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1

A Fabry-Perot interferometer for sub-meV x-ray energy resolution  

Science Conference Proceedings (OSTI)

The optical theory of Fabry-Perot interferometers (FPIs) for x rays using dynamically diffracting thin perfect crystals as reflectors is developed. Application to a device using high diffraction orders in silicon crystals of thickness of the order of 100 {mu}m or more shows that energy resolutions of the order of a tenth of a meV are achievable. The effect that various features, such as gap and mirror thickness, lattice mismatches, etc., have on the FPI resonances is studied. {copyright} {ital 1996 American Institute of Physics.}

Caticha, A.; Aliberti, K. [Department of Physics, The University at Albany-SUNY, Albany, NY 12222 (United States)] [Department of Physics, The University at Albany-SUNY, Albany, NY 12222 (United States); Caticha-Ellis, S. [Departamento de Materiais, Faculdade de Engenharia Mecanica, Universidade Estadual de Campinas, Campinas, S.P. 13083-970 (Brazil)] [Departamento de Materiais, Faculdade de Engenharia Mecanica, Universidade Estadual de Campinas, Campinas, S.P. 13083-970 (Brazil)

1996-09-01T23:59:59.000Z

2

High energy resolution inelastic x-ray scattering at the SRI-CAT  

SciTech Connect

This report is a combination of vugraphs and two papers. The vugraphs give information on the beamline at the APS for IXS and the science addressable by IXS. They also cover the 10 milli-eV resolution spectrometer and the 200 milli-eV resolution spectrometer. The first paper covers the performance of the focusing Ge(444) backscattering analyzers for the inelastic x-ray scattering. The second paper discusses inelastic x-ray scattering from TiC and Ti single crystals.

Macrander, A.T.

1996-08-01T23:59:59.000Z

3

Multiple Crystal Cavities for Unlimited X-ray Energy Resolution and  

NLE Websites -- All DOE Office Websites (Extended Search)

An Intriguing Twist in the Structure of a Cobalt Oxide Catalyst An Intriguing Twist in the Structure of a Cobalt Oxide Catalyst Breaking Records in Neurological Microradiology Exposing Valence-Bond Model Inadequacies Plants' Rapid Response System Revealed Rewriting the Organofluorine Playbook Science Highlights Archives: 2013 | 2012 | 2011 | 2010 2009 | 2008 | 2007 | 2006 2005 | 2004 | 2003 | 2002 2001 | 2000 | 1998 | Subscribe to APS Science Highlights rss feed Multiple Crystal Cavities for Unlimited X-ray Energy Resolution and Coherence AUGUST 21, 2012 Bookmark and Share Fabry-Perot resonance spectra (right) of a single-cavity resonator, two cascaded resonators, and a monolithic two-cavity resonator, respectively. Note the significant background of T1 as the Bragg reflectivity from a 10-μm diamond plate is only 59%. By comparison, spectra T2 and T3 are very

4

Broadband high resolution X-ray spectral analyzer  

DOE Patents (OSTI)

A broad bandwidth high resolution x-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces x-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available x-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for x-ray microanalysis or in research applications such as laboratory and astrophysical x-ray and particle spectroscopy.

Silver, Eric H. (Berkeley, CA); Legros, Mark (Berkeley, CA); Madden, Norm W. (Livermore, CA); Goulding, Fred (Lafayette, CA); Landis, Don (Pinole, CA)

1998-01-01T23:59:59.000Z

5

Broadband high resolution X-ray spectral analyzer  

DOE Patents (OSTI)

A broad bandwidth high resolution X-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces X-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available X-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for X-ray microanalysis or in research applications such as laboratory and astrophysical X-ray and particle spectroscopy. 6 figs.

Silver, E.H.; Legros, M.; Madden, N.W.; Goulding, F.; Landis, D.

1998-07-07T23:59:59.000Z

6

High Energy Resolution Fluorescence Detection X-Ray Absorption Spectroscopy: Detection of Adsorption Sites in Supported Metal Catalysts  

Science Conference Proceedings (OSTI)

High energy resolution fluorescence detection (HERFD) X-ray adsorption spectroscopy (XAS) is demonstrated as a new tool to identify the geometry of metal adsorption sites and the orbitals involved in bonding. The type of CO adsorption site on a nanoparticular Pt-Al2O3 catalyst is determined. The orbitals involved in the Pt - CO bonding are identified using theoretical FEFF8.0 calculations. In situ application of HERFD XAS is applicable to a large number of catalytic systems and will provide fundamental insights in structure - performance relationships.

Tromp, Moniek [University of Southampton, School of Chemistry, Highfield, Southampton, SO17 1BJ (United Kingdom); Bokhoven, Jeroen A. van [Institute for chemical and bioengineering ETH Zurich (Switzerland); Safonova, Olga V.; Glatzel, Pieter [ESRF, Grenoble (France); Groot, Frank M. F. de [Utrecht University, Utrecht (Netherlands); Evans, John [University of Southampton, School of Chemistry, Highfield, Southampton, SO17 1BJ (United Kingdom); Diamond Light Source, Didcot (United Kingdom)

2007-02-02T23:59:59.000Z

7

High-Resolution X-ray Spectroscopy  

Science Conference Proceedings (OSTI)

... In support of these efforts, we also maintain laboratory x-ray sources from 1 keV to 300 keV, energy and intensity calibration facilities, and a vacuum ...

2013-02-26T23:59:59.000Z

8

X-ray Transition Energies Search Form  

Science Conference Proceedings (OSTI)

[skip navigation] X-ray Transition Energies Database Main Page Search for X-ray transition energies by element(s), transition ...

9

Photon Sciences | Beamlines | SRX: Submicron Resolution X-ray Spectroscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

SRX: Submicron Resolution X-ray Spectroscopy SRX: Submicron Resolution X-ray Spectroscopy Poster | Fact Sheet | Preliminary Design Report Scientific Scope Scientific communities such as environmental sciences, life sciences, and material sciences have identified the need to develop analytical resources to advance the understanding of complex natural and engineered systems that are heterogeneous on the micron to nanometer scale. These needs for high intensity x-ray nanoprobes resulted in the commitment of the NSLS-II Project to build the Submicron Resolution X-ray (SRX) Spectroscopy beamline showing a unique combination of high spectral resolution over a very broad energy range and very high beam intensity in a sub-micrometer spot. NSLS-II will provide one of the best sources in the world for such an instrument.

10

High resolution x-ray microscope  

Science Conference Proceedings (OSTI)

The authors present x-ray images of grid meshes and biological material obtained using a microspot x-ray tube with a multilayer optic and a 92-element parabolic compound refractive lens (CRL) made of a plastic containing only hydrogen and carbon. Images obtained using this apparatus are compared with those using an area source with a spherical lens and a spherical lens with multilayer condenser. The authors found the best image quality using the multilayer condenser with a parabolic lens, compared to images with a spherical lens and without the multilayer optics. The resolution was measured using a 155-element parabolic CRL and a multilayer condenser with the microspot tube. The experiment demonstrates about 1.1 {mu}m resolution.

Gary, C. K.; Park, H.; Lombardo, L. W.; Piestrup, M. A.; Cremer, J. T.; Pantell, R. H.; Dudchik, Y. I. [Adelphi Technology, Inc. 981-B Industrial Road, San Carlos, California 94070 (United States); Department of Electrical Engineering, Stanford University, Stanford, California 94305 (United States); Institute of Applied Physics Problems, Kurchatova 7, Minsk 220064 (Belarus)

2007-04-30T23:59:59.000Z

11

High-Energy Nanoscale-Resolution X-ray Microscopy Based on Refractive Optics on a Long Beamline  

Science Conference Proceedings (OSTI)

The long length and good coherence properties of ID11 at the ESRF have led to the development of x-ray microscopy based on compound refractive lenses (CRLs). For the highest resolution full-field microscopy, the sample is placed {approx}40 m from the source, which can be micro-focused by a transfocator as a condenser. Due to the long length of the beamline and consequent long sample-detector distance, a CRL objective can be placed up to a meter behind the sample and still allow for magnification of 60x on a detector located at 99 m--enough to achieve easily 100-nm resolution with a typical high-resolution detector.

Snigireva, I.; Vaughan, G. B. M.; Snigirev, A. [European Synchrotron Radiation Facility (ESRF), 38043 Grenoble (France)

2011-09-09T23:59:59.000Z

12

An active-optic x-ray fluorescence analyzer with high energy resolution, large solid angle coverage, and a large tuning range  

SciTech Connect

A crystal-optic x-ray fluorescence energy analyzer has been designed and tested, which combines the features of electron-volt energy resolution, large solid angle coverage, and tunability over several kilo-electron-volts. The design is based upon the principle of active optics, with ten actuators available to optimally adjust the shape of a silicon crystal used in the Bragg geometry. In most applications the shape is that of a logarithmic spiral for high energy resolution with a spatially nonresolving detector, but a wide range of other shapes is also possible for applications such as imaging or single-shot spectroscopy in a spectral range of the operator's choosing.

Adams, Bernhard W.; Attenkofer, Klaus [Argonne National Laboratory, Argonne, Illinois 60439 (United States)

2008-02-15T23:59:59.000Z

13

NIST X-Ray Transition Energies  

Science Conference Proceedings (OSTI)

... with the International System of measurement ... titled "X-ray transition energies: new approach ... and by NIST's Systems Integration for Manufacturing ...

2011-12-09T23:59:59.000Z

14

Energy Determination of X-Ray Transition Energies Using the ...  

Science Conference Proceedings (OSTI)

... We chose to measure x-ray transition energies from NIST ... This resulted in the production of x-ray emission ... would yield not only an energy scale for ...

2012-10-02T23:59:59.000Z

15

Calibration of High-Resolution X-Ray Tomography With ...  

Science Conference Proceedings (OSTI)

... The x-ray attenuation of the sample at this energy was close to the ... J. Coal Geol. ... G. Xu, DE Eastman, I. McNulty, SP Frigo, Y. Wang, CC Retsch, IC ...

2001-04-11T23:59:59.000Z

16

High-Resolution X-ray Imaging of the Colliding Wind Shock in WR147  

E-Print Network (OSTI)

We analyze new high-resolution Chandra X-ray images of the Wolf-Rayet binary system WR147. This system contains a WN8 star with an early-type companion located 0.6'' to its north, and is the only known early-type binary with a separation on the sky large enough for the wind-wind collision between the stars to currently be resolved at X-ray energies. The 5 ksec Chandra HRC-I image provides the first direct evidence for spatially extended X-ray emission in an early-type binary system. The X-ray emission peaks close to the position of the radio bow shock and north of the WN8 star. A deeper X-ray image is needed to accurately determine the degree of spatial extension, to exactly align the X-ray and optical/radio frames, and to determine whether part of the detected X-ray emission arises in the individual stellar winds. Simulated X-ray images of the wind-wind collision have a FWHM consistent with the data, and maximum likelihood fits suggest that a deeper observation may also constrain the inclination and wind momentum ratio of this system. However, as the WR wind dominates the colliding wind X-ray emission it appears unlikely that the mass-loss rate and the terminal velocity of the companion wind can be separately determined from X-ray observations. We also note an inconsistency between numerical and analytical estimates of the X-ray luminosity ratio of the stronger and weaker wind components, and conclude that the analytical results are in error.

J. M. Pittard; I. R. Stevens; P. M. Williams; A. M. T. Pollock; S. L. Skinner; M. F. Corcoran; A. F. J. Moffat

2002-04-12T23:59:59.000Z

17

TENDER ENERGY X-RAY ABSORPTION  

NLE Websites -- All DOE Office Websites (Extended Search)

TENDER ENERGY X-RAY ABSORPTION TENDER ENERGY X-RAY ABSORPTION SPECTROSCOPY (TES) Project Team: S. Bare 1,2 , J. Brandes 3 , T. Buonassisi 4 , J. Chen 5,2 , M. Croft 6 , E. DiMasi 7 , A. Frenkel 8,2 , D. Hesterberg 9 , S. Hulbert 7,2 , S. Khalid 7 , S. Myneni 10 , P. Northrup 7,11 , E.T. Rasbury 11 , B. Ravel 12 , R. Reeder 11 , J. Rodriguez 7,2 , D. Sparks 5,13 , V. Stojanoff 7 , G. Waychunas 14 1 UOP LLC, 2 Synchrotron Catalysis Consortium, 3 Skidaway Inst. of Oceanography, 4 MIT Laboratory for Photovoltaics Research, 5 Univ. of Delaware, 6 Rutgers Univ., 7 Brookhaven National Lab, 8 Yeshiva Univ., 9 North Carolina State Univ., 10 Princeton Univ., 11 Stony Brook Univ., 12 NIST, 13 Delaware Environmental Inst., 14 Lawrence Berkeley National Lab TECHNIQUES: High performance and in-situ X-ray absorption spectroscopy and spatially-resolved XAS of

18

Development of a High Resolution X-Ray Imaging Crystal Spectrometer for Measurement of Ion-Temperature and Rotation-Velocity Profiles in Fusion Energy Research Plasmas  

SciTech Connect

A new imaging high resolution x-ray crystal spectrometer (XCS) has been developed to measure continuous profiles of ion temperature and rotation velocity in fusion plasmas. Following proof-of-principle tests on the Alcator C-Mod tokamak and the NSTX spherical tokamak, and successful testing of a new silicon, pixilated detector with 1MHz count rate capability per pixel, an imaging XCS is being designed to measure full profiles of Ti and v? on C-Mod. The imaging XCS design has also been adopted for ITER. Ion-temperature uncertainty and minimum measurable rotation velocity are calculated for the C-Mod spectrometer. The affects of x-ray and nuclear-radiation background on the measurement uncertainties are calculated to predict performance on ITER.

Hill, K W; Broennimann, Ch; Eikenberry, E F; Ince-Cushman, A; Lee, S G; Rice, J E; Scott, S

2008-02-27T23:59:59.000Z

19

The Road to Ultrahigh-Resolution X-ray Spectrometers | Advanced Photon  

NLE Websites -- All DOE Office Websites (Extended Search)

How Atoms Behave: Characteristics of Microstructural Avalanches How Atoms Behave: Characteristics of Microstructural Avalanches Iodate Refuses to Intimidate Creating the Heart of a Planet in the Heart of a Gem How a Powerful Antibody Neutralizes HIV Taking a Page from Nature to Build Better Nanomaterials Science Highlights Archives: 2013 | 2012 | 2011 | 2010 2009 | 2008 | 2007 | 2006 2005 | 2004 | 2003 | 2002 2001 | 2000 | 1998 | Subscribe to APS Science Highlights rss feed The Road to Ultrahigh-Resolution X-ray Spectrometers NOVEMBER 22, 2011 Bookmark and Share Basic phenomena underlying the AD&AT x-ray optics. In x-ray Bragg diffraction from atomic planes composing nonzero angle η to the crystal entrance face, the crystal acts (a) like an optical prism dispersing the photons into a divergent x-ray fan with photons of different energies E

20

Chest x-Rays | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Chest x-Rays Chest x-Rays Chest x-Rays Chest X-ray B-Reading The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica. The B-reading is considered a special reading because doctors who are certified by NIOSH to perform B-readings use a specific protocol to read and record the findings as developed by the International Labour Organization (ILO). The ILO's protocol provides rules for systematically examining the x-ray in a step-by-step method and recording certain abnormalities or changes on the chest x-ray that can be attributable to

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

Neutron and X-ray Scattering Investigations of Microscopic Energy ...  

Science Conference Proceedings (OSTI)

A Case Study in Future Energy Challenges: Towards In Situ Hard X-ray Microscopy of ... of Crystal Structure and Domain Character in Lead Free Piezoceramics.

22

NIST X-Ray Transition Energies Version History  

Science Conference Proceedings (OSTI)

... Jr., P. Indelicato, L. de Billy, E. Lindroth, and J. Anton, "X-ray transition energies: new approach to a ... [Type of medium] Available: URL [Access date]. ...

2010-10-05T23:59:59.000Z

23

Cryogenic, high-resolution x-ray detector with high count rate capability  

DOE Patents (OSTI)

A cryogenic, high-resolution X-ray detector with high count rate capability has been invented. The new X-ray detector is based on superconducting tunnel junctions (STJs), and operates without thermal stabilization at or below 500 mK. The X-ray detector exhibits good resolution (.about.5-20 eV FWHM) for soft X-rays in the keV region, and is capable of counting at count rates of more than 20,000 counts per second (cps). Simple, FET-based charge amplifiers, current amplifiers, or conventional spectroscopy shaping amplifiers can provide the electronic readout of this X-ray detector.

Frank, Matthias (Oakland, CA); Mears, Carl A. (Windsor, CA); Labov, Simon E. (Berkeley, CA); Hiller, Larry J. (Livermore, CA); Barfknecht, Andrew T. (Menlo Park, CA)

2003-03-04T23:59:59.000Z

24

Applications of High Resolution X-ray Computed Tomography in ...  

Science Conference Proceedings (OSTI)

... data, including concentration profiles from x-ray absorption measurements during ... Dynamic Evolution of Liquid-liquid Phase Separation While Cooling in a

25

High-energy x-ray production with pyroelectric crystals  

Science Conference Proceedings (OSTI)

The invention of pyroelectric x-ray generator technology has enabled researchers to develop ultraportable, low-power x-ray sources for use in imaging, materials analysis, and other applications. For many applications, the usefulness of an x-ray source is determined by its yield and endpoint energy. In x-ray fluorescence, for example, high-energy sources enable the excitation of the K-shell x-ray peaks for high-Z materials as well as the lower-energy L-shell peaks, allowing more positive sample identification. This report shows how a paired-crystal pyroelectric source can be used to approximately double the endpoint x-ray energy, in addition to doubling the x-ray yield, versus a single-crystal source. As an example of the advantage of a paired-crystal system, we present a spectrum showing the fluorescence of the K shell of thorium using a pyroelectric source, as well as a spectrum showing the fluorescence of the K shell of lead. Also shown is an x-ray spectrum with an endpoint energy of 215 keV.

Geuther, Jeffrey A.; Danon, Yaron [Department of Mechanical, Aerospace, and Nuclear Engineering, Rensselaer Polytechnic Institute, Troy, New York 12180 (United States)

2005-05-15T23:59:59.000Z

26

Hard x-ray monochromator with milli-electron volt bandwidth for high-resolution diffraction studies of diamond crystals  

SciTech Connect

We report on design and performance of a high-resolution x-ray monochromator with a spectral bandwidth of {Delta}E{sub X}{approx_equal} 1.5 meV, which operates at x-ray energies in the vicinity of the backscattering (Bragg) energy E{sub H} = 13.903 keV of the (008) reflection in diamond. The monochromator is utilized for high-energy-resolution diffraction characterization of diamond crystals as elements of advanced x-ray crystal optics for synchrotrons and x-ray free-electron lasers. The monochromator and the related controls are made portable such that they can be installed and operated at any appropriate synchrotron beamline equipped with a pre-monochromator.

Stoupin, Stanislav; Shvyd'ko, Yuri; Shu Deming; Khachatryan, Ruben; Xiao, Xianghui; DeCarlo, Francesco; Goetze, Kurt; Roberts, Timothy; Roehrig, Christian; Deriy, Alexey [Advanced Photon Source, Argonne National Laboratory, Illinois 60439 (United States)

2012-02-15T23:59:59.000Z

27

Hard x-ray monochromator with milli-electron volt bandwidth for high-resolution diffraction studies of diamond crystals.  

Science Conference Proceedings (OSTI)

We report on design and performance of a high-resolution x-ray monochromator with a spectral bandwidth of {Delta}E{sub x} {approx_equal} 1.5 meV, which operates at x-ray energies in the vicinity of the backscattering (Bragg) energy E{sub H} = 13.903 keV of the (008) reflection in diamond. The monochromator is utilized for high-energy-resolution diffraction characterization of diamond crystals as elements of advanced x-ray crystal optics for synchrotrons and x-ray free-electron lasers. The monochromator and the related controls are made portable such that they can be installed and operated at any appropriate synchrotron beamline equipped with a pre-monochromator.

Stoupin, S.; Shvydko, Y.; Shu, D.; Khachatryan, R.; Xiao, X. (X-Ray Science Division)

2012-01-01T23:59:59.000Z

28

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Wednesday, 31 August 2005 00:00 Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

29

High-energy x-ray backlighter spectrum measurements using calibrated image plates  

Science Conference Proceedings (OSTI)

The x-ray spectrum between 18 and 88 keV generated by a petawatt laser driven x-ray backlighter target was measured using a 12-channel differential filter pair spectrometer. The spectrometer consists of a series of filter pairs on a Ta mask coupled with an x-ray sensitive image plate. A calibration of Fuji{trademark} MS and SR image plates was conducted using a tungsten anode x-ray source and the resulting calibration applied to the design of the Ross pair spectrometer. Additionally, the fade rate and resolution of the image plate system were measured for quantitative radiographic applications. The conversion efficiency of laser energy into silver K{alpha} x rays from a petawatt laser target was measured using the differential filter pair spectrometer and compared to measurements using a single photon counting charge coupled device.

Maddox, B.R.; Park, H.S.; Remington, B.A.; Izumi, N.; Chen, S.; Chen, C.; Kimminau, G.; Ali, Z.; Haugh, M.J.; Ma, Q. (LLNL); (NWU); (Oxford); (NSTec)

2012-10-10T23:59:59.000Z

30

High-energy x-ray backlighter spectrum measurements using calibrated image plates  

Science Conference Proceedings (OSTI)

The x-ray spectrum between 18 and 88 keV generated by a petawatt laser driven x-ray backlighter target was measured using a 12-channel differential filter pair spectrometer. The spectrometer consists of a series of filter pairs on a Ta mask coupled with an x-ray sensitive image plate. A calibration of Fuji MS and SR image plates was conducted using a tungsten anode x-ray source and the resulting calibration applied to the design of the Ross pair spectrometer. Additionally, the fade rate and resolution of the image plate system were measured for quantitative radiographic applications. The conversion efficiency of laser energy into silver K{alpha} x rays from a petawatt laser target was measured using the differential filter pair spectrometer and compared to measurements using a single photon counting charge coupled device.

Maddox, B. R.; Park, H. S.; Remington, B. A.; Izumi, N.; Chen, S.; Chen, C. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Kimminau, G. [Department of Physics, Clarendon Laboratory, University of Oxford, Parks Road, Oxford OX1 3PU (United Kingdom); Ali, Z.; Haugh, M. J. [National Security Technologies, LLC, Livermore, California 94550 (United States); Ma, Q. [DND-CAT, Argonne National Laboratory, Argonne, Illinois 60439-4857 (United States)

2011-02-15T23:59:59.000Z

31

X-ray microscopy of laser fusion targets in four energy bands from 0.7 to 4.0 keV  

SciTech Connect

A grazing x-ray microscope was shown to be able to photograph the x-ray emission from laser-produced plasmas between 0.8 and 4.0 keV with a spatial resolution of approximately 3 microns. The calibration of the x-ray mirror energy response functions and the x-ray film allow absolute measurements of the spatial and spectral distribution of the x-ray emission from laser fusion targets. (MOW)

Boyle, M.J.; Seward, F.D.; Harper, T.L.; Koppel, L.N.; Pettipiece, K.J.; Ahlstrom, H.G.

1975-10-15T23:59:59.000Z

32

Exploring electronic structure through high-resolution hard x-ray  

NLE Websites -- All DOE Office Websites (Extended Search)

Exploring electronic structure through high-resolution hard x-ray Exploring electronic structure through high-resolution hard x-ray spectroscopies Tuesday, July 23, 2013 - 11:00am SLAC, Conference Room 137-322 Presented by Dimosthenis Sokaras, Stanford Synchrotron Radiation Lightsource, SLAC National Accelerator Laboratory Modern high brilliance beamlines coupled with recent advances in hard-x-ray optics are establishing high-resolution hard x-ray spectroscopies as a powerful analytical tool for routine electronic structure investigations. Their advantageous characteristics like the chemical sensitivity or the hard x-rays penetration depth, that permits the implementation of difficult sample environments, expand the applicability of the relevant studies to multidisciplinary scientific fields. Simultaneously, the experimental

33

Application of In-Situ High Energy-Resolution Fluorescence Detection and Time-Resolved X-Ray Spectroscopy: Catalytic Activation of Oxygen over Supported Gold Catalysts  

SciTech Connect

Life-time-broadening reduction in high-energy-resolution fluorescence detected XAS produced spectra of unprecedented detail. Au L3 edge spectra of a Au/Al2O3 catalyst under various reaction conditions showed the interaction of oxygen with the gold particles on this catalyst. A reaction path on the gold particle in the oxidation of CO was established.

Bokhoven, Jeroen A. van [Institute for Chemical and Bioengineering, ETH Zurich (Switzerland); Tromp, Moniek [University of Southampton, School of Chemistry, Southampton (United Kingdom); Glatzel, Pieter; Safonova, Olga [European Synchrotron Radiation Facility, Grenoble (France)

2007-02-02T23:59:59.000Z

34

X-ray pulse preserving single-shot optical cross-correlation method for improved experimental temporal resolution  

Science Conference Proceedings (OSTI)

We measured the relative arrival time between an optical pulse and a soft x-ray pulse from a free-electron laser. This femtosecond cross-correlation measurement was achieved by observing the change in optical reflectivity induced through the absorption of a fraction of the x-ray pulse. The main x-ray pulse energy remained available for an independent pump-probe experiment where the sample may be opaque to soft x-rays. The method was employed to correct the two-pulse delay data from a canonical pump-probe experiment and demonstrate 130 {+-} 20 fs (FWHM) temporal resolution. We further analyze possible timing jitter sources and point to future improvements.

Beye, M. [SIMES, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Helmholtz-Zentrum Berlin fuer Materialien und Energie GmbH, 12489 Berlin (Germany); Krupin, O. [LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); European XFEL GmbH, 22607 Hamburg (Germany); Hays, G.; Jong, S. de; Lee, S.; Coffee, R.; Holmes, M. R.; Fry, A. R.; White, W. E.; Bostedt, C.; Schlotter, W. F. [LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Reid, A. H. [SIMES, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Radboud University Nijmegen, Institute for Molecules and Materials, 6525 AJ Nijmegen (Netherlands); Rupp, D. [Technische Universitaet Berlin, 10623 Berlin (Germany); LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Lee, W.-S.; Scherz, A. O. [SIMES, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Chuang, Y.-D. [Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Cryan, J. P.; Glownia, J. M. [PULSE, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Foehlisch, A. [Helmholtz-Zentrum Berlin fuer Materialien und Energie GmbH, 12489 Berlin (Germany); Durr, H. A. [SIMES, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); PULSE, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States)

2012-03-19T23:59:59.000Z

35

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

36

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

37

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

38

High-Resolution Structure of the Photosynthetic Mn4Ca Catalyst from X-ray Spectroscopy  

E-Print Network (OSTI)

the Photosynthetic Mn 4 Ca Catalyst from X-ray Spectroscopystructure of the Mn 4 Ca catalyst at high-resolution whichthe structure of Mn 4 Ca catalyst as it cycles through the

Yano, Junko

2008-01-01T23:59:59.000Z

39

High resolution, high rate x-ray spectrometer  

DOE Patents (OSTI)

It is an object of the invention to provide a pulse processing system for use with detected signals of a wide dynamic range which is capable of very high counting rates, with high throughput, with excellent energy resolution and a high signal-to-noise ratio. It is a further object to provide a pulse processing system wherein the fast channel resolving time is quite short and substantially independent of the energy of the detected signals. Another object is to provide a pulse processing system having a pile-up rejector circuit which will allow the maximum number of non-interfering pulses to be passed to the output. It is also an object of the invention to provide new methods for generating substantially symmetrically triangular pulses for use in both the main and fast channels of a pulse processing system.

Goulding, F.S.; Landis, D.A.

1983-07-14T23:59:59.000Z

40

Single atom identification by energy dispersive x-ray spectroscopy  

SciTech Connect

Using aberration-corrected scanning transmission electron microscope and energy dispersive x-ray spectroscopy, single, isolated impurity atoms of silicon and platinum in monolayer and multilayer graphene are identified. Simultaneously acquired electron energy loss spectra confirm the elemental identification. Contamination difficulties are overcome by employing near-UHV sample conditions. Signal intensities agree within a factor of two with standardless estimates.

Lovejoy, T. C.; Dellby, N.; Krivanek, O. L. [Nion, 1102 8th St., Kirkland, Washington 98033 (United States); Ramasse, Q. M. [SuperSTEM Laboratory, STFC Daresbury, Keckwick Lane, Daresbury WA4 4AD (United Kingdom); Falke, M.; Kaeppel, A.; Terborg, R. [Bruker Nano GmbH, Schwarzschildstr. 12, 12489 Berlin (Germany); Zan, R. [School of Physics and Astronomy, University of Manchester, Manchester M13 9PL (United Kingdom)

2012-04-09T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Acoustically Mounted Microcrystals Yield High-Resolution X-ray Structures  

SciTech Connect

We demonstrate a general strategy for determining structures from showers of microcrystals. It uses acoustic droplet ejection to transfer 2.5 nL droplets from the surface of microcrystal slurries, through the air, onto mounting micromesh pins. Individual microcrystals are located by raster-scanning a several-micrometer X-ray beam across the cryocooled micromeshes. X-ray diffraction data sets merged from several micrometer-sized crystals are used to determine 1.8 {angstrom} resolution crystal structures.

Soares, Alexei S.; Engel, Matthew A.; Stearns, Richard; Datwani, Sammy; Olechno, Joe; Ellson, Richard; Skinner, John M.; Allaire, Marc; Orville, Allen M. (Labcyte); (BNL)

2012-10-25T23:59:59.000Z

42

Absolute x-ray energy calibration over a wide energy range using a diffraction-based iterative method  

SciTech Connect

In this paper, we report a method of precise and fast absolute x-ray energy calibration over a wide energy range using an iterative x-ray diffraction based method. Although accurate x-ray energy calibration is indispensable for x-ray energy-sensitive scattering and diffraction experiments, there is still a lack of effective methods to precisely calibrate energy over a wide range, especially when normal transmission monitoring is not an option and complicated micro-focusing optics are fixed in place. It is found that by using an iterative algorithm the x-ray energy is only tied to the relative offset of sample-to-detector distance, which can be readily varied with high precision of the order of 10{sup -5}-10{sup -6} spatial resolution using gauge blocks. Even starting with arbitrary initial values of 0.1 A, 0.3 A, and 0.4 A, the iteration process converges to a value within 3.5 eV for 31.122 keV x-rays after three iterations. Different common diffraction standards CeO{sub 2}, Au, and Si show an energy deviation of 14 eV. As an application, the proposed method has been applied to determine the energy-sensitive first sharp diffraction peak of network forming GeO{sub 2} glass at high pressure, exhibiting a distinct behavior in the pressure range of 2-4 GPa. Another application presented is pair distribution function measurement using calibrated high-energy x-rays at 82.273 keV. Unlike the traditional x-ray absorption-based calibration method, the proposed approach does not rely on any edges of specific elements, and is applicable to the hard x-ray region where no appropriate absorption edge is available.

Hong Xinguo; Chen Zhiqiang [Mineral Physics Institute, Stony Brook University, Stony Brook, New York 11794 (United States); Duffy, Thomas S. [Department of Geosciences, Princeton University, Princeton, New Jersey 08544 (United States)

2012-06-15T23:59:59.000Z

43

The Application of Monochromatic Energies to Investigate Multiphase Porous Media Systems using Synchrotron X-ray Tomography  

SciTech Connect

X-ray computed tomography (CT) is becoming a useful tool for nondestructive imaging of many geoenvironmental and geotechnical systems. Conventional X-ray CT systems typically utilize a polychromatic X-ray beam. While providing a high throughput of photons, the use of polychromatic energy can make quantifying material concentrations, densities or composition very difficult or impossible without appropriate standards. Synchrotron X-rays have an extremely small angular divergence, thus permitting spatial resolution that is only limited by the optical components of the system. In addition, the ability to tune to a monochromatic X-ray energy allows better phase contrast by reducing beam hardening and allowing for elemental discrimination. In this work we will show how monochromatic energy can be used to provide high-quality images allowing for phase separation several different porous media systems thus improving our ability to quantify a range of processes and phenomena.

Ham, Kyungmin; Willson, Clinton S. (LSU)

2006-01-31T23:59:59.000Z

44

X-ray Observations of Galaxies: The Importance of Deep High-Resolution Observations  

E-Print Network (OSTI)

X-ray observations of galaxies have grown from a curiosity into a full-fledged field of astronomy. These observations provide unique information on black holes, binary stars, and the hot phase of the ISM, which can be used to constrain the chemical evolution of the Universe, and the joint evolution of galaxies and massive black holes. These exciting results are due in large part to the high-resolution capability of {\\it Chandra}. To follow on {\\it Chandra} and push forward this science past the present capabilities, our community must build a high-resolution (sub-arcsecond) large-area (several square meters) X-ray telescope.

G. Fabbiano

2007-11-05T23:59:59.000Z

45

Demonstration of 12 nm resolution Fresnel zone plate lens based soft x-ray microscopy  

Science Conference Proceedings (OSTI)

To extend soft x-ray microscopy to a resolution of order 10 nm or better, we developed a new nanofabrication process for Fresnel zone plate lenses. The new process, based on the double patterning technique, has enabled us to fabricate high quality gold zone plates with 12 nm outer zones. Testing of the zone plate with the full-field transmission x-ray microscope, XM-1, in Berkeley, showed that the lens clearly resolved 12 nm lines and spaces. This result represents a significant step towards 10 nm resolution and beyond.

Chao, W.; Kim, J.; Rekawa, S.; Fischer, P.; Anderson, E. H.

2009-06-05T23:59:59.000Z

46

High-Resolution Structure of the Photosynthetic Mn4Ca Catalyst from X-ray Spectroscopy  

Science Conference Proceedings (OSTI)

The application of high-resolution X-ray spectroscopy methods to study the photosynthetic water oxidizing complex, which contains a unique hetero-nuclear catalytic Mn4Ca cluster, are described. Issues of X-ray damage especially at the metal sites in the Mn4Ca cluster are discussed. The structure of the Mn4Ca catalyst at high-resolution which has so far eluded attempts of determination by X-ray diffraction, EXAFS and other spectroscopic techniques has been addressed using polarized EXAFS techniques applied to oriented PS II membrane preparations and PS II single crystals. A review of how the resolution of traditional EXAFS techniques can be improved, using methods such as range-extended EXAFS is presented, and the changes that occur in the structure of the cluster as it advances through the catalytic cycle are described. X-ray absorption and emission techniques (XANES and K? emission) have been used earlier to determine the oxidation states of the Mn4Ca cluster, and in this report we review the use of X-ray resonant Raman spectroscopy to understand the electronic structure of the Mn4Ca cluster as it cycles through the intermediate S-states.

Yachandra, Vittal; Yano, Junko; Kern, Jan; Pushkar, Yulia; Sauer, Kenneth; Glatzel, Pieter; Bergmann, Uwe; Messinger, Johannes; Zouni, Athina; Yachandra, Vittal K.

2007-08-01T23:59:59.000Z

47

Residual stress measurement with high energy x-rays at the Advanced Photon Source.  

SciTech Connect

Preliminary measurements with high energy x-rays from the SRI CAT 1-ID beam line at the Advanced Photon show great promise for the measurement of stress and strain using diffraction. Comparisons are made with neutron measurements. Measurements of strains in a 2 mm thick 304 stainless steel weld show that excellent strain and spatial resolutions are possible. With 200 {micro}m slits, strain resolutions of 1 x 10{sup {minus}5} were achieved.

Winholtz, R. A.; Haeffner, D. R.; Green, R.E.L.; Varma, R.; Hammond, D.

2000-03-02T23:59:59.000Z

48

Refractive optical elements and optical system for high energy x-ray microscopy  

Science Conference Proceedings (OSTI)

In material science, X-ray radiation with photon energies above 25 keV is used because of its penetration into high density materials. Research of the inner structure of novel materials, such as electrodes in high power batteries for engines, require X-ray microscopes operating in the hard X-ray energy range. A flexible X-ray microscope for hard X-rays with photon energies higher than 25 keV will be realized at the synchrotron source ANKA in Karlsruhe, Germany. The device will use refractive X-ray lenses as condenser as well as objective lenses.

Simon, M.; Altapova, V.; Baumbach, T.; Kluge, M.; Last, A.; Marschall, F.; Mohr, J.; Nazmov, V.; Vogt, H. [Karlsruhe Institute of Technology, Institute of Microstructure Technology, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany); Karlsruhe Institute of Technology, Laboratory for Applications of Synchrotron Radiation, Engesser Strasse 15, 76131 Karlsruhe (Germany); Karlsruhe Institute of Technology, Institute of Microstructure Technology, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany)

2012-05-17T23:59:59.000Z

49

High spatial resolution X-ray and gamma ray imaging system using diffraction crystals  

DOE Patents (OSTI)

A method and a device for high spatial resolution imaging of a plurality of sources of x-ray and gamma-ray radiation are provided. The device comprises a plurality of arrays, with each array comprising a plurality of elements comprising a first collimator, a diffracting crystal, a second collimator, and a detector.

Smither, Robert K. (Hinsdale, IL)

2011-05-17T23:59:59.000Z

50

Submicrometre-Resolution Polychromatic Three-dimensional X-ray Microscopy  

Science Conference Proceedings (OSTI)

The ability to study the structure, microstructure and evolution of materials with increasing spatial resolution is fundamental to achieving a full understanding of the underlying science of materials. Polychromatic three-dimensional X-ray microscopy (3DXM) is a recently developed nondestructive diffraction technique that enables crystallographic phase identification, determination of local crystal orientations, grain morphologies, grain interface types and orientations, and in favorable cases direct determination of the deviatoric elastic strain tensor with submicrometre spatial resolution in all three dimensions. With the added capability of an energy-scanning incident beam monochromator, the determination of absolute lattice parameters is enabled, allowing specification of the complete elastic strain tensor with three- dimensional spatial resolution. The methods associated with 3DXM are described and key applications of 3DXM are discussed, including studies of deformation in single-crystal and polycrystalline metals and semiconductors, indentation deformation, thermal grain growth in polycrystalline aluminium, the metal insulator transition in nanoplatelet VO 2 , interface strengths in metal matrix composites, high-pressure science, Sn whisker growth, and electromigra- tion processes. Finally, the outlook for future developments associated with this technique is described.

Larson, Ben C [ORNL; Levine, Lyle E. [National Institute of Standards and Technology (NIST)

2013-01-01T23:59:59.000Z

51

High resolution stationary digital breast tomosynthesis using distributed carbon nanotube x-ray source array  

Science Conference Proceedings (OSTI)

Purpose: The purpose of this study is to investigate the feasibility of increasing the system spatial resolution and scanning speed of Hologic Selenia Dimensions digital breast tomosynthesis (DBT) scanner by replacing the rotating mammography x-ray tube with a specially designed carbon nanotube (CNT) x-ray source array, which generates all the projection images needed for tomosynthesis reconstruction by electronically activating individual x-ray sources without any mechanical motion. The stationary digital breast tomosynthesis (s-DBT) design aims to (i) increase the system spatial resolution by eliminating image blurring due to x-ray tube motion and (ii) reduce the scanning time. Low spatial resolution and long scanning time are the two main technical limitations of current DBT technology. Methods: A CNT x-ray source array was designed and evaluated against a set of targeted system performance parameters. Simulations were performed to determine the maximum anode heat load at the desired focal spot size and to design the electron focusing optics. Field emission current from CNT cathode was measured for an extended period of time to determine the stable life time of CNT cathode for an expected clinical operation scenario. The source array was manufactured, tested, and integrated with a Selenia scanner. An electronic control unit was developed to interface the source array with the detection system and to scan and regulate x-ray beams. The performance of the s-DBT system was evaluated using physical phantoms. Results: The spatially distributed CNT x-ray source array comprised 31 individually addressable x-ray sources covering a 30 angular span with 1 pitch and an isotropic focal spot size of 0.6 mm at full width at half-maximum. Stable operation at 28 kV(peak) anode voltage and 38 mA tube current was demonstrated with extended lifetime and good source-to-source consistency. For the standard imaging protocol of 15 views over 14, 100 mAs dose, and 2 x 2 detector binning, the projection resolution along the scanning direction increased from 4.0 cycles/mm [at 10% modulation-transfer-function (MTF)] in DBT to 5.1 cycles/mm in s-DBT at magnification factor of 1.08. The improvement is more pronounced for faster scanning speeds, wider angular coverage, and smaller detector pixel sizes. The scanning speed depends on the detector, the number of views, and the imaging dose. With 240 ms detector readout time, the s-DBT system scanning time is 6.3 s for a 15-view, 100 mAs scan regardless of the angular coverage. The scanning speed can be reduced to less than 4 s when detectors become faster. Initial phantom studies showed good quality reconstructed images. Conclusions: A prototype s-DBT scanner has been developed and evaluated by retrofitting the Selenia rotating gantry DBT scanner with a spatially distributed CNT x-ray source array. Preliminary results show that it improves system spatial resolution substantially by eliminating image blur due to x-ray focal spot motion. The scanner speed of s-DBT system is independent of angular coverage and can be increased with faster detector without image degration. The accelerated lifetime measurement demonstrated the long term stability of CNT x-ray source array with typical clinical operation lifetime over 3 years.

Qian Xin; Tucker, Andrew; Gidcumb, Emily; Shan Jing; Yang Guang; Calderon-Colon, Xiomara; Sultana, Shabana; Lu Jianping; Zhou, Otto; Spronk, Derrek; Sprenger, Frank; Zhang Yiheng; Kennedy, Don; Farbizio, Tom; Jing Zhenxue [Department of Physics and Astronomy, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States); Department of Biomedical Engineering, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States); Curriculum in Applied Sciences and Engineering, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States); Department of Physics and Astronomy, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States); Curriculum in Applied Sciences and Engineering, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States); Department of Physics and Astronomy, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States) and Department of Biomedical Engineering, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States); Department of Physics and Astronomy, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States) Department of Biomedical Engineering, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States) and Lineberger Comprehensive Cancer Center, University of North Carolina at Chapel Hill, Chapel Hill, North Carolina 27599 (United States); XinRay Systems, Inc., Research Triangle Park, North Carolina 27709 (United States); Hologic, Inc., Bedford, Massachusetts 01730 (United States)

2012-04-15T23:59:59.000Z

52

Microstructural Mapping Using High-Energy X-Ray Scattering  

Science Conference Proceedings (OSTI)

Abstract Scope, Advanced characterization methods at the APS permit unique in- situ ... The combination of an undulator source, brilliance preserving optics and focusing .... Ultra-Small-Angle X-Ray ScatteringX-Ray Photon Correlation...

53

High?resolution x?ray microscopy using an undulator source, photoelectron studies with MAXIMUM  

Science Conference Proceedings (OSTI)

We present the first results of high?spatial resolution x?ray imaging studies with an upgraded version of the scanning photoemission multiple application x?ray imaging undulator microscope. The microscope is a multilayercoated Schwarzschild objective that focuses undulator radiation onto the sample. The recent upgrade improved the spatial resolution by a factor six reaching a full width at half maximum value of 0.5 ?m. Highly polished mirrors reduced the diffuse background by almost two orders of magnitude and drastically improved the contrast. The improved microscope was used to perform a series of tests on microgrids and reverse Fresnel zone plates. The microscope capability to detect chemical and topological contrast was verified by using patterned metal overlayers on Si and GaAs substrates. Further improvements to increase the flux and the spatial resolution are underway; this includes the installation of a new undulator beamline.

C. Capasso; A. K. Ray?Chaudhuri; W. Ng; S. Liang; R. K. Cole; J. Wallace; F. Cerrina; G. Margaritondo; J. H. Underwood; J. B. Kortright; R. C. C. Perera

1991-01-01T23:59:59.000Z

54

Wolter-like high resolution x-ray imaging microscope for Rayleigh Taylor instabilities studies  

SciTech Connect

In the context of the inertial confinement fusion, experiments have been carried out on the Phebus laser facility to study the Rayleigh-Taylor instabilities (RTIs) at the ablation front. Premodulated brominated plastic targets (25 {mu}m thick) with a modulation wavelength between 12 and 50 {mu}m were accelerated with a temporally shaped soft x-ray pulse emitted from a hohlraum with a maximum radiation temperature of about 115 eV. The RTI growth was measured by face-on radiography using a microscope coupled with an x-ray streak camera, which has spatial and temporal resolutions of about 5 {mu}m and 50 ps, respectively. The acceleration was derived from side-on velocity measurements. The microscope we have developed is a Wolter-like microscope which consists of two toroiedal mirrors. We will present the experimental and theoretical potentialities of this microscope: characterization with an x-ray generator and plasma laser x-ray source (Phebus facility) for two-dimensional (2D) and 1D time-resolved imaging studies. Spatial resolution of about 4 {mu}m was achieved in the 1-5 keV range. The Wolter-like constitutes an interesting device for laser plasma diagnostics and will be very useful in the Laser Megajoules experiments conducted with more powerful lasers.

Troussel, Ph.; Meyer, B.; Reverdin, R.; Angelier, B.; Lidove, G.; Salvatore, P.; Richard, A. [Commissariat a l'Energie Atomique, DAM-Ile de France, BP 12, 91680 Bruyeres-les-Chatel (France); Commissariat a l'Energie Atomique, Saclay 91191 (France); Commissariat a l'Energie Atomique, CESTA, BP2, 33114 Le Barp (France)

2005-06-15T23:59:59.000Z

55

HSQ double patterning process for 12 nm resolution x-ray zone plates  

DOE Green Energy (OSTI)

Soft x-ray zone plate microscopy is a powerful nano-analytic technique used for a wide variety of scientific and technological studies. Pushing its spatial resolution to 10 nm and below is highly desired and feasible due to the short wavelength of soft x-rays. Instruments using Fresnel zone plate lenses achieve a spatial resolution approximately equal to the smallest, outer most zone width. We developed a double patterning zone plate fabrication process based on a high-resolution resist, hydrogen silsesquioxane (HSQ), to bypass the limitations of conventional single exposure fabrication to pattern density, such as finite beam size, scattering in resist and modest intrinsic resist contrast. To fabricate HSQ structures with zone widths in the order of 10 nm on gold plating base, a surface conditioning process with (3-mercaptopropyl) trimethoxysilane, 3-MPT, is used, which forms a homogeneous hydroxylation surface on gold surface and provides good anchoring for the desired HSQ structures. Using the new HSQ double patterning process, coupled with an internally developed, sub-pixel alignment algorithm, we have successfully fabricated in-house gold zone plates of 12 nm outer zones. Promising results for 10 nm zone plates have also been obtained. With the 12 nm zone plates, we have achieved a resolution of 12 nm using the full-field soft x-ray microscope, XM-1.

Chao, Weilun; Kim, Jihoon; Rekawa, Senajith; Fischer, Peter; Anderson, Erik H.

2009-06-16T23:59:59.000Z

56

Regularized energy-dependent solar flare hard x-ray spectral index  

E-Print Network (OSTI)

The deduction from solar flare X-ray photon spectroscopic data of the energy dependent model-independent spectral index is considered as an inverse problem. Using the well developed regularization approach we analyze the energy dependency of spectral index for a high resolution energy spectrum provided by Ramaty High Energy Solar Spectroscopic Imager (RHESSI). The regularization technique produces much smoother derivatives while avoiding additional errors typical of finite differences. It is shown that observations imply a spectral index varying significantly with energy, in a way that also varies with time as the flare progresses. The implications of these findings are discussed in the solar flare context.

Eduard P. Kontar; Alexander L. MacKinnon

2005-06-05T23:59:59.000Z

57

Definition: X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) Jump to: navigation, search Dictionary.png X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) is a laboratory-based technique commonly used for identification of crystalline materials and analysis of unit cell dimensions. One of two primary types of XRD analysis (X-ray powder diffraction and single-crystal XRD) is commonly applied to samples to obtain specific information about the crystalline material under investigation. X-ray powder diffraction is widely used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline substances (typically in less than 20 minutes). A pure, finely ground, and homogenized sample is required for determination of the bulk composition. Additional uses include detailed

58

X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: X-Ray Diffraction (XRD) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Lab Analysis Techniques Exploration Sub Group: Rock Lab Analysis Parent Exploration Technique: Rock Lab Analysis Information Provided by Technique Lithology: Rapid and unambiguous identification of unknown minerals.[1] Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png X-Ray Diffraction (XRD): X-Ray Diffraction (XRD) is a laboratory-based technique commonly used for identification of crystalline materials and analysis of unit cell dimensions. One of two primary types of XRD analysis (X-ray powder diffraction and single-crystal XRD) is commonly applied to samples to

59

X-Ray Fluorescence (XRF) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Fluorescence (XRF) X-Ray Fluorescence (XRF) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: X-Ray Fluorescence (XRF) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Lab Analysis Techniques Exploration Sub Group: Rock Lab Analysis Parent Exploration Technique: Rock Lab Analysis Information Provided by Technique Lithology: Bulk and trace element analysis of rocks, minerals, and sediments. Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png X-Ray Fluorescence (XRF): X-Ray Fluorescence is a lab-based technique used for bulk chemical analysis of rock, mineral, sediment, and fluid samples. The technique depends on the fundamental principles of x-ray interactions with solid materials, similar

60

Portable X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

Portable X-Ray Diffraction (XRD) Portable X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: Portable X-Ray Diffraction (XRD) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Field Techniques Exploration Sub Group: Data Collection and Mapping Parent Exploration Technique: Data Collection and Mapping Information Provided by Technique Lithology: Rapid and unambiguous identification of unknown minerals.[1] Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png Portable X-Ray Diffraction (XRD): Portable X-Ray Diffraction (XRD) is a field-based technique that can be used for identification of crystalline materials and analysis of unit cell dimensions. Portable XRD analysis is similar to X-ray powder diffraction,

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

In situ X-ray Characterization of Energy Storage Materials |...  

NLE Websites -- All DOE Office Websites (Extended Search)

to accurately characterize the dynamic electrochemical processes at the nanometer and atomic level, we have employed a set of complementary, in situ X-ray characterization...

62

X-ray Tube with Magnetic Electron Steering - Energy ...  

The high average power large area X-ray tube provides ... Solar Photovoltaic; Solar ... Description This invention consists of a cathode and anode ...

63

High resolution x-ray and gamma ray imaging using diffraction lenses with mechanically bent crystals  

DOE Patents (OSTI)

A method for high spatial resolution imaging of a plurality of sources of x-ray and gamma-ray radiation is provided. High quality mechanically bent diffracting crystals of 0.1 mm radial width are used for focusing the radiation and directing the radiation to an array of detectors which is used for analyzing their addition to collect data as to the location of the source of radiation. A computer is used for converting the data to an image. The invention also provides for the use of a multi-component high resolution detector array and for narrow source and detector apertures.

Smither, Robert K. (Hinsdale, IL)

2008-12-23T23:59:59.000Z

64

THE NUCLEAR SPECTROSCOPIC TELESCOPE ARRAY (NuSTAR) HIGH-ENERGY X-RAY MISSION  

SciTech Connect

The Nuclear Spectroscopic Telescope Array (NuSTAR) mission, launched on 2012 June 13, is the first focusing high-energy X-ray telescope in orbit. NuSTAR operates in the band from 3 to 79 keV, extending the sensitivity of focusing far beyond the {approx}10 keV high-energy cutoff achieved by all previous X-ray satellites. The inherently low background associated with concentrating the X-ray light enables NuSTAR to probe the hard X-ray sky with a more than 100-fold improvement in sensitivity over the collimated or coded mask instruments that have operated in this bandpass. Using its unprecedented combination of sensitivity and spatial and spectral resolution, NuSTAR will pursue five primary scientific objectives: (1) probe obscured active galactic nucleus (AGN) activity out to the peak epoch of galaxy assembly in the universe (at z {approx}< 2) by surveying selected regions of the sky; (2) study the population of hard X-ray-emitting compact objects in the Galaxy by mapping the central regions of the Milky Way; (3) study the non-thermal radiation in young supernova remnants, both the hard X-ray continuum and the emission from the radioactive element {sup 44}Ti; (4) observe blazars contemporaneously with ground-based radio, optical, and TeV telescopes, as well as with Fermi and Swift, to constrain the structure of AGN jets; and (5) observe line and continuum emission from core-collapse supernovae in the Local Group, and from nearby Type Ia events, to constrain explosion models. During its baseline two-year mission, NuSTAR will also undertake a broad program of targeted observations. The observatory consists of two co-aligned grazing-incidence X-ray telescopes pointed at celestial targets by a three-axis stabilized spacecraft. Deployed into a 600 km, near-circular, 6 Degree-Sign inclination orbit, the observatory has now completed commissioning, and is performing consistent with pre-launch expectations. NuSTAR is now executing its primary science mission, and with an expected orbit lifetime of 10 yr, we anticipate proposing a guest investigator program, to begin in late 2014.

Harrison, Fiona A.; Cook, W. Rick; Forster, Karl; Grefenstette, Brian W.; Madsen, Kristin K.; Mao, Peter H.; Miyasaka, Hiromasa [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Craig, William W.; Pivovaroff, Michael J. [Lawrence Livermore National Laboratory, Livermore, CA 94550 (United States); Christensen, Finn E. [DTU Space, National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Hailey, Charles J.; Koglin, Jason E.; Mori, Kaya [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Zhang, William W. [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Boggs, Steven E. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Stern, Daniel; Kim, Yunjin [Jet Propulsion Laboratory, California Institute of Technology, Pasadena, CA 91109 (United States); Giommi, Paolo; Perri, Matteo [ASI Science Data Center, c/o ESRIN, via G. Galilei, I-00044 Frascati (Italy); Kitaguchi, Takao, E-mail: fiona@srl.caltech.edu [INAF-Osservatorio Astronomico di Roma, via di Frascati 33, I-00040 Monteporzio (Italy); and others

2013-06-20T23:59:59.000Z

65

High-resolution x-ray spectroscopy with the EBIT Calorimeter Spectrometer  

Science Conference Proceedings (OSTI)

The EBIT Calorimeter Spectrometer (ECS) is a production-class 36 pixel x-ray calorimeter spectrometer that has been continuously operating at the Electron Beam Ion Trap (EBIT) facility at Lawrence Livermore National Laboratory for almost 2 years. The ECS was designed to be a long-lifetime, turn-key spectrometer that couples high performance with ease of operation and minimal operator intervention. To this end, a variant of the Suzaku/XRS spaceflight detector system has been coupled to a low-maintenance cryogenic system consisting of a long-lifetime liquid He cryostat, and a closed cycle, {sup 3}He pre-cooled adiabatic demagnetization refrigerator. The ECS operates for almost 3 weeks between cryogenic servicing and the ADR operates at 0.05 K for more than 60 hours between automatic recycles under software control. Half of the ECS semiconductor detector array is populated with mid-band pixels that have a resolution of 4.5 eV FWHM, a bandpass from 0.05-12 keV, and a quantum efficiency of 95% at 6 keV. The other half of the array has thick HgTe absorbers that have a bandpass from 0.3 to over 100 keV, an energy resolution of 33 eV FWHM, and a quantum efficiency of 32% at 60 keV. In addition, the ECS uses a real-time, autonomous, data collection and analysis system developed for the Suzaku/XRS instrument and implemented in off-the-shelf hardware for the ECS. Here we will discuss the performance of the ECS instrument and its implementation as a turnkey cryogenic detector system.

Porter, F S; Adams, J S; Beiersdorfer, P; Brown, G V; Clementson, J; Frankel, M; Kahn, S M; Kelley, R L; Kilbourne, C A

2009-10-01T23:59:59.000Z

66

LM Completes X-Ray Film Digitization Project | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Completes X-Ray Film Digitization Project Completes X-Ray Film Digitization Project LM Completes X-Ray Film Digitization Project January 7, 2013 - 12:02pm Addthis Nearly 400,000 x-rays of former DOE contractor employees have been digitized to support LM records retention requirements. Nearly 400,000 x-rays of former DOE contractor employees have been digitized to support LM records retention requirements. What does this project do? Goal 2. Preserve, protect, and share records and information The U.S. Department of Energy (DOE) Office of Legacy Management (LM) has successfully completed a project to digitize nearly 400,000 medical x-rays of former DOE contractor employees. The x-rays, from the Rocky Flats and Grand Junction, Colorado; Fernald, Mound, and Ashtabula, Ohio; and Pinellas, Florida; sites, are needed to

67

Measurement Services for Low-to-Medium Energy X-rays  

Science Conference Proceedings (OSTI)

Development of measurement services to calibratewavelength-dispersive detectors and spectrometers for low- to medium-energy x rays (10 to 300 ...

2010-10-05T23:59:59.000Z

68

Definition: Portable X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

Definition Definition Edit with form History Facebook icon Twitter icon » Definition: Portable X-Ray Diffraction (XRD) Jump to: navigation, search Dictionary.png Portable X-Ray Diffraction (XRD) Portable X-Ray Diffraction (XRD) is a field-based technique that can be used for identification of crystalline materials and analysis of unit cell dimensions. Portable XRD analysis is similar to X-ray powder diffraction, which has traditionally been used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline substances. Portable XRD analysis allows for simpler sample preparation, faster analytical times than traditional methods (less than 2 minutes), and can be performed at the sampling site in the field. A pure, finely ground

69

High-resolution spectroscopic diagnostics of very high-temperature plasmas in the hard x-ray regime  

SciTech Connect

Motivated by the need for establishing a reliable database useful for the application of x-ray spectroscopic tools for the diagnostic of very high temperature plasmas, high-resolution crystal spectrometer measurements have been performed investigating the characteristic K-shell radiation of highly charged krypton and xenon. The measurements, which have been performed at the Electron-Beam-Ion-Trap (EBIT) facility of the Lawrence Livermore National Laboratory, include the investigation of the n = 2 {yields} 1 transitions in heliumlike krypton (Kr{sup 34+}) and innershell excited lithiumlike krypton (Kr{sup 33+}) utilizing a conventional reflection-type crystal spectrometer of von Hamos geometry. The electron-excitation-energy selective measurements map the contribution of the dielectronic recombination lines providing the means of accurate interpretation of the line profiles of the characteristic K{alpha} x-ray emission of plasmas. The high-resolution measurements of the n = 2 {yields} 1 transitions in heliumlike xenon (Xe{sup 52+}) and hydrogenlike xenon (Xe{sup 53+}) were based on a new transmission-type crystal spectrometer of DuMond geometry. The resolving power of the developed spectrometer was sufficient for charge state specific observation allowing the determination of the electron-impact excitation cross section for the hydrogen- and heliumlike K{alpha} transitions. The disagreement with theoretically predicted values is a measure of the magnitude of the Breit interaction for the highly charged high-Z ions.

Widmann, K

1999-12-06T23:59:59.000Z

70

High resolution biomedical imaging system with direct detection of x-rays via a charge coupled device  

DOE Patents (OSTI)

An imaging system is provided for direct detection of x-rays from an irradiated biological tissue. The imaging system includes an energy source for emitting x-rays toward the biological tissue and a charge coupled device (CCD) located immediately adjacent the biological tissue and arranged transverse to the direction of irradiation along which the x-rays travel. The CCD directly receives and detects the x-rays after passing through the biological tissue. The CCD is divided into a matrix of cells, each of which individually stores a count of x-rays directly detected by the cell. The imaging system further includes a pattern generator electrically coupled to the CCD for reading a count from each cell. A display device is provided for displaying an image representative of the count read by the pattern generator from the cells of the CCD.

Atac, Muzaffer (Wheaton, IL); McKay, Timothy A. (Ann Arbor, MI)

1998-01-01T23:59:59.000Z

71

TMX-upgrade. X-ray diagnostic: low-energy temperature determination  

Science Conference Proceedings (OSTI)

In order to properly design the x-ray filter set, a reasonable computational model of the plasma emission had to be developed. The radiation continuum computed consisted of two components: bremsstrahlung and recombination radiation. The contribution of line radiation from low Z impurities was estimated to be negligible for x-ray energies above 1 keV.

Jacoby, B.A.

1981-05-01T23:59:59.000Z

72

High Energy X-ray Diffraction Microscopy Microstructure Mapping  

Science Conference Proceedings (OSTI)

P1-04: 3D Microstructural Characterization of Uranium Oxide as a Surrogate Nuclear ... P1-15: Gating System Optimisation Design Study of a Cast Automobile ... P2-27: Characterization of Carbonate Rocks through X-ray Microtomography.

73

High-resolution bent-crystal spectrometer for the ultra-soft x-ray region  

SciTech Connect

A multichannel vacuum Brag-crystal spectrometer has been developed for high-resolution measurements of the line emission from tokamak plasmas in the wavelength region between 4 and 25 /angstrom/. The spectrometer employs a bent crystal in Johann geometry and a microchannel-plate intensified photodiode array. The instrument is capable of measuring high-resolution spectra (lambda/..delta..lambda approx. 3000) with fast time resolution (4 msec per spectrum) and good spatial resolution (3 cm). The spectral bandwidth is ..delta..lambda/lambda/sub 0/ = 8/angstrom/. A simple tilt mechanism allows access to different wavelength intervals. In order to illustrate the utility of the new spectrometer, time- and space-resolved measurements of the n = 3 to n = 2 spectrum of selenium from the Princeton Large Torus tokamak plasmas are presented. The data are used to determine the plasma transport parameters and to infer the radial distribution of fluorinelike, neonlike, and sodiumlike ions of selenium in the plasma. The new ultra-soft x-ray spectrometer has thus enabled us to demonstrate the utility of high-resolution L-shell spectroscopy of neonlike ions as a fusion diagnostic. 43 refs., 23 figs.

Beiersdorfer, P.; von Goeler, S.; Bitter, M.; Hill, K.W.; Hulse, R.A.; Walling, R.S.

1988-10-01T23:59:59.000Z

74

High-resolution Bent-crystal Spectrometer for the Ultra-soft X-ray Region  

DOE R&D Accomplishments (OSTI)

A multichannel vacuum Brag-crystal spectrometer has been developed for high-resolution measurements of the line emission from tokamak plasmas in the wavelength region between 4 and 25 angstrom. The spectrometer employs a bent crystal in Johann geometry and a microchannel-plate intensified photodiode array. The instrument is capable of measuring high-resolution spectra (lambda/..delta..lambda approx. 3000) with fast time resolution (4 msec per spectrum) and good spatial resolution (3 cm). The spectral bandwidth is ..delta..lambda/lambda{sub 0} = 8 angstrom. A simple tilt mechanism allows access to different wavelength intervals. In order to illustrate the utility of the new spectrometer, time- and space-resolved measurements of the n = 3 to n = 2 spectrum of selenium from the Princeton Large Torus tokamak plasmas are presented. The data are used to determine the plasma transport parameters and to infer the radial distribution of fluorinelike, neonlike, and sodiumlike ions of selenium in the plasma. The new ultra-soft x-ray spectrometer has thus enabled us to demonstrate the utility of high-resolution L-shell spectroscopy of neonlike ions as a fusion diagnostic.

Beiersdorfer, P.; von Goeler, S.; Bitter, M.; Hill, K. W.; Hulse, R. A.; Walling, R. S.

1988-10-00T23:59:59.000Z

75

Low-energy x-ray emission from magnetic-fusion plasmas  

SciTech Connect

Complex, transient, spatially inhomogeneous tokamak plasmas require careful diagnosis. As the reactor regime is approached, soft x rays become more important as a versatile diagnostic tool and an energy-loss mechanism. Continuum emission provides a measure of electron temperature and light impurity content. Impurity lines serve as a probe for ion and electron temperature, impurity behavior, and radiative cooling. The entire spectrum yields vital information on instabilities and disruptions. The importance of impurities is illustrated by the extensive efforts toward understanding impurity production, effects, and control. Minute heavy impurity concentrations can prevent reactor ignition. Si(Li) - detector arrays give a broad overview of continuum and line x-ray emission (.3 to 50 keV) with moderate energy (200 eV) and time (50 ms) resolution. Bragg crystal and grating spectrometers provide detailed information on impurity lines with moderate to excellent (E/..delta..E = 100 to 23,000) resolving power and 1 to 50 ms time resolution. Imaging detector arrays measure rapid (approx. 10 ..mu..s) fluctuations due to MHD instabilities and probe impurity behavior and radiative cooling. Future tokamaks require more diagnostic channels to avoid spatial scanning, higher throughput for fast, single-shot diagnosis, increased spectral information per sample period via fast scanning or use of multi-element detectors with dispersive elements, and radiation shielding and hardening of detectors.

Hill, K.W.; Bitter, M.; Eames, D.; von Goeler, S.; Goldman, M.; Sauthoff, N.R.; Silver, E.

1982-04-01T23:59:59.000Z

76

Low Dose Radiation Research Program: A Variable-Energy Soft X-Ray  

NLE Websites -- All DOE Office Websites (Extended Search)

A Variable-Energy Soft X-Ray Microprobe to Investigate Mechanisms of A Variable-Energy Soft X-Ray Microprobe to Investigate Mechanisms of the Radiation -Induced Bystander Effect. Authors: Melvyn Folkard, Borivoj Vojnovic, Giuseppe Schettino, Kirk Atkinson, Kevin M Prise, Barry D Michael Institutes: Gray Cancer Institute, PO Box 100, Mount Vernon Hospital, Northwood, HA6 2JR, UK For over a decade, the Gray Cancer Institute (GCI) has been actively engaged in the development and use of micro-irradiation techniques applied to radiobiological research. Our initial investigations made use of a charged-particle microbeam capable of irradiating individual cells with collimated energetic protons or 3He ions. By the end of the 1990's, a second facility had been constructed, which uses diffractive X-ray optics to focus ultrasoft X-rays to a sub-micron spot. The X-ray microprobe was

77

Low Dose Radiation Research Program: A Variable-Energy Soft X-Ray  

NLE Websites -- All DOE Office Websites (Extended Search)

A Variable-Energy Soft X-Ray Microprobe to Investigate Mechanisms of A Variable-Energy Soft X-Ray Microprobe to Investigate Mechanisms of the Radiation-Induced Bystander Effect. Authors: Melvyn Folkard, Borivoj Vojnovic, Giuseppe Schettino, Kirk Atkinson, Kevin M Prise, Barry D Michael Institutions: Gray Cancer Institute, PO BO Box100, Mount Vernon Hospital, Northwood, HA6 2JR, UK The Gray Cancer Institute (GCI) has pioneered the use of X-ray focussing techniques to develop systems for micro-irradiating individual cells and sub-cellular targets. Our prototype X-ray microprobe was developed alongside our existing charged-particle microbeam to address problems specific to low LET radiations, or where very precise targeting accuracy and dose delivery are required. This facility was optimised for focusing 278 eV CK X-rays; however there are a number of reasons for extending the

78

High-Resolution X-Ray and Light Beam Induced Current (LBIC) Measurements of Multcrystalline Silicon Solar Cells  

DOE Green Energy (OSTI)

High-resolution, spatially-resolved x-ray Laue patterns and high-resolution light beam induced current (LBIC) measurements are combined to study two multicrystalline solar cells made from the Heat Exchanger Method (HEM) and the Sting Ribbon Growth technique. The LBIC measurements were made at 4 different wavelengths (488, 633, 780, and 980 nm), resulting in penetration depths ranging from <1 {mu}m to >100 {mu}m. There is a strong correlation between the x-ray and LBIC measurements, showing that some twins and grain boundaries are effective in the reduction of local quantum efficiency, while others are benign.

Jellison Jr, Gerald Earle [ORNL; Budai, John D [ORNL; Bennett, Charlee J C [ORNL; Tischler, Jonathan Zachary [ORNL; Duty, Chad E [ORNL; Yelundur, V. [Georgia Institute of Technology; Rohatgi, A. [Georgia Institute of Technology

2010-01-01T23:59:59.000Z

79

High-energy x-ray response of photographic films: models and measurement  

SciTech Connect

A detailed characterization has been established for the new, high-sensitivity double-emulsion Kodak Direct Exposure Film (DEF). The experimental data base consisted of density-versus-exposure measurements that were duplicated at several laboratories for x radiations in the 1000-10,000-eV region. The absortpion and geometric properties of the film were determined, which, along with the density-exposure data, permitted the application of a relatively simple analytical model description for the optical density, D, as a function of the intensity, I (photons/..mu..m/sup 2/), the photon energy, E (eV), and the angle of incidence, 0, of the exposing radiation. A detailed table is presented for the I values corresponding to optical densities in the 0.2--2.0 range and to photon energies, E (eV), in the 1000-10,000-eV region. Experimentally derived conversion relations have been obtained that allow the density values to be expressed as either diffuse of specular. Also presented here is a similar characterization of the complementary, single-emulsion x-ray film, Kodak SB-5 (or 392). For the 1000-10,000-eV region this x-ray film is appreciably less sensitive but has higher resolution.

Henke, B.L.; Uejio, J.Y.; Stone, G.F.; Dittmore, C.H.; Fujiwara, F.G.

1986-11-01T23:59:59.000Z

80

High-Energy Synchrotron X-Ray Diffraction for In-Situ Study of ...  

Science Conference Proceedings (OSTI)

At the APS high-energy x-ray beamline 11-ID-C, we have employed 115 keV ... ( Use of the Advanced Photon Source was supported by the U. S. Department of...

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81

Low Dose Radiation Research Program: A Variable Energy Soft X-ray  

NLE Websites -- All DOE Office Websites (Extended Search)

Variable Energy Soft X-ray Microprobe to Investigate Mechanisms of the Variable Energy Soft X-ray Microprobe to Investigate Mechanisms of the Radiation-Induced Bystander Effect Melvyn Folkard Gray Cancer Institute Why This Project The aim of this project is to determine the effects of low radiation doses using a machine that makes it possible to radiate one cell at a time. Our soft X-ray microprobe can irradiate individual cells, or locations within cells with defined doses and with sub-micron precision. We can use low doses approaching that of a single electron track, which is of relevance to environmental level exposures. Much of our work is concentrating on irradiating specified individual cells within cell populations to identify "bystander responses" where non-radiated cells respond to signals from nearby radiated cells. Higher energy x-rays are being generated to extend

82

THE NEXT GENERATION ATLAS OF QUASAR SPECTRAL ENERGY DISTRIBUTIONS FROM RADIO TO X-RAYS  

SciTech Connect

We have produced the next generation of quasar spectral energy distributions (SEDs), essentially updating the work of Elvis et al. by using high-quality data obtained with several space- and ground-based telescopes, including NASA's Great Observatories. We present an atlas of SEDs of 85 optically bright, non-blazar quasars over the electromagnetic spectrum from radio to X-rays. The heterogeneous sample includes 27 radio-quiet and 58 radio-loud quasars. Most objects have quasi-simultaneous ultraviolet-optical spectroscopic data, supplemented with some far-ultraviolet spectra, and more than half also have Spitzer mid-infrared Infrared Spectrograph spectra. The X-ray spectral parameters are collected from the literature where available. The radio, far-infrared, and near-infrared photometric data are also obtained from either the literature or new observations. We construct composite SEDs for radio-loud and radio-quiet objects and compare these to those of Elvis et al., finding that ours have similar overall shapes, but our improved spectral resolution reveals more detailed features, especially in the mid- and near-infrared.

Shang Zhaohui; Li Jun; Xie Yanxia [Department of Physics, Tianjin Normal University, Tianjin 300387 (China); Brotherton, Michael S.; Cales, Sabrina L.; Dale, Daniel A.; Runnoe, Jessie C.; Kelly, Benjamin J. [Department of Physics and Astronomy, University of Wyoming, Laramie, WY 82071 (United States); Wills, Beverley J.; Wills, D. [Department of Astronomy, University of Texas at Austin, 1 University Station, C1400 Austin, TX 78712 (United States); Green, Richard F. [Large Binocular Telescope Observatory, University of Arizona, 933 North Cherry Avenue, Tucson, AZ 85721 (United States); Nemmen, Rodrigo S. [NASA/Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Gallagher, Sarah C. [Department of Physics and Astronomy, University of Western Ontario, London, ON N6A 3K7 (Canada); Ganguly, Rajib [Department of Computer Science, Engineering, and Physics, University of Michigan-Flint, 213 Murchie Science Building, 303 Kearsley Street, Flint, MI 48502 (United States); Hines, Dean C. [Space Science Institute, 4750 Walnut Street, Suite 205, Boulder, CO 80301 (United States); Kriss, Gerard A. [Space Telescope Science Institute, 3700 San Martin Drive, Baltimore, MD 21218 (United States); Tang, Baitian, E-mail: zshang@gmail.com [Department of Physics, 1245 Webster Hall, Washington State University, Pullman, WA 99164-2814 (United States)

2011-09-01T23:59:59.000Z

83

Low Dose Radiation Research Program: A Variable Energy Soft X-ray  

NLE Websites -- All DOE Office Websites (Extended Search)

Variable Energy Soft X-ray Microprobe to Investigate Mechanisms of Variable Energy Soft X-ray Microprobe to Investigate Mechanisms of the Radiation Induced Bystander Effect. Authors: Melvyn Folkard, Borivoj Vojnovic, Giuseppe Schettino, Kevin M Prise and Barry D Michael. Institutions: Gray Cancer Institute. We are currently engaged on two projects in the Low-dose Program: "Low dose studies with focused X-rays in cell and tissue models: mechanisms of bystander and genomic instability responses" (DE-FG07-99ER62877) and "Mechanistic modeling of bystander effects: An integrated theoretical and experimental approach" (DE-FG02-02ER63305). Central to both of these studies is a unique micro irradiation facility that uses ultrasoft X-rays focused to a sub micron beam for individual cell and sub cellular targeting. This facility allows us to selectively irradiate individual

84

A 1.5 A resolution X-ray structure of the catalytic module of Caldicellulosiruptor bescii family 3 pectate lyase  

NLE Websites -- All DOE Office Websites (Extended Search)

1498 1498 doi:10.1107/S1744309111038449 Acta Cryst. (2011). F67, 1498-1500 Acta Crystallographica Section F Structural Biology and Crystallization Communications ISSN 1744-3091 A 1.5 A ˚ resolution X-ray structure of the catalytic module of Caldicellulosiruptor bescii family 3 pectate lyase Markus Alahuhta, a Puja Chandrayan, b Irina Kataeva, b Michael W. W. Adams, b Michael E. Himmel a and Vladimir V. Lunin a * a BioSciences Center, National Renewable Energy Laboratory, 1617 Cole Boulevard, Golden, CO 80401, USA, and b Department of Biochemistry and Molecular Biology, University of Georgia, Athens, GA 30602-7229, USA Correspondence e-mail: vladimir.lunin@nrel.gov Received 17 August 2011 Accepted 19 September 2011 PDB Reference: family 3 pectate lyase catalytic module, 3t9g. A 1.5 A ˚ resolution X-ray structure of the catalytic module of Caldicellulosi- ruptor bescii

85

Multi-energy x-ray imaging and sensing for diagnostic and control of the burning plasma  

Science Conference Proceedings (OSTI)

New diagnostic and sensor designs are needed for future burning plasma (BP) fusion experiments, having good space and time resolution and capable of prolonged operation in the harsh BP environment. We evaluate the potential of multi-energy x-ray imaging with filtered detector arrays for BP diagnostic and control. Experimental studies show that this simple and robust technique enables measuring with good accuracy, speed, and spatial resolution the T{sub e} profile, impurity content, and MHD activity in a tokamak. Applied to the BP this diagnostic could also serve for non-magnetic sensing of the plasma position, centroid, ELM, and RWM instability. BP compatible x-ray sensors are proposed using 'optical array' or 'bi-cell' detectors.

Stutman, D.; Tritz, K.; Finkenthal, M. [Department of Physics and Astronomy, Johns Hopkins University, Baltimore, Maryland 21218 (United States)

2012-10-15T23:59:59.000Z

86

Edge-enhanced imaging obtained with very broad energy band x-rays  

SciTech Connect

We demonstrate both theoretically and experimentally that edge-enhancement effects are produced when objects, in contact with the x-ray detector, are imaged by using very broad x-ray spectra. Radiographs of thin Al objects have been obtained with a table-top synchrotron source which generates x-rays in the energy range from a few kilo-electron-volts up to 6 MeV. Edge-enhancement effects arise from the combination of x-ray absorption (kilo-electron-volt part of the spectrum) and secondary particle emission (mega-electron-volt part of the spectrum) within the sample. The exact contribution of absorption and emission profiles in the edge-enhanced images has been calculated via Monte Carlo simulation.

Taibi, A.; Cardarelli, P.; Di Domenico, G.; Marziani, M.; Gambaccini, M. [Department of Physics, University of Ferrara, INFN Section of Ferrara, via Saragat 1, 44100 Ferrara (Italy); Hanashima, T. [Photon Production Laboratory Ltd., 1-1-1 Nojihigashi, Kusatsu, Shiga 525-8577 (Japan); Yamada, H. [Synchrotron Light Life Science Center, Ritsumeikan University, 1-1-1 Nojihigashi, Kusatsu, Shiga 525-8577 (Japan)

2010-04-05T23:59:59.000Z

87

A high-resolution large-acceptance analyzer for X-ray fluorescence and Raman spectroscopy  

E-Print Network (OSTI)

E. Berman and Z. Yin, at the NSLS as well as Dr. H. Tompkinswhich was taken at the NSLS beamline X-25 shows a cleanwith soft X-rays. At the NSLS wiggler beamline X-25, we

Bergmann, Uwe; Cramer, Stephen P.

2001-01-01T23:59:59.000Z

88

Thin optic surface analysis for high resolution X-ray telescopes  

E-Print Network (OSTI)

The art of glass developed throughout the years has covered artifacts ranging from crude ornaments to high precision optics used in flat panel displays, hard disk drives, and x-ray telescopes. Methods for manufacturing ...

Akilian, Mireille

2004-01-01T23:59:59.000Z

89

Compensational scintillation detector with a flat energy response for flash X-ray measurements  

SciTech Connect

To measure the intensity of flash X-ray sources directly, a novel scintillation detector with a fast time response and flat energy response is developed by combining film scintillators of doped ZnO crystal and fast organic scintillator together. Through compensation design, the dual-scintillator detector (DSD) achieved a flat energy response to X-rays from tens of keV to several MeV, and sub-nanosecond time response by coupling to ultrafast photo-electronic devices. A prototype detector was fabricated according to the theoretical design; it employed ZnO:In and EJ228 with thicknesses of 0.3 mm and 0.1 mm, respectively. The energy response of this detector was tested on monoenergetic X-ray and {gamma}-ray sources. The detector performs very well with a sensitivity fluctuation below 5% for 8 discrete energy points within the 40-250 keV energy region and for other energies of 662 keV and 1.25 MeV as well, showing good accordance with the theoretical design. Additionally, the detector works properly for the application to the flash X-ray radiation field absolute intensity measurement. This DSD may be very useful for the diagnosis of time-resolved dynamic physical processes of flash X-ray sources without knowing the exact energy spectrum.

Chen Liang; Quan Lin; Zhang Zhongbing [Radiation Detection Research Center, Northwest Institute of Nuclear Technology, P.O. Box 69-9, Xi'an, Shaanxi 710024 (China); Ouyang Xiaoping [Radiation Detection Research Center, Northwest Institute of Nuclear Technology, P.O. Box 69-9, Xi'an, Shaanxi 710024 (China); School of Nuclear Science and Engineering, North China Electric Power University, Beijing 102206 (China); Department of Engineering Physics, Tsinghua University, Beijing 100084 (China); Liu Bin [School of Nuclear Science and Engineering, North China Electric Power University, Beijing 102206 (China); Liu Jinliang [Radiation Detection Research Center, Northwest Institute of Nuclear Technology, P.O. Box 69-9, Xi'an, Shaanxi 710024 (China); Department of Engineering Physics, Tsinghua University, Beijing 100084 (China)

2013-01-15T23:59:59.000Z

90

Plasma Diagnostic Calibration and Characterizations with High Energy X-rays  

SciTech Connect

National Security Technologies High Energy X-ray (HEX) Facility is unique in the U.S. Department of Energy complex. The HEX provides fluorescent X-rays of 5 keV to 100 keV with fluence of 10^510^6 photons/cm^2/second at the desired line energy. Low energy lines can be filtered, and both filters and fluorescers can be changed rapidly. We present results of calibrating image plates (sensitivity and modulation transfer function), a Bremsstrahlung spectrometer (stacked filters and image plates), and the National Ignition Facilitys Filter- Fluorescer Experiment (FFLEX) high energy X-ray spectrometer. We also show results of a scintillator light yield and alignment study for a neutron imaging system.

Zaheer Ali

2009-06-05T23:59:59.000Z

91

High Energy X-Ray Diffraction Microscopy Tracking of Internal ...  

Science Conference Proceedings (OSTI)

Measurements are carried out at the Advanced Photon Source; analysis uses high performance computing to extract micron scale resolution structures spanning...

92

In situ X-ray Characterization of Energy Storage Materials | Stanford  

NLE Websites -- All DOE Office Websites (Extended Search)

X-ray Characterization of Energy Storage Materials X-ray Characterization of Energy Storage Materials Tuesday, July 9, 2013 - 11:00am SLAC, Conference Room 137-322 Presented by Johanna Nelson, Stanford Postdoctoral Scholar, SSRL MSD Hard X-ray Department A key factor in the global move towards clean, renewable energy is the electrification of the automobile. Current battery technology limits EV (electric vehicles) to a short travel range, slow recharge, and costly price tag. Li-ion batteries promise the high specific capacity required for EVs to travel 300+ miles on a single charge with a number of possible earth abundant anode and cathode materials; however, set backs such as capacity fading hinder the full capability of these rechargeable batteries. In order to accurately characterize the dynamic electrochemical processes at the

93

Spectral resolution for a five-element, filtered, x-ray detector array using the method of Backus and Gilbert  

Science Conference Proceedings (OSTI)

The generalized method of Backus and Gilbert (BG) is described and applied to the inverse problem of obtaining the spectrum from a five-channel, filtered array of x-ray detectors. This diagnostic is routinely fielded on the Z facility at Sandia National Laboratories to study soft x-ray photons ({approx}100-2300 eV), emitted by high density Z-pinch plasmas. The BG method defines spectral resolution limits on the system of response functions that are in good agreement with a classical unfold method, based on a histogram representation of the source spectrum. The resolution so defined is independent of the source spectrum. For noise-free, simulated data the BG approximating function is also in reasonable agreement with the source spectrum (150 eV blackbody) and the unfolded spectrum. This function may be used as an initial trial function for iterative methods or a regularization model.(c) 2000 American Institute of Physics. (c)

Fehl, D. L. [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States)] [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States); Biggs, F. [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States)] [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States); Chandler, G. A. [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States)] [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States); Stygar, W. A. [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States)] [Sandia National Laboratories, Albuquerque, New Mexico 87185-1196 (United States)

2000-08-01T23:59:59.000Z

94

Spectral Resolution for Five-Element, Filtered, X-Ray Detector (XRD) Arrays Using the Methods of Backus and Gilbert  

SciTech Connect

The generalized method of Backus and Gilbert (BG) is described and applied to the inverse problem of obtaining spectra from a 5-channel, filtered array of x-ray detectors (XRD's). This diagnostic is routinely fielded on the Z facility at Sandia National Laboratories to study soft x-ray photons ({le}2300 eV), emitted by high density Z-pinch plasmas. The BG method defines spectral resolution limits on the system of response functions that are in good agreement with the unfold method currently in use. The resolution so defined is independent of the source spectrum. For noise-free, simulated data the BG approximating function is also in reasonable agreement with the source spectrum (150 eV black-body) and the unfold. This function may be used as an initial trial function for iterative methods or a regularization model.

FEHL,DAVID LEE; BIGGS,F.; CHANDLER,GORDON A.; STYGAR,WILLIAM A.

2000-01-17T23:59:59.000Z

95

High Spectral Resolution X-ray Observation of Magnetic CVs: EX Hya  

SciTech Connect

In magnetic cataclysmic variables (CVs) the primary is a highly magnetized white dwarf (WD) whose field controls the accretion flow close to the WD, leading to a shock and accretion column that radiate chiefly in X-rays. We present preliminary results from a 500 ks Chandra HETG observation of the brightest magnetic CV EX Hya. From the observational dataset we are able to measure the temperature and density at different points of the cooling accretion column using sensitive line ratios. We also construct line-based light curves to search for rotational modulation of the X-ray emission.

Luna, G; Brickhouse, N S; Mauche, C W

2008-04-07T23:59:59.000Z

96

An energy dispersive x-ray absorption spectroscopy beamline, X6A, at NSLS  

Science Conference Proceedings (OSTI)

An energy dispersive x-ray absorption spectroscopy instrument has been built at the X6A beam port of the x-ray ring at the National Synchrotron Light Source (NSLS). This instrument allows the collection of extended x-ray-absorption fine structure and/or x-ray absorption near-edge structure spectra for many elements on the millisecond time scale. The beamline employs a four-point crystal bender and a rectangular Si 220 crystal to access incident energies between 6.5 and 21 keV. Because the polychromator focuses the synchrotron beam to a narrow 100-[mu]m line, this experimental apparatus is ideal for x-ray absorption spectroscopy experiments in special environments such as at high pressures, for [ital in] [ital situ] experiments, and/or for very small samples. In this manuscript we will describe the instrument design and present data with which to evaluate the instrument. This beamline is available through the NSLS user proposal system.

Lee, P.L.; Beno, M.A.; Jennings, G.; Ramanathan, M.; Knapp, G.S.; Huang, K. (Materials Science Division, Argonne National Laboratory, Argonne, Illinois 60439 (United States)); Bai, J. (Materials Science Division, Argonne National Laboratory, Argonne, Illinois 60439 (United States) Department of Physics, Brooklyn College of CUNY, Brooklyn, New York 11210 (United States)); Montano, P.A. (Materials Science Division, Argonne National Laboratory, Argonne, Illinois 60439 (United States) Department of Physics, University of Illinois, Chicago, Chicago, Illinois 60680 (United States))

1994-01-01T23:59:59.000Z

97

Quantitative discrimination between geological materials with variable density contrast by high resolution X-ray computed tomography: An example using amygdule size-distribution in ancient lava flows  

Science Conference Proceedings (OSTI)

The bubble-size distribution in 2.7 billion year old lava flows can be used as a proof of concept illustrating a new set of techniques for measuring volumes of geological materials with variable density contrasts using high-resolution X-ray computed ... Keywords: Amygdules, Bootstrap resampling, Bubble-size distribution, Central limit theorem, Dynamic thresholding, X-ray tomography

Sanjoy M. Som, James W. Hagadorn, Weston A. Thelen, Alan R. Gillespie, David C. Catling, Roger Buick

2013-04-01T23:59:59.000Z

98

X-ray Transtion Energies Database - Theoretical Trans. ...  

Science Conference Proceedings (OSTI)

... are used to generate the theory portion of ... in the calculation minimizes the energy (with relativistic ... must be done with proper nuclear charge models ...

99

Design of a triaxial residual stress measurement system using high energy x-ray diffraction  

Science Conference Proceedings (OSTI)

Previous design studies in developing concepts for residual stress measurement in engineering materials have been extended. A pre-prototype energy dispersive x-ray diffraction (EDXRD) system has been fabricated. A 300 kV radiography source is used in conjunction with an intrinsic germanium detector and a MacII/LabVIEW data acquisition system. Specimens up to 25mm equivalent steel thickness (and one meter gross dimensions) can now be evaluated. The pre-prototype system serves as the hard x-ray, bulk stress measurement component of the previously reported hybrid stress measuring system (which would include a traditional multi-angle surface measurement system using soft x-rays). In addition, a detailed study of residual stress analytical equations has been completed and applied to various metallic and ceramic materials. During the grant period, related studies were completed on stress measurement using synchrotron radiation and on a critical review of the residual stress literature. 6 refs., 3 figs.

Shackelford, J.F.; Brown, B.D.; Park, J.S.

1989-01-01T23:59:59.000Z

100

Thermal Acoustic Sensor for High Pulse Energy X-ray FEL Beams  

SciTech Connect

The pulse energy density of X-ray FELs will saturate or destroy conventional X-ray diagnostics, and the use of large beam attenuation will result in a beam that is dominated by harmonics. We present preliminary results at the LCLS from a pulse energy detector based on the thermal acoustic effect. In this type of detector an X-ray resistant material (boron carbide in this system) intercepts the beam. The pulse heating of the target material produces an acoustic pulse that can be detected with high frequency microphones to produce a signal that is linear in the absorbed energy. The thermal acoustic detector is designed to provide first- and second-order calorimetric measurement of X-ray FEL pulse energy. The first-order calorimetry is a direct temperature measurement of a target designed to absorb all or most of the FEL pulse power with minimal heat leak. The second-order measurement detects the vibration caused by the rapid thermoelastic expansion of the target material each time it absorbs a photon pulse. Both the temperature change and the amplitude of the acoustic signal are directly related to the photon pulse energy.

Smith, T.J.; Frisch, J.C.; Kraft, E.M.; Loos, J.; /SLAC; Bentsen, G.S.; /Rochester U.

2011-12-13T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
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101

Quick-scanning x-ray absorption spectroscopy system with a servo-motor-driven channel-cut monochromator with a temporal resolution of 10 ms  

SciTech Connect

We have developed a quick-scanning x-ray absorption fine structure (QXAFS) system and installed it at the recently constructed synchrotron radiation beamline BL33XU at the SPring-8. Rapid acquisition of high-quality QXAFS data was realized by combining a servo-motor-driven Si channel-cut monochromator with a tapered undulator. Two tandemly aligned monochromators with channel-cut Si(111) and Si(220) crystals covered energy ranges of 4.0-28.2 keV and 6.6-46.0 keV, respectively. The system allows the users to adjust instantly the energy ranges of scans, the starting angles of oscillations, and the frequencies. The channel-cut crystals are cooled with liquid nitrogen to enable them to withstand the high heat load from the undulator radiation. Deformation of the reflecting planes is reduced by clamping each crystal with two cooling blocks. Performance tests at the Cu K-edge demonstrated sufficiently high data quality for x-ray absorption near-edge structure and extended x-ray absorption fine-structure analyses with temporal resolutions of up to 10 and 25 ms, respectively.

Nonaka, T.; Dohmae, K.; Araki, T.; Hayashi, Y.; Hirose, Y. [Toyota Central R and D Labs., Inc., Nagakute, Aichi 480-1192 (Japan); Uruga, T.; Yamazaki, H.; Tanida, H.; Goto, S. [JASRI/Spring-8, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan); Mochizuki, T. [JASRI/Spring-8, 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan); Toyama Corp., Zama, Kanagawa 228-0003 (Japan)

2012-08-15T23:59:59.000Z

102

Filter-fluorescer measurement of low-voltage simulator x-ray energy spectra  

SciTech Connect

X-ray energy spectra of the Maxwell Laboratories MBS and Physics International Pulserad 737 were measured using an eight-channel filter-fluorescer array. The PHOSCAT computer code was used to calculate channel response functions, and the UFO code to unfold spectrum.

Baldwin, G.T.; Craven, R.E.

1986-01-01T23:59:59.000Z

103

Resonant x-ray emission spectroscopy of liquid water: novel instrumentation, high resolution, and the"map" approach  

DOE Green Energy (OSTI)

Techniques to study the electronic structure of liquids are rare. Most recently, resonant x-ray emission spectroscopy (XES) has been shown to be an extremely versatile spectroscopy to study both occupied and unoccupied electronic states for liquids in thermodynamic equilibrium. However, XES requires high-brilliance soft x-ray synchrotron radiation and poses significant technical challenges to maintain a liquid sample in an ultra-high vacuum environment. Our group has therefore developed and constructed a novel experimental setup for the study of liquids, with the long-term goal of investigating the electronic structure of biological systems in aqueous environments. We have developed a flow-through liquid cell in which the liquid is separated from vacuum by a thin Si3N4 or SiC window and which allows a precise control of temperature. This approach has significant advantages compared to static liquids cells used in the past. Furthermore, we have designed a dedicated high-transmission, high-resolution soft x-ray spectrometer. The high transmission makes it possible to measure complete resonant XES"maps" in less than an hour, giving unprecedented detailed insight into the electronic structure of the investigated sample. Using this new equipment we have investigated the electronic structure of liquid water. Furthermore, our XES spectra and maps give information about ultra-fast dissociation on the timescale of the O 1s core hole lifetime, which is strongly affected by the initial state hydrogen bonding configuration.

Weinhardt, L.; Fuchs, O.; Blum, M.; Br, M.; Weigand, M.; Denlinger, J.D.; Zubavichus, Y.; Zharnikov, M.; Grunze, M.; Heske, C.; Umbach, E.

2008-06-17T23:59:59.000Z

104

X-ray Microscopy and Imaging: 2-BM  

NLE Websites -- All DOE Office Websites (Extended Search)

BM BM Introduction The 2-BM beamline offers measurement capabilities for x-ray microtomography, x-ray topography and x-ray microdiffraction. X-ray microtomography and x-ray diffraction instruments are installed on separate optical tables for independent operation with fast switch over time. Optically-coupled high-resolution CCD system is used for microtomography and topography with up to 1 micron spatial resolution. X-ray microdiffraction setup consists of KB microfocussing mirrors (~3 micron minimum spot), four-circle Huber diffractometer, high-precision translation sample stage, two orthogonally-mounted video cameras for viewing sample, fluorescence detector (Si-drift diode) and diffraction detector (a scintillation detector or a CCD). Three different levels of monochromaticity are available. Conventional monochromatic x-rays from a double-bounced Si (111) crystal monochromator (DCM, D E/E=1E-4), wide band-pass monochromatic x-rays from a double multilayer monochromator (DMM, D E/E=1~4E-2) and pink beam. The available x-ray range is from 5 keV to 30 keV. The lower limit is due to the x-ray windows and the upper limit is due to the critical angle of the x-ray mirror. Two different coatings (Cr and Pt) for the x-ray mirror allow either 20 keV or 30 keV energy cutoff.

105

Critical-angle transmission grating spectrometer for high-resolution soft x-ray spectroscopy on the International X-ray Observatory  

E-Print Network (OSTI)

High-resolution spectroscopy at energies below 1 keV covers the lines of C, N, O, Ne and Fe ions, and is central to studies of the Interstellar Medium, the Warm Hot Intergalactic Medium, warm absorption and outflows in ...

Heilmann, Ralf K.

106

A High-Speed FPGA-Based Lossless Data Compression Design for the X-ray Spectrometer Solar Energy Spectra  

Science Conference Proceedings (OSTI)

In order to meet the real-time compression requirements effectively for the solar energy spectrum data of the X-ray spectrometer used as a key payload of Chang'E Mission, the design and implementation of the bit wise OR algorithm based on FPGA is presented ... Keywords: data compression, X-ray spectrometer, bitwise OR algorithm, FPGA

RuiMin Ma; HuanYu Wang

2011-09-01T23:59:59.000Z

107

High-Energy X-ray Studies of Real Materials Under Real Conditions and in Real Time  

SciTech Connect

High-energy x-rays from 3rd generation synchrotron sources, including the APS, possess a unique combination of high penetration power and high spatial, reciprocal space, and temporal resolution. These characteristics can be exploited to non-destructively measure phase, texture and strain distributions under extreme environments including thermo-mechanical loading, high-pressure, irradiation and supercritical environments. Over the past several years, the 1-ID beamline has developed a number of programs for these purposes, namely (i) high-energy diffraction microscopy, in which grain and sub-grain volumes are mapped in polycrystalline aggregates, and (ii) combined small-and wide-angle x-ray scattering which permits information over a broad range of length scales to be collected from the same (micron-level) volume. These programs have been increasingly used to test and extend predictive simulations of materials behavior over size scales ranging from nm to mm. Select studies will be presented including nucleation and growth of nanomaterials, void and structural evolution in complex composites under thermo-mechanical and irradiated environments, and microstructural changes in layered systems including thermal-barrier coatings, batteries and fuel cells. Finally, extension of these programs, through the planned APS upgrade, to higher spatio-temporal resolution will be described.

Almer, Jonathan (ANL)

2011-05-11T23:59:59.000Z

108

X-Ray Energy Responses of Silicon Tomography Detectors Irradiated with Fusion Produced Neutrons  

Science Conference Proceedings (OSTI)

In order to clarify the effects of fusion-produced neutron irradiation on silicon semiconductor x-ray detectors, the x-ray energy responses of both n- and p-type silicon tomography detectors used in the Joint European Torus (JET) tokamak (n-type) and the GAMMA 10 tandem mirror (p-type) are studied using synchrotron radiation at the Photon Factory of the National Laboratory for High Energy Accelerator Research Organization (KEK). The fusion neutronics source (FNS) of Japan Atomic Energy Research Institute (JAERI) is employed as well-calibrated D-T neutron source with fluences from 10{sup 13} to 10{sup 15} neutrons/cm{sup 2} onto these semiconductor detectors. Different fluence dependence is found between these two types of detectors; that is, (i) for the n-type detector, the recovery of the degraded response is found after the neutron exposure beyond around 10{sup 13} neutrons/cm{sup 2} onto the detector. A further finding is followed as a 're-degradation' by a neutron irradiation level over about 10{sup 14} neutrons/cm{sup 2}. On the other hand, (ii) the energy response of the p-type detector shows only a gradual decrease with increasing neutron fluences. These properties are interpreted by our proposed theory on semiconductor x-ray responses in terms of the effects of neutrons on the effective doping concentration and the diffusion length of a semiconductor detector.

Kohagura, J. [Plasma Research Centre, University of Tsukuba (Japan); Cho, T. [Plasma Research Centre, University of Tsukuba (Japan); Hirata, M. [Plasma Research Centre, University of Tsukuba (Japan); Numakura, T. [Plasma Research Centre, University of Tsukuba (Japan); Yokoyama, N. [Plasma Research Centre, University of Tsukuba (Japan); Fukai, T. [Plasma Research Centre, University of Tsukuba (Japan); Tomii, Y. [Plasma Research Centre, University of Tsukuba (Japan); Tokioka, S. [Plasma Research Centre, University of Tsukuba (Japan); Miyake, Y. [Plasma Research Centre, University of Tsukuba (Japan); Kiminami, S. [Plasma Research Centre, University of Tsukuba (Japan); Shimizu, K. [Plasma Research Centre, University of Tsukuba (Japan); Miyoshi, S. [Plasma Research Centre, University of Tsukuba (Japan); Hirano, K. [High Energy Accelerator Research Organization (Japan); Yoshida, M. [Japan Atomic Energy Research Institute (Japan); Yamauchi, M. [Japan Atomic Energy Research Institute (Japan); Kondoh, T. [Japan Atomic Energy Research Institute (Japan); Nishitani, T. [Japan Atomic Energy Research Institute (Japan)

2005-01-15T23:59:59.000Z

109

High-energy X-rays shine light on mystery of Picasso's paints | Argonne  

NLE Websites -- All DOE Office Websites (Extended Search)

energy X-rays shine light on mystery of Picasso's paints energy X-rays shine light on mystery of Picasso's paints By Tona Kunz * February 6, 2013 Tweet EmailPrint LEMONT, Ill. - The Art Institute of Chicago teamed up with Argonne National Laboratory to help unravel a decades-long debate among art scholars about what kind of paint Picasso used to create his masterpieces. The results published last month in the journal Applied Physics A: Materials Science & Processing add significant weight to the widely held theory that Picasso was one of the first master painters to use common house paint rather than traditional artists' paint. That switch in painting material gave birth to a new style of art marked by canvasses covered in glossy images with marbling, muted edges, and occasional errant paint drips, but devoid of brush marks. Fast-drying enamel house paint enabled

110

High-Energy X-ray Diffraction Study of Internal Stresses in Metal Matrix  

NLE Websites -- All DOE Office Websites (Extended Search)

High-Energy X-ray Diffraction Study of Internal Stresses in Metal Matrix High-Energy X-ray Diffraction Study of Internal Stresses in Metal Matrix Composites Metal matrix composites (MMCs) comprise an intriguing new class of materials coming to prominence in the aerospace, electronics, and automotive industries. Internal stresses play an important role in the behavior and successful application of MMCs and multi-phase alloys. These stresses form during processing and service due to transformation or thermal expansion mismatch, as well as elastic and plastic mismatch during deformation. In order to develop a deeper understanding of the thermo-mechanical behavior of these materials, it is of key interest to examine the development of mean stresses in the phases of the composite as a function of time upon changes of temperature and/or external load.

111

3-D Measurement of Deformation Microstructure of Al(0.2%)Mg Using Submicron Resolution White X-Ray Microbeams  

SciTech Connect

We have used submicron-resolution white x-ray microbeams on the MHATT-CAT beamline 7-ID at the Advanced Photon Source to develop techniques for three-dimensional investigation of the deformation microstructure in a 20% plane strain compressed Al(0.2%)Mg tri-crystal. Kirkpatrick-Baez mirrors were used to focus white radiation from an undulator to a 0.7 x 0.7 {micro}m{sup 2} beam that was scanned over bi- and tri-crystal regions near the triple-junction of the tri-crystal. Depth resolution along the x-ray microbeam of less than 5 microns was achieved by triangulation to the diffractibn source point using images taken at a series of CCD distances from the microbeam. Computer indexing of the deformation cell structure in the bi-crystal region provided orientations of individual subgrains to {approximately}0.01 degrees, making possible detailed measurements of the rotation axes between individual cells.

Larson, B.C.; tamura, N.; Chung, J.-S.; Ice, G.E.; Budai, J.D.; Tischler, J.Z.; Yang, W.; Weiland, H.; Lowe, W.P.

1999-11-29T23:59:59.000Z

112

Back-scattering channel-cut high-resolution monochromator for inelastic x-ray scattering  

SciTech Connect

We report on a design and on some experimental results for the performance of a new high energy resolution monochromator. It is a large channel-cut Si crystal with a 197 mm separation between the two faces designed to operate in a near-backscattering regime. The device was tested as a second monochromator on Sector 3 of the Synchrotron Radiation Instrumentation Collaborative Access Team (SRI-CAT) at the Advanced Photon Source using the Si(777) reflection at a photon energy of 13.84 keV. The same monochromator can be used for other energies with reflections of the type (hhh). Special care has been taken to equalize the temperature of the two faces by employing a Peltier heat pump. A Si(111) double-crystal pre-monochromator designed to withstand the high heat load of the undulator radiation was used upstream on the beamline. The measured throughput efficiency of the Si(777) channel-cut monochromator was less ideal by a factor of 1.9. Dynamical diffraction theory was used to calculate the throughput of an ideally perfect crystal.

Kushnir, V.I.; Abbamonte, P.M.; Macrander, A.T.; Schwoerer-Boehning, M.

1997-08-01T23:59:59.000Z

113

'Optical' soft x-ray arrays for fluctuation diagnostics in magnetic fusion energy experiments  

Science Conference Proceedings (OSTI)

We are developing large pixel count, fast ({>=}100 kHz) and continuously sampling soft x-ray (SXR) array for the diagnosis of magnetohydrodynamics (MHD) and turbulent fluctuations in magnetic fusion energy plasmas. The arrays are based on efficient scintillators, high thoughput multiclad fiber optics, and multichannel light amplification and integration. Compared to conventional x-ray diode arrays, such systems can provide vastly increased spatial coverage, and access to difficult locations with small neutron noise and damage. An eight-channel array has been built using columnar CsI:Tl as an SXR converter and a multianode photomultiplier tube as photoamplifier. The overall system efficiency is measured using laboratory SXR sources, while the time response and signal-to-noise performance have been evaluated by recording MHD activity from the spherical tori (ST) Current Drive Experiment-Upgrade and National Spherical Torus Experiment, both at Princeton Plasma Physics Laboratory.

Delgado-Aparicio, L.F.; Stutman, D.; Tritz, K.; Finkenthal, M.; Kaita, R.; Roquemore, L.; Johnson, D.; Majeski, R. [Johns Hopkins University, Department of Physics and Astronomy, Plasma Spectroscopy Group, Bloomberg Center 3400 N. Charles Street, Baltimore, Maryland 21218 (United States); Princeton University Plasma Physics Laboratory, P. O. Box 451, Princeton, New Jersey 08543 (United States)

2004-10-01T23:59:59.000Z

114

Review on Active Galactic Nuclei at hard X-ray energies  

E-Print Network (OSTI)

Hard X-ray surveys are an important tool for the study of active galactic nuclei (AGN): they provide almost an unbiased view of absorption in the extragalactic population, allow the study of spectral features such as reflection and high energy cut-off which would otherwise be unexplored and favour the discovery of some blazars at high redshift. Here, we present the absorption properties of a large sample of INTEGRAL detected AGN, including an update on the fraction of Compton thick objects. For a sub-sample of 87 sources, which represent a complete set of bright AGN, we will discuss the hard X-ray (20-100 keV) spectral properties, also in conjunction with Swift/BAT 58 month data, providing information on BAT/IBIS cross-calibration constant, average spectral shape and spectral complexity. For this complete sample, we will also present broad-band data using soft X-ray observations, in order to explore the complexity of AGN spectra both at low and high energies and to highlight the variety of shapes. Future pros...

Bassani, Loredana; Malizia, A; Panessa, F; Landi, R; Bazzano, A; Ubertini, P; Bird, A J; Stephen, J B

2013-01-01T23:59:59.000Z

115

DIFFUSE HARD X-RAY EMISSION IN STARBURST GALAXIES AS SYNCHROTRON FROM VERY HIGH ENERGY ELECTRONS  

SciTech Connect

The origin of the diffuse hard X-ray (2-10 keV) emission from starburst galaxies is a long-standing problem. We suggest that synchrotron emission of 10-100 TeV electrons and positrons (e {sup {+-}}) can contribute to this emission, because starbursts have strong magnetic fields. We consider three sources of e {sup {+-}} at these energies: (1) primary electrons directly accelerated by supernova remnants, (2) pionic secondary e {sup {+-}} created by inelastic collisions between cosmic ray (CR) protons and gas nuclei in the dense interstellar medium of starbursts, and (3) pair e {sup {+-}} produced between the interactions between 10 and 100 TeV {gamma}-rays and the intense far-infrared (FIR) radiation fields of starbursts. We create one-zone steady-state models of the CR population in the Galactic center (R {<=} 112 pc), NGC 253, M82, and Arp 220's nuclei, assuming a power-law injection spectrum for electrons and protons. We consider different injection spectral slopes, magnetic field strengths, CR acceleration efficiencies, and diffusive escape times, and include advective escape, radiative cooling processes, and secondary and pair e {sup {+-}}. We compare these models to extant radio and GeV and TeV {gamma}-ray data for these starbursts, and calculate the diffuse synchrotron X-ray and inverse Compton (IC) luminosities of these starbursts in the models which satisfy multiwavelength constraints. If the primary electron spectrum extends to {approx}PeV energies and has a proton/electron injection ratio similar to the Galactic value, we find that synchrotron emission contributes 2%-20% of their unresolved, diffuse hard X-ray emission. However, there is great uncertainty in this conclusion because of the limited information on the CR electron spectrum at these high energies. IC emission is likewise a minority of the unresolved X-ray emission in these starbursts, from 0.1% in the Galactic center to 10% in Arp 220's nuclei, with the main uncertainty being the starbursts' magnetic field. We also model generic starbursts, including submillimeter galaxies, in the context of the FIR-X-ray relation, finding that anywhere between 0% and 16% of the total hard X-ray emission is synchrotron for different parameters, and up to 2% in the densest starbursts assuming an E {sup -2.2} injection spectrum and a diffusive escape time of 10 Myr (E/3 GeV){sup -1/2} (h/100 pc). Neutrino observations by IceCube and TeV {gamma}-ray data from HESS, VERITAS, and CTA can further constrain the synchrotron X-ray emission of starbursts. Our models do not constrain the possibility of hard, second components of primary e {sup {+-}} from sources like pulsars in starbursts, which could enhance the synchrotron X-ray emission further.

Lacki, Brian C. [Institute for Advanced Study, Princeton, NJ 08540 (United States)] [Institute for Advanced Study, Princeton, NJ 08540 (United States); Thompson, Todd A. [Department of Astronomy, The Ohio State University, Columbus, OH 43210 (United States)] [Department of Astronomy, The Ohio State University, Columbus, OH 43210 (United States)

2013-01-01T23:59:59.000Z

116

Photon Sciences | Beamlines | IXS: Inelastic X-ray Scattering  

NLE Websites -- All DOE Office Websites (Extended Search)

IXS: Inelastic X-ray Scattering IXS: Inelastic X-ray Scattering Poster | Fact Sheet | Preliminary Design Report Scientific Scope Many hot topics related to the high frequency dynamics of condensed matter require both a narrower and steeper resolution function and access to a broader dynamic range than what are currently available. This represents a sort of "no man's land" that falls right in the dynamic gap lying between the high frequency spectroscopies, such as inelastic x-ray scattering (IXS), and the low frequency ones. New IXS spectrometers with improved energy and momentum resolutions would be required to fill this gap. To achieve this goal, a new x-ray optics concept for both the monochromatization and energy analysis of x-rays will be implemented at the NSLS-II Inelastic X-ray Scattering beamline. This solution exploits the

117

The Discovery of Broad P Cygni X-ray Lines from Circinus X-1 with the Chandra High Energy Transmission Grating Spectrometer  

E-Print Network (OSTI)

We present the first grating-resolution X-ray spectra of the X-ray binary Cir X-1, obtained with the High Energy Transmission Grating Spectrometer on Chandra. These reveal a rich set of lines from H-like and/or He-like Ne, Mg, Si, S and Fe detected with a high signal-to-noise ratio. The lines are broad (+/- 2000 km/s) and show P Cygni profiles. The absorption components of the lines extend to low velocity, and they have about the same widths and strengths as the corresponding emission components. The widths of the X-ray P Cygni lines are comparable to that of the broad component of the strong, asymmetric H-alpha line from Cir X-1, suggesting that the two phenomena may be related. We discuss outflow models and propose that the P Cygni profiles may arise in the moderate temperature (5 x 10^6 K) region of the wind from an X-ray heated accretion disk. This basic picture strengthens the idea that the accretion disk in Cir X-1 is viewed in a relatively edge-on manner, and it suggests that Cir X-1 is the X-ray binary analog of a Broad Absorption Line quasar.

W. N. Brandt; N. S. Schulz

2000-07-26T23:59:59.000Z

118

Kaonic Atom X?ray Spectra  

Science Conference Proceedings (OSTI)

In kaonic atoms energy displacement and broadening of states result from the strong interaction. The most simple kaonic atoms like kaonic hydrogen and deuterium open the possibility to measure this strong interaction induced shift and width by x?ray spectroscopy. In the SIDDHARTA experiment al LNF (Frascati) the DA?NE electron?positron collider delivers nearly mono?energetic negatively charged kaons from ? meson decay. This unique kaon source is used to form kaonic atoms. New high performance x?ray detectors (silicon drift detectors) arranged in an array allow x?ray spectroscopy with high energy resolution combined with timing capability. High precision x?ray measurements like SIDDHARTA at LNF will open the way to study the low energy regime of the strong force in the antikaon?nucleon interaction. The experiment and its current status is presented in this talk.

J. Marton; on behalf of the SIDDHARTA Collaboration

2009-01-01T23:59:59.000Z

119

Tunable X-ray source  

DOE Patents (OSTI)

A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

Boyce, James R. (Williamsburg, VA)

2011-02-08T23:59:59.000Z

120

A High-Energy, Ultrashort-Pulse X-Ray System for the Dynamic Study of Heavy, Dense Materials  

Science Conference Proceedings (OSTI)

Thomson-scattering based x-ray radiation sources, in which a laser beam is scattered off a relativistic electron beam resulting in a high-energy x-ray beam, are currently being developed by several groups around the world to enable studies of dynamic material properties which require temporal resolution on the order of tens of femtoseconds to tens of picoseconds. These sources offer pulses that are shorter than available from synchrotrons, more tunable than available from so-called Ka sources, and more penetrating and more directly probing than ultrafast lasers. Furthermore, Thomson-scattering sources can scale directly up to x-ray energies in the few MeV range, providing peak brightnesses far exceeding any other sources in this regime. This dissertation presents the development effort of one such source at Lawrence Livermore National Laboratory, the Picosecond Laser-Electron InterAction for the Dynamic Evaluation of Structures (PLEIADES) project, designed to target energies from 30 keV to 200 keV, with a peak brightness on the order of 10{sup 18} photons {center_dot} s{sup -1} {center_dot} mm{sup -2} {center_dot} mrad{sup -2} {center_dot} 0.01% bandwidth{sup -1}. A 10 TW Ti:Sapphire based laser system provides the photons for the interaction, and a 100 MeV accelerator with a 1.6 cell S-Band photoinjector at the front end provides the electron beam. The details of both these systems are presented, as is the initial x-ray production and characterization, validating the theory of Thomson scattering. In addition to the systems used to enable PLEIADES, two alternative systems are discussed. An 8.5 GHz X-Band photoinjector, capable of sustaining higher accelerating gradients and producing lower emittance electron beams in a smaller space than the S-Band gun, is presented, and the initial operation and commissioning of this gun is presented. Also, a hybrid chirped-pulse amplification system is presented as an alternative to the standard regenerative amplifier technology in high-power ultrafast laser systems. This system combines an optical-parametric chirped-pulse amplification (OPCPA) system with a titanium:sapphire-based four-pass amplifier to provide the high pre-pulse contrast and ease of assembly of an OPCPA using a commercial pump laser while avoiding the loss of efficiency such a system would normally entail.

Gibson, D J

2004-09-17T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
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121

X-ray Sources by Energy Recovered Linacs and Their Needed R&D  

Science Conference Proceedings (OSTI)

In this paper we review the current state of research on energy recovered linacs as drivers for future X-ray sources. For many types of user experiments, such sources may have substantial advantages compared to the workhorse sources of the present: high energy storage rings. Energy recovered linacs need to be improved beyond present experience in both energy and average current to support this application. To build an energy recovered linac based X-ray user facility presents many interesting challenges. We present summaries on the Research and Development (R&D) topics needed for full development of such a source, including the discussion at the Future Light Sources Workshop held in Gaithersburg, Maryland on September 15- 17, 2009. A #12;rst iteration of an R&D plan is presented that is founded on the notion of building a set of succeedingly larger test accelerators exploring cathode physics, high average current injector physics, and beam recirculation and beam energy recovery at high average current. Our basic conclusion is that a reviewable design of such a source can be developed after an R&D period of #12;ve to ten years.

Benson, Stephen; Douglas, David; Dowell, David; Hernandez-Garcia, Carlos; Kayran, D; Krafft, Geoffrey; Legg, Robert; Moog, E; Obina, T; Rimmer, Robert

2011-05-01T23:59:59.000Z

122

Energy distribution measurement of narrow-band ultrashort x-ray beams via K-edge filters subtraction  

Science Conference Proceedings (OSTI)

The characterization of novel x-ray sources includes the measurement of the photon flux and the energy distribution of the produced beam. The aim of BEATS2 experiment at the SPARC-LAB facility of the INFN National Laboratories of Frascati (Rome, Italy) is to investigate possible medical applications of an x-ray source based on Thomson relativistic back-scattering. This source is expected to produce a pulsed quasi-monochromatic x-ray beam with an instantaneous flux of 10{sup 20} ph/s in pulses 10 ps long and with an average energy of about 20 keV. A direct measurement of energy distribution of this beam is very difficult with traditional detectors because of the extremely high photon flux. In this paper, we present a method for the evaluation of the energy distribution of quasi-monochromatic x-ray beams based on beam filtration with K-edge absorbing foils in the energy range of interest (16-22 keV). The technique was tested measuring the energy distribution of an x-ray beam having a spectrum similar to the expected one (SPARC-LAB Thomson source) by using a tungsten anode x-ray tube properly filtered and powered. The energy distribution obtained has been compared with the one measured with a HPGe detector showing very good agreement.

Cardarelli, Paolo; Di Domenico, Giovanni; Marziani, Michele; Mucollari, Irena; Pupillo, Gaia; Sisini, Francesco; Taibi, Angelo; Gambaccini, Mauro [Dipartimento di Fisica, Universita di Ferrara and INFN - Ferrara, via Saragat 1, I-44122 Ferrara (Italy)

2012-10-01T23:59:59.000Z

123

Beyond 3-D X-ray Imaging: Methodology Development and Applications in  

NLE Websites -- All DOE Office Websites (Extended Search)

Beyond 3-D X-ray Imaging: Methodology Development and Applications in Beyond 3-D X-ray Imaging: Methodology Development and Applications in Material Science Thursday, September 6, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Yijin Liu Seminar There was a revolutionary development of X-ray imaging over the past few decades. The most substantial advancements in this field are closely related to the availability of the new generation of X-ray sources and the advanced X-ray optics. The advanced X-ray Optics along with novel methodology has made it possible to extract information that is related to different interactions between the X-rays and the specimen at very fine spatial resolution. The energy tunability of the X-rays has made it possible to combine the energy scan with imaging technique. And the brilliance of the X-ray source has made it practical for many sophisticated

124

Analysis of nuclear materials by energy dispersive x-ray fluorescence and spectral effects of alpha decay  

SciTech Connect

Energy dispersive X-ray fluorescence (EDXRF) spectra collected from alpha emitters are complicated by artifacts inherent to the alpha decay process, particularly when using portable instruments. For example, {sup 239}Pu EDXRF spectra exhibit a prominent uranium L X-ray emission peak series due to sample alpha decay rather than source-induced X-ray fluorescence. A portable EDXRF instrument was used to collect spectra from plutonium, americium, and a Pu-contaminated steel sample. The plutonium sample was also analyzed by wavelength dispersive XRF to demonstrate spectral differences observed when using these very different instruments.

Worley, Christopher G [Los Alamos National Laboratory

2009-01-01T23:59:59.000Z

125

Tabletop soft-x-ray Fourier transform holography with 50 nm resolution  

E-Print Network (OSTI)

Synchrotron Radiation Laboratory, SLAC National Accelerator Laboratory, Menlo Park, California 94025, USA 4. We also demonstrate that FT holography can be used effectively with short exposure times of 30 s resolution images of whole unstained cells, magnetic permalloy wires, internal structures in nanocrystals

Miao, Jianwei "John"

126

Pulse pileup statistics for energy discriminating photon counting x-ray detectors  

SciTech Connect

Purpose: Energy discriminating photon counting x-ray detectors can be subject to a wide range of flux rates if applied in clinical settings. Even when the incident rate is a small fraction of the detector's maximum periodic rate N{sub 0}, pulse pileup leads to count rate losses and spectral distortion. Although the deterministic effects can be corrected, the detrimental effect of pileup on image noise is not well understood and may limit the performance of photon counting systems. Therefore, the authors devise a method to determine the detector count statistics and imaging performance. Methods: The detector count statistics are derived analytically for an idealized pileup model with delta pulses of a nonparalyzable detector. These statistics are then used to compute the performance (e.g., contrast-to-noise ratio) for both single material and material decomposition contrast detection tasks via the Cramer-Rao lower bound (CRLB) as a function of the detector input count rate. With more realistic unipolar and bipolar pulse pileup models of a nonparalyzable detector, the imaging task performance is determined by Monte Carlo simulations and also approximated by a multinomial method based solely on the mean detected output spectrum. Photon counting performance at different count rates is compared with ideal energy integration, which is unaffected by count rate. Results: The authors found that an ideal photon counting detector with perfect energy resolution outperforms energy integration for our contrast detection tasks, but when the input count rate exceeds 20%N{sub 0}, many of these benefits disappear. The benefit with iodine contrast falls rapidly with increased count rate while water contrast is not as sensitive to count rates. The performance with a delta pulse model is overoptimistic when compared to the more realistic bipolar pulse model. The multinomial approximation predicts imaging performance very close to the prediction from Monte Carlo simulations. The monoenergetic image with maximum contrast-to-noise ratio from dual energy imaging with ideal photon counting is only slightly better than with dual kVp energy integration, and with a bipolar pulse model, energy integration outperforms photon counting for this particular metric because of the count rate losses. However, the material resolving capability of photon counting can be superior to energy integration with dual kVp even in the presence of pileup because of the energy information available to photon counting. Conclusions: A computationally efficient multinomial approximation of the count statistics that is based on the mean output spectrum can accurately predict imaging performance. This enables photon counting system designers to directly relate the effect of pileup to its impact on imaging statistics and how to best take advantage of the benefits of energy discriminating photon counting detectors, such as material separation with spectral imaging.

Wang, Adam S.; Harrison, Daniel; Lobastov, Vladimir; Tkaczyk, J. Eric [Departments of Electrical Engineering and Radiology, Stanford University, Stanford, California 94305 (United States); GE Global Research Center, Niskayuna, New York 12309 (United States)

2011-07-15T23:59:59.000Z

127

Modeling energy dependence of the inner-shell x-ray emission produced by femtosecond-pulse laser irradiation of xenon clusters  

Science Conference Proceedings (OSTI)

We employ the Los Alamos suite of atomic physics codes to model the inner-shell x-ray emission spectrum of xenon and compare results with those obtained via high-resolution x-ray spectroscopy of xenon clusters irradiated by 30 fs Ti:Sa laser pulses. We find that the commonly employed configuration average approximation breaks down and significant spin-orbit splitting necessitates a detailed level accounting. Additionally, we reproduce an interesting spectral trend for a series of experimental spectra taken with varying pulse energy for fixed pulse duration. To simulate the experimental measurements at increasing beam energies, we find that spectral modeling requires an increased hot electron fraction, but decreased atomic density and bulk electron temperature. We believe these latter conditions to be a result of partial cluster destruction due to the increased energy in the laser prepulse.

Colgan, James P [Los Alamos National Laboratory

2008-01-01T23:59:59.000Z

128

X-ray Imaging Shows Feather Patterns of First Birds | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

X-ray Imaging Shows Feather Patterns of First Birds X-ray Imaging Shows Feather Patterns of First Birds X-ray Imaging Shows Feather Patterns of First Birds June 30, 2011 - 2:56pm Addthis A collage of images. Top, optical images of: blue jay feather, squid, and fossil fish with feather. Bottom: x-ray images showing the distribution of copper (red) in the same organisms. | Photo Courtesy of Gregory Stewart, SLAC National Accelerator Laboratory A collage of images. Top, optical images of: blue jay feather, squid, and fossil fish with feather. Bottom: x-ray images showing the distribution of copper (red) in the same organisms. | Photo Courtesy of Gregory Stewart, SLAC National Accelerator Laboratory Niketa Kumar Niketa Kumar Public Affairs Specialist, Office of Public Affairs What are the key facts? Through x-ray fluorescent imaging techniques developed at the

129

Using High Energy X-ray Experiments and Crystal-Based ...  

Science Conference Proceedings (OSTI)

... Magnetic Composite Materials X-Ray Studies of Structural Effects Induced by Pulsed (30 Tesla), High Magnetic Fields at the Advanced Photon Source...

130

RHESSI MICROFLARE STATISTICS. II. X-RAY IMAGING, SPECTROSCOPY, AND ENERGY DISTRIBUTIONS I. G. Hannah, S. Christe,1  

E-Print Network (OSTI)

RHESSI MICROFLARE STATISTICS. II. X-RAY IMAGING, SPECTROSCOPY, AND ENERGY DISTRIBUTIONS I. G distribution of RHESSI flares and compare it to previous thermal energy distributions of transient events. We flares down to nanoflares. The fre- quency distribution of the energy in these events has been studied

California at Berkeley, University of

131

Harmonic Generation at Lower Electron Energies for a Hard X-ray FEL  

SciTech Connect

There are several schemes currently being investigated to pre-bunch the electron beam and step the coherent bunching up to higher harmonics, all which require modulator sections which introduce additional energy modulation. X-ray FELs operate in a regime where the FEL parameter, {rho} is equal to or less than the effective energy spread introduced from the emittance in the electron beam. Because of this large effective energy spread, the energy modulation introduced from harmonic generation schemes would seriously degrade FEL performance. This problem can be mitigated by incorporating the harmonic generation scheme at a lower electron kinetic energy than the energy at the final undulator. This will help because the effective energy spread from emittance is reduced at lower energies, and can be further reduced by making the beam transversely large. Then the beam can be squeezed down slowly enough in the subsequent accelerator sections so that geometric debunching is mitigated. The beam size inside the dispersive chicanes and in the accelerator sections must be carefully optimized to avoid debunching, and each subharmonic modulator section must generate enough energy modulation to overcome the SASE noise without significantly increasing the gain length in the final undulator. Here we show analytical results that demonstrate the feasibility of this harmonic pre-bunching scheme.

Marksteiner, Quinn R. [Los Alamos National Laboratory

2011-01-01T23:59:59.000Z

132

X-ray microtomography  

SciTech Connect

In this tutorial, we describe X-ray microtomography as a technique to nondestructively characterize material microstructure in three dimensions at a micron level spatial resolution. While commercially available laboratory scale instrumentation is available, we focus our attention on synchrotron-based systems, where we can exploit a high flux, monochromatic X-ray beam to produce high fidelity three-dimensional images. A brief description of the physics and the mathematical analysis behind the technique is followed by example applications to specific materials characterization problems, with a particular focus on the utilization of three-dimensional image processing that can be used to extract a wide range of useful information.

Landis, Eric N., E-mail: landis@maine.edu [Department of Civil and Environmental Engineering, University of Maine, 5711 Boardman Hall, Orono, Maine 04469 (United States); Keane, Denis T., E-mail: dtkeane@northwestern.edu [Department of Materials Science and Engineering, Northwestern University (United States); DND-CAT, Advanced Photon Source, Argonne National Laboratory, Bldg. 432/A002, 9700 S. Cass Ave, Argonne, Illinois 60439 (United States)

2010-12-15T23:59:59.000Z

133

X-ray lithography source  

SciTech Connect

A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and elminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an exellent moderate-priced X-ray source for lithography.

Piestrup, Melvin A. (Woodside, CA); Boyers, David G. (Mountain View, CA); Pincus, Cary (Sunnyvale, CA)

1991-01-01T23:59:59.000Z

134

X-ray lithography source  

DOE Patents (OSTI)

A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits is disclosed. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and eliminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an excellent moderate-priced X-ray source for lithography. 26 figures.

Piestrup, M.A.; Boyers, D.G.; Pincus, C.

1991-12-31T23:59:59.000Z

135

CO-ANALYSIS OF SOLAR MICROWAVE AND HARD X-RAY SPECTRAL EVOLUTIONS. I. IN TWO FREQUENCY OR ENERGY RANGES  

SciTech Connect

Solar microwave and hard X-ray spectral evolutions are co-analyzed in the 2000 June 10 and 2002 April 10 flares, and are simultaneously observed by the Owens-Valley Solar Array in the microwave band and by Yohkoh/Hard X-ray Telescope or RHESSI in the hard X-ray band, with multiple subpeaks in their light curves. The microwave and hard X-ray spectra are fitted by a power law in two frequency ranges of the optical thin part and two photon energy ranges, respectively. Similar to an earlier event in Shao and Huang, the well-known soft-hard-soft pattern of the lower energy range changed to the hard-soft-hard (HSH) pattern of the higher energy range during the spectral evolution of each subpeak in both hard X-ray flares. This energy dependence is actually supported by a positive correlation between the overall light curves and spectral evolution in the lower energy range, while it becomes an anti-correlation in the higher energy range. Regarding microwave data, the HSH pattern appears in the spectral evolution of each subpeak in the lower frequency range, which is somewhat similar to Huang and Nakajima. However, it returns back to the well-known pattern of soft-hard-harder for the overall spectral evolution in the higher frequency range of both events. This frequency dependence is confirmed by an anti-correlation between the overall light curves and spectral evolution in the lower frequency range, but it becomes a positive correlation in the higher frequency range. The possible mechanisms are discussed, respectively, for reasons why hard X-ray and microwave spectral evolutions have different patterns in different energy and frequency intervals.

Song Qiwu; Huang Guangli [Purple Mountain Observatory, Nanjing 210008 (China); Nakajima, Hiroshi, E-mail: songqw@pmo.ac.cng, E-mail: lhuang@pmo.ac.cn, E-mail: nakaji15@dia.janis.or.jp [Nobeyama Solar Radio Observatory, Nobeyama, Minamisaku, Nagano 384-1305 (Japan)

2011-06-20T23:59:59.000Z

136

Synchrotron X-ray Measurements  

Science Conference Proceedings (OSTI)

... fine structure (EXAFS) spectroscopy; (3) variable kinetic energy X-ray ... advanced materials is critical to the development and optimization of products ...

2012-10-04T23:59:59.000Z

137

A high resolution view of the jet termination shock in a hot spot of the nearby radio galaxy Pictor A: implications for X-ray models of radio galaxy hot spots  

E-Print Network (OSTI)

Images made with the VLBA have resolved the region in a nearby radio galaxy, Pictor A, where the relativistic jet that originates at the nucleus terminates in an interaction with the intergalactic medium, a so-called radio galaxy hot spot. This image provides the highest spatial resolution view of such an object to date (16 pc), more than three times better than previous VLBI observations of similar objects. The north-west Pictor A hot spot is resolved into a complex set of compact components, seen to coincide with the bright part of the hot spot imaged at arcsecond-scale resolution with the VLA. In addition to a comparison with VLA data, we compare our VLBA results with data from the HST and Chandra telescopes, as well as new Spitzer data. The presence of pc-scale components in the hot spot, identifying regions containing strong shocks in the fluid flow, leads us to explore the suggestion that they represent sites of synchrotron X-ray production, contributing to the integrated X-ray flux of the hot spot, along with X-rays from synchrotron self-Compton scattering. This scenario provides a natural explanation for the radio morphology of the hot spot and its integrated X-ray emission, leading to very different predictions for the higher energy X-ray spectrum compared to previous studies. From the sizes of the individual pc-scale components and their angular spread, we estimate that the jet width at the hot spot is in the range 70 - 700 pc, which is comparable to similar estimates in PKS 2153-69, 3C 205, and 4C 41.17. The lower limit in this range arises from the suggestion that the jet may dither in its direction as it passes through hot spot backflow material close to the jet termination point, creating a "dentist drill" effect on the inside of a cavity 700 pc in diameter.

S. J. Tingay; E. Lenc; G. Brunetti; M. Bondi

2008-10-02T23:59:59.000Z

138

Hand-held X-Ray Fluorescence (XRF) | Open Energy Information  

Open Energy Info (EERE)

Hand-held X-Ray Fluorescence (XRF) Hand-held X-Ray Fluorescence (XRF) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: Hand-held X-Ray Fluorescence (XRF) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Field Techniques Exploration Sub Group: Data Collection and Mapping Parent Exploration Technique: Data Collection and Mapping Information Provided by Technique Lithology: Bulk and trace element analysis of rocks, minerals, and sediments. Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png Hand-held X-Ray Fluorescence (XRF): Hand-held X-Ray Fluorescence is a portable analytical technique derived from the instrumentation used in traditional lab-based XRF analysis. The technique is used for bulk chemical analysis of rock, mineral, and sediment

139

Space X-ray Solves Mysteries of Black Holes | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Space X-ray Solves Mysteries of Black Holes Space X-ray Solves Mysteries of Black Holes Space X-ray Solves Mysteries of Black Holes March 13, 2013 - 3:57pm Addthis Space X-ray Solves Mysteries of Black Holes Anne M. Stark Senior Public Information Officer, Lawrence Livermore National Laboratory "We know that black holes have a strong link to their host galaxy." Astrophysicist Bill Craig, a member of the LLNL team An international team including Lawrence Livermore National Laboratory scientists has definitively measured the spin rate of a supermassive black hole for the first time. The findings, made by the two X-ray space observatories, NASA's Nuclear Spectroscopic Telescope Array (NuSTAR) and the European Space Agency's XMM-Newton, solve a long-standing debate about similar measurements in

140

The World's First Free-Electron X-ray Laser | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

First Free-Electron X-ray Laser First Free-Electron X-ray Laser The World's First Free-Electron X-ray Laser August 17, 2010 - 6:19pm Addthis The World's First Free-Electron X-ray Laser John Schueler John Schueler Former New Media Specialist, Office of Public Affairs Yesterday, Secretary Chu participated in the dedication of the world's first free-electron and most powerful X-ray laser, the Linac Coherent Light Source (LCLS). In light of this occasion (pun intended), we posted an in-depth look at the innovative nature of this new instrument and its potential to tackle some of life's biggest mysteries. The Secretary seemed just as geeked about the possibilities of the LCLS, stating that "this is a new instrument that will enable us to see the structure of materials that we could not determine by any other means ... Knowing those

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

The X-ray afterglow flat segment in short GRB 051221A: Energy injection from a millisecond magnetar?  

E-Print Network (OSTI)

The flat segment lasting $\\sim 10^4$ seconds in the X-ray afterglow of GRB051221A represents the first clear case of strong energy injection in the external shock of a short GRB afterglow. In this work, we show that a millisecond pulsar with dipole magnetic field $\\sim 10^{14}$ Gauss could well account for that energy injection. The good quality X-ray flat segment thus suggests that the central engine of this short burst may be a millisecond magnetar.

Yizhong Fan; Dong Xu

2006-05-18T23:59:59.000Z

142

Chandra High-Resolution X-Ray Spectrum of Supernova Remnant 1E0102.2-7219  

E-Print Network (OSTI)

Chandra High Energy Transmission Grating Spectrometer observations of the supernova remnant 1E0102.2-7219 in the Small Magellanic Cloud reveal a spectrum dominated by X-ray emission lines from hydrogen-like and helium-like ions of oxygen, neon, magnesium and silicon, with little iron. The dispersed spectrum shows a series of monochromatic images of the source in the light of individual spectral lines. Detailed examination of these dispersed images reveals Doppler shifts within the supernova remnant, indicating bulk matter velocities on the order of 1000 km/s. These bulk velocities suggest an expanding ring-like structure with additional substructure, inclined to the line of sight. A two-dimensional spatial/velocity map of the SNR shows a striking spatial separation of redshifted and blueshifted regions, and indicates a need for further investigation before an adequate 3D model can be found. The radii of the ring-like images of the dispersed spectrum vary with ionization stage, supporting an interpretation of progressive ionization due to passage of the reverse shock through the ejecta. Plasma diagnostics with individual emission lines of oxygen are consistent with an ionizing plasma in the low density limit, and provide temperature and ionization constraints on the plasma. Assuming a pure metal plasma, the mass of oxygen is estimated at ~6 solar masses, consistent with a massive progenitor.

K. A. Flanagan; C. R. Canizares; D. Dewey; J. C. Houck; A. C. Fredericks; M. L. Schattenburg; T. H. Markert; D. S. Davis

2003-12-18T23:59:59.000Z

143

Chandra High-Resolution X-Ray Spectrum of Supernova Remnant 1E0102.2-7219  

E-Print Network (OSTI)

Chandra High Energy Transmission Grating Spectrometer observations of the supernova remnant 1E0102.2-7219 in the Small Magellanic Cloud reveal a spectrum dominated by X-ray emission lines from hydrogen-like and helium-like ions of oxygen, neon, magnesium and silicon, with little iron. The dispersed spectrum shows a series of monochromatic images of the source in the light of individual spectral lines. Detailed examination of these dispersed images reveals Doppler shifts within the supernova remnant, indicating bulk matter velocities on the order of 1000 km/s. These bulk velocities suggest an expanding ring-like structure with additional substructure, inclined to the line of sight. A two-dimensional spatial/velocity map of the SNR shows a striking spatial separation of redshifted and blueshifted regions, and indicates a need for further investigation before an adequate 3D model can be found. The radii of the ring-like images of the dispersed spectrum vary with ionization stage, supporting an interpretation of ...

Flanagan, K A; Dewey, D; Houck, J C; Fredericks, A C; Schattenburg, M L; Markert, T H; Davis, D S

2004-01-01T23:59:59.000Z

144

Proton induced quasi-monochromatic x-ray beams for soft x-ray spectroscopy studies and selective x-ray fluorescence analysis  

Science Conference Proceedings (OSTI)

We present the analytical features and performance of an x-ray spectroscopy end station of moderate energy resolution operating with proton-induced quasi-monochromatic x-ray beams. The apparatus was designed, installed and operated at the 5.5 MV Tandem VdG Accelerator Laboratory of the Institute of Nuclear Physics, N.C.S.R. 'Demokritos,' Athens. The setup includes a two-level ultrahigh vacuum chamber that hosts in the lower level up to six primary targets in a rotatable holder; there, the irradiation of pure element materials-used as primary targets-with few-MeV high current ({approx}{mu}A) proton beams produces intense quasi-monochromatic x-ray beams of selectable energy. In the chamber's upper level, a six-position rotatable sample holder hosts the targets considered for x-ray spectroscopy studies. The proton-induced x-ray beam, after proper collimation, is guided to the sample position whereas various filters can be also inserted along the beam's path to eliminate the backscattered protons or/and to absorb selectively components of the x-ray beam. The apparatus incorporates an ultrathin window Si(Li) spectrometer (FWHM 136 eV at 5.89 keV) coupled with low-noise electronics capable of efficiently detecting photons down to carbon K{alpha}. Exemplary soft x-ray spectroscopy studies and results of selective x-ray fluorescence analysis are presented.

Sokaras, D. [Institute of Nuclear Physics, N.C.S.R. Demokritos, Aghia Paraskevi, 15310 Athens (Greece); Zarkadas, Ch. [PANalytical B.V., 7600 AA Almelo (Netherlands); Fliegauf, R.; Beckhoff, B. [Physikalisch-Technische Bundesanstalt, Abbestrasse 2-12, 10587 Berlin (Germany); Karydas, A. G. [Institute of Nuclear Physics, N.C.S.R. Demokritos, Aghia Paraskevi, 15310 Athens (Greece); Nuclear Spectrometry and Applications Laboratory, IAEA Laboratories, A-2444 Seibersdorf (Austria)

2012-12-15T23:59:59.000Z

145

Refractive Optics for Hard X-ray Transmission Microscopy  

Science Conference Proceedings (OSTI)

For hard x-ray transmission microscopy at photon energies higher than 15 keV we design refractive condenser and imaging elements to be used with synchrotron light sources as well as with x-ray tube sources. The condenser lenses are optimized for low x-ray attenuation--resulting in apertures greater than 1 mm--and homogeneous intensity distribution on the detector plane, whereas the imaging enables high-resolution (condenser and imaging lenses are being developed. The imaging lenses (compound refractive lenses, CRLs) are made of SU-8 negative resist by deep x-ray lithography. SU-8 shows high radiation stability. The fabrication technique enables high-quality lens structures regarding surface roughness and arrangement precision with arbitrary 2D geometry. To provide point foci, crossed pairs of lenses are used. Condenser lenses have been made utilizing deep x-ray lithographic patterning of thick SU-8 layers, too, whereas in this case, the aperture is limited due to process restrictions. Thus, in terms of large apertures, condenser lenses made of structured and rolled polyimide film are more attractive. Both condenser types, x-ray mosaic lenses and rolled x-ray prism lenses (RXPLs), are considered to be implemented into a microscope setup. The x-ray optical elements mentioned above are characterized with synchrotron radiation and x-ray laboratory sources, respectively.

Simon, M.; Last, A.; Mohr, J.; Nazmov, V.; Reznikova, E. [Institute for Microstructure Technology, Karlsruhe Institute of Technology Kaiserstrasse 12, 76131 Karlsruhe (Germany); Ahrens, G.; Voigt, A. [Microresist Technology, Koepenikerstrasse 325, 12555 Berlin (Germany)

2011-09-09T23:59:59.000Z

146

Cosmological constraints on Chaplygin gas dark energy from galaxy clusters X-ray and supernova data  

E-Print Network (OSTI)

The recent observational evidences for the present accelerated stage of the Universe have stimulated renewed interest for alternative cosmologies. In general, such models contain an unknown negative-pressure dark component that explains the supernova results and reconciles the inflationary flatness prediction ($Omega_{rm{T}} = 1$) and the cosmic microwave background measurements with the dynamical estimates of the quantity of matter in the Universe ($Omega_{rm{m}} simeq 0.3 pm 0.1$). In this paper we study some observational consequences of a dark energy candidate, the so-called generalized Chaplygin gas which is characterized by an equation of state $p_{C} = -A/rho_{C}^{alpha}$, where $A$ and $alpha$ are positive constants. We investigate the prospects for constraining the equation of state of this dark energy component by combining Chandra observations of the X-ray luminosity of galaxy clusters, independent measurements of the baryonic matter density, the latest measurements of the Hubble parameter as given...

Cunha, J V; Lima, J A S

2004-01-01T23:59:59.000Z

147

Relationship between pulse width and energy in GRB 060124: from X-ray to gamma-ray bands  

E-Print Network (OSTI)

GRB 060124 is the first event that both prompt and afterglow emission were observed simultaneously by the three \\emph{Swift} instruments. Its main peak also triggered Konus-Wind and HETE-II. Therefore, investigation on both the temporal and spectral properties of the prompt emission can be extended to X-ray bands. We perform a detailed analysis on the two well identified pulses of this burst, and find that the pulses are narrower at higher energies, and both X-rays and gamma-rays follow the same $w - E$ relation for an individual pulse. However, there is no a universal power-law index of the $w - E$ relation among pulses. We find also that the rise-to-decay ratio $r/d$ seems not to evolve with $E$ and the $r/d$ values are well consistent with that observed in typical GRBs. The broadband spectral energy distribution also suggest that the X-rays are consistent with the spectral behavior of the gamma-rays. These results indicates that the X-ray emission tracks the gamma-ray emission and the emissions in the two energy bands are likely to be originated from the same physical mechanism.

Fu-Wen Zhang; Yi-Ping Qin

2008-06-07T23:59:59.000Z

148

Miniature x-ray source  

DOE Patents (OSTI)

A miniature x-ray source capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature x-ray source comprises a compact vacuum tube assembly containing a cathode, an anode, a high voltage feedthru for delivering high voltage to the anode, a getter for maintaining high vacuum, a connection for an initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is highly x-ray transparent and made, for example, from boron nitride. The compact size and potential for remote operation allows the x-ray source, for example, to be placed adjacent to a material sample undergoing analysis or in proximity to the region to be treated for medical applications.

Trebes, James E. (Livermore, CA); Stone, Gary F. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA); Chornenky, Victor I. (Minnetonka, MN)

2002-01-01T23:59:59.000Z

149

Probing buried layers by photoelectron spectromicroscopy with hard x-ray excitation  

SciTech Connect

We report about a proof-of-principle experiment which explores the perspectives of performing hard x-ray photoemission spectromicroscopy with high lateral resolution. Our results obtained with an energy-filtered photoemission microscope at the PETRA III storage ring facility using hard x-ray excitation up to 6.5 keV photon energy demonstrate that it is possible to obtain selected-area x-ray photoemission spectra from regions less than 500 nm in diameter.

Wiemann, C.; Patt, M.; Cramm, S. [Peter Gruenberg Institute (PGI-6) and JARA-FIT, Research Centre Juelich, D-52425 Juelich (Germany); Escher, M.; Merkel, M. [FOCUS GmbH, D-65510 Huenstetten (Germany); Gloskovskii, A. [Institut fuer Anorganische Chemie und Analytische Chemie, Johannes Gutenberg-Universitaet Mainz, D-55128 Mainz (Germany); Thiess, S.; Drube, W. [DESY Photon Science, Deutsches Elektronen-Synchrotron, D-22603 Hamburg (Germany); Schneider, C. M. [Peter Gruenberg Institute (PGI-6) and JARA-FIT, Research Centre Juelich, D-52425 Juelich (Germany); Fakultaet f. Physik and Center for Nanointegration Duisburg-Essen (CENIDE), Universitaet Duisburg-Essen, D-47048 Duisburg (Germany)

2012-05-28T23:59:59.000Z

150

Application of PILATUS II Detector Modules for High Resolution X-Ray Imaging Crystal Spectrometers on the Alcator C-Mod Tokamak  

Science Conference Proceedings (OSTI)

A new type of X-ray imaging crystal spectrometer for Doppler measurements of the radial profiles of the ion temperature and plasma rotation velocity in tokamak plasmas is presently being developed in a collaboration between various laboratories. The spectrometer will consist of a spherically bent crystal and a two-dimensional position sensitive detector; and it will record temporally and spatially resolved X-ray line spectra from highly-charged ions. The detector must satisfy challenging requirements with respect to count rate and spatial resolution. The paper presents the results from a recent test of a PILATUS II detector module on Alcator C-Mod, which demonstrate that the PILATUS II detector modules will satisfy these requirements.

M.L. Bitter, Ch. Borennimann, E.F. Eikenberry, K.W. Hill, A. Ince-Chushman, S.G. Lee, J.E. Rice, and S. Scott.

2007-07-23T23:59:59.000Z

151

Compact x-ray source and panel  

SciTech Connect

A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

Sampayon, Stephen E. (Manteca, CA)

2008-02-12T23:59:59.000Z

152

Copper Ridges Nearly Double X-ray Sensor Performance  

Science Conference Proceedings (OSTI)

... Physics Letters,* can measure X-ray energies with an ... X-rays and measure the energy based on ... by NASA and the NIST Office of Microelectronics ...

2011-10-03T23:59:59.000Z

153

Sandia National Laboratories X-ray Tube with Magnetic Electron ...  

... for the U.S. Department of Energys National ... high average power large area X-ray tube provides increased X-ray generation efficiency through ...

154

High Energy X-Ray System Specification for the Device Assembly Facility (DAF) at the NNSS  

SciTech Connect

This specification establishes requirements for an X-Ray System to be used at the Device Assembly Facility (DAF) at the Nevada National Security Site (NNSS) to support radiography of experimental assemblies for Laboratory (LANL, LLNL, SNL) programs conducting work at the NNSS.

Fry, David A. [Los Alamos National Laboratory

2012-08-10T23:59:59.000Z

155

Study of the Stability of 3C-SiC Single Crystals Using High-Resolution Diffuse X-Ray Scattering  

SciTech Connect

The stability of (001)-oriented 3C silicon carbide crystals is studied by a method coupling high resolution x-ray diffraction and numerical simulations. The analysis of the diffuse scattering intensity distribution along selected directions in reciprocal space allows us to obtain qualitative and quantitative informations regarding the 3C-6H transition. Our latest results concerning the influence of the initial crystal quality (presence of defects) and of annealing time on the 3C-6H transition are presented in this article.

Dompoint, D.; Boulle, A. [Science des Procedes Ceramiques et de Traitements de Surface (SPCTS) CNRS UMR 6638, ENSCI, 47 avenue Albert Thomas 87065 Limoges Cedex (France); Galben-Sandulache, I. G.; Chaussende, D. [Laboratoire des Materiaux et du Genie Physique (LMGP) CNRS UMR 5628, Grenoble INP, Minatec, 3 parvis Louis Neel, BP 257, 38016 Grenoble Cedex 01 (France)

2010-11-01T23:59:59.000Z

156

The Optical and Ultraviolet Spectral Energy Distributions of Short Period Black Hole X-ray Transients in Outburst  

E-Print Network (OSTI)

We compile optical and UV spectra of a sample of 'typical' short period black hole X-ray transients in outburst. We also survey determinations of interstellar extinction and distance in order to deredden spectra and compare absolute fluxes. Hence we perform a comparative study of the broad-band spectral energy distributions (SED). We find that given such a homogeneous sample of typical sources, the optical SEDs form a relatively uniform set, all exhibiting quasi-power-law spectra with Fnu proportional to nu^alpha, where 0.5source, with irradiative heating dominating over viscous. The UV-hard state is well described by a viscously heated disk, although this requires very high mass flow rates in the case of Nova Muscae. Alternatively, a UV-hard spectrum can be produced if the disk is illuminated by a vertically extended X-ray source such as a central scattering corona or jet. [Abridged

R. I. Hynes

2004-12-20T23:59:59.000Z

157

Calibration of X-ray detectors in the 8 to 115 keV energy range and their application to diagnostics on the National Ignition Facility  

Science Conference Proceedings (OSTI)

The calibration of X-ray diagnostics is of paramount importance to the National Ignition Facility (NIF) at Lawrence Livermore National Laboratory (LLNL). National Security Technologies LLC (NSTec) fills this need by providing a wide variety of calibration and diagnostic development services in support of the ongoing research efforts at NIF. The X-ray source in the High Energy X-ray lab utilizes induced fluorescence in a variety of metal foils to produce a beam of characteristic X rays ranging from 8 to 111 keV. Presented are the methods used for calibrating a High Purity Germanium detector, which has been absolutely calibrated using radioactive check sources, compared against a silicon photodiode calibrated at Physikalisch Technische Bundesanstalt (PTB). Also included is a limited presentation of results from the recent calibration of the upgraded Filter Fluorescer X ray Spectrometer.

J. J. Lee, M. J. Haugh, G. LaCaille, and P. Torres

2012-10-01T23:59:59.000Z

158

High-Energy Processes in Young Stars: Chandra X-ray Spectroscopy of HDE 283572, RY Tau, and LkCa 21  

E-Print Network (OSTI)

Weak-lined T Tauri stars (WTTS) represent the important stage of stellar evolution between the accretion phase and the zero-age main sequence. At this stage, the star decouples from its accretion disk, and spins up to a higher rotation rate than in the preceding classical T Tauri phase. Consequently, dynamo processes can be expected to become even stronger at this stage. High energy processes can have effects on the remaining circumstellar material, possibly including protoplanets and planetesimals, and these effects may account for certain observable properties of asteroids in the current solar system. Chandra observed for 100 ks the WTTS HDE 283572 which probes the PMS stage of massive A-type stars. We present first results of the analysis of its high-resolution X-ray spectrum obtained with the High-Energy Transmission Grating Spectrometer. A wide range of Fe lines of high ionization states are observed, indicating a continuous emission measure distribution. No significant signal is detected longward of the O \\textsc{viii} Ly$\\alpha$ line because of the high photoelectric absorption. We also report on the preliminary analysis of the zeroth order spectra of RY Tau and LkCa21. In particular, we show evidence of an emission line in RY Tau at 6.4 keV that we identify as fluorescent emission by neutral Fe caused by a strong X-ray flare which illuminated some structure in (or surrounding) the CTTS. A comparison of X-ray spectra of classical T Tau stars, other WTTS, and young main-sequence stars is made.

Marc Audard; Stephen L. Skinner; Kester W. Smith; Manuel Guedel; Roberto Pallavicini

2004-09-13T23:59:59.000Z

159

Tokamak x ray diagnostic instrumentation  

SciTech Connect

Three classes of x-ray diagnostic instruments enable measurement of a variety of tokamak physics parameters from different features of the x-ray emission spectrum. (1) The soft x-ray (1 to 50 keV) pulse-height-analysis (PHA) diagnostic measures impurity concentrations from characteristic line intensities and the continuum enhancement, and measures the electron temperature from the continuum slope. (2) The Bragg x-ray crystal spectrometer (XCS) measures the ion temperature and neutral-beam-induced toroidal rotation velocity from the Doppler broadening and wavelength shift, respectively, of spectral lines of medium-Z impurity ions. Impurity charge state distributions, precise wavelengths, and inner-shell excitation and recombination rates can also be studied. X rays are diffracted and focused by a bent crystal onto a position-sensitive detector. The spectral resolving power E/..delta..E is greater than 10/sup 4/ and time resolution is 10 ms. (3) The x-ray imaging system (XIS) measures the spatial structure of rapid fluctuations (0.1 to 100 kHZ) providing information on MHD phenomena, impurity transport rates, toroidal rotation velocity, plasma position, and the electron temperature profile. It uses an array of silicon surface-barrier diodes which view different chords of the plasma through a common slot aperture and operate in current (as opposed to counting) mode. The effectiveness of shields to protect detectors from fusion-neutron radiation effects has been studied both theoretically and experimentally.

Hill, K.W.; Beiersdorfer, P.; Bitter, M.; Fredrickson, E.; Von Goeler, S.; Hsuan, H.; Johnson, L.C.; Liew, S.L.; McGuire, K.; Pare, V.

1987-01-01T23:59:59.000Z

160

NIST: X-Ray Mass Attenuation Coefficients  

Science Conference Proceedings (OSTI)

... NIST reserves the right to charge for these data in the ... ?/? and the mass energy-absorption coefficient ... The tables cover energies of the photon (x-ray ...

2011-12-09T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

High resolution scanning tunnelling microscopy and extended x-ray-absorption fine structure study of the (533) silicide structure on Cu(001)  

E-Print Network (OSTI)

Using low energy electron diffraction (LEED), scanning tunnelling microscopy (STM) and x-ray absorption spectroscopy (XAS) techniques, we have studied the first steps of silicon adsorption onto Cu (001) single crystal substrate. For low coverage (~ 0.5 ML) and after annealing at 100{\\deg}C, STM images and LEED patterns reveal the formation of an ordered quasi commensurate superstructure. From a quantitative analysis of XAS data, we extract the Si-Cu distance and detail the local atomic arrangement of the structure.

B. Lalmi; M. Chorro; R. Belkhou

2013-08-09T23:59:59.000Z

162

Multivariate Curve Resolution Analysis for Interpretation of Dynamic Cu K-Edge X-ray Absorption Spectroscopy Spectra for a Cu Doped V2O5 Lithium Battery  

DOE Green Energy (OSTI)

Vanadium pentoxide materials prepared through sol-gel processes act as excellent intercalation hosts for lithium as well as polyvalent cations. A chemometric approach has been applied to study the X-ray absorption near-edge structure (XANES) evolution during in situ scanning of the Cu{sub 0.1}V{sub 2}O{sub 5} xerogel/Li ions battery. Among the more common techniques, the fixed size windows evolving factor analysis (FSWEFA) permits the number of species involved in the experiment to be determined and the range of existence of each of them. This result, combined with the constraints of the invariance of the total concentration and non-negativity of both concentrations and spectra, enabled us to obtain the spectra of the pure components using a multivariate curve resolution refined by an alternate least squares fitting procedure. This allowed the normalized concentration profile to be understood. This data treatment evidenced the occurrence, for the first time, of three species during the battery charging. This fact finds confirmation by comparison of the pure spectra with the experimental ones. Extended X-ray absorption fine structure (EXAFS) analysis confirms the occurrence of three different chemical environments of Cu during battery charging.

Conti, P.; Zamponi, S; Giorgetti, M; Berrettoni, M; Smyrl, W

2010-01-01T23:59:59.000Z

163

High resolution soft x-ray spectroscopy of low Z K-shell emission from laser-produced plasmas  

SciTech Connect

A large radius, R = 44.3 m, High Resolution Grating Spectrometer (HRGS) with 2400 line/mm variable line spacing has been designed for laser-produced plasma experiments conducted at the Lawrence Livermore National Laboratory Jupiter Laser Facility. The instrument has been run with a low-noise, charge-coupled device detector to record high signal-to-noise spectra in the 10-50 {angstrom} wavelength range. The instrument can be run with a 10-20 {micro}m wide slit to achieve the best spectral resolving power, approaching 1000 and similar to crystal spectrometers at 12-20 {angstrom}, or in slitless operation with a small symmetrical emission source. We describe preliminary spectra emitted from various H-like and He-like low Z ion plasmas heated by 100-500 ps (FWHM), 527 nm wavelength laser pulses. This instrument can be developed as a useful spectroscopy platform relevant to laboratory-based astrophysics as well as high energy density plasma studies.

Dunn, J; Magee, E W; Shepherd, R; Chen, H; Hansen, S B; Moon, S J; Brown, G V; Gu, M; Beiersdorfer, P; Purvis, M A

2008-05-21T23:59:59.000Z

164

Highly sensitive x-ray detectors in the low-energy range on n-type 4H-SiC epitaxial layers  

Science Conference Proceedings (OSTI)

Schottky diodes on n-type 4H-SiC epitaxial layers have been fabricated for low-energy x-ray detection. The detectors were highly sensitive to soft x-rays and showed improved response compared to the commercial SiC UV photodiodes. Current-voltage characteristics at 475 K showed low leakage current revealing the possibility of high temperature operation. The high quality of the epi-layer was confirmed by x-ray diffraction and chemical etching. Thermally stimulated current measurements performed at 94-550 K revealed low density of deep levels which may cause charge trapping. No charge trapping on detectors' responsivity in the low x-ray energy was found.

Mandal, Krishna C.; Muzykov, Peter G. [Department of Electrical Engineering, University of South Carolina, Columbia, South Carolina 29208 (United States); Russell Terry, J. [Space Science and Applications Group (ISR-1), Intelligence and Space Research Division, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)

2012-07-30T23:59:59.000Z

165

Direct three-dimensional coherently scattered x-ray microtomography  

Science Conference Proceedings (OSTI)

Purpose: It has been shown that coherently scattered x rays can be used to discriminate and identify specific components in a mixture of low atomic weight materials. The authors demonstrated a new method of doing coherently scattered x-ray tomography with a thin sheet of x ray. Methods: A collimated x-ray fan-beam, a parallel polycapillary collimator, and a phantom consisting of several biocompatible materials of low attenuation-based contrast were used to investigate the feasibility of the method. Because of the particular experimental setup, only the phantom translation perpendicular to the x-ray beam is needed and, thus, there is no need of Radon-type tomographic reconstruction, except for the correction of the attenuation to the primary and scattered x rays, which was performed by using a conventional attenuation-based tomographic image data set. The coherent scatter image contrast changes with momentum transfer among component materials in the specimen were investigated with multiple x-ray sources with narrow bandwidth spectra generated with anode and filter combinations of Cu/Ni (8 keV), Mo/Zr (18 keV), and Ag/Pd (22 keV) and at multiple scatter angles by orienting the detector and polycapillary collimator at different angles to the illuminating x ray. Results: The contrast among different materials changes with the x-ray source energy and the angle at which the image was measured. The coherent scatter profiles obtained from the coherent scatter images are consistent with the published results. Conclusions: This method can be used to directly generate the three-dimensional coherent scatter images of small animal, biopsies, or other small objects with low atomic weight biological or similar synthetic materials with low attenuation contrast. With equipment optimized, submillimeter spatial resolution may be achieved.

Cui Congwu; Jorgensen, Steven M.; Eaker, Diane R.; Ritman, Erik L. [Department of Medical Physics, CancerCare Manitoba, 675 McDermot Avenue, Winnipeg, Manitoba R3E 0V9 (Canada); Department of Physiology and Biomedical Engineering, Mayo Clinic, 200 First Street Southwest, Alfred Building 2-409, Rochester, Minnesota 55905 (United States)

2010-12-15T23:59:59.000Z

166

Miniature x-ray source  

DOE Patents (OSTI)

A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

Trebes, James E. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA)

2000-01-01T23:59:59.000Z

167

X-ray data booklet. Revision  

SciTech Connect

A compilation of data is presented. Included are properties of the elements, electron binding energies, characteristic x-ray energies, fluorescence yields for K and L shells, Auger energies, energy levels for hydrogen-, helium-, and neonlike ions, scattering factors and mass absorption coefficients, and transmission bands of selected filters. Also included are selected reprints on scattering processes, x-ray sources, optics, x-ray detectors, and synchrotron radiation facilities. (WRF)

Vaughan, D. (ed.)

1986-04-01T23:59:59.000Z

168

HIGH BRILLIANCE X-RAY SCATTERING FOR  

NLE Websites -- All DOE Office Websites (Extended Search)

BRILLIANCE X-RAY SCATTERING FOR BRILLIANCE X-RAY SCATTERING FOR LIFE SCIENCES (LIX) Group Leader: Lin Yang Proposal Team: O. Bilsel 1 , B. Hsiao 2 , H. Huang 3 , T. Irving 4 , A. Menzel 5 , L. Pollack 6 , C. Riekel 7 , J. Rubert 8 , H. Tsuruta 9 , L. Yang 10 1 University of Massachusetts, 2 Stony Brook University, 3 Rice University, 4 IIT, 5SLS, 6 Cornell University, 7 European Synchrotron Radiation Facility, 8 NEU, 9 Stanford Synchrotron Radiation Lightsource, 10 Brookhaven National Laboratory TECHNIQUES AND CAPABILITIES APPLICATIONS ADDITIONAL INFORMATION * Energy range 2-20keV using undulator source. Simultaneous SAXS/WAXS to cover 0.003-3Å -1 at 12keV with 1 micron spot size * Time-resolved solution scattering with resolution of (1) microseconds to milliseconds using continuous-flow mixing (5µm x 10µm spot size) and (2) milliseconds using stopped-

169

Improved constraints on dark energy from Chandra X-ray observations of the largest relaxed galaxy clusters  

E-Print Network (OSTI)

We present constraints on the mean matter density, Omega_m, dark energy density, Omega_de, and the dark energy equation of state parameter, w, using Chandra measurements of the X-ray gas mass fraction (fgas) in 42 hot (kT>5keV), X-ray luminous, dynamically relaxed galaxy clusters spanning the redshift range 0.05energy has a negligible effect on the measurements, we measure Omega_m=0.28+-0.06 (68% confidence, using standard priors on the Hubble Constant, H_0, and mean baryon density, Omega_bh^2). Analyzing the data for all 42 clusters, employing only weak priors on H_0 and Omega_bh^2, we obtain a similar result on Omega_m and detect the effects of dark energy on the distances to the clusters at ~99.99% confidence, with Omega_de=0.86+-0.21 for a non-flat LCDM model. The detection of dark energy is comparable in significance to recent SNIa studies and represents strong, independent evidence for cosmic acceleration. Systematic scatter remains undetected in the fgas data, despite a weighted mean statistical scatter in the distance measurements of only ~5%. For a flat cosmology with constant w, we measure Omega_m=0.28+-0.06 and w=-1.14+-0.31. Combining the fgas data with independent constraints from CMB and SNIa studies removes the need for priors on Omega_bh^2 and H_0 and leads to tighter constraints: Omega_m=0.253+-0.021 and w=-0.98+-0.07 for the same constant-w model. More general analyses in which we relax the assumption of flatness and/or allow evolution in w remain consistent with the cosmological constant paradigm. Our analysis includes conservative allowances for systematic uncertainties. The small systematic scatter and tight constraints bode well for future dark energy studies using the fgas method. (Abridged)

S. W. Allen; D. A. Rapetti; R. W. Schmidt; H. Ebeling; G. Morris; A. C. Fabian

2007-06-01T23:59:59.000Z

170

GRPANL: a program for fitting complex peak groupings for gamma and x-ray energies and intensities  

SciTech Connect

GRPANL is a general-purpose peak-fitting program that calculates gamma-ray and x-ray energies and intensities from a given spectral region. The program requires that the user supply input information such as the first and last channels of the region, the channels to be used as pre- and post-region background, the system gain and zero-intercept, and a list of approximate energy values at which peaks occur in the region. Because the peak position and peak-shape parameters enter nonlinearly into the peak-fitting algorithm, an iterative least-square procedure is used in the fitting process. The program iterates until either all convergence criteria are met or ten iterations have elapsed. The code described here allows for twenty free parameters and a region as large as 240 data channels. This code runs on an LSI-11 computer with 32K memory and disk-storage capability.

Gunnink, R.; Ruhter, W.D.

1980-01-01T23:59:59.000Z

171

Rise time measurement for ultrafast X-ray pulses  

Science Conference Proceedings (OSTI)

A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

Celliers, Peter M. (Berkeley, CA); Weber, Franz A. (Oakland, CA); Moon, Stephen J. (Tracy, CA)

2005-04-05T23:59:59.000Z

172

Rise Time Measurement for Ultrafast X-Ray Pulses  

DOE Patents (OSTI)

A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

Celliers, Peter M.; Weber, Franz A.; Moon, Stephen J.

2005-04-05T23:59:59.000Z

173

Analysis of porosity in lower Ismay phylloid algal packstone using high-resolution computed x-ray tomography  

SciTech Connect

Three-dimensional images of porosity were created using high- resolution computed tomographic (CT) analysis as part of a larger study of phylloid algal packstone from bioherms in the lower Ismay (Des Moinesian, Paradox Formation). The sample imaged was collected at Eight Foot Rapids along the San Juan River in southeastern Utah 40 km west of the Aneth field. The larger study includes analysis of lithofacies, diagenesis, and quantitative analysis of porosity. Our goal is to predictively model porosity in phylloid algal reservoirs. Field observations suggest a relationship between porosity and lithology. Porosity is best established in phylloid algal packstone such as the one chosen for three-dimensional imaging. Locally, porosity is also associated with fractures and stylolitization. Petrographic observations suggest that formation of moldic and vuggy porosity in this sample was controlled by multiple episodes of dissolution and infill of blocky calcite. Porosity in thin section (5.94%) was measured using NIH Image (public domain) on a Macintosh desktop computer. High-resolution CT radiography of a 2.3 cm diameters cm high, cylindrical sample generated a series of 110 images at 0.1 mm intervals. Three-dimensional isosurface images of porosity reveal the degree of interconnection, pore size (up to 12 mm long and from 0.5 mm to 7 mm wide), and their highly irregular shape. These images can also be used to create animations of scans through the rock and three-dimensional, rotating images of the pores.

Beall, J.L., Gordon, I.T.; Gournay, J.P. (Univ. of Texas, Austin, TX (United States)) (and others)

1996-01-01T23:59:59.000Z

174

Energy band alignment of InGaZnO{sub 4}/Si heterojunction determined by x-ray photoelectron spectroscopy  

SciTech Connect

X-ray photoelectron spectroscopy was utilized to determine the valence band offset ({Delta}E{sub V}) of the InGaZnO{sub 4} (IGZO)/Si heterojunction. The IGZO films were grown on Si (100) using radio frequency magnetron sputtering. A value of {Delta}E{sub V} = 2.53 eV was obtained by using In 3d{sub 5/2}, Ga 2p{sub 3/2} core energy levels as references. Taking into consideration the experimental band gap of 3.20 eV of the IGZO, this would result in a conduction band offset {Delta}E{sub C} = 0.45 eV in this heterostructure.

Xie Zhangyi; Lu Hongliang; Xu Saisheng; Geng Yang; Sun Qingqing; Ding Shijin; Zhang, David Wei [State Key Laboratory of ASIC and System, Department of Microelectronics, Fudan University, Shanghai 200433 (China)

2012-12-17T23:59:59.000Z

175

X-ray lasers and methods utilizing two component driving illumination provided by optical laser means of relatively low energy and small physical size  

DOE Patents (OSTI)

An X-ray laser (10), and related methodology, are disclosed wherein an X-ray laser target (12) is illuminated with a first pulse of optical laser radiation (14) of relatively long duration having scarcely enough energy to produce a narrow and linear cool plasma of uniform composition (38). A second, relatively short pulse of optical laser radiation (18) is uniformly swept across the length, from end to end, of the plasma (38), at about the speed of light, to consecutively illuminate continuously succeeding portions of the plasma (38) with optical laser radiation having scarcely enough energy to heat, ionize, and invert them into the continuously succeeding portions of an X-ray gain medium. This inventive double pulse technique results in a saving of more than two orders of magnitude in driving optical laser energy, when compared to the conventional single pulse approach.

Rosen, Mordecai D. (Berkeley, CA); Matthews, Dennis L. (El Granada, CA)

1991-01-01T23:59:59.000Z

176

X-Ray Topography  

Science Conference Proceedings (OSTI)

Sep 17, 2009 ... Stress Mapping Analysis by Ray Tracing (SMART): A New Technique ... technique of synchrotron X-ray topography, where a grid made out of...

177

Viewing spin structures with soft x-ray microscopy  

SciTech Connect

The spin of the electron and its associated magnetic moment marks the basic unit for magnetic properties of matter. Magnetism, in particular ferromagnetism and antiferromagnetism is described by a collective order of these spins, where the interaction between individual spins reflects a competition between exchange, anisotropy and dipolar energy terms. As a result the energetically favored ground state of a ferromagnetic system is a rather complex spin configuration, the magnetic domain structure. Magnetism is one of the eldest scientific phenomena, yet it is one of the most powerful and versatile utilized physical effects in modern technologies, such as in magnetic storage and sensor devices. To achieve highest storage density, the relevant length scales, such as the bit size in disk drives is now approaching the nanoscale and as such further developments have to deal with nanoscience phenomena. Advanced characterization tools are required to fully understand the underlying physical principles. Magnetic microscopes using polarized soft X-rays offer a close-up view into magnetism with unique features, these include elemental sensitivity due to X-ray magnetic dichroism effects as contrast mechanism, high spatial resolution provided by state-of-the-art X-ray optics and fast time resolution limited by the inherent time structure of current X-ray sources, which will be overcome with the introduction of ultrafast and high brilliant X-ray sources.

Fischer, Peter

2010-06-01T23:59:59.000Z

178

Flat Field Anomalies in an X-ray CCD Camera Measured Using a Manson X-ray Source  

SciTech Connect

The Static X-ray Imager (SXI) is a diagnostic used at the National Ignition Facility (NIF) to measure the position of the X-rays produced by lasers hitting a gold foil target. The intensity distribution taken by the SXI camera during a NIF shot is used to determine how accurately NIF can aim laser beams. This is critical to proper NIF operation. Imagers are located at the top and the bottom of the NIF target chamber. The CCD chip is an X-ray sensitive silicon sensor, with a large format array (2k x 2k), 24 ?m square pixels, and 15 ?m thick. A multi-anode Manson X-ray source, operating up to 10kV and 10W, was used to characterize and calibrate the imagers. The output beam is heavily filtered to narrow the spectral beam width, giving a typical resolution E/?E?10. The X-ray beam intensity was measured using an absolute photodiode that has accuracy better than 1% up to the Si K edge and better than 5% at higher energies. The X-ray beam provides full CCD illumination and is flat, within 1% maximum to minimum. The spectral efficiency was measured at 10 energy bands ranging from 930 eV to 8470 eV. We observed an energy dependent pixel sensitivity variation that showed continuous change over a large portion of the CCD. The maximum sensitivity variation occurred at 8470 eV. The geometric pattern did not change at lower energies, but the maximum contrast decreased and was not observable below 4 keV. We were also able to observe debris, damage, and surface defects on the CCD chip. The Manson source is a powerful tool for characterizing the imaging errors of an X-ray CCD imager. These errors are quite different from those found in a visible CCD imager.

M. J. Haugh and M. B. Schneider

2008-10-31T23:59:59.000Z

179

X-ray transmissive debris shield  

DOE Patents (OSTI)

A composite window structure is described for transmitting x-ray radiation and for shielding radiation generated debris. In particular, separate layers of different x-ray transmissive materials are laminated together to form a high strength, x-ray transmissive debris shield which is particularly suited for use in high energy fluences. In one embodiment, the composite window comprises alternating layers of beryllium and a thermoset polymer.

Spielman, Rick B. (Albuquerque, NM)

1994-01-01T23:59:59.000Z

180

X-ray lasers and methods utilizing two component driving illumination provided by optical laser means of relatively low energy and small physical size  

DOE Patents (OSTI)

It is an object of this invention to provide an X-ray laser that is driven by an optical laser or lasers of relatively low energy and small physical size. Another object of this invention is to provide a method of driving an X-ray laser with an optical laser or lasers of relatively low energy and small physical size. Additional objects, advantages and novel features of the invention are set forth in part in the description included in this report. The objects and advantages of the invention may be realized and attained by means of the instrumentalities and combinations particularly pointed out in the appended claims. 8 figs.

Rosen, M.D.; Matthews, D.L.

1989-10-18T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

CANDIDATE X-RAY-EMITTING OB STARS IN THE CARINA NEBULA IDENTIFIED VIA INFRARED SPECTRAL ENERGY DISTRIBUTIONS  

Science Conference Proceedings (OSTI)

We report the results of a new survey of massive, OB stars throughout the Carina Nebula using the X-ray point source catalog provided by the Chandra Carina Complex Project (CCCP) in conjunction with infrared (IR) photometry from the Two Micron All-Sky Survey and the Spitzer Space Telescope Vela-Carina survey. Mid-IR photometry is relatively unaffected by extinction, hence it provides strong constraints on the luminosities of OB stars, assuming that their association with the Carina Nebula, and hence their distance, is confirmed. We fit model stellar atmospheres to the optical (UBV) and IR spectral energy distributions (SEDs) of 182 OB stars with known spectral types and measure the bolometric luminosity and extinction for each star. We find that the extinction law measured toward the OB stars has two components: A{sub V} = 1-1.5 mag produced by foreground dust with a ratio of total-to-selective absorption R{sub V} = 3.1 plus a contribution from local dust with R{sub V} > 4.0 in the Carina molecular clouds that increases as A{sub V} increases. Using X-ray emission as a strong indicator of association with Carina, we identify 94 candidate OB stars with L{sub bol} {approx}> 10{sup 4} L{sub sun} by fitting their IR SEDs. If the candidate OB stars are eventually confirmed by follow-up spectroscopic observations, the number of cataloged OB stars in the Carina Nebula will increase by {approx}50%. Correcting for incompleteness due to OB stars falling below the L{sub bol} cutoff or the CCCP detection limit, these results potentially double the size of the young massive stellar population.

Povich, Matthew S.; Townsley, Leisa K.; Broos, Patrick S.; Getman, Konstantin V. [Department of Astronomy and Astrophysics, Pennsylvania State University, 525 Davey Laboratory, University Park, PA 16802 (United States); Gagne, Marc [Department of Geology and Astronomy, West Chester University, West Chester, PA 19383 (United States); Babler, Brian L.; Meade, Marilyn R.; Townsend, Richard H. D. [Department of Astronomy, University of Wisconsin, 475 N. Charter Street, Madison, WI 53706 (United States); Indebetouw, Remy; Majewski, Steven R. [Department of Astronomy, University of Virginia, P.O. Box 400325, Charlottesville, VA 22904-4325 (United States); Robitaille, Thomas P., E-mail: povich@astro.psu.edu [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States)

2011-05-01T23:59:59.000Z

182

X-ray beamsplitter  

DOE Patents (OSTI)

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

Ceglio, Natale M. (Livermore, CA); Stearns, Daniel S. (Mountain View, CA); Hawryluk, Andrew M. (Modesto, CA); Barbee, Jr., Troy W. (Palo Alto, CA)

1989-01-01T23:59:59.000Z

183

X-ray generator  

DOE Patents (OSTI)

Apparatus and method for producing coherent secondary x-rays that are controlled as to direction by illuminating a mixture of high z and low z gases with an intense burst of primary x-rays. The primary x-rays are produced with a laser activated plasma, and these x-rays strip off the electrons of the high z atoms in the lasing medium, while the low z atoms retain their electrons. The neutral atoms transfer electrons to highly excited states of the highly striped high z ions giving an inverted population which produces the desired coherent x-rays. In one embodiment, a laser, light beam provides a laser spark that produces the intense burst of coherent x-rays that illuminates the mixture of high z and low z gases, whereby the high z atoms are stripped while the low z ones are not, giving the desired mixture of highly ionized and neutral atoms. To this end, the laser spark is produced by injecting a laser light beam, or a plurality of beams, into a first gas in a cylindrical container having an adjacent second gas layer co-axial therewith, the laser producing a plasma and the intense primary x-rays in the first gas, and the second gas containing the high and low atomic number elements for receiving the primary x-rays, whereupon the secondary x-rays are produced therein by stripping desired ions in a neutral gas and transfer of electrons to highly excited states of the stripped ions from the unionized atoms. Means for magnetically confining and stabilizing the plasma are disclosed for controlling the direction of the x-rays.

Dawson, John M. (Los Angeles, CA)

1976-01-01T23:59:59.000Z

184

A fine-focusing x-ray source using carbon-nanofiber field emitter  

Science Conference Proceedings (OSTI)

A fine-focusing x-ray source has been constructed employing a field electron emitter prepared by growing carbon-nanofibers (CNFs) on a metal tip. The x-ray source is composed of a CNF field electron emitter, an electrostatic lens, two magnetic lenses, and a W-target for generating x-rays by electron impact. The CNFs provided field electrons with a current density of J{approx}5x10{sup 9} A/m{sup 2}, which was evaluated with the aid of Fowler-Nordheim theory. The electron beam extracted from the CNF emitter was accelerated to the energies of E=10-25 keV, and then focused by the lenses. By recording the x-ray images of test charts, the optimum resolution of the x-ray source was estimated to be approximately D{sub x}=0.5 {mu}m.

Sugimoto, W.; Sugita, S.; Sakai, Y.; Goto, H.; Watanabe, Y.; Ohga, Y.; Kita, S. [Graduate School of Engineering, Nagoya Institute of Technology, Gokiso-cho, Showa-ku, Nagoya 466-8555 (Japan); Ohara, T. [Topcon Corporation, 75-1 Hasunuma-cho, Itabashi-ku, Tokyo 174-8580 (Japan)

2010-08-15T23:59:59.000Z

185

Real time x-ray studies during nanostructure formation on silicon via low energy ion beam irradiation using ultrathin iron films  

SciTech Connect

Real time grazing incidence small angle x-ray scattering and x-ray fluorescence (XRF) are used to elucidate nanodot formation on silicon surfaces during low energy ion beam irradiation of ultrathin iron-coated silicon substrates. Four surface modification stages were identified: (1) surface roughening due to film erosion, (2) surface smoothing and silicon-iron mixing, (3) structure formation, and (4) structure smoothing. The results conclude that 2.5 Multiplication-Sign 10{sup 15} iron atoms in a 50 nm depth triggers surface nanopatterning with a correlated nanodots distance of 25 nm. Moreover, there is a wide window in time where the surface can have correlated nanostructures even after the removal of all the iron atoms from the sample as confirmed by XRF and ex-situ x-ray photoelectron spectroscopy (XPS). In addition, in-situ XPS results indicated silicide formation, which plays a role in the structure formation mechanism.

El-Atwani, Osman [School of Materials Engineering, Purdue University, West Lafayette, Indiana 47907 (United States); Birck Nanotechnology Center, Purdue University, West Lafayette, Indiana 47907 (United States); Suslova, Anastassiya; Gonderman, Sean; Fowler, Justin; El-Atwani, Mohamad [School of Nuclear Engineering, Purdue University, West Lafayette, Indiana, 47907 (United States); DeMasi, Alexander; Ludwig, Karl [Physics Department, Boston University, Boston, Massachusetts 02215 (United States); Paul Allain, Jean [School of Materials Engineering, Purdue University, West Lafayette, Indiana 47907 (United States); Birck Nanotechnology Center, Purdue University, West Lafayette, Indiana 47907 (United States); School of Nuclear Engineering, Purdue University, West Lafayette, Indiana, 47907 (United States)

2012-12-24T23:59:59.000Z

186

Photon Sciences | Beamlines | XPD: X-ray Powder Diffraction  

NLE Websites -- All DOE Office Websites (Extended Search)

XPD: X-ray Powder Diffraction XPD: X-ray Powder Diffraction Poster | Fact Sheet | Preliminary Design Report Scientific Scope XPD is a tunable facility with the ability to collect diffraction data at high x-ray energies (40keV-80keV), offering rapid acquisition (millisecond) and high angular resolution capabilities on the same instrument. XPD addresses future scientific challenges in, for example, hydrogen storage, CO2 sequestration, advanced structural ceramics, catalysis, and materials processing. Such materials of high technological value often are complex, nanostructured and heterogeneous. The scientific grand challenge is to obtain robust and quantitative (micro)structural information, not only in the ground state at ambient conditions, but also in situ or in operando with varying temperature, pressure, magnetic/electric/stress

187

High-brightness, high-spatial-resolution, 6.151 keV x-ray imaging of inertial confinement fusion capsule implosion and complex hydrodynamics experiments on Sandia's Z accelerator (invited)  

SciTech Connect

When used for the production of an x-ray imaging backlighter source on Sandia National Laboratories' 20 MA, 100 ns rise-time Z accelerator [M. K. Matzen et al., Phys. Plasmas 12, 055503 (2005)], the terawatt-class, multikilojoule, 526.57 nm Z-Beamlet laser (ZBL) [P. K. Rambo et al., Appl. Opt. 44, 2421 (2005)], in conjunction with the 6.151 keV, Mn-He{sub {alpha}} curved-crystal imager [D. B. Sinars et al., Rev. Sci. Instrum. 75, 3672 (2004)], is capable of providing a high quality x radiograph per Z shot for various high-energy-density physics experiments. Enhancements to this imaging system during 2005 have led to the capture of inertial confinement fusion capsule implosion and complex hydrodynamics images of significantly higher quality. The three main improvements, all leading effectively to enhanced image plane brightness, were bringing the source inside the Rowland circle to approximately double the collection solid angle, replacing direct exposure film with Fuji BAS-TR2025 image plate (read with a Fuji BAS-5000 scanner), and generating a 0.3-0.6 ns, {approx}200 J prepulse 2 ns before the 1.0 ns, {approx}1 kJ main pulse to more than double the 6.151 keV flux produced compared with a single 1 kJ pulse. It appears that the 20{+-}5 {mu}m imaging resolution is limited by the 25 {mu}m scanning resolution of the BAS-5000 unit, and to this end, a higher resolution scanner will replace it. ZBL is presently undergoing modifications to provide two temporally separated images ('two-frame') per Z shot for this system before the accelerator closes down in summer 2006 for the Z-refurbished (ZR) upgrade. In 2008, after ZR, it is anticipated that the high-energy petawatt (HEPW) addition to ZBL will be completed, possibly allowing high-energy 11.2224 and 15.7751 keV K{alpha}{sub 1} curved-crystal imaging to be performed. With an ongoing several-year project to develop a highly sensitive multiframe ultrafast digital x-ray camera (MUDXC), it is expected that two-frame HEPW 11 and 16 keV imaging and four-frame ZBL 6.151 keV curved-crystal imaging will be possible. MUDXC will be based on the technology of highly cooled silicon and germanium photodiode arrays and ultrafast, radiation-hardened integrated circuitry.

Bennett, G. R.; Sinars, D. B.; Wenger, D. F.; Cuneo, M. E.; Adams, R. G.; Barnard, W. J.; Beutler, D. E.; Burr, R. A.; Campbell, D. V.; Claus, L. D.; Foresi, J. S.; Johnson, D. W.; Keller, K. L.; Lackey, C.; Leifeste, G. T.; McPherson, L. A.; Mulville, T. D.; Neely, K. A.; Rambo, P. K.; Rovang, D. C. [Sandia National Laboratories, P.O. Box 5800, Albuquerque, New Mexico 87185-1106 (United States)] (and others)

2006-10-15T23:59:59.000Z

188

A multi-crystal wavelength dispersive x-ray spectrometer  

Science Conference Proceedings (OSTI)

A multi-crystal wavelength dispersive hard x-ray spectrometer with high-energy resolution and large solid angle collection is described. The instrument is specifically designed for time-resolved applications of x-ray emission spectroscopy (XES) and x-ray Raman scattering (XRS) at X-ray Free Electron Lasers (XFEL) and synchrotron radiation facilities. It also simplifies resonant inelastic x-ray scattering (RIXS) studies of the whole 2d RIXS plane. The spectrometer is based on the Von Hamos geometry. This dispersive setup enables an XES or XRS spectrum to be measured in a single-shot mode, overcoming the scanning needs of the Rowland circle spectrometers. In conjunction with the XFEL temporal profile and high-flux, it is a powerful tool for studying the dynamics of time-dependent systems. Photo-induced processes and fast catalytic reaction kinetics, ranging from femtoseconds to milliseconds, will be resolvable in a wide array of systems circumventing radiation damage.

Alonso-Mori, Roberto; Montanez, Paul; Delor, James; Bergmann, Uwe [LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Kern, Jan [LCLS, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Physical Biosciences Division, Lawrence Berkeley National Laboratory, Berkeley, California 94720-8099 (United States); Sokaras, Dimosthenis; Weng, Tsu-Chien; Nordlund, Dennis [SSRL, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States); Tran, Rosalie; Yachandra, Vittal K.; Yano, Junko [Physical Biosciences Division, Lawrence Berkeley National Laboratory, Berkeley, California 94720-8099 (United States)

2012-07-15T23:59:59.000Z

189

Photon Sciences | Beamlines | HXN: Hard X-ray Nanoprobe  

NLE Websites -- All DOE Office Websites (Extended Search)

HXN: Hard X-ray Nanoprobe HXN: Hard X-ray Nanoprobe Poster | Fact Sheet | Preliminary Design Report Scientific Scope The Hard X-ray Nanoprobe beamline and endstation instruments (HXN) will be designed and constructed to explore new frontiers of hard x-ray microscopy applications with the highest achievable spatial resolution. Currently the available spatial resolution for scientific applications, provided by scanning x-ray microscopes in the hard x-ray regime, is limited to ~50nm, which is still insufficient for probing the nanoscale interfacial structures critical in determining properties and functionalities of material and biological systems. The HXN beamline aims to enable x-ray experiments at spatial resolutions ranging from 10 to 30 nm with an ultimate goal of ~1 nm. Beamline Description

190

Gamma Radiation & X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Gamma Radiation and X-Rays 1. Gamma radiation and X-rays are electromagnetic radiation like visible light, radio waves, and ultraviolet light. These electromagnetic radiations...

191

X-ray flashes and X-ray rich gamma ray bursts. Memorie della Societa Astronomica Italiana  

E-Print Network (OSTI)

Abstract. X-ray flashes are detected in the Wide Field Cameras on BeppoSAX in the energy range 2-25 keV as bright X-ray sources lasting of the order of minutes, but remaining undetected in the Gamma Ray Bursts Monitor on BeppoSAX. They have properties very similar to the x-ray counterparts of GRBs and account for some of the Fast X-ray Transient events seen in almost every x-ray satellite. We review their X-ray properties and show that x-ray flashes are in fact very soft, x-ray rich, untriggered gamma ray bursts, in which the peak energy in 2-10 keV x-rays could be up to a factor of 100 larger than the peak energy in the 50-300 keV gamma ray range. The frequency is ? 100 yr ?1. 1 Fast X-ray Transients/High-latitude X-ray Transients Fast X-ray Transients have been observed with many x-ray satellites. In particular they are seen with x-ray instruments that scan the entire sky on a regular basis. Such events are detected in one sky scan and disappeared in the next, typically limiting the duration to be longer than a minute and shorter than a few hours. For this reason they are called Fast Transients. The first transients

John Heise; Jean In t Z; Peter M. Woods

2001-01-01T23:59:59.000Z

192

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless X-Ray Imaging in Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

193

A von Hamos x-ray spectrometer based on a segmented-type diffraction crystal for single-shot x-ray emission spectroscopy and time-resolved resonant inelastic x-ray scattering studies  

SciTech Connect

We report on the design and performance of a wavelength-dispersive type spectrometer based on the von Hamos geometry. The spectrometer is equipped with a segmented-type crystal for x-ray diffraction and provides an energy resolution in the order of 0.25 eV and 1 eV over an energy range of 8000 eV-9600 eV. The use of a segmented crystal results in a simple and straightforward crystal preparation that allows to preserve the spectrometer resolution and spectrometer efficiency. Application of the spectrometer for time-resolved resonant inelastic x-ray scattering and single-shot x-ray emission spectroscopy is demonstrated.

Szlachetko, J. [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Institute of Physics, Jan Kochanowski University, 25-406 Kielce (Poland); Nachtegaal, M.; Boni, E. de; Willimann, M.; Safonova, O.; Sa, J.; Smolentsev, G.; Szlachetko, M.; Bergamaschi, A.; Schmitt, B.; David, C.; Luecke, A. [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Bokhoven, J. A. van [Paul Scherrer Institut, 5232 Villigen PSI (Switzerland); Institute for Chemical and Bioengineering, ETH Zurich, 8093 Zuerich (Switzerland); Dousse, J.-Cl.; Hoszowska, J.; Kayser, Y. [Department of Physics, University of Fribourg, 1700 Fribourg (Switzerland); Jagodzinski, P. [University of Technology, Kielce (Poland)

2012-10-15T23:59:59.000Z

194

A System for Conducting Sophisticated Mechanical Tests in Situ with High Energy Synchrotron X-Rays Final Technical Report  

SciTech Connect

This is the final technical report for the SBIR Phase I project titled 'A System for Conducting Sophisticated Mechanical Tests in Situ with High Energy Synchrotron X-Rays.' Experiments using diffraction of synchrotron radiation that help scientists understand engineering material failure modes, such as fracture and fatigue, require specialized machinery. This machinery must be able to induce these failure modes in a material specimen while adhering to strict size, weight, and geometric limitations prescribed by diffraction measurement techniques. During this Phase I project, Mechanical Solutions, Inc. (MSI) developed one such machine capable of applying uniaxial mechanical loading to a material specimen in both tension and compression, with zero backlash while transitioning between the two. Engineers currently compensate for a lack of understanding of fracture and fatigue by employing factors of safety in crucial system components. Thus, mechanical and structural parts are several times bigger, thicker, and heavier than they need to be. The scientific discoveries that result from diffraction experiments which utilize sophisticated mechanical loading devices will allow for broad material, weight, fuel, and cost savings in engineering design across all industries, while reducing the number of catastrophic failures in transportation, power generation, infrastructure, and all other engineering systems. With an existing load frame as the starting point, the research focused on two main areas: (1) the design of a specimen alignment and gripping system that enables pure uniaxial tension and compression loading (and no bending, shear, or torsion), and (2) development of a feedback control system that is adaptive and thus can maintain a load set point despite changing specimen material properties (e.g. a decreasing stiffness during yield).

Jeremy Weiss

2012-08-02T23:59:59.000Z

195

Imaging of High-Energy X-Ray Emission from Cryogenic Thermonuclear Fuel Implosions on the NIF  

SciTech Connect

Accurately assessing and optimizing the implosion performance of inertial confinement fusion capsules is a crucial step to achieving ignition on the NIF. We have applied differential filtering (matched Ross filter pairs) to provide spectrally resolved time-integrated absolute x-ray self-emission images of the imploded core of cryogenic layered targets. Using bremsstrahlung assumptions, the measured absolute x-ray brightness allows for the inference of electron temperature, electron density, hot spot mass, mix mass, and pressure. Current inertial confinement fusion (ICF) experiments conducted on the National Ignition Facility (NIF) seek to indirectly drive a spherical implosion, compressing and igniting a deuterium-tritium fuel. This DT fuel capsule is cryogenically prepared as a solid ice layer surrounded by a low-Z ablator material. Ignition will occur when the hot spot approaches sufficient temperature ({approx}3-4 keV) and {rho}R ({approx}0.3 g/cm{sup 2}) such that alpha deposition can further heat the hot spot and generate a self-sustaining burn wave. During the implosion, the fuel mass becomes hot enough to emit large amounts of x-ray radiation, the spectra and spatial variation of which contains key information that can be used to evaluate the implosion performance. The Ross filter diagnostic employs differential filtering to provide spectrally resolved, time-integrated, absolute x-ray self-emission images of the imploded core of cryogenic layered targets.

Ma, T

2012-05-01T23:59:59.000Z

196

A New Measurement of Kaonic Hydrogen X rays  

E-Print Network (OSTI)

The $\\bar{K}N$ system at threshold is a sensitive testing ground for low energy QCD, especially for the explicit chiral symmetry breaking. Therefore, we have measured the $K$-series x rays of kaonic hydrogen atoms at the DA$\\Phi$NE electron-positron collider of Laboratori Nazionali di Frascati, and have determined the most precise values of the strong-interaction energy-level shift and width of the $1s$ atomic state. As x-ray detectors, we used large-area silicon drift detectors having excellent energy and timing resolution, which were developed especially for the SIDDHARTA experiment. The shift and width were determined to be $\\epsilon_{1s} = -283 \\pm 36 \\pm 6 {(syst)}$ eV and $\\Gamma_{1s} = 541 \\pm 89 {(stat)} \\pm 22 {(syst)}$ eV, respectively. The new values will provide vital constraints on the theoretical description of the low-energy $\\bar{K}N$ interaction.

M. Bazzi; G. Beer; L. Bombelli; A. M. Bragadireanu; M. Cargnelli; G. Corradi; C. Curceanu; A. d'Uffizi; C. Fiorini; T. Frizzi; F. Ghio; B. Girolami; C. Guaraldo; R. S. Hayano; M. Iliescu; T. Ishiwatari; M. Iwasaki; P. Kienle; P. Levi Sandri; A. Longoni; V. Lucherini; J. Marton; S. Okada; D. Pietreanu; T. Ponta; A. Rizzo; A. Romero Vidal; A. Scordo; H. Shi; D. L. Sirghi; F. Sirghi; H. Tatsuno; A. Tudorache; V. Tudorache; O. Vazquez Doce; E. Widmann; J. Zmeskal

2011-05-16T23:59:59.000Z

197

Ellipsoidal and parabolic glass capillaries as condensers for x-ray microscopes  

Science Conference Proceedings (OSTI)

Single-bounce ellipsoidal and paraboloidal glass capillary focusing optics have been fabricated for use as condenser lenses for both synchrotron and tabletop x-ray microscopes in the x-ray energy range of 2.5-18 keV. The condenser numerical apertures (NAs) of these devices are designed to match the NA of x-ray zone plate objectives, which gives them a great advantage over zone plate condensers in laboratory microscopes. The fabricated condensers have slope errors as low as 20 {mu}rad rms. These capillaries provide a uniform hollow-cone illumination with almost full focusing efficiency, which is much higher than what is available with zone plate condensers. Sub-50 nm resolution at 8 keV x-ray energy was achieved by utilizing this high-efficiency condenser in a laboratory microscope based on a rotating anode generator.

Zeng Xianghui; Duewer, Fred; Feser, Michael; Huang, Carson; Lyon, Alan; Tkachuk, Andrei; Yun Wenbing

2008-05-01T23:59:59.000Z

198

Strengthened lithium for x-ray blast windows  

Science Conference Proceedings (OSTI)

Lithium's high x-ray transparency makes it an attractive material for windows intended to protect soft x-ray diagnostics in high energy density experiments. Pure lithium is soft and weak, but lithium mixed with lithium hydride powder becomes harder and stronger, in principle without any additional x-ray absorption. A comparison with the standard material for x-ray windows, beryllium, suggests that lithium or lithium strengthened by lithium hydride may well be an excellent option for such windows.

Pereira, N. R. [Ecopulse Inc., P.O. Box 528, Springfield, Virginia 22150 (United States); Imam, M. A. [Materials Science and Technology Division, Naval Research Laboratory, Washington, DC 20375 (United States)

2008-05-15T23:59:59.000Z

199

Imaging of high-energy x-ray emission from cryogenic thermonuclear fuel implosions on the NIF  

Science Conference Proceedings (OSTI)

Accurately assessing and optimizing the implosion performance of inertial confinement fusion capsules is a crucial step to achieving ignition on the NIF. We have applied differential filtering (matched Ross filter pairs) to provide broadband time-integrated absolute x-ray self-emission images of the imploded core of cryogenic layered implosions. This diagnostic measures the temperature- and density-sensitive bremsstrahlung emission and provides estimates of hot spot mass, mix mass, and pressure.

Ma, T.; Izumi, N.; Tommasini, R.; Bradley, D. K.; Bell, P.; Cerjan, C. J.; Dixit, S.; Doeppner, T.; Jones, O.; Landen, O. L.; LePape, S.; Mackinnon, A. J.; Park, H.-S.; Patel, P. K.; Prasad, R. R.; Ralph, J.; Smalyuk, V. A.; Springer, P. T.; Suter, L.; Town, R. P. J. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); and others

2012-10-15T23:59:59.000Z

200

Application of high-energy x-rays and pair-distribution-function analysis to nano-scale structural studies in catalysis.  

SciTech Connect

We investigate the structure of supported Pt catalysts using high-energy X-ray scattering coupled with Pair-Distribution-Function (PDF) analysis. Recently, experimental approaches that enable the collection of PDF data in situ have been developed with time-resolution sufficient to study the structure of Pt nano-particles as they form. The differential PDF approach is utilized which allows the atom-atom correlations involving only Pt to be selectively recovered, enabling structural investigation of the supported particles and the mechanism of their formation. In parallel to the in situ analysis, we have examined samples prepared ex situ. Data collected on the ex situ samples show that the initial deposition of Pt{sup 4+} occurs as the PtCl{sub 6}{sup 2-} species which are retained even when annealed in an oxygen atmosphere. The Pt differential PDFs of the samples reduced in hydrogen at 200 and 500 C indicated nano-crystalline face-centered-cubic (fcc) metallic Pt particles. The ex situ reduced samples also contain a weak correlations at 2.1 {angstrom}, which we assign to Pt-O interactions between the particles and the support surface. The in situ experiments, following the reduction of Pt{sup 4+} from 0 to 227 C, indicate that the initial Pt nano-particles formed are ca. 1 nm in size, and become larger and more crystalline by 200 C. The data suggest a particle growth mechanism where the initial particles that form are small (<1 nm), then agglomerate into ensembles of many small particles and lastly anneal to form larger well-ordered particles. Lastly, we discus potential future developments in operando PDF studies, and identify opportunities for synchronous application of complementary methods.

Chupas, P. J.; Chapman, K. W.; Chen, H.; Grey, C.; X-Ray Science Division; State Univ. of New York

2009-07-30T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

Full-field Transmission X-ray Microscopy | Stanford Synchrotron Radiation  

NLE Websites -- All DOE Office Websites (Extended Search)

BL6-2c / Transmission X-ray Microscopy BL6-2c / Transmission X-ray Microscopy Home Researchers Publications Science Highlights Department of Energy Office of Science Search form Search Search TXM Search Full-field Transmission X-ray Microscopy Capabilities Full-field TXM is an excellent method to examine nanoscale heterogeneties in many materials, including complex hierarchical systems such as catalysts, fuel cells and battery electrodes, and biological and environmental samples, at 30 nm resolution.The transmission X-ray microscope (TXM) on beam line 6-2c at SSRL is capable of 2D imaging and tomography, as well as spectroscopic imaging for 2D and 3D elemental mapping and chemical mapping over tens of microns (up to mm in 2D). The field of view (FOV) is 30 microns, but mosaic images can be collected to

202

X-ray grid-detector apparatus  

DOE Patents (OSTI)

A hybrid grid-detector apparatus for x-ray systems wherein a microchannel plate structure has an air-interspaced grid portion and a phosphor/optical fluid-filled grid portion. The grids are defined by multiple adjacent channels separated by lead-glass septa. X-rays entering the air-interspaced grid portion at an angle of impingement upon the septa are attenuated, while non-impinging x-rays pass through to the phosphor/fluid filled portion. X-ray energy is converted to luminescent energy in the phosphor/fluid filled portion and the resultant beams of light are directed out of the phosphor/optical fluid filled portion to an imaging device.

Boone, John M. (Folsom, CA); Lane, Stephen M. (Oakland, CA)

1998-01-27T23:59:59.000Z

203

Argonne CNM: X-Ray Microscopy Capabilities  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Microscopy Facilities X-Ray Microscopy Facilities The Hard X-Ray Nanoprobe (HXN) facility provides scanning fluorescence, scanning diffraction, and full-field transmission and tomographic imaging capabilities with a spatial resolution of 30 nm over a spectral range of 6-12 keV. Modes of Operation Full-Field Transmission Imaging and Nanotomography X-ray transmission imaging uses both the absorption and phase shift of the X-ray beam by the sample as contrast mechanisms. Absorption contrast is used to map the sample density. Elemental constituents can be located by using differential edge contrast in this mode. Phase contrast can be highly sensitive to edges and interfaces even when the X-ray absorption is weak. These contrast mechanisms are exploited to image samples rapidly in full-field transmission mode under various environmental conditions, or combined with nanotomography methods to study the three-dimensional structure of complex and amorphous nanomaterials with the HXN.

204

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

205

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

206

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

207

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

208

X-ray Detection with Large Area Avalanche Photodiodes for ...  

Science Conference Proceedings (OSTI)

... The primary photon detector was a 12-element ... The overall energy range for the experiment was ... to directly detect X-rays with energies between 0.3 ...

2013-07-23T23:59:59.000Z

209

Fluctuation X-Ray Scattering  

SciTech Connect

The work supported by the grant was aimed at developing novel methods of finding the structures of biomolecules using x-rays from novel sources such as the x-ray free electron laser and modern synchrotrons

Saldin, PI: D. K.; Co-I's: J. C. H. Spence and P. Fromme

2013-01-25T23:59:59.000Z

210

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

211

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

212

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

213

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

214

X-ray Security Screening  

Science Conference Proceedings (OSTI)

National and International Standards for X-ray Security Screening Applications. Summary: The primary objective of this ...

2013-03-13T23:59:59.000Z

215

High-resolution x-ray guided three-dimensional diffuse optical tomography of joint tissues in hand osteoarthritis: Morphological and functional assessments  

SciTech Connect

Purpose: The aim of this study was to investigate the potential use of multimodality functional imaging techniques to identify the quantitative optical findings that can be used to distinguish between osteoarthritic and normal finger joints. Methods: Between 2006 and 2009, the distal interphalangeal finger joints from 40 female subjects including 22 patients and 18 healthy controls were examined clinically and scanned by a hybrid imaging system. This system integrated x-ray tomosynthetic setup with a diffuse optical imaging system. Optical absorption and scattering images were recovered based on a regularization-based hybrid reconstruction algorithm. A receiver operating characteristic curve was used to calculate the statistical significance of specific optical features obtained from osteoarthritic and healthy joints groups. Results: The three-dimensional optical and x-ray images captured made it possible to quantify optical properties and joint space width of finger joints. Based on the recovered optical absorption and scattering parameters, the authors observed statistically significant differences between healthy and osteoarthritis finger joints. Conclusions: The statistical results revealed that sensitivity and specificity values up to 92% and 100%, respectively, can be achieved when optical properties of joint tissues were used as classifiers. This suggests that these optical imaging parameters are possible indicators for diagnosing osteoarthritis and monitoring its progression.

Yuan Zhen; Zhang Qizhi; Sobel, Eric S.; Jiang Huabei [Department of Biomedical Engineering, University of Florida, Gainesville, Florida 32611 (United States); Division of Rheumatology, College of Medicine, University of Florida, Gainesville, Florida 32611 (United States); Department of Biomedical Engineering, University of Florida, Gainesville, Florida 32611 (United States)

2010-08-15T23:59:59.000Z

216

X-ray chemistry in envelopes around young stellar objects  

E-Print Network (OSTI)

We present chemical models of the envelope of a young stellar object (YSO) exposed to a central X-ray source. The models are applied to the massive star-forming region AFGL 2591 for different X-ray fluxes. The total X-ray ionization rate is dominated by the `secondary' ionization rate of H2 resulting from fast electrons. The carbon, sulphur and nitrogen chemistries are discussed. It is found that He+ and H3+ are enhanced and trigger a peculiar chemistry. Several molecular X-ray tracers are found and compared to tracers of the far ultraviolet (FUV) field. Like ultraviolet radiation fields, X-rays enhance simple hydrides, ions and radicals. In contrast to ultraviolet photons, X-rays can penetrate deep into the envelope and affect the chemistry even at large distances from the source. Whereas the FUV enhanced species cover a region of 200-300 AU, the region enhanced by X-rays is >1000 AU. Best-fit models for AFGL 2591 predict an X-ray luminosity LX > 1e+31 ergs/s with a hard X-ray spectrum TX > 3e+07 K. Furthermore, we find LX/Lbol ~ 1e-6. The chemistry of the bulk of the envelope mass is dominated by cosmic-ray induced reactions rather than by X-ray induced ionization for X-ray luminosities LX < 1e+33 ergs/s. The calculated line intensities of HCO+ and HCS+ show that high-J lines are more affected than lower J lines by the presence of X-rays due to their higher critical densities, and that such differences are detectable even with large aperture single-dish telescopes. Future instruments such as Herschel-HIFI or SOFIA will be able to observe X-ray enhanced hydrides whereas the sensitivity and spatial resolution of ALMA is well-suited to measure the size and geometry of the region affected by X-rays.

P. Staeuber; S. D. Doty; E. F. van Dishoeck; A. O. Benz

2005-06-14T23:59:59.000Z

217

Compton backscattered collimated x-ray source  

SciTech Connect

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

1998-01-01T23:59:59.000Z

218

Compton backscattered collmated X-ray source  

SciTech Connect

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

2000-01-01T23:59:59.000Z

219

Tautomerism in liquid 1,2,3-triazole: a combined Energy-Dispersive X-Ray Diffraction, Molecular Dynamics and FTIR study  

E-Print Network (OSTI)

In this work, we report a multitechnique (energy-dispersive X-Ray diffraction, computational methods and FT-IR spectroscopy) study of the tautomeric equilibrium of 1,2,3-triazole, one of the few small nitrogen-containing eterocycles liquid at room temperature. The T-2H form (C2v symmetry) is found to be strongly favored in gas and solid phases, whereas the neat liquid gives diffraction patterns that can be interpreted satisfactorily with the structure functions calculated from some molecular dynamics results for both T-2H and T-1H tautomers, although the T-2H form gives a slightly better agreement.

Marco Bellagamba; Luigi Bencivenni; Lorenzo Gontrani; Leonardo Guidoni; Claudia Sadun

2013-01-18T23:59:59.000Z

220

Scanning x-ray microscope  

Science Conference Proceedings (OSTI)

A scanning x-ray microscope is described including: an x-ray source capable of emitting a beam of x-rays; a collimator positioned to receive the beam of x-rays and to collimate this beam, a focusing cone means to focus the beam of x-rays, directed by the collimator, onto a focal plane, a specimen mount for supporting a specimen in the focal plane to receive the focused beam of x-rays, and x-ray beam scanning means to relatively move the specimen and the focusing cone means and collimator to scan the focused x-ray beam across the specimen. A detector is disposed adjacent the specimen to detect flourescent photons emitted by the specimen upon exposure to the focused beam of x-rays to provide an electrical output representative of this detection. Means are included for displaying and/or recording the information provided by the output from the detector, as are means for providing information to the recording and/or display means representative of the scan rate and position of the focused x-ray beam relative to the specimen whereby the recording and/or display means can correlate the information received to record and/or display quantitive and distributive information as to the quantity and distribution of elements detected in the specimen. Preferably there is provided an x-ray beam modulation means upstream, relative to the direction of emission of the xray beam, of the focusing cone means.

Wang, C.

1982-02-23T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

Alcator C-Mod soft X-ray pulse height analysis system  

E-Print Network (OSTI)

A pulse height analysis (PHA) system has been installed on the Alcator C-Mod magnetic confinement fusion experiment. The PHA utilizes a Si(Li) detector to measure soft X-rays in the 1-30 keV range with an energy resolution ...

Gamboa, Eliseo (Eliseo J.)

2007-01-01T23:59:59.000Z

222

Radiographic X-Ray Pulse Jitter  

Science Conference Proceedings (OSTI)

The Dual Beam Radiographic Facility consists of two identical radiographic sources. Major components of the machines are: Marx generator, water-filled pulse-forming line (PFL), water-filled coaxial transmission line, three-cell inductive voltage adder, and rod-pinch diode. The diode pulse has the following electrical specifications: 2.25-MV, 60-kA, 60-ns. Each source has the following x-ray parameters: 1-mm-diameter spot size, 4-rad at 1 m, 50-ns full width half max. The x-ray pulse is measured with PIN diode detectors. The sources were developed to produce high resolution images on single-shot, high-value experiments. For this application it is desirable to maintain a high level of reproducibility in source output. X-ray pulse jitter is a key metric for analysis of reproducibility. We will give measurements of x-ray jitter for each machine. It is expected that x-ray pulse jitter is predominantly due to PFL switch jitter, and therefore a correlation of the two will be discussed.

Mitton, C. V., Good, D. E., Henderson, D. J., Hogge, K. W.

2011-01-15T23:59:59.000Z

223

NIST X-Ray Mass Attenuation Coefficients - Version History  

Science Conference Proceedings (OSTI)

... year, month day with database access date.) Hubbell, JH and Seltzer, SM (2004), Tables of X-Ray Mass Attenuation Coefficients and Mass Energy- ...

2010-10-05T23:59:59.000Z

224

dosimetry of x-rays, gamma rays and electrons  

Science Conference Proceedings (OSTI)

... NIST and BIPM Standards for Air Kerma in Medium-Energy X-rays ... of the codes are available from the Government Printing Office, Washington, DC ...

2013-06-28T23:59:59.000Z

225

Phase Sensitive X-ray Imager for More Accurate Digital ...  

Livermore Lab Report. News Archive. News ... use of higher energy X-rays which would result in a lower amount of absorbed radiation to the ... testing ...

226

SLAC National Accelerator Laboratory - X-ray Science  

NLE Websites -- All DOE Office Websites (Extended Search)

energy technologies. SLAC's unique X-ray facilities - the Linac Coherent Light Source (LCLS) and the Stanford Synchrotron Radiation Lightsource (SSRL) - attract thousands of...

227

New Directions in X-ray Scattering - SSRL  

NLE Websites -- All DOE Office Websites (Extended Search)

associated with chemically and radioactively contaminated ground-water. Ability to probe weak scattering from single crystals as function of energy (resonance) and x-ray...

228

Grain Boundary Deformation Analyzed Via X-Ray Diffraction ...  

Science Conference Proceedings (OSTI)

Modeling the Influence of the Second Phase Particle Spatial Distribution on Recrystallization of AA 7050 Near-Field High Energy X-ray Diffraction Microscopy...

229

Temporal multiplexing radiography for dynamic x-ray imaging  

Science Conference Proceedings (OSTI)

All current x-ray imaging devices acquire images sequentially, one at a time. Using a spatially distributed multibeam x-ray source we recently demonstrated the feasibility for multiplexing x-ray imaging, which can significantly increase the data collection speed. Here we present a general methodology for dynamic x-ray imaging of an object in cyclic motion with temporal multiplexing. Compared to the conventional sequential imaging technique, where 2N-1 phase images are required and N exposures are needed for a single phase image, a temporal multiplexing of dimension 2N-1 can reduce the imaging time by a factor of N while maintaining the temporal resolution.

Cao Guohua [Department of Physics and Astronomy, University of North Carolina, Chapel Hill, North Carolina 27599 (United States); Zhang Jian [Department of Radiation Oncology and Department of Physics and Astronomy, University of North Carolina, Chapel Hill, North Carolina 27599 (United States); Zhou, Otto; Lu Jianping [Department of Physics and Astronomy and Curriculum in Applied Sciences and Engineering, University of North Carolina, Chapel Hill, North Carolina, 27599 (United States)

2009-09-15T23:59:59.000Z

230

Development of a portable x-ray computed tomographic imaging system for drill-site investigation of recovered core  

SciTech Connect

A portable x-ray computed tomography (CT) system was constructed for imaging core at drill sites. Performing drill-site-based x-ray scanning and CT analysis permits rapid evaluation of core properties (such as density, lithologic structure, and macroporosity distribution) and allows for real-time decision making for additional core-handling procedures. Because of the speed with which scanning is performed, systematic imaging and electronic cataloging of all retrieved core is feasible. Innovations (such as a novel clamshell shielding arrangement integrated with system interlocks) permit safe operation of the x-ray system in a busy core handling area. The minimization of the volume encapsulated with shielding reduces the overall system weight and facilitates instrument portability. The x-ray system as originally fabricated had a 110 kV x-ray source with a fixed 300-micron focal spot size. A 15 cm image intensifier with a cesium iodide phosphor input screen was coupled to a CCD for image capture. The CT system has since been modified with a 130 kV micro-focal x-ray source. With the x-ray system's variable focal spot size, high-resolution studies (10-micron resolution) can be performed on core plugs and coarser (100-micron resolution) images can be acquired of whole drill cores. The development of an aluminum compensator has significantly improved the dynamic range and accuracy of the system. An x-ray filter has also been incorporated, permitting rapid acquisition of multi-energy scans for more quantitative analysis of sample mineralogy. The x-ray CT system has operated reliably under extreme field conditions, which have varied from shipboard to arctic.

Freifeld, Barry M.; Kneafsey, Timothy J.; Tomutsa, Liviu; Pruess, Jacob

2003-05-01T23:59:59.000Z

231

Standing-wave excited soft x-ray photoemission microscopy: application to Co microdot magnetic arrays  

SciTech Connect

We demonstrate the addition of depth resolution to the usual two-dimensional images in photoelectron emission microscopy (PEEM), with application to a square array of circular magnetic Co microdots. The method is based on excitation with soft x-ray standing-waves generated by Bragg reflection from a multilayer mirror substrate. Standing wave is moved vertically through sample simply by varying the photon energy around the Bragg condition. Depth-resolved PEEM images were obtained for all of the observed elements. Photoemission intensities as functions of photon energy were compared to x-ray optical calculations in order to quantitatively derive the depth-resolved film structure of the sample.

Gray, Alexander; Kronast, Florian; Papp, Christian; Yang, See-Hun; Cramm, Stefan; Krug, Ingo P.; Salmassi, Farhad; Gullikson, Eric M.; Hilken, Dawn L.; Anderson, Erik H.; Fischer, Peter; Durr, Hermann A.; Schneider, Claus M.; Fadley, Charles S.

2010-10-29T23:59:59.000Z

232

Interferometric hard x-ray phase contrast imaging at 204 nm grating period  

SciTech Connect

We report on hard x-ray phase contrast imaging experiments using a grating interferometer of approximately 1/10th the grating period achieved in previous studies. We designed the gratings as a staircase array of multilayer stacks which are fabricated in a single thin film deposition process. We performed the experiments at 19 keV x-ray energy and 0.8 {mu}m pixel resolution. The small grating period resulted in clear separation of different diffraction orders and multiple images on the detector. A slitted beam was used to remove overlap of the images from the different diffraction orders. The phase contrast images showed detailed features as small as 10 {mu}m, and demonstrated the feasibility of high resolution x-ray phase contrast imaging with nanometer scale gratings.

Wen Han; Gomella, Andrew A.; Miao, Houxun; Lynch, Susanna K. [Imaging Physic Laboratory, Biophysics and Biochemistry Center, National Heart, Lung and Blood Institute, National Institutes of Health, Bethesda, Maryland 20892 (United States); Wolfe, Douglas E. [Applied Research Laboratory, Penn State University, State College, Pennsylvania 16804 (United States); Xiao Xianghui; Liu Chian [X-Ray Science Division, Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Morgan, Nicole [National Institute of Biomedical Imaging and Bioengineering, National Institutes of Health, Bethesda, Maryland 20892 (United States)

2013-01-15T23:59:59.000Z

233

The Soft-X-Ray Spectral Shape of X-Ray-Weak Seyferts  

E-Print Network (OSTI)

(I) We observed eight Seyfert~2s and two X--ray--weak Seyfert~1/QSOs with the ROSAT PSPC, and one Seyfert~2 with the ROSAT HRI. These targets were selected from the Extended 12\\um\\ Galaxy Sample. (II) Both Seyfert~1/QSOs vary by factors of 1.5---2. The photon indices steepen in the more luminous state, consistent with the variability being mainly due to the softest X--rays, which are confined to a size of less than a parsec. (III) Both the Seyfert~2s and Seyfert~1/QSOs are best fit with a photon index of $\\Gamma\\sim3$, which is steeper than the canonical value of $\\Gamma\\sim1.7$ measured for X--ray--strong Seyferts by ROSAT and at higher energies. Several physical explanations are suggested for the steeper slopes of X--ray--weak objects. (IV) We observed one Seyfert~2, NGC~5005, with the ROSAT HRI, finding about 13\\% of the soft X--rays to come from an extended component. This and other observations suggest that different components to the soft X--ray spectrum of some, if not all, X--ray--weak Seyferts may come from spatially distinct regions.

Brian Rush; Matthew A. Malkan

1995-07-27T23:59:59.000Z

234

Improvement of X-ray Analysis of Nano-scaled Materials by Means...  

NLE Websites -- All DOE Office Websites (Extended Search)

Improvement of X-ray Analysis of Nano-scaled Materials by Means of High Resolution X-ray Emission Spectrometry Monday, August 1, 2011 - 2:00pm SSRL Bldg. 137 Conference Room...

235

X-ray Absorption Spectroscopy  

SciTech Connect

This review gives a brief description of the theory and application of X-ray absorption spectroscopy, both X-ray absorption near edge structure (XANES) and extended X-ray absorption fine structure (EXAFS), especially, pertaining to photosynthesis. The advantages and limitations of the methods are discussed. Recent advances in extended EXAFS and polarized EXAFS using oriented membranes and single crystals are explained. Developments in theory in understanding the XANES spectra are described. The application of X-ray absorption spectroscopy to the study of the Mn4Ca cluster in Photosystem II is presented.

Yano, Junko; Yachandra, Vittal K.

2009-07-09T23:59:59.000Z

236

Development of mirror manipulator for hard-x-ray nanofocusing at sub-50-nm level  

Science Conference Proceedings (OSTI)

X-ray focusing using Kirkpatrick-Baez (KB) mirrors is promising owing to their capability of highly efficient and energy-tunable focusing. We report the development of a mirror manipulator which enables KB mirror alignment with a high degree of accuracy. Mirror alignment tolerances were estimated using two types of simulators. On the basis of the simulation results, the mirror manipulator was developed to achieve an optimum KB mirror setup. As a result of focusing tests at BL29XUL of SPring-8, the beam size of 48x36 nm{sup 2} (VxH) was achieved in the full width at half maximum at an x-ray energy of 15 keV. Spatial resolution tests showed that a scanning x-ray microscope equipped with the KB focusing system could resolve line-and-space patterns of 80 nm linewidth in a high visibility of 60%.

Matsuyama, S.; Mimura, H.; Yumoto, H.; Hara, H.; Yamamura, K.; Sano, Y.; Endo, K.; Mori, Y.; Yabashi, M.; Nishino, Y.; Tamasaku, K.; Ishikawa, T.; Yamauchi, K. [Department of Precision Science and Technology, Graduate School of Engineering, Osaka University, 2-1 Yamada-oka, Suita, Osaka 565-0871 (Japan); Research Center for Ultra-Precision Science and Technology, Graduate School of Engineering, Osaka University, 2-1 Yamada-oka, Suita, Osaka 565-0871 (Japan); Department of Precision Science and Technology, Graduate School of Engineering, Osaka University, 2-1 Yamada-oka, Suita, Osaka 565-0871 (Japan); Research Center for Ultra-Precision Science and Technology, Graduate School of Engineering, Osaka University, 2-1 Yamada-oka, Suita, Osaka 565-0871 (Japan); SPring-8/Japan Synchrotron Radiation Research Institute (JASRI), 1-1-1 Kouto, Mikazuki, Hyogo 679-5148 (Japan); SPring-8/RIKEN, 1-1-1 Kouto, Mikazuki, Hyogo 679-5148 (Japan); Department of Precision Science and Technology, Graduate School of Engineering, Osaka University, 2-1 Yamada-oka, Suita, Osaka 565-0871 (Japan)

2006-09-15T23:59:59.000Z

237

A soft x-ray transmission grating imaging-spectrometer for the National Ignition Facility  

SciTech Connect

A soft x-ray transmission grating spectrometer has been designed for use on high energy-density physics experiments at the National Ignition Facility (NIF); coupled to one of the NIF gated x-ray detectors (GXD) it records sixteen time-gated spectra between 250 and 1000eV with 100ps temporal resolution. The trade-off between spectral and spatial resolution leads to an optimized design for measurement of emission around the peak of a 100-300eV blackbody spectrum. Performance qualification results from the NIF, the Trident Laser Facility and VUV beamline at the National Synchrotron Light Source (NSLS), evidence a <100{micro}m spatial resolution in combination with a source-size limited spectral resolution that is <10eV at photon energies of 300eV.

Moore, A S; Guymer, T M; Kline, J L; Morton, J; Taccetti, M; Lanier, N E; Bentley, C; Workman, J; Peterson, B; Mussack, K; Cowan, J; Prasad, R; Richardson, M; Burns, S; Kalantar, D H; Benedetti, L R; Bell, P; Bradley, D; Hsing, W; Stevenson, M

2012-05-01T23:59:59.000Z

238

A soft x-ray transmission grating imaging-spectrometer for the National Ignition Facility  

SciTech Connect

A soft x-ray transmission grating spectrometer has been designed for use on high energy-density physics experiments at the National Ignition Facility (NIF); coupled to one of the NIF gated x-ray detectors it records 16 time-gated spectra between 250 and 1000 eV with 100 ps temporal resolution. The trade-off between spectral and spatial resolution leads to an optimized design for measurement of emission around the peak of a 100-300 eV blackbody spectrum. Performance qualification results from the NIF, the Trident Laser Facility and vacuum ultraviolet beamline at the National Synchrotron Light Source, evidence a <100 {mu}m spatial resolution in combination with a source-size limited spectral resolution that is <10 eV at photon energies of 300 eV.

Moore, A. S.; Guymer, T. M.; Morton, J.; Bentley, C.; Stevenson, M. [Directorate Science and Technology, AWE Aldermaston, Reading, RG7 4PR (United Kingdom); Kline, J. L.; Taccetti, M.; Lanier, N. E.; Workman, J.; Peterson, B.; Mussack, K.; Cowan, J. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Prasad, R.; Richardson, M.; Burns, S.; Kalantar, D. H.; Benedetti, L. R.; Bell, P.; Bradley, D.; Hsing, W. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551-0808 (United States)

2012-10-15T23:59:59.000Z

239

Low energy cut-offs and hard X-ray spectra in high-z radio-loud quasars: the Suzaku view of RBS315  

E-Print Network (OSTI)

We present the results from the Suzaku observation of the powerful radio-loud quasar RBS315 (z=2.69), for which a previous XMM-Newton observation showed an extremely flat X-ray continuum up to 10 keV (photon index Gamma=1.26) and indications of strong intrinsic absorption (N_H~10^22 cm^{-2} assuming neutral gas). The instrument for hard X-rays HXD/PIN allows us a detection of the source up to 50 keV. The broad-band continuum (0.5-50 keV) can be well modeled with a power-law with slope Gamma=1.5 (definitively softer than the continuum measured by XMM-Newton) above 1 keV with strong deficit of soft photons. The low-energy cut-off can be well fitted either with intrinsic absorption (with column density N_H~10^22 cm^{-2} in the quasar rest frame) or with a break in the continuum, with an extremely hard (Gamma =0.7) power-law below 1 keV. We construct the Spectral Energy Distribution of the source, using also optical-UV measurements obtained through a quasi-simultaneous UVOT/SWIFT observation. The shape of the SED is similar to that of other Flat Spectrum Radio Quasars (FSRQs) with similar power, making this source an excellent candidate for the detection in gamma-rays by GLAST. We model the SED with the synchrotron-Inverse Compton model usually applied to FSRQs, showing that the deficit of soft photons can be naturally interpreted as due to an intrinsic curvature of the spectrum near the low energy end of the IC component rather than to intrinsic absorption, although the latter possibility cannot be ruled out. We propose that in at least a fraction of the radio-loud QSOs at high redshift the cut-off in the soft X-ray band can be explained in a similar way. Further studies are required to distinguish between the two alternatives.

F. Tavecchio; L. Maraschi; G. Ghisellini; J. Kataoka; L. Foschini; R. M. Sambruna; G. Tagliaferri

2007-05-02T23:59:59.000Z

240

Isotope and Temperature Effects in Liquid Water Probed by X-RayAbsorption and Resonant X-Ray Emission Spectroscopy  

DOE Green Energy (OSTI)

High-resolution x-ray absorption and emission spectra ofliquid water exhibit a strong isotope effect. Further, the emissionspectra show a splitting of the 1b1 emission line, a weak temperatureeffect, and a pronounced excitation-energy dependence. They can bedescribed as a superposition of two independent contributions. Bycomparing with gasphase, ice, and NaOH/NaOD, we propose that the twocomponents are governed by the initial state hydrogen bondingconfiguration and ultrafast dissociation on the time scale of the O 1score hole decay.

Fuchs, O.; Zharnikov, M.; Weinhardt, L.; Blum, M.; Weigand, M.; Zubavichus, Y.; Bar, M.; Maier, F.; Denlinger, J.D.; Heske, C.; Grunze,M.; Umbach, E.

2007-03-10T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

APS 7-BM Beamline: X-Ray Resources  

NLE Websites -- All DOE Office Websites (Extended Search)

Useful Websites Useful Websites X-Ray Interactions with Matter from CRXO at LBNL. Intuitive interface for x-ray transmission and reflectivity for a wide range of materials. X-Ray Data Booklet from LBNL. Slightly outdated in places, but many useful tables of edge energies, fluorescence lines, and crystal lattice spacings. NIST XCOM Database. Powerful database of photoelectric absorption, elastic scattering, and Compton scattering cross-sections for a wide range of materials. X-Ray Server. Maintained by Sergey Stepanov at GMCA at the APS, this website has several powerful calculators for simulating x-ray reflection and diffraction. Software X-Ray Oriented Programs (XOP). This program, written by scientists at the ESRF and APS, is widely used in the synchrotron research community.

242

Fabrication process for a gradient index x-ray lens  

DOE Patents (OSTI)

A process for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments m the soft x-ray region.

Bionta, Richard M. (Livermore, CA); Makowiecki, Daniel M. (Livermore, CA); Skulina, Kenneth M. (Livermore, CA)

1995-01-01T23:59:59.000Z

243

Fabrication process for a gradient index x-ray lens  

DOE Patents (OSTI)

A process is disclosed for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments in the soft x-ray region. 13 figures.

Bionta, R.M.; Makowiecki, D.M.; Skulina, K.M.

1995-01-17T23:59:59.000Z

244

X-ray streak and framing camera techniques  

SciTech Connect

This paper reviews recent developments and applications of ultrafast diagnostic techniques for x-ray measurements. These techniques, based on applications of image converter devices, are already capable of significantly important resolution capabilities. Techniques capable of time resolution in the sub-nanosecond regime are being considered. Mechanical cameras are excluded from considerations as are devices using phosphors or fluors as x-ray converters.

Coleman, L.W.; Attwood, D.T.

1975-12-23T23:59:59.000Z

245

Comparison of SOFC Cathode Microstructure Quantified using X-ray Nanotomography and Focused Ioni Beam-scanning Electron Microscopy  

Science Conference Proceedings (OSTI)

X-ray nanotomography and focused ion beam scanning electron microscopy (FIB-SEM) have been applied to investigate the complex 3D microstructure of solid oxide fuel cell (SOFC) electrodes at spatial resolutions of 45 nm and below. The application of near edge differential absorption for x-ray nanotomography and energy selected backscatter detection for FIB-SEM enable elemental mapping within the microstructure. Using these methods, non-destructive 3D x-ray imaging and FIB-SEM serial sectioning have been applied to compare three-dimensional elemental mapping of the LSM, YSZ, and pore phases in the SOFC cathode microstructure. The microstructural characterization of an SOFC cathode is reported based on these measurements. The results presented demonstrate the viability of x-ray nanotomography as a quantitative characterization technique and provide key insights into the SOFC cathode microstructure.

G Nelson; W Harris; J Lombardo; J Izzo Jr.; W Chiu; P Tanasini; M Cantoni; J Van herle; C Comninellis; et al.

2011-12-31T23:59:59.000Z

246

Diagnostics of underwater electrical wire explosion through a time- and space-resolved hard x-ray source  

SciTech Connect

A time- and space-resolved hard x-ray source was developed as a diagnostic tool for imaging underwater exploding wires. A {approx}4 ns width pulse of hard x-rays with energies of up to 100 keV was obtained from the discharge in a vacuum diode consisting of point-shaped tungsten electrodes. To improve contrast and image quality, an external pulsed magnetic field produced by Helmholtz coils was used. High resolution x-ray images of an underwater exploding wire were obtained using a sensitive x-ray CCD detector, and were compared to optical fast framing images. Future developments and application of this diagnostic technique are discussed.

Sheftman, D.; Shafer, D.; Efimov, S.; Gruzinsky, K.; Gleizer, S.; Krasik, Ya. E. [Physics Department, Technion, Haifa 32000 (Israel)

2012-10-15T23:59:59.000Z

247

Massively parallel X-ray scattering simulations  

Science Conference Proceedings (OSTI)

Although present X-ray scattering techniques can provide tremendous information on the nano-structural properties of materials that are valuable in the design and fabrication of energy-relevant nano-devices, a primary challenge remains in the analyses ...

Abhinav Sarje; Xiaoye S. Li; Slim Chourou; Elaine R. Chan; Alexander Hexemer

2012-11-01T23:59:59.000Z

248

Small Angle X-Ray Scattering Detector  

DOE Patents (OSTI)

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

Hessler, Jan P.

2004-06-15T23:59:59.000Z

249

Background X-ray Spectrum of Radioactive Samples  

Science Conference Proceedings (OSTI)

An energy-dispersive X-ray spectrometer (EDS) is commonly used with a scanning electron microscope (SEM) to analyze the elemental compositions and microstructures of a variety of samples. For example, the microstructures of nuclear fuels are commonly investigated with this technique. However, the radioactivity of some materials introduces additional X-rays that contribute to the EDS background spectrum. These X-rays are generally not accounted for in spectral analysis software, and can cause misleading results. X-rays from internal conversion [1], Bremsstrahlung [2] radiation associated with alpha ionizations and beta particle interactions [3], and gamma rays from radioactive decay can all elevate the background of radioactive materials.

Shannon Yee; Dawn E. Janney

2008-02-01T23:59:59.000Z

250

SOFT INELASTIC X-RAY SCATTERING (SIX) Group Leader: Ignace Jarrige  

NLE Websites -- All DOE Office Websites (Extended Search)

INELASTIC X-RAY SCATTERING (SIX) INELASTIC X-RAY SCATTERING (SIX) Group Leader: Ignace Jarrige 1 Proposal Team: D. Arena 1 , A. Baron 2 , Y. Cai 1 , Y.-D. Chuang 3 , F. de Groot 4 , J. Guo 3 , J.P. Hill 1 , S. Hulbert 1 , C. McGuinness 5 , R. Reininger 9 , J.E. Rubenson 6 , C. Sanchez-Hanke 1 , T. Schmitt 7 , K. Smith 8 1 Brookhaven National Laboratory, 2 SPring-8, 3 Lawrence Berkeley Laboratory, 4 Utrecht University, 5 Trinity College Dublin, 6 Uppsala University, 7 Paul Scherrer Institute, 8 Boston University, 9 Argonne National Laboratory TECHNIQUE AND CAPABILITIES APPLICATIONS ADDITIONAL INFORMATION * Resonant inelastic x-ray scattering (RIXS) at unprecedented resolution (10 meV @ 1000 eV) to revolutionize study of low energy excitations in many important materials. * Continuously tunable momentum transfer (q) to study the

251

In Situ X-Ray Probing Reveals Fingerprints of Surface Platinum Oxide  

DOE Green Energy (OSTI)

In situ x-ray absorption spectroscopy (XAS) at the Pt L{sub 3} edge is a useful probe for Pt-O interactions at polymer electrolyte membrane fuel cell (PEMFC) cathodes. We show that XAS using the high energy resolution fluorescence detection (HERFD) mode, applied to a well-defined monolayer Pt/Rh(111) sample where the bulk penetrating hard x-rays probe only surface Pt atoms, provides a unique sensitivity to structure and chemical bonding at the Pt-electrolyte interface. Ab initio multiple-scattering calculations using the FEFF8 code and complementary extended x-ray absorption fine structure (EXAFS) results indicate that the commonly observed large increase of the white-line at high electrochemical potentials on PEMFC cathodes originates from platinum oxide formation, whereas previously proposed chemisorbed oxygen-containing species merely give rise to subtle spectral changes.

Friebel, Daniel

2011-08-24T23:59:59.000Z

252

X-Ray Interactions with Matter  

DOE Data Explorer (OSTI)

The primary interactions of low-energy x-rays within condensed matter, viz. photoabsorption and coherent scattering, are described for photon energies outside the absorption threshold regions by using atomic scattering factors. The atomic scattering factors may be accurately determined from the atomic photoabsorption cross sections using modified Kramers-Kronig dispersion relations. From a synthesis of the currently available experimental data and recent theoretical calculations for photoabsorption, the angle-independent, forward-scattering components of the atomic scattering factors have been thus semiempirically determined and tabulated here for 92 elements and for the region 50-30,000 eV. Atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction. The incoherent scattering contributions that become significant for the light elements at the higher photon energies are similarly determined. The basic x-ray interaction relations that are used in applied x-ray physics are presented here in terms of the atomic scattering factors. The bulk optical constants are also related to the atomic scattering factors. These atomic and optical relations are applied to the detailed calculation of the reflectivity characteristics of a series of practical x-ray mirror, multilayer, and crystal monochromators. Comparisons of the results of this semiempirical,"atom-like", description of x-ray interactions for the low-energy region with those of experiment and ab initio theory are presented. (Taken from the abstract in OSTI Record 6131765) (Specialized Interface)

Henke, B.L.; Gullikson, E.M.; Davis, J.C.

253

High-brightness beamline for X-ray spectroscopy at the Advanced Light Source  

SciTech Connect

Beamline 9.3.1 at the Advanced Light Source (ALS) is a windowless beamline, covering the 1-6 keV photon-energy range, designed to achieve the goals of high energy resolution, high flux, and high brightness at the sample. When completed later this year, it will be the first ALS monochromatic hard-x-ray beamline, and its brightness will be an order-of-magnitude higher than presently available in this energy range. In addition, it will provide flux and resolution comparable to any other beamline now in operation. To achieve these goals, two technical improvements, relative to existing x-ray beamlines, were incorporated. First, a somewhat novel optical design for x-rays, in which matched toroidal mirrors are positioned before and after the double-crystal monochromator, was adopted. This configuration allows for high resolution by passing a collimated beam through the monochromator, and for high brightness by focusing the ALS source on the sample with unit magnification. Second, a new ''Cowan type'' double-crystal monochromator based on the design used at NSLS beamline X-24A was developed. The measured mechanical precision of this new monochromator shows significant improvement over existing designs, without using positional feedback available with piezoelectric devices. Such precision is essential because of the high brightness of the radiation and the long distance (12m) from the source (sample) to the collimating (focusing) mirror. This combination of features will provide a bright, high resolution, and stable x-ray beam for use in the x-ray spectroscopy program at the ALS.

Perera, R.C.C.; Jones, G. [Lawrence Berkeley Lab., CA (US); Lindle, D.W. [Univ. of Nevada, Las Vegas, NV (US). Dept. of Chemistry

1994-08-01T23:59:59.000Z

254

X-ray attenuation properties of stainless steel (u)  

SciTech Connect

Stainless steel vessels are used to enclose solid materials for studying x-ray radiolysis that involves gas release from the materials. Commercially available stainless steel components are easily adapted to form a static or a dynamic condition to monitor the gas evolved from the solid materials during and after the x-ray irradiation. Experimental data published on the x-ray attenuation properties of stainless steel, however, are very scarce, especially over a wide range of x-ray energies. The objective of this work was to obtain experimental data that will be used to determine how a poly-energetic x-ray beam is attenuated by the stainless steel container wall. The data will also be used in conjunction with MCNP (Monte Carlos Nuclear Particle) modeling to develop an accurate method for determining energy absorbed in known solid samples contained in stainless steel vessels. In this study, experiments to measure the attenuation properties of stainless steel were performed for a range of bremsstrahlung x-ray beams with a maximum energy ranging from 150 keV to 10 MeV. Bremsstrahlung x-ray beams of these energies are commonly used in radiography of engineering and weapon components. The weapon surveillance community has a great interest in understanding how the x-rays in radiography affect short-term and long-term properties of weapon materials.

Wang, Lily L [Los Alamos National Laboratory; Berry, Phillip C [Los Alamos National Laboratory

2009-01-01T23:59:59.000Z

255

X-ray Imaging Workshop  

NLE Websites -- All DOE Office Websites (Extended Search)

Imaging and Spectro-microscopy: Imaging and Spectro-microscopy: the Present and the Future Stanford Synchrotron Radiation Laboratory October 8-9, 2002 Organizers: John Miao & Keith Hodgson A workshop on "X-ray Imaging and Spectro-microscopy: the Present and the Future" was held on October 8-9, 2002. This workshop, organized by John Miao (SSRL) and Keith Hodgson (SSRL) provided a forum to discuss the scientific applications of a variety of imaging and spectro-microscopic techniques, including photoemission electron microscopy (PEEM), angle resolved photoemission spectroscopy (ARPES), coherent diffraction imaging, x-ray microscopy, micro-tomography, holographic imaging, and x-ray micro-probe. Twelve invited speakers discussed the important scientific applications of these techniques, and also predicted the future scientific directions with the advance of instrumentation and x-ray sources. The workshop was well attended with over fifty registered attendees.

256

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

257

Structural and Kinetic Studies of Structure I Gas Hydrates via Low Temperature X-Ray Diffraction and High Resolution Neutron Diffraction.  

E-Print Network (OSTI)

??Gas hydrates are materials of interest as sources for clean energy, carbon sequestration, greenhouse gas mitigation, and gas storage. This body of work presents two (more)

Everett, Susan Michelle

2013-01-01T23:59:59.000Z

258

Sharper Focusing of Hard X-rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Sharper Focusing of Hard X-rays FROM: Physics News Update Number 773 #1, April 12, 2006, by Phil Schewe and Ben Stein Note: This text has been slightly modified from the original. Sharper focusing of hard x-rays has been achieved with a device developed at Argonne National Lab. Because of their high energy, x-rays are hard to focus: they can be reflected from a surface but only at a glancing angle (less than a tenth of a degree); they can be refracted but the index of refraction is very close to 1, so that making efficient lenses becomes a problem; and they can be diffracted, but the relatively thick, variable pitch grating required for focusing is tricky to achieve. The Argonne device is of the diffraction type, and it consists of a stack of alternating layers of metal and silicon, made by depositing progressively thicker layers. When the x-rays fall on such a structure, nearly edge-on, what they see is a grating (called a linear zone plate) consisting of a sort of bar-code pattern.

259

Sixth International Conference on X-ray Microscopy  

SciTech Connect

More than 180 participants from around the world crowded the Clark Kerr Campus of the University of California, Berkeley, from August 1-6, 1999 for the Sixth International Conference on X-Ray Microscopy (XRM99). Held every three years since 1983, the XRM conferences have become the primary international forum for the presentation and discussion of advances in high-spatial-resolution x-ray imaging and applications (including the use of x-ray spectroscopic and analytical techniques) in biological and medical sciences, environmental and soil sciences, and materials and surface sciences.

Robinson, Arthur L.

1999-08-23T23:59:59.000Z

260

X-ray Polarization  

Science Conference Proceedings (OSTI)

... of crystal spectrometers where the energy dispersion is polarization selective. ... by observing forbidden (M1) transitions within the ground term of ...

2010-12-07T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

Dilation x-ray imager a new/faster gated x-ray imager for the NIF  

SciTech Connect

As the yield on implosion shots increases it is expected that the peak x-ray emission reduces to a duration with a FWHM as short as 20 ps for {approx}7 Multiplication-Sign 10{sup 18} neutron yield. However, the temporal resolution of currently used gated x-ray imagers on the NIF is 40-100 ps. We discuss the benefits of the higher temporal resolution for the NIF and present performance measurements for dilation x-ray imager, which utilizes pulse-dilation technology [T. J. Hilsabeck et al., Rev. Sci. Instrum. 81, 10E317 (2010)] to achieve x-ray imaging with temporal gate times below 10 ps. The measurements were conducted using the COMET laser, which is part of the Jupiter Laser Facility at the Lawrence Livermore National Laboratory.

Nagel, S. R.; Bell, P. M.; Bradley, D. K.; Ayers, M. J.; Barrios, M. A.; Felker, B.; Smith, R. F.; Collins, G. W.; Jones, O. S.; Piston, K.; Raman, K. S. [Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, California 94550 (United States); Hilsabeck, T. J.; Kilkenny, J. D.; Chung, T.; Sammuli, B. [General Atomics, P.O. Box 85608, San Diego, California 92186-5608 (United States); Hares, J. D.; Dymoke-Bradshaw, A. K. L. [Kentech Instruments Ltd., Wallingford, Oxfordshire OX10 (United Kingdom)

2012-10-15T23:59:59.000Z

262

X-ray imaging with grazing-incidence microscopes developed for the LIL program  

SciTech Connect

This article describes x-ray imaging with grazing-incidence microscopes, developed for the experimental program carried out on the Ligne d'Integration Laser (LIL) facility [J. P. Le Breton et al., Inertial Fusion Sciences and Applications 2001 (Elsevier, Paris, 2002), pp. 856-862] (24 kJ, UV--0.35 nm). The design includes a large target-to-microscope (400-700 mm) distance required by the x-ray ablation issues anticipated on the Laser MegaJoule facility [P. A. Holstein et al., Laser Part. Beams 17, 403 (1999)] (1.8 MJ) which is under construction. Two eight-image Kirkpatrick-Baez microscopes [P. Kirkpatrick and A. V. Baez J. Opt. Soc. Am. 38, 766 (1948)] with different spectral wavelength ranges and with a 400 mm source-to-mirror distance image the target on a custom-built framing camera (time resolution of {approx}80 ps). The soft x-ray version microscope is sensitive below 1 keV and its spatial resolution is better than 30 {mu}m over a 2-mm-diam region. The hard x-ray version microscope has a 10 {mu}m resolution over an 800-{mu}m-diam region and is sensitive in the 1-5 keV energy range. Two other x-ray microscopes based on an association of toroidal/spherical surfaces (T/S microscopes) produce an image on a streak camera with a spatial resolution better than 30 {mu}m over a 3 mm field of view in the direction of the camera slit. Both microscopes have been designed to have, respectively, a maximum sensitivity in the 0.1-1 and 1-5 keV energy range. We present the original design of these four microscopes and their test on a dc x-ray tube in the laboratory. The diagnostics were successfully used on LIL first experiments early in 2005. Results of soft x-ray imaging of a radiative jet during conical shaped laser interaction are shown.

Rosch, R.; Boutin, J. Y.; Le Breton, J. P.; Gontier, D.; Jadaud, J. P.; Reverdin, C.; Soullie, G.; Lidove, G.; Maroni, R. [CEA/DIF, BP 12, 91680 Bruyeres-Le-Chatel (France)

2007-03-15T23:59:59.000Z

263

Formation of deformation textures in face-centered-cubic materials studied by in-situ high-energy x-ray diffraction and self-consistent model.  

Science Conference Proceedings (OSTI)

The evolution of deformation textures in copper and a brass that are representative of fcc metals with different stacking fault energies (SFEs) during cold rolling is predicted using a self-consistent (SC) model. The material parameters used for describing the micromechanical behavior of each metal are determined from the high-energy X-ray (HEXRD) diffraction data. At small reductions, a reliable prediction of the evolution of the grain orientation distribution that is represented as the continuous increase of the copper and brass components is achieved for both metals when compared with the experimental textures. With increasing deformation, the model could characterize the textures of copper, i.e., the strengthening of the copper component, when dislocation slip is still the dominant mechanism. For a brass at moderate and large reductions, a reliable prediction of its unique feature of texture evolution, i.e., the weakening of the copper component and the strengthening of the brass component, could only be achieved when proper boundary conditions together with some specified slip/twin systems are considered in the continuum micromechanics mainly containing twinning and shear banding. The present investigation suggests that for fcc metals with a low SFE, the mechanism of shear banding is the dominant contribution to the texture development at large deformations.

Jia, N.; Nie, Z. H.; Ren, Y.; Peng, R. L.; Wang, Y. D.; Zhao, X.; X-Ray Science Division; Northeastern Univ.; Linkoping Univ.; Beijing Inst. of Tech.

2010-05-01T23:59:59.000Z

264

A highly modular beamline electrostatic levitation facility, optimized for in situ high-energy x-ray scattering studies of equilibrium and supercooled liquids  

Science Conference Proceedings (OSTI)

High-energy x-ray diffraction studies of metallic liquids provide valuable information about structural evolution on the atomic length scale, leading to insights into the origin of the nucleation barrier and the processes of supercooling and glass formation. The containerless processing of the beamline electrostatic levitation (BESL) facility allows coordinated thermophysical and structural studies of equilibrium and supercooled liquids to be made in a contamination-free, high-vacuum ({approx}10{sup -8} Torr) environment. To date, the incorporation of electrostatic levitation facilities into synchrotron beamlines has been difficult due to the large footprint of the apparatus and the difficulties associated with its transportation and implementation. Here, we describe a modular levitation facility that is optimized for diffraction studies of high-temperature liquids at high-energy synchrotron beamlines. The modular approach used in the apparatus design allows it to be easily transported and quickly setup. Unlike most previous electrostatic levitation facilities, BESL can be operated by a single user instead of a user team.

Mauro, N.A.; Kelton, K.F. (WU)

2011-10-27T23:59:59.000Z

265

In situ synchrotron x-ray studies of LiMn{sub 2}O{sub 4} cathodes  

DOE Green Energy (OSTI)

LiCoO{sub 2} cathodes are now used in most commercial lithium ion batteries. LiMn{sub 2}O{sub 4} is an attractive low cost alternative. However, it is difficult to make reproducibly. At Brookhaven National Laboratory two in situ synchrotron x-ray techniques, that are available at the National Synchrotron Light Source (NSLS), have been used to investigate LiMn{sub 2}O{sub 4}. The techniques are x-ray absorption and high resolution x-ray diffraction. With x-ray absorption it is possible to follow the changes in the Mn oxidation state and the changes in the Mn-O and Mn-Mn bond lengths on cycling. Also it is possible to detect amorphous phases. The high energy x-rays at the diffraction Beam Lines at the NSLS (up to 24 KeV) permit in situ x-ray diffraction, in the transmission mode, in thin lithium and lithium ion cells. The evolution of the structural chances that occur on cycling can be followed. These in situ measurements were done on Li/LiMn{sub 2}O{sub 4} cells with a liquid electrolyte (1 M LiPF{sub 6} in a 1:1:3 PC:EC:DMC solvent).

McBreen, J.; Mukerjee, S.; Yang, X.Q. [and others

1997-05-01T23:59:59.000Z

266

Investigation of GEM-Micromegas Detector on X-ray Beam of Synchrotron Radiation  

E-Print Network (OSTI)

To solve the discharge of the standard Bulk Micromegas and GEM detector, the GEM-Micromegas detector was developed in Institute of High Energy Physics. Taking into account the advantages of the two detectors, one GEM foil was set as a preamplifier on the mesh of Micromegas in the structure and the GEM preamplification decreased the working voltage of Micromegas to reduce the effect of the discharge significantly. In the paper, the performance of detector in X-ray beam was studied at 1W2B laboratory of Beijing Synchrotron Radiation Facility. Finally, the result of the energy resolution under various X-ray energies was given in different working gases. It indicated that the GEM-Micromegas detector had the energy response capability in all the energy range and it could work better than the standard Bulk-Micromegas.

YuLian Zhang; HuiRong Qi; BiTao Hu; ShengNan Fan; Bo Wang; Mei Liu; Jian Zhang; RongGuang Liu; GuangCai Chang; Peng Liu; Qun Ouyang; YuanBo Chen; FuTing Yi

2013-05-10T23:59:59.000Z

267

Suppressing Thermal Energy Drift In The LLNL Flash X-Ray Accelerator Using Linear Disk Resistor Stacks  

SciTech Connect

This paper addresses thermal drift in sodium thiosulfate liquid resistors and their replacement with linear disk resistors from HVR Advanced Power Components. Sodium thiosulfate resistors in the FXR induction linear accelerator application have a temperature coefficient of {approx}1.8%/C. The FXR Marx banks send an 8kJ pulse through eight 524 cm{sup 3} liquid resistors at a repetition rate of up to 1 every 45 seconds. Every pulse increases the temperature of the solution by {approx}0.4 C which produces a 0.7% change in resistance. The typical cooling rate is {approx}0.4 C per minute which results in {approx}0.1% energy drop per pulse during continuous pulsed operations. A radiographic accelerator is extraordinarily sensitive to energy variations. Changes in beam energy produce movement in beam transport, changes in spot size, and large dose variations. If self-heating were the only problem, we could predict the increase in input voltage required to compensate for the energy loss. However, there are other variables that influence the temperature of the resistors such as focus magnet heating, changes in room temperature, changes in cooling water, where the cell is located, etc. Additionally not all of the resistors have equivalent cooling rates and as many as 32 resistors are driven from a single power source. The FXR accelerator group elected to replace the sodium thiosulfate resistors with HVR Linear Disk Resistors in a stack type configuration. With data limited for these resistors when used in oil and at low resistance values, a full characterization needed to be performed. High currents (up to 15kA), high voltages (up to 400kV), and Fast Rise times (<10ns) made a resistor choice difficult. Other solid resistors have been tried and had problems at the connection points and with the fact that the resistivity changed as they absorbed oil. The selected HVR resistors have the advantage of being manufactured with the oil impregnated in to them so this characteristic is minimized while still offering the desired low temperature coefficient of resistance compared to sodium thiosulfate. The characterization experiments and comparison with the sodium thiosulfate liquid resistors will be fully discussed and the final design described.

Kreitzer, B R; Houck, T L; Luchterhand, O C

2011-07-19T23:59:59.000Z

268

Exploring nanomagnetism with soft x-ray microscopy  

SciTech Connect

Magnetic soft X-ray microscopy images magnetism in nanoscale systems with a spatial resolution down to 15nm provided by state-of-the-art Fresnel zone plate optics. X-ray magnetic circular dichroism (X-MCD) is used as element-specific magnetic contrast mechanism similar to photoemission electron microscopy (PEEM), however, with volume sensitivity and the ability to record the images in varying applied magnetic fields which allows to study magnetization reversal processes at fundamental length scales. Utilizing a stroboscopic pump-probe scheme one can investigate fast spin dynamics with a time resolution down to 70 ps which gives access to precessional and relaxation phenomena as well as spin torque driven domain wall dynamics in nanoscale systems. Current developments in zone plate optics aim for a spatial resolution towards 10nm and at next generation X-ray sources a time resolution in the fsec regime can be envisioned.

Fischer, P.; Kim, D.-H.; Mesler, B.L.; Chao, W.; Sakdinawat,A.E.; Anderson, E.H.

2006-10-30T23:59:59.000Z

269

Predicting Fracture Toughness of TRIP 800 using Phase Properties Characterized by In-Situ High Energy X-Ray Diffraction  

Science Conference Proceedings (OSTI)

TRansformation Induced Plasticity (TRIP) steel is a typical representative of 1st generation advanced high strength steel (AHSS) which exhibits a combination of high strength and excellent ductility due to its multiphase microstructure. In this paper, we study the crack propagation behavior and fracture resistance of a TRIP 800 steel using a microstructure-based finite element method with the various phase properties characterized by in-situ high energy Xray diffraction (HEXRD) technique. Uniaxial tensile tests on the notched TRIP 800 sheet specimens were also conducted, and the experimentally measured tensile properties and R-curves (Resistance curves) were used to calibrate the modeling parameters and to validate the overall modeling results. The comparison between the simulated and experimentally measured results suggests that the micromechanics based modeling procedure can well capture the overall complex crack propagation behaviors and the fracture resistance of TRIP steels. The methodology adopted here may be used to estimate the fracture resistance of various multiphase materials.

Soulami, Ayoub; Choi, Kyoo Sil; Liu, Wenning N.; Sun, Xin; Khaleel, Mohammad A.; Ren, Yang; Wang, Yan-Dong

2010-05-01T23:59:59.000Z

270

X-ray emission from laser-produced plasmas  

SciTech Connect

The intensity and spectral characteristics of x-ray emitted from laser-produced plasmas have been investigated computatinoally and experimentally. a two-dimensional implosi code was used successfully to calculate laser-plasma radiation characteristics and to aid in the design of laser targets for high-yield x-ray production. Other computer codes, in use or under development predict lime strengths and energies for laser-plasma x-ray emission. An experimental effort is aimed at reliable measurements of x-ray yields and spectra. a wide variety of x-ray detection methods have been evaluated, and x-ray yields have been measured from plasmas produced with two dissimilar laser systems. The high energy x-ray spectrum, from about 10 to 140 keV, has been studied using high-gain scintillatino detectors and thick K-edge filters. Various supplementary measurements have provided information concerning characteristics of the target-reflected laser light, the ion energies, and the laser intensity patterns.

Violet, C.E. [ed.

1974-07-01T23:59:59.000Z

271

Chandra X-ray Observatory Detection of Extended X-ray Emission from the Planetary Nebula BD+303639  

E-Print Network (OSTI)

We report the detection of well resolved, extended X-ray emission from the young planetary nebula BD+303639 using the Advanced CCD Imaging Spectrometer (ACIS) aboard the Chandra X-ray Observatory. The X-ray emission from BD+303639 appears to lie within, but is concentrated to one side of, the interior of the shell of ionized gas seen in high-resolution optical and IR images. The relatively low X-ray temperature (Tx ~ 3x10^6 K) and asymmetric morphology of the X-ray emission suggests that conduction fronts are present and/or mixing of shock-heated and photoionized gas has occurred and, furthermore, hints at the presence of magnetic fields. The ACIS spectrum suggests that the X-ray emitting region is enriched in the products of helium burning. Our detection of extended X-ray emission from BD+303639 demonstrates the power and utility of Chandra imaging as applied to the study of planetary nebulae.

Kstner, J H; Vrtilek, S D; Dgani, R; Kastner, Joel H.; Soker, Noam; Vrtilek, Saeqa; Dgani, Ruth

2000-01-01T23:59:59.000Z

272

Chandra X-ray Observatory Detection of Extended X-ray Emission from the Planetary Nebula BD+303639  

E-Print Network (OSTI)

We report the detection of well resolved, extended X-ray emission from the young planetary nebula BD+303639 using the Advanced CCD Imaging Spectrometer (ACIS) aboard the Chandra X-ray Observatory. The X-ray emission from BD+303639 appears to lie within, but is concentrated to one side of, the interior of the shell of ionized gas seen in high-resolution optical and IR images. The relatively low X-ray temperature (Tx ~ 3x10^6 K) and asymmetric morphology of the X-ray emission suggests that conduction fronts are present and/or mixing of shock-heated and photoionized gas has occurred and, furthermore, hints at the presence of magnetic fields. The ACIS spectrum suggests that the X-ray emitting region is enriched in the products of helium burning. Our detection of extended X-ray emission from BD+303639 demonstrates the power and utility of Chandra imaging as applied to the study of planetary nebulae.

Joel H. Kastner; Noam Soker; Saeqa Vrtilek; Ruth Dgani

2000-10-09T23:59:59.000Z

273

X-Ray Emission Spectrometer Design with Single-Shot Pump-Probe and Resonant Excitation Capabilities  

Science Conference Proceedings (OSTI)

Core-level spectroscopy in the soft X-ray regime is a powerful tool for the study of chemical bonding processes. The ultrafast, ultrabright X-ray pulses generated by the Linac Coherent Light Source (LCLS) allow these reactions to be studied in greater detail than ever before. In this study, we investigated a conceptual design of a spectrometer for the LCLS with imaging in the non-dispersive direction. This would allow single-shot collection of X-ray emission spectroscopy (XES) measurements with varying laser pump X-ray probe delay or a variation of incoming X-ray energy over the illuminated area of the sample. Ray-tracing simulations were used to demonstrate how the components of the spectrometer affect its performance, allowing a determination of the optimal final design. These simulations showed that the spectrometer's non-dispersive focusing is extremely sensitive to the size of the sample footprint; the spectrometer is not able to image a footprint width larger than one millimeter with the required resolution. This is compatible with a single shot scheme that maps out the laser pump X-ray probe delay in the non-dispersive direction as well as resonant XES applications at normal incidence. However, the current capabilities of the Soft X-Ray (SXR) beamline at the LCLS do not produce the required energy range in a small enough sample footprint, hindering the single shot resonant XES application at SXR for chemical dynamics studies at surfaces. If an upgraded or future beamline at LCLS is developed with lower monochromator energy dispersion the width can be made small enough at the required energy range to be imaged by this spectrometer design.

Spoth, Katherine; /SUNY, Buffalo /SLAC

2012-08-28T23:59:59.000Z

274

Study of Thick CZT Detectors for X-ray and Gamma-ray Astronomy  

Science Conference Proceedings (OSTI)

CdZnTe (CZT) is a wide bandgap II-VI semiconductor developed for the spectroscopic detection of X-rays and {gamma}-rays at room temperature. The Swift Burst Alert Telescope is using an 5240 cm{sup 2} array of 2 mm thick CZT detectors for the detection of 15-150 keV X-rays from Gamma-ray Bursts. We report on the systematic tests of thicker (0.5 cm) CZT detectors with volumes between 2 cm{sup 3} and 4 cm{sup 3} which are potential detector choices for a number of future X-ray telescopes that operate in the 10 keV to a few MeV energy range. The detectors contacted in our laboratory achieve Full Width Half Maximum energy resolutions of 2.7 keV (4.5%) at 59 keV, 3 keV (2.5%) at 122 keV and 4 keV (0.6%) at 662 keV. The 59 keV and 122 keV energy resolutions are among the world-best results for 0.5 cm thick CZT detectors. We use the data set to study trends of how the energy resolution depends on the detector thickness and on the pixel pitch. Unfortunately, we do not find clear trends, indicating that even for the extremely good energy resolutions reported here, the achievable energy resolutions are largely determined by the properties of individual crystals. Somewhat surprisingly, we achieve the reported results without applying a correction of the anode signals for the depth of the interaction. Measuring the interaction depths thus does not seem to be a pre-requisite for achieving sub-1% energy resolutions at 662 keV.

Li Q.; De Geronimo G.; Beilicke, M.; Lee, K.; Garson III, A.; Guo, Q.; Martin, J.; Yin, Y.; Dowkontt, P.; Jung, I.; Krawczynski, H.

2011-02-12T23:59:59.000Z

275

Radiological Safety Training for Radiation-Producing (X-Ray)...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

for General Radiation Safety Installations Using Non-Medical X-Ray and Sealed Gamma-Ray Sources, Energies up to 10 MEV, ANSI Standard N43.3, American National Standards...

276

SLAC National Accelerator Laboratory - X-rays Reveal How Soil...  

NLE Websites -- All DOE Office Websites (Extended Search)

2012 Menlo Park, Calif. - Researchers working at the U.S. Department of Energy's (DOE) SLAC National Accelerator Laboratory have used powerful X-rays to help decipher how certain...

277

SLAC National Accelerator Laboratory - X-ray Laser Sees Photosynthesis...  

NLE Websites -- All DOE Office Websites (Extended Search)

new window on the way plants generate the oxygen we breathe, researchers used an X-ray laser at the Department of Energy's (DOE) SLAC National Accelerator Laboratory to...

278

SLAC National Accelerator Laboratory - X-rays Capture Electron...  

NLE Websites -- All DOE Office Websites (Extended Search)

X-rays Capture Electron 'Dance' By Glenn Roberts Jr. January 30, 2013 The way electrons move within and between molecules, transferring energy as they go, plays an important role...

279

Resolute Marine Energy Inc | Open Energy Information  

Open Energy Info (EERE)

Resolute Marine Energy Inc Resolute Marine Energy Inc Jump to: navigation, search Name Resolute Marine Energy Inc Address 3 Post Office Square 3rd floor Place Massachusetts Zip 02109-3905 Country United States Sector Marine and Hydrokinetic Product Resolute is a wave-power technology developer operating in Massachusetts. Year founded 2007 Number of employees 12 Phone number 917-626-6790 Website http://www.resolutemarine.com References Resolute Marine Energy LinkedIn Connections CrunchBase Profile No CrunchBase profile. Create one now! This company is listed in the Marine and Hydrokinetic Technology Database. This company is involved in the following MHK Projects: Ocean Trials Ver 2 SurgeWEC Ocean Testing 1 This company is involved in the following MHK Technologies: AirWEC SurgeWEC

280

Magnetic soft x-ray microscopy-imaging fast spin dynamics inmagnetic nanostructures  

SciTech Connect

Magnetic soft X-ray microscopy combines 15nm spatial resolution with 70ps time resolution and elemental sensitivity. Fresnel zone plates are used as X-ray optics and X-ray magnetic circular dichroism serves as magnetic contrast mechanism. Thus scientifically interesting and technologically relevant low dimensional nanomagnetic systems can be imaged at fundamental length and ultrafast time scales in a unique way. Studies include magnetization reversal in magnetic multilayers, nanopatterned systems, vortex dynamics in nanoelements and spin current induced phenomena.

Fischer, Peter; Kim, Dong-Hyun; Mesler, Brooke L.; Chao, Weilun; Sakdinawat, Anne E.; Anderson, Erik H.

2007-06-01T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
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281

Development of Ta-based Superconducting Tunnel Junction X-ray Detectors for Fluorescence XAS  

SciTech Connect

We are developing superconducting tunnel junction (STJ) soft X-ray detectors for chemical analysis of dilute samples by fluorescence-detected X-ray absorption spectroscopy (XAS). Our 36-pixel Nb-based STJ spectrometer covers a solid angle {Omega}/4{pi} {approx} 10{sup -3}, offers an energy resolution of {approx}10-20 eV FWHM for energies up to {approx}1 keV, and can be operated at total count rates of {approx}10{sup 6} counts/s. For increased quantum efficiency and cleaner response function, we have now started the development of Ta-based STJ detector arrays. Initial devices modeled after our Nb-based STJs have an energy resolution below 10 eV FWHM for X-ray energies below 1 keV, and pulse rise time discrimination can be used to improve their response function for energies up to several keV. We discuss the performance of the Ta-STJs and outline steps towards the next-generation of large STJ detector arrays with higher sensitivity.

Friedrich, S; Drury, O; Hall, J; Cantor, R

2009-09-23T23:59:59.000Z

282

THE NuSTAR EXTRAGALACTIC SURVEY: A FIRST SENSITIVE LOOK AT THE HIGH-ENERGY COSMIC X-RAY BACKGROUND POPULATION  

SciTech Connect

We report on the first 10 identifications of sources serendipitously detected by the Nuclear Spectroscopic Telescope Array (NuSTAR) to provide the first sensitive census of the cosmic X-ray background source population at {approx}> 10 keV. We find that these NuSTAR-detected sources are Almost-Equal-To 100 times fainter than those previously detected at {approx}> 10 keV and have a broad range in redshift and luminosity (z = 0.020-2.923 and L{sub 10-40{sub keV}} Almost-Equal-To 4 Multiplication-Sign 10{sup 41}-5 Multiplication-Sign 10{sup 45} erg s{sup -1}); the median redshift and luminosity are z Almost-Equal-To 0.7 and L{sub 10-40{sub keV}} Almost-Equal-To 3 Multiplication-Sign 10{sup 44} erg s{sup -1}, respectively. We characterize these sources on the basis of broad-band Almost-Equal-To 0.5-32 keV spectroscopy, optical spectroscopy, and broad-band ultraviolet-to-mid-infrared spectral energy distribution analyses. We find that the dominant source population is quasars with L{sub 10-40{sub keV}} > 10{sup 44} erg s{sup -1}, of which Almost-Equal-To 50% are obscured with N{sub H} {approx}> 10{sup 22} cm{sup -2}. However, none of the 10 NuSTAR sources are Compton thick (N{sub H} {approx}> 10{sup 24} cm{sup -2}) and we place a 90% confidence upper limit on the fraction of Compton-thick quasars (L{sub 10-40{sub keV}} > 10{sup 44} erg s{sup -1}) selected at {approx}> 10 keV of {approx}< 33% over the redshift range z = 0.5-1.1. We jointly fitted the rest-frame Almost-Equal-To 10-40 keV data for all of the non-beamed sources with L{sub 10-40{sub keV}} > 10{sup 43} erg s{sup -1} to constrain the average strength of reflection; we find R < 1.4 for {Gamma} = 1.8, broadly consistent with that found for local active galactic nuclei (AGNs) observed at {approx}> 10 keV. We also constrain the host-galaxy masses and find a median stellar mass of Almost-Equal-To 10{sup 11} M{sub Sun }, a factor Almost-Equal-To 5 times higher than the median stellar mass of nearby high-energy selected AGNs, which may be at least partially driven by the order of magnitude higher X-ray luminosities of the NuSTAR sources. Within the low source-statistic limitations of our study, our results suggest that the overall properties of the NuSTAR sources are broadly similar to those of nearby high-energy selected AGNs but scaled up in luminosity and mass.

Alexander, D. M.; Del Moro, A.; Lansbury, G. B.; Aird, J. [Department of Physics, Durham University, Durham DH1 3LE (United Kingdom); Stern, D.; Assef, R. J. [Jet Propulsion Laboratory, California Institute of Technology, 4800 Oak Grove Drive, Mail Stop 169-221, Pasadena, CA 91109 (United States); Ajello, M.; Boggs, S. E. [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Ballantyne, D. R. [Center for Relativistic Astrophysics, School of Physics, Georgia Institute of Technology, Atlanta, GA 30332 (United States); Bauer, F. E. [Departamento de Astronomia y Astrofisica, Pontificia Universidad Catolica de Chile, Casilla 306, Santiago 22 (Chile); Brandt, W. N. [Department of Astronomy and Astrophysics, 525 Davey Lab, The Pennsylvania State University, University Park, PA 16802 (United States); Christensen, F. E.; Craig, W. W. [DTU Space-National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Civano, F.; Hickox, R. C. [Department of Physics and Astronomy, Dartmouth College, 6127 Wilder Laboratory, Hanover, NH 03755 (United States); Comastri, A. [INAF-Osservatorio Astronomico di Bologna, Via Ranzani 1, I-40127 Bologna (Italy); Elvis, M. [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Grefenstette, B. W.; Harrison, F. A. [Cahill Center for Astrophysics, 1216 East California Boulevard, California Institute of Technology, Pasadena, CA 91125 (United States); Hailey, C. J. [Columbia Astrophysics Laboratory, 550 W 120th Street, Columbia University, NY 10027 (United States); and others

2013-08-20T23:59:59.000Z

283

Hard X-ray Variability of AGN  

E-Print Network (OSTI)

Aims: Active Galactic Nuclei are known to be variable throughout the electromagnetic spectrum. An energy domain poorly studied in this respect is the hard X-ray range above 20 keV. Methods: The first 9 months of the Swift/BAT all-sky survey are used to study the 14 - 195 keV variability of the 44 brightest AGN. The sources have been selected due to their detection significance of >10 sigma. We tested the variability using a maximum likelihood estimator and by analysing the structure function. Results: Probing different time scales, it appears that the absorbed AGN are more variable than the unabsorbed ones. The same applies for the comparison of Seyfert 2 and Seyfert 1 objects. As expected the blazars show stronger variability. 15% of the non-blazar AGN show variability of >20% compared to the average flux on time scales of 20 days, and 30% show at least 10% flux variation. All the non-blazar AGN which show strong variability are low-luminosity objects with L(14-195 keV) < 1E44 erg/sec. Conclusions: Concerning the variability pattern, there is a tendency of unabsorbed or type 1 galaxies being less variable than the absorbed or type 2 objects at hardest X-rays. A more solid anti-correlation is found between variability and luminosity, which has been previously observed in soft X-rays, in the UV, and in the optical domain.

V. Beckmann; S. D. Barthelmy; T. J. -L. Courvoisier; N. Gehrels; S. Soldi; J. Tueller; G. Wendt

2007-09-14T23:59:59.000Z

284

Resonant Auger Effect at High X-Ray Intensity  

SciTech Connect

The resonant Auger effect of atomic neon exposed to high-intensity x-ray radiation in resonance with the 1s {yields} 3p transition is discussed. High intensity here means that the x-ray peak intensity is sufficient ({approx} 10{sup 18} W/cm{sup 2}) to induce Rabi oscillations between the neon ground state and the 1s{sup -1}3p ({sup 1}P) state within the relaxation lifetime of the inner-shell vacancy. For the numerical analysis presented, an effective two-level model, including a description of the resonant Auger decay process, is employed. Both coherent and chaotic x-ray pulses are treated. The latter are used to simulate radiation from x-ray free-electron lasers based on the principle of self-amplified spontaneous emission. Observing x-ray-driven atomic population dynamics in the time domain is challenging for chaotic pulse ensembles. A more practical option for experiments using x-ray free-electron lasers is to measure the line profiles in the kinetic energy distribution of the resonant Auger electron. This provides information on both atomic population dynamics and x-ray pulse properties.

Rohringer, N; Santra, R

2008-03-27T23:59:59.000Z

285

Ultrafast x-ray diagnostics for laser fusion experiments  

SciTech Connect

Temporally, spectrally, and spatially resolved x-ray emission diagnostics are important tools in the study of the heating and compression of laser fusion targets by sub-nanosecond laser pulses. The use of the Livermore 15 psec resolution x-ray streak camera to make such measurements is reviewed. Temporal histories of spectrally resolved x-ray emission in the 1 to 10 keV range have been obtained. These data have served to further define the x-ray streak camera as a quantative diagnostic tool and have also provided data relating to the absorption and compression phases of laser heating. The x-ray streak camera has been used in conjunction with a specially designed pinhole imaging system to temporally record images of laser compressed targets with a spatial resolution of approximately 6 ..mu..m. Implosion characteristics are presented for experiments with glass microshell targets. The concept, development, and testing of an ultrafast framing camera for full two-dimensional time resolved imaging is discussed. A prototype camera, based on the image dissection-restoration concept, has achieved an approximately 200 psec frame period with a resolution of 50 ..mu..m.

Coleman, L.W.

1976-08-16T23:59:59.000Z

286

Low dose hard x-ray contact microscopy assisted by a photoelectric conversion layer  

SciTech Connect

Hard x-ray contact microscopy provides images of dense samples at resolutions of tens of nanometers. However, the required beam intensity can only be delivered by synchrotron sources. We report on the use of a gold photoelectric conversion layer to lower the exposure dose by a factor of 40 to 50, allowing hard x-ray contact microscopy to be performed with a compact x-ray tube. We demonstrate the method in imaging the transmission pattern of a type of hard x-ray grating that cannot be fitted into conventional x-ray microscopes due to its size and shape. Generally the method is easy to implement and can record images of samples in the hard x-ray region over a large area in a single exposure, without some of the geometric constraints associated with x-ray microscopes based on zone-plate or other magnifying optics.

Gomella, Andrew; Martin, Eric W.; Lynch, Susanna K.; Wen, Han [Imaging Physics Laboratory, Biophysics and Biochemistry Center, National Heart, Lung and Blood Institute, National Institutes of Health, Bethesda, MD, 20892 (United States); Morgan, Nicole Y. [Intramural Research Programs, National Institute of Biomedical Imaging and Bioengineering, National Institutes of Health, Bethesda, MD, 20892 (United States)

2013-04-15T23:59:59.000Z

287

Method and apparatus for molecular imaging using X-rays at resonance wavelengths  

DOE Patents (OSTI)

Holographic X-ray images are produced representing the molecular structure of a microscopic object, such as a living cell, by directing a beam of coherent X-rays upon the object to produce scattering of the X-rays by the object, producing interference on a recording medium between the scattered X-rays from the object and unscattered coherent X-rays and thereby producing holograms on the recording surface, and establishing the wavelength of the coherent X-rays to correspond with a molecular resonance of a constituent of such object and thereby greatly improving the contrast, sensitivity and resolution of the holograms as representations of molecular structures involving such constituent. For example, the coherent X-rays may be adjusted to the molecular resonant absorption line of nitrogen at about 401.3 eV to produce holographic images featuring molecular structures involving nitrogen.

Chapline, Jr., George F. (Alamo, CA)

1985-01-01T23:59:59.000Z

288

High-efficiency high-energy Ka source for the critically-required maximum illumination of x-ray optics on Z using Z-petawatt-driven laser-breakout-afterburner accelerated ultrarelativistic electrons LDRD .  

Science Conference Proceedings (OSTI)

Under the auspices of the Science of Extreme Environments LDRD program, a <2 year theoretical- and computational-physics study was performed (LDRD Project 130805) by Guy R Bennett (formally in Center-01600) and Adam B. Sefkow (Center-01600): To investigate novel target designs by which a short-pulse, PW-class beam could create a brighter K{alpha} x-ray source than by simple, direct-laser-irradiation of a flat foil; Direct-Foil-Irradiation (DFI). The computational studies - which are still ongoing at this writing - were performed primarily on the RedStorm supercomputer at Sandia National Laboratories Albuquerque site. The motivation for a higher efficiency K{alpha} emitter was very clear: as the backlighter flux for any x-ray imaging technique on the Z accelerator increases, the signal-to-noise and signal-to-background ratios improve. This ultimately allows the imaging system to reach its full quantitative potential as a diagnostic. Depending on the particular application/experiment this would imply, for example, that the system would have reached its full design spatial resolution and thus the capability to see features that might otherwise be indiscernible with a traditional DFI-like x-ray source. This LDRD began FY09 and ended FY10.

Sefkow, Adam B.; Bennett, Guy R.

2010-09-01T23:59:59.000Z

289

A new bend magnet beam line for scanning transmission x-ray microscopy at the Advanced Light Source  

Science Conference Proceedings (OSTI)

The high brightness of the bend magnets at the Advanced Light Source has been exploited to illuminate a Scanning Transmission X-ray Microscope (STXM). This is the first diffraction-limited scanning x-ray microscope to operate with useful count rate on a synchrotron bend magnet source. A simple, dedicated beam line has been built covering the range of photon energy from 250 eV to 600 eV. Ease of use and operational availability are radically improved compared to previous installations using undulator beams. This facility provides radiation for C 1s, N 1s and O 1s near edge x-ray absorption spectro-microscopy with a spectral resolution up to about 1:5000 and with STXM count rates in excess of 1 MHz.

Warwick, Tony; Ade, Harald; Kilcoyne, A.L. David; Kritscher, Michael; Tylisczcak, Tolek; Fakra, Sirine; Hitchcock, Adam P.; Hitchcock, Peter; Padmore, Howard A.

2001-12-12T23:59:59.000Z

290

Microgap x-ray detector  

DOE Patents (OSTI)

An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

Wuest, Craig R. (Danville, CA); Bionta, Richard M. (Livermore, CA); Ables, Elden (Livermore, CA)

1994-01-01T23:59:59.000Z

291

Imaging X-ray Thomson Scattering Spectrometer Design and Demonstration  

SciTech Connect

In many laboratory astrophysics experiments, intense laser irradiation creates novel material conditions with large, one-dimensional gradients in the temperature, density, and ionization state. X-ray Thomson scattering is a powerful technique for measuring these plasma parameters. However, the scattered signal has previously been measured with little or no spatial resolution, which limits the ability to diagnose inhomogeneous plasmas. We report on the development of a new imaging x-ray Thomson spectrometer (IXTS) for the Omega laser facility. The diffraction of x-rays from a toroidally-curved crystal creates high-resolution images that are spatially resolved along a one-dimensional profile while spectrally dispersing the radiation. This focusing geometry allows for high brightness while localizing noise sources and improving the linearity of the dispersion. Preliminary results are presented from a scattering experiment that used the IXTS to measure the temperature profile of a shocked carbon foam.

Gamboa, E.J. [University of Michigan; Huntington, C.M. [University of Michigan; Trantham, M.R. [University of Michigan; Keiter, P.A [University of Michigan; Drake, R.P. [University of Michigan; Montgomery, David [Los Alamos National Laboratory; Benage, John F. [Los Alamos National Laboratory; Letzring, Samuel A. [Los Alamos National Laboratory

2012-05-04T23:59:59.000Z

292

Fast microtomography using bright monochromatic x-rays  

Science Conference Proceedings (OSTI)

A fast microtomography system for high-resolution high-speed imaging has been developed using bright monochromatic x-rays at the BL29XU beamline of SPring-8. The shortest scan time for microtomography we attained was 0.25 s in 1.25 {mu}m effective pixel size by combining the bright monochromatic x-rays, a fast rotating sample stage, and a high performance x-ray imaging detector. The feasibility of the tomography system was successfully demonstrated by visualization of rising bubbles in a viscous liquid, an interesting issue in multiphase flow physics. This system also provides a high spatial (a measurable feature size of 300 nm) or a very high temporal (9.8 {mu}s) resolution in radiographs.

Jung, J. W.; Lee, J. S.; Park, S. J.; Chang, S.; Pyo, J. [X-ray Imaging Center, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); Department of Materials Science and Engineering, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); Kwon, N.; Kim, J. [X-ray Imaging Center, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); School of Interdisciplinary Bioscience and Bioengineering, Pohang University of Science and Technology, Pohang 790-784 (Korea, Republic of); Kohmura, Y.; Nishino, Y.; Yamamoto, M.; Ishikawa, T. [RIKEN/SPring-8, 1-1-1 Kouto, Mikazuki-cho, Sayo-gun, Hyogo 679-5148 (Japan); Je, J. H. [X-ray Imaging Center, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); Department of Materials Science and Engineering, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); School of Interdisciplinary Bioscience and Bioengineering, Pohang University of Science and Technology, Pohang 790-784 (Korea, Republic of); RIKEN/SPring-8, 1-1-1 Kouto, Mikazuki-cho, Sayo-gun, Hyogo 679-5148 (Japan)

2012-09-15T23:59:59.000Z

293

Spectral analysis of X-ray binaries  

E-Print Network (OSTI)

In this thesis, I present work from three separate research projects associated with observations of X-ray binaries. Two of those revolve around spectral characteristics of neutron star low-mass X-ray binaries (NS-LMXBs), ...

Fridriksson, Joel Karl

2011-01-01T23:59:59.000Z

294

Structural Characterization of Doped GaSb Single Crystals by X-ray Topography  

Science Conference Proceedings (OSTI)

We characterized GaSb single crystals containing different dopants (Al, Cd and Te), grown by the Czochralski method, by x-ray topography and high angular resolution x-ray diffraction. Lang topography revealed dislocations parallel and perpendicular to the crystal's surface. Double-crystal GaSb 333 x-ray topography shows dislocations and vertical stripes than can be associated with circular growth bands. We compared our high-angular resolution x-ray diffraction measurements (rocking curves) with the findings predicted by the dynamical theory of x-ray diffraction. These measurements show that our GaSb single crystals have a relative variation in the lattice parameter ({Delta}d/d) on the order of 10{sup -5}. This means that they can be used as electronic devices (detectors, for example) and as x-ray monochromators.

Honnicke, M.G.; Mazzaro, I.; Manica, J.; Benine, E.; M da Costa, E.; Dedavid, B. A.; Cusatis, C.; Huang, X. R.

2009-09-13T23:59:59.000Z

295

Imaging X-ray spectroscopy with micro-X and Chandra  

E-Print Network (OSTI)

High spectral resolution observations of X-ray phenomena have the potential to uncover new physics. Currently, only point sources can be probed with high resolution spectra, using gratings. Extended objects like supernova ...

Rutherford, John (John Morton)

2013-01-01T23:59:59.000Z

296

Cryotomography x-ray microscopy state  

Science Conference Proceedings (OSTI)

An x-ray microscope stage enables alignment of a sample about a rotation axis to enable three dimensional tomographic imaging of the sample using an x-ray microscope. A heat exchanger assembly provides cooled gas to a sample during x-ray microscopic imaging.

Le Gros, Mark (Berkeley, CA); Larabell, Carolyn A. (Berkeley, CA)

2010-10-26T23:59:59.000Z

297

High energy resolution five-crystal spectrometer for high quality fluorescence and absorption measurements on an X-ray Absorption  

E-Print Network (OSTI)

at the Los Alamos Neutron Science Center (LANSCE). It will be unique among nuclear fuel irradiation at Idaho National Laboratory for fabrication of metallic nuclear fuels rods. A small bench scale caster and emission applications, and study their optical properties. Colloidal nanomaterials for light harvesting

298

X-Ray Diffraction on NIF  

SciTech Connect

The National Ignition Facility (NIF) is currently a 192 beam, 1.6 MJ laser. NIF Ramp-Compression Experiments have already made the relevant exo-planet pressure range from 1 to 50 Mbar accessible. We Proposed to Study Carbon Phases by X-Ray Diffraction on NIF. Just a few years ago, ultra-high pressure phase diagrams for materials were very 'simple'. New experiments and theories point out surprising and decidedly complex behavior at the highest pressures considered. High pressures phases of aluminum are also predicted to be complex. Recent metadynamics survey of carbon proposed a dynamic pathway among multiple phases. We need to develop diagnostics and techniques to explore this new regime of highly compressed matter science. X-Ray Diffraction - Understand the phase diagram/EOS/strength/texture of materials to 10's of Mbar. Strategy and physics goals: (1) Powder diffraction; (2) Begin with diamond; (3) Continue with metals etc.; (4) Explore phase diagrams; (5) Develop liquid diffraction; and (6) Reduce background/improve resolution.

Eggert, J H; Wark, J

2012-02-15T23:59:59.000Z

299

USING THE X-RAY EMISSION LINES OF SEYFERT 2 AGN TO MEASURE ABUNDANCE RATIOS  

E-Print Network (OSTI)

We measure the metal abundance ratios in the X-ray photoionized gas located near the narrow line region of a sample of Seyfert 2 AGN. The high-resolution X-ray spectra observed with the Chandra high- and low-energy transmission grating spectrometers are compared with models of the resonant scattering and recombination emission from a plasma in thermal balance, and with multiple temperature zones. The abundance ratios in the sample are close to the Solar values, with slight over-abundances of N in NGC 1068, and of Ne in NGC 4151. Our X-ray spectral models use fewer degrees of freedom than previous works. Motivation. Our goal is to use X-ray abundance measurements to cross-calibrate with the optical spectra of quasars. These optical spectra are used to measure the star formation history of the early Universe. 1 To Determine the Abundance Ratios, we fit the Seyfert 2 spectra with models of photoionized plasmas, and then search for deviations in the data from Solar abundances, as shown in Fig. 1. The fluxes of radiative recombination continuum (RRC) features and the radiative recombination (RR) forbidden lines depend little on radiation transfer effects, so they are the most reliable abundance indicators. At low continuum optical depths, the recombination emission flux scales linearly with abundances. Our model allows us to fit the RRC and RR fluxes by accounting for the broad ionization distribution in the plasma. X-ray Emission Line Model. We model a photoionized plasma in ionization equilibrium and thermal balance with a grid of zones, each with ionization parameter log ? = 1.0, 1.5,...4.5 (in c.g.s. units). The XSTAR plasma code yields the charge state distribution of each zone. 2 In order to calculate the recombination emission, we use the photoelectric cross sections

Mario A. Jimenez-garate; Toan Khu

2004-01-01T23:59:59.000Z

300

Design and Assembly of a Telecentric Zoom Lens for the Cygnus X-ray Source  

Science Conference Proceedings (OSTI)

Cygnus is a high-energy radiographic x-ray source. The rod-pinch x-ray diode produces a point source measuring 1 mm diameter. The target object is placed 1.5 m from the x-ray source, with a large LYSO scintillator at 2.4 m. Different-sized objects are imploded within a containment vessel. A large pellicle deflects the scintillator light out of the x-ray path into an 11-element zoom lens coupled to a CCD camera. The zoom lens and CCD must be as close as possible to the scintillator to maximize light collection. A telecentric lens design minimizes image blur from a volume source. To maximize the resolution of test objects of different sizes, the scintillator and zoom lens can be translated along the x-ray axis. Zoom lens magnifications are changed when different-sized scintillators and recording cameras are used (50 or 62 mm square format). The LYSO scintillator measures 200 200 mm and is 5 mm thick. The scintillator produces blue light peaking at 435 nm, so special lens materials are required. By swapping out one lens element and allowing all lenses to move, the zoom lens can also use a CsI(Tl) scintillator that produces green light centered at 550 nm. All lenses are coated with anti-reflective coating for both wavelength bands. Two sets of doublets, the stop, and the CCD camera move during zoom operations. One doublet has XY compensation. The first three lenses use fused silica for radiation damage control. The 60 lb of glass inside the 340 lb mechanical structure is oriented vertically.

Malone, R M; Brown, K K; Curtis, A H; Esquibel, D L; Frayer, D K; Frogget, B C; Furlanetto, M R; Garten, J R; Haines, T J; Howe, R A; Huerta, J A; Kaufman, M I; King, N.S. P; Lutz, S S; McGillivray, K D

2012-10-01T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
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301

Elemental and magnetic sensitive imaging using x-ray excited luminescence microscopy  

Science Conference Proceedings (OSTI)

We demonstrate the potential of x-ray excited luminescence microscopy for full-field elemental and magnetic sensitive imaging using a commercially available optical microscope, mounted on preexisting synchrotron radiation (SR) beamline end stations. The principal components of the instrument will be described. Bench top measurements indicate that a resolution of 1 {mu}m or better is possible; this value was degraded in practice due to vibrations and/or drift in the end station and associated manipulator. X-ray energy dependent measurements performed on model solar cell materials and lithographically patterned magnetic thin film structures reveal clear elemental and magnetic signatures. The merits of the apparatus will be discussed in terms of conventional SR imaging techniques.

Rosenberg, R. A.; Zohar, S.; Keavney, D. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Divan, R.; Rosenmann, D. [Center for Nanoscale Materials, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Mascarenhas, A.; Steiner, M. A. [National Renewable Energy Lab, Golden, Colorado 80401 (United States)

2012-07-15T23:59:59.000Z

302

Cryogenic detector development at LLNL: ultraviolet x-ray, gamma-ray and biomolecule spectroscopy  

SciTech Connect

We are developing low-temperature detectors for optical, ultraviolet, X-ray, and gamma-ray spectroscopy, and for biomolecular mass spectrometry. We present development work on these detectors and materials analysis and biomolecular mass spectrometry. We have measured thin-film Nb/Al/Al2O3/AlNb superconducting tunnel junction (STJ) X-ray detectors in the 0.2 to 1 keV band with a range of different junction sizes and aluminum film thicknesses. In one case, we have achieved the statistical limit to the energy resolution of 13 eV FWHM at 227 eV with an output count rate of 20,600 cts/s.

Labov, S.E.; Frank, M.; le Grand, J.B. [and others

1997-08-12T23:59:59.000Z

303

X-ray transmissive debris shield  

DOE Patents (OSTI)

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, R.B.

1996-05-21T23:59:59.000Z

304

X-ray transmissive debris shield  

DOE Patents (OSTI)

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, Rick B. (Albuquerque, NM)

1996-01-01T23:59:59.000Z

305

X-RAY NONLINEAR OPTICAL PROCESSES IN ATOMS USING A SELF-AMPLIFIED SPONTANEOUS EMISSION FREE-ELECTRON LASER  

SciTech Connect

X-ray free electron lasers (xFEL) will open new avenues to the virtually unexplored territory of non-linear interactions of x rays with matter. Initially xFELs will be based on the principle of self-amplified spontaneous emission (SASE). Each SASE pulse consists of a number of coherent intensity spikes of random amplitude, i.e. the process is chaotic and pulses are irreproducible. The coherence time of SASE xFELs will be a few femtoseconds for a photon energy near 1 keV. The importance of coherence properties of light in non-linear optical processes was theoretically discovered in the early 1960s. In this contribution we will illustrate the impact of field chaoticity on x-ray non-linear optical processes on neon for photon energies around 1 keV and intensities up to 10{sup 18} W/cm{sup 2}. Resonant and non-resonant processes are discussed. The first process to be addressed is the formation of a double-core hole in neon by photoionization with x rays above 1.25 keV energy. In contrast to the long-wavelength regime, non-linear optical processes in the x-ray regime are characterized in general by sequential single-photon single-electron interactions. Despite this fact, the sequential absorption of multiple x-ray photons depends on the statistical properties of the radiation field. Treating the x rays generated by a SASE FEL as fully chaotic, a quantum-mechanical analysis of inner-shell two-photon absorption is performed. By solving a system of time-dependent rate equations, we demonstrate that double-core hole formation in neon via x-ray two-photon absorption is enhanced by chaotic photon statistics. At an intensity of 10{sup 16} W/cm{sup 2}, the statistical enhancement is about 30%, much smaller than typical values in the optical regime. The second part of this presentation discusses the resonant Auger effect of atomic neon at the 1s-3p transition (at 867.1 eV). For low X-ray intensity, the excitation process 1s {yields} 3p in Neon can be treated perturbatively. The core-hole excited 1s{sup -1} 3p state is embedded in the continuum and decays via Auger-process on the timescale of approximately 5 fs. Increasing the x-ray intensity above 1.5 x 10{sup 18} W/cm{sup 2}, a peak intensity accessible with xFEL sources in the near future, x-ray induced emission from 3p back to 1s becomes possible, i.e. Rabi oscillations between these two levels can be induced. For the numerical analysis of this process, an effective two-level model, including a description of the resonant Auger decay process, is employed. The observation of x-ray-driven atomic populations dynamics in the time domain is challenging for chaotic xFEL pulses. In addition to requiring single-shot measurements, sub-femtosecond temporal resolution would be needed. The Rabi oscillations will, however, be imprinted on the kinetic energy distribution of the resonant Auger electron (see Fig. 1). Measuring the resonant Auger-electron line profile will provide information on both atomic population dynamics and x-ray pulse properties.

Rohringer, N

2008-08-08T23:59:59.000Z

306

X-ray Microscopy and Imaging (XSD-XMI)  

NLE Websites -- All DOE Office Websites (Extended Search)

Imaging (XMI) Imaging (XMI) About XMI Science and Research Beamlines Highlights Software and Tools Intranet Search APS... Argonne Home > Advanced Photon Source > Contacts FAQs Beamlines News Publications APS Email Portal APS Intranet APS Phonebook APS Quick Links for Users APS Safety and Training Welcome to the X-ray Microscopy and Imaging group (XMI)! X-ray Microscopy and Imaging is part of the X-ray Science Division at the Advanced Photon Source. We develop and support a diverse and multidisciplinary user research program at Sectors 2 and 32 of the APS, with the overall goal to image and study materials structures at spatial and temporal resolutions that are most scientifically relevant to the cutting-edge advances in materials, biological, environmental, and biomedical sciences. To achieve this goal, we actively engage in various research activities including

307

X-Ray Diffraction Project Final Report, Fiscal Year 2006  

SciTech Connect

An x-ray diffraction diagnostic system was developed for determining real-time shock-driven lattice parameter shifts in single crystals at the gas gun at TA-IV at Sandia National Laboratories (SNL). The signal-to-noise ratio and resolution of the system were measured using imaging plates as the detector and by varying the slit width. This report includes tests of the x-ray diffraction system using a phosphor coupled to a charge-coupled device (CCD) camera by a coherent fiber-optic bundle. The system timing delay was measured with a newly installed transistor-transistor logic (TTL) bypass designed to reduce the x-ray delay time. The axial misalignment of the Bragg planes was determined with respect to the optical axis for a set of eight LiF [lithium fluoride] crystals provided by SNL to determine their suitability for gas gun experiments.

Dane V. Morgan

2006-10-01T23:59:59.000Z

308

Stress Management: X-Rays Reveal Si Thin-Film Defects  

Science Conference Proceedings (OSTI)

Stress Management: X-Rays Reveal Si Thin-Film Defects. ... Advanced Photon Source, and supported in part by the Department of Energy. ...

2011-04-26T23:59:59.000Z

309

The Use of Micro-X-ray Fluorescence in a Scanning Electron ...  

Science Conference Proceedings (OSTI)

An X-ray gun with focusing capillary fiber optics interfaced with a scanning electron microscope (SEM) is used for semi-quantitative XRF microanalysis by energy...

310

Advanced Data Analysis Tools for World-Wide X-ray ...  

Science Conference Proceedings (OSTI)

... of ifeffit, a multi-platform, open-source XAS data analysis software ... The energy dependent interaction of the intense synchrotron X-ray beam with ...

2012-10-01T23:59:59.000Z

311

Carbon nanotube based microfocus field emission x-ray source for microcomputed tomography  

Science Conference Proceedings (OSTI)

Microcomputed tomography is now widely used for in vivo small animal imaging for cancer studies. Achieving high imaging quality of live objects requires the x-ray source to have both high spatial and temporal resolutions. Preliminary studies have shown that carbon nanotube (CNT) based field emission x-ray source has significant intrinsic advantages over the conventional thermionic x-ray tube including better temporal resolution and programmability. Here we report the design and characterization of a CNT based field emission x-ray source that also affords a high spatial resolution. The device uses modified asymmetric Einzel lenses for electron focusing and an elliptical shaped CNT cathode patterned by photolithography. Stable and small isotropic x-ray focal spot sizes were obtained.

Liu Zejian; Yang Guang; Lee, Yueh Z.; Bordelon, David; Lu Jianping; Zhou, Otto [Department of Physics and Astronomy, University of North Carolina, Chapel Hill, North Carolina 27599 (United States); School of Medicine, University of North Carolina, Chapel Hill, North Carolina 27599 (United States); Curriculum in Applied and Materials Sciences, University of North Carolina, Chapel Hill, North Carolina 27599 (United States); Department of Physics and Astronomy, University of North Carolina, Chapel Hill, North Carolina 27599 and Curriculum in Applied and Materials Sciences, University of North Carolina, Chapel Hill, North Carolina 27599 (United States)

2006-09-04T23:59:59.000Z

312

K-alpha conversion efficiency measurments for x-ray scattering in inertial confinement fusion plasmas  

SciTech Connect

The conversion efficiency of ultra short-pulse laser radiation to K-{alpha} x-rays has been measured for various chlorine-containing targets to be used as x-ray scattering probes of dense plasmas. The spectral and temporal properties of these sources will allow spectrally-resolved x-ray scattering probing with picosecond temporal resolution required for measuring the plasma conditions in inertial confinement fusion experiments. Simulations of x-ray scattering spectra from these plasmas show that fuel capsule density, capsule ablator density, and shock timing information may be inferred.

Kritcher, A L; Neumayer, P; Urry, M K; Robey, H; Niemann, C; Landen, O L; Morse, E; Glenzer, S H

2006-11-21T23:59:59.000Z

313

ZnTe:O phosphor development for x-ray imaging applications  

Science Conference Proceedings (OSTI)

An efficient ZnTe:O x-ray powder phosphor was prepared by a dry synthesis process using gaseous doping and etching medias. The x-ray luminescent properties were evaluated and compared to standard commercial phosphors exhibited an x-ray luminescent efficiency equivalent to 76% of Gd{sub 2}O{sub 2}S:Tb and an equal resolution of 2.5 lines/mm. In addition, the fast decay time, low afterglow, and superior spectral match to conventional charge-coupled devices-indicate that ZnTe:O is a very promising phosphor candidate for x-ray imaging applications.

Kang, Z.T.; Summers, C.J.; Menkara, H.; Wagner, B.K.; Durst, R.; Diawara, Y.; Mednikova, G.; Thorson, T. [Phosphor Technology Center of Excellence, School of Materials Science and Engineering, Georgia Institute of Technology, Atlanta, Georgia 30332-0245 (United States); Georgia Tech Research Institute, Georgia Institute of Technology, Atlanta, Georgia 30332-0826 (United States); Bruker AXS 5465 East Cheryl Parkway, Madison Wisconson 53711 (United States)

2006-03-13T23:59:59.000Z

314

Ultra-Short Electron Bunch and X-Ray Temporal Diagnostics with an X-Band Transverse Deflector  

Science Conference Proceedings (OSTI)

The measurement of ultra-short electron bunches on the femtosecond time scale constitutes a very challenging problem. In X-ray free-electron laser facilities such as the Linac Coherent Light Source (LCLS), generation of sub-ten femtosecond X-ray pulses is possible, and some efforts have been put into both ultra-short electron and X-ray beam diagnostics. Here we propose a single-shot method using a transverse rf deflector (X-band) after the undulator to reconstruct both the electron bunch and X-ray temporal profiles. Simulation studies show that about 1 fs (rms) time resolution may be achievable in the LCLS and is applicable to a wide range of FEL wavelengths and pulse lengths. The jitter, resolution and other related issues will be discussed. The successful operation of the Linac Coherent Light Source (LCLS), with its capability of generating free-electron laser (FEL) X-ray pulses from a few femtoseconds (fs) up to a few hundred fs, opens up vast opportunities for studying atoms and molecules on this unprecedented ultrashort time scale. However, tremendous challenges remain in the measurement and control of these ultrashort pulses with femtosecond precision, for both the electron beam (e-beam) and the X-ray pulses. For ultrashort e-beam bunch length measurements, a standard method has been established at LCLS using an S-band radio-frequency (rf) deflector, which works like a streak camera for electrons and is capable of resolving bunch lengths as short as {approx} 10 fs rms. However, the e-beam with low charges of 20 pC at LCLS, which is expected to be less than 10 fs in duration, is too short to be measured using this transverse deflector. The measurement of the electron bunch length is helpful in estimating the FEL X-ray pulse duration. However, for a realistic beam, such as that with a Gaussian shape or even a spiky profile, the FEL amplification varies along the bunch due to peak current or emittance variation. This will cause differences between the temporal shape or duration of the electron bunch and the X-ray pulse. Initial experiments at LCLS have revealed that characterization of the X-ray pulse duration on a shot-by-shot basis is critical for the interpretation of the data. However, a reliable x-ray pulse temporal diagnostic tool is not available so far at the LCLS. We propose a novel method in this paper to characterize the FEL X-ray pulse duration and shape. A transverse rf deflector is used in conjunction with an e-beam energy spectrometer, located after the FEL undulator. By measuring the difference in the e-beam longitudinal phase space between FEL-on and FEL-off, we can obtain the time-resolved energy loss and energy spread induced from the FEL radiation, allowing the FEL X-ray temporal shape to be reconstructed.

Ding, Y.; Emma, P.; Frisch, J.; Huang, Z.; Loos, H.; Krejcik, P.; Wang, M-H.; /SLAC; Behrens, C.; /DESY

2011-12-13T23:59:59.000Z

315

X-RAY STRIPES IN TYCHO'S SUPERNOVA REMNANT: SYNCHROTRON FOOTPRINTS OF A NONLINEAR COSMIC-RAY-DRIVEN INSTABILITY  

Science Conference Proceedings (OSTI)

High-resolution Chandra observations of Tycho's supernova remnant (SNR) have revealed several sets of quasi-steady, high-emissivity, nearly parallel X-ray stripes in some localized regions of the SNR. These stripes are most likely the result of cosmic-ray (CR) generated magnetic turbulence at the SNR blast wave. However, for the amazingly regular pattern of these stripes to appear, simultaneous action of a number of shock-plasma phenomena is required, which is not predicted by most models of magnetic field amplification. A consistent explanation of these stripes yields information on the complex nonlinear plasma processes connecting efficient CR acceleration and magnetic field fluctuations in strong collisionless shocks. The nonlinear diffusive shock acceleration (NL-DSA) model described here, which includes magnetic field amplification from a CR-current-driven instability, does predict stripes consistent with the synchrotron observations of Tycho's SNR. We argue that the local ambient mean magnetic field geometry determines the orientation of the stripes and therefore it can be reconstructed with the high-resolution X-ray imaging. The estimated maximum energy of the CR protons responsible for the stripes is {approx}10{sup 15} eV. Furthermore, the model predicts that a specific X-ray polarization pattern, with a polarized fraction {approx}50%, accompanies the stripes, which can be tested with future X-ray polarimeter missions.

Bykov, Andrei M.; Osipov, Sergei M.; Uvarov, Yury A. [Ioffe Physical-Technical Institute, St. Petersburg (Russian Federation); Ellison, Donald C. [Department of Physics, North Carolina State University, Raleigh, NC 27695-8202 (United States); Pavlov, George G., E-mail: byk@astro.ioffe.ru, E-mail: osm@astro.ioffe.ru, E-mail: uv@astro.ioffe.ru, E-mail: don_ellison@ncsu.edu, E-mail: pavlov@astro.psu.edu [525 Davey Laboratory, Pennsylvania State University, University Park, PA 16802 (United States)

2011-07-10T23:59:59.000Z

316

Neutron and X-Ray Scattering - Argonne National Laboratories, Materials  

NLE Websites -- All DOE Office Websites (Extended Search)

Home Home Neutron and X-Ray Scattering Neutron and X-ray Scattering Science Recent advances in neutron and x-ray scattering instrumentation at major DOE facilities such as the Spallation Neutron Source and Advanced Photon Source provide unprecedented insights into complex phenomena in bulk and interfacial materials. The vision of our group is to harness the complementarity of neutrons and x-rays to study how materials respond on a range of length and time scales to phase competition, so that we can learn to control emergent behavior and generate functional properties in energy-related materials. We use neutrons and x-rays to investigate the structure and dynamics of bulk and interfacial materials with properties that are useful for energy applications, such as superconductivity, magnetism and thermoelectricity. Phase competition can generate or enhance such properties, but it is extremely challenging to characterize fluctuations in the competing order, whether in bulk disordered materials, or artificial heterostructures. Our goal is to utilize efficient techniques that we have been developing for measuring nanoscale phase fluctuations, both static and dynamic, to enable the rational design of new materials for energy within MSD.

317

Studying Nanoscale Magnetism and its Dynamics with Soft X-ray Microscopy  

Science Conference Proceedings (OSTI)

Magnetic soft X-ray microscopy allows for imaging magnetic structures at a spatial resolution down to 15nm and a time resolution in the sub-100ps regime. Inherent elemental specificity can be used to image the magnetic response of individual components such as layers in multilayered systems. This review highlights current achievements and discusses the future potential of magnetic soft X-ray microscopy at fsec X-ray sources where snapshot images of ultrafast spin dynamics with a spatial resolution below 10nm will become feasible.

Mccall, Monnikue M; Fischer, Peter

2008-05-01T23:59:59.000Z

318

Lessening X-ray damage is healthy for protein discovery data too | Argonne  

NLE Websites -- All DOE Office Websites (Extended Search)

The brightness and energy of X-ray beams are critical properties for The brightness and energy of X-ray beams are critical properties for research. The APS Upgrade will make our X-ray beams brighter, meaning more X-rays can be focused onto a smaller, laser-like spot, allowing researchers to gather more data in greater detail in less time. Lessening X-ray damage is healthy for protein discovery data too December 16, 2013 Tweet EmailPrint New recommendations for using X-rays promise to speed investigations aimed at understanding the structure and function of biologically important proteins - information critical to the development of new drugs. Scientists from two U.S. Department of Energy national laboratories, Argonne and Brookhaven, and the University of Washington, Seattle, evaluated options to remedy problems affecting data collection in their new

319

Secretary Chu Dedicates World's Most Powerful X-ray Laser | Department of  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Dedicates World's Most Powerful X-ray Laser Dedicates World's Most Powerful X-ray Laser Secretary Chu Dedicates World's Most Powerful X-ray Laser August 16, 2010 - 12:00am Addthis Washington, D.C. - U.S. Energy Secretary Steven Chu today dedicated the Linac Coherent Light Source (LCLS), the world's first and most powerful X-ray laser, at the Department of Energy's SLAC National Accelerator Laboratory. The LCLS will play an essential role in addressing the scientific needs of the 21st century by exploring new ways to create better energy sources and enabling advances in a range of scientific fields. The LCLS produces pulses of X-rays more than a billion times brighter than the most powerful existing sources. The ultrafast X-ray pulses are used much like flashes from a high-speed strobe light, enabling scientists to take

320

Measurement of plutonium in spent nuclear fuel by self-induced x-ray fluorescence  

Science Conference Proceedings (OSTI)

Direct measurement of the plutonium content in spent nuclear fuel is a challenging problem in non-destructive assay. The very high gamma-ray flux from fission product isotopes overwhelms the weaker gamma-ray emissions from plutonium and uranium, making passive gamma-ray measurements impossible. However, the intense fission product radiation is effective at exciting plutonium and uranium atoms, resulting in subsequent fluorescence X-ray emission. K-shell X-rays in the 100 keV energy range can escape the fuel and cladding, providing a direct signal from uranium and plutonium that can be measured with a standard germanium detector. The measured plutonium to uranium elemental ratio can be used to compute the plutonium content of the fuel. The technique can potentially provide a passive, non-destructive assay tool for determining plutonium content in spent fuel. In this paper, we discuss recent non-destructive measurements of plutonium X-ray fluorescence (XRF) signatures from pressurized water reactor spent fuel rods. We also discuss how emerging new technologies, like very high energy resolution microcalorimeter detectors, might be applied to XRF measurements.

Hoover, Andrew S [Los Alamos National Laboratory; Rudy, Cliff R [Los Alamos National Laboratory; Tobin, Steve J [Los Alamos National Laboratory; Charlton, William S [Los Alamos National Laboratory; Stafford, A [TEXAS A& M; Strohmeyer, D [TEXAS A& M; Saavadra, S [ORNL

2009-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

Method and apparatus for micromachining using hard X-rays  

DOE Patents (OSTI)

An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures.

Siddons, David Peter (Shoreham, NY); Johnson, Erik D. (Ridge, NY); Guckel, Henry (Madison, WI); Klein, Jonathan L. (Madison, WI)

1997-10-21T23:59:59.000Z

322

Method and apparatus for micromachining using hard X-rays  

DOE Patents (OSTI)

An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures. 21 figs.

Siddons, D.P.; Johnson, E.D.; Guckel, H.; Klein, J.L.

1997-10-21T23:59:59.000Z

323

X-ray Time Lags in TeV Blazars  

E-Print Network (OSTI)

We use Monte Carlo/Fokker-Planck simulations to study the X-ray time lags. Our results show that soft lags will be observed as long as the decay of the flare is dominated by radiative cooling, even when acceleration and cooling timescales are similar. Hard lags can be produced in presence of a competitive achromatic particle energy loss mechanism if the acceleration process operates on a timescale such that particles are slowly moved towards higher energy while the flare evolves. In this type of scenario, the {\\gamma} -ray/X-ray quadratic relation is also reproduced.

Chen, Xuhui; Liang, Edison; Bttcher, Markus

2011-01-01T23:59:59.000Z

324

Cooled window for X-rays or charged particles  

DOE Patents (OSTI)

A window is disclosed that provides good structural integrity and a very high capacity for removal of the heat deposited by x-rays, electrons, or ions, with minimum attenuation of the desired beam. The window is cooled by providing microchannels therein through which a coolant is pumped. For example, the window may be made of silicon with etched microchannels therein and covered by a silicon member. A window made of silicon with a total thickness of 520 {micro}m transmits 96% of the x-rays at an energy of 60 keV, and the transmission is higher than 90% for higher energy photons. 1 fig.

Logan, C.M.

1996-04-16T23:59:59.000Z

325

Cooled window for X-rays or charged particles  

DOE Patents (OSTI)

A window that provides good structural integrity and a very high capacity for removal of the heat deposited by x-rays, electrons, or ions, with minimum attenuation of the desired beam. The window is cooled by providing microchannels therein through which a coolant is pumped. For example, the window may be made of silicon with etched microchannels therein and covered by a silicon member. A window made of silicon with a total thickness of 520 .mu.m transmits 96% of the x-rays at an energy of 60 keV, and the transmission is higher than 90% for higher energy photons.

Logan, Clinton M. (Pleasanton, CA)

1996-01-01T23:59:59.000Z

326

Application of an EMCCD Camera for Calibration of Hard X-Ray Telescopes  

SciTech Connect

Recent technological innovations now make it feasible to construct hard x-ray telescopes for space-based astronomical missions. Focusing optics are capable of improving the sensitivity in the energy range above 10 keV by orders of magnitude compared to previously used instruments. The last decade has seen focusing optics developed for balloon experiments and they will soon be implemented in approved space missions such as the Nuclear Spectroscopic Telescope Array (NuSTAR) and ASTRO-H. The full characterization of x-ray optics for astrophysical and solar imaging missions, including measurement of the point spread function (PSF) as well as scattering and reflectivity properties of substrate coatings, requires a very high spatial resolution, high sensitivity, photon counting and energy discriminating, large area detector. Novel back-thinned Electron Multiplying Charge-Coupled Devices (EMCCDs) are highly suitable detectors for ground-based calibrations. Their chip can be optically coupled to a microcolumnar CsI(Tl) scintillator via a fiberoptic taper. Not only does this device exhibit low noise and high spatial resolution inherent to CCDs, but the EMCCD is also able to handle high frame rates due to its controllable internal gain. Additionally, thick CsI(Tl) yields high detection efficiency for x-rays. This type of detector has already proven to be a unique device very suitable for calibrations in astrophysics: such a camera was used to support the characterization of the performance for all NuSTAR optics. Further optimization will enable similar cameras to be improved and used to calibrate x-ray telescopes for future space missions. In this paper, we discuss the advantages of using an EMCCD to calibrate hard x-ray optics. We will illustrate the promising features of this detector solution using examples of data obtained during the ground calibration of the NuSTAR telescopes performed at Columbia University during 2010/2011. Finally, we give an outlook on ongoing development and optimizations, such as the use of single photon counting mode to enhance spectral resolution.

Vogel, J K; Pivovaroff, M J; Nagarkar, V V; Kudrolli, H; Madsen, K K; Koglin, J E; Christensen, F E; Brejnholt, N F

2011-11-08T23:59:59.000Z

327

Spectral unfolds of PITHON Flash X-ray source.  

SciTech Connect

Using a differential absorption spectrometer we obtained experimental spectral information for the PITHON Flash X-ray Machine located in San Leandro, California at L-3 Communications. Spectral information we obtained pertained to the 200 keV to 800 keV endpoint operation of PITHON. We also obtained data on the temporal behavior of high energy and low energy spectral content.

Zarick, Thomas Andrew; Sheridan, Timothy J.; Hartman, E. Frederick; Riordan, John C. (L-3 Pulse Sciences)

2007-11-01T23:59:59.000Z

328

An X-ray photometry system I: Chandra ACIS  

E-Print Network (OSTI)

We present a system of X-ray photometry for the Chandra satellite. X-ray photometry can be a powerful tool to obtain flux estimates, hardness ratios, and colors unbiased by assumptions about spectral shape and independent of temporal and spatial changes in instrument characteristics. The system we have developed relies on our knowledge of effective area and the energy-to-channel conversion to construct filters similar to photometric filters in the optical bandpass. We show that the filters are well behaved functions of energy and that this X-ray photometric system is able to reconstruct fluxes to within about 20%, without color corrections, for non-pathological spectra. Even in the worst cases it is better than 50%. Our method also treats errors in a consistent manner, both statistical as well as systematic.

Grimm, H -J; Fabbiano, G; Elvis, M

2008-01-01T23:59:59.000Z

329

X-ray Line Profile Analysis  

Science Conference Proceedings (OSTI)

... Magnetic Composite Materials X-Ray Studies of Structural Effects Induced by Pulsed (30 Tesla), High Magnetic Fields at the Advanced Photon Source...

330

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray...

331

Hard X-Ray Quad Collimator  

Technology Development and Commercialization Division One of the best ways to obtain small?size x?ray beams for structural biology research is to ...

332

X-ray Diagnostics of Broad Absorption Line Quasar Geometry  

E-Print Network (OSTI)

A new generation of sensitive X-ray measurements are indicating that the existence of X-ray attenuation column densities, $N_{H}>10^{24}\\mathrm{cm}^{-2}$ is quite common amongst broad absorption line quasars (BALQSOs). This is significant to the geometry of the broad absorption line (BAL) outflow. In particular, such an X-ray shield also shields equatorial accretion disk winds from the UV, thereby preventing high velocity equatorial outflows from being launched. By contrast, bipolar winds initiated by continuum radiation pressure from the funnel of a slim accretion disk flare outward (like a trumpet) and offer vastly different absorbing columns to the X-ray and UV emission which are emitted from distinct regions of the disk, $\\sim 6M$ and $\\sim 10M-40M$, respectively (where $M$ is the radius of the black hole). Recent numerical work indicates that it is also possible to launch bipolar outflows from the inner regions of a thin disk. The recent discovery with VLBI that the Galactic analog of a BALQSO, the X-ray binary Circinus X-1 (with high velocity P Cygni X-ray absorption lines) is viewed virtually along the radio jet axis (and therefore along the spin axis of the black hole and the normal to the accretion disk) has rekindled interest in the bipolar models of BALQSOs. We explore this possibility by studying the nearest BAL QSO, MRK 231. High resolution 2-D optical spectroscopy and VLBI mappings of the radio jet axis indicates that the BAL outflow is parallel to the parsec scale radio jet.

Brian Punsly; Sebastian Lipari

2005-03-09T23:59:59.000Z

333

YOHKOH remnants: partially occulted flares in hard X-rays  

E-Print Network (OSTI)

Flares being partially occulted by the solar limb, are the best reservoir of our knowledge about hard X-ray loop-top sources. Recently, the survey of partially occulted flares observed by the RHESSI has been published (Krucker & Lin 2008). The extensive YOHKOH database still awaits such activities. This work is an attempt to fill this gap. Among from 1286 flares in the YOHKOH Hard X-ray Telescope Flare Catalogue, for which the hard X-ray images had been enclosed, we identified 98 events that occurred behind the solar limb. We investigated their hard X-ray spectra and spatial structure. We found that in most cases the hard X-ray spectrum of partially occulted flares consists of two components, non-thermal and thermal, which are co-spatial. The photon energy spectra of the partially occulted flares are systematically steeper than spectra of the non-occulted flares. Such a difference we explain as a consequence of intrinsically dissimilar conditions ruling in coronal parts of flares, in comparison with the f...

Tomczak, M

2009-01-01T23:59:59.000Z

334

Electronic State Interferences in Resonant X-Ray Emission after K-Shell Excitation in HCl  

SciTech Connect

We have measured a series of high-resolution x-ray spectra emitted upon resonant photoexcitation of HCl. The photon energy was tuned across the dissociative 1s{yields}6{sigma}* resonance and the Rydberg states converging to the Cl 1s{sup -1} threshold, and inelastic photon scattering was observed in the region of KL emission lines. Excellent agreement is found between fully ab initio calculated and measured spectra if interferences between different excitation-emission paths are taken into account. The effect of electronic state interferences is enhanced due to dynamical broadening of the 6{sigma}* resonance in HCl.

Kavcic, M.; Zitnik, M.; Bucar, K.; Mihelic, A.; Carniato, S.; Journel, L.; Guillemin, R.; Simon, M. [Jozef Stefan Institute, Post Office Box 3000, SI-1001 Ljubljana (Slovenia); UPMC Univ Paris 06, UMR 7614, Laboratoire de Chimie Physique Matiere et Rayonnement, F-75005 Paris (France); CNRS, UMR 7614, Laboratoire de Chimie Physique Matiere et Rayonnement, F-75005 Paris (France)

2010-09-10T23:59:59.000Z

335

X?ray Fluorescence (XRF) Assay Using Laser Compton Scattered (LCS) X?rays  

Science Conference Proceedings (OSTI)

Laser Compton Scattered (LCS) X?rays are produced as a result of the interaction between accelerated electrons and a laser beam. The yield of LCS X?rays is dependent on the laser power

Syed F. Naeem; Khalid Chouffani; Douglas P. Wells

2009-01-01T23:59:59.000Z

336

X-ray spectroscopy of neutron star low-mass X-ray binaries  

E-Print Network (OSTI)

In this thesis, I present work spanning a variety of topics relating to neutron star lowmass X-ray binaries (LMXBs) and utilize spectral information from X-ray observations to further our understanding of these sources. ...

Krauss, Miriam Ilana

2007-01-01T23:59:59.000Z

337

X-Ray Multilayer Database from the LBL Center for X-Ray Optics (CXRO)  

DOE Data Explorer (OSTI)

An important activity of the Center for X-ray Optics (CXRO) is research on x-ray mirrors and their use in optical devices to focus and deflect x-ray beams. The two kinds of mirrors most widely used are glancing incidence reflectors and multilayer coatings. The X-Ray Multilayer Database is based on the results of surveys taken at the biennial Physics of X-Ray Multilayer Structures conferences. It contains measured x-ray reflectances reported for various multilayers. The database is provided as a service to the x-ray and multilayer research communities and is intended to reflect the state-of-the-art in multilayer x-ray mirrors. (Specialized Interface)

338

X-ray movies reveal insect flight, muscle motion  

NLE Websites -- All DOE Office Websites (Extended Search)

BioCAT BioCAT X-ray movies reveal insect flight, muscle motion Photo credit: Michael Dickinson Watching flies fly may not seem like high-tech science, but for researchers using the Western Hemisphere's most brilliant X-rays, from the Advanced Photon Source located at the U.S. Department of Energy's Argonne National Laboratory, it not only helps explain how insects fly but also may someday aid in understanding human heart function. The researchers, from the Illinois Institute of Technology (IIT), Caltech and the University of Vermont, merged two distinct technologies, intense X-ray beams and electronic flight simulators, to study how insect muscles can generate such extraordinary levels of power. The results are published in the the January 20,. 2005, issue of the journal Nature.

339

X-ray and Optical Filaments in M87  

E-Print Network (OSTI)

We compare a very deep X-ray image of M87, at the center of the Virgo Cluster, to high-quality optical images of the low excitation emission-line gas in the same region. There are striking coincidences of detail between the two. We explore the possiblity that this represents a thermal interaction between hot gas at 10^7 K and warm gas at 10^4 K. We find two temperatures are present in the X-ray gas, with the lower more prevelant in the vicinity of the optical filaments. Electron conduction from the hot phase to the cooler one provides a quantitatively acceptable energy source for the optical filaments, and we show additionally that it can do so for the brightest X-ray cluster, Perseus. If operative, conduction in the presence of gas-rich galaxy mergers, may explain the presence of "cool cores" in clusters of galaxies.

William B. Sparks; Megan Donahue; Andres Jordan; Laura Ferrarese; Patrick Cote

2004-02-09T23:59:59.000Z

340

Materials Analysis by Soft x-ray Scanning Transmission X-ray ...  

Science Conference Proceedings (OSTI)

About this Abstract. Meeting, Materials Science & Technology 2013. Symposium, Optical and X-ray Imaging Techniques for Material Characterization.

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Bragg x-ray survey spectrometer for ITER  

Science Conference Proceedings (OSTI)

Several potential impurity ions in the ITER plasmas will lead to loss of confined energy through line and continuum emission. For real time monitoring of impurities, a seven channel Bragg x-ray spectrometer (XRCS survey) is considered. This paper presents design and analysis of the spectrometer, including x-ray tracing by the Shadow-XOP code, sensitivity calculations for reference H-mode plasma and neutronics assessment. The XRCS survey performance analysis shows that the ITER measurement requirements of impurity monitoring in 10 ms integration time at the minimum levels for low-Z to high-Z impurity ions can largely be met.

Varshney, S. K.; Jakhar, S. [ITER-India, Institute for Plasma Research, Bhat, Gandhinagar, Gujarat 382428 (India); Barnsley, R. [ITER Organization, Route de Vinon sur Verdon, 13115 Saint Paul Lez Durance (France); O'Mullane, M. G. [Department of Physics, University of Strathclyde, Glasgow G4 0NG (United Kingdom)

2012-10-15T23:59:59.000Z

342

The First Angstrom X-Ray Free-Electron Laser  

SciTech Connect

The Linac Coherent Light Source produced its first x-ray laser beam on 10 April 2009. Today it is routinely producing x-ray pulses with energy >2 mJ across the operating range from 820-8,200 eV. The facility has begun operating for atomic/molecular/optical science experiments. Performance of the facility in its first user run (1 October - 21 December) and current machine development activities will be presented. Early results from the preparations for the start of the second user run is also reported.

Galayda, John; /SLAC

2012-08-24T23:59:59.000Z

343

Soft X-Ray Microscopy at HZB: Zone Plate Development and Imaging Using the Third Order of Diffraction  

Science Conference Proceedings (OSTI)

The Helmholtz-Zentrum Berlin (HZB) operates a transmission x-ray microscope (TXM) in the soft x-ray photon energy range with an energy resolution up to E/{Delta}E = 10{sup 4}. An approach to achieve ultrahigh spatial resolution with conventional, standard zone plate optics is to employ higher orders of diffraction of the zone plate objective. In this paper, we demonstrate that 11-nm lines and spaces of a multilayer test structure are clearly resolved by the x-ray microscope using the third order of diffraction of a zone plate objective with 20-nm outermost zone width. The disadvantage of high-order imaging is an about one order of magnitude lower diffraction efficiency of the used zone plates employed in the third order compared to the first order of diffraction. In addition, the measured background signal in the TXM images is no longer negligible. Therefore, we worked on the fabrication of zone plates with sub-20-nm outermost zone width to increase the spatial resolution in the first order of diffraction. A new high-resolution 100-keV e-beam lithography system from VISTEC, which was recently installed at the Helmholtz-Zentrum Berlin, makes these developments possible. Initial results on zone plates with an outermost zone width down to 15 nm exposed with the new e-beam system are presented. Furthermore, the contrast transfer function of the transmission x-ray microscope operating in partial coherence mode is measured by using the first and third diffraction order of the zone plate objective.

Rehbein, S.; Guttmann, P.; Werner, S.; Schneider, G. [Helmholtz-Zentrum Berlin fuer Materialien und Energie GmbH, Wilhelm-Conrad-Roentgen-Campus, BESSY II, Albert-Einstein-Str. 15, 12489 Berlin (Germany)

2011-09-09T23:59:59.000Z

344

X-Ray Microdiffraction for VLSI  

Science Conference Proceedings (OSTI)

Energy windows, with resolutions Ehkl(2 )/Ehkl(2 )=0.03, were then opened in the multichannel analyzer (MCA), and the scattered intensities Ihkl were...

345

Superconducting Tunnel Junctions X-ray Spectrometer  

The high energy resolution combined with the high count rate capabilities and high quantum efficiency of STJ detectors greatly enhance the sensitivity ...

346

Fresnel zone plates for Achromatic Imaging Survey of X-ray sources  

SciTech Connect

A telescope with Fresnel Zone Plates has been contemplated to be an excellent imaging mask in X-rays and gamma-rays for quite some time. With a proper choice of zone plate material, spacing and an appropriate readout system it is possible to achieve any theoretical angular resolution. We provide the results of numerical simulations of how a large number of X-ray sources could be imaged at a high resolution. We believe that such an imager would be an excellent tool for a future survey mission for X-ray and gamma-ray sources which we propose.

Palit, Sourav [Indian Centre for Space Physics (ICSP), Chalantika 43, Garia Station Rd., Kolkata, 700084 (India); Chakrabarti, S. K. [S. N. Bose National Center for Basic Sciences, JD-Block, Salt Lake, Kolkata, 700098 (India); Debnath, D. [Indian Centre for Space Physics (ICSP), Chalantika 43, Garia Station Road Kolkata 700084 (India); Yadav, Vipin; Nandi, Anuj [Indian Centre for Space Physics (ICSP), Chalantika 43, Garia Station Road Kolkata 700084 (India); On deputation from Indian Space Research Organization HQ, Bangalore 560 231 (India)

2008-10-08T23:59:59.000Z

347

X-ray Image Bank Open for Business - NERSC Center News, Feb 22, 2011  

NLE Websites -- All DOE Office Websites (Extended Search)

X-ray Image Bank Open X-ray Image Bank Open for Business X-ray Image Bank Open for Business February 22, 2011 Filipe Maia is building a data bank where scientists from around the world can deposit and share images generated by coherent x-ray light sources. A post-doctoral researcher with the National Energy Research Scientific Computing Center (NERSC), Maia hopes the Coherent X-ray Imaging Data Bank, or CXIDB (http://www.cxidb.org) can help researchers make the most of their valuable data. Scientists use light sources to shoot intense x-ray beams into molecules, such as proteins, in order to understand their shapes and structures. The resulting diffraction patterns are painstakingly reconstructed to deduce an image. "It kind of works like a microscope, but it has no lens," Maia says.

348

Dispute Resolution Information | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Department of the Navy ADR DOE's Office of Civil Rights and Diversity EEOC Federal Sector Alternative Dispute Resolution EEOC Laws, Regulations & Policy Guidance Federal Energy...

349

Hard X-ray Phase-Contrast Tomographic Nanoimaging  

Science Conference Proceedings (OSTI)

Synchrotron-based full-field tomographic microscopy established itself as a tool for noninvasive investigations. Many beamlines worldwide routinely achieve micrometer spatial resolution while the isotropic 100-nm barrier is reached and trespassed only by few instruments, mainly in the soft x-ray regime. We present an x-ray, full-field microscope with tomographic capabilities operating at 10 keV and with a 3D isotropic resolution of 144 nm recently installed at the TOMCAT beamline of the Swiss Light Source. Custom optical components, including a beam-shaping condenser and phase-shifting dot arrays, were used to obtain an ideal, aperture-matched sample illumination and very sensitive phase-contrast imaging. The instrument has been successfully used for the nondestructive, volumetric investigation of single, unstained cells.

Stampanoni, M. [Paul Scherrer Institut, 5232 Villigen (Switzerland); Institute for Biomedical Engineering, University and ETH Zuerich, 8092 Zuerich (Switzerland); Marone, F.; Vila-Comamala, J.; Gorelick, S.; David, C.; Mokso, R. [Paul Scherrer Institut, 5232 Villigen (Switzerland); Trtik, P.; Jefimovs, K. [EMPA, Swiss Federal Laboratories for Materials Science and Technology, 8600 Duebendorf (Switzerland)

2011-09-09T23:59:59.000Z

350

The MOXE X-ray all-sky monitor for Spectrum-X-Gamma  

SciTech Connect

MOXE is an X-ray all-sky monitor to be flown on the Russian Spectrum-X-Gamma satellite, to be launched in a few years. It will monitor several hundred X-ray sources on a daily basis, and will be the first instrument to monitor most of the X-ray sky most of the time. MOXE will alert users of more sensitive instruments on Russia`s giant high energy astrophysics observatory and of other instruments to transient activity. MOXE consists of an array of 6 X-ray pinhole cameras, sensitive from 3 to 25 keV, which views 4{pi} steradians (except for a 20{degree} {times} 80{degree} patch which includes the Sun). The pinhole apertures of 0.625 {times} 2.556 cm{sup 2} imply an angular resolution of 2{degree}.4 {times} 9{degree}.7 (on-axis). The MOXE hardware program includes an engineering model, now delivered, and a flight model. The flight instrument will mass approximately 118 kg and draw 38 Watts. For a non-focusing all-sky instrument that is limited by sky background, the limiting sensitivity is a function only of detector area. MOXE, with 6,000 cm{sup 2} of detector area, will, for a 24 hrs exposure, have a sensitivity of approximately 2 mCrab. MOXE distinguishes itself with respect to other all-sky monitors in its high duty cycle, thus being particularly sensitive to transient phenomena with time scales between minutes and hours.

In`t Zand, J.J.M.; Priedhorsky, W.C.; Moss, C.E. [and others

1994-08-01T23:59:59.000Z

351

Compact X-ray Light Source Workshop Report  

SciTech Connect

This report, produced jointly by EMSL and FCSD, is the result of a workshop held in September 2011 that examined the utility of a compact x-ray light source (CXLS) in addressing many scientific challenges critical to advancing energy science and technology.

Thevuthasan, Suntharampillai; Evans, James E.; Terminello, Louis J.; Koppenaal, David W.; Manke, Kristin L.; Plata, Charity

2012-12-01T23:59:59.000Z

352

CALIBRATION OF X-RAY IMAGING DEVICES FOR ACCURATE INTENSITY MEASUREMENT  

SciTech Connect

National Security Technologies (NSTec) has developed calibration procedures for X-ray imaging systems. The X-ray sources that are used for calibration are both diode type and diode/fluorescer combinations. Calibrating the X-ray detectors is key to accurate calibration of the X-ray sources. Both energy dispersive detectors and photodiodes measuring total flux were used. We have developed calibration techniques for the detectors using radioactive sources that are traceable to the National Institute of Standards and Technology (NIST). The German synchrotron at Physikalische Technische Bundestalt (PTB) is used to calibrate silicon photodiodes over the energy range from 50 eV to 60 keV. The measurements on X-ray cameras made using the NSTec X-ray sources have included quantum efficiency averaged over all pixels, camera counts per photon per pixel, and response variation across the sensor. The instrumentation required to accomplish the calibrations is described. X-ray energies ranged from 720 eV to 22.7 keV. The X-ray sources produce narrow energy bands, allowing us to determine the properties as a function of X-ray energy. The calibrations were done for several types of imaging devices. There were back illuminated and front illuminated CCD (charge coupled device) sensors, and a CID (charge injection device) type camera. The CCD and CID camera types differ significantly in some of their properties that affect the accuracy of X-ray intensity measurements. All cameras discussed here are silicon based. The measurements of quantum efficiency variation with X-ray energy are compared to models for the sensor structure. Cameras that are not back-thinned are compared to those that are.

Haugh, M J; Charest, M R; Ross, P W; Lee, J J; Schneider, M B; Palmer, N E; Teruya, A T

2012-02-16T23:59:59.000Z

353

Fast synchrotron X-ray tomography study of the rod packing structures  

SciTech Connect

We present a fast synchrotron X-ray tomography study of the packing structures of rods under tapping. Utilizing the high flux of the X-rays generated from the third-generation synchrotron source, we can complete a tomography scan within several seconds, after which the three-dimensional (3D) packing structure can be obtained for the subsequent structural analysis. Due to the high-energy nature of the X-ray beam, special image processing steps including image phase-retrieval has been implemented. Overall, this study suggests the possibility of acquiring statistically significant static packing structures within a reasonable time scale using high-intensity X-ray sources.

Zhang Xiaodan; Xia Chengjie; Sun Haohua; Wang Yujie [Department of Physics, Shanghai Jiao Tong University, 800 Dong Chuan Road, Shanghai 200240 (China)

2013-06-18T23:59:59.000Z

354

Single shot spatial and temporal coherence properties of the SLAC linac coherent light source in the hard x-ray regime  

Science Conference Proceedings (OSTI)

We measured the transverse and longitudinal coherence properties of the Linac Coherent Light Source (LCLS) at SLAC in the hard x-ray regime at 9 keV photon energy on a single shot basis. Speckle patterns recorded in the forward direction from colloidal nanoparticles yielded the transverse coherence properties of the focused LCLS beam. Speckle patterns from a gold nanopowder recorded with atomic resolution allowed us to measure the shot-to-shot variations of the spectral properties of the x-ray beam. The focused beam is in the transverse direction fully coherent with a mode number close to 1. The average number of longitudinal modes behind the Si(111) monochromator is about 14.5 and the average coherence time {tau}{sub c} = (2.0 {+-} 1.0) fs. The data suggest a mean x-ray pulse duration of (29 {+-} 14) fs behind the monochromator for (100 {+-} 14) fs long electron pulses.

Gutt, C.; Wochner, P.; Fischer, B.; Conrad, H.; Castro-Colin, M.; Lee, S.; Lehmkuhler, F.; Steinke, I.; Sprung, M.; Roseker, W.; Zhu, D.; Lemke, H.; Bogle, S.; Fuoss, P. H.; Stephenson, G. B.; Cammarata, M.; Fritz, D. M.; Robert, A.; Grubel, G. (Materials Science Division); (Deutsches Elektronen-Synchrotron); (Max-Planck-Institut fur Intelligene Systeme); (LCLS, SLAC Nat. Accelerator Lab.)

2012-01-01T23:59:59.000Z

355

Design and imaging performance of achromatic diffractive/refractive X-ray and Gamma-ray Fresnel lenses  

E-Print Network (OSTI)

Achromatic combinations of a diffractive Phase Fresnel Lens and a refractive correcting element have been proposed for X-ray and gamma-ray astronomy and for microlithography, but considerations of absorption often dictate that the refractive component be given a stepped profile, resulting in a double Fresnel lens. The imaging performance of corrected Fresnel lenses, with and without `stepping' is investigated and the trade-off between resolution and useful bandwidth in different circumstances is discussed. Provided the focal ratio is large, correction lenses made of low atomic number materials can be used with X-rays in the range approximately 10--100 keV without stepping. The use of stepping extends the possibility of correction to higher aperture systems, to energies as low as a few kilo electron volts and to gamma-rays of $\\sim$ mega electron volt energy.

Gerald K. Skinner

2004-07-21T23:59:59.000Z

356

Five-element Johann-type x-ray emission spectrometer with a single-photon-counting pixel detector  

Science Conference Proceedings (OSTI)

A Johann-type spectrometer with five spherically bent crystals and a pixel detector was constructed for a range of hard x-ray photon-in photon-out synchrotron techniques, covering a Bragg-angle range of 60 deg. - 88 deg. The spectrometer provides a sub emission line width energy resolution from sub-eV to a few eV and precise energy calibration, better than 1.5 eV for the full range of Bragg angles. The use of a pixel detector allows fast and easy optimization of the signal-to-background ratio. A concentration detection limit below 0.4 wt% was reached at the Cu K{alpha}{sub 1} line. The spectrometer is designed as a modular mobile device for easy integration in a multi-purpose hard x-ray synchrotron beamline, such as the SuperXAS beamline at the Swiss Light Source.

Kleymenov, Evgeny; Bokhoven, Jeroen A. van [Paul Scherrer Institut, 5232 Villigen (Switzerland); ETH Zurich, Institute for Chemical and Bioengineering, 8093 Zurich (Switzerland); David, Christian; Janousch, Markus; Studer, Marco; Willimann, Markus; Bergamaschi, Anna; Henrich, Beat; Nachtegaal, Maarten [Paul Scherrer Institut, 5232 Villigen (Switzerland); Glatzel, Pieter [European Synchrotron Radiation Facility, 6 Rue Jules Horowitz, 38043 Grenoble (France); Alonso-Mori, Roberto [SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, California 94025 (United States)

2011-06-15T23:59:59.000Z

357

Imaging nanoscale magnetic structures with polarized soft x-ray photons  

SciTech Connect

Imaging nanoscale magnetic structures and their fast dynamics is scientifically interesting and technologically of highest relevance. The combination of circularly polarized soft X-ray photons which provide a strong X-ray magnetic circular dichroism effect at characteristic X-ray absorption edges, with a high resolution soft X-ray microscope utilizing Fresnel zone plate optics allows to study in a unique way the stochastical behavior in the magnetization reversal process of thin films and the ultrafast dynamics of magnetic vortices and domain walls in confined ferromagnetic structures. Future sources of fsec short and high intense soft X-ray photon pulses hold the promise of magnetic imaging down to fundamental magnetic length and time scales.

Fischer, P.; Im, M.-Y.

2010-01-18T23:59:59.000Z

358

Sure, a textbook can tell you about Bragg's Law and the x-ray absorption energies for any element in the periodic table, but it can't tell you how to plan and carry out an x-ray scattering experiment at one of the 50 or so synchrotron radiation facilitie  

NLE Websites -- All DOE Office Websites (Extended Search)

Report Report SSRL 6 th Annual School on Synchrotron X-ray Scattering Techniques in Materials and Environmental Sciences: Theory and Application SSRL SR-XRS participants. Synchrotron-based X-ray scattering (SR-XRS) techniques offer the ability to probe nano- and atomic-scale structure that dictates the properties of advanced technological and environmental materials. Important materials studied at the Stanford Synchrotron Radiation Lightsource (SSRL) include organic and inorganic thin films and interfaces, nanoparticles, complex oxides, solutions, polymers, minerals and poorly crystalline materials. Good planning and a good working knowledge of beam lines and techniques are required to successfully conduct SR-XRS measurements. This sixth annual School at SSRL on Synchrotron X-ray

359

The soft x-ray instrument for materials studies at the linac coherent light source x-ray free-electron laser  

Science Conference Proceedings (OSTI)

The soft x-ray materials science instrument is the second operational beamline at the linac coherent light source x-ray free electron laser. The instrument operates with a photon energy range of 480-2000 eV and features a grating monochromator as well as bendable refocusing mirrors. A broad range of experimental stations may be installed to study diverse scientific topics such as: ultrafast chemistry, surface science, highly correlated electron systems, matter under extreme conditions, and laboratory astrophysics. Preliminary commissioning results are presented including the first soft x-ray single-shot energy spectrum from a free electron laser.

Schlotter, W. F.; Turner, J. J.; Rowen, M.; Holmes, M.; Messerschmidt, M.; Moeller, S.; Krzywinski, J.; Lee, S.; Coffee, R.; Hays, G. [LCLS, SLAC National Accelerator Laboratory, 2575 Sand Hill Rd., Menlo Park, California 94025 (United States); Heimann, P. [LCLS, SLAC National Accelerator Laboratory, 2575 Sand Hill Rd., Menlo Park, California 94025 (United States); Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Krupin, O. [LCLS, SLAC National Accelerator Laboratory, 2575 Sand Hill Rd., Menlo Park, California 94025 (United States); European XFEL GmbH, Albert-Einstein-Ring 19, 22761 Hamburg (Germany); Soufli, R.; Fernandez-Perea, M.; Hau-Riege, S. [Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, California 94550 (United States); Kelez, N. [Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Beye, M.; Gerken, N.; Sorgenfrei, F.; Wurth, W. [Institute for Experimental Physics and CFEL, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg (Germany); and others

2012-04-15T23:59:59.000Z

360

PMCO: Issue Resolution | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

PMCO: Issue Resolution PMCO: Issue Resolution PMCO: Issue Resolution The expertise available within the Project Management Coordination Office (PMCO) team is regularly called upon to resolve issues that cut across technology offices and require prompt resolution. PMCO prioritizes these actions to ensure they are successfully brought to closure. Examples include: Management of Congressionally Directed Projects (CDPs) and CDP Portfolio Oversight; improving Financial Assistance Closeout performance; and developing and executing the application receipt, review and selection process for 48C tax credit requests. Responsibilities Resolves Office of Energy Efficiency and Renewable Energy (EERE) issues in an efficient and expedited manner Mobilizes small and nimble teams to address specific problem sets

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

APS Bending Magnet X-rays and  

NLE Websites -- All DOE Office Websites (Extended Search)

Irradiation of Nd-Fe-B Permanent Magnets with Irradiation of Nd-Fe-B Permanent Magnets with APS Bending Magnet X-rays and 60 Co γ-rays J. Alderman and P.K. Job APS Operations Division Advanced Photon Source J. Puhl Ionizing Radiation Division National Institute of Standards and Technology June 2000 Table of Contents Introduction Radiation-Induced Demagnetization of Permanent Magnets Resources Required γ-ray Irradiation Results and Analysis of γ-ray Irradiation X-ray Irradiation Results and Analysis of X-ray Irradiation Summary and Conclusions Acknowledgements References Tables and Figures Introduction The Advanced Photon Source (APS), as well as other third-generation synchrotron light sources, uses permanent magnets in the insertion devices to produce x-rays for scientific

362

X-ray image intensifier phosphor  

DOE Patents (OSTI)

Y/sub 1-x/Gd/sub x/.PO$sub 4$:Tb$sup 3+$ is an effective phosphor for use in X-ray intensifier screens and in nuclear radiation detection systems.

D' Silva, A.P.; Fassel, V.A.

1975-12-01T23:59:59.000Z

363

World's First Hard X-ray Laser  

NLE Websites -- All DOE Office Websites (Extended Search)

LCLS is the world's most powerful X-ray laser. Its highly focused beam, which arrives in staccato bursts a few quadrillionths of a second long, allows researchers to probe complex,...

364

X-Ray Nanoimaging: Instruments and Methods  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http:spie.orgOP318 August 28-29, 2013; San Diego, California, USA...

365

X-Ray Scattering Group, Condensed Matter Physics & Materials...  

NLE Websites -- All DOE Office Websites (Extended Search)

- Brookhaven National Laboratory, Upton, NY Beamline X1A2 - Soft x-ray diffraction and nano-imaging Beamline X17 - X-ray powder diffraction Beamline X22C - Resonant x-ray...

366

X-Ray Emission from Compact Sources  

SciTech Connect

This paper presents a review of the physical parameters of neutron stars and black holes that have been derived from X-ray observations. I then explain how these physical parameters can be used to learn about the extreme conditions occurring in regions of strong gravity, and present some recent evidence for relativistic effects seen in these systems. A glossary of commonly used terms and a short tutorial on the names of X-ray sources are also included.

Cominsky, L

2004-03-23T23:59:59.000Z

367

Soft x-ray diagnostics for pulsed power machines  

SciTech Connect

A variety of soft x-ray diagnostics are being fielded on the Los Alamos National Laboratory Pegasus and Procyon pulsed power systems and also being fielded on joint US/Russian magnetized target fusion experiments known as MAGO (Magnitoye Obzhatiye). The authors have designed a low-cost modular photoemissive detector designated the XRD-96 that uses commercial 1100 series aluminum for the photocathode. In addition to photocathode detectors a number of designs using solid state silicon photodiodes have been designed and fielded. They also present a soft x-ray time-integrated pinhole camera system that uses standard type TMAX-400 photographic film that obviates the need for expensive and no longer produced zero-overcoat soft x-ray emulsion film. In a typical experiment the desired spectral energy cuts, signal intensity levels, and desired field of view will determine diagnostic geometry and x-ray filters selected. The authors have developed several computer codes to assist in the diagnostic design process and data deconvolution. Examples of the diagnostic design process and data analysis for a typical pulsed power experiment are presented.

Idzorek, G.C.; Coulter, W.L.; Walsh, P.J.; Montoya, R.R.

1995-08-01T23:59:59.000Z

368

Optimal focusing for a linac-based hard x-ray source  

Science Conference Proceedings (OSTI)

In spite of having a small average beam current limit, a linac can have features that make it attractive as an x-ray source: high energy, ultralow emittance and energy spread, and flexible beamline optics. Unlike a storage ring, in which an (undulator) radiation source is necessarily short and positioned at an electron beam waist, in a linac the undulator can be long and the electron beam can be adjusted to have a (virtual) waist far downstream toward the x-ray target. Using a planned CEBAF beamline as an example, this paper shows that a factor of 2000 in beam current can be overcome to produce a monochromatic hard x-ray source comparable with, or even exceeding, the performance of an x-ray line at a third generation storage ring. Optimal electron beam focusing conditions for x-ray flux density and brilliance are derived, and are verified by simulations using the SRW code.

Liu, C.; Krafft, G.; Talman, R.

2011-03-28T23:59:59.000Z

369

Imaging of lateral spin valves with soft x-ray microscopy  

SciTech Connect

We investigated Co/Cu lateral spin valves by means of high-resolution transmission soft x-ray microscopy with magnetic contrast that utilizes x-ray magnetic circular dichroism (XMCD). No magnetic XMCD contrast was observed at the Cu L{sub 3} absorption edge, which should directly image the spin accumulation in Cu. Although electrical transport measurements in a non-local geometry clearly detected the spin accumulation in Cu, which remained unchanged during illumination with circular polarized x-rays at the Co and Cu L{sub 3} absorption edges.

Mosendz, O.; Mihajlovic, G.; Pearson, J. E.; Fischer, P.; Im, M.-Y.; Bader, S. D.; Hoffmann, A.

2009-05-01T23:59:59.000Z

370

The Gated X-ray Detector for the National Ignition Facility  

Science Conference Proceedings (OSTI)

Two new gated x-ray imaging cameras have recently been designed, constructed and delivered to the National Ignition Facility in Livermore, CA. These Gated X-ray Detectors are each designed to fit within an aluminum airbox with a large capacity cooling plane and are fitted with an array of environmental housekeeping sensors. These instruments are significant different from earlier generations of gated x-ray images due in parts to an innovative impendence matching scheme, advanced phosphor screens, pulsed phosphor circuits, precision assembly fixturing, unique system monitoring and complete remote computer control. Preliminary characterization has shown repeatable uniformity between imaging strips, improved spatial resolution and no detectable impendence reflections.

Oertel, J A; Barnes, C; Archuleta, T; Casper, L; Fatherley, V; Heinrichs, T; King, R; Landers, D; Lopez, F; Sanchez, P; Sandoval, G; Schrank, L; Walsh, P; Bell, P; Brown, M; Costa, R; Holder, J; Montalongo, S; Pederson, N

2006-05-18T23:59:59.000Z

371

An X-ray Reprocessing Model of Disk Thermal Emission in Type 1 Seyfert Galaxies  

E-Print Network (OSTI)

Using a geometry consisting of a hot central Comptonizing plasma surrounded by a thin accretion disk, we model the optical through hard X-ray spectral energy distributions of the type 1 Seyfert galaxies NGC 3516 and NGC 7469. As in the model proposed by Poutanen, Krolik, & Ryde for the X-ray binary Cygnus X-1 and later applied to Seyfert galaxies by Zdziarski, Lubi\\'nski, & Smith, feedback between the radiation reprocessed by the disk and the thermal Comptonization emission from the hot central plasma plays a pivotal role in determining the X-ray spectrum, and as we show, the optical and ultraviolet spectra as well. Seemingly uncorrelated optical/UV and X-ray light curves, similar to those which have been observed from these objects can be explained by variations in the size, shape, and temperature of the Comptonizing plasma. Furthermore, by positing a disk mass accretion rate which satisfies a condition for global energy balance between the thermal Comptonization luminosity and the power available from accretion, one can predict the spectral properties of the hard X-ray continuum above $\\sim 50$ keV in type 1 Seyfert galaxies. Forthcoming measurements of the hard X-ray continuum by more sensitive hard X-ray and soft $\\gamma$-ray telescopes, in conjunction with simultaneous optical, UV, and soft X-ray monitoring, will allow the mass accretion rates to be directly constrained for these sources in the context of this model.

James Chiang

2002-02-12T23:59:59.000Z

372

Inelastic X-ray and Nuclear Resonant Scattering  

NLE Websites -- All DOE Office Websites (Extended Search)

Beamlines Divisions Argonne Home > Advanced Photon Source > Inelastic X-ray and Nuclear Resonant Scattering The Inelastic X-ray and Nuclear Resonant Scattering group...

373

Transient x-ray diffraction and its application to materials science and x-ray optics  

SciTech Connect

Time resolved x-ray diffraction and scattering have been applied to the measurement of a wide variety of physical phenomena from chemical reactions to shock wave physics. Interest in this method has heightened in recent years with the advent of versatile, high power, pulsed x-ray sources utilizing laser plasmas, electron beams and other methods. In this article, we will describe some of the fundamentals involved in time resolved x-ray diffraction, review some of the history of its development, and describe some recent progress in the field. In this article we will emphasize the use of laser-plasmas as the x-ray source for transient diffraction.

Hauer, A.A.; Kopp, R.; Cobble, J.; Kyrala, G.; Springer, R. [and others

1997-12-01T23:59:59.000Z

374

Kinematics of Compton backscattering x-ray source for angiography  

SciTech Connect

Calculations of X-Ray production rates, energy spread, and spectrum of Compton-backscattered photons from a Free Electron Laser on an electron beam in a low energy (136-MeV) compact (8.5-m circumference) storage ring indicate that an X-Ray intensity of 34.6 10{sup 7} X-Ray photons per 0.5-mm {times} 0.5-mm pixel for Coronary Angiography near the 33.169-keV iodine K-absorption edge can be achieved in a 4-msec pulse within a scattering cone of 1-mrad half angle. This intensity, at 10-m from the photon-electron interaction point to the patient is about a factor of 10 larger than presently achieved from a 4.5-T superconducting wiggler source in the NSLS 2.5-GeV storage ring and over an area about 5 times larger. The 2.2-keV energy spread of the Compton-backscattered beam is, however, much larger than the 70-eV spread presently attained form the wiggler source and use of a monochromator. The beam spot at the 10-m interaction point-to-patient distance is 20-mm diameter; larger spots are attainable at larger distances but with a corresponding reduction in X-Ray flux. Such a facility could be an inexpensive clinical alternative to present methods of non-invasive Digital Subtraction Angiography (DSA), small enough to be deployed in an urban medical center, and could have other medical, industrial and aerospace applications. Problems with the Compton backscattering source include laser beam heating of the mirror in the FEL oscillator optical cavity, achieving a large enough X-Ray beam spot at the patient, and obtaining radiation damping of the transverse oscillations and longitudinal emittance dilution of the storage ring electron beam resulting from photon-electron collisions without going to higher electron energy where the X-Ray energy spread becomes excessive for DSA. 38 refs.

Blumberg, L.N.

1992-05-01T23:59:59.000Z

375

Scanning transmission x-ray microscopy: A new ``looking glass`` into coal chemical structure  

SciTech Connect

This paper reports the use of scanning transmission x-ray microscopy to spatially map the chemistry of aromatic and aliphatic carbon functionalities in coal to a resolution of less than 0.1 {mu}m. Localized x-ray absorption spectroscopy recorded at the carbon K absorption edge was also used to facilitate analysis of variations in fundamental chemistry at maceral interfaces and within maceral boundaries.

Botto, R.E.; Cody, G.D.

1994-02-01T23:59:59.000Z

376

X-ray Diffraction Crystal Calibration and Characterization  

SciTech Connect

National Security Technologies X-ray Laboratory is comprised of a multi-anode Manson type source and a Henke type source that incorporates a dual goniometer and XYZ translation stage. The first goniometer is used to isolate a particular spectral band. The Manson operates up to 10 kV and the Henke up to 20 kV. The Henke rotation stages and translation stages are automated. Procedures have been developed to characterize and calibrate various NIF diagnostics and their components. The diagnostics include X-ray cameras, gated imagers, streak cameras, and other X-ray imaging systems. Components that have been analyzed include filters, filter arrays, grazing incidence mirrors, and various crystals, both flat and curved. Recent efforts on the Henke system are aimed at characterizing and calibrating imaging crystals and curved crystals used as the major component of an X-ray spectrometer. The presentation will concentrate on these results. The work has been done at energies ranging from 3 keV to 16 keV. The major goal was to evaluate the performance quality of the crystal for its intended application. For the imaging crystals we measured the laser beam reflection offset from the X-ray beam and the reflectivity curves. For the curved spectrometer crystal, which was a natural crystal, resolving power was critical. It was first necessary to find sources of crystals that had sufficiently narrow reflectivity curves. It was then necessary to determine which crystals retained their resolving power after being thinned and glued to a curved substrate.

Michael J. Haugh; Richard Stewart; Nathan Kugland

2009-06-05T23:59:59.000Z

377

The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into  

NLE Websites -- All DOE Office Websites (Extended Search)

The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into Focus Print The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into Focus Print Studying the world of the ultrasmall and the ultrafast is at the frontier of scientific research. Two x-ray approaches can be used for ultrafast examinations. The first entails developing sources that have short x-ray pulses such as free-electron lasers and slicing sources, which will provide the ultrafast temporal information. The other approach is to develop a detector that is fast enough to resolve the ultrafast details of the dynamical processes. ALS researchers are taking the second path but adding a spatial resolution capability; that is, they are developing a high-speed x-ray streak camera with high spatial resolution to watch, in real time, the motion of the atoms in materials. So far, a temporal resolution of 233 fs and a spatial resolution of 10 mm have been demonstrated. This is the first time that such a high temporal resolution has been combined with high spatial resolution in a streak camera.

378

The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into  

NLE Websites -- All DOE Office Websites (Extended Search)

The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into Focus Print The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into Focus Print Studying the world of the ultrasmall and the ultrafast is at the frontier of scientific research. Two x-ray approaches can be used for ultrafast examinations. The first entails developing sources that have short x-ray pulses such as free-electron lasers and slicing sources, which will provide the ultrafast temporal information. The other approach is to develop a detector that is fast enough to resolve the ultrafast details of the dynamical processes. ALS researchers are taking the second path but adding a spatial resolution capability; that is, they are developing a high-speed x-ray streak camera with high spatial resolution to watch, in real time, the motion of the atoms in materials. So far, a temporal resolution of 233 fs and a spatial resolution of 10 mm have been demonstrated. This is the first time that such a high temporal resolution has been combined with high spatial resolution in a streak camera.

379

The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into  

NLE Websites -- All DOE Office Websites (Extended Search)

The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into Focus Print The ALS X-Ray Streak Camera: Bringing the Ultrafast and Ultrasmall into Focus Print Studying the world of the ultrasmall and the ultrafast is at the frontier of scientific research. Two x-ray approaches can be used for ultrafast examinations. The first entails developing sources that have short x-ray pulses such as free-electron lasers and slicing sources, which will provide the ultrafast temporal information. The other approach is to develop a detector that is fast enough to resolve the ultrafast details of the dynamical processes. ALS researchers are taking the second path but adding a spatial resolution capability; that is, they are developing a high-speed x-ray streak camera with high spatial resolution to watch, in real time, the motion of the atoms in materials. So far, a temporal resolution of 233 fs and a spatial resolution of 10 mm have been demonstrated. This is the first time that such a high temporal resolution has been combined with high spatial resolution in a streak camera.

380

Nuclear transitions induced by synchrotron x-rays.  

DOE Green Energy (OSTI)

We discuss two rare but interesting processes by which synchrotron x-rays with energies up to about 100 keV may be used to induce nuclear transitions. In the NEET (Nuclear Excitation by Electronic Transition) process, an intense x-ray beam is employed to make vacancies, e.g. K-holes, in the atoms of a specific nuclear isotope. When a vacancy is filled by an electronic transition from a higher atomic level, there is some probability that instead of the usual x-ray or Auger emission, the nucleus of the atom itself will be excited. This is then followed by a nuclear decay exhibiting characteristic gamma-rays or other types of radiation, with time delays typical of the nuclear states involved. The probability for NEET increases when the energies of the atomic and the nuclear transitions become close. We address some theoretical aspects of the process and describe experimental efforts to observe it in {sup 189}Os and {sup 197}Au. The second process to be discussed is the possibility of ''triggering'' the decay of a nuclear isomer by irradiation with an x-ray beam. We focus on the case of the 31-year, 2.4-MeV, 16+ isomer of {sup 178}Hf. There has been speculation that if one could isolate gram quantities, say, of this isomer and then have the capability to accelerate its decay in a controlled way, one would have a powerful triggerable source of enormous energy. This could be used to generate explosions, for rapid irradiations, or for more general energy-storage applications, depending on the rate of energy release. We describe attempts to observe this process.

Gemmell, D. S.

2002-06-05T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

Fiber fed x-ray/gamma ray imaging apparatus  

SciTech Connect

X-ray/gamma ray imaging apparatus is disclosed for detecting the position, energy, and intensity of x-ray/gamma ray radiation comprising scintillation means disposed in the path of such radiation and capable of generating photons in response to such radiation; first photodetection means optically bonded to the scintillation means and capable of generating an electrical signal indicative of the intensity, and energy of the radiation detected by the scintillation means; second photodetection means capable of generating an electrical signal indicative of the position of the radiation in the radiation pattern; and means for optically coupling the scintillation means to the second photodetection means. The photodetection means are electrically connected to control and storage means which may also be used to screen out noise by rejecting a signal from one photodetection means not synchronized to a signal from the other photodetection means; and also to screen out signals from scattered radiation.

Hailey, Charles J. (San Francisco, CA); Ziock, Klaus-Peter (Livermore, CA)

1992-01-01T23:59:59.000Z

382

Development and characterization of a novel compact x-ray source  

E-Print Network (OSTI)

For elemental analysis, x-ray fluorescence spectroscopy (XRF) is a rapid and simple method of analysis, which provides both quantitative and qualitative information. In general, most XRF instruments are not suited for use as portable field instruments. Most commercial XRF spectrometers require cooling units for the anode, large power supplies and, in some cases, liquid nitrogen to cool the x-ray detectors. Alternative x-ray sources using radioactive isotopes have been considered for portable XRF, but safety regulations and public concerns have hampered their usage. An x-ray source has been developed which uses a solid state electron multiplier to enhance the electron gain from a simple filament. The overall gain from the electron multiplier is sufficient to generate x-rays. However, the novel source produces less heating of the anode, eliminating the cooling unit requirement. This feature along with the small size of the electron multiplier, allows for a compact design, which lends itself to portability. An additional feature is that the power consumption of the system is lower than a typical xray tube system. Initial studies have shown that the system behaves similar to a conventional x-ray tube. Increasing anode voltage (electron energy) causes improved yield of the higher energy x-rays. Also, increasing the electron multiplier voltage (electron intensity) increases overall intensity of the x-ray output. Using the new source for XRF studies, the limits of detection were comparable with values reported in the literature. It was necessary, however, to prepare the samples using single elements to reduce matrix affects and lessen effects of overlapping peaks. In general the x-ray source shows potential as a portable x-ray source that may be used in the field.

Woo, Ronald Yut

1996-01-01T23:59:59.000Z

383

ON THE TRUE SHAPE OF X-RAY SPECTRA  

SciTech Connect

A method for obtaining the true shape of x-ray spectra was developed for the particular case of dispersive distortions. The method is of value in the correction of the shape of the spectrum for the distortion introduced by the outside level of the atom and in showing the correct shape of the energy dependence of the density of states n(E)p(E) where p(E) is the probability of the corresponding transition. (J.S.R.)

Blokhin, M.A.

1956-03-01T23:59:59.000Z

384

X-ray Flares in Orion Low Mass Stars  

E-Print Network (OSTI)

Context. X-ray flares are common phenomena in pre-main sequence stars. Their analysis gives insights into the physics at work in young stellar coronae. The Orion Nebula Cluster offers a unique opportunity to study large samples of young low mass stars. This work is part of the Chandra Orion Ultradeep project (COUP), an ~10 day long X-ray observation of the Orion Nebula Cluster (ONC). Aims. Our main goal is to statistically characterize the flare-like variability of 165 low mass (0.1-0.3 M_sun) ONC members in order to test and constrain the physical scenario in which flares explain all the observed emission. Methods. We adopt a maximum likelihood piece-wise representation of the observed X-ray light curves and detect flares by taking into account both the amplitude and time derivative of the count-rate. We then derive the frequency and energy distribution of the flares. Results. The high energy tail of the energy distribution of flares is well described by a power-law with index 2.2. We test the hypothesis that light curves are built entirely by overlapping flares with a single power law energy distribution. We constrain the parameters of this simple model for every single light curve. The analysis of synthetic light curves obtained from the model indicates a good agreement with the observed data. Comparing low mass stars with stars in the mass interval (0.9-1.2M_sun), we establish that, at ~1 Myr, low mass and solar mass stars of similar X-ray luminosity have very similar flare frequencies. Conclusions. Our observational results are consistent with the following model/scenario: the light curves are entirely built by over- lapping flares with a power-law intensity distribution; the intense flares are individually detected, while the weak ones merge and form a pseudo-quiescent level, which we indicate as the characteristic level.

M. Caramazza; E. Flaccomio; G. Micela; F. Reale; S. J. Wolk; E. D. Feigelson

2007-06-11T23:59:59.000Z

385

X-Ray Data from the X-Ray Data Booklet Online  

DOE Data Explorer (OSTI)

The original X-Ray Data Booklet, published in 1985, became a classic reference source. The online version has been significantly revised and updated to reflect today's science. Hundreds of pages of authoritative data provide the x-ray properties of elements, information on synchrotron radiation, scattering processes, optics and detectors, and other related calculations, formulas, and data tables.

Thompson, Albert C.; Attwood, David T.; Gullikson, Eric M.; Howells, Malcolm R.; Kortright, Jeffrey B.; Robinson, Arthur L.; Underwood, James H.; Kim, Kwang-Je; Kirz, Janos; Lindau, Ingolf; Pianetta, Piero; Winick, Herman; Williams, Gwyn P.; Scofield, James H.

386

Frontiers in X-Ray Science  

Science Conference Proceedings (OSTI)

The year 2010 marked the fiftieth anniversary of the optical laser and the first anniversary of the world's first hard x-ray free-electron laser, the Linac Coherent Light Source (LCLS) at SLAC. This exciting, new accelerator-based source of x-rays provides peak brilliances roughly a billion times greater than currently available from synchrotron sources such as the Advanced Photon Source at Argonne, and thus explores a qualitatively different parameter space. This talk will describe the first experiments at the LCLS aimed at understanding the nature of high intensity x-ray interactions, related applications in ultrafast imaging on the atomic scale and sketch nascent plans for the extension of both linac and storage-ring based photon sources.

Linda Young

2011-02-23T23:59:59.000Z

387

Absolute, soft x-ray calorimetry on the Z facility at Sandia National Laboratories  

SciTech Connect

Simple and reliable x-ray fluence measurements, in addition to time-resolved diagnostics, are needed to understand the physics of hot Z-pinch plasmas. A commercially available laser calorimeter has been modified for measuring soft x-ray fluence from the Z facility at Sandia National Laboratories. The x-ray absorber of this calorimeter is an aluminum disk, attached to a two-dimensional thermopile and surrounded by an isoperibol shroud. The time-integral and the maximum of the thermopile voltage signal are both proportional to the x-ray energy deposited. Data are collected for 90 seconds, and the instrument has, thus far, been used in the 1--25 mJ range. A wider dynamic measuring range for x-ray fluence (energy/area) can be achieved by varying the area of the defining aperture. The calorimeter is calibrated by an electrical substitution method. Calibrations are performed before and after each x-ray experiment on the Z facility. The calibration of the time-integral of the thermopile voltage vs. energy deposited (or the peak of thermopile voltage vs. energy deposited) is linear with zero offset at the 95% confidence level. The irreproducibility of the calibration is <2%, and the imprecision in the measurement of the incident x-ray energy (inferred from signal noise and the calibration) is estimated to be {approximately}0.9 mJ (95% confidence level). The inaccuracy is estimated at {+-}10%, due to correctable systematic errors (e.g., baseline shifts). Comparisons have been made of the calorimeter to time-resolved x-ray diagnostics, e.g., bolometers and XRD (x-ray diode) arrays, by integrating the flux measured by these instruments over time.

Fehl, D.L.; Muron, D.J.; Leeper, R.J.; Chandler, G.A.; Deeney, C.; Spielman, R.B.

1998-05-01T23:59:59.000Z

388

Radiobiological studies using gamma and x rays.  

Science Conference Proceedings (OSTI)

There are approximately 500 self-shielded research irradiators used in various facilities throughout the U.S. These facilities use radioactive sources containing either 137Cs or 60Co for a variety of biological investigations. A report from the National Academy of Sciences[1] described the issues with security of particular radiation sources and the desire for their replacement. The participants in this effort prepared two peer-reviewed publications to document the results of radiobiological studies performed using photons from 320-kV x rays and 137Cs on cell cultures and mice. The effectiveness of X rays was shown to vary with cell type.

Potter, Charles Augustus; Longley, Susan W.; Scott, Bobby R. [Lovelace Respiratory Research Institute, Albuquerque, NM; Lin, Yong [Lovelace Respiratory Research Institute, Albuquerque, NM; Wilder, Julie [Lovelace Respiratory Research Institute, Albuquerque, NM; Hutt, Julie A. [Lovelace Respiratory Research Institute, Albuquerque, NM; Padilla, Mabel T. [Lovelace Respiratory Research Institute, Albuquerque, NM; Gott, Katherine M. [Lovelace Respiratory Research Institute, Albuquerque, NM

2013-02-01T23:59:59.000Z

389

X-ray Science Division: Groups  

NLE Websites -- All DOE Office Websites (Extended Search)

Division: Groups Division: Groups Atomic, Molecular and Optical Physics (AMO) Primary Contact: Stephen Southworth Work focuses on understanding how strong optical and x-ray fields interact with matter, with an emphasis on photonic control of electronic, atomic and molecular motion. Chemical and Materials Science (CMS) Primary Contact: Randy Winans Research Disciplines: Chemistry, Materials Science Detectors (DET) Primary Contact: Antonino Miceli GMCA Structural Biology Facility (MX) Primary Contact: Robert Fischetti Research Disciplines: Biology, Life Sciences Imaging (IMG) Primary Contact: Francesco DeCarlo Research Disciplines: Materials Science, Biology, Physics, Life Sciences Inelastic X-ray & Nuclear Resonant Scattering (IXN) Primary Contact: Thomas Gog Research Disciplines: Condensed Matter Physics, Geophysics, Materials

390

Conflict Resolution Day | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Conflict Resolution Day Conflict Resolution Day Conflict Resolution Day October 18, 2012 10:00AM EDT All events in the Department of Energy's Forrestal Main Auditorium, Germantown employees can watch a VTC broadcast in Germantown A-117 and Cloverleaf 2071. Conflict Resolution Day takes a look at mediation, conciliation, negotiation, arbitration, the ombudsman, and facilitation to resolve conflict in the workplace. Employees and contractors are invited to join for any/all of the following events: 10:00am - 10:30am Cookies, Coffee, and Conversation 10:30am - 11:30am Self-Mediation presentation 11:30am - 12:00pm De-Stressing in a Stressful Environment presentation 12:00pm - 1:00pm Informal Information Session 1:00pm - 2:00pm Ergonomics IL Creations Forrestal Cafetaria will be offering a Conflict Resolution Day

391

X-ray Variability in M87 1992-1998  

E-Print Network (OSTI)

Beginning in 1995 June, we have obtained an observation of M87 with the ROSAT High Resolution Imager (HRI) every 6 months. We present the measurements of X-ray intensity for the core and knot A through 1998 January. We find significant changes in both components. For the core, intensities measured in 95 Jun, 96 Dec, and 97 Dec are roughly 30% higher than values obtained at three intervening times. For knot A, a secular decrease of approximately 15% is interrupted only by an intensity jump (3 sigma) in 1997 Dec. Because the background used for subtraction is probably underestimated, we suspect the actual variation is somewhat greater than these values indicate.

Harris, D E; Junor, W

1998-01-01T23:59:59.000Z

392

12.141 Electron Microprobe Analysis by Wavelength Dispersive X-ray Spectrometry, January (IAP) 2006  

E-Print Network (OSTI)

Introduction to the theory of x-ray microanalysis through the electron microprobe including ZAF matrix corrections. Techniques to be discussed are wavelength and energy dispersive spectrometry, scanning backscattered ...

Chatterjee, Nilanjan

393

Sub-Picosecond X-Ray Pulses Workshop  

NLE Websites -- All DOE Office Websites (Extended Search)

International Workshop on the Interactions of Intense Sub-Picosecond X-Ray International Workshop on the Interactions of Intense Sub-Picosecond X-Ray Pulses with Matter (SLAC, January 23-24, 1997) During the last five years studies have been conducted at the Stanford Linear Accelerator Center (SLAC) and the Deutsches Elektronen-Synchrotron (DESY) in Hamburg concerning the feasibility of driving an Angstrom-wavelength Free-Electron Laser (FEL) with a high energy rf linac. Recent promising advances in linac, rf gun, and insertion device technologies make it seem likely that such a device can be constructed. The output radiation predicted for this type of source will be characterized by full transverse coherence, extreme pulse brevity (~50-100 fs), high peak power (10-100 GW), and very high unfocused peak power density (0.4-4.1013

394

LCLS - The X-ray Laser Has Turned On  

SciTech Connect

On April 10, 2009 the Linac Coherent Light Source (LCLS), the world's first hard x-ray free electron laser, was brought to lasing. Producing an x-ray beam with over a billion times higher peak brightness that then most powerful existing syncrotron sources, it marked the beginning of a new era of science. The LCLS pulses arrive at a rate of 60 - 120 Hz in an energy range from 480 eV to 10 keV, with pulse lengths as short as a few fs to about 300 fs. Since October 2009, users have been performing experiments at the LCLS, and currently three of the six planned instruments are available. Although we stand only at the beginning of LCLS science, there is no doubt about the strong sense of early excitement.

Bergmann, Uwe [Linac Coherent Light Source

2010-11-03T23:59:59.000Z

395

An X-ray Polarimeter for Constellation-X  

E-Print Network (OSTI)

Polarimetry remains a largely unexploited technique in observational X-ray astronomy which could provide insight in the study of the strong gravity and magnetic fields at the core of the Constellation-X observational program. Adding a polarization capability to the Constellation-X instrumentation would be immensely powerful. It would make Constellation the first space observatory to simultaneously measure all astrophysically relevant parameters of source X-ray photons; their position (imaging), energy (spectroscopy), arrival time (timing), and polarization. Astrophysical polarimetry requires sensitive well-calibrated instruments. Many exciting objects are extra-galactic (i.e. faint) and may have small polarization. Recent advances in efficiency and bandpass make it attractive to consider a polarimetry Science Enhancement Package for the Constellation-X mission.

K. Jahoda; K. Black; P. Deines-Jones; J. E. Hill; T. Kallman; T. Strohmayer; J. H. Swank

2007-01-04T23:59:59.000Z

396

X-ray tomography of preserved samples from The Geysers scientific corehole  

DOE Green Energy (OSTI)

Approximately 800 ft. of continuous core was recovered from borehole SB-15 D (on unit 15, near the site of the abandoned Geysers Resort) during a recently completed drilling operation funded by the USDOE. Sections of this core were collected at 50 ft intervals for subsequent examination as drilling proceeded. Five foot sections were not removed at the drill site, but were sealed in the innermost sleeve of a triple tube coring system to minimize drying and disturbance of the core. All cores remained sealed and were radiographed within 72 hours of drilling: the five foot core from near 1400 ft. was scanned within 18 hours of drilling. A third generation x-ray scanner, which uses high energy radiation to penetrate the aluminum sleeve and 3.5 inch cores, was used to make preliminary radiographs and to collect multiple views of the sample as the core is rotated in front of the beam. True three dimensional tomographs are then reconstructed from the data. At present, the images have a spatial resolution of approximately 140 micrometers and can resolve contrast differences of 0.2%. The tomographs clearly show differences in lithology with depth in the reservoir. Partially filled fractures, vein selvage and vuggy porosity are all evident in parts of the core. A principle goal of the imaging effort is to help determine the fluid content of the reservoir. Important questions to investigate include water loss during core recovery, infiltration of drilling fluid, and the heterogeneous distribution of pore fluid. Images show that radial gradients in x-ray attenuation commonly occur in jacketed cores. Regions of excess attenuation extend about halfway into the 3.5 in. core, and are probably caused by mud invasion induced by capillarity of the small scale porosity of the graywacke matrix. X-ray measurements will be coordinated with other independent measurements of fluid content underway in separate studies, particularly NMR spectroscopy of frozen ''pressure core'', and compressional velocity and electrical resistivity measurements.

Bonner, B.P.; Roberts, J.J.; Schneberk, D.J.; Marsh, A.; Ruddle, C.; Updike, E.

1995-01-26T23:59:59.000Z

397

3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone at the  

NLE Websites -- All DOE Office Websites (Extended Search)

3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone 3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone at the Nanoscale Scientists studying osteoporosis and other skeletal diseases are interested in the 3D structure of bone and its responses to conditions such as weightlessness, radiation (of particular interest to astronauts) and vitamin D deficiency. The current gold standard, micro-computed tomography (micro-CT), provides 3D images of trabeculae, the small interior struts of bone tissue, and electron microscopy can provide nanometer resolution of thin tissue slices. Hard X-ray transmission microscopy has provided the first 3D view of bone structure within individual trabeculae on the nanoscale. figure 1 Figure 1 Micro-CT (left) shows trabecular structure inside of bone. Transmission X-ray microscopy (TXM; center and right) can reveal localized details of osteocyte lacunae and their processes.

398

Probing Material Reactivity Using X-ray Pair Distribution Function Methods  

NLE Websites -- All DOE Office Websites (Extended Search)

Material Reactivity Using X-ray Pair Distribution Material Reactivity Using X-ray Pair Distribution Function Methods Karena W. Chapman X-ray Science Division, Advanced Photon Source, Argonne National Laboratory, Argonne, IL 60439, USA Understanding how advanced functional materials react and transform, at an atomic scale, is a characterization challenge with many diverse phenomena possible; components with varying particle size, morphology, and microstructure can evolve from multi-atom clusters to multi-million atom crystals. The pair distribution function (PDF) method shows great promise for providing quantitative insight such reactions. Recent advances in experimental methods, have improved the efficiency of X-ray PDF measurements, to allow time-resolved experiments with sufficient resolution to study reactions in solid

399

Advanced experimental applications for x-ray transmission gratings spectroscopy using a novel grating fabrication method  

Science Conference Proceedings (OSTI)

A novel fabrication method for soft x-ray transmission grating and other optical elements is presented. The method uses focused-ion-beam technology to fabricate high-quality free standing grating bars on transmission electron microscopy grids. High quality transmission gratings are obtained with superb accuracy and versatility. Using these gratings and back-illuminated CCD camera, absolutely calibrated x-ray spectra can be acquired for soft x-ray source diagnostics in the 100-3000 eV spectral range. Double grating combinations of identical or different parameters are easily fabricated, allowing advanced one-shot application of transmission grating spectroscopy. These applications include spectroscopy with different spectral resolutions, bandwidths, dynamic ranges, and may serve for identification of high-order contribution, and spectral calibrations of various x-ray optical elements.

Hurvitz, G.; Ehrlich, Y.; Shpilman, Z.; Levy, I.; Fraenkel, M. [Plasma Physics Department, Applied Physics Division, Soreq NRC, Yavne (Israel); Strum, G. [Solid State Department, Applied Physics Division, Soreq NRC, Yavne (Israel)

2012-08-15T23:59:59.000Z

400

A carbon nanotube field emission multipixel x-ray array source for microradiotherapy application  

Science Conference Proceedings (OSTI)

The authors report a carbon nanotube (CNT) field emission multipixel x-ray array source for microradiotherapy for cancer research. The developed multipixel x-ray array source has 50 individually controllable pixels and it has several distinct advantages over other irradiation source including high-temporal resolution (millisecond level), the ability to electronically shape the form, and intensity distribution of the radiation fields. The x-ray array was generated by a CNT cathode array (5x10) chip with electron field emission. A dose rate on the order of >1.2 Gy/min per x-ray pixel beam is achieved at the center of the irradiated volume. The measured dose rate is in good agreement with the Monte Carlo simulation result.

Wang Sigen [Department of Radiation Oncology, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Department of Physics and Astronomy, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Calderon, Xiomara; Peng Rui [Curriculum of Applied and Materials Sciences, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Schreiber, Eric C. [Department of Radiation Oncology, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Zhou, Otto [Department of Physics and Astronomy, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Curriculum of Applied and Materials Sciences, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Lineberger Comprehensive Cancer Center, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Chang, Sha [Department of Radiation Oncology, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Department of Physics and Astronomy, University of North Carolina at Chapel Hill, North Carolina 27599 (United States); Lineberger Comprehensive Cancer Center, University of North Carolina at Chapel Hill, North Carolina 27599 (United States)

2011-05-23T23:59:59.000Z

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401

Molecular orientation in soft matter thin films studied by resonant soft X-ray reflectivity  

SciTech Connect

We present a technique to study depth profiles of molecular orientation in soft matter thin films with nanometer resolution. The method is based on dichroism in resonant soft X-ray reflectivity using linear s- and p-polarization. It combines the chemical sensitivity of Near-Edge X-ray Absorption Fine Structure spectroscopy to specific molecular bonds and their orientation relative to the polarization of the incident beam with the precise depth profiling capability of X-ray reflectivity. We demonstrate these capabilities on side chain liquid crystalline polymer thin films with soft X-ray reflectivity data at the carbon K edge. Optical constants of the anisotropic refractive index ellipsoid were obtained from a quantitative analysis using the Berreman formalism. For films up to 50 nm thickness we find that the degree of orientation of the long axis exhibits no depth variation and isindependent of the film thickness.

Mezger, Markus; Jerome, Blandine; Kortright, Jeffrey B.; Valvidares, Manuel; Gullikson, Eric; Giglia, Angelo; Mahne, Nicola; Nannarone, Stefano

2011-01-12T23:59:59.000Z

402

Computational Simulations of High Intensity X-Ray Matter Interaction  

SciTech Connect

Free electron lasers have the promise of producing extremely high-intensity short pulses of coherent, monochromatic radiation in the 1-10 keV energy range. For example, the Linac Coherent Light Source at Stanford is being designed to produce an output intensity of 2 x 10{sup 14} W/cm{sup 2} in a 230 fs pulse. These sources will open the door to many novel research studies. However, the intense x-ray pulses may damage the optical components necessary for studying and controlling the output. At the full output intensity, the dose to optical components at normal incidence ranges from 1-10 eV/atom for low-Z materials (Z < 14) at photon energies of 1 keV. It is important to have an understanding of the effects of such high doses in order to specify the composition, placement, and orientation of optical components, such as mirrors and monochromators. Doses of 10 eV/atom are certainly unacceptable since they will lead to ablation of the surface of the optical components. However, it is not precisely known what the damage thresholds are for the materials being considered for optical components for x-ray free electron lasers. In this paper, we present analytic estimates and computational simulations of the effects of high-intensity x-ray pulses on materials. We outline guidelines for the maximum dose to various materials and discuss implications for the design of optical components.

London, R A; Rionta, R; Tatchyn, R; Roessler, S

2001-08-02T23:59:59.000Z

403

Soft x-ray scattering using FEL radiation for probing near-solid density plasmas at few electronvolt temperatures  

DOE Green Energy (OSTI)

We report on soft x-ray scattering experiments on cryogenic hydrogen and simple metal targets. As a source of intense and ultrashort soft x-ray pulses we have used free-electron laser radiation at 92 eV photon energy from FLASH at DESY, Hamburg. X-ray pulses with energies up to 100 {micro}J and durations below 50 fs provide interaction with the target leading simultaneously to plasma formation and scattering. Experiments exploiting both of these interactions have been carried out, using the same experimental setup. Firstly, recording of soft x-ray inelastic scattering from near-solid density hydrogen plasmas at few electronvolt temperatures confirms the feasibility of this diagnostics technique. Secondly, the soft x-ray excitation of few electronvolt solid-density plasmas in simple metals could be studied by recording soft x-ray line and continuum emission integrated over emission times from fs to ns.

Toleikis, S; Faustlin, R R; Cao, L; Doppner, T; Dusterer, S; Forster, E; Fortmann, C; Glenzer, S H; Gode, S; Gregori, G; Irsig, R; Laarmann, T; Lee, H J; Li, B; Meiwes-Broer, K; Przystawik, A; Radcliffe, P; Redmer, R; Tavella, F; Thiele, R; Tiggesbaumker, J; Truong, N X; Uschmann, I; Zastrau, U; Tschentscher, T

2009-03-03T23:59:59.000Z

404

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

405

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Lensless Imaging of Whole Biological Cells with Soft X-Rays Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Wednesday, 26 May 2010 00:00 A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

406

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

407

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

408

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

409

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

410

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

411

Image plates as x-ray detectors in plasma physics experiments  

SciTech Connect

The performance of image plates based on the photostimulable phosphor BaF(Br,l):Eu{sup 2+} has been investigated and compared with x-ray film. Evaluation of detective quantum efficiency (DQE), sensitivity, dynamic range, and linearity was carried out for several types of commercially available image plate, using the Excalibur soft x-ray calibration facility at AWE. Image plate response was found to be linear over a dynamic range of 5 orders of magnitude. One type of image plate was found to have a number of advantages for soft x-ray detection, with a measured sensitivity 1 order of magnitude greater than that of Kodak Industrex CX and DEF-5 x-ray film. The DQE of this plate was found to be superior to that of film at low [less than 10{sup 3} photons/(50 {mu}m){sup 2}] and high fluxes [greater than 10{sup 4} photons/(50 {mu}m){sup 2}]. The spatial resolution of image plates, scanned with several models of commercial image plate readers, has been evaluated using a USAF resolution test target. The highest spatial resolution measured is 35 {mu}m. Though this is significantly lower than the resolution possible with film, it is sufficient for many applications. Image plates were fielded in a refractive x-ray lens imaging diagnostic on the 1 TW Helen laser and these results are discussed.

Gales, S.G.; Bentley, C.D. [AWE Aldermaston, Reading RG7 4PR (United Kingdom)

2004-10-01T23:59:59.000Z

412

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

413

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

414

Multiple wavelength x-ray monochromators  

DOE Patents (OSTI)

An apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined second distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focussing the separate first and second output x-ray radiation wavelengths into separate focal points.

Steinmeyer, P.A.

1991-01-01T23:59:59.000Z

415

Multiple wavelength x-ray monochromators  

DOE Patents (OSTI)

An apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined second distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focussing the separate first and second output x-ray radiation wavelengths into separate focal points.

Steinmeyer, P.A.

1991-12-31T23:59:59.000Z

416

X-Ray and Neutron Diffraction  

Science Conference Proceedings (OSTI)

Oct 20, 2010 ... Advanced X-Ray Scattering Techniques for Multi-Length Scale ... ?-Ti using the 3DXRD station 34-ID-E at the Advanced Photon Source, Argonne National Laboratory. ... Research at APS 34-ID-E, partly funded by BES/DOE.

417

Soft x-ray laser microscope  

Science Conference Proceedings (OSTI)

The program consisted of two phases (Phase I and Phase II). The goal of the Phase I (first year program) was to design and construct the Soft X-ray Laser Contact Microscope. Such microscope was constructed and adapted to PPL's 18.2nm soft X-ray Laser (SXL), which in turn was modified and prepared for microscopy experiments. Investigation of the photoresist response to 18.2nm laser radiation and transmissivity of 0.1m thick silicion-nitride (Si[sub 3]N[sub 4]) windows were important initial works. The goal of the first year of Phase II was to construct X-ray contact microscope in combination with existing optical phase microscope, already used by biologists. In the second year of Phase II study of dehydrated Horeseshoe Crab and Hela cancer cells were performed with COXRALM. Also during Phase II, the Imaging X-Ray Laser Microscope (IXRALM) was designed and constructed. This paper describes the development of each of the microscopes and their application for research.

Suckewer, P.I.

1990-10-01T23:59:59.000Z

418

Determining the electron-phonon coupling strength from Resonant Inelastic X-ray Scattering at transition metal L-edges  

SciTech Connect

We show that high-resolution Resonant Inelastic X-ray Scattering (RIXS) provides direct, element-specific and momentum-resolved information on the electron-phonon (e-p) coupling strength. Our theoretical analysis indicates how the e-p coupling can be extracted from RIXS spectra by determining the differential phonon scattering cross-section. An alternative manner to extract the coupling is to use the one- and two-phonon loss ratio, which is governed by the e-p coupling strength and the core-hole lifetime. This allows the determination of the e-p coupling on an absolute energy scale.

Ament, L.J.P.; van Veenendaal, M.; van den Brink, J. (Leiden); (NIU); (IFW Dresden)

2012-04-02T23:59:59.000Z

419

Estimating The Reliability of the Lawrence Livermore National Laboratory (LLNL) Flash X-ray (FXR) Machine  

Science Conference Proceedings (OSTI)

At Lawrence Livermore National Laboratory (LLNL), our flash X-ray accelerator (FXR) is used on multi-million dollar hydrodynamic experiments. Because of the importance of the radiographs, FXR must be ultra-reliable. Flash linear accelerators that can generate a 3 kA beam at 18 MeV are very complex. They have thousands, if not millions, of critical components that could prevent the machine from performing correctly. For the last five years, we have quantified and are tracking component failures. From this data, we have determined that the reliability of the high-voltage gas-switches that initiate the pulses, which drive the accelerator cells, dominates the statistics. The failure mode is a single-switch pre-fire that reduces the energy of the beam and degrades the X-ray spot-size. The unfortunate result is a lower resolution radiograph. FXR is a production machine that allows only a modest number of pulses for testing. Therefore, reliability switch testing that requires thousands of shots is performed on our test stand. Study of representative switches has produced pre-fire statistical information and probability distribution curves. This information is applied to FXR to develop test procedures and determine individual switch reliability using a minimal number of accelerator pulses.

Ong, M M; Kihara, R; Zentler, J M; Kreitzer, B R; DeHope, W J

2007-06-27T23:59:59.000Z

420

Theoretical treatments of the bound-free contribution and experimental best practice in X-ray Thomson scattering from warm dense matter  

SciTech Connect

By comparison with high-resolution synchrotron x-ray experimental results, we assess several theoretical treatments for the bound-free (core-electron) contribution to x-ray Thomson scattering (i.e., also known as nonresonant inelastic x-ray scattering). We identify an often overlooked source of systematic error in the plane-wave form factor approximation (PWFFA) used in the inference of temperature, ionization state, and free electron density in some laser-driven compression studies of warm dense matter. This error is due to a direct violation of energy conservation in the PWFFA. We propose an improved practice for the bound-free term that will be particularly relevant for XRTS experiments performed with somewhat improved energy resolution at the National Ignition Facility or the Linac Coherent Light Source. Our results raise important questions about the accuracy of state variable determination in XRTS studies, given that the limited information content in low-resolution XRTS spectra does not strongly constrain the models of electronic structure being used to fit the spectra.

Mattern, Brian A.; Seidler, Gerald T. [Department of Physics, University of Washington, Seattle, Washington 98195-1560 (United States)

2013-02-15T23:59:59.000Z

Note: This page contains sample records for the topic "x-ray energy resolution" from the National Library of Energ