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1

Dynamic Transmission Electron Microscopy  

SciTech Connect

Dynamic transmission electron microscopy (DTEM) combines the benefits of high spatial resolution electron microscopy with the high temporal resolution of ultrafast lasers. The incorporation of these two components into a single instrument provides a perfect platform for in situ observations of material processes. However, previous DTEM applications have focused on observing structural changes occurring in samples exposed to high vacuum. Therefore, in order to expand the pump-probe experimental regime to more natural environmental conditions, in situ gas and liquid chambers must be coupled with Dynamic TEM. This chapter describes the current and future applications of in situ liquid DTEM to permit time-resolved atomic scale observations in an aqueous environment, Although this chapter focuses mostly on in situ liquid imaging, the same research potential exists for in situ gas experiments and the successful integration of these techniques promises new insights for understanding nanoparticle, catalyst and biological protein dynamics with unprecedented spatiotemporal resolution.

Evans, James E.; Jungjohann, K. L.; Browning, Nigel D.

2012-10-12T23:59:59.000Z

2

Directly correlated transmission electron microscopy and atom...  

NLE Websites -- All DOE Office Websites (Extended Search)

Directly correlated transmission electron microscopy and atom probe tomography of grain boundary oxidation in a Ni-Al binary Directly correlated transmission electron microscopy...

3

Electron microscopy and microanalysis Two transmission electron microscopes  

E-Print Network (OSTI)

Electron microscopy and microanalysis Two transmission electron microscopes (TEM) and three scanning electron micro- scopes (SEM) are operated by the De- partment. Attachments for TEM include energy dispersive X-ray spectrometer (EDS), scanning transmission attachment, serial electron energy loss

4

In-situ Transmission Electron Microscopy and Spectroscopy Studies...  

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Transmission Electron Microscopy and Spectroscopy Studies of Interfaces in Li-ion Batteries: Challenges and In-situ Transmission Electron Microscopy and Spectroscopy Studies of...

5

TRANSMISSION ELECTRON MICROSCOPY OF WEAKLY DEFORMED ALKALI HALIDE CRYSTALS  

E-Print Network (OSTI)

377 TRANSMISSION ELECTRON MICROSCOPY OF WEAKLY DEFORMED ALKALI HALIDE CRYSTALS H. STRUNK Max'importance croissante du durcissement de la solution solide. Abstract. 2014 Transmission electron microscopy (TEM Abstracts 7j66 - 7 I' 1. Introduction. - It is only some years ago that transmission electron microscopy

Boyer, Edmond

6

New Developments in Transmission Electron Microscopy for Nanotechnology**  

E-Print Network (OSTI)

New Developments in Transmission Electron Microscopy for Nanotechnology** By Zhong Lin Wang* 1. Electron Microscopy and Nanotechnology Nanotechnology, as an international initiative for science manufacturing are the foundation of nanotechnology. Tracking the historical background of why nanotechnology

Wang, Zhong L.

7

Instrument Series: Microscopy Environmental Transmission Electron Microscope  

NLE Websites -- All DOE Office Websites (Extended Search)

Environmental Transmission Environmental Transmission Electron Microscope EMSL's environmental transmission electron microscope (ETEM) provides in situ capabilities that enable atomic-resolution imaging and spectroscopic studies of materials under dynamic operating conditions. In contrast to traditional operation of TEM under high vacuum, EMSL's ETEM uniquely allows imaging within high- temperature and gas environments-with a gas pressure up to 20 Torr. With a spherical aberration corrector for the objective lens, the ETEM captures atomic-level processes as they occur, enabling vital research across a range of scientific fields. Research Applications Chemical science and engineering - providing in situ observation of catalytic processes with atomic-level resolution Materials science and engineering - allowing

8

Scanning Transmission Electron Microscopy Investigations of Complex Oxides  

NLE Websites -- All DOE Office Websites (Extended Search)

Scanning Transmission Electron Microscopy Investigations of Complex Oxides Scanning Transmission Electron Microscopy Investigations of Complex Oxides Monday, May 23, 2011 - 3:30pm SSRL Conference room 137-322 Professor Tom Vogt, NanoCenter & Department of Chemistry, University of South Carolina High-Angle-Annular-Dark-Field/Scanning Transmission Electron Microscopy (HAADF/STEM) is a technique uniquely suited for detailed studies of the structure and composition of complex oxides. The HAADF detector collects electrons which have interact inelastically with the potentials of the atoms in the specimen and therefore resembles the better known Z2 (Z is atomic number) Rutherford scattering. One class of important catalysts consists of bronzes based on pentagonal {Mo6O21} building units; these include Mo5O14 and Mo17O47. In the last 20 years, new materials doped with

9

Combined Scanning Transmission Electron Microscopy Tilt- and Focal Series  

SciTech Connect

In this study, a combined tilt- and focal series is proposed as a new recording scheme for high-angle annular dark-field scanning transmission electron microscopy (STEM) tomography. Three-dimensional (3D) data were acquired by mechanically tilting the specimen, and recording a through-focal series at each tilt direction. The sample was a whole-mount macrophage cell with embedded gold nanoparticles. The tilt focal algebraic reconstruction technique (TF-ART) is introduced as a new algorithm to reconstruct tomograms from such combined tilt- and focal series. The feasibility of TF-ART was demonstrated by 3D reconstruction of the experimental 3D data. The results were compared with a conventional STEM tilt series of a similar sample. The combined tilt- and focal series led to smaller missing wedge artifacts, and a higher axial resolution than obtained for the STEM tilt series, thus improving on one of the main issues of tilt series-based electron tomography.

Dahmen, Tim [German Research Center for Artificial Intelligence (DFKI), Germany] [German Research Center for Artificial Intelligence (DFKI), Germany; Baudoin, Jean-Pierre G [ORNL] [ORNL; Lupini, Andrew R [ORNL] [ORNL; Kubel, Christian [Karlsruhe Institute of Technology, Leopoldshafen, Germany] [Karlsruhe Institute of Technology, Leopoldshafen, Germany; Slusallek, Phillip [German Research Center for Artificial Intelligence (DFKI), Germany] [German Research Center for Artificial Intelligence (DFKI), Germany; De Jonge, Niels [ORNL] [ORNL

2014-01-01T23:59:59.000Z

10

Fabrication of curved-line nanostructures on membranes for transmission electron microscopy investigations of domain walls  

E-Print Network (OSTI)

Fabrication of curved-line nanostructures on membranes for transmission electron microscopy, Cambridge CB2 3QZ, United Kingdom Available online 28 February 2006 Abstract We have fabricated curved-line ferromagnetic nanostructures on membranes for transmission electron microscopy investigations of the equilibrium

Dunin-Borkowski, Rafal E.

11

A Transmission Electron Microscopy Study of Presolar Hibonite  

Science Journals Connector (OSTI)

We report isotopic and microstructural data on five presolar hibonite grains (KH1, KH2, KH6, KH15, and KH21) identified in an acid residue of the Krymka LL3.1 ordinary chondrite. Isotopic measurements by secondary ion mass spectrometry (SIMS) verified a presolar circumstellar origin for the grains. Transmission electron microscopy (TEM) examination of the crystal structure and chemistry of the grains was enabled by in situ sectioning and lift-out with a focused-ion-beam scanning-electron microscope (FIB-SEM). Comparisons of isotopic compositions with models indicate that four of the five grains formed in low-mass stars that evolved through the red giant/asymptotic giant branches (RGBs/AGBs), whereas one grain formed in the ejecta of a Type II supernova. Selected-area electron-diffraction patterns show that all grains are single crystals of hibonite. Some grains contain minor structural perturbations (stacking faults) and small spreads in orientation that can be attributed to a combination of growth defects and mechanical processing by grain-grain collisions. The similar structure of the supernova grain to those from RGB/AGB stars indicates a similarity in the formation conditions. Radiation damage (e.g., point defects), if present, occurs below our detection limit. Of the five grains we studied, only one has the pure hibonite composition of CaAl12O19. All others contain minor amounts of Mg, Si, Ti, and Fe. The microstructural data are generally consistent with theoretical predictions, which constrain the circumstellar condensation temperature to a range of 1480-1743 K, assuming a corresponding total gas pressure between 1 ? 10–6 and 1 ? 10–3 atm. The TEM data were also used to develop a calibration for SIMS determination of Ti contents in oxide grains. Grains with extreme 18O depletions, indicating deep mixing has occurred in their parent AGB stars, are slightly Ti enriched compared with grains from stars without deep mixing, most likely reflecting differences in grain condensation conditions.

Thomas J. Zega; Conel M. O'D. Alexander; Larry R. Nittler; Rhonda M. Stroud

2011-01-01T23:59:59.000Z

12

In-Situ Electrochemical Transmission Electron Microscopy for Battery Research  

SciTech Connect

The recent development of in-situ liquid stages for (scanning) transmission electron microscopes now makes it possible for us to study the details of electrochemical processes under operando conditions. As electrochemical processes are complex, care must be taken to calibrate the system before any in-situ/operando observations. In addition, as the electron beam can cause effects that look similar to electrochemical processes at the electrolyte/electrode interface, an understanding of the role of the electron beam in modifying the operando observations must also be understood. In this paper we describe the design, assembly, and operation of an in-situ electrochemical cell, paying particular attention to the method for controlling and quantifying the experimental parameters. The use of this system is then demonstrated for the lithiation/delithiation of silicon nanowires.

Mehdi, Beata L [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Gu, Meng [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Parent, Lucas [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Xu, WU [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Nasybulin, Eduard [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Chen, Xilin [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Unocic, Raymond R [ORNL] [ORNL; Xu, Pinghong [University of California, Davis] [University of California, Davis; Welch, David [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Abellan, Patricia [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Zhang, Ji-Guang [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Liu, Jun [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Wang, Chongmin [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Arslan, Ilke [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Evans, James E [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL); Browning, Nigel [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL)

2014-01-01T23:59:59.000Z

13

Visualizing Macromolecular Complexes with In Situ Liquid Scanning Transmission Electron Microscopy  

SciTech Connect

A central focus of biological research is understanding the structure/function relationship of macromolecular protein complexes. Yet conventional transmission electron microscopy techniques are limited to static observations. Here we present the first direct images of purified macromolecular protein complexes using in situ liquid scanning transmission electron microscopy. Our results establish the capability of this technique for visualizing the interface between biology and nanotechnology with high fidelity while also probing the interactions of biomolecules within solution. This method represents an important advancement towards allowing future high-resolution observations of biological processes and conformational dynamics in real-time.

Evans, James E.; Jungjohann, K. L.; Wong, Peony C. K.; Chiu, Po-Lin; Dutrow, Gavin H.; Arslan, Ilke; Browning, Nigel D.

2012-11-01T23:59:59.000Z

14

Imaging and microanalysis of thin ionomer layers by scanning transmission electron microscopy  

SciTech Connect

Improved conditions for imaging and spectroscopic mapping of thin perfluorosulfonic acid (PFSA) ionomer layers in fuel cell electrodes by scanning transmission electron microscopy (STEM) have been investigated. These conditions are first identified on model systems of Nafion ionomer-coated nanostructured thin films and nanoporous Si. The optimized conditions are then applied in a quantitative study of the ionomer through-layer loading for two typical electrode catalyst coatings using electron energy loss and energy dispersive X-ray spectroscopy in the transmission electron microscope. The e-beam induced damage to the perfluorosulfonic acid (PFSA) ionomer is quantified by following the fluorine mass loss with electron exposure and is then mitigated by a few orders of magnitude using cryogenic specimen cooling and a higher incident electron voltage. Multivariate statistical analysis is also applied to the analysis of spectrum images for data denoising and unbiased separation of independent components related to the catalyst, ionomer, and support.

Cullen, David A [ORNL; Koestner, Roland [General Motors Corporation; Kukreja, Ratan [General Motors Corporation; Minko, Sergiy [Clarkson University, Potsdam, NY; Trotsenko, Oleksandr [Clarkson University, Potsdam, NY; Tokarev, Alexander V [ORNL; Guetaz, Laure [French Atomic Energy Commission (CEA), Grenoble; Meyer III, Harry M [ORNL; Parish, Chad M [ORNL; More, Karren Leslie [ORNL

2014-01-01T23:59:59.000Z

15

In situ transmission electron microscopy observation of silver oxidation in ionized/atomic gas.  

SciTech Connect

The interaction between silver and ionized and atomic gas was observed directly by in situ transmission electron microscopy with an environmental cell for the first time. The electron beam provides dual functions as the source of both gas ionization and imaging. The concentration of ionized gas was tuned via adjusting the current density of the electron beam. Oxidation of the silver is observed in situ, indicating the presence of ionized and/or atomic oxygen. The evolution of microstructure and phase constituents was characterized. Then the oxidation rate was measured, and the relationships among grain size, mass transport rate, and electron flux were characterized. The role of the electron beam is discussed, and the results are rationalized with respect to ex situ results from the literature.

Sun, L.; Noh, K. W.; Wen, J-G.; Dillon, S. J. (Materials Science Division); (Massachusetts Inst. Tech.); (Univ. Illinois - Urbana)

2011-10-17T23:59:59.000Z

16

In situ transmission electron microscopy analysis of conductive filament during solid electrolyte resistance switching  

SciTech Connect

An in situ transmission electron microscopy (TEM) analysis of a solid electrolyte, Cu-GeS, during resistance switching is reported. Real-time observations of the filament formation and disappearance process were performed in the TEM instrument and the conductive-filament-formation model was confirmed experimentally. Narrow conductive filaments were formed corresponding to resistance switching from high- to low-resistance states. When the resistance changed to high-resistance state, the filament disappeared. It was also confirmed by use of selected area diffractometry and energy-dispersive x-ray spectroscopy that the conductive filament was made of nanocrystals composed mainly of Cu.

Fujii, Takashi; Arita, Masashi; Takahashi, Yasuo [Graduate School of Information Science and Technology, Hokkaido University, Sapporo 060-0814 (Japan); Fujiwara, Ichiro [Semiconductor Technology Academic Research Center, 3-17-2 Shinyokohama, Kohoku-ku, Yokohama 222-0033 (Japan)

2011-05-23T23:59:59.000Z

17

Structural defects in GaN revealed by Transmission Electron Microscopy  

SciTech Connect

This paper reviews the various types of structural defects observed by Transmission Electron Microscopy in GaN heteroepitaxial layers grown on foreign substrates and homoepitaxial layers grown on bulk GaN substrates. The structural perfection of these layers is compared to the platelet self-standing crystals grown by High Nitrogen Pressure Solution. Defects in undoped and Mg doped GaN are discussed. Some models explaining the formation of inversion domains in heavily Mg doped layers that are possible defects responsible for the difficulties of p-doping in GaN are also reviewed.

Liliental-Weber, Zuzanna

2014-04-18T23:59:59.000Z

18

Mapping the Valence States of Transition-Metal Elements Using Energy-Filtered Transmission Electron Microscopy  

E-Print Network (OSTI)

spectrum of MnO2 acquired at 200 kV using a Hitachi HF-2000 transmission electron microscope equipped lines observed in electron energy-loss spectroscopy in a transmission electron microscope (TEMMapping the Valence States of Transition-Metal Elements Using Energy-Filtered Transmission Electron

Wang, Zhong L.

19

Biological Applications and Transmission Electron Microscopy Investigations of Mesoporous Silica Nanoparticles  

SciTech Connect

The research presented and discussed within involves the development of novel biological applications of mesoporous silica nanoparticles (MSN) and an investigation of mesoporous material by transmission electron microscopy (TEM). Mesoporous silica nanoparticles organically functionalized shown to undergo endocytosis in cancer cells and drug release from the pores was controlled intracellularly and intercellularly. Transmission electron microscopy investigations demonstrated the variety of morphologies produced in this field of mesoporous silica nanomaterial synthesis. A series of room-temperature ionic liquid (RTIL) containing mesoporous silica nanoparticle (MSN) materials with various particle morphologies, including spheres, ellipsoids, rods, and tubes, were synthesized. By changing the RTIL template, the pore morphology was tuned from the MCM-41 type of hexagonal mesopores to rotational moire type of helical channels, and to wormhole-like porous structures. These materials were used as controlled release delivery nanodevices to deliver antibacterial ionic liquids against Escherichia coli K12. The involvement of a specific organosiloxane function group, covalently attached to the exterior of fluorescein doped mesoporous silica nanoparticles (FITC-MSN), on the degree and kinetics of endocytosis in cancer and plant cells was investigated. The kinetics of endocystosis of TEG coated FITC-MSN is significantly quicker than FITC-MSN as determined by flow cytometry experiments. The fluorescence confocal microscopy investigation showed the endocytosis of TEG coated-FITC MSN triethylene glycol grafted fluorescein doped MSN (TEG coated-FITC MSN) into both KeLa cells and Tobacco root protoplasts. Once the synthesis of a controlled-release delivery system based on MCM-41-type mesoporous silica nanorods capped by disulfide bonds with superparamagnetic iron oxide nanoparticles was completed. The material was characterized by general methods and the dosage and kinetics of the antioxidant dependent release was measured. Finally, the biological interaction of the material was determined along with TEM measurements. An electron investigation proved that the pore openings of the MSN were indeed blocked by the Fe{sub 3}O{sub 4} nanoparticles. The biological interaction investigation demonstrated Fe{sub 3}O{sub 4}-capped MSN endocytosis into HeLa cells. Not only does the material enter the cells through endocytosis, but it seems that fluorescein was released from the pores most probably caused by disulfide bond reducing molecules, antioxidants. In addition to endocytosis and release, the Fe{sub 3}O{sub 4}-capped MSN propelled the cells across a cuvette upon induction of a magnet force. Finally, an important aspect of materials characterization is transmission electron microscopy. A TEM investigation demonstrated that incorporating different functional groups during the synthesis (co-condensation) changed the particle and pore morphologies.

Brian G. Trewyn

2006-05-01T23:59:59.000Z

20

Transmission Electron Microscopy Study of Eu-Doped Y2O3 Nanosheets and Nanotubes  

SciTech Connect

A hydrothermal method was used to synthesize high-purity Eu-doped Y{sub 2}O{sub 3} nanosheets and nanotubes with an approximate molar ratio of (0.1):(1.0) for Eu:Y. High-resolution transmission electron microscopy, energy dispersive X-ray spectroscopy analysis and synchrotron X-ray diffraction were used to characterize these nanomaterials. A body-centered cubic structure was confirmed for the nanotubes. The lattice parameter of Eu-doped Y{sub 2}O{sub 3} nanotubes were 0.12% larger as compared to that of pure Y{sub 2}O{sub 3} which was attributed to the larger ionic radius of Eu{sup 3+} (0.947 {angstrom}) than that of Y{sup 3+} (0.900 {angstrom}). The nanosheets had a similar structure. Nanosheets of approximate dimensions 600 to 800 nm length and width were obtained using a slightly lower pH value, and they were highly textured. The high resolution transmission electron microscopy images showed that the nanotubes are fully crystalline. The nanotubes were typically 1.5-3 {micro}m in length and 50-200 nm in diameter. Using a pH value of approximately 10, stable nanotubes were obtained. It is anticipated that nanosheets might have rolled to form more stable nanotubes.

H Sun; T Chaudhuri; E Kenik; H Zhu; Y Ma

2011-12-31T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

Atomic-Scale Imaging and Spectroscopy for In Situ Liquid Scanning Transmission Electron Microscopy  

SciTech Connect

Observation of growth, synthesis, dynamics and electrochemical reactions in the liquid state is an important yet largely unstudied aspect of nanotechnology. The only techniques that can potentially provide the insights necessary to advance our understanding of these mechanisms is simultaneous atomic-scale imaging and quantitative chemical analysis (through spectroscopy) under environmental conditions in the transmission electron microscope (TEM). In this study we describe the experimental and technical conditions necessary to obtain electron energy loss (EEL) spectra from a nanoparticle in colloidal suspension using aberration corrected scanning transmission electron microscopy (STEM) combined with the environmental liquid stage. At a fluid path length below 400 nm, atomic resolution images can be obtained and simultaneous compositional analysis can be achieved. We show that EEL spectroscopy can be used to quantify the total fluid path length around the nanoparticle, and demonstrate characteristic core-loss signals from the suspended nanoparticles can be resolved and analyzed to provide information on the local interfacial chemistry with the surrounding environment. The combined approach using aberration corrected STEM and EEL spectra with the in situ fluid stage demonstrates a plenary platform for detailed investigations of solution based catalysis and biological research.

Jungjohann, K. L.; Evans, James E.; Aguiar, Jeff; Arslan, Ilke; Browning, Nigel D.

2012-06-04T23:59:59.000Z

22

Characterization of polysilicon films by Raman spectroscopy and transmission electron microscopy: A comparative study  

SciTech Connect

Samples of chemically-vapor-deposited micrometer and sub-micrometer-thick films of polysilicon were analyzed by transmission electron microscopy (TEM) in cross-section and by Raman spectroscopy with illumination at their surface. TEM and Raman spectroscopy both find varying amounts of polycrystalline and amorphous silicon in the wafers. Raman spectra obtained using blue, green and red excitation wavelengths to vary the Raman sampling depth are compared with TEM cross-sections of these films. Films showing crystalline columnar structures in their TEM micrographs have Raman spectra with a band near 497 cm{sup {minus}1} in addition to the dominant polycrystalline silicon band (521 cm{sup {minus}1}). The TEM micrographs of these films have numerous faulted regions and fringes indicative of nanometer-scale silicon structures, which are believed to correspond to the 497cm{sup {minus}1} Raman band.

Tallant, D.R.; Headley, T.J.; Medernach, J.W. [Sandia National Labs., Albuquerque, NM (United States); Geyling, F. [SEMATECH, Austin, TX (United States)

1993-11-12T23:59:59.000Z

23

Novel scheme for the preparation of transmission electron microscopy specimens with a focused ion beam  

Science Journals Connector (OSTI)

A novel scheme is presented for the preparation of cross?section transmission electron microscopy(TEM) specimens with a focused ion beam(FIB). This scheme is particularly suitable for highly structured substrates such as integrated circuits. The specimen is made by cutting a thin slice of material from the substrate by sputtering with the FIB. The position of the specimen can be selected with submicron resolution. The specimen is subsequently removed from the substrate and transported to a standard TEM?specimen holder. A specimen ready for TEM inspection can be prepared within 2 hs. The samples are of excellent quality as is illustrated with cross?section TEM images of FIB?made specimens of an electrically programmable read?only memory.

M. H. F. Overwijk; F. C. van den Heuvel; C. W. T. Bulle?Lieuwma

1993-01-01T23:59:59.000Z

24

Advances in cryogenic transmission electron microscopy for the characterization of dynamic self-assembling nanostructures  

Science Journals Connector (OSTI)

Elucidating the structural information of nanoscale materials in their solvent-exposed state is crucial, as a result, cryogenic transmission electron microscopy (cryo-TEM) has become an increasingly popular technique in the materials science, chemistry, and biology communities. Cryo-TEM provides a method to directly visualize the specimen structure in a solution-state through a thin film of vitrified solvent. This technique complements X-ray, neutron, and light scattering methods that probe the statistical average of all species present; furthermore, cryo-TEM can be used to observe changes in structure over time. In the area of self-assembly, this tool has been particularly powerful for the characterization of natural and synthetic small molecule assemblies, as well as hybrid organic–inorganic composites. In this review, we discuss recent advances in cryogenic TEM in the context of self-assembling systems with emphasis on characterization of transitions observed in response to external stimuli.

Christina J. Newcomb; Tyson J. Moyer; Sungsoo S. Lee; Samuel I. Stupp

2012-01-01T23:59:59.000Z

25

Transmission electron microscopy of oxide dispersion strengthened (ODS) molybdenum: effects of irradiation on material microstructure  

SciTech Connect

Oxide dispersion strengthened (ODS) molybdenum has been characterized using transmission electron microscopy (TEM) to determine the effects of irradiation on material microstructure. This work describes the results-to-date from TEM characterization of unirradiated and irradiated ODS molybdenum. The general microstructure of the unirradiated material consists of fine molybdenum grains (< 5 {micro}m average grain size) with numerous low angle boundaries and isolated dislocation networks. 'Ribbon'-like lanthanum oxides are aligned along the working direction of the product form and are frequently associated with grain boundaries, serving to inhibit grain boundary and dislocation movement. In addition to the 'ribbons', discrete lanthanum oxide particles have also been detected. After irradiation, the material is characterized by the presence of nonuniformly distributed large ({approx} 20 to 100 nm in diameter), multi-faceted voids, while the molybdenum grain size and oxide morphology appear to be unaffected by irradiation.

Baranwal, R. and Burke, M.G.

2003-03-03T23:59:59.000Z

26

Rendering graphene supports hydrophilic with non-covalent aromatic functionalization for transmission electron microscopy  

SciTech Connect

Amorphous carbon films have been routinely used to enhance the preparation of frozen-hydrated samples for transmission electron microscopy (TEM), either in retaining protein concentration, providing mechanical stability or dissipating sample charge. However, strong background signal from the amorphous carbon support obstructs that of the sample, and the insulating properties of thin amorphous carbon films preclude any efficiency in dispersing charge. Graphene addresses the limitations of amorphous carbon. Graphene is a crystalline material with virtually no phase or amplitude contrast and unparalleled, high electrical carrier mobility. However, the hydrophobic properties of graphene have prevented its routine application in Cryo-TEM. This Letter reports a method for rendering graphene TEM supports hydrophilic—a convenient approach maintaining graphene's structural and electrical properties based on non-covalent, aromatic functionalization.

Pantelic, Radosav S., E-mail: pantelic@imbb.forth.gr [National Cancer Institute, 50 South Drive, Building 50, Room 4306, Bethesda, Maryland 20892 (United States); Fu, Wangyang; Schoenenberger, Christian [Department of Physics, University of Basel, Klingelbergstrasse 82, Basel CH-4056 (Switzerland); Stahlberg, Henning [Center for Cellular Imaging and NanoAnalytics, Biozentrum, University of Basel, Mattenstrasse 26, WRO-1058, Basel CH-4058 (Switzerland)

2014-03-31T23:59:59.000Z

27

TRANSMISSION ELECTRON MICROSCOPY OF Al-RICH SILICATE STARDUST FROM ASYMPTOTIC GIANT BRANCH STARS  

SciTech Connect

We report on transmission electron microscopy (TEM) investigations of two mineralogically unusual stardust silicates to constrain their circumstellar condensation conditions. Both grains were identified by high spatial resolution nano secondary ion mass spectrometry (NanoSIMS) in the Acfer 094 meteorite, one of the most pristine carbonaceous chondrites available for study. One grain is a highly crystalline, highly refractory (Fe content < 0.5 at%), structurally undisturbed orthopyroxene (MgSiO{sub 3}) with an unusually high Al content (1.8 {+-} 0.5 at%). This is the first TEM documentation of a single crystal pyroxene within the complete stardust silicate data set. We interpret the microstructure and chemistry of this grain as being a direct condensate from a gas of locally non-solar composition (i.e., with a higher-than-solar Al content and most likely also a lower-than-solar Mg/Si ratio) at (near)-equilibrium conditions. From the overabundance of crystalline olivine (six reported grains to date) compared to crystalline pyroxene (only documented as a single crystal in this work) we infer that formation of olivine over pyroxene is favored in circumstellar environments, in agreement with expectations from condensation theory and experiments. The second stardust silicate consists of an amorphous Ca-Si rich material which lacks any crystallinity based on TEM observations in which tiny (<20 nm) hibonite nanocrystallites are embedded. This complex assemblage therefore attests to the fast cooling and rapidly changing chemical environments under which dust grains in circumstellar shells form.

Vollmer, Christian [Institute for Mineralogy, University of Muenster, Correnssstr. 24, D-48149 Muenster (Germany); Hoppe, Peter [Max Planck Institute for Chemistry, Particle Chemistry Department, Hahn-Meitner-Weg 1, D-55128 Mainz (Germany); Brenker, Frank E., E-mail: christian.vollmer@wwu.de [Institute of Geoscience/Mineralogy, Goethe-University Frankfurt, Altenhoeferallee 1, D-60438 Frankfurt (Germany)

2013-05-20T23:59:59.000Z

28

Electron Microscopy Lab  

NLE Websites -- All DOE Office Websites (Extended Search)

Facilities » Facilities » Electron Microscopy Lab Electron Microscopy Lab Focusing on the study of microstructures with electron and ion beam instruments, including crystallographic and chemical techniques. April 12, 2012 Transmission electron microscope Rob Dickerson examines a multiphase oxide scale using the FEI Titan 80-300 transmission electron microscope. Contact Rob Dickerson (505) 667-6337 Email Rod McCabe (505) 606-1649 Email Pat Dickerson (505) 665-3036 Email Tom Wynn (505) 665-6861 Email Dedicated to the characterization of materials through imaging, chemical, and crystallographic analyses of material microstructures in support of Basic Energy Science, Laboratory Directed Research and Development, DoD, DOE, Work for Others, nuclear energy, and weapons programs. Go to full website »

29

High-energy-resolution monochromator for aberration-corrected scanning transmission electron microscopy/electron energy-loss spectroscopy  

Science Journals Connector (OSTI)

...R. F. 1996 Electron energy-loss spectroscopy in...microscope, 2nd edn. New York, NYPlenum. Egerton...Transmission electron energy loss spectrometry in materials...energy-gain spectroscopy. New J. Phys. 10, 1367-2630...

2009-01-01T23:59:59.000Z

30

Probing the electronic structure of graphene sheets with various thicknesses by scanning transmission X-ray microscopy  

SciTech Connect

The electronic structure of an aggregation of graphene sheets with various thicknesses was probed by scanning transmission X-ray microscopy. A uniform oxidation of the graphene sheets in the flat area was observed regardless of the thickness, while in the folded area the result could be strongly affected by the geometry. Moreover, thick parts of the aggregation showed strong angle-dependence to the incident X-ray, while thin parts showed less angle-dependence, which might be related to the surface wrinkles and ripples. The electronic structure differences due to the geometry and thickness suggest a complicated situation in the aggregation of graphene sheets.

Bai, Lili; Liu, Jinyin; Zhao, Guanqi; Gao, Jing; Sun, Xuhui, E-mail: xhsun@suda.edu.cn, E-mail: jzhong@suda.edu.cn; Zhong, Jun, E-mail: xhsun@suda.edu.cn, E-mail: jzhong@suda.edu.cn [Soochow University-Western University Centre for Synchrotron Radiation Research, Institute of Functional Nano and Soft Materials Laboratory (FUNSOM) and Collaborative Innovation Center of Suzhou Nano Science and Technology, Soochow University, Suzhou 215123 (China)] [Soochow University-Western University Centre for Synchrotron Radiation Research, Institute of Functional Nano and Soft Materials Laboratory (FUNSOM) and Collaborative Innovation Center of Suzhou Nano Science and Technology, Soochow University, Suzhou 215123 (China)

2013-12-16T23:59:59.000Z

31

Gas mixing system for imaging of nanomaterials under dynamic environments by environmental transmission electron microscopy  

SciTech Connect

A gas mixing manifold system that is capable of delivering a stable pressure stream of a desired composition of gases into an environmental transmission electron microscope has been developed. The system is designed to provide a stable imaging environment upon changes of either the composition of the gas mixture or upon switching from one gas to another. The design of the system is described and the response of the pressure inside the microscope, the sample temperature, and sample drift in response to flow and composition changes of the system are reported.

Akatay, M. Cem [School of Materials Engineering and Birck Nanotechnology Center, Purdue University, West Lafayette, Indiana 47907 (United States)] [School of Materials Engineering and Birck Nanotechnology Center, Purdue University, West Lafayette, Indiana 47907 (United States); Zvinevich, Yury; Ribeiro, Fabio H., E-mail: fabio@purdue.edu, E-mail: estach@bnl.gov [Forney Hall of Chemical Engineering, Purdue University, West Lafayette, Indiana 47907 (United States); Baumann, Philipp [Computer Sciences, University of Applied Sciences of Northeastern Switzerland, 4132 Muttenz, Switzerland and Department of Physics, Yeshiva University, New York, New York 10016 (United States)] [Computer Sciences, University of Applied Sciences of Northeastern Switzerland, 4132 Muttenz, Switzerland and Department of Physics, Yeshiva University, New York, New York 10016 (United States); Stach, Eric A., E-mail: fabio@purdue.edu, E-mail: estach@bnl.gov [Center for Functional Nanomaterials, Brookhaven National Laboratory, Upton, New York 11973 (United States)

2014-03-15T23:59:59.000Z

32

Studying Fischer-Tropsch catalysts using transmission electron microscopy and model systems of nanoparticles on planar supports.  

SciTech Connect

Nanoparticle model systems on planar supports form a versatile platform for studying morphological and compositional changes of catalysts due to exposure to realistic reaction conditions. We review examples from our work on iron and cobalt catalysts, which can undergo significant rearrangement in the reactive environment of the Fischer-Tropsch synthesis. The use of specially designed, silicon based supports with thin film SiO{sub 2} enables the application of transmission electron microscopy, which has furnished important insight into e.g. the mechanisms of catalyst regeneration.

Thune, P. C.; Weststrate, C. J.; Moodley, P.; Saib, A. M.; van de Loosdrecht, J.; Miller, J. T.; Niemantsverdriet, J. W. (Chemical Sciences and Engineering Division); (Eindhoven Univ. of Technology); (Sasol Technology)

2011-01-01T23:59:59.000Z

33

Three-Dimensional Aberration-Corrected Scanning Transmission Electron Microscopy for Biology  

SciTech Connect

Recent instrumental developments have enabled greatly improved resolution of scanning transmission electron microscopes (STEM) through aberration correction. An additional and previously unanticipated advantage of aberration correction is the greatly improved depth sensitivity that has led to the reconstruction of a three-dimensional (3D) image from a focal series. In this chapter the potential of aberration-corrected 3D STEM to provide major improvements in the imaging capabilities for biological samples will be discussed. This chapter contains a brief overview ofthe various high-resolution 3D imaging techniques, a historical perspective of the development of STEM, first estimates of the dose-limited axial and lateral resolution on biological samples and initial experiments on stained thin sections.

De Jonge, Niels [ORNL; Sougrat, Rachid [ORNL; Pennycook, Stephen J [ORNL; Peckys, Diana B [ORNL; Lupini, Andrew R [ORNL

2007-01-01T23:59:59.000Z

34

Thermodynamic Prediction of Compositional Phases Confirmed by Transmission Electron Microscopy on Tantalum-Based Alloy Weldments  

SciTech Connect

Tantalum alloys have been used by the U.S. Department of Energy as structural alloys for radioisotope based thermal to electrical power systems since the 1960s. Tantalum alloys are attractive for high temperature structural applications due to their high melting point, excellent formability, good thermal conductivity, good ductility (even at low temperatures), corrosion resistance, and weldability. Tantalum alloys have demonstrated sufficient high-temperature toughness to survive prolonged exposure to the radioisotope power-system working environment. Typically, the fabrication of power systems requires the welding of various components including the structural members made of tantalum alloys. Issues such as thermodynamics, lattice structure, weld pool dynamics, material purity and contamination, and welding atmosphere purity all potentially confound the understanding of the differences between the weldment properties of the different tantalum-based alloys. The objective of this paper is to outline the thermodynamically favorable material phases in tantalum alloys, with and without small amounts of hafnium, during and following solidification, based on the results derived from the FactSage(c) Integrated Thermodynamic Databank. In addition, Transition Electron Microscopy (TEM) data will show for the first time, the changes occurring in the HfC before and after welding, and the data will elucidate the role HfC plays in pinning grain boundaries.

Moddeman, William E.; Birkbeck, Janine C. [BWXT Pantex, Amarillo, Texas 79120-0020 (United States); Barklay, Chadwick D.; Kramer, Daniel P. [University of Dayton Research Institute, Dayton OH 45469-0102 (United States); Miller, Roger G.; Allard, Lawrence F. [Oak Ridge National Laboratory, Oak Ridge, TN 37831-6064 (United States)

2007-01-30T23:59:59.000Z

35

Microstructure of highly strained BiFeO{sub 3} thin films: Transmission electron microscopy and electron-energy loss spectroscopy studies  

SciTech Connect

Microstructure and electronic structure of highly strained bismuth ferrite (BiFeO{sub 3}) thin films grown on lanthanum aluminate substrates are studied using high-resolution transmission and scanning transmission electron microscopies and electron energy loss spectroscopy (EELS). Monoclinic and tetragonal phases were observed in films grown at different temperatures, and a mix of both phases was detected in a film grown at intermediate temperature. In this film, a smooth transition of the microstructure was found between the monoclinic and the tetragonal phases. A considerable increase in the c-axis parameters was observed in both phases compared with the rhombohedral bulk phase. The off-center displacement of iron (Fe) ions was increased in the monoclinic phase as compared with the tetragonal phase. EEL spectra show different electronic structures in the monoclinic and the tetragonal phases. These experimental observations are well consistent with the results of theoretical first-principle calculations performed.

Heon Kim, Young, E-mail: young.h.kim@kriss.re.kr [Max Planck Institute of Microstructure Physics, Weinberg 2, D-06120 Halle (Germany); Korea Research Institute of Standards and Science (KRISS), Daejeon 305-340 (Korea, Republic of); Bhatnagar, Akash; Pippel, Eckhard; Hesse, Dietrich [Max Planck Institute of Microstructure Physics, Weinberg 2, D-06120 Halle (Germany); Alexe, Marin [Max Planck Institute of Microstructure Physics, Weinberg 2, D-06120 Halle (Germany); University of Warwick, Coventry CV4 7AL, West Midlands (United Kingdom)

2014-01-28T23:59:59.000Z

36

A transmission electron microscopy investigation of inverse melting in Nb{sub 45}Cr{sub 55}  

SciTech Connect

In inverse melting, a supersaturated crystalline phase transforms polymorphously under heat treatment to the amorphous state. Inverse melting of body-centered cubic (bcc) Nb{sub 45}Cr{sub 55} is studied using transmission electron microscopy (TEM) and high resolution TEM (HRTEM). The crystalline to amorphous transformation is heterogeneous, initiating at the bcc grain boundaries. HRTEM reveals 2-3 nm domains with medium range order (MRO) in the amorphous phase. Preferred orientation of MRO domains is found on a scale corresponding to the precursor bcc grain size. Using HRTEM and calorimetry, MRO development in cosputtered Nb{sub 45}Cr{sub 55} films is characterized and compared to that in the amorphous phase produced by inverse melting. {copyright} {ital 1997 Materials Research Society.}

Sinkler, W.; Michaelsen, C.; Bormann, R. [Institute for Materials Research, GKSS Research Center, 21502 Geesthacht (Germany)

1997-07-01T23:59:59.000Z

37

Transmission electron microscopy characterization of laser-clad iron-based alloy on Al-Si alloy  

SciTech Connect

Microstructure characterization is important for controlling the quality of laser cladding. In the present work, a detailed microstructure characterization by transmission electron microscopy was carried out on the iron-based alloy laser-clad on Al-Si alloy and an unambiguous identification of phases in the coating was accomplished. It was found that there is austenite, Cr{sub 7}C{sub 3} and Cr{sub 23}C{sub 6} in the clad region; {alpha}-Al, NiAl{sub 3}, Fe{sub 2}Al{sub 5} and FeAl{sub 2} in the interface region; and {alpha}-Al and silicon in the heat-affected region. A brief discussion was given for their existence based on both kinetic and thermodynamic principles.

Mei, Z. [State Key Lab of Die and Mould Technology, Huazhong University of Science and Technology, Wuhan 430074 (China)]. E-mail: mikemei_99@yahoo.com; Wang, W.Y. [Institute of Materials Science and Engineering, Henan University of Science and Technology, Luoyang 471003 (China); Wang, A.H. [State Key Lab of Die and Mould Technology, Huazhong University of Science and Technology, Wuhan 430074 (China)

2006-04-15T23:59:59.000Z

38

New views of materials through aberration-corrected scanning transmission electron microscopy  

Science Journals Connector (OSTI)

......analysis to solving energy problems. Phil...eds. (2007) New York: Springer...and electron energy loss spectroscopy...eds. (2011) New York: Springer...for electron energy loss spectroscopy...can now give new insights into......

S. J. Pennycook; M. Varela

2011-08-01T23:59:59.000Z

39

Electron Microscopy | Center for Functional Nanomaterials  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron Microscopy Facility Electron Microscopy Facility Electron Microscopy This facility consists of four top-of-the line transmission electron microscopes, two of which are highly specialized instruments capable of extreme levels of resolution, achieved through spherical aberration correction. The facility is also equipped with extensive sample-preparation capabilities. The scientific interests of the staff focus on understanding the microscopic origin of the physical and chemical behavior of materials, with specific emphasis on in-situ studies of materials in native, functional environments. Capabilities Atomic-resolution imaging of internal materials structure with scanning transmission and transmission electron microscopy Spectroscopic characterization with energy dispersive x-ray

40

Probing the Degradation Mechanisms in Electrolyte Solutions for Li-ion Batteries by In-Situ Transmission Electron Microscopy  

SciTech Connect

One of the goals in the development of new battery technologies is to find new electrolytes with increased electrochemical stability. In-situ (scanning) transmission electron microscopy ((S)TEM) using an electrochemical fluid cell provides the ability to rapidly and directly characterize electrode/electrolyte interfacial reactions under battery relevant electrochemical conditions. Furthermore, as the electron beam itself causes a localized electrochemical reaction when it interacts with the electrolyte, the breakdown products that occur during the first stages of battery operation can potentially be simulated and characterized using a straightforward in-situ liquid stage (without electrochemical biasing capabilities). In this paper, we have studied the breakdown of a range of inorganic/salt complexes that are used in state-of-the-art Li-ion battery systems. The results of the in-situ (S)TEM experiments matches with previous stability tests performed during battery operation and the breakdown products and mechanisms are also consistent with known mechanisms. This analysis indicates that in-situ liquid stage (S)TEM observations can be used to directly test new electrolyte designs and provide structural insights into the origin of the solid electrolyte interphase (SEI) formation mechanism.

Abellan Baeza, Patricia; Mehdi, Beata L.; Parent, Lucas R.; Gu, Meng; Park, Chiwoo; Xu, Wu; Zhang, Yaohui; Arslan, Ilke; Zhang, Jiguang; Wang, Chong M.; Evans, James E.; Browning, Nigel D.

2014-02-21T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Structural Transformations in self-assembled Semiconductor Quantum Dots as inferred by Transmission Electron Microscopy  

E-Print Network (OSTI)

electronic and optoelectronic devices.1-3 ZnO is a promising material for UV optoelectronics due to its of the results have been widely reproduced or resulted in stable optoelectronic devices. p-type ZnO NWs have also

Moeck, Peter

42

Transmission electron microscopy and atom probe specimen preparation from mechanically alloyed powder using the focused ion-beam lift-out technique  

Science Journals Connector (OSTI)

......prepared by consolidation of amorphous powders in the supercooled liquid region. Intermetallics (2004) 12:1109-1113. 6 Overwijk M H F , Van Den Heuvel F C, Bulle-Lieuwma C W T. Novel scheme for the preparation of transmission electron microscopy specimens......

Pyuck-Pa Choi; Young-Soon Kwon; Ji-Soon Kim; Tala?at Al-Kassab

2007-04-01T23:59:59.000Z

43

Separating strain from composition in unit cell parameter maps obtained from aberration corrected high resolution transmission electron microscopy imaging  

SciTech Connect

Based on the evaluation of lattice parameter maps in aberration corrected high resolution transmission electron microscopy images, we propose a simple method that allows quantifying the composition and disorder of a semiconductor alloy at the unit cell scale with high accuracy. This is realized by considering, next to the out-of-plane, also the in-plane lattice parameter component allowing to separate the chemical composition from the strain field. Considering only the out-of-plane lattice parameter component not only yields large deviations from the true local alloy content but also carries the risk of identifying false ordering phenomena like formations of chains or platelets. Our method is demonstrated on image simulations of relaxed supercells, as well as on experimental images of an In{sub 0.20}Ga{sub 0.80}N quantum well. Principally, our approach is applicable to all epitaxially strained compounds in the form of quantum wells, free standing islands, quantum dots, or wires.

Schulz, T.; Remmele, T.; Korytov, M.; Markurt, T.; Albrecht, M. [Leibniz-Institut für Kristallzüchtung, Max-Born-Straße 2, 12489 Berlin (Germany); Duff, A.; Lymperakis, L.; Neugebauer, J. [Max-Planck-Institut für Eisenforschung, Max-Planck-Straße 1, 40237 Düsseldorf (Germany); Chèze, C. [TopGaN Sp. z o.o., Sokolowska 29/37, 01-142 Warsaw (Poland); Skierbiszewski, C. [TopGaN Sp. z o.o., Sokolowska 29/37, 01-142 Warsaw (Poland); Institute of High Pressure Physics, Polish Academy of Sciences, Sokolowska 29/37, 01-142 Warsaw (Poland)

2014-01-21T23:59:59.000Z

44

Atomic-resolution study of polarity reversal in GaSb grown on Si by scanning transmission electron microscopy  

SciTech Connect

The atomic-resolved reversal of the polarity across an antiphase boundary (APB) was observed in GaSb films grown on Si by high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). The investigation of the interface structure at the origin of the APB reveals that coalescence of two domains with Ga-prelayer and Sb-prelayer causes the sublattice reversal. The local strain and lattice rotation distributions of the APB, attributed to the discordant bonding length at the APB with the surrounding GaSb lattice, were further studied using the geometric phase analysis technique. The crystallographic characteristics of the APBs and their interaction with other planar defects were observed with HAADF-STEM. The quantitative agreement between experimental and simulated images confirms the observed polarities in the acquired HAADF-STEM data. The self-annihilation mechanism of the APBs is addressed based on the rotation induced by anti-site bonds and APBs' faceting.

Hosseini Vajargah, S.; Woo, S. Y.; Botton, G. A. [Department of Materials Science and Engineering, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Brockhouse Institute for Material Research, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Canadian Centre for Electron Microscopy, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Ghanad-Tavakoli, S. [Centre for Emerging Device Technologies, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Kleiman, R. N.; Preston, J. S. [Brockhouse Institute for Material Research, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Centre for Emerging Device Technologies, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Department of Engineering Physics, McMaster University, Hamilton, Ontario L8S 4L7 (Canada)

2012-11-01T23:59:59.000Z

45

Iran Thomas Auditorium, 8600 Environmental Transmission Electron...  

NLE Websites -- All DOE Office Websites (Extended Search)

April 26, 2012 11:00 am Iran Thomas Auditorium, 8600 Environmental Transmission Electron Microscopy for Catalysis Research: The Example of Carbon Nanotubes Eric A. Stach Center for...

46

High-energy-resolution monochromator for aberration-corrected scanning transmission electron microscopy/electron energy-loss spectroscopy  

Science Journals Connector (OSTI)

...equal to the beam current per unit area per unit solid angle per unit energy interval, CFE electron sources with their...Monochromated, spatially resolved electron energy-loss spectroscopic measurements of gold nanoparticles in the plasmon range...

2009-01-01T23:59:59.000Z

47

Transmission electron microscopy study of the effect of selenium doping on the ordering of GalnP2  

Science Journals Connector (OSTI)

Selenium doped Ga0.51In0.49P films have been grown by metalorganic chemical vapour deposition at 600, 670 and 740° C. The extent of ordering of the Group III sublattice has been monitored by transmission electron...

J. P. Goral; Sarah R. Kurtz; J. M. Olson; A. Kibbler

48

Transmission electron microscopy and Monte Carlo simulations of ordering in Au-Cu clusters produced in a laser vaporization source  

Science Journals Connector (OSTI)

Au-Cu bimetallic alloy clusters are produced in a laser vaporization source starting from Au-Cu alloy targets with different stoichiometric compositions. The clusters are deposited on two different substrates—amorphous carbon and crystalline MgO—and are characterized by electron diffraction and high-resolution electron microscopy. The experiments show that the overall chemical composition in the clusters is the same as the chemical composition of the target material; but the crystal structure of the Au-Cu alloy clusters differs from their known bulk crystal structure. Electron microscopy experiments provide evidence that no chemical ordering exists between Au and Cu atoms and that the clusters are solid solutions. Monte Carlo simulations using the second moment tight-binding approximation, however, predict Cu3Au clusters ordered in the core but with a disordered mantle. The possible origins of the differences between experiment and Monte Carlo simulations are discussed.

B. Pauwels; G. Van Tendeloo; E. Zhurkin; M. Hou; G. Verschoren; L. Theil Kuhn; W. Bouwen; P. Lievens

2001-03-27T23:59:59.000Z

49

Dynamic imaging with electron microscopy  

ScienceCinema (OSTI)

Livermore researchers have perfected an electron microscope to study fast-evolving material processes and chemical reactions. By applying engineering, microscopy, and laser expertise to the decades-old technology of electron microscopy, the dynamic transmission electron microscope (DTEM) team has developed a technique that can capture images of phenomena that are both very small and very fast. DTEM uses a precisely timed laser pulse to achieve a short but intense electron beam for imaging. When synchronized with a dynamic event in the microscope's field of view, DTEM allows scientists to record and measure material changes in action. A new movie-mode capability, which earned a 2013 R&D 100 Award from R&D Magazine, uses up to nine laser pulses to sequentially capture fast, irreversible, even one-of-a-kind material changes at the nanometer scale. DTEM projects are advancing basic and applied materials research, including such areas as nanostructure growth, phase transformations, and chemical reactions.

Campbell, Geoffrey; McKeown, Joe; Santala, Melissa

2014-05-30T23:59:59.000Z

50

Dynamic imaging with electron microscopy  

SciTech Connect

Livermore researchers have perfected an electron microscope to study fast-evolving material processes and chemical reactions. By applying engineering, microscopy, and laser expertise to the decades-old technology of electron microscopy, the dynamic transmission electron microscope (DTEM) team has developed a technique that can capture images of phenomena that are both very small and very fast. DTEM uses a precisely timed laser pulse to achieve a short but intense electron beam for imaging. When synchronized with a dynamic event in the microscope's field of view, DTEM allows scientists to record and measure material changes in action. A new movie-mode capability, which earned a 2013 R&D 100 Award from R&D Magazine, uses up to nine laser pulses to sequentially capture fast, irreversible, even one-of-a-kind material changes at the nanometer scale. DTEM projects are advancing basic and applied materials research, including such areas as nanostructure growth, phase transformations, and chemical reactions.

Campbell, Geoffrey; McKeown, Joe; Santala, Melissa

2014-02-20T23:59:59.000Z

51

Comparison between direct methods for determination of microbial cell volume: electron microscopy and electronic particle sizing.  

Science Journals Connector (OSTI)

...than those processed for electronic particle sizing, reflecting...Electron Microscopy and Electronic Particle Sizing E. MONTESINOS...ofMicrobiology and Institute for Fundamental Biology, Autonomous University...transmission electron microscopy and electronic particle sizing. Statistically...

E Montesinos; I Esteve; R Guerrero

1983-05-01T23:59:59.000Z

52

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Acknowledgment Acknowledgment EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Acknowledgment Please acknowledge your use of the EMC in your publications and presentations with the following acknowledgment statement: The electron microscopy was accomplished at the Electron Microscopy Center at Argonne National Laboratory, a U.S. Department of Energy Office of Science Laboratory operated under Contract No. DE-AC02-06CH11357 by UChicago Argonne, LLC.

53

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

SAMM SAMM EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Sub-Ã…ngstrom Microscopy and Microanalysis Facility In order to meet the scientific challenges of the future, the EMC has built a new state-of-the-art laboratory space for advanced electron microscopy. The new building has been designed to provide next- generation science with an operating environment that cannot be attained by renovating existing facilities. The EMC staff learned as much as possible from similar efforts around the world, including the SuperSTEM building at Daresbury, the Triebenberg Special Laboratory, the AML at Oak Ridge National Laboratory, the new NIST building, and various facilities for nanoscience.

54

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites

Laboratory Laboratory Electron Microscopy Center Argonne Home > EMC > EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers An Office of Science User Facility The Electron Microscopy Center (EMC) at Argonne National Laboratory develops and maintains unique capabilities for electron beam characterization and applies those capabilities to solve materials problems. The EMC staff carry out research with collaborators and users from Argonne, universities, and other laboratories. The expertise and facilities of the EMC additionally serve a group of national and international researchers. The EMC emphasizes three major areas: materials research, technique and instrumentation development, and operation as a national research facility. Research by EMC personnel includes microscopy based studies in high Tc superconducting materials, irradiation effects in metals and semiconductors, phase transformations, and processing related structure and chemistry of interfaces in thin films.

55

In situ transmission electron microscopy investigation of the interfacial reaction between Ni and Al during rapid heating in a nanocalorimeter  

SciTech Connect

The Al/Ni formation reaction is highly exothermic and of both scientific and technological significance. In this report, we study the evolution of intermetallic phases in this reaction at a heating rate of 830 K/s. 100-nm-thick Al/Ni bilayers were deposited onto nanocalorimeter sensors that enable the measurement of temperature and heat flow during rapid heating. Time-resolved transmission electron diffraction patterns captured simultaneously with thermal measurements allow us to identify the intermetallic phases present and reconstruct the phase transformation sequence as a function of time and temperature. The results show a mostly unaltered phase transformation sequence compared to lower heating rates.

Grapes, Michael D., E-mail: mgrapes1@jhu.edu, E-mail: david.lavan@nist.gov, E-mail: weihs@jhu.edu [Department of Materials Science and Engineering, Johns Hopkins University, Baltimore, Maryland 21218 (United States); Material Measurement Laboratory, Materials Measurement Science Division, National Institute of Standards and Technology, Gaithersburg, Maryland 20899 (United States); LaGrange, Thomas; Reed, Bryan W.; Campbell, Geoffrey H. [Lawrence Livermore National Laboratory, Materials Science and Technology Division, Livermore, California 94550 (United States); Woll, Karsten [Department of Materials Science and Engineering, Johns Hopkins University, Baltimore, Maryland 21218 (United States); Institute of Applied Materials, Karlsruhe Institute of Technology, 76344 Eggenstein-Leopoldshafen (Germany); LaVan, David A., E-mail: mgrapes1@jhu.edu, E-mail: david.lavan@nist.gov, E-mail: weihs@jhu.edu [Material Measurement Laboratory, Materials Measurement Science Division, National Institute of Standards and Technology, Gaithersburg, Maryland 20899 (United States); Weihs, Timothy P., E-mail: mgrapes1@jhu.edu, E-mail: david.lavan@nist.gov, E-mail: weihs@jhu.edu [Department of Materials Science and Engineering, Johns Hopkins University, Baltimore, Maryland 21218 (United States)

2014-11-01T23:59:59.000Z

56

Transmission electron microscopy assisted in-situ joule heat dissipation study of individual InAs nanowires  

SciTech Connect

Managing heat transport at nanoscale is an important and challenging task for nanodevice applications and nanostructure engineering. Herein, through in-situ engineering nanowire (NW)-electrode contacts with electron beam induced carbon deposition in a transmission electron microscope, Joule heat dissipation along individual suspended Indium Arsenide NWs is well managed to obtain pre-designed temperature profiles along NWs. The temperature profiles are experimentally determined by the breakdown site of NWs under Joule heating and breakdown temperature measurement. A model with NW-electrode contacts being well considered is proposed to describe heat transport along a NW. By fitting temperature profiles with the model, thermal conductance at NW-electrode contacts is obtained. It is found that, the temperature profile along a specific NW is mainly governed by the relative thermal conductance at the two NW-electrode contacts, which is engineered in experiments.

Xu, T. T.; Wei, X. L., E-mail: weixl@pku.edu.cn, E-mail: qingchen@pku.edu.cn; Shu, J. P.; Chen, Q., E-mail: weixl@pku.edu.cn, E-mail: qingchen@pku.edu.cn [Key Laboratory for the Physics and Chemistry of Nanodevices and Department of Electronics, Peking University, Beijing 100871 (China)

2013-11-04T23:59:59.000Z

57

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

An Office of Science User Facility An Office of Science User Facility The Electron Microscopy Center (EMC) at Argonne National Laboratory develops and maintains unique capabilities for electron beam characterization and applies those capabilities to solve materials problems. The EMC staff carry out research with collaborators and users from Argonne, universities, and other laboratories. The expertise and facilities of the EMC additionally serve a group of national and international researchers. The EMC emphasizes three major areas: materials research, technique and instrumentation development, and operation as a national research facility. Research by EMC personnel includes microscopy based studies in high Tc superconducting materials, irradiation effects in metals and semiconductors, phase transformations, and processing related structure and chemistry of interfaces in thin films.

58

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Training Training EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers User Training Prior Training in Electron Microscopy: People who wish to operate TEMs must have at least one college-level course in TEM with a lab component or previous TEM experience. The college course can't be one in which TEM was just one of many topics. For researchers who lack academic training and/or practical experience in electron microscopy, we suggest the short courses in TEM at the Hooke College of Applied Sciences, and the hands-on TEM courses at Northwestern University or the University of Chicago or Northern Illinois University.

59

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Overview Overview The mission of the Electron Microscopy Center (EMC) is to: Conduct materials research using advanced microstructural characterization methods; Maintain unique resources and facilities for scientific research for the both the Argonne National Laboratory and national scientific community. Develop and expand the frontiers of microanalysis by fostering the evolution of synergistic state-of-the-art resources in instrumentation, techniques and scientific expertise; The staff members of the EMC carry out their own research as well as participate in collaborative programs with other scientists at Argonne National Laboratory as well as researchers, educators and students worldwide. The Electron Microscopy Center (EMC) at Argonne National Laboratory develops and maintains unique capabilities for electron beam characterization and applies those capabilities to solve materials problems. The EMC staff perform collaborative research with members of other Divisions at Argonne National Laboratory and with collaborators from universities and other laboratories. The expertise and facilities of the EMC additionally serve a group of national and international researchers. The EMC emphasizes three major areas: materials research, technique and instrumentation development, and operation as a national research facility. Research by EMC personnel includes microscopy based studies in high Tc superconducting materials, irradiation effects in metals and semiconductors, phase transformations, and processing related structure and chemistry of interfaces in thin films.

60

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

iTEAM iTEAM The in situ Transmission Electron Aberration Corrected Microscope (iTEAM) is a proposed project to develop a microscope with powerful capabilities for in situ studies of materials in their native environment. iTEAM will build on the success of the TEAM project by utilizing both spherical and chromatic aberration correction in an electron microscope to provide unprecedented capabilities to study materials in controlled environments of temperature, pressure, or fluidic states with the high-resolution in imaging, diffraction, and spectroscopy typical of electron probes. The capabilities of iTEAM will lead to new ways to understand the behavior of materials in native environments, with particular relevance to major energy initiatives such as catalysis, solar conversion, fuel cells, and batteries. In addition, iTEAM will provide new capabilities to understand organic/inorganic interfaces, functionalized nanoparticles, and biomaterials under natural conditions.

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

Application of focused ion beam techniques and transmission electron microscopy to thin-film transistor failure analysis  

Science Journals Connector (OSTI)

......microscopy, failure analysis, nanometer-scale, pinpoint analysis...device performance, reliability and manufacturing...part of failure analysis. In view of the...vapour deposition reactor. The source/drain......

Satoshi Tsuji; Katsuhiro Tsujimoto; Kotaro Kuroda; Hiroyasu Saka

2004-10-01T23:59:59.000Z

62

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Submit an EMC Proposal Submit an EMC Proposal EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Submit an EMC Proposal EMC Proposal Submission Deadline Dates for FY2014: November 1, 2013 March 7, 2014 July 11, 2014 Is your proposal a multi-facility proposal? In other words, do you intend to submit proposals to EMC and APS or CNM for your research project? If your answer is "yes," go now to the Proposal Gateway.

63

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

EMC Users Committee EMC Users Committee EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers EMC Users Committee An EMC Users Committee has been organized to enhance communication between the user community and the EMC. While the EMC relies on and encourages strong interaction among its users and between its staff and users, the Users Committee provides an additional formal mechanism for user input into EMC planning and operations to ensure that users' needs and concerns are addressed.

64

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

End-of-Proposal Report End-of-Proposal Report EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers End-of-Proposal Report In accordance with the User Agreement, please provide the EMC with the following information when your proposal expires (one year after its acceptance date or when the experiments end, whichever is sooner). A research summary/progress report using these two templates:

65

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Becoming a User Becoming a User EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÃ…MM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Procedure to Become a User at the EMC 1. Summary All users have to fulfill certain requirements before access to the EMC can be granted. The following list provides short descriptions of the requirements. Details can be found on this page and via the relevant links at the left. Register for access to Argonne's scientific user facilities (or update your user registration information).

66

A transmission electron microscopy study of the deformation behavior underneath nanoindents in nano-scale Al-TiN multilayered composites  

SciTech Connect

Nano-scale multilayered Al-TiN composites were deposited with DC magnetron sputtering technique in two different layer thickness ratios - Al:TiN = 1:1 and Al:TiN = 9:1. The Al layer thickness varied from 2 nm to 450 nm. The hardness of the samples was tested by nanoindentation using a Berkovich tip. Cross-sectional Transmission Electron Microscopy (TEM) was carried out on samples extracted with Focused Ion Beam (FIB) from below the nanoindents. This paper presents the results of the hardness tests in the Al-TiN multilayers with the two different thickness ratios and the observations from the cross-sectional TEM studies of the regions underneath the indents. These studies showed remarkable strength in the multilayers, as well as some very interesting deformation behavior in the TiN layers at extremely small length scales, where the hard TiN layers undergo co-deformation with the Al layers.

Bhattacharyya, Dhriti [Los Alamos National Laboratory; Mara, Nathan A [Los Alamos National Laboratory; Dickerson, Patricia O [Los Alamos National Laboratory; Misra, Amit [Los Alamos National Laboratory; Hoagland, R G [Los Alamos National Laboratory

2009-01-01T23:59:59.000Z

67

Investigation of aged organic solar cell stacks by cross-sectional transmission electron microscopy coupled with elemental analysis  

Science Journals Connector (OSTI)

Polymer solar cells are of great interest as candidates for...61...-butyric acid methyl ester (P3HT and PCBM, respectively). Phase segregation of the blend has been extensively investigated by transmission electr...

P. Favia; E. Voroshazi; P. Heremans; H. Bender

2013-04-01T23:59:59.000Z

68

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

General Information for EMC Users General Information for EMC Users The Electron Microscopy Center (EMC) is an Office of Science User Facility operated for the U.S. Department of Energy Office of Science by Argonne National Laboratory. It is one of three scientific user facilities for electron beam microcharacterization and one of several National User Facilities located at Argonne National Laboratory. As a scientific user facility, the EMC supports user-accessible instruments (Resources) for high spatial resolution microanalysis, field imaging, nanoscale structural characterization, nanoscale fabrication and manipulation, and unique in situ studies of materials under the influence of ion-beam irradiation. These capabilities are used in a diverse variety of research areas to address grand challenge scientific questions encompassing, for example, energy-related studies, biology, astrophysics, archaeology, superconductivity, nanotechnology, environmental engineering, tribology, and ferroelectricity. The research is performed both by users and by EMC staff. While many users work independently, the most challenging research activities require extensive contributions from EMC staff.

69

STRUCTURAL AND CHEMICAL STUDIES ON CdTe/CdS THIN FILM SOLAR CELLS WITH ANALYTICAL TRANSMISSION ELECTRON MICROSCOPY  

E-Print Network (OSTI)

STRUCTURAL AND CHEMICAL STUDIES ON CdTe/CdS THIN FILM SOLAR CELLS WITH ANALYTICAL TRANSMISSION, A. N. Tiwari Thin Film Physics Group, Laboratory for Solid State Physics, Technopark ETH-Building, Technoparkstr. 1, CH-8005 Zurich, Switzerland ABSTRACT: CdTe/CdS thin £lm solar cells have been grown by closed

Romeo, Alessandro

70

Spin torque and heating effects in current-induced domain wall motion probed by transmission electron microscopy  

E-Print Network (OSTI)

Spin torque and heating effects in current-induced domain wall motion probed by transmission- ternative to the use of conventional external magnetic fields, therefore opening up a route for simple device fabrication, where no field-generating strip lines are necessary. While current-induced domain

Dunin-Borkowski, Rafal E.

71

Structural defects in epitaxial graphene layers synthesized on C-terminated 4H-SiC (0001{sup ¯}) surface—Transmission electron microscopy and density functional theory studies  

SciTech Connect

The principal structural defects in graphene multilayers synthesized on the carbon-terminated face of a 4H-SiC (0001{sup ¯}) substrate were investigated using the high-resolution transmission electron microscopy. The analyzed systems include a wide variety of defected structures such as edge dislocations, rotational multilayers, and grain boundaries. It was shown that graphene layers are composed of grains of the size of several nanometres or larger; they differ in a relative rotation by large angles, close to 30°. The structure of graphene multilayers results from the synthesis on a SiC (0001{sup ¯}) surface, which proceeds via intensive nucleation of new graphene layers that coalesce under various angles creating an immense orientational disorder. Structural defects are associated with a built-in strain resulting from a lattice mismatch between the SiC substrate and the graphene layers. The density functional theory data show that the high-angular disorder of AB stacked bi-layers is not restoring the hexagonal symmetry of the lattice.

Borysiuk, J., E-mail: jolanta.borysiuk@ifpan.edu.pl [Institute of Physics, Polish Academy of Sciences, Al. Lotników 32/46, 02-668 Warsaw (Poland); Faculty of Physics, University of Warsaw, Ho?a 69, 00-681 Warsaw (Poland); So?tys, J.; Piechota, J. [Interdisciplinary Centre for Mathematical and Computational Modelling, University of Warsaw, Pawi?skiego 5a, 02-106 Warsaw (Poland); Krukowski, S. [Interdisciplinary Centre for Mathematical and Computational Modelling, University of Warsaw, Pawi?skiego 5a, 02-106 Warsaw (Poland); Institute of High Pressure Physics, Polish Academy of Sciences, Soko?owska 29/37, 01-142 Warsaw (Poland); Baranowski, J. M. [Faculty of Physics, University of Warsaw, Ho?a 69, 00-681 Warsaw (Poland); Institute of Electronic Materials Technology, Wólczy?ska 133, 01-919 Warsaw (Poland); St?pniewski, R. [Faculty of Physics, University of Warsaw, Ho?a 69, 00-681 Warsaw (Poland)

2014-02-07T23:59:59.000Z

72

Transmission Electron Microscope and Scanning Electron Microscopes -  

NLE Websites -- All DOE Office Websites (Extended Search)

Facilities > Transmission Electron Facilities > Transmission Electron Microscope and Scanning Electron Microscopes FACILITIES Transmission Electron Microscope and Scanning Electron Microscopes Overview Other Facilities Work with Argonne Contact us For Employees Site Map Help Join us on Facebook Follow us on Twitter NE on Flickr Transmission Electron Microscope and Scanning Electron Microscopes The research activities of the Corrosion and Mechanics of Materials Section are supported by complete metallography/sample preparation rooms equipped with several optical and electron microscopes: a Transmission Electron Microscope and two Scanning Electron Microscopes. Bookmark and Share Transmission electron microscope (TEM) Detail of JEOL 100CXII TEM Figure 1: Detail of JEOL 100CXII TEM. Click on image to view larger image.

73

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

CM30T TEM CM30T TEM Instrument capabilities: Instrument specifications: Accelerating voltages: 100-300 kV LaB6 emitter Resolution (at 300 kV): ~ 0.25 nm point; ~ 0.14 nm line Minimum probe size: ~ 9 nm Operating modes: CTEM, CBED, SAED, light element XEDS CCD camera: 1 Mp, 14 bits, AVI capture possible at 15 fps Specimen holders: Double Tilt (+/- 60 degrees alpha, +/- 30 degrees beta): with Be cup for XEDS liquid nitrogen cooled (96 K) with Be cup heating (1270 K) Tilt/rotate (+/- 60 degrees alpha, rotation 360 degrees) Single Tilt (+/- 60 degrees alpha) Typical experiments (examples): Quantitative XEDS Morphological and diffraction contrast studies of defects In situ heating & cooling studies Electron crystallography Weak beam studies of defects This page can be downloaded here as an Adobe PDF file.

74

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

FEI Tecnai F20ST TEM/STEM FEI Tecnai F20ST TEM/STEM Instrument capabilities: Instrument specifications: Accelerating voltages: 80-200 kV Schottky FEG emitter Resolution (at 200 kV): ~0.24 nm point; ~0.1 nm line; probe size ~0.2-1 nm Operating modes: CTEM, STEM (BF/ADF, HAADF), CBED, SAED, light element XEDS, EELS, spectrum imaging, energy-filtered imaging (EFI), Lorentz magnetic imaging (LMI), electron holographic imaging (EHI), other computationally-mediated modes. On-axis CCD camera: 16 Mp, 16 bits, 61x61 mm chip size. EMC-owned specimen holders: Double Tilt (+/- 40 degrees alpha, +/- 30 degrees beta): with Be cup for XEDS liquid nitrogen cooled (96 K) with Be cup heating (1270 K) In-plane magnetic field (tilt +/- 40 degrees alpha) Liquid He cooled (tilt +/- 40 degrees alpha, rotate 360 degrees)

75

Los Alamos: MST-MTM: EML: Electron Microscopy Laboratory  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron Microscopy Laboratory, MST-6 Electron Microscopy Laboratory, MST-6 MST-6 Home Home In the MSL FEI Tecnai F30 Analytical TEM/STEM JEOL 6300FXV High Resolution SEM JEOL 3000F High Resolution Transmission Electron Microscope Philips XL30 F Scanning Electron Microscope & Orientation Imaging System Phillips CM30 Transmission Electron Microscope In the Sigma Building JEOL 840 EPMA with Wavelength Dispersive Spectroscopy FEI Strata DB235 FIB/SEM FEI XL30 Environmental Scanning Electron Microscope & Orientation Imaging System CONTACTS Bob Field 665.3938 Pat Dickerson 665.3036 Rob Dickerson 667.6337 Rod McCabe 606.1649 The Electron Microscopy Laboratory's Capabilities The Electron Microscopy Laboratory's Capabilities The Electron Microscopy Laboratory (EML) is part of MST-6, the Materials Technology - Metallurgy Group within the Materials Science and Technology Division at Los Alamos National Laboratory. It is a facility dedicated to the characterization of materials primarily through imaging, chemical, and crystallographic analyses of material microstructures with several electron and ion beam instruments. Accessory characterization techniques and equipment include energy dispersive x-ray analysis (EDS), wavelength dispersive x-ray analysis (WDS), electron backscatter diffraction (EBSD) and orientation imaging microscopy (OIM), and electron energy loss spectroscopy (EELS).

76

Microscopy. II. Electron Microscopy: A Review  

Science Journals Connector (OSTI)

...the best image under the lower resolving power of optical microscopes. For example...Experimental Infection with the Virus of Foot and Mouth Disease. J. Exper. Med...Further Improvements in the Resolving Power of the Electron Microscope. J. Appi...

Cecily Cannan Selby

1953-11-01T23:59:59.000Z

77

Direct electron detection in transmission electron microscopy  

E-Print Network (OSTI)

Duttweiler, J. Bouwer, S. Peltier, M. Ellisman, P. Denes, F.J. C. Bouwer, S. T. Peltier, M. Ellisman and N. -H. Xuong (J. C. Bouwer, S. T. Peltier, M. H. Ellisman and N. H.

Jin, Liang

2009-01-01T23:59:59.000Z

78

Direct electron detection in transmission electron microscopy  

E-Print Network (OSTI)

a three-stage thermoelectric cooling module was coupled withbetween the thermoelectric cooling module and the backside

Jin, Liang

2009-01-01T23:59:59.000Z

79

Defect microstructural evolution in ion irradiated metallic nanofoils: Kinetic Monte Carlo simulation versus cluster dynamics modeling and in situ transmission electron microscopy experiments  

SciTech Connect

Understanding materials degradation under intense irradiation is important for the development of next generation nuclear power plants. Here we demonstrate that defect microstructural evolution in molybdenum nanofoils in situ irradiated and observed on a transmission electron microscope can be reproduced with high fidelity using an object kinetic Monte Carlo (OKMC) simulation technique. Main characteristics of defect evolution predicted by OKMC, namely, defect density and size distribution as functions of foil thickness, ion fluence and flux, are in excellent agreement with those obtained from the in situ experiments and from previous continuum-based cluster dynamics modeling. The combination of advanced in situ experiments and high performance computer simulation/modeling is a unique tool to validate physical assumptions/mechanisms regarding materials response to irradiation, and to achieve the predictive power for materials stability and safety in nuclear facilities.

Xu Donghua; Wirth, Brian D. [Department of Nuclear Engineering, University of Tennessee, Knoxville, Tennessee 37996 (United States); Li Meimei [Division of Nuclear Engineering, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Kirk, Marquis A. [Division of Materials Science, Argonne National Laboratory, Argonne, Illinois 60439 (United States)

2012-09-03T23:59:59.000Z

80

Faculty Position in Materials Electron Microscopy  

E-Print Network (OSTI)

Faculty Position in Materials Electron Microscopy at the Ecole Polytechnique Fédérale de Lausanne in electron microscopy of materials within its Institute of Materials. We seek exceptional individuals who community. Top-level applications are invited from candidates at the cutting edge of electron microscopic

Candea, George

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


81

Strain relief and AlSb buffer layer morphology in GaSb heteroepitaxial films grown on Si as revealed by high-angle annular dark-field scanning transmission electron microscopy  

SciTech Connect

The interfacial misfit (IMF) dislocation array of an epitaxial GaSb film on a Si substrate has been imaged with high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). The mismatch strain accommodation through dislocation formation has been investigated using geometric phase analysis (GPA) on HAADF-STEM images with atomic resolution to probe the defects' local strain distribution. These measurements indicate that the lattice parameter of the epitaxial film recovers its bulk value within three unit cells from the interface due to the relaxation through IMF dislocations. The atomic number contrast of the HAADF-STEM images and energy dispersive x-ray spectrometry illustrate the formation of islands of AlSb buffer layer along the interface. The role of the AlSb buffer layer in facilitating the GaSb film growth on Si is further elucidated by investigating the strain field of the islands with the GPA.

Vajargah, S. Hosseini; Couillard, M.; Cui, K. [Department of Material Science and Engineering, McMaster University, 1280 Main St. W., Hamilton, Ontario L8S 4M1 (Canada); Tavakoli, S. Ghanad; Robinson, B.; Kleiman, R. N.; Preston, J. S. [Department of Engineering Physics, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Botton, G. A. [Department of Material Science and Engineering, McMaster University, 1280 Main St. W., Hamilton, Ontario L8S 4M1 (Canada); Canadian Centre for Electron Microscopy, McMaster University, Hamilton, Ontario L8S 4M1 (Canada)

2011-02-21T23:59:59.000Z

82

NCEM National Center for Electron Microscopy: Becoming an NCEM User  

NLE Websites -- All DOE Office Websites (Extended Search)

New Research New Research Gallery Microscopy Links Becoming an NCEM User Step 1: Submit a proposal Step 2: Before you begin your research Step 3: Instrument qualification Step 4: Accessing NCEM facilities and performing research Step 1: Submit a proposal Deadlines for new proposals are March 15, June 15, September 15, December 15. Access to NCEM facilities is granted to researchers whose proposals are accepted by the NCEM proposal review committee. NCEM users are expected to have a strong background in transmission electron microscopy, and submitted proposals should include evidence of prior electron microscopy experience by the intended operator. Researchers who do not have sufficient experience in electron microscopy may be able to use NCEM facilities through a collaborative project.

83

Fast electron microscopy via compressive sensing  

DOE Patents (OSTI)

Various technologies described herein pertain to compressive sensing electron microscopy. A compressive sensing electron microscope includes a multi-beam generator and a detector. The multi-beam generator emits a sequence of electron patterns over time. Each of the electron patterns can include a plurality of electron beams, where the plurality of electron beams is configured to impart a spatially varying electron density on a sample. Further, the spatially varying electron density varies between each of the electron patterns in the sequence. Moreover, the detector collects signals respectively corresponding to interactions between the sample and each of the electron patterns in the sequence.

Larson, Kurt W; Anderson, Hyrum S; Wheeler, Jason W

2014-12-09T23:59:59.000Z

84

Study of Interactions Between Microbes and Minerals by Scanning Transmission X-Ray Microscopy (STXM)  

SciTech Connect

Scanning Transmission X-ray Microscopy (STXM) and Transmission Electron Microscopy (TEM) were combined to characterize various samples of geomicrobiological interest down to the nanometer scale. An approach based on energy-filtered imaging was used to examine microbe-mineral interactions and the resulting biominerals, as well as biosignatures in simplified laboratory samples. This approach was then applied to natural samples, including natural biofilms entombed in calcium carbonate precipitates and bioweathered silicates and facilitated location of bacterial cells and provided unique insights about their biogeochemical interactions with minerals at the 30-40 nm scale.

Benzerara, K.; /Paris U., VI-VII, LMCP; Tyliszczak, T.; /LBNL, ALS; Brown, G.E., Jr.; /Stanford U., Geo. Environ. Sci. /SLAC, SSRL

2007-01-03T23:59:59.000Z

85

Ultra-High Resolution Electron Microscopy for Catalyst Characterizatio...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Ultra-High Resolution Electron Microscopy for Catalyst Characterization Ultra-High Resolution Electron Microscopy for Catalyst Characterization 2011 DOE Hydrogen and Fuel Cells...

86

Ultra-high Resolution Electron Microscopy for Catalyst Characterizatio...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

high Resolution Electron Microscopy for Catalyst Characterization Ultra-high Resolution Electron Microscopy for Catalyst Characterization 2009 DOE Hydrogen Program and Vehicle...

87

Ultra-High Resolution Electron Microscopy for Catalyst Characterizatio...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

High Resolution Electron Microscopy for Catalyst Characterization Ultra-High Resolution Electron Microscopy for Catalyst Characterization 2010 DOE Vehicle Technologies and Hydrogen...

88

Instrument Series: Microscopy Aberration-Corrected Scanning/Transmission  

NLE Websites -- All DOE Office Websites (Extended Search)

Aberration-Corrected Aberration-Corrected Scanning/Transmission Electron Microscope EMSL's aberration-corrected Titan 80-300(tm) scanning/transmission electron microscope (S/TEM) provides high-resolution imaging with sub-angstrom resolution and spectroscopic capabilities. This state-of-the-art instrument is equipped with a Schottky field-emission electron source, an electron gun monochromator, CEOS hexapole spherical aberration corrector for the probe-forming lens, high-angle annular dark field (HAADF) detector, an X-ray spectrometer (EDS), and a high-resolution Gatan Imaging Filter (GIF). The selection of electron energy between 80 kV and 300 kV enables optimized imaging for a variety of samples, including electron beam sensitive materials. Research Applications

89

Atomic Force and Scanning Electron Microscopy of Atmospheric Particles  

E-Print Network (OSTI)

conducted so as to characterize atmospheric aerosols from anthropogenic (pollution) and natural (sea saltAtomic Force and Scanning Electron Microscopy of Atmospheric Particles ZAHAVA BARKAY,1 * AMIT 69978, Israel KEY WORDS atmospheric aerosols; atomic force microscopy; scanning electron microscopy

Shapira, Yoram

90

High-resolution scanning transmission electron microscopy  

Science Journals Connector (OSTI)

...where, is the brightness of the source and bs/80 is the ratio of the real image of the...im-age (0.61A/a). The quantity bs/80 can be most easily defined in the source...tube can be ac-quired at a reasonable cost and is com-patible with full-color displays...

AV Crewe

1983-07-22T23:59:59.000Z

91

In situ environmental transmission electron microscopy study...  

NLE Websites -- All DOE Office Websites (Extended Search)

aqueous electrolytes. 16 Based on previous studies of the oxida- tion behavior of bulk TiC 17-19 in various temperature ranges, and under various oxygen partial pressures, it is...

92

Tomography and High-Resolution Electron Microscopy Study of Surfaces...  

NLE Websites -- All DOE Office Websites (Extended Search)

Tomography and High-Resolution Electron Microscopy Study of Surfaces and Porosity in a Plate-Like ?-Al2O3. Tomography and High-Resolution Electron Microscopy Study of...

93

NCEM National Center for Electron Microscopy: Staff  

NLE Websites -- All DOE Office Websites (Extended Search)

Staff Staff Scientific Technical / Admin. Postdoctoral and Visitors Uli Dahmen, Head Jane Cavlina / Administrator Abhay Gautam Christian Kisielowski John Turner Helmut Poppa Andrew Minor ChengYu Song Frances Allen Andreas Schmid Marissa Libbee Tamara Radetic Peter Ercius Karen Bustillo Haimei Zheng Jim Ciston Alpha N'Diaye Colin Ophus Gong Chen Burak Ozdol Velimir Radmilovic Sara Kiani Hua Guo Christian Liebscher Josh Kacher Chris Nelson Xiuguang Jin Qian Yu Mary Scott Search the LBNL directory services page for other LBNL staff. Scientific Staff Uli Dahmen udahmen@lbl.gov (510) 486-4627 Ulrich Dahmen is Director of the National Center for Electron Microscopy. His current research interests include embedded nanostructures and interfaces in materials. Embedded nanostructures. Size- and shape-dependence of structural phase

94

TITLE: Environmental Electron Microscopy Study of the Nucleation and Growth of Si and Ge AUTHORS: Stephan Hofmann  

E-Print Network (OSTI)

transmission electron microscopy study of Si nanowire nucleation from Pd [1] and Ni under disilane exposure advances by lateral propagation of ledges, driven by catalytic dissociation of disilane and coupled Pd

Dunin-Borkowski, Rafal E.

95

In-Situ Electron Microscopy of Electrical Energy Storage Materials...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

of Electrical Energy Storage Materials In-Situ Electron Microscopy of Electrical Energy Storage Materials 2011 DOE Hydrogen and Fuel Cells Program, and Vehicle Technologies...

96

In-Situ Electron Microscopy of Electrical Energy Storage Materials...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

of Electrical Energy Storage Materials In-Situ Electron Microscopy of Electrical Energy Storage Materials 2012 DOE Hydrogen and Fuel Cells Program and Vehicle Technologies...

97

Ponderomotive phase plate for transmission electron microscopes  

DOE Patents (OSTI)

A ponderomotive phase plate system and method for controllably producing highly tunable phase contrast transfer functions in a transmission electron microscope (TEM) for high resolution and biological phase contrast imaging. The system and method includes a laser source and a beam transport system to produce a focused laser crossover as a phase plate, so that a ponderomotive potential of the focused laser crossover produces a scattering-angle-dependent phase shift in the electrons of the post-sample electron beam corresponding to a desired phase contrast transfer function.

Reed, Bryan W. (Livermore, CA)

2012-07-10T23:59:59.000Z

98

A transmission electron microscope for lecture demonstrations  

Science Journals Connector (OSTI)

A simple transmission electron microscope (TEM) suitable for lecture demonstrations is described. In this TEM electrons are created in a glow discharge between two parallel electrodes in air at a reduced pressure. The electrons are collimated by a small hole in the anode focused by a solenoid that acts as an electromagnetic lens and imaged on a thin layer of phosphor deposited inside an Erlenmeyer flask. An image of a biological sample placed between the source and the lens can be magnified about 20 times. The microscope uses inexpensive components that can be quickly assembled during a demonstration. The TEM provides a visual and memorable display that highlights phenomena such as mean-free-path charged particle optics electrical discharges and cathodoluminescence.

J. A. Panitz; Gertrude Rempfer

2006-01-01T23:59:59.000Z

99

In Situ Analytical Electron Microscopy for Probing Nanoscale Electrochemistry  

SciTech Connect

Oxides and their tailored structures are at the heart of electrochemical energy storage technologies and advances in understanding and controlling the dynamic behaviors in the complex oxides, particularly at the interfaces, during electrochemical processes will catalyze creative design concepts for new materials with enhanced and better-understood properties. Such knowledge is not accessible without new analytical tools. New innovative experimental techniques are needed for understanding the chemistry and structure of the bulk and interfaces, more importantly how they change with electrochemical processes in situ. Analytical Transmission Electron Microscopy (TEM) is used extensively to study electrode materials ex situ and is one of the most powerful tools to obtain structural, morphological, and compositional information at nanometer scale by combining imaging, diffraction and spectroscopy, e.g., EDS (energy dispersive X-ray spectrometry) and Electron Energy Loss Spectrometry (EELS). Determining the composition/structure evolution upon electrochemical cycling at the bulk and interfaces can be addressed by new electron microscopy technique with which one can observe, at the nanometer scale and in situ, the dynamic phenomena in the electrode materials. In electrochemical systems, for instance in a lithium ion battery (LIB), materials operate under conditions that are far from equilibrium, so that the materials studied ex situ may not capture the processes that occur in situ in a working battery. In situ electrochemical operation in the ultra-high vacuum column of a TEM has been pursued by two major strategies. In one strategy, a 'nano-battery' can be fabricated from an all-solid-state thin film battery using a focused ion beam (FIB). The electrolyte is either polymer based or ceramic based without any liquid component. As shown in Fig. 1a, the interfaces between the active electrode material/electrolyte can be clearly observed with TEM imaging, in contrast to the composite electrodes/electrolyte interfaces in conventional lithium ion batteries, depicted in Fig.1b, where quantitative interface characterization is extremely difficult if not impossible. A second strategy involves organic electrolyte, though this approach more closely resembles the actual operation conditions of a LIB, the extreme volatility In Situ Analytical Electron Microscopy for Probing Nanoscale Electrochemistry by Ying Shirley Meng, Thomas McGilvray, Ming-Che Yang, Danijel Gostovic, Feng Wang, Dongli Zeng, Yimei Zhu, and Jason Graetz of the organic electrolytes present significant challenges for designing an in situ cell that is suitable for the vacuum environment of the TEM. Significant progress has been made in the past few years on the development of in situ electron microscopy for probing nanoscale electrochemistry. In 2008, Brazier et al. reported the first cross-section observation of an all solid-state lithium ion nano-battery by TEM. In this study the FIB was used to make a 'nano-battery,' from an all solid-state battery prepared by pulsed laser deposition (PLD). In situ TEM observations were not possible at that time due to several key challenges such as the lack of a suitable biasing sample holder and vacuum transfer of sample. In 2010, Yamamoto et al. successfully observed changes of electric potential in an all-solid-state lithium ion battery in situ with electron holography (EH). The 2D potential distribution resulting from movement of lithium ions near the positive-electrode/electrolyte interface was quantified. More recently Huang et al. and Wang et al. reported the in situ observations of the electrochemical lithiation of a single SnO{sub 2} nanowire electrode in two different in situ setups. In their approach, a vacuum compatible ionic liquid is used as the electrolyte, eliminating the need for complicated membrane sealing to prevent the evaporation of carbonate based organic electrolyte into the TEM column. One main limitation of this approach is that EELS spectral imaging is not possible due to the high plasmon signal of the ionic li

Graetz J.; Meng, Y.S.; McGilvray, T.; Yang, M.-C.; Gostovic, D.; Wang, F.; Zeng, D.; Zhu, Y.

2011-10-31T23:59:59.000Z

100

Slow positron annihilation spectroscopy and electron microscopy of electron beam evaporated cobalt and nickel silicides  

SciTech Connect

Metal silicide thin films on single-crystal silicon substrates are the subject of much research, due to their applications as electrical contacts and interconnects, diffusion barriers, low resistance gates, and field-assisted positron moderators, among others. Defects within the silicide layer and/or at the silicide/silicon interface are detrimental to device performance, since they can act as traps for charge carriers, as well as positrons. Pinholes penetrating the film are another detriment particularly for cobalt silicide films, since they allow electrons to permeate the film, rather than travel ballistically, in addition to greatly increasing surface area for recombination events. A series of epitaxial cobalt and nickel silicide thin films, deposited via electron-beam evaporation and annealed at various temperatures, have been grown on single-crystal silicon (111) substrates, in an effort to establish a relationship between deposition and processing parameters and film quality. The films have been analyzed by transmission and scanning electron microscopy, sputter depth profile Auger, and slow positron annihilation spectroscopy. The latter has been shown to both correlate and complement the traditional electron microscopy results.

Frost, R.L.; DeWald, A.B. (Georgia Institute of Technology, Atlanta, Georgia 30332 (USA)); Zaluzec, M.; Rigsbee, J.M. (University of Illinois, Urbana, Illinois 61801 (USA)); Nielsen, B.; Lynn, K.G. (Brookhaven National Laboratory, Upton, New York 11973 (USA))

1990-07-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

Full-field Transmission X-ray Microscopy | Stanford Synchrotron Radiation  

NLE Websites -- All DOE Office Websites (Extended Search)

BL6-2c / Transmission X-ray Microscopy BL6-2c / Transmission X-ray Microscopy Home Researchers Publications Science Highlights Department of Energy Office of Science Search form Search Search TXM Search Full-field Transmission X-ray Microscopy Capabilities Full-field TXM is an excellent method to examine nanoscale heterogeneties in many materials, including complex hierarchical systems such as catalysts, fuel cells and battery electrodes, and biological and environmental samples, at 30 nm resolution.The transmission X-ray microscope (TXM) on beam line 6-2c at SSRL is capable of 2D imaging and tomography, as well as spectroscopic imaging for 2D and 3D elemental mapping and chemical mapping over tens of microns (up to mm in 2D). The field of view (FOV) is 30 microns, but mosaic images can be collected to

102

Nonlinear transmission line based electron beam driver  

SciTech Connect

Gated field emission cathodes can provide short electron pulses without the requirement of laser systems or cathode heating required by photoemission or thermionic cathodes. The large electric field requirement for field emission to take place can be achieved by using a high aspect ratio cathode with a large field enhancement factor which reduces the voltage requirement for emission. In this paper, a cathode gate driver based on the output pulse train from a nonlinear transmission line is experimentally demonstrated. The application of the pulse train to a tufted carbon fiber field emission cathode generates short electron pulses. The pulses are approximately 2 ns in duration with emission currents of several mA, and the train contains up to 6 pulses at a frequency of 100 MHz. Particle-in-cell simulation is used to predict the characteristic of the current pulse train generated from a single carbon fiber field emission cathode using the same technique.

French, David M.; Hoff, Brad W.; Tang Wilkin; Heidger, Susan; Shiffler, Don [Directed Energy Directorate, Air Force Research Laboratory, Kirtland AFB, New Mexico 87117 (United States); Allen-Flowers, Jordan [Program in Applied Mathematics, University of Arizona, Tucson, Arizona 85721 (United States)

2012-12-15T23:59:59.000Z

103

Ion-induced electron emission microscopy  

DOE Patents (OSTI)

An ion beam analysis system that creates multidimensional maps of the effects of high energy ions from an unfocussed source upon a sample by correlating the exact entry point of an ion into a sample by projection imaging of the secondary electrons emitted at that point with a signal from a detector that measures the interaction of that ion within the sample. The emitted secondary electrons are collected in a strong electric field perpendicular to the sample surface and (optionally) projected and refocused by the electron lenses found in a photon emission electron microscope, amplified by microchannel plates and then their exact position is sensed by a very sensitive X Y position detector. Position signals from this secondary electron detector are then correlated in time with nuclear, atomic or electrical effects, including the malfunction of digital circuits, detected within the sample that were caused by the individual ion that created these secondary electrons in the fit place.

Doyle, Barney L. (Albuquerque, NM); Vizkelethy, Gyorgy (Albuquerque, NM); Weller, Robert A. (Brentwood, TN)

2001-01-01T23:59:59.000Z

104

Los Alamos: MST-MTM: EML: Electron Microscopy Laboratory  

NLE Websites -- All DOE Office Websites (Extended Search)

3000F High Resolution Transmission Electron Microscope 3000F High Resolution Transmission Electron Microscope JEOL 3000F High Resolution Transmission Electron Microscope This is a high-resolution TEM equipped with an electron energy-loss spectrometer and a CCD camera for digital image acquisition. This microscope is used primarily for imaging the atomic structure of defects and interfaces in materials. Field emission electron source. Coherent source with an energy spread of 0.8 eV. Operation at accelerating voltages of up to 300 kV. +/- 10° of eucentric specimen tilt. Point to point resolution of 0.17 nm; 0.10 nm resolution can be extracted by computer processing. Gatan Multiscan CCD Camera for digital image acquisition. Automated microscope alignment: defocus calibration/adjustment, astigmatism correction and beam-tilt correction (automatic coma-free alignment).

105

Imaging Hydrated Microbial Extracellular Polymers: Comparative Analysis by Electron Microscopy  

SciTech Connect

Microbe-mineral and -metal interactions represent a major intersection between the biosphere and geosphere but require high-resolution imaging and analytical tools for investigating microscale associations. Electron microscopy has been used extensively for geomicrobial investigations and although used bona fide, the traditional methods of sample preparation do not preserve the native morphology of microbiological components, especially extracellular polymers. Herein, we present a direct comparative analysis of microbial interactions using conventional electron microscopy approaches of imaging at room temperature and a suite of cryo-electron microscopy methods providing imaging in the close-to-natural hydrated state. In situ, we observed an irreversible transformation of bacterial extracellular polymers during the traditional dehydration-based sample preparation that resulted in the collapse of hydrated gel-like EPS into filamentous structures. Dehydration-induced polymer collapse can lead to inaccurate spatial relationships and hence could subsequently affect conclusions regarding nature of interactions between microbial extracellular polymers and their environment.

Dohnalkova, Alice; Marshall, Matthew J.; Arey, Bruce W.; Williams, Kenneth H.; Buck, Edgar C.; Fredrickson, Jim K.

2011-02-01T23:59:59.000Z

106

NCEM National Center for Electron Microscopy: About NCEM  

NLE Websites -- All DOE Office Websites (Extended Search)

NCEM NCEM The National Center for Electron Microscopy (NCEM) is one of the world's foremost centers for electron microscopy and microcharacterization. It is an Office of Science User Facility operated for the U.S. Department of Energy by Lawrence Berkeley National Laboratory. Located adjacent to the University of California, Berkeley, NCEM was established in 1983 to maintain a forefront research center for electron-optical characterization of materials with state-of-the-art instrumentation and expertise. As a national user facility, NCEM is open to scientists from universities, government and industrial laboratories. The center provides cutting-edge instrumentation, techniques and expertise for advanced electron beam microcharacterization of materials at high spatial

107

X-ray Phase Imaging Microscopy using a Fresnel Zone Plate and a Transmission Grating  

SciTech Connect

We report on a hard X-ray phase imaging microscopy (a phase-difference microscopy) that consists of an objective and a transmission grating. The simple optical system provides a quantitative phase image, and does not need a wave field mostly coherent on the objective. Our method has a spatial resolution almost same as that of the absorption contrast microscope image obtained by removing the grating. We demonstrate how our approach provides a phase image from experimentally obtained images. Our approach is attractive for easily appending a quantitative phase-sensitive mode to normal X-ray microscopes, and has potentially broad applications in biology and material sciences.

Yashiro, Wataru; Momose, Atsushi [Department of Advanced Materials Science, Graduate School of Frontier Sciences, University of Tokyo, 5-1-5, Kashiwanoha, Kashiwa, Chiba, 277-8561 (Japan); Takeuchi, Akihisa; Suzuki, Yoshio [Japan Synchrotron Radiation Research Institute (JASRI), 1-1-1, Kouto, Sayo-cho, Sayo-gun, Hyogo, 679-5198 (Japan)

2010-06-23T23:59:59.000Z

108

Investigation of white etching layers on rails by optical microscopy, electron microscopy, X-ray and synchrotron X-ray diffraction  

Science Journals Connector (OSTI)

Patches of white etching layers on rail surfaces were investigated using sophisticated techniques like cross-sectional transmission electron microscopy (XTEM) and synchroton X-ray diffraction. Optical microscopy failed to resolve the microstructure, but in the TEM submicron grains with high dislocation densities and occasional twins, which are characteristic features of high carbon martensite, were observed. The martensitic structure was confirmed by evaluation of synchroton X-ray diffraction line profiles. The latter technique also allowed to determine dislocation densities of the order of 1012 cm?2 and residual compressive stresses of about 200 MPa.

W. Österle; H. Rooch; A. Pyzalla; L. Wang

2001-01-01T23:59:59.000Z

109

CFN Operations and Safety Awareness (COSA) Checklist Electron Microscopy Facility  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron Microscopy Facility Electron Microscopy Facility Building 735 This COSA form must be completed for all experimenters working in the CFN and must be submitted to the CFN User Office for badge access. CFN Safety Awareness Policy: Each user must be instructed in the safe procedures in CFN related activities. CFN Facility Laboratory personnel shall keep readily available all relevant instructions and safety literature. Employee/Guest Name Life/Guest Number Department/Division ES&H Coordinator/Ext. Facility Manager COSA Trainer Guest User Staff USER ADMINISTRATION Checked in at User Administration and has valid BNL ID badge Safety Approval Form (SAF) approved. Training requirements completed (Indicate additional training specified in SAF or ESR in lines provided below):

110

Recent advances in electron imaging, image interpretation and applications: environmental scanning electron microscopy  

Science Journals Connector (OSTI)

...A treatment of the physics governing this phenomenon...electron microscopy, the physics of which provides much...Varaprasad, L. H. 1991 Handbook of optical constants...ed.) 1991 CRC handbook of chemistry and physics. Boca Raton, FL...

2003-01-01T23:59:59.000Z

111

A New Cubic B-C-N Compound Revealed by High-Resolution Analytical Electron Microscopy  

Science Journals Connector (OSTI)

......nitride by electron energy-loss spectroscopy...Egerton RF: Electron energy loss spectroscopy...electron microscope. New York and London: Plenum...electron microscopy. New York: Plenum Press...system by electron energy loss spectroscopy......

Yoshio Bando; Satoshi Nakano; Keiji Kurashima

1996-04-01T23:59:59.000Z

112

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

NLE Websites -- All DOE Office Websites (Extended Search)

CM 200 FEG CM 200 FEG AEME The Philips CM200/FEG is a versatile instrument that is designed for analysis of the physical, chemical and magnetic microstructure at high spatial resolution. In addition to high resolution imaging capability, the machine is optimized for analytical electron microscopy and Lorentz imaging, under normal as well as dynamic conditions of variable temperature (77K - 1250K) and applied magnetic fields. Spatially resolved compositional analysis by X-ray emission spectroscopy (Z > 5), local electronic structure measurements by electron energy-loss spectroscopy (Z > 2), convergent beam electron diffraction for three-dimensional structure information, and energy-filtered imaging at the nanometer scale are some of the techniques available on this instrument. In addition, a TEM differential phase

113

In Situ Transmission Electron Microscopy Characterization of Nanomaterials  

E-Print Network (OSTI)

on the grain boundary sliding and grain rotation while the grain boundary interacting with dislocations [7-9]. The discoveries of new nanomaterials such as carbon nanotubes, nanowires and graphene have shown large potential impacts in the developments... with nanometer sized width [18]. Next, graphene nanosheet or thin film can be explained as a two dimensional nanostructured material with nanosized thickness [12, 19]. And finally, bulk nanostructed material can be exampled as a three dimensional...

Lee, Joon Hwan 1977-

2012-11-27T23:59:59.000Z

114

In Situ Transmission Electron Microscopy Observation of Microstructure...  

NLE Websites -- All DOE Office Websites (Extended Search)

This prototype lithium ion battery was built using a single SnO&8322; nanowire as the anode, an air stable salt: lithium bis(trifluoromethansulfonyl) imide (LiTFSI) in a...

115

Coal Combustion Fly Ash Characterization: Electron Spectroscopy for Chemical Analysis, Energy Dispersive X-ray Analysis, and Scanning Electron Microscopy  

Science Journals Connector (OSTI)

The surface and bulk properties of five samples of fly ash have been examined by electron spectroscopy for chemical analysis (ESCA), scanning electron microscopy (SEM) and energy...

Rothenberg, S J; Denee, P; Holloway, P

1980-01-01T23:59:59.000Z

116

Electron Microscopy of Myosin Molecules from Muscle and Non-Muscle Sources  

Science Journals Connector (OSTI)

...1976 research-article Electron Microscopy of Myosin...Muscle and Non-Muscle Sources A. Elliott G. Offer...give the two heads). Electron microscopy of myosin...muscle and non-muscle sources. | Journal Article...Chickens Microscopy, Electron Muscle Proteins Myosins...

1976-01-01T23:59:59.000Z

117

Laser Doppler holographic microscopy in transmission: application to fish embryo imaging  

E-Print Network (OSTI)

We have extended Laser Doppler holographic microscopy to transmission geometry. The technique is validated with living fish embryos imaged by a modified upright bio-microcope. By varying the frequency of the holographic reference beam, and the combination of frames used to calculate the hologram, multimodal imaging has been performed. Doppler images of the blood vessels for different Doppler shifts, images where the flow direction is coded in RGB colors or movies showing blood cells individual motion have been obtained as well. The ability to select the Fourier space zone that is used to calculate the signal, makes the method quantitative.

Verrier, Nicolas; Gross, Michel

2014-01-01T23:59:59.000Z

118

Aberration-Coreected Electron Microscopy at Brookhaven National Laboratory  

SciTech Connect

The last decade witnessed the rapid development and implementation of aberration correction in electron optics, realizing a more-than-70-year-old dream of aberration-free electron microscopy with a spatial resolution below one angstrom [1-9]. With sophisticated aberration correctors, modern electron microscopes now can reveal local structural information unavailable with neutrons and x-rays, such as the local arrangement of atoms, order/disorder, electronic inhomogeneity, bonding states, spin configuration, quantum confinement, and symmetry breaking [10-17]. Aberration correction through multipole-based correctors, as well as the associated improved stability in accelerating voltage, lens supplies, and goniometers in electron microscopes now enables medium-voltage (200-300kV) microscopes to achieve image resolution at or below 0.1nm. Aberration correction not only improves the instrument's spatial resolution but, equally importantly, allows larger objective lens pole-piece gaps to be employed thus realizing the potential of the instrument as a nanoscale property-measurement tool. That is, while retaining high spatial resolution, we can use various sample stages to observe the materials response under various temperature, electric- and magnetic- fields, and atmospheric environments. Such capabilities afford tremendous opportunities to tackle challenging science and technology issues in physics, chemistry, materials science, and biology. The research goal of the electron microscopy group at the Dept. of Condensed Matter Physics and Materials Science and the Center for Functional Nanomaterials, as well as the Institute for Advanced Electron Microscopy, Brookhaven National Laboratory (BNL), is to elucidate the microscopic origin of the physical- and chemical-behavior of materials, and the role of individual, or groups of atoms, especially in their native functional environments. We plan to accomplish this by developing and implementing various quantitative electron microscopy techniques in strongly correlated electron systems and nanostructured materials. As a first step, with the support of Materials Science Division, Office of Basic Energy Science, US Department of Energy, and the New York State Office of Science, Technology, and Academic Research, recently we acquired three aberration-corrected electron microscopes from the three major microscope manufacturers, i.e., JEOL, Hitachi, and FEI. The Hitachi HD2700C is equipped with a probe corrector, the FEI Titan 80-300 has an imaging corrector, while the JEOL2200MCO has both. All the correctors are of the dual-hexapole type, designed and manufactured by CEOS GmbH based on the design due to Rose and Haider [3, 18]. All these three are one-of-a-kind in the US, designed for specialized capabilities in characterizing nanoscale structure. In this chapter, we review the performance of these state-of-the art instruments and the new challenges associated with the improved spatial resolution, including the environment requirements of the laboratory that hosts these instruments. Although each instrument we describe here has its own strengths and drawbacks, it is not our intention to rank them in terms of their performance, especially their spatial resolution in imaging.

Zhu,Y.; Wall, J.

2008-04-01T23:59:59.000Z

119

Power electronics in electric utilities: HVDC power transmission systems  

SciTech Connect

High Voltage Direct Current (HVDC) power transmission systems constitute an important application of power electronics technology. This paper reviews salient aspects of this growing industry. The paper summarizes the history of HVDC transmission and discusses the economic and technical reasons responsible for development of HVDC systems. The paper also describes terminal design and basic configurations of HVDC systems, as well as major equipments of HVDC transmission system. In this regard, the state-of-the-art technology in the equipments constructions are discussed. Finally, the paper reviews future developments in the HVDC transmission systems, including promising technologies, such as multiterminal configurations, Gate Turn-Off (GTO) devices, forced commutation converters, and new advances in control electronics.

Nozari, F.; Patel, H.S.

1988-04-01T23:59:59.000Z

120

In situ redox cycle of a nickelYSZ fuel cell anode in an environmental transmission electron microscope  

E-Print Network (OSTI)

of a nickel/yttria-stabilized zirconia solid oxide fuel cell anode. The results reveal that the transfer transmission electron microscopy (ETEM); Solid oxide fuel cell (SOFC); Reduction; Oxidation; Density functional theory (DFT) 1. Introduction Solid oxide fuel cell (SOFC) technology is a promising energy conversion

Dunin-Borkowski, Rafal E.

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


121

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

NLE Websites -- All DOE Office Websites (Extended Search)

0.5 0.5 The TEAM 0.5 microscope is a double-aberration-corrected (scanning) transmission electron microscope (STEM/TEM) capable of producing images with 50 pm resolution. The basic instrument is a modified FEI Titan 80-300 microscope equipped with a special high-brightness Schottky-field emission electron source, a gun monochromator, a high-resolution GIF Tridiem energy-filter, and two CEOS hexapole-type spherical aberration correctors. The illumination aberration corrector corrects coherent axial aberrations up to 4th order, as well as 5th order spherical aberration and six-fold astigmatism. The imaging aberration corrector fully corrects for coherent axial aberrations up to 3rd order and partially compensates for 4th and 5th order aberrations. The microscope has two 2048x2048 slow-scan CCD

122

An electron microscopy study of the microstructure and microarchitecture of the Strombus gigas shell  

SciTech Connect

A scanning and transmission electron microscopy study is presented of the microstructure of the Strombus gigas shell. The hierarchical nature of this crossed-lamellar structure and the defect content of the mineral component are described. The mineral component consists of small single crystal grains of aragonite, the metastable orthorhombic polymorph of CaCO{sub 3}. The habit and morphology of the grains discussed here have not been determined previously. The observed habit and defect structure suggest that the organic matrix exerts a high degree of control over the crystal growth of the mineral phase and is responsible for the long range order in the microarhitecture. Electron beam heating of the mineral component leads to certain phase changes and these are discussed. 15 refs., 6 figs.

Rieke, P.C.; Laraia, V.J. (Pacific Northwest Lab., Richland, WA (USA)); Heuer, A.H. (Case Western Reserve Univ., Cleveland, OH (USA)); Aindow, M. (Ohio State Univ., Columbus, OH (USA))

1989-11-01T23:59:59.000Z

123

Hetero-epitaxial EuO interfaces studied by analytic electron microscopy  

SciTech Connect

With nearly complete spin polarization, the ferromagnetic semiconductor europium monoxide could enable next-generation spintronic devices by providing efficient ohmic spin injection into silicon. Spin injection is greatly affected by the quality of the interface between the injector and silicon. Here, we use atomic-resolution scanning transmission electron microscopy in conjunction with electron energy loss spectroscopy to directly image and chemically characterize a series of EuO|Si and EuO|YAlO{sub 3} interfaces fabricated using different growth conditions. We identify the presence of europium silicides and regions of disorder at the EuO|Si interfaces, imperfections that could significantly reduce spin injection efficiencies via spin-flip scattering.

Mundy, Julia A. [School of Applied and Engineering Physics, Cornell University, Ithaca, New York 14853 (United States); Hodash, Daniel; Melville, Alexander; Held, Rainer [Department of Materials Science and Engineering, Cornell University, Ithaca, New York 14853 (United States); Mairoser, Thomas; Schmehl, Andreas [Zentrum für Elektronische Korrelationen und Magnetismus, Universität Augsburg, Universitätsstraße 1, D-86159 Augsburg (Germany); Muller, David A.; Kourkoutis, Lena F. [School of Applied and Engineering Physics, Cornell University, Ithaca, New York 14853 (United States); Kavli Institute at Cornell for Nanoscale Science, Ithaca, New York 14853 (United States); Schlom, Darrell G. [Department of Materials Science and Engineering, Cornell University, Ithaca, New York 14853 (United States); Kavli Institute at Cornell for Nanoscale Science, Ithaca, New York 14853 (United States)

2014-03-03T23:59:59.000Z

124

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

NLE Websites -- All DOE Office Websites (Extended Search)

SPLEEM SPLEEM Publications Imaging Spin Reorientation Transitions in Consecutive Atomic Co layers, Farid El Gabaly, Silvia Gallego, M. Carmen Munoz, Laszlo Szunyogh, Peter Weinberger, Kevin F. McCarty, Christof Klein, Andreas K. Schmid, Juan de la Figuera, submitted Direct imaging of spin-reorientation transitions in ultra-thin Ni films by spin-polarized low-energy electron microscopy, C. Klein, A. K. Schmid, R. Ramchal, and M. Farle, submitted Controlling the kinetic order of spin-reorientation transitions in Ni/Cu(100) films by tuning the substrate step-structure, C. Klein, R. Ramchal, A.K. Schmid, M. Farle, submitted Self-organization and magnetic domain microstructure of Fe nanowire arrays, N. Rougemaille and A.K. Schmid, submitted Self-Assembled Nanofold Network Formation on Layered Crystal Surfaces

125

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

NLE Websites -- All DOE Office Websites (Extended Search)

Specimen Preparation Specimen Preparation Preparation of samples with large transparent areas and flat surfaces is a key element of electron microscopy. In particular, the interpretation of lattice or holographic images is often limited by the sample's geometry and surface roughness. These parameters are largely determined by a particular sample preparation procedure. The increasing demand for microscopes with a spatial resolution of better than 1Ã… increases the need for improved sample preparation techniques. A substantial effort at NCEM is devoted to the development of reliable and specialized thinning techniques. Current programs explore the application of chemicals to shape the surfaces of thin films, the use of nanospheres for observation of small particles, and the

126

Electron and Scanning Probe Microscopies | U.S. DOE Office of Science (SC)  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron and Scanning Probe Microscopies Electron and Scanning Probe Microscopies Materials Sciences and Engineering (MSE) Division MSE Home About Research Areas Energy Frontier Research Centers (EFRCs) DOE Energy Innovation Hubs BES Funding Opportunities The Computational Materials and Chemical Sciences Network (CMCSN) Theoretical Condensed Matter Physics Scientific Highlights Reports and Activities Principal Investigators' Meetings BES Home Research Areas Electron and Scanning Probe Microscopies Print Text Size: A A A RSS Feeds FeedbackShare Page This research area supports basic research in condensed matter physics and materials physics using electron scattering and microscopy and scanning probe techniques. The research includes experiments and theory to understand the atomic, electronic, and magnetic structures of materials.

127

E-Print Network 3.0 - analytical electron microscopy Sample Search...  

NLE Websites -- All DOE Office Websites (Extended Search)

Director Rutgers Research Showcase Summary: Electron Microscopy Nuclear Magnetic Resonance Spectroscopy X-Ray Diffraction Facility (XRD) Micro-Analytical... for...

128

Versatile Silicon Photodiode Detector Technology for Scanning Electron Microscopy with High-Efficiency Sub-5 keV Electron Detection  

E-Print Network (OSTI)

Versatile Silicon Photodiode Detector Technology for Scanning Electron Microscopy with High for Scanning Electron Microscopy, based on ultrashallow p+ n boron-layer photodiodes, features nm-thin anodes, closely-packed photodiodes and through-wafer apertures allow flexible configurations for optimal material

Technische Universiteit Delft

129

An electron microscopy study of wear in polysilicon microelectromechanical systems in ambient air  

E-Print Network (OSTI)

. © 2006 Elsevier B.V. All rights reserved. Keywords: Silicon; MEMS; Wear; Electron microscopy 1An electron microscopy study of wear in polysilicon microelectromechanical systems in ambient air D.H. Alsem a,b,c,, E.A. Stach d , M.T. Dugger e , M. Enachescu b , R.O. Ritchie a,b a Department of Materials

Ritchie, Robert

130

STUDIES OF DENGUE FEVER VIRUS BY ELECTRON MICROSCOPY  

Science Journals Connector (OSTI)

...MICROSCOPY Reginald L. Reagan A. L. Brueckner Live Stock Sanitary Service Laboratory...MICROSCOPY REGINALD L. REAGAN AND A. L. BRUECKNER Live Stock Sanitary Service Laboratory...material 233 REGINALD L. REAGAN AND A. L. BRUECKNER Figure 1. Dengue fever virus (mouse...

Reginald L. Reagan; A. L. Brueckner

1952-08-01T23:59:59.000Z

131

Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy  

SciTech Connect

Gold nanoparticle films are of interest in several branches of science and technology, and accurate sample characterization is needed but technically demanding. We prepared such films by DC magnetron sputtering and recorded their mass thickness by Rutherford backscattering spectroscopy. The geometric thickness d{sub g}—from the substrate to the tops of the nanoparticles—was obtained by scanning electron microscopy (SEM) combined with image analysis as well as by atomic force microscopy (AFM). The various techniques yielded an internally consistent characterization of the films. In particular, very similar results for d{sub g} were obtained by SEM with image analysis and by AFM.

Lansåker, Pia C., E-mail: pia.lansaker@angstrom.uu.se; Niklasson, Gunnar A.; Granqvist, Claes G. [Department of Engineering Sciences, The Ångström Laboratory, Uppsala University, P. O. Box 534, SE-751 21 Uppsala (Sweden); Hallén, Anders [Royal Institute of Technology, KTH-ICT, Elektrum 229, Kista, SE-164 40 Stockholm (Sweden)

2014-10-15T23:59:59.000Z

132

A Comparison of Image Quality Evaluation Techniques for Transmission X-Ray Microscopy  

SciTech Connect

Beamline 6-2c at Stanford Synchrotron Radiation Lightsource (SSRL) is capable of Transmission X-ray Microscopy (TXM) at 30 nm resolution. Raw images from the microscope must undergo extensive image processing before publication. Since typical data sets normally contain thousands of images, it is necessary to automate the image processing workflow as much as possible, particularly for the aligning and averaging of similar images. Currently we align images using the 'phase correlation' algorithm, which calculates the relative offset of two images by multiplying them in the frequency domain. For images containing high frequency noise, this algorithm will align noise with noise, resulting in a blurry average. To remedy this we multiply the images by a Gaussian function in the frequency domain, so that the algorithm ignores the high frequency noise while properly aligning the features of interest (FOI). The shape of the Gaussian is manually tuned by the user until the resulting average image is sharpest. To automatically optimize this process, it is necessary for the computer to evaluate the quality of the average image by quantifying its sharpness. In our research we explored two image sharpness metrics, the variance method and the frequency threshold method. The variance method uses the variance of the image as an indicator of sharpness while the frequency threshold method sums up the power in a specific frequency band. These metrics were tested on a variety of test images, containing both real and artificial noise. To apply these sharpness metrics, we designed and built a MATLAB graphical user interface (GUI) called 'Blur Master.' We found that it is possible for blurry images to have a large variance if they contain high amounts of noise. On the other hand, we found the frequency method to be quite reliable, although it is necessary to manually choose suitable limits for the frequency band. Further research must be performed to design an algorithm which automatically selects these parameters.

Bolgert, Peter J; /Marquette U. /SLAC

2012-08-31T23:59:59.000Z

133

A CCD Camera with Electron Decelerator for Intermediate Voltage Electron Microscopy  

SciTech Connect

Electron microscopists are increasingly turning to Intermediate Voltage Electron Microscopes (IVEMs) operating at 300 - 400 kV for a wide range of studies. They are also increasingly taking advantage of slow-scan charge coupled device (CCD) cameras, which have become widely used on electron microscopes. Under some conditions CCDs provide an improvement in data quality over photographic film, as well as the many advantages of direct digital readout. However, CCD performance is seriously degraded on IVEMs compared to the more conventional 100 kV microscopes. In order to increase the efficiency and quality of data recording on IVEMs, we have developed a CCD camera system in which the electrons are decelerated to below 100 kV before impacting the camera, resulting in greatly improved performance in both signal quality and resolution compared to other CCDs used in electron microscopy. These improvements will allow high-quality image and diffraction data to be collected directly with the CCD, enabling improvements in data collection for applications including high-resolution electron crystallography, single-particle reconstruction of protein structures, tomographic studies of cell ultrastructure and remote microscope operation. This approach will enable us to use even larger format CCD chips that are being developed with smaller pixels.

Downing, Kenneth H; Downing, Kenneth H.; Mooney, Paul E.

2008-03-17T23:59:59.000Z

134

Microstructural development in PWA-1480 electron beam welds: An atom probe field ion microscopy study  

SciTech Connect

The microstructure development in PWA-1480 superalloy electron beam weld (Ni-11.0 at. % Al-11.5% Cr-1.9% Ti-5.1% Co-4.0% Ta-1.3% W) was characterized. Optical microscopy revealed a branched dendritic structure in the weld metal. Transmission electron microscopy of these welds, in the as-welded condition, showed fine cuboidal (0.05--0.5 {mu}m) L1{sub 2}-ordered {gamma}{prime} precipitates within the y grains. The average volume percentage of {gamma}{prime} precipitates was found to be {approx}5%. Atom probe analyses revealed that the composition of {gamma} matrix was Ni-4.6 at. % Al-25.5% Cr-0.4% Ti-9.4% Co-0.8% Ta-2.9% W and that of {gamma}{prime} precipitates was Ni-17.3 at. % Al-2.6% Cr-2.4% Ti-3.0% Co-7.4% Ta-1.3% W. These compositions were compared with the previous APFIM analyses of commercial PWA-1480 single crystals that had received conventional heat treatments. Small differences were found in the chromium and aluminum levels and these may be due to the nonequilibrium nature of phase transformations that occur during weld cooling. No solute segregation was detected at the {gamma}-{gamma}{prime}interface. The APFIM results were also compared with the thermodynamic calculations of alloying element partitioning between {gamma} and {gamma}{prime} using the ThermoCalc{trademark} software.

David, S.A.; Miller, M.K. [Oak Ridge National Lab., TN (United States); Babu, S.S. [The Pennsylvania State Univ., State College, PA (United States)

1995-12-31T23:59:59.000Z

135

Analytical electron microscopy characterization of uranium-contaminated soils from the Fernald Site, FY1993 report  

SciTech Connect

A combination of optical microscopy, scanning electron microscopy with backscattered electron detection (SEM/BSE), and analytical electron microscopy (AEM) is being used to determine the nature of uranium in soils from the Fernald Environmental Management Project. The information gained from these studies is being used to develop and test remediation technologies. Investigations using SEM have shown that uranium is contained within particles that are typically 1 to 100 {mu}m in diameter. Further analysis with AEM has shown that these uranium-rich regions are made up of discrete uranium-bearing phases. The distribution of these uranium phases was found to be inhomogeneous at the microscopic level.

Buck, E.C.; Cunnane, J.C.; Brown, N.R.; Dietz, N.L.

1994-10-01T23:59:59.000Z

136

Los Alamos: MST: MST-6: EML: Electron Microscopy Laboratory  

NLE Websites -- All DOE Office Websites (Extended Search)

Strata DB235 FIB/SEM (Focused Ion Beam/High Reolution Scanning Electron Microscope) Strata DB235 FIB/SEM (Focused Ion Beam/High Reolution Scanning Electron Microscope) FEI Strata DB235 FIB/SEM (Focused Ion Beam/High Reolution Scanning Electron Microscope) This is a versatile field emission scanning electron microscope integrated with a focused ion beam column that is used for sophisticated SEM and TEM sample preparation, micromachining, and ultrahigh resolution SEM imaging. The microscope is also equipped for x-ray microanalysis and crystallographic orientation imaging. Microscope consists of a Hexalens SFEG electron beam column, and a Magnum ion beam column with a gallium liquid metal ion source. Imaging with both secondary electrons and ions. Digital image acquisition. Small, stable, high brightness Schottky based field emission electron source provides 1.5 nm resolution at 30 kV. Three electron beam lens modes - normal imaging, high resolution imaging, and EDS imaging.

137

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......Thoracic Lymphatics of Living Rabbits and Sites of Escape of Car- bon Particles from the Vessels: Fumihiko KATO (First Dept...deafness. Using light and elect- ron microscopy he studied the defective organ of Corti in Shaker-1 mouse, one strain of congeni......

ABSTRACTS

1967-01-01T23:59:59.000Z

138

Morphological properties of pillared layered materials investigated by electron microscopy technique  

E-Print Network (OSTI)

Scanning electron microscopy was used to investigate morphological features of a diverse range of pillared layered materials. Pillared layered zirconium phosphates, zirconium polyimine phosphonates and anion exchanger derivatives, zinc...

Navas de Mascianglioli, Margarit

2012-06-07T23:59:59.000Z

139

Dynamics of a nanodroplet under a transmission electron microscope  

SciTech Connect

We investigate the cyclical stick-slip motion of water nanodroplets on a hydrophilic substrate viewed with and stimulated by a transmission electron microscope. Using a continuum long wave theory, we show how the electrostatic stress imposed by non-uniform charge distribution causes a pinned convex drop to deform into a toroidal shape, with the shape characterized by the competition between the electrostatic stress and the surface tension of the drop, as well as the charge density distribution which follows a Poisson equation. A horizontal gradient in the charge density creates a lateral driving force, which when sufficiently large, overcomes the pinning induced by surface heterogeneities in the substrate disjoining pressure, causing the drop to slide on the substrate via a cyclical stick-slip motion. Our model predicts step-like dynamics in drop displacement and surface area jumps, qualitatively consistent with experimental observations.

Leong, Fong Yew, E-mail: leongfy@ihpc.a-star.edu.sg [A-STAR Institute of High Performance Computing, 1 Fusionopolis Way, Connexis, Singapore 138632 (Singapore); Mirsaidov, Utkur M. [Department of Physics, National University of Singapore, 2 Science Drive 3, Singapore 117551 (Singapore); Center for BioImaging Sciences, National University of Singapore, Science Drive 4, Singapore 117543 (Singapore); Matsudaira, Paul [Center for BioImaging Sciences, National University of Singapore, Science Drive 4, Singapore 117543 (Singapore); MechanoBiology Institute, National University of Singapore, 5A Engineering Drive 1, Singapore 117411 (Singapore); Department of Biological Sciences, National University of Singapore, 14 Science Drive 4, Singapore 117543 (Singapore); Singapore-MIT Alliance for Research and Technology Center, Science Drive 2, Singapore 117543 (Singapore); Mahadevan, L. [School of Engineering and Applied Sciences, Harvard University, Cambridge, Massachusetts 02138, USA and Department of Physics, Harvard University, Cambridge, Massachusetts 02138 (United States)

2014-01-15T23:59:59.000Z

140

Effectiveness of electron-cyclotron and transmission resonance heating in inductively coupled plasmas  

E-Print Network (OSTI)

Effectiveness of electron-cyclotron and transmission resonance heating in inductively coupled October 2005 The electron-cyclotron and transmission resonances in magnetically enhanced low-pressure one. It is shown that, for a high discharge frequency, the plasma resistance is greatly enhanced at electron-cyclotron

Economou, Demetre J.

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

Detecting Cellulase Penetration Into Corn Stover Cell Walls by Immuno-Electron Microscopy  

SciTech Connect

In general, pretreatments are designed to enhance the accessibility of cellulose to enzymes, allowing for more efficient conversion. In this study, we have detected the penetration of major cellulases present in a commercial enzyme preparation (Spezyme CP) into corn stem cell walls following mild-, moderate- and high-severity dilute sulfuric acid pretreatments. The Trichoderma reesei enzymes, Cel7A (CBH I) and Cel7B (EG I), as well as the cell wall matrix components xylan and lignin were visualized within digested corn stover cell walls by immuno transmission electron microscopy (TEM) using enzyme- and polymer-specific antibodies. Low severity dilute-acid pretreatment (20 min at 100 C) enabled <1% of the thickness of secondary cell walls to be penetrated by enzyme, moderate severity pretreatment at (20 min at 120 C) allowed the enzymes to penetrate {approx}20% of the cell wall, and the high severity (20 min pretreatment at 150 C) allowed 100% penetration of even the thickest cell walls. These data allow direct visualization of the dramatic effect dilute-acid pretreatment has on altering the condensed ultrastructure of biomass cell walls. Loosening of plant cell wall structure due to pretreatment and the subsequently improved access by cellulases has been hypothesized by the biomass conversion community for over two decades, and for the first time, this study provides direct visual evidence to verify this hypothesis. Further, the high-resolution enzyme penetration studies presented here provide insight into the mechanisms of cell wall deconstruction by cellulolytic enzymes.

Donohoe, B. S.; Selig, M. J.; Viamajala, S.; Vinzant, T. B.; Adney, W. S.; Himmel, M. E.

2009-06-15T23:59:59.000Z

142

HIGH-POWER MILLIMETREWAVE TRANSMISSION SYSTEMS AND COMPONENTS FOR ELECTRON CYCLOTRON HEATING OF FUSION PLASMAS  

Science Journals Connector (OSTI)

At the Institute for Plasma Research at the University of Stuttgart, high-power millimetre wave transmission systems for electron cyclotron heating (ECRH) and current drive (ECCD)...

W. Kasparek; G. Dammertz; V. Erckmann…

2005-01-01T23:59:59.000Z

143

Observation of buried interfaces with low energy electron microscopy  

Science Journals Connector (OSTI)

In this Letter we show that a coherent low energy electron beam (<100 eV) can be used to obtain real space images of structures and defects buried deep below the surface of the sample. The elastic strain fields of such buried structures, extending to the free surface, are found to give rise to localized phase shifts in the reflected electron waves, resulting in excellent image contrast under slight objective lens defocus conditions. We can now image the formation and evolution of buried interfaces and defects in situ, and in real time. Because of the very low electron energies used, this imaging method is nondestructive.

R. M. Tromp, A. W. Denier van der Gon, F. K. LeGoues, and M. C. Reuter

1993-11-15T23:59:59.000Z

144

Scanning transmission X-ray microscopy probe for in situ mechanism study of graphene-oxide-based resistive random access memory  

Science Journals Connector (OSTI)

An in situ probe for scanning transmission X-ray microscopy has been developed and applied to the study of the bipolar resistive switching mechanism in an Al/graphene oxide/Al resistive random access memory device.

Nho, H.W.

2013-11-28T23:59:59.000Z

145

In-situ UHV Electron Microscopy of Surfaces  

Science Journals Connector (OSTI)

Recently great progress has been made in surface science due to the development of ultra-high-vacuum (UHV) techniques and related surface-analytical methods like ... (LEED), Auger electron spectroscopy (AES), UHV

Katsumichi Yagi; Kunio Takayanagi; Goro Honjo

1982-01-01T23:59:59.000Z

146

Tailoring of electron flow current in magnetically insulated transmission lines J. P. Martin,2,3  

E-Print Network (OSTI)

Tailoring of electron flow current in magnetically insulated transmission lines J. P. Martin,2,3 M of the drive pulse. It is clear that neither fixed gap nor constant-impedance transmission lines are optimal the impedance profiles developed in a radial disk magnetically insulated transmission line geometry. The input

147

THE THIRTY-EIGHTH ANNUAL MEETING OF THE JAPANESE SOCIETY OF ELECTRON MICROSCOPY:  

Science Journals Connector (OSTI)

......electron- opaque material. Intramembranous...the presynaptic active zone. Third type...microscopy. Membranous materials extended from the...gun with a point cathode Kohki NIMURA, Masahiko...464 Japan A point cathode triode electron...made of magnetic materials (pure iron......

The Thirty-eighth Annual Meeting of the Japanese Society of Electron Microscopy: held at Komaba Eminence; Tokyo; May 26?28; 1982

1982-01-01T23:59:59.000Z

148

Quantifying Transient States in Materials with the Dynamic Transmission Electron Microscope  

SciTech Connect

The Dynamic Transmission Electron Microscope (DTEM) offers a means of capturing rapid evolution in a specimen through in-situ microscopy experiments by allowing 15 ns electron micrograph exposure times. The rapid exposure time is enabled by creating a burst of electrons at the emitter by ultraviolet pulsed laser illumination. This burst arrives a specified time after a second laser initiates the specimen reaction. The timing of the two Q-switched lasers is controlled by high-speed pulse generators with a timing error much less than the pulse duration. Both diffraction and imaging experiments can be performed, just as in a conventional TEM. The brightness of the emitter and the total current control the spatial and temporal resolutions. We have demonstrated 7 nm spatial resolution in single 15 ns pulsed images. These single-pulse imaging experiments have been used to study martensitic transformations, nucleation and crystallization of an amorphous metal, and rapid chemical reactions. Measurements have been performed on these systems that are possible by no other experimental approaches currently available.

Campbell, G; LaGrange, T; Kim, J; Reed, B; Browning, N

2009-09-21T23:59:59.000Z

149

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......branches expand upwards according to physiolo- gical and ecological conditions. B-65-17O. Cyclic changes of the Golgi body...further it was assumed" that the network of smooth ER might be vehicles'of precursor of steroid hormone.- B-66-115. An Electron......

ABSTRACTS

1967-01-01T23:59:59.000Z

150

PROOF COPY 034509PHP Effectiveness of electron-cyclotron and transmission resonant heating  

E-Print Network (OSTI)

PROOF COPY 034509PHP PROOF COPY 034509PHP Effectiveness of electron-cyclotron and transmission resonant heating in inductively coupled plasmas Oleg V. Polomarov and Constantine E. Theodosiou University June 2005 The electron-cyclotron and transmission resonances in magnetically enhanced low-pressure one

Kaganovich, Igor

151

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

NLE Websites -- All DOE Office Websites (Extended Search)

AEM AEM AEME The Analytical Electron Microscope is optimized for elemental microanalysis. The basic instrument is a JEOL 200CX microscope with a side-entry double-tilt goniometer stage and an assortment of specimen holders. This machine can be operated at between 80 and 200 kV in the TEM or STEM mode. Electron energy loss and x-ray signals for elemental microanalysis or spectral imaging can be collected either separately or simultaneously using probe diameters from 6nm to 100nm. Diffraction modes include convergent beam diffraction for three-dimensional structure information and micro-diffraction with a minimum probe size of 20nm. For updates or details, contact Zonghoon Lee or Velimir Radmilovic. The instrument is equipped with two Kevex EDXS detectors and a Gatan PEELS

152

Time-resolved observation in transmission electron microscopy by means of spatially resolved electron correlation spectroscopy  

Science Journals Connector (OSTI)

......The cross-sectional diagram and electric field distribution of a Si-APD...the reversed bias and thus the electric field (>10 V/m) accelerates...mechanical nanotubes produced by arc discharge method are now ^kctron intensjty......

Nobuyuki Osakabe; Tetsuji Kodama; Tsuneyuki Urakami; Shinji Ohsuka; Hiroshi Tsuchiya; Yutaka Tsuchiya; Junji Endo; Akira Tonomura

1998-01-01T23:59:59.000Z

153

High-resolution transmission electron microscopy and electron energy loss spectroscopy of doped nanocarbons.  

E-Print Network (OSTI)

??Graphene, a one-atom thick sheet of carbon, is the thinnest, strongest and most electrically conductive material ever discovered. Alongside carbon nanotubes it is part of… (more)

Pierce, William Renton

2014-01-01T23:59:59.000Z

154

Laboratory-Based Cryogenic Soft X-ray Tomography with Correlative Cryo-Light and Electron Microscopy  

SciTech Connect

Here we present a novel laboratory-based cryogenic soft X-ray microscope for whole cell tomography of frozen hydrated samples. We demonstrate the capabilities of this compact cryogenic microscope by visualizing internal sub-cellular structures of Saccharomyces cerevisiae cells. The microscope is shown to achieve better than 50 nm spatial resolution with a Siemens star test sample. For whole biological cells, the microscope can image specimens up to 5 micrometers thick. Structures as small as 90 nm can be detected in tomographic reconstructions at roughly 70 nm spatial resolution following a low cumulative radiation dose of only 7.2 MGy. Furthermore, the design of the specimen chamber utilizes a standard sample support that permits multimodal correlative imaging of the exact same unstained yeast cell via cryo-fluorescence light microscopy, cryo-soft x-ray microscopy and cryo-transmission electron microscopy. This completely laboratory-based cryogenic soft x-ray microscope will therefore enable greater access to three-dimensional ultrastructure determination of biological whole cells without chemical fixation or physical sectioning.

Carlson, David B.; Gelb, Jeff; Palshin, Vadim; Evans, James E.

2013-02-01T23:59:59.000Z

155

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

NLE Websites -- All DOE Office Websites (Extended Search)

LIBRA LIBRA The 200kV Zeiss monochromated LIBRA 200MC is designed to produce high contrast imaging for TEM and STEM and either convergent beam or parallel beam diffraction using Koehler illumination.In addition, the incorporation of a monochromator into the field emission gun enables energy resolution of ~0.15eV for electron energy loss spectroscopy. The dedicated in-column Omega Filter implemented in this microscope also can be used for both spectroscopic analysis and energy-filtered imaging with a 2048x2048 CCD camera. The high tilt capability of the stage and pole piece accepts various types of analytical holders.This microscope is optimized for soft materials applications that require either the high contrast imaging performance or analytical methods such as EF-TEM and STEM.( Instrument

156

Development of a surface conductivity measurement system for ultrahigh vacuum transmission electron microscope  

SciTech Connect

The surface conductivity measurement system using a micro-four-point probe (M4PP) had been developed for the ultrahigh vacuum transmission electron microscope (UHV-TEM). Since the current distribution in the sample crystals during the current voltage measurement by the M4PP is localized within the depth of several micrometers from the surface, the system is sensitive to the surface conductivity, which is related with the surface superstructure. It was installed in the main chamber of the TEM and the surface conductivity can be measured in situ. The surface structures were observed by reflection electron microscopy and diffraction (REM-RHEED). REM-RHEED enables us to observe the surface superstructures and their structure defects such as surface atomic steps and domain boundaries of the surface superstructure. Thus the effects of the defects on the surface conductivity can be investigated. In the present paper we present the surface conductivity measurement system and its application to the Si(111)-{radical}(3)x{radical}(3)-Ag surface prepared on the Si(111) vicinal surfaces. The result clearly showed that the surface conductivity was affected by step configuration.

Minoda, H. [Department of Applied Physics, Tokyo University of Agriculture and Technology, Koganei, Tokyo 184-8588 (Japan); CREST, Japan Science and Technology Agency, Kawaguchi, Saitama 332-0012 (Japan); Hatano, K.; Yazawa, H. [Department of Applied Physics, Tokyo University of Agriculture and Technology, Koganei, Tokyo 184-8588 (Japan)

2009-11-15T23:59:59.000Z

157

In Situ, Real-Time Characterization of Silicide Nanostructure Coarsening Dynamics by Photo-Electron Emission Microscopy.  

E-Print Network (OSTI)

??Photo-electron emission microscopy (PEEM) was used to observe the growth and coarsening dynamics of transition metal (TM) silicide and rare earth (RE) silicide nanostructures on… (more)

Zeman, Matthew Casimir

2007-01-01T23:59:59.000Z

158

Momentum-resolved Electron Energy-Loss Spectroscopy Master Thesis, Electron Microscopy Group of Materials Science, Prof. Ute Kaiser  

E-Print Network (OSTI)

of Materials Science, Prof. Ute Kaiser Background Electron energy-loss spectroscopy (EELS) is a well like plasmons at a few 10eV, to core-shell excitations at high energy losses. In addition to the energy Microscopy group of Material Sciences in Ulm has gained experience in the acquisition and analysis of energy

Pfeifer, Holger

159

Microcalorimeter-type energy dispersive X-ray spectrometer for a transmission electron microscope  

Science Journals Connector (OSTI)

......Microscopy (1986) New York: Plenum Press. 4...Garratt-Reed A J , Bell D C. Energy-Dispersive X-ray...Microscopy (1996) New York: Plenum Press. 19...Microcalorimeter-type energy dispersive X-ray...electron microscope. | A new energy dispersive......

Toru Hara; Keiichi Tanaka; Keisuke Maehata; Kazuhisa Mitsuda; Noriko Y. Yamasaki; Mitsuaki Ohsaki; Katsuaki Watanabe; Xiuzhen Yu; Takuji Ito; Yoshihiro Yamanaka

2010-02-01T23:59:59.000Z

160

A method for the alignment of heterogeneous macromolecules from electron microscopy  

E-Print Network (OSTI)

dataset. Ã? 2009 Published by Elsevier Inc. 1. Introduction Single-particle electron microscopy (EM and Microbial Biology, University of California, Berkeley, CA 94720-3102, USA b Physical Biosciences Division, Lawrence Berkeley National Laboratory, CA 94720, USA a r t i c l e i n f o Article history: Received 13

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

Rumen microbial degradation of modified lignin plants observed by electron microscopy  

E-Print Network (OSTI)

Rumen microbial degradation of modified lignin plants observed by electron microscopy C Mign6, E-Genès-Champanelle, France The microbial degradation of modified lignin tobacco (Samson variety) plants (homozygous line 40 to the corresponding cinnamyl alcohols which are the direct monomeric precursors of the lignin. Only the stems were

Paris-Sud XI, Université de

162

Dynamic Characterization of Graphene Growth and Etching by Oxygen on Ru(0001) by Photoemission Electron Microscopy  

E-Print Network (OSTI)

Dynamic Characterization of Graphene Growth and Etching by Oxygen on Ru(0001) by Photoemission of graphene on Ru(0001) was investigated by photoemission electron microscopy (PEEM) and scanning tunneling, we show that graphene overlayers with sizes ranging from nanometers to sub-millimeters have been

Bao, Xinhe

163

FtsZ Condensates: An In Vitro Electron Microscopy Study David Popp,1  

E-Print Network (OSTI)

FtsZ Condensates: An In Vitro Electron Microscopy Study David Popp,1 Mitsusada Iwasa,1 Akihiro in vitro system of supramolecular condensates experimentally and theoretically is DNA, which also exists in highly condensed, tightly packed states in viruses and sperm cells in vivo.2 The principle morphologies

Erickson, Harold P.

164

Nano-mineralogy studies by advanced electron microscopy Chi Ma and George R. Rossman  

E-Print Network (OSTI)

Nano-mineralogy studies by advanced electron microscopy Chi Ma and George R. Rossman Division and planetary materials easier and faster down to nano-scales. Small but new minerals with important geological significance are being discovered. Nano-features are being discovered in many common minerals and gems, which

Ma, Chi

165

Pressure-induced densification in GeO{sub 2} glass: A transmission x-ray microscopy study  

SciTech Connect

Nanoscale transmission x-ray microscopy measurements have been performed to determine the effect of pressure (P) on the volume (V) change in GeO{sub 2} glass up to 38.5?GPa. The P-V data show a continuous increase upon compression, indicating that the density-driven structural transformation is a gradual process. Over the pressure range studied, a transition is observed at approximately 10–13?GPa, where the material displays distinct compression behaviors. The pressure-induced densification that involves the coordination number change has been discussed. Using this newly developed high-pressure imaging technique with tens of nanometer resolution, we have provided a direct and unequivocal way for measuring density of amorphous materials to much higher pressures with accuracy rivaling x-ray diffraction of crystalline solids.

Lin, Yu, E-mail: lyforest@stanford.edu; Zeng, Qiaoshi [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States)] [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States); Yang, Wenge [High Pressure Synergetic Consortium, Geophysical Laboratory, Carnegie Institution of Washington, Argonne, Illinois 60439 (United States)] [High Pressure Synergetic Consortium, Geophysical Laboratory, Carnegie Institution of Washington, Argonne, Illinois 60439 (United States); Mao, Wendy L. [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States) [Department of Geological and Environmental Sciences, Stanford University, Stanford, California 94305 (United States); Photon Science, SLAC National Accelerator Laboratory, Menlo Park, California 94025 (United States)

2013-12-23T23:59:59.000Z

166

From electron energy-loss spectroscopy to multi-dimensional and multi-signal electron microscopy  

Science Journals Connector (OSTI)

......4 Colliex C . Electron Energy Loss Spectroscopy in the...eds. (1984) Vol. 9. New York: Academic Press. 65-177. 5 Egerton R . Electron Energy Loss Spectroscopy in the Electron Microscope (1986) New York: Plenum Press. 6 Isaacson......

Christian Colliex

2011-08-01T23:59:59.000Z

167

Electronically controllable transmission line design for traveling wave array antenna feed network  

E-Print Network (OSTI)

In this thesis, an electronically controllable transmission line (ECTL) is presented. By modulating the conductivity of a doped Si modulator in the ECTL, the wave propagation constant in the ECTL is controlled. Measured results show a phase...

Shin, Chang-Seok

2012-06-07T23:59:59.000Z

168

Real-time studies of battery electrochemical reactions inside a transmission electron microscope.  

SciTech Connect

We report the development of new experimental capabilities and ab initio modeling for real-time studies of Li-ion battery electrochemical reactions. We developed three capabilities for in-situ transmission electron microscopy (TEM) studies: a capability that uses a nanomanipulator inside the TEM to assemble electrochemical cells with ionic liquid or solid state electrolytes, a capability that uses on-chip assembly of battery components on to TEM-compatible multi-electrode arrays, and a capability that uses a TEM-compatible sealed electrochemical cell that we developed for performing in-situ TEM using volatile battery electrolytes. These capabilities were used to understand lithiation mechanisms in nanoscale battery materials, including SnO{sub 2}, Si, Ge, Al, ZnO, and MnO{sub 2}. The modeling approaches used ab initio molecular dynamics to understand early stages of ethylene carbonate reduction on lithiated-graphite and lithium surfaces and constrained density functional theory to understand ethylene carbonate reduction on passivated electrode surfaces.

Leung, Kevin; Hudak, Nicholas S.; Liu, Yang; Liu, Xiaohua H.; Fan, Hongyou; Subramanian, Arunkumar; Shaw, Michael J.; Sullivan, John Patrick; Huang, Jian Yu

2012-01-01T23:59:59.000Z

169

Transmission and Backscattering of 4.0- to 12.0-MeV Electrons  

Science Journals Connector (OSTI)

Transmission and backscattering coefficients were measured for 4.0- to 12.0-MeV monoenergetic electrons normally incident on solid targets of C, Al, Cu, Ag, Ta, and U. Transmitted and backscattered electrons were collected by biased Faraday cups, each subtending ?90% of 2? sr. Number transmission coefficients at 10 MeV agree with Berger and Seltzer's Monte Carlo results, and saturation backscattering coefficients generally agree with Tabata's results to within ±10%. Empirical formulas for determining the extrapolated range and both the transmission and backscattering coefficients as a function of Z, energy, and thickness have been developed.

P. J. Ebert, A. F. Lauzon, and E. M. Lent

1969-07-10T23:59:59.000Z

170

Transmission  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Transmission Transmission ,... ,...vc- "' ""'\ S I r;. Dr. Jerry Pell, CCM Principal NEP A Document Manager Permitting, Siting, and Analysis (OE-20) Office of Electricity Delivery and Energy Reliability U.S. Department of Energy 1 000 Independence A venue SW Washington, D.C. 20585-0001 Subject: Champlain Hudson Power Express Project Submittal of Amendment Application Dear Dr. Pell: February 28, 2012 On January 25, 2010, Transmission Developers, Inc. ("TDI") submitted on behalf of Champlain Hudson Power Express, Inc. ("CHPEI") an application to the U.S. Department of Energy ("DOE") for a Presidential Permit ("Application) in connection with the Champlain Hudson Power Express project ("Project"). The Application proposed to connect clean sources

171

Transmission electron energy-loss spectroscopy study of carbon nanotubes upon high temperature treatment  

E-Print Network (OSTI)

Transmission electron energy-loss spectroscopy study of carbon nanotubes upon high temperature electron energy-loss spectroscopy study of carbon nanotubes upon high temperature treatment B. W. Reed, M of carbon nanotube materials, grown with a pulsed-laser deposition technique but purified and heat treated

Bertsch George F.

172

CFN | Hitachi HD2700C Scanning Transmission Electron Microscope  

NLE Websites -- All DOE Office Websites (Extended Search)

spectroscopy (EELS) can be as small as 0.35 eV, due to its cold field emission electron gun (FEG) and the presence of a high-resolution parallel EELS detector (Gatan Enfina-ER)....

173

A new approach to nuclear microscopy: The ion-electron emission microscope  

SciTech Connect

A new multidimensional high lateral resolution ion beam analysis technique, Ion-Electron Emission Microscopy or IEEM is described. Using MeV energy ions, IEEM is shown to be capable of Ion Beam Induced Charge Collection (IBICC) measurements in semiconductors. IEEM should also be capable of microscopically and multidimensionally mapping the surface and bulk composition of solids. As such, IIEM has nearly identical capabilities as traditional nuclear microprobe analysis, with the advantage that the ion beam does not have to be focused. The technique is based on determining the position where an individual ion enters the surface of the sample by projection secondary electron emission microscopy. The x-y origination point of a secondary electron, and hence the impact coordinates of the corresponding incident ion, is recorded with a position sensitive detector connected to a standard photoemission electron microscope (PEEM). These signals are then used to establish coincidence with IBICC, atomic, or nuclear reaction induced ion beam analysis signals simultaneously caused by the incident ion.

Doyle, B.L.; Vizkelethy, G.; Walsh, D.S. [Sandia National Labs., Albuquerque, NM (United States); Senftinger, B. [Staib Instrumente GmbH, Langenbach (Germany); Mellon, M. [Quantar Technologies Inc., Santa Cruz, CA (United States)

1998-11-01T23:59:59.000Z

174

Recent advances in electron imaging, image interpretation and applications: environmental scanning electron microscopy  

Science Journals Connector (OSTI)

...specimens in a more `natural' state. As early...the presence of a gas in the specimen chamber...Ionizing collisions with gas molecules generate...SEs, causing a `cascade' of electrons...turn influencing gas cascade amplification. Add...

2003-01-01T23:59:59.000Z

175

Electronic structure of wurtzite II-VI compound semiconductor cleavage surfaces studied by scanning tunneling microscopy  

Science Journals Connector (OSTI)

We report atomically resolved scanning tunneling microscopy (STM) images of cleavage surfaces of wurtzite II-VI compound semiconductors. CdSe(112¯0), CdSe(101¯0), and CdS(101¯0) were investigated. The STM images confirm a 1×1 reconstruction for all surfaces. At negative and positive sample voltages the occupied and empty dangling-bond states above anions and cations, respectively, dominate the contrast of the STM images. No states in the band gap were found. The electronic structure of the surface permits the observation of dopant atoms in subsurface layers and thus also cross-sectional scanning tunneling microscopy studies of point defects and heterostructures.

B. Siemens, C. Domke, Ph. Ebert, and K. Urban

1997-11-15T23:59:59.000Z

176

Structure of the dimeric RC–LH1–PufX complex from Rhodobaca bogoriensis investigated by electron microscopy  

Science Journals Connector (OSTI)

...j.boekema@rug.nl ). 1 Electron Microscopy Group, Groningen Biomolecular Sciences and Biotechnology Institute, University of Groningen, , Nijenborgh 7, 9747 AG, Groningen, The Netherlands 2 IBDML - Developmental Biology Institute...

2012-01-01T23:59:59.000Z

177

Periodicity faults in chain silicates: A new type of planar lattice fault observed with high resolution electron microscopy  

Science Journals Connector (OSTI)

The existence of errors in the periodicity of the tetrahedral chains in pyroxenes and pyroxenoids is predicted. With high resolution electron microscopy of rhodonite, (Mn, Ca)5[Si5O15], and pyroxmangite, (Mn,Fe,C...

M. Czank; F. Liebau

1980-07-01T23:59:59.000Z

178

Microstructure development in particulate coatings examined with high-resolution cryogenic scanning electron microscopy  

SciTech Connect

The authors used cryogenic scanning electron microscopy to examine the early stages of latex film formation. They visualized the influence of ionic strength and extent of carboxylation in latex-calcium carbonate formulations and in latex-only formulations. Results demonstrated that latex particles deposited on calcium carbonate surfaces creating a suspension of carboxylic acid-stabilized calcium carbonate particles. Images of consolidation fronts showed that variation of ionic strength and extent of carboxylation dramatically changes the way latex particles consolidate and form films.

Sheehan, J.G.; Davis, H.T.; Scriven, L.E. [Univ. of Minnesota, Minneapolis, MN (United States); Takamura, Koichi [BASF Corp., Charlotte, NC (United States)

1993-12-01T23:59:59.000Z

179

Quantification of nanoscale density fluctuations using electron microscopy: Light-localization properties of biological cells  

SciTech Connect

We report a study of the nanoscale mass-density fluctuations of heterogeneous optical dielectric media, including nanomaterials and biological cells, by quantifying their nanoscale light-localization properties. Transmission electron microscope images of the media are used to construct corresponding effective disordered optical lattices. Light-localization properties are studied by the statistical analysis of the inverse participation ratio (IPR) of the localized eigenfunctions of these optical lattices at the nanoscale. We validated IPR analysis using nanomaterials as models of disordered systems fabricated from dielectric nanoparticles. As an example, we then applied such analysis to distinguish between cells with different degrees of aggressive malignancy.

Pradhan, Prabhakar; Damania, Dhwanil; Turzhitsky, Vladimir; Subramanian, Hariharan; Backman, Vadim [Department of Biomedical Engineering, Northwestern University, Evanston, Illinois 60208 (United States); Joshi, Hrushikesh M.; Dravid, Vinayak P. [Department of Material Science and Engineering, Northwestern University, Evanston, Illinois 60208 (United States); Roy, Hemant K. [Department of Internal Medicine, NorthShore University HealthSystem, Evanston, Illinois 60201 (United States); Taflove, Allen [Department of Electrical Engineering and Computer Science, Northwestern University, Evanston, Illinois 60208 (United States)

2010-12-13T23:59:59.000Z

180

Preparation of Combinatorial Arrays of Polymer Thin Films for Transmission Electron Microscopy Analysis  

Science Journals Connector (OSTI)

Overwijk, M. H. F., Vandenheuvel, F. C., and Bullelieuwma, C. W. T. J. Vac. ... Overwijk, M. H. F.; van den Heuvel, F. C.; Bulle-Lieuwma, C. W. T. ...

Kristen E. Roskov; Thomas H. Epps; III; Brian C. Berry; Steven D. Hudson; Maëva S. Tureau; Michael J. Fasolka

2008-10-20T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

Reactive ion etching: Optimized diamond membrane fabrication for transmission electron microscopy  

E-Print Network (OSTI)

Commonly used preparation method for thin diamond membranes by focused ion beam (FIB) techniques results in surface damage. Here, the authors introduce an alternative method based on reactive ion etching (RIE). To compare ...

Li, Luozhou

182

A review of focused ion beam technology and its applications in transmission electron microscopy  

Science Journals Connector (OSTI)

......as the "trench" method. In a variation of this method, Overwijk et al. [15] proposed a novel scheme in 1993 for the preparation...15 Overwijk M H F, van den Heuvel F C, and Bulle-Lieuwma C W T (1993......

Masaaki Sugiyama; Genichi Sigesato

2004-10-01T23:59:59.000Z

183

Platelet Adhesion in Rabbit Arteries observed by Scanning and Transmission Electron Microscopy  

Science Journals Connector (OSTI)

... the endothelium is removed from the mid-abdominal aorta of a rabbit, by passing a roughened probe into the lumen, only single platelets or small platelet clumps adhere to the ...

B. L. SHEPPARD; J. E. FRENCH

1970-03-14T23:59:59.000Z

184

Aberration-corrected scanning transmission electron microscopy: from atomic imaging and analysis to solving energy problems  

Science Journals Connector (OSTI)

...in solving the pressing energy problems facing us today...Discussion Meeting Issue New possibilities with aberration-corrected...Wang), pp.152-191. New York, NY: Springer. Pennycook...and analysis to solving energy problems. | The new possibilities of aberration-corrected...

2009-01-01T23:59:59.000Z

185

A review of focused ion beam technology and its applications in transmission electron microscopy  

Science Journals Connector (OSTI)

......fabrication technologies. Damage issues...twodimensional,cell-basedtopographysimulations...of polymer solar cells deposited on...progress of FIB technology and its applications...observation technology of binder...of polymer solar cells deposited on......

Masaaki Sugiyama; Genichi Sigesato

2004-10-01T23:59:59.000Z

186

In Situ Transmission Electron Microscopy Study of Electrochemical Sodiation and Potassiation of Carbon Nanofibers  

E-Print Network (OSTI)

to store large amounts of electrical energy from intermittent renewable sources such as solar and wind Mexico 87185, United States Department of Mechanical Engineering, University of Maryland, College Park The large-scale storage of electrical energy for applications in electrical grids requires battery systems

Zhu, Ting

187

Development of a large format direct detection device for three dimensional transmission electron microscopy  

E-Print Network (OSTI)

F. Duttweiler, J.C. Bouwer, S.T. Peltier, M.H. Ellisman, andDuttweiler, J.C. Bouwer, S.T. Peltier, M. Ellisman, and N.H.Duttweiler, J.C. Bouwer, S.T. Peltier, A.C. Milazzo, and M.

Milazzo, Anna-Clare

2009-01-01T23:59:59.000Z

188

Investigating the Optical Properties of Dislocations by Scanning Transmission Electron Microscopy  

E-Print Network (OSTI)

investigation for solid-state lighting and display applications, and dislocations are known to be nonradiative the radiative pathway and contribute to the enormous savings in energy use and greenhouse gas emissions expected with efficient solid-state lighting. CL Studies of Dislocations One of the key advantages of a scanning micro

Pennycook, Steve

189

Aberration-corrected scanning transmission electron microscopy: from atomic imaging and analysis to solving energy problems  

Science Journals Connector (OSTI)

...fuels, but the conversion efficiency of...into electrical energy is limited by...functionality in energy conversion devices such as...insights into the carrier dynamics in the...ability to study energy conversion processes in materials...

2009-01-01T23:59:59.000Z

190

Validation of Pisum sativum agglutinin fluorescent marker for stallion spermatozoal acrosomes with transmission electron microscopy  

E-Print Network (OSTI)

. Either 1 uM or 10 uM A23187 (a calcium ionophore) was added to each ejaculate and incubated for 1,2 and 3 hours at two different temperatures (37C? and 22C?). Raw semen or extender were fixed at time zero to serve as baseline controls. Other untreated...

Carrell, Betty Pauline

2012-06-07T23:59:59.000Z

191

Optimizing the environment for sub-0.2 nm scanning transmission electron microscopy  

Science Journals Connector (OSTI)

......where the manufacturer's specifications will be most complete) are...or neoprene greatly damps thermal fluctuations (Fig. 7...with neoprene for improved thermal stability. D. A. Muller...column helps greatly, better insulation of the stage drives and objective......

A Muller; J Grazul

2001-05-01T23:59:59.000Z

192

Transmission electron microscopy of synthetic and natural Fünferketten and Siebenerketten pyroxenoids  

Science Journals Connector (OSTI)

A new type of fault, called a chain periodicity fault, has been observed in Fünferketten and Siebenerketten pyroxenoids. The faults are mainly parallel to (001) and are due to irregularities in the periodicity...

H. Ried; M. Korekawa

1980-04-01T23:59:59.000Z

193

TRANSMISSION ELECTRON MICROSCOPY AND RUTHERFORD BACKSCATTERING STUDIES OF DIFFERENT DAMAGE STRUCTURES IN p+ IMPLANTED Si  

E-Print Network (OSTI)

Peregainus, Stevenage) )970 and AERE Report R 6496 (1970).Jim Stephens and D. Chivers of AERE Harewell (England) for

Sadana, D.K.

2013-01-01T23:59:59.000Z

194

Transmission electron microscopy studies of GaN/gamma-LiAlO 2 heterostructures.  

E-Print Network (OSTI)

??Die vorliegende Arbeit beschaeftigt sich mit dem strukturellen Aufbau von (1-100) M-plane GaN, das mit plasmaunterstuetzter Molekularstrahlepitaxie auf gamma-LiAlO2(100) Substraten gewachsen wurde. Die heteroepitaktische Ausrichtung… (more)

Liu, Tian-Yu

2005-01-01T23:59:59.000Z

195

Assembly of Large Three-Dimensional Volumes from Serial-Section Transmission Electron Microscopy  

E-Print Network (OSTI)

Pavel Koshevoy1, Tolga Tasdizen1, Ross Whitaker1, Bryan Jones2 and Robert Marc2 1Scientific Computing size and limited field of view: each section must be assembled from many overlapping tiles, a process, data-driven descriptions of microscopic structures are very important in neurobiology. While neural

Utah, University of

196

A review of focused ion beam technology and its applications in transmission electron microscopy  

Science Journals Connector (OSTI)

......Observation of the configuration of binder latex in coating layer -Direct observation technology of binder. In: Proc. Japan TAPPI Annual Meeting, pp. 679-685....................

Masaaki Sugiyama; Genichi Sigesato

2004-10-01T23:59:59.000Z

197

A review of focused ion beam technology and its applications in transmission electron microscopy  

Science Journals Connector (OSTI)

......a technique that requires high electric fields (10 6 V/cm) to be applied...and metal at the same time. In automobile tyres, a steel cord is plated with...effects of implanted Ga on high electric field diamond devices fabricated......

Masaaki Sugiyama; Genichi Sigesato

2004-10-01T23:59:59.000Z

198

Structural defects in GaN revealed by Transmission Electron Microscopy  

E-Print Network (OSTI)

67, 410 (1985). 23) M. Tachikawa and M Yamaguchi, Appl.Fig. 2. 20) However, Tachikawa and Yamaguchi model adapted

Liliental-Weber, Zuzanna

2014-01-01T23:59:59.000Z

199

Scanning electron microscopy and electron probe microanalyses of the crystalline components of human and animal dental calculi  

SciTech Connect

A review of the use of scanning electron microscopy (SEM) and electron probe microanalyses in the study of dental calculus showed that such studies provided confirmatory and supplementary data on the morphological features of human dental calculi but gave only limited information on the identity of the crystalline or inorganic components. This study aimed to explore the potential of combined SEM and microanalyses in the identification of the crystalline components of the human and animal dental calculi. Human and animal calculi were analyzed. Identification of the crystalline components were made based on the combined information of the morphology (SEM) and Ca/P molar ratios of the crystals with the morphology and Ca/P molar ratio of synthetic calcium phosphates (brushite or DCPD; octacalcium phosphate, OCP; Mg-substituted whitlockite, beta-TCMP; CO/sub 3/-substituted apatite, (CHA); and calcite. SEM showed similarities in morphological features of human and animal dental calculi but differences in the forms of crystals present. Microanalyses and crystal morphology data suggested the presence of CaCO/sub 3/ (calcite) and CHA in the animal (cat, dog, tiger) and of OCP, beta-TCMP and CHA in human dental calculi. X-ray diffraction and infrared (IR) absorption analyses confirmed these results. This exploratory study demonstrated that by taking into consideration what is known about the crystalline components of human and animal dental calculi, combined SEM and microanalyses can provide qualitative identification.

LeGeros, R.Z.; Orly, I.; LeGeros, J.P.; Gomez, C.; Kazimiroff, J.; Tarpley, T.; Kerebel, B.

1988-03-01T23:59:59.000Z

200

Complex modes and new amplification regimes in periodic multi transmission lines interacting with an electron beam  

E-Print Network (OSTI)

We show the existence of a new regime of operation for travelling wave tubes (TWTs) composed of slow-wave periodic structures that support two or more electromagnetic modes, with at least two synchronized with an electron beam. The interaction between the slow-wave structure and an electron beam is quantified using a multi transmission line approach (MTL) and transfer matrix analysis leading to the identification of modes with complex Bloch wavenumber. In particular, we report a new operation condition for TWTs based on an electron beam synchronous to two modes exhibiting a degeneracy condition near a band edge in a MTL slow-wave periodic structure. We show a phenomenological change in the band structure of periodic TWT where we observe at least two growing modal cooperating solutions as opposed to a uniform MTL interacting with an electron beam where there is strictly only one growing mode solution.

Othman, Mohamed; Capolino, Filippo

2014-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

Extension of Pierce model to multiple transmission lines interacting with an electron beam  

E-Print Network (OSTI)

A possible route towards achieving high power microwave devices is through the use of novel slow-wave structures employing multiple coupled transmission lines (MTLs) whose behavior when coupled to electron beams have not been sufficiently explored. We present the extension of the one-dimensional linearized Pierce theory to MTLs coupled to a single electron beam. We develop multiple formalisms to calculate the k-{\\omega} dispersion relation of the system and find that the existence of a growing wave solution is always guaranteed if the electron propagation constant is larger than or equal to the largest propagation constant of the MTL system. We verify our findings with illustrative examples which bring to light unique properties of the system in which growing waves were found to exist within finite bands of the electron propagation constant and discuss possible approach to improve the gain. By treating the beam-MTL interaction as distributed dependent current generators in the MTL, we derive relations charact...

Tamma, Venkata Ananth

2013-01-01T23:59:59.000Z

202

Chuaria circularis from the early Mesoproterozoic Suket Shale, Vindhyan Supergroup, India: Insights from light and electron microscopy and pyrolysis-gas chromatography  

Science Journals Connector (OSTI)

Chuaria circularis (Walcott 1899) from the Suket Shale of the Vindhyan Supergroup (central India) ... composition using biostatistics, electron microscopy and pyrolysis-gas chromatography. Morpho...

Suryendu Dutta; Michael Steiner; Santanu Banerjee…

2006-02-01T23:59:59.000Z

203

Low-temperature scanning tunneling microscopy and transport measurements on adsorbate-induced two-dimensional electron systems  

SciTech Connect

We have performed not only magnetotransport measurements on two-dimensional electron systems (2DESs) formed at the cleaved surfaces of p-InAs but also observations of the surface morphology of the adsorbate atoms, which induced the 2DES at the surfaces of narrow band-gap semiconductors, with use of a scanning tunneling microscopy. The electron density of the 2DESs is compared to the atomic density of the isolated Ag adatoms on InAs surfaces.

Masutomi, Ryuichi; Triyama, Naotaka; Okamoto, Tohru [Department of Physics, University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-0033 (Japan)

2013-12-04T23:59:59.000Z

204

Characterization of plutonium-bearing wastes by chemical analysis and analytical electron microscopy  

SciTech Connect

This report summarizes the results of characterization studies of plutonium-bearing wastes produced at the US Department of Energy weapons production facilities. Several different solid wastes were characterized, including incinerator ash and ash heels from Rocky Flats Plant and Los Alamos National Laboratory; sand, stag, and crucible waste from Hanford; and LECO crucibles from the Savannah River Site. These materials were characterized by chemical analysis and analytical electron microscopy. The results showed the presence of discrete PuO{sub 2}PuO{sub 2{minus}x}, and Pu{sub 4}O{sub 7} phases, of about 1{mu}m or less in size, in all of the samples examined. In addition, a number of amorphous phases were present that contained plutonium. In all the ash and ash heel samples examined, plutonium phases were found that were completely surrounded by silicate matrices. Consequently, to achieve optimum plutonium recovery in any chemical extraction process, extraction would have to be coupled with ultrafine grinding to average particle sizes of less than 1 {mu}m to liberate the plutonium from the surrounding inert matrix.

Behrens, R.G. [Los Alamos National Lab., NM (United States); Buck, E.C.; Dietz, N.L.; Bates, J.K.; Van Deventer, E.; Chaiko, D.J. [Argonne National Lab., IL (United States)

1995-09-01T23:59:59.000Z

205

Microwave Transmission Measurements of the Electron Cloud density In the Positron Ring of PEP-II  

SciTech Connect

Clouds of electrons in the vacuum chambers of accelerators of positively charged particle beams present a serious limitation for operation of these machines at high currents. Because of the size of these accelerators, it is difficult to probe the low energy electrons clouds over substantial lengths of the beam pipe. We applied a novel technique to directly measure the electron cloud density via the phase shift induced in a TE wave which is independently excited and transmitted over a straight section of the accelerator. The modulation in the wave transmission which appears to increase in depth when the clearing solenoids are switched off, seem to be directly correlated to the electron cloud density in the section. Furthermore, we expect a larger phase shift of a wave transmitted through magnetic dipole field regionsif the transmitted wave couples with the gyration motion of the electrons. We have used this technique to measure the average electron cloud density (ECD) specifically for the first time in magnetic field regions of a new 4-dipole chicane in the positron ring of the PEP-II collider at SLAC. In this paper we present and discuss the measurements taken in the Low Energy Ring (LER) between 2006 and 2008.

Pivi, Mauro T.F.; Krasnykh, Anatoly K.; Byrd, John; De Santis, Stefano; Sonnaad, Kiran G.; Caspers, Fritz; Kroyer, Tom

2008-06-18T23:59:59.000Z

206

In-situ Study of Dynamic Phenomena at Metal Nanosolder Interfaces Using Aberration Corrected Scanning Transmission Electron Microcopy.  

SciTech Connect

Controlling metallic nanoparticle (NP) interactions plays a vital role in the development of new joining techniques (nanosolder) that bond at lower processing temperatures but remain viable at higher temperatures. The pr imary objective of this project is t o develop a fundamental understanding of the actual reaction processes, associated atomic mechanisms, and the resulting microstructure that occur during thermally - driven bond formation concerning metal - metal nano - scale (<50nm) interfaces. In this LDRD pr oject, we have studied metallic NPs interaction at the elevated temperatures by combining in - situ transmission electron microscopy (TEM ) using an aberration - corrected scanning transmission electron microscope (AC - STEM) and atomic - scale modeling such as m olecular dynamic (MD) simulations. Various metallic NPs such as Ag, Cu and Au are synthesized by chemical routines. Numerous in - situ e xperiments were carried out with focus of the research on study of Ag - Cu system. For the first time, using in - situ STEM he ating experiments , we directly observed t he formation of a 3 - dimensional (3 - D) epitaxial Cu - Ag core - shell nanoparticle during the thermal interaction of Cu and Ag NPs at elevated temperatures (150 - 300 o C). The reaction takes place at temperatures as low as 150 o C and was only observed when care was taken to circumvent the effects of electron beam irradiation during STEM imaging. Atomic - scale modeling verified that the Cu - Ag core - shell structure is energetically favored, and indicated that this phenomenon is a nano - scale effect related to the large surface - to - volume ratio of the NPs. The observation potentially can be used for developing new nanosolder technology that uses Ag shell as the %22glue%22 that stic ks the particles of Cu together. The LDRD has led to several journal publications and numerous conference presentations, and a TA. In addition, we have developed new TEM characterization techniques and phase - field modeling tools that can be used for future materials research at Sandia. Acknowledgeme nts This work was supported by the Laboratory Directed Research and Development (LDRD) program of Sandia National Laboratories. Sandia National Laboratories is a multi - program laboratory managed and operated by Sandia Corporation, a wholly owned subsidia ry of Lockheed Martin Corporation, for the US Department of Energy's National Nuclear Security Administration under contract DE - AC04 - 94AL85000.

Lu, Ping

2014-10-01T23:59:59.000Z

207

Measurement of vibrational spectrum of liquid using monochromated scanning transmission electron microscopy–electron energy loss spectroscopy  

Science Journals Connector (OSTI)

......application to lithium-ion battery and hence has been well studied...Atom-by-atom spectroscopy at graphene edge. Nature (2010) 468...temperature molten salts as lithium battery electrolyte. Electrochim...additive systems as lithium-ion battery ionic liquid electrolytes......

Tomohiro Miyata; Mao Fukuyama; Akihide Hibara; Eiji Okunishi; Masaki Mukai; Teruyasu Mizoguchi

2014-10-01T23:59:59.000Z

208

SCANNING ELECTRON MICROSCOPY AND X-RAY DIFFRACTION ANALYSIS OF TANK 18 SAMPLES  

SciTech Connect

The F-Area Tank Farm (FTF) Performance Assessment (PA) utilizes waste speciation in the waste release model used in the FTF fate and transport modeling. The waste release modeling associated with the residual plutonium in Tank 18 has been identified as a primary contributor to the Tank 18 dose uncertainty. In order to reduce the uncertainty related to plutonium in Tank 18, a better understanding of the plutonium speciation in the Tank 18 waste (including the oxidation state and stoichiometry) is desired. Savannah River National Laboratory (SRNL) utilized Scanning Electron Microscopy (SEM) and X-ray Diffraction (XRD) to analyze Tank 18 samples to provide information on the speciation of plutonium in the waste material. XRD analysis of the Tank 18 samples did not identify any plutonium mineral phases in the samples. These indicates the crystalline mineral phases of plutonium are below the detection limits of the XRD method or that the plutonium phase(s) lack long range order and are present as amorphous or microcrystalline solids. SEM analysis of the Tank 18 samples did locate particles containing plutonium. The plutonium was found as small particles, usually <1 {micro}m but ranging up to several micrometers in diameter, associated with particles of an iron matrix and at low concentration in other elemental matrices. This suggests the plutonium has an affinity for the iron matrix. Qualitatively, the particles of plutonium found in the SEM analysis do not appear to account for all of the plutonium in the sample based on concentrations determined from the chemical analysis of the Tank 18 samples. This suggests that plutonium is also distributed throughout the solids in low concentrations.

Hay, M.; O'Rourke, P.; Ajo, H.

2012-03-08T23:59:59.000Z

209

Electronic properties of the Ga vacancy in GaP(110) surfaces determined by scanning tunneling microscopy  

Science Journals Connector (OSTI)

The electronic properties of uncharged Ga monovacancies in GaP(110) surfaces are determined from voltage-dependent scanning tunneling microscopy images. The signatures of localized defect states in the band gap are analyzed and their spatial location is determined. Empty and occupied defect states exist. Depressed dangling bonds in the occupied-state images indicate an inward relaxation of the neighboring P atoms. The results agree with recent theoretical work.

Ph. Ebert and K. Urban

1998-07-15T23:59:59.000Z

210

Demonstration of Ballistic Electron Emission Microscopy / Spectroscopy on the Au/Si (001) system  

E-Print Network (OSTI)

microscopy; hence, the analytical capabilities of BEEM are on a manometer scale. To use BEEM, low-noise Au/Si (001) Schottky diodes have been fabricated. The diodes were macroscopically tested for their electrical properties using conventional current...

Drummond, Mary Alyssa

2012-06-07T23:59:59.000Z

211

E-Print Network 3.0 - analytical transmission electron Sample...  

NLE Websites -- All DOE Office Websites (Extended Search)

through a Slit Aperture E... ) We demonstrate optical control over the transmission of terahertz (THz) radiation through a single... can contribute to the transmission. A...

212

In situ electron microscopy study of growth of WO3 and MoO3 nanowhiskers  

Science Journals Connector (OSTI)

WO3 and MoO3 nanowhiskers were grown from nanosize WO3 and MoO3 powders intensely irradiated with electrons in an electron microscope. Solid and hollow nanowhiskers of these materials were observed. A growth mech...

1 R. T. Malkhasyan; R. K. Karakhanyan; M. N. Nazaryan…

2003-05-01T23:59:59.000Z

213

Electron holographic mapping of two-dimensional doping areas in cross-sectional device specimens prepared by the lift-out technique based on a focused ion beam  

Science Journals Connector (OSTI)

................................... 8 Overwijk MHF, vanden Heuvel FC, and Bulle-Lieuwma CWT(1993) Novel scheme for the preparation of transmission electron microscopy......

Zhou-Guang Wang; Naoko Kato; Katsuhiro Sasaki; Tsukasa Hirayama; Hiroyasu Saka

2004-04-01T23:59:59.000Z

214

Application of electron microscopy and x-ray structural analysis for the determination of sizes of structural elements in nanocrystalline materials (Review)  

Science Journals Connector (OSTI)

The possibilities of determining the sizes of structural elements in various nanocrystalline materials by electron microscopy and X-ray structural analysis are analyzed. It is shown that these sizes depend on ...

Yu. D. Yagodkin; S. V. Dobatkin

2008-12-01T23:59:59.000Z

215

High precision two-dimensional strain mapping in semiconductor devices using nanobeam electron diffraction in the transmission electron microscope  

SciTech Connect

A classical method used to characterize the strain in modern semiconductor devices is nanobeam diffraction (NBD) in the transmission electron microscope. One challenge for this method lies in the fact that the smaller the beam becomes, the more difficult it becomes to analyze the resulting diffraction spot pattern. We show that a carefully designed fitting algorithm enables us to reduce the sampling area for the diffraction patterns on the camera chip dramatically (?1/16) compared to traditional settings without significant loss of precision. The resulting lower magnification of the spot pattern permits the presence of an annular dark field detector, which in turn makes the recording of images for drift correction during NBD acquisition possible. Thus, the reduced sampling size allows acquisition of drift corrected NBD 2D strain maps of up to 3000 pixels while maintaining a precision of better than 0.07%. As an example, we show NBD strain maps of a modern field effect transistor (FET) device. A special filtering feature used in the analysis makes it is possible to measure strain in silicon devices even in the presence of other crystalline materials covering the probed area, which is important for the characterization of the next generation of devices (Fin-FETs).

Baumann, Frieder H., E-mail: fhbauman@us.ibm.com [IBM Microelectronics Division, 2070 Route 52, Hopewell Junction, New York 12533 (United States)

2014-06-30T23:59:59.000Z

216

The Engineering Analysis in Support of the ITER Electron Cyclotron Heating and Current Drive Transmission Lines  

Science Journals Connector (OSTI)

Technical Paper / Sixteenth Joint Workshop on Electron Cyclotron Emission and Electron Cyclotron Resonance Heating (EC-16)

D. M. S. Ronden; M. A. Henderson; B. Becket; T. Bigelow; J. Caughman; C. Darbos; F. Gandini; C. Nazare; D. Rasmussen; V. Udintsev

217

Reflection Electron Microscopy and Spectroscopy for Surface Analysis Georgia Institute of Technology  

E-Print Network (OSTI)

.4 Fourier transformation 1.5 Scattering factor and charge density function 1.6 Single scattering theory 1 Historical background Scope of the book Chapter 1. Kinematical electron diffraction 1.1 Electron wavelength 1.7 Reciprocal space and reciprocal lattice vector 1.8 Bragg's law and Ewald sphere 1.9 Abbe's imaging theory 1

Wang, Zhong L.

218

The Thirty-fifth Annual Meeting of the Japanese Society of Electron Microscopy  

Science Journals Connector (OSTI)

......ment of a magnetic sector type electron energy...Ltd., Kyoto Design, construction and performance test...qhtp) by further heating with the stronger electron...and c = 30.1 A. The space group of the crystal...the model in which the construction rule on the U-W connection......

The Thirty-fifth Annual Meeting of the Japanese Society of Electron Microscopy

1979-01-01T23:59:59.000Z

219

The Thirty-seventh Annual Meeting of the Japanese Society of Electron Microscopy  

Science Journals Connector (OSTI)

......beam from a hairpin cathode electron gun. A...fer- romagnetic materials I. Magnetic domain...Geoclemmys in an active state, small specific...electron-translucent material (Type II), were...Japan and **Tokyo Cathode Lab. Co., Ltd...and fuel cladding material due to thermal and......

Morris J. KARNOVSKY

1981-01-01T23:59:59.000Z

220

Understanding Atom Probe Tomography of Oxide-Supported Metal Nanoparticles by Correlation with Atomic Resolution Electron Microscopy and Field Evaporation Simulation  

SciTech Connect

Metal-dielectric composite materials, specifically metal nanoparticles supported on or embedded in metal oxides, are widely used in catalysis. The accurate optimization of such nanostructures warrants the need for detailed three-dimensional characterization. Atom probe tomography is uniquely capable of generating sub-nanometer structural and compositional data with part-per-million mass sensitivity, but there are reconstruction artifacts for composites containing materials with strongly differing fields of evaporation, as for oxide-supported metal nanoparticles. By correlating atom probe tomography with scanning transmission electron microscopy for Au nanoparticles embedded in an MgO support, deviations from an ideal topography during evaporation are demonstrated directly, and correlated with compositional errors in the reconstructed data. Finite element simulations of the field evaporation process confirm that protruding Au nanoparticles will evolve on the tip surface, and that evaporation field variations lead to an inaccurate assessment of the local composition, effectively lowering the spatial resolution of the final reconstructed dataset. Cross-correlating the experimental data with simulations results in a more detailed understanding of local evaporation aberrations during APT analysis of metal-oxide composites, paving the way towards a more accurate three-dimensional characterization of this technologically important class of materials.

Devaraj, Arun; Colby, Robert J.; Vurpillot, F.; Thevuthasan, Suntharampillai

2014-03-26T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

A Laves phase-body-centered cubic structural relationship determined using high voltage electron microscopy  

SciTech Connect

High energy electron and ion irradiation of a TiCr{sub 2} Laves compound were found previously to result in a transformation to a body-centered cubic (bcc) solid solution. In the case of electron irradiation, the precipitating bcc phase exhibits preferential crystallographic orientation with respect to the initial compound crystal for irradiation temperatures above 200 K. This article presents an analysis of the electron diffraction data gathered in the course of the electron irradiation-induced Laves phase to bcc transformation in TiCr{sub 2}. A structural relationship between the bcc and Laves compound crystal lattices is determined which can account for all observations of preferentially oriented bcc precipitates. The significance of this mechanism for transformations between bcc and the Laves phases is discussed. In addition, the possible significance for deformation mechanisms of the Laves compounds is explored.

Sinkler, W. [GKSS Forschungszentrum, Geesthacht (Germany). Inst. fuer Werkstofforschung] [GKSS Forschungszentrum, Geesthacht (Germany). Inst. fuer Werkstofforschung

1996-04-01T23:59:59.000Z

222

Electron microscopy of GaAs/AlGaAs quantum cascade laser  

Science Journals Connector (OSTI)

The quantum cascade laser (QCL) is based on a different principle comparing to bipolar semiconductor lasers, because it uses only one type of ... — electrons and therefore is called an unipolar laser.

A. ?aszcz; J. Ratajczak; A. Czerwinski…

2008-01-01T23:59:59.000Z

223

VOLUME 71, NUMBER 21 PH YSICAL R EV I EW LETTERS 22 NOVEMBER 1993 Structure of Si(100)-(2 x 1) Surface Using UHV Transmission Electron Diffraction  

E-Print Network (OSTI)

) Surface Using UHV Transmission Electron Diffraction Ganesh Jayaram, P. Xu, and L. D. Marks Department) Details of the atomic structure for the Si(100)-(2X1) surface using UHV transmission electron diffraction]), ultrahigh vacuum (UHV) conditions are therefore paramount. In this Letter, we present details

Marks, Laurence D.

224

The Reactivity and Structural Dynamics of Supported Metal Nanoclusters Using Electron Microscopy, in situ X-Ray Spectroscopy, Electronic Structure Theories, and Molecular Dynamics Simulations.  

SciTech Connect

The distinguishing feature of our collaborative program of study is the focus it brings to emergent phenomena originating from the unique structural/electronic environments found in nanoscale materials. We exploit and develop frontier methods of atomic-scale materials characterization based on electron microscopy (Yang) and synchrotron X-ray absorption spectroscopy (Frenkel) that are in turn coupled innately with advanced first principles theory and methods of computational modeling (Johnson). In the past year we have made significant experimental advances that have led to important new understandings of the structural dynamics of what are unquestionably the most important classes of heterogeneous catalysts—the materials used to both produce and mitigate the consequences of the use of liquid hydrocarbon fuels.

Judith C. Yang; Ralph G. Nuzzo, Duane Johnson, Anatoly Frenkel

2008-07-01T23:59:59.000Z

225

The Thirty-seventh Annual Meeting of the Japanese Society of Electron Microscopy  

Science Journals Connector (OSTI)

......of metals such as Ta, Zr, Hf, Nb and Ti. As a hydrocarbon...was examined from electron, laser and computer diffrac- tograms...TEM findings disclosed the fusion of PC with MGC in as- sociation...cholesterol during mem- brane fusion at early stage of exocytosis......

Morris J. KARNOVSKY

1981-01-01T23:59:59.000Z

226

The Forty-sixth Annual Meeting of the Japanese Society of Electron Microscopy  

Science Journals Connector (OSTI)

......completed, specimens are trimed with an air turbine bur or a dianond disk in a cold buffer...been developed to improve the detection efficiency. Needless to say, hard X-ray apertures...detection of DQE%1 is realized. 3)High efficiency collection of elastically scattered electrons......

Harunori ISHIKAWA

1990-08-01T23:59:59.000Z

227

The Forty-sixth Annual Meeting of the Japanese Society of Electron Microscopy  

Science Journals Connector (OSTI)

......possible roles in nuclear events. 17a-B-MSl...membrane. 17a-B-MS2 Energy distribution of electron...K1r1tan1 Department of Nuclear Engineering, School...defects, 3) Threshold energy for displacement...Klnoshita, Department of Nuclear Engineering, Kyushu...the effect of low energy primary knock-on......

Harunori ISHIKAWA

1990-08-01T23:59:59.000Z

228

THE THIRTY-THIRD ANNUAL MEETING OF THE JAPANESE SOCIETY OF ELECTRON MICROSCOPY:  

Science Journals Connector (OSTI)

......seen between the lamellae of the inner bulb. Axons were directly invested with collagenous...were found among them. These findings led us to conclude that efferent nerve fibers...influence of reflected electrons, a non- fluorescent acrylic sheet was stuck on the receiving......

The Thirty-third Annual Meeting of the Japanese Society of Electron Microscopy

1977-01-01T23:59:59.000Z

229

The Thirty-seventh Annual Meeting of the Japanese Society of Electron Microscopy  

Science Journals Connector (OSTI)

......stain and weakly posi- tive in PAS, Sudan B and Luxol Fast Blue. Electron microscopically...type. In these experiments, in situ thermal stability of dislocations, phase transformation...fuel and fuel cladding material due to thermal and fast neutrons. For obtaining examina......

Morris J. KARNOVSKY

1981-01-01T23:59:59.000Z

230

TWENTIETH SCIENTIFIC MEETING OF THE JAPANESE SOCIETY OF ELECTRON-MICROSCOPY:  

Science Journals Connector (OSTI)

......two hours after incoulation elementary bodies 0.3-0.5/* in...similar to viral replication. Elementary bodies seem to result from...membrane has a high degree of resistance against electron bom- bardment...Shinagawa-ku Tokyo There are electric-chemical and physical-chemi......

Twentieth Scientific Meeting of the Japanese Society of Electron-Microscopy: Held at Tokushima University; May 16; 17; 1964

1964-01-01T23:59:59.000Z

231

Development of the program EOD for design in electron and ion microscopy  

Science Journals Connector (OSTI)

The paper surveys new features of the EOD program, a complete workplace for the design of electron and ion microscopes. The extensions of the program for space charge computations, interaction with gases in the specimen chamber and misalignments are handled as plug-ins, keeping the program as a single unit. The current status of the tolerancing plug-in is described in more detail.

J. Zlámal; B. Lencová

2011-01-01T23:59:59.000Z

232

Analytical electron microscopy examination of solid reaction products in long-term test of SRL 200 waste glasses  

SciTech Connect

Alteration phases, found on the leached surfaces and present as colloids in the leachates of 200-based frit (fully active and simulated) nuclear waste glass, reacted under static test conditions, at a surface area to leachate volume ratio of 20,000 m{sup {minus}1} for 15 days to 728 days, have been examined by analytical electron microscopy. The compositions of the secondary phases were determined using x-ray energy dispersive spectroscopy and electron energy loss spectroscopy, and structural analysis was accomplished by electron diffraction. Long-term samples of simulated glass, which had undergone an acceleration of reaction after 182 days, possessed a number of silicate secondary phases, including; smectite (iron silicate and potassium iron alumina-silicate, weeksite (uranium silicate), zeolite (calcium potassium alumino-silicate), tobermorite (calcium silicate), and a pure silica phase. However, uranium silicates and smectite have also been observed in tests, which have not undergone the acceleration of reaction, in both the leachate and leached layer, suggesting that these phases are not responsible for the acceleration of reaction.

Buck, E.C.; Fortner, J.A.; Bates, J.K.; Feng, X.; Dietz, N.L.; Bradley, C.R.; Tani, B.S.

1993-12-31T23:59:59.000Z

233

EMSL: Capabilities: Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Microscopy Microscopy Additional Information Meet the Microscopy Experts Related EMSL User Projects Microscopy Tools are Applied to all Science Themes Watch the Microscopy capability video on EMSL's YouTube channel and read the transcript. Microscopy brochure Quiet Wing brochure EMSL hosts a variety of sophisticated microscopy instruments, including electron microscopes, optical microscopes, scanning probe microscopes, and computer-controlled microscopes for automated particle analysis. These tools are used to image a range of sample types with nanoscale-and even atomic-resolution with applications to surface, environmental, biogeochemical, atmospheric, and biological science. Each state-of-the-art instrument and customized capability is equipped with features for specific

234

Using Synchrotron Radiation and Electron Microscopy to Map the Huge Structural Changes that Occur in Viruses During Their Life Cycle  

SciTech Connect

The crystallographic techniques for structure determination of proteins and neucleic acids at near atomic resolution using synchrotron X-radiation has become almost automatic. However the limits of this procedure are determined by the availability of crystals. As the size and complexity of the molecular assemblies being studied increases, the likelihood of growing useful crystals diminishes. Cryo electron microscopy and tomography have extended the range of biological objects that can be determined at near atomic resolution. Furthermore it is now becoming apparent that the function of the molecular assemblies most often requires very large conformational changes that could never be contained within a crystal, Examples will be presented of the structural changes that occur in viruses as they assembly and prepare to infect new cells.

Rossman, Michael (Purdue University) [Purdue University

2011-09-07T23:59:59.000Z

235

Comparison of SOFC Cathode Microstructure Quantified using X-ray Nanotomography and Focused Ion Beam - Scanning Electron Microscopy  

SciTech Connect

X-ray nanotomography and focused ion beam scanning electron microscopy (FIB?SEM) have been applied to investigate the complex 3D microstructure of solid oxide fuel cell (SOFC) electrodes at spatial resolutions of 45 nm and below. The application of near edge differential absorption for x-ray nanotomography and energy selected backscatter detection for FIB–SEM enable elemental mapping within the microstructure. Using these methods, non?destructive 3D x-ray imaging and FIB–SEM serial sectioning have been applied to compare three?dimensional elemental mapping of the LSM, YSZ, and pore phases in the SOFC cathode microstructure. The microstructural characterization of an SOFC cathode is reported based on these measurements. The results presented demonstrate the viability of x-ray nanotomography as a quantitative characterization technique and provide key insights into the SOFC cathode microstructure.

Nelson, George J.; Harris, William H.; Lombardo, Jeffrey J.; Izzo, Jr., John R.; Chiu, W. K. S.; Tanasini, Pietro; cantoni, Marco; Van herle, Jan; Comninellis, Christos; Andrews, Joy C.; Liu, Yijin; Pianetta, Piero; Chu, Yong

2011-01-01T23:59:59.000Z

236

In-situ and ex-situ observations of lithium de-intercalation from LiCoO? : atomic force microscopy and transmission electron microscopy studies  

E-Print Network (OSTI)

Lithium cobalt dioxide is the most commonly used material for positive electrodes in lithium rechargeable batteries. During lithium de-intercalation from this material, ... undergoes a number of phase transitions, which ...

Clémençon, Anne

2005-01-01T23:59:59.000Z

237

The TE Wave Transmission Method for Electron Cloud Measurements at Cesr-TA  

E-Print Network (OSTI)

CLOUD MEASUREMENTS AT CESR-TA* S. De Santis # , J. Byrd,Wave measurements at the Cesr-TA ring at Cornell University.CBP-836 THE TE WAVE TRANSMISSION METHOD FOR

Desantis, S.

2010-01-01T23:59:59.000Z

238

TRANSMISSION ELECTRON MICROSCOPY ANALYSIS OF A PRESOLAR SPINEL GRAIN. T. J. Ze-, C. M. O'D. Alexander2  

E-Print Network (OSTI)

Federal Reserve Bank of Boston Fidelity Investments First Wind Forest Laboratories, Inc. General Electric Company General Mills Hasbro, Inc. Houghton Mifflin Harcourt IBM Global Services Johnson & Johnson Jones

Nittler, Larry R.

239

In-Situ Transmission Electron Microscopy Probing of Native Oxide and Artificial Layers on Silicon Nanoparticles for Lithium Ion Batteries  

SciTech Connect

Surface modification of silicon nanoparticle via molecular layer deposition (MLD) has been recently proved to be an effective way for dramatically enhancing the cyclic performance in lithium ion batteries. However, the fundamental mechanism as how this thin layer of coating function is not known, which is even complicated by the inevitable presence of native oxide of several nanometers on the silicon nanoparticle. Using in-situ TEM, we probed in detail the structural and chemical evolution of both uncoated and coated silicon particles upon cyclic lithiation/delithation. We discovered that upon initial lithiation, the native oxide layer converts to crystalline Li2O islands, which essentially increases the impedance on the particle, resulting in ineffective lithiation/delithiation, and therefore low coulombic efficiency. In contrast, the alucone MLD coated particles show extremely fast, thorough and highly reversible lithiation behaviors, which are clarified to be associated with the mechanical flexibility and fast Li+/e- conductivity of the alucone coating. Surprisingly, the alucone MLD coating process chemically changes the silicon surface, essentially removing the native oxide layer and therefore mitigates side reaction and detrimental effects of the native oxide. This study provides a vivid picture of how the MLD coating works to enhance the coulombic efficiency and preserve capacity and clarifies the role of the native oxide on silicon nanoparticles during cyclic lithiation and delithiation. More broadly, this work also demonstrated that the effect of the subtle chemical modification of the surface during the coating process may be of equal importance as the coating layer itself.

He, Yang; Piper, Daniela M.; Gu, Meng; Travis, Jonathan J.; George, Steven M.; Lee, Se-Hee; Genc, Arda; Pullan, Lee; Liu, Jun; Mao, Scott X.; Zhang, Jiguang; Ban, Chunmei; Wang, Chong M.

2014-10-27T23:59:59.000Z

240

Phase identifications in crud from commercial boiling-water reactors at the Idaho National Laboratory by transmission electron microscopy  

SciTech Connect

Summarizes results of two studies of "crud" at the INL. All data is from INL/EXT-06-11742 and INL/JOU-06-11507 and has been previously released for publication.

Dawn E. Janney; Douglas L. Porter; Joshua L. Peterson

2007-09-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

Bioactivity and the First Transmission Electron Microscopy Immunogold Studies of Short De Novo-Designed Antimicrobial Peptides  

Science Journals Connector (OSTI)

...peptide was recovered via vacuum filtration through a...from each sample was vacuum centrifuged overnight...Vacufuge 5301 centrifugal vacuum concentrator. Peptide...CD spectroscopy and 1H nuclear magnetic resonance...filled with LR White-accelerator solution (2 drops of...

Marisa Ann Azad; Heidi Esther Katrina Huttunen-Hennelly; Cynthia Ross Friedman

2011-02-07T23:59:59.000Z

242

Single-particle cryo-electron microscopy of Rift Valley fever virus  

SciTech Connect

Rift Valley fever virus (RVFV; Bunyaviridae; Phlebovirus) is an emerging human and veterinary pathogen causing acute hepatitis in ruminants and has the potential to cause hemorrhagic fever in humans. We report a three-dimensional reconstruction of RVFV vaccine strain MP-12 (RVFV MP-12) by cryo-electron microcopy using icosahedral symmetry of individual virions. Although the genomic core of RVFV MP-12 is apparently poorly ordered, the glycoproteins on the virus surface are highly symmetric and arranged on a T = 12 icosahedral lattice. Our RVFV MP-12 structure allowed clear identification of inter-capsomer contacts and definition of possible glycoprotein arrangements within capsomers. This structure provides a detailed model for phleboviruses, opens new avenues for high-resolution structural studies of the bunyavirus family, and aids the design of antiviral diagnostics and effective subunit vaccines.

Sherman, Michael B. [Department of Biochemistry and Molecular Biology, University of Texas Medical Branch, Galveston, TX 77555 (United States); Sealy Center for Structural Biology and Molecular Biophysics, University of Texas Medical Branch, Galveston, TX 77555 (United States); Freiberg, Alexander N. [Department of Pathology, University of Texas Medical Branch, Galveston, TX 77555 (United States); Center for Biodefense and Emerging Infectious Diseases, University of Texas Medical Branch, Galveston, TX 77555 (United States); Holbrook, Michael R. [Department of Pathology, University of Texas Medical Branch, Galveston, TX 77555 (United States); Center for Biodefense and Emerging Infectious Diseases, University of Texas Medical Branch, Galveston, TX 77555 (United States); Institute for Human Infections and Immunity, University of Texas Medical Branch, Galveston, TX 77555 (United States); Watowich, Stanley J., E-mail: watowich@xray.utmb.ed [Department of Biochemistry and Molecular Biology, University of Texas Medical Branch, Galveston, TX 77555 (United States); Sealy Center for Structural Biology and Molecular Biophysics, University of Texas Medical Branch, Galveston, TX 77555 (United States); Center for Biodefense and Emerging Infectious Diseases, University of Texas Medical Branch, Galveston, TX 77555 (United States); Institute for Human Infections and Immunity, University of Texas Medical Branch, Galveston, TX 77555 (United States)

2009-04-25T23:59:59.000Z

243

Radiation damage of polyethylene single crystals in electron microscopy between 1 and 2.5 MV. II. The influence of temperature  

E-Print Network (OSTI)

1043 Radiation damage of polyethylene single crystals in electron microscopy between 1 and 2.5 MV mécanismes réels décrits par les chimistes. Abstract. 2014 The critical dose measured for polyethylene single. Introduction. Polyethylene single crystals, like every organic sub- stance, lose their crystallinity when

Paris-Sud XI, Université de

244

Profile of Professor of High-Resolution Electron Microscopy for Nanomaterials in the Quantum Nanoscience department (Kavli Institute, faculty of Applied Sciences)  

E-Print Network (OSTI)

Nanoscience department (Kavli Institute, faculty of Applied Sciences) Workload and duration The Quantum Nanoscience department is planning to appoint a permanent full-time professor in the research area of High the High-Resolution Electron Microscopy (HREM) group in the Quantum Nanoscience department at TU Delft

245

Electron Microscopy Study of Novel Ru Doped La0.8Sr0.2CrO3 as Anode Materials for Solid Oxide Fuel Cells (SOFCs)  

E-Print Network (OSTI)

Electron Microscopy Study of Novel Ru Doped La0.8Sr0.2CrO3 as Anode Materials for Solid Oxide Fuel of Materials Science and Engineering, Northwestern University, 2220 Campus Dr. Evanston, IL 60208 Solid Oxide Fuel Cells (SOFCs) have been the center of research activities with the goal of improving energy

Marks, Laurence D.

246

Development of a user-friendly system for image processing of electron microscopy by integrating a web browser and PIONE with Eos  

Science Journals Connector (OSTI)

......of electron microscopy by integrating a web browser and PIONE with Eos Takafumi Tsukamoto...expert for CUI. Thus we extended Eos to a web system independent of OS with graphical user interfaces (GUI) by integrating web browser. Advantage to use web browser is......

Takafumi Tsukamoto; Takuo Yasunaga

2014-11-01T23:59:59.000Z

247

High resolution, high speed ultrahigh vacuum microscopy  

SciTech Connect

The history and future of transmission electron microscopy (TEM) is discussed as it refers to the eventual development of instruments and techniques applicable to the real time in situ investigation of surface processes with high resolution. To reach this objective, it was necessary to transform conventional high resolution instruments so that an ultrahigh vacuum (UHV) environment at the sample site was created, that access to the sample by various in situ sample modification procedures was provided, and that in situ sample exchanges with other integrated surface analytical systems became possible. Furthermore, high resolution image acquisition systems had to be developed to take advantage of the high speed imaging capabilities of projection imaging microscopes. These changes to conventional electron microscopy and its uses were slowly realized in a few international laboratories over a period of almost 40 years by a relatively small number of researchers crucially interested in advancing the state of the art of electron microscopy and its applications to diverse areas of interest; often concentrating on the nucleation, growth, and properties of thin films on well defined material surfaces. A part of this review is dedicated to the recognition of the major contributions to surface and thin film science by these pioneers. Finally, some of the important current developments in aberration corrected electron optics and eventual adaptations to in situ UHV microscopy are discussed. As a result of all the path breaking developments that have led to today's highly sophisticated UHV-TEM systems, integrated fundamental studies are now possible that combine many traditional surface science approaches. Combined investigations to date have involved in situ and ex situ surface microscopies such as scanning tunneling microscopy/atomic force microscopy, scanning Auger microscopy, and photoemission electron microscopy, and area-integrating techniques such as x-ray photoelectron spectroscopy, ultraviolet photoelectron spectroscopy, Auger electron spectroscopy, low-energy electron diffraction, temperature programmed desorption, high-resolution electron energy-loss and Fourier-transform infrared spectroscopies, and others. Material systems ranging from atomic layers of metals and semiconductors to biology related depositions are being investigated. In the case of biological materials, however, strict limitations to high-resolution applications are imposed by electron radiation damage considerations.

Poppa, Helmut [National Center for Electron Microscopy, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States)

2004-09-01T23:59:59.000Z

248

Transmission-mode imaging in the environmental scanning electron microscope (ESEM)  

E-Print Network (OSTI)

sources function by heating a material until it starts to emit electrons (by increasing the energy of free electrons to above the Fermi surface of the material) and field-emission sources function by applying an electric field strong enough that electrons... obtained from studying E. coli, C. necator, and S. Typhimurium (Chapter 8) have been accepted for publication in Scanning, titled “The application of STEM and in-situ controlled dehydration to bac- terial systems using ESEM”. i Acknowledgements This project...

Staniewicz, Lech Thomas Leif

2012-02-07T23:59:59.000Z

249

Construction of the Magnetic Phase Diagram of FeMn/Ni/Cu(001) Using Photoemission Electron Microscopy  

SciTech Connect

Single crystalline FeMn/Ni bilayer was epitaxially grown on Cu(001) substrate and investigated by photoemission electron microscopy (PEEM). The FeMn and Ni films were grown into two cross wedges to facilitate an independent control of the FeMn (0-20 ML) and Ni (0-20 ML) film thicknesses. The Ni magnetic phases were determined by Ni domain images as a function of the Ni thickness (d{sub Ni}) and the FeMn thickness (d{sub FeMn}). The result shows that as the Ni thickness increases, the Ni film undergoes a paramagnetic-to-ferromagnetic state transition at a critical thickness of d{sub FM} and an in-plane to out-of-plane spin reorientation transition at a thicker thickness d{sub SRT}. The phase diagram shows that both d{sub FM} and d{sub SRT} increase as the FeMn film establishes its antiferromagnetic order.

Wu, J.; Scholl, A.; Arenholz, E.; Hwang, C.; Qiu, Z. Q.

2011-01-04T23:59:59.000Z

250

Investigation of metal dusting mechanism in Fe-base alloys using Raman spectroscopy, x-ray diffraction, and electron microscopy.  

SciTech Connect

The metal-dusting phenomenon, which is a metal loss process that occurs in hot reactive gases, was investigated in iron and certain iron-base alloys by Raman scattering, X-ray diffraction (XRD), and scanning-electron microscopy (SEM). Coke from metal dusting exhibits six Raman bands at 1330(D band), 1580(G band), 1617, 2685, 3920, and 3235 cm-1. The bandwidths and the relative intensities of the 1330 and 1580 cm-1 bands are related to the crystallinity and defect structure of the coke. Both Raman and XRD analyses suggest that the metal-dusting process influences the catalytic crystallization of carbon. A new mechanism of metal dusting is, therefore, proposed, based on the premise that coke cannot crystallize well by deposition from carburizing gases at low temperature without catalytic activation because of its strong C-C bonds and high melting temperature. Cementite or iron participates in the coke-crystallizing process in a manner that tends to improve the crystallinity of the coke. At the same time, fine iron or cementite particles are liberated from the pure metal or alloys.

Zeng, Z.; Natesan, K.; Maroni, V. A.

2002-08-01T23:59:59.000Z

251

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Publications Publications The publications listed below are based on work carried out in the EMC. Publication time period: October 1, 2009, through September 30, 2010 Published journal articles (refereed): C. An, S. Peng, Y. Sun, “Facile Synthesis of Sunlight-Driven Plasmonic AgCl:Ag Nanophotocatalysts," Adv. Mater. 22, 2570 (2010). S. Avci, Z. L. Xiao, J. Hua, A. Imre, R. Divan, J. Pearson, U. Welp, W. K. Kwok, and G. W. Crabtree, “Matching effect and dynamic phases of vortex matter in Bi2Sr2CaCu2O8 nanoribbon with a periodic array of holes,” Appl. Phys. Lett. 97, 042511 (2010). A. Belkin, V. Novosad, M. Iavarone, R. Divan, J. Hiller, T. Prolier, J. E. Pearson, and G. Karapetrov “Giant conductance anisotropy in magnetically coupled F/S/F structures,” Appl. Phys. Lett. 96, 092513 (2010)

252

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Proposal Access Guidelines Proposal Access Guidelines One part of the EMC mission is to provide unique instrumentation and expertise to the scientific community. Important to achieving this goal is the effective management of EMC instrumentation and staff for maximum scientific impact. Broad and fair access to these resources is achieved through a proposal review process and scheduling and access policies. The type of access granted is based on the nature of the proposed work, the qualifications of the user, and the instrumentation requested. Research projects may be allocated a specific amount of instrument time or may be granted continuous access. Allocated Access: Under allocated access, a user is allocated a specific amount of instrument time to complete the proposed project. Allocated access is utilized primarily to manage instrument time for those instruments that have very high demand and for projects that require exceptional staff assistance.

253

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Resources for EMC staff members Resources for EMC staff members Gain access to proposals and other records in the EMC proposal database There are two methods, and both require a username and password. You will have access to the following layouts: AEM Proposals for Tech Review, IVEM Proposals for Tech Review, Users' Data, and Technical Reviews. You will not be able to view Personally Identifiable Information (PII). Do not let EMC users access these layouts! Users are limited to submitting proposals via the guest login or editing their proposals via a temporary login given to them by the database administrator. The best method is to use FileMaker Pro. From the File menu, choose Open Remote, then the Host jude.cnm.anl.gov, and then the emc_proposal database. The second method is to use a web browser. The URL for the proposal database is https://pico.cnm.anl.gov/proposals. Login with your web username and password that you have received from the database administrator; these can be different from your FileMaker network login.

254

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

FEI Quanta 400F ESEM FEI Quanta 400F ESEM Instrument capabilities: Instrument specifications: Accelerating voltages: 2-30 kV Schottky FEG emitter SEI resolution (actual) at 30 kV: 3 nm at 1330 Pa; 10 nm at 2660 Pa Operating modes: SEI; BEI; specimen chamber pressures from high vacuum to 2660 Pa; various specimen chamber gases (air & water vapor standard; Ar, N2 and He also tested; other gases may be possible); XEDS (Be window – no elements below Na); telepresence. Specimen stage: 5-axis motorized Maximum sample size: 100 x 100 mm (XY) Heating (1770 K) Peltier-cooled (248 K to 328 K) Typical experiments (examples): Imaging of insulating/dielectric materials Imaging biomaterials and polymers at high water vapor pressures In situ materials processing XEDS mapping and spectrum imaging

255

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

(Purdue U.); X.-M. Lin (Argonne-CNM) Functionalized Aligned Carbon Nanotubes as Electrocatalyst for Fuel Cell Applications J. Yang (Argonne-CSE) Growth of Anisotropic Silver...

256

Electron Microscopy Center  

NLE Websites -- All DOE Office Websites (Extended Search)

Resources Resources The EMC currently operates and administers seven full-time user instruments together with support facilities that include specimen preparation, image analysis and computational resources. The instruments are grouped below according to their function and capabilities. Detailed information about the capabilities of each user-accessible resource is available via the underlined links below. The major-capability instruments are generally available by allocated access while the core instruments are generally available by continuous access. Instrument Access Type User Status Separate Proposal? ACAT Allocated Assisted yes IVEM Allocated Assisted yes FEI Tecnai F20ST TEM/STEM Continuous or Allocated User or Assisted Any or all of these instruments may be requested in one proposal.

257

Uranium-contaminated soils: Ultramicrotomy and electron beam analysis  

SciTech Connect

Uranium contaminated soils from the Fernald Operation Site, Ohio, have been examined by a combination of optical microscopy, scanning electron microscopy with backscattered electron detection (SEM/BSE), and analytical electron microscopy (AEM). A method is described for preparing of transmission electron microscopy (TEM) thin sections by ultramicrotomy. By using these thin sections, SEM and TEM images can be compared directly. Uranium was found in iron oxides, silicates (soddyite), phosphates (autunites), and fluorite. Little uranium was associated with clays. The distribution of uranium phases was found to be inhomogeneous at the microscopic level.

Buck, E.C.; Dietz, N.L.; Bates, J.K.; Cunnane, J.C.

1994-04-01T23:59:59.000Z

258

Novel Approaches to Soft X-ray Spectroscopy: Scanning TransmissionX-ray Microscopy and Ambient Pressure X-Ray PhotoelectronSpectroscopy  

SciTech Connect

This workshop focused on novel spectroscopies at Beamlines 11.0.2, 5.3.2 and 9.3.2 at the ALS. The workshop brought together users from a wide range of fields to highlight recent experimental and technical developments both in scanning transmission X-ray spectroscopy (STXM) and ambient pressure photoelectron spectroscopy (APPES). The morning session featured talks on experiments involving new developments at the STXM, while the afternoon session was devoted to those using APXPS. In the morning session, Tolek Tyliszczak discussed the improved detector developments at the STXM, such as an avalanche photodiode detector and fluorescence and electron detection, as well as the continued development of in situ cells for heating, gas flow, and electrochemical cells. Of these, only the avalanche photodiode in combination with a novel multichannel photon-counting system is in routine use in time-resolved studies. Bartel Van Waeyenberge (Ghent University) presented results of magnetic imaging with a time resolution of 70-100 ps combined with a lateral resolution of 20-40 nm performed with the STXM (Beamline 11.0.2). As a complement to the time-domain ''pump-and-probe'' measurements, they developed a frequency-domain ''sine-excitation'' technique in order to study specific eigenmodes of these ferromagnetic patterns with high spatial resolution. This new approach was used to study the gyrotropic vortex motions in micron-sized ferromagnetic patterns. Adam Hitchcock (McMaster University) presented the development, in collaboration with Daniel Guay (INRS, Varennes) and Sherry Zhang, of the apparatus and techniques for applying STXM to in-situ studies of electrochemistry, in particular electrochromism in polyaniline. In addition, substantial progress was reported on a joint project to develop substrates and methods for chemically selective lithography of multilayer polymer systems. Selective patterns, such as that displayed in the figure, can now be written efficiently with the bend magnet STXM on Beamline 5.3.2. Yves Acremann (SSRL) discussed time and spatially resolved X-ray magnetic circular dichroism (XMCD) experiments on spin transfer devices at the STXM (Beamline 11.0.2). These elegant experiments explore time resolved measurements of the magnetization dynamics within a 100 x 150 nm sample influenced by a spin-polarized current. This experiment shows that the magnetization in these magnetic nanostructures are not uniform, as they are influenced by the Oersted field of the charge current needed to generate the spin current. The implementation of a novel multichannel photon counting system in combination with an avalanche photon detector decreased the data-acquisition time by a factor of 10, owing to its ability to resolve the structure of multi bunch mode. Gordon E. Brown, Jr. (Stanford University and SSRL) described ''Applications of STXM to Microbial Bioweathering and Biomineralization''. In the interaction of bacteria with ferrihydrite nanoparticles, microenvironments that were very different than the bulk material were observed, showing that bulk thermodynamics may not be useful for predicting micro phases. Gordon also presented work showing that iron nanoparticles are attracted to the negatively charged bacteria and form a coating that reduces iron oxide minerals. The afternoon session started with presentations by Simon Mun and Hendrik Bluhm, who discussed the current status and the future plans for the two APPES end-stations at the ALS, which are located at Beamlines 9.3.2 and 11.0.2, respectively. In both end-stations, samples can be measured in gaseous environments at pressures of up to several Torr, which makes possible the investigation of numerous phenomena, in particular in the fields of atmospheric and environmental science as well as heterogeneous catalysis. Specific examples of the application of APPES were shown in the following presentations. John Hemminger (University of California, Irvine) reported on APPES investigations at Beamlines 9.3.2 and 11.0.2 of the interaction of alkali halide surfaces with water. The m

Bluhm, Hendrik; Gilles, Mary K.; Mun, Simon B.; Tyliszczak, Tolek

2006-02-01T23:59:59.000Z

259

Simulating realistic imaging conditions for in situ liquid microscopy  

SciTech Connect

In situ transmission electron microscopy enables the imaging of biological cells, macromolecular protein complexes, nanoparticles, and other systems in a near-native environment. In order to improve interpretation of image contrast features and also predict ideal imaging conditions ahead of time, new virtual electron microscopic techniques are needed. A technique for virtual fluid-stage high-angle annular dark-field scanning transmission electron microscopy with the multislice method is presented that enables the virtual imaging of model fluid-stage systems composed of millions of atoms. The virtual technique is exemplified by simulating images of PbS nanoparticles under different imaging conditions and the results agree with previous experimental findings. General insight is obtained on the influence of the effects of fluid path length, membrane thickness, nanoparticle position, defocus and other microscope parameters on attainable image quality.

Welch, David A.; Faller, Roland; Evans, James E.; Browning, Nigel D.

2013-12-01T23:59:59.000Z

260

IEEE ELECTRON DEVICE LETTERS, VOL. 30, NO. 5, MAY 2009 433 RF Transmission Line Method for  

E-Print Network (OSTI)

. Jain, J. Yang, X. Hu, and R. Gaska are with Sensor Electronic Technology, Inc., Columbia, SC 29209 USA model (TLM) technique, which em- ploys the C3 electrodes. The technique is applied Polytechnic Institute, Troy, NY 12180 USA (e-mail: shurm13@gmail.com). N. Pala was with Rensselaer Polytechnic

Pala, Nezih

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

Towards 0.1 nm resolution with the first spherically corrected transmission electron microscope  

Science Journals Connector (OSTI)

......defocus-modulation image processing. Ultramiaysco/y'41: 323-333. means of an appropriate monochromator. 24 Thust A, Overwijk M H, Coene W M J, and Lentzen M (1996) M. Haider et al. Corrected electron microscope 405 Numerical correction of lenaberrations......

Maximilian Haider; Herald Rose; Stephan Uhlemann; Bernd Kabius; Knut Urban

1998-01-01T23:59:59.000Z

262

Electron line shape and transmission function of the KATRIN monitor spectrometer  

SciTech Connect

Knowledge of the neutrino mass is of particular interest in modern neutrino physics. Besides the neutrinoless double beta decay and cosmological observation information about the neutrino mass is obtained from single beta decay by observing the shape of the electron spectrum near the endpoint. The KATRIN ? decay experiment aims to push the limit on the effective electron antineutrino mass down to 0.2 eV/c{sup 2}. To reach this sensitivity several systematic effects have to be under control. One of them is the fluctuations of the absolute energy scale, which therefore has to be continuously monitored at very high precision. This paper shortly describes KATRIN, the technique for continuous monitoring of the absolute energy scale and recent improvements in analysis of the monitoring data.

Slezák, M. [Faculty of Mathematics and Physics, Charles University, Ke Karlovu 3, 12116 Prague, Czech Republic and Nuclear Physics Institute, Academy of Sciences of the Czech Republic, Hlavní 130, 25068 ?ež (Czech Republic)

2013-12-30T23:59:59.000Z

263

High-power microwave transmission systems for electron-cyclotron-resonance plasma heating  

SciTech Connect

This progress report is for the sixth year of a grant from the US Department of Energy for the design, development, and fabrication of ECRH transmission and mode conversion systems to transport microwave power from a gyrotron to a magnetically confined plasma. The design and low-power testing of new and improved components for such systems and development of underlying theory is the focus of this project. Devising and improving component testing and diagnostic techniques is also an important part of this effort. The development of possible designs for sections of gyrotrons themselves, such as tapers or Vlasov-type launchers, in support of the Varian gyrotron development program is also considered when appropriate. We also provide support to other groups working on ECR heating of magnetically confined plasmas such as the groups at General Atomics, the University of Texas at Austin, and Lawrence Livermore National Laboratory. During the last year, we designed and had fabricated a two-dimensional Vlasov antenna system for a 110 GHz TE{sub 15,2} mode gyrotron for possible use at General Atomics. The system included the launcher section, a visor, main reflector, and focusing reflector. Programs to generate the tool-path profiles to cut the General Atomics'' Vlasov components on a milling machine were developed. We have also developed state-of-the art theory and programs for three-dimensional whispering-gallery-mode Vlasov antenna systems. A design for a 110 GHz TE{sub 01}-TE{sub 15,2} mode converter system for cold testing WGM Vlasov antenna systems was developed and is currently being fabricated also.

Vernon, R.J.

1991-08-01T23:59:59.000Z

264

3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone at the  

NLE Websites -- All DOE Office Websites (Extended Search)

3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone 3D View Inside the Skeleton with X-ray Microscopy: Imaging Bone at the Nanoscale Scientists studying osteoporosis and other skeletal diseases are interested in the 3D structure of bone and its responses to conditions such as weightlessness, radiation (of particular interest to astronauts) and vitamin D deficiency. The current gold standard, micro-computed tomography (micro-CT), provides 3D images of trabeculae, the small interior struts of bone tissue, and electron microscopy can provide nanometer resolution of thin tissue slices. Hard X-ray transmission microscopy has provided the first 3D view of bone structure within individual trabeculae on the nanoscale. figure 1 Figure 1 Micro-CT (left) shows trabecular structure inside of bone. Transmission X-ray microscopy (TXM; center and right) can reveal localized details of osteocyte lacunae and their processes.

265

Particularities of high-voltage electron microscopy: instrument design, defect imaging and in situ investigation in 'thick' specimens  

Science Journals Connector (OSTI)

......microscopy: instrument design, defect imaging and in situ investigation in 'thick' specimens Roger Valle1 and Alain Marraud2 'DMSC, ONERA, 29 Av. de la Division Leclerc, F-92322 Chatillon Cedex and 2 LMSSM, ECP, Grande Voie des Vignes, F-92295 Chatenay-Malabry......

Roger Valle; Alain Marraud

1999-01-01T23:59:59.000Z

266

Topography, complex refractive index, and conductivity of graphene layers measured by correlation of optical interference contrast, atomic force, and back scattered electron microscopy  

SciTech Connect

The optical phase shift by reflection on graphene is measured by interference contrast microscopy. The height profile across graphene layers on 300?nm thick SiO{sub 2} on silicon is derived from the phase profile. The complex refractive index and conductivity of graphene layers on silicon with 2?nm thin SiO{sub 2} are evaluated from a phase profile, while the height profile of the layers is measured by atomic force microscopy. It is observed that the conductivity measured on thin SiO{sub 2} is significantly greater than on thick SiO{sub 2}. Back scattered electron contrast of graphene layers is correlated to the height of graphene layers.

Vaupel, Matthias, E-mail: Matthias.vaupel@zeiss.com; Dutschke, Anke [Training Application Support Center, Carl Zeiss Microscopy GmbH, Königsallee 9-21, 37081 Göttingen (Germany); Wurstbauer, Ulrich; Pasupathy, Abhay [Department of Physics, Columbia University New York, 538 West 120th Street, New York, New York 10027 (United States); Hitzel, Frank [DME Nanotechnologie GmbH, Geysostr. 13, D-38106 Braunschweig (Germany)

2013-11-14T23:59:59.000Z

267

IEEE TRANSACTIONS ON ELECTRON DEVICES, VOL. 53, NO. 2, FEBRUARY 2006 235 De-Embedding Transmission Line Measurements for  

E-Print Network (OSTI)

of parasitic structures from transmission line measurements is presented and applied to microstrip lines technologies, integrated circuits, interconnect, losses, microstrip lines, slotted ground planes, transmission comparable to on-chip component dimensions. Hence, transmission lines play an in- creasingly vital role

Voinigescu, Sorin Petre

268

Abstract--The increase in use of power electronics in transmission and distribution applications is the driving  

E-Print Network (OSTI)

is the driving force for development of high power devices. Utility applications like FACTS and HVDC require cost and compared for SiC and Si devices. These loss models are integrated with an HVDC transmission system to study of the systems. High Voltage DC (HVDC) transmission and Flexible AC Transmission Systems (FACTS) are the widely

Tolbert, Leon M.

269

Microscopy. II. Electron Microscopy: A Review  

Science Journals Connector (OSTI)

...important role in regulation of energy metabolism and will be the subject...a P 0.001) are marked in dark gray. Light gray boxes indicate...translation factor eIF4E: a survey of its expression in breast...revealed marked up-regulation of energy, protein translation, and...

Cecily Cannan Selby

1953-11-01T23:59:59.000Z

270

Electron-microscopy study of the triple-q to single-q phase transition in the incommensurate phase of quartz under stress  

Science Journals Connector (OSTI)

The triple-q to single-q phase transition in quartz has been studied by electron microscopy using a heating straining device, stress being applied along the x axis. The interpretation of the experimental images obtained for small values of stress is in agreement with theoretical predictions. The presence of an intermediate state between the triple-q and single-q modulated phases has been observed for higher values of stress. It can be described as a double-q state where the two wave vectors are tilted from the y direction by an angle of +cphi and -cphi that decreases to 0 in the single-q stripe phase.

E. Snoeck and C. Roucau

1992-06-01T23:59:59.000Z

271

Development of a Silicon Based Electron Beam Transmission Window for Use in a KrF Excimer Laser System  

SciTech Connect

The Princeton Plasma Physics Laboratory (PPPL), in collaboration with the Naval Research Laboratory (NRL), is currently investigating various novel materials (single crystal silicon, <100>, <110> and <111>) for use as electron-beam transmission windows in a KrF excimer laser system. The primary function of the window is to isolate the active medium (excimer gas) from the excitation mechanism (field-emission diodes). Chosen window geometry must accommodate electron energy transfer greater than 80% (750 keV), while maintaining structural integrity during mechanical load (1.3 to 2.0 atm base pressure differential, approximate 0.5 atm cyclic pressure amplitude, 5 Hz repetition rate) and thermal load across the entire hibachi area (approximate 0.9 W {center_dot} cm superscript ''-2''). In addition, the window must be chemically resistant to attack by fluorine free-radicals (hydrofluoric acid, secondary). In accordance with these structural, functional, and operational parameters, a 22.4 mm square silicon prototype window, coated with 500 nm thin-film silicon nitride (Si{sub 3}N{sub 4}), has been fabricated. The window consists of 81 square panes with a thickness of 0.019 mm {+-} 0.001 mm. Stiffened (orthogonal) sections are 0.065 mm in width and 0.500 mm thick (approximate). Appended drawing (Figure 1) depicts the window configuration. Assessment of silicon (and silicon nitride) material properties and CAD modeling and analysis of the window design suggest that silicon may be a viable solution to inherent parameters and constraints.

C.A. Gentile; H.M. Fan; J.W. Hartfield; R.J. Hawryluk; F. Hegeler; P.J. Heitzenroeder; C.H. Jun; L.P. Ku; P.H. LaMarche; M.C. Myers; J.J. Parker; R.F. Parsells; M. Payen; S. Raftopoulos; J.D. Sethian

2002-11-21T23:59:59.000Z

272

Improvement of windowed type environmental-cell transmission electron microscope for in situ observation of gas-solid interactions  

SciTech Connect

We have developed an improved, windowed type environmental-cell (E-cell) transmission electron microscope (TEM) for in situ observation of gas-solid interactions, such as catalytic reactions at atmospheric pressure. Our E-cell TEM includes a compact E-cell specimen holder with mechanical stability, resulting in smoother introduction of the desired gases compared with previous E-cell TEMs. In addition, the gas control unit was simplified by omitting the pressure control function of the TEM pre-evacuation chamber. This simplification was due to the successful development of remarkably tough thin carbon films as the window material. These films, with a thickness of <10 nm, were found to withstand pressure differences >2 atm. Appropriate arrangement of the specimen position inside the E-cell provided quantitatively analyzable TEM images, with no disturbances caused by the windowed films. As an application, we used this E-cell TEM to observe the dynamic shape change in a catalytic gold nanoparticle supported on TiO{sub 2} during the oxidation of CO gas.

Kawasaki, Tadahiro [Graduate School of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya 464-8603 (Japan); PRESTO-JST, 4-1-8 Honcho, Kawaguchi, Saitama 332-0012 (Japan); Ueda, Kouta [Graduate School of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya 464-8603 (Japan); Ichihashi, Mikio; Tanji, Takayoshi [EcoTopia Science Institute, Nagoya University, Furo-cho, Chikusa-ku, Nagoya 464-8603 (Japan)

2009-11-15T23:59:59.000Z

273

Electron  

Science Journals Connector (OSTI)

Absolute grand total cross sections (TCSs) for electron-disilane (Si2H6) scattering have been measured over the energy range from 1 to 370 eV in a linear transmission experiment. The low-energy TCS is dominated by a broad resonant-like enhancement. In the region of the maximum the present grand TCS values appeared to be distinctly lower than previously reported integral elastic cross section data. A comparison of total electron scattering cross sections for the two simplest silicon hydrides and relevant hydrocarbons is given.

Czeslaw Szmytkowski; Pawel Mozejko; Grzegorz Kasperski

2001-01-01T23:59:59.000Z

274

Direct observation of the intergrown {alpha}-phase in {beta}-TmAlB{sub 4} via high-resolution electron microscopy  

SciTech Connect

A TmAlB{sub 4} crystal with a ThMoB{sub 4}-type ({beta}-type) structure phase related to a hexagonal AlB{sub 2}-type structure was studied by electron diffraction and high-resolution electron microscopy. A high-resolution image clearly exhibits an intergrown lamellar structure of a YCrB{sub 4}-type ({alpha}-type) phase in the matrix of the {beta}-type phase in TmAlB{sub 4} crystal. The lamellar structure can be characterized by a tiling of deformed hexagons, which are a common structure unit in the {alpha}-type and {beta}-type structures. The intergrown nanostructure is considered to be attributed to the origin of low temperature anomalies in physical properties.

Yubuta, Kunio, E-mail: yubuta@imr.tohoku.ac.jp [Institute for Materials Research, Tohoku University, Katahira 2-1-1, Aoba-ku, Sendai 980-8577 (Japan); Mori, Takao [International Center for Materials Nanoarchitectonics (MANA), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan); Leithe-Jasper, Andreas; Grin, Yuri [Max-Plank-Institut fuer Chemische Physik fester Stoeffe, 01187 Dresden (Germany); Okada, Shigeru [Department of Science and Engineering, Kokushikan University, Tokyo 154-8515 (Japan); Shishido, Toetsu [Institute for Materials Research, Tohoku University, Katahira 2-1-1, Aoba-ku, Sendai 980-8577 (Japan)

2009-08-05T23:59:59.000Z

275

Temperature-induced martensite in magnetic shape memory Fe{sub 2}MnGa observed by photoemission electron microscopy  

SciTech Connect

The magnetic domain structure in single crystals of a Heusler shape memory compound near the composition Fe{sub 2}MnGa was observed during phase transition by photoelectron emission microscopy at Beamline 11.0.1.1 of the Advanced Light Source. The behavior is comparable with recent observations of an adaptive martensite phase in prototype Ni{sub 2}MnGa, although the pinning in the recent work is an epitaxial interface and in this work the e#11;ective pinning plane is a boundary between martensitic variants that transform in a self-accommodating way from the single crystal austenite phase present at high temperatures. Temperature dependent observations of the twinning structure give information as to the coupling behavior between the magnetism and the structural evolution.

Jenkins, Catherine; Scholl, Andreas; Kainuma, R.; Elmers, Hans-Joachim; Omori, Toshihiro

2012-01-18T23:59:59.000Z

276

Role of Colostrum and Milk in the Natural Transmission of the Bovine Leukemia Virus  

Science Journals Connector (OSTI)

...cellular uptake, NP uptake route characterization, and...estimated by zetasizer and transmission electron microscopy...BO2 and MCF-7 cell lines, due to cell cycle arrest...cytometry). Uptake route characterization studies...group in MCF-7 cell line. These results provide...

Jorge F. Ferrer and Charles E. Piper

1981-12-01T23:59:59.000Z

277

Spectroscopic ellipsometric modeling of a Bi–Te–Se write layer of an optical data storage device as guided by atomic force microscopy, scanning electron microscopy, and X-ray diffraction  

Science Journals Connector (OSTI)

Abstract Conventional magnetic tape is the most widely used medium for archival data storage. However, data stored on it need to be migrated every ca. 5 years. Recently, optical discs that store information for hundreds, or even more than 1000 years, have been introduced to the market. We recently proposed that technology in these optical discs be used to make an optical tape that would show greater permanence than its magnetic counterpart. Here we provide a detailed optical characterization of a sputtered thin film of bismuth, tellurium, and selenium (BTS) that is a proposed data storage layer for these devices. The methodology described herein should be useful in the future development of related materials. Spectroscopic ellipsometry (SE) data are obtained using interference enhancement, and the modeling of this data is guided by results from atomic force microscopy (AFM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-ray reflectivity (XRR). By AFM, ca. 40 nm BTS films show ca. 10 nm roughness. SEM images also suggest considerable roughness in the films and indicate that they are composed of 13.1 ± 5.9 nm grains. XRD confirms that the films are crystalline and predicts a grain size of 17 ± 2 nm. XRD results are consistent with the composition of the films — a mildly oxidized BTS material. Three models of increasing complexity are investigated to explain the SE data. The first model consists of a smooth, homogeneous BTS film. The second model adds a roughness layer to the previous model. The third model also has two layers. The bottom layer is modeled as a mixture of BTS and void using a Bruggeman effective medium approximation. The upper layer is similarly modeled, but with a gradient. The first model was unable to adequately model the SE data. The second model was an improvement — lower MSE (4.4) and good agreement with step height measurements. The third model was even better — very low MSE (2.6) and good agreement with AFM results. The third SE model predicted ca. 90% void at the film surface. XRR modeling of the film agreed well with the predictions from SE. The uniquenesses of the SE models were confirmed.

Hao Wang; Nitesh Madaan; Jacob Bagley; Anubhav Diwan; Yiqun Liu; Robert C. Davis; Barry M. Lunt; Stacey J. Smith; Matthew R. Linford

2014-01-01T23:59:59.000Z

278

Study of hard disk and slider surfaces using X-ray photoemission electron microscopy and near-edge X-ray absorption fine structure spectroscopy  

SciTech Connect

X-ray Photo Emission Electron Microscopy (X-PEEM) and Near Edge X-ray Absorption Fine Structure (NEXAFS) spectroscopy were applied to study the properties of amorphous hard carbon overcoats on disks and sliders, and the properties of the lubricant. The modification of lubricants after performing thermal desorption studies was measured by NEXAFS, and the results are compared to the thermal desorption data. The study of lubricant degradation in wear tracks is described. Sliders were investigated before and after wear test, and the modification of the slider coating as well as the transfer of lubricant to the slider was studied. The studies show that the lubricant is altered chemically during the wear. Fluorine is removed and carboxyl groups are formed.

Anders, S.; Stammler, T. [Lawrence Berkeley National lab., CA (United States). Advanced Light Source Div.; Bhatia, C.S. [SSD/IBM, San Jose, CA (United States); Stoehr, J. [IBM Research Div., San Jose, CA (United States). Almaden Research Center; Fong, W.; Chen, C.Y.; Bogy, D.B. [Univ. of California, Berkeley, CA (United States)

1998-04-01T23:59:59.000Z

279

Single-walled carbon nanotubes and nanocrystalline graphene reduce beam-induced movements in high-resolution electron cryo-microscopy of ice-embedded biological samples  

E-Print Network (OSTI)

For single particle electron cryo-microscopy (cryoEM), contrast loss due to beam-induced charging and specimen movement is a serious problem, as the thin films of vitreous ice spanning the holes of a holey carbon film are particularly susceptible to beam-induced movement. We demonstrate that the problem is at least partially solved by carbon nanotechnology. Doping ice-embedded samples with single-walled carbon nanotubes (SWNT) in aqueous suspension or adding nanocrystalline graphene supports, obtained by thermal conversion of cross-linked self-assembled biphenyl precursors, significantly reduces contrast loss in high-resolution cryoEM due to the excellent electrical and mechanical properties of SWNTs and graphene.

Daniel Rhinow; Nils-Eike Weber; Andrey Turchanin; Armin Gölzhäuser; Werner Kühlbrandt

2011-10-06T23:59:59.000Z

280

Electronic structures and bonding properties of chlorine-treated nitrogenated carbon nanotubes: X-ray absorption and scanning photoelectron microscopy studies  

SciTech Connect

The electronic and bonding properties of nitrogenated carbon nanotubes (N-CNTs) exposed to chlorine plasma were investigated using C and N K-edge x-ray absorption near-edge structure (XANES) and scanning photoelectron microscopy (SPEM). The C and N K-edge XANES spectra of chlorine-treated N-CNTs consistently reveal the formation of pyridinelike N-CNTs by the observation of 1s{yields}{pi}*(e{sub 2u}) antibonding and 1s{yields}{pi}*(b{sub 2g}) bonding states. The valence-band photoemission spectra obtained from SPEM images indicate that chlorination of the nanotubes enhances the C-N bonding. First-principles calculations of the partial densities of states in conjunction with C K-edge XANES data identify the presence of C-Cl bonding in chlorine treated N-CNTs.

Ray, S. C.; Pao, C. W.; Tsai, H. M.; Chiou, J. W.; Pong, W. F.; Chen, C. W.; Tsai, M.-H.; Papakonstantinou, P.; Chen, L. C.; Chen, K. H.; Graham, W. G. [Department of Physics, Tamkang University, Tamsui 251, Taiwan (China); Department of Materials Science and Engineering, National Taiwan University, Taipei 106, Taiwan (China); Department of Physics, National Sun Yat-Sen University, Kaohsiung 804, Taiwan (China); NRI, School of Electrical and Mechanical Engineering, University of Ulster at Jordanstown, Newtownabbey, County Antrim BT37OQB, Northern Ireland (United Kingdom); Center for Condensed Matter Sciences, National Taiwan University, Taipei 106, Taiwan (China); Institute of Atomic and Molecular Sciences, Academia Sinica, Taipei 106, Taiwan (China); Department of Physics and Astronomy, Queens University of Belfast, Belfast, Antrim BT71NN, Northern Ireland (United Kingdom)

2007-05-07T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

Analytical electron microscopy investigation of elemental composition and bonding structure at the Sb-doped Ni-fully-silicide/SiO{sub 2} interface  

SciTech Connect

It is very important to control the elemental composition and bonding structure at the gate electrode/gate dielectrics interface in metal-oxide-semiconductor transistor devices because this determines the threshold voltage of the gate electrode. In this study, we investigated the structure at the interface between the antimony (Sb)-doped nickel-fully-silicide gate electrode and SiO{sub 2} dielectrics by employing high-spatial resolution techniques such as energy dispersive x-ray spectroscopy and electron energy-loss spectroscopy using a scanning transmission electron microscope. In one region, we found a thin nickel layer at the NiSi/SiO{sub 2} interface originating from the migration of native oxide at the face of the poly-silicon. In another region, a Sb pileup was detected at the NiSi/SiO{sub 2} interface where the Ni L{sub 3}-edge spectrum showed Ni-Sb bonding, then it was suggested that Sb atoms exist at the bottom of NiSi, substituting for Si atoms in NiSi.

Kawasaki, Naohiko; Sugiyama, Naoyuki; Otsuka, Yuji; Hashimoto, Hideki [Morphological Research Laboratory, Toray Research Center Inc., Otsu, Shiga (Japan); Kurata, Hiroki; Isoda, Seiji [Institute for Chemical Research, Kyoto University, Uji, Kyoto (Japan)

2011-03-15T23:59:59.000Z

282

Characterization of the Binding of Gallium, Platinum, and Uranium to Pseudomonas fluorescens by Small-Angle X-Ray Scattering and Transmission Electron Microscopy  

Science Journals Connector (OSTI)

...that combined small-angle neutron scattering and small-angle X-ray scattering...by small-angle X-ray and neutron scattering. Plenum Press, New York...of biological structures by neutron scattering from solution. Rep. Prog...

Susan Krueger; Gregory J. Olson; David Johnsonbaugh; T. J. Beveridge

1993-12-01T23:59:59.000Z

283

Grain boundary atomic structures and light-element visualization in ceramics: combination of Cs-corrected scanning transmission electron microscopy and first-principles calculations  

Science Journals Connector (OSTI)

......materials for electrolytes in solid oxide fuel cells and catalysis because of their unique...electrochemical processes occurring during the battery use. Figure-13a shows an HAADF-STEM...behavior and capacity fade in lithium ion batteries with LiMn2O4 as the cathode material......

Yuichi Ikuhara

2011-08-01T23:59:59.000Z

284

Influence of Surface Preparation on Scanning Kelvin Probe Microscopy and Electron Backscatter Diffraction Analysis of Cross Sections of CdTe/CdS Solar Cells  

SciTech Connect

Electron backscatter diffraction (EBSD) provides information on the crystallographic structure of a sample, while scanning Kelvin probe microscopy (SKPM) provides information on its electrical properties. The advantage of these techniques is their high spatial resolution, which cannot be attained with any other techniques. However, because these techniques analyze the top layers of the sample, surface or cross section features directly influence the results of the measurements, and sample preparation is a main step in the analysis. In this work we investigated different methods to prepare cross sections of CdTe/CdS solar cells for EBSD and SKPM analyses. We observed that procedures used to prepare surfaces for EBSD are not suitable to prepare cross sections, and we were able to develop a process using polishing and ion-beam milling. This process resulted in very good results and allowed us to reveal important aspects of the cross section of the CdTe films. For SKPM, polishing and a light ion-beam milling resulted in cross sections that provided good data. We were able to observe the depletion region on the CdTe film and the p-n junction as well as the interdiffusion layer between CdTe and CdS. However, preparing good-quality cross sections for SKPM is not a reproducible process, and artifacts are often observed.

Moutinho, H. R.; Dhere, R. G.; Jiang, C. S.; Al-Jassim, M. M.

2011-01-01T23:59:59.000Z

285

Direct comparison between X-ray nanotomography and scanning electron microscopy for the microstructure characterization of a solid oxide fuel cell anode  

SciTech Connect

X-ray computed nanotomography (nano-CT) and scanning electron microscopy (SEM) have been applied to characterize the microstructure of a Solid Oxide Fuel Cell (SOFC) anode. A direct comparison between the results of both methods is conducted on the same region of the microstructure to assess the spatial resolution of the nano-CT microstructure, SEM being taken as a reference. A registration procedure is proposed to find out the position of the SEM image within the nano-CT volume. It involves a second SEM observation, which is taken along an orthogonal direction and gives an estimate reference SEM image position, which is then refined by an automated optimization procedure. This enables an unbiased comparison between the cell porosity morphologies provided by both methods. In the present experiment, nano-CT is shown to underestimate the number of pores smaller than 1 ?m and overestimate the size of the pores larger than 1.5 ?m. - Highlights: ? X-ray computed nanotomography (nano-CT) and SEM are used to characterize an SOFC anode. ? A methodology is proposed to compare the nano-CT and SEM data on the same region. ? The spatial resolution of the nano-CT data is assessed from that comparison.

Quey, R., E-mail: quey@emse.fr [CEA, LETI, MINATEC Campus, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France); École des Mines de Saint-Étienne, CNRS UMR 5307, 158 cours Fauriel, 42023 Saint-Étienne, Cedex 2 (France); Suhonen, H., E-mail: heikki.suhonen@esrf.fr [European Synchrotron Radiation Facility (ESRF), 6 Rue Jules Horowitz BP 220, 38043 Grenoble (France); Laurencin, J., E-mail: jerome.laurencin@cea.fr [CEA-Liten, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France); Cloetens, P., E-mail: peter.cloetens@esrf.fr [European Synchrotron Radiation Facility (ESRF), 6 Rue Jules Horowitz BP 220, 38043 Grenoble (France); Bleuet, P., E-mail: pierre.bleuet@cea.fr [CEA, LETI, MINATEC Campus, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France)

2013-04-15T23:59:59.000Z

286

Elemental relationships in rock varnish as seen with SEM/EDX (scanning electron microscopy/energy dispersive x-ray) elemental line profiling  

SciTech Connect

The heterogeneous nature of rock varnish requires a thorough survey of elemental and mineralogic compositions before relating chemical variability of rock varnish to past geochemical environments. Elemental relationships in rock varnish can be examined using scanning electron microscopy (SEM) in conjunction with an elemental line profiling routine using semi-quantitative, energy dispersive x-ray (EDX) analysis. Results of SEM/EDX analysis suggest: variations in cation concentrations used in varnish cation ratio dating relate more specifically to variations in detritus within the varnish than to element mobility as defined by weathering indices; Mn concentration rather than Mn:Fe ratios may be a more appropriate indicator of paleoclimatic fluctuations; and the Mn-oxide phase existing in varnish is most likely a Ba-enriched phase rather than birnessite. Element line profiling offers great potential for gaining insights into geochemical processes affecting the deposition and diagenesis of rock varnish and for testing hypotheses relating to its chemical variability. 27 refs., 9 figs.

Raymond, R. Jr.; Reneau, S.L.; Harrington, C.D.

1990-01-01T23:59:59.000Z

287

UHV high-resolution electron microscopy and chemical analysis of room-temperature Au deposition on Si(001)-2×1  

Science Journals Connector (OSTI)

Investigations of Au on Si(001) have suggested that room-temperature deposition of Au on a clean Si surface results in an interfacial reaction and the formation of a gold-silicide. However, these investigations typically lack direct information about the surface morphology or the exact structure at the interface. Utilizing the capabilities of a surface chemical analysis system attached to a Hitachi UHV H-9000 microscope, a layer plus island growth mode has been observed by high-resolution electron microscopy showing multiply twinned small particles on the surface. The presence of small particles for various coverages has been correlated with the shifts seen in the Si 2p and Au 4f binding energies as well as the peak splitting in the Si LVV Auger transition. Our chemical data are consistent with observed shifts in the binding energies of small metal clusters deposited on various substrates, and with the published data for this surface. In addition, the results are consistent with our previous studies of Ag on Si(001), and indicate the growth morphology plays a crucial role in understanding spectroscopic information as well as its correlation to the structure and chemical state of the interface and surface morphology.

E. Landree, D. Grozea, C. Collazo-Davila, and L. D. Marks

1997-03-15T23:59:59.000Z

288

Quantification of Artifacts in Scanning Electron Microscopy Tomography: Improving the Reliability of Calculated Transport Parameters in Energy Applications such as Fuel Cell and Battery Electrodes  

Science Journals Connector (OSTI)

Abstract Focused ion beam and scanning electron microscopy tomography (FIB-SEMt) is commonly used to extract reactant transport relevant parameters from nano-porous materials in energy applications, such as fuel cells or batteries. Here we present an approach to virtually model the errors in FIB-SEMt which are caused by the FIB cutting distance. The errors are evaluated in terms of connectivity, solid volume fraction (SVF), conductivity, diffusivity, as well as mean grain and pore sizes. For state-of-the-art FIB-SEMt experiments, where a hydrogen fuel cell catalyst layer with 60 nm mean grain size and 40 % SVF is sectioned with a cutting distance of 15 nm, the error in our simulation ranges up to 51 % (conductivity), whereas other parameters remain largely unaffected (Laplace diffusivity, 4 %). We further present a method, employing virtual coarsening and back interpolation, to reduce FIB cutting distance errors in all investigated parameters. Both error evaluation and correction are applicable to sphere based porous materials with relevance for the energy conversion and storage sector such as polymer electrolyte membrane fuel cell catalyst layer (PEMFC CL), battery carbon binder domain (CBD) or supercapacitor electrodes.

Matthias Klingele; Roland Zengerle; Simon Thiele

2014-01-01T23:59:59.000Z

289

The structures and dynamics of atomic and molecular adsorbates on metal surfaces by scanning tunneling microscopy and low energy electron diffraction  

SciTech Connect

Studies of surface structure and dynamics of atoms and molecules on metal surfaces are presented. My research has focused on understanding the nature of adsorbate-adsorbate and adsorbate-substrate interactions through surface studies of coverage dependency and coadsorption using both scanning tunneling microscopy (STM) and low energy electron diffraction (LEED). The effect of adsorbate coverage on the surface structures of sulfur on Pt(111) and Rh(111) was examined. On Pt(111), sulfur forms p(2x2) at 0.25 ML of sulfur, which transforms into a more compressed ({radical}3x{radical}3)R30{degrees} at 0.33 ML. On both structures, it was found that sulfur adsorbs only in fcc sites. When the coverage of sulfur exceeds 0.33 ML, it formed more complex c({radical}3x7)rect structure with 3 sulfur atoms per unit cell. In this structure, two different adsorption sites for sulfur atoms were observed - two on fcc sites and one on hcp site within the unit cell.

Yoon, Hyungsuk Alexander

1996-12-01T23:59:59.000Z

290

Three-dimensional reconstruction of the -AlCrFe phase by electron crystallography  

Science Journals Connector (OSTI)

The three-dimensional structure of the huge quasicrystal approxi­mant -AlFeCr was solved by electron crystallography, using high-resolution transmission-electron-microscopy (HREM) images and selected-area electron diffraction patterns from 13 different zone axes. This is the first example of an inorganic structure with over 100 unique atoms being solved to atomic resolution by electron crystallography.

Zou, X.D.

2003-10-28T23:59:59.000Z

291

Optical Microscopy and 4Optical Microscopy and 4 Pi MicroscopyPi Microscopy  

E-Print Network (OSTI)

Optical Microscopy and 4Optical Microscopy and 4 Pi MicroscopyPi Microscopy Carolyn A. SuttonCarolyn A. Sutton PH 464PH 464 #12;OverviewOverview The OpticalThe Optical MicroscopeMicroscopy 4 Pi Microscopy4 Pi Microscopy Optical Microscope for Metallography #12;Optical Microscope: OriginsOptical

La Rosa, Andres H.

292

SunShot Initiative: Transmission Grid Integration  

NLE Websites -- All DOE Office Websites (Extended Search)

Transmission Grid Integration to Transmission Grid Integration to someone by E-mail Share SunShot Initiative: Transmission Grid Integration on Facebook Tweet about SunShot Initiative: Transmission Grid Integration on Twitter Bookmark SunShot Initiative: Transmission Grid Integration on Google Bookmark SunShot Initiative: Transmission Grid Integration on Delicious Rank SunShot Initiative: Transmission Grid Integration on Digg Find More places to share SunShot Initiative: Transmission Grid Integration on AddThis.com... Concentrating Solar Power Photovoltaics Systems Integration Research, Development, & Demonstration Distribution Grid Integration Transmission Grid Integration Solar Resource Assessment Technology Validation Power Electronics & Balance of System Hardware Technologies Competitive Awards

293

Geochemistry Atomic Force Microscopy | EMSL  

NLE Websites -- All DOE Office Websites (Extended Search)

imaging modes: contact, intermittent contact, phase imaging, magnetic force microscopy, electric force microscopy, surface potential microscopy, scanning capacitance microscopy,...

294

Respective Roles of Serological Status and Blood Specific Antihuman Herpesvirus 8 Antibody Levels in Human Herpesvirus 8 Intrafamilial Transmission in a Highly Endemic Area  

Science Journals Connector (OSTI)

...cellular uptake, NP uptake route characterization, and...estimated by zetasizer and transmission electron microscopy...BO2 and MCF-7 cell lines, due to cell cycle arrest...cytometry). Uptake route characterization studies...group in MCF-7 cell line. These results provide...

Sabine Plancoulaine; Laurent Abel; David Trégouët; Renan Duprez; Monique van Beveren; Patricia Tortevoye; Alain Froment; and Antoine Gessain

2004-12-01T23:59:59.000Z

295

Direct and large scale electric arc discharge synthesis of boron and nitrogen doped single-walled carbon nanotubes and their electronic properties  

Science Journals Connector (OSTI)

Boron and nitrogen co-doped single-walled carbon nanotubes (BN-SWCNTs) were directly synthesized at large scale using an electric arc discharge method. X-ray photoelectron spectroscopy, scanning electron microscopy, transmission electron microscopy and UV–vis–NIR spectroscopy were performed to investigate structure and properties of BN-SWCNTs. These results show that the band gaps of \\{SWCNTs\\} have been tuned greatly with B and N doping.

Bin Wang; Yanfeng Ma; Yingpeng Wu; Na Li; Yi Huang; Yongsheng Chen

2009-01-01T23:59:59.000Z

296

Diamondoids Improve Electron Emitters  

NLE Websites -- All DOE Office Websites (Extended Search)

is unique to diamondoid, is believed to enable the development of a new generation of electron emitters with unprecedented properties. In Photoemission Electron Microscopy...

297

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray...

298

Scanning Probe Microscopy Studies of Carbon Nanotubes  

E-Print Network (OSTI)

Scanning Probe Microscopy Studies of Carbon Nanotubes Teri Wang Odom1 , Jason H. Hafner1 relationship between Single-Walled Carbon Nanotube (SWNT) atomic structure and electronic properties, (2, properties and application of carbon nanotube probe microscopy tips to ultrahigh resolution and chemically

Odom, Teri W.

299

Electrostatically focused addressable field emission array chips (AFEA's) for high-speed massively parallel maskless digital E-beam direct write lithography and scanning electron microscopy  

DOE Patents (OSTI)

Systems and methods are described for addressable field emission array (AFEA) chips. A method of operating an addressable field-emission array, includes: generating a plurality of electron beams from a pluralitly of emitters that compose the addressable field-emission array; and focusing at least one of the plurality of electron beams with an on-chip electrostatic focusing stack. The systems and methods provide advantages including the avoidance of space-charge blow-up.

Thomas, Clarence E. (Knoxville, TN); Baylor, Larry R. (Farragut, TN); Voelkl, Edgar (Oak Ridge, TN); Simpson, Michael L. (Knoxville, TN); Paulus, Michael J. (Knoxville, TN); Lowndes, Douglas H. (Knoxville, TN); Whealton, John H. (Oak Ridge, TN); Whitson, John C. (Clinton, TN); Wilgen, John B. (Oak Ridge, TN)

2002-12-24T23:59:59.000Z

300

Coherence of Electron Wave and Contrast of Electron Image  

Science Journals Connector (OSTI)

......other Symposium of the Society of Japanese Electron Microscopy Coherence of Electron Wave and Contrast of Electron Image Tadatoshi...Measurements, Tohoku University (21) 207 0 Jfc & ft* ffi Coherence of Electron Wave and Contrast of Electron Image Tadatoshi......

Tadatoshi HIBI; Shoichi Takahashi

1964-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

Electron  

NLE Websites -- All DOE Office Websites (Extended Search)

to measure the electron density gradient and its fluctuations. Two separate laser beams with slight spatial offset and frequency difference are coupled into a single mixer...

302

Electronic and structural properties of the InP(1 0 0)(2 × 4) surface studied by core-level photoemission and scanning tunneling microscopy  

Science Journals Connector (OSTI)

The (2 × 4)-reconstructed InP(1 0 0) surfaces have been investigated by scanning tunneling microscopy (STM) and synchrotron-radiation core-level photoelectron spectroscopy. STM observations show that the ?2 model describes the atomic structure of the InP(1 0 0)(2 × 4) surface in a limited range of the surface-preparation conditions, as predicted theoretically but not previously observed. STM results also support the accuracy of the previously found mixed-dimer structure for the InP(1 0 0)(2 × 4) surface under less P-rich conditions. A study of P 2p core-level photoelectron spectra, measured with different surface-sensitivity conditions, demonstrates that P 2p photoemission from the mixed-dimer InP(1 0 0)(2 × 4) surface consists of at least two surface-core-level-shift (SCLS) components which have kinetic energies approximately 0.4 eV higher and 0.3 eV lower than the bulk emission. On the basis of the surface-sensitivity difference between these SCLSs, they are related to the third-layer and top-layer P sites in the mixed-dimer structure, respectively.

P. Laukkanen; J. Pakarinen; M. Ahola-Tuomi; M. Kuzmin; R.E. Perälä; I.J. Väyrynen; A. Tukiainen; V. Rimpiläinen; M. Pessa; M. Adell; J. Sadowski

2006-01-01T23:59:59.000Z

303

Experimental procedures to mitigate electron beam induced artifacts during in situ fluid imaging of nanomaterials  

SciTech Connect

Currently there are few standardized experimental practices in the field of fluid stage transmission electron microscopy. To obtain consistency in this emerging field, a crucial step is to establish the common artifacts and electron beam-sample interactions that can occur. Recently many unintended phenomena have been observed during in situ fluid stage scanning transmission electron microscopy (STEM) experiments, including growth of crystals on the fluid stage windows, repulsion of particles from the irradiated area, bubble formation, and the loss of atomic information during prolonged imaging of individual nanoparticles. Here we provide a comprehensive review of these fluid stage artifacts, and we present new experimental evidence that sheds light on their origins in terms of experimental apparatus issues and indirect electron beam sample interactions with the fluid layer. The results here will provide a methodology for minimizing fluid stage imaging artifacts and acquiring quantitative in situ observations of nanomaterial behavior in a liquid environment.

Woehl, Taylor J.; Jungjohann, K. L.; Evans, James E.; Arslan, Ilke; Ristenpart, William D.; Browning, Nigel D.

2013-04-01T23:59:59.000Z

304

Electron  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron thermal transport within magnetic islands in the reversed-field pinch a... H. D. Stephens, 1,b D. J. Den Hartog, 1,3 C. C. Hegna, 1,2 and J. A. Reusch 1 1 Department of...

305

Atomic Resolution Coordination Mapping in Ca2FeCoO5 Brownmillerite by Spatially Resolved Electron Energy-Loss Spectroscopy  

Science Journals Connector (OSTI)

Using a combination of high-angle annular dark field scanning transmission electron microscopy and atomically resolved electron energy-loss spectroscopy at high energy resolution in an aberration-corrected electron microscope, we demonstrate the capability of coordination mapping in complex oxides. ... (b) Survey image indicating the area used for octahedral (red) and tetrahedral (blue) data summation (3 pixel width). ... B atoms that have energetic preference for tetrahedral coordination geometry are esp. ...

Stuart Turner; Johan Verbeeck; Farshid Ramezanipour; John E. Greedan; Gustaaf Van Tendeloo; Gianluigi A. Botton

2012-04-25T23:59:59.000Z

306

Negative differential transmission in graphene  

Science Journals Connector (OSTI)

By using the Kubo linear response theory with the Keldysh Green function approach, we investigate the mechanism leading to the negative differential transmission in a system with the equilibrium electron density much smaller than the photon-excited one. It is shown that the negative differential transmission can appear at low probe-photon energy (in the order of the scattering rate) or at high energy (much larger than the scattering rate). For the low probe-photon energy case, the negative differential transmission is found to come from the increase of the intraband conductivity due to the large variation of electron distribution after the pumping. As for the high probe-photon energy case, the negative differential transmission is shown to tend to appear with the hot-electron temperature being closer to the equilibrium one and the chemical potential higher than the equilibrium one but considerably smaller than half of the probe-photon energy. We also show that this negative differential transmission can come from both the inter- and the intraband components of the conductivity. Especially, for the interband component, its contribution to the negative differential transmission is shown to come from both the Hartree-Fock self-energy and the scattering. Furthermore, the influence of the Coulomb-hole self-energy is also addressed.

B. Y. Sun and M. W. Wu

2013-12-17T23:59:59.000Z

307

Transmission Investment: A Primer  

SciTech Connect

This primer highlights recent trends in transmission investment, summarizes the division of jurisdictional authority over transmission, and presents four alternative models for transmission ownership. (author)

McGarvey, Joe

2006-10-15T23:59:59.000Z

308

Transmission | Open Energy Information  

Open Energy Info (EERE)

Transmission Lattice.jpg High-voltage transmission lines form the backbone of electricity systems. Transmission lines are designed to carry large amounts of electricity at...

309

Chemical Imaging Analysis of Environmental Particles Using the Focused Ion Beam/Scanning Electron Microscopy Technique: Microanalysis Insights into Atmospheric Chemistry of Fly Ash  

SciTech Connect

Airborne fly ash from coal combustion may represent a source of bioavailable iron (Fe) in the open ocean. However, few studies have been made focusing on Fe speciation and distribution in coal fly ash. In this study, chemical imaging of fly ash has been performed using a dual-beam FIB/SEM (focused ion beam/scanning electron microscope) system for a better understanding of how simulated atmospheric processing modify the morphology, chemical compositions and element distributions of individual particles. A novel approach has been applied for cross-sectioning of fly ash specimen with a FIB in order to explore element distribution within the interior of individual particles. Our results indicate that simulated atmospheric processing causes disintegration of aluminosilicate glass, a dominant material in fly ash particles. Aluminosilicate-phase Fe in the inner core of fly ash particles is more easily mobilized compared with oxide-phase Fe present as surface aggregates on fly ash spheres. Fe release behavior depends strongly on Fe speciation in aerosol particles. The approach for preparation of cross-sectioned specimen described here opens new opportunities for particle microanalysis, particular with respect to inorganic refractive materials like fly ash and mineral dust.

Chen, Haihan; Grassian, Vicki H.; Saraf, Laxmikant V.; Laskin, Alexander

2013-01-21T23:59:59.000Z

310

Imaging Local Electronic Corrugations and Doped Regions in Graphene  

SciTech Connect

Electronic structure heterogeneities are ubiquitous in two-dimensional graphene and profoundly impact the transport properties of this material. Here we show the mapping of discrete electronic domains within a single graphene sheet using scanning transmission X-ray microscopy in conjunction with ab initio density functional theory calculations. Scanning transmission X-ray microscopy imaging provides a wealth of detail regarding the extent to which the unoccupied levels of graphene are modified by corrugation, doping and adventitious impurities, as a result of synthesis and processing. Local electronic corrugations, visualized as distortions of the {pi}*cloud, have been imaged alongside inhomogeneously doped regions characterized by distinctive spectral signatures of altered unoccupied density of states. The combination of density functional theory calculations, scanning transmission X-ray microscopy imaging, and in situ near-edge X-ray absorption fine structure spectroscopy experiments also provide resolution of a longstanding debate in the literature regarding the spectral assignments of pre-edge and interlayer states.

B Schultz; C Patridge; V Lee; C Jaye; P Lysaght; C Smith; J Barnett; D Fischer; D Prendergast; S Banerjee

2011-12-31T23:59:59.000Z

311

Optoelectronics 514 Transmission Hologram Transmission Hologram  

E-Print Network (OSTI)

Optoelectronics 514 Transmission Hologram Transmission Hologram Purpose: To learn about making Procedure: 1. HeNe Laser: #12;Optoelectronics 514 Transmission Hologram Mount the laser along the long axis. Development #12;Optoelectronics 514 Transmission Hologram Put the plate in the developer emulsion side up

Collins, Gary S.

312

Measuring Large Optical Transmission Matrices of Disordered Media  

E-Print Network (OSTI)

We report a measurement of the large optical transmission matrix (TM) of a complex turbid medium. The TM is acquired using polarization-sensitive, full-field interferometric microscopy equipped with a rotating galvanometer ...

Yu, Hyeonseung

313

Transmission | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Transmission Transmission Transmission Below are resources for Tribes on transmission. Transmission 101 Presentation from the National Council on Electricity Policy's Transmissions Technologies workshop. Includes information on transmission technology, costs, and how to plan the system. Transmission on Tribal Land Basics The Tribal Energy and Environmental Information Clearinghouse provides resources for development on tribal lands. Topics covered include transmission technology basics, potential impacts, law and regulations, and tribal incentives. Transmission Pre-Feasibility Study for Tribes Presentation on the components of a pre-feasibility study including generation location, sizing, and desirability, ability and cost to deliver, capacity versus energy, time of delivery versus peak, request for

314

Argonne CNM: X-Ray Microscopy Capabilities  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Microscopy Facilities X-Ray Microscopy Facilities The Hard X-Ray Nanoprobe (HXN) facility provides scanning fluorescence, scanning diffraction, and full-field transmission and tomographic imaging capabilities with a spatial resolution of 30 nm over a spectral range of 6-12 keV. Modes of Operation Full-Field Transmission Imaging and Nanotomography X-ray transmission imaging uses both the absorption and phase shift of the X-ray beam by the sample as contrast mechanisms. Absorption contrast is used to map the sample density. Elemental constituents can be located by using differential edge contrast in this mode. Phase contrast can be highly sensitive to edges and interfaces even when the X-ray absorption is weak. These contrast mechanisms are exploited to image samples rapidly in full-field transmission mode under various environmental conditions, or combined with nanotomography methods to study the three-dimensional structure of complex and amorphous nanomaterials with the HXN.

315

Electronic  

NLE Websites -- All DOE Office Websites (Extended Search)

contribution contribution to friction on GaAs: An atomic force microscope study Yabing Qi, 1,2 J. Y. Park, 2 B. L. M. Hendriksen, 2 D. F. Ogletree, 2 and M. Salmeron 2,3 1 Applied Science and Technology Graduate Group, University of California, Berkeley, California 94720, USA 2 Materials Sciences Division, Lawrence Berkeley National Laboratory, University of California, Berkeley, California 94720, USA 3 Department of Materials Sciences and Engineering, University of California, Berkeley, California 94720, USA ͑Received 23 January 2008; revised manuscript received 11 April 2008; published 7 May 2008͒ The electronic contribution to friction at semiconductor surfaces was investigated by using a Pt-coated tip with 50 nm radius in an atomic force microscope sliding against an n-type GaAs͑100͒ substrate. The GaAs surface was covered by an approximately 1 nm thick oxide layer. Charge accumulation

316

Simulation of electron-matter interaction during wet-STEM electron tomography  

SciTech Connect

Tomography is an efficient tool to probe the 3 dimensional (3D) structure of materials. In the laboratory, a device has been developed to perform electron tomography in an environmental scanning electron microscopy (ESEM). The configuration of Scanning Transmission Electron Microscopy (STEM) in Environmental Scanning Electron Microscopy (ESEM) provides a novel approach for the characterization of the 3D structure of materials and optimizes a compromise between the resolution level of a few nm and the large tomogram due to the high thickness of transparency. Moreover, STEM allows the observation in 2D of wet samples in an ESEM by finely controlling the sample temperature and the water pressure of the sample environment. It has been recently demonstrated that it was possible to acquire image series of hydrated objects and thus to attain 3D characterization of wet samples. In order to get reliable and quantitative data, the present study deals with the simulation of electron-matter interactions. From such simulation on the MCM-41 material, we determine the minimum quantity of water layer which can be detected on wet materials.

Septiyanto, Rahmat Firman, E-mail: karine.masenelli-varlot@insa-lyon.fr [MATEIS, INSA-Lyon, CNRS UMR5510, F-69621, France and Physics of Electronic Material, Departement of Physics, Faculty of Mathematic and Natural Sciences, ITB Jalan Ganesha No. 10, Bandung 40132 (Indonesia); Masenelli-Varlot, Karine [MATEIS, INSA-Lyon, CNRS UMR5510, F-69621 (France); Iskandar, Ferry [Physics of Electronic Material, Departement of Physics, Faculty of Mathematic and Natural Sciences, ITB Jalan Ganesha No. 10, Bandung 40132 (Indonesia)

2014-02-24T23:59:59.000Z

317

Analytical electron microscopy of rapidly solidified metals  

SciTech Connect

Examples of the need to characterize rapidly solidified metals on submicron scale are given for centrifugally atomized steel powder and electrohydrodynamically atomized submicron spheres. Materials studied include Fe-40wt% Ni, 304 SS, Fe-20at.%Co, and pure V.

Kelly, T.F.; Holzman, L.M.; Shin, K.; Kim, Y.W.; Bae, J.C.; Flinn, J.E.; Camus, P.P.; Melmed, A.J.

1991-12-31T23:59:59.000Z

318

NC-JRA-001_Electron Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

samples between labs and buildings SBMS Transportation, PPE, training N 1 3 2 2 12 *Risk: 0 to 20 21 to 40 41-60 61 to 80 81 or greater Negligible Acceptable Moderate...

319

HIGH STABILITY CURRENT SUPPLY FOR ELECTRON MICROSCOPY  

E-Print Network (OSTI)

Improvements. Dordrecht, The Netherland: Kluwer AcademicESSENTIALS. Dordrecht, The Netherland: Springer, pages 181-

Motamedi, Maryam Melani

2012-01-01T23:59:59.000Z

320

Electron Microscopy of Irradiation Effects in Space  

Science Journals Connector (OSTI)

...frequency of periods of low solar wind energy at the moon. The lowest energy...2000-year periods of high solar wind energy at the moon, with the highest...indication of any change in the mean solar wind energy over geologic time. Solar wind...

M. Maurette; P. B. Price

1975-01-17T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

Photothermal imaging scanning microscopy  

DOE Patents (OSTI)

Photothermal Imaging Scanning Microscopy produces a rapid, thermal-based, non-destructive characterization apparatus. Also, a photothermal characterization method of surface and subsurface features includes micron and nanoscale spatial resolution of meter-sized optical materials.

Chinn, Diane (Pleasanton, CA); Stolz, Christopher J. (Lathrop, CA); Wu, Zhouling (Pleasanton, CA); Huber, Robert (Discovery Bay, CA); Weinzapfel, Carolyn (Tracy, CA)

2006-07-11T23:59:59.000Z

322

Survey of Transmission Cost Allocation Methodologies for Regional Transmission Organizations  

SciTech Connect

The report presents transmission cost allocation methodologies for reliability transmission projects, generation interconnection, and economic transmission projects for all Regional Transmission Organizations.

Fink, S.; Porter, K.; Mudd, C.; Rogers, J.

2011-02-01T23:59:59.000Z

323

Feature Article NEXAFS microscopy and resonant scattering  

E-Print Network (OSTI)

and conven- tional electron, X-ray and neutron scattering. We provide an overview of these synchrotron based and derivative struc- tures, ranging from spectroscopy to mechanical analysis and neutron scattering [9,10]. SomeFeature Article NEXAFS microscopy and resonant scattering: Composition and orientation probed

Hitchcock, Adam P.

324

Transmission Business Unit Manager  

Energy.gov (U.S. Department of Energy (DOE))

(See Frequently Asked Questions for more information). Where would I be working? Western Area Power Administration Rocky Mountain Region Transmission Services, (J7300) Transmission Busiess Unit 615...

325

Electronic Structure and Chemical Bonding of Amorphous Chromium Carbide Thin Films  

E-Print Network (OSTI)

The microstructure, electronic structure, and chemical bonding of chromium carbide thin films with different carbon contents have been investigated with high-resolution transmission electron microscopy, electron energy loss spectroscopy and soft x-ray absorption-emission spectroscopies. Most of the films can be described as amorphous nanocomposites with non-crystalline CrCx in an amorphous carbon matrix. At high carbon contents, graphene-like structures are formed in the amorphous carbon matrix. At 47 at% carbon content, randomly oriented nanocrystallites are formed creating a complex microstructure of three components. The soft x-ray absorption-emission study shows additional peak structures exhibiting non-octahedral coordination and bonding.

Magnuson, Martin; Lu, Jun; Hultman, Lars; Jansson, Ulf; 10.1088/0953-8984/24/22/225004

2012-01-01T23:59:59.000Z

326

Experimental procedures to mitigate electron beam induced artifacts during in situ fluid imaging of nanomaterials  

E-Print Network (OSTI)

of nanomaterials Taylor J. Woehl a,n , Katherine L. Jungjohann a , James E. Evans b,c , Ilke Arslan a,c , William D, USA a r t i c l e i n f o Available online 27 July 2012 Keywords: in situ TEM in situ STEM in situ fluid in situ liquid a b s t r a c t Scanning transmission electron microscopy of various fluid

Ristenpart, William

327

Nonlinear vibrational microscopy  

DOE Patents (OSTI)

The present invention is a method and apparatus for microscopic vibrational imaging using coherent Anti-Stokes Raman Scattering or Sum Frequency Generation. Microscopic imaging with a vibrational spectroscopic contrast is achieved by generating signals in a nonlinear optical process and spatially resolved detection of the signals. The spatial resolution is attained by minimizing the spot size of the optical interrogation beams on the sample. Minimizing the spot size relies upon a. directing at least two substantially co-axial laser beams (interrogation beams) through a microscope objective providing a focal spot on the sample; b. collecting a signal beam together with a residual beam from the at least two co-axial laser beams after passing through the sample; c. removing the residual beam; and d. detecting the signal beam thereby creating said pixel. The method has significantly higher spatial resolution then IR microscopy and higher sensitivity than spontaneous Raman microscopy with much lower average excitation powers. CARS and SFG microscopy does not rely on the presence of fluorophores, but retains the resolution and three-dimensional sectioning capability of confocal and two-photon fluorescence microscopy. Complementary to these techniques, CARS and SFG microscopy provides a contrast mechanism based on vibrational spectroscopy. This vibrational contrast mechanism, combined with an unprecedented high sensitivity at a tolerable laser power level, provides a new approach for microscopic investigations of chemical and biological samples.

Holtom, Gary R. (Richland, WA); Xie, Xiaoliang Sunney (Richland, WA); Zumbusch, Andreas (Munchen, DE)

2000-01-01T23:59:59.000Z

328

Materials Applications of Photoelectron Emission Microscopy....  

NLE Websites -- All DOE Office Websites (Extended Search)

Applications of Photoelectron Emission Microscopy. Materials Applications of Photoelectron Emission Microscopy. Abstract: Photoelectron emission microscopy (PEEM) is a versatile...

329

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in...

330

SUBMOLECULAR IMAGING OF EPITAXIALLY CRYSTALLIZED HELICAL POLYOLEFINS BY ATOMIC FORCE MICROSCOPY  

E-Print Network (OSTI)

Digital Instruments, Inc., Santa Barbara, Cal. USA. Images were taken with an A­type scan head (max. scan microscopy EM and electron diffraction ED. AFM pictures with high resolution could be obtained when using polypropylene has been determined by electron microscopy EM and electron diffraction ED: chain conformation

Peters, Achim

331

Microscopy. I: A Review  

Science Journals Connector (OSTI)

...indicates the spindle to be an orienting force through which a co-ordinated con tractile...asoT,E. M. and M@&soN,C. W. Handbook of Chemi cal Microscopy. Vol. 1. 1st...498 "586,1950. 164. NAORA, H. Fundamental Studies on the Determination of Desoxypentose-Nucleic...

Robert C. Mellors

1953-02-01T23:59:59.000Z

332

San Luis Transmission Project  

NLE Websites -- All DOE Office Websites (Extended Search)

Luis Transmission Project EIS/EIR Luis Transmission Project EIS/EIR San Luis Transmission Project EIS/EIR Western proposes to construct, own, operate, and maintain a new 230-kilovolt transmission line about 62 miles in length between Western's Tracy Substation and Western's San Luis Substation and a new 70-kV transmission line about 5 miles in length between the San Luis and O'Neill Substations. Western also will consider other transmission construction options including: A new 500-kV transmission line about 62 miles in length operated at 230-kV between Western's Tracy and San Luis Substations; A new 500-kV transmission line operated at 500-kV about 62 miles in length between the Tracy Substation and Pacific Gas and Electric's Los Banos Substation; and A new 230-kV transmission line about 18 miles in length between San Luis Substation and Dos Amigos Substation.

333

National Transmission Grid Study  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Grid Study Grid Study U.S. Department of Energy The Honorable Spencer Abraham Secretary of Energy May 2002 ii National Transmission Grid Study National Transmission Grid Study i ii National Transmission Grid Study National Transmission Grid Study iii How This Study Was Conducted The National Energy Policy Plan directed the U.S. Department of Energy (DOE) to conduct a study to examine the benefits of establishing a national electricity transmission grid and to identify transmission bottlenecks and measures to address them. DOE began by conducting an independent analysis of U.S. electricity markets and identifying transmission system bottlenecks using DOE's Policy Office Electricity Modeling System (POEMS). DOE's analysis, presented in Section 2, confirms the central role of the nation's transmission

334

Transmission | Open Energy Information  

Open Energy Info (EERE)

Gateway Gateway Edit History Facebook icon Twitter icon » Transmission (Redirected from Transmission) Jump to: navigation, search Transmission header.png Transmission Dashboard Permitting Atlas Compare States Arizona California Colorado Idaho Montana Nevada New Mexico Oregon Utah Washington Wyoming Resource Library NEPA Database Transmission Lattice.jpg High-voltage transmission lines form the backbone of electricity systems. Transmission lines are designed to carry large amounts of electricity at high voltages, typically 115 to 500 kilovolts (kV), across long distances. Networks of transmission lines transfer electricity from power plants or other interconnections to substations. At substations, the high-voltage electricity is "stepped down" to a lower voltage, which can be carried

335

STRATEGIC TRANSMISSION INVESTMENT PLAN  

E-Print Network (OSTI)

CALIFORNIA ENERGY COMMISSION STRATEGIC TRANSMISSION INVESTMENT PLAN Prepared in Support of the 2007. Blevins #12; i ACKNOWLEDGEMENTS The 2007 Strategic Transmission Investment Plan was prepared Investment Plan. California Energy Commission, Engineering Office. CEC7002007018CTF. #12; ii #12; iii

336

STRATEGIC TRANSMISSION INVESTMENT PLAN  

E-Print Network (OSTI)

CALIFORNIA ENERGY COMMISSION STRATEGIC TRANSMISSION INVESTMENT PLAN Prepared in Support of the 2007 Investment Plan was prepared with contribution from the following Energy Commission staff and consultants Kondoleon, Chuck Najarian. 2007 Strategic Transmission Investment Plan. California Energy Commission

337

Transmission Utilization Group (TUG)  

NLE Websites -- All DOE Office Websites (Extended Search)

Improvement (CBPI) Customer Forum Energy Imbalance Market Generator Interconnection Reform Implementation Intertie Initiatives Intertie Open Season Transmission Utilization...

338

Transmission Commercial Project Integration  

NLE Websites -- All DOE Office Websites (Extended Search)

Improvement (CBPI) Customer Forum Energy Imbalance Market Generator Interconnection Reform Implementation Network Integration Transmission Service (NT Service) Network Open...

339

Underground Power Transmission  

Science Journals Connector (OSTI)

...The type of transmission line for a particular...will force rt transmission lines to be ground near...history of power transmission shows that d-c...characteristics of a d-c line, it is easy to...Best data fit III II I...

P. H. Rose

1970-10-16T23:59:59.000Z

340

Vice President, Transmission Marketing & Sales  

Energy.gov (U.S. Department of Energy (DOE))

Within Transmission Services at Bonneville Power Administration (BPA), Transmission Marketing and Sales (TS) provides open access to the Federal Transmission System (FTS) consistent with...

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Nuclear emission microscopies B.L. Doyle a,*, D.S. Walsh a  

E-Print Network (OSTI)

Nuclear emission microscopies B.L. Doyle a,*, D.S. Walsh a , S.N. Renfrow a,b , G. Vizkelethy a,1 Abstract Alternatives to traditional nuclear microprobe analysis (NMA) emerged two years ago with the invention of ion electron emission microscopy (IEEM). With nuclear emission microscopy (NEM) the ion beam

342

Transmission | Open Energy Information  

Open Energy Info (EERE)

source source History View New Pages Recent Changes All Special Pages Semantic Search/Querying Get Involved Help Apps Datasets Community Login | Sign Up Search Gateway Edit History Facebook icon Twitter icon » Transmission Jump to: navigation, search Transmission header.png Transmission Dashboard Permitting Atlas Compare States Arizona California Colorado Idaho Montana Nevada New Mexico Oregon Utah Washington Wyoming Resource Library NEPA Database Transmission Lattice.jpg High-voltage transmission lines form the backbone of electricity systems. Transmission lines are designed to carry large amounts of electricity at high voltages, typically 115 to 500 kilovolts (kV), across long distances. Networks of transmission lines transfer electricity from power plants or other interconnections to substations. At substations, the high-voltage

343

Mapping Ionic Currents and Reactivity on the Nanoscale: Electrochemical Strain Microscopy  

SciTech Connect

Solid-state electrochemical processes in oxides underpin a broad spectrum of energy and information storage devices, ranging from Li-ion and Li-air batteries, to solid oxide fuel cells (SOFC) to electroresistive and memristive systems. These functionalities are controlled by the bias-driven diffusive and electromigration transport of mobile ionic species, as well as intricate a set of electrochemical and defect-controlled reactions at interfaces and in bulk. Despite the wealth of device-level and atomistic studies, little is known on the mesoscopic mechanisms of ion diffusion and electronic transport on the level of grain clusters, individual grains, and extended defects. The development of the capability for probing ion transport on the nanometer scale is a key to deciphering complex interplay between structure, functionality, and performance in these systems. Here we introduce Electrochemical Strain Microscopy, a scanning probe microscopy technique based on strong strain-bias coupling in the systems in which local ion concentrations are changed by electrical fields. The imaging capability, as well as time- and voltage spectroscopies analogous to traditional current based electrochemical characterization methods are developed. The reversible intercalation of Li and mapping electrochemical activity in LiCoO2 is demonstrated, illustrating higher Li diffusivity at non-basal planes and grain boundaries. In Si-anode device structure, the direct mapping of Li diffusion at extended defects and evolution of Li-activity with charge state is explored. The electrical field-dependence of Li mobility is studied to determine the critical bias required for the onset of electrochemical transformation, allowing reaction and diffusion processes in the battery system to be separated at each location. Finally, the applicability of ESM for probing oxygen vacancy diffusion and oxygen reduction/evolution reactions is illustrated, and the high resolution ESM maps are correlated with aberration corrected scanning transmission electron microscopy imaging. The future potential for deciphering mechanisms of electrochemical transformations on an atomically-defined single-defect level is discussed.

Kalinin, S.V. (Center for Nanophase Materials Sciences, ORNL) [Center for Nanophase Materials Sciences, ORNL

2010-10-19T23:59:59.000Z

344

Cryo-Transmission Electron Microscope (TEM) | EMSL  

NLE Websites -- All DOE Office Websites (Extended Search)

film consisting of glucose oxidasePtfunctional graphene sheetschitosan (GODPtFGSchitosan) for glucose sensing was... Multiplexed Electrochemical Immunoassay of...

345

Advanced electron microscopic techniques applied to the characterization of irradiation effects and fission product identification of irradiated TRISO coated particles from the AGR-1 experiment  

SciTech Connect

Preliminary electron microscopy of coated fuel particles from the AGR-1 experiment was conducted using characterization techniques such as scanning electron microscopy (SEM), transmission electron microscopy (TEM), energy dispersive spectroscopy (EDS), and wavelength dispersive spectroscopy (WDS). Microscopic quantification of fission-product precipitates was performed. Although numerous micro- and nano-sized precipitates observed in the coating layers during initial SEM characterization of the cross-sections, and in subsequent TEM diffraction patterns, were indexed as UPd{sub 2}Si{sub 2}, no Ag was conclusively found. Additionally, characterization of these precipitates highlighted the difficulty of measuring low concentrations of Ag in precipitates in the presence of significantly higher concentrations of Pd and U. The electron microscopy team followed a multi-directional and phased approach in the identification of fission products in irradiated TRISO fuel. The advanced electron microscopy techniques discussed in this paper, not only demonstrate the usefulness of the equipment (methods) as relevant research tools, but also provide relevant scientific results which increase the knowledge about TRISO fuel particles microstructure and fission products transport.

Rooyen, I.J. van; Lillo, T.M.; Trowbridge, T.L.; Madden, J.M. [Idaho National Laboratory, Idaho Falls, ID 83415-6188 (United States); Wu, Y.Q. [Boise State University, Boise, ID 83725-2090 (United States); Center for Advanced Energy Studies, Idaho Falls, ID 83401 (United States); Goran, D. [Brucker Nano Gmbh, Berlin, 12489 (Germany)

2013-07-01T23:59:59.000Z

346

Series Transmission Line Transformer  

DOE Patents (OSTI)

A series transmission line transformer is set forth which includes two or more of impedance matched sets of at least two transmissions lines such as shielded cables, connected in parallel at one end ans series at the other in a cascading fashion. The cables are wound about a magnetic core. The series transmission line transformer (STLT) which can provide for higher impedance ratios and bandwidths, which is scalable, and which is of simpler design and construction.

Buckles, Robert A. (Livermore, CA); Booth, Rex (Livermore, CA); Yen, Boris T. (El Cerrito, CA)

2004-06-29T23:59:59.000Z

347

Instrument Series: Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Quanta 3D FEG Quanta 3D FEG This instrument is now available in EMSL's Radiochemistry Annex. The Quanta 3D FEG is the most versatile high-resolution, low vacuum SEM/FIB for 2D and 3D material characterization and analysis. Featuring three imaging modes - high vacuum, low vacuum and ESEM - it accommodates the widest range of samples of any SEM system. The Quanta 3D FEG's novel, field-emission electron source delivers clear and sharp electron imaging and increased electron beam current enhances EDS and EBSP analysis. This system also offers the capability for in situ study of the dynamic behavior of materials at different humidity levels (up to 100% RH) and temperatures (up to 1500 °C). Quanta 3D FEG's unprecedented high- current FIB enables fast material removal.

348

Stream Control Transmission Protocol  

Science Journals Connector (OSTI)

This document describes the Stream Control Transmission Protocol (SCTP). SCTP is designed to transport PSTN signaling messages over IP networks, but is capable of broader applications.

R. Stewart; Q. Xie; K. Morneault; C. Sharp; H. Schwarzbauer; T. Taylor; I. Rytina; M. Kalla; L. Zhang; V. Paxson

2000-10-01T23:59:59.000Z

349

STRATEGIC TRANSMISSION INVESTMENT PLAN  

E-Print Network (OSTI)

CALIFORNIA ENERGY COMMISSION STRATEGIC TRANSMISSION INVESTMENT PLAN Prepared in Support of the 2005............................................................................................ 5 Project Investment Recommendations ............................................................... 6 Actions to Implement Investments

350

STRATEGIC TRANSMISSION INVESTMENT PLAN  

E-Print Network (OSTI)

CALIFORNIA ENERGY COMMISSION STRATEGIC TRANSMISSION INVESTMENT PLAN Prepared in Support of the 2005............................................................................................ 5 Project Investment Recommendations ............................................................... 5 Actions to Implement Investments

351

Probing graphene defects and estimating graphene quality with optical microscopy  

SciTech Connect

We report a simple and accurate method for detecting graphene defects that utilizes the mild, dry annealing of graphene/Cu films in air. In contrast to previously reported techniques, our simple approach with optical microscopy can determine the density and degree of dislocation of defects in a graphene film without inducing water-related damage or functionalization. Scanning electron microscopy, confocal Raman and atomic force microscopy, and X-ray photoelectron spectroscopy analysis were performed to demonstrate that our nondestructive approach to characterizing graphene defects with optimized thermal annealing provides rapid and comprehensive determinations of graphene quality.

Lai, Shen [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Center for Human Interface Nanotechnology (HINT), Suwon 440-746 (Korea, Republic of); Kyu Jang, Sung [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Jae Song, Young, E-mail: yjsong@skku.edu [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Department of Physics, Sungkyunkwan University (SKKU), Suwon 440-746 (Korea, Republic of); Lee, Sungjoo, E-mail: leesj@skku.edu [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Center for Human Interface Nanotechnology (HINT), Suwon 440-746 (Korea, Republic of); College of Information and Communication Engineering, Sungkyunkwan University (SKKU), Suwon 440-746 (Korea, Republic of)

2014-01-27T23:59:59.000Z

352

Single-crystal nanowires grown via electron-beam-induced deposition  

SciTech Connect

Electron-beam-induced deposition (EBID) is a useful technique for direct-writing of 3-dimensional dielectric, semiconductor, and metallic materials with nanoscale precision and resolution. The EBID process, however, has been limited in many cases because precursor byproducts (typically from organic precursors like W(CO)6) are incorporated into the deposited material resulting in contaminated and amorphous structures. In this manuscript, we have investigated the structure and composition of EBID tungsten nanostructures as-deposited from a tungsten hexafluoride (WF6) precursor. High-resolution transmission electron microscopy, electron diffraction and electron spectroscopy were employed to determine the effects that the electron beam scanning conditions have on the deposit characteristics. The results show that slow, one-dimensional lateral scanning produces textured -tungsten nanowire cores surrounded by an oxide secondary layer, while stationary vertical growth leads to single-crystal [100]-oriented W3O nanowires. Furthermore we correlate how the growth kinetics affect the resultant nanowire structure and composition.

Klein, Kate L [ORNL; Randolph, Steven J [ORNL; Fowlkes, Jason Davidson [ORNL; Allard Jr, Lawrence Frederick [ORNL; Meyer III, Harry M [ORNL; Simpson, Michael L [ORNL; Rack, Philip D [ORNL

2008-01-01T23:59:59.000Z

353

Introduction to Photoelectron Emission Microscopy: Principles...  

NLE Websites -- All DOE Office Websites (Extended Search)

Introduction to Photoelectron Emission Microscopy: Principles and Applications. Introduction to Photoelectron Emission Microscopy: Principles and Applications. Abstract: In the...

354

Magnetically insulated transmission line oscillator  

DOE Patents (OSTI)

A magnetically insulated transmission line oscillator employs self-generated magnetic fields to generate microwave energy. An anode of the oscillator includes slow-wave structures which are formed of a plurality of thin conductive vanes defining cavities therebetween, and a gap is formed between the anode and a cathode of the oscillator. In response to a pulsed voltage applied to the anode and cathode, self-generated magnetic fields arfe produced in a cross-field orientation with respect to the orientation of the electric field between the anode and the cathode. The cross-field magnetic fields insulate the flow of electrons in the gap and confine the flow of electrons within the gap.

Bacon, Larry D. (Albuquerque, NM); Ballard, William P. (Albuquerque, NM); Clark, M. Collins (Albuquerque, NM); Marder, Barry M. (Albuquerque, NM)

1988-01-01T23:59:59.000Z

355

Chapter 11 - Light sheet microscopy  

Science Journals Connector (OSTI)

Abstract This chapter introduces the concept of light sheet microscopy along with practical advice on how to design and build such an instrument. Selective plane illumination microscopy is presented as an alternative to confocal microscopy due to several superior features such as high-speed full-frame acquisition, minimal phototoxicity, and multiview sample rotation. Based on our experience over the last 10 years, we summarize the key concepts in light sheet microscopy, typical implementations, and successful applications. In particular, sample mounting for long time-lapse imaging and the resulting challenges in data processing are discussed in detail.

Michael Weber; Michaela Mickoleit; Jan Huisken

2014-01-01T23:59:59.000Z

356

Transmission Line Security Monitor  

SciTech Connect

The Transmission Line Security Monitor is a multi-sensor monitor that mounts directly on high-voltage transmission lines to detect, characterize and communicate terrorist activity, human tampering and threatening conditions around support towers. For more information about INL's critical infrastructure protection research, visit http://www.facebook.com/idahonationallaboratory.

None

2011-01-01T23:59:59.000Z

357

Transmission Line Security Monitor  

ScienceCinema (OSTI)

The Transmission Line Security Monitor is a multi-sensor monitor that mounts directly on high-voltage transmission lines to detect, characterize and communicate terrorist activity, human tampering and threatening conditions around support towers. For more information about INL's critical infrastructure protection research, visit http://www.facebook.com/idahonationallaboratory.

None

2013-05-28T23:59:59.000Z

358

WHOLE CELL TOMOGRAPHY/MOLECULAR BIOLOGY/STRUCTURAL BIOLOGY: Affordable x-ray microscopy with nanoscale resolution  

SciTech Connect

Biological research spans 10 orders of magnitude from angstroms to meters. While electron microscopy can reveal structural details at most of these spatial length scales, transmission electron tomography only reliably reconstructs three-dimensional (3-D) volumes of cellular material with a spatial resolution between 1-5 nm from samples less than 500 nm thick1. Most biological cells are 2-30 times thicker than this threshold, which means that a cell must be cut into consecutive slices with each slice reconstructed individually in order to approximate the contextual information of the entire cell. Fortunately, due to a larger penetration depth2, X-ray computed tomography bypasses the need to physically section a cell and enables imaging of intact cells and tissues on the micrometer or larger scale with tens to hundreds of nanometer spatial resolution. While the technique of soft x-ray microscopy has been extensively developed in synchrotron facilities, advancements in laboratory x-ray source designs now increase its accessibility by supporting commercial systems suitable for a standard laboratory. In this paper, we highlight a new commercial compact cryogenic soft x-ray microscope designed for a standard laboratory setting and explore its capabilities for mesoscopic investigations of intact prokaryotic and eukaryotic cells.

Evans, James E.; Blackborow, Paul; Horne, Stephen J.; Gelb, Jeff

2013-03-01T23:59:59.000Z

359

Subject: SPPR Proposed ED5 to Palo Verde Transmission Project  

NLE Websites -- All DOE Office Websites (Extended Search)

Date: 832010 4:02 PM Subject: SPPR Proposed ED5 to Palo Verde Transmission Project VIA ELECTRONIC MAIL TO: DSWFPP@wapa.gov August 3, 2010 Mr. Darrick...

360

Subject: SPPR Proposed ED5 to Palo Verde Transmission Project  

NLE Websites -- All DOE Office Websites (Extended Search)

Date: 832010 4:04 PM Subject: SPPR Proposed ED5 to Palo Verde Transmission Project VIA ELECTRONIC MAIL TO: DSWFPP@wapa.gov August 3, 2010 Mr. Darrick...

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

EIS-0411: Transmission Agency of Northern California Transmission Project  

Energy.gov (U.S. Department of Energy (DOE))

This EIS is for the Western Area Power Administration construction, operation, and maintenance of the proposed transmission agency of Northern California Transmission Project, California.

362

Foil Electron Multiplier  

NLE Websites -- All DOE Office Websites (Extended Search)

Foil Electron Multiplier Foil Electron Multiplier Foil Electron Multiplier An apparatus for electron multiplication by transmission that is designed with at least one foil having a front side for receiving incident particles and a back side for transmitting secondary electrons that are produced from the incident particles transiting through the foil. Available for thumbnail of Feynman Center (505) 665-9090 Email Foil Electron Multiplier An apparatus for electron multiplication by transmission that is designed with at least one foil having a front side for receiving incident particles and a back side for transmitting secondary electrons that are produced from the incident particles transiting through the foil. The foil thickness enables the incident particles to travel through the foil and continue on

363

Transmission Access Resources  

Energy.gov (U.S. Department of Energy (DOE))

Historically, the addition of new electric generation facilities has been accompanied by new transmission systems. For example, large nuclear and coal plants built in the 1960s and 1970s required...

364

Performance Incentives for Transmission  

E-Print Network (OSTI)

The Federal Energy Regulatory Commission's Standard Market Design Notice of Public Rule- making (SMD NOPRPerformance Incentives for Transmission FERC's Standard Market Design should accommodate of California at Berkeley. The research described in this article was supported by National Grid, USA

Oren, Shmuel S.

365

Designing electricity transmission auctions  

E-Print Network (OSTI)

The UK has ambitious plans for exploiting offshore wind for electricity production in order to meet its challenging target under the EU Renewable Energy Directive. This could involve investing up to 20bn in transmission assets to bring electricity...

Greve, Thomas; Pollitt, Michael G.

2012-10-26T23:59:59.000Z

366

Electric Transmission Lines (Iowa)  

Energy.gov (U.S. Department of Energy (DOE))

Electric transmission lines capable of operating at 69 kV or greater cannot be constructed along, across, or over any public highways or grounds outside of cities without a franchise from the...

367

Audio Transmission Systems  

Science Journals Connector (OSTI)

Audio transmission systems are the means by which audio signals are routed, processed, and assigned to the desired monitor and recording output channels. In the early days of electrical recording, rarely more ...

John Eargle

1986-01-01T23:59:59.000Z

368

Transmission Grid Integration  

Energy.gov (U.S. Department of Energy (DOE))

The levels of solar energy penetration envisioned by the DOE SunShot Initiative must be interconnected effectively onto the transmission grid. This interconnection requires an in-depth...

369

Honda Transmission Technical Center  

Russells Point, OH The Honda Transmission Technical Center is located on the Honda of America Manufacturing Plant facility site in Russells Point, Ohio. This facility is used for product engineering and market quality testing and analysis of automatic transmissions. The building contains a large workshop area for ten cars, a future dynamometer, two laboratories, an open office area, three conference rooms, a break room, restrooms, and related support areas.

370

EC Transmission Line Risk Identification and Analysis  

SciTech Connect

The purpose of this document is to assist in evaluating and planning for the cost, schedule, and technical project risks associated with the delivery and operation of the EC (Electron cyclotron) transmission line system. In general, the major risks that are anticipated to be encountered during the project delivery phase associated with the implementation of the Procurement Arrangement for the EC transmission line system are associated with: (1) Undefined or changing requirements (e.g., functional or regulatory requirements) (2) Underperformance of prototype, first unit, or production components during testing (3) Unavailability of qualified vendors for critical components Technical risks associated with the design and operation of the system are also identified.

Bigelow, Tim S [ORNL

2012-04-01T23:59:59.000Z

371

Transmission Right Of Way  

NLE Websites -- All DOE Office Websites (Extended Search)

About SNR > Right Of Way About SNR > Right Of Way Right Of Way Preferred Vegetation List - Redding & Foothills (XLS - 23K) Preferred Vegetation List - Sacramento Valley (XLS - 170K) WESTERN AREA POWER ADMINISTRATION GENERAL GUIDELINES CONCERNING THE USE OF ELECTRIC TRANSMISSION LINE RIGHTS-OF-WAY Western Area Power Administration (Western) owns a right-of-way easement along the length of the transmission line (width varies by transmission line). Western's rights within the easement include the right to construct, reconstruct, operate, maintain, and patrol the transmission line. Rights usually reserved to the landowner include the right to cultivate, occupy, and use the land for any purpose that does not conflict with Western's use of its easement. To avoid potential conflicts, it is Western's policy to review all proposed uses within the transmission line easement. We consider (1) Safety of the public, (2) Safety of our Employees, (3) Restrictions covered in the easement, (4) Western's maintenance requirements, and (5) Protection of the transmission line structures and (6) Road or street crossings.

372

Open Access Transmission Tariff  

NLE Websites -- All DOE Office Websites (Extended Search)

Transmission | OATT Transmission | OATT Skip Navigation Links Transmission Functions Infrastructure projects Interconnection OASIS OATT Western Open Access Transmission Service Tariff Revision Western Area Power Administration submitted its revised Open Access Transmission Service Tariff with the Federal Energy Regulatory Commission on Sept. 30, 2009. The tariff became effective on Dec. 1, 2009, as modified by Western's March 2, 2011 compliance filing. The revised tariff was developed to comply with FERC Order No. 890 and to be consistent with Western's statutory and regulatory requirements. It addresses changes in transmission services and planning. FERC issued an order on Dec. 2, 2010, granting Western's petition for a Declaratory Order approving the tariff as an acceptable reciprocity tariff, subject to Western making a compliance filing within 30 days to address items in Attachment C, Attachment P and Attachment Q. Western made its compliance filing on March 2, 2010, addressing FERC's Dec. 2, 2010, order. FERC accepted Western's March 2, 2011 compliance filing on April 25, 2011. Western has made several ministerial filings to its OATT as part of FERC's eTariff viewer system, the last of these was approved on March 29, 2013. Further detail can be found in the links below.Current OATT

373

Colorado/Transmission/Agencies | Open Energy Information  

Open Energy Info (EERE)

Agencies < Colorado | Transmission Jump to: navigation, search Colorado Transmission Roadmap Agency Links Local Regulations State Regulations Summary General Transmission...

374

National Electric Transmission Congestion Study Webinars | Department...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

National Electric Transmission Congestion Study National Electric Transmission Congestion Study Webinars National Electric Transmission Congestion Study Webinars The Department...

375

Transmission Planning | Department of Energy  

Office of Environmental Management (EM)

Planning Transmission Planning Modernizing America's electricity infrastructure is one of the U.S. Department of Energy's top priorities. The National Transmission Grid Study made...

376

E-Print Network 3.0 - atomic resolution transmission Sample Search...  

NLE Websites -- All DOE Office Websites (Extended Search)

Colorado at Boulder Collection: Physics 38 Spectroscopic Imaging of Single AtomsWithin a Bulk Solid S. D. Findlay,2 Summary: transmission electron microscope (STEM) allows not...

377

Electricity Transmission, A Primer | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Transmission, A Primer Electricity Transmission, A Primer This primer on electric transmission is intended to help policymakers understand the physics of the transmission system,...

378

Hybrid Transmission Corridor study  

SciTech Connect

Hybrid Transmission Corridors are areas where High Voltage Alternating Current (HVAC) transmission lines and High Voltage Direct Current (HVDC) transmission lines exist in close proximity of each other. Because of the acceptance of HVDC as a means of transporting electric power over long distances and the difficulties associated with obtaining new right-of-ways, HVDC lines may have to share the same transmission corridor with HVAC lines. The interactions between conductors energized with different types of voltages causes changes in the electrical stresses applied to the conductors and insulators. As a result, corona phenomena, field effects and insulation performance can be affected. This report presents the results of an investigation of the HVAC-HVDC interaction and its effect on corona and AC and DC electric field phenomena. The method of investigation was based on calculation methods developed at the EPRI High Voltage Transmission Research Center (HVTRC) and supported by the results of full and reduced-scale line tests. Also, a survey of existing hybrid corridors is given along with the results of measurements made at one of those corridors. A number of examples in which an existing AC corridor may be transformed into a hybrid corridor are discussed. The main result of the research is an analytical/empirical model for predicting the electrical/environmental performance of hybrid corridors, a definition of ACDC interaction and a set of criteria for specifying when the interaction becomes significant, and a set of design rules.

Clairmont, B.A.; Johnson, G.B.; Zaffanella, L.E. (General Electric Co., Lenox, MA (United States))

1992-06-01T23:59:59.000Z

379

transmission | OpenEI  

Open Energy Info (EERE)

transmission transmission Dataset Summary Description This dataset represents a historical repository of all the numerical data from the smartgrid.gov website condensed into spreadsheets to enable analysis of the data. Below are a couple of things worth noting: Source Smartgrid.gov Date Released March 04th, 2013 (9 months ago) Date Updated March 04th, 2013 (9 months ago) Keywords AMI costs distribution smart grid transmission Data application/vnd.openxmlformats-officedocument.spreadsheetml.sheet icon SmartGrid.gov Quarterly Data Summary 4Q12 (xlsx, 112.1 KiB) application/vnd.openxmlformats-officedocument.spreadsheetml.sheet icon SmartGrid.gov Quarterly Data Summary 3Q12 (xlsx, 107.9 KiB) application/vnd.openxmlformats-officedocument.spreadsheetml.sheet icon SmartGrid.gov Quarterly Data Summary 2Q12 (xlsx, 111.9 KiB)

380

NREL: Energy Analysis: Transmission Infrastructure  

NLE Websites -- All DOE Office Websites (Extended Search)

Transmission Infrastructure Transmission Infrastructure Grid expansion and planning to allow large scale deployment of renewable generation Large scale deployment of renewable electricity generation will require additional transmission to connect renewable resources, which are wide-spread across the US, but regionally-constrained, to load centers. Long-term transmission planning, based on potential future growth in electric loads and generation resource expansion options, is critical to maintaining the necessary flexibility required for a reliable and robust transmission system. NREL's analyses support transmission infrastructure planning and expansion to enable large-scale deployment of renewable energy in the future. NREL's transmission infrastructure expansion and planning analyses show

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

Printed circuit dispersive transmission line  

DOE Patents (OSTI)

A printed circuit dispersive transmission line structure is disclosed comprising an insulator, a ground plane formed on one surface of the insulator, a first transmission line formed on a second surface of the insulator, and a second transmission line also formed on the second surface of the insulator and of longer length than the first transmission line and periodically intersecting the first transmission line. In a preferred embodiment, the transmission line structure exhibits highly dispersive characteristics by designing the length of one of the transmission line between two adjacent periodic intersections to be longer than the other. 5 figures.

Ikezi, H.; Lin-Liu, Y.R.; DeGrassie, J.S.

1991-08-27T23:59:59.000Z

382

Printed circuit dispersive transmission line  

DOE Patents (OSTI)

A printed circuit dispersive transmission line structure is disclosed comprising an insulator, a ground plane formed on one surface of the insulator, a first transmission line formed on a second surface of the insulator, and a second transmission line also formed on the second surface of the insulator and of longer length than the first transmission line and periodically intersecting the first transmission line. In a preferred embodiment, the transmission line structure exhibits highly dispersive characteristics by designing the length of one of the transmission line between two adjacent periodic intersections to be longer than the other.

Ikezi, Hiroyuki (Rancho Santa Fe, CA); Lin-Liu, Yuh-Ren (San Diego, CA); DeGrassie, John S. (Encinitas, CA)

1991-01-01T23:59:59.000Z

383

Transmission line capital costs  

SciTech Connect

The displacement or deferral of conventional AC transmission line installation is a key benefit associated with several technologies being developed with the support of the U.S. Department of Energy`s Office of Energy Management (OEM). Previous benefits assessments conducted within OEM have been based on significantly different assumptions for the average cost per mile of AC transmission line. In response to this uncertainty, an investigation of transmission line capital cost data was initiated. The objective of this study was to develop a database for preparing preliminary estimates of transmission line costs. An extensive search of potential data sources identified databases maintained by the Bonneville Power Administration (BPA) and the Western Area Power Administration (WAPA) as superior sources of transmission line cost data. The BPA and WAPA data were adjusted to a common basis and combined together. The composite database covers voltage levels from 13.8 to 765 W, with cost estimates for a given voltage level varying depending on conductor size, tower material type, tower frame type, and number of circuits. Reported transmission line costs vary significantly, even for a given voltage level. This can usually be explained by variation in the design factors noted above and variation in environmental and land (right-of-way) costs, which are extremely site-specific. Cost estimates prepared from the composite database were compared to cost data collected by the Federal Energy Regulatory Commission (FERC) for investor-owned utilities from across the United States. The comparison was hampered because the only design specifications included with the FERC data were voltage level and line length. Working within this limitation, the FERC data were not found to differ significantly from the composite database. Therefore, the composite database was judged to be a reasonable proxy for estimating national average costs.

Hughes, K.R.; Brown, D.R.

1995-05-01T23:59:59.000Z

384

Even-odd oscillation and valley polarization of transmission between multilayer graphenes  

SciTech Connect

Electron transmission through a boundary between multi-layer graphenes with Bernal stacking consisting of different number of layers is studied. A valley polarization in transmission probability appears as in monolayer and bilayer systems, exhibits considerable oscillation depending of even or odd layer numbers, and its amplitude gradually decreases with the layer number. The total transmission shows oscillation with much smaller amplitude.

Nakanishi, Takeshi [Nanosystem Research Institute, AIST, 1-1-1 Umezono, Tsukuba 305-8568 (Japan); Ando, Tsuneya [Department of Physics, Tokyo Institute of Technology, 2-12-1 Ookayama, Meguro-ku, Tokyo 152-8551 (Japan)

2013-12-04T23:59:59.000Z

385

PHYSICAL REVIEW B 87, 144301 (2013) Parametric amplification in Josephson junction embedded transmission lines  

E-Print Network (OSTI)

transmission lines O. Yaakobi,1,* L. Friedland,2 C. Macklin,3 and I. Siddiqi3 1 INRS-EMT, 1650 Boul. Lionel; published 1 April 2013) An electronic transmission line that contains an array of nonlinear elements of the node flux along the transmission line is derived. It is shown that due to the nonlinearity

Friedland, Lazar

386

Enhanced Transmission Line Theory: Frequency-Dependent Line Parameters And Their Insertion in a  

E-Print Network (OSTI)

Enhanced Transmission Line Theory: Frequency- Dependent Line Parameters And Their Insertion in a Classical Transmission Line Equation Solver S. Chabane, P. Besnier IETR: Institute of Electronics--In this paper, a modified enhanced transmission- line theory taking into account higher-order modes is described

Paris-Sud XI, Université de

387

Electric Transmission System Workshop  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Lauren Azar Lauren Azar Senior Advisor to Secretary Chu November 2, 2012 Electric Transmission System Workshop We all have "visions," in one form or another: * Corporations call them strategic plans * RTOs ... transmission expansion plans or Order 1000 plans * State PUCs ... integrated resource plans * Employees ... career goals Visions for the Future Artist: Paolo Frattesi Artist: Paolo Frattesi Uncertainty = changing industry Changes in technology, threats and policies Can we make decisions in the face of change? .......How can we not? Can we agree on several key design attributes for the future grid? Taking Action in the Face of Uncertainty Step 1: Establish common ground on key design attributes GTT's Proposed Key Design Attributes:

388

10-Yr. Transmission Plan  

NLE Websites -- All DOE Office Websites (Extended Search)

Power Marketing Rates Power Marketing Rates 10-Yr Transmission Plan 2012 Customer Meeting Announcement Agenda 120611 CRSP South Projects CRSP South PowerPoint Presentation CRSP South 2009-2011 Capitalized Execution CRSP North Projects CRSP North PowerPoint Presentation CRSP North 2009-2011 Capitalized Execution About Power Marketing Transmission Newsroom Business Policies Products Plan contents OASIS News features Careers No FEAR act Organization chart Plan processes Functions News releases Doing business Privacy policy History General power contract provisions OATT Revisions Fact sheets Energy Services Accessibility Financial information Rates and Repayment Interconnection Publications EPTC Adobe PDF Power projects EPAMP Infrastructure projects Federal Register Notices

389

Transmission SEAB Presentation  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Overcoming Overcoming Institutional Barriers to Infrastructure Development Lauren Azar Senior Advisor to the Secretary U.S. Department of Energy January 31, 2012 Lauren"s Initiatives 1. Rapid Response Team for Transmission 2. Power Marketing Administrations 3. Project Development in the Southwest 4. Congestion Study and NIETC Designations 5. Miscellaneous  EPA Regulations  Market Power

390

Continuously variable transmission  

SciTech Connect

This patent describes a power transmission apparatus. It comprises: a body, a pinion gear, a cam means, first and second gear rack pairs, preventing means;l first and second rack support means, a rotor mounted for rotation about a rotor axis, the rotor having rotor engaging means for engaging the rack support means so as to transmit power therebetween.

Irvin, P.J.E.

1992-07-14T23:59:59.000Z

391

Autonomous data transmission apparatus  

DOE Patents (OSTI)

A autonomous borehole data transmission apparatus for transmitting measurement data from measuring instruments at the downhole end of a drill string by generating pressure pulses utilizing a transducer longitudinally responsive to magnetic field pulses caused by electrical pulses corresponding to the measured downhole parameters.

Kotlyar, Oleg M. (4675 W. 3825 S, Salt Lake City, UT 84120)

1997-01-01T23:59:59.000Z

392

Borehole data transmission apparatus  

DOE Patents (OSTI)

A borehole data transmission apparatus is described whereby a centrifugal pump impeller(s) is used to provide a turbine stage having substantial pressure characteristics in response to changing rotational speed of a shaft for the pressure pulsing of data from the borehole through the drilling mud to the surface of the earth.

Kotlyar, O.M.

1993-03-23T23:59:59.000Z

393

X-Ray Diffraction Microscopy of Magnetic Structures  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

394

X-Ray Diffraction Microscopy of Magnetic Structures  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

395

X-Ray Diffraction Microscopy of Magnetic Structures  

NLE Websites -- All DOE Office Websites (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

396

Extraordinary optical transmission through patterned subwavelength apertures.  

SciTech Connect

Light propagating through a subwavelength aperture can be dramatically increased by etching a grating in the metal around the hole. Moreover, light that would typically broadly diverge when passing through an unpatterned subwavelength hole can be directed into a narrow beam by utilizing a specific pattern around the aperture. While the increased transmission and narrowed angular emission appear to defy far-field diffraction theory, they are consistent with a fortuitous plasmon/photon coupling. In addition, the coupling between photons and surface plasmons affects the emissivity of a surface comprised of such structures. These properties are useful across several strategic areas of interest to Sandia. A controllable emission spectrum could benefit satellite and military application areas. Photolithography and near-field microscopy are natural applications for a system that controls light beyond the diffraction limit in a manner that is easily parallelizable. Over the one year of this LDRD, we have built or modified the numerical tools necessary to model such structures. These numerical codes and the knowledge base for using them appropriately will be available in the future for modeling work on surface plasmons or other optical modeling at Sandia. Using these tools, we have designed and optimized structures for various transmission or emission properties. We demonstrate the ability to design a metallic skin with an emissivity peak at a pre-determined wavelength in the spectrum. We optimize structures for maximum light transmission and show transmitted beams that beat the far-field diffraction limit.

Kemme, Shanalyn A.; El-Kady, Ihab Fathy; Hadley, G. Ronald; Peters, David William; Lanes, Chris E.

2004-12-01T23:59:59.000Z

397

Regulations for Electric Transmission and Fuel Gas Transmission Lines Ten  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Electric Transmission and Fuel Gas Transmission Electric Transmission and Fuel Gas Transmission Lines Ten or More Miles Long (New York) Regulations for Electric Transmission and Fuel Gas Transmission Lines Ten or More Miles Long (New York) < Back Eligibility Commercial Fuel Distributor Investor-Owned Utility Municipal/Public Utility Rural Electric Cooperative Tribal Government Utility Savings Category Buying & Making Electricity Water Home Weatherization Solar Wind Program Info State New York Program Type Siting and Permitting Provider New York State Public Service Commission Any person who wishes to construct an electric or gas transmission line that is more than ten miles long must file documents describing the construction plans and potential land use and environmental impacts of the proposed transmission line. The regulations describe application and review

398

Transmission Developers Inc.  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

% ~ % ~ Transmission Developers Inc. July 7, 2011 Mr. Anthony J. Como Director, Permitting and Siting Office ofElectricity Delivery and Energy Reliability (OE-20) U.S. Department of Energy 1000 Independence A venue SW, Room 8G-024 Washington, D.C. 20585 Subject: Champlain Hudson Power Express Project U.S. Department of Energy Presidential Permit Application PP-362 Dear Mr. Como: On January 25, 2010, Transmission Developers, Inc. ("TDI'' or "Applicants") submitted on behalf of Champlain Hudson Power Express, Inc. ("CHPEI") an application to the U.S. Department of Energy ("DOE") for a Presidential Permit and an amendment on August 5, 2010 (collectively, the "Application") in connection with the Champlain Hudson Power Express

399

Transmission Siting_071508.indd  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Coordinating Interstate Electric Coordinating Interstate Electric Transmission Siting: An Introduction to the Debate The National Council on Electricity Policy 2 DISCLAIMER: The National Council on Electricity Policy is funded by the U.S. Department of Energy and the U.S. Environmental Protection Agency. The views and opinions expressed herein are strictly those of the authors and may not necessarily agree with the positions of the National Council on Electricity Policy, its committ ee members or the organizations they represent, the National Council funders, or those who commented on the paper during its draft ing. ACKNOWLEDGMENTS Coordinating Interstate Electric Transmission Siting: An Introduction to the Debate was prepared with the fi nancial assistance of a grant from the U.S. Department of Energy (DOE) Offi ce of Electricity Delivery

400

Drill string transmission line  

DOE Patents (OSTI)

A transmission line assembly for transmitting information along a downhole tool comprising a pin end, a box end, and a central bore traveling between the pin end and the box end, is disclosed in one embodiment of the invention as including a protective conduit. A transmission line is routed through the protective conduit. The protective conduit is routed through the central bore and the ends of the protective conduit are routed through channels formed in the pin end and box end of the downhole tool. The protective conduit is elastically forced into a spiral or other non-linear path along the interior surface of the central bore by compressing the protective conduit to a length within the downhole tool shorter than the protective conduit.

Hall, David R. (Provo, UT); Hall, Jr., H. Tracy (Provo, UT); Pixton, David S. (Lehi, UT); Bradford, Kline (Orem, UT); Fox, Joe (Spanish Fork, UT)

2006-03-28T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

Patterns of Transmission Investment  

E-Print Network (OSTI)

long term performance contracts with a developer of an HVDC transmission link to expand “interconnection” capacity between TSOs with no or limited interconnections and with large sustained differences in prices. Merchant investments supported... truly separate AC networks. For example, by building HVDC inter-connectors between two separate networks, opportunities to increase trades of power from high price to low priced areas can be exploited. The HVDC link between the England and France...

Joskow, Paul

2006-03-14T23:59:59.000Z

402

Boardman to Hemingway Transmission Project  

NLE Websites -- All DOE Office Websites (Extended Search)

Improvement (CBPI) Customer Forum Energy Imbalance Market Generator Interconnection Reform Implementation Network Integration Transmission Service (NT Service) Network Open...

403

Modulated microwave microscopy and probes used therewith  

DOE Patents (OSTI)

A microwave microscope including a probe tip electrode vertically positionable over a sample and projecting downwardly from the end of a cantilever. A transmission line connecting the tip electrode to the electronic control system extends along the cantilever and is separated from a ground plane at the bottom of the cantilever by a dielectric layer. The probe tip may be vertically tapped near or at the sample surface at a low frequency and the microwave signal reflected from the tip/sample interaction is demodulated at the low frequency. Alternatively, a low-frequency electrical signal is also a non-linear electrical element associated with the probe tip to non-linearly interact with the applied microwave signal and the reflected non-linear microwave signal is detected at the low frequency. The non-linear element may be semiconductor junction formed near the apex of the probe tip or be an FET formed at the base of a semiconducting tip.

Lai, Keji; Kelly, Michael; Shen, Zhi-Xun

2012-09-11T23:59:59.000Z

404

Free electron laser  

DOE Patents (OSTI)

A high gain, single-pass free electron laser formed of a high brilliance electron injector source, a linear accelerator which imparts high energy to the electron beam, and an undulator capable of extremely high magnetic fields, yet with a very short period. The electron injector source is the first stage (gap) of the linear accelerator or a radial line transformer driven by fast circular switch. The linear accelerator is formed of a plurality of accelerating gaps arranged in series. These gaps are energized in sequence by releasing a single pulse of energy which propagates simultaneously along a plurality of transmission lines, each of which feeds the gaps. The transmission lines are graduated in length so that pulse power is present at each gap as the accelerated electrons pass therethrough. The transmission lines for each gap are open circuited at their ends. The undualtor has a structure similar to the accelerator, except that the transmission lines for each gap are substantially short circuited at their ends, thus converting the electric field into magnetic field. A small amount of resistance is retained in order to generate a small electric field for replenishing the electron bunch with the energy lost as it traverses through the undulator structure.

Villa, Francesco (Alameda, CA)

1990-01-01T23:59:59.000Z

405

Transmission Line Circuit Alexander Glasser  

E-Print Network (OSTI)

Chaos in a Transmission Line Circuit Alexander Glasser Marshal Miller With... Prof. Edward Ott Prof times become shorter, circuit connections behave more and more like transmission lines. Theoretical(t) - Transmission Line (Zo, T) #12;5 Cf/Cr 1000 Vf Capacitance Voltage Cf Cr Model for Nonlinear Capacitor

Anlage, Steven

406

Characterization and Evolution of Tetrameric Photosystem I from the Thermophilic Cyanobacterium Chroococcidiopsis sp TS-821  

Science Journals Connector (OSTI)

...transmission electron microscopy|TEM, transmission electron microscopy...splitting of water with the reduction...ultracentrifugation (AUC), electron microscopy...a similar treatment was applied...gradient after dialysis and concentration...

Meng Li; Dmitry A. Semchonok; Egbert J. Boekema; Barry D. Bruce

2014-03-28T23:59:59.000Z

407

NREL: Transmission Grid Integration - Transmission Planning and Analysis  

NLE Websites -- All DOE Office Websites (Extended Search)

Transmission Planning and Analysis Transmission Planning and Analysis Thumbnail of map the United States that shows wind resources and transmission lines. Enlarge image This map shows the location of wind resources and transmission lines in the United States. See a larger image or state maps. NREL researchers are engaged in transmission planning and analysis to strengthen the electric power system through the integration of solar and wind power. As demand for electricity increases, electric power system operators must plan for and construct new generation and transmission lines. However, variable generation such as solar and wind power plants are often located far from the loads they serve. They depend on transmission lines to transport the electricity they produce to load centers. NREL is working with industry and utilities to address issues related to

408

Optical data transmission at the superconducting super collider  

SciTech Connect

Digital and analog data transmissions via fiber optics for the Superconducting Super Collider have been investigated. The state of the art of optical transmitters, low loss fiber waveguides, receivers and associated electronics components are reviewed and summarized. Emphasis is placed on the effects of the radiation environment on the performance of an optical data transmission system components. Also, the performance of candidate components of the wide band digital and analog transmission systems intended for deployment of the Superconducting Super Collider Detector is discussed. 27 refs., 15 figs.

Leskovar, B.

1989-02-01T23:59:59.000Z

409

Transmission/Photo Gallery | Open Energy Information  

Open Energy Info (EERE)

Colorado transmission 2.jpg Bird diverters.jpg Transmission insulators.jpg Retrieved from "http:en.openei.orgwindex.php?titleTransmissionPhotoGallery&oldid687595...

410

NREL: Transmission Grid Integration - Publications  

NLE Websites -- All DOE Office Websites (Extended Search)

Publications Publications Want updates about future transmission grid integration webinars and publications? Join our mailing list. NREL has an extensive collection of publications related to transmission integration research. Explore the resources below to learn more. Selected Project Publications Read selected publications related to these transmission integration projects: Western Wind and Solar Integration Study Eastern Renewable Generation Integration Study Oahu Wind Integration and Transmission Study Flexible Energy Scheduling Tool for Integration of Variable generation (FESTIV) Active power controls Forecasting Grid Simulation. NREL Publications Database NREL's publications database offers a variety of documents related to transmission integration that were written by NREL staff and

411

Electric Transmission Line Siting Compact  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Electric Transmission Line Siting Compact Electric Transmission Line Siting Compact 1 ______________________________________________________________________________ 2 ARTICLE I 3 PURPOSE 4 5 Siting electric transmission lines across state borders and federal lands is an issue for states, the 6 federal government, transmission utilities, consumers, environmentalists, and other stakeholders. 7 The current, multi-year application review process by separate and equal jurisdictions constitutes 8 a sometimes inefficient and redundant process for transmission companies and complicates the 9 efforts of state and federal policy-makers and other stakeholders to develop more robust 10 economic opportunities, increase grid reliability and security, and ensure the consumers have the 11 lowest cost electricity possible. 12

412

Transmission Workshop | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

DOE Grid Tech Team » Activities/Outreach » GTT DOE Grid Tech Team » Activities/Outreach » GTT Activities » Transmission Workshop Transmission Workshop Transmission Workshop GTT Transmission Workshop - November 1-2, 2012 On November 1-2, 2012, the GTT presented a workshop on grid integration on the transmission system at the DoubleTree Crystal City near Washington, DC. A draft of the DOE Action Plan Addressing the Electricity Transmission System was discussed during the workshop, which addressed the challenges and opportunities presented by the integration of 21st century energy technologies into the electricity transmission system. Parallel sessions addressed the challenges and opportunities of modernizing the grid and drilled down into key technology areas associated with each of these: System visibility: what advances are needed to "see" the state of

413

Terahertz Quantum-Cascade Transmission-Line Metamaterials  

E-Print Network (OSTI)

Terahertz Transmission-Line Metamaterials . . . . . . .CRLH Transmission Lines . . . . . . . . . . . . . . . .Terahertz CRLH Transmission-Line Metamaterials . . . . . . .

Tavallaee, Amir Ali

2012-01-01T23:59:59.000Z

414

Abstract --Under a context of transmission open access, a methodology to define a common transmission trunk system  

E-Print Network (OSTI)

Terms--Transmission systems, Transmission pricing, Cooperative games, Shapley value, Transmission open

Catholic University of Chile (Universidad Católica de Chile)

415

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

NLE Websites -- All DOE Office Websites (Extended Search)

3010 In-Situ 3010 In-Situ AEME The 300 kV JEOL 3010 offers greater specimen penetration than 200kV instruments, with significantly improved spatial resolution and probe forming capabilities. The side-entry stage allows ±45° tilt and can be operated with piezo-drift compensation. A flexible condenser system permits CBED, LACBED, and imaging with hollow cone and Koehler illumination. In addition to a standard film camera, a Gatan Orius CCD, and a Gatan 622 intensified TV camera and VCR are available for recording experiments at video rates. Specific capabilities include: high-resolution imaging at 2.1Å and ±40° tilt during simultaneous heating; very-high-resolution imaging at 1.7 Å and ±10° tilt during simultaneous heating; and high magnification Lorentz and Foucault imaging of magnetic samples. Various

416

NCEM National Center for Electron Microscopy: Heating holder guidelines  

NLE Websites -- All DOE Office Websites (Extended Search)

Heating holder guidelines Heating holder guidelines If you plan to use heating holders for in-situ experiments, we require your careful review and compliance with the following guidelines. 1. Include in your proposal target temperature and all phase diagrams of material with those of the tantalum furnaces and tantalum and/or molybdenum washers. Eutectic melting or bonding to the furnace body can occur at much lower temperatures than expected. 2. Holders are individually marked with the maximum temperature displayed on the specimen rod. Do not exceed this marked maximum temperature. It is easy to overshoot target temperature, so approach with caution. 3. Pre-schedule time for technical training and assistance by NCEM staff, especially if you are an infrequent or first-time user.

417

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......relationship was found between the appearance of aerial mycelia, production of soluble pigments...Intestine : Saburo ISHII (Dept. of Anat., Fukushima Med. Col., Sugitsuma-cho, Fukushima) Fukushima J. Med. Sci., 12 (1-2), 67~87......

ABSTRACT

1966-01-01T23:59:59.000Z

418

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......Kazumi MAEDA (Dept. of Ophth., Osaka Univ. Medical School, Fukushima-ku, Osaka) Folia Ophthalmologica Japonica, 16 (10...Yakuho 166 (3), 28~36 (1965) (in Japanese). Hairy aerial mycelia of certain fungi (Aspergilli and Tricophyton are difficult......

ABSTRACTS

1967-01-01T23:59:59.000Z

419

The 39th Symposium of Japanese Society or Electron Microscopy  

Science Journals Connector (OSTI)

......Department rf Bacteriology...macrophages. A large hmellapodia...density (non-ctathrin...the coated area. 1-4 Three-dimensionaldiitribotioniof...the apical plasma membrane...atereoregularlty, lower thermal expansion...m cost, large amount...diversified Into atmospheric slate, gaseous...beneath the plasma membrane...it was how large area of silver......

Takeshi Hoshino

1995-02-01T23:59:59.000Z

420

Exploring aberration-corrected electron microscopy for compound semiconductors  

Science Journals Connector (OSTI)

......at atomic dimensions. Cryst. Res. Technol. (2005) 40:149-160. doi:10.1002/crat.200410318 . 26 Thust A , Overwijk M H F, Coene W M N, Lentzen M. Numerical correction of lens aberrations in phase-retrieval HRTEM. Ultramicroscopy (1996......

David J. Smith; Toshihiro Aoki; John Mardinly; Lin Zhou; Martha R. McCartney

2013-06-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

Cryo-Electron Microscopy Structure of Lactococcal Siphophage 1358 Virion  

Science Journals Connector (OSTI)

...cryo-EM, after blotting for 4 s, the grid was plunged into liquid ethane for vitrification...reassembled structure. (C) This 1358 phage hybrid structure was assembled from separately...ANR-11-BSV8-004-01 Lactophages and French Infrastructure for Integrated Structural Biology [FRISBI...

Silvia Spinelli; Cecilia Bebeacua; Igor Orlov; Denise Tremblay; Bruno P. Klaholz; Sylvain Moineau; Christian Cambillau

2014-05-28T23:59:59.000Z

422

Cryo-Electron Microscopy Structure of Lactococcal Siphophage 1358 Virion  

Science Journals Connector (OSTI)

...Finally, we processed this data set with the appropriate helical...conformations. Consequently, our data set included two subsets...analyses and other published data, these decorations might be...ANR-11-BSV8-004-01 Lactophages and French Infrastructure for Integrated Structural Biology...

Silvia Spinelli; Cecilia Bebeacua; Igor Orlov; Denise Tremblay; Bruno P. Klaholz; Sylvain Moineau; Christian Cambillau

2014-05-28T23:59:59.000Z

423

THE ELECTRON MICROSCOPY OF HYDROCARBON PRODUCTION IN PARTHENIUM ARGENTATUM (GUAYULE)  

E-Print Network (OSTI)

conversion of solar energy is the production of hydrocarbonsproduction of hydrocarbons. Mankind's use of biologically converted solar energy

Bauer, T.E.

2010-01-01T23:59:59.000Z

424

The origins and evolution of freeze-etch electron microscopy  

Science Journals Connector (OSTI)

......upon this quite by accident, during a teaching session at the Marine Biology Laboratory in Woods Hole. While explaining the freeze-fracture...filters onto a silver screen, which required our audiences to wear polarizing glasses like people did while watching the old 3D......

John E. Heuser

2011-08-01T23:59:59.000Z

425

DISLOCATION IMAGES IN HIGH RESOLUTION SCANNING ELECTRON MICROSCOPY  

E-Print Network (OSTI)

. There are several dislocation images in the back scattered mode which are distinctly of excess/defect contrast observed in the dark field : two seperate conditions cars. be found. There is a set of dislocations having

Paris-Sud XI, Université de

426

THE ELECTRON MICROSCOPY OF HYDROCARBON PRODUCTION IN PARTHENIUM ARGENTATUM (GUAYULE)  

E-Print Network (OSTI)

in later stages of rubber production will be pre- sentedhas embarked on a rubber production effort designed to useas a crop are its high rubber production~~up to 26% of its

Bauer, T.E.

2010-01-01T23:59:59.000Z

427

Cryogenic Electron Microscopy Study of Nanoemulsion Formation from Microemulsions  

Science Journals Connector (OSTI)

A small amount (?1 ?L) of the sample was applied to a brass planchet (Type A, Ted Pella Inc., Redding, CA) designed for use with a high-pressure-freezer. ... Delmas, T.; Piraux, H.; Couffin, A. C.; Texier, I.; Vinet, F.; Poulin, P.; Cates, M. E.; Bibette, J.How to prepare and stabilize very small nanoemulsions Langmuir 2011, 27, 1683– 1692 ...

Han Seung Lee; Eric D. Morrison; Chris D. Frethem; Joseph A. Zasadzinski; Alon V. McCormick

2014-08-20T23:59:59.000Z

428

The use of nonparametric statistics in quantitative electron microscopy  

Science Journals Connector (OSTI)

......w e e n Groups Single Factor Kruskal-Wallis Test (ANOVA), g g 8 12 9 14...i'6" >2 Two Faaor ANOVA Kruskal-Wallis Test (ANOVA) ~ ~ '. ~ ~ 7...The data were evaluated by the Kruskal-Wallis Test. Note that when n = 10......

Randal E. Morris

2000-01-01T23:59:59.000Z

429

Picoscale science and nanoscale engineering by electron microscopy  

Science Journals Connector (OSTI)

......properties of a solid material at a high spatial resolution...situ TEM is becoming an active field of research that is directly related to materials science, nanomechanics...cobalt dioxide (LiCoO2) cathode-and the in situ observation...5-V against a LiCoO2 cathode. The single-crystal......

Zhong Lin Wang

2011-08-01T23:59:59.000Z

430

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......were examined by means of the fluorescent antibody method. Identification...cerebrospinal fluid by the fluorescent antibody method may contribute...299 Bulbus olfactorius have led to the following con- clusions...after excision of the olfactory bulb, the endoplasmic reticulum......

ABSTRACT

1966-01-01T23:59:59.000Z

431

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......fixation, might possibly have led to erroneous interpretations...Japanese). Histochemical and fluorescent microscopic ob- servations...enucleation of the ocular bulb at the follow- ing 5 post-irradiation...crystal formation contro'led by the epitaxial effect......

ABSTRACTS

1967-01-01T23:59:59.000Z

432

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......dehydration. It is thought that the foam cells are playing the main role...electrode is ap- plied through an insulated coaxial cable whose exterior surface is kept at...is supplied through an insulating cable to the 10 stage ac- celerator in......

ABSTRACTS

1967-01-01T23:59:59.000Z

433

In commemoration of Journal of Electron Microscopy's 60th anniversary  

Science Journals Connector (OSTI)

......troublesome for the users could be achieved according to the process on the display, thus greatly improving the ease of operation...aberration corrector (Cs-corrector). With the triggering of commercialization of the Cs-corrector by CEOS in Germany in 1999, a joint......

Yoshiyasu Harada

2011-08-01T23:59:59.000Z

434

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......HIRATA, Kazuo IWATA (Department of Microbiology, Faculty of Medicine, University of...syndrome; endo- plasmic reticulum in Gilbert's disease; and lyso- some in Wilson's...ITAGAKI (Laboratory of Nutrition and Microbiology, Niigata Women's College, Niigata......

ABSTRACTS

1967-01-01T23:59:59.000Z

435

Study of Polyanilines by High-Resolution Electron Microscopy  

Science Journals Connector (OSTI)

CECM, CNRS, 14 rue Georges Urbain, 94407 Vitry-sur-Seine, France; LADIR, CNRS-Université Pierre et Marie Curie, 2 rue Henry Dunant 94320 Thiais, France; and DMSC, ONERA, BP 72, 92322 Chatillon, France ...

Léo Mazerolles; Sandrine Folch; Philippe Colomban

1999-11-13T23:59:59.000Z

436

In-Situ Electron Microscopy of Electrical Energy Storage Materials  

Energy.gov (U.S. Department of Energy (DOE))

2013 DOE Hydrogen and Fuel Cells Program and Vehicle Technologies Program Annual Merit Review and Peer Evaluation Meeting

437

In-Situ Electron Microscopy of Electrical Energy Storage Materials  

Energy.gov (U.S. Department of Energy (DOE))

2011 DOE Hydrogen and Fuel Cells Program, and Vehicle Technologies Program Annual Merit Review and Peer Evaluation

438

In-Situ Electron Microscopy of Electrical Energy Storage Materials  

Energy.gov (U.S. Department of Energy (DOE))

2012 DOE Hydrogen and Fuel Cells Program and Vehicle Technologies Program Annual Merit Review and Peer Evaluation Meeting

439

Scanning Electron Microscopy in Concrete Petrography Paul E. Stutzman  

E-Print Network (OSTI)

hydroxide, needle-like habit of ettringite, and the sheet-like habit of calcium- silicate I C-S-H, platy-Type II C-S-H, and ettringite needles. Calcium Hydroxide Ettringite Calcium Hydroxide Ettringite Calcium-Silicate-Hydrate 15 µµm 10 µµm #12;#12;Calcium Hydroxide in Concrete 63 Figure 2

Bentz, Dale P.

440

VOLUME CONTENTS OF JOURNAL OF ELECTRON MICROSCOPY VOL. 14 (1965):  

Science Journals Connector (OSTI)

......in the Urinary Epithelium of Striped Snake (Elaphe quadrivirgata)) Tatsuo EBE...for Embedding with Epoxy Resin at Room Temperature Hiroshi KUSHIDA (275) The Fine Structure...OUTSTANDING LEVEL Consecutive research and development carried on by Hitachi over 26 years in......

Contents of Journal of Electron Microscopy

1965-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


441

ABSTRACTS OF REPORTS CONSERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......the tests, the measurements of electric resistance and stress relaxation were carried...lation between the corrosion resistance of anodic oxide films of SAP...namely sphe- roid bodies and elementary granules, are pro- fusely present......

ABSTRACTS

1966-01-01T23:59:59.000Z

442

The Cost of Transmission for Wind Energy: A Review of Transmission Planning Studies  

E-Print Network (OSTI)

Equipment Transmission Lines 765 kV (no description) 500Montana-Alberta Tie 230 kV Transmission Line: TransmissionMontana-Alberta Tie 230 kV Transmission Line: Transmission

Mills, Andrew D.

2009-01-01T23:59:59.000Z

443

National Electric Transmission Congestion Study: Preliminary...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

National Electric Transmission Congestion Study: Preliminary Findings National Electric Transmission Congestion Study: Preliminary Findings The Department hosted three webinars in...

444

Hydrogen Delivery Technologies and Systems - Pipeline Transmission...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Hydrogen Delivery Technologies and Systems - Pipeline Transmission of Hydrogen Hydrogen Delivery Technologies and Systems - Pipeline Transmission of Hydrogen Hydrogen Delivery...

445

E-Print Network 3.0 - analytical scanning electron Sample Search...  

NLE Websites -- All DOE Office Websites (Extended Search)

Electron Microscope Philips CM20 Analytical Scanning... during formation of the carbide particles. 12;Philips CM20 Analytical Scanning Transmission Electron... at SCSAM ...

446

AGENDA: PETROLEUM PRODUCT TRANSMISSION & DISTRIBUTION  

Energy.gov (U.S. Department of Energy (DOE))

The agenda for the Quadrennial Energy Review (QER) public stakeholder meeting in New Orleans on petroleum product transmission, distribution, and storage.

447

Transmission Reliability | Department of Energy  

Energy Savers (EERE)

design, long-term supply and transmission investment, renewable integration, demand response, and environmental impacts. Researchers use models and simulations to assess how...

448

NREL: Transmission Grid Integration - Projects  

NLE Websites -- All DOE Office Websites (Extended Search)

Projects NREL's transmission integration projects provide data and models that help utilities and policymakers make informed decisions about the integration of variable generation,...

449

Chapter 4 Transmission Adequacy | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Chapter 4 Transmission Adequacy Chapter 4 Transmission Adequacy Chapter 4 Transmission Adequacy Transmission lines are the critical link between the point of electricity generation and consumers. The U.S. transmission grid infrastructure is owned and operated by approximately 3,000 distribution utilities and 500 transmission owners. This structure presents a distinct set of challenges in transmission planning, siting, cost allocation, grid operations and management, technological innovation, financing and construction. The development and deployment of a national strategy on transmission that meets the needs of all parties is extremely complex; however, a solution is desperately needed. Chapter 4 Transmission Adequacy More Documents & Publications Draft Chapter 4: Transmission Adequacy

450

Hyperspectral Microscopy of Explosives Particles Using an External Cavity Quantum Cascade Laser  

SciTech Connect

Using infrared hyperspectral imaging, we demonstrate microscopy of small particles of the explosives compounds RDX, tetryl, and PETN with near diffraction-limited performance. The custom microscope apparatus includes an external cavity quantum cascade laser illuminator scanned over its tuning range of 9.13-10.53 µm in four seconds, coupled with a microbolometer focal plane array to record infrared transmission images. We use the hyperspectral microscopy technique to study the infrared absorption spectra of individual explosives particles, and demonstrate sub-nanogram detection limits.

Phillips, Mark C.; Bernacki, Bruce E.

2012-12-26T23:59:59.000Z

451

HVDC power transmission technology assessment  

SciTech Connect

The purpose of this study was to develop an assessment of the national utility system`s needs for electric transmission during the period 1995-2020 that could be met by future reduced-cost HVDC systems. The assessment was to include an economic evaluation of HVDC as a means for meeting those needs as well as a comparison with competing technologies such as ac transmission with and without Flexible AC Transmission System (FACTS) controllers. The role of force commutated dc converters was to be assumed where appropriate. The assessment begins by identifying the general needs for transmission in the U.S. in the context of a future deregulated power industry. The possible roles for direct current transmission are then postulated in terms of representative scenarios. A few of the scenarios are illustrated with the help of actual U.S. system examples. non-traditional applications as well as traditional applications such as long lines and asynchronous interconnections are discussed. The classical ``break-even distance`` concept for comparing HVDC and ac lines is used to assess the selected scenarios. The impact of reduced-cost converters is reflected in terms of the break-even distance. This report presents a comprehensive review of the functional benefits of HVDC transmission and updated cost data for both ac and dc system components. It also provides some provocative thoughts on how direct current transmission might be applied to better utilize and expand our nation`s increasingly stressed transmission assets.

Hauth, R.L.; Tatro, P.J.; Railing, B.D. [New England Power Service Co., Westborough, MA (United States); Johnson, B.K.; Stewart, J.R. [Power Technologies, Inc., Schenectady, NY (United States); Fink, J.L.

1997-04-01T23:59:59.000Z

452

Hydrogen Transmission and Distribution Workshop  

Energy.gov (U.S. Department of Energy (DOE))

Proceedings from the Hydrogen Transmission and Distribution Workshop held February 25-26, 2014, in Golden, Colorado. The objective was to discuss and share information on the research, development, and demonstration needs and challenges for low-cost, effective hydrogen transmission and distribution from centralized production facilities to the point of use.

453

Direct current power transmission systems  

SciTech Connect

This book represents text on HVDC transmission available. It deals with the various aspects of the state of the art in HVDC transmission technology. This book presents many aspects of interactions of AC/DC systems. Modeling and analysis of DC systems are also discussed in detail.

Padiyar, K.R.

1991-01-01T23:59:59.000Z

454

An all-cryogenic THz transmission spectrometer P. J. Burkea)  

E-Print Network (OSTI)

An all-cryogenic THz transmission spectrometer P. J. Burkea) and J. P. Eisenstein Condensed Matter contained in a cryogenic environment. Cyclotron emission from a two-dimensional electron gas 2DEG heated microwave to optical frequencies.2 In this article an all-cryogenic spectrometer is presented that bypasses

Eisenstein, Jim

455

Transmission Reliability | Department of Energy  

NLE Websites -- All DOE Office Websites (Extended Search)

Transmission Reliability Transmission Reliability Transmission Reliability Modernizing America's electricity infrastructure is one of the U.S. Department of Energy's top priorities. The DOE Strategic Plan states that today's electric grid needs to be more efficient, reliable, and secure. A modern, smarter electric grid may save consumers money, help our economy run more efficiently, allow rapid growth in renewable energy sources, and enhance energy reliability. The Department's research into a variety of tools that will improve advanced system monitoring, visualization, control, operations, and market structure will ultimately modernize the electricity transmission infrastructure to ease congestion, allow for increases in demand, and provide a greater degree of security. The Transmission Reliability Program is aligned with this strategic plan

456

ITC Transmission | Open Energy Information  

Open Energy Info (EERE)

ITC Transmission ITC Transmission Jump to: navigation, search Name ITC Transmission Place Michigan Utility Id 56068 Utility Location Yes Ownership T NERC RFC Yes ISO MISO Yes Activity Transmission Yes Alt Fuel Vehicle Yes Alt Fuel Vehicle2 Yes References EIA Form EIA-861 Final Data File for 2010 - File1_a[1] LinkedIn Connections CrunchBase Profile No CrunchBase profile. Create one now! This article is a stub. You can help OpenEI by expanding it. Utility Rate Schedules Grid-background.png No rate schedules available. Average Rates No Rates Available References ↑ "EIA Form EIA-861 Final Data File for 2010 - File1_a" Retrieved from "http://en.openei.org/w/index.php?title=ITC_Transmission&oldid=410858" Categories: EIA Utility Companies and Aliases Utility

457

Regional Transmission Projects: Finding Solutions  

SciTech Connect

The Keystone Center convened and facilitated a year-long Dialogue on "Regional Transmission Projects: Finding Solutions" to develop recommendations that will help address the difficult and contentious issues related to expansions of regional electric transmission systems that are needed for reliable and economic transmission of power within and across regions. This effort brought together a cross-section of affected stakeholders and thought leaders to address the problem with the collective wisdom of their experience and interests. Transmission owners sat at the table with consumer advocates and environmental organizations. Representatives from regional transmission organizations exchanged ideas with state and federal regulators. Generation developers explored common interests with public power suppliers. Together, the Dialogue participants developed consensus solutions about how to begin unraveling some of the more intractable issues surrounding identification of need, allocation of costs, and reaching consensus on siting issues that can frustrate the development of regional transmission infrastructure. The recommendations fall into three broad categories: 1. Recommendations on appropriate institutional arrangements and processes for achieving regional consensus on the need for new or expanded transmission infrastructure 2. Recommendations on the process for siting of transmission lines 3. Recommendations on the tools needed to support regional planning, cost allocation, and siting efforts. List of Dialogue participants: List of Dialogue Participants: American Electric Power American Transmission Company American Wind Energy Association California ISO Calpine Corporation Cinergy Edison Electric Institute Environmental Defense Federal Energy Regulatory Commission Great River Energy International Transmission Company ISO-New England Iowa Public Utility Board Kanner & Associates Midwest ISO National Association of Regulatory Utility Commissioners National Association of State Utility Consumer Advocates National Grid Northeast Utilities PA Office of Consumer Advocates Pacific Gas & Electric Corporation Pennsylvania Public Utility Commission PJM Interconnection The Electricity Consumers Resource Council U.S. Department of Energy US Department of the Interior Van Ness Feldman Western Interstate Energy Board Wind on the Wires Wisconsin Public Service Commission Xcel Energy

The Keystone Center

2005-06-15T23:59:59.000Z

458

Fact #850: December 8, 2014 Automatic Transmissions have closed the Fuel Economy Gap with Manual Transmissions  

Energy.gov (U.S. Department of Energy (DOE))

Historically, manual transmissions have delivered better fuel economy than automatic transmissions. However, improvements in the efficiency of automatic transmissions have closed that gap in recent...

459

High resolution electron microscopic studies on ferrosilite III  

Science Journals Connector (OSTI)

High resolution transmission electron microscopic (HRTEM) studies on ferrosilite (Fs) III confirmed the periodicity nine (p=9) of the tetrahedral chains in this silicate. Various chain periodicit...

M. Czank; B. Simons

1983-05-01T23:59:59.000Z

460

Energy Transmission and Infrastructure  

SciTech Connect

The objective of Energy Transmission and Infrastructure Northern Ohio (OH) was to lay the conceptual and analytical foundation for an energy economy in northern Ohio that will: • improve the efficiency with which energy is used in the residential, commercial, industrial, agricultural, and transportation sectors for Oberlin, Ohio as a district-wide model for Congressional District OH-09; • identify the potential to deploy wind and solar technologies and the most effective configuration for the regional energy system (i.e., the ratio of distributed or centralized power generation); • analyze the potential within the district to utilize farm wastes to produce biofuels; • enhance long-term energy security by identifying ways to deploy local resources and building Ohio-based enterprises; • identify the policy, regulatory, and financial barriers impeding development of a new energy system; and • improve energy infrastructure within Congressional District OH-09. This objective of laying the foundation for a renewable energy system in Ohio was achieved through four primary areas of activity: 1. district-wide energy infrastructure assessments and alternative-energy transmission studies; 2. energy infrastructure improvement projects undertaken by American Municipal Power (AMP) affiliates in the northern Ohio communities of Elmore, Oak Harbor, and Wellington; 3. Oberlin, OH-area energy assessment initiatives; and 4. a district-wide conference held in September 2011 to disseminate year-one findings. The grant supported 17 research studies by leading energy, policy, and financial specialists, including studies on: current energy use in the district and the Oberlin area; regional potential for energy generation from renewable sources such as solar power, wind, and farm-waste; energy and transportation strategies for transitioning the City of Oberlin entirely to renewable resources and considering pedestrians, bicyclists, and public transportation as well as drivers in developing transportation policies; energy audits and efficiency studies for Oberlin-area businesses and Oberlin College; identification of barriers to residential energy efficiency and development of programming to remove these barriers; mapping of the solar-photovoltaic and wind-energy supply chains in northwest Ohio; and opportunities for vehicle sharing and collaboration among the ten organizations in Lorain County from the private, government, non-profit, and educational sectors. With non-grant funds, organizations have begun or completed projects that drew on the findings of the studies, including: creation of a residential energy-efficiency program for the Oberlin community; installation of energy-efficient lighting in Oberlin College facilities; and development by the City of Oberlin and Oberlin College of a 2.27 megawatt solar photovoltaic facility that is expected to produce 3,000 megawatt-hours of renewable energy annually, 12% of the College’s yearly power needs. Implementation of these and other projects is evidence of the economic feasibility and technical effectiveness of grant-supported studies, and additional projects are expected to advance to implementation in the coming years. The public has benefited through improved energydelivery systems and reduced energy use for street lighting in Elmore, Oak Harbor, and Wellington; new opportunities for assistance and incentives for residential energy efficiency in the Oberlin community; new opportunities for financial and energy savings through vehicle collaboration within Lorain County; and decreased reliance on fossil fuels and expanded production of renewable energy in the region. The dissemination conference and the summary report developed for the conference also benefited the public, but making the findings and recommendations of the regional studies broadly available to elected officials, city managers, educators, representatives of the private sector, and the general public.

Mathison, Jane

2012-12-31T23:59:59.000Z

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

462

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

463

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

464

Biological Imaging by Soft X-Ray Diffraction Microscopy  

NLE Websites -- All DOE Office Websites (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

465

Testing of the Data Transmission System Monika Grothe, Ariane Frey, Massimiliano Turri, Max Wilder  

E-Print Network (OSTI)

Testing of the Data Transmission System Components Monika Grothe, Ariane Frey, Massimiliano Turri August 1999 Abstract This note provides a description of the set­up for testing the data transmission system electronics for the BaBar Silicon Vertex Tracker. #12; Contents 1 List of tested Components 3 2

California at Santa Cruz, University of

466

Observation de super-rseaux CdTe-HgTe par microscopie lectronique en transmission  

E-Print Network (OSTI)

-conducteurs II-VI a été beaucoup plus tardive [2]. Dans cette dernière famille, le système CdTe- HgTe présente l'avantage d'un accord de maille quasi parfait entre les deux composés (a = 0,648 nm pour CdTe contre a = 0 JET MOL�CULAIRE. - Les super- réseaux CdTe-HgTe ont été épitaxiés sur un substrat CdTe d

Paris-Sud XI, Université de

467

Scanning Transmission X-ray Microscopy: Applications in Atmospheric Aerosol Research  

E-Print Network (OSTI)

related to the total atomic absorption cross section, ? A (number. Tabulations of atomic absorption cross sections areC are the mass absorption coefficients and atomic masses for

Moffet, Ryan C.

2011-01-01T23:59:59.000Z

468

Bibliography on transmission access issues  

SciTech Connect

This paper presents a bibliography on issues related to transmission access in electric power systems. There are 233 citations referenced in this bibliography. This bibliography presents a collection of selected literature on issues related to transmission access. It does not contain all of the material available on this subject or the categories contained herein. Some readers may feel that citations within this bibliography should be strictly limited to transmission system issues and not include energy pricing or reliability issues. However, it was the decision of the Subcommittee of the IEEE Task Force on Transmission Access and Nonutility Generation that selected entries relating to reliability and energy pricing, most relevant to transmission access, should be included. This decision was made because certain issues relating to reliability, transmission and energy pricing are perceived by the industry to be critical in the discussion of transmission access. The bibliography has been divided into the following sections or sub-sections: 2.0 Operational (Engineering) Issues, 3.0 Planning, 4.0 Reliability, 5.1 Economics: Costing, 5.2(a) Economics: Location-Differentiated Pricing, 5.2(b) Economics: Time-Differentiated Pricing, 5.3 Economics: Brokering, Bidding, and Auctioning, 6.0 Regulatory, and 7.0 General. Although the content of many publications spanned two or more of these sections, the desire to limit document length required that all publications be placed in the single most appropriate section. Publications are sorted according to author or publication resource.

Lankford, C.B. [Oklahoma Gas and Electric Co., Oklahoma City, OK (United States)] [Oklahoma Gas and Electric Co., Oklahoma City, OK (United States); McCalley, J.D. [Iowa State Univ., Ames, IA (United States)] [Iowa State Univ., Ames, IA (United States); Saini, N.K. [Entergy Services Corp., Metairie, LA (United States)] [Entergy Services Corp., Metairie, LA (United States)

1996-02-01T23:59:59.000Z

469

Polarizer with Nonrectangular Grooves in the HE11 Mode Transmission Line  

Science Journals Connector (OSTI)

This paper presents experimental results on polarizers with nonrectangular grooves to be used in high power millimeter wave transmission lines for electron cyclotron heating (ECH) of fusion plasmas. A low-powe...

K. Nagasaki; Y. Itoh; H. Morioka; T. Obiki

1999-05-01T23:59:59.000Z

470

Microscopy charges ahead | Argonne National Laboratory  

NLE Websites -- All DOE Office Websites (Extended Search)

Microscopy charges ahead By Jared Sagoff * May 28, 2014 Tweet EmailPrint ARGONNE, Ill. - Ferroelectric materials - substances in which there is a slight and reversible shift of...

471

Design of Flexure-based Precision Transmission Mechanisms using Screw Theory  

SciTech Connect

This paper enables the synthesis of flexure-based transmission mechanisms that possess multiple decoupled inputs and outputs of any type (e.g. rotations, translations, and/or screw motions), which are linked by designer-specified transmission ratios. A comprehensive library of geometric shapes is utilized from which every feasible concept that possesses the desired transmission characteristics may be rapidly conceptualized and compared before an optimal concept is selected. These geometric shapes represent the rigorous mathematics of screw theory and uniquely link a body's desired motions to the flexible constraints that enable those motions. This paper's impact is most significant to the design of nano-positioners, microscopy stages, optical mounts, and sensors. A flexure-based microscopy stage was designed, fabricated, and tested to demonstrate the utility of the theory.

Hopkins, J B; Panas, R M

2011-02-07T23:59:59.000Z

472

Electrical transmission line diametrical retainer  

DOE Patents (OSTI)

The invention is a mechanism for retaining an electrical transmission line. In one embodiment of the invention it is a system for retaining an electrical transmission line within down hole components. In accordance with one aspect of the invention, the system includes a plurality of downhole components, such as sections of pipe in a drill string. The system also includes a coaxial cable running between the first and second end of a drill pipe, the coaxial cable having a conductive tube and a conductive core within it. The invention allows the electrical transmission line to with stand the tension and compression of drill pipe during routine drilling cycles.

Hall, David R. (Provo, UT); Hall, Jr., H. Tracy (Provo, UT); Pixton, David (Lehi, UT); Dahlgren, Scott (Provo, UT); Sneddon, Cameron (Provo, UT); Briscoe, Michael (Lehi, UT); Fox, Joe (Spanish Fork, UT)

2004-12-14T23:59:59.000Z

473

In-situ spectro-microscopy on organic films: Mn-Phthalocyanine on Ag(100)  

SciTech Connect

Metal phthalocyanines are attracting significant attention, owing to their potential for applications in chemical sensors, solar cells and organic magnets. As the electronic properties of molecular films are determined by their crystallinity and molecular packing, the optimization of film quality is important for improving the performance of organic devices. Here, we present the results of in situ low-energy electron microscopy / photoemission electron microscopy (LEEM/PEEM) studies of incorporation-limited growth [1] of manganese-phthalocyanine (MnPc) on Ag(100) surfaces. MnPc thin films were grown on both, bulk Ag(100) surface and thin Ag(100)/Fe(100) films, where substrate spin-polarized electronic states can be modified through tuning the thickness of the Ag film [2]. We also discuss the electronic structure and magnetic ordering in MnPc thin films, investigated by angle- and spin-resolved photoemission spectroscopy.

Al-Mahboob A.; Vescovo, E.; Sadowski, J.T.

2013-08-18T23:59:59.000Z

474

Coordination of Transmission Line Transfer Capabilities  

E-Print Network (OSTI)

Coordination of Transmission Line Transfer Capabilities Final Project Report Power Systems since 1996 PSERC #12;Power Systems Engineering Research Center Coordination of Transmission Line Summary The maximum power that can be transferred over any transmission line, called the transfer capacity

475

Transmission Planning | Department of Energy  

NLE Websites -- All DOE Office Websites (Extended Search)

Planning Planning Transmission Planning Modernizing America's electricity infrastructure is one of the U.S. Department of Energy's top priorities. The National Transmission Grid Study (PDF 2.0 MB) made clear that without dramatic improvements and upgrades over the next decade our nation's transmission system will fall short of the reliability standards our economy requires, and will result in higher electricity costs to consumers. The Department's research into a variety of tools that will improve advanced system monitoring, visualization, control, operations, and market structure will ultimately modernize the electricity transmission infrastructure to ease congestion, allow for increases in demand, and provide a greater degree of security. The next generation supervisory control and data acquisition (SCADA) and

476

Video transmission over wireless networks  

E-Print Network (OSTI)

Compressed video bitstream transmissions over wireless networks are addressed in this work. We first consider error control and power allocation for transmitting wireless video over CDMA networks in conjunction with multiuser detection. We map a...

Zhao, Shengjie

2005-08-29T23:59:59.000Z

477

National Electric Transmission Congestion Studies  

Energy.gov (U.S. Department of Energy (DOE))

Section 216(a) of the Federal Power Act, as amended by the Energy Policy Act of 2005, directs the U.S. Department of Energy (DOE) to conduct a study every three years on electric transmission congestion and constraints within the Eastern and Western Interconnections. The American Reinvestment and Recovery Act of 2009 (Recovery Act) further directed the Secretary to include in the 2009 Congestion Study an analysis of significant potential sources of renewable energy that are constrained by lack of adequate transmission capacity. Based on this study, and comments concerning it from states and other stakeholders, the Secretary of Energy may designate any geographic area experiencing electric transmission capacity constraints or congestion as a national interest electric transmission corridor (National Corridor).

478

National Transmission Grid Study: 2002  

Energy.gov (U.S. Department of Energy (DOE))

National Transmission Grid Study: The National Energy Policy Plan directed the U.S. Department of Energy (DOE) to conduct a study to examine the benefits of establishing a national electricity...

479

OpenEI Community - transmission  

Open Energy Info (EERE)

black out brown out bulk power system electricity grid future grid grid history security Smart Grid transmission Smart Grid Fri, 31 Oct 2014 17:58:14 +0000 Dc 955 at...

480

Nonlinear Dark-Field Microscopy Hayk Harutyunyan,  

E-Print Network (OSTI)

/20/2010 Published on Web: 11/16/2010 FIGURE 1. Illustration of the nonlinear dark-field imaging method. Two incidentNonlinear Dark-Field Microscopy Hayk Harutyunyan, Stefano Palomba, Jan Renger, Romain Quidant Dark-field microscopy is a background-free imaging method that provides high sensitivity and a large

Novotny, Lukas

Note: This page contains sample records for the topic "transmission electron microscopy" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


481

Multiphoton microscopy with near infrared contrast  

E-Print Network (OSTI)

Multiphoton microscopy with near infrared contrast agents Siavash Yazdanfar,a, * Chulmin Joo,a Chun limited to the visible spectrum. We introduce a paradigm for MPM of near-infrared NIR fluorescent Engineers. DOI: 10.1117/1.3420209 Keywords: two-photon microscopy; ultrafast fiber lasers; near-infrared

Larson-Prior, Linda

482

DOE Transmission Capacity Report | Department of Energy  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Transmission Capacity Report Transmission Capacity Report DOE Transmission Capacity Report DOE Transmission Capacity Report: Transmission lines, substations, circuit breakers, capacitors, and other equipment provide more than just a highway to deliver energy and power from generating units to distribution systems. Transmission systems both complement and substitute for generation. Transmission generally enhances reliability; lowers the cost of electricity delivered to consumers; limits the ability of generators to exercise market power; and provides flexibility to protect against uncertainties about future fuel prices, load growth, generator construction, and other factors affecting the electric system. DOE Transmission Capacity Report More Documents & Publications Report to Congress:Impacts of the Federal Energy Regulatory Commission's

483

AGENDA: PETROLEUM PRODUCT TRANSMISSION & DISTRIBUTION | Department...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

AGENDA: PETROLEUM PRODUCT TRANSMISSION & DISTRIBUTION AGENDA: PETROLEUM PRODUCT TRANSMISSION & DISTRIBUTION A Public Meeting on the Quadrennial Energy Review, Hosted by the United...

484

Briefing Memo: Petroleum Product Transmission & Distribution...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Briefing Memo: Petroleum Product Transmission & Distribution Briefing Memo: Petroleum Product Transmission & Distribution Click below to download a PDF of the briefing memo....

485

Natural Gas Transmission and Distribution Module  

Gasoline and Diesel Fuel Update (EIA)

U.S. Energy Information Administration | Assumptions to the Annual Energy Outlook 2013 Natural Gas Transmission and Distribution Module The NEMS Natural Gas Transmission and...

486

Agenda: Natural Gas: Transmission, Storage and Distribution ...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Natural Gas: Transmission, Storage and Distribution Agenda: Natural Gas: Transmission, Storage and Distribution A Public Meeting on the Quadrennial Energy Review, Hosted by the...

487

2006 National Electric Transmission Congestion Study Federal...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

6 National Electric Transmission Congestion Study Federal Register Notice & Comments 2006 National Electric Transmission Congestion Study Federal Register Notice & Comments The...

488

National Electric Transmission Congestion Study | Department...  

NLE Websites -- All DOE Office Websites (Extended Search)

Study National Electric Transmission Congestion Study National Electric Transmission Congestion Study Section 1221(a) of the Energy Policy Act of 2005, codified at 16 U.S.C....

489

2009 National Electric Transmission Congestion Study | Department...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

9 National Electric Transmission Congestion Study 2009 National Electric Transmission Congestion Study Section 216(a) of the Federal Power Act, as amended by the Energy Policy Act...

490

Electric Transmission Siting | Open Energy Information  

Open Energy Info (EERE)

navigation, search OpenEI Reference LibraryAdd to library Legal Document- OtherOther: Electric Transmission SitingLegal Abstract Electric Transmission Siting at the California...

491

2006 National Electric Transmission Congestion Study | Department...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

6 National Electric Transmission Congestion Study 2006 National Electric Transmission Congestion Study Section 216(a) of the Federal Power Act, as amended by the Energy Policy Act...

492

National Electric Transmission Congestion Study Workshops | Department...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

National Electric Transmission Congestion Study Workshops National Electric Transmission Congestion Study Workshops DOE hosted four regional pre-study workshops to receive input...

493

WINDExchange Offshore Wind Webinar: Transmission Planning and...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Offshore Wind Webinar: Transmission Planning and Interconnection for Offshore Wind WINDExchange Offshore Wind Webinar: Transmission Planning and Interconnection for Offshore Wind...

494

Agenda: Electricity Transmission and Distribution - East | Department...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Electricity Transmission and Distribution - East Agenda: Electricity Transmission and Distribution - East A Public Meeting on the Quadrennial Energy Review, Hosted by the United...

495

Agenda: Electricity Transmission, Storage and Distribution -...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

Electricity Transmission, Storage and Distribution - West Agenda: Electricity Transmission, Storage and Distribution - West A Public Meeting on the Quadrennial Energy Review,...

496

Southline Transmission Line | Open Energy Information  

Open Energy Info (EERE)

Impact Statement for the Southline Transmission Line Project General NEPA Document Info Energy Sector Transmission Environmental Analysis Type EIS Applicant Southline...

497

CX-005074: Categorical Exclusion Determination | Department of...  

Energy.gov (U.S. Department of Energy (DOE)) Indexed Site

analysis and scanning electron microscopy, transmission electron microscopy, x-ray diffraction and x-ray fluorescence. DOCUMENT(S) AVAILABLE FOR DOWNLOAD CX-005074.pdf...

498

Young’s double-slit interference experiment with electrons  

Science Journals Connector (OSTI)

In this short Note we report a method for producing samples containing two nano-sized slits suitable for demonstrating to undergraduate and graduate students the double-slit electron interference experiment in a conventional transmission electron microscope.

S. Frabboni; G. C. Gazzadi; G. Pozzi

2007-01-01T23:59:59.000Z

499

Electronic, dielectric, and optical properties of individual composite silver halide microcrystals using the EELS and LMTO-ASA techniques  

Science Journals Connector (OSTI)

The low-loss fine structure in electron energy-loss spectra (EELS) of individual composite high-aspect-ratio tabular AgX(X=Br, I) microcrystals between 4 and 26 eV was investigated by cryo-EELS and energy-filtering transmission electron microscopy. Local dielectric permittivity, refractive index, and absorption coefficient have been determined using Kramers-Kronig relationships. Quantum-mechanical calculations of the AgBr band structure and dielectric permittivity by the linear muffin-tin orbital method in the atomic spheres approximation have been used to assign the structure attributed to exciton peaks. Experimental local dielectric parameters and joint optical density of states were found to be in fair general agreement with calculated dielectric properties and densities of states.

Vladimir Oleshko; Marc Amkreutz; Harald Overhof

2003-03-17T23:59:59.000Z

500

Multi-transmission-line-beam interactive system  

SciTech Connect

We construct here a Lagrangian field formulation for a system consisting of an electron beam interacting with a slow-wave structure modeled by a possibly non-uniform multiple transmission line (MTL). In the case of a single line we recover the linear model of a traveling wave tube due to J. R. Pierce. Since a properly chosen MTL can approximate a real wave