jets has been detected with both XMM-Newton and Chandra satellites, but the physical mechanism which can give rise to this emission is still unclear. We performed an extensive exploration of a wide space of the main parameters influencing the jet/ambient interaction. Aims include: 1) to constrain the jet/ambient interaction regimes leading to the X-ray emission observed in Herbig-Haro objects in terms of the emission by a shock forming at the interaction front between a continuous supersonic jet and the surrounding medium; 2) to derive detailed predictions to be compared with optical and X-ray observations of protostellar jets; 3) to get insight into the protostellar jet's physical conditions. We performed a set of bidimensional hydrodynamic numerical simulations, in cylindrical coordinates, modeling supersonic jets ramming a uniform ambient medium. The model takes into account the most relevant physical effects, namely the thermal conduction and the radiative losses. Our model explains the observed X-ray emission from protostellar jets in a natural way. In particular we find that the case of a protostellar jet less dense than the ambient medium reproduces well the observations of the nearest Herbig-Haro object, HH154, and allows us to make detailed predictions of a possible X-ray source proper motion (vsh = 500 km/s), detectable with Chandra. Furthermore our results suggest that the simulated protostellar jets which best reproduce the X-rays observations cannot drive molecular outflows.

  18. One-Up On L1: Can X-rays Provide Longer Advanced Warning of Solar Wind Flux Enhancements Than Upstream Monitors?

    E-Print Network [OSTI]

    M. R. Collier; T. E. Moore; S. L. Snowden; K. D. Kuntz

    2005-02-17

    Observations of strong solar wind proton flux correlations with ROSAT X-ray rates along with high spectral resolution Chandra observations of X-rays from the dark Moon show that soft X-ray emission mirrors the behavior of the solar wind. In this paper, based on an analysis of an X-ray event observed by XMM-Newton resulting from charge exchange of high charge state solar wind ions and contemporaneous neutral solar wind data, we argue that X-ray observations may be able to provide reliable advance warning, perhaps by as much as half a day, of dramatic increases in solar wind flux at Earth. Like neutral atom imaging, this provides the capability to monitor the solar wind remotely rather than in-situ.

  19. The X-ray Spectrum of Cyg X-2

    E-Print Network [OSTI]

    C. Done; P. T. Zycki; D. A. Smith

    2001-11-27

    The spectra of disc accreting neutron stars generally show complex curvature, and individual components from the disc, boundary layer and neutron star surface cannot be uniquely identified. Here we show that much of the confusion over the spectral form derives from inadequate approximations for comptonization and for the iron line. There is an intrinsic low energy cutoff in comptonised spectra at the seed photon energy. It is very important to model this correctly in neutron star systems as these have expected seed photon temperatures (from either the neutron star surface, inner disc or self-absorbed cyclotron) of ~1 keV, clearly within the observed X-ray energy band. There is also reflected continuum emission which must accompany the observed iron line, which distorts the higher energy spectrum. We illustrate these points by a reanalysis of the GINGA spectra of Cyg X-2 at all points along its Z track, and show that the spectrum can be well fit by models in which the low energy spectrum is dominated by the disc, while the higher energy spectrum is dominated by comptonised emission from the boundary layer, together with its reflected spectrum from a relativistically smeared, ionised disc.

  20. Study of LINER sources with broad H(alpha) emission. X-ray properties and comparision to luminous AGN and X-ray binaries

    E-Print Network [OSTI]

    George, Younes; Sabra, B; Reeves, J N

    2011-01-01

    [Abridged]We study the X-ray properties of LINER sources with definite detection of a broad H(alpha) emission line in their optical spectra, LINER 1s from Ho et al. sample. These objects preferentially harbor a low luminosity active nucleus at the center and show small or no intrinsic absorption (<10^(22) cm^(-1)). We analyzed all available X-ray archived XMM-Newton and Chandra observations of 13 LINER 1s satisfying the above criterion in a systematic homogeneous way. We looked for any correlations between the X-ray properties and the intrinsic parameters of our sample of LINER 1s. An absorbed power-law gave a good fit to the spectra of 9 out of the 13 sources. A thermal component and an absorbed power-law were required in the remaining 4 sources. We found a photon index between 1.3\\pm0.2 for the hardest source and 2.4^(+0.2)_(-0.3) for the softest one with a mean value of 1.9\\pm0.2 and a dispersion sigma=0.3. The thermal component had a mean temperature kT~0.6 keV. Significant short (hours to days) time-s...