Powered by Deep Web Technologies
Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


1

Full-field Transmission X-ray Microscopy | Stanford Synchrotron Radiation  

NLE Websites -- All DOE Office Websites (Extended Search)

BL6-2c / Transmission X-ray Microscopy BL6-2c / Transmission X-ray Microscopy Home Researchers Publications Science Highlights Department of Energy Office of Science Search form Search Search TXM Search Full-field Transmission X-ray Microscopy Capabilities Full-field TXM is an excellent method to examine nanoscale heterogeneties in many materials, including complex hierarchical systems such as catalysts, fuel cells and battery electrodes, and biological and environmental samples, at 30 nm resolution.The transmission X-ray microscope (TXM) on beam line 6-2c at SSRL is capable of 2D imaging and tomography, as well as spectroscopic imaging for 2D and 3D elemental mapping and chemical mapping over tens of microns (up to mm in 2D). The field of view (FOV) is 30 microns, but mosaic images can be collected to

2

X-ray Phase Imaging Microscopy using a Fresnel Zone Plate and a Transmission Grating  

SciTech Connect

We report on a hard X-ray phase imaging microscopy (a phase-difference microscopy) that consists of an objective and a transmission grating. The simple optical system provides a quantitative phase image, and does not need a wave field mostly coherent on the objective. Our method has a spatial resolution almost same as that of the absorption contrast microscope image obtained by removing the grating. We demonstrate how our approach provides a phase image from experimentally obtained images. Our approach is attractive for easily appending a quantitative phase-sensitive mode to normal X-ray microscopes, and has potentially broad applications in biology and material sciences.

Yashiro, Wataru; Momose, Atsushi [Department of Advanced Materials Science, Graduate School of Frontier Sciences, University of Tokyo, 5-1-5, Kashiwanoha, Kashiwa, Chiba, 277-8561 (Japan); Takeuchi, Akihisa; Suzuki, Yoshio [Japan Synchrotron Radiation Research Institute (JASRI), 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo, 679-5198 (Japan)

2010-06-23T23:59:59.000Z

3

Study of Interactions Between Microbes and Minerals by Scanning Transmission X-Ray Microscopy (STXM)  

SciTech Connect

Scanning Transmission X-ray Microscopy (STXM) and Transmission Electron Microscopy (TEM) were combined to characterize various samples of geomicrobiological interest down to the nanometer scale. An approach based on energy-filtered imaging was used to examine microbe-mineral interactions and the resulting biominerals, as well as biosignatures in simplified laboratory samples. This approach was then applied to natural samples, including natural biofilms entombed in calcium carbonate precipitates and bioweathered silicates and facilitated location of bacterial cells and provided unique insights about their biogeochemical interactions with minerals at the 30-40 nm scale.

Benzerara, K.; /Paris U., VI-VII, LMCP; Tyliszczak, T.; /LBNL, ALS; Brown, G.E., Jr.; /Stanford U., Geo. Environ. Sci. /SLAC, SSRL

2007-01-03T23:59:59.000Z

4

Probing the electronic structure of graphene sheets with various thicknesses by scanning transmission X-ray microscopy  

SciTech Connect

The electronic structure of an aggregation of graphene sheets with various thicknesses was probed by scanning transmission X-ray microscopy. A uniform oxidation of the graphene sheets in the flat area was observed regardless of the thickness, while in the folded area the result could be strongly affected by the geometry. Moreover, thick parts of the aggregation showed strong angle-dependence to the incident X-ray, while thin parts showed less angle-dependence, which might be related to the surface wrinkles and ripples. The electronic structure differences due to the geometry and thickness suggest a complicated situation in the aggregation of graphene sheets.

Bai, Lili; Liu, Jinyin; Zhao, Guanqi; Gao, Jing; Sun, Xuhui, E-mail: xhsun@suda.edu.cn, E-mail: jzhong@suda.edu.cn; Zhong, Jun, E-mail: xhsun@suda.edu.cn, E-mail: jzhong@suda.edu.cn [Soochow University-Western University Centre for Synchrotron Radiation Research, Institute of Functional Nano and Soft Materials Laboratory (FUNSOM) and Collaborative Innovation Center of Suzhou Nano Science and Technology, Soochow University, Suzhou 215123 (China)] [Soochow University-Western University Centre for Synchrotron Radiation Research, Institute of Functional Nano and Soft Materials Laboratory (FUNSOM) and Collaborative Innovation Center of Suzhou Nano Science and Technology, Soochow University, Suzhou 215123 (China)

2013-12-16T23:59:59.000Z

5

A Comparison of Image Quality Evaluation Techniques for Transmission X-Ray Microscopy  

SciTech Connect

Beamline 6-2c at Stanford Synchrotron Radiation Lightsource (SSRL) is capable of Transmission X-ray Microscopy (TXM) at 30 nm resolution. Raw images from the microscope must undergo extensive image processing before publication. Since typical data sets normally contain thousands of images, it is necessary to automate the image processing workflow as much as possible, particularly for the aligning and averaging of similar images. Currently we align images using the 'phase correlation' algorithm, which calculates the relative offset of two images by multiplying them in the frequency domain. For images containing high frequency noise, this algorithm will align noise with noise, resulting in a blurry average. To remedy this we multiply the images by a Gaussian function in the frequency domain, so that the algorithm ignores the high frequency noise while properly aligning the features of interest (FOI). The shape of the Gaussian is manually tuned by the user until the resulting average image is sharpest. To automatically optimize this process, it is necessary for the computer to evaluate the quality of the average image by quantifying its sharpness. In our research we explored two image sharpness metrics, the variance method and the frequency threshold method. The variance method uses the variance of the image as an indicator of sharpness while the frequency threshold method sums up the power in a specific frequency band. These metrics were tested on a variety of test images, containing both real and artificial noise. To apply these sharpness metrics, we designed and built a MATLAB graphical user interface (GUI) called 'Blur Master.' We found that it is possible for blurry images to have a large variance if they contain high amounts of noise. On the other hand, we found the frequency method to be quite reliable, although it is necessary to manually choose suitable limits for the frequency band. Further research must be performed to design an algorithm which automatically selects these parameters.

Bolgert, Peter J; /Marquette U. /SLAC

2012-08-31T23:59:59.000Z

6

Novel Approaches to Soft X-ray Spectroscopy: Scanning TransmissionX-ray Microscopy and Ambient Pressure X-Ray PhotoelectronSpectroscopy  

SciTech Connect

This workshop focused on novel spectroscopies at Beamlines 11.0.2, 5.3.2 and 9.3.2 at the ALS. The workshop brought together users from a wide range of fields to highlight recent experimental and technical developments both in scanning transmission X-ray spectroscopy (STXM) and ambient pressure photoelectron spectroscopy (APPES). The morning session featured talks on experiments involving new developments at the STXM, while the afternoon session was devoted to those using APXPS. In the morning session, Tolek Tyliszczak discussed the improved detector developments at the STXM, such as an avalanche photodiode detector and fluorescence and electron detection, as well as the continued development of in situ cells for heating, gas flow, and electrochemical cells. Of these, only the avalanche photodiode in combination with a novel multichannel photon-counting system is in routine use in time-resolved studies. Bartel Van Waeyenberge (Ghent University) presented results of magnetic imaging with a time resolution of 70-100 ps combined with a lateral resolution of 20-40 nm performed with the STXM (Beamline 11.0.2). As a complement to the time-domain ''pump-and-probe'' measurements, they developed a frequency-domain ''sine-excitation'' technique in order to study specific eigenmodes of these ferromagnetic patterns with high spatial resolution. This new approach was used to study the gyrotropic vortex motions in micron-sized ferromagnetic patterns. Adam Hitchcock (McMaster University) presented the development, in collaboration with Daniel Guay (INRS, Varennes) and Sherry Zhang, of the apparatus and techniques for applying STXM to in-situ studies of electrochemistry, in particular electrochromism in polyaniline. In addition, substantial progress was reported on a joint project to develop substrates and methods for chemically selective lithography of multilayer polymer systems. Selective patterns, such as that displayed in the figure, can now be written efficiently with the bend magnet STXM on Beamline 5.3.2. Yves Acremann (SSRL) discussed time and spatially resolved X-ray magnetic circular dichroism (XMCD) experiments on spin transfer devices at the STXM (Beamline 11.0.2). These elegant experiments explore time resolved measurements of the magnetization dynamics within a 100 x 150 nm sample influenced by a spin-polarized current. This experiment shows that the magnetization in these magnetic nanostructures are not uniform, as they are influenced by the Oersted field of the charge current needed to generate the spin current. The implementation of a novel multichannel photon counting system in combination with an avalanche photon detector decreased the data-acquisition time by a factor of 10, owing to its ability to resolve the structure of multi bunch mode. Gordon E. Brown, Jr. (Stanford University and SSRL) described ''Applications of STXM to Microbial Bioweathering and Biomineralization''. In the interaction of bacteria with ferrihydrite nanoparticles, microenvironments that were very different than the bulk material were observed, showing that bulk thermodynamics may not be useful for predicting micro phases. Gordon also presented work showing that iron nanoparticles are attracted to the negatively charged bacteria and form a coating that reduces iron oxide minerals. The afternoon session started with presentations by Simon Mun and Hendrik Bluhm, who discussed the current status and the future plans for the two APPES end-stations at the ALS, which are located at Beamlines 9.3.2 and 11.0.2, respectively. In both end-stations, samples can be measured in gaseous environments at pressures of up to several Torr, which makes possible the investigation of numerous phenomena, in particular in the fields of atmospheric and environmental science as well as heterogeneous catalysis. Specific examples of the application of APPES were shown in the following presentations. John Hemminger (University of California, Irvine) reported on APPES investigations at Beamlines 9.3.2 and 11.0.2 of the interaction of alkali halide surfaces with water. The m

Bluhm, Hendrik; Gilles, Mary K.; Mun, Simon B.; Tyliszczak, Tolek

2006-02-01T23:59:59.000Z

7

Scanning transmission X-ray microscopy probe for in situ mechanism study of graphene-oxide-based resistive random access memory  

Science Journals Connector (OSTI)

An in situ probe for scanning transmission X-ray microscopy has been developed and applied to the study of the bipolar resistive switching mechanism in an Al/graphene oxide/Al resistive random access memory device.

Nho, H.W.

2013-11-28T23:59:59.000Z

8

Pressure-induced densification in GeO{sub 2} glass: A transmission x-ray microscopy study  

SciTech Connect

Nanoscale transmission x-ray microscopy measurements have been performed to determine the effect of pressure (P) on the volume (V) change in GeO{sub 2} glass up to 38.5?GPa. The P-V data show a continuous increase upon compression, indicating that the density-driven structural transformation is a gradual process. Over the pressure range studied, a transition is observed at approximately 10–13?GPa, where the material displays distinct compression behaviors. The pressure-induced densification that involves the coordination number change has been discussed. Using this newly developed high-pressure imaging technique with tens of nanometer resolution, we have provided a direct and unequivocal way for measuring density of amorphous materials to much higher pressures with accuracy rivaling x-ray diffraction of crystalline solids.

Lin, Yu, E-mail: lyforest@stanford.edu; Zeng, Qiaoshi [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States)] [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States); Yang, Wenge [High Pressure Synergetic Consortium, Geophysical Laboratory, Carnegie Institution of Washington, Argonne, Illinois 60439 (United States)] [High Pressure Synergetic Consortium, Geophysical Laboratory, Carnegie Institution of Washington, Argonne, Illinois 60439 (United States); Mao, Wendy L. [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States) [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States); Photon Science, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States)

2013-12-23T23:59:59.000Z

9

Argonne CNM: X-Ray Microscopy Capabilities  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Microscopy Facilities X-Ray Microscopy Facilities The Hard X-Ray Nanoprobe (HXN) facility provides scanning fluorescence, scanning diffraction, and full-field transmission and tomographic imaging capabilities with a spatial resolution of 30 nm over a spectral range of 6-12 keV. Modes of Operation Full-Field Transmission Imaging and Nanotomography X-ray transmission imaging uses both the absorption and phase shift of the X-ray beam by the sample as contrast mechanisms. Absorption contrast is used to map the sample density. Elemental constituents can be located by using differential edge contrast in this mode. Phase contrast can be highly sensitive to edges and interfaces even when the X-ray absorption is weak. These contrast mechanisms are exploited to image samples rapidly in full-field transmission mode under various environmental conditions, or combined with nanotomography methods to study the three-dimensional structure of complex and amorphous nanomaterials with the HXN.

10

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray...

11

X-Ray Diffraction Microscopy of Magnetic Structures  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing...

12

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in...

13

X-Ray Laser Sources for Microscopy  

Science Journals Connector (OSTI)

Progress and prospects in soft X-ray laser development at Princeton are presented. A comparison to plasma and synchrotron sources is made with a...

C. H. Skinner; D. E. Kim; A. Wouters; D. Voorhees; S. Suckewer

1988-01-01T23:59:59.000Z

14

3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone at the  

NLE Websites -- All DOE Office Websites (Extended Search)

3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone 3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone at the Nanoscale Scientists studying osteoporosis and other skeletal diseases are interested in the 3D structure of bone and its responses to conditions such as weightlessness, radiation (of particular interest to astronauts) and vitamin D deficiency. The current gold standard, micro-computed tomography (micro-CT), provides 3D images of trabeculae, the small interior struts of bone tissue, and electron microscopy can provide nanometer resolution of thin tissue slices. Hard X-ray transmission microscopy has provided the first 3D view of bone structure within individual trabeculae on the nanoscale. figure 1 Figure 1 Micro-CT (left) shows trabecular structure inside of bone. Transmission X-ray microscopy (TXM; center and right) can reveal localized details of osteocyte lacunae and their processes.

15

X-Ray Diffraction Microscopy of Magnetic Structures  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

16

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

17

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

18

X-Ray Diffraction Microscopy of Magnetic Structures  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

19

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

20

X-Ray Diffraction Microscopy of Magnetic Structures  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

22

X-ray transmissive debris shield  

DOE Patents (OSTI)

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, R.B.

1996-05-21T23:59:59.000Z

23

X-ray transmissive debris shield  

DOE Patents (OSTI)

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, Rick B. (Albuquerque, NM)

1996-01-01T23:59:59.000Z

24

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental...  

NLE Websites -- All DOE Office Websites (Extended Search)

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental Science Beamline at the Advanced Light Source. Soft X-Ray Microscopy and Spectroscopy at the Molecular...

25

Investigation of white etching layers on rails by optical microscopy, electron microscopy, X-ray and synchrotron X-ray diffraction  

Science Journals Connector (OSTI)

Patches of white etching layers on rail surfaces were investigated using sophisticated techniques like cross-sectional transmission electron microscopy (XTEM) and synchroton X-ray diffraction. Optical microscopy failed to resolve the microstructure, but in the TEM submicron grains with high dislocation densities and occasional twins, which are characteristic features of high carbon martensite, were observed. The martensitic structure was confirmed by evaluation of synchroton X-ray diffraction line profiles. The latter technique also allowed to determine dislocation densities of the order of 1012 cm?2 and residual compressive stresses of about 200 MPa.

W. Österle; H. Rooch; A. Pyzalla; L. Wang

2001-01-01T23:59:59.000Z

26

Characterization of the Binding of Gallium, Platinum, and Uranium to Pseudomonas fluorescens by Small-Angle X-Ray Scattering and Transmission Electron Microscopy  

Science Journals Connector (OSTI)

...that combined small-angle neutron scattering and small-angle X-ray scattering...by small-angle X-ray and neutron scattering. Plenum Press, New York...of biological structures by neutron scattering from solution. Rep. Prog...

Susan Krueger; Gregory J. Olson; David Johnsonbaugh; T. J. Beveridge

1993-12-01T23:59:59.000Z

27

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

28

Cryogenic X-Ray Diffraction Microscopy for Biological Samples  

Science Journals Connector (OSTI)

X-ray diffraction microscopy (XDM) is well suited for nondestructive, high-resolution biological imaging, especially for thick samples, with the high penetration power of x rays and without limitations imposed by a lens. We developed nonvacuum, cryogenic (cryo-) XDM with hard x rays at 8 keV and report the first frozen-hydrated imaging by XDM. By preserving samples in amorphous ice, the risk of artifacts associated with dehydration or chemical fixation is avoided, ensuring the imaging condition closest to their natural state. The reconstruction shows internal structures of intact D. radiodurans bacteria in their natural contrast.

Enju Lima; Lutz Wiegart; Petra Pernot; Malcolm Howells; Joanna Timmins; Federico Zontone; Anders Madsen

2009-11-05T23:59:59.000Z

29

Cryogenic X-ray Diffraction Microscopy for Biological Samples  

SciTech Connect

X-ray diffraction microscopy (XDM) is well suited for nondestructive, high-resolution biological imaging, especially for thick samples, with the high penetration power of x rays and without limitations imposed by a lens. We developed nonvacuum, cryogenic (cryo-) XDM with hard x rays at 8 keV and report the first frozen-hydrated imaging by XDM. By preserving samples in amorphous ice, the risk of artifacts associated with dehydration or chemical fixation is avoided, ensuring the imaging condition closest to their natural state. The reconstruction shows internal structures of intact D. radiodurans bacteria in their natural contrast.

E Lima; L Wiegart; P Pernot; M Howells; J Timmins; F Zontone; A Madsen

2011-12-31T23:59:59.000Z

30

X-ray Microscopy and Imaging (XSD-XMI)  

NLE Websites -- All DOE Office Websites (Extended Search)

Imaging (XMI) Imaging (XMI) About XMI Science and Research Beamlines Highlights Software and Tools Intranet Search APS... Argonne Home > Advanced Photon Source > Contacts FAQs Beamlines News Publications APS Email Portal APS Intranet APS Phonebook APS Quick Links for Users APS Safety and Training Welcome to the X-ray Microscopy and Imaging group (XMI)! X-ray Microscopy and Imaging is part of the X-ray Science Division at the Advanced Photon Source. We develop and support a diverse and multidisciplinary user research program at Sectors 2 and 32 of the APS, with the overall goal to image and study materials structures at spatial and temporal resolutions that are most scientifically relevant to the cutting-edge advances in materials, biological, environmental, and biomedical sciences. To achieve this goal, we actively engage in various research activities including

31

Soft X-Ray Diffraction Microscopy of a Frozen Hydrated Yeast Cell Xiaojing Huang,1  

E-Print Network (OSTI)

Soft X-Ray Diffraction Microscopy of a Frozen Hydrated Yeast Cell Xiaojing Huang,1 Johanna Nelson,1 eukaryotic cell using x-ray diffraction microscopy, or coherent x-ray diffraction imaging. By plunge freezingV x rays were recorded and reconstructed to reveal a budding yeast cell at a resolution better than 25

Mohseni, Hooman

32

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Wednesday, 31 August 2005 00:00...

33

Demonstration of 12 nm resolution Fresnel zone plate lens based soft x-ray microscopy  

SciTech Connect

To extend soft x-ray microscopy to a resolution of order 10 nm or better, we developed a new nanofabrication process for Fresnel zone plate lenses. The new process, based on the double patterning technique, has enabled us to fabricate high quality gold zone plates with 12 nm outer zones. Testing of the zone plate with the full-field transmission x-ray microscope, XM-1, in Berkeley, showed that the lens clearly resolved 12 nm lines and spaces. This result represents a significant step towards 10 nm resolution and beyond.

Chao, W.; Kim, J.; Rekawa, S.; Fischer, P.; Anderson, E. H.

2009-06-05T23:59:59.000Z

34

X-ray microscopy using grazing-incidence reflection optics  

SciTech Connect

The Kirkpatrick-Baez microscopes are described along with their role as the workhorse of the x-ray imaging devices. This role is being extended with the development of a 22X magnification Kirkpatrick-Baez x-ray microscope with multilayer x-ray mirrors. These mirrors can operate at large angles, high x-ray energies, and have a narrow, well defined x-ray energy bandpass. This will make them useful for numerous experiments. However, where a large solid angle is needed, the Woelter microscope will still be necessary and the technology needed to build them will be useful for many other types of x-ray optics.

Price, R.H.

1981-08-06T23:59:59.000Z

35

X-ray Microscopy and Imaging: 2-BM  

NLE Websites -- All DOE Office Websites (Extended Search)

BM BM Introduction The 2-BM beamline offers measurement capabilities for x-ray microtomography, x-ray topography and x-ray microdiffraction. X-ray microtomography and x-ray diffraction instruments are installed on separate optical tables for independent operation with fast switch over time. Optically-coupled high-resolution CCD system is used for microtomography and topography with up to 1 micron spatial resolution. X-ray microdiffraction setup consists of KB microfocussing mirrors (~3 micron minimum spot), four-circle Huber diffractometer, high-precision translation sample stage, two orthogonally-mounted video cameras for viewing sample, fluorescence detector (Si-drift diode) and diffraction detector (a scintillation detector or a CCD). Three different levels of monochromaticity are available. Conventional monochromatic x-rays from a double-bounced Si (111) crystal monochromator (DCM, D E/E=1E-4), wide band-pass monochromatic x-rays from a double multilayer monochromator (DMM, D E/E=1~4E-2) and pink beam. The available x-ray range is from 5 keV to 30 keV. The lower limit is due to the x-ray windows and the upper limit is due to the critical angle of the x-ray mirror. Two different coatings (Cr and Pt) for the x-ray mirror allow either 20 keV or 30 keV energy cutoff.

36

Electron microscopy and microanalysis Two transmission electron microscopes  

E-Print Network (OSTI)

Electron microscopy and microanalysis Two transmission electron microscopes (TEM) and three scanning electron micro- scopes (SEM) are operated by the De- partment. Attachments for TEM include energy dispersive X-ray spectrometer (EDS), scanning transmission attachment, serial electron energy loss

37

Microcalorimeter-type energy dispersive X-ray spectrometer for a transmission electron microscope  

Science Journals Connector (OSTI)

......Microscopy (1986) New York: Plenum Press. 4...Garratt-Reed A J , Bell D C. Energy-Dispersive X-ray...Microscopy (1996) New York: Plenum Press. 19...Microcalorimeter-type energy dispersive X-ray...electron microscope. | A new energy dispersive......

Toru Hara; Keiichi Tanaka; Keisuke Maehata; Kazuhisa Mitsuda; Noriko Y. Yamasaki; Mitsuaki Ohsaki; Katsuaki Watanabe; Xiuzhen Yu; Takuji Ito; Yoshihiro Yamanaka

2010-02-01T23:59:59.000Z

38

Soft X-Ray Diffraction Microscopy of a Frozen Hydrated Yeast Cell  

SciTech Connect

We report the first image of an intact, frozen hydrated eukaryotic cell using x-ray diffraction microscopy, or coherent x-ray diffraction imaging. By plunge freezing the specimen in liquid ethane and maintaining it below -170 deg. C, artifacts due to dehydration, ice crystallization, and radiation damage are greatly reduced. In this example, coherent diffraction data using 520 eV x rays were recorded and reconstructed to reveal a budding yeast cell at a resolution better than 25 nm. This demonstration represents an important step towards high resolution imaging of cells in their natural, hydrated state, without limitations imposed by x-ray optics.

Huang Xiaojing; Nelson, Johanna; Lima, Enju; Miao, Huijie; Steinbrener, Jan; Stewart, Andrew; Turner, Joshua J.; Jacobsen, Chris [Department of Physics and Astronomy, Stony Brook University, Stony Brook, New York 11794-3800 (United States); Kirz, Janos [Department of Physics and Astronomy, Stony Brook University, Stony Brook, New York 11794-3800 (United States); Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Marchesini, Stefano; Shapiro, David [Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Neiman, Aaron M. [Department of Biochemistry and Cell Biology, Stony Brook University, Stony Brook, New York 11794-5215 (United States)

2009-11-06T23:59:59.000Z

39

Fabrication and performance of blazed transmission gratings for x-ray astronomy  

E-Print Network (OSTI)

We have developed a new type of soft x-ray diffraction grating. This critical-angle transmission (CAT) grating combines the advantages of traditional transmission gratings (low mass, extremely relaxed alignment and flatness ...

Schattenburg, Mark Lee

40

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Wednesday, 31 August 2005 00:00 Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Schmahl, Kirz Receive Compton Award for Contributions to X-ray Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Schmahl, Kirz Received Compton Award for Contributions to X-ray Microscopy Schmahl, Kirz Received Compton Award for Contributions to X-ray Microscopy Image of Compton Award The Advanced Photon Source (APS) and APS Users Organization (APSUO) are very pleased to announce that the 2005 Arthur H. Compton Award was given to Günter Schmahl and Janos Kirz for pioneering and developing the field of x-ray microscopy using Fresnel zone plates. Because of their leadership over the last 30 years, x-ray microscopy has evolved into a powerful method for the study of nanoscale structures and phenomena in many areas of science. Their achievements have opened up productive research avenues in biology, polymers, electronic nanostructures, magnetic materials, meteoritics, and environmental sciences. " Günter Schmahl and Janos Kirz have created a

42

Application of X-ray synchrotron microscopy instrumentation in biology  

SciTech Connect

X-ray micro-fluorescence imaging technique has been used as a significant tool in order to investigate minerals contents in some kinds of materials. The aim of this study was to evaluate the elemental distribution of calcium and zinc in bone substitute materials (nano-hydroxyapatite spheres) and cortical bones through X-Ray Micro-fluorescence analysis with the increment of Synchrotron Radiation in order to evaluate the characteristics of the newly formed bone and its interface, the preexisting bone and biomaterials by the arrangement of collagen fibers and its birefringence. The elemental mapping was carried out at Brazilian Synchrotron Light Laboratory, Campinas - Sao Paulo, Brazil working at D09-XRF beam line. Based on this study, the results suggest that hydroxyapatite-based biomaterials are biocompatible, promote osteo-conduction and favored bone repair. (authors)

Gasperini, F. M. [Medical Science Program, Fluminense Federal Univ., Niteroi (Brazil); Pereira, G. R. [Dept. of Metallurgical and Materials Engineering, Federal Univ. of Rio de Janeiro (Brazil); Granjeiro, J. M. [Molecular and Cell Biology Dept., Fluminense Federal Univ., Niteroi, Rio de Janeiro (Brazil); Calasans-Maia, M. D. [Oral Surgery Dept., Fluminense Federal Univ., Niteroi, Rio de Janeiro (Brazil); Rossi, A. M. [Biomaterials Laboratory, Brazilian Center of Physics Research, Rio de Janeiro (Brazil); Perez, C. A. [Brazilian Synchrotron Laboratory, Campinas, Sao Paulo (Brazil); Lopes, R. T.; Lima, I. [Nuclear Engineering Laboratory, Federal Univ. of Rio de Janeiro (Brazil)

2011-07-01T23:59:59.000Z

43

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

44

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

45

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

NLE Websites -- All DOE Office Websites (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical devices with nanoscale accuracy has allowed researchers in Berkeley Lab's Center for X-Ray Optics (CXRO), which built and operates the XM-1, to achieve an extraordinary resolution of better than 15 nm, with the promise of even higher resolution in the near future.

46

X-ray holographic microscopy experiments at the Brookhaven synchrotron light source  

SciTech Connect

Soft x-ray holographic microscopy is discussed from an experimental point of view. Three series of measurements have been carried out using the Brookhaven 750 MeV storage ring as an x-ray source. Young slits fringes, Gabor (in line) holograms and various data pertaining to the soft x-ray performance of photographic plates are reported. The measurements are discussed in terms of the technique for recording them and the experimental limitations in effect. Some discussion is also given of the issues involved in reconstruction using visible light.

Howells, M.R.; Iarocci, M.; Kenney, J.; Kirz, J.; Rarback, H.

1983-01-01T23:59:59.000Z

47

The X-ray microscopy beamline UE46-PGM2 at BESSY  

SciTech Connect

The Max Planck Institute for Metal Physics in Stuttgart and the Helmholtz Center Berlin operate a soft X-ray microscopy beamline at the storage ring BESSY II. A collimated PGM serves as monochromator for a scanning X-ray microscope and a full field X-ray microscope at the helical undulator UE46. The selection between both instruments is accomplished via two switchable focusing mirrors. The scanning microscope (SM) is based on the ALS STXM microscope and fabricated by the ACCEL company. The full field microscope (FFM) is currently in operation at the U41-SGM beamline and will be relocated to its final location this year.

Follath, R.; Schmidt, J. S. [Helmholtz-Center Berlin, Albert-Einstein-Strasse 15, 12489 Berlin (Germany); Weigand, M. [Max Planck Institute for Metals Research, Heisenbergstrasse 3, 70569 Stuttgart (Germany); Fauth, K. [University Erlangen, Experimental Physics 4, Am Hubland, 97074 Wuerzburg (Germany)

2010-06-23T23:59:59.000Z

48

WHOLE CELL TOMOGRAPHY/MOLECULAR BIOLOGY/STRUCTURAL BIOLOGY: Affordable x-ray microscopy with nanoscale resolution  

SciTech Connect

Biological research spans 10 orders of magnitude from angstroms to meters. While electron microscopy can reveal structural details at most of these spatial length scales, transmission electron tomography only reliably reconstructs three-dimensional (3-D) volumes of cellular material with a spatial resolution between 1-5 nm from samples less than 500 nm thick1. Most biological cells are 2-30 times thicker than this threshold, which means that a cell must be cut into consecutive slices with each slice reconstructed individually in order to approximate the contextual information of the entire cell. Fortunately, due to a larger penetration depth2, X-ray computed tomography bypasses the need to physically section a cell and enables imaging of intact cells and tissues on the micrometer or larger scale with tens to hundreds of nanometer spatial resolution. While the technique of soft x-ray microscopy has been extensively developed in synchrotron facilities, advancements in laboratory x-ray source designs now increase its accessibility by supporting commercial systems suitable for a standard laboratory. In this paper, we highlight a new commercial compact cryogenic soft x-ray microscope designed for a standard laboratory setting and explore its capabilities for mesoscopic investigations of intact prokaryotic and eukaryotic cells.

Evans, James E.; Blackborow, Paul; Horne, Stephen J.; Gelb, Jeff

2013-03-01T23:59:59.000Z

49

Laboratory-Based Cryogenic Soft X-ray Tomography with Correlative Cryo-Light and Electron Microscopy  

SciTech Connect

Here we present a novel laboratory-based cryogenic soft X-ray microscope for whole cell tomography of frozen hydrated samples. We demonstrate the capabilities of this compact cryogenic microscope by visualizing internal sub-cellular structures of Saccharomyces cerevisiae cells. The microscope is shown to achieve better than 50 nm spatial resolution with a Siemens star test sample. For whole biological cells, the microscope can image specimens up to 5 micrometers thick. Structures as small as 90 nm can be detected in tomographic reconstructions at roughly 70 nm spatial resolution following a low cumulative radiation dose of only 7.2 MGy. Furthermore, the design of the specimen chamber utilizes a standard sample support that permits multimodal correlative imaging of the exact same unstained yeast cell via cryo-fluorescence light microscopy, cryo-soft x-ray microscopy and cryo-transmission electron microscopy. This completely laboratory-based cryogenic soft x-ray microscope will therefore enable greater access to three-dimensional ultrastructure determination of biological whole cells without chemical fixation or physical sectioning.

Carlson, David B.; Gelb, Jeff; Palshin, Vadim; Evans, James E.

2013-02-01T23:59:59.000Z

50

Elimination of higher-order diffraction using zigzag transmission grating in soft x-ray region  

SciTech Connect

We present a realization of the sinusoidal transmission function using a series of zigzag-profiled strips where the transmission takes on the binary values 0 and 1 in a two-dimensional distribution. A zigzag transmission grating of 1000 line/mm has been fabricated and demonstrated on the soft x-ray beam of synchrotron radiation. The axial single-order diffraction indicates that the zigzag transmission grating is adequate for spectroscopic application.

Zang, H. P.; Wang, C. K. [Research Center of Laser Fusion, China Academy of Engineering Physics, Mianyang, Sichuan 621900 (China); Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065 (China); Gao, Y. L.; Zhou, W. M.; Kuang, L. Y.; Wei, L.; Fan, W.; Zhang, W. H.; Zhao, Z. Q.; Cao, L. F.; Gu, Y. Q.; Zhang, B. H. [Research Center of Laser Fusion, China Academy of Engineering Physics, Mianyang, Sichuan 621900 (China); Jiang, G. [Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065 (China); Zhu, X. L.; Xie, C. Q. [Institute of Microelectronics, Chinese Academy of Sciences, Beijing 100029 (China); Zhao, Y. D.; Cui, M. Q. [Institute of High Energy Physics, Chinese Academy of Sciences, Beijing 100049 (China)

2012-03-12T23:59:59.000Z

51

X-ray optics for scanning fluorescence microscopy and other applications  

SciTech Connect

Scanning x-ray fluorescence microscopy is analogous to scanning electron microscopy. Maps of chemical element distribution are produced by scanning with a very small x-ray beam. Goal is to perform such scanning microscopy with resolution in the range of <1 to 10 {mu}m, using standard laboratory x-ray tubes. We are investigating mirror optics in the Kirkpatrick-Baez (K-B) configuration. K-B optics uses two curved mirrors mounted orthogonally along the optical axis. The first mirror provides vertical focus, the second mirror provides horizontal focus. We have used two types of mirrors: synthetic multilayers and crystals. Multilayer mirrors are used with lower energy radiation such as Cu K{alpha}. At higher energies such as Ag K{alpha}, silicon wafers are used in order to increase the incidence angles and thereby the photon collection efficiency. In order to increase the surface area of multilayers which reflects x-rays at the Bragg angle, we have designed mirrors with the spacing between layers graded along the optic axis in order to compensate for the changing angle of incidence. Likewise, to achieve a large reflecting surface with silicon, the wafers are placed on a specially designed lever arm which is bent into a log spiral by applying force at one end. In this way, the same diffracting angle is maintained over the entire surface of the wafer, providing a large solid angle for photon collection.

Ryon, R.W. [Lawrence Livermore National Lab., CA (United States); Warburton, W.K. [X-Ray Instrumentation Associates, Menlo Park, CA (United States)

1992-05-01T23:59:59.000Z

52

Cryogenic x-ray diffraction microscopy utilizing high-pressure cryopreservation  

Science Journals Connector (OSTI)

We present cryo x-ray diffraction microscopy of high-pressure-cryofixed bacteria and report high-convergence imaging with multiple image reconstructions. Hydrated D. radiodurans cells were cryofixed at 200 MPa pressure into ?10??m-thick water layers and their unstained, hydrated cellular environments were imaged by phasing diffraction patterns, reaching sub-30-nm resolutions with hard x-rays. Comparisons were made with conventional ambient-pressure-cryofixed samples, with respect to both coherent small-angle x-ray scattering and the image reconstruction. The results show a correlation between the level of background ice signal and phasing convergence, suggesting that phasing difficulties with frozen-hydrated specimens may be caused by high-background ice scattering.

Enju Lima; Yuriy Chushkin; Peter van der Linden; Chae Un Kim; Federico Zontone; Philippe Carpentier; Sol M. Gruner; Petra Pernot

2014-10-15T23:59:59.000Z

53

Nanoscale chemical imaging using synchrotron x-ray enhanced scanning tunneling microscopy  

SciTech Connect

The combination of synchrotron radiation with scanning tunneling microscopy provides a promising new concept for chemical imaging of nanoscale structures. It employs detection of local x-ray absorption, which directly yields chemical, electronic, and magnetic sensitivity. The study of the tip current in the far field (800 nm tip/sample separation) shows that insulator-coated tips have to be considered in order to reduce the background from stray photoelectron. A picture of the different channels contributing to the x-ray enhanced STM process is proposed. If during electron tunneling the sample is illuminated with monochromatic x-rays, characteristic absorption will arise, and core electrons are excited, which might modulate the conventional tunnel current and facilitate chemical imaging at the nanoscale.

Rose, Volker; Freeland, John W. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)

2010-06-23T23:59:59.000Z

54

X-ray intravital microscopy for functional imaging in rat hearts using synchrotron radiation coronary microangiography  

SciTech Connect

An X-ray intravital microscopy technique was developed to enable in vivo visualization of the coronary, cerebral, and pulmonary arteries in rats without exposure of organs and with spatial resolution in the micrometer range and temporal resolution in the millisecond range. We have refined the system continually in terms of the spatial resolution and exposure time. X-rays transmitted through an object are detected by an X-ray direct-conversion type detector, which incorporates an X-ray SATICON pickup tube. The spatial resolution has been improved to 6 {mu}m, yielding sharp images of small arteries. The exposure time has been shortened to around 2 ms using a new rotating-disk X-ray shutter, enabling imaging of beating rat hearts. Quantitative evaluations of the X-ray intravital microscopy technique were extracted from measurements of the smallest-detectable vessel size and detection of the vessel function. The smallest-diameter vessel viewed for measurements is determined primarily by the concentration of iodinated contrast material. The iodine concentration depends on the injection technique. We used ex vivo rat hearts under Langendorff perfusion for accurate evaluation. After the contrast agent is injected into the origin of the aorta in an isolated perfused rat heart, the contrast agent is delivered directly into the coronary arteries with minimum dilution. The vascular internal diameter response of coronary arterial circulation is analyzed to evaluate the vessel function. Small blood vessels of more than about 50 {mu}m diameters were visualized clearly at heart rates of around 300 beats/min. Vasodilation compared to the control was observed quantitatively using drug manipulation. Furthermore, the apparent increase in the number of small vessels with diameters of less than about 50 {mu}m was observed after the vasoactive agents increased the diameters of invisible small blood vessels to visible sizes. This technique is expected to offer the potential for direct investigation of mechanisms of vascular dysfunctions.

Umetani, K. [Japan Synchrotron Radiation Research Institute, SPring-8, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan); Fukushima, K. [National Cerebral and Cardiovascular Center Hospital, Fujishirodai, Suita-shi, Osaka 565-8565 (Japan)

2013-03-15T23:59:59.000Z

55

Dynamic Transmission Electron Microscopy  

SciTech Connect

Dynamic transmission electron microscopy (DTEM) combines the benefits of high spatial resolution electron microscopy with the high temporal resolution of ultrafast lasers. The incorporation of these two components into a single instrument provides a perfect platform for in situ observations of material processes. However, previous DTEM applications have focused on observing structural changes occurring in samples exposed to high vacuum. Therefore, in order to expand the pump-probe experimental regime to more natural environmental conditions, in situ gas and liquid chambers must be coupled with Dynamic TEM. This chapter describes the current and future applications of in situ liquid DTEM to permit time-resolved atomic scale observations in an aqueous environment, Although this chapter focuses mostly on in situ liquid imaging, the same research potential exists for in situ gas experiments and the successful integration of these techniques promises new insights for understanding nanoparticle, catalyst and biological protein dynamics with unprecedented spatiotemporal resolution.

Evans, James E.; Jungjohann, K. L.; Browning, Nigel D.

2012-10-12T23:59:59.000Z

56

Simbol-X Mirror Module Thermal Shields: I - Design and X-Ray Transmission  

SciTech Connect

The Simbol-X mission is designed to fly in formation flight configuration. As a consequence, the telescope has both ends open to space, and thermal shielding at telescope entrance and exit is required to maintain temperature uniformity throughout the mirrors. Both mesh and meshless solutions are presently under study for the shields. We discuss the design and the X-ray transmission.

Collura, A.; Varisco, S. [INAF-OAPA Via G.F. Ingrassia, 31 90123 Palermo (Italy); Barbera, M. [INAF-OAPA Via G.F. Ingrassia, 31 90123 Palermo (Italy); DSFA Universita di Palermo, Via Archirafi 36, 90123 Palermo (Italy); Basso, S.; Pareschi, G.; Tagliaferri, G. [INAF-OAB, via E. bianchi 46, 23807 Merate (Italy); Ayers, T. [Luxel Corporation, Friday Harbor, WA 98250 (United States)

2009-05-11T23:59:59.000Z

57

Single x-ray transmission system for bone mineral density determination  

SciTech Connect

Bones are the support of the body. They are composed of many inorganic compounds and other organic materials that all together can be used to determine the mineral density of the bones. The bone mineral density is a measure index that is widely used as an indicator of the health of the bone. A typical manner to evaluate the quality of the bone is a densitometry study; a dual x-ray absorptiometry system based study that has been widely used to assess the mineral density of some animals' bones. However, despite the success stories of utilizing these systems in many different applications, it is a very expensive method that requires frequent calibration processes to work properly. Moreover, its usage in small species applications (e.g., rodents) has not been quite demonstrated yet. Following this argument, it is suggested that there is a need for an instrument that would perform such a task in a more reliable and economical manner. Therefore, in this paper we explore the possibility to develop a new, affordable, and reliable single x-ray absorptiometry system. The method consists of utilizing a single x-ray source, an x-ray image sensor, and a computer platform that all together, as a whole, will allow us to calculate the mineral density of the bone. Utilizing an x-ray transmission theory modified through a version of the Lambert-Beer law equation, a law that expresses the relationship among the energy absorbed, the thickness, and the absorption coefficient of the sample at the x-rays wavelength to calculate the mineral density of the bone can be advantageous. Having determined the parameter equation that defines the ratio of the pixels in radiographies and the bone mineral density [measured in mass per unit of area (g/cm{sup 2})], we demonstrated the utility of our novel methodology by calculating the mineral density of Wistar rats' femur bones.

Jimenez-Mendoza, Daniel; Vargas-Vazquez, Damian [Division de Investigacion y Posgrado, Facultad de Ingenieria, Universidad Autonoma de Queretaro, Cerro de las Campanas s/n., C.P. 76010, Queretaro, Qro. (Mexico); Espinosa-Arbelaez, Diego G. [Posgrado en Ciencia e Ingenieria en Materiales, Instituto de Investigaciones en Materiales, Universidad Nacional Autonoma de Mexico, Av. Universidad 3000, C.P. 04510, Coyoacan, Mexico D.F. (Mexico); Departamento de Nanotecnologia, Centro de Fisica Aplicada y Tecnologia Avanzada, Universidad Nacional Autonoma de Mexico, Campus Juriquilla, Boulevard Juriquilla 3001, C.P. 76230, A.P. 1-1010, Juriquilla, Qro. (Mexico); Giraldo-Betancur, Astrid L. [Centro de Investigacion y de Estudios Avanzados del Instituto Politecnico Nacional, Libramiento Norponiente 2000, C.P. 76230, Fracc. Real de Juriquilla, Qro. (Mexico); Hernandez-Urbiola, Margarita I. [Posgrado en Investigaciones Biomedicas, Universidad Nacional Autonoma de Mexico, Campus Juriquilla, Boulevard Juriquilla 3001, C.P. 76230, A.P. 1-1010, Juriquilla, Qro. (Mexico); Departamento de Nanotecnologia, Centro de Fisica Aplicada y Tecnologia Avanzada, Universidad Nacional Autonoma de Mexico, Campus Juriquilla, Boulevard Juriquilla 3001, C.P. 76230, A.P. 1-1010, Juriquilla, Qro. (Mexico); Rodriguez-Garcia, Mario E. [Departamento de Nanotecnologia, Centro de Fisica Aplicada y Tecnologia Avanzada, Universidad Nacional Autonoma de Mexico, Campus Juriquilla, Boulevard Juriquilla 3001, C.P. 76230, A.P. 1-1010, Juriquilla, Qro. (Mexico)

2011-12-15T23:59:59.000Z

58

Hard-x-ray microscopy with Fresnel zone plates reaches 40 nm Rayleigh resolution  

SciTech Connect

Substantial improvements in the nanofabrication and characteristics of gold Fresnel zone plates yielded unprecedented resolution levels in hard-x-ray microscopy. Tests performed on a variety of specimens with 8-10 keV photons demonstrated a first-order lateral resolution below 40 nm based on the Rayleigh criterion. Combined with the use of a phase contrast technique, this makes it possible to view features in the 30 nm range; good-quality images can be obtained at video rate, down to 50 ms/frame. The important repercussions on materials science, nanotechnology, and the life sciences are discussed.

Chu, Y. S.; Yi, J. M.; De Carlo, F.; Shen, Q.; Lee, Wah-Keat [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Wu, H. J.; Wang, C. L.; Wang, J. Y.; Liu, C. J.; Wang, C. H. [Institute of Physics, Academia Sinica, Taipei 115, Taiwan (China); Wu, S. R.; Chien, C. C. [Institute of Physics, Academia Sinica, Taipei 115, Taiwan (China); Department of Engineering Science and System, National Tsing Hua University, Hsinchu 300, Taiwan (China); Hwu, Y. [Institute of Physics, Academia Sinica, Taipei 115, Taiwan (China); Department of Engineering Science and System, National Tsing Hua University, Hsinchu 300, Taiwan (China); Institute of Optoelectronic Sciences, National Taiwan Ocean University, Keelung 202, Taiwan (China); National Synchrotron Radiation Research Center, Hsinchu 300, Taiwan (China); Tkachuk, A.; Yun, W.; Feser, M. [Xradia Inc., 5052 Commercial Circle, Concord, California 94520 (United States); Liang, K. S. [National Synchrotron Radiation Research Center, Hsinchu 300, Taiwan (China); Yang, C. S. [Center for Nanomedicine, National Health Research Institutes, Miaoli 350, Taiwan (China); Je, J. H. [X-ray Imaging Center, Pohang University of Science and Technology, Pohang 790-784 (Korea, Republic of); Margaritondo, G. [Ecole Polytechnique Federale de Lausanne (EPFL), CH-1015 Lausanne (Switzerland)

2008-03-10T23:59:59.000Z

59

Study of hard disk and slider surfaces using X-ray photoemission electron microscopy and near-edge X-ray absorption fine structure spectroscopy  

SciTech Connect

X-ray Photo Emission Electron Microscopy (X-PEEM) and Near Edge X-ray Absorption Fine Structure (NEXAFS) spectroscopy were applied to study the properties of amorphous hard carbon overcoats on disks and sliders, and the properties of the lubricant. The modification of lubricants after performing thermal desorption studies was measured by NEXAFS, and the results are compared to the thermal desorption data. The study of lubricant degradation in wear tracks is described. Sliders were investigated before and after wear test, and the modification of the slider coating as well as the transfer of lubricant to the slider was studied. The studies show that the lubricant is altered chemically during the wear. Fluorine is removed and carboxyl groups are formed.

Anders, S.; Stammler, T. [Lawrence Berkeley National lab., CA (United States). Advanced Light Source Div.; Bhatia, C.S. [SSD/IBM, San Jose, CA (United States); Stoehr, J. [IBM Research Div., San Jose, CA (United States). Almaden Research Center; Fong, W.; Chen, C.Y.; Bogy, D.B. [Univ. of California, Berkeley, CA (United States)

1998-04-01T23:59:59.000Z

60

A soft x-ray transmission grating imaging-spectrometer for the National Ignition Facility  

SciTech Connect

A soft x-ray transmission grating spectrometer has been designed for use on high energy-density physics experiments at the National Ignition Facility (NIF); coupled to one of the NIF gated x-ray detectors (GXD) it records sixteen time-gated spectra between 250 and 1000eV with 100ps temporal resolution. The trade-off between spectral and spatial resolution leads to an optimized design for measurement of emission around the peak of a 100-300eV blackbody spectrum. Performance qualification results from the NIF, the Trident Laser Facility and VUV beamline at the National Synchrotron Light Source (NSLS), evidence a <100{micro}m spatial resolution in combination with a source-size limited spectral resolution that is <10eV at photon energies of 300eV.

Moore, A S; Guymer, T M; Kline, J L; Morton, J; Taccetti, M; Lanier, N E; Bentley, C; Workman, J; Peterson, B; Mussack, K; Cowan, J; Prasad, R; Richardson, M; Burns, S; Kalantar, D H; Benedetti, L R; Bell, P; Bradley, D; Hsing, W; Stevenson, M

2012-05-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

A soft x-ray transmission grating imaging-spectrometer for the National Ignition Facility  

SciTech Connect

A soft x-ray transmission grating spectrometer has been designed for use on high energy-density physics experiments at the National Ignition Facility (NIF); coupled to one of the NIF gated x-ray detectors it records 16 time-gated spectra between 250 and 1000 eV with 100 ps temporal resolution. The trade-off between spectral and spatial resolution leads to an optimized design for measurement of emission around the peak of a 100-300 eV blackbody spectrum. Performance qualification results from the NIF, the Trident Laser Facility and vacuum ultraviolet beamline at the National Synchrotron Light Source, evidence a <100 {mu}m spatial resolution in combination with a source-size limited spectral resolution that is <10 eV at photon energies of 300 eV.

Moore, A. S.; Guymer, T. M.; Morton, J.; Bentley, C.; Stevenson, M. [Directorate Science and Technology, AWE Aldermaston, Reading, RG7 4PR (United Kingdom); Kline, J. L.; Taccetti, M.; Lanier, N. E.; Workman, J.; Peterson, B.; Mussack, K.; Cowan, J. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Prasad, R.; Richardson, M.; Burns, S.; Kalantar, D. H.; Benedetti, L. R.; Bell, P.; Bradley, D.; Hsing, W. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551-0808 (United States)

2012-10-15T23:59:59.000Z

62

Fabrication of high-throughput critical-angle X-ray transmission gratings for wavelength-dispersive spectroscopy  

E-Print Network (OSTI)

The development of the critical-angle transmission (CAT) grating seeks both an order of magnitude improvement in the effective area, and a factor of three increase in the resolving power of future space-based, soft x-ray ...

Bruccoleri, Alexander Robert

2013-01-01T23:59:59.000Z

63

Directly correlated transmission electron microscopy and atom...  

NLE Websites -- All DOE Office Websites (Extended Search)

Directly correlated transmission electron microscopy and atom probe tomography of grain boundary oxidation in a Ni-Al binary Directly correlated transmission electron microscopy...

64

Comparison of SOFC Cathode Microstructure Quantified using X-ray Nanotomography and Focused Ion Beam - Scanning Electron Microscopy  

SciTech Connect

X-ray nanotomography and focused ion beam scanning electron microscopy (FIB?SEM) have been applied to investigate the complex 3D microstructure of solid oxide fuel cell (SOFC) electrodes at spatial resolutions of 45 nm and below. The application of near edge differential absorption for x-ray nanotomography and energy selected backscatter detection for FIB–SEM enable elemental mapping within the microstructure. Using these methods, non?destructive 3D x-ray imaging and FIB–SEM serial sectioning have been applied to compare three?dimensional elemental mapping of the LSM, YSZ, and pore phases in the SOFC cathode microstructure. The microstructural characterization of an SOFC cathode is reported based on these measurements. The results presented demonstrate the viability of x-ray nanotomography as a quantitative characterization technique and provide key insights into the SOFC cathode microstructure.

Nelson, George J.; Harris, William H.; Lombardo, Jeffrey J.; Izzo, Jr., John R.; Chiu, W. K. S.; Tanasini, Pietro; cantoni, Marco; Van herle, Jan; Comninellis, Christos; Andrews, Joy C.; Liu, Yijin; Pianetta, Piero; Chu, Yong

2011-01-01T23:59:59.000Z

65

Determination of the polarization state of x rays with the help of anomalous transmission  

SciTech Connect

Besides intensity and direction, the polarization of an electromagnetic wave provides characteristic information on the crossed medium. Here, we present two methods for the determination of the polarization state of x rays by polarizers based on anomalous transmission (Borrmann effect). Using a polarizer-analyzer setup, we have measured a polarization purity of less than 1.5?×?10{sup ?5}, three orders of magnitude better than obtained in earlier work. Using the analyzer crystal in multiple-beam case with slightly detuned azimuth, we show how the first three Stokes parameters can be determined with a single angular scan. Thus, polarization analyzers based on anomalous transmission make it possible to detect changes of the polarization in a range from degrees down to arcseconds.

Schulze, K. S., E-mail: kai.sven.schulze@uni-jena.de; Uschmann, I.; Förster, E. [Institut für Optik und Quantenelektronik, Friedrich-Schiller-Universität Jena, Max-Wien-Platz 1, D-07743 Jena (Germany); Helmholtz-Institut Jena, Fröbelstieg 3, D-07743 Jena (Germany); Marx, B.; Paulus, G. G. [Institut für Optik und Quantenelektronik, Friedrich-Schiller-Universität Jena, Max-Wien-Platz 1, D-07743 Jena (Germany); Stöhlker, T. [Helmholtz-Institut Jena, Fröbelstieg 3, D-07743 Jena (Germany)

2014-04-14T23:59:59.000Z

66

Spatial Gradients in Particle Reinforced Polymers Characterized by X-Ray Attenuation and Laser Confocal Microscopy  

SciTech Connect

The goal of this work is to develop techniques for measuring gradients in particle concentration within filled polymers, such as encapsulant. A high concentration of filler particles is added to such materials to tailor physical properties such as thermal expansion coefficient. Sedimentation and flow-induced migration of particles can produce concentration gradients that are most severe near material boundaries. Therefore, techniques for measuring local particle concentration should be accurate near boundaries. Particle gradients in an alumina-filled epoxy resin are measured with a spatial resolution of 0.2 mm using an x-ray beam attenuation technique, but an artifact related to the finite diameter of the beam reduces accuracy near the specimen's edge. Local particle concentration near an edge can be measured more reliably using microscopy coupled with image analysis. This is illustrated by measuring concentration profiles of glass particles having 40 {micro}m median diameter using images acquired by a confocal laser fluorescence microscope. The mean of the measured profiles of volume fraction agrees to better than 3% with the expected value, and the shape of the profiles agrees qualitatively with simple theory for sedimentation of monodisperse particles. Extending this microscopy technique to smaller, micron-scale filler particles used in encapsulant for microelectronic devices is illustrated by measuring the local concentration of an epoxy resin containing 0.41 volume fraction of silica.

LAGASSE,ROBERT R.; THOMPSON,KYLE R.

2000-06-12T23:59:59.000Z

67

A comparative study of X-ray tomographic microscopy on shales at different synchrotron facilities: ALS, APS and SLS  

Science Journals Connector (OSTI)

The 3D microstructure of shales is important to assess elastic anisotropic characteristics. In this study, microporosity and mineral components in two shale samples were investigated with X-ray tomographic microscopy at three synchrotron facilities: ALS, APS and SLS, and excellent agreement was observed.

Kanitpanyacharoen, W.

2012-11-22T23:59:59.000Z

68

Three-dimensional plastic response in polycrystalline copper via near-field high-energy X-ray diffraction microscopy  

Science Journals Connector (OSTI)

The evolution of the crystallographic orientation field in a polycrystalline sample of copper is mapped in three dimensions as tensile strain is applied. Using forward-modeling analysis of high-energy X-ray diffraction microscopy data, the ability to track intragranular orientation variations is demonstrated.

Li, S.F.

2012-10-25T23:59:59.000Z

69

X-ray microscopy: An emerging technique for semiconductor microstructure characterization  

SciTech Connect

The advent of third generation synchrotron radiation x-ray sources, such as the Advanced Light Source (ALS) at Berkeley have enabled the practical realization of a wide range of new techniques in which mature chemical or structural probes such as x-ray photoelectron spectroscopy (XPS) and x-ray diffraction are used in conjunction with microfocused x-ray beams. In this paper the characteristics of some of these new microscopes are described, particularly in reference to their applicability to the characterization of semiconductor microstructures.

Padmore, H.A.

1998-05-01T23:59:59.000Z

70

Signal-to-noise and radiation exposure considerations in conventional and diffraction x-ray microscopy  

Science Journals Connector (OSTI)

Using a signal-to-noise ratio estimation based on correlations between multiple simulated images, we compare the dose efficiency of two soft x-ray imaging systems: incoherent...

Huang, Xiaojing; Miao, Huijie; Steinbrener, Jan; Nelson, Johanna; Shapiro, David; Stewart, Andrew; Turner, Joshua; Jacobsen, Chris

2009-01-01T23:59:59.000Z

71

Characterization of thin film CCD filters on board the German astronomy satellite ABRIXAS by soft x-ray transmission measurements  

SciTech Connect

We have developed optical filters for the German X-ray astronomy satellite ABRIXAS (A BRoadband Imaging X-ray All Sky Survey)(1). Specific CCD's (2) will be used as detectors in the focal plane on board the observatory. Since these detectors are sensitive from the X-ray to the near infrared spectral range, X-ray observations require optical filters, which combine high transmittance for photon energies in the soft X-ray region and a high absorptance for ultraviolet and visible radiation. With respect to the mission goal in orbit a spectral transmission function is required attenuating radiation below photon energies of 10 eV by more than 7 orders of magnitude and transmitting soft X-ray photon energies above 1000 eV by more than 90 percent. This was realized by a 0.80 {mu}m thick polypropylene foil, which is coated with approximately 60 nm aluminum on both sides. The filters have an effective diameter of 73 mm without any support structure. Environmental tests have been performed and proved the filters to be resistant against sound pressure and vibrational load stresses during the launch of the spacecraft. Synchroton radiation was used to characterize the properties of the filters in the soft X-ray photon energy range 60 eVtransmission topography at discrete photon energies across the effective area, and present the resulting performance data.

Stephan, K.-H.; Braeuninger, H.; Haberl, F.; Predehl, P. [Max-Planck-Institut fuer extraterrestrische Physik, 85748 Garching (Germany); Maier, H. J. [Sektion Physik, Ludwig-Maximilians-Universitaet Muenchen, 85748 Garching (Germany); Friedrich, J. [Institut fuer Angewandte Physik, Heinrich Heine Universitaet Duesseldorf, 40255 Duesseldorf (Germany); Schmitz, D.; Scholze, F.; Ulm, G. [Physikalisch-Technische Bundesanstalt, 10587 Berlin (Germany)

1999-06-10T23:59:59.000Z

72

SCANNING ELECTRON MICROSCOPY AND X-RAY DIFFRACTION ANALYSIS OF TANK 18 SAMPLES  

SciTech Connect

The F-Area Tank Farm (FTF) Performance Assessment (PA) utilizes waste speciation in the waste release model used in the FTF fate and transport modeling. The waste release modeling associated with the residual plutonium in Tank 18 has been identified as a primary contributor to the Tank 18 dose uncertainty. In order to reduce the uncertainty related to plutonium in Tank 18, a better understanding of the plutonium speciation in the Tank 18 waste (including the oxidation state and stoichiometry) is desired. Savannah River National Laboratory (SRNL) utilized Scanning Electron Microscopy (SEM) and X-ray Diffraction (XRD) to analyze Tank 18 samples to provide information on the speciation of plutonium in the waste material. XRD analysis of the Tank 18 samples did not identify any plutonium mineral phases in the samples. These indicates the crystalline mineral phases of plutonium are below the detection limits of the XRD method or that the plutonium phase(s) lack long range order and are present as amorphous or microcrystalline solids. SEM analysis of the Tank 18 samples did locate particles containing plutonium. The plutonium was found as small particles, usually <1 {micro}m but ranging up to several micrometers in diameter, associated with particles of an iron matrix and at low concentration in other elemental matrices. This suggests the plutonium has an affinity for the iron matrix. Qualitatively, the particles of plutonium found in the SEM analysis do not appear to account for all of the plutonium in the sample based on concentrations determined from the chemical analysis of the Tank 18 samples. This suggests that plutonium is also distributed throughout the solids in low concentrations.

Hay, M.; O'Rourke, P.; Ajo, H.

2012-03-08T23:59:59.000Z

73

Low-energy X-ray fluorescence microscopy opening new opportunities for bio-related research  

Science Journals Connector (OSTI)

...and (g) zinc. Photon energy: 1467 eV. Dwell time...magnesium. Excitation photon energy 1686 eV. Dwell time per...Development of a low-energy X-ray fluorescence system...Spence), pp. 835-926. New York, NY: Springer. ( doi...

2009-01-01T23:59:59.000Z

74

Application of electron microscopy and x-ray structural analysis for the determination of sizes of structural elements in nanocrystalline materials (Review)  

Science Journals Connector (OSTI)

The possibilities of determining the sizes of structural elements in various nanocrystalline materials by electron microscopy and X-ray structural analysis are analyzed. It is shown that these sizes depend on ...

Yu. D. Yagodkin; S. V. Dobatkin

2008-12-01T23:59:59.000Z

75

High-energy x-ray microscopy of laser-fusion plasmas at the National Ignition Facility  

SciTech Connect

Multi-keV x-ray microscopy will be an important laser-produced plasma diagnostic at future megajoule facilities such as the National Ignition Facility (NIF).In preparation for the construction of this facility, we have investigated several instrumentation options in detail, and we conclude that near normal incidence single spherical or toroidal crystals may offer the best general solution for high-energy x-raymicroscopy at NIF and at similar large facilities. Kirkpatrick-Baez microscopes using multi-layer mirrors may also be good secondary options, particularly if apertures are used to increase the band-width limited field of view.

Koch, J.A.; Landen, O.L.; Hammel, B.A. [and others

1997-08-26T23:59:59.000Z

76

A liquid densitometer with improved sensitivity employing X-ray transmission techniques  

E-Print Network (OSTI)

A CKNOWLEDGEMENTS LIST OF FIGURES I. INTRODUCTION II. DETERMINATION OFLIQUID DENSITY WITH RADIOISOTOPES Selection of Technique and Radiation Type 3 Selection of Detection System Theory of Density Determinsiion by Radiation Trensmission... Selection of Radioisotope III. DETECTION OF LOW ENERGY X-RAYS IV. DESIGN OF DENSITOMETER 13 18 Design Criteria Density Measuring Cell V. CALIBRATION'OF THE DENSITOMETER VI. RESULTS VII. SUMMARY AND CONCLUSIONS APPENDIX I. APPENDIX II. APPENDIX...

Reuscher, Jon Arthur

1962-01-01T23:59:59.000Z

77

Center for X-Ray Optics, 1992  

SciTech Connect

This report discusses the following topics: Center for X-Ray Optics; Soft X-Ray Imaging wit Zone Plate Lenses; Biological X-Ray microscopy; Extreme Ultraviolet Lithography for Nanoelectronic Pattern Transfer; Multilayer Reflective Optics; EUV/Soft X-ray Reflectometer; Photoemission Microscopy with Reflective Optics; Spectroscopy with Soft X-Rays; Hard X-Ray Microprobe; Coronary Angiography; and Atomic Scattering Factors.

Not Available

1993-08-01T23:59:59.000Z

78

TiO2 Nanoparticles as a Soft X-ray Molecular Probe  

SciTech Connect

With the emergence of soft x-ray techniques for imaging cells, there is a pressing need to develop protein localization probes that can be unambiguously identified within the region of x-ray spectrum used for imaging. TiO2 nanocrystal colloids, which have a strong absorption cross-section within the "water-window" region of x-rays, areideally suited as soft x-ray microscopy probes. To demonstrate their efficacy, TiO2-streptavidin nanoconjugates were prepared and subsequently labeled microtubules polymerized from biotinylated tubulin. The microtubules were imaged using scanning transmission x-ray microscopy (STXM), and the TiO2 nanoparticle tags were specifically identified using x-ray absorption near edge spectroscopy (XANES). These experiments demonstrate that TiO2 nanoparticles are potential probes for protein localization analyses using soft x-ray microscopy.

Larabell, Carolyn; Ashcroft, Jared M.; Gu, Weiwei; Zhang, Tierui; Hughes, Steven M.; Hartman, Keith B.; Hofmann, Cristina; Kanaras, Antonios G.; Kilcoyne, David A.; Le Gros, Mark; Yin, Yadong; Alivisatos, A. Paul; Larabell, Carolyn A.

2007-06-30T23:59:59.000Z

79

In-situ Transmission Electron Microscopy and Spectroscopy Studies...  

NLE Websites -- All DOE Office Websites (Extended Search)

Transmission Electron Microscopy and Spectroscopy Studies of Interfaces in Li-ion Batteries: Challenges and In-situ Transmission Electron Microscopy and Spectroscopy Studies of...

80

Research and Design of a Sample Heater for Beam Line 6-2c Transmission X-ray Microscope  

SciTech Connect

There exists a need for environmental control of samples to be imaged by the Transmission X-Ray Microscope (TXM) at the SSRLs Beam Line 6-2c. In order to observe heat-driven chemical or morphological changes that normally occur in situ, microscopes require an additional component that effectively heats a given sample without heating any of the microscope elements. The confinement of the heat and other concerns about the heaters integrity limit which type of heater is appropriate for the TXM. The bulk of this research project entails researching different heating methods used previously in microscopes, but also in other industrial applications, with the goal of determining the best-fitting method, and finally in designing a preliminary sample heater.

Policht, Veronica; /Loyola U., Chicago /SLAC

2012-08-27T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


81

X-ray laser  

DOE Patents (OSTI)

An X-ray laser (10) that lases between the K edges of carbon and oxygen, i.e. between 44 and 23 Angstroms, is provided. The laser comprises a silicon (12) and dysprosium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state nickel-like dysprosium ions (34) are resonantly photo-pumped to their upper X-ray laser state by line emission from hydrogen-like silicon ions (32). The novel X-ray laser should prove especially useful for the microscopy of biological specimens.

Nilsen, Joseph (Livermore, CA)

1991-01-01T23:59:59.000Z

82

Humidity-controlled preparation of frozen-hydrated biological samples for cryogenic coherent x-ray diffraction microscopy  

SciTech Connect

Coherent x-ray diffraction microscopy (CXDM) has the potential to visualize the structures of micro- to sub-micrometer-sized biological particles, such as cells and organelles, at high resolution. Toward advancing structural studies on the functional states of such particles, here, we developed a system for the preparation of frozen-hydrated biological samples for cryogenic CXDM experiments. The system, which comprised a moist air generator, microscope, micro-injector mounted on a micromanipulator, custom-made sample preparation chamber, and flash-cooling device, allowed for the manipulation of sample particles in the relative humidity range of 20%-94%rh at 293 K to maintain their hydrated and functional states. Here, we report the details of the system and the operation procedure, including its application to the preparation of a frozen-hydrated chloroplast sample. Sample quality was evaluated through a cryogenic CXDM experiment conducted at BL29XUL of SPring-8. Taking the performance of the system and the quality of the sample, the system was suitable to prepare frozen-hydrated biological samples for cryogenic CXDM experiments.

Takayama, Yuki; Nakasako, Masayoshi [Department of Physics, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Kanagawa 223-8522 (Japan); RIKEN Harima Institute/SPring-8, 1-1-1 Kouto, Mikaduki, Sayo, Hyogo 679-5148 (Japan)

2012-05-15T23:59:59.000Z

83

Investigation of metal dusting mechanism in Fe-base alloys using Raman spectroscopy, x-ray diffraction, and electron microscopy.  

SciTech Connect

The metal-dusting phenomenon, which is a metal loss process that occurs in hot reactive gases, was investigated in iron and certain iron-base alloys by Raman scattering, X-ray diffraction (XRD), and scanning-electron microscopy (SEM). Coke from metal dusting exhibits six Raman bands at 1330(D band), 1580(G band), 1617, 2685, 3920, and 3235 cm-1. The bandwidths and the relative intensities of the 1330 and 1580 cm-1 bands are related to the crystallinity and defect structure of the coke. Both Raman and XRD analyses suggest that the metal-dusting process influences the catalytic crystallization of carbon. A new mechanism of metal dusting is, therefore, proposed, based on the premise that coke cannot crystallize well by deposition from carburizing gases at low temperature without catalytic activation because of its strong C-C bonds and high melting temperature. Cementite or iron participates in the coke-crystallizing process in a manner that tends to improve the crystallinity of the coke. At the same time, fine iron or cementite particles are liberated from the pure metal or alloys.

Zeng, Z.; Natesan, K.; Maroni, V. A.

2002-08-01T23:59:59.000Z

84

A new Scanning Transmission X-ray Microscope at the ALS for operation up to 2500eV  

SciTech Connect

We report on the design and construction of a higher energy Scanning Transmission X-ray Microscope on a new bend magnet beam line at the Advanced Light Source. Previously we have operated such an instrument on a bend magnet for C, N and O 1s NEXAFS spectroscopy. The new instrument will have similar performance at higher energies up to and including the S 1s edge at 2472eV. A new microscope configuration is planned. A more open geometry will allow a fluorescence detector to count emitted photons from the front surface of the sample. There will be a capability for zone plate scanning in addition to the more conventional sample scanning mode. This will add the capability for imaging a massive sample at high resolution over a limited field of view, so that heavy reaction cells may be used to study processes in-situ, exploiting the longer photon attenuation length and the longer zone plate working distances available at higher photon energy. The energy range will extend down to include the C1s edge at 300eV, to allow high energy NEXAFS microscopic studies to correlate with the imaging of organics in the same sample region of interest.

Kilcoyne, David; Ade, Harald; Attwood, David; Hitchcock, Adam; McKean, Pat; Mitchell, Gary; Monteiro, Paulo; Tyliszczak, Tolek; Warwick, Tony

2010-01-31T23:59:59.000Z

85

X-ray fluorescence microscopy allows geochemists to map the distributions of many different elements simultaneously in  

E-Print Network (OSTI)

molecular and atomic orbitals. Clorg compounds display discrete absorption maxima corresponding to 1s-ray absorption spectroscopy is highly sensitive to the bonding state of Cl, allowing distinctions to be drawn procedures. The dramatic increase in X-ray absorption around 2,822 eV (Cl K-absorption edge

Duffy, Thomas S.

86

TRANSMISSION ELECTRON MICROSCOPY OF WEAKLY DEFORMED ALKALI HALIDE CRYSTALS  

E-Print Network (OSTI)

377 TRANSMISSION ELECTRON MICROSCOPY OF WEAKLY DEFORMED ALKALI HALIDE CRYSTALS H. STRUNK Max'importance croissante du durcissement de la solution solide. Abstract. 2014 Transmission electron microscopy (TEM Abstracts 7j66 - 7 I' 1. Introduction. - It is only some years ago that transmission electron microscopy

Boyer, Edmond

87

X-ray Imaging Workshop  

NLE Websites -- All DOE Office Websites (Extended Search)

Imaging and Spectro-microscopy: Imaging and Spectro-microscopy: the Present and the Future Stanford Synchrotron Radiation Laboratory October 8-9, 2002 Organizers: John Miao & Keith Hodgson A workshop on "X-ray Imaging and Spectro-microscopy: the Present and the Future" was held on October 8-9, 2002. This workshop, organized by John Miao (SSRL) and Keith Hodgson (SSRL) provided a forum to discuss the scientific applications of a variety of imaging and spectro-microscopic techniques, including photoemission electron microscopy (PEEM), angle resolved photoemission spectroscopy (ARPES), coherent diffraction imaging, x-ray microscopy, micro-tomography, holographic imaging, and x-ray micro-probe. Twelve invited speakers discussed the important scientific applications of these techniques, and also predicted the future scientific directions with the advance of instrumentation and x-ray sources. The workshop was well attended with over fifty registered attendees.

88

In situ transmission electron microscopy analysis of conductive filament during solid electrolyte resistance switching  

SciTech Connect

An in situ transmission electron microscopy (TEM) analysis of a solid electrolyte, Cu-GeS, during resistance switching is reported. Real-time observations of the filament formation and disappearance process were performed in the TEM instrument and the conductive-filament-formation model was confirmed experimentally. Narrow conductive filaments were formed corresponding to resistance switching from high- to low-resistance states. When the resistance changed to high-resistance state, the filament disappeared. It was also confirmed by use of selected area diffractometry and energy-dispersive x-ray spectroscopy that the conductive filament was made of nanocrystals composed mainly of Cu.

Fujii, Takashi; Arita, Masashi; Takahashi, Yasuo [Graduate School of Information Science and Technology, Hokkaido University, Sapporo 060-0814 (Japan); Fujiwara, Ichiro [Semiconductor Technology Academic Research Center, 3-17-2 Shinyokohama, Kohoku-ku, Yokohama 222-0033 (Japan)

2011-05-23T23:59:59.000Z

89

Scanning Transmission X-ray Microscopy: Applications in Atmospheric Aerosol Research  

E-Print Network (OSTI)

related to the total atomic absorption cross section, ? A (number. Tabulations of atomic absorption cross sections areC are the mass absorption coefficients and atomic masses for

Moffet, Ryan C.

2011-01-01T23:59:59.000Z

90

New Developments in Transmission Electron Microscopy for Nanotechnology**  

E-Print Network (OSTI)

New Developments in Transmission Electron Microscopy for Nanotechnology** By Zhong Lin Wang* 1. Electron Microscopy and Nanotechnology Nanotechnology, as an international initiative for science manufacturing are the foundation of nanotechnology. Tracking the historical background of why nanotechnology

Wang, Zhong L.

91

High-resolution, high-transmission soft x-ray spectrometer for the study of biological samples  

SciTech Connect

We present a variable line-space grating spectrometer for soft x-rays that covers the photon energy range between 130 and 650 eV. The optical design is based on the Hettrick-Underwood principle and tailored to synchrotron-based studies of radiation-sensitive biological samples. The spectrometer is able to record the entire spectral range in one shot, i.e., without any mechanical motion, at a resolving power of 1200 or better. Despite its slitless design, such a resolving power can be achieved for a source spot as large as 30x3000 mu m2, which is important for keeping beam damage effects in radiation-sensitive samples low. The high spectrometer efficiency allows recording of comprehensive two-dimensional resonant inelastic soft x-ray scattering (RIXS) maps with good statistics within several minutes. This is exemplarily demonstrated for a RIXS map of highly oriented pyrolytic graphite, which was taken within 10 min.

Fuchs, Oliver; Weinhardt, L.; Blum, M.; Weigand, M.; Umbach, E.; Bar, M.; Heske, Clemens; Denlinger, Jonathan; Chuang, Y.-D.; McKinney, Wayne; Hussain, Zahid; Gullikson, Eric; Jones, M.; Batson, Phil; Nelles, B.; Follath, R.

2009-03-09T23:59:59.000Z

92

Transmission Electron Microscopy Study of Eu-Doped Y2O3 Nanosheets and Nanotubes  

SciTech Connect

A hydrothermal method was used to synthesize high-purity Eu-doped Y{sub 2}O{sub 3} nanosheets and nanotubes with an approximate molar ratio of (0.1):(1.0) for Eu:Y. High-resolution transmission electron microscopy, energy dispersive X-ray spectroscopy analysis and synchrotron X-ray diffraction were used to characterize these nanomaterials. A body-centered cubic structure was confirmed for the nanotubes. The lattice parameter of Eu-doped Y{sub 2}O{sub 3} nanotubes were 0.12% larger as compared to that of pure Y{sub 2}O{sub 3} which was attributed to the larger ionic radius of Eu{sup 3+} (0.947 {angstrom}) than that of Y{sup 3+} (0.900 {angstrom}). The nanosheets had a similar structure. Nanosheets of approximate dimensions 600 to 800 nm length and width were obtained using a slightly lower pH value, and they were highly textured. The high resolution transmission electron microscopy images showed that the nanotubes are fully crystalline. The nanotubes were typically 1.5-3 {micro}m in length and 50-200 nm in diameter. Using a pH value of approximately 10, stable nanotubes were obtained. It is anticipated that nanosheets might have rolled to form more stable nanotubes.

H Sun; T Chaudhuri; E Kenik; H Zhu; Y Ma

2011-12-31T23:59:59.000Z

93

Soft x-ray laser microscope  

SciTech Connect

The program consisted of two phases (Phase I and Phase II). The goal of the Phase I (first year program) was to design and construct the Soft X-ray Laser Contact Microscope. Such microscope was constructed and adapted to PPL's 18.2nm soft X-ray Laser (SXL), which in turn was modified and prepared for microscopy experiments. Investigation of the photoresist response to 18.2nm laser radiation and transmissivity of 0.1m thick silicion-nitride (Si[sub 3]N[sub 4]) windows were important initial works. The goal of the first year of Phase II was to construct X-ray contact microscope in combination with existing optical phase microscope, already used by biologists. In the second year of Phase II study of dehydrated Horeseshoe Crab and Hela cancer cells were performed with COXRALM. Also during Phase II, the Imaging X-Ray Laser Microscope (IXRALM) was designed and constructed. This paper describes the development of each of the microscopes and their application for research.

Suckewer, P.I.

1990-10-01T23:59:59.000Z

94

Coal Combustion Fly Ash Characterization: Electron Spectroscopy for Chemical Analysis, Energy Dispersive X-ray Analysis, and Scanning Electron Microscopy  

Science Journals Connector (OSTI)

The surface and bulk properties of five samples of fly ash have been examined by electron spectroscopy for chemical analysis (ESCA), scanning electron microscopy (SEM) and energy...

Rothenberg, S J; Denee, P; Holloway, P

1980-01-01T23:59:59.000Z

95

Direct comparison between X-ray nanotomography and scanning electron microscopy for the microstructure characterization of a solid oxide fuel cell anode  

SciTech Connect

X-ray computed nanotomography (nano-CT) and scanning electron microscopy (SEM) have been applied to characterize the microstructure of a Solid Oxide Fuel Cell (SOFC) anode. A direct comparison between the results of both methods is conducted on the same region of the microstructure to assess the spatial resolution of the nano-CT microstructure, SEM being taken as a reference. A registration procedure is proposed to find out the position of the SEM image within the nano-CT volume. It involves a second SEM observation, which is taken along an orthogonal direction and gives an estimate reference SEM image position, which is then refined by an automated optimization procedure. This enables an unbiased comparison between the cell porosity morphologies provided by both methods. In the present experiment, nano-CT is shown to underestimate the number of pores smaller than 1 ?m and overestimate the size of the pores larger than 1.5 ?m. - Highlights: ? X-ray computed nanotomography (nano-CT) and SEM are used to characterize an SOFC anode. ? A methodology is proposed to compare the nano-CT and SEM data on the same region. ? The spatial resolution of the nano-CT data is assessed from that comparison.

Quey, R., E-mail: quey@emse.fr [CEA, LETI, MINATEC Campus, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France); École des Mines de Saint-Étienne, CNRS UMR 5307, 158 cours Fauriel, 42023 Saint-Étienne, Cedex 2 (France); Suhonen, H., E-mail: heikki.suhonen@esrf.fr [European Synchrotron Radiation Facility (ESRF), 6 Rue Jules Horowitz BP 220, 38043 Grenoble (France); Laurencin, J., E-mail: jerome.laurencin@cea.fr [CEA-Liten, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France); Cloetens, P., E-mail: peter.cloetens@esrf.fr [European Synchrotron Radiation Facility (ESRF), 6 Rue Jules Horowitz BP 220, 38043 Grenoble (France); Bleuet, P., E-mail: pierre.bleuet@cea.fr [CEA, LETI, MINATEC Campus, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France)

2013-04-15T23:59:59.000Z

96

Electronic structures and bonding properties of chlorine-treated nitrogenated carbon nanotubes: X-ray absorption and scanning photoelectron microscopy studies  

SciTech Connect

The electronic and bonding properties of nitrogenated carbon nanotubes (N-CNTs) exposed to chlorine plasma were investigated using C and N K-edge x-ray absorption near-edge structure (XANES) and scanning photoelectron microscopy (SPEM). The C and N K-edge XANES spectra of chlorine-treated N-CNTs consistently reveal the formation of pyridinelike N-CNTs by the observation of 1s{yields}{pi}*(e{sub 2u}) antibonding and 1s{yields}{pi}*(b{sub 2g}) bonding states. The valence-band photoemission spectra obtained from SPEM images indicate that chlorination of the nanotubes enhances the C-N bonding. First-principles calculations of the partial densities of states in conjunction with C K-edge XANES data identify the presence of C-Cl bonding in chlorine treated N-CNTs.

Ray, S. C.; Pao, C. W.; Tsai, H. M.; Chiou, J. W.; Pong, W. F.; Chen, C. W.; Tsai, M.-H.; Papakonstantinou, P.; Chen, L. C.; Chen, K. H.; Graham, W. G. [Department of Physics, Tamkang University, Tamsui 251, Taiwan (China); Department of Materials Science and Engineering, National Taiwan University, Taipei 106, Taiwan (China); Department of Physics, National Sun Yat-Sen University, Kaohsiung 804, Taiwan (China); NRI, School of Electrical and Mechanical Engineering, University of Ulster at Jordanstown, Newtownabbey, County Antrim BT37OQB, Northern Ireland (United Kingdom); Center for Condensed Matter Sciences, National Taiwan University, Taipei 106, Taiwan (China); Institute of Atomic and Molecular Sciences, Academia Sinica, Taipei 106, Taiwan (China); Department of Physics and Astronomy, Queens University of Belfast, Belfast, Antrim BT71NN, Northern Ireland (United Kingdom)

2007-05-07T23:59:59.000Z

97

The Reactivity and Structural Dynamics of Supported Metal Nanoclusters Using Electron Microscopy, in situ X-Ray Spectroscopy, Electronic Structure Theories, and Molecular Dynamics Simulations.  

SciTech Connect

The distinguishing feature of our collaborative program of study is the focus it brings to emergent phenomena originating from the unique structural/electronic environments found in nanoscale materials. We exploit and develop frontier methods of atomic-scale materials characterization based on electron microscopy (Yang) and synchrotron X-ray absorption spectroscopy (Frenkel) that are in turn coupled innately with advanced first principles theory and methods of computational modeling (Johnson). In the past year we have made significant experimental advances that have led to important new understandings of the structural dynamics of what are unquestionably the most important classes of heterogeneous catalysts—the materials used to both produce and mitigate the consequences of the use of liquid hydrocarbon fuels.

Judith C. Yang; Ralph G. Nuzzo, Duane Johnson, Anatoly Frenkel

2008-07-01T23:59:59.000Z

98

Imaging and microanalysis of thin ionomer layers by scanning transmission electron microscopy  

SciTech Connect

Improved conditions for imaging and spectroscopic mapping of thin perfluorosulfonic acid (PFSA) ionomer layers in fuel cell electrodes by scanning transmission electron microscopy (STEM) have been investigated. These conditions are first identified on model systems of Nafion ionomer-coated nanostructured thin films and nanoporous Si. The optimized conditions are then applied in a quantitative study of the ionomer through-layer loading for two typical electrode catalyst coatings using electron energy loss and energy dispersive X-ray spectroscopy in the transmission electron microscope. The e-beam induced damage to the perfluorosulfonic acid (PFSA) ionomer is quantified by following the fluorine mass loss with electron exposure and is then mitigated by a few orders of magnitude using cryogenic specimen cooling and a higher incident electron voltage. Multivariate statistical analysis is also applied to the analysis of spectrum images for data denoising and unbiased separation of independent components related to the catalyst, ionomer, and support.

Cullen, David A [ORNL; Koestner, Roland [General Motors Corporation; Kukreja, Ratan [General Motors Corporation; Minko, Sergiy [Clarkson University, Potsdam, NY; Trotsenko, Oleksandr [Clarkson University, Potsdam, NY; Tokarev, Alexander V [ORNL; Guetaz, Laure [French Atomic Energy Commission (CEA), Grenoble; Meyer III, Harry M [ORNL; Parish, Chad M [ORNL; More, Karren Leslie [ORNL

2014-01-01T23:59:59.000Z

99

Sorption of cadmium on humic acid: Mechanistic and kinetic studies with atomic force microscopy and X-ray  

E-Print Network (OSTI)

Sorption of cadmium on humic acid: Mechanistic and kinetic studies with atomic force microscopy, Upton, New York 593-5000 USA. Liu, C., Frenkel, A. I., Vairavamurthy, A. and Huang, P. M. 2001. Sorption of Cd sorption by HAs, especially those pertaining to the surface features and structure of the Cd

Frenkel, Anatoly

100

High-resolution, high-transmission soft x-ray spectrometer for the study of biological samples  

SciTech Connect

We present a variable line-space grating spectrometer for soft s-rays that coverst the photon energy range between 130 and 650 eV. The optical design is based on the Hettrick-Underwood principle and tailored to synchrotron-based studies of radiation-sensitive biological samples. The spectrometer is able to record the entire spectral range in one shot, i.e., without any mechanical motion, at a resolving power of 1200 or better. Despite is slitless design, such a resolving power can be achieved for a source spot as large as (30 x 3000) micrometers squared, which is important for keeping beam damage effects in radiation-sensitive samples low. The high spectrometer efficiency allows recording of comprehensive two-dimensional resonant inelastic soft x-ray scatters (RIXS) maps with good statistics within several minutes. This is exemplarily demonstrated for a RIXS map of highly oriented pyrolytic graphite, which was taken with 10 min.

Fuchs, Oliver; Weinhardt, L.; Blum, M.; Welgand, M.; Umbach, E.; Bar, M.; Heske, C.; Denlinger, J.; Chuang, Y.-D.; McKinney, W.; Hussain, Z.; Gullikson, E.; Jones, M.; Batson, P.; Nelles, B.; Follath, R.

2009-06-11T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

Instrument Series: Microscopy Environmental Transmission Electron Microscope  

NLE Websites -- All DOE Office Websites (Extended Search)

Environmental Transmission Environmental Transmission Electron Microscope EMSL's environmental transmission electron microscope (ETEM) provides in situ capabilities that enable atomic-resolution imaging and spectroscopic studies of materials under dynamic operating conditions. In contrast to traditional operation of TEM under high vacuum, EMSL's ETEM uniquely allows imaging within high- temperature and gas environments-with a gas pressure up to 20 Torr. With a spherical aberration corrector for the objective lens, the ETEM captures atomic-level processes as they occur, enabling vital research across a range of scientific fields. Research Applications Chemical science and engineering - providing in situ observation of catalytic processes with atomic-level resolution Materials science and engineering - allowing

102

Instrument Series: Microscopy Aberration-Corrected Scanning/Transmission  

NLE Websites -- All DOE Office Websites (Extended Search)

Aberration-Corrected Aberration-Corrected Scanning/Transmission Electron Microscope EMSL's aberration-corrected Titan 80-300(tm) scanning/transmission electron microscope (S/TEM) provides high-resolution imaging with sub-angstrom resolution and spectroscopic capabilities. This state-of-the-art instrument is equipped with a Schottky field-emission electron source, an electron gun monochromator, CEOS hexapole spherical aberration corrector for the probe-forming lens, high-angle annular dark field (HAADF) detector, an X-ray spectrometer (EDS), and a high-resolution Gatan Imaging Filter (GIF). The selection of electron energy between 80 kV and 300 kV enables optimized imaging for a variety of samples, including electron beam sensitive materials. Research Applications

103

Advances in cryogenic transmission electron microscopy for the characterization of dynamic self-assembling nanostructures  

Science Journals Connector (OSTI)

Elucidating the structural information of nanoscale materials in their solvent-exposed state is crucial, as a result, cryogenic transmission electron microscopy (cryo-TEM) has become an increasingly popular technique in the materials science, chemistry, and biology communities. Cryo-TEM provides a method to directly visualize the specimen structure in a solution-state through a thin film of vitrified solvent. This technique complements X-ray, neutron, and light scattering methods that probe the statistical average of all species present; furthermore, cryo-TEM can be used to observe changes in structure over time. In the area of self-assembly, this tool has been particularly powerful for the characterization of natural and synthetic small molecule assemblies, as well as hybrid organic–inorganic composites. In this review, we discuss recent advances in cryogenic TEM in the context of self-assembling systems with emphasis on characterization of transitions observed in response to external stimuli.

Christina J. Newcomb; Tyson J. Moyer; Sungsoo S. Lee; Samuel I. Stupp

2012-01-01T23:59:59.000Z

104

X-ray lithography using holographic images  

DOE Patents (OSTI)

A non-contact X-ray projection lithography method for producing a desired X-ray image on a selected surface of an X-ray-sensitive material, such as photoresist material on a wafer, the desired X-ray image having image minimum linewidths as small as 0.063 .mu.m, or even smaller. A hologram and its position are determined that will produce the desired image on the selected surface when the hologram is irradiated with X-rays from a suitably monochromatic X-ray source of a selected wavelength .lambda.. On-axis X-ray transmission through, or off-axis X-ray reflection from, a hologram may be used here, with very different requirements for monochromaticity, flux and brightness of the X-ray source. For reasonable penetration of photoresist materials by X-rays produced by the X-ray source, the wavelength X, is preferably chosen to be no more than 13.5 nm in one embodiment and more preferably is chosen in the range 1-5 nm in the other embodiment. A lower limit on linewidth is set by the linewidth of available microstructure writing devices, such as an electron beam.

Howells, Malcolm R. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1995-01-01T23:59:59.000Z

105

Elemental relationships in rock varnish as seen with SEM/EDX (scanning electron microscopy/energy dispersive x-ray) elemental line profiling  

SciTech Connect

The heterogeneous nature of rock varnish requires a thorough survey of elemental and mineralogic compositions before relating chemical variability of rock varnish to past geochemical environments. Elemental relationships in rock varnish can be examined using scanning electron microscopy (SEM) in conjunction with an elemental line profiling routine using semi-quantitative, energy dispersive x-ray (EDX) analysis. Results of SEM/EDX analysis suggest: variations in cation concentrations used in varnish cation ratio dating relate more specifically to variations in detritus within the varnish than to element mobility as defined by weathering indices; Mn concentration rather than Mn:Fe ratios may be a more appropriate indicator of paleoclimatic fluctuations; and the Mn-oxide phase existing in varnish is most likely a Ba-enriched phase rather than birnessite. Element line profiling offers great potential for gaining insights into geochemical processes affecting the deposition and diagenesis of rock varnish and for testing hypotheses relating to its chemical variability. 27 refs., 9 figs.

Raymond, R. Jr.; Reneau, S.L.; Harrington, C.D.

1990-01-01T23:59:59.000Z

106

Scanning Transmission Electron Microscopy Investigations of Complex Oxides  

NLE Websites -- All DOE Office Websites (Extended Search)

Scanning Transmission Electron Microscopy Investigations of Complex Oxides Scanning Transmission Electron Microscopy Investigations of Complex Oxides Monday, May 23, 2011 - 3:30pm SSRL Conference room 137-322 Professor Tom Vogt, NanoCenter & Department of Chemistry, University of South Carolina High-Angle-Annular-Dark-Field/Scanning Transmission Electron Microscopy (HAADF/STEM) is a technique uniquely suited for detailed studies of the structure and composition of complex oxides. The HAADF detector collects electrons which have interact inelastically with the potentials of the atoms in the specimen and therefore resembles the better known Z2 (Z is atomic number) Rutherford scattering. One class of important catalysts consists of bronzes based on pentagonal {Mo6O21} building units; these include Mo5O14 and Mo17O47. In the last 20 years, new materials doped with

107

Overview of the program on soft x-ray lasers and their applications at Princeton  

SciTech Connect

In the last several years, rapid progress in the development of soft x-ray lasers (SXL) has been observed at a number of laboratories worldwide. Although SXLs are very young'' devices they have already been used for microscopy and holography, and new ideas emerging for broader application of SXLs to microscopy, holography and lithography. This paper describes the work at Princeton University on the development of a soft x-ray imaging transmission microscopy using a SXL as a radiation source and work on the development of a novel soft x-ray reflection microscope and its application to biological cell studies and lithography. Progress in the development of a photopumped VUV laser (60 nm), and programs for the development of a small scale SXL and for the application of a powerful subpicosecond KrF laser system are also discussed. 35 refs., 9 figs., 1 tab.

Suckewer, S.; Ilcisin, K. (Princeton Univ., NJ (USA). Plasma Physics Lab. Princeton Univ., NJ (USA). Dept. of Mechanical and Aerospace Engineering)

1991-05-01T23:59:59.000Z

108

Correlation between Charge State of Insulating NaCl Surfaces and Ionic Mobility Induced by Water Adsorption: A Combined Ambient Pressure X-ray Photoelectron Spectroscopy and Scanning Force Microscopy Study  

SciTech Connect

In situ ambient pressure X-ray photoelectron spectroscopy (APPES) and scanning force microscopy were used to characterize the surface discharge induced by water layers grown on (001) surfaces of sodium chloride single crystals. The APPES studies show that both kinetic energy (KE) and full width at half-maximum (FWHM) of the Na 2s and Cl 2p core level peaks, monitored as a function of relative humidity (RH), mimic surface conductivity curves measured using scanning force microscopy. The KE position and FWHM of the core level peaks therefore are directly related to the solvation and diffusion of ions at the NaCl(100) surface upon adsorption of water.

Verdaguer, Albert; Jose Segura, Juan; Fraxedas, Jordi; Bluhm, Hendrik; Salmeron, Miquel

2008-09-03T23:59:59.000Z

109

Spectroscopic ellipsometric modeling of a Bi–Te–Se write layer of an optical data storage device as guided by atomic force microscopy, scanning electron microscopy, and X-ray diffraction  

Science Journals Connector (OSTI)

Abstract Conventional magnetic tape is the most widely used medium for archival data storage. However, data stored on it need to be migrated every ca. 5 years. Recently, optical discs that store information for hundreds, or even more than 1000 years, have been introduced to the market. We recently proposed that technology in these optical discs be used to make an optical tape that would show greater permanence than its magnetic counterpart. Here we provide a detailed optical characterization of a sputtered thin film of bismuth, tellurium, and selenium (BTS) that is a proposed data storage layer for these devices. The methodology described herein should be useful in the future development of related materials. Spectroscopic ellipsometry (SE) data are obtained using interference enhancement, and the modeling of this data is guided by results from atomic force microscopy (AFM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-ray reflectivity (XRR). By AFM, ca. 40 nm BTS films show ca. 10 nm roughness. SEM images also suggest considerable roughness in the films and indicate that they are composed of 13.1 ± 5.9 nm grains. XRD confirms that the films are crystalline and predicts a grain size of 17 ± 2 nm. XRD results are consistent with the composition of the films — a mildly oxidized BTS material. Three models of increasing complexity are investigated to explain the SE data. The first model consists of a smooth, homogeneous BTS film. The second model adds a roughness layer to the previous model. The third model also has two layers. The bottom layer is modeled as a mixture of BTS and void using a Bruggeman effective medium approximation. The upper layer is similarly modeled, but with a gradient. The first model was unable to adequately model the SE data. The second model was an improvement — lower MSE (4.4) and good agreement with step height measurements. The third model was even better — very low MSE (2.6) and good agreement with AFM results. The third SE model predicted ca. 90% void at the film surface. XRR modeling of the film agreed well with the predictions from SE. The uniquenesses of the SE models were confirmed.

Hao Wang; Nitesh Madaan; Jacob Bagley; Anubhav Diwan; Yiqun Liu; Robert C. Davis; Barry M. Lunt; Stacey J. Smith; Matthew R. Linford

2014-01-01T23:59:59.000Z

110

Soft x-ray laser microscope. Final report  

SciTech Connect

The program consisted of two phases (Phase I and Phase II). The goal of the Phase I (first year program) was to design and construct the Soft X-ray Laser Contact Microscope. Such microscope was constructed and adapted to PPL`s 18.2nm soft X-ray Laser (SXL), which in turn was modified and prepared for microscopy experiments. Investigation of the photoresist response to 18.2nm laser radiation and transmissivity of 0.1m thick silicion-nitride (Si{sub 3}N{sub 4}) windows were important initial works. The goal of the first year of Phase II was to construct X-ray contact microscope in combination with existing optical phase microscope, already used by biologists. In the second year of Phase II study of dehydrated Horeseshoe Crab and Hela cancer cells were performed with COXRALM. Also during Phase II, the Imaging X-Ray Laser Microscope (IXRALM) was designed and constructed. This paper describes the development of each of the microscopes and their application for research.

Suckewer, P.I.

1990-10-01T23:59:59.000Z

111

Development of x-ray laminography under an x-ray microscopic condition  

SciTech Connect

An x-ray laminography system under an x-ray microscopic condition was developed to obtain a three-dimensional structure of laterally-extended planar objects which were difficult to observe by x-ray tomography. An x-ray laminography technique was introduced to an x-ray transmission microscope with zone plate optics. Three prototype sample holders were evaluated for x-ray imaging laminography. Layered copper grid sheets were imaged as a laminated sample. Diatomite powder on a silicon nitride membrane was measured to confirm the applicability of this method to non-planar micro-specimens placed on the membrane. The three-dimensional information of diatom shells on the membrane was obtained at a spatial resolution of sub-micron. Images of biological cells on the membrane were also obtained by using a Zernike phase contrast technique.

Hoshino, Masato; Uesugi, Kentaro; Takeuchi, Akihisa; Suzuki, Yoshio; Yagi, Naoto [Japan Synchrotron Radiation Research Institute JASRI/SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)

2011-07-15T23:59:59.000Z

112

Chest x-Rays  

Energy.gov (U.S. Department of Energy (DOE))

The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica.

113

X-ray beamsplitter  

DOE Patents (OSTI)

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5--50 pairs of alternate Mo/Si layers with a period of 20--250 A. The support membrane is 10--200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window. 6 figs.

Ceglio, N.M.; Stearns, D.G.; Hawryluk, A.M.; Barbee, T.W. Jr.

1987-08-07T23:59:59.000Z

114

X-ray beamsplitter  

DOE Patents (OSTI)

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

Ceglio, Natale M. (Livermore, CA); Stearns, Daniel S. (Mountain View, CA); Hawryluk, Andrew M. (Modesto, CA); Barbee, Jr., Troy W. (Palo Alto, CA)

1989-01-01T23:59:59.000Z

115

X-ray binaries  

E-Print Network (OSTI)

We review the nuclear astrophysics aspects of accreting neutron stars in X-ray binaries. We summarize open astrophysical questions in light of recent observations and their relation to the underlying nuclear physics. Recent progress in the understanding of the nuclear physics, especially of X-ray bursts, is also discussed.

H. Schatz; K. E. Rehm

2006-08-01T23:59:59.000Z

116

End station for nanoscale magnetic materials study: Combination of scanning tunneling microscopy and soft X-ray magnetic circular dichroism spectroscopy  

SciTech Connect

We have constructed an end station for nanoscale magnetic materials study at the soft X-ray beamline HiSOR BL-14 at Hiroshima Synchrotron Radiation Center. An ultrahigh-vacuum scanning tunneling microscope (STM) was installed for an in situ characterization of nanoscale magnetic materials in combination with soft X-ray magnetic circular dichroism (XMCD) spectroscopy experiment. The STM was connected to the XMCD experimental station via damper bellows to isolate it from environmental vibrations, thus achieving efficient spatial resolution for observing Si(111) surface at atomic resolution. We performed an in situ experiment with STM and XMCD spectroscopy on Co nanoclusters on an Au(111) surface and explored its practical application to investigate magnetic properties for well-characterized nanoscale magnetic materials.

Ueno, Tetsuro; Sawada, Masahiro; Namatame, Hirofumi [Hiroshima Synchrotron Radiation Center, Hiroshima University, 2-313 Kagamiyama, Higashi-Hiroshima 739-0046 (Japan); Kishimizu, Yusuke; Kimura, Akio [Graduate School of Science, Hiroshima University, 1-3-1 Kagamiyama, Higashi-Hiroshima 739-8526 (Japan); Taniguchi, Masaki [Hiroshima Synchrotron Radiation Center, Hiroshima University, 2-313 Kagamiyama, Higashi-Hiroshima 739-0046 (Japan); Graduate School of Science, Hiroshima University, 1-3-1 Kagamiyama, Higashi-Hiroshima 739-8526 (Japan)

2012-12-15T23:59:59.000Z

117

Investigation of early growth of calcium hydroxide crystals in cement solution by soft x-ray transmission microscopy  

E-Print Network (OSTI)

method of generating ettringite and significant early-ageto be CH phase, but not ettringite. To a certain degree thisfor formation exist for ettringite [8]. On the other hand,

Harutyunyan, V. S.

2009-01-01T23:59:59.000Z

118

Classification of Multiple Types of Organic Carbon Composition in Atmospheric Particles by Scanning Transmission X-Ray Microscopy Analysis  

E-Print Network (OSTI)

al. , 2005), and biomass combustion (Braun, 2005; Tivanskigenerated from biomass (wood) combustion, however, it is

Takahama, S.

2008-01-01T23:59:59.000Z

119

X-ray absorption spectroscopy  

E-Print Network (OSTI)

009-9473-8 REVIEW X-ray absorption spectroscopy Junko Yano Æand application of X-ray absorption spectroscopy, bothX-ray absorption near-edge structure (XANES) and extended X-

Yano, Junko; Yachandra, Vittal K.

2009-01-01T23:59:59.000Z

120

X-ray Absorption Spectroscopy  

E-Print Network (OSTI)

type: Review X-ray Absorption Spectroscopy Junko Yano andPhotosystem II; XAS, X-ray absorption spectroscopy; EXAFS,X-ray absorption fine structure; EPR, electron paramagnetic

Yano, Junko

2010-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


121

Controllable variation of the intensity of diffracted X-ray beams and double modulation of such beams for transmission and reception of audio information  

Science Journals Connector (OSTI)

This paper discusses research devoted to the study of the intensity change of diffracted and transmitted X-ray beams under the action of a temperature gradient or acoustic oscillations, as well as the techniques for `controllable complete reflection' of transmitted X-radiation in the direction of the diffracted beam.

Navasardyan, M.A.

2001-11-17T23:59:59.000Z

122

X-Ray Generators  

Science Journals Connector (OSTI)

There are many types of X-ray generators sold commercially. The following are some of ... that should be considered when selecting a particular generator for a particular purpose. All the companies listed below s...

Reuben Rudman

1972-01-01T23:59:59.000Z

123

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless X-Ray Imaging in Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

124

Photon Sciences | Beamlines | HXN: Hard X-ray Nanoprobe  

NLE Websites -- All DOE Office Websites (Extended Search)

HXN: Hard X-ray Nanoprobe HXN: Hard X-ray Nanoprobe Poster | Fact Sheet | Preliminary Design Report Scientific Scope The Hard X-ray Nanoprobe beamline and endstation instruments (HXN) will be designed and constructed to explore new frontiers of hard x-ray microscopy applications with the highest achievable spatial resolution. Currently the available spatial resolution for scientific applications, provided by scanning x-ray microscopes in the hard x-ray regime, is limited to ~50nm, which is still insufficient for probing the nanoscale interfacial structures critical in determining properties and functionalities of material and biological systems. The HXN beamline aims to enable x-ray experiments at spatial resolutions ranging from 10 to 30 nm with an ultimate goal of ~1 nm. Beamline Description

125

X-ray beam finder  

DOE Patents (OSTI)

An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

Gilbert, H.W.

1983-06-16T23:59:59.000Z

126

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

127

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

128

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

129

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

130

Combined Scanning Transmission Electron Microscopy Tilt- and Focal Series  

SciTech Connect

In this study, a combined tilt- and focal series is proposed as a new recording scheme for high-angle annular dark-field scanning transmission electron microscopy (STEM) tomography. Three-dimensional (3D) data were acquired by mechanically tilting the specimen, and recording a through-focal series at each tilt direction. The sample was a whole-mount macrophage cell with embedded gold nanoparticles. The tilt focal algebraic reconstruction technique (TF-ART) is introduced as a new algorithm to reconstruct tomograms from such combined tilt- and focal series. The feasibility of TF-ART was demonstrated by 3D reconstruction of the experimental 3D data. The results were compared with a conventional STEM tilt series of a similar sample. The combined tilt- and focal series led to smaller missing wedge artifacts, and a higher axial resolution than obtained for the STEM tilt series, thus improving on one of the main issues of tilt series-based electron tomography.

Dahmen, Tim [German Research Center for Artificial Intelligence (DFKI), Germany] [German Research Center for Artificial Intelligence (DFKI), Germany; Baudoin, Jean-Pierre G [ORNL] [ORNL; Lupini, Andrew R [ORNL] [ORNL; Kubel, Christian [Karlsruhe Institute of Technology, Leopoldshafen, Germany] [Karlsruhe Institute of Technology, Leopoldshafen, Germany; Slusallek, Phillip [German Research Center for Artificial Intelligence (DFKI), Germany] [German Research Center for Artificial Intelligence (DFKI), Germany; De Jonge, Niels [ORNL] [ORNL

2014-01-01T23:59:59.000Z

131

The first X-ray diffraction measurements on Mars  

Science Journals Connector (OSTI)

The X-ray diffraction/X-ray fluorescence instrument CheMin on the Curiosity rover is a shoebox-sized device using transmission geometry and an energy-discriminating CCD detector. The instrument has returned the first X-ray diffraction data for soil and drilled samples from Mars outcrops, revealing a suite of primary basaltic minerals, amorphous components and varied hydrous alteration products including phyllosilicates.

Bish, D.

2014-10-21T23:59:59.000Z

132

X-ray Spectrometry  

Science Journals Connector (OSTI)

These provide excellent energy resolution for a wide range of X-ray energies, from the optical range up to several kiloelectronvolts. ... The Astro-E2 launched in 2005 was the first mission that contained a low-temperature microcalorimeter-based observatory, and three more low-temperature detector-based observatories are being developed (NeXT, Constellation-X, ZEUS). ...

Imre Szalóki; János Osán; René E. Van Grieken

2006-05-10T23:59:59.000Z

133

X-ray lithography using holographic images  

DOE Patents (OSTI)

Methods for forming X-ray images having 0.25 {micro}m minimum line widths on X-ray sensitive material are presented. A holographic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required. 15 figs.

Howells, M.S.; Jacobsen, C.

1997-03-18T23:59:59.000Z

134

X-ray lithography using holographic images  

DOE Patents (OSTI)

Methods for forming X-ray images having 0.25 .mu.m minimum line widths on X-ray sensitive material are presented. A holgraphic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required.

Howells, Malcolm S. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1997-01-01T23:59:59.000Z

135

APS 7-BM Beamline: X-Ray Resources  

NLE Websites -- All DOE Office Websites (Extended Search)

Useful Websites Useful Websites X-Ray Interactions with Matter from CRXO at LBNL. Intuitive interface for x-ray transmission and reflectivity for a wide range of materials. X-Ray Data Booklet from LBNL. Slightly outdated in places, but many useful tables of edge energies, fluorescence lines, and crystal lattice spacings. NIST XCOM Database. Powerful database of photoelectric absorption, elastic scattering, and Compton scattering cross-sections for a wide range of materials. X-Ray Server. Maintained by Sergey Stepanov at GMCA at the APS, this website has several powerful calculators for simulating x-ray reflection and diffraction. Software X-Ray Oriented Programs (XOP). This program, written by scientists at the ESRF and APS, is widely used in the synchrotron research community.

136

Tunable X-ray source  

DOE Patents (OSTI)

A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

Boyce, James R. (Williamsburg, VA)

2011-02-08T23:59:59.000Z

137

Direct observation of temperature dependent magnetic domain structure of the multiferroic La{sub 0.66}Sr{sub 0.34}MnO{sub 3}/BiFeO{sub 3} bilayer system by x-ray linear dichroism- and x-ray magnetic circular dichroism-photoemission electron microscopy  

SciTech Connect

Low-thickness La{sub 0.66}Sr{sub 0.34}MnO{sub 3} (LSMO)/BiFeO{sub 3} (BFO) thin film samples deposited on SrTiO{sub 3} were imaged by high resolution x-ray microscopy at different temperatures. The ultra-thin thickness of the top layer allows to image both the ferromagnetic domain structure of LSMO and the multiferroic domain structure of the buried BFO layer, opening a path to a direct observation of coupling at the interface on a microscopic level. By comparing the domain size and structure of the BFO and LSMO, we observed that, in contrast to LSMO single layers, LSMO/BFO multilayers show a strong temperature dependence of the ferromagnetic domain structure of the LSMO. Particularly, at 40?K, a similar domain size for BFO and LSMO is observed. This indicates a persistence of exchange coupling on the microscopic scale at a temperature, where the exchange bias as determined by magnetometer measurements is vanishing.

Mix, C.; Finizio, S.; Jakob, G.; Kläui, M. [Institut für Physik, Johannes Gutenberg Universität Mainz, Staudingerweg 7, D-55128 Mainz (Germany); Buzzi, M.; Nolting, F. [Swiss Light Source, Paul Scherrer Institut, CH-5232 Villigen PSI (Switzerland); Kronast, F. [Helmholtz-Zentrum-Berlin für Materialien und Energie GmbH, Albert-Einstein Straße 15, D-12489 Berlin (Germany)

2014-05-21T23:59:59.000Z

138

Fabrication of curved-line nanostructures on membranes for transmission electron microscopy investigations of domain walls  

E-Print Network (OSTI)

Fabrication of curved-line nanostructures on membranes for transmission electron microscopy, Cambridge CB2 3QZ, United Kingdom Available online 28 February 2006 Abstract We have fabricated curved-line ferromagnetic nanostructures on membranes for transmission electron microscopy investigations of the equilibrium

Dunin-Borkowski, Rafal E.

139

Copyright The Discussion Group of X-Ray Analysis,  

E-Print Network (OSTI)

-2900. 3 In Situ Spatial and Time-Resolved Studies of Electrochemical Reactions by Scanning Transmission X the Signal-to-Noise Ratio of X-ray Diffraction Profiles by Smoothed Principal Component Analysis Zeng Ping

Jun, Kawai

140

X-ray Spectrometry  

Science Journals Connector (OSTI)

The segmented STJ operated at total count rates of above 105 counts/s, and the best-achieved energy resolution of their single STJ was found to be 10 eV for X-ray energies below 1 keV. ... The Mo?Au TES, with an operating temperature of 230 mK, was developed for the Constellation-X mission and the energy resolution of the spectrometer is ?28 eV at 3.3 keV. ...

Imre Szalóki; Szabina B. Török; Jasna Injuk; René E. Van Grieken

2002-05-18T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

Modeling the high resolution X-ray spectra from the relativistic jets of the X-ray binary SS 433  

E-Print Network (OSTI)

We test the physical model of the relativistic jets in the galactic X-ray binary SS 433 that was proposed by Marshall et al. 2002 (Paper I) using additional observations from the Chandra High Energy Transmission Grating ...

Lopez, Laura Ann, 1982-

2004-01-01T23:59:59.000Z

142

3D Imaging of Nickel Oxidation States using Full Field X-ray Absorption Near Edge Structure Nanotomography  

SciTech Connect

Reduction-oxidation (redox) cycling of the nickel electrocatalyst phase in the solid oxide fuel cell (SOFC) anode can lead to performance degradation and cell failure. A greater understanding of nickel redox mechanisms at the microstructural level is vital to future SOFC development. Transmission x-ray microscopy (TXM) provides several key techniques for exploring oxidation states within SOFC electrode microstructure. Specifically, x-ray nanotomography and x-ray absorption near edge structure (XANES) spectroscopy have been applied to study samples of varying nickel (Ni) and nickel oxide (NiO) compositions. The imaged samples are treated as mock SOFC anodes containing distinct regions of the materials in question. XANES spectra presented for the individual materials provide a basis for the further processing and analysis of mixed samples. Images of composite samples obtained are segmented, and the distinct nickel and nickel oxide phases are uniquely identified using full field XANES spectroscopy. Applications to SOFC analysis are discussed.

Nelson, George; Harris, William; Izzo, John; Grew, Kyle N. (Connecticut); (USARL)

2012-01-20T23:59:59.000Z

143

A Transmission Electron Microscopy Study of Presolar Hibonite  

Science Journals Connector (OSTI)

We report isotopic and microstructural data on five presolar hibonite grains (KH1, KH2, KH6, KH15, and KH21) identified in an acid residue of the Krymka LL3.1 ordinary chondrite. Isotopic measurements by secondary ion mass spectrometry (SIMS) verified a presolar circumstellar origin for the grains. Transmission electron microscopy (TEM) examination of the crystal structure and chemistry of the grains was enabled by in situ sectioning and lift-out with a focused-ion-beam scanning-electron microscope (FIB-SEM). Comparisons of isotopic compositions with models indicate that four of the five grains formed in low-mass stars that evolved through the red giant/asymptotic giant branches (RGBs/AGBs), whereas one grain formed in the ejecta of a Type II supernova. Selected-area electron-diffraction patterns show that all grains are single crystals of hibonite. Some grains contain minor structural perturbations (stacking faults) and small spreads in orientation that can be attributed to a combination of growth defects and mechanical processing by grain-grain collisions. The similar structure of the supernova grain to those from RGB/AGB stars indicates a similarity in the formation conditions. Radiation damage (e.g., point defects), if present, occurs below our detection limit. Of the five grains we studied, only one has the pure hibonite composition of CaAl12O19. All others contain minor amounts of Mg, Si, Ti, and Fe. The microstructural data are generally consistent with theoretical predictions, which constrain the circumstellar condensation temperature to a range of 1480-1743 K, assuming a corresponding total gas pressure between 1 ? 10–6 and 1 ? 10–3 atm. The TEM data were also used to develop a calibration for SIMS determination of Ti contents in oxide grains. Grains with extreme 18O depletions, indicating deep mixing has occurred in their parent AGB stars, are slightly Ti enriched compared with grains from stars without deep mixing, most likely reflecting differences in grain condensation conditions.

Thomas J. Zega; Conel M. O'D. Alexander; Larry R. Nittler; Rhonda M. Stroud

2011-01-01T23:59:59.000Z

144

Electron Microscopy | Center for Functional Nanomaterials  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron Microscopy Facility Electron Microscopy Facility Electron Microscopy This facility consists of four top-of-the line transmission electron microscopes, two of which are highly specialized instruments capable of extreme levels of resolution, achieved through spherical aberration correction. The facility is also equipped with extensive sample-preparation capabilities. The scientific interests of the staff focus on understanding the microscopic origin of the physical and chemical behavior of materials, with specific emphasis on in-situ studies of materials in native, functional environments. Capabilities Atomic-resolution imaging of internal materials structure with scanning transmission and transmission electron microscopy Spectroscopic characterization with energy dispersive x-ray

145

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism  

NLE Websites -- All DOE Office Websites (Extended Search)

Unexpected Angular Dependence of Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Wednesday, 29 August 2007 00:00 Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and x-ray polarization, but their orientation relative to the crystallographic axes must be taken into account for accurate interpretation of XMLD data. Magnetism and X Rays

146

X-ray Absorption Spectroscopy  

SciTech Connect

This review gives a brief description of the theory and application of X-ray absorption spectroscopy, both X-ray absorption near edge structure (XANES) and extended X-ray absorption fine structure (EXAFS), especially, pertaining to photosynthesis. The advantages and limitations of the methods are discussed. Recent advances in extended EXAFS and polarized EXAFS using oriented membranes and single crystals are explained. Developments in theory in understanding the XANES spectra are described. The application of X-ray absorption spectroscopy to the study of the Mn4Ca cluster in Photosystem II is presented.

Yano, Junko; Yachandra, Vittal K.

2009-07-09T23:59:59.000Z

147

X-ray fluorescence mapping  

NLE Websites -- All DOE Office Websites (Extended Search)

biololgical cells, over the measurement of impurities in solar cells, to the rare earth content of geological materials. A somewhat 'typical' layout for a X-ray fluorescence...

148

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering Resonant Soft X-Ray Scattering of Tri-Block Copolymers Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Wednesday, 30 May 2012 00:00 In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

149

Biological soft X-ray tomography on beamline 2.1 at the Advanced Light Source  

Science Journals Connector (OSTI)

Beamline 2.1, a transmission soft X-ray microscope at the Advanced Light Source of Lawrence Berkeley National Laboratory, is described.

Le Gros, M.A.

2014-10-01T23:59:59.000Z

150

Attenuation corrections for X-ray and neutron fibre diffraction studies  

Science Journals Connector (OSTI)

The form of the transmission factor for sample geometries encountered in X-ray and neutron fibre diffraction studies is considered.

Langan, P.

1995-02-01T23:59:59.000Z

151

X-ray Photoelectron Spectroscopy Studies of Oxidized and Reduced CeO?(111) Surfaces  

SciTech Connect

We have studied the electronic structure of oxidized and reduced CeO? (111) surfaces using X-ray photoelectron spectroscopy (XPS). The 50 nm thick Co?(111) film was grown on a YSZ(111) substrate using oxygen plasma assisted molecular beam epitaxy (OPA-MBE). This film has been characterized using in-situ RHEED (reflection high energy electron diffraction) and ex-situ XRD (X-ray diffraction), HRTEM (high resolution transmission electron microscopy) and RBS (Rutherford backscattering spectroscopy). The lattice mismatch between CeO?(111) and YSZ(111) is less than 5% and yields a flat surface that is comprised of an equivalent number of Ce?? and O?? ions. Oxidation with O? at 773 K under UHV conditions was sufficient to fully oxidize the CeO?(111). Surface reduction was carried out by annealing in UHV at 973 K.

Engelhard, Mark H.; Azad, Samina; Peden, Charles HF; Thevuthasan, Suntharampillai

2004-12-01T23:59:59.000Z

152

X-ray shearing interferometer  

DOE Patents (OSTI)

An x-ray interferometer for analyzing high density plasmas and optically opaque materials includes a point-like x-ray source for providing a broadband x-ray source. The x-rays are directed through a target material and then are reflected by a high-quality ellipsoidally-bent imaging crystal to a diffraction grating disposed at 1.times. magnification. A spherically-bent imaging crystal is employed when the x-rays that are incident on the crystal surface are normal to that surface. The diffraction grating produces multiple beams which interfere with one another to produce an interference pattern which contains information about the target. A detector is disposed at the position of the image of the target produced by the interfering beams.

Koch, Jeffrey A. (Livermore, CA)

2003-07-08T23:59:59.000Z

153

X-ray Microscopy and Imaging: FAQs  

NLE Websites -- All DOE Office Websites (Extended Search)

Frequently Asked Questions Frequently Asked Questions How to get beamtime ? 80% and more of our beamtime is awarded to General Users through the General User Proposal system. So, in order to receive beamtime for an experiment you have in mind, you would have to complete a short proposal form (specific instructions as to deadlines, etc), which can be found following this link. We are well oversubscribed, so prospective users may not get beamtime the first time they apply, but as proposals age, the score increases. Often, it is helpful for 'new' users to contact beamline staff first before submitting, so that potential pitfalls in experiments are avoided. For that purpose, you may wish to browse our webpages, and see who does what kind of science and applications, and directly email the person you think is most likely appropriate. When in doubt, you can also always send an email to Qun Shen, who then will make sure it reaches the appropriate people.

154

Generated Aerosols: X-ray Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

of any inorganic in the particles. When particles are collected in an impactor, lower viscosity particles will flatten more upon impaction and will be thinner (for a given size)...

155

Optics for X-Ray Laser and Laser Plasma Soft X-Ray Radiation  

Science Journals Connector (OSTI)

Focusing X-ray grazing incidence optics for X-ray laser and laser plasma soft X-ray radiation has been studied. ... computer code. Parabolic axisymmetric mirror for focusing Princeton X-ray laser beam and ellipso...

L. Pina; A. Inneman; R. Hudec

1996-01-01T23:59:59.000Z

156

SMB, X-Ray Spectroscopy & Imaging  

NLE Websites -- All DOE Office Websites (Extended Search)

Home X-Ray Spectroscopy & Imaging X-Ray Spectroscopy & Imaging SSRL has five hard X-ray Spectroscopy beamlines and three Microfocus Imaging beamlines dedicated to Biological and...

157

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has...

158

Miniature x-ray source  

DOE Patents (OSTI)

A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

Trebes, James E. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA)

2000-01-01T23:59:59.000Z

159

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking  

E-Print Network (OSTI)

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking Tom Aldcroft SAO/CXC #12;X-ray Stacking 2008 analysis for a sample Stacking ­ mean properties of sample Chandra X-ray data (faint point sources) are photon-limited with low background => stacking in X-rays is very effective #12;X-ray Stacking 2008-Apr-22

Wolfe, Patrick J.

160

Center for X-Ray Optics, 1991  

SciTech Connect

This report discusses: Soft-X-Ray imaging with zone-plate lenses; multilayer reflective optics; and spectroscopy with x-rays.

Not Available

1992-03-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

SMB, X-ray Absorption Spectroscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Absorption Spectroscopy X-ray Absorption Spectroscopy X-ray absorption spectroscopy (XAS) is a well-established technique for simultaneous local geometric and electronic structure...

162

Tokamak x ray diagnostic instrumentation  

SciTech Connect

Three classes of x-ray diagnostic instruments enable measurement of a variety of tokamak physics parameters from different features of the x-ray emission spectrum. (1) The soft x-ray (1 to 50 keV) pulse-height-analysis (PHA) diagnostic measures impurity concentrations from characteristic line intensities and the continuum enhancement, and measures the electron temperature from the continuum slope. (2) The Bragg x-ray crystal spectrometer (XCS) measures the ion temperature and neutral-beam-induced toroidal rotation velocity from the Doppler broadening and wavelength shift, respectively, of spectral lines of medium-Z impurity ions. Impurity charge state distributions, precise wavelengths, and inner-shell excitation and recombination rates can also be studied. X rays are diffracted and focused by a bent crystal onto a position-sensitive detector. The spectral resolving power E/..delta..E is greater than 10/sup 4/ and time resolution is 10 ms. (3) The x-ray imaging system (XIS) measures the spatial structure of rapid fluctuations (0.1 to 100 kHZ) providing information on MHD phenomena, impurity transport rates, toroidal rotation velocity, plasma position, and the electron temperature profile. It uses an array of silicon surface-barrier diodes which view different chords of the plasma through a common slot aperture and operate in current (as opposed to counting) mode. The effectiveness of shields to protect detectors from fusion-neutron radiation effects has been studied both theoretically and experimentally.

Hill, K.W.; Beiersdorfer, P.; Bitter, M.; Fredrickson, E.; Von Goeler, S.; Hsuan, H.; Johnson, L.C.; Liew, S.L.; McGuire, K.; Pare, V.

1987-01-01T23:59:59.000Z

163

Spectroscopic imaging, diffraction, and holography with x-ray photoemission  

SciTech Connect

X-ray probes are capable of determining the spatial structure of an atom in a specific chemical state, over length scales from about a micron all the way down to atomic resolution. Examples of these probes include photoemission microscopy, energy-dependent photoemission diffraction, photoelectron holography, and X-ray absorption microspectroscopy. Although the method of image formation, chemical-state sensitivity, and length scales can be very different, these X-ray techniques share a common goal of combining a capability for structure determination with chemical-state specificity. This workshop will address recent advances in holographic, diffraction, and direct imaging techniques using X-ray photoemission on both theoretical and experimental fronts. A particular emphasis will be on novel structure determinations with atomic resolution using photoelectrons.

Not Available

1992-02-01T23:59:59.000Z

164

In-Situ Electrochemical Transmission Electron Microscopy for Battery Research  

SciTech Connect

The recent development of in-situ liquid stages for (scanning) transmission electron microscopes now makes it possible for us to study the details of electrochemical processes under operando conditions. As electrochemical processes are complex, care must be taken to calibrate the system before any in-situ/operando observations. In addition, as the electron beam can cause effects that look similar to electrochemical processes at the electrolyte/electrode interface, an understanding of the role of the electron beam in modifying the operando observations must also be understood. In this paper we describe the design, assembly, and operation of an in-situ electrochemical cell, paying particular attention to the method for controlling and quantifying the experimental parameters. The use of this system is then demonstrated for the lithiation/delithiation of silicon nanowires.

Mehdi, Beata L [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Gu, Meng [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Parent, Lucas [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Xu, WU [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Nasybulin, Eduard [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Chen, Xilin [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Unocic, Raymond R [ORNL] [ORNL; Xu, Pinghong [University of California, Davis] [University of California, Davis; Welch, David [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Abellan, Patricia [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Zhang, Ji-Guang [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Liu, Jun [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Wang, Chongmin [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Arslan, Ilke [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Evans, James E [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Browning, Nigel [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL)

2014-01-01T23:59:59.000Z

165

Visualizing Macromolecular Complexes with In Situ Liquid Scanning Transmission Electron Microscopy  

SciTech Connect

A central focus of biological research is understanding the structure/function relationship of macromolecular protein complexes. Yet conventional transmission electron microscopy techniques are limited to static observations. Here we present the first direct images of purified macromolecular protein complexes using in situ liquid scanning transmission electron microscopy. Our results establish the capability of this technique for visualizing the interface between biology and nanotechnology with high fidelity while also probing the interactions of biomolecules within solution. This method represents an important advancement towards allowing future high-resolution observations of biological processes and conformational dynamics in real-time.

Evans, James E.; Jungjohann, K. L.; Wong, Peony C. K.; Chiu, Po-Lin; Dutrow, Gavin H.; Arslan, Ilke; Browning, Nigel D.

2012-11-01T23:59:59.000Z

166

X-ray Emission from Massive Stars  

E-Print Network (OSTI)

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore be related to the production of X-rays on massive stars. If so, massive stars' X-rays are much different than those found our own Sun and other cooler stars like the Sun that produce X-rays via magnetic activity

Cohen, David

167

X-ray Emission from Massive Stars  

E-Print Network (OSTI)

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore #12;What is the mechanism by which massive stars produce x-rays? New results from the Chandra X-ray Observatory ­ high-resolution x-ray spectroscopy: measuring Doppler broadening in emission lines Testing

Cohen, David

168

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

169

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

170

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

171

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

172

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

173

Compact x-ray source and panel  

DOE Patents (OSTI)

A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

Sampayon, Stephen E. (Manteca, CA)

2008-02-12T23:59:59.000Z

174

Ultrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS)  

E-Print Network (OSTI)

: ultrafast x-rays, x-ray absorption spectroscopy, terawatt lasers, ultrafast reaction dynamics, atomic motion atomic motion by scrutinizing the changes in x- ray absorption spectra during reactions. FirstUltrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS) Guangjun

Guo, Ting

175

Focused X-ray source  

DOE Patents (OSTI)

Disclosed is an intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator. 8 figs.

Piestrup, M.A.; Boyers, D.G.; Pincus, C.I.; Maccagno, P.

1990-08-21T23:59:59.000Z

176

A Laboratory-based Hard X-ray Monochromator for High-Resolution X-ray Emission Spectroscopy and X-ray Absorption Near Edge Structure Measurements  

E-Print Network (OSTI)

We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low poer x-ray (bremsstrahlung) tube source, a spherically-bent crystal analyzer (SBCA), and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of 5 keV to 10 keV while also dmeonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy (XES) comparable to those achived at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure (XANES), the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-powered line-foc...

Seidler, G T; Remesnik, A J; Pacold, J I; Ball, N A; Barry, N; Styczinski, M; Hoidn, O R

2014-01-01T23:59:59.000Z

177

Single atom identification by energy dispersive x-ray spectroscopy  

SciTech Connect

Using aberration-corrected scanning transmission electron microscope and energy dispersive x-ray spectroscopy, single, isolated impurity atoms of silicon and platinum in monolayer and multilayer graphene are identified. Simultaneously acquired electron energy loss spectra confirm the elemental identification. Contamination difficulties are overcome by employing near-UHV sample conditions. Signal intensities agree within a factor of two with standardless estimates.

Lovejoy, T. C.; Dellby, N.; Krivanek, O. L. [Nion, 1102 8th St., Kirkland, Washington 98033 (United States); Ramasse, Q. M. [SuperSTEM Laboratory, STFC Daresbury, Keckwick Lane, Daresbury WA4 4AD (United Kingdom); Falke, M.; Kaeppel, A.; Terborg, R. [Bruker Nano GmbH, Schwarzschildstr. 12, 12489 Berlin (Germany); Zan, R. [School of Physics and Astronomy, University of Manchester, Manchester M13 9PL (United Kingdom)

2012-04-09T23:59:59.000Z

178

Femtosecond x-ray absorption spectroscopy with hard x-ray free electron laser  

SciTech Connect

We have developed a method of dispersive x-ray absorption spectroscopy with a hard x-ray free electron laser (XFEL), generated by a self-amplified spontaneous emission (SASE) mechanism. A transmission grating was utilized for splitting SASE-XFEL light, which has a relatively large bandwidth (?E/E ? 5 × 10{sup ?3}), into several branches. Two primary split beams were introduced into a dispersive spectrometer for measuring signal and reference spectra simultaneously. After normalization, we obtained a Zn K-edge absorption spectrum with a photon-energy range of 210 eV, which is in excellent agreement with that measured by a conventional wavelength-scanning method. From the analysis of the difference spectra, the noise ratio was evaluated to be ?3 × 10{sup ?3}, which is sufficiently small to trace minute changes in transient spectra induced by an ultrafast optical laser. This scheme enables us to perform single-shot, high-accuracy x-ray absorption spectroscopy with femtosecond time resolution.

Katayama, Tetsuo; Togashi, Tadashi; Tono, Kensuke; Kameshima, Takashi [Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan)] [Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan); Inubushi, Yuichi; Sato, Takahiro; Hatsui, Takaki; Yabashi, Makina [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan)] [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan); Obara, Yuki; Misawa, Kazuhiko [Department of Applied Physics, Tokyo University of Agriculture and Technology, 2-24-16 Naka-cho, Koganei, Tokyo 184-8588 (Japan)] [Department of Applied Physics, Tokyo University of Agriculture and Technology, 2-24-16 Naka-cho, Koganei, Tokyo 184-8588 (Japan); Bhattacharya, Atanu; Kurahashi, Naoya [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan)] [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan); Ogi, Yoshihiro [Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198 (Japan)] [Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198 (Japan); Suzuki, Toshinori [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan) [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan); Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198 (Japan)

2013-09-23T23:59:59.000Z

179

13 - X-ray and Neutron Scattering  

Science Journals Connector (OSTI)

Abstract This chapter describes the use of neutrons and X-rays as probes in the study of structural and dynamic properties of metallic materials. Crystalline materials are characterized by their diffraction peaks related to their average crystallographic structure. In real crystals, locally displaced atoms and chemically (or isotopically for neutrons) different species may lead not only to changes of peak shapes and positions, but also to additional (diffuse) scattering between Bragg peak, including scattering around the primary beam (small-angle scattering). All these features can be used to extract information about the state of a sample, its compositional and structural variations on a scale depending on the scattering, in static and time-resolved kinetic studies. Energy-resolved scattering also offers an insight into solid-state dynamics on a microscopic scale. Some of the most important methods will be described and illustrated by instructive examples. The presentation offers a combined view of neutron and X-ray scattering, with the necessary simplifications dictated by space limitations. The special properties of thermal neutrons and of hard X-rays (now widely available at synchrotron radiation sources), their mutual combination, and combinations with other methods, in particular electron microscopy, offer ample opportunity to better understand and control materials properties. After a brief introduction to scattering from real crystals and some general ideas about long-range strains and Bragg peaks, the vicinity of Bragg peaks (displacement scattering at large scattering angles), the scattering far away from Bragg peaks (chemical heterogeneities, short-range order), and, in greater detail, small-angle scattering (which is not sensitive to the extent of crystallinity, but to nanoscale variations of chemical composition and of magnetization, precipitation) will be described, along with classical and more recent applications related to short-range ordering and precipitation in bulk and nanostructured alloys. Some other fields are only briefly addressed (grazing-incidence studies of surfaces, radiography, absorption spectroscopies, coherent X-rays). The final section offers some information on the influence of defects on lattice dynamics and on (slow) diffusive motion in materials.

Gernot Kostorz

2014-01-01T23:59:59.000Z

180

Microgap x-ray detector  

DOE Patents (OSTI)

An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

Wuest, Craig R. (Danville, CA); Bionta, Richard M. (Livermore, CA); Ables, Elden (Livermore, CA)

1994-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

Chest x-Rays | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Chest x-Rays Chest x-Rays Chest x-Rays Chest X-ray B-Reading The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica. The B-reading is considered a special reading because doctors who are certified by NIOSH to perform B-readings use a specific protocol to read and record the findings as developed by the International Labour Organization (ILO). The ILO's protocol provides rules for systematically examining the x-ray in a step-by-step method and recording certain abnormalities or changes on the chest x-ray that can be attributable to

182

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs...

183

Lensless X-Ray Imaging in Reflection  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities...

184

Producing X-rays at the APS  

ScienceCinema (OSTI)

An introduction and overview of the Advanced Photon Source at Argonne National Laboratory, the technology that produces the brightest X-ray beams in the Western Hemisphere, and the research carried out by scientists using those X-rays.

None

2013-04-19T23:59:59.000Z

185

SMB, X-ray Fluorescence Imaging  

NLE Websites -- All DOE Office Websites (Extended Search)

Fluorescence Imaging X-ray Fluorescence Imaging X-ray fluorescence imaging utilizes the high brightness of SPEAR3 and focused beam generated by the uses of K-B optics, capillaries...

186

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism  

NLE Websites -- All DOE Office Websites (Extended Search)

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and x-ray polarization, but their orientation relative to the crystallographic axes must be taken into account for accurate interpretation of XMLD data. Magnetism and X Rays The ancient Greeks and also the Chinese knew about strange and rare stones with the power to attract iron. Moreover, when freely suspended these objects pointed north-south. Throughout the past, we have used this phenomenon-magnetism-for navigation and more recently for power production and digital information storage, all while trying to explore and understand its origins. In 1986 researchers at a facility similar to the ALS observed for the first time that the absorption of x rays depends not only on the composition of a material-that is, if it contains iron, nickel, or other elements-but also on its magnetism. The effect is unique in that it allows us to distinguish which atomic species magnetism originates from and provides information about their local atomic environment-for example, whether a magnetic species is surrounded by 4 or 6 oxygen atoms. A research team at the ALS has now shown that the relationship between magnetic order and absorption of x rays is even more complex and exciting than has been assumed for the past 20 years, leading to a reassessment of previous results.

187

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism  

NLE Websites -- All DOE Office Websites (Extended Search)

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and x-ray polarization, but their orientation relative to the crystallographic axes must be taken into account for accurate interpretation of XMLD data. Magnetism and X Rays The ancient Greeks and also the Chinese knew about strange and rare stones with the power to attract iron. Moreover, when freely suspended these objects pointed north-south. Throughout the past, we have used this phenomenon-magnetism-for navigation and more recently for power production and digital information storage, all while trying to explore and understand its origins. In 1986 researchers at a facility similar to the ALS observed for the first time that the absorption of x rays depends not only on the composition of a material-that is, if it contains iron, nickel, or other elements-but also on its magnetism. The effect is unique in that it allows us to distinguish which atomic species magnetism originates from and provides information about their local atomic environment-for example, whether a magnetic species is surrounded by 4 or 6 oxygen atoms. A research team at the ALS has now shown that the relationship between magnetic order and absorption of x rays is even more complex and exciting than has been assumed for the past 20 years, leading to a reassessment of previous results.

188

Chandra X-ray Observatory Center  

E-Print Network (OSTI)

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St in hot gas about 250 million light years from Earth. (Credit: X-ray: NASA/CXC/SAO/E.Bulbul, et al-Newton has revealed a mysterious X-ray signal in the data. This signal is represented in the circled data

189

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network (OSTI)

2/9/07 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 9, 07] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

190

Chandra X-ray Observatory Center  

E-Print Network (OSTI)

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St million light years from Earth. (Credit: X-ray: NASA/CXC/Wesleyan Univ./R.Kilgard, et al; Optical: NASA with optical data from the Hubble Space Telescope (red, green, and blue). The X-ray data reveal hundreds

191

X-ray Spectroscopy of Cool Stars  

E-Print Network (OSTI)

High-resolution X-ray spectroscopy has addressed not only various topics in coronal physics of stars, but has also uncovered important features relevant for our understanding of stellar evolution and the stellar environment. I summarize recent progress in coronal X-ray spectroscopy and in particular also discuss new results from studies of X-rays from pre-main sequence stars.

M. Guedel

2006-09-11T23:59:59.000Z

192

X-Ray Physics Evan Berkowitz  

E-Print Network (OSTI)

X-Ray Physics Evan Berkowitz Junior, MIT Department of Physics (Dated: October 25, 2006) We measure a variety of phenomena related to X-Ray absorption and production. We present data which conforms within, as are 22 Na electron-positron annhilation lines. The importance of understanding x-rays is demonstrated

193

Chandra X-ray Observatory Center  

E-Print Network (OSTI)

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St 200 million light years from Earth. (Credit: X-ray: NASA/CXC/UAH/M.Sun et al; Optical: NASA, ESA, & the Hubble Heritage Team (STScI/AURA) Caption: This composite image from the Chandra X-ray Observatory (blue

194

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network (OSTI)

9/6/09 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 6, 09] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

195

Chandra X-ray Observatory Center  

E-Print Network (OSTI)

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St. Cambridge, MA 02138 USA http://chandra.harvard.edu Four Supernova Remnants: NASA's Chandra X-ray Observatory's Chandra X-ray Observatory, four newly processed images of supernova remnants dramatically illustrate

196

Using Light to Control How X Rays Interact with Matter  

NLE Websites -- All DOE Office Websites (Extended Search)

ultrafast x-ray spectroscopy. ALS femtosecond spectroscopy beamline layout. Femtosecond x-ray and laser pulses derive from a single 800-nm laser oscillator. Femtosecond x rays...

197

X-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336342  

E-Print Network (OSTI)

X-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336­342 Published online in Wiley InterScience (www.interscience.wiley.com) DOI: 10.1002/xrs.980 Fish otolith trace element maps: new approaches with synchrotron microbeam x-ray of elements as they accrete through a fish's life. We apply synchrotron microbeam x-ray fluorescence methods

Limburg, Karin E.

198

X-ray Pulsations in the Supersoft X-ray Binary CAL 83  

E-Print Network (OSTI)

X-ray data reveal that the supersoft X-ray binary CAL 83 exhibits 38.4 minute pulsations at some epochs. These X-ray variations are similar to those found in some novae and are likely to be caused by nonradial pulsations the white dwarf. This is the first detection of pulsations in a classical supersoft X-ray binary.

P. C. Schmidtke; A. P. Cowley

2005-09-28T23:59:59.000Z

199

X-ray Spectroscopy of Cooling Cluster  

SciTech Connect

We review the X-ray spectra of the cores of clusters of galaxies. Recent high resolution X-ray spectroscopic observations have demonstrated a severe deficit of emission at the lowest X-ray temperatures as compared to that expected from simple radiative cooling models. The same observations have provided compelling evidence that the gas in the cores is cooling below half the maximum temperature. We review these results, discuss physical models of cooling clusters, and describe the X-ray instrumentation and analysis techniques used to make these observations. We discuss several viable mechanisms designed to cancel or distort the expected process of X-ray cluster cooling.

Peterson, J.R.; /SLAC; Fabian, A.C.; /Cambridge U., Inst. of Astron.

2006-01-17T23:59:59.000Z

200

X-ray Spectroscopy of Cooling Clusters  

E-Print Network (OSTI)

We review the X-ray spectra of the cores of clusters of galaxies. Recent high resolution X-ray spectroscopic observations have demonstrated a severe deficit of emission at the lowest X-ray temperatures as compared to that expected from simple radiative cooling models. The same observations have provided compelling evidence that the gas in the cores is cooling below half the maximum temperature. We review these results, discuss physical models of cooling clusters, and describe the X-ray instrumentation and analysis techniques used to make these observations. We discuss several viable mechanisms designed to cancel or distort the expected process of X-ray cluster cooling.

J. R. Peterson; A. C. Fabian

2005-12-21T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

X-ray Observations of Mrk 231  

E-Print Network (OSTI)

This paper presents new X-ray observations of Mrk 231, an active galaxy of particular interest due to its large infrared luminosity and the presence of several blueshifted broad absorption line (BAL) systems, a phenomenon observed in a small fraction of QSOs. A ROSAT HRI image of Mrk 231 is presented, this shows an extended region of soft X-ray emission, covering several tens of kpc, consistent with the extent of the host galaxy. An ASCA observation of Mrk 231 is also presented. Hard X-rays are detected but the data show no significant variability in X-ray flux. The hard X-ray continuum is heavily attenuated and X-ray column estimates range from ~ 2 x 10^{22} - 10^{23} cm^{-2} depending on whether the material is assumed to be neutral or ionized, and on the model assumed for the extended X-ray component. These ASCA data provide only the second hard X-ray spectrum of a BAL AGN presented to date. The broad-band spectral-energy-distribution of the source is discussed. While Mrk 231 is X-ray weak compared to Seyfert 1 galaxies, it has an optical-to-X-ray spectrum typical of a QSO.

T. J. Turner

1998-08-10T23:59:59.000Z

202

Laser Doppler holographic microscopy in transmission: application to fish embryo imaging  

E-Print Network (OSTI)

We have extended Laser Doppler holographic microscopy to transmission geometry. The technique is validated with living fish embryos imaged by a modified upright bio-microcope. By varying the frequency of the holographic reference beam, and the combination of frames used to calculate the hologram, multimodal imaging has been performed. Doppler images of the blood vessels for different Doppler shifts, images where the flow direction is coded in RGB colors or movies showing blood cells individual motion have been obtained as well. The ability to select the Fourier space zone that is used to calculate the signal, makes the method quantitative.

Verrier, Nicolas; Gross, Michel

2014-01-01T23:59:59.000Z

203

Structural defects in GaN revealed by Transmission Electron Microscopy  

SciTech Connect

This paper reviews the various types of structural defects observed by Transmission Electron Microscopy in GaN heteroepitaxial layers grown on foreign substrates and homoepitaxial layers grown on bulk GaN substrates. The structural perfection of these layers is compared to the platelet self-standing crystals grown by High Nitrogen Pressure Solution. Defects in undoped and Mg doped GaN are discussed. Some models explaining the formation of inversion domains in heavily Mg doped layers that are possible defects responsible for the difficulties of p-doping in GaN are also reviewed.

Liliental-Weber, Zuzanna

2014-04-18T23:59:59.000Z

204

Strain relief and AlSb buffer layer morphology in GaSb heteroepitaxial films grown on Si as revealed by high-angle annular dark-field scanning transmission electron microscopy  

SciTech Connect

The interfacial misfit (IMF) dislocation array of an epitaxial GaSb film on a Si substrate has been imaged with high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). The mismatch strain accommodation through dislocation formation has been investigated using geometric phase analysis (GPA) on HAADF-STEM images with atomic resolution to probe the defects' local strain distribution. These measurements indicate that the lattice parameter of the epitaxial film recovers its bulk value within three unit cells from the interface due to the relaxation through IMF dislocations. The atomic number contrast of the HAADF-STEM images and energy dispersive x-ray spectrometry illustrate the formation of islands of AlSb buffer layer along the interface. The role of the AlSb buffer layer in facilitating the GaSb film growth on Si is further elucidated by investigating the strain field of the islands with the GPA.

Vajargah, S. Hosseini; Couillard, M.; Cui, K. [Department of Material Science and Engineering, McMaster University, 1280 Main St. W., Hamilton, Ontario L8S 4M1 (Canada); Tavakoli, S. Ghanad; Robinson, B.; Kleiman, R. N.; Preston, J. S. [Department of Engineering Physics, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Botton, G. A. [Department of Material Science and Engineering, McMaster University, 1280 Main St. W., Hamilton, Ontario L8S 4M1 (Canada); Canadian Centre for Electron Microscopy, McMaster University, Hamilton, Ontario L8S 4M1 (Canada)

2011-02-21T23:59:59.000Z

205

Hard x-ray imaging from explorer  

SciTech Connect

Coded aperture X-ray detectors were applied to obtain large increases in sensitivity as well as angular resolution. A hard X-ray coded aperture detector concept is described which enables very high sensitivity studies persistent hard X-ray sources and gamma ray bursts. Coded aperture imaging is employed so that approx. 2 min source locations can be derived within a 3 deg field of view. Gamma bursts were located initially to within approx. 2 deg and X-ray/hard X-ray spectra and timing, as well as precise locations, derived for possible burst afterglow emission. It is suggested that hard X-ray imaging should be conducted from an Explorer mission where long exposure times are possible.

Grindlay, J.E.; Murray, S.S.

1981-11-01T23:59:59.000Z

206

Development of x-ray photoelectron microscope with an x-ray laser source  

Science Journals Connector (OSTI)

We have constructed an x-ray photoelectron microscopic system with an x-ray laser as an x-ray source. The lasing line is the Li-like Al 3d-4f transition at 15.47 nm where the recombining Al plasma is used as the x-ray laser medium. The beam from the x-ray laser cavity was then focused by using a Schwarzschild mirror coated with Mo/Si multilayers. The x-ray beam size with a diameter less than 0.5 ?m and the estimated photon number of about 2×10 6 ? photons/shot into the spot were achieved.

Tadayuki Ohchi; Naohiro Yamaguchi; Chiemi Fujikawa; Tamio Hara; Katsumi Watanabe; Ibuki Tanaka; Masami Taguchi

2000-01-01T23:59:59.000Z

207

Applications of soft x-ray lasers  

SciTech Connect

The high brightness and short pulse duration of soft x-ray lasers provide unique advantages for novel applications. Imaging of biological specimens using x-ray lasers has been demonstrated by several groups. Other applications to fields such as chemistry, material science, plasma diagnostics, and lithography are beginning to emerge. We review the current status of soft x-ray lasers from the perspective of applications, and present an overview of the applications currently being developed.

Skinner, C.H.

1993-08-01T23:59:59.000Z

208

High speed x-ray beam chopper  

DOE Patents (OSTI)

A fast, economical, and compact x-ray beam chopper with a small mass and a small moment of inertia whose rotation can be synchronized and phase locked to an electronic signal from an x-ray source and be monitored by a light beam is disclosed. X-ray bursts shorter than 2.5 microseconds have been produced with a jitter time of less than 3 ns.

McPherson, Armon (Oswego, IL); Mills, Dennis M. (Naperville, IL)

2002-01-01T23:59:59.000Z

209

The Soft X-ray Polarimeter and Applications at BSRF  

SciTech Connect

A novel compact polarimeter for the use in soft x-ray region having high-precision eight-axis automatically driven and two-axis manually driven equipped with multilayer polarizers was developed at the Beijing Synchrotron Radiation Facility (BSRF). The polarimeter was designed to utilize reflection and transmission geometry. Four operational modes have been designed and carried out with the polarimeter. Some experiments have been performed by using this polarimeter with various modes.

Cui Mingqi; Sun Lijuan; Zhu, Jie; Chen Kai; Yan Fen; Zheng Lei; Zhao Yidong [Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, 100049 (China); Wang Zhanshan; Zhu Jingtao [Department of Physics, Tongji University, Shanghai, 200092 (China); Xue Song [Shanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai, 201204 (China)

2010-06-23T23:59:59.000Z

210

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma  

E-Print Network (OSTI)

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma P. L plasmas in which efficient x-ray laser frequency near-doubling is expected for a number of available x-ray of coherent x rays and tunable optical radiation may result in tunable coherent x-ray radiation powerful

Kaplan, Alexander

211

Colloid Coalescence with Focused X Rays  

SciTech Connect

We show direct evidence that focused x rays enable us to merge polymer colloidal particles at room temperature. This phenomenon is ascribed to the photochemical scission of colloids with x rays, reducing the molecular weight, glass transition temperature, surface tension, and viscosity of colloids. The observation of the neck bridge growth with time shows that the x-ray-induced colloid coalescence is analogous to viscoelastic coalescence. This finding suggests a feasible protocol of photonic nanofabrication by sintering or welding of polymers, without thermal damage, using x-ray photonics.

Weon, B. M.; Kim, J. T.; Je, J. H. [X-ray Imaging Center, Department of Materials Science and Engineering, Pohang University of Science and Technology, Pohang, 790-784 (Korea, Republic of); Yi, J. M. [Samsung Advanced Institute of Technology, Yongin, Gyeonggi, 446-712 (Korea, Republic of); Wang, S.; Lee, W.-K. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)

2011-07-01T23:59:59.000Z

212

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE  

E-Print Network (OSTI)

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE USER'S HANDBOOK Version 1.0 (June 1994) prepared by John . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Chapter Two: XRMB History

213

X-ray laser microscope apparatus  

DOE Patents (OSTI)

A microscope consisting of an x-ray contact microscope and an optical microscope. The optical, phase contrast, microscope is used to align a target with respect to a source of soft x-rays. The source of soft x-rays preferably comprises an x-ray laser but could comprise a synchrotron or other pulse source of x-rays. Transparent resist material is used to support the target. The optical microscope is located on the opposite side of the transparent resist material from the target and is employed to align the target with respect to the anticipated soft x-ray laser beam. After alignment with the use of the optical microscope, the target is exposed to the soft x-ray laser beam. The x-ray sensitive transparent resist material whose chemical bonds are altered by the x-ray beam passing through the target mater GOVERNMENT LICENSE RIGHTS This invention was made with government support under Contract No. De-FG02-86ER13609 awarded by the Department of Energy. The Government has certain rights in this invention.

Suckewer, Szymon (Princeton, NJ); DiCicco, Darrell S. (Plainsboro, NJ); Hirschberg, Joseph G. (Coral Gables, FL); Meixler, Lewis D. (East Windsor, NJ); Sathre, Robert (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ)

1990-01-01T23:59:59.000Z

214

Automation in X-Ray Crystallography  

Science Journals Connector (OSTI)

Automation in X-Ray Crystallography ... But in the past few years, automation procedures have been applied to intrinsically superior experimental methods. ...

S.C. ABRAHAMS

1963-06-03T23:59:59.000Z

215

Compound refractive X-ray lens  

DOE Patents (OSTI)

An apparatus and method for focusing X-rays. In one embodiment, his invention is a commercial-grade compound refractive X-ray lens. The commercial-grade compound refractive X-ray lens includes a volume of low-Z material. The volume of low-Z material has a first surface which is adapted to receive X-rays of commercially-applicable power emitted from a commercial-grade X-ray source. The volume of low-Z material also has a second surface from which emerge the X-rays of commercially-applicable power which were received at the first surface. Additionally, the commercial-grade compound refractive X-ray lens includes a plurality of openings which are disposed between the first surface and the second surface. The plurality of openings are oriented such that the X-rays of commercially-applicable power which are received at the first surface, pass through the volume of low-Z material and through the plurality openings. In so doing, the X-rays which emerge from the second surface are refracted to a focal point.

Nygren, David R. (Berkeley, CA); Cahn, Robert (Walnut Creek, CA); Cederstrom, Bjorn (Traellborg, SE); Danielsson, Mats (Stocksund, SE); Vestlund, Jonas (Stockholm, SE)

2000-01-01T23:59:59.000Z

216

X-Ray Science Division (XSD)  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Science Division (XSD) Search Button About Welcome Overview Visiting the APS Mission & Goals Find People Organization Charts Committees Job Openings User Information...

217

Quantitative description of microstructure defects in hexagonal boron nitrides using X-ray diffraction analysis  

SciTech Connect

A routine for simultaneous quantification of turbostratic disorder, amount of puckering and the dislocation and stacking fault density in hexagonal materials was proposed and tested on boron nitride powder samples that were synthesised using different methods. The routine allows the individual microstructure defects to be recognised according to their effect on the anisotropy of the X-ray diffraction line broadening. For quantification of the microstructure defects, the total line broadening is regarded as a linear combination of the contributions from the particular defects. The total line broadening is obtained from the line profile fitting. As testing material, graphitic boron nitride (h-BN) was employed in the form of hot-isostatically pressed h-BN, pyrolytic h-BN or a h-BN, which was chemically vapour deposited at a low temperature. The kind of the dominant microstructure defects determined from the broadening of the X-ray diffraction lines was verified by high resolution transmission electron microscopy. Their amount was attempted to be verified by alternative methods. - Highlights: • Reliable method for quantification of microstructure defects in BN was suggested. • The method is based on the analysis of anisotropic XRD line broadening. • This XRD line broadening is unique and characteristic of the respective defect. • Thus, the quantification of coexistent microstructure defects is possible. • The method was tested on hexagonal BN, which was produced by different techniques.

Schimpf, C., E-mail: schimpf@iww.tu-freiberg.de; Motylenko, M.; Rafaja, D.

2013-12-15T23:59:59.000Z

218

Biological Applications and Transmission Electron Microscopy Investigations of Mesoporous Silica Nanoparticles  

SciTech Connect

The research presented and discussed within involves the development of novel biological applications of mesoporous silica nanoparticles (MSN) and an investigation of mesoporous material by transmission electron microscopy (TEM). Mesoporous silica nanoparticles organically functionalized shown to undergo endocytosis in cancer cells and drug release from the pores was controlled intracellularly and intercellularly. Transmission electron microscopy investigations demonstrated the variety of morphologies produced in this field of mesoporous silica nanomaterial synthesis. A series of room-temperature ionic liquid (RTIL) containing mesoporous silica nanoparticle (MSN) materials with various particle morphologies, including spheres, ellipsoids, rods, and tubes, were synthesized. By changing the RTIL template, the pore morphology was tuned from the MCM-41 type of hexagonal mesopores to rotational moire type of helical channels, and to wormhole-like porous structures. These materials were used as controlled release delivery nanodevices to deliver antibacterial ionic liquids against Escherichia coli K12. The involvement of a specific organosiloxane function group, covalently attached to the exterior of fluorescein doped mesoporous silica nanoparticles (FITC-MSN), on the degree and kinetics of endocytosis in cancer and plant cells was investigated. The kinetics of endocystosis of TEG coated FITC-MSN is significantly quicker than FITC-MSN as determined by flow cytometry experiments. The fluorescence confocal microscopy investigation showed the endocytosis of TEG coated-FITC MSN triethylene glycol grafted fluorescein doped MSN (TEG coated-FITC MSN) into both KeLa cells and Tobacco root protoplasts. Once the synthesis of a controlled-release delivery system based on MCM-41-type mesoporous silica nanorods capped by disulfide bonds with superparamagnetic iron oxide nanoparticles was completed. The material was characterized by general methods and the dosage and kinetics of the antioxidant dependent release was measured. Finally, the biological interaction of the material was determined along with TEM measurements. An electron investigation proved that the pore openings of the MSN were indeed blocked by the Fe{sub 3}O{sub 4} nanoparticles. The biological interaction investigation demonstrated Fe{sub 3}O{sub 4}-capped MSN endocytosis into HeLa cells. Not only does the material enter the cells through endocytosis, but it seems that fluorescein was released from the pores most probably caused by disulfide bond reducing molecules, antioxidants. In addition to endocytosis and release, the Fe{sub 3}O{sub 4}-capped MSN propelled the cells across a cuvette upon induction of a magnet force. Finally, an important aspect of materials characterization is transmission electron microscopy. A TEM investigation demonstrated that incorporating different functional groups during the synthesis (co-condensation) changed the particle and pore morphologies.

Brian G. Trewyn

2006-05-01T23:59:59.000Z

219

Materials Small-angle X-ray Scattering (SAXS) | Stanford Synchrotron  

NLE Websites -- All DOE Office Websites (Extended Search)

Materials Small-angle X-ray Scattering (SAXS) Materials Small-angle X-ray Scattering (SAXS) Small Angle X-ray Scattering for Materials Science Small-angle X-ray scattering (SAXS) is a well-established characterization method for microstructure investigations in various materials. It probes electron density differences to give information about structural inhomogeneities from the near atomic scale (1 nm) to the micron scale (1 000 nm). The method involves measuring the scattered X-ray intensity as a function of (typically small) scattering angles and is generally performed in transmission. SAXS is used to characterize the size scale of inhomogeneities (e.g. pores, inclusions, second phase regions) in polymer blends, micro-emulsions, geological materials, bones, cements and ceramics. Instrumentation

220

X-ray spectroscopy of neutron star low-mass X-ray binaries  

E-Print Network (OSTI)

In this thesis, I present work spanning a variety of topics relating to neutron star lowmass X-ray binaries (LMXBs) and utilize spectral information from X-ray observations to further our understanding of these sources. ...

Krauss, Miriam Ilana

2007-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

Ultraluminous X-ray Sources: The most extreme X-ray binaries  

E-Print Network (OSTI)

1 Ultraluminous X-ray Sources: The most extreme X-ray binaries Luca Zampieri INAF ULXs ­ Lubiana ­ May 11, 2012- LZ #12;6 · X-ray observations of nearby galaxies show a population of pointlike, off-nuclear sources with L >> Ledd for 1 Msun (L>1.0e39 erg/s) UltraLuminous X-ray Sources (e

Â?umer, Slobodan

222

X-ray Diffraction (XRD) 1.0 What is X-ray Diffraction  

E-Print Network (OSTI)

X-ray Diffraction (XRD) · 1.0 What is X-ray Diffraction · 2.0 Basics of Crystallography · 3.0 Production of X-rays · 4.0 Applications of XRD · 5.0 Instrumental Sources of Error · 6.0 Conclusions #12 why the cleavage faces of crystals appear to reflect X-ray beams at certain angles of incidence (theta

Moeck, Peter

223

Aneta Siemiginowska Chandra X-ray Center  

E-Print Network (OSTI)

-ray and gamma-ray · High Energy Sky · Chandra X-ray Observatory · examples of typical X-ray data, · an example of a data analysis process · statistical challenges · what do we learn from the data? #12;What is Astronomy and phenomena do we study and how? Solar System: Sun and sollar wind, planets, moons, asteroids, comets Our

Wolfe, Patrick J.

224

Watershed in X-ray Astronomy  

Science Journals Connector (OSTI)

... extent the article on page 96 of this issue of Nature from the X-ray astronomy group at the Massachusetts Institute of Technology is a record of disappointments. That is ... near the galactic centre. Now that the first satellite to be devoted to X-ray astronomy has been launched, and is apparently working successfully, the MIT article and another from ...

1971-01-08T23:59:59.000Z

225

X-Ray Identification of Element 104  

Science Journals Connector (OSTI)

The daughter x-ray identification technique has been applied to the identification of element 104. The characteristic K-series x rays from the ?-decay daughter isotope, nobelium (Z=102), have been observed in coincidence with ? particles from the decay of 4.5-sec 104257, thus providing an unequivocal determination of the parent atomic number, Z=104.

C. E. Bemis; Jr.; R. J. Silva; D. C. Hensley; O. L. Keller; Jr.; J. R. Tarrant; L. D. Hunt; P. F. Dittner; R. L. Hahn; C. D. Goodman

1973-09-03T23:59:59.000Z

226

The Center for X-ray Optics - Now hiring engineers. Apply Today.  

NLE Websites -- All DOE Office Websites (Extended Search)

Database Nanomagnetism X-Ray Microscopy EUV Lithography EUV Mask Database Nanomagnetism X-Ray Microscopy EUV Lithography EUV Mask Imaging Reflectometry Zoneplate Lenses Coherent Optics Nanofabrication Optical Coatings Engineering Education Careers Publications Contact LBNL-Logo The Center for X-Ray Optics is a multi-disciplined research group within Lawrence Berkeley National Laboratory's (LBNL) Materials Sciences Division (MSD). Notice to users. Precision Engineering Building the tools that make nanoscience possible. A high-precision stage fabricated by CXRO's Instrument Fabrication Facility Zone plates Diffractive lenses for a new generation of x-ray beamlines. SEM image of a zoneplate fabricated by CXRO Interferometry Wavefront control with sub-angstrom sensitivity Null interferogram, in preparation for EUV metrology of the SEMATECH Berkeley Microfield Exposure Tool (MET)

227

Zircaloy-2 secondary phase precipitate analysis by X-ray microspectroscopy  

Science Journals Connector (OSTI)

Secondary phase precipitates of a Zircaloy sample have been characterised by X-ray microspectroscopy. In Zircaloy-2 X-ray microscopy reveals pictures with a 40 nm resolution identifying Fe, Cr and to a lower occurrence Ni phases up to size of the micrometer. Analysis by X-ray spectroscopy defines the structure of specific secondary phase precipitates. The feasibility tests demonstrate that the characterisation of Fe and Cr can be performed on 100 nm size phases allowing the analysis of the Fe or Cr atoms environment in these secondary phase precipitates.

C. Degueldre; J. Raabe; G. Kuri; S. Abolhassani

2008-01-01T23:59:59.000Z

228

Online in situ x-ray diffraction setup for structural modification studies during swift heavy ion irradiation  

SciTech Connect

The high energy density of electronic excitations due to the impact of swift heavy ions can induce structural modifications in materials. We present an x-ray diffractometer called ALIX (''Analyse en Ligne sur IRRSUD par diffraction de rayons X''), which has been set up at the low-energy beamline (IRRadiation SUD - IRRSUD) of the Grand Accelerateur National d'Ions Lourds facility, to allow the study of structural modification kinetics as a function of the ion fluence. The x-ray setup has been modified and optimized to enable irradiation by swift heavy ions simultaneously to x-ray pattern recording. We present the capability of ALIX to perform simultaneous irradiation-diffraction by using energy discrimination between x-rays from diffraction and from ion-target interaction. To illustrate its potential, results of sequential or simultaneous irradiation-diffraction are presented in this article to show radiation effects on the structural properties of ceramics. Phase transition kinetics have been studied during xenon ion irradiation of polycrystalline MgO and SrTiO{sub 3}. We have observed that MgO oxide is radiation-resistant to high electronic excitations, contrary to the high sensitivity of SrTiO{sub 3}, which exhibits transition from the crystalline to the amorphous state during irradiation. By interpreting the amorphization kinetics of SrTiO{sub 3}, defect overlapping models are discussed as well as latent track characteristics. Together with a transmission electron microscopy study, we conclude that a single impact model describes the phase transition mechanism.

Grygiel, C.; Lebius, H.; Bouffard, S.; Quentin, A.; Ramillon, J. M.; Madi, T.; Guillous, S.; Been, T.; Guinement, P.; Lelievre, D.; Monnet, I. [CIMAP, CEA-CNRS-ENSICAEN-UCBN, BP 5133, 14070 Caen Cedex 5 (France)

2012-01-15T23:59:59.000Z

229

Quantitative Measurements of X-ray Intensity  

SciTech Connect

This chapter describes the characterization of several X-ray sources and their use in calibrating different types of X-ray cameras at National Security Technologies, LLC (NSTec). The cameras are employed in experimental plasma studies at Lawrence Livermore National Laboratory (LLNL), including the National Ignition Facility (NIF). The sources provide X-rays in the energy range from several hundred eV to 110 keV. The key to this effort is measuring the X-ray beam intensity accurately and traceable to international standards. This is accomplished using photodiodes of several types that are calibrated using radioactive sources and a synchrotron source using methods and materials that are traceable to the U.S. National Institute of Standards and Technology (NIST). The accreditation procedures are described. The chapter begins with an introduction to the fundamental concepts of X-ray physics. The types of X-ray sources that are used for device calibration are described. The next section describes the photodiode types that are used for measuring X-ray intensity: power measuring photodiodes, energy dispersive photodiodes, and cameras comprising photodiodes as pixel elements. Following their description, the methods used to calibrate the primary detectors, the power measuring photodiodes and the energy dispersive photodiodes, as well as the method used to get traceability to international standards are described. The X-ray source beams can then be measured using the primary detectors. The final section then describes the use of the calibrated X-ray beams to calibrate X-ray cameras. Many of the references are web sites that provide databases, explanations of the data and how it was generated, and data calculations for specific cases. Several general reference books related to the major topics are included. Papers expanding some subjects are cited.

Haugh, M. J., Schneider, M.

2011-09-01T23:59:59.000Z

230

Characterization of polysilicon films by Raman spectroscopy and transmission electron microscopy: A comparative study  

SciTech Connect

Samples of chemically-vapor-deposited micrometer and sub-micrometer-thick films of polysilicon were analyzed by transmission electron microscopy (TEM) in cross-section and by Raman spectroscopy with illumination at their surface. TEM and Raman spectroscopy both find varying amounts of polycrystalline and amorphous silicon in the wafers. Raman spectra obtained using blue, green and red excitation wavelengths to vary the Raman sampling depth are compared with TEM cross-sections of these films. Films showing crystalline columnar structures in their TEM micrographs have Raman spectra with a band near 497 cm{sup {minus}1} in addition to the dominant polycrystalline silicon band (521 cm{sup {minus}1}). The TEM micrographs of these films have numerous faulted regions and fringes indicative of nanometer-scale silicon structures, which are believed to correspond to the 497cm{sup {minus}1} Raman band.

Tallant, D.R.; Headley, T.J.; Medernach, J.W. [Sandia National Labs., Albuquerque, NM (United States); Geyling, F. [SEMATECH, Austin, TX (United States)

1993-11-12T23:59:59.000Z

231

Novel scheme for the preparation of transmission electron microscopy specimens with a focused ion beam  

Science Journals Connector (OSTI)

A novel scheme is presented for the preparation of cross?section transmission electron microscopy(TEM) specimens with a focused ion beam(FIB). This scheme is particularly suitable for highly structured substrates such as integrated circuits. The specimen is made by cutting a thin slice of material from the substrate by sputtering with the FIB. The position of the specimen can be selected with submicron resolution. The specimen is subsequently removed from the substrate and transported to a standard TEM?specimen holder. A specimen ready for TEM inspection can be prepared within 2 hs. The samples are of excellent quality as is illustrated with cross?section TEM images of FIB?made specimens of an electrically programmable read?only memory.

M. H. F. Overwijk; F. C. van den Heuvel; C. W. T. Bulle?Lieuwma

1993-01-01T23:59:59.000Z

232

Transmission electron microscopy of oxide dispersion strengthened (ODS) molybdenum: effects of irradiation on material microstructure  

SciTech Connect

Oxide dispersion strengthened (ODS) molybdenum has been characterized using transmission electron microscopy (TEM) to determine the effects of irradiation on material microstructure. This work describes the results-to-date from TEM characterization of unirradiated and irradiated ODS molybdenum. The general microstructure of the unirradiated material consists of fine molybdenum grains (< 5 {micro}m average grain size) with numerous low angle boundaries and isolated dislocation networks. 'Ribbon'-like lanthanum oxides are aligned along the working direction of the product form and are frequently associated with grain boundaries, serving to inhibit grain boundary and dislocation movement. In addition to the 'ribbons', discrete lanthanum oxide particles have also been detected. After irradiation, the material is characterized by the presence of nonuniformly distributed large ({approx} 20 to 100 nm in diameter), multi-faceted voids, while the molybdenum grain size and oxide morphology appear to be unaffected by irradiation.

Baranwal, R. and Burke, M.G.

2003-03-03T23:59:59.000Z

233

Rendering graphene supports hydrophilic with non-covalent aromatic functionalization for transmission electron microscopy  

SciTech Connect

Amorphous carbon films have been routinely used to enhance the preparation of frozen-hydrated samples for transmission electron microscopy (TEM), either in retaining protein concentration, providing mechanical stability or dissipating sample charge. However, strong background signal from the amorphous carbon support obstructs that of the sample, and the insulating properties of thin amorphous carbon films preclude any efficiency in dispersing charge. Graphene addresses the limitations of amorphous carbon. Graphene is a crystalline material with virtually no phase or amplitude contrast and unparalleled, high electrical carrier mobility. However, the hydrophobic properties of graphene have prevented its routine application in Cryo-TEM. This Letter reports a method for rendering graphene TEM supports hydrophilic—a convenient approach maintaining graphene's structural and electrical properties based on non-covalent, aromatic functionalization.

Pantelic, Radosav S., E-mail: pantelic@imbb.forth.gr [National Cancer Institute, 50 South Drive, Building 50, Room 4306, Bethesda, Maryland 20892 (United States); Fu, Wangyang; Schoenenberger, Christian [Department of Physics, University of Basel, Klingelbergstrasse 82, Basel CH-4056 (Switzerland); Stahlberg, Henning [Center for Cellular Imaging and NanoAnalytics, Biozentrum, University of Basel, Mattenstrasse 26, WRO-1058, Basel CH-4058 (Switzerland)

2014-03-31T23:59:59.000Z

234

In situ transmission electron microscopy observation of silver oxidation in ionized/atomic gas.  

SciTech Connect

The interaction between silver and ionized and atomic gas was observed directly by in situ transmission electron microscopy with an environmental cell for the first time. The electron beam provides dual functions as the source of both gas ionization and imaging. The concentration of ionized gas was tuned via adjusting the current density of the electron beam. Oxidation of the silver is observed in situ, indicating the presence of ionized and/or atomic oxygen. The evolution of microstructure and phase constituents was characterized. Then the oxidation rate was measured, and the relationships among grain size, mass transport rate, and electron flux were characterized. The role of the electron beam is discussed, and the results are rationalized with respect to ex situ results from the literature.

Sun, L.; Noh, K. W.; Wen, J-G.; Dillon, S. J. (Materials Science Division); (Massachusetts Inst. Tech.); (Univ. Illinois - Urbana)

2011-10-17T23:59:59.000Z

235

Micro-array collimators for X-rays and neutrons  

SciTech Connect

The authors describe the fabrication techniques of novel, compact optical elements for collimating and/or focusing beams of X-rays or thermal neutrons. These optical elements are solid composite arrays consisting of regular stacks of alternating micro-foils, analogous in action to Soller slit collimators, but up to three orders of magnitude smaller. The arrays are made of alternating metals with suitable refractive indices for reflection and/or absorption of the specific radiation. In one implementation, the arrays are made of stacked micro-foils of transmissive elements (Al, Cu) coated and/or electroplated with absorbing elements (Gd, Cd), which are repeatedly rolled or drawn and restacked to achieve the required collimation parameters. The authors present results of these collimators using both X-rays and neutrons. The performance of the collimating element is limited only by the choice of micro-foil materials and the uniformity of their interfaces.

Cimmino, A.; Allman, B.E.; Klein, A.G. [Univ. of Melbourne, Parkville (Australia). School of Physics; Hamilton, W.A. [Oak Ridge National Lab., TN (United States). Solid State Div.; Anderson, I.S.; Hamelin, B.; Joeghoej, P. [Inst. Laue-Langevin, Grenoble (France); Bastie, P. [Univ. Joseph Fourier-Grenoble, Saint-Martin-d`Heres (France). Lab. de Spectrometrie Physique

1998-08-01T23:59:59.000Z

236

Using nonexponential absorption to demonstrate that anode x rays are polychromatic  

Science Journals Connector (OSTI)

Refinements are reported to the technique suggested by TELTRON for student demonstration of the polychromatic nature of the x rays generated by a conventional x?ray tube such as the TEL?X?OMETER apparatus by observing nonexponential absorption in aluminum. Excluding a linear fit on the semilog plot of transmission versus absorber thickness requires a thorough error analysis propagating the uncertainty estimates. A stored program is described which accomplishes that analysis using the minitab statistics package.

Richard D. Piccard; Sue A. Carter

1989-01-01T23:59:59.000Z

237

X-ray Practicals Series 1 Advanced Data Reduction  

E-Print Network (OSTI)

X-ray Practicals Series 1 Advanced Data Reduction Instructor J. Reibenspies, Ph. D. Nattamai Bhuvanesh, Ph.D. Version 1.0.0 #12;X-ray Practicals Series 2 #12;X-ray Practicals Series 3 #12;X-ray is good. The y direction is shifting the most, but the shift is ok #12;X-ray Practicals Series 5 Other

Meagher, Mary

238

Atomic-Scale Imaging and Spectroscopy for In Situ Liquid Scanning Transmission Electron Microscopy  

SciTech Connect

Observation of growth, synthesis, dynamics and electrochemical reactions in the liquid state is an important yet largely unstudied aspect of nanotechnology. The only techniques that can potentially provide the insights necessary to advance our understanding of these mechanisms is simultaneous atomic-scale imaging and quantitative chemical analysis (through spectroscopy) under environmental conditions in the transmission electron microscope (TEM). In this study we describe the experimental and technical conditions necessary to obtain electron energy loss (EEL) spectra from a nanoparticle in colloidal suspension using aberration corrected scanning transmission electron microscopy (STEM) combined with the environmental liquid stage. At a fluid path length below 400 nm, atomic resolution images can be obtained and simultaneous compositional analysis can be achieved. We show that EEL spectroscopy can be used to quantify the total fluid path length around the nanoparticle, and demonstrate characteristic core-loss signals from the suspended nanoparticles can be resolved and analyzed to provide information on the local interfacial chemistry with the surrounding environment. The combined approach using aberration corrected STEM and EEL spectra with the in situ fluid stage demonstrates a plenary platform for detailed investigations of solution based catalysis and biological research.

Jungjohann, K. L.; Evans, James E.; Aguiar, Jeff; Arslan, Ilke; Browning, Nigel D.

2012-06-04T23:59:59.000Z

239

X-ray sources in globular clusters  

E-Print Network (OSTI)

The twelve bright (Lx>10(36) erg/s) X-ray sources in the globular clusters have lower luminosities than the brightest sources in the bulge of our galaxy. The dim (Lx<10(35) erg/s) X-ray sources in globular clusters reach higher luminosities than the cataclysmic variables in the disk of our galaxy. The first difference is a statistical fluke, as comparison with M31 indicates. The second difference is explained because the brightest of the dim sources are not cataclysmic variables, but soft X-ray transients in quiescence. This article describes the BeppoSAX, ROSAT and first Chandra observations leading to these conclusions.

Frank Verbunt

2001-11-22T23:59:59.000Z

240

X-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND  

E-Print Network (OSTI)

with the occurrence of solar X-ray flare, when light travel time delay is accounted, suggesting that X-rays fromX-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND ANIL BHARDWAJ Flight center, Greenbelt, MD 20771, USA Scattering of solar X-ray radiation mainly produces the non

Ã?stgaard, Nikolai

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art  

E-Print Network (OSTI)

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art diffractometers offering both single crystal and powder X-Ray diffraction. Powder X-Ray Diffraction High resolution data For more details on powder X-Ray analysis contact Dr J Hriljac on 0121 414 4458 or email: j

Birmingham, University of

242

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray Source  

E-Print Network (OSTI)

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray of an intense, tunable, polarized, and quasi-monochromatic X-ray source has been ongoing at Rensselaer Polytechnic Institute since 2001 [1, 2, 3, 4, 5, 6]. This X-ray source, known as Parametric X-rays (PXR

Danon, Yaron

243

X-ray Absorption Spectroscopy of Biologically Relevant Systems  

E-Print Network (OSTI)

308, Messer, B. M. X-ray Absorption Spectroscopy of AqueousSarcosine via X-ray Absorption Spectroscopy 5.1 Introductionwith Carboxylate by X-Ray Absorption Spectroscopy of Liquid

Uejio, Janel Sunayo

2010-01-01T23:59:59.000Z

244

Compact X-Ray Light Source Workshop | EMSL  

NLE Websites -- All DOE Office Websites (Extended Search)

Compact X-Ray Light Source Workshop Compact X-Ray Light Source Workshop Teller R, Terminello L, Thevuthasan T, Moncton D. 2012. "Compact X-Ray Light Source Workshop Report."...

245

APS Bending Magnet X-rays and  

NLE Websites -- All DOE Office Websites (Extended Search)

Irradiation of Nd-Fe-B Permanent Magnets with Irradiation of Nd-Fe-B Permanent Magnets with APS Bending Magnet X-rays and 60 Co γ-rays J. Alderman and P.K. Job APS Operations Division Advanced Photon Source J. Puhl Ionizing Radiation Division National Institute of Standards and Technology June 2000 Table of Contents Introduction Radiation-Induced Demagnetization of Permanent Magnets Resources Required γ-ray Irradiation Results and Analysis of γ-ray Irradiation X-ray Irradiation Results and Analysis of X-ray Irradiation Summary and Conclusions Acknowledgements References Tables and Figures Introduction The Advanced Photon Source (APS), as well as other third-generation synchrotron light sources, uses permanent magnets in the insertion devices to produce x-rays for scientific

246

X-ray source for mammography  

DOE Patents (OSTI)

An x-ray source utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms.

Logan, Clinton M. (Pleasanton, CA)

1994-01-01T23:59:59.000Z

247

Ultrafast X-Ray Sources and Science  

Science Journals Connector (OSTI)

X-ray science is entering the ultrafast and ultraintense era - spurred by developments in coherent, short-wavelength sources that range from tabletop to accelerator-based. These...

Young, Linda

248

X-ray induced optical reflectivity  

The change in optical reflectivity induced by intense x-ray pulses can now be used to study ultrafast many body responses in solids in the femtosecond time domain. X-ray absorption creates photoelectrons and core level holes subsequently filled by Auger or fluorescence processes, and these excitations ultimately add conduction and valence band carriers that perturb optical reflectivity.Optical absorption associated with band filling and band gap narrowing is shown to explain the basic features found in recent measurements on an insulator (silicon nitride, Si3N4), a semiconductor(gallium arsenide,GaAs), and a metal (gold,Au), obtained with ?100 fs x-ray pulses at 500-2000 eV and probed with 800 nm laser pulses. In particular GaAs exhibits an abrupt drop in reflectivity, persisting only for a time comparable to the x-ray excitation pulse duration, consistent with prompt band gap narrowing.

Durbin, Stephen M.

2012-01-01T23:59:59.000Z

249

SMB, X-ray Emission Spectroscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Emission Spectroscopy Beam Line 6-2b X-ray Emission Spectroscopy Beam Line 6-2b is an advanced spectroscopy experimental station on the multidisciplinary general user wiggler Beam...

250

X-raying galaxies: A Chandra legacy  

Science Journals Connector (OSTI)

...Astronomy, University of Massachusetts, Amherst, MA 01003 This presentation...stellar x-ray sources in the solar neighborhood (8). The...elements—Meteoritic and solar . Geochim Cosmochim Acta 53...Astronomy, University of Massachusetts, Amherst, MA 01003, USA...

Q. Daniel Wang

2010-01-01T23:59:59.000Z

251

Small Angle X-Ray Scattering Detector  

DOE Patents (OSTI)

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

Hessler, Jan P.

2004-06-15T23:59:59.000Z

252

X-Ray Nanoimaging: Instruments and Methods  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http:spie.orgOP318 August 28-29, 2013; San Diego, California, USA...

253

Femtosecond X-ray protein nanocrystallography  

NLE Websites -- All DOE Office Websites (Extended Search)

Femtosecond X-ray protein nanocrystallography Authors: Chapman, H.N., Fromme, P., Barty, A., White, T.A., Kirian, R.A., Aquila, A., Hunter, M.S., Schulz, J., DePonte, D.P.,...

254

X-ray source for mammography  

DOE Patents (OSTI)

An x-ray source is described utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms. 6 figures.

Logan, C.M.

1994-12-20T23:59:59.000Z

255

Using X-Ray Computed Tomography in Pore Structure Characterization...  

NLE Websites -- All DOE Office Websites (Extended Search)

Using X-Ray Computed Tomography in Pore Structure Characterization for a Berea Sandstone: Resolution Effect. Using X-Ray Computed Tomography in Pore Structure Characterization for...

256

The Constellation X-ray mission  

Science Journals Connector (OSTI)

The Constellation-X mission is a large collecting area X-ray facility, emphasizing observations at high spectral resolution (E/?E?300–3000) while covering a broad energy band (0.25–40 keV). By increasing the telescope aperture and utilizing efficient spectrometers the mission will achieve a factor of 100 increased sensitivity over current high-resolution X-ray spectroscopy missions. The use of focussing optics across the 10–40 keV band will provide a similar factor of 100 increased sensitivity in this band. Key technologies under development for the mission include lightweight high throughput X-ray optics, multilayer coatings to enhance the hard X-ray performance of X-ray optics, micro-calorimeter spectrometer arrays with 2 eV resolution, low-power and low-weight CCD arrays, lightweight gratings and hard X-ray detectors. When observations commence towards the end of the next decade, Constellation-X will address many pressing questions concerning the extremes of gravity and the evolution of the Universe.

N.E White; H Tananbaum

1999-01-01T23:59:59.000Z

257

X-Ray Observations of Radio Galaxies  

E-Print Network (OSTI)

We review some of the ways that X-ray observations provide unique information on radio galaxies. Thermal bremsstrahlung X-ray emission provides detailed data on ambient densities and temperatures. These parameters in turn can be used for pressure balance calculations and can demonstrate how the ambient gas affects radio source structure. Additionally, many signatures of the interaction of radio jets and lobes with the hot gas are found in high resolution X-ray maps. Non-thermal X-ray emission from knots and hotspots of radio jets can give us constraints on the relativistic electron population for energies greater that that normally sampled in the radio (in the case of synchrotron emission) or can give us an independent estimate of the average magnetic field strength (if inverse Compton emission is the origin of the X-rays). From recent ROSAT HRI observations of 3C 390.3 and 3C 120, we show evidence that X-ray emission from knots and hotspots appears to be associated with regions of large gradients in the radio surface brightness; i.e. at the location of powerful shocks.

D. E. Harris

1998-04-20T23:59:59.000Z

258

Compton backscattered collimated x-ray source  

DOE Patents (OSTI)

A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

Ruth, R.D.; Huang, Z.

1998-10-20T23:59:59.000Z

259

Compton backscattered collmated X-ray source  

DOE Patents (OSTI)

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

2000-01-01T23:59:59.000Z

260

Compton backscattered collimated x-ray source  

DOE Patents (OSTI)

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

1998-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

X-ray views of neutron star low-mass X-ray binaries  

E-Print Network (OSTI)

A neutron star low-mass X-ray binary is a binary stellar system with a neutron star and a low-mass companion star rotating around each other. In this system the neutron star accretes mass from the companion, and as this matter falls into the deep potential well of the neutron star, the gravitational potential energy is released primarily in the X-ray wavelengths. Such a source was first discovered in X-rays in 1962, and this discovery formally gave birth to the "X-ray astronomy". In the subsequent decades, our knowledge of these sources has increased enormously by the observations with several X-ray space missions. Here we give a brief overview of our current understanding of the X-ray observational aspects of these systems.

Sudip Bhattacharyya

2010-02-24T23:59:59.000Z

262

X-ray tomographic image magnification process, system and apparatus therefor  

DOE Patents (OSTI)

A computerized three-dimensional x-ray tomographic microscopy system is disclosed, comprising: a) source means for providing a source of parallel x-ray beams, b) staging means for staging and sequentially rotating a sample to be positioned in the path of the c) x-ray image magnifier means positioned in the path of the beams downstream from the sample, d) detecting means for detecting the beams after being passed through and magnified by the image magnifier means, and e) computing means for analyzing values received from the detecting means, and converting the values into three-dimensional representations. Also disclosed is a process for magnifying an x-ray image, and apparatus therefor.

Kinney, John H. (Danville, CA); Bonse, Ulrich K. (Dortmund, DE); Johnson, Quintin C. (Livermore, CA); Nichols, Monte C. (Livermore, CA); Saroyan, Ralph A. (Livermore, CA); Massey, Warren N. (Livermore, CA); Nusshardt, Rudolph (Waltrop, DE)

1993-01-01T23:59:59.000Z

263

X-ray tomographic image magnification process, system and apparatus therefor  

DOE Patents (OSTI)

A computerized three-dimensional x-ray tomographic microscopy system is disclosed, comprising: (a) source means for providing a source of parallel x-ray beams, (b) staging means for staging and sequentially rotating a sample to be positioned in the path of the (c) x-ray image magnifier means positioned in the path of the beams downstream from the sample, (d) detecting means for detecting the beams after being passed through and magnified by the image magnifier means, and (e) computing means for analyzing values received from the detecting means, and converting the values into three-dimensional representations. Also disclosed is a process for magnifying an x-ray image, and apparatus therefor. 25 figures.

Kinney, J.H.; Bonse, U.K.; Johnson, Q.C.; Nichols, M.C.; Saroyan, R.A.; Massey, W.N.; Nusshardt, R.

1993-09-14T23:59:59.000Z

264

Is linear response to x-rays suitable for digital dental x-ray imaging systems? —Theoretical and experimental considerations  

Science Journals Connector (OSTI)

The purpose of this study was to consider theoretically and experimentally the suitability of linear response to x-rays for digital dental x-ray imaging systems.

Keiichi Nishikawa PhD; Mamoru Wakoh DDS; PhD; Kinya Kuroyanagi DDS; PhD

2003-06-01T23:59:59.000Z

265

TRANSMISSION ELECTRON MICROSCOPY OF Al-RICH SILICATE STARDUST FROM ASYMPTOTIC GIANT BRANCH STARS  

SciTech Connect

We report on transmission electron microscopy (TEM) investigations of two mineralogically unusual stardust silicates to constrain their circumstellar condensation conditions. Both grains were identified by high spatial resolution nano secondary ion mass spectrometry (NanoSIMS) in the Acfer 094 meteorite, one of the most pristine carbonaceous chondrites available for study. One grain is a highly crystalline, highly refractory (Fe content < 0.5 at%), structurally undisturbed orthopyroxene (MgSiO{sub 3}) with an unusually high Al content (1.8 {+-} 0.5 at%). This is the first TEM documentation of a single crystal pyroxene within the complete stardust silicate data set. We interpret the microstructure and chemistry of this grain as being a direct condensate from a gas of locally non-solar composition (i.e., with a higher-than-solar Al content and most likely also a lower-than-solar Mg/Si ratio) at (near)-equilibrium conditions. From the overabundance of crystalline olivine (six reported grains to date) compared to crystalline pyroxene (only documented as a single crystal in this work) we infer that formation of olivine over pyroxene is favored in circumstellar environments, in agreement with expectations from condensation theory and experiments. The second stardust silicate consists of an amorphous Ca-Si rich material which lacks any crystallinity based on TEM observations in which tiny (<20 nm) hibonite nanocrystallites are embedded. This complex assemblage therefore attests to the fast cooling and rapidly changing chemical environments under which dust grains in circumstellar shells form.

Vollmer, Christian [Institute for Mineralogy, University of Muenster, Correnssstr. 24, D-48149 Muenster (Germany); Hoppe, Peter [Max Planck Institute for Chemistry, Particle Chemistry Department, Hahn-Meitner-Weg 1, D-55128 Mainz (Germany); Brenker, Frank E., E-mail: christian.vollmer@wwu.de [Institute of Geoscience/Mineralogy, Goethe-University Frankfurt, Altenhoeferallee 1, D-60438 Frankfurt (Germany)

2013-05-20T23:59:59.000Z

266

X-ray Pinhole Camera Measurements  

SciTech Connect

The development of the rod pinch diode [1] has led to high-resolution radiography for dynamic events such as explosive tests. Rod pinch diodes use a small diameter anode rod, which extends through the aperture of a cathode plate. Electrons borne off the aperture surface can self-insulate and pinch onto the tip of the rod, creating an intense, small x-ray source (Primary Pinch). This source has been utilized as the main diagnostic on numerous experiments that include high-value, single-shot events. In such applications there is an emphasis on machine reliability, x-ray reproducibility, and x-ray quality [2]. In tests with the baseline rod pinch diode, we have observed that an additional pinch (Secondary Pinch) occurs at the interface near the anode rod and the rod holder. This suggests that stray electrons exist that are not associated with the Primary Pinch. In this paper we present measurements on both pinches using an x-ray pinhole camera. The camera is placed downstream of the Primary Pinch at an angle of 60° with respect to the diode centerline. This diagnostic will be employed to diagnose x-ray reproducibility and quality. In addition, we will investigate the performance of hybrid diodes relating to the formation of the Primary and Secondary Pinches.

Nelson, D. S. [NSTec; Berninger, M. J. [NSTec; Flores, P. A. [NSTec; Good, D. E. [NSTec; Henderson, D. J. [NSTec; Hogge, K. W. [NSTec; Huber, S. R. [NSTec; Lutz, S. S. [NSTec; Mitchell, S. E. [NSTec; Howe, R. A. [NSTec; Mitton, C. V. [NSTec; Molina, I. [NSTec; Bozman, D. R. [SNL; Cordova, S. R. [SNL; Mitchell, D. R. [SNL; Oliver, B. V. [SNL; Ormond, E. C. [SNL

2013-07-01T23:59:59.000Z

267

Nonlinear X-ray Compton Scattering  

E-Print Network (OSTI)

X-ray scattering is a weak linear probe of matter. It is primarily sensitive to the position of electrons and their momentum distribution. Elastic X-ray scattering forms the basis of atomic structural determination while inelastic Compton scattering is often used as a spectroscopic probe of both single-particle excitations and collective modes. X-ray free-electron lasers (XFELs) are unique tools for studying matter on its natural time and length scales due to their bright and coherent ultrashort pulses. However, in the focus of an XFEL the assumption of a weak linear probe breaks down, and nonlinear light-matter interactions can become ubiquitous. The field can be sufficiently high that even non-resonant multiphoton interactions at hard X-rays wavelengths become relevant. Here we report the observation of one of the most fundamental nonlinear X-ray-matter interactions, the simultaneous Compton scattering of two identical photons producing a single photon at nearly twice the photon energy. We measure scattered...

Fuchs, Matthias; Chen, Jian; Ghimire, Shambhu; Shwartz, Sharon; Kozina, Michael; Jiang, Mason; Henighan, Thomas; Bray, Crystal; Ndabashimiye, Georges; Bucksbaum, P H; Feng, Yiping; Herrmann, Sven; Carini, Gabriella; Pines, Jack; Hart, Philip; Kenney, Christopher; Guillet, Serge; Boutet, Sebastien; Williams, Garth; Messerschmidt, Marc; Seibert, Marvin; Moeller, Stefan; Hastings, Jerome B; Reis, David A

2015-01-01T23:59:59.000Z

268

Oscillations During Thermonuclear X-ray Bursts  

E-Print Network (OSTI)

High amplitude, nearly coherent X-ray brightness oscillations during thermonuclear X-ray bursts were discovered with the Rossi X-ray Timing Explorer (RXTE) in early 1996. Spectral and timing evidence strongly supports the conclusion that these oscillations are caused by rotational modulation of the burst emission and that they reveal the spin frequency of neutron stars in low mass X-ray binaries, a long sought goal of X-ray astronomy. Studies carried out over the past year have led to the discovery of burst oscillations in four new sources, bringing to ten the number with confirmed burst oscillations. I review the status of our knowledge of these oscillations and indicate how they can be used to probe the physics of neutron stars. For a few burst oscillation sources it has been proposed that the strongest and most ubiquitous frequency is actually the first overtone of the spin frequency and hence that two nearly antipodal hot spots are present on the neutron star. This inference has important implications for both the physics of thermonuclear burning as well as the mass - radius relation for neutron stars, so its confirmation is crucial. I discuss recent attempts to confirm this hypothesis for 4U 1636-53, the source for which a signal at the putative fundamental (290 Hz) has been claimed.

Tod E. Strohmayer

2001-01-12T23:59:59.000Z

269

Predicted X-ray backgrounds for the International X-ray Observatory  

E-Print Network (OSTI)

The background that will be observed by IXO's X-ray detectors naturally separates into two components: (1) a Cosmic X-ray Background (CXB), primarily due to unresolved point sources at high energies (E>2 keV), along with ...

Bautz, Marshall W.

270

Reflection soft X-ray microscope and method  

DOE Patents (OSTI)

A reflection soft X-ray microscope is provided by generating soft X-ray beams, condensing the X-ray beams to strike a surface of an object at a predetermined angle, and focusing the X-ray beams reflected from the surface onto a detector, for recording an image of the surface or near surface features of the object under observation.

Suckewer, Szymon (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ); Rosser, Roy (Princeton, NJ)

1993-01-01T23:59:59.000Z

271

Differential phase contrast X-ray imaging system and components  

DOE Patents (OSTI)

A differential phase contrast X-ray imaging system includes an X-ray illumination system, a beam splitter arranged in an optical path of the X-ray illumination system, and a detection system arranged in an optical path to detect X-rays after passing through the beam splitter.

Stutman, Daniel; Finkenthal, Michael

2014-07-01T23:59:59.000Z

272

X-ray variability in M87  

E-Print Network (OSTI)

We present the evidence for X-ray variability from the core and from knot A in the M87 jet based on data from two observations with the Einstein Observatory High Resolution Imager (HRI) and three observations with the ROSAT HRI. The core intensity showed a 16% increase in 17 months ('79-'80); a 12% increase in the 3 years '92 to '95; and a 17% drop in the last half of 1995. The intensity of knot A appears to have decreased by 16% between 92Jun and 95Dec. Although the core variability is consistent with general expectations for AGN nuclei, the changes in knot A provide constraints on the x-ray emission process and geometry. Thus we predict that the x-ray morphology of knot A will differ significantly from the radio and optical structure.

D. E. Harris; J. A. Biretta; W. Junor

1996-12-05T23:59:59.000Z

273

Displaced Vertices from X-ray Lines  

E-Print Network (OSTI)

We present a simple model of weak-scale thermal dark matter that gives rise to X-ray lines. Dark matter consists of two nearly degenerate states near the weak scale, which are populated thermally in the early universe via co-annihilation with slightly heavier states that are charged under the Standard Model. The X-ray line arises from the decay of the heavier dark matter component into the lighter one via a radiative dipole transition, at a rate that is slow compared to the age of the universe. The model predicts observable signatures at the LHC in the form of exotic events with missing energy and displaced leptons and jets. As an application, we show how this model can explain the recently observed 3.55 keV X-ray line.

Adam Falkowski; Yonit Hochberg; Joshua T. Ruderman

2014-09-09T23:59:59.000Z

274

X-ray focal spot locating apparatus and method  

DOE Patents (OSTI)

An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

Gilbert, Hubert W. (Cedar Crest, NM)

1985-07-30T23:59:59.000Z

275

X-ray Science Division: Groups  

NLE Websites -- All DOE Office Websites (Extended Search)

Division: Groups Division: Groups Atomic, Molecular and Optical Physics (AMO) Primary Contact: Stephen Southworth Work focuses on understanding how strong optical and x-ray fields interact with matter, with an emphasis on photonic control of electronic, atomic and molecular motion. Chemical and Materials Science (CMS) Primary Contact: Randy Winans Research Disciplines: Chemistry, Materials Science Detectors (DET) Primary Contact: Antonino Miceli GMCA Structural Biology Facility (MX) Primary Contact: Robert Fischetti Research Disciplines: Biology, Life Sciences Imaging (IMG) Primary Contact: Francesco DeCarlo Research Disciplines: Materials Science, Biology, Physics, Life Sciences Inelastic X-ray & Nuclear Resonant Scattering (IXN) Primary Contact: Thomas Gog Research Disciplines: Condensed Matter Physics, Geophysics, Materials

276

Cosmology with X-ray Cluster Baryons  

SciTech Connect

X-ray cluster measurements interpreted with a universal baryon/gas mass fraction can theoretically serve as a cosmological distance probe. We examine issues of cosmological sensitivity for current (e.g., Chandra X-ray Observatory, XMM-Newton) and next generation (e.g., Con-X, XEUS) observations, along with systematic uncertainties and biases. To give competitive next generation constraints on dark energy, we find that systematics will need to be controlled to better than 1percent and any evolution in f_gas (and other cluster gas properties) must be calibrated so the residual uncertainty is weaker than (1+z)0.03.

Linder, Eric V.

2007-04-10T23:59:59.000Z

277

Phase recovery for x-ray crystallography  

Science Journals Connector (OSTI)

For many years people have believed that in conventional x-ray crystallography one can only record the diffraction intensities but not the phases. In order to obtain the atomic arrangements, one usually has to guess a structure and then fit the intensity data by refining its parameters. Here, we show that the phases are in fact hidden in the intensity data, and can be directly recovered from the peak profiles. This method is demonstrated by the normal two-beam x-ray diffraction of a noncentrosymmetric crystal, and nontrivial phases are recovered from the intensity data alone.

G. Xu, G. E. Zhou, and X. Y. Zhang

1999-04-01T23:59:59.000Z

278

Time-resolved x-ray diagnostics  

SciTech Connect

Techniques for time-resolved x-ray diagnostics will be reviewed with emphasis on systems utilizing x-ray diodes or scintillators. System design concerns for high-bandwidth (> 1 GHz) diagnostics will be emphasized. The limitations of a coaxial cable system and a technique for equalizing to improve bandwidth of such a system will be reviewed. Characteristics of new multi-GHz amplifiers will be presented. An example of a complete operational system on the Los Alamos Helios laser will be presented which has a bandwidth near 3 GHz over 38 m of coax. The system includes the cable, an amplifier, an oscilloscope, and a digital camera readout.

Lyons, P.B.

1981-01-01T23:59:59.000Z

279

Mapping the Valence States of Transition-Metal Elements Using Energy-Filtered Transmission Electron Microscopy  

E-Print Network (OSTI)

spectrum of MnO2 acquired at 200 kV using a Hitachi HF-2000 transmission electron microscope equipped lines observed in electron energy-loss spectroscopy in a transmission electron microscope (TEMMapping the Valence States of Transition-Metal Elements Using Energy-Filtered Transmission Electron

Wang, Zhong L.

280

Quantitative X-Ray Phase-Contrast Microtomography from a Compact Laser Driven Betatron Source  

E-Print Network (OSTI)

X-ray phase-contrast imaging has recently led to a revolution in resolving power and tissue contrast in biomedical imaging, microscopy and materials science. The necessary high spatial coherence is currently provided by either large-scale synchrotron facilities with limited beamtime access or by microfocus X-ray tubes with rather limited flux. X-rays radiated by relativistic electrons driven by well-controlled high-power lasers offer a promising route to a proliferation of this powerful imaging technology. A laser-driven plasma wave accelerates and wiggles electrons, giving rise to brilliant keV X-ray emission. This so-called Betatron radiation is emitted in a collimated beam with excellent spatial coherence and remarkable spectral stability. Here we present the first phase-contrast micro-tomogram revealing quantitative electron density values of a biological sample using betatron X-rays, and a comprehensive source characterization. Our results suggest that laser-based X-ray technology offers the potential fo...

Wenz, J; Khrennikov, K; Bech, M; Thibault, P; Heigoldt, M; Pfeiffer, F; Karsch, S

2014-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

THREE-DIMENSIONAL IMAGING OF NANOSCALE MATERIALS BY UISNG COHERENT X-RAYS  

SciTech Connect

X-ray crystallography is currently the primary methodology used to determine the 3D structure of materials and macromolecules. However, many nanostructures, disordered materials, biomaterials, hybrid materials and biological specimens are noncrystalline and, hence, their structures are not accessible by X-ray crystallography. Probing these structures therefore requires the employment of different approaches. A very promising technique currently under rapid development is X-ray diffraction microscopy (or lensless imaging), in which the coherent X-ray diffraction pattern of a noncrystalline specimen is measured and then directly phased to obtain a high-resolution image. Through the DOE support over the past three years, we have applied X-ray diffraction microscopy to quantitative imaging of GaN quantum dot particles, and revealed the internal GaN-Ga2O3 core shell structure in three dimensions. By exploiting the abrupt change in the scattering cross-section near electronic resonances, we carried out the first experimental demonstration of resonant X-ray diffraction microscopy for element specific imaging. We performed nondestructive and quantitative imaging of buried Bi structures inside a Si crystal by directly phasing coherent X-ray diffraction patterns acquired below and above the Bi M5 edge. We have also applied X-ray diffraction microscopy to nondestructive imaging of mineral crystals inside biological composite materials - intramuscular fish bone - at the nanometer scale resolution. We identified mineral crystals in collagen fibrils at different stages of mineralization and proposed a dynamic mechanism to account for the nucleation and growth of mineral crystals in the collagen matrix. In addition, we have also discovered a novel 3D imaging modality, denoted ankylography, which allows for complete 3D structure determination without the necessity of sample titling or scanning. We showed that when the diffraction pattern of a finite object is sampled at a sufficiently fine scale on the Ewald sphere, the 3D structure of the object is determined by the 2D spherical pattern. We confirmed the theoretical analysis by performing 3D numerical reconstructions of a sodium silicate glass structure at 2 Ã? resolution from a 2D spherical diffraction pattern alone. As X-ray free electron lasers are under rapid development worldwide, ankylography may open up a new horizon to obtain the 3D structure of a non-crystalline specimen from a single pulse and allow time-resolved 3D structure determination of disordered materials.

Jianwei Miao

2011-04-18T23:59:59.000Z

282

Applying x-ray digital imaging to the verification of cadmium in fuel-storage components  

SciTech Connect

The High Flux Isotope Reactor utilizes large underwater fuel-storage arrays to stage irradiated fuel before it is shipped from the facility. Cadmium is required as a thermal neutron absorber in these fuel-storage arrays to produce an acceptable margin of nuclear subcriticality during both normal and off-normal operating conditions. Due to incomplete documentation from the time of their fabrication, the presence of cadmium within two stainless-steel parts of fuel-storage arrays must be experimentally verified before they are reused in new fuel-storage arrays. A cadmium-verification program has been developed in association with the Waste Examination and Assay Facility located at the Oak Ridge national Laboratory to nondestructively examine these older shroud assemblies. The program includes the following elements (1) x-ray analog imaging, (2) x-ray digital imaging, (3) prompt-gamma-ray spectroscopy measurements, and (4) neutron-transmission measurements. X-ray digital imaging utilizes an analog-to-digital convertor to record attenuated x-ray intensities observed on a fluorescent detector by a video camera. These x-ray intensities are utilized in expressions for cadmium thickness based upon x-ray attenuation theory.

Dabbs, R.D.; Cook, D.H.

1997-03-01T23:59:59.000Z

283

X-Ray Microscopy and Imaging: Science and Research  

NLE Websites -- All DOE Office Websites (Extended Search)

fields: Biology and Life Sciences Environmental Sciences Materials Science Nanoscience Optics and Fundamental Physics Our research often employs the following techniques:...

284

Sharper Focusing of Hard X-rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Sharper Focusing of Hard X-rays FROM: Physics News Update Number 773 #1, April 12, 2006, by Phil Schewe and Ben Stein Note: This text has been slightly modified from the original. Sharper focusing of hard x-rays has been achieved with a device developed at Argonne National Lab. Because of their high energy, x-rays are hard to focus: they can be reflected from a surface but only at a glancing angle (less than a tenth of a degree); they can be refracted but the index of refraction is very close to 1, so that making efficient lenses becomes a problem; and they can be diffracted, but the relatively thick, variable pitch grating required for focusing is tricky to achieve. The Argonne device is of the diffraction type, and it consists of a stack of alternating layers of metal and silicon, made by depositing progressively thicker layers. When the x-rays fall on such a structure, nearly edge-on, what they see is a grating (called a linear zone plate) consisting of a sort of bar-code pattern.

285

Radioactive Thulium for X-Rays  

Science Journals Connector (OSTI)

Radioactive power from thulium makes Argonne x-ray unit a potential for medical and industrial use ... Active component of the instrument is a tiny particle (one-fifth gram) of thulium-170 which has been made radioactive in a heavy water nuclear reactor at Arco, Idaho. ...

1954-05-03T23:59:59.000Z

286

X-ray spectroscopy of manganese clusters  

SciTech Connect

Much of this thesis represents the groundwork necessary in order to probe Mn clusters more productively than with conventional Mn K-edge XAS and is presented in Part 1. Part 2 contains the application of x-ray techniques to Mn metalloproteins and includes a prognosis at the end of each chapter. Individual Mn oxidation states are more readily distinguishable in Mn L-edge spectra. An empirical mixed valence simulation routine for determining the average Mn oxidation state has been developed. The first Mn L-edge spectra of a metalloprotein were measured and interpreted. The energy of Mn K{beta} emission is strongly correlated with average Mn oxidation state. K{beta} results support oxidation states of Mn(III){sub 2}(IV){sub 2} for the S{sub 1} state of Photosystem II chemical chemically reduced preparations contain predominantly Mn(II). A strength and limitation of XAS is that it probes all of the species of a particular element in a sample. It would often be advantageous to selectively probe different forms of the same element. The first demonstration that chemical shifts in x-ray fluorescence energies can be used to obtain oxidation state-selective x-ray absorption spectra is presented. Spin-dependent spectra can also be used to obtain a more simplified picture of local structure. The first spin-polarized extended x-ray absorption fine structure using Mn K{beta} fluorescence detection is shown.

Grush, M.M. [Univ. of California, Davis, CA (United States). Dept. of Applied Science; [Lawrence Berkeley National Lab., CA (United States). Energy and Environment Div.

1996-06-01T23:59:59.000Z

287

Multiple wavelength X-ray monochromators  

DOE Patents (OSTI)

An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focusing the separate first and second output x-ray radiation wavelengths into separate focal points. 3 figs.

Steinmeyer, P.A.

1992-11-17T23:59:59.000Z

288

Small Angle X-Ray Scattering Detector  

DOE Patents (OSTI)

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., q.sub.max /q.sub.min.congruent.100.

Hessler, Jan P. (Downers Grove, IL)

2004-06-15T23:59:59.000Z

289

SLAC All Access: X-ray Microscope  

ScienceCinema (OSTI)

SLAC physicists Johanna Nelson and Yijin Liu give a brief overview of the X-ray microscope at the Stanford Synchrotron Radiation Lightsource (SSRL) that is helping improve rechargeable-battery technology by letting researchers peek into the inner workings of batteries as they operate.

Nelson, Johanna; Liu, Yijin

2014-06-13T23:59:59.000Z

290

Synchrotron x-ray fluorescence and extended x-ray absorption fine structure analysis  

SciTech Connect

The advent of dedicated synchrotron radiation sources has led to a significant increase in activity in many areas of science dealing with the interaction of x-rays with matter. Synchrotron radiation provides intense, linearly polarized, naturally collimated, continuously tunable photon beams, which are used to determine not only the elemental composition of a complex, polyatomic, dilute material but also the chemical form of the elements with improved accuracy. Examples of the application of synchrotron radiation include experiments in synchrotron x-ray fluorescence (SXRF) analysis and extended x-ray absorption fine structure (EXAFS) analysis. New synchrotron radiation x-ray microprobes for elemental analysis in the parts per billion range are under construction at several laboratories. 76 references, 24 figures.

Chen, J.R.; Gordon, B.M.; Hanson, A.L.; Jones, K.W.; Kraner, H.W.; Chao, E.C.T.; Minkin, J.A.

1984-01-01T23:59:59.000Z

291

X-ray imaging crystal spectrometer for extended X-ray sources  

DOE Patents (OSTI)

Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

Bitter, Manfred L. (Princeton, NJ); Fraenkel, Ben (Jerusalem, IL); Gorman, James L. (Bordentown, NJ); Hill, Kenneth W. (Lawrenceville, NJ); Roquemore, A. Lane (Cranbury, NJ); Stodiek, Wolfgang (Princeton, NJ); von Goeler, Schweickhard E. (Princeton, NJ)

2001-01-01T23:59:59.000Z

292

Rise Time Measurement for Ultrafast X-Ray Pulses  

DOE Patents (OSTI)

A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

Celliers, Peter M.; Weber, Franz A.; Moon, Stephen J.

2005-04-05T23:59:59.000Z

293

X-RAY POINT-SOURCE POPULATIONS CONSTITUTING THE GALACTIC RIDGE X-RAY EMISSION  

SciTech Connect

Apparently diffuse X-ray emission has been known to exist along the central quarter of the Galactic Plane since the beginning of X-ray astronomy; this is referred to as the Galactic Ridge X-ray emission (GRXE). Recent deep X-ray observations have shown that numerous X-ray point sources account for a large fraction of the GRXE in the hard band (2-8 keV). However, the nature of these sources is poorly understood. Using the deepest X-ray observations made in the Chandra bulge field, we present the result of a coherent photometric and spectroscopic analysis of individual X-ray point sources for the purpose of constraining their nature and deriving their fractional contributions to the hard-band continuum and Fe K line emission of the GRXE. Based on the X-ray color-color diagram, we divided the point sources into three groups: A (hard), B (soft and broad spectrum), and C (soft and peaked spectrum). The group A sources are further decomposed spectrally into thermal and non-thermal sources with different fractions in different flux ranges. From their X-ray properties, we speculate that the group A non-thermal sources are mostly active galactic nuclei and the thermal sources are mostly white dwarf (WD) binaries such as magnetic and non-magnetic cataclysmic variables (CVs), pre-CVs, and symbiotic stars, whereas the group B and C sources are X-ray active stars in flares and quiescence, respectively. In the log N-log S curve of the 2-8 keV band, the group A non-thermal sources are dominant above Almost-Equal-To 10{sup -14} erg cm{sup -2} s{sup -1}, which is gradually taken over by Galactic sources in the fainter flux ranges. The Fe K{alpha} emission is mostly from the group A thermal (WD binaries) and the group B (X-ray active stars) sources.

Morihana, Kumiko [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan)] [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Tsujimoto, Masahiro; Ebisawa, Ken [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan)] [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan); Yoshida, Tessei, E-mail: morihana@crab.riken.jp [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)] [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)

2013-03-20T23:59:59.000Z

294

Beyond hard x-ray photoelectron spectroscopy: Simultaneous combination with x-ray diffraction  

SciTech Connect

Hard x-ray photoelectron spectroscopy (HAXPES) is a powerful and novel emerging technique for the nondestructive determination of electronic properties and chemical composition of bulk, buried interfaces and surfaces. It benefits from the exceptionally large escape depth of high kinetic energy photoelectrons, increasing the information depth up to several tens of nanometers. Complementing HAXPES with an atomic structure sensitive technique (such as x-ray diffraction) opens a new research field with major applications for materials science. At SpLine, the Spanish CRG beamline at the European Synchrotron Radiation Facility, we have developed a novel experimental set-up that combines HAXPES and x-ray diffraction (x-ray reflectivity, surface x-ray diffraction, grazing incidence x-ray diffraction, and reciprocal space maps). Both techniques can be operated simultaneously on the same sample and using the same excitation source. The set-up includes a robust 2S + 3D diffractometer hosting a ultrahigh vacuum chamber equipped with a unique photoelectron spectrometer (few eV < electron kinetic energy < 15 keV), x-ray tube (Mg/Ti), 15 keV electron gun, and auxiliary standard surface facilities (molecular beam epitaxy evaporator, ion gun, low energy electron diffraction, sample heating/cooling system, leak valves, load-lock sample transfer, etc.). This end-station offers the unique possibility of performing simultaneous HAXPES + x-ray diffraction studies. In the present work, we describe the experimental set-up together with two experimental examples that emphasize its outstanding capabilities: (i) nondestructive characterization of the Si/Ge and HfO{sub 2}/SiO{sub 2} interfaces on Ge-based CMOS devices, and (ii) strain study on La{sub 0.7}Ca{sub 0.3}MnO{sub 3} ultrathin films grown on SrTiO{sub 3}(001) substrate.

Rubio-Zuazo, Juan; Castro, German R. [SpLine, Spanish CRG beamline at the European Synchrotron Radiation Facility, B.P. 220, F-38043 Grenoble (France) and ICMM-CSIC Cantoblanco, E-28049 Madrid (Spain)

2013-05-15T23:59:59.000Z

295

Los Alamos: MST-MTM: EML: Electron Microscopy Laboratory  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron Microscopy Laboratory, MST-6 Electron Microscopy Laboratory, MST-6 MST-6 Home Home In the MSL FEI Tecnai F30 Analytical TEM/STEM JEOL 6300FXV High Resolution SEM JEOL 3000F High Resolution Transmission Electron Microscope Philips XL30 F Scanning Electron Microscope & Orientation Imaging System Phillips CM30 Transmission Electron Microscope In the Sigma Building JEOL 840 EPMA with Wavelength Dispersive Spectroscopy FEI Strata DB235 FIB/SEM FEI XL30 Environmental Scanning Electron Microscope & Orientation Imaging System CONTACTS Bob Field 665.3938 Pat Dickerson 665.3036 Rob Dickerson 667.6337 Rod McCabe 606.1649 The Electron Microscopy Laboratory's Capabilities The Electron Microscopy Laboratory's Capabilities The Electron Microscopy Laboratory (EML) is part of MST-6, the Materials Technology - Metallurgy Group within the Materials Science and Technology Division at Los Alamos National Laboratory. It is a facility dedicated to the characterization of materials primarily through imaging, chemical, and crystallographic analyses of material microstructures with several electron and ion beam instruments. Accessory characterization techniques and equipment include energy dispersive x-ray analysis (EDS), wavelength dispersive x-ray analysis (WDS), electron backscatter diffraction (EBSD) and orientation imaging microscopy (OIM), and electron energy loss spectroscopy (EELS).

296

Scientists combine X-rays and microscopes for precise experiments | Argonne  

NLE Websites -- All DOE Office Websites (Extended Search)

This insulator-coated "smart tip" for synchrotron X-ray scanning tunneling microscopy confines the signal detection to a tiny region of a sample. The nanofabricated tips have been developed by an Argonne team led by Argonne nanoscientist Volker Rose to improve the sensitivity of the SXSTM technique. To view a larger version of the image, click on it. This insulator-coated "smart tip" for synchrotron X-ray scanning tunneling microscopy confines the signal detection to a tiny region of a sample. The nanofabricated tips have been developed by an Argonne team led by Argonne nanoscientist Volker Rose to improve the sensitivity of the SXSTM technique. To view a larger version of the image, click on it. This insulator-coated "smart tip" for synchrotron X-ray scanning tunneling microscopy confines the signal detection to a tiny region of a sample. The nanofabricated tips have been developed by an Argonne team led by Argonne nanoscientist Volker Rose to improve the sensitivity of the SXSTM technique. To view a larger version of the image, click on it. Scientists combine X-rays and microscopes for precise experiments

297

X-rays Illuminate Ancient Archimedes Text  

NLE Websites -- All DOE Office Websites (Extended Search)

Related Links: Related Links: May 2005 Headlines TIP Article Press Release Walters Art Museum SSRL Home Page SLAC Home Page Stanford Home Page Tuesday, 31 May 2005 X-rays Illuminate Ancient Archimedes Text (contact: Uwe Bergmann, bergmann@slac.stanford.edu) Archimedes Figure Image provided by Will Noel, The Walters Art Museum An early transcription of Archimedes' mathematical theories has been brought to light through the probing of high-intensity x-rays at SSRL's BL6-2. The text contains part of the Method of Mechanical Theorems, one of Archimedes' most important works, which was probably copied out by a scribe in the tenth century. The parchment on which it was written was later scraped down and reused as pages in a twelfth century prayer book, producing a document known as a palimpsest (which comes from the Greek,

298

HIGH BRILLIANCE X-RAY SCATTERING FOR  

NLE Websites -- All DOE Office Websites (Extended Search)

BRILLIANCE X-RAY SCATTERING FOR BRILLIANCE X-RAY SCATTERING FOR LIFE SCIENCES (LIX) Group Leader: Lin Yang Proposal Team: O. Bilsel 1 , B. Hsiao 2 , H. Huang 3 , T. Irving 4 , A. Menzel 5 , L. Pollack 6 , C. Riekel 7 , J. Rubert 8 , H. Tsuruta 9 , L. Yang 10 1 University of Massachusetts, 2 Stony Brook University, 3 Rice University, 4 IIT, 5SLS, 6 Cornell University, 7 European Synchrotron Radiation Facility, 8 NEU, 9 Stanford Synchrotron Radiation Lightsource, 10 Brookhaven National Laboratory TECHNIQUES AND CAPABILITIES APPLICATIONS ADDITIONAL INFORMATION * Energy range 2-20keV using undulator source. Simultaneous SAXS/WAXS to cover 0.003-3Å -1 at 12keV with 1 micron spot size * Time-resolved solution scattering with resolution of (1) microseconds to milliseconds using continuous-flow mixing (5µm x 10µm spot size) and (2) milliseconds using stopped-

299

Element 104 identified by characteristic x rays  

Science Journals Connector (OSTI)

A research team at the Oak Ridge National Laboratory has recently announced that they have conclusively identified the 257 isotope of element 104. This new work shows promise of shedding light on the controversy between Albert Ghiorso and Georgi N. Flerov the leaders respectively of the groups at Lawrence Berkeley Laboratory and the Joint Institute for Nuclear Research Dubna. The isotope 104 X 257 decays by alpha emission to 102 No 253 with a half?life of 4.3 seconds. The Oak Ridge group observed the K?series x rays from nobelium in coincidence with the alpha particles from 104 X 257 ; the observation of x?ray spectra has never been reported previously by the Berkeley or Dubna workers according to Curtis E. Bemis Jr spokesman for the group.

Ronald J. Cohn

1973-01-01T23:59:59.000Z

300

X-ray radiography for container inspection  

DOE Patents (OSTI)

Arrangements of X-ray inspection systems are described for inspecting high-z materials in voluminous objects such as containers. Inspection methods may involve generating a radiographic image based on detected attenuation corresponding to a pulsed beams of radiation transmitted through a voluminous object. The pulsed beams of radiation are generated by a high-energy source and transmitted substantially downward along an incident angle, of approximately 1.degree. to 30.degree., to a vertical axis extending through the voluminous object. The generated radiographic image may be analyzed to detect on localized high attenuation representative of high-z materials and to discriminate high-z materials from lower and intermediate-z materials on the basis of the high density and greater attenuation of high-z material for higher energy (3-10 MeV) X-rays, and the compact nature of threatening masses of fissionable materials.

Katz, Jonathan I. (Clayton, MO); Morris, Christopher L. (Los Alamos, NM)

2011-06-07T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

Sample holder for X-ray diffractometry  

DOE Patents (OSTI)

A sample holder for use with X-ray diffractometers with the capability to rotate the sample, as well as to adjust the position of the sample in the x, y, and z directions. Adjustment in the x direction is accomplished through loosening set screws, moving a platform, and retightening the set screws. Motion translators are used for adjustment in the y and z directions. An electric motor rotates the sample, and receives power from the diffractometer.

Hesch, Victor L. (Los Alamos, NM)

1992-01-01T23:59:59.000Z

302

Columbia University X-Ray Measurements  

E-Print Network (OSTI)

V-720 keV · NaI 2x2x2" detector views an energy range of 1 keV-3 MeV Store signal in the tree. computer configuration. Plasmas were created using multi-frequency ECRH, and we find that most of the plasma energy is stored in the fast electrons. The energy spectrum of the x-ray emission below 740 keV is measured

303

Silicon Absolute X-Ray Detectors  

SciTech Connect

The responsivity of silicon photodiodes having no loss in the entrance window, measured using synchrotron radiation in the 1.75 to 60 keV range, was compared to the responsivity calculated using the silicon thickness measured using near-infrared light. The measured and calculated responsivities agree with an average difference of 1.3%. This enables their use as absolute x-ray detectors.

Seely, John F. [Naval Research Laboratory, Washington, D.C. 20375 (United States); Korde, Raj; Sprunck, Jacob [International Radiation Detectors, Inc., Torrance, CA 90505-5243 (United States); Medjoubi, Kadda; Hustache, Stephanie [Synchrotron SOLEIL, L'Orme des Merisiers, Saint-Aubin, BP 48, 91192 Gif-sur-Yvette CEDEX (France)

2010-06-23T23:59:59.000Z

304

Ultrashort x-ray backlighters and applications  

SciTech Connect

Previously, using ultrashort laser pulses focused onto solid targets, we have experimentally studied a controllable ultrafast broadband radiation source in the extreme ultraviolet for time-resolved dynamical studies in ultrafast science [J. Workman, A. Maksimchuk, X. Llu, U. Ellenberger, J. S. Coe, C.-Y. Chien, and D. Umstadter, ``Control of Bright Picosecond X-Ray Emission from Intense Sub- Picosecond Laser-Plasma Interactions,`` Phys. Rev. Lett. 75, 2324 (1995)]. Once armed with a bright ultrafast broadband continuum x-ray source and appropriate detectors, we used the source as a backlighter to study a remotely produced plasma. The application of the source to a problem relevant to high-density matter completes the triad: creating and controlling, efficiently detecting, and applying the source. This work represented the first use of an ultrafast laser- produced x-ray source as a time-resolving probe in an application relevant to atomic, plasma and high-energy-density matter physics. Using the x-ray source as a backlighter, we adopted a pump-probe geometry to investigate the dynamic changes in electronic structure of a thin metallic film as it is perturbed by an ultrashort laser pulse. Because the laser deposits its energy in a skin depth of about 100 {Angstrom} before expansion occurs, up to gigabar pressure shock waves lasting picosecond in duration have been predicted to form in these novel plasmas. This raises the possibility of studying high- energy-density matter relevant to inertial confinement fusion (ICF) and astrophysics in small-scale laboratory experiments. In the past, time-resolved measurements of K-edge shifts in plasmas driven by nanosecond pulses have been used to infer conditions in highly compressed materials. In this study, we used 100-fs laser pulses to impulsively drive shocks into a sample (an untamped 1000 {Angstrom} aluminum film on 2000 {Angstrom} of parylene-n), measuring L-edge shifts.

Umstadter, D., University of Michigan

1997-08-01T23:59:59.000Z

305

X-ray holography at Lawrence Livermore National Laboratory  

SciTech Connect

The x-ray holography program at the Lawrence Livermore National Laboratory has two principal goals: (1) the development of x-ray diffraction techniques for DNA sequence analysis and (2) the development of x-ray laser holography for structural analysis of intact biological cells and organelles. DNA sequence analysis will be accomplished by applying x-ray diffraction techniques to determine the ensemble average of the sequence of labels along the individual elements of crystalline DNA. X-ray laser holographic imaging will be accomplished by applying three dimensional x-ray holography to elucidate the structure of few hundred angstrom objects such as 300 {Angstrom} chromatin fibers, nuclear pores and nucleic acid replication complexes in living cells. Existing laboratory x-ray lasers will be utilized to produce flash x-ray holograms of the biological structures.

Trebes, J.; Annese, C.; Birdsall, D.; Brase, J.; Gray, J.; Lane, S.; London, R.; Matthews, D.; Peters, D.; Pinkel, D.; Stone, G.; Rapp, D.; Rosen, M.; Weier, U.; Yorkey, T.

1990-10-11T23:59:59.000Z

306

X-ray diffraction study of zirconia pillared clays  

Science Journals Connector (OSTI)

X-ray powder diffraction (XRPD) and X-ray radial electronic distribution density (RED) of initial and zirconia-pillared interlayered clays (Zr-PILC) were studied. After pillaring, the basal ... under air to 17.7 ...

D.A. Zyuzin; E.M. Moroz; T.G. Kuznetsova…

2004-01-01T23:59:59.000Z

307

Development of a Schwarzschild-type x-ray microscope  

Science Journals Connector (OSTI)

A Schwarzschild-type x-ray microscope has been designed, constructed, and tested. Ni/C multilayers were used as the x-ray mirrors, with a thickness (2d) of 7 nm and 30 layer pairs. The...

Kado, M; Yamashita, K; Ohtani, M; Tanaka, K A; Kodama, R; Kitamoto, S; Yamanaka, T; Nakai, S

1991-01-01T23:59:59.000Z

308

A Record Run for the APS X-ray Source  

NLE Websites -- All DOE Office Websites (Extended Search)

2004 | 2003 | 2002 | 2001 2000 Subscribe to APS News rss feed A Record Run for the APS X-ray Source FEBRUARY 23, 2012 Bookmark and Share The APS storage ring. X-ray beams and...

309

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscop...  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Refinement Friday, September 28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray...

310

TENDER ENERGY X-RAY ABSORPTION  

NLE Websites -- All DOE Office Websites (Extended Search)

TENDER ENERGY X-RAY ABSORPTION TENDER ENERGY X-RAY ABSORPTION SPECTROSCOPY (TES) Project Team: S. Bare 1,2 , J. Brandes 3 , T. Buonassisi 4 , J. Chen 5,2 , M. Croft 6 , E. DiMasi 7 , A. Frenkel 8,2 , D. Hesterberg 9 , S. Hulbert 7,2 , S. Khalid 7 , S. Myneni 10 , P. Northrup 7,11 , E.T. Rasbury 11 , B. Ravel 12 , R. Reeder 11 , J. Rodriguez 7,2 , D. Sparks 5,13 , V. Stojanoff 7 , G. Waychunas 14 1 UOP LLC, 2 Synchrotron Catalysis Consortium, 3 Skidaway Inst. of Oceanography, 4 MIT Laboratory for Photovoltaics Research, 5 Univ. of Delaware, 6 Rutgers Univ., 7 Brookhaven National Lab, 8 Yeshiva Univ., 9 North Carolina State Univ., 10 Princeton Univ., 11 Stony Brook Univ., 12 NIST, 13 Delaware Environmental Inst., 14 Lawrence Berkeley National Lab TECHNIQUES: High performance and in-situ X-ray absorption spectroscopy and spatially-resolved XAS of

311

The X-ray Telescope of CAST  

E-Print Network (OSTI)

The Cern Axion Solar Telescope (CAST) is in operation and taking data since 2003. The main objective of the CAST experiment is to search for a hypothetical pseudoscalar boson, the axion, which might be produced in the core of the sun. The basic physics process CAST is based on is the time inverted Primakoff effect, by which an axion can be converted into a detectable photon in an external electromagnetic field. The resulting X-ray photons are expected to be thermally distributed between 1 and 7 keV. The most sensitive detector system of CAST is a pn-CCD detector combined with a Wolter I type X-ray mirror system. With the X-ray telescope of CAST a background reduction of more than 2 orders off magnitude is achieved, such that for the first time the axion photon coupling constant g_agg can be probed beyond the best astrophysical constraints g_agg < 1 x 10^-10 GeV^-1.

M. Kuster; H. Bräuninger; S. Cébrian; M. Davenport; C. Elefteriadis; J. Englhauser; H. Fischer; J. Franz; P. Friedrich; R. Hartmann; F. H. Heinsius; D. H. H. Hoffmann; G. Hoffmeister; J. N. Joux; D. Kang; K. Königsmann; R. Kotthaus; T. Papaevangelou; C. Lasseur; A. Lippitsch; G. Lutz; J. Morales; A. Rodríguez; L. Strüder; J. Vogel; K. Zioutas

2007-05-10T23:59:59.000Z

312

Applications of holography to x-ray imaging  

SciTech Connect

In this paper we consider various applications of holographic techniques to the problem of soft x-ray imaging. We give special attention to imaging biological material using x-rays in the wavelength range 24 to 45A. We describe some experiments on formation and reconstruction of x-ray holograms and propose some ways in which holographic techniques might contribute to the difficult problem of fabricating optical elements for use in the soft x-ray region.

Howells, M.; Iarocci, M.; Kenney, J.; Rarback, H.; Rosser, R.; Yun, W.

1985-03-01T23:59:59.000Z

313

Applications of holography to X-ray imaging  

SciTech Connect

In this paper the authors consider various applications of holographic techniques to the problem of soft x-ray imaging. Special attention is given to imaging biological material using x-rays in the wavelength range 24-45A. The authors describe some experiments on formation and reconstruction of x-ray holograms and propose some ways in which holographic techniques might contribute to the difficult problem of fabricating optical elements for use in the soft x-ray region.

Howells, M.; Iarocci, M.; Kenney, J.; Rarback, H.; Rosser, R.; Yun, W.

1985-01-01T23:59:59.000Z

314

X-ray MicroCT Training Presentation  

E-Print Network (OSTI)

X-ray MicroCT Training Presentation T. Fettah Kosar, PhD Center for Nanoscale Systems Harvard) Model: HMXST225 (max. 225 kV) #12;Overview 3 Introduction to X-ray imaging and Computed Tomography (CT) · What are X-rays and how do we generate and image them? · How do we magnify X-ray images and keep them

315

THE HARD X-RAY SPECTRUM OF NGC 1365: SCATTERED LIGHT, NOT BLACK HOLE SPIN  

SciTech Connect

Active galactic nuclei (AGNs) show excess X-ray emission above 10 keV compared with extrapolation of spectra from lower energies. Risaliti et al. have recently attempted to model the hard X-ray excess in the type 1.8 AGN NGC 1365, concluding that the hard excess most likely arises from Compton-scattered reflection of X-rays from an inner accretion disk close to the black hole. Their analysis disfavored a model in which the hard excess arises from a high column density of circumnuclear gas partially covering a primary X-ray source, despite such components being required in the NGC 1365 data below 10 keV. Using a Monte Carlo radiative transfer approach, we demonstrate that this conclusion is invalidated by (1) use of slab absorption models, which have unrealistic transmission spectra for partial covering gas, (2) neglect of the effect of Compton scattering on transmitted spectra, and (3) inadequate modeling of the spectrum of scattered X-rays. The scattered spectrum is geometry-dependent and, for high global covering factors, may dominate above 10 keV. We further show that, in models of circumnuclear gas, the suppression of the observed hard X-ray flux by reprocessing may be no larger than required by the ''light bending'' model invoked for inner disk reflection, and the expected emission line strengths lie within the observed range. We conclude that the time-invariant ''red wing'' in AGN X-ray spectra is probably caused by continuum transmitted through and scattered from circumnuclear gas, not by highly redshifted line emission, and that measurement of black hole spin is not possible.

Miller, L. [Department of Physics, Oxford University, Denys Wilkinson Building, Keble Road, Oxford OX1 3RH (United Kingdom); Turner, T. J. [Department of Physics, University of Maryland Baltimore County, Baltimore, MD 21250 (United States)

2013-08-10T23:59:59.000Z

316

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

317

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

318

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

319

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

320

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

322

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Lensless Imaging of Whole Biological Cells with Soft X-Rays Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Wednesday, 26 May 2010 00:00 A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

323

Benchmarking the x-ray phase contrast imaging for ICF DT ice characterization using roughened surrogates  

SciTech Connect

We use x-ray phase contrast imaging to characterize the inner surface roughness of DT ice layers in capsules planned for future ignition experiments. It is therefore important to quantify how well the x-ray data correlates with the actual ice roughness. We benchmarked the accuracy of our system using surrogates with fabricated roughness characterized with high precision standard techniques. Cylindrical artifacts with azimuthally uniform sinusoidal perturbations with 100 um period and 1 um amplitude demonstrated 0.02 um accuracy limited by the resolution of the imager and the source size of our phase contrast system. Spherical surrogates with random roughness close to that required for the DT ice for a successful ignition experiment were used to correlate the actual surface roughness to that obtained from the x-ray measurements. When comparing average power spectra of individual measurements, the accuracy mode number limits of the x-ray phase contrast system benchmarked against surface characterization performed by Atomic Force Microscopy are 60 and 90 for surrogates smoother and rougher than the required roughness for the ice. These agreement mode number limits are >100 when comparing matching individual measurements. We will discuss the implications for interpreting DT ice roughness data derived from phase-contrast x-ray imaging.

Dewald, E; Kozioziemski, B; Moody, J; Koch, J; Mapoles, E; Montesanti, R; Youngblood, K; Letts, S; Nikroo, A; Sater, J; Atherton, J

2008-06-26T23:59:59.000Z

324

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

325

Lensless Imaging of Whole Biological Cells with Soft X-Rays  

NLE Websites -- All DOE Office Websites (Extended Search)

Lensless Imaging of Whole Biological Cells with Soft X-Rays Print Lensless Imaging of Whole Biological Cells with Soft X-Rays Print A team of scientists has used x-ray diffraction microscopy at ALS Beamline 9.0.1 to make images of whole yeast cells, achieving the highest resolution-11 to 13 nanometers (billionths of a meter)-ever obtained with this method for biological specimens. Their success indicates that full 3-D tomography of whole cells at equivalent resolution should soon be possible. The National Center for X-Ray Tomography at ALS Beamline 2.1 images whole, frozen hydrated cells in 3-D (see highlight "Imaging Antifungal Drug Molecules in Action using Soft X-Ray Tomography"). Large numbers of cells can currently be processed in a short time at resolutions of 40 to 60 nanometers, but the ability to increase resolution to the 10-nanometer range would enhance research capabilities in both biology and materials sciences.

326

Studying Fischer-Tropsch catalysts using transmission electron microscopy and model systems of nanoparticles on planar supports.  

SciTech Connect

Nanoparticle model systems on planar supports form a versatile platform for studying morphological and compositional changes of catalysts due to exposure to realistic reaction conditions. We review examples from our work on iron and cobalt catalysts, which can undergo significant rearrangement in the reactive environment of the Fischer-Tropsch synthesis. The use of specially designed, silicon based supports with thin film SiO{sub 2} enables the application of transmission electron microscopy, which has furnished important insight into e.g. the mechanisms of catalyst regeneration.

Thune, P. C.; Weststrate, C. J.; Moodley, P.; Saib, A. M.; van de Loosdrecht, J.; Miller, J. T.; Niemantsverdriet, J. W. (Chemical Sciences and Engineering Division); (Eindhoven Univ. of Technology); (Sasol Technology)

2011-01-01T23:59:59.000Z

327

Quantitative x-ray imager (abstract)  

SciTech Connect

We report on development of a quantitative x-ray imager (QXI) for the national Inertial Confinement Fusion Program. Included in this development is a study of photocathode response as a function of photon energy, 2--17.5 keV, which is related to diagnostic development on the National Ignition Facility (NIF). The QXI is defined as being a quantative imager due to the repeated characterization. This instrument is systematically checked out, electronically as well as its photocathode x-ray response, both on a direct current and pulsed x-ray sources, before and after its use on a shot campaign. The QXI is a gated x-ray imager1 used for a variety of experiments conducted in the Inertial Confinement Fusion and Radiation Physics Program. The camera was assembled in Los Alamos and has been under development since 1997 and has now become the workhorse framing camera by the program. The electronics were built by Grant Applied Physics of San Fransisco, CA.2 The QXI has been used at the LANL Trident, LLNL Nova, and University of Rochester Laboratory OMEGA laser facilities. The camera consists of a grated microchannel plate (MCP), a phosphor coated fiberoptic faceplate coupled to film for data readout, along with high speed electronic pulsers to drive the x-ray detector. The QXI has both a two-strip and a four-strip detection head and has the ability to individually bias the gain of each of the strips. The timing of the QXI was done at the Trident short pulse laboratory, using 211 nm light. Single strip jitter was looked at as well and determined to be <25 ps. Flatfielding of the photocathode across the MCP was done with the Trident main laser with 150 J on a gold disk with a 1 ns. Spatial resolution was determined to be <5 {mu}m by using the same laser conditions as before and a backlit 1000 lp/in. grid. The QXI has been used on cylindrical implosion work at the Nova Laser Facility, and on direct-drive cylinder mix and indirect-drive high convergence implosion experiments at OMEGA. Its two-strip module has provided the capability to look at point backlighters, as part of technique development for experiments on the NIF. Its next use will be in March 2000 with its off axis viewer nose at Omega, providing a perpendicular view of Rayleigh--Taylor spike dissipation.

Evans, Scott C.; Archuleta, Tom N.; Oertel, John A.; Walsh, Peter J.

2001-01-01T23:59:59.000Z

328

Improvement of YOHKOH Hard X-Ray Imaging  

Science Journals Connector (OSTI)

......Figure la shows the X-ray penetration rate through a single, 0.5 mm...index Fig. 1. (a) X-ray penetration rate through a single tung- sten...the K-escape. (b) X-ray penetration rates averaged over the HXT M2 and......

Jun Sato; Takeo Kosugi; Kazuo Makishima

1999-02-01T23:59:59.000Z

329

Small Angle X-ray Scattering (SAXS) Laboratory Learning Experiences  

E-Print Network (OSTI)

.A. & Svergun D.I. (1987). Structure Analysis by Small-Angle X-Ray and Neutron Scattering. NY: Plenum PressSmall Angle X-ray Scattering (SAXS) Laboratory Learning Experiences o - Use of small angle X-ray scattering instrumentation o - Programs that you will use SAXS (BRUKER AXS) PRIMUS (Konarev, Volkov, Koch

Meagher, Mary

330

X-ray Diffraction Laboratory Department of Chemistry  

E-Print Network (OSTI)

X-ray Diffraction Laboratory Department of Chemistry Texas A & M University College Station, Texas Phone : 979-845-9125 www.chem.tamu.edu/xray xray@tamu.edu X-rayDiffractionLaboratory DepartmentofChemistry 3255TAMU CollegeStation,TX77843-3255 Mission The purpose of our laboratory is to provide X-ray

Meagher, Mary

331

X-ray Diffraction Practicals 1 Graphics Programs  

E-Print Network (OSTI)

X-ray Diffraction Practicals 1 Graphics Programs that will read SHELX or CIF files J. Reibenspies, N. Bhuvanesh ver 1.0.0 #12;X-ray Diffraction Practicals 2 Free software. Gretep : Reads SHELX files shelx files or output thermal ellipsoid plots. http://www.umass.edu/microbio/rasmol/ #12;X-ray

Meagher, Mary

332

X-ray Emission from Massive Stars David Cohen  

E-Print Network (OSTI)

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore University, Oct. 13, 2005 astro.swarthmore.edu/~cohen/ #12;Outline 1. What you need to know: a. X-rays from the Sun - magnetic activity, x-ray spectra b. Hot stars c. Radiation-driven winds and the Doppler shift d

Cohen, David

333

X-Ray Photoelectron Spectroscopy XPS Mark Engelhard  

E-Print Network (OSTI)

X-Ray Photoelectron Spectroscopy XPS Mark Engelhard 1 #12;EMSL XPS Instrumentation 2 Physical Electronics Quantera XPS High Energy Resolution Focused X-ray Beam Capability Catalysis reaction and processing chamber with inert atmosphere glove box connected to a PHI Quantera Scanning X-ray Microprobe

334

X-Ray Absorption Spectroscopy of Transition Metal-Magnesium Hydride Thin  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Absorption Spectroscopy of Transition Metal-Magnesium Hydride Thin X-Ray Absorption Spectroscopy of Transition Metal-Magnesium Hydride Thin Films Title X-Ray Absorption Spectroscopy of Transition Metal-Magnesium Hydride Thin Films Publication Type Journal Article LBNL Report Number LBNL-50574 Year of Publication 2002 Authors Richardson, Thomas J., Baker Farangis, Jonathan L. Slack, Ponnusamy Nachimuthu, Rupert C. C. Perera, Nobumichi Tamura, and Michael D. Rubin Journal Journal of Alloys and Compounds Volume 356-357 Start Page 204 Pagination 204-207 Date Published 08/2003 Keywords A. hydrogen storage materials, NEXAFS, thin film s; C. EXAFS, x-ray diffraction Abstract Mixed metal thin films containing magnesium and a first-row transition element exhibit very large changes in both reflectance and transmittance on exposure to hydrogen gas. Changes in electronic structure and coordination of the magnesium and transition metal atoms during hydrogen absorption were studied using dynamic in situ transmission mode X-ray absorption spectroscopy. Mg K-edge and Ni, Co, and Ti L-edge spectra reflect both reversible and irreversible changes in the metal environments. A significant shift in the nickel L absorption edge shows it to be an active participant in hydride formation. The effect on cobalt and titanium is much less dramatic, suggesting that these metals act primarily as catalysts for formation of magnesium hydride.

335

Backscatter x-ray development for space vehicle thermal protection systems  

SciTech Connect

The Backscatter X-Ray (BSX) imaging technique is used for various single sided inspection purposes. Previously developed BSX techniques for spray-on-foam insulation (SOFI) have been used for detecting defects in Space Shuttle External Tank foam insulation. The developed BSX hardware and techniques are currently being enhanced to advance Non-Destructive Evaluation (NDE) methods for future space vehicle applications. Various Thermal Protection System (TPS) materials were inspected using the enhanced BSX imaging techniques, investigating the capability of the method to detect voids and other discontinuities at various locations within each material. Calibration standards were developed for the TPS materials in order to characterize and develop enhanced BSX inspection capabilities. The ability of the BSX technique to detect both manufactured and natural defects was also studied and compared to through-transmission x-ray techniques. The energy of the x-ray, source to object distance, angle of x-ray, focal spot size and x-ray detector configurations were parameters playing a significant role in the sensitivity of the BSX technique to image various materials and defects. The image processing of the results also showed significant increase in the sensitivity of the technique. The experimental results showed BSX to be a viable inspection technique for space vehicle TPS systems.

Bartha, Bence B.; Hope, Dale; Vona, Paul; Born, Martin; Corak, Tony [USA NDE, United Space Alliance, Cape Canaveral, FL 32920 (United States)

2011-06-23T23:59:59.000Z

336

Improved backscatter x-ray detection for anti-terrorist applications  

SciTech Connect

Currently the most common method to determine the contents of a package suspected of containing an explosive device is to use transmission radiography. This technique requires that an x-ray source and film be placed on opposite sides of the package. This poses a problem if the package is placed so that only one side is accessible, such as against a wall. There is also a threat to personnel and property since explosive devices may be booby trapped. The authors have developed a method to x-ray a package using backscattered x-rays based on similar work for landmine detection. This procedure eliminates the use of film behind the target. All of the detection is done from the same side as the source. Backscatter experiments at Sandia National Laboratories have been conducted on mock bombs in packages. They are able to readily identify the bomb components. The images that are obtained in this procedure are done in real time and the image is displayed on a computer screen. Preliminary experiments have also imaged objects within or behind a wall. They are currently using a scanning x-ray source and scintillating plastic detectors. It can take several hours to image a briefcase size object. This time could be reduced if better x-ray detection methods could be used. They have looked at using pinhole photography and CCD cameras to reduce this time.

Shope, S.L.; Lockwood, G.J.; Selph, M.M.; Wehlburg, J.C.

1999-12-01T23:59:59.000Z

337

X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO)  

DOE Data Explorer (OSTI)

The primary interactions of low-energy x-rays within condensed matter, viz. photoabsorption and coherent scattering, are described for photon energies outside the absorption threshold regions by using atomic scattering factors. The atomic scattering factors may be accurately determined from the atomic photoabsorption cross sections using modified Kramers-Kronig dispersion relations. From a synthesis of the currently available experimental data and recent theoretical calculations for photoabsorption, the angle-independent, forward-scattering components of the atomic scattering factors have been thus semiempirically determined and tabulated here for 92 elements and for the region 50-30,000 eV. Atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction. The incoherent scattering contributions that become significant for the light elements at the higher photon energies are similarly determined. The basic x-ray interaction relations that are used in applied x-ray physics are presented here in terms of the atomic scattering factors. The bulk optical constants are also related to the atomic scattering factors. These atomic and optical relations are applied to the detailed calculation of the reflectivity characteristics of a series of practical x-ray mirror, multilayer, and crystal monochromators. Comparisons of the results of this semiempirical,"atom-like", description of x-ray interactions for the low-energy region with those of experiment and ab initio theory are presented.

Henke, B.L.; Gullikson, E.M.; Davis, J.C.

338

Generation of first hard X-ray pulse at Tsinghua Thomson Scattering X-ray Source  

SciTech Connect

Tsinghua Thomson Scattering X-ray Source (TTX) is the first-of-its-kind dedicated hard X-ray source in China based on the Thomson scattering between a terawatt ultrashort laser and relativistic electron beams. In this paper, we report the experimental generation and characterization of the first hard X-ray pulses (51.7 keV) via head-on collision of an 800 nm laser and 46.7 MeV electron beams. The measured yield is 1.0 Multiplication-Sign 10{sup 6} per pulse with an electron bunch charge of 200 pC and laser pulse energy of 300 mJ. The angular intensity distribution and energy spectra of the X-ray pulse are measured with an electron-multiplying charge-coupled device using a CsI scintillator and silicon attenuators. These measurements agree well with theoretical and simulation predictions. An imaging test using the X-ray pulse at the TTX is also presented.

Du Yingchao; Yan Lixin; Hua Jianfei; Du Qiang; Zhang Zhen; Li Renkai; Qian Houjun; Huang Wenhui; Chen Huaibi; Tang Chuanxiang [Accelerator Laboratory, Department of Engineering Physics, Tsinghua University, Beijing 100084 (China); Key Laboratory of Particle and Radiation Imaging, Tsinghua University, Ministry of Education, Beijing 100084 (China); Key Laboratory of High Energy Radiation Imaging Fundamental Science for National Defense, Tsinghua University, Beijing 100084 (China)

2013-05-15T23:59:59.000Z

339

Synchrotron x-ray absorption spectroscopy study of self-assembled nanoparticles synthesized from Fe(acac)3 and Pt(acac)2  

Science Journals Connector (OSTI)

The synchrotron X-ray absorption technique was used to complement electron microscopy in the investigation of nanoparticles synthesized from the coreduction of iron acetylacetonate, Fe(acac)3 and platinum acetylacetonate, Pt(acac)2. ...

K. Chokprasombat; C. Sirisathitkul; P. Harding; S. Chandarak; R. Yimnirun

2012-01-01T23:59:59.000Z

340

Calibration of a gated flat field spectrometer as a function of x-ray intensity  

SciTech Connect

We present an experimental determination of the response of a gated flat-field spectrometer at the Shenguang-II laser facility. X-rays were emitted from a target that was heated by laser beams and then were divided into different intensities with a step aluminum filter and collected by a spectrometer. The transmission of the filter was calibrated using the Beijing Synchrotron Radiation Facility. The response characteristics of the spectrometer were determined by comparing the counts recorded by the spectrometer with the relative intensities of the x-rays transmitted through the step aluminum filter. The response characteristics were used to correct the transmission from two shots of an opacity experiment using the same samples. The transmissions from the two shots are consistent with corrections, but discrepant without corrections.

Xiong, Gang; Yang, Guohong; Li, Hang; Zhang, Jiyan, E-mail: zhangjiyanzjy@sina.com; Zhao, Yang; Hu, Zhimin; Wei, Minxi; Qing, Bo; Yang, Jiamin; Liu, Shenye; Jiang, Shaoen [Research Center of Laser Fusion, China Academy of Engineering Physics, P. O. Box 919-986, Mianyang 621900 (China)] [Research Center of Laser Fusion, China Academy of Engineering Physics, P. O. Box 919-986, Mianyang 621900 (China)

2014-04-15T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Calibrating X-ray Imaging Devices for Accurate Intensity Measurement  

SciTech Connect

The purpose of the project presented is to develop methods to accurately calibrate X-ray imaging devices. The approach was to develop X-ray source systems suitable for this endeavor and to develop methods to calibrate solid state detectors to measure source intensity. NSTec X-ray sources used for the absolute calibration of cameras are described, as well as the method of calibrating the source by calibrating the detectors. The work resulted in calibration measurements for several types of X-ray cameras. X-ray camera calibration measured efficiency and efficiency variation over the CCD. Camera types calibrated include: CCD, CID, back thinned (back illuminated), front illuminated.

Haugh, M. J.

2011-07-28T23:59:59.000Z

342

X-Ray Imaging Crystal Spectrometer for Extended X-Ray Sources  

SciTech Connect

Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokamak fusion experiment to provide spatially and temporally resolved data on plasma parameters such as ion temperature, toroidal and poloidal rotation, electron temperature, impurity ion charge-state distributions, and impurity transport. The imaging properties of these spherically or toroidally curved crystals provide both spectrally and spatially resolved X-ray data from the plasma using only one small spherically or toroidally curved crystal, thus eliminating the requirement for a large array of crystal spectrometers and the need to cross-calibrate the various crystals.

Bitter, Manfred L.; Fraekel, Benjamin; Gorman, James L.; Hill, Kenneth W.; Roquemore, Lane A.; Stodiek, Wolfgang; Goeler, Schweickhard von

1999-05-01T23:59:59.000Z

343

X-Ray Source Based on the Parametric X-Rays  

E-Print Network (OSTI)

Prospects of parametric x-rays (PXR) application for the development of a tuneable quasi-monochromatic x-ray source for medical imaging are discussed. Analysis of basic requirements for electron accelerator shows that it must be relatively low-energy and high-current linac. In comparison with known ultra-relativistic cases, at low energies PXR properties will be modified to a great extent by multiple scattering of the electrons. PXR intensity dependence on target thickness and beam energy are calculated taking multiple scattering into account. It is concluded that PXR source based on real medical accelerators is feasible and can provide x-ray flux needful for obtaining high quality medical images.

Alexander Lobko; Olga Lugovskaya

2005-09-02T23:59:59.000Z

344

Apparatus for monitoring X-ray beam alignment  

DOE Patents (OSTI)

A self-contained, hand-held apparatus is provided for minitoring alignment of an X-ray beam in an instrument employing an X-ray source. The apparatus includes a transducer assembly containing a photoresistor for providing a range of electrical signals responsive to a range of X-ray beam intensities from the X-ray beam being aligned. A circuit, powered by a 7.5 VDC power supply and containing an audio frequency pulse generator whose frequency varies with the resistance of the photoresistor, is provided for generating a range of audible sounds. A portion of the audible range corresponds to low X-ray beam intensity. Another portion of the audible range corresponds to high X-ray beam intensity. The transducer assembly may include an a photoresistor, a thin layer of X-ray fluorescent material, and a filter layer transparent to X-rays but opaque to visible light. X-rays from the beam undergoing alignment penetrate the filter layer and excite the layer of fluorescent material. The light emitted from the fluorescent material alters the resistance of the photoresistor which is in the electrical circuit including the audio pulse generator and a speaker. In employing the apparatus, the X-ray beam is aligned to a complete alignment by adjusting the X-ray beam to produce an audible sound of the maximum frequency.

Steinmeyer, Peter A. (Arvada, CO)

1991-10-08T23:59:59.000Z

345

Introduction to Neutron and X-Ray Scattering  

NLE Websites -- All DOE Office Websites (Extended Search)

Scattering Studies of Thin Scattering Studies of Thin Polymer Films Introduction to Neutron and X-Ray Scattering Sunil K. Sinha UCSD/LANL Acknowledgements: Prof. R.Pynn( Indiana U.) Prof. M.Tolan (U. Dortmund) Wilhelm Conrad Röntgen 1845-1923 1895: Discovery of X-Rays 1901 W. C. Röntgen in Physics for the discovery of x-rays. 1914 M. von Laue in Physics for x-ray diffraction from crystals. 1915 W. H. Bragg and W. L. Bragg in Physics for crystal structure determination. 1917 C. G. Barkla in Physics for characteristic radiation of elements. 1924 K. M. G. Siegbahn in Physics for x-ray spectroscopy. 1927 A. H. Compton in Physics for scattering of x-rays by electrons. 1936 P. Debye in Chemistry for diffraction of x-rays and electrons in gases.

346

Hard X-ray tails and cyclotron features in X-ray pulsars  

E-Print Network (OSTI)

We review the physical processes occurring in the magnetosphere of accreting X-ray pulsars, with emphasis on those processes that give rise to observable effects in their high (E>10 keV) energy spectra. In the second part we compare the empirical spectral laws used to fit the observed spectra with theoretical models, at the light of the BeppoSAX results on the broad-band characterization of the X-ray pulsar continuum, and the discovery of new (multiple) cyclotron resonance features.

Mauro Orlandini; Daniele Dal Fiume

2001-07-27T23:59:59.000Z

347

High efficiency multilayer blazed gratings for EUV and soft X-rays: Recent developments  

SciTech Connect

Multilayer coated blazed gratings with high groove density are the best candidates for use in high resolution EUV and soft x-ray spectroscopy. Theoretical analysis shows that such a grating can be potentially optimized for high dispersion and spectral resolution in a desired high diffraction order without significant loss of diffraction efficiency. In order to realize this potential, the grating fabrication process should provide a perfect triangular groove profile and an extremely smooth surface of the blazed facets. Here we report on recent progress achieved at the Advanced Light Source (ALS) in fabrication of high quality multilayer coated blazed gratings. The blazed gratings were fabricated using scanning beam interference lithography followed by wet anisotropic etching of silicon. A 200 nm period grating coated with a Mo/Si multilayer composed with 30 bi-layers demonstrated an absolute efficiency of 37.6percent in the 3rd diffraction order at 13.6 nm wavelength. The groove profile of the grating was thoroughly characterized with atomic force microscopy before and after the multilayer deposition. The obtained metrology data were used for simulation of the grating efficiency with the vector electromagnetic PCGrate-6.1 code. The simulations showed that smoothing of the grating profile during the multilayer deposition is the main reason for efficiency losses compared to the theoretical maximum. Investigation of the grating with cross-sectional transmission electron microscopy revealed a complex evolution of the groove profile in the course of the multilayer deposition. Impact of the shadowing and smoothing processes on growth of the multilayer on the surface of the sawtooth substrate is discussed.

Voronov, Dmitriy; Ahn, Minseung; Anderson, Erik; Cambie, Rossana; Chang, Chih-Hao; Goray, Leonid; Gullikson, Eric; Heilmann, Ralf; Salmassi, Farhad; Schattenburg, Mark; Warwick, Tony; Yashchuk, Valeriy; Padmore, Howard

2011-07-26T23:59:59.000Z

348

The constellation X-ray mission  

Science Journals Connector (OSTI)

The Constellation-X mission is a large collecting area X-ray facility emphasizing observations at high spectral resolution (E/?E?300–3000) while covering a broad energy band (0.25–40 keV). This mission will achieve a factor of 100 increased sensitivity over current capabilities and is optimized to observe the effects of extreme gravity close to black holes and test models for the formation of large scale structure in the Universe. It is apart of NASA’s strategic plan for launch towards the end of the first decade of the 21st century.

N. E. White; H. Tananbaum

2001-01-01T23:59:59.000Z

349

RYLLA. [X-ray transport code  

SciTech Connect

This paper describes a computer code, RYLLA, which models the deposition of x-rays into thin metal slabs, and transports the resulting photoelectrons, finding the distribution of electrons leaving the slab from both the front and back surfaces. The slab must be homogeneous, but can contain a mixture of up to 5 different elements. Due to the short electron mean free path at low electron energies, RYLLA should be used only for studying thin slabs, roughly < 100 mg/cm/sup 2/ for low Z metals, and < 10 mg/cm/sup 2/ for high Z metals. X-ray energies should be in the range of 1 to 150 keV, as they are deposited only via photoionization and Compton scattering processes. Following photoionization, a hole exists in the electron cloud of the absorbing atom. This fills either by Auger or fluoresence, resulting in lower energy holes which are also filled. Fluoresence photons are transported and absorbed in the same manner as the primary photons, except that they are isotropically produced. Once all photons have been transported and absorbed, and all holes have been filled, a space- and energy-dependent electron source spectrum has been obtained. This is used in a discrete ordinate expansion solution of the 1-D transport equation, which gives the output electron spectra at the two slab surfaces. This paper discusses both the physics and coding of RYLLA. Examples of user input are given, as are some comparisons with other codes.

Hyde, R.A.

1983-06-08T23:59:59.000Z

350

X-Ray Diffraction on NIF  

SciTech Connect

The National Ignition Facility (NIF) is currently a 192 beam, 1.6 MJ laser. NIF Ramp-Compression Experiments have already made the relevant exo-planet pressure range from 1 to 50 Mbar accessible. We Proposed to Study Carbon Phases by X-Ray Diffraction on NIF. Just a few years ago, ultra-high pressure phase diagrams for materials were very 'simple'. New experiments and theories point out surprising and decidedly complex behavior at the highest pressures considered. High pressures phases of aluminum are also predicted to be complex. Recent metadynamics survey of carbon proposed a dynamic pathway among multiple phases. We need to develop diagnostics and techniques to explore this new regime of highly compressed matter science. X-Ray Diffraction - Understand the phase diagram/EOS/strength/texture of materials to 10's of Mbar. Strategy and physics goals: (1) Powder diffraction; (2) Begin with diamond; (3) Continue with metals etc.; (4) Explore phase diagrams; (5) Develop liquid diffraction; and (6) Reduce background/improve resolution.

Eggert, J H; Wark, J

2012-02-15T23:59:59.000Z

351

Gas mixing system for imaging of nanomaterials under dynamic environments by environmental transmission electron microscopy  

SciTech Connect

A gas mixing manifold system that is capable of delivering a stable pressure stream of a desired composition of gases into an environmental transmission electron microscope has been developed. The system is designed to provide a stable imaging environment upon changes of either the composition of the gas mixture or upon switching from one gas to another. The design of the system is described and the response of the pressure inside the microscope, the sample temperature, and sample drift in response to flow and composition changes of the system are reported.

Akatay, M. Cem [School of Materials Engineering and Birck Nanotechnology Center, Purdue University, West Lafayette, Indiana 47907 (United States)] [School of Materials Engineering and Birck Nanotechnology Center, Purdue University, West Lafayette, Indiana 47907 (United States); Zvinevich, Yury; Ribeiro, Fabio H., E-mail: fabio@purdue.edu, E-mail: estach@bnl.gov [Forney Hall of Chemical Engineering, Purdue University, West Lafayette, Indiana 47907 (United States); Baumann, Philipp [Computer Sciences, University of Applied Sciences of Northeastern Switzerland, 4132 Muttenz, Switzerland and Department of Physics, Yeshiva University, New York, New York 10016 (United States)] [Computer Sciences, University of Applied Sciences of Northeastern Switzerland, 4132 Muttenz, Switzerland and Department of Physics, Yeshiva University, New York, New York 10016 (United States); Stach, Eric A., E-mail: fabio@purdue.edu, E-mail: estach@bnl.gov [Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, New York 11973 (United States)

2014-03-15T23:59:59.000Z

352

Development of procedures for refurbishing x-ray optics at the Advanced Light Source  

E-Print Network (OSTI)

Development of procedures for refurbishing x-ray optics atpractical and robust procedures for refurbishing x-ray

Yashchuk, Valeriy V.

2013-01-01T23:59:59.000Z

353

A transmission electron microscopy investigation of inverse melting in Nb{sub 45}Cr{sub 55}  

SciTech Connect

In inverse melting, a supersaturated crystalline phase transforms polymorphously under heat treatment to the amorphous state. Inverse melting of body-centered cubic (bcc) Nb{sub 45}Cr{sub 55} is studied using transmission electron microscopy (TEM) and high resolution TEM (HRTEM). The crystalline to amorphous transformation is heterogeneous, initiating at the bcc grain boundaries. HRTEM reveals 2-3 nm domains with medium range order (MRO) in the amorphous phase. Preferred orientation of MRO domains is found on a scale corresponding to the precursor bcc grain size. Using HRTEM and calorimetry, MRO development in cosputtered Nb{sub 45}Cr{sub 55} films is characterized and compared to that in the amorphous phase produced by inverse melting. {copyright} {ital 1997 Materials Research Society.}

Sinkler, W.; Michaelsen, C.; Bormann, R. [Institute for Materials Research, GKSS Research Center, 21502 Geesthacht (Germany)

1997-07-01T23:59:59.000Z

354

Transmission electron microscopy characterization of laser-clad iron-based alloy on Al-Si alloy  

SciTech Connect

Microstructure characterization is important for controlling the quality of laser cladding. In the present work, a detailed microstructure characterization by transmission electron microscopy was carried out on the iron-based alloy laser-clad on Al-Si alloy and an unambiguous identification of phases in the coating was accomplished. It was found that there is austenite, Cr{sub 7}C{sub 3} and Cr{sub 23}C{sub 6} in the clad region; {alpha}-Al, NiAl{sub 3}, Fe{sub 2}Al{sub 5} and FeAl{sub 2} in the interface region; and {alpha}-Al and silicon in the heat-affected region. A brief discussion was given for their existence based on both kinetic and thermodynamic principles.

Mei, Z. [State Key Lab of Die and Mould Technology, Huazhong University of Science and Technology, Wuhan 430074 (China)]. E-mail: mikemei_99@yahoo.com; Wang, W.Y. [Institute of Materials Science and Engineering, Henan University of Science and Technology, Luoyang 471003 (China); Wang, A.H. [State Key Lab of Die and Mould Technology, Huazhong University of Science and Technology, Wuhan 430074 (China)

2006-04-15T23:59:59.000Z

355

Three-Dimensional Aberration-Corrected Scanning Transmission Electron Microscopy for Biology  

SciTech Connect

Recent instrumental developments have enabled greatly improved resolution of scanning transmission electron microscopes (STEM) through aberration correction. An additional and previously unanticipated advantage of aberration correction is the greatly improved depth sensitivity that has led to the reconstruction of a three-dimensional (3D) image from a focal series. In this chapter the potential of aberration-corrected 3D STEM to provide major improvements in the imaging capabilities for biological samples will be discussed. This chapter contains a brief overview ofthe various high-resolution 3D imaging techniques, a historical perspective of the development of STEM, first estimates of the dose-limited axial and lateral resolution on biological samples and initial experiments on stained thin sections.

De Jonge, Niels [ORNL; Sougrat, Rachid [ORNL; Pennycook, Stephen J [ORNL; Peckys, Diana B [ORNL; Lupini, Andrew R [ORNL

2007-01-01T23:59:59.000Z

356

Photon Sciences | Beamlines | IXS: Inelastic X-ray Scattering  

NLE Websites -- All DOE Office Websites (Extended Search)

IXS: Inelastic X-ray Scattering IXS: Inelastic X-ray Scattering Poster | Fact Sheet | Preliminary Design Report Scientific Scope Many hot topics related to the high frequency dynamics of condensed matter require both a narrower and steeper resolution function and access to a broader dynamic range than what are currently available. This represents a sort of "no man's land" that falls right in the dynamic gap lying between the high frequency spectroscopies, such as inelastic x-ray scattering (IXS), and the low frequency ones. New IXS spectrometers with improved energy and momentum resolutions would be required to fill this gap. To achieve this goal, a new x-ray optics concept for both the monochromatization and energy analysis of x-rays will be implemented at the NSLS-II Inelastic X-ray Scattering beamline. This solution exploits the

357

X-Ray Fluorescence (XRF) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Fluorescence (XRF) X-Ray Fluorescence (XRF) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: X-Ray Fluorescence (XRF) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Lab Analysis Techniques Exploration Sub Group: Rock Lab Analysis Parent Exploration Technique: Rock Lab Analysis Information Provided by Technique Lithology: Bulk and trace element analysis of rocks, minerals, and sediments. Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png X-Ray Fluorescence (XRF): X-Ray Fluorescence is a lab-based technique used for bulk chemical analysis of rock, mineral, sediment, and fluid samples. The technique depends on the fundamental principles of x-ray interactions with solid materials, similar

358

Definition: X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) Jump to: navigation, search Dictionary.png X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) is a laboratory-based technique commonly used for identification of crystalline materials and analysis of unit cell dimensions. One of two primary types of XRD analysis (X-ray powder diffraction and single-crystal XRD) is commonly applied to samples to obtain specific information about the crystalline material under investigation. X-ray powder diffraction is widely used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline substances (typically in less than 20 minutes). A pure, finely ground, and homogenized sample is required for determination of the bulk composition. Additional uses include detailed

359

X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: X-Ray Diffraction (XRD) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Lab Analysis Techniques Exploration Sub Group: Rock Lab Analysis Parent Exploration Technique: Rock Lab Analysis Information Provided by Technique Lithology: Rapid and unambiguous identification of unknown minerals.[1] Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png X-Ray Diffraction (XRD): X-Ray Diffraction (XRD) is a laboratory-based technique commonly used for identification of crystalline materials and analysis of unit cell dimensions. One of two primary types of XRD analysis (X-ray powder diffraction and single-crystal XRD) is commonly applied to samples to

360

Density gradient free electron collisionally excited X-ray laser  

DOE Patents (OSTI)

An operational X-ray laser (30) is provided that amplifies 3p-3s transition X-ray radiation along an approximately linear path. The X-ray laser (30) is driven by a high power optical laser. The driving line focused optical laser beam (32) illuminates a free-standing thin foil (34) that may be associated with a substrate (36) for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the X-ray laser gain medium. The X-ray laser (30) may be driven by more than one optical laser beam (32, 44). The X-ray laser (30) has been successfully demonstrated to function in a series of experimental tests.

Campbell, Edward M. (Pleasanton, CA); Rosen, Mordecai D. (Berkeley, CA)

1989-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

Density gradient free electron collisionally excited x-ray laser  

DOE Patents (OSTI)

An operational x-ray laser is provided that amplifies 3p-3s transition x-ray radiation along an approximately linear path. The x-ray laser is driven by a high power optical laser. The driving line focused optical laser beam illuminates a free-standing thin foil that may be associated with a substrate for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the x-ray laser gain medium. The x-ray laser may be driven by more than one optical laser beam. The x-ray laser has been successfully demonstrated to function in a series of experimental tests.

Campbell, E.M.; Rosen, M.D.

1984-11-29T23:59:59.000Z

362

Formation of microbeam using tabletop soft X-ray laser  

Science Journals Connector (OSTI)

An X-ray microprobe with a sub-micron size beam and high intensity can provide X-ray analyses with a remarkable spatial resolution. We have performed focusing of an X-ray laser output into a sub-micron beam for the first time. In our experiment, an X-ray laser of Li-like Al 3d–4f transition at 15.47 nm was delivered from an unstable cavity consisting of a concave mirror and a flat mirror with a square orifice of 100×100 ?m in size. The beam from the orifice was then focused by using a Schwarzschild mirror coated with a Mo/Si multilayer. An X-ray beam size with a diameter of about 0.45 ?m and an estimated photon number of about 2×106 photons per shot was achieved. Such sources could be well suited for the realization of X-ray microprobes.

Tadayuki Ohchi; Naohiro Yamaguchi; Chiemi Fujikawa; Tamio Hara

1999-01-01T23:59:59.000Z

363

Portable X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

Portable X-Ray Diffraction (XRD) Portable X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: Portable X-Ray Diffraction (XRD) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Field Techniques Exploration Sub Group: Data Collection and Mapping Parent Exploration Technique: Data Collection and Mapping Information Provided by Technique Lithology: Rapid and unambiguous identification of unknown minerals.[1] Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png Portable X-Ray Diffraction (XRD): Portable X-Ray Diffraction (XRD) is a field-based technique that can be used for identification of crystalline materials and analysis of unit cell dimensions. Portable XRD analysis is similar to X-ray powder diffraction,

364

X-ray Pinhole Camera Measurements  

SciTech Connect

The rod pinch diode is made up of a cathode plate and a small diameter anode rod that extends through the cathode hole. The anode is charged positively. The rod tip is made of a high-z material which is chosen for its bremsstrahlung efficiency. When the diode is pulsed it produces an intense x-ray source used for pulsed radiography. The baseline or reference diode consists of a 0.75 mm diameter Tungsten (W) tapered anode rod which extends 10 mm through a 9 mm diameter 3 mm thick aluminum (Al) aperture. The majority of the current in the electron beam is created on the edges of the cathode aperture and when properly configured, the electrons will self insulate, travel down the extension of the rod, and pinch onto the tip of the rod. In this presentation, performance of hybrid diodes will be compared with the baseline diode.

Nelson, D. S. [NSTec; Berninger, M. J. [NSTec; Flores, P. A. [NSTec; Good, D. E. [NSTec; Henderson, D. J. [NSTec; Hogge, K. W. [NSTec; Huber, S. R. [NSTec; Lutz, S. S. [NSTec; Mitchell, S. E. [NSTec; Howe, R. A. [NSTec; Mitton, C. V. [NSTec; Molina, I. [NSTec; Bozman, D. R. [SNL; Cordova, S. R. [SNL; Mitchell, D. R. [SNL; Oliver, B. V. [SNL; Ormond, E. C. [SNL

2013-06-20T23:59:59.000Z

365

Gray scale x-ray mask  

DOE Patents (OSTI)

The present invention describes a method for fabricating an embossing tool or an x-ray mask tool, providing microstructures that smoothly vary in height from point-to-point in etched substrates, i.e., structure which can vary in all three dimensions. The process uses a lithographic technique to transfer an image pattern in the surface of a silicon wafer by exposing and developing the resist and then etching the silicon substrate. Importantly, the photoresist is variably exposed so that when developed some of the resist layer remains. The remaining undeveloped resist acts as an etchant barrier to the reactive plasma used to etch the silicon substrate and therefore provides the ability etch structures of variable depths.

Morales, Alfredo M. (Livermore, CA); Gonzales, Marcela (Seattle, WA)

2006-03-07T23:59:59.000Z

366

Nonlinear optics with focused x-ray lasers  

SciTech Connect

We have investigated the possibility of focusing x-ray lasers with the use of multilayered mirrors or zone plates. The results indicate that x-ray intensities as high as 10{sup 14} W/cm{sup 2} can be achieved by focusing saturated Ne-like x-ray lasers. These intensities should be adequate for studying nonlinear optical phenomena. 9 refs., 2 figs.

DaSilva, L.B.; Muendel, M.H.; Falcone, R.W.; Fields, D.J.; Kortright, J.B.; MacGowan, B.J.; Matthews, D.L.; Mrowka, S.; Shimkaveg, G.M.; Trebes, J.E.

1990-12-12T23:59:59.000Z

367

Process and device for x-ray system quality assurance  

SciTech Connect

This invention relates to medical radiography test systems, and more particularly to a method and apparatus for providing evaluation of a medical or dental x-ray system consisting of x-ray generator, film and processor on a daily basis and to thereby assure the production of useful radiographs from the system with no need to repeat patient exposure because of problems with the x-ray system.

Van Pelt, W.F.; Peterson, R.W.

1982-11-10T23:59:59.000Z

368

On X-Ray Waveguiding in Nanochannels: Channeling Formalism  

E-Print Network (OSTI)

The question on X-ray extreme focusing (smallest reachable spot size) brings us to the idea for using the wave features of X-ray propagation in media. As known, wave features are revealed at propagation in ultra-narrow collimators as well as at glancing reflection from smooth flat and/or strongly curved surfaces. All these phenomena can be described within the general formalism of X-ray channeling.

S. B. Dabagov

2006-11-20T23:59:59.000Z

369

X-Ray Imaging of the Dynamic Magnetic Vortex Core Deformation  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Imaging of the Dynamic X-Ray Imaging of the Dynamic Magnetic Vortex Core Deformation X-Ray Imaging of the Dynamic Magnetic Vortex Core Deformation Print Wednesday, 25 November 2009 00:00 Magnetic thin-film nanostructures can exhibit a magnetic vortex state in which the magnetization vectors lie in the film plane and curl around in a closed loop. At the very center of the vortex, a small, stable core exists where the magnetization points either up or down out of the plane. Three years ago, the discovery of an easy core reversal mechanism at the ALS not only made the possibility of using such systems as magnetic memories much more realistic, it also initiated investigation of the core switching mechanism itself. Now, a Belgian-German-ALS collaboration has used high-resolution, time-resolved, magnetic x-ray microscopy to experimentally reveal the first step of the reversal process: the dynamic deformation of the vortex core. The group also measured a critical vortex velocity above which reversal occurs. Both these observations provide the first experimental support for the postulated reversal mechanism.

370

Atomic-scale X-ray structural analysis of self-assembled monolayers on Silicon  

SciTech Connect

Two related self-assembled monolayers (SAMs), 4-bromostyrene (BrSty) and 4-bromophenylacetylene (BPA), are photochemically grown from solution on to the monohydride-terminated Si(111) surface. The atomic-scale structures of the resulting SAMs are examined by X-ray standing waves (XSW), X-ray reflectivity (XRR), X-ray fluorescence, atomic-force microscopy (AFM), X-ray photoelectron spectroscopy (XPS), and density functional theory (DFT). The coverage is 0.5 ML. The results show that in each case the molecule covalently bonds to a single Si T{sub 1} site and stands up-right with a slight molecular tilt of 17{sup o} that leaves the Br terminal end over a neighboring T{sub 4} site. The Br height is 8.5 {angstrom} (BrSty) and 8.6 {angstrom} (BPA) above the top surface Si atom. The combined XSW and XRR results rule-out two alternative bonding models predicted by DFT that have the root of the molecule bonded to two neighboring top Si surface atoms. Based on the XSW 111 and 333 coherent fractions, the BPA/Si(111) has a reduced vertical Br distribution width in comparison to BrSty. This greater rigidity in the molecular structure is correlated to a C=C bond at the root.

Lin, J.-C.; Kellar, J.A.; Kim, J.-H.; Yoder, N.L.; Bevan, K.H.; Nguyen, S.T.; Hersam, M.C.; Bedzyk, M.J.; (NWU); (Purdue)

2009-04-02T23:59:59.000Z

371

THE GEODESIC X-RAY TRANSFORM WITH FOLD CAUSTICS The ...  

E-Print Network (OSTI)

Aug 28, 2012 ... THE GEODESIC X-RAY TRANSFORM WITH FOLD CAUSTICS. PLAMEN STEFANOV AND GUNTHER UHLMANN. ABSTRACT. We give a ...

2012-08-28T23:59:59.000Z

372

Inelastic X-ray and Nuclear Resonant Scattering  

NLE Websites -- All DOE Office Websites (Extended Search)

... Search About User Information News & Events Science & Education Beamlines Divisions Argonne Home > Advanced Photon Source > Inelastic X-ray and Nuclear Resonant Scattering...

373

Advances in X-Ray Diagnostics of Diesel Fuel Sprays  

Energy.gov (U.S. Department of Energy (DOE))

Recent advances in high-speed X-ray imaging has shown several distinct behaviors of commercial fuel injectors that cannot be seen with more conventional techniques.

374

New intraoral x-ray fluorographic imaging for dentistry  

SciTech Connect

A new dental x-ray fluorographic unit has been developed. This unit is composed of small intraoral x-ray tube, a compact x-ray image intensifier, and a high-resolution TV system. The purposes for developing this equipment were to (1) directly observe the tooth during endodontic procedures and (2) reduce x-ray exposure to the patient and the dentist. The radiation exposure can be reduced to about 1/600 the exposure used with conventional dental film. In clinical trials, a satisfactory fluorographic dental image for endodontic treatment was obtained with this new device.

Higashi, T.; Osada, T.; Aoyama, W.; Iguchi, M.; Suzuki, S.; Kanno, M.; Moriya, K.; Yoshimura, M.; Tusuda, M.

1983-06-01T23:59:59.000Z

375

Normal incidence x-ray mirror for chemical microanalysis  

DOE Patents (OSTI)

An x-ray mirror for both electron column instruments and micro x-ray fluorescence instruments for making chemical, microanalysis comprises a non-planar mirror having, for example, a spherical reflecting surface for x-rays comprised of a predetermined number of alternating layers of high atomic number material and low atomic number material contiguously formed on a substrate and whose layers have a thickness which is a multiple of the wavelength being reflected. For electron column instruments, the wavelengths of interest lie above 1.5nm, while for x-ray fluorescence instruments, the range of interest is below 0.2nm. 4 figs.

Carr, M.J.; Romig, A.D. Jr.

1987-08-05T23:59:59.000Z

376

Self-terminating diffraction gates femtosecond X-ray nanocrystallograp...  

NLE Websites -- All DOE Office Websites (Extended Search)

Self-terminating diffraction gates femtosecond X-ray nanocrystallography measurements Authors: Barty, A., Caleman, C., Aquila, A., Timneanu, N., Lomb, L., White, T. A., Andreasson,...

377

High intensity x-ray source using liquid gallium target  

DOE Patents (OSTI)

A high intensity x-ray source that uses a flowing stream of liquid gallium as a target with the electron beam impinging directly on the liquid metal.

Smither, Robert K. (Hinsdale, IL); Knapp, Gordon S. (Cupertino, CA); Westbrook, Edwin M. (Chicago, IL); Forster, George A. (Westmont, IL)

1990-01-01T23:59:59.000Z

378

X-ray Diffuse Scattering Measurements of Nucleation Dynamics...  

NLE Websites -- All DOE Office Websites (Extended Search)

X-ray Diffuse Scattering Measurements of Nucleation Dynamics at Femtosecond Resolution Real-time measurement and control of the non-equilibrium properties of materials represents...

379

XRMS: X-Ray Spectroscopy of Magnetic Solids  

NLE Websites -- All DOE Office Websites (Extended Search)

XRMS: X-Ray Spectroscopy of Magnetic Solids October 22-23, 2011 SLAC National Accelerator Laboratory, Menlo Park, CA More information...

380

X-ray absorption fine structure and magnetization characterization...  

NLE Websites -- All DOE Office Websites (Extended Search)

characterization of the metallic Co component in Co-doped ZnO thin films . X-ray absorption fine structure and magnetization characterization of the metallic Co...

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

Thermodynamic Prediction of Compositional Phases Confirmed by Transmission Electron Microscopy on Tantalum-Based Alloy Weldments  

SciTech Connect

Tantalum alloys have been used by the U.S. Department of Energy as structural alloys for radioisotope based thermal to electrical power systems since the 1960s. Tantalum alloys are attractive for high temperature structural applications due to their high melting point, excellent formability, good thermal conductivity, good ductility (even at low temperatures), corrosion resistance, and weldability. Tantalum alloys have demonstrated sufficient high-temperature toughness to survive prolonged exposure to the radioisotope power-system working environment. Typically, the fabrication of power systems requires the welding of various components including the structural members made of tantalum alloys. Issues such as thermodynamics, lattice structure, weld pool dynamics, material purity and contamination, and welding atmosphere purity all potentially confound the understanding of the differences between the weldment properties of the different tantalum-based alloys. The objective of this paper is to outline the thermodynamically favorable material phases in tantalum alloys, with and without small amounts of hafnium, during and following solidification, based on the results derived from the FactSage(c) Integrated Thermodynamic Databank. In addition, Transition Electron Microscopy (TEM) data will show for the first time, the changes occurring in the HfC before and after welding, and the data will elucidate the role HfC plays in pinning grain boundaries.

Moddeman, William E.; Birkbeck, Janine C. [BWXT Pantex, Amarillo, Texas 79120-0020 (United States); Barklay, Chadwick D.; Kramer, Daniel P. [University of Dayton Research Institute, Dayton OH 45469-0102 (United States); Miller, Roger G.; Allard, Lawrence F. [Oak Ridge National Laboratory, Oak Ridge, TN 37831-6064 (United States)

2007-01-30T23:59:59.000Z

382

X-ray driven channeling acceleration in crystals and carbon nanotubes  

SciTech Connect

Acceleration of particles channeling in a crystal by means of diffracted x-rays via Bormann anomalous transmission was conceived for heavy ions and muons by Tajima and Cavenago [Phys. Rev. Lett. 59, 1440 (1987)], which potentially offers an appreciably high field gradient on the order of GV/cm. The theoretical model of the high gradient acceleration has been studied in two kinds of atomic structure, crystals and carbon nanotubes (CNTs), with analytic calculations and electromagnetic eigenmode simulations. A range of acceleration gradients and cutoffs of the x-ray power (the lowest power limit to overcome the Bremsstrahlung radiation losses) are characterized in terms of the lattice constants, unit cell sizes, and photon energies. The parametric analysis indicates that the required x-ray power can be reduced to an order of megawatt by replacing crystals with CNTs. Eventually, the equivalent dielectric approximation of a multi-wall nanotube shows that 250–810 MeV muons can be synchronously coupled with x-rays of 0.65–1.32 keV in the accelerating structure.

Shin, Young-Min [Department of Physics, Northern Illinois Center for Accelerator and Detector Development (NICADD), Northern Illinois University, Dekalb, Illinois 60115 (United States) [Department of Physics, Northern Illinois Center for Accelerator and Detector Development (NICADD), Northern Illinois University, Dekalb, Illinois 60115 (United States); Fermi National Accelerator Laboratory, Batavia, Illinois 60510 (United States); Still, Dean A.; Shiltsev, Vladimir [Fermi National Accelerator Laboratory, Batavia, Illinois 60510 (United States)] [Fermi National Accelerator Laboratory, Batavia, Illinois 60510 (United States)

2013-12-15T23:59:59.000Z

383

X-ray laser system, x-ray laser and method  

DOE Patents (OSTI)

Disclosed is an x-ray laser system comprising a laser containing generating means for emitting short wave length radiation, and means external to said laser for energizing said generating means, wherein when the laser is in an operative mode emitting radiation, the radiation has a transverse coherence length to width ratio of from about 0.05 to 1. Also disclosed is a method of adjusting the parameters of the laser to achieve the desired coherence length to laser width ratio.

London, Richard A. (Oakland, CA); Rosen, Mordecai D. (Berkeley, CA); Strauss, Moshe (Omer, IL)

1992-01-01T23:59:59.000Z

384

Constraints on jet X-ray emission in low/hard state X-ray binaries  

E-Print Network (OSTI)

We show that the combination of the similarities between the X-ray properties of low luminosity accreting black holes and accreting neutron stars, combined with the differences in their radio properties argues that the X-rays from these systems are unlikely to be formed in the relativistic jets. Specifically, the spectra of extreme island state neutron stars and low/hard state black holes are known to be indistinguishable, while the power spectra from these systems are known to show only minor differences beyond what would be expected from scaling the characteristic variability frequencies by the mass of the compact object. The spectral and temporal similarities thus imply a common emission mechanism that has only minor deviations from having all key parameters scaling linearly with the mass of the compact object, while we show that this is inconsistent with the observations that the radio powers of neutron stars are typically about 30 times lower than those of black holes at the same X-ray luminosity. We also show that an abrupt luminosity change would be expected when a system makes a spectral state transition from a radiatively inefficient jet dominated accretion flow to a thin disk dominated flow, but that such a change is not seen.

Thomas J. Maccarone

2005-03-31T23:59:59.000Z

385

Isotropic star in low-mass X-ray binaries and X-ray pulsars  

E-Print Network (OSTI)

We present a model for compact stars in the low mass X-ray binaries(LMXBs) and X-ray pulsars using a metric given by John J. Matese and Patrick G. Whitman \\citep{Matese and Whitman1980}. Here the field equations are reduced to a system of two algebraic equations considering the isotropic pressure. Compact star candidates 4U 1820-30(radius=10km) in LMXBs, and Her X-1(radius=7.7km), SAX J 1808.4-3658(SS1)(radius=7.07km) and SAX J 1808.4-3658(SS2)(radius=6.35km) in X-ray pulsars satisfy all the energy conditions, TOV-equation and stability condition. From our model, we have derived mass($M$), central density($\\rho_{0}$), suface density($\\rho_{b}$), central pressure($p_{0}$), surface pressure($p_{b}$) and surface red-shift($Z_{s}$) of the above mentioned stars, which are very much consistant with the observed/reported datas\\citep{N. K. Glendenning1997,Gondek2000}. We have also observe the adiabatic index($\\gamma$>4/3) of the above steller objects.

Mehedi Kalam; Sk. Monowar Hossein; Sajahan Molla

2014-10-01T23:59:59.000Z

386

Burning plasmas with ultrashort soft-x-ray flashing  

SciTech Connect

Fast ignition with narrow-band coherent x-ray pulses has been revisited for cryogenic deuterium-tritium (DT) plasma conditions achieved on the OMEGA Laser System. In contrast to using hard-x-rays (hv = 3-6 keV) proposed in the original x-ray fast-ignition proposal, we find that soft-x-ray sources with hv Almost-Equal-To 500 eV photons can be suitable for igniting the dense DT-plasmas achieved on OMEGA. Two-dimensional radiation-hydrodynamics simulations have identified the break-even conditions for realizing such a 'hybrid' ignition scheme (direct-drive compression with soft-x-ray heating) with 50-{mu}m-offset targets: {approx}10 ps soft-x-ray pulse (hv Almost-Equal-To 500 eV) with a total energy of 500-1000 J to be focused into a 10 {mu}m spot-size. A variety of x-ray pulse parameters have also been investigated for optimization. It is noted that an order of magnitude increase in neutron yield has been predicted even with x-ray energy as low as {approx}50 J. Scaling this idea to a 1 MJ large-scale target, a gain above {approx}30 can be reached with the same soft-x-ray pulse at 1.65 kJ energy. Even though such energetic x-ray sources do not currently exist, we hope that the proposed ignition scheme may stimulate efforts on generating powerful soft-x-ray sources in the near future.

Hu, S. X.; Goncharov, V. N.; Skupsky, S. [Laboratory for Laser Energetics, University of Rochester, 250 East River Road, Rochester, New York 14623-1299 (United States)

2012-07-15T23:59:59.000Z

387

Combined energy dispersive EXAFS and x?ray diffraction  

Science Journals Connector (OSTI)

An in situ experiment to measure both x?ray absorption spectroscopy and x?ray diffraction of aurichalcite is described. The experiment uses position sensitive detectors to enable both data sets to be collected while the sample is slowly decomposed in air and then reduced in hydrogen. ?

A. J. Dent; M. P. Wells; R. C. Farrow; C. A. Ramsdale; G. E. Derbyshire; G. N. Greaves; J. W. Couves; J. M. Thomas

1992-01-01T23:59:59.000Z

388

Fresnel and refractive lenses for X-rays  

Science Journals Connector (OSTI)

We present a Gaussian beam analysis of X-ray refractive and Fresnel lenses. The X-ray refractive lens is featured by an intrinsic soft (Gaussian) aperture due to strong absorption of X-rays by materials. We defined a parameter N0, the critical Fresnel number (CFN), to describe this optical property. The values of N0 for all practical materials are below 1000 for photon energies exceeding 30 eV, still lower for high-Z materials. The maximum effective Fresnel number of a lens is determined by its material to be 2N0 and its maximum enhancement of X-ray intensity is limited to (2?N0)2, independent of its shape. We found that the refractive lens is likely to be useful for manipulating nearly diffraction limited beam in the hard X-ray region and its application is severely restricted by available fabrication capabilities today. X-ray Fresnel lenses, both in cylindrical and linear forms, are proposed as superior focusing elements for hard X-rays. Their high efficiency, up to 100% in optimal construction, will enable us to manipulate beams with multiple lenses and obtain higher performance optics. Their design and fabrication are discussed in reference to those of X-ray Fresnel zone plates and micro Fresnel lenses for optoelectronics.

B.X. Yang

1993-01-01T23:59:59.000Z

389

X-ray attenuation properties of stainless steel (u)  

SciTech Connect

Stainless steel vessels are used to enclose solid materials for studying x-ray radiolysis that involves gas release from the materials. Commercially available stainless steel components are easily adapted to form a static or a dynamic condition to monitor the gas evolved from the solid materials during and after the x-ray irradiation. Experimental data published on the x-ray attenuation properties of stainless steel, however, are very scarce, especially over a wide range of x-ray energies. The objective of this work was to obtain experimental data that will be used to determine how a poly-energetic x-ray beam is attenuated by the stainless steel container wall. The data will also be used in conjunction with MCNP (Monte Carlos Nuclear Particle) modeling to develop an accurate method for determining energy absorbed in known solid samples contained in stainless steel vessels. In this study, experiments to measure the attenuation properties of stainless steel were performed for a range of bremsstrahlung x-ray beams with a maximum energy ranging from 150 keV to 10 MeV. Bremsstrahlung x-ray beams of these energies are commonly used in radiography of engineering and weapon components. The weapon surveillance community has a great interest in understanding how the x-rays in radiography affect short-term and long-term properties of weapon materials.

Wang, Lily L [Los Alamos National Laboratory; Berry, Phillip C [Los Alamos National Laboratory

2009-01-01T23:59:59.000Z

390

Shining Soft X-rays on Magnetic Structures  

Science Journals Connector (OSTI)

...2) demonstrate the power of x-ray magneto-optics in a synchroton study of single crystalline FePd layers, which provides...2) demonstrate the power of x-ray magneto-optics in a synchroton study of single crystalline FePd layers, which provides detailed...

Ulrich Hillebrecht

1999-06-25T23:59:59.000Z

391

Human genome sequencing with direct x-ray holographic imaging  

SciTech Connect

Direct holographic imaging of biological materials is widely applicable to the study of the structure, properties and action of genetic material. This particular application involves the sequencing of the human genome where prospective genomic imaging technology is composed of three subtechnologies, name an x-ray holographic camera, suitable chemistry and enzymology for the preparation of tagged DNA samples, and the illuminator in the form of an x-ray laser. We report appropriate x-ray camera, embodied by the instrument developed by MCR, is available and that suitable chemical and enzymatic procedures exist for the preparation of the necessary tagged DNA strands. Concerning the future development of the x-ray illuminator. We find that a practical small scale x-ray light source is indeed feasible. This outcome requires the use of unconventional physical processes in order to achieve the necessary power-compression in the amplifying medium. The understanding of these new physical mechanisms is developing rapidly. Importantly, although the x-ray source does not currently exist, the understanding of these new physical mechanisms is developing rapidly and the research has established the basic scaling laws that will determine the properties of the x-ray illuminator. When this x-ray source becomes available, an extremely rapid and cost effective instrument for 3-D imaging of biological materials can be applied to a wide range of biological structural assays, including the base-pair sequencing of the human genome and many questions regarding its higher levels of organization.

Rhodes, C.K.

1993-06-08T23:59:59.000Z

392

Twelfth National School on Neutron and X-ray Scattering  

E-Print Network (OSTI)

Twelfth National School on Neutron and X-ray Scattering June 12 � June 26, 2010 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

393

National School on Neutron and X-ray Scattering  

E-Print Network (OSTI)

National School on Neutron and X-ray Scattering May 30 � June 13, 2009 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

394

National School on Neutron and X-ray Scattering  

E-Print Network (OSTI)

15th National School on Neutron and X-ray Scattering August 10 - 24, 2013 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

395

Fourteenth National School on Neutron and X-ray Scattering  

E-Print Network (OSTI)

Fourteenth National School on Neutron and X-ray Scattering August 12 - 25, 2012 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

Pennycook, Steve

396

Thirteenth National School on Neutron and X-ray Scattering  

E-Print Network (OSTI)

Thirteenth National School on Neutron and X-ray Scattering June 11 ­ June 25, 2011 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

397

Neutron and X-ray Scattering Study of Magnetic Manganites  

E-Print Network (OSTI)

Neutron and X-ray Scattering Study of Magnetic Manganites Graeme Eoin Johnstone A Thesis submitted are performed using a variety of neutron scattering and x-ray scattering techniques. The electronic ground for analysing the results of the polarised neutron scattering experiment. There are a large number of people who

Boothroyd, Andrew

398

Sixteenth National School on Neutron and X-ray Scattering  

E-Print Network (OSTI)

Sixteenth National School on Neutron and X-ray Scattering June 14-28, 2014 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major's Neutron Scattering Science Division. Scientific Directors: Suzanne G.E. te Velthuis, Esen Ercan Alp

Pennycook, Steve

399

Tenth National School on Neutron and X-ray Scattering  

E-Print Network (OSTI)

Tenth National School on Neutron and X-ray Scattering September 24 - October 11, 2008 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

400

X-ray spectra transmitted through Compton-thick absorbers  

E-Print Network (OSTI)

X-ray spectra transmitted through matter which is optically thick to Compton scattering are computed by means of Monte Carlo simulations. Applications to the BeppoSAX data of the Seyfert 2 galaxy in Circinus, and to the spectral modeling of the Cosmic X-ray Background, are discussed.

Giorgio Matt; Fulvio Pompilio; Fabio La Franca

1999-04-24T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

Laser Copper Plasma X-ray Source Debris Characterization  

E-Print Network (OSTI)

Laser Copper Plasma X-ray Source Debris Characterization A Thesis Presented by David Hurley 3, 2007 Vice President for Research and Dean of Graduate studies #12;Abstract Laser copper plasma for x-ray lithography. Copper debris in the form of vapor, ions, dust, and high-speed particles

Huston, Dryver R.

402

Millisecond oscillations during thermonuclear X-ray bursts  

E-Print Network (OSTI)

I analyze 68 oscillation trains detected in a search of 159 thermonuclear bursts from eight neutron star X-ray binaries observed with the Rossi X-ray Timing Explorer. I use all data that were public as of September 2001. ...

Muno, Michael Patrick, 1975-

2002-01-01T23:59:59.000Z

403

X rays following the alpha decay of Pa231  

Science Journals Connector (OSTI)

More detailed information is presented concerning the L and K x-ray spectra due to internal conversion of the electromagnetic transitions following the ? decay of Pa231. Some of the difficulties discussed in Ref. 1 are clarified by the new results.[RADIOACTIVITY Pa231; measured L and K Ac x-ray components, ?? and ?XL coin Ac227 deduced levels, ICC.

A. G. de Pinho; L. T. Auler; A. G. da Silva

1974-05-01T23:59:59.000Z

404

Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure  

Science Journals Connector (OSTI)

This paper describes a scheme utilizing a set of low-cost and compact Kirkpatrick-Baez mirrors for upgrading the optical system of the Taiwan Inelastic X-ray Scattering beamline at SPring-8 for high-pressure experiments using diamond-anvil cells. The scheme as implemented improves the focus to 13 µm × 16 µm with transmission of up to 72%.

Huang, C.-Y.

2007-12-18T23:59:59.000Z

405

A Comparison of Mammographic X-ray Spectra: Simulation with EGSnrc and Experiment with CdTe Detector  

Science Journals Connector (OSTI)

......66-04-320-2374, E-mail: khatayut.n@dmsc.mail.go.th 1 Department of Physics...quality Transmission curve and HVL are the standard indices of x-ray beam quality.4...line can become large. Moreover, if the standard condition for the measurement with the......

Khatayut Nigapruke; Patana Puwanich; Nakorn Phaisangittisakul; Wiwat Youngdee

2009-11-01T23:59:59.000Z

406

Transmission electron microscopy and atom probe specimen preparation from mechanically alloyed powder using the focused ion-beam lift-out technique  

Science Journals Connector (OSTI)

......prepared by consolidation of amorphous powders in the supercooled liquid region. Intermetallics (2004) 12:1109-1113. 6 Overwijk M H F , Van Den Heuvel F C, Bulle-Lieuwma C W T. Novel scheme for the preparation of transmission electron microscopy specimens......

Pyuck-Pa Choi; Young-Soon Kwon; Ji-Soon Kim; Tala?at Al-Kassab

2007-04-01T23:59:59.000Z

407

Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic  

NLE Websites -- All DOE Office Websites (Extended Search)

Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Techniques Wednesday, September 5, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Gang Chen Seminar: Structures at atomic scales are traditionally determined through X-ray crystallography that amplifies scattering intensities by introducing spatial periodicity. For amorphous materials and many macromolecules, such as viruses, proteins and biofilms, it is hard to determine structures due to their incapability to crystallize or change of configuration during crystallization. In this talk, I will present the application of X-ray reflectivity and a newly developed fluctuation X-ray scattering technique to study the structures of lipid membranes and randomly oriented nanoparticles. Three different types of domain registrations occurring with

408

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic  

NLE Websites -- All DOE Office Websites (Extended Search)

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Refinement Friday, September 28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray absorption spectroscopy has become an important tool in understanding the electronic structure of materials. Resonant absorption edges in the soft x-ray regime are especially interesting as they allow the study of the lighter elements, such as in organic or organo-metallic substances, as well as important L-edges of the 3d transition metals important in magnetic and oxide systems. Measurements of soft x-ray absorption spectra are inherently surface sensitive, and are plagued by issues such as extinction (in electron yield measurements) or self absorption (in fluorescence yield

409

Incoherent x-ray scattering in single molecule imaging  

E-Print Network (OSTI)

Imaging of the structure of single proteins or other biomolecules with atomic resolution would be enormously beneficial to structural biology. X-ray free-electron lasers generate highly intense and ultrashort x-ray pulses, providing a route towards imaging of single molecules with atomic resolution. The information on molecular structure is encoded in the coherent x-ray scattering signal. In contrast to crystallography there are no Bragg reflections in single molecule imaging, which means the coherent scattering is not enhanced. Consequently, a background signal from incoherent scattering deteriorates the quality of the coherent scattering signal. This background signal cannot be easily eliminated because the spectrum of incoherently scattered photons cannot be resolved by usual scattering detectors. We present an ab initio study of incoherent x-ray scattering from individual carbon atoms, including the electronic radiation damage caused by a highly intense x-ray pulse. We find that the coherent scattering pa...

Slowik, Jan Malte; Dixit, Gopal; Jurek, Zoltan; Santra, Robin

2014-01-01T23:59:59.000Z

410

Transmission  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Transmission Transmission ,... ,...vc- "' ""'\ S I r;. Dr. Jerry Pell, CCM Principal NEP A Document Manager Permitting, Siting, and Analysis (OE-20) Office of Electricity Delivery and Energy Reliability U.S. Department of Energy 1 000 Independence A venue SW Washington, D.C. 20585-0001 Subject: Champlain Hudson Power Express Project Submittal of Amendment Application Dear Dr. Pell: February 28, 2012 On January 25, 2010, Transmission Developers, Inc. ("TDI") submitted on behalf of Champlain Hudson Power Express, Inc. ("CHPEI") an application to the U.S. Department of Energy ("DOE") for a Presidential Permit ("Application) in connection with the Champlain Hudson Power Express project ("Project"). The Application proposed to connect clean sources

411

X-ray Emission from Massive StarsX-ray Emission from Massive Stars David CohenDavid Cohen  

E-Print Network (OSTI)

X-ray Emission from Massive StarsX-ray Emission from Massive Stars David CohenDavid Cohen/s)Velocity (km/s) #12;absorption emission emission occulted emission emission UV telescope side side front back #12;absorption emission emission occulted emission emission UV telescope side side front back #12;The

Cohen, David

412

MICROANALYSIS OF NY/NJ HARBOR SEDIMENTS USING SYNCHROTRON X-RAY BEAMS.  

SciTech Connect

Sediments found in the New York/New Jersey Harbor are widely contaminated with organic and inorganic compounds of anthropogenic origin. As a result, the environmental health of the Harbor has deteriorated and the efficient operation of the Port compromised by difficulties in disposing of sediments resulting from maintenance and improvements of navigational channels. Knowledge of the properties of the sediments on a micro-scale is useful in understanding the transport of contaminants through the environment, for developing effective methods for sediment decontamination, and for subsequent beneficial use of the cleaned sediments. We have investigated several properties of these sediments using synchrotron radiation techniques. These include computed microtomography using absorption and fluorescence contrast mechanisms, x-ray microscopy, microbeam x-ray fluorescence, and Fourier Transform Infrared Spectroscopy (FTIR) for measurements of microstructure, distribution of metals on individual sediment particles, and chemical forms of the contaminants on a micrometer scale. Typical results obtained with these techniques are presented.

JONES,K.W.FENG,H.LANZIROTTI,A.MARINKOVIC,N.ET AL.

2003-12-31T23:59:59.000Z

413

Off-Specular X-ray and Neutron Reflectometry for the Structural Characterization of Buried Interfaces  

SciTech Connect

Off-specular reflectivity or diffuse scattering is sensitive to lateral compositional variations at surfaces and interfaces. It is particularly well-suited as a means of measuring the form and amplitude of surface roughness, as well as separating contributions from physical roughness and gradients in material density. The roughness and lateral correlation lengths of model rough surfaces were cross-correlated using neutron and x-ray off-specular reflectivity (OSNR and OSXR, respectively), and using power spectral density (PSD) analysis of atomic force microscopy (AFM) data. These experiments highlight the advantages of the technique for the investigation of buried interfaces while illustrating how x-ray and neutron techniques work complementarily to measure interfacial roughness.

Lavery, Kristopher A.; Prabhu, Vivek M.; Lin, Eric K.; Wu, Wen-li [Polymers Division and Center for Neutron Research, National Institute of Standards and Technology, Gaithersburg, MD (United States); Satija, Sushil [Center for Neutron Research, National Institute of Standards and Technology, Gaithersburg, MD (United States); Wormington, Matthew [Bede Scientific Inc., Englewood, CO (United States)

2007-09-26T23:59:59.000Z

414

Separating strain from composition in unit cell parameter maps obtained from aberration corrected high resolution transmission electron microscopy imaging  

SciTech Connect

Based on the evaluation of lattice parameter maps in aberration corrected high resolution transmission electron microscopy images, we propose a simple method that allows quantifying the composition and disorder of a semiconductor alloy at the unit cell scale with high accuracy. This is realized by considering, next to the out-of-plane, also the in-plane lattice parameter component allowing to separate the chemical composition from the strain field. Considering only the out-of-plane lattice parameter component not only yields large deviations from the true local alloy content but also carries the risk of identifying false ordering phenomena like formations of chains or platelets. Our method is demonstrated on image simulations of relaxed supercells, as well as on experimental images of an In{sub 0.20}Ga{sub 0.80}N quantum well. Principally, our approach is applicable to all epitaxially strained compounds in the form of quantum wells, free standing islands, quantum dots, or wires.

Schulz, T.; Remmele, T.; Korytov, M.; Markurt, T.; Albrecht, M. [Leibniz-Institut für Kristallzüchtung, Max-Born-Straße 2, 12489 Berlin (Germany); Duff, A.; Lymperakis, L.; Neugebauer, J. [Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf (Germany); Chèze, C. [TopGaN Sp. z o.o., Sokolowska 29/37, 01-142 Warsaw (Poland); Skierbiszewski, C. [TopGaN Sp. z o.o., Sokolowska 29/37, 01-142 Warsaw (Poland); Institute of High Pressure Physics, Polish Academy of Sciences, Sokolowska 29/37, 01-142 Warsaw (Poland)

2014-01-21T23:59:59.000Z

415

Probing the Degradation Mechanisms in Electrolyte Solutions for Li-ion Batteries by In-Situ Transmission Electron Microscopy  

SciTech Connect

One of the goals in the development of new battery technologies is to find new electrolytes with increased electrochemical stability. In-situ (scanning) transmission electron microscopy ((S)TEM) using an electrochemical fluid cell provides the ability to rapidly and directly characterize electrode/electrolyte interfacial reactions under battery relevant electrochemical conditions. Furthermore, as the electron beam itself causes a localized electrochemical reaction when it interacts with the electrolyte, the breakdown products that occur during the first stages of battery operation can potentially be simulated and characterized using a straightforward in-situ liquid stage (without electrochemical biasing capabilities). In this paper, we have studied the breakdown of a range of inorganic/salt complexes that are used in state-of-the-art Li-ion battery systems. The results of the in-situ (S)TEM experiments matches with previous stability tests performed during battery operation and the breakdown products and mechanisms are also consistent with known mechanisms. This analysis indicates that in-situ liquid stage (S)TEM observations can be used to directly test new electrolyte designs and provide structural insights into the origin of the solid electrolyte interphase (SEI) formation mechanism.

Abellan Baeza, Patricia; Mehdi, Beata L.; Parent, Lucas R.; Gu, Meng; Park, Chiwoo; Xu, Wu; Zhang, Yaohui; Arslan, Ilke; Zhang, Jiguang; Wang, Chong M.; Evans, James E.; Browning, Nigel D.

2014-02-21T23:59:59.000Z

416

Atomic-resolution study of polarity reversal in GaSb grown on Si by scanning transmission electron microscopy  

SciTech Connect

The atomic-resolved reversal of the polarity across an antiphase boundary (APB) was observed in GaSb films grown on Si by high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). The investigation of the interface structure at the origin of the APB reveals that coalescence of two domains with Ga-prelayer and Sb-prelayer causes the sublattice reversal. The local strain and lattice rotation distributions of the APB, attributed to the discordant bonding length at the APB with the surrounding GaSb lattice, were further studied using the geometric phase analysis technique. The crystallographic characteristics of the APBs and their interaction with other planar defects were observed with HAADF-STEM. The quantitative agreement between experimental and simulated images confirms the observed polarities in the acquired HAADF-STEM data. The self-annihilation mechanism of the APBs is addressed based on the rotation induced by anti-site bonds and APBs' faceting.

Hosseini Vajargah, S.; Woo, S. Y.; Botton, G. A. [Department of Materials Science and Engineering, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Brockhouse Institute for Material Research, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Canadian Centre for Electron Microscopy, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Ghanad-Tavakoli, S. [Centre for Emerging Device Technologies, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Kleiman, R. N.; Preston, J. S. [Brockhouse Institute for Material Research, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Centre for Emerging Device Technologies, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Department of Engineering Physics, McMaster University, Hamilton, Ontario L8S 4L7 (Canada)

2012-11-01T23:59:59.000Z

417

The X-Ray Microcalorimeter Spectrometer for the International X-Ray Observatory  

SciTech Connect

The International X-Ray Observatory (IXO) is under formulation by NASA, ESA and JAXA for deployment in 2022. IXO emerged over the last 18 months as the NASA Constellation-X and ESA/JAXA X-Ray Evolving Universe Spectrometer (XEUS) missions were combined. The driving performance requirements for the X-Ray Microcalorimeter Spectrometer (XMS) are a spectral resolution of 2.5 eV over the central 2'x2' in the 0.3-7.0 keV band, and 10 eV to the edge of the 5'x5' field of view (FOV). The XMS is now based on a microcalorimeter array of Transition-Edge Sensor (TES) thermometers with Au/Bi absorbers and a SQUID MUX readout. One of the concepts studied as part of the mission formulation has a core 40x40 array corresponding to a 2'x2' FOV with 3'' pixels surrounded by an outer, annular 52x52 array of 6'' pixels that extends the field of view to 5.4'x5.4' with better than 10 eV resolution. There are several options for implementing the readout and cooling system of the XMS under study in the US, Europe and Japan. The ADR system will have from two to five stages depending on the performance of the cryocooler. Mechanical coolers with sufficient cooling power at 4K are available now, and {approx}2K coolers are under development. In this paper we give an overview of the XMS instrument, and some of the tradeoffs to be addressed for this observatory instrument.

Kelley, R. L.; Bandler, S. R.; Kilbourne, C. A.; Porter, F. S.; Shirron, P.; Smith, S. J.; Whitehouse, P. [NASA/Goddard Space Flight Center, Greenbelt, MD (United States); Doriese, W. B.; Irwin, K. [National Institute of Standards and Technology, Boulder, CO (United States); Ezoe, Y.; Ishisaki, Y.; Ohashi, T. [Tokyo Metropolitan University, Hachioji, Tokyo (Japan); Fujimoto, R.; Sato, K. [Faculty of Mathematics and Physics, Kanazawa University, Kanazawa (Japan); Gottardi, L.; Hartog, R. den; Herder, J.-W. den; Hoevers, H.; Korte, P. de; Kuur, J. van der [SRON Netherlands Institute for Space Research, Utrecht (Netherlands)] (and others)

2009-12-16T23:59:59.000Z

418

Milestones and basic principles of grating-based x-ray and neutron phase-contrast imaging  

SciTech Connect

This is a review of the most important milestones in the last ten years of development in the field of grating-based x-ray and neutron imaging. It provides a description of the basic imaging principles of grating-based phase-contrast and dark-field radiography and present some exemplary multimodal radiography results obtained with x-rays and neutrons. Furthermore, it reviews the theory of grating-based quantitative transmission, phase-contrast, and dark-field scattering computed tomography.

Pfeiffer, Franz [Technical University Munich, 85748 Garching (Germany)

2012-07-31T23:59:59.000Z

419

SOFT X-RAY EMISSIONS FROM PLANETS, MOONS, AND COMETS A. Bhardwaj(1)  

E-Print Network (OSTI)

SOFT X-RAY EMISSIONS FROM PLANETS, MOONS, AND COMETS A. Bhardwaj(1) , G. R. Gladstone(2) , R. F to radiate in the soft x-ray energy ( the generation of soft x-rays from these objects, whereas in the hard x-ray energy range (>10 keV) x-rays mainly

Johnson, Robert E.

420

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate  

E-Print Network (OSTI)

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate an effect of a partially reversible x-ray-induced increase of diffuse x-ray scattering in both congruent been attributed to x-ray-induced decay of the ferroelectric phase at room temperature. The x-ray

Byer, Robert L.

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

A Hard X-ray View of Accreting X-ray Binary Pulsars  

E-Print Network (OSTI)

The study of the hard (E>10 keV) energy spectra of X-ray binary pulsars can give a wealth of information on the physical processes that occur close to the neutron star surface. Extreme matter regimes are probed, and precious information on how matter and radiation behave and interact in critical conditions can be obtained. We will give an overview on the most recent results obtained by RXTE and BeppoSAX on this class of objects, in order to pass the baton onto just launched experiments, like INTEGRAL, or soon to be launched, like AGILE and ASTRO-E2.

Mauro Orlandini

2004-02-26T23:59:59.000Z

422

Apparatus for generating x-ray holograms  

DOE Patents (OSTI)

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced.

Rhodes, Charles K. (Chicago, IL); Boyer, Keith (Los Alamos, NM); Solem, Johndale C. (Los Alamos, NM); Haddad, Waleed S. (Chicago, IL)

1990-01-01T23:59:59.000Z

423

Apparatus for generating x-ray holograms  

DOE Patents (OSTI)

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced. 7 figs.

Rhodes, C.K.; Boyer, K.; Solem, J.C.; Haddad, W.S.

1990-09-11T23:59:59.000Z

424

Femtosecond Time-Delay X-ray Holography  

NLE Websites -- All DOE Office Websites (Extended Search)

Time-Delay X-ray Holography Time-Delay X-ray Holography X-ray free-electron lasers (XFELs) will produce photon pulses with a unique and desirable combination of properties. Their short X-ray wavelengths allow penetration into materials and the ability to probe structure at and below the nanometer scale. Their ultra-short duration gives information about this structure at the fundamental time-scales of atoms and molecules. The extreme intensity of the pulses will allow this information to be acquired in a single shot, so that these studies can be carried out on non-repeatable processes or on weakly-scattering objects that will be modified by the pulse. A fourth property of XFEL pulses is their high transverse coherence, which brings the promise of decades of innovation in visible optics to the X-ray regime, such as holography, interferometry, and laser-based imaging. Making an effective use of XFEL pulses, however, will benefit from innovations that are new to both X-ray science and coherent optics. One such innovation is the new method of time-delay X-ray holography [i], recently demonstrated at the FLASH FEL at DESY in Hamburg, to measure the evolution of objects irradiated by intense pulses.

425

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi Center 091 Chemistry Bldg. / College Park, MD 20742  

E-Print Network (OSTI)

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi. or advisor confirmation e-mail X-ray Diffractometer that will be used: User Level and Status Smart Apex2X'Pert Pro MRD (Reflectivity & low angles) Xeuss (Small/Wide Angle X-ray Scattering) Submitting user ­ only

Thirumalai, Devarajan

426

Lunar X-ray fluorescence observations by the Chandrayaan-1 X-ray Spectrometer (C1XS): Results from the nearside southern highlands  

E-Print Network (OSTI)

Lunar X-ray fluorescence observations by the Chandrayaan-1 X-ray Spectrometer (C1XS): Results from Spectroscopy a b s t r a c t The Chandrayaan-1 X-ray Spectrometer (C1XS) flown on-board the first Indian lunar mission Chan- drayaan-1, measured X-ray fluorescence spectra during several episodes of solar flares

Wieczorek, Mark

427

Low-Dimensional Water on Ru(0001)Model System for X-ray Absorption Spectroscopy Studies of Liquid Water  

SciTech Connect

We present an x-ray absorption spectroscopy results for fully broken to a complete H-bond network of water molecules on Ru(0001) by varying the morphology from isolated water molecules via two-dimensional clusters to a fully covered monolayer as probed by scanning tunneling microscopy. The sensitivity of x-ray absorption to the symmetry of H-bonding is further elucidated for the amino (-NH{sub 2}) group in glycine adsorbed on Cu(110) where the E-vector is parallel either to the NH donating an H-bond or to the non-H-bonded NH. The results give further evidence for the interpretation of the various spectral features of liquid water and for the general applicability of x-ray absorption spectroscopy to analyze H-bonded systems.

Nordlund, D

2012-02-14T23:59:59.000Z

428

Low-Dimensional Water on Ru(0001); Model System for X-ray Absorption Spectroscopy Studies of Liquid Water  

SciTech Connect

We present an x-ray absorption spectroscopy results for fully broken to a complete H-bond network of water molecules on Ru(0001) by varying the morphology from isolated water molecules via two-dimensional clusters to a fully covered monolayer as probed by scanning tunneling microscopy. The sensitivity of x-ray absorption to the symmetry of H-bonding is further elucidated for the amino (-NH{sub 2}) group in glycine adsorbed on Cu(110) where the E-vector is parallel either to the NH donating an H-bond or to the non-H-bonded NH. The results give further evidence for the interpretation of the various spectral features of liquid water and for the general applicability of x-ray absorption spectroscopy to analyze H-bonded systems.

Nordlund, D.; Ogasawara, H.; Andersson, K.J.; Tatarkhanov, M.; Salmeron, M.; Pettersson, L. G. M.; Nilsson, A.

2009-05-11T23:59:59.000Z

429

National Ignition Facility core x-ray streak camera  

SciTech Connect

The National Ignition Facility (NIF) core x-ray streak camera will be used for laser performance verification experiments as well as a wide range of physics experiments in the areas of high-energy-density science, inertial confinement fusion, and basic science. The x-ray streak camera system is being designed to record time-dependent x-ray emission from NIF targets using an interchangeable family of snouts for measurements such as one-dimensional (1D) spatial imaging or spectroscopy. the NIF core x-ray streak camera will consist of an x-ray-sensitive photocathode that detects x rays with 1D spatial resolution coupled to an electron streak tube to detect a continuous time history of the x rays incident on the photocathode over selected time periods. A charge-coupled-device (CCD) readout will record the signal from the streak tube. The streak tube, CCD, and associated electronics will reside in an electromagnetic interference, and electromagnetic pulse protected, hermetically sealed, temperature-controlled box whose internal pressure is approximately 1 atm. The streak tube itself will penetrate through the wall of the box into the target chamber vacuum. We are working with a goal of a spatial resolution of 15 lp/mm with 50% contrast transfer function at the photocathode and adjustment sweep intervals of 1--50 ns. The camera spectral sensitivity extends from soft x rays to 20 keV x rays, with varying quantum efficiency based on photocathode selection. The system will have remote control, monitoring, and Ethernet communications through an embedded controller. The core streak camera will be compatible with the instrument manipulators at the OMEGA (University of Rochester) and NIF facilities.

Kimbrough, J. R.; Bell, P. M.; Christianson, G. B.; Lee, F. D.; Kalantar, D. H.; Perry, T. S.; Sewall, N. R.; Wootton, A. J.

2001-01-01T23:59:59.000Z

430

The radiation-tolerant x-ray monitor  

SciTech Connect

A vacuum photoelectric detector (monitor) (VPD) designed for plasma tomography, megnetohydrodynamics monitoring, and imaging with the help of thermal x-ray radiation on the ITER facility is described. Laboratory experiments demonstrate that VPD has high sensitivity to thermal x rays and low sensitivity to hard gamma rays and neutrons. The results of tests of a prototype of this monitor on a {sup 60}Co source of gamma rays, on nuclear reactor and its calibration using radiation from an x-ray tube, and tests of its serviceability on the T-10 facility are presented.

Gott, Yu. V.; Stepanenko, M. M. [Nuclear Fusion Institute, Russian Research Center 'Kurchatov Institute', Kurchatov Sq. 1, Moscow 123182 (Russian Federation)

2008-10-15T23:59:59.000Z

431

X-ray backscatter imaging of nuclear materials  

DOE Patents (OSTI)

The energy of an X-ray beam and critical depth are selected to detect structural discontinuities in a material having an atomic number Z of 57 or greater. The critical depth is selected by adjusting the geometry of a collimator that blocks backscattered radiation so that backscattered X-ray originating from a depth less than the critical depth is not detected. Structures of Lanthanides and Actinides, including nuclear fuel rod materials, can be inspected for structural discontinuities such as gaps, cracks, and chipping employing the backscattered X-ray.

Chapman, Jeffrey Allen; Gunning, John E; Hollenbach, Daniel F; Ott, Larry J; Shedlock, Daniel

2014-09-30T23:59:59.000Z

432

X-Ray Afterglows from Gamma-Ray Bursts  

Science Journals Connector (OSTI)

We consider possible interpretations of the recently detected X-ray afterglow from the gamma-ray burst source GRB 970228. Cosmological and Galactic models of gamma-ray bursts predict different flux and spectral evolution of X-ray afterglows. We show that models based on adiabatic expansion of relativistic forward shocks require very efficient particle energization or postburst reacceleration during the expansion. Cooling neutron star models predict a very distinctive spectral and flux evolution that can be tested in current X-ray data.

M. Tavani

1997-01-01T23:59:59.000Z

433

Current Problems for X-ray Emission from Radio Jets  

E-Print Network (OSTI)

A list is presented of known extragalactic radio jets which also have associated X-ray emission. The canonical emission processes for the production of X-rays are reviewed and the sources are categorized on the basis of our current understanding. Although it seems clear that the X-ray emission is non-thermal, the two competing processes, synchrotron and inverse Compton emissions, arise from extremely high energy (synchrotron) or extremely low energy (beaming models with IC emission), relativistic electrons. Only synchrotron self-Compton emission from a few hotspots provides information on the `normal' energy range of the electrons responsible for the observed radio emission.

D. E. Harris

2000-12-17T23:59:59.000Z

434

Dynamic model of anisotropic x-ray refraction  

Science Journals Connector (OSTI)

General mechanisms of anisotropic x-ray refraction at the resonance energy are investigated on the basis of dynamic-scattering theory. The deductions show that x rays within the crystals that have anisotropic susceptibility are completely polarized and have two elliptical polarization states. Analytical expressions of the elliptical axes, refractive indices, and absorption coefficients for these two types of polarized waves are obtained in terms of the anisotropic components of the susceptibility tensor. Anisotropic birefringence and dichroism effects associated with the polarization properties of the x-ray waves are also illustrated theoretically.

X. R. Huang, Yong Li, W. J. Liu, and S. S. Jiang

1997-11-01T23:59:59.000Z

435

X-Ray Directional Dichroism of a Polar Ferrimagnet  

Science Journals Connector (OSTI)

In a polar ferrimagnet GaFeO3, we have found a novel magneto-optical effect, termed x-ray nonreciprocal directional dichroism (XNDD), that the x-ray absorption at around the K edge of an Fe ion depends on whether the x-ray propagation vector is parallel or antiparallel to the outer product of the magnetization and electric-polarization vectors. The XNDD spectroscopy as demonstrated here can be a useful tool to probe the local magnetism in noncentrosymmetric systems such as magnetic interfaces and nanostructures.

M. Kubota, T. Arima, Y. Kaneko, J. P. He, X. Z. Yu, and Y. Tokura

2004-03-29T23:59:59.000Z

436

Characterization of X-ray generator beam profiles.  

SciTech Connect

T to compute the radiography properties of various materials, the flux profiles of X-ray sources must be characterized. This report describes the characterization of X-ray beam profiles from a Kimtron industrial 450 kVp radiography system with a Comet MXC-45 HP/11 bipolar oil-cooled X-ray tube. The empirical method described here uses a detector response function to derive photon flux profiles based on data collected with a small cadmium telluride detector. The flux profiles are then reduced to a simple parametric form that enables computation of beam profiles for arbitrary accelerator energies.

Mitchell, Dean J; Harding, Lee T.; Thoreson, Gregory G.; Theisen, Lisa Anne; Parmeter, John Ethan; Thompson, Kyle Richard

2013-07-01T23:59:59.000Z

437

Spatiotemporal focusing dynamics in plasmas at X-ray wavelength  

SciTech Connect

Using a finite curvature beam, we investigate here the spatiotemporal focusing dynamics of a laser pulse in plasmas at X-ray wavelength. We trace the dependence of curvature parameter on the focusing of laser pulse and recognize that the self-focusing in plasma is more intense for the X-ray laser pulse with curved wavefront than with flat wavefront. The simulation results demonstrate that spatiotemporal focusing dynamics in plasmas can be controlled with the appropriate choice of beam-plasma parameters to explore the high intensity effects in X-ray regime.

Sharma, A., E-mail: a-physics2001@yahoo.com; Tibai, Z. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary)] [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Hebling, J. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary) [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Szentagothai Research Centre, University of Pecs, Pecs-7624 (Hungary); Mishra, S. K. [Institute for Plasma Research, Gandhinagar (India)] [Institute for Plasma Research, Gandhinagar (India)

2014-03-15T23:59:59.000Z

438

Soft x-ray resist characterization: Studies with a laser plasma x-ray source  

SciTech Connect

Little work has been performed to characterize the exposure sensitivity, contrast, and tone of candidate resists for photon energies between 100--300 eV, the range in which projection soft x-ray lithography will be developed. We report here the characterization of near-edge x-ray absorption fine structure (NEXAFS) spectra, exposure sensitivity, contrast, and post-exposure processing of selected polysilane resists at photon energies close to the Si L{sub 2,3} absorption edge (100 eV). We find absorption resonance features in the NEXAFS spectra which we assign to excitation into Si--Si and Si--C {sigma}* orbitals. Using monochromatized XUV exposures on the Si--Si {sigma}* resonance at 105 eV, followed by solvent dissolution development, we have measured the exposure sensitivity curves of these resists. We find sensitivities in the range of 600--3000 mJ/cm{sup 2} and contrasts in the range from 0.5--1.4, depending on the polysilane side chain. We have also performed exposure sensitivity measurements at 92 eV, below the edge. Sensitivity decreases slightly compared to 105 eV exposures and the saturation depth and contrast both increase, as expected. We find also that exposing resist films to oxygen after XUV exposure, but before development increases the sensitivity markedly. 7 figs.

Kubiak, G.D.; Outka, D.A. (Sandia National Labs., Livermore, CA (USA)); Zeigler, J.M. (Sandia National Labs., Albuquerque, NM (USA))

1990-01-01T23:59:59.000Z

439

Thermonuclear (Type I) X-Ray Bursts Observed by the Rossi X-Ray Timing Explorer  

Science Journals Connector (OSTI)

We have assembled a sample of 1187 thermonuclear (type I) X-ray bursts from observations of 48 accreting neutron stars by the Rossi X-ray Timing Explorer, spanning more than 10 years. The sample contains examples of two of the three theoretical ignition regimes (confirmed via comparisons with numerical models) and likely examples of the third. We present a detailed analysis of the variation of the burst profiles, energetics, recurrence times, presence of photospheric radius expansion, and presence of burst oscillations, as a function of accretion rate. We estimated the distance for 35 sources exhibiting radius-expansion bursts, and found that the peak flux of such bursts varies typically by 13%. We classified sources into two main groups based on the burst properties: (1) both long and short bursts (indicating mixed H/He accretion), and (2) consistently short bursts (primarily He accretion), and we calculated the mean burst rate as a function of accretion rate for the two groups. The decrease in burst rate observed at > 0.06Edd$0.06˙{M}Edd$ --> ( -->2 ? 1037 ergs s?1) is associated with a transition in the persistent spectral state and (as has been suggested previously) may be related to the increasing role of steady He burning. We found many examples of bursts with recurrence times

Duncan K. Galloway; Michael P. Muno; Jacob M. Hartman; Dimitrios Psaltis; Deepto Chakrabarty

2008-01-01T23:59:59.000Z

440

Synchrotron-Radiation Induced X-Ray Emission (SRIXE)  

SciTech Connect

Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change and increase in scientific use can be maintained for the synchrotron x-ray source. A short summary of the present state of the synchrotron radiation-induced x-ray emission (SRIXE) method is presented here. Basically, SRIXE experiments can include any that depend on the detection. of characteristic x-rays produced by the incident x-ray beam born the synchrotron source as they interact with a sample. Thus, experiments done to measure elemental composition, chemical state, crystal, structure, and other sample parameters can be considered in a discussion of SRIXE. It is also clear that the experimentalist may well wish to use a variety of complementary techniques for study of a given sample. For this reason, discussion of computed microtomography (CMT) and x-ray diffraction is included here. It is hoped that this present discussion will serve as a succinct introduction to the basic ideas of SRIXE for those not working in the field and possibly help to stimulate new types of work by those starting in the field as well as by experienced practitioners of the art. The topics covered include short descriptions of (1) the properties of synchrotron radiation, (2) a description of facilities used for its production, (3) collimated microprobe, (4) focused microprobes, (5) continuum and monoenergetic excitation, (6) detection limits, (7) quantitation, (8) applications of SRIXE, (9) computed microtomography (CMT), and (10)chemical speciation using x-ray absorption near-edge structure (XANES) and extended x-ray absorption fine structure (EXAFS). An effort has been made to cite a wide variety of work from different laboratories to show the vital nature of the field.

Jones, Keith W.

1999-09-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


441

E-Print Network 3.0 - airborne lead x-ray Sample Search Results  

NLE Websites -- All DOE Office Websites (Extended Search)

Pulsars... you'd . . . Active Galactic . . . X-ray binaries Pulsars and relatives Gamma-ray bursts Gravitational... 1 - Type 2 X-ray binaries - Low mass X-ray binaries (LMXBs)...

442

E-Print Network 3.0 - advanced x-ray timing Sample Search Results  

NLE Websites -- All DOE Office Websites (Extended Search)

AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND Summary: with the occurrence of solar X-ray flare, when light travel time delay is accounted, suggesting that X-rays...

443

X-RAY ABSORPTION STUDIES OF GRAPHITE INTERCALATES AND METAL-AMMONIA SOLUTION  

E-Print Network (OSTI)

I. INTRODUCTION A. X-Ray Absorption Spectroscopy B. Graphiteacknowledged. The X-Ray absorption data could not have beenI INTRODUCTION X-ray absorption, spectroscopy (XAS) has been

Robertson, A.S.

2010-01-01T23:59:59.000Z

444

AN X-RAY ABSORPTION SPECTROSCOPY STUDY OF MANGANESE CONTAINING COMPOUNDS AND PHOTOSYNTHETIC SPINACH CHLOROPLASTS  

E-Print Network (OSTI)

II. Extended X-ray Absorption Fine Structure (EXAFS) TheoryIII. X-ray Absorption Spectroscopy (XAS) ExperimentIII. EXTENDED X-RAY ABSORPTION FINE STRUCTURE (EXAFS) DATA

Kirby, Jon Allan

2012-01-01T23:59:59.000Z

445

X-ray Absorption Spectroscopy Study of Prototype Chemical Systems: Theory vs. Experiment  

E-Print Network (OSTI)

acids by Near Edge X-ray Absorption Fine Structure (NEXAFS)X-ray Absorption Spectroscopy Study of Prototype ChemicalGlaeser Spring 2010 X-ray Absorption Spectroscopy Study of

Schwartz, Craig Philip

2010-01-01T23:59:59.000Z

446

X-ray absorption spectroscopy at the Ni-K edge in Stackhousia tryonii Bailey hyperaccumulator  

E-Print Network (OSTI)

X-ray absorption spectroscopy at the Ni–K edge inin vivo by micro x-ray absorption spectroscopy (XAS) at theNi–K edge. Both x-ray absorption near edge structure and

Kachenko, A.

2009-01-01T23:59:59.000Z

447

Long-term X-ray stability and UV variability of the ionized absorption in NGC 3783  

E-Print Network (OSTI)

We present the results of recent Chandra High-Energy Transmission Grating Spectrometer and Hubble Space Telescope Cosmic Origins Spectrograph observations of the nearby Seyfert 1 galaxy NGC 3783 which shows a strong, non-varying X-ray warm absorber and physically related and kinematically varying UV absorption. We compare our new observations to high-resolution, high signal-to-noise archival data from 2001, allowing a unique investigation into the long-term variations of the absorption over a 12 yr period. We find no statistically significant changes in the physical properties of the X-ray absorber, but there is a significant drop of ~40% in the UV and X-ray flux, and a significant flattening of the underlying X-ray power-law slope. Large kinematic changes are seen in the UV absorbers, possibly due to radial deceleration of the material. Similar behavior is not observed in the X-ray data, likely due to its lower velocity resolution, which shows an outflow velocity of v ~ -655 km/s in both epochs. The narrow i...

Scott, A E; Behar, E; Crenshaw, D M; Gabel, J R; Gibson, R R; Kaspi, S; Kraemer, S B; Turner, T J

2014-01-01T23:59:59.000Z

448

Definition: Portable X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

Definition Definition Edit with form History Facebook icon Twitter icon » Definition: Portable X-Ray Diffraction (XRD) Jump to: navigation, search Dictionary.png Portable X-Ray Diffraction (XRD) Portable X-Ray Diffraction (XRD) is a field-based technique that can be used for identification of crystalline materials and analysis of unit cell dimensions. Portable XRD analysis is similar to X-ray powder diffraction, which has traditionally been used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline substances. Portable XRD analysis allows for simpler sample preparation, faster analytical times than traditional methods (less than 2 minutes), and can be performed at the sampling site in the field. A pure, finely ground

449

Plasma debris sputter resistant x-ray mirror  

Science Journals Connector (OSTI)

A diamond-like carbon (DLC) mirror, used as a grazing incident mirror in a plasma x-ray source, exhibits a high resistance to plasma debris sputtering. Good mirror reflectivity at a...

Amano, Sho; Inoue, Tomoaki; Harada, Tetsuo

2013-01-01T23:59:59.000Z

450

New Directions in X-ray Scattering - SSRL  

NLE Websites -- All DOE Office Websites (Extended Search)

6, 2006 A summary of the workshop on New Directions in X-ray Scattering On Dec 6th, we held a day long workshop to solicit user input on the new directions that the SSRL...

451

Synchroton X-Ray Studies of Liquid-Vapor Interfaces  

Science Journals Connector (OSTI)

The variation of density across the liquid-vapor interface from essentially zero density far out in the vapor phase to a homogeneous density deep in the liquid phase can be determined by X-ray reflectivity mea...

J. Als-Nielsen

1988-01-01T23:59:59.000Z

452

Energy weighted x-ray dark-field imaging  

Science Journals Connector (OSTI)

The dark-field image obtained in grating-based x-ray phase-contrast imaging can provide information about the objects’ microstructures on a scale smaller than the pixel size...

Pelzer, Georg; Zang, Andrea; Anton, Gisela; Bayer, Florian; Horn, Florian; Kraus, Manuel; Rieger, Jens; Ritter, Andre; Wandner, Johannes; Weber, Thomas; Fauler, Alex; Fiederle, Michael; Wong, Winnie S; Campbell, Michael; Meiser, Jan; Meyer, Pascal; Mohr, Jürgen; Michel, Thilo

2014-01-01T23:59:59.000Z

453

Magnetic fields of neutron stars in X-ray binaries  

E-Print Network (OSTI)

A substantial fraction of the known neutron stars resides in X-ray binaries -- systems in which one compact object accretes matter from a companion star. Neutron stars in X-ray binaries have magnetic fields among the highest found in the Universe, spanning at least the range from $\\sim10^8$ to several 10$^{13}$ G. The magnetospheres around these neutron stars have a strong influence on the accretion process, which powers most of their emission. The magnetic field intensity and geometry, are among the main factors responsible for the large variety of spectral and timing properties observed in the X-ray energy range, making these objects unique laboratories to study the matter behavior and the radiation processes in magnetic fields unaccessible on Earth. In this paper we review the main observational aspects related to the presence of magnetic fields in neutron star X-ray binaries and some methods that are used to estimate their strength.

Revnivtsev, Mikhail

2014-01-01T23:59:59.000Z

454

X-ray emission from the terrestrial magnetosheath  

E-Print Network (OSTI)

[1] X-rays are generated throughout the terrestrial magnetosheath as a consequence of charge transfer collisions between heavy solar wind ions and geocoronal neutrals. The solar wind ions resulting from these collisions ...

Robertson, Ina Picket; Cravens, Thomas Edward

2003-04-29T23:59:59.000Z

455

Lensless Imaging of Magnetic Nanostructures by X-ray Spectro...  

NLE Websites -- All DOE Office Websites (Extended Search)

co-workers. Their implementation of the technique is an extension of lensless Fourier transform holography to the x-ray regime, which detects the far field diffraction pattern of a...

456

Polarization Entangled Photons at X-Ray Energies  

E-Print Network (OSTI)

We show that polarization entangled photons at x-ray energies can be generated via spontaneous parametric down conversion. Each of the four Bell states can be generated by choosing the angle of incidence and polarization of the pumping beam.

S. Shwartz; S. E. Harris

2010-12-16T23:59:59.000Z

457

Towards hard x-ray imaging at GHz frame rate  

SciTech Connect

Gigahertz (GHz) imaging using hard x-rays ( Greater-Than-Or-Equivalent-To 10 keV) can be useful to high-temperature plasma experiments, as well as research and applications using coherent photons from synchrotron radiation and x-ray free electron lasers. GHz framing rate can be achieved by using multiple cameras through multiplexing. The advantages and trade-offs of single-photon detection mode, when no more than one x-ray photon is detected per pixel, are given. Two possible paths towards x-ray imaging at GHz frame rates using a single camera are: (a) avalanche photodiode arrays of high-Z materials and (b) microchannel plate photomultipliers in conjunction with materials with large indices of refraction.

Wang Zhehui; Morris, C. L.; Kapustinsky, J. S.; Kwiatkowski, K.; Luo, S.-N. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)

2012-10-15T23:59:59.000Z

458

Towards hard X-ray imaging at GHz frame rate  

SciTech Connect

Gigahertz (GHz) imaging using hard X-rays ({approx}> 10 keV) can be useful to high-temperature plasma experiments, as well as research using coherent photons from synchrotron radiation and X-ray free electron lasers. GHz framing rate can be achieved by using multiple cameras through multiplexing. The advantages and trade-offs of single-photon detection mode, when no more than one X-ray photon is detected per pixel, are given. Two possible paths towards X-ray imaging at GHz frame rates using a single camera are (a) Avalanche photodiode arrays of high-Z materials and (b) Microchannel plate photomultipliers in conjunction with materials with large indices of refraction.

Wang, Zhehui [Los Alamos National Laboratory; Morris, Christopher [Los Alamos National Laboratory; Luo, Shengnian [Los Alamos National Laboratory; Kwiatkowski, Kris K. [Los Alamos National Laboratory; Kapustinsky, Jon S. [Los Alamos National Laboratory

2012-05-02T23:59:59.000Z

459

Magnetism studies using resonant, coherent, x-ray scattering...  

NLE Websites -- All DOE Office Websites (Extended Search)

Magnetism studies using resonant, coherent, x-ray scattering Monday, September 10, 2012 - 10:00am SLAC, Bldg. 137, Room 226 Keoki Seu Seminar: With the advent of free electron...

460

X-Ray Astronomy to Resonant Theranostics for Cancer Treatment  

E-Print Network (OSTI)

X-Ray Astronomy to Resonant Theranostics for Cancer Treatment Sultana N. Nahar Department-Plasma Theranostics or RNPT, which gives indication for one most efficient way for destruction of malignant cells. 1

Nahar, Sultana Nurun

Note: This page contains sample records for the topic "transmission x-ray microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Vitreous carbon mask substrate for X-ray lithography  

DOE Patents (OSTI)

The present invention is directed to the use of vitreous carbon as a substrate material for providing masks for X-ray lithography. The new substrate also enables a small thickness of the mask absorber used to pattern the resist, and this enables improved mask accuracy. An alternative embodiment comprised the use of vitreous carbon as a LIGA substrate wherein the VC wafer blank is etched in a reactive ion plasma after which an X-ray resist is bonded. This surface treatment provides a surface enabling good adhesion of the X-ray photoresist and subsequent nucleation and adhesion of the electrodeposited metal for LIGA mold-making while the VC substrate practically eliminates secondary radiation effects that lead to delamination of the X-ray resist form the substrate, the loss of isolated resist features, and the formation of a resist layer adjacent to the substrate that is insoluble in the developer.

Aigeldinger, Georg (Livermore, CA); Skala, Dawn M. (Fremont, CA); Griffiths, Stewart K. (Livermore, CA); Talin, Albert Alec (Livermore, CA); Losey, Matthew W. (Livermore, CA); Yang, Chu-Yeu Peter (Dublin, CA)

2009-10-27T23:59:59.000Z

462

Optical and X-ray Variability of AGNs  

E-Print Network (OSTI)

I present new comparisons of AGN optical, UV, and X-ray variations. These reveal complex relationships between the different passbands that can change with time in a given object. While there is evidence from several objects that X-ray and optical activity levels are correlated on long timescales, variations on shorter timescales can occur independently. It is proposed that the combination of correlated and uncorrelated short-timescale variability is a consequence of anisotropic high-energy emission. It is also argued that the correlation between X-ray and optical variability on long timescales must be due to a common underlying factor and not to reprocessing of X-ray radiation.

C. Martin Gaskell

2006-12-30T23:59:59.000Z

463

,~ Abstract Submitted to 1997 Denver X-Ray Conference  

E-Print Network (OSTI)

,~ Abstract Submitted to 1997 Denver X-Ray Conference Denver, Colorado -August 4-8, 1997 BNL-.64346 being distributed through the entire volume of the particle needs further investigation. *Work supported

Brookhaven National Laboratory

464

Photon Sciences | Beamlines | SRX: Submicron Resolution X-ray Spectroscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

SRX: Submicron Resolution X-ray Spectroscopy SRX: Submicron Resolution X-ray Spectroscopy Poster | Fact Sheet | Preliminary Design Report Scientific Scope Scientific communities such as environmental sciences, life sciences, and material sciences have identified the need to develop analytical resources to advance the understanding of complex natural and engineered systems that are heterogeneous on the micron to nanometer scale. These needs for high intensity x-ray nanoprobes resulted in the commitment of the NSLS-II Project to build the Submicron Resolution X-ray (SRX) Spectroscopy beamline showing a unique combination of high spectral resolution over a very broad energy range and very high beam intensity in a sub-micrometer spot. NSLS-II will provide one of the best sources in the world for such an instrument.

465

X-ray Raman scattering study of aligned polyfluorene  

E-Print Network (OSTI)

We present a non-resonant inelastic x-ray scattering study at the carbon K-edge on aligned poly[9,9-bis(2-ethylhexyl)-fluorene-2,7-diyl] and show that the x-ray Raman scattering technique can be used as a practical alternative to x-ray absorption measurements. We demonstrate that this novel method can be applied to studies on aligned $\\pi$-conjugated polymers complementing diffraction and optical studies. Combining the experimental data and a very recently proposed theoretical scheme we demonstrate a unique property of x-ray Raman scattering by performing the symmetry decomposition on the density of unoccupied electronic states into $s$- and $p$-type symmetry contributions.

S. Galambosi; M. Knaapila; J. A. Soininen; K. Nyg\\aard; S. Huotari; F. Galbrecht; U. Scherf; A. P. Monkman; K. Hämäläinen

2006-08-29T23:59:59.000Z

466

X-Ray Photoelectron Spectroscopy (XPS) Applied to Soot & What...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Photoelectron Spectroscopy (XPS) Applied to Soot & What It Can Do for You X-Ray Photoelectron Spectroscopy (XPS) Applied to Soot & What It Can Do for You Presentation given at DEER...

467

Gravitational and Relativistic Deflection of X-Ray Superradiance  

E-Print Network (OSTI)

Exploring Einstein's theories of relativity in quantum systems, for example by using atomic clocks at high speeds can deepen our knowledge in physics. However, many challenges still remain on finding novel methods for detecting effects of gravity and of special relativity and their roles in light-matter interaction. Here we introduce a scheme of x-ray quantum optics that allows for a millimeter scale investigation of the relativistic redshift by directly probing a fixed nuclear crystal in Earth's gravitational field with x-rays. Alternatively, a compact rotating crystal can be used to force interacting x-rays to experience inhomogeneous clock tick rates in a crystal. We find that an association of gravitational or special-relativistic time dilation with quantum interference will be manifested by deflections of x-ray photons. Our protocol suggests a new and feasible tabletop solution for probing effects of gravity and special relativity in the quantum world.

Wen-Te Liao; Sven Ahrens

2014-11-27T23:59:59.000Z

468

High performance x-ray anti-scatter grid  

DOE Patents (OSTI)

Disclosed are an x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury. 4 Figs.

Logan, C.M.

1995-05-23T23:59:59.000Z

469

Pixel detectors for x-ray imaging spectroscopy in space  

Science Journals Connector (OSTI)

Pixelated semiconductor detectors for X-ray imaging spectroscopy are foreseen as key components of the payload of various future space missions exploring the x-ray sky. Located on the platform of the new Spectrum-Roentgen-Gamma satellite, the eROSITA (extended Roentgen Survey with an Imaging Telescope Array) instrument will perform an imaging all-sky survey up to an X-ray energy of 10 keV with unprecedented spectral and angular resolution. The instrument will consist of seven parallel oriented mirror modules each having its own pnCCD camera in the focus. The satellite born X-ray observatory SIMBOL-X will be the first mission to use formation-flying techniques to implement an X-ray telescope with an unprecedented focal length of around 20 m. The detector instrumentation consists of separate high- and low energy detectors, a monolithic 128 ? 128 DEPFET macropixel array and a pixellated CdZTe detector respectively, making energy band between 0.5 to 80 keV accessible. A similar concept is proposed for the next generation X-ray observatory IXO. Finally, the MIXS (Mercury Imaging X-ray Spectrometer) instrument on the European Mercury exploration mission BepiColombo will use DEPFET macropixel arrays together with a small X-ray telescope to perform a spatially resolved planetary XRF analysis of Mercury's crust. Here, the mission concepts and their scientific targets are briefly discussed, and the resulting requirements on the detector devices together with the implementation strategies are shown.

J Treis; R Andritschke; R Hartmann; S Herrmann; P Holl; T Lauf; P Lechner; G Lutz; N Meidinger; M Porro; R H Richter; F Schopper; H Soltau; L Strüder

2009-01-01T23:59:59.000Z

470

The Hard X-ray Sky: Recent Observational Progress  

SciTech Connect

The last fifty years have witnessed the birth, development, and maturation to full potential of hard X-ray astrophysics. The primary force driving the history of the field has been the development of space-based instrumentation optimized for getting the maximum science out of observations of high-energy photons from astrophysical sources. Hard X-ray telescopes are leading research in areas such as galactic diffuse emission, galactic transients, and active galactic nuclei.

Gehrels, Neil [NASA/GSFC/ASD/Code 661, Greenbelt, Md 20071 (United States); Cannizzo, John K. [CRESST/UMBC/NASA/GSFC/ASD/Code 661, Greenbelt, Md 20071 (United States)

2009-05-11T23:59:59.000Z

471

The X-ray background and the evolution of AGN  

E-Print Network (OSTI)

We discuss the constraints on the AGN evolution from the cosmic X-ray background and source counts. A synthesis model to fit the X-ray background is presented. In the model, the spectrum of type 2 AGN has been modeled including Compton down--scattering within the absorbing material. Besides, we introduced a dependence on redshift of the relative number of obscured sources and found a decrease of the fraction of type 2 AGN at redshifts larger than 2.

Fulvio Pompilio; Fabio La Franca; Giorgio Matt

1999-09-23T23:59:59.000Z

472

Sapphire analyzers for high-resolution x-ray spectroscopy.  

SciTech Connect

We present a sapphire (Al{sub 2}O{sub 3}) analyzer for high-resolution X-ray spectroscopy with 31-meV energy resolution. The analyzer is designed for resonant inelastic X-ray scattering (RIXS) measurements at the CuK{sub a} absorption edge near 8990 eV. The performance of the analyzer is demonstrated by measuring phonon excitations in beryllium because of its known dynamical structure and high counting rates.

Yavas, H.; Alp, E.; Sinn, H.; Alatas, A.; Said, A.; Shvydko, Y.; Toellner, T.; Khachatryan, R.; Billinge, S.; Hasan, Z.; Sturhahn, W.; Michigan State Univ.; Princeton Univ.; DESY

2007-11-11T23:59:59.000Z

473

X-ray tube with magnetic electron steering  

DOE Patents (OSTI)

An X-ray tube uses a magnetic field to steer electrons. The magnetic field urges electrons toward the anode, increasing the proportion of electrons emitted from the cathode that reach desired portions of the anode and consequently contribute to X-ray production. The magnetic field also urges electrons reflected from the anode back to the anode, further increasing the efficiency of the tube.

Reed, Kim W. (Albuquerque, NM); Turman, Bobby N. (Albuquerque, NM); Kaye, Ronald J. (Albuquerque, NM); Schneider, Larry X. (Albuquerque, NM)

2000-01-01T23:59:59.000Z

474

Ris-M-2751 X-Ray Energy Dispersive  

E-Print Network (OSTI)

(PHOT) k«V 50 Risø National Laboratory, DK-4000 Roskilde, Denmark October 1988 #12;Ris*-M-2751 X-ray energy is impinging on the sample (Fig. lb). Its wavelength (photon energy) is in the course of measurements changedm ii. S Risø-M-2751 X-Ray Energy Dispersive Diffraction Lecture Notes Bronislaw Buras BaKo 30 40 E

475

A compact scanning soft X-ray microscope  

SciTech Connect

Soft x-ray microscopes operating at wavelengths between 2.3 nm and 4.4 nm are capable of imaging wet biological cells with a resolution many times that of a visible light microscope. Several such soft x-ray microscopes have been constructed. However, with the exception of contact microscopes, all use synchrotrons as the source of soft x-ray radiation and Fresnel zone plates as the focusing optics. These synchrotron based microscopes are very successful but have the disadvantage of limited access. This dissertation reviews the construction and performance of a compact scanning soft x-ray microscope whose size and accessibility is comparable to that of an electron microscope. The microscope uses a high-brightness laser-produced plasma as the soft x-ray source and normal incidence multilayer-coated mirrors in a Schwarzschild configuration as the focusing optics. The microscope operates at a wavelength of 14 nm, has a spatial resolution of 0.5 {mu}m, and has a soft x-ray photon flux through the focus of 10{sup 4}-10{sup 5} s{sup {minus}1} when operated with only 170 mW of average laser power. The complete system, including the laser, fits on a single 4{prime} x 8{prime} optical table. The significant components of the compact microscope are the laser-produced plasma (LPP) source, the multilayer coatings, and the Schwarzschild objective. These components are reviewed, both with regard to their particular use in the current microscope and with regard to extending the microscope performance to higher resolution, higher speed, and operation at shorter wavelengths. Measurements of soft x-ray emission and debris emission from our present LPP source are presented and considerations given for an optimal LPP source. The LPP source was also used as a broadband