Sample records for test specimen surface

  1. Infrared Thermography Measurements of Window Thermal Test Specimen Surface Temperatures

    E-Print Network [OSTI]

    Infrared Thermography Measurements of Window Thermal Test Specimen Surface Temperatures Brent T Temperatures of Window Specimens: Infrared Thermography Laboratory Measurements Brent T. Griffith1 , Howdy and cold sides, respectively. Surface temperature maps were compiled using an infrared thermographic system

  2. Small Specimen Mechanical Property Testing at PNNL

    E-Print Network [OSTI]

    McDonald, Kirk

    Small Specimen Mechanical Property Testing at PNNL Mychailo Toloczko, Dave Senor Pacific Northwest National Laboratory December, 2013 1 #12;Overview of PNNL Capabilities for Small Specimen Testing Long

  3. Apparatus for automated testing of biological specimens

    DOE Patents [OSTI]

    Layne, Scott P. (Los Angeles, CA); Beugelsdijk, Tony J. (Los Alamos, NM)

    1999-01-01T23:59:59.000Z

    An apparatus for performing automated testing of infections biological specimens is disclosed. The apparatus comprise a process controller for translating user commands into test instrument suite commands, and a test instrument suite comprising a means to treat the specimen to manifest an observable result, and a detector for measuring the observable result to generate specimen test results.

  4. Apparatus for tensile testing plate-type ceramic specimens

    DOE Patents [OSTI]

    Liu, K.C.

    1993-08-24T23:59:59.000Z

    Apparatus is described for gripping a plate-type tensile specimen having generally T-shaped end regions in a dynamic tension fatigue testing apparatus comprising an annular housing having an open-ended elongated cavity therein, a plurality of hydraulic piston means supported by the housing in a spaced array about the cavity, and a specimen-supporting plate means overlying the piston means at one end of the elongated cavity and displaceable by said piston means in a longitudinal direction with respect to the longitudinal axis of the cavity, said apparatus for gripping a flat plate-type tensile specimen comprising: a pair of elongated pull rods each having oppositely disposed first and second end regions; a pair of mounting means carried by said plate means with each mounting means for pivotally attaching the first end region of each of said pull rods in a central region of said plate means for supporting said pair of elongated pull rods in a side-by-side relationship along a common longitudinal centerline within said cavity; recess means in the second end region of each of said pull rods in adjacently disposed surface regions thereof with said recess means facing one another and each adapted to receive one side of one of the generally T-shaped end regions of the plate-type tensile specimen; and load-bearing means positionable in each of said recess means and adapted to bear against a shoulder on each side of the generally T-shaped end region of the plate-type tensile specimen when a tensile loading is applied thereon.

  5. IEA W-GIFT-6 SMALL SPECIMEN TEST TECHNIQUE

    E-Print Network [OSTI]

    McDonald, Kirk

    IEA W-GIFT-6 SMALL SPECIMEN TEST TECHNIQUE UNDER IFMIF/EVEDA PROJECT OF BA FOR FATIGUE AND FRACTURE,t[%] Number of cycles to failure, Nf F82H-IEA HG-1.25 HG-1.25 (Hirose, Kim) RB-1 RB-7 RB-4, -7 RB-7, -10 of cycles to failure, Nf JLF-1 HG-1.25 HG-1.25 HG-6 (Hirose) RB-1 RB-8 (Nishimura&Li) F82H-IEA (Grain size

  6. Load apparatus and method for bolt-loaded compact tension test specimen

    DOE Patents [OSTI]

    Buescher, B.J. Jr.; Lloyd, W.R.; Ward, M.B.; Epstein, J.S.

    1997-02-04T23:59:59.000Z

    A bolt-loaded compact tension test specimen load apparatus includes: (a) a body having first and second opposing longitudinal ends, the first end comprising an externally threaded portion sized to be threadedly received within the test specimen threaded opening; (b) a longitudinal loading rod having first and second opposing longitudinal ends, the loading rod being slidably received in a longitudinal direction within the body internally through the externally threaded portion and slidably extending longitudinally outward of the body first longitudinal end; (c) a force sensitive transducer slidably received within the body and positioned to engage relative to the loading rod second longitudinal end; and (d) a loading bolt threadedly received relative to the body, the loading bolt having a bearing end surface and being positioned to bear against the transducer to forcibly sandwich the transducer between the loading bolt and loading rod. Also disclosed is a method of in situ determining applied force during crack propagation in a bolt-loaded compact tension test specimen. 6 figs.

  7. Load apparatus and method for bolt-loaded compact tension test specimen

    DOE Patents [OSTI]

    Buescher, Jr., Brent J. (Idaho Falls, ID); Lloyd, W. Randolph (Idaho Falls, ID); Ward, Michael B. (Idaho Falls, ID); Epstein, Jonathan S. (Idaho Falls, ID)

    1997-01-01T23:59:59.000Z

    A bolt-loaded compact tension test specimen load apparatus includes: a) a body having first and second opposing longitudinal ends, the first end comprising an externally threaded portion sized to be threadedly received within the test specimen threaded opening; b) a longitudinal loading rod having first and second opposing longitudinal ends, the loading rod being slidably received in a longitudinal direction within the body internally through the externally threaded portion and slidably extending longitudinally outward of the body first longitudinal end; c) a force sensitive transducer slidably received within the body and positioned to engage relative to the loading rod second longitudinal end; and d) a loading bolt threadedly received relative to the body, the loading bolt having a bearing end surface and being positioned to bear against the transducer to forcibly sandwich the transducer between the loading bolt and loading rod. Also disclosed is a method of in situ determining applied force during crack propagation in a bolt-loaded compact tension test specimen.

  8. Capillary test specimen, system, and methods for in-situ visualization of capillary flow and fillet formation

    DOE Patents [OSTI]

    Hall, Aaron C. (Albuquerque, NM); Hosking, F. Michael (Albuquerque, NM),; Reece, Mark (Albuquerque, NM)

    2003-06-24T23:59:59.000Z

    A capillary test specimen, method, and system for visualizing and quantifying capillary flow of liquids under realistic conditions, including polymer underfilling, injection molding, soldering, brazing, and casting. The capillary test specimen simulates complex joint geometries and has an open cross-section to permit easy visual access from the side. A high-speed, high-magnification camera system records the location and shape of the moving liquid front in real-time, in-situ as it flows out of a source cavity, through an open capillary channel between two surfaces having a controlled capillary gap, and into an open fillet cavity, where it subsequently forms a fillet on free surfaces that have been configured to simulate realistic joint geometries. Electric resistance heating rapidly heats the test specimen, without using a furnace. Image-processing software analyzes the recorded images and calculates the velocity of the moving liquid front, fillet contact angles, and shape of the fillet's meniscus, among other parameters.

  9. Small-scale Specimen Testing of Monolithic U-Mo Fuel Foils

    SciTech Connect (OSTI)

    Ramprashad Prabhakaran; Douglas E. Burkes; James I. Cole; Indrajit Charit; Daniel M. Wachs

    2008-10-01T23:59:59.000Z

    The objective of this investigation is to develop a shear punch testing (SPT) procedure and standardize it to evaluate the mechanical properties of irradiated fuels in a hot-cell so that the tensile behavior can be predicted using small volumes of material and at greatly reduced irradiation costs. This is highly important in the development of low-enriched uranium fuels for nuclear research and test reactors. The load-displacement data obtained using SPT can be interpreted in terms of and correlated with uniaxial mechanical properties. In order to establish a correlation between SPT and tensile data, sub-size tensile and microhardness testing were performed on U-Mo alloys. In addition, efforts are ongoing to understand the effect of test parameters (such as specimen thickness, surface finish, punch-die clearance, crosshead velocity and carbon content) on the measured mechanical properties, in order to rationalize the technique, prior to employing it on a material of unknown strength.

  10. Improved flywheel materials : characterization of nanofiber modified flywheel test specimen.

    SciTech Connect (OSTI)

    Boyle, Timothy J.; Bell, Nelson Simmons; Ehlen, Mark Andrew; Anderson, Benjamin John; Miller, William Kenneth

    2013-09-01T23:59:59.000Z

    As alternative energy generating devices (i.e., solar, wind, etc) are added onto the electrical energy grid (AC grid), irregularities in the available electricity due to natural occurrences (i.e., clouds reducing solar input or wind burst increasing wind powered turbines) will be dramatically increased. Due to their almost instantaneous response, modern flywheel-based energy storage devices can act a mechanical mechanism to regulate the AC grid; however, improved spin speeds will be required to meet the necessary energy levels to balance thesegreen' energy variances. Focusing on composite flywheels, we have investigated methods for improving the spin speeds based on materials needs. The so-called composite flywheels are composed of carbon fiber (C-fiber), glass fiber, and aglue' (resin) to hold them together. For this effort, we have focused on the addition of fillers to the resin in order to improve its properties. Based on the high loads required for standard meso-sized fillers, this project investigated the utility of ceramic nanofillers since they can be added at very low load levels due to their high surface area. The impact that TiO2 nanowires had on the final strength of the flywheel material was determined by athree-point-bend' test. The results of the introduction of nanomaterials demonstrated an increase instrength' of the flywheel's C-fiber-resin moiety, with an upper limit of a 30% increase being reported. An analysis of the economic impact concerning the utilization of the nanowires was undertaken and after accounting for new-technology and additional production costs, return on improved-nanocomposite investment was approximated at 4-6% per year over the 20-year expected service life. Further, it was determined based on the 30% improvement in strength, this change may enable a 20-30% reduction in flywheel energy storage cost (%24/kW-h).

  11. The significance of specimen end restraint in high pressure triaxial testing of cohesive soil

    E-Print Network [OSTI]

    Casey, Brendan (Brendan Anthony)

    2011-01-01T23:59:59.000Z

    This thesis investigates the mechanical behaviour of cohesive soil at relatively high stresses with a particular emphasis on the significance of specimen end restraint on the interpretation of triaxial test results. Undrained ...

  12. Miniature Specimen Testing The Small Punch Test (SPT) has successfully been used in the US and in Japan

    E-Print Network [OSTI]

    Berlin,Technische Universität

    and in Japan to assess the material behavior of steels in nuclear reactor and pressure vessels as well1 Miniature Specimen Testing The Small Punch Test (SPT) has successfully been used in the US joints used therein Conventional tensile tests, shear tests as well as thermal cycle tests are used

  13. COMPARISON OF SHEAR STRENGTH OF CERAMIC JOINTS DETERMINED BY VARIOUS TEST METHODS WITH SMALL SPECIMENS

    SciTech Connect (OSTI)

    Shih, Chunghao Phillip [ORNL; Katoh, Yutai [ORNL; Kiggans Jr, James O [ORNL; Koyanagi, Takaaki [ORNL; Khalifa, Hesham [General Atomics, San Diego; Back, Christina A. [General Atomics, San Diego; Hinoki, Tatsuya [Kyoto University, Japan; Ferraris, Monica [Politecnico di Torino

    2015-01-01T23:59:59.000Z

    Four different shear test methods i.e. doubled notched shear test, asymmetrical four point bend test, Iosipescu test, and torsion test, were investigated for their ability to evaluate one standard SiC to SiC ceramic brittle joint while using small size specimens. Double notched shear test showed higher stress concentration at the notch base and a lower nominal shear strength. Both asymmetrical four point bend test and Iosipescu test utilized epoxy jointed metal extensors, which failed during test and caused misalignment and tensile type of failure. Torsion test can deliver true shear loading. However, base material failure was observed for the torsion joint samples in this study. None of the tests can successfully induce true shear failure of the joint because the joint is stronger and tougher than the SiC substrate. Torsion test appears to be promising because of the pure shear loading, less stress concentration, and easy alignment.

  14. Recent Accomplishments in the Irradiation Testing of Engineering-Scale Monolithic Fuel Specimens

    SciTech Connect (OSTI)

    N.E. Woolstenhulme; D.M. Wachs; M.K. Meyer; H.W. Glunz; R.B. Nielson

    2012-10-01T23:59:59.000Z

    The US fuel development team is focused on qualification and demonstration of the uranium-molybdenum monolithic fuel including irradiation testing of engineering-scale specimens. The team has recently accomplished the successful irradiation of the first monolithic multi-plate fuel element assembly within the AFIP-7 campaign. The AFIP-6 MKII campaign, while somewhat truncated by hardware challenges, exhibited successful irradiation of a large-scale monolithic specimen under extreme irradiation conditions. The channel gap and ultrasonic data are presented for AFIP-7 and AFIP-6 MKII, respectively. Finally, design concepts are summarized for future irradiations such as the base fuel demonstration and design demonstration experiment campaigns.

  15. Material Open Test Assembly Specimen Retrieval from Hanford's Shielded Material Facility

    SciTech Connect (OSTI)

    Valdez, Patrick LJ; Rinker, Michael W.

    2009-06-14T23:59:59.000Z

    Hanford’s 324 Building, the Shielded Material Facility (SMF), was developed to provide containment for research and fabrication development studies on highly radioactive metallic and ceramic nuclear reactor fuels and structural materials. Between 1983 and 1992, the SMF was used in support of the Department of Energy (DOE)-funded Fast Flux Test Facility (FFTF) Materials Open Test Assembly (MOTA) program. In this program, metallurgical specimens were irradiated in FFTF and then sent to SMF for processing and storage in two cabinets. This effort was abruptly ended in early 1990s due to programmatic shifts within the DOE, leaving many specimens unexamined. In recent years, these specimens have become of high value to new DOE programs. Pacific Northwest National Laboratory (PNNL) was tasked with retrieving specimens from one of the cabinets in support of fuel clad and duct development for the Advanced Fuel Cycle Initiative. Cesium contamination of the cell and failure of the overhead crane system utilized for opening the cabinets prevented PNNL from using the built-in hot cell equipment to gain access to the cabinets. PNNL designed and tested a lifting device to fit through a standard 10 inch diameter mechanical manipulator port in the SMF South Cell wall. The tool was successfully deployed in June 2008 with the support of Washington Closure Hanford.

  16. High heat flux testing of a two-tube copper panel specimen for LLNL at ASURF

    SciTech Connect (OSTI)

    Easoz, J.R.; Sink, D.A.

    1984-12-01T23:59:59.000Z

    This letter documents the results of the test program conducted for Lawrence Livermore National Laboratory (LLNL) by Westinghouse Advanced Energy Systems Division (AESD) in fulfillment of the Third Amendment to Subcontract 9125401. The original test matrix of 20,000 heating cycles on two test articles called for in the contract was not technically feasible due to the inability of the test articles supplied by LLNL to perform successfully at the required test conditions. Burnout occurred in one of the tubes of a two-tube target during the first series of tests. As a result, the work scope was changed by LLNL such that the tests on the milled copper plate panel specimen were replaced by a second set of heating tests on the second tube of the two-tube copper panel specimen to confirm the conditions for burnout failure. The testing requirements were completed following failure of the second tube at nominally identical conditions under which the first tube failed, and verification of these conditions. This letter completes all contractual obligations by serving as the final report on the test program.

  17. Apparatus and method for fatigue testing of a material specimen in a high-pressure fluid environment

    DOE Patents [OSTI]

    Wang, Jy-An; Feng, Zhili; Anovitz, Lawrence M; Liu, Kenneth C

    2013-06-04T23:59:59.000Z

    The invention provides fatigue testing of a material specimen while the specimen is disposed in a high pressure fluid environment. A specimen is placed between receivers in an end cap of a vessel and a piston that is moveable within the vessel. Pressurized fluid is provided to compression and tension chambers defined between the piston and the vessel. When the pressure in the compression chamber is greater than the pressure in the tension chamber, the specimen is subjected to a compression force. When the pressure in the tension chamber is greater than the pressure in the compression chamber, the specimen is subjected to a tension force. While the specimen is subjected to either force, it is also surrounded by the pressurized fluid in the tension chamber. In some examples, the specimen is surrounded by hydrogen.

  18. Manipulator having thermally conductive rotary joint for transferring heat from a test specimen

    DOE Patents [OSTI]

    Haney, S.J.; Stulen, R.H.; Toly, N.F.

    1983-05-03T23:59:59.000Z

    A manipulator for rotatably moving a test specimen in an ultra-high vacuum chamber includes a translational unit movable in three mutually perpendicular directions. A manipulator frame is rigidly secured to the translational unit for rotatably supporting a rotary shaft. A first copper disc is rigidly secured to an end of the rotary shaft for rotary movement within the vacuum chamber. A second copper disc is supported upon the first disc. The second disc receives a cryogenic cold head and does not rotate with the first disc. The second disc receives a cryogenic cold head and does not rotate with the first disc. A sapphire plate is interposed between the first and second discs to prevent galling of the copper material while maintaining high thermal conductivity between the first and second discs. A spring is disposed on the shaft to urge the second disc toward the first disc and compressingly engage the interposed sapphire plate. A specimen mount is secured to the first disc for rotation within the vacuum chamber. The specimen maintains high thermal conductivity with the second disc receiving the cryogenic transfer line.

  19. Manipulator having thermally conductive rotary joint for transferring heat from a test specimen

    DOE Patents [OSTI]

    Haney, Steven J. (Tracy, CA); Stulen, Richard H. (Livermore, CA); Toly, Norman F. (Livermore, CA)

    1985-01-01T23:59:59.000Z

    A manipulator for rotatably moving a test specimen in an ultra-high vacuum chamber includes a translational unit movable in three mutually perpendicular directions. A manipulator frame is rigidly secured to the translational unit for rotatably supporting a rotary shaft. A first copper disc is rigidly secured to an end of the rotary shaft for rotary movement within the vacuum chamber. A second copper disc is supported upon the first disc. The second disc receives a cryogenic cold head and does not rotate with the first disc. A sapphire plate is interposed between the first and second discs to prevent galling of the copper material while maintaining high thermal conductivity between the first and second discs. A spring is disposed on the shaft to urge the second disc toward the first disc and compressingly engage the interposed sapphire plate. A specimen mount is secured to the first disc for rotation within the vacuum chamber. The specimen maintains high thermal conductivity with the second disc receiving the cryogenic transfer line.

  20. Fracture assessment of HSST Plate 14 shallow-flaw cruciform bend specimens tested under biaxial loading conditions

    SciTech Connect (OSTI)

    Bass, B.R.; McAfee, W.J.; Williams, P.T.; Pennell, W.E.

    1998-06-01T23:59:59.000Z

    A technology to determine shallow-flaw fracture toughness of reactor pressure vessel (RPV) steels is being developed for application to the safety assessment of RPVs containing postulated shallow surface flaws. Matrices of cruciform beam tests were developed to investigate and quantify the effects of temperature, biaxial loading, and specimen size on fracture initiation toughness of two-dimensional (constant depth), shallow, surface flaws. The cruciform beam specimens were developed at Oak Ridge National Laboratory (ORNL) to introduce a far-field, out-of-plane biaxial stress component in the test section that approximates the nonlinear stresses resulting from pressurized-thermal-shock or pressure-temperature loading of an RPV. Tests were conducted under biaxial load ratios ranging from uniaxial to equibiaxial. These tests demonstrated that biaxial loading can have a pronounced effect on shallow-flaw fracture toughness in the lower transition temperature region for an RPV material. The cruciform fracture toughness data were used to evaluate fracture methodologies for predicting the observed effects of biaxial loading on shallow-flaw fracture toughness. Initial emphasis was placed on assessment of stress-based methodologies, namely, the J-Q formulation, the Dodds-Anderson toughness scaling model, and the Weibull approach. Applications of these methodologies based on the hydrostatic stress fracture criterion indicated an effect of loading-biaxiality on fracture toughness; the conventional maximum principal stress criterion indicated no effect. A three-parameter Weibull model based on the hydrostatic stress criterion is shown to correlate the experimentally observed biaxial effect on cleavage fracture toughness by providing a scaling mechanism between uniaxial and biaxial loading states.

  1. Apparatus for pre-stress-straining rod-type specimens in tension for in-situ passive fracture testing

    DOE Patents [OSTI]

    Wang, John Jy-an (Oak Ridge, TN); Liu, Ken C. (Oak Ridge, TN); Feng, Zhili (Knoxville, TN)

    2013-07-31T23:59:59.000Z

    A stress-strain testing apparatus imposes a stress-strain on a specimen while disposed in a controlled environment. Each end of the specimen is fastened to an end cap and a strain gage is attached to the specimen. An adjusting mechanism and a compression element are disposed between the end caps forming a frame for applying forces to the end caps and thereby stress-straining the specimen. The adjusting mechanism may be extended or retracted to increase or decrease the imposed stress-strain on the specimen, and the stress-strain is measured by the strain gage on the specimen while the apparatus is exposed to an environment such as high pressure hydrogen. Strain gages may be placed on the frame to measure stress-strains in the frame that may be caused by the environment.

  2. Surface Power Radiative Cooling Tests

    SciTech Connect (OSTI)

    Vaughn, Jason; Schneider, Todd [Environmental Effects Branch, EM50, NASA Marshall Space Flight Center, AL 35812 (United States)

    2006-01-20T23:59:59.000Z

    Terrestrial nuclear power plants typically maintain their temperature through convective cooling, such as water and forced air. However, the space environment is a vacuum environment, typically 10-8 Torr pressure, therefore in proposed missions to the lunar surface, power plants would have to rely on radiative cooling to remove waste heat. Also, the Martian surface has a very tenuous atmosphere (e.g. {approx}5 Torr CO2), therefore, the main heat transfer method on the Martian surface is also radiative. Because of the lack of atmosphere on the Moon and the tenuous atmosphere on Mars, surface power systems on both the Lunar and Martian surface must rely heavily on radiative heat transfer. Because of the large temperature swings on both the lunar and the Martian surfaces, trying to radiate heat is inefficient. In order to increase power system efficiency, an effort is underway to test various combinations of materials with high emissivities to demonstrate their ability to survive these degrading atmospheres to maintain a constant radiator temperature improving surface power plant efficiency. An important part of this effort is the development of a unique capability that would allow the determination of a materials emissivity at high temperatures. A description of the test capability as well as initial data is presented.

  3. Failure Surface Analysis of Polyimide/Titanium Notched Coating Adhesion Specimens

    SciTech Connect (OSTI)

    GIUNTA,RACHEL K.; KANDER,RONALD G.

    2000-12-18T23:59:59.000Z

    Adhesively bonded joints of LaRC{trademark} PETI-5, a phenylethynyl-terminated polyimide, with chromic acid anodized titanium were fabricated and debonded interfacially. The adhesive-substrate failure surfaces were investigated using several surface analysis techniques. From Auger spectroscopy, field emission scanning electron microscopy, and atomic force microscopy studies, polymer appears to be penetrating the pores of the anodized substrate to a depth of approximately 100 nm. From x-ray photoelectron spectroscopy data, the polymer penetrating the pores appears to be in electrical contact with the titanium substrate, leading to differential charging. These analyses confirm that the polymer is becoming mechanically interlocked within the substrate surface.

  4. Test surfaces useful for calibration of surface profilometers

    DOE Patents [OSTI]

    Yashchuk, Valeriy V; McKinney, Wayne R; Takacs, Peter Z

    2013-12-31T23:59:59.000Z

    The present invention provides for test surfaces and methods for calibration of surface profilometers, including interferometric and atomic force microscopes. Calibration is performed using a specially designed test surface, or the Binary Pseudo-random (BPR) grating (array). Utilizing the BPR grating (array) to measure the power spectral density (PSD) spectrum, the profilometer is calibrated by determining the instrumental modulation transfer.

  5. Methods for identifying cancellous bone specimen location and size for the Reduced Platen Compression Test 

    E-Print Network [OSTI]

    Cowen, Kyle Ray

    2013-02-22T23:59:59.000Z

    , and stimuli on the skeleton and its ability to perform these everyday functions. The current state of bone testing is focused on understanding the mechanical properties of bone through use of traditional mechanical testing procedures such as three point...

  6. Method for thinning specimen

    DOE Patents [OSTI]

    Follstaedt, David M.; Moran, Michael P.

    2005-03-15T23:59:59.000Z

    A method for thinning (such as in grinding and polishing) a material surface using an instrument means for moving an article with a discontinuous surface with an abrasive material dispersed between the material surface and the discontinuous surface where the discontinuous surface of the moving article provides an efficient means for maintaining contact of the abrasive with the material surface. When used to dimple specimens for microscopy analysis, a wheel with a surface that has been modified to produce a uniform or random discontinuous surface significantly improves the speed of the dimpling process without loss of quality of finish.

  7. Fracture toughness testing of Linde 1092 reactor vessel welds in the transition range using Charpy-sized specimens

    SciTech Connect (OSTI)

    Pavinich, W.A. [Framatome Technologies Inc., Knoxville, TN (United States); Yoon, K.K. [Framatome Technologies Inc., Lynchburg, VA (United States); Hour, K.Y. [Babcock and Wilcox Co., Lynchburg, VA (United States). Research and Development Div.; Hoffman, C.L. [ABB-CE, Windsor, CT (United States)

    1999-10-01T23:59:59.000Z

    The present reference toughness method for predicting the change in fracture toughness can provide over estimates of these values because of uncertainties in initial RT{sub NDT} and shift correlations. It would be preferable to directly measure fracture toughness. However, until recently, no standard method was available to characterize fracture toughness in the transition range. ASTM E08 has developed a draft standard that shows promise for providing lower bound transition range fracture toughness using the master curve approach. This method has been successfully implemented using 1T compact fracture specimens. Combustion Engineering reactor vessel surveillance programs do not have compact fracture specimens. Therefore, the CE Owners Group developed a program to validate the master curve method for Charpy-sized and reconstituted Charpy-sized specimens for future application on irradiated specimens. This method was validated for Linde 1092 welds using unirradiated Charpy-sized and reconstituted Charpy-sized specimens by comparison of results with those from compact fracture specimens.

  8. Biaxial Creep Specimen Fabrication

    SciTech Connect (OSTI)

    JL Bump; RF Luther

    2006-02-09T23:59:59.000Z

    This report documents the results of the weld development and abbreviated weld qualification efforts performed by Pacific Northwest National Laboratory (PNNL) for refractory metal and superalloy biaxial creep specimens. Biaxial creep specimens were to be assembled, electron beam welded, laser-seal welded, and pressurized at PNNL for both in-pile (JOYO reactor, O-arai, Japan) and out-of-pile creep testing. The objective of this test campaign was to evaluate the creep behavior of primary cladding and structural alloys under consideration for the Prometheus space reactor. PNNL successfully developed electron beam weld parameters for six of these materials prior to the termination of the Naval Reactors program effort to deliver a space reactor for Project Prometheus. These materials were FS-85, ASTAR-811C, T-111, Alloy 617, Haynes 230, and Nirnonic PE16. Early termination of the NR space program precluded the development of laser welding parameters for post-pressurization seal weldments.

  9. Fabrication Control Plan for ORNL RH-LOCA ATF Test Specimens to be Irradiated in the ATR

    SciTech Connect (OSTI)

    Kevin G. Field; Richard Howard; Michael Teague

    2014-06-01T23:59:59.000Z

    The purpose of this fabrication plan is (1) to summarize the design of a set of rodlets that will be fabricated and then irradiated in the Advanced Test Reactor (ATR) and (2) provide requirements for fabrication and acceptance criteria for inspections of the Light Water Reactor (LWR) – Accident Tolerant Fuels (ATF) rodlet components. The functional and operational (F&OR) requirements for the ATF program are identified in the ATF Test Plan. The scope of this document only covers fabrication and inspections of rodlet components detailed in drawings 604496 and 604497. It does not cover the assembly of these items to form a completed test irradiation assembly or the inspection of the final assembly, which will be included in a separate INL final test assembly specification/inspection document. The controls support the requirements that the test irradiations must be performed safely and that subsequent examinations must provide valid results.

  10. Determination of Interfacial Mechanical Properties of Ceramic Composites by the Compression of Micro-pillar Test Specimens

    SciTech Connect (OSTI)

    Shih, Chunghao [ORNL; Katoh, Yutai [ORNL; Leonard, Keith J [ORNL; Bei, Hongbin [ORNL; Lara-Curzio, Edgar [ORNL

    2013-01-01T23:59:59.000Z

    A novel method to determine the fiber-matrix interfacial properties of ceramic matrix composites is proposed and evaluated; where micro- pillar samples containing inclined fiber/matrix interfaces were prepared from a SiC fiber reinforced SiC matrix composites then compression-tested using the nano-indentation technique. This new test method employs a simple geometry and mitigates the uncertainties associated with complex stress state in the conventional single filament push-out method for the determination of interfacial properties. Based on the test results using samples with different interface orientations , the interfacial debond shear strength and the internal friction coefficient are explicitly determined and compared with values obtained by other test methods.

  11. Apparatuses for prestressing rod-type specimens in torsion for in-situ passive fracture toughness testing in an extremely high-pressure environment of hydrogen

    DOE Patents [OSTI]

    Wang, Jy-an (Oak Ridge, TN); Liu, Ken C. (Oak Ridge, TN); Feng, Zhili (Knoxville, TN)

    2012-05-15T23:59:59.000Z

    An in-situ specimen fixture particularly adapted for prestressing rod-type SNTT-type specimens comprising a tube and end cap wherein the specimen is secured at one end to the tube, and at the opposite end to the end cap. The end cap is rotatable relative to the tube, and may be fixedly secured for creating a torsional force prestressing the specimen enclosed within the tube.

  12. ARM: Surface Radiation Measurement Quality Control testing, including climatologically configurable limits

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Hodges, Gary; Stoffel, Tom; Kutchenreiter, Mark; Kay, Bev; Habte, Aron; Ritsche, Michael; Morris, Victor; Anderberg, Mary

    Surface Radiation Measurement Quality Control testing, including climatologically configurable limits

  13. Multiple Irradiation Capsule Experiment (MICE)-3B Irradiation Test of Space Fuel Specimens in the Advanced Test Reactor (ATR) - Close Out Documentation for Naval Reactors (NR) Information

    SciTech Connect (OSTI)

    M. Chen; CM Regan; D. Noe

    2006-01-09T23:59:59.000Z

    Few data exist for UO{sub 2} or UN within the notional design space for the Prometheus-1 reactor (low fission rate, high temperature, long duration). As such, basic testing is required to validate predictions (and in some cases determine) performance aspects of these fuels. Therefore, the MICE-3B test of UO{sub 2} pellets was designed to provide data on gas release, unrestrained swelling, and restrained swelling at the upper range of fission rates expected for a space reactor. These data would be compared with model predictions and used to determine adequacy of a space reactor design basis relative to fission gas release and swelling of UO{sub 2} fuel and to assess potential pellet-clad interactions. A primary goal of an irradiation test for UN fuel was to assess performance issues currently associated with this fuel type such as gas release, swelling and transient performance. Information learned from this effort may have enabled use of UN fuel for future applications.

  14. Development of Reconstitution Technology for Surveillance Specimens

    SciTech Connect (OSTI)

    Yasushi Atago; Shunichi Hatano; Eiichiro Otsuka [Japan Power Engineering and Inspection Corporation, KDX Shibadaimon Bldg. 3FL., 10-12, 2-chome Shiba-daimon, Minato-ku, Tokyo, 105-0012 (Japan)

    2002-07-01T23:59:59.000Z

    The Japan Power Engineering and Inspection Corporation (JAPEIC) has been carrying out the project titled 'Nuclear Power Plant Integrated Management Technology (PLIM)' consigned by Japanese Ministry of Economy, Trade and Industry (METI) since 1996FY as a 10-years project. As one of the project themes, development of reconstitution technology for reactor pressure vessel (RPV/RV) surveillance specimens, which are installed in RPVs to monitor the neutron irradiation embrittlement on RPV/RV materials, is now on being carried out to deal with the long-term operation of nuclear power plants. The target of this theme is to establish the technical standard for applicability of reconstituted surveillance specimens including the reconstitution of the Charpy specimens and Compact Tension (CT) specimens. With the Charpy specimen reconstitution, application of 10 mm length inserts is used, which enables the conversion of tests from the LT-direction to the TL-direction. This paper presents the basic data from Charpy and CT specimens of RPV materials using the surveillance specimens obtained for un-irradiated materials including the following. 1) Reconstitution Technology of Charpy Specimens. a) The interaction between plastic zone and Heat Affected Zone (HAZ). b) The effects of the possible deviations from the standard specimens for the reconstituted specimens. 2) Reconstitution Technology of CT specimens. a) The correlation between fracture toughness and plastic zone width. Because the project is now in progress, this paper describes the outline of the results obtained as of the end of 2000 FY. (authors)

  15. Test probe for surface mounted leadless chip carrier

    DOE Patents [OSTI]

    Meyer, Kerry L. (Raytown, MO); Topolewski, John (Lenexa, KS)

    1989-05-23T23:59:59.000Z

    A test probe for a surface mounted leadless chip carrier is disclosed. The probed includes specially designed connector pins which allow size reductions in the probe. A thermoplastic housing provides spring action to ensure good mechanical and electrical contact between the pins and the contact strips of a leadless chip carrier. Other features include flexible wires molded into the housing and two different types of pins alternately placed in the housing. These features allow fabrication of a smaller and simpler test probe.

  16. Specimen illumination apparatus with optical cavity for dark field illumination

    DOE Patents [OSTI]

    Pinkel, Daniel (Walnut Creek, CA); Sudar, Damir (Walnut Creek, CA); Albertson, Donna (Lafayette, CA)

    1999-01-01T23:59:59.000Z

    An illumination apparatus with a specimen slide holder, an illumination source, an optical cavity producing multiple reflection of illumination light to a specimen comprising a first and a second reflective surface arranged to achieve multiple reflections of light to a specimen is provided. The apparatus can further include additional reflective surfaces to achieve the optical cavity, a slide for mounting the specimen, a coverslip which is a reflective component of the optical cavity, one or more prisms for directing light within the optical cavity, antifading solutions for improving the viewing properties of the specimen, an array of materials for analysis, fluorescent components, curved reflective surfaces as components of the optical cavity, specimen detection apparatus, optical detection equipment, computers for analysis of optical images, a plane polarizer, fiberoptics, light transmission apertures, microscopic components, lenses for viewing the specimen, and upper and lower mirrors above and below the specimen slide as components of the optical cavity. Methods of using the apparatus are also provided.

  17. Surface-enhanced raman medical probes and system for disease diagnosis and drug testing

    DOE Patents [OSTI]

    Vo-Dinh, Tuan (Knoxville, TN)

    1999-01-01T23:59:59.000Z

    A probe for a surface-enhanced Raman scattering spectrometer includes a member of optically transmissive material for receiving the excitation radiation from a laser and for carrying the radiation emitted from a specimen to a detector. An end of the member for placing against the specimen has a coating that produces surface enhancement of the specimen during Raman scattering spectroscopic analysis. Specifically the coating is formed by a first layer of microparticles on the member and a metal layer over the first layer. The first layer may form a microstructure surface over which a metal layer is applied. Alternatively the coating may be a material containing microparticles of a metal. An optional layer of a material may be applied to the metal layer to concentrate onto the probe compounds of analytical interest onto the probe.

  18. Surface-enhanced Raman medical probes and system for disease diagnosis and drug testing

    DOE Patents [OSTI]

    Vo-Dinh, T.

    1999-01-26T23:59:59.000Z

    A probe for a surface-enhanced Raman scattering spectrometer includes a member of optically transmissive material for receiving the excitation radiation from a laser and for carrying the radiation emitted from a specimen to a detector. An end of the member for placing against the specimen has a coating that produces surface enhancement of the specimen during Raman scattering spectroscopic analysis. Specifically the coating is formed by a first layer of microparticles on the member and a metal layer over the first layer. The first layer may form a microstructure surface over which a metal layer is applied. Alternatively the coating may be a material containing microparticles of a metal. An optional layer of a material may be applied to the metal layer to concentrate onto the probe compounds of analytical interest onto the probe. 39 figs.

  19. Test probe for surface mounted leadless chip carrier

    DOE Patents [OSTI]

    Meyer, K.L.; Topolewski, J.

    1987-10-02T23:59:59.000Z

    A test probe for a surface mounted leadless chip carrier is disclosed. The probe includes specially designed connector pins which allow size reductions in the probe. A thermoplastic housing provides spring action to ensure good mechanical and electrical contact between the pins and the contact strips of a leadless chip carrier. Other features include flexible wires molded into the housing and two different types of pins alternately placed in the housing. These features allow fabrication of a smaller and simpler test probe. 1 fig.

  20. : runout specimen max : maximum fatigue stress

    E-Print Network [OSTI]

    High Performance Fibre Reinforced Concrete (UHPFRC) layer to concrete bridge deck slab was conceived was drawn without runout specimens .) Figure 6 Fatigue fracture surface of (a) UHPFRC, (b) steel rebar (a influenced by fibre distribution and orientation. Fatigue fracture surface of UHPFRC is similar

  1. Fabrication of specimens with controlled flaws

    SciTech Connect (OSTI)

    Edwards, R.L.; Gruber, G.J.; Watson, P.D. [Southwest Research Inst., San Antonio, TX (United States)

    1995-10-01T23:59:59.000Z

    Most nondestructive evaluation (NDE) codes and standards require that the NDE equipment be calibrated using a calibration block. Ultrasonic testing (UT) historically has required the use of side-drilled or flat-bottom holes or notches. Recent technology has recognized that the acoustic response of real flaws is not directly comparable to artificial reflectors. The need arose to manufacture UT test specimens that contained real flaws of known size, shape, position, and orientation. The 1989 Section XI ASME Code, Appendix VIII (ASME Code, 1989), requires NDE qualification of equipment, procedures, and personnel utilizing full-scale test specimens with actual (real) flaws. The same technology could prove of great benefit to industries other than nuclear, particularly for the fracture mechanics approach to fitness-for-purpose or lifetime-extension programs. This paper describes an approach to the design and fabrication of NDE test specimens with controlled flaws.

  2. STRESS CORROSION CRACKING IN TEAR DROP SPECIMENS

    SciTech Connect (OSTI)

    Lam, P; Philip Zapp, P; Jonathan Duffey, J; Kerry Dunn, K

    2009-05-01T23:59:59.000Z

    Laboratory tests were conducted to investigate the stress corrosion cracking (SCC) of 304L stainless steel used to construct the containment vessels for the storage of plutonium-bearing materials. The tear drop corrosion specimens each with an autogenous weld in the center were placed in contact with moist plutonium oxide and chloride salt mixtures. Cracking was found in two of the specimens in the heat affected zone (HAZ) at the apex area. Finite element analysis was performed to simulate the specimen fabrication for determining the internal stress which caused SCC to occur. It was found that the tensile stress at the crack initiation site was about 30% lower than the highest stress which had been shifted to the shoulders of the specimen due to the specimen fabrication process. This finding appears to indicate that the SCC initiation took place in favor of the possibly weaker weld/base metal interface at a sufficiently high level of background stress. The base material, even subject to a higher tensile stress, was not cracked. The relieving of tensile stress due to SCC initiation and growth in the HAZ and the weld might have foreclosed the potential for cracking at the specimen shoulders where higher stress was found.

  3. Land surface cleanup of plutonium at the Nevada Test Site

    SciTech Connect (OSTI)

    Ebeling, L.L.; Evans, R.B.; Walsh, E.J.

    1991-01-01T23:59:59.000Z

    The Nevada Test Site (NTS) covers approximately 3300 km{sup 2} of high desert and is located approximately 100 km northwest of Las Vegas, Nevada. Soil contaminated by plutonium exists on the NTS and surrounding areas from safety tests conducted in the 1950s and 1960s. About 150 curies of contamination have been measured over 1200 hectares of land surface. Most contamination is found in the top 5 cm of soil but may be found deep as 25 cm. The cost of conventional removal and disposal of the full soil volume has been estimated at over $500,000,000. This study is directed toward minimizing the volume of waste which must be further processed and disposed of by precisely controlling soil removal depth. The following soil removal machines were demonstrated at the NTS: (1) a CMI Corporation Model PR-500FL pavement profiler, (2) a CMI Corporation Model Tr-225B trimmer reclaimer, (3) a Caterpillar Model 623 elevating scraper equipped with laser depth control, (4) a Caterpillar Model 14G motor grader equipped with laser depth control, (5) a Caterpillar Model 637 auger scraper, and (6) a XCR Series Guzzler vacuum truck. 5 refs., 5 figs.

  4. Model Test Setup and Program for Experimental Estimation of Surface Loads of the SSG Kvitsy

    E-Print Network [OSTI]

    Model Test Setup and Program for Experimental Estimation of Surface Loads of the SSG Kvitsøy Pilot Engineering No. 32 ISSN: 1603-9874 Model Test Setup and Program for Experimental Estimation of Surface Loads University October, 2005 #12;#12;Preface This report presents the preparations done prior to model tests

  5. Ultrasonic thickness testing of aging offshore structures

    E-Print Network [OSTI]

    Ellison, Brian Kirk

    1999-01-01T23:59:59.000Z

    . 14 2. 15 2. 16 2. 17 2. 18 New Anode. Spent Anode 1989 JIP Specimens. Dual Transducer Sound Paths. Specimens for Feasibility Studies (View I). Specimens for Feasibility Studies (View 2) . General Nomenclature. Transducer / Surface... study in an attempt to improve the effectiveness of ultrasonic thickness testing. Motivation for research stems from a joint industry project (JIP) that took place at Texas AIkM University (TAMU) from 1989 to 1990 (Moehlman 1990). In 1989, several...

  6. Page 1 of 8 2012 MSU Center for Biofilm Engineering Testing Surface Disinfectants

    E-Print Network [OSTI]

    Dyer, Bill

    Center for Biofilm Engineering As an example of the recognition that concurrent controls are importantPage 1 of 8 © 2012 MSU Center for Biofilm Engineering Testing Surface Disinfectants This series The importance of concurrent control carriers in laboratory tests of surface disinfectants [Key Words: efficacy

  7. Surface runoff features on Mars: Testing the carbon dioxide formation hypothesis

    E-Print Network [OSTI]

    Nimmo, Francis

    materials and properties; KEYWORDS: Mars, gullies, seepage, runoff, carbon dioxide, water Citation: StewartSurface runoff features on Mars: Testing the carbon dioxide formation hypothesis Sarah T. Stewart1, S. T., and F. Nimmo, Surface runoff features on Mars: Testing the carbon dioxide formation

  8. Manufacturing of Plutonium Tensile Specimens

    SciTech Connect (OSTI)

    Knapp, Cameron M [Los Alamos National Laboratory

    2012-08-01T23:59:59.000Z

    Details workflow conducted to manufacture high density alpha Plutonium tensile specimens to support Los Alamos National Laboratory's science campaigns. Introduces topics including the metallurgical challenge of Plutonium and the use of high performance super-computing to drive design. Addresses the utilization of Abaqus finite element analysis, programmable computer numerical controlled (CNC) machining, as well as glove box ergonomics and safety in order to design a process that will yield high quality Plutonium tensile specimens.

  9. Langasite Surface Acoustic Wave Sensors: Fabrication and Testing

    SciTech Connect (OSTI)

    Zheng, Peng; Greve, David W.; Oppenheim, Irving J.; Chin, Tao-Lun; Malone, Vanessa

    2012-02-01T23:59:59.000Z

    We report on the development of harsh-environment surface acoustic wave sensors for wired and wireless operation. Surface acoustic wave devices with an interdigitated transducer emitter and multiple reflectors were fabricated on langasite substrates. Both wired and wireless temperature sensing was demonstrated using radar-mode (pulse) detection. Temperature resolution of better than ±0.5°C was achieved between 200°C and 600°C. Oxygen sensing was achieved by depositing a layer of ZnO on the propagation path. Although the ZnO layer caused additional attenuation of the surface wave, oxygen sensing was accomplished at temperatures up to 700°C. The results indicate that langasite SAW devices are a potential solution for harsh-environment gas and temperature sensing.

  10. On Surface Cryogenic System Comissioning Preliminary Test Results

    E-Print Network [OSTI]

    McDonald, Kirk

    Drain Line TL1 Filling TL2 TL3 SURFACE UNDERGROUND TT10TT2TT2a Heat Echanger Heater 20kW Event/10 SafetyvalvescollectorDN50 DN20Ø16/14 TBD ATM. Ø12/10 Ø12/10 DN15 DN25 DN50 DN32 DN25 DN32 DN15 #12;Step 1 : Fill Phase by CV202. Step 2 : Fill Cryostat from LN2 phase separator - open CV204 which connects the phase

  11. The reconstitution of Charpy-size tensile specimens

    SciTech Connect (OSTI)

    Ransbeeck, T. van; Walle, E. van; Fabry, A.; Puzzolante, J.L.; Velde, J. van de [SCK-CEN, Mol (Belgium)

    1996-12-31T23:59:59.000Z

    Charpy-size tensile specimens have been reconstituted starting from broken Charpy specimens. Precautions have been taken to prevent fracture in the weld regions of the reconstituted specimens. Careful qualification of the tensile properties of the reconstituted tensile bars has been established and is in agreement with test results on ASTM/E8-size tensile specimens. The tensile properties of the unirradiated weld material of the Belgian PWR Doel 2 and of the unirradiated base metal of the German BWR Philippsburg 1 have been determined using this methodology. Both the resulting yield and maximum loads are in agreement with the actual expectations. Qualification to apply the technique on irradiated specimens is in preparation.

  12. Do et al. 1 Full Scale Tests for the Assessment of Wear of Pavement Surfaces

    E-Print Network [OSTI]

    Boyer, Edmond

    Do et al. 1 Full Scale Tests for the Assessment of Wear of Pavement Surfaces Minh-Tan Do subjected to heavy traffic. Reports can be found in (1)(2). Evolution of pavements during its whole service shown in the figure 2. By this way, during tests on one track, pavement construction can be carried out

  13. Plutonium-238 observations as a test of modeled transport and surface deposition of meteoric smoke particles

    E-Print Network [OSTI]

    Chipperfield, Martyn

    Plutonium-238 observations as a test of modeled transport and surface deposition of meteoric smoke chemistry-climate model (CCM) to simulate the transport and deposition of plutonium- 238 oxide nanoparticles. P. Chipperfield, and J. M. C. Plane (2013), Plutonium-238 observations as a test of modeled

  14. Development of a hybrid microcircuit test vehicle for surface mount applications

    SciTech Connect (OSTI)

    Hernandez, C.L.; Hosking, F.M.; Vianco, P.T.

    1997-08-01T23:59:59.000Z

    The technology drivers of the electronics industry continue to be systems miniaturization and reliability, in addition to addressing a variety of important environmental concerns. Surface mount technology (SMT) has evolved in response to these issues. Prototype hybrid test vehicles have been developed at Sandia National Laboratories to evaluate three lead-free solders for Au-Pt-Pd thick film soldering. The alloys are based on the Sn-Ag, Sn-Ag-Bi and Sn-Ag-Bi-Au systems. Populated test vehicles with surface mount devices were designed and fabricated to evaluate actual solder joints. Pastes were screen printed on the test substrates and reflowed with the components in place. The test components consist of a variety of dummy chip capacitors and leadless ceramic chip carriers (LCC`s). The development of the reflow profiles will be discussed. Comprehensive defect analysis will also be presented.

  15. Feasibility of Ground Testing a Moon and Mars Surface Power Reactor in EBR-II

    SciTech Connect (OSTI)

    Sheryl Morton; Carl Baily; Tom Hill; Jim Werner

    2006-02-01T23:59:59.000Z

    Ground testing of a surface fission power system would be necessary to verify the design and validate reactor performance to support safe and sustained human exploration of the Moon and Mars. The Idaho National Laboratory (INL) has several facilities that could be adapted to support a ground test. This paper focuses on the feasibility of ground testing at the Experimental Breeder Reactor II (EBR-II) facility and using other INL existing infrastructure to support such a test. This brief study concludes that the INL EBR-II facility and supporting infrastructure are a viable option for ground testing the surface power system. It provides features and attributes that offer advantages to locating and performing ground testing at this site, and it could support the National Aeronautics and Space Administration schedules for human exploration of the Moon. This study used the initial concept examined by the U.S. Department of Energy Inter-laboratory Design and Analysis Support Team for surface power, a lowtemperature, liquid-metal, three-loop Brayton power system. With some facility modification, the EBR-II can safely house a test chamber and perform long-term testing of the space reactor power system. The INL infrastructure is available to receive and provide bonded storage for special nuclear materials. Facilities adjacent to EBR-II can provide the clean room environment needed to assemble and store the test article assembly, disassemble the power system at the conclusion of testing, and perform posttest examination. Capability for waste disposal is also available at the INL.

  16. Detection of Macrosegregation in a Large Metallic Specimen Using XRF

    E-Print Network [OSTI]

    Cambridge, University of

    Detection of Macrosegregation in a Large Metallic Specimen Using XRF E.J. Pickeringa , M. Hollandb the removal of significant quantitites of material. X-ray fluorescence (XRF) spectroscopy, on the other hand being enclosed in a vacuum or destroyed beyond basic surface preparation. XRF spectroscopy has its

  17. Evaluation of methods to measure surface level in waste storage tanks: Second test sequence

    SciTech Connect (OSTI)

    Peters, T.J.; Park, W.R.

    1993-09-01T23:59:59.000Z

    This report describes the results of a program conducted at the Pacific Northwest Laboratory (PNL) and Westinghouse Hanford Company (WHC) to identify alternative methods to measure the surface level in the waste tanks. This program examined commercially available devices for measuring the distance to a target. This is a continuation of a program started in FY93. In the first test sequence, tests were performed.on five devices to determine their applicability to measure the surface level in the waste tanks. The devices were the Enraf-Nonius{trademark} Model 872 Radar Gauge, the Enraf-Nonius{trademark} Model 854 Advanced Technology Gauge (ATG), the Stanley Tool Laser Measuring Device, the Robertshaw Inven-Tel{reg_sign} Precision Level Gauge, and the Micro Switch Model 942 Acoustic Sensor. In addition, discussions were held with several manufacturer representatives regarding other potential devices. The results of these tests were documented in a previous report. Two additional devices were tested in this test sequence. The devices were the Krohne Model BM-70 level radar gauge and the L&J Technologies Model MCG-1500XL Servo Gauge. In addition, a 4--20 ma output board was installed in the ATG and the current output was monitored to determine the accuracy of the gauge through this board. Also, tests were conducted with a redesigned displacer for the ATG. The displacer was designed to minimize the possibility of (1) getting caught in the riser and (2) obtaining crystal growth on the surface.

  18. Disk-shaped Compact Tension Test for Asphalt Concrete Fracture

    E-Print Network [OSTI]

    Paulino, Glaucio H.

    Disk-shaped Compact Tension Test for Asphalt Concrete Fracture by M.P.Wagoner, W.G. Buttlar and G geometry is the ability to test cylindrical cores obtained from in-place asphalt concrete pavements finalizing the specimen geometry, a typical asphalt concrete surface mixture was tested at various

  19. Evaluation of the upper shelf energy for ferritic steels from miniaturized Charpy specimen data

    SciTech Connect (OSTI)

    Kurishita, Hiroaki; Narui, Minoru; Kayano, Hideo [Tohoku Univ., Oarai, Ibaraki (Japan). Inst. for Materials Research; Shibahara, Itaru; Mizuta, Syunji [Power Reactor and Nuclear Fuel Development Corp., Oarai, Ibaraki (Japan)

    1996-12-31T23:59:59.000Z

    The small specimen technology is required in mechanical testing of irradiated materials because of very limited irradiation volume in currently available high flux reactors and future accelerator-based high energy neutron sources. In order to develop the methodology to evaluate the upper shelf energy (USE) for full size Charpy specimens of ferritic steels from miniaturized specimen data, the effects of specimen size and notch dimensions (notch root radius and notch depth) on the USE were studied for high strength ferritic steels with relatively low USE values of 135 and 107 J. The USE for miniaturized specimens, normalized by Bb{sup 2} or (Bb){sup 3/2} (B is the specimen thickness, b is the ligament size), was essentially independent of specimen size and tended to decrease with increasing the elastic stress concentration factor, K{sub t}, but the K{sub t} dependence was not significant. The normalized USE for full size specimens was considerably lower than that for miniaturized specimens. A general relationship was found that allows to determine the USE of full size specimens of ferritic steels directly from miniaturized specimen data.

  20. A study of coal particle shape and three-body wear: Part 1, Design and development of a new three-body wear testing machine: Part 2, Particle shape and three-body wear

    SciTech Connect (OSTI)

    Clark, N.N.; Means, K.H.; James, R.; Thompson, T.

    1991-01-01T23:59:59.000Z

    Three-body wear involves two surfaces and an intermediate particle trapped between the two surfaces. A machine has been constructed to measure normal and frictional forces due to three-body wear. This machine accurately positions specimens a predetermined distance apart from each other and introduces particles to the interface between the specimens. Different types of specimen combinations have been tested to give a variety of data. Loads that result from the wear test are sampled and stored. Wear coefficients and rates of wear have been calculated for all specimens. (VC)

  1. Midtemperature solar systems test facility predictions for thermal performance based on test data. Toltec two-axis tracking solar collector with 3M acrylic polyester film reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-06-01T23:59:59.000Z

    Thermal performance predictions based on test data are presented for the Toltec solar collector, with acrylic film reflector surface, for three output temperatures at five cities in the United States.

  2. Midtemperature solar systems test facility predictions for thermal performance based on test data. Polisolar Model POL solar collector with glass reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-05-01T23:59:59.000Z

    Thermal performance predictions based on test data are presented for the Polisolar Model POL solar collector, with glass reflector surfaces, for three output temperatures at five cities in the United States.

  3. Effect of metallic coatings on the thermal contact conductance of turned surfaces

    E-Print Network [OSTI]

    Kang, Tik Kwie

    1989-01-01T23:59:59.000Z

    transfer mechanism in joints and verify the existing analyses. In this study four different types of metals of different surface finish including 6061 T6 aluminum were tested in a vacuum. The load (0 to 7800 tips) was varied in ascending and descending... fabricated in the same manner. After exposure to the atmosphere for several days, all specimens were kept in vacuum to prevent continued oxidation. The temperatures along the test specimen:; were measured using Chromel- Alumel AWG-30 thermocouples which...

  4. Midtemperature Solar Systems Test Facility predictions for thermal performance based on test data: Custom Engineering trough with glass reflector surface and Sandia-designed receivers

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-05-01T23:59:59.000Z

    Thermal performance predictions based on test data are presented for the Custom Engineering trough and Sandia-designed receivers, with glass reflector surface, for three output temperatures at five cities in the United States. Two experimental receivers were tested, one with an antireflective coating on the glass envelope around the receiver tube and one without the antireflective coating.

  5. Test of the Fluctuation Relation in lagrangian turbulence on a free surface

    E-Print Network [OSTI]

    M. M. Bandi; J. R. Cressman Jr.; W. I. Goldburg

    2007-03-07T23:59:59.000Z

    The statistics of lagrangian velocity divergence are studied for an assembly of particles in compressible turbulence on a free surface. Under an appropriate definition of entropy, the two-dimensional lagrangian velocity divergence of a particle trajectory represents the local entropy rate, a random variable. The statistics of this rate are shown to be in agreement with the fluctuation relation (FR) over a limited range. The probability distribution functions (PDFs) obtained in this analysis exhibit features different from those observed in previous experimental tests.

  6. Surfaces

    E-Print Network [OSTI]

    DeMaio, Ernest Vincent, 1964-

    1989-01-01T23:59:59.000Z

    Surfaces is a collection of four individual essays which focus on the characteristics and tactile qualities of surfaces within a variety of perceived landscapes. Each essay concentrates on a unique surface theme and purpose; ...

  7. Extreme Resistance of Superhydrophobic Surfaces to Impalement: Reversible Electrowetting Related to the Impacting/Bouncing Drop Test

    E-Print Network [OSTI]

    Brunet, Philippe

    Extreme Resistance of Superhydrophobic Surfaces to Impalement: Reversible Electrowetting Related reports on the comparison of the wetting properties of superhydrophobic silicon nanowires (NWs), usingPa, while most of the superhydrophobic surfaces tested so far have impalement thresholds smaller than 10 k

  8. Closeout of JOYO-1 Specimen Fabrication Efforts

    SciTech Connect (OSTI)

    ME Petrichek; JL Bump; RF Luther

    2005-10-31T23:59:59.000Z

    Fabrication was well under way for the JOYO biaxial creep and tensile specimens when the NR Space program was canceled. Tubes of FS-85, ASTAR-811C, and T-111 for biaxial creep specimens had been drawn at True Tube (Paso Robles, CA), while tubes of Mo-47.5 Re were being drawn at Rhenium Alloys (Cleveland, OH). The Mo-47.5 Re tubes are now approximately 95% complete. Their fabrication and the quantities produced will be documented at a later date. End cap material for FS-85, ASTAR-811C, and T-111 had been swaged at Pittsburgh Materials Technology, Inc. (PMTI) (Large, PA) and machined at Vangura (Clairton, PA). Cutting of tubes, pickling, annealing, and laser engraving were in process at PMTI. Several biaxial creep specimen sets of FS-85, ASTAR-811C, and T-111 had already been sent to Pacific Northwest National Laboratory (PNNL) for weld development. In addition, tensile specimens of FS-85, ASTAR-811C, T-111, and Mo-47.5 Re had been machined at Kin-Tech (North Huntington, PA). Actual machining of the other specimen types had not been initiated. Flowcharts 1-3 detail the major processing steps each piece of material has experienced. A more detailed description of processing will be provided in a separate document [B-MT(SRME)-51]. Table 1 lists the in-process materials and finished specimens. Also included are current metallurgical condition of these materials and specimens. The available chemical analyses for these alloys at various points in the process are provided in Table 2.

  9. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Underground Nuclear Tests - 2010

    SciTech Connect (OSTI)

    Pawloski, G A

    2011-01-03T23:59:59.000Z

    This report evaluates collapse evolution for selected Lawrence Livermore National Laboratory (LLNL) underground nuclear tests at the Nevada National Security Site (NNSS, formerly called the Nevada Test Site). The work is being done at the request of Navarro-Interra LLC, and supports environmental restoration efforts by the Department of Energy, National Nuclear Security Administration for the Nevada Site Office. Safety decisions must be made before a surface crater area, or potential surface crater area, can be reentered for any work. Our statements on cavity collapse and surface crater formation are input into their safety decisions. These statements do not include the effects of erosion that may modify the surface collapse craters over time. They also do not address possible radiation dangers that may be present. Subject matter experts from the LLNL Containment Program who had been active in weapons testing activities performed these evaluations. Information used included drilling and hole construction, emplacement and stemming, timing and sequence of the selected test and nearby tests, geology, yield, depth of burial, collapse times, surface crater sizes, cavity and crater volume estimations, and ground motion. Both classified and unclassified data were reviewed. Various amounts of information are available for these tests, depending on their age and other associated activities. Lack of data can hamper evaluations and introduce uncertainty. We make no attempt to quantify this uncertainty.

  10. Testing, Modeling, and Monitoring to Enable Simpler, Cheaper, Longer-Lived Surface Caps

    SciTech Connect (OSTI)

    Piet, Steven James; Breckenridge, Robert Paul; Burns, Douglas Edward

    2003-02-01T23:59:59.000Z

    Society has and will continue to generate hazardous wastes whose risks must be managed. For exceptionally toxic, long-lived, and feared waste, the solution is deep burial, e.g., deep geological disposal at Yucca Mtn. For some waste, recycle or destruction/treatment is possible. The alternative for other wastes is storage at or near the ground level (in someone’s back yard); most of these storage sites include a surface barrier (cap) to prevent downward water migration. Some of the hazards will persist indefinitely. As society and regulators have demanded additional proof that caps are robust against more threats and for longer time periods, the caps have become increasingly complex and expensive. As in other industries, increased complexity will eventually increase the difficulty in estimating performance, in monitoring system/component performance, and in repairing or upgrading barriers as risks are managed. An approach leading to simpler, less expensive, longer-lived, more manageable caps is needed. Our project, which started in April 2002, aims to catalyze a Barrier Improvement Cycle (iterative learning and application) and thus enable Remediation System Performance Management (doing the right maintenance neither too early nor too late). The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions, improve barrier management, and enable improved solutions for future decisions. We believe it will be possible to develop simpler, longer-lived, less expensive caps that are easier to monitor, manage, and repair. The project is planned to: a) improve the knowledge of degradation mechanisms in times shorter than service life; b) improve modeling of barrier degradation dynamics; c) develop sensor systems to identify early degradation; and d) provide a better basis for developing and testing of new barrier systems. This project combines selected exploratory studies (benchtop and field scale), coupled effects accelerated aging testing at the intermediate meso-scale, testing of new monitoring concepts, and modeling of dynamic systems. The emphasis on meso-scale (coupled) tests, accelerated effects testing, and dynamic modeling differentiates the project from other efforts, while simultaneously building on that body of knowledge. The performance of evapotranspiration, capillary, and grout-based barriers is being examined. To date, the project can report new approaches to the problem, building new experimental and modeling capabilities, and a few preliminary results.

  11. Testing, Modeling, and Monitoring to Enable Simpler, Cheaper, Longer-lived Surface Caps

    SciTech Connect (OSTI)

    Piet, S. J.; Breckenridge, R. P.; Burns, D. E.

    2003-02-25T23:59:59.000Z

    Society has and will continue to generate hazardous wastes whose risks must be managed. For exceptionally toxic, long-lived, and feared waste, the solution is deep burial, e.g., deep geological disposal at Yucca Mtn. For some waste, recycle or destruction/treatment is possible. The alternative for other wastes is storage at or near the ground level (in someone's back yard); most of these storage sites include a surface barrier (cap) to prevent downward water migration. Some of the hazards will persist indefinitely. As society and regulators have demanded additional proof that caps are robust against more threats and for longer time periods, the caps have become increasingly complex and expensive. As in other industries, increased complexity will eventually increase the difficulty in estimating performance, in monitoring system/component performance, and in repairing or upgrading barriers as risks are managed. An approach leading to simpler, less expensive, longer-lived, more manageable caps is needed. Our project, which started in April 2002, aims to catalyze a Barrier Improvement Cycle (iterative learning and application) and thus enable Remediation System Performance Management (doing the right maintenance neither too early nor too late). The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions, improve barrier management, and enable improved solutions for future decisions. We believe it will be possible to develop simpler, longer-lived, less expensive caps that are easier to monitor, manage, and repair. The project is planned to: (a) improve the knowledge of degradation mechanisms in times shorter than service life; (b) improve modeling of barrier degradation dynamics; (c) develop sensor systems to identify early degradation; and (d) provide a better basis for developing and testing of new barrier systems. This project combines selected exploratory studies (benchtop and field scale), coupled effects accelerated aging testing at the intermediate meso-scale, testing of new monitoring concepts, and modeling of dynamic systems. The emphasis on meso-scale (coupled) tests, accelerated effects testing, and dynamic modeling differentiates the project from other efforts, while simultaneously building on that body of knowledge. The performance of evapotranspiration, capillary, and grout-based barriers is being examined. To date, the project can report new approaches to the problem, building new experimental and modeling capabilities, and a few preliminary results.

  12. Corrective Action Decision Document for Corrective Action Unit 417: Central Nevada Test Area Surface, Nevada

    SciTech Connect (OSTI)

    U.S. Department of Energy Nevada Operations Office

    1999-04-02T23:59:59.000Z

    This Corrective Action Decision Document (CADD) identifies and rationalizes the U.S. Department of Energy, Nevada Operations Office's selection of a recommended corrective action alternative (CAA) appropriate to facilitate the closure of Corrective Action Unit (CAU) 417: Central Nevada Test Area Surface, Nevada, under the Federal Facility Agreement and Consent Order. Located in Hot Creek Valley in Nye County, Nevada, and consisting of three separate land withdrawal areas (UC-1, UC-3, and UC-4), CAU 417 is comprised of 34 corrective action sites (CASs) including 2 underground storage tanks, 5 septic systems, 8 shaker pad/cuttings disposal areas, 1 decontamination facility pit, 1 burn area, 1 scrap/trash dump, 1 outlier area, 8 housekeeping sites, and 16 mud pits. Four field events were conducted between September 1996 and June 1998 to complete a corrective action investigation indicating that the only contaminant of concern was total petroleum hydrocarbon (TPH) which was found in 18 of the CASs. A total of 1,028 samples were analyzed. During this investigation, a statistical approach was used to determine which depth intervals or layers inside individual mud pits and shaker pad areas were above the State action levels for the TPH. Other related field sampling activities (i.e., expedited site characterization methods, surface geophysical surveys, direct-push geophysical surveys, direct-push soil sampling, and rotosonic drilling located septic leachfields) were conducted in this four-phase investigation; however, no further contaminants of concern (COCs) were identified. During and after the investigation activities, several of the sites which had surface debris but no COCs were cleaned up as housekeeping sites, two septic tanks were closed in place, and two underground storage tanks were removed. The focus of this CADD was to identify CAAs which would promote the prevention or mitigation of human exposure to surface and subsurface soils with contaminant concentrations above preliminary action levels. Based on the potential exposure pathways, several risk-based CAAs were developed and evaluated against the individual CAS requirements. It was determined that a combination of the CAAs would be recommended to meet all applicable state and federal regulations for closure of these sites and to eliminate potential future exposure pathways to the TPH-contaminated soils.

  13. X-ray holography of biological specimens

    SciTech Connect (OSTI)

    Solem, J.C.

    1984-01-01T23:59:59.000Z

    The author reviews the reasons for x-ray imaging of biological specimens and the techniques presently being used for x-ray microscopy. The author points out the advantages of x-ray holography and the difficulties of obtaining the requisite coherence with conventional sources. The author discusses the problems of radiation damage and the remarkable fact that short pulse x-ray sources circumvent these problems and obtain high-resolution images of specimens in the living state. Finally, the author reviews some of the efforts underway to develop high-intensity coherent x-ray sources for the laboratory. 14 references, 5 figures, 2 tables.

  14. Fatigue Crack Propagation from Notched Specimens of 304 SS in elevated Temperature Aqueous Environment

    SciTech Connect (OSTI)

    Wire, G. L.; Mills, W. J.

    2002-08-01T23:59:59.000Z

    Fatigue crack propagation (FCP) rates for 304 stainless steel (304SS) were determined in 24 degree C and 288 degree C air and 288 degree C water using double-edged notch (DEN) specimens of 304 stainless steel (304 SS). Test performed at matched loading conditions in air and water at 288 degree C with 20-6- cc h[sub]2/kg h[sub]2O provided a direct comparison of the relative crack growth rates in air and water over a wide range of crack growth rates. The DEN crack extension ranged from short cracks (0.03-0.25 mm) to long cracks up to 4.06 mm, which are consistent with conventional deep crack tests. Crack growth rates of 304 SS in water were about 12 times the air rate. This 12X environmental enhancement persisted to crack extensions up to 4.06 mm, far outside the range associated with short crack effects. The large environmental degradation for 304 SS crack growth is consistent with the strong reduction of fatigue life in high hydrogen water. Further, very similar environmental effects w ere reported in fatigue crack growth tests in hydrogen water chemistry (HWC). Most literature data in high hydrogen water show only a mild environmental effect for 304 SS, of order 2.5 times air or less, but the tests were predominantly performed at high cyclic stress intensity or equivalently, high air rates. The environmental effect in low oxygen environments at low stress intensity depends strongly on both the stress ratio, R, and the load rise time, T[sub]r, as recently reported for austenitic stainless steel in BWR water. Fractography was performed for both tests in air and water. At 288 degree C in water, the fracture surfaces were crisply faceted with a crystallographic appearance, and showed striations under high magnification. The cleavage-like facets on the fracture surfaces suggest that hydrogen embrittlement is the primary cause of accelerated cracking.

  15. The evaluation of micro-surfacing mixture design procedures and the effects of material variation on the test responses

    E-Print Network [OSTI]

    Andrews, Edward Mensah

    1994-01-01T23:59:59.000Z

    the potential of the fore-mentioned ISSA test methods for assessing mixture design adequacy. As previously mentioned the ISSA Technical Design Guidelines (JAN 1991) form the basis of the tests to be performed. The procedures and apparatus needed and used... as materials are varied is reiterated. Suggestions for further research needed are made. ISSA MIXTURE DESIGN PROCEDURES General The International Slurry Surfacing Association design technical bulletin (Jan 1991) (5) contains guidelines for the laboratory...

  16. NGNP Graphite Testing and Qualification Specimen Selection Strategy

    SciTech Connect (OSTI)

    Robert Bratton

    2005-05-01T23:59:59.000Z

    The available grades of graphite for the NGNP are reviewed. A selection matrix is presented outlining the available grades for the NGNP graphite irradiation program based upon input from potential NGNP vendors, graphite manufactures, and graphite experts.

  17. A Search for Channel Deformation in Irradiated Vanadium Tensile Specimens

    SciTech Connect (OSTI)

    Gelles, David S.; Toloczko, Mychailo B.; Kurtz, Richard J.

    2010-02-26T23:59:59.000Z

    A miniature tensile specimen of V-4Cr-4Ti which had be irradiated in the 17J test at 425°C to 3.7 dpa was mechanically polished, deformed to 3.9% strain at room temperature, and examined by scanning and transmission electron microscopy in order to look for evidence of channel deformation. It was found that uniform deformation can occur without channel deformation, but evidence for channeling was found with channels appearing most prominently after the onset of necking. The channeling occurs on wavy planes with large variations in localized deformation from channel to channel.

  18. The development of a skill achievement test for beginning skiers on an artificial surface

    E-Print Network [OSTI]

    Gregory, William Bres

    1977-01-01T23:59:59.000Z

    of the Test Battery . . . . . . . . . . . . Test Validation . Establishment of Norms for the Final Test Battery Summary 57 58 59 63 63 70 74 75 V SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS Summary Conclusions Recommendations REFERENCES... members of the beginning ski classes at Texas A&B University. These subjects were tested with a 16-item test battery which had been consol1dated from a composite of suggestions from selected expert sk1ers at Texas A&V University. This method...

  19. Motorized manipulator for positioning a TEM specimen

    DOE Patents [OSTI]

    Schmid, Andreas Karl (Berkeley, CA); Andresen, Nord (Berkeley, CA)

    2010-12-14T23:59:59.000Z

    The invention relates to a motorized manipulator for positioning a TEM specimen holder with sub-micron resolution parallel to a y-z plane and rotating the specimen holder in the y-z plane, the manipulator comprising a base (2), and attachment means (30) for attaching the specimen holder to the manipulator, characterized in that the manipulator further comprises at least three nano-actuators (3.sup.a, 3.sup.b, 3.sup.c) mounted on the base, each nano-actuator showing a tip (4.sup.a, 4.sup.b, 4.sup.c), the at least three tips defining the y-z plane, each tip capable of moving with respect to the base in the y-z plane; a platform (5) in contact with the tips of the nano-actuators; and clamping means (6) for pressing the platform against the tips of the nano-actuators; as a result of which the nano-actuators can rotate the platform with respect to the base in the y-z plane and translate the platform parallel to the y-z plane.

  20. Treatability test plan for the 200-BP-1 prototype surface barrier

    SciTech Connect (OSTI)

    Not Available

    1993-06-01T23:59:59.000Z

    The US Department of Energy (DOE), Hanford Site, in Washington State is organized into numerically designated operational areas including the 100, 200, 300, 400, 600, and 1100 Areas. The US Environmental Protection Agency (EPA), in November of 1989, included the 200 Areas of the Hanford Site on the National Priority List (NPL) under the Comprehensive Environmental Response, compensation, and Liability Act of 1980 (CERCLA). The 200 Area is divided into operable units based on waste disposal information, location, facility, type, and other characteristics. The 200-BP-1 operable unit is one specific site located within the 200 East Area. Inclusion on the NPL initiated the remedial investigation (RI) process for characterizing the nature and extent of contamination and assessing risks to human health and the environment at the 200-BP-1 operable unit. In March of 1990, a remedial investigation/feasibility study (RI/FS) work plan for the 200-BP-1 operable unit was issued (DOE-RL 1990a). The work plan outlined the first phase of site characterization activities, which were completed in March of 1993 with the issuance of Phase I Remedial Investigation Report for the 200-BP-1 Operable Unit (DOE-RL 1993, Draft A). Remedial action objectives outlined in the RI report suggest that a likely remedial action at the 200-BP-1 operable unit could involve the use of a surface barrier. To further evaluate this technology, additional performance and constructability data are needed to implement this remedial action. This test plan describes the general methodology for conducting a prototype barrier treatability study. The objectives of this treatability study are to determine overall performance and constructability data on an actual waste site in conjunction with the Hanford Site Barrier Development Program.

  1. Inverse modeling of surface emissions for local pollution: A new methodology applied to academic test cases

    E-Print Network [OSTI]

    Menut, Laurent

    Inverse modeling of surface emissions for local pollution: A new methodology applied to academic; (2) LISA Creteil France Needs: Optimize surface emissions using daily recorded ozone and NOX by PRIMEQUAL2, program of the french ministry of environment Firstguess emissions inventory for the Paris

  2. Influence of specimen design on the deformation and failure of zircaloy cladding

    SciTech Connect (OSTI)

    Bates, D. W.; Koss, D. A.; Motta, A. T.; Majumdar S.

    2000-02-17T23:59:59.000Z

    Experimental as well as computational analyses have been used to examine the deformation and failure behavior of ring-stretch specimens of Zircaloy-4 cladding tubes. The results show that, at least for plastically anisotropic unirradiated cladding, specimens with a small gauge length l to width w ratio (l/w {approx} 1) exhibit pronounced non-uniform deformation along their length. As a result, specimen necking occurs upon yielding when the specimen is fully plastic. Finite element analysis indicates a minimum l/w of 4 before a significant fraction of the gauge length deforms homogeneously. A brief examination of the contrasting deformation and failure behavior between uniaxial and plane-strain ring tension tests further supports the use of the latter geometry for determining cladding failure ductility data that are relevant to certain reactivity-initiated accident conditions.

  3. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Underground Nuclear Tests - 2011, Part 2

    SciTech Connect (OSTI)

    Pawloski, G A

    2012-01-30T23:59:59.000Z

    This report evaluates collapse evolution for selected Lawrence Livermore National Laboratory (LLNL) underground nuclear tests at the Nevada National Security Site (NNSS, formerly called the Nevada Test Site). The work is being done to support several different programs that desire access to the ground surface above expended underground nuclear tests. The programs include: the Borehole Management Program, the Environmental Restoration Program, and the National Center for Nuclear Security Gas-Migration Experiment. Safety decisions must be made before a crater area, or potential crater area, can be reentered for any work. Evaluation of cavity collapse and crater formation is input into the safety decisions. Subject matter experts from the LLNL Containment Program who participated in weapons testing activities perform these evaluations. Information used included drilling and hole construction, emplacement and stemming, timing and sequence of the selected test and nearby tests, geology, yield, depth of burial, collapse times, surface crater sizes, cavity and crater volume estimations, ground motion, and radiological release information. Both classified and unclassified data were reviewed. The evaluations do not include the effects of erosion that may modify the collapse craters over time. They also do not address possible radiation dangers that may be present. Various amounts of information are available for these tests, depending on their age and other associated activities. Lack of data can hamper evaluations and introduce uncertainty. We make no attempt to quantify this uncertainty. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Underground Nuclear Tests - 2011 was published on March 2, 2011. This report, considered Part 2 of work undertaken in calendar year 2011, compiles evaluations requested after the March report. The following unclassified summary statements describe collapse evolution and crater stability in response to a recent request to review 6 LLNL test locations in Yucca Flat, Rainier Mesa, and Pahute Mesa. They include: Baneberry in U8d; Clearwater in U12q; Wineskin in U12r, Buteo in U20a and Duryea in nearby U20a1; and Barnwell in U20az.

  4. A three-dimensional surface waveocean circulation coupled model and its initial testing

    E-Print Network [OSTI]

    Ezer,Tal

    models is established based on Reynolds stresses and fluxes terms derived from surface wave to 0.93 with wave influence. The wave-induced Reynolds stress can reach up to about 5% of the wind stress in high latitudes, and drive 2­3 Sv transport in the global ocean in the form of mesoscale eddies

  5. Apparatus and method for magnetically processing a specimen

    DOE Patents [OSTI]

    Ludtka, Gerard M; Ludtka, Gail M; Wilgen, John B; Kisner, Roger A; Jaramillo, Roger A

    2013-09-03T23:59:59.000Z

    An apparatus for magnetically processing a specimen that couples high field strength magnetic fields with the magnetocaloric effect includes a high field strength magnet capable of generating a magnetic field of at least 1 Tesla and a magnetocaloric insert disposed within a bore of the high field strength magnet. A method for magnetically processing a specimen includes positioning a specimen adjacent to a magnetocaloric insert within a bore of a magnet and applying a high field strength magnetic field of at least 1 Tesla to the specimen and to the magnetocaloric insert. The temperature of the specimen changes during the application of the high field strength magnetic field due to the magnetocaloric effect.

  6. $?$--PhotoZ: Photometric Redshifts by Inverting the Tolman Surface Brightness Test

    E-Print Network [OSTI]

    Michael J. Kurtz; Margaret J. Geller; Daniel G. Fabricant; William F. Wyatt; Ian P. Dell'Antonio

    2007-07-03T23:59:59.000Z

    Surface brightness is a fundamental observational parameter of galaxies. We show, for the first time in detail, how it can be used to obtain photometric redshifts for galaxies, the $\\mu$-PhotoZ method. We demonstrate that the Tolman surface brightness relation, $\\mu \\propto (1+z)^{-4}$, is a powerful tool for determining galaxy redshifts from photometric data. We develop a model using $\\mu$ and a color percentile (ranking) measure to demonstrate the $\\mu$-PhotoZ method. We apply our method to a set of galaxies from the SHELS survey, and demonstrate that the photometric redshift accuracy achieved using the surface brightness method alone is comparable with the best color-based methods. We show that the $\\mu$-PhotoZ method is very effective in determining the redshift for red galaxies using only two photometric bands. We discuss the properties of the small, skewed, non-gaussian component of the error distribution. We calibrate $\\mu_r, (r-i)$ from the SDSS to redshift, and tabulate the result, providing a simple, but accurate look up table to estimate the redshift of distant red galaxies.

  7. Friction factor data for flat plate tests of smooth and honeycomb surfaces

    E-Print Network [OSTI]

    Ha, Tae Woong

    1989-01-01T23:59:59.000Z

    are needed. The purpose of this report is to present the air flow friction factor data for honeycomb surfaces (i.e., 1.57 mm, 0.79 mm and 0.51 mm in cell width, 3.81 mm and 2.29 mm in cell depth) with a flat plate tester. The flat plate tester is designed....2bar, and 17.9bar, respectively and 3 clearances between honeycombs which are 0.25mm, 0.38mm and 0.51mm. These clearance values are representative of actual seals used in the turbomachinary. The following questions wil l be answered: 1) Does...

  8. The development of scratch test methodology and characterization of surface damage of polypropylene

    E-Print Network [OSTI]

    Wong, Min Hao

    2004-11-15T23:59:59.000Z

    of products has brought attention to the ability of the polymers to withstand damages during service life. Electronics components, such as notebook casings and compact discs, to automotive parts, such as car interior instrument panels and console modules... and coatings industry because of their simplicity. A more systematic method that is popular among automotive?related companies is the Ford five-finger test. This method employs stainless steel styli to scratch TPOs that are mainly used in the interior of a...

  9. On the modeling of the Taylor cylinder impact test for orthotropic textured materials: Calculations and experiments

    SciTech Connect (OSTI)

    Maudlin, P.J.; Bingert, J.F.; House, J.W.

    1997-04-01T23:59:59.000Z

    Taylor impact tests using specimens cut from a rolled plate of Ta were conducted. The Ta was well-characterized in terms of flow stress and crystallographic texture. A piece-wise yield surface was interrogated from this orthotropic texture, and used in EPIC-95 3D simulations of the Taylor test. Good agreement was realized between the calculations and the post-test geometries in terms of major and minor side profiles and impact-interface footprints.

  10. Calibration of the modulation transfer function of surface profilometers with binary pseudo-random test standards: expanding the application range

    SciTech Connect (OSTI)

    Yashchuk, Valeriy V.; Anderson, Erik H.; Barber, Samuel K.; Bouet, Nathalie; Cambie, Rossana; Conley, Raymond; McKinney, Wayne R.; Takacs, Peter Z.; Voronov, Dmitriy L.

    2011-03-14T23:59:59.000Z

    A modulation transfer function (MTF) calibration method based on binary pseudo-random (BPR) gratings and arrays [Proc. SPIE 7077-7 (2007), Opt. Eng. 47, 073602 (2008)] has been proven to be an effective MTF calibration method for a number of interferometric microscopes and a scatterometer [Nucl. Instr. and Meth. A616, 172 (2010)]. Here we report on a further expansion of the application range of the method. We describe the MTF calibration of a 6 inch phase shifting Fizeau interferometer. Beyond providing a direct measurement of the interferometer's MTF, tests with a BPR array surface have revealed an asymmetry in the instrument's data processing algorithm that fundamentally limits its bandwidth. Moreover, the tests have illustrated the effects of the instrument's detrending and filtering procedures on power spectral density measurements. The details of the development of a BPR test sample suitable for calibration of scanning and transmission electron microscopes are also presented. Such a test sample is realized as a multilayer structure with the layer thicknesses of two materials corresponding to BPR sequence. The investigations confirm the universal character of the method that makes it applicable to a large variety of metrology instrumentation with spatial wavelength bandwidths from a few nanometers to hundreds of millimeters.

  11. Midtemperature Solar Systems Test Facility predictions for thermal performance based on test data. Alpha Solarco Model 104 solar collector with 0. 125-inch Schott low-iron glass reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-04-01T23:59:59.000Z

    Thermal performance predictions based on test data are presented for the Alpha Solarco Model 104 solar collector, with 0.125-inch Schott low-iron glass reflector surface, for three output temperatures at five cities in the United States.

  12. Flow Components in a NaK Test Loop Designed to Simulate Conditions in a Nuclear Surface Power Reactor

    SciTech Connect (OSTI)

    Polzin, Kurt A.; Godfroy, Thomas J. [NASA Marshall Space Flight Center Propulsion Research and Technology Applications Branch/ER24, MSFC, AL 35812 (United States)

    2008-01-21T23:59:59.000Z

    A test loop using NaK as the working fluid is presently in use to study material compatibility effects on various components that comprise a possible nuclear reactor design for use on the lunar surface. A DC electromagnetic (EM) pump has been designed and implemented as a means of actively controlling the NaK flow rate through the system and an EM flow sensor is employed to monitor the developed flow rate. These components allow for the matching of the flow rate conditions in test loops with those that would be found in a full-scale surface-power reactor. The design and operating characteristics of the EM pump and flow sensor are presented. In the EM pump, current is applied to a set of electrodes to produce a Lorentz body force in the fluid. A measurement of the induced voltage (back-EMF) in the flow sensor provides the means of monitoring flow rate. Both components are compact, employing high magnetic field strength neodymium magnets thermally coupled to a water-cooled housing. A vacuum gap limits the heat transferred from the high temperature NaK tube to the magnets and a magnetically-permeable material completes the magnetic circuit. The pump is designed to produce a pressure rise of 34.5 kPa, and the flow sensor's predicted output is roughly 20 mV at the loop's nominal flow rate of 0.114 m{sup 3}/hr.

  13. Soil surface stabilization using an in situ plutonium coating techniuqe at the Nevada Test Site

    SciTech Connect (OSTI)

    Lew, J.; Snipes, R. [Environmental Management and Enrichment Facilities, Oak Ridge, TN (United States); Tamura, T.

    1996-12-31T23:59:59.000Z

    The Hazardous Waste Remedial Actions Program (HAZWRAP), in collaboration with the University of Nevada at Reno (UNR), has developed and is investigating an in situ plutonium treatment for soils at the Nevada Test Site (NTS). The concept, conceived by Dr. T. Tamura and refined at HAZWRAP, was developed during the Nevada Applied Ecology Program investigation. In analyzing for plutonium in soils, it was noted that the alpha emanation of plutonium was greatly attenuated if traces of iron or manganese oxides were present in the final electroplating stage. The technique would reduce resuspension of alpha particles into the air by coating the contaminants in soils in situ with an environmentally compatible, durable, and nontoxic material. The coating materials (calcium hydroxide, ferrous sulfate) reduce resuspension by providing a cementitious barrier against radiation penetration while retaining soil porosity. This technique not only stabilizes plutonium-contaminated soils, but also provides an additional protection from worker exposure to radiation during remediation activities. Additionally, the coating would decrease the water solubility of the contaminant and, thus, reduce its migration through soil and uptake by plants.

  14. Corrective Action Plan for Corrective Action Unit 417: Central Nevada Test Area Surface, Nevada

    SciTech Connect (OSTI)

    K. Campbell

    2000-04-01T23:59:59.000Z

    This Corrective Action Plan provides methods for implementing the approved corrective action alternative as provided in the Corrective Action Decision Document for the Central Nevada Test Area (CNTA), Corrective Action Unit (CAU) 417 (DOE/NV, 1999). The CNTA is located in the Hot Creek Valley in Nye County, Nevada, approximately 137 kilometers (85 miles) northeast of Tonopah, Nevada. The CNTA consists of three separate land withdrawal areas commonly referred to as UC-1, UC-3, and UC-4, all of which are accessible to the public. CAU 417 consists of 34 Corrective Action Sites (CASs). Results of the investigation activities completed in 1998 are presented in Appendix D of the Corrective Action Decision Document (DOE/NV, 1999). According to the results, the only Constituent of Concern at the CNTA is total petroleum hydrocarbons (TPH). Of the 34 CASs, corrective action was proposed for 16 sites in 13 CASs. In fiscal year 1999, a Phase I Work Plan was prepared for the construction of a cover on the UC-4 Mud Pit C to gather information on cover constructibility and to perform site management activities. With Nevada Division of Environmental Protection concurrence, the Phase I field activities began in August 1999. A multi-layered cover using a Geosynthetic Clay Liner as an infiltration barrier was constructed over the UC-4 Mud Pit. Some TPH impacted material was relocated, concrete monuments were installed at nine sites, signs warning of site conditions were posted at seven sites, and subsidence markers were installed on the UC-4 Mud Pit C cover. Results from the field activities indicated that the UC-4 Mud Pit C cover design was constructable and could be used at the UC-1 Central Mud Pit (CMP). However, because of the size of the UC-1 CMP this design would be extremely costly. An alternative cover design, a vegetated cover, is proposed for the UC-1 CMP.

  15. Comparison of the results of short-term static tests and single-pass flow-through tests with LRM glass.

    SciTech Connect (OSTI)

    Ebert, W. L.; Chemical Engineering

    2007-01-29T23:59:59.000Z

    Static dissolution tests were conducted to measure the forward dissolution rate of LRM glass at 70 C and pH(RT) 11.7 {+-} 0.1 for comparison with the rate measured with single-pass flow-through (SPFT) tests in an interlaboratory study (ILS). The static tests were conducted with monolithic specimens having known geometric surface areas, whereas the SPFT tests were conducted with crushed glass that had an uncertain specific surface area. The error in the specific surface area of the crushed glass used in the SPFT tests, which was calculated by modeling the particles as spheres, was assessed based on the difference in the forward dissolution rates measured with the two test methods. Three series of static tests were conducted at 70 C following ASTM standard test method C1220 using specimens with surfaces polished to 600, 800, and 1200 grit and a leachant solution having the same composition as that used in the ILS. Regression of the combined results of the static tests to the affinity-based glass dissolution model gives a forward rate of 1.67 g/(m{sup 2}d). The mean value of the forward rate from the SPFT tests was 1.64 g/(m{sup 2}d) with an extended uncertainty of 1.90 g/(m{sup 2}d). This indicates that the calculated surface area for the crushed glass used in the SPFT tests is less than 2% higher than the actual surface area, which is well within the experimental uncertainties of measuring the forward dissolution rate using each test method. These results indicate that the geometric surface area of crushed glass calculated based on the size of the sieves used to isolate the fraction used in a test is reliable. In addition, the C1220 test method provides a means for measuring the forward dissolution rate of borosilicate glasses that is faster, easier, and more economical than the SPFT test method.

  16. The Hubble Wide Field Camera 3 Test of Surfaces in the Outer Solar System: Spectral Variation on Kuiper Belt Objects

    E-Print Network [OSTI]

    Fraser, Wesley C; Glass, Florian

    2015-01-01T23:59:59.000Z

    Here we present additional photometry of targets observed as part of the Hubble Wide Field Camera 3 Test of Surfaces in the Outer Solar System. 12 targets were re-observed with the Wide Field Camera 3 in optical and NIR wavebands designed to compliment those used during the first visit. Additionally, all observations originally presented by Fraser and Brown (2012) were reanalyzed through the same updated photometry pipeline. A reanalysis of the optical and NIR colour distribution reveals a bifurcated optical colour distribution and only two identifiable spectral classes, each of which occupies a broad range of colours and have correlated optical and NIR colours, in agreement with our previous findings. We report the detection of significant spectral variations on 5 targets which cannot be attributed to photometry errors, cosmic rays, point spread function or sensitivity variations, or other image artifacts capable of explaining the magnitude of the variation. The spectrally variable objects are found to have ...

  17. Resonance test system

    DOE Patents [OSTI]

    Musial, Walter (Boulder, CO); White, Darris (Superior, CO)

    2011-05-31T23:59:59.000Z

    An apparatus (10) for applying at least one load to a specimen (12) according to one embodiment of the invention may comprise a mass (18). An actuator (20) mounted to the specimen (12) and operatively associated with the mass (18) moves the mass (18) along a linear displacement path (22) that is perpendicular to a longitudinal axis of the specimen (12). A control system (26) operatively associated with the actuator (20) operates the actuator (20) to reciprocate the mass (18) along the linear displacement path (22) at a reciprocating frequency, the reciprocating frequency being about equal to a resonance frequency of the specimen (12) in a test configuration.

  18. Calibration of the modulation transfer function of surface profilometers with binary pseudo-random test standards: Expanding the application range

    E-Print Network [OSTI]

    Yashchuk, Valeriy V

    2010-01-01T23:59:59.000Z

    Grating Standard for Calibration of Surface Profilometers,"Gratings and Arrays for Calibration of Surface ProfileGratings and Arrays for Calibration of Modulation Transfer

  19. Calibration of the modulation transfer function of surface profilometers with binary pseudo-random test standards: expanding the application range

    E-Print Network [OSTI]

    Yashchuk, Valeriy V.

    2011-01-01T23:59:59.000Z

    Grating Standard for Calibration of Surface Profilometers,"Gratings and Arrays for Calibration of Surface ProfileGratings and Arrays for Calibration of Modulation Transfer

  20. Fabrication of specimens with controlled flaws for procedure development and personnel training and qualification

    SciTech Connect (OSTI)

    Edwards, R.L.; Watson, P.D.; Gruber, G.J. [Southwest Research Inst., San Antonio, TX (United States)

    1994-12-31T23:59:59.000Z

    Over the years, instances of service-induced flaws in vessel and piping components have prompted many utilities to acquire full-scale mockups to demonstrate the performance of nondestructive evaluation (NDE) procedures. Also, the newly invoked Appendix 8 requirement to the 1989 Section 11 ASME Code requires qualification of equipment, procedures, and personnel utilizing full-scale test specimens with actual flaws. This has increased the need for flaws that can be produced and accurately controlled in various test specimens. The typical service-induced flaws may consist of one of the following, depending on the material type and service conditions: mechanical fatigue; thermal fatigue; intergranular stress-corrosion (IGSC) cracking; and weld-induced flaws (during manufacture) such as slag, porosity, or incomplete fusion.

  1. University of Connecticut Daily Temperature Log Specimen Refrigerator Log

    E-Print Network [OSTI]

    Oliver, Douglas L.

    University of Connecticut Daily Temperature Log ­ Specimen Refrigerator Log Month / Year Clinical ___ Fac. Mgmt. Resolution: 31 ___ Fac. Mgmt. Resolution: If the refrigerator temperature falls out refrigerator. This record must be kept for one year and then destroyed per State requirement

  2. Ultra high vacuum heating and rotating specimen stage

    DOE Patents [OSTI]

    Coombs, A.W. III

    1995-05-02T23:59:59.000Z

    A heating and rotating specimen stage provides for simultaneous specimen heating and rotating. The stage is ideally suited for operation in ultrahigh vacuum (1{times}10{sup {minus}9} torr or less), but is useful at atmosphere and in pressurized systems as well. A specimen is placed on a specimen holder that is attached to a heater that, in turn, is attached to a top housing. The top housing is rotated relative to a bottom housing and electrically connected thereto by electrically conductive brushes. This stage is made of materials that are compatible with UHV, able to withstand high temperatures, possess low outgassing rates, are gall and seize resistant, and are able to carry substantial electrical loading without overheating. 5 figs.

  3. Ultra high vacuum heating and rotating specimen stage

    DOE Patents [OSTI]

    Coombs, III, Arthur W. (Patterson, CA)

    1995-01-01T23:59:59.000Z

    A heating and rotating specimen stage provides for simultaneous specimen heating and rotating. The stage is ideally suited for operation in ultrahigh vacuum (1.times.10.sup.-9 torr or less), but is useful at atmosphere and in pressurized systems as well. A specimen is placed on a specimen holder that is attached to a heater that, in turn, is attached to a top housing. The top housing is rotated relative to a bottom housing and electrically connected thereto by electrically conductive brushes. This stage is made of materials that are compatible with UHV, able to withstand high temperatures, possess low outgassing rates, are gall and seize resistant, and are able to carry substantial electrical loading without overheating.

  4. Experimental deformation of multilithologic specimens simulating sedimentary facies changes 

    E-Print Network [OSTI]

    Dyke, Lawrence Dana

    1976-01-01T23:59:59.000Z

    EXPERIMENTAL DEFORMATION OF MULTILITHOLOGIC SPECIMENS SIMULATING SEDIMENTARY FACIES CHANGES A Thesis by LAWRENCE DANA DYKE Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirement for the degree... of MASTER OF SCIENCE December 1976 Major Subject: Geology EXPERIMENTAL DEFORMATION OF MULTILITHOLOGIC SPECIMENS SIMULATING SEDIMENTARY FACIES CHANGES A Thesis by LAWRENCE DANA DYKE Approved as to style and content by: (Chai n Committee) (Head...

  5. Experimental deformation of multilithologic specimens simulating sedimentary facies changes

    E-Print Network [OSTI]

    Dyke, Lawrence Dana

    1976-01-01T23:59:59.000Z

    EXPERIMENTAL DEFORMATION OF MULTILITHOLOGIC SPECIMENS SIMULATING SEDIMENTARY FACIES CHANGES A Thesis by LAWRENCE DANA DYKE Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirement for the degree... of MASTER OF SCIENCE December 1976 Major Subject: Geology EXPERIMENTAL DEFORMATION OF MULTILITHOLOGIC SPECIMENS SIMULATING SEDIMENTARY FACIES CHANGES A Thesis by LAWRENCE DANA DYKE Approved as to style and content by: (Chai n Committee) (Head...

  6. Notch reorientation of Charpy-V specimens of the BWR Philippsburg 1 through reconstitution

    SciTech Connect (OSTI)

    Walle, E. van; Fabry, A.; Ransbeeck, T. van; Puzzolante, J.L.; Velde, J. van de [SCK-CEN, Mol (Belgium); Tulke, K. [Kernkraftwerk Philippsburg Gmbh (Germany). Div. Nuclear Technology; Backfisch, W. [TUV Suedwest e.V., Mannheim (Germany). Div. Nuclear Technology and Radiation Protection

    1996-12-31T23:59:59.000Z

    10 x 10 x 10 mm cubes, made from broken halves of un-irradiated and irradiated L-T oriented Charpy-V surveillance specimens of the Boiling Water Reactor (BWR) Philippsburg 1, were reconstituted to L-T and T-L oriented Charpy-V bars using the stud-gun welding technique of the Belgian Nuclear Research Centre SCK-CEN. Instrumented Charpy-V (C{sub V}) impact testing, according to the European Standard EN10045, was performed in order to determine the T-L transition curves of the reconstituted surveillance material. Losses of fracture energy and lateral expansion, mainly as a consequence of constraint of plastic flow due to the reconstitution welds, were detected. No change in shear fracture appearance was observed. The transition curves of the tested T-L reconstituted specimens represent conservative lower bounds that fulfill the C{sub V} upper shelf energy requirements of the Regulator. A correction curve allows estimation of the T-L transition curves of non-reconstituted T-L specimens.

  7. Investigation of temperature dependence of fracture toughness in high-dose HT9 steel using small-specimen reuse technique

    SciTech Connect (OSTI)

    Baek, Jong-Hyuk [KAERI] [KAERI; Byun, Thak Sang [ORNL] [ORNL; Maloy, S [Los Alamos National Laboratory (LANL)] [Los Alamos National Laboratory (LANL); Toloczko, M [Pacific Northwest National Laboratory (PNNL)] [Pacific Northwest National Laboratory (PNNL)

    2014-01-01T23:59:59.000Z

    The temperature dependence of fracture toughness in HT9 steel irradiated to 3 145 dpa at 380 503 C was investigated using miniature three-point bend (TPB) fracture specimens. A miniature-specimen reuse technique has been established: the tested halves of subsize Charpy impact specimens with dimensions of 27 mm 3mm 4 mm were reused for this fracture test campaign by cutting a notch with a diamond-saw in the middle of each half, and by fatigue-precracking to generate a sharp crack tip. It was confirmed that the fracture toughness of HT9 steel in the dose range depends more strongly on the irradiation temperature than the irradiation dose. At an irradiation temperature <430 C, the fracture toughness of irradiated HT9 increased with the test temperature, reached an upper shelf of 180 200 MPa ffiffiffiffiffi m p at 350 450 C, and then decreased with the test temperature. At an irradiation temperatureP430 C, the fracture toughness was nearly unchanged up to about 450 C and decreased slowly with test temperatures in a higher temperature range. Such a rather monotonic test temperature dependence after high-temperature irradiation is similar to that observed for an archive material generally showing a higher degree of toughness. A brittle fracture without stable crack growth occurred in only a few specimens with relatively lower irradiation and test temperatures. In this discussion, these TPB fracture toughness data are compared with previously published data from 12.7 mm diameter disc compact tension (DCT) specimens.

  8. Investigation of temperature dependence of fracture toughness in high-dose HT9 steel using small-specimen reuse technique

    SciTech Connect (OSTI)

    Baek, Jong-Hyuk; Byun, Thak Sang; Maloy, Stuart A.; Toloczko, Mychailo B.

    2014-01-01T23:59:59.000Z

    The temperature dependence of fracture toughness in HT9 steel irradiated to 3–145 dpa at 380–503 degrees*C was investigated using miniature three-point bend (TPB) fracture specimens. A miniature-specimen reuse technique has been established: the tested halves of subsize Charpy impact specimens with dimensions of 27 mm *3mm* 4 mm were reused for this fracture test campaign by cutting a notch with a diamond-saw in the middle of each half, and by fatigue-precracking to generate a sharp crack tip. It was confirmed that the fracture toughness of HT9 steel in the dose range depends more strongly on the irradiation temperature than the irradiation dose. At an irradiation temperature <430 *degreesC, the fracture toughness of irradiated HT9 increased with the test temperature, reached an upper shelf of 180—200 MPa*m^.5 at 350–450 degrees*C, and then decreased with the test temperature. At an irradiation temperature >430 degrees*C, the fracture toughness was nearly unchanged up to about 450 *degreesC and decreased slowly with test temperatures in a higher temperature range. Such a rather monotonic test temperature dependence after high-temperature irradiation is similar to that observed for an archive material generally showing a higher degree of toughness. A brittle fracture without stable crack growth occurred in only a few specimens with relatively lower irradiation and test temperatures. In this discussion, these TPB fracture toughness data are compared with previously published data from 12.7 mm diameter disc compact tension (DCT) specimens.

  9. WAFER TEST CAVITY -Linking Surface Microstructure to RF Performance: a ‘Short-­?Sample Test Facility’ for characterizing superconducting materials for SRF cavities.

    SciTech Connect (OSTI)

    Pogue, Nathaniel; Comeaux, Justin; McIntyre, Peter

    2014-05-30T23:59:59.000Z

    The Wafer Test cavity was designed to create a short sample test system to determine the properties of the superconducting materials and S?I?S hetero?structures. The project, funded by ARRA, was successful in accomplishing several goals to achieving a high gradient test system for SRF research and development. The project led to the design and construction of the two unique cavities that each severed unique purposes: the Wafer test Cavity and the Sapphire Test cavity. The Sapphire Cavity was constructed first to determine the properties of large single crystal sapphires in an SRF environment. The data obtained from the cavity greatly altered the design of the Wafer Cavity and provided the necessary information to ascertain the Wafer Test cavity’s performance.

  10. Measurement of surface tension and viscosity by open capillary techniques

    DOE Patents [OSTI]

    Rye,Robert R. (Albuquerque, NM), Yost,Frederick G. (Cedar Crest, NM)

    1998-01-01T23:59:59.000Z

    An open-channel capillary is provided, having preferably a v-shaped groove in a flat wettable surface. The groove has timing marks and a source marker in which the specimen to be tested is deposited. The time of passage between the timing marks is recorded, and the ratio of surface tension .gamma. to viscosity .mu. is determined from the equation given below: ##EQU1## where h.sub.0 is the groove depth, .alpha. is the groove angle, .theta. is the liquid/solid contact angle, and t is the flow time. It has been shown by the

  11. RESULTS OF THE EXAMINATION OF ELECTROCHEMICAL NOISE PROBE SPECIMENS REMOVED FROM TANK 241-AN-107 JUNE 2010

    SciTech Connect (OSTI)

    COOKE GA; WYRWAS RB; DUNCAN JB

    2010-11-11T23:59:59.000Z

    An Integrated Multi-function Corrosion Probe (IMCP) was installed in Tank 241-AN-107 on September 20, 2006. A portion of the probe was retrieved on June 8, 2010 and the sections holding the detectors were delivered to the 222-S Laboratory for analysis. The examination and disassembly of the probe sections encountered a number of challenges. However, disassembly and relevant analyses were successfully completed. The following summarizes our observations. Brittle failure of the fiberglass probe in the middle of detector 2 resulted in the recovery of only three vapor space C-rings and six supernatant bullet specimens. The design of the bullets and how they were attached to the probe made the recovery of the components more difficult. The use of glue/epoxy on the bullets and the attachment of the flat bottom of the bullets to the curved surface of the fiberglass probe body meant that weight loss on cleaning and surface area of the specimens could not be determined with acceptable accuracy. Macrophotography of all specimens reveals that corrosion was slight in the vapor space and extremely slight in the supernatant. The one pre-cracked C-ring recovered from the vapor space still had the stress bulge visible on the polished surface, indicating that crack propagation had not occurred in the tank. No photographs were taken of the C-ring before deployment. No further analysis was conducted on this specimen. A detailed discussion and photographic documentation are provided in this report.

  12. Midtemperature solar systems test facility predictions for thermal performance of the Acurex solar collector with FEK 244 reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-01-01T23:59:59.000Z

    Thermal performance predictions are presented for the Acurex solar collector, with FEK 244 reflector surface, for three output temperatures at five cities in the United States.

  13. Fractographic examination of reduced activation ferritic/martensitic steel charpy specimens irradiated to 30 dpa at 370{degrees}C

    SciTech Connect (OSTI)

    Gelles, D.S.; Hamilton, M.L. [Pacific Northwest National Lab., Richland, WA (United States); Schubert, L.E. [Univ. of Missouri, Rolla, MO (United States)

    1996-10-01T23:59:59.000Z

    Fractographic examinations are reported for a series of reduced activation ferritic/Martensitic steel Charpy impact specimens tested following irradiation to 30 dpa at 370{degrees}C in FFTF. One-third size specimens of six low activation steels developed for potential application as structural materials in fusion reactors were examined. A shift in brittle fracture appearance from cleavage to grain boundary failure was noted with increasing manganese content. The results are interpreted in light of transmutation induced composition changes in a fusion environment.

  14. Effects of extreme pressure additive chemistry on rolling element bearing surface durability

    SciTech Connect (OSTI)

    Evans, Ryan D. [Timken Company; Nixon, H. P. [Timken Company; Darragh, Craig V. [Timken Company; Howe, Jane Y [ORNL; Coffey, Dorothy W [ORNL

    2007-01-01T23:59:59.000Z

    Lubricant additives have been known to affect rolling element bearing surface durability for many years. Tapered roller bearings were used in fatigue testing of lubricants formulated with gear oil type additive systems. These systems have sulfur- and phosphoruscontaining compounds used for gear protection as well as bearing lubrication. Several variations of a commercially available base additive formulation were tested having modified sulfur components. The variations represent a range of ''active'' extreme pressure (EP) chemistries. The bearing fatigue test results were compared with respect to EP formulation and test conditions. Inner ring near-surface material in selected test bearings was evaluated on two scales: the micrometer scale using optical metallography and the nanometer scale using transmission electron microscopy (TEM). Focused-ion beam (FIB) techniques were used for TEM specimen preparation. Imaging and chemical analysis of the bearing samples revealed near-surface material and tribofilm characteristics. These results are discussed with respect to the relative fatigue lives.

  15. Use of laser extensometer for mechanical test on irradiated materials

    SciTech Connect (OSTI)

    Brillaud, C.; Meylogan, T.; Salathe, P. [Electricite de France, Avoine (France)

    1996-12-31T23:59:59.000Z

    Techniques have been developed by EDF`s hot laboratory in Chinon for performing mechanical tests on irradiated materials. Some of these techniques aim to facilitate strain measurements, which are particularly difficult to perform on irradiated specimens at high temperatures or on subsize specimens. Recent progress has been driven by laser technology combined with software development. The use of this technique, which allows strain measurements without contact on the specimen, is described for tensile (especially on subsize specimens), fatigue and creep tests.

  16. Infrared Temperature Sensing of Mechanically Loaded Specimens: Thermal Analysis

    E-Print Network [OSTI]

    Rabin, Yoed

    , not the instantaneous effect of heating within a single loading cycle. KEY WORDS--Infrared, temperature measurement, meInfrared Temperature Sensing of Mechanically Loaded Specimens: Thermal Analysis by Y. Rabin and D. Rittel ABSTRACT--Infrared temperature-sensing techniques have the major advantages of virtually

  17. Computer Science Specimen Curriculum City University Hong Kong, China

    E-Print Network [OSTI]

    Simaan, Nabil

    Computer Science Specimen Curriculum City University Hong Kong, China Spring Semester Junior Year Communications 3 CS 3103 (CS 281) Operating Systems Principles 3 CS 250 Algorithms 3 CS DEPTH Computer Science Depth 6 CS 270 Programming Languages 3 LAC Liberal Arts Core 3 CS DEPTH Computer Science Depth 3 15 LAC

  18. Computer Science Specimen Curriculum City University Hong Kong, China

    E-Print Network [OSTI]

    Simaan, Nabil

    Computer Science Specimen Curriculum City University Hong Kong, China Fall Semester Junior Year) Algorithms 3 CS 281 Operating System Principles 3 OPEN ELEC Open Elective 3 CS PROJ Computer Science Project 3 CS DEPTH Computer Science Depth 3 CS DEPTH Computer Science Depth 3 LAC Liberal Arts Core 3 LAC

  19. Computer Science Specimen Curriculum National University of Singapore

    E-Print Network [OSTI]

    Simaan, Nabil

    Computer Science Specimen Curriculum National University of Singapore Fall Semester Junior Year Science Project 3 CS DEPTH Computer Science Depth 3 CS DEPTH Computer Science Depth 3 LAC Liberal Arts MATH ELEC Math Elective 3 CS DEPTH Computer Science Depth 6 CS DEPTH Computer Science Depth 6 OPEN ELEC

  20. Apparatus for testing for infection by a retrovirus

    DOE Patents [OSTI]

    Layne, Scott P. (Los Angeles, CA); Beugelsdijk, Tony J. (Los Alamos, NM)

    1999-01-01T23:59:59.000Z

    An apparatus for testing specimens for infection by a retrovirus is described. The apparatus comprises a process controller including a communications module for translating user commands into test instrument suite commands and a means for communicating specimen test results to a user. The apparatus further comprises a test instrument suite including a means for treating the specimen to manifest an observable result and a detector for measuring the observable result.

  1. ?A cylindrical specimen holder for electron cryo-tomography

    E-Print Network [OSTI]

    Palmer, Colin Michael

    2013-03-12T23:59:59.000Z

    . . . . . . . . . . . . . . . . . . . . . . . . . 57 3.6 Characterisation of carbon nanopipettes . . . . . . . . . . . . . . . . 59 3.7 Discussion of the manufacturing process . . . . . . . . . . . . . . . . 63 4 Cryo-tomography 67 4.1 Specimen preparation I... . . . . . . . . . . . . . . . . . 60 3.7 Elemental maps and longitudinal EDX linescan of a carbon nanopipette 61 3.8 Transverse EDX linescan of a carbon nanopipette . . . . . . . . . . . 62 4.1 Transmission electron micrograph of a blocked carbon nanopipette tip 68 4.2 A carbon...

  2. Critical heat flux test apparatus

    DOE Patents [OSTI]

    Welsh, Robert E. (West Mifflin, PA); Doman, Marvin J. (McKeesport, PA); Wilson, Edward C. (West Mifflin, PA)

    1992-01-01T23:59:59.000Z

    An apparatus for testing, in situ, highly irradiated specimens at high temperature transients is provided. A specimen, which has a thermocouple device attached thereto, is manipulated into test position in a sealed quartz heating tube by a robot. An induction coil around a heating portion of the tube is powered by a radio frequency generator to heat the specimen. Sensors are connected to monitor the temperatures of the specimen and the induction coil. A quench chamber is located below the heating portion to permit rapid cooling of the specimen which is moved into this quench chamber once it is heated to a critical temperature. A vacuum pump is connected to the apparatus to collect any released fission gases which are analyzed at a remote location.

  3. Combined UHV/high-pressure catalysis setup for depth-resolved near-surface spectroscopic characterization and catalytic testing of model catalysts

    SciTech Connect (OSTI)

    Mayr, Lukas; Klötzer, Bernhard; Penner, Simon [Institute of Physical Chemistry, University of Innsbruck, Innrain 52a, 6020 Innsbruck (Austria)] [Institute of Physical Chemistry, University of Innsbruck, Innrain 52a, 6020 Innsbruck (Austria); Rameshan, Raffael [Institute of Physical Chemistry, University of Innsbruck, Innrain 52a, 6020 Innsbruck (Austria) [Institute of Physical Chemistry, University of Innsbruck, Innrain 52a, 6020 Innsbruck (Austria); Department of Inorganic Chemistry, Fritz Haber Institute of the Max Planck Society, Faradayweg 4-6, 14195 Berlin (Germany); Rameshan, Christoph [Institute of Physical Chemistry, University of Innsbruck, Innrain 52a, 6020 Innsbruck (Austria) [Institute of Physical Chemistry, University of Innsbruck, Innrain 52a, 6020 Innsbruck (Austria); Institute of Materials Chemistry, Vienna University of Technology, Getreidemarkt 9/BC/01, 1060 Vienna (Austria)

    2014-05-15T23:59:59.000Z

    An ultra-high vacuum (UHV) setup for “real” and “inverse” model catalyst preparation, depth-resolved near-surface spectroscopic characterization, and quantification of catalytic activity and selectivity under technologically relevant conditions is described. Due to the all-quartz reactor attached directly to the UHV-chamber, transfer of the catalyst for in situ testing without intermediate contact to the ambient is possible. The design of the UHV-compatible re-circulating batch reactor setup allows the study of reaction kinetics under close to technically relevant catalytic conditions up to 1273 K without contact to metallic surfaces except those of the catalyst itself. With the attached differentially pumped exchangeable evaporators and the quartz-microbalance thickness monitoring equipment, a reproducible, versatile, and standardised sample preparation is possible. For three-dimensional near-surface sample characterization, the system is equipped with a hemispherical analyser for X-ray photoelectron spectroscopy (XPS), electron-beam or X-ray-excited Auger-electron spectroscopy, and low-energy ion scattering measurements. Due the dedicated geometry of the X-ray gun (54.7°, “magic angle”) and the rotatable sample holder, depth analysis by angle-resolved XPS measurements can be performed. Thus, by the combination of characterisation methods with different information depths, a detailed three-dimensional picture of the electronic and geometric structure of the model catalyst can be obtained. To demonstrate the capability of the described system, comparative results for depth-resolved sample characterization and catalytic testing in methanol steam reforming on PdGa and PdZn near-surface intermetallic phases are shown.

  4. A compact and versatile microfluidic probe for local processing of tissue sections and biological specimens

    E-Print Network [OSTI]

    Cors, J F; Delamarche, E; Kaigala, G V

    2014-01-01T23:59:59.000Z

    The microfluidic probe (MFP) is a non-contact, scanning microfluidic technology for local (bio)chemical processing of surfaces based on hydrodynamically confining nanoliter volumes of liquids over tens of micrometers. We present here a compact MFP (cMFP) that can be used on a standard inverted microscope and assist in the local processing of tissue sections and biological specimens. The cMFP has a footprint of 175 X 100 X 140 mm^3 and can scan an area of 45 X 45 mm^2 on a surface with an accuracy of +-15 um. The cMFP is compatible with standard surfaces used in life science laboratories such as microscope slides and Petri dishes. For ease of use, we developed self-aligned mounted MFP heads with standardized chip-to-world and chip-to-platform interfaces. Switching the processing liquid in the flow confinement is performed within 90 seconds using a selector valve with a dead-volume of approximately 5 uL. We further implemented height-compensation that allows a cMFP head to follow non-planar surfaces common in t...

  5. Corrective Action Investigation Plan for Corrective Action Unit 556: Dry Wells and Surface Release Points Nevada Test Site, Nevada (Draft), Revision 0

    SciTech Connect (OSTI)

    Grant Evenson

    2007-02-01T23:59:59.000Z

    Corrective Action Unit  (CAU) 556, Dry Wells and Surface Release Points, is located in Areas 6 and 25 of the Nevada Test Site, 65 miles northwest of Las Vegas, Nevada. Corrective Action Unit 556 is comprised of four corrective action sites (CASs) listed below: •06-20-04, National Cementers Dry Well •06-99-09, Birdwell Test Hole •25-60-03, E-MAD Stormwater Discharge and Piping •25-64-01, Vehicle Washdown and Drainage Pit These sites are being investigated because existing information on the nature and extent of potential contamination is insufficient to evaluate and recommend corrective action alternatives. Additional information will be obtained by conducting a corrective action investigation before evaluating corrective action alternatives and selecting the appropriate corrective action for each CAS. The results of the field investigation will support a defensible evaluation of viable corrective action alternatives that will be presented in the Corrective Action Decision Document.

  6. New specimens of Propotamochoerus (Suidae, Mammalia) from the late Miocene of the Balkans

    E-Print Network [OSTI]

    Boyer, Edmond

    New specimens of Propotamochoerus (Suidae, Mammalia) from the late Miocene of the Balkans Denis. hysudricus or P. hyotherioides. It is likely that these Balkan specimens belong to a species of their own

  7. Development of Advanced Surface Enhancement Technology for Decreasing Wear and Corrosion of Equipment Used for Mineral Processing

    SciTech Connect (OSTI)

    Daniel Tao; R. Honaker; B. K. Parekh

    2007-09-20T23:59:59.000Z

    Equipment wear is a major concern in the mineral processing industry, which dramatically increases the maintenance cost and adversely affects plant operation efficiency. In this research, novel surface treatment technologies, High Density Infrared (HDI) and Laser Surface Engineering (LSE) surface coating processes were developed for the surface enhancement of selected mineral and coal processing equipment. Microstructural and mechanical properties of the coated specimens were characterized. Laboratory-simulated wear tests were conducted to evaluate the tribological performance of the coated components. Test results indicate that the wear resistance of ASTM A36 (raw coal screen section) and can be significantly increased by applying HDI and LSE coating processes. Field testing has been performed using a LSE-treated screen panel and it showed a significant improvement of the service life.

  8. Influence of specimen design on the ductility of zircaloy cladding: Experiment and analysis

    SciTech Connect (OSTI)

    Bates, D. W.; Majumdar, S.; Koss, D. A.; Motta, A. T.

    1999-11-12T23:59:59.000Z

    In a reactivity-initiated accident (RIA), a control rod ejection or drop causes a sudden increase in reactor power, which in turn deposits a large amount of energy into the fuel. The resulting thermal expansion and fission gas release loads the cladding into the plastic regime and may cause it to fail. In order to predict cladding survivability, there has been considerable interest and effort in supplementing integral WA tests with separate-effects ring tests of cladding tubes. Such tests can give one insight into failure mechanisms and measure relevant mechanical properties (such as yield strength, uniform elongation, uniaxial stress-strain curve, etc.), for use in computer codes that attempt to predict cladding response during an RIA. The accuracy of such model predictions obviously depends on appropriate and accurate failure data. This study concerns itself with the proper development of ring tensile tests that (i) are similar to the loading conditions present in an RIA, (ii) measure the relevant mechanical properties and (iii) provide insight regarding the influence of the strain paths on the failure mechanisms present if Zircaloy cladding. Based on both experiments and computational modeling, the authors investigate the failure of Zircaloy tubing as a function of specimen geometry, and discuss the limitations of certain ring-test geometries in yielding failure ductility data that are applicable to RIA situations.

  9. Analysis, comparison, and modeling of radar interferometry, date of surface deformation signals associated with underground explosions, mine collapses and earthquakes. Phase I: underground explosions, Nevada Test Site

    SciTech Connect (OSTI)

    Foxall, W; Vincent, P; Walter, W

    1999-07-23T23:59:59.000Z

    We have previously presented simple elastic deformation modeling results for three classes of seismic events of concern in monitoring the CTBT--underground explosions, mine collapses and earthquakes. Those results explored the theoretical detectability of each event type using synthetic aperture radar interferometry (InSAR) based on commercially available satellite data. In those studies we identified and compared the characteristics of synthetic interferograms that distinguish each event type, as well the ability of the interferograms to constrain source parameters. These idealized modeling results, together with preliminary analysis of InSAR data for the 1995 mb 5.2 Solvay mine collapse in southwestern Wyoming, suggested that InSAR data used in conjunction with regional seismic monitoring holds great potential for CTBT discrimination and seismic source analysis, as well as providing accurate ground truth parameters for regional calibration events. In this paper we further examine the detectability and ''discriminating'' power of InSAR by presenting results from InSAR data processing, analysis and modeling of the surface deformation signals associated with underground explosions. Specifically, we present results of a detailed study of coseismic and postseismic surface deformation signals associated with underground nuclear and chemical explosion tests at the Nevada Test Site (NTS). Several interferograms were formed from raw ERS-1/2 radar data covering different time spans and epochs beginning just prior to the last U.S. nuclear tests in 1992 and ending in 1996. These interferograms have yielded information about the nature and duration of the source processes that produced the surface deformations associated with these events. A critical result of this study is that significant post-event surface deformation associated with underground nuclear explosions detonated at depths in excess of 600 meters can be detected using differential radar interferometry. An immediate implication of this finding is that underground nuclear explosions may not need to be captured coseismically by radar images acquired before and after an event in order to be detectable. This has obvious advantages in CTBT monitoring since suspect seismic events--which usually can be located within a 100 km by 100 km area of an ERS-1/2 satellite frame by established seismic methods-can be imaged after the event has been identified and located by existing regional seismic networks. Key Words: InSAR, SLC images, interferogram, synthetic interferogram, ERS-1/2 frame, phase unwrapping, DEM, coseismic, postseismic, source parameters.

  10. Corrective Action Investigation plan for Corrective Action Unit 546: Injection Well and Surface Releases, Nevada Test Site, Nevada, Revision 0

    SciTech Connect (OSTI)

    Alfred Wickline

    2008-03-01T23:59:59.000Z

    Corrective Action Unit (CAU) 546 is located in Areas 6 and 9 of the Nevada Test Site, which is approximately 65 miles northwest of Las Vegas, Nevada. Corrective Action Unit 546 is comprised of two Corrective Action Sites (CASs) listed below: •06-23-02, U-6a/Russet Testing Area •09-20-01, Injection Well These sites are being investigated because existing information on the nature and extent of potential contamination is insufficient to evaluate and recommend corrective action alternatives. Additional information will be obtained by conducting a corrective action investigation (CAI) before evaluating corrective action alternatives and selecting the appropriate corrective action for each CAS. The results of the field investigation will support a defensible evaluation of viable corrective action alternatives that will be presented in the Corrective Action Decision Document. The sites will be investigated based on the data quality objectives (DQOs) developed on November 8, 2007, by representatives of the Nevada Division of Environmental Protection and U.S. Department of Energy (DOE), National Nuclear Security Administration Nevada Site Office. The DQO process has been used to identify and define the type, amount, and quality of data needed to develop and evaluate appropriate corrective actions for CAU 546.

  11. Automation for Cryo-TEM: From Specimen Grid to 3D

    E-Print Network [OSTI]

    Automation for Cryo-TEM: From Specimen Grid to 3D Map B. Carragher, D. Fellmann, N. Kisseberth, R://www.itg.uiuc.edu #12;AUTOMATION FOR CRYO-TEM: FROM SPECIMEN GRID TO 3D MAP B. Carragher, D. Fellmann, N. Kisseberth, R map of a macromolecular structure automatically and within hours of inserting a specimen

  12. Specimen coordinate automated measuring machine/fiducial automated measuring machine

    DOE Patents [OSTI]

    Hedglen, Robert E. (Bethel Park, PA); Jacket, Howard S. (Pittsburgh, PA); Schwartz, Allan I. (Turtle Creek, PA)

    1991-01-01T23:59:59.000Z

    The Specimen coordinate Automated Measuring Machine (SCAMM) and the Fiducial Automated Measuring Machine (FAMM) is a computer controlled metrology system capable of measuring length, width, and thickness, and of locating fiducial marks. SCAMM and FAMM have many similarities in their designs, and they can be converted from one to the other without taking them out of the hot cell. Both have means for: supporting a plurality of samples and a standard; controlling the movement of the samples in the +/- X and Y directions; determining the coordinates of the sample; compensating for temperature effects; and verifying the accuracy of the measurements and repeating as necessary. SCAMM and FAMM are designed to be used in hot cells.

  13. Flow localization in sheet specimens with pairs of holes

    SciTech Connect (OSTI)

    Geltmacher, A.B. [FM Technologies, Fairfax, VA (United States); Koss, D.A. [Pennsylvania State Univ., University Park, PA (United States). Dept. of Metals Science and Engineering; Stout, M.G. [Los Alamos National Lab., NM (United States); Matic, P. [Naval Research Lab., Washington, DC (United States). Mechanics of Materials Dept.

    1998-03-01T23:59:59.000Z

    The deformation localization behavior of sheet specimens containing geometric perturbations in the form of pairs of through-thickness holes is examined. Both experiments and computational modeling are performed in either uniaxial or equal-biaxial tension in order to examine the effect of applied loading path on the far-field strain needed to initiate localized necking in the ligament between the hole pairs. The models also examine the influence of hole spacing and matrix strain hardening on ligament localization. The far-field strain needed to cause the localization of the ligament is shown to increase as the biaxiality of the loading path increases, the hole spacing increases, and the strain-hardening exponent increases. The present study also indicates that the onset of localized necking can be predicted by employing the Hill criterion, if the local strain states within the ligament are taken into account.

  14. NESC-VII: Fracture Mechanics Analyses of WPS Experiments on Large-scale Cruciform Specimen

    SciTech Connect (OSTI)

    Yin, Shengjun [ORNL; Williams, Paul T [ORNL; Bass, Bennett Richard [ORNL

    2011-01-01T23:59:59.000Z

    This paper describes numerical analyses performed to simulate warm pre-stress (WPS) experiments conducted with large-scale cruciform specimens within the Network for Evaluation of Structural Components (NESC-VII) project. NESC-VII is a European cooperative action in support of WPS application in reactor pressure vessel (RPV) integrity assessment. The project aims in evaluation of the influence of WPS when assessing the structural integrity of RPVs. Advanced fracture mechanics models will be developed and performed to validate experiments concerning the effect of different WPS scenarios on RPV components. The Oak Ridge National Laboratory (ORNL), USA contributes to the Work Package-2 (Analyses of WPS experiments) within the NESCVII network. A series of WPS type experiments on large-scale cruciform specimens have been conducted at CEA Saclay, France, within the framework of NESC VII project. This paper first describes NESC-VII feasibility test analyses conducted at ORNL. Very good agreement was achieved between AREVA NP SAS and ORNL. Further analyses were conducted to evaluate the NESC-VII WPS tests conducted under Load-Cool-Transient- Fracture (LCTF) and Load-Cool-Fracture (LCF) conditions. This objective of this work is to provide a definitive quantification of WPS effects when assessing the structural integrity of reactor pressure vessels. This information will be utilized to further validate, refine, and improve the WPS models that are being used in probabilistic fracture mechanics computer codes now in use by the NRC staff in their effort to develop risk-informed updates to Title 10 of the U.S. Code of Federal Regulations (CFR), Part 50, Appendix G.

  15. Apparatus for X-ray diffraction microscopy and tomography of cryo specimens

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Beetz, T.; Howells, M. R.; Jacobsen, C.; Kao, C. -C.; Kirz, J.; Lima, E.; Mentes, T. O.; Miao, H.; Sanchez-Hanke, C.; Sayre, D.; et al

    2005-06-01T23:59:59.000Z

    An apparatus for diffraction microscopy of biological and materials science specimens is described. In this system, a coherent soft X-ray beam is selected with a pinhole, and the illuminated specimen is followed by an adjustable beamstop and CCD camera to record diffraction data from non-crystalline specimens. In addition, a Fresnel zone plate can be inserted to allow for direct imaging. The system makes use of a cryogenic specimen holder with cryotransfer capabilities to allow frozen hydrated specimens to be loaded. The specimen can be tilted over a range of ± 80 ° degrees for three-dimensional imaging; this is done bymore »computer-controlled motors, enabling automated alignment of the specimen through a tilt series. The system is now in use for experiments in soft X-ray diffraction microscopy.« less

  16. Apparatus for X-ray diffraction microscopy and tomography of cryo specimens

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Beetz, T.; Howells, M.R.; Jacobsen, C.; Kao, C.-C.; Kirz, J.; Lima, E.; Mentes, T.O.; Miao, H.; Sanchez-Hanke, C.; Sayre, D.; Shapiro, D.

    2005-06-01T23:59:59.000Z

    An apparatus for diffraction microscopy of biological and materials science specimens is described. In this system, a coherent soft X-ray beam is selected with a pinhole, and the illuminated specimen is followed by an adjustable beamstop and CCD camera to record diffraction data from non-crystalline specimens. In addition, a Fresnel zone plate can be inserted to allow for direct imaging. The system makes use of a cryogenic specimen holder with cryotransfer capabilities to allow frozen hydrated specimens to be loaded. The specimen can be tilted over a range of +/- 80 degrees for three-dimensional imaging; this is done by computer-controlled motors, enabling automated alignment of the specimen through a tilt series. The system is now in use for experiments in soft X-ray diffraction microscopy.

  17. Apparatus for X-ray diffraction microscopy and tomography of cryo specimens

    SciTech Connect (OSTI)

    Beetz, T. [Stony Brook Univ., Stony Brook, NY (United States); Howells, M. R. [Brookhaven National Laboratory (BNL), Upton, NY (United States). National Synchrotron Light Source; Brookhaven National Laboratory (BNL), Upton, NY (United States). Center for Functional Nanomaterials; Jacobsen, C. [Stony Brook Univ., Stony Brook, NY (United States); Kao, C. -C. [Brookhaven National Laboratory (BNL), Upton, NY (United States). National Synchrotron Light Source; Kirz, J. [Stony Brook Univ., Stony Brook, NY (United States); Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States). Advanced Light Source; Lima, E. [Stony Brook Univ., Stony Brook, NY (United States); Mentes, T. O. [Stony Brook Univ., Stony Brook, NY (United States); TASC-INFM National Lab, Trieste (Italy); Miao, H. [Stony Brook Univ., Stony Brook, NY (United States); Sanchez-Hanke, C. [Brookhaven National Laboratory (BNL), Upton, NY (United States). National Synchrotron Light Source; Sayre, D. [Stony Brook Univ., Stony Brook, NY (United States); Shapiro, D. [Stony Brook Univ., Stony Brook, NY (United States)

    2005-06-01T23:59:59.000Z

    An apparatus for diffraction microscopy of biological and materials science specimens is described. In this system, a coherent soft X-ray beam is selected with a pinhole, and the illuminated specimen is followed by an adjustable beamstop and CCD camera to record diffraction data from non-crystalline specimens. In addition, a Fresnel zone plate can be inserted to allow for direct imaging. The system makes use of a cryogenic specimen holder with cryotransfer capabilities to allow frozen hydrated specimens to be loaded. The specimen can be tilted over a range of ± 80 ° degrees for three-dimensional imaging; this is done by computer-controlled motors, enabling automated alignment of the specimen through a tilt series. The system is now in use for experiments in soft X-ray diffraction microscopy.

  18. In-situ and thin-specimen aging of experimental polyisocyanurate roof insulation foamed with alternative blowing agents

    SciTech Connect (OSTI)

    Christian, J.E.; Courville, G.E.; Graves, R.S.; Linkous, R.L.; McElroy, D.L.; Weaver, F.J.; Yarbrough, D.W.

    1991-01-01T23:59:59.000Z

    This paper reports apparent thermal conductivity (k) values from field and laboratory aging tests on a set of industry-produced, experimental polyisocyanurate (PIR) laminated boardstock foamed with hydrochlorofluorocarbons (HCFCs) as alternatives to chlorofluorocarbon (CFC). The PIR boards were blown with five gases: CFC-11, HCFC-123, HCFC-14lb, and 50/50 and 65/35 blends of HCFC-123/HCFC-14lb. The k-values were determined from 0 to 50{degree}C (30 to 120{degree}F) using techniques that meet ASTM C 114 (Thin Heater Apparatus) and ASTM C 518 (Heat Flow Meter Apparatus). Results on laminate boards with facers provide an independent laboratory check on the increase in k observed for field exposure in the ORNL Roof Thermal Research Apparatus (RTRA). The observed laboratory increase in k was between 8% and 11% for a 240 day field exposure in the RTRA. A thin-specimen aging procedure established the long-term thermal resistance of gas-filled foams. Thin specimens were planed from the industry-produced boardstock foams and aged at 24 and 65{degree}C (75{degree}F and 150{degree}F) for up to 300 days. An exponential dependency of k with the quantity (diffusion coefficient X time){sup {1/2}}/ thickness, provide effective diffusion coefficients for air components into the foams and blowing agent out of the foams. The foams blown with alternative blowing agents exhibited k-values 3 to 16% (average 9.4%) above CFC-11 foams under similar conditions. Field exposures were conducted on specimens under single ply EPDM membranes in the RTRA for over 400 days. Hourly averages of panel temperature and heat flux were analyzed to obtain K as a function of mean temperature on a week by week basis. The relative performance of test specimens of HCFC-14B under a black and under a white membrane is reported. 29 refs., 10 figs., 10 tabs.

  19. Post-Closure Inspection and Monitoring Report for Corrective Action Unit 417: Central Nevada Test Area Surface, Hot Creek Valley, Nevada

    SciTech Connect (OSTI)

    None

    2009-10-01T23:59:59.000Z

    This report presents results of data collected during the annual post-closure site inspection conducted at the Central Nevada Test Area, surface Corrective Action Unit (CAU) 417 in June 2009. The annual post-closure site inspection included inspections of the UC-1, UC-3, and UC-4 sites in accordance with the Post-Closure Monitoring Plan provided in the CAU 417 Closure Report (NNSA/NV 2001). The annual inspection conducted at the UC-1 Central Mud Pit (CMP) indicated that the site and soil cover were in good condition. Three new fractures were identified in the soil cover and were filled with bentonite chips during the inspection. The vegetation on the soil cover was adequate but showed signs of the area's ongoing drought. No issues were identified with the CMP fence, gate, or subsidence monuments. No issues were identified with the warning signs and monuments at the other two UC-1 locations

  20. A comparison of the toughness of ductile iron to cast steel using modified charpy test specimens

    E-Print Network [OSTI]

    McKinney, Keith Elison

    1984-01-01T23:59:59.000Z

    transition temperature exhibited by cast steel was surprising since these materials had 48 CA + I th + 0 s V) Cg Z CA I I Ci 0 ID ID z I CL o o C 0 lA I Ql P 0 a E EU pQ 0 I- IA (U I ID IA I I CD ( UIIU/P) NAOU3 'UIJON 49 V...) ( + V) V) Z I CI CQ Vl ( ICI CD CD El O CI Cl CD ! + + 8 CD O LA IJ III ( CL PJ m CD IA ( I((i((yP) At(Je((3 . u(JON 50 Ch X I VJ I Z V ) + L In 8 I LIJ In + r L 0 CU 0 ~O N In I o In It WIIIyf'j /5aaug 'm&ON Z...

  1. CHARPY IMPACT TEST RESULTS ON FIVE MAERIALS AND NIST VERIFICATION SPECIMENS USING INSTRUMENTED

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office511041clothAdvanced Materials Advanced. C o w l i t z C o . C l a r k C o'IUHopper3 Environmental8,4,

  2. Corrective Action Decision Document/Closure Report for Corrective Action Unit 546: Injection Well and Surface Releases Nevada Test Site, Nevada, Revision 0

    SciTech Connect (OSTI)

    Alfred Wickline

    2008-12-01T23:59:59.000Z

    This Corrective Action Decision Document/Closure Report has been prepared for Corrective Action Unit 546, Injection Well and Surface Releases, at the Nevada Test Site, Nevada, in accordance with the Federal Facility Agreement and Consent Order (FFACO, 1996; as amended February 2008). Corrective Action Unit (CAU) 546 is comprised of two corrective action sites (CASs): • 06-23-02, U-6a/Russet Testing Area • 09-20-01, Injection Well The purpose of this Corrective Action Decision Document/Closure Report is to provide justification and documentation supporting the recommendation for closure of CAU 546. To achieve this, corrective action investigation (CAI) activities were performed from May 5 through May 28, 2008, as set forth in the Corrective Action Investigation Plan for Corrective Action Unit 546: Injection Well and Surface Releases, Nevada Test Site, Nevada (NNSA/NSO, 2008). The purpose of the CAI was to fulfill the following data needs as defined during the data quality objective (DQO) process: • Determine whether a contaminant of concern is present at a given CAS. • Determine whether sufficient information is available to evaluate potential corrective action alternatives at each CAS. The CAU 546 dataset from the investigation results was evaluated based on the data quality indicator parameters. This evaluation demonstrated the quality and acceptability of the dataset for use in fulfilling the DQO data needs. Because DQO data needs were met, and corrective actions have been implemented, it has been determined that no further corrective action (based on risk to human receptors) is necessary for the CAU 546 CASs. The U.S. Department of Energy, National Nuclear Security Administration Nevada Site Office provides the following recommendations: • No further corrective actions are needed for CAU 546 CASs. • No Corrective Action Plan is required. • A Notice of Completion to the U.S. Department of Energy, National Nuclear Security Administration Nevada Site Office is requested from the Nevada Division of Environmental Protection for closure of CAU 546. • Corrective Action Unit 546 should be moved from Appendix III to Appendix IV of the Federal Facility Agreement and Consent Order. Analytes detected during the CAI were evaluated against final action levels established in this document. No analytes were detected at concentrations exceeding final action levels. However, contaminants of concern were presumed to be present in the subsurface soil at CAS 09-20-01. Therefore, the corrective action of close in place was selected as the preferred alternative for this CAS. Potential source material was removed from CAS 06-23-02; therefore, the corrective action of clean closure was selected as the preferred alternative at this CAS.

  3. Microstructural and Mechanical Characterization of Actively Brazed Alumina Specimens

    SciTech Connect (OSTI)

    Hosking, F.M.; Cadden, C.H.; Stephens, J.J.; Glass, S.J.; Yang, N.Y.C.; Vianco, P.V.; Walker, C.A.

    1999-08-26T23:59:59.000Z

    Alumina (94 and 99.8% grade compositions) was brazed directly to itself with gold-based active brazing alloys (ABA's) containing vanadium additions of 1,2 and 3 weight percent. The effects of brazing conditions on the joint properties were investigated. Wetting behavior, interfacial reactions, microstructure, hermeticity and tensile strength were determined. Wetting was fair to good for the ABA and base material combinations. Microanalysis identified a discontinuous Al-V-O spinel reaction product at the alumina-braze interface. Tensile strength results for 94% alumina were uniformly good and generally not sensitive to the vanadium concentration, with tensile values of 85-105 MPa. There was more variability in the 99.8% alumina strength results, with values ranging from 25-95 MPa. The highest vanadium concentration (3 wt. %) yielded the highest joint strength for the brazed 99.8% alumina. Failures in the 99.8% alumina samples occurred at the braze-alumina interface, while the 94% alumina specimens exhibited fracture of the ceramic substrate.

  4. Standard test method for creep-fatigue testing

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2009-01-01T23:59:59.000Z

    1.1 This test method covers the determination of mechanical properties pertaining to creep-fatigue deformation or crack formation in nominally homogeneous materials, or both by the use of test specimens subjected to uniaxial forces under isothermal conditions. It concerns fatigue testing at strain rates or with cycles involving sufficiently long hold times to be responsible for the cyclic deformation response and cycles to crack formation to be affected by creep (and oxidation). It is intended as a test method for fatigue testing performed in support of such activities as materials research and development, mechanical design, process and quality control, product performance, and failure analysis. The cyclic conditions responsible for creep-fatigue deformation and cracking vary with material and with temperature for a given material. 1.2 The use of this test method is limited to specimens and does not cover testing of full-scale components, structures, or consumer products. 1.3 This test method is primarily ...

  5. Optical caliper with compensation for specimen deflection and method

    DOE Patents [OSTI]

    Bernacki, B.E.

    1997-12-09T23:59:59.000Z

    An optical non-contact profilometry system and method provided by an optical caliper with matched optical sensors that are arranged conjugate to each other so that the surface profile and thickness of an article can be measured without using a fixed reference surface and while permitting the article to deflect in space within the acquisition range of the optical sensors. The output signals from the two optical sensors are algebraically added to compensate for any such deflection of the article and provide a so compensated signal, the balance and sign of which provides a measurement of the actual thickness of the article at the optical sensors. 2 figs.

  6. Optical caliper with compensation for specimen deflection and method

    DOE Patents [OSTI]

    Bernacki, Bruce E. (Knoxville, TN)

    1997-01-01T23:59:59.000Z

    An optical non-contact profilometry system and method provided by an optical caliper with matched optical sensors that are arranged conjugate to each other so that the surface profile and thickness of an article can be measured without using a fixed reference surface and while permitting the article to deflect in space within the acquisition range of the optical sensors. The output signals from the two optical sensors are algebraically added to compensate for any such deflection of the article and provide a so compensated signal, the balance and sign of which provides a measurement of the actual thickness of the article at the optical sensors.

  7. Effect of conductivity between fasteners and aluminum skin on eddy current specimens

    SciTech Connect (OSTI)

    Moore, D.G. [Sandia National Labs., Albuquerque, NM (United States); Hutchinson, M.C. [Boeing Co., Seattle, WA (United States). Commercial Airplane Group

    1997-04-01T23:59:59.000Z

    The Federal Aviation Administration Airworthiness Assurance Nondestructive Inspection Validation Center (FAA-AANC) and Boeing Commercial Airplane Group are currently developing a study pertaining to the detection of cracks in multi-layered aluminum sheets. The specimen panels model pertinent aspects of the lap splice joints for Boeing 737 aircraft, Line Numbers 292 - 2565. Upon initial characterization of the specimen panels, it became clear that signals produced from a sliding probe at fastener sites were not representative of an in-service lap splice, and therefore, could not be used in a probability of detection experiment. This paper discusses specimen characterization and steps taken to make the specimens useful for nondestructive technology assessment.

  8. Measurements of elastic modulus using laser-induced surface waves

    SciTech Connect (OSTI)

    Chang, D.J.; Amimoto, S.T.; Gross, R.W.F. [Aerospace Corporation, Los Angeles, CA (United States); Glenn, T. [Massachusetts Institute of Technology, Cambridge, MA (United States)

    1995-12-31T23:59:59.000Z

    In general, the mechanical testing methods that are utilized for alloys and polymers, e.g., dogbone, rheovibron, etc., are not applicable to thin film structures. We wish to report noncontacting measurements of the surface acoustic wave (SAW) velocity and the elastic modulus applicable to thin films of moderate thickness. An accompanying paper extends this technique to smaller film dimensions. A 15 ns pulsed YAG laser was used as the energy source to thermoelastically excite surface waves. The propagation of the waves was then observed by a second, independent He-Ne laser at a distance from the excitation spot. using the knife edge/beam deflection technique. A cylindrical lens was used to reduce the energy loading of the YAG laser on the sample to avoid damaging the surface of the specimen. The Rayleigh wave velocity is calculated from measurements of the arrival time of the surface wave as a function of distance from the ND:YAG laser spot. The shear modulus, G, can be determined from the measured speed of the surface waves, V, the specimen density, p, and Poisson`s ratio, v, according to the following relationship: V = R(v){sm_bullet}(G/p){sup {1/2}} where R(v), expressed as (0.862 + 1.14v)/(l + v), is the ratio of the Rayleigh wave velocity to the shear wave velocity and ranges from 0.86 to 0.95 Table below lists the measured surface wave velocities and the calculated shear modulus for our experimental results and the published values. Excellent agreement is observed. The depth of the SAW is approximately equal to the SAW wavelength which is approximately the laser spot size. Typically 30 {mu}m spot sizes can be readily achieved. In conclusion, SAW velocities and the modulus of elasticity of various materials have been measured. We have demonstrated that this non-contacting method can be used to characterize moderately thin films.

  9. A versatile elevated-pressure reactor combined with an ultrahigh vacuum surface setup for efficient testing of model and powder catalysts under clean gas-phase conditions

    SciTech Connect (OSTI)

    Morfin, Franck; Piccolo, Laurent [Institut de recherches sur la catalyse et l'environnement de Lyon (IRCELYON), UMR 5256 CNRS and Université Lyon 1, 2 avenue Albert Einstein, F-69626 Villeurbanne (France)] [Institut de recherches sur la catalyse et l'environnement de Lyon (IRCELYON), UMR 5256 CNRS and Université Lyon 1, 2 avenue Albert Einstein, F-69626 Villeurbanne (France)

    2013-09-15T23:59:59.000Z

    A small-volume reaction cell for catalytic or photocatalytic testing of solid materials at pressures up to 1000 Torr has been coupled to a surface-science setup used for standard sample preparation and characterization under ultrahigh vacuum (UHV). The reactor and sample holder designs allow easy sample transfer from/to the UHV chamber, and investigation of both planar and small amounts of powder catalysts under the same conditions. The sample is heated with an infrared laser beam and its temperature is measured with a compact pyrometer. Combined in a regulation loop, this system ensures fast and accurate temperature control as well as clean heating. The reaction products are automatically sampled and analyzed by mass spectrometry and/or gas chromatography (GC). Unlike previous systems, our GC apparatus does not use a recirculation loop and allows working in clean conditions at pressures as low as 1 Torr while detecting partial pressures smaller than 10{sup ?4} Torr. The efficiency and versatility of the reactor are demonstrated in the study of two catalytic systems: butadiene hydrogenation on Pd(100) and CO oxidation over an AuRh/TiO{sub 2} powder catalyst.

  10. Design, Construction, and Initial Test of High Spatial Resolution Thermometry Arrays for Detection of Surface Temperature Profiles on SRF Cavities in Super Fluid Helium

    SciTech Connect (OSTI)

    Ari Palczewski, Rongli Geng, Grigory Eremeev

    2011-07-01T23:59:59.000Z

    We designed and built two high resolution (0.6-0.55mm special resolution [1.1-1.2mm separation]) thermometry arrays prototypes out of the Allen Bradley 90-120 ohm 1/8 watt resistor to measure surface temperature profiles on SRF cavities. One array was designed to be physically flexible and conform to any location on a SRF cavity; the other was modeled after the common G-10/stycast 2850 thermometer and designed to fit on the equator of an ILC (Tesla 1.3GHz) SRF cavity. We will discuss the advantages and disadvantages of each array and their construction. In addition we will present a case study of the arrays performance on a real SRF cavity TB9NR001. TB9NR001 presented a unique opportunity to test the performance of each array as it contained a dual (4mm separation) cat eye defect which conventional methods such as OST (Oscillating Superleak second-sound Transducers) and full coverage thermometry mapping were unable to distinguish between. We will discuss the new arrays ability to distinguish between the two defects and their preheating performance.

  11. Post-Closure Inspection and Monitoring Report for Corrective Action Unit 417: Central Nevada Test Area Surface, Hot Creek Valley, Nevada

    SciTech Connect (OSTI)

    None

    2013-03-01T23:59:59.000Z

    This report presents results of data collected during the annual post-closure site inspections conducted at the Central Nevada Test Area surface Corrective Action Unit (CAU) 417 in May 2011 and July 2012. The annual post-closure site inspections included inspections of the UC-1, UC-3, and UC-4 sites in accordance with the Post-Closure Monitoring Plan provided in the CAU 417 Closure Report (NNSA/NV 2001). The annual inspections conducted at the UC-1 Central Mud Pit (CMP) indicated that the site and soil cover were in good condition. No new fractures or extension of existing fractures were observed and no issues with the fence or gate were identified. The vegetation on the cover continues to look healthy, but the biennial vegetation survey conducted during the 2012 inspection indicated that the total foliar cover was slightly higher in 2009 than in 2012. This may be indicative of a decrease in precipitation observed during the 2-year monitoring period. The precipitation totaled 9.9 inches from July 1, 2010, through June 30, 2011, and 5 inches from July 1, 2011, through June 30, 2012. This decrease in precipitation is also evident in the soil moisture data obtained from the time domain reflectometry sensors. Soil moisture content data show that the UC-1 cover is performing as designed, and evapotranspiration is effectively removing water from the cover.

  12. POST CLOSURE INSPECTION AND MONITORING REPORT FOR CORRECTIVE ACTION UNIT 417: CENTRAL NEVADA TEST AREA - SURFACE, HOT CREEK VALLEY, NEVADA, FOR CALENDAR YEAR 2004

    SciTech Connect (OSTI)

    BECHTEL NEVADA; NNSA NEVADA SITE OFFICE

    2005-04-01T23:59:59.000Z

    This post-closure inspection and monitoring report has been prepared according to the stipulations laid out in the Closure Report (CR) for Corrective Action Unit (CAU) 417, Central Nevada Test Area (CNTA)--Surface (U.S. Department of Energy, National Nuclear Security Administration Nevada Operations Office [NNSA/NV], 2001), and the Federal Facility Agreement and Consent Order (FFACO, 1996). This report provides an analysis and summary of site inspections, subsidence surveys, meteorological information, and soil moisture monitoring data for CAU 417, which is located in Hot Creek Valley, Nye County, Nevada. This report covers Calendar Year 2004. Inspections at CAU 417 are conducted quarterly to document the physical condition of the UC-1, UC-3, and UC-4 soil covers, monuments, signs, fencing, and use restricted areas. The physical condition of fencing, monuments, and signs is noted, and any unusual conditions that could impact the integrity of the covers are reported. The objective of the soil moisture monitoring program is to monitor the stability of soil moisture conditions within the upper 1.2 meters (m) (4 feet [ft]) of the UC-1 Central Mud Pit (CMP) cover and detect changes that may be indicative of moisture movement exceeding the cover design performance expectations.

  13. Corrective Action Decision Document/ Closure Report for Corrective Action Unit 556: Dry Wells and Surface Release Points, Nevada Test Site, Nevada with Errata Sheet, Revision 0

    SciTech Connect (OSTI)

    Grant Evenson

    2008-09-01T23:59:59.000Z

    This Corrective Action Decision Document (CADD)/Closure Report (CR) has been prepared for Corrective Action Unit 556, Dry Wells and Surface Release Points, located at the Nevada Test Site, Nevada, in accordance with the Federal Facility Agreement and Consent Order (FFACO, 1996; as amended February 2008). Corrective Action Unit (CAU) 556 is comprised of four corrective action sites (CASs): • 06-20-04, National Cementers Dry Well • 06-99-09, Birdwell Test Hole • 25-60-03, E-MAD Stormwater Discharge and Piping • 25-64-01, Vehicle Washdown and Drainage Pit The purpose of this CADD/CR is to provide justification and documentation supporting the recommendation for closure of CAU 556 with no further corrective action. To achieve this, corrective action investigation (CAI) activities began on February 7 and were completed on June 19, 2008, as set forth in the Corrective Action Investigation Plan for Corrective Action Unit 556: Dry Wells and Surface Release Points, Nevada Test Site, Nevada (NNSA/NSO, 2007). The purpose of the CAI was to fulfill the following data needs as defined during the data quality objective (DQO) process: • Determine whether contaminants of concern (COCs) are present. • If COCs are present, determine their nature and extent. • Provide sufficient information and data to complete appropriate corrective actions. The CAU 556 data were evaluated based on the data quality assessment process, which demonstrated the quality and acceptability of the data for use in fulfilling the DQO data needs. Analytes detected during the CAI were evaluated against appropriate final action levels (FALs) to identify the COCs for each CAS. The results of the CAI identified COCs at one of the four CASs in CAU 556 that required the completion of a corrective action. Assessment of the data generated from investigation activities conducted at CAU 556 revealed the following: • Corrective Action Sites 06-20-04, 06-99-09, and 25-64-01 do not contain contamination at concentrations exceeding the FALs. • Polychlorinated biphenyl (PCB) contamination above the FAL was identified in the surface and/or shallow subsurface soils at the outfall and around Catch Basin 2, and in soils contained within the catch basins and the manhole at CAS 25-60-03. A corrective action of close in place with a soil removal action and use restriction (UR) was completed at CAS 25-60-03. The PCB-contaminated soils were removed from the outfall area and around Catch Basin 2, and disposed of at a Nevada Test Site landfill as part of a removal action. The catch basins and the manhole were sealed shut by filling them with grout. The end of the outfall pipe was plugged using grout, covered with soil, and the area was regraded. A UR was applied to the entire stormwater system at CAS 25-60-03, which includes the three catch basins, manhole, and associated piping. No further action is the corrective action for CASs 06-20-04, 06-99-09, and 25-64-01. The liquids in the test holes at CAS 06-99-09 were removed for disposal and the features were filled with grout as a best management practice. The drainage pipe between the vehicle washdown pad and the drainage pit at CAS 25-64-01 was sealed at each end as a best management practice. The corrective actions were evaluated on technical merit focusing on performance, reliability, feasibility, safety, and cost. They were judged to meet all requirements for the technical components evaluated. The corrective actions meet all applicable federal and state regulations for closure of the site and will reduce potential exposure pathways to the contaminated media to an acceptable level at CAU 556. Therefore, the U.S. Department of Energy, National Nuclear Security Administration Nevada Site Office provides the following recommendations: • Maintain a UR for the entire stormwater drainage system (i.e., three catch basins, one manhole, and associated piping) at CAS 25-60-03. • No further corrective action for CAU 556. • A Notice of Completion to the U.S. Department of Energy, National Nuclear Security Administration Nevada

  14. Non-destructive testing method and apparatus

    DOE Patents [OSTI]

    Akers, Douglas W. (Idaho Falls, ID)

    2011-10-04T23:59:59.000Z

    Non-destructive testing apparatus may comprise a photon source and a source material that emits positrons in response to bombardment of the source material with photons. The source material is positionable adjacent the photon source and a specimen so that when the source material is positioned adjacent the photon source it is exposed to photons produced thereby. When the source material is positioned adjacent the specimen, the specimen is exposed to at least some of the positrons emitted by the source material. A detector system positioned adjacent the specimen detects annihilation gamma rays emitted by the specimen. Another embodiment comprises a neutron source and a source material that emits positrons in response to neutron bombardment.

  15. Test Automation Test Automation

    E-Print Network [OSTI]

    Mousavi, Mohammad

    Test Automation Test Automation Mohammad Mousavi Eindhoven University of Technology, The Netherlands Software Testing 2013 Mousavi: Test Automation #12;Test Automation Outline Test Automation Mousavi: Test Automation #12;Test Automation Why? Challenges of Manual Testing Test-case design: Choosing inputs

  16. Post-Closure Inspection and Monitoring Report for Corrective Action Unit 417: Central Nevada Test Area Surface, Hot Creek Valley, Nevada For Calendar Year 2006

    SciTech Connect (OSTI)

    None

    2007-06-01T23:59:59.000Z

    Corrective Action Unit (CAU) 417, Central Nevada Test Area - Surface, is located in Hot Creek Valley in northern Nye County, Nevada, and consists of three areas commonly referred to as UC-1, UC-3, and UC-4. CAU 417 consists of 34 Corrective Action Sites (CASs) which were closed in 2000 (U.S. Department of Energy, National Nuclear Security Administration Nevada Operations Office, 2001). Three CASs at UC-1 were closed in place with administrative controls. At CAS 58-09-01, Central Mud Pit (CMP), a vegetated soil cover was constructed over the mud pit. At the remaining two sites, CAS 58-09-02, Mud Pit, and CAS 58-09-05, Mud Pits (3), aboveground monuments and warning signs were installed to mark the CAS boundaries. Three CASs at UC-3 were closed in place with administrative controls. Aboveground monuments and warning signs were installed to mark the site boundaries at CAS 58-09-06, Mud Pits (5), CAS 58-25-01, Spill, and CAS 58-10-01, Shaker Pad Area. Two CASs that consist of five sites at UC-4 were closed in place with administrative controls. At CAS 58-09-03, Mud Pits (5), an engineered soil cover was constructed over Mud Pit C. At the remaining three sites in CAS 58-09-03 and at CAS 58-10-05, Shaker Pad Area, aboveground monuments and warning signs were installed to mark the site boundaries. The remaining 26 CASs at CAU 417 were either clean-closed or closed by taking no further action.

  17. Midtemperature Solar Systems Test Facility predictions for thermal performance of the Suntec solar collector with heat-formed glass reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1980-11-01T23:59:59.000Z

    Thermal performance predictions are presented for the Suntec solar collector, with heat-formed glass reflector surface, for three output temperatures at five cities in the United States.

  18. RIS-M-2586 ELASTIC-PLASTIC FRACTURE MECHANICS ANALYSIS OF A CT-SPECIMEN

    E-Print Network [OSTI]

    RISØ-M-2586 ELASTIC-PLASTIC FRACTURE MECHANICS ANALYSIS OF A CT-SPECIMEN - A TWO-DIMENSIONAL APPROACH Gunner C. Larsen Abstract. This report documents the results obtained from an elastic-plastic

  19. Test Series 2. 3 detailed test plan

    SciTech Connect (OSTI)

    Not Available

    1983-12-01T23:59:59.000Z

    Test Series 2.3 is chronologically the second of the five sub-series of tests which comprise Test Series 2, the second major Test Series as part of the combustion research phase to be carried out at the Grimethorpe Experimental Pressurised Fluidised Bed Combustion Facility. Test Series 2.3 will consist of 700 data gathering hours which is expected to require some 1035 coal burning hours. The tests will be performed using US supplied coal and dolomite. This will be the first major series of tests on the Facility with other than the UK datum coal and dolomite. The document summarises the background to the facility and the experimental program. Described are modifications which have been made to the facility following Test Series 2.1 and a series of Screening Tests. Detailed test objectives are specified as are the test conditions for the experiments which comprise the test series. The test results will provide information on the effects of the bed temperature, excess air level, Ca/S ratio, number of coal feed lines, and combustion efficiency and sulphur retention. A significant aspect of the test series will be part load tests which will investigate the performance of the facility under conditions of turn down which simulate load following concepts specified for two combined cycle concepts, i.e., their CFCC combined cycle and a turbo charged combined cycle. The material test plan is also presented. The principal feature of the materials programme is the planned exposure of a set of static turbine blade specimens in a cascade test loop to the high temperature, high pressure flue gas. A schedule for the programme is presented as are contingency plans.

  20. A comparison of several surface finish measurement methods as applied to ground ceramic and metal surfaces

    SciTech Connect (OSTI)

    Blau, P.J.; Martin, R.L.; Riester, L.

    1996-01-01T23:59:59.000Z

    Surface finish is one of the most common measures of surface quality of ground ceramics and metal parts and a wide variety of methods and parameters have been developed to measure it. The purpose of this investigation was to compare the surface roughness parameters obtained on the same two specimens from three different types of measuring instruments: a traditional mechanical stylus system, a non-contact laser scanning system, and the atomic force microscope (two different AFM systems were compared). The same surface-ground silicon nitride and Inconel 625 alloy specimens were used for all measurements in this investigation. Significant differences in arithmetic average roughness, root-mean-square roughness, and peak-to-valley roughness were obtained when comparing data from the various topography measuring instruments. Non-contact methods agreed better with the others on the metal specimen than on the ceramic specimen. Reasons for these differences include the effective dimensions and geometry of the probe with respect to the surface topography; the reflectivity of the surface, and the type of filtering scheme Results of this investigation emphasize the importance of rigorously specifying the manner of surface roughness measurement when either reporting roughness data or when requesting that roughness data be provided.

  1. Midtemperature Solar Systems Test Facility predictions for thermal performance of the Solar Kinetics T-700 solar collector with FEK 244 reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1980-11-01T23:59:59.000Z

    Thermal performance predictions are presented for the Solar Kinetics T-700 solar collector, with FEK 244 reflector surface, for three output temperatures at five cities in the United States.

  2. Long-Term Materials Test Program: materials exposure test plan

    SciTech Connect (OSTI)

    None

    1981-12-01T23:59:59.000Z

    The Long Term Materials Test Program is designed to identify promising corrosion resistant materials for coal-fired gas turbine applications. Resistance of materials to long term accelerated corrosion will be determined through realistic PFB environmental exposure of candidate turbine materials for up to 14,000 hours. Selected materials also will be evaluated for their ability to withstand the combined erosive and corrosive aspects of the PFB effluent. A pressurized fluidized bed combustor facility has been constructed at the General Electric Coal Utilization Research Laboratory at Malta, New York. The 12-inch diameter combustor will burn high sulfur coal with moderate-to-high chlorine and alkali levels and utilize dolomite as the sulfur sorbent. Hot gas cleanup is achieved using three stages of cyclone separators. Downstream of the cylone separators, a low velocity test section (approx. 30 ft/s) capable of housing 180 pin specimens 1/4'' diameter has been installed to assess the corrosion resistance of the various materials at three different temperatures ranging from 1300 to 1600/sup 0/F. Following the low velocity test section is a high velocity test section consisting of four cascades of airfoil shaped specimens, six specimens per cascade. This high velocity test section is being used to evaluate the combined effects of erosion and corrosion on the degradation of gas turbine materials at gas velocities of 800 to 1400 ft/s. This report summarizes the materials selection and materials exposure test plan for the Long Term Materials Test.

  3. Investigation Of The Friction Factor Behavior for Flat Plate Tests Of Smooth And Roughened Surfaces With Supply Pressures Up To 84 Bars

    E-Print Network [OSTI]

    Kheireddin, Bassem A.

    2010-10-12T23:59:59.000Z

    friction factor data and measure dynamic pressure oscillations. A detailed description of the test facility is described, and a theory for determining the friction factor is reviewed. Three clearances were investigated: 0.635, 0.381, and 0.254 mm. Tests...

  4. In-Situ Creep Testing Capability for the Advanced Test Reactor

    SciTech Connect (OSTI)

    B. G. Kim; J. L. Rempe; D. L. Knudson; K. G. Condie; B. H. Sencer

    2012-09-01T23:59:59.000Z

    An instrumented creep testing capability is being developed for specimens irradiated in Pressurized Water Reactor (PWR) coolant conditions at the Advanced Test Reactor (ATR). The test rig has been developed such that samples will be subjected to stresses ranging from 92 to 350 MPa at temperatures between 290 and 370 °C up to at least 2 dpa (displacement per atom). The status of Idaho National Laboratory (INL) efforts to develop the test rig in-situ creep testing capability for the ATR is described. In addition to providing an overview of in-pile creep test capabilities available at other test reactors, this paper reports efforts by INL to evaluate a prototype test rig in an autoclave at INL’s High Temperature Test Laboratory (HTTL). Initial data from autoclave tests with 304 stainless steel (304 SS) specimens are reported.

  5. An unstructured C-grid based method for 3-D global ocean dynamics: Free-surface formulations and tidal test cases

    E-Print Network [OSTI]

    Peltier, W. Richard

    and tidal test cases G.R. Stuhne *, W.R. Peltier Department of Physics, University of Toronto, 60 St. George rights reserved. 1. Introduction In a previous paper (Stuhne and Peltier, 2006, hereafter SP), we

  6. Joint Industry/Government Research Project: Comparison of thermal aging for roof exposures and thin-specimens of experimental polyisocyanurate insulation foamed with alternative blowing agents

    SciTech Connect (OSTI)

    Graves, R.S.; Christian, J.E.; McElroy, D.L.

    1991-01-01T23:59:59.000Z

    This paper reports apparent thermal conductivity (k) values from field exposures and laboratory aging of a set of industry-produced, experimental polyisocyanurate (PIR) laminated boardstock foamed with hydrochlorofluorocarbons (HCFCs) as alternative to chlorofluorocarbons (CFCs). The k-values were determined from 0 to 50{degree}C using techniques that meet ASTM C 1114 (Thin Heater Apparatus) and ASTM C 518 (Heat Flow Meter Apparatus). The increase in k observed for field exposure in the ORNL Roof Thermal Research Apparatus (RTRA) was confirmed by independent laboratory tests. The observed laboratory increase in k was about the same, between 17 and 22%, for all three blowing agent foams for a 450 day field exposure in the RTRA. Thin specimens were planed from the industry-produced boardstock foams and aged at 24 and 65{degree}C for up to 460 days. The foams blown with alternative blowing agents exhibited long-term k-values 7 to 15% above those for CFC foams under similar conditions. Field exposures were conducted on specimens under single ply EPDM membranes in the RTRA for over 680 days. Hourly averages of panel temperature and heat flux were analyzed to obtain k as a function of mean insulation temperature on a week-by-week basis. The k-values derived from the field data provided effective diffusion coefficients for air in the foam, which were within 7% of those obtained from the thin-specimen aging procedure at 24%C except for one sample. The relative performance of test specimens of HCFC-141b under a black and under a white membrane is reported, and data suggest that differences are relatively small. 26 refs., 10 figs., 8 tabs.

  7. A proposed benchmark for simulation in radiographic testing

    SciTech Connect (OSTI)

    Jaenisch, G.-R.; Deresch, A.; Bellon, C. [Federal Institute for Materials Research and Testing Unter den Eichen 87, 12205 Berlin (Germany); Schumm, A.; Guerin, P. [EDF R and D, 1 avenue du Général de Gaulle, 92141 Clamart (France)

    2014-02-18T23:59:59.000Z

    The purpose of this benchmark study is to compare simulation results predicted by various models of radiographic testing, in particular those that are capable of separately predicting primary and scatter radiation for specimens of arbitrary geometry.

  8. POST CLOSURE INSPECTION AND MONITORING REPORT FOR CORRECTIVE ACTION UNIT 417: CENTRAL NEVADA TEST AREA - SURFACE, HOT CREEK VALLEY, NEVADA; FOR CALENDAR YEAR 2005

    SciTech Connect (OSTI)

    NONE

    2006-04-01T23:59:59.000Z

    Corrective Action Unit (CAU) 417, Central Nevada Test Area - Surface, is located in Hot Creek Valley in northern Nye County, Nevada, and consists of three areas commonly referred to as UC-1, UC-3, and UC-4. CAU 417 consists of 34 Corrective Action Sites (CASs) which were closed in 2000 (U. S. Department of Energy, National Nuclear Security Administration Nevada Operations Office, 2001). Three CASs at UC-1 were closed in place with administrative controls. At CAS 58-09-01, Central Mud Pit (CMP), a vegetated soil cover was constructed over the mud pit. At the remaining two sites CAS 58-09-02, Mud Pit and 58-09-05, Mud Pits (3), aboveground monuments and warning signs were installed to mark the CAS boundaries. Three CASs at UC-3 were closed in place with administrative controls. Aboveground monuments and warning signs were installed to mark the site boundaries at CAS 58-09-06, Mud Pits (5), CAS 58-25-01, Spill and CAS 58-10-01, Shaker Pad Area. Two CASs that consist of five sites at UC-4 were closed in place with administrative controls. At CAS 58-09-03, Mud Pits 9, an engineered soil cover was constructed over Mud Pit C. At the remaining three sites in CAS 58-09-03 and at CAS 58-10-05, Shaker Pad Area, aboveground monuments and warning signs were installed to mark the site boundaries. The remaining 26 CASs at CAU 417 were either clean-closed or closed by taking no further action. Quarterly post-closure inspections are performed at the CASs that were closed in place at UC-I, UC-3, and UC-4. During calendar year 2005, site inspections were performed on March 15, June 16, September 22, and December 7. The inspections conducted at the UC-1 CMP documented that the site was in good condition and continued to show integrity of the cover unit. No new cracks or fractures were observed until the December inspection. A crack on the west portion of the cover showed evidence of lateral expansion; however, it is not at an actionable level. The crack will be sealed by filling with bentonite during the first quarter of 2006 and monitored during subsequent inspections. The cover vegetation was healthy and well established. No issues were identified with the CMP fence, gate, or subsidence monuments. No issues were identified with the warning signs and monuments at the other two UC-1 locations. The inspections at UC-3 indicated that the sites are in excellent condition. All monuments and signs showed no displacement, damage, or removal. A small erosion gully from spring rain runoff was observed during the June inspection, but it did not grow to an actionable level during 2005. No other issues or concerns were identified. Inspections performed at UC-4 Mud Pit C cover revealed that erosion rills were formed during March and September exposing the geosynthetic clay liner. Both erosion rills were repaired within 90 days of reporting. Sparse vegetation is present on the cover. The overall condition of the monuments, fence, and gate are in good condition. No issues were identified with the warning signs and monuments at the other four UC-4 locations. Subsidence surveys were conducted at UC-1 CMP and UC-4 Mud Pit C in March and September of 2005. The results of the subsidence surveys indicate that the covers are performing as expected, and no unusual subsidence was observed. The June vegetation survey of the UC-1 CMP cover and adjacent areas indicated that the revegetation has been very successful. The vegetation should continue to be monitored to document any changes in the plant community and identify conditions that could potentially require remedial action in order to maintain a viable vegetative cover on the site. Vegetation surveys should be conducted only as required. Precipitation during 2005 was above average, with an annual rainfall total of 21.79 centimeters (8.58 inches). Soil moisture content data show that the UC-1 CMP cover is performing as designed, with evapotranspiration effectively removing water from the cover. It is recommended to continue quarterly site inspections and the collection of soil moisture data for the UC-1 CMP cove

  9. Process for measuring low cadmium levels in blood and other biological specimens

    DOE Patents [OSTI]

    Peterson, David P. (Orland Park, IL); Huff, Edmund A. (Lemont, IL); Bhattacharyya, Maryka H. (Naperville, IL)

    1994-01-01T23:59:59.000Z

    A process for measuring low levels of cadmium in blood and other biological specimens is provided without interference from high levels of alkali metal contaminants by forming an aqueous solution and without contamination by environmental cadmium absent the proteins from the specimen, selectively removing cadmium from the aqueous solution on an anion exchange resin, thereby removing the alkali metal contaminants, resolubilizing cadmium from the resin to form a second solution and analyzing the second solution for cadmium, the process being carried out in a cadmium-free environment.

  10. Process for measuring low cadmium levels in blood and other biological specimens

    DOE Patents [OSTI]

    Peterson, David P.; Huff, Edmund A.; Bhattacharyya, Maryka H.

    1994-05-03T23:59:59.000Z

    A process for measuring low levels of cadmium in blood and other biological specimens is provided without interference from high levels of alkali metal contaminants by forming an aqueous solution and without contamination by environmental cadmium absent the proteins from the specimen, selectively removing cadmium from the aqueous solution on an anion exchange resin, thereby removing the alkali metal contaminants, resolubilizing cadmium from the resin to form a second solution and analyzing the second solution for cadmium, the process being carried out in a cadmium-free environment.

  11. A shallow subsurface controlled release facility in Bozeman, Montana, USA, for testing near surface CO2 detection techniques and transport models

    SciTech Connect (OSTI)

    Spangler, L.H.; Dobeck, L.M.; Nehrir, A.; Humphries, S.; Barr, J.; Keith, C.; Shaw, J.; Rouse, J.; Cunningham, A.; Benson, S.; Repasky, K.S.; Lewicki, J.; Wells, A.; Diehl, R.; Strazisar, B.; Fessenden, J.; Rahn, T.; Amonette, J.; Barr, J.; Pickles, W.; Jacobson, J.; Silver, E.; Male, E.; Rauch, H.; Gullickson, K.; Trautz, R.; Kharaka, Y.; Birkholzer, J.T.; Wielopolski, L.; Oldenburg, C.M.

    2009-10-20T23:59:59.000Z

    A controlled field pilot has been developed in Bozeman, Montana, USA, to study near surface CO2 transport and detection technologies. A slotted horizontal well divided into six zones was installed in the shallow subsurface. The scale and CO2 release rates were chosen to be relevant to developing monitoring strategies for geological carbon storage. The field site was characterized before injection, and CO2 transport and concentrations in saturated soil and the vadose zone were modeled. Controlled releases of CO2 from the horizontal well were performed in the summers of 2007 and 2008, and collaborators from six national labs, three universities, and the U.S. Geological Survey investigated movement of CO2 through the soil, water, plants, and air with a wide range of near surface detection techniques. An overview of these results will be presented.

  12. Design of a non-contact vibration measurement and analysis system for electronic board testing

    E-Print Network [OSTI]

    Arn, Krissa Elizabeth, 1980-

    2004-01-01T23:59:59.000Z

    Traditional vibration measurement methods involve placing accelerometers at discrete locations on a test object. In cases where the test specimen is small in mass, the addition of these measurement transducers can alter ...

  13. Sampling and analytical testing of groundwater and surface water at the Colorado School of Mines Research Institute (CSMRI) has been conducted on a quarterly basis since early

    E-Print Network [OSTI]

    is being consumed, changing the water chemistry, and leading to lower uranium concentrations with flow, Th-230, Th-232, and uranium), and metals (arsenic, barium calcium, cadmium, chromium, lead, manganese and analytical testing for radium, calcium, magnesium, potassium, sodium, uranium, and zinc will continue

  14. A surface ionization source 

    E-Print Network [OSTI]

    Buzatu, Daniel J.

    1995-01-01T23:59:59.000Z

    The main part of the work described herein is the development and testing of a surface ionization source for use on a collinear fast beam laser spectroscopy apparatus. A description of the previously existing fast beam apparatus is given...

  15. A surface ionization source

    E-Print Network [OSTI]

    Buzatu, Daniel J.

    1995-01-01T23:59:59.000Z

    The main part of the work described herein is the development and testing of a surface ionization source for use on a collinear fast beam laser spectroscopy apparatus. A description of the previously existing fast beam apparatus is given...

  16. Solderability test system

    DOE Patents [OSTI]

    Yost, F.; Hosking, F.M.; Jellison, J.L.; Short, B.; Giversen, T.; Reed, J.R.

    1998-10-27T23:59:59.000Z

    A new test method to quantify capillary flow solderability on a printed wiring board surface finish. The test is based on solder flow from a pad onto narrow strips or lines. A test procedure and video image analysis technique were developed for conducting the test and evaluating the data. Feasibility tests revealed that the wetted distance was sensitive to the ratio of pad radius to line width (l/r), solder volume, and flux predry time. 11 figs.

  17. Solderability test system

    DOE Patents [OSTI]

    Yost, Fred (Cedar Crest, NM); Hosking, Floyd M. (Albuquerque, NM); Jellison, James L. (Albuquerque, NM); Short, Bruce (Beverly, MA); Giversen, Terri (Beverly, MA); Reed, Jimmy R. (Austin, TX)

    1998-01-01T23:59:59.000Z

    A new test method to quantify capillary flow solderability on a printed wiring board surface finish. The test is based on solder flow from a pad onto narrow strips or lines. A test procedure and video image analysis technique were developed for conducting the test and evaluating the data. Feasibility tests revealed that the wetted distance was sensitive to the ratio of pad radius to line width (l/r), solder volume, and flux predry time.

  18. Addendum to the Closure Report for Corrective Action Unit 484: Surface Debris, Waste Sites, and Burn Area, Tonopah Test Range, Nevada (Revision 0)

    SciTech Connect (OSTI)

    Mark Burmeister

    2011-03-01T23:59:59.000Z

    Corrective Action Unit (CAU) 484 Streamlined Approach for Environmental Restoration (SAFER) activities called for the identification and remediation of surface hot spot depleted uranium (DU) with some excavation to determine the vertical extent of contamination (NNSA/NSO, 2004). During the CAU 484 SAFER investigation (conducted November 2003 through August 2007), approximately 50 locations containing DU were identified on Antelope Lake. All but four locations (CA-1, SA-5-9, SA-12-15, and SA-4) were remediated. Figure 1-1 shows locations of the four use restriction (UR) sites. The four locations were determined to have failed the SAFER conceptual site model assumption of a small volume hot spot. Two of the locations (CA-1 and SA-5-9) were excavated to depths of 3.5 to 7 feet (ft) below ground surface (bgs), and a third location (SA-12-15) with a footprint of 30 by 60 ft was excavated to a depth of 0.5 ft. At the fourth site (SA-4), the discovery of unexploded ordnance (UXO) halted the excavation due to potential safety concerns. Remediation activities on Antelope Lake resulted in the removal of approximately 246 cubic yards (yd3) of DU-impacted soil from the four UR sites; however, Kiwi surveys confirmed that residual DU contamination remained at each of the four sites. (The Kiwi was a Remote Sensing Laboratory [RSL] vehicle equipped with a data-acquisition system and four sodium iodide gamma detectors. Surveys were conducted with the vehicle moving at a rate of approximately 10 miles per hour with the gamma detectors positioned 14 to 28 inches [in.] above the ground surface [NNSA/NSO, 2004]).

  19. Propagation of guided Lamb waves in bonded specimens using piezoelectric wafer active sensors

    E-Print Network [OSTI]

    Giurgiutiu, Victor

    Propagation of guided Lamb waves in bonded specimens using piezoelectric wafer active sensors and principles used for generation and propagation of ultrasonic guided waves (Lamb waves) using piezoelectric wafer active sensors (PWAS). Keywords: Ultrasonic, Lamb waves, Damage detection, NDE, Wave propagation

  20. An investigation of microstructures and yield strengths in irradiated austenitic stainless steels using small specimen techniques

    SciTech Connect (OSTI)

    Toloczko, M.B.; Lucas, G.E.; Odette, G.R. [Univ. of California, Santa Barbara, CA (United States). Dept. of Chemical and Nuclear Engineering; Stoller, R.E. [Oak Ridge National Lab., TN (United States); Hamilton, M.L. [Pacific Northwest Lab., Richland, WA (United States)

    1996-12-31T23:59:59.000Z

    Transmission electron microscopy (TEM) specimens of a first core heat of 316 stainless steel, in both the solution annealed and 20% cold worked condition, were irradiated to 46 dpa at 420 C, to 49 dpa at 520 C, and to 34 dpa at 600 C in FFTF/MOTA. Prior to irradiation, some of the specimens were pre-implanted with approximately 100 appm of helium over one-third of the specimen thickness. Microstructures and mechanical properties of these specimens were examined. Microstructural data was taken from unimplanted zones and were consistent with data in the literature for unimplanted 316 SS. Where possible, irradiation hardening of the alloys was experimentally evaluated by microhardness and shear punch. For comparison, irradiation hardening was also calculated using a barrier hardening model and the microstructural data. Experimentally measured values of yield stress were in agreement with the range of values reported in the literature regardless of helium pre-implantation and were similar to the calculated values.

  1. Focused ion beam specimen preparation for electron holography of electrically biased thin film solar cells

    E-Print Network [OSTI]

    Dunin-Borkowski, Rafal E.

    solar cells M. Duchamp1 , M. den Hertog2 , R. Imlau1 , C. B. Boothroyd1 , A. Kovács1 , A. H. Tavabi1, biased TEM specimen, thin film solar cell, FIB Thin films of hydrogenated Si (Si:H) can be used as active absorber layers in solar cells deposited on low cost substrates using plasma-enhanced chemical vapour

  2. Testing the Influence of Surface Tension and Finite Width of QGP Bags on the QCD Matter EOS Properties at NICA Energies

    E-Print Network [OSTI]

    Kyrill A. Bugaev

    2009-09-03T23:59:59.000Z

    Here I give some strong arguments that the central issues for theoretical studies of the (tri)critical endpoint of the QCD phase diagram are the surface tension of large/heavy QGP bags and their medium dependent width. Then I discuss three major directions to further develop the realistic exactly solvable statistical models which simultaneously are able to describe the 1-st order deconfinement phase transition, the 2-nd order one and the cross-over. Also I analyze the most necessary projects that have to be studied in order to formulate the reliable and convincing signals of the mixed phase formation at NICA energies.

  3. A shallow subsurface controlled release facility in Bozeman, Montana, USA, for testing near surface CO2 detection techniques and transport models

    SciTech Connect (OSTI)

    Spangler, Lee H.; Dobeck, Laura M.; Repasky, Kevin S.; Nehrir, Amin R.; Humphries, Seth D.; Barr, Jamie L.; Keith, Charlie J.; Shaw, Joseph A.; Rouse, Joshua H.; Cunningham, Alfred B.; Benson, Sally M.; Oldenburg, Curtis M.; Lewicki, Jennifer L.; Wells, Arthur W.; Diehl, J. R.; Strazisar, Brian; Fessenden, Julianna; Rahn, Thom A.; Amonette, James E.; Barr, Jonathan L.; Pickles, William L.; Jacobson, James D.; Silver, Eli A.; Male, Erin J.; Rauch, Henry W.; Gullickson, Kadie; Trautz, Robert; Kharaka, Yousif; Birkholzer, Jens; Wielopolski, Lucien

    2010-03-01T23:59:59.000Z

    A facility has been constructed to perform controlled shallow releases of CO2 at flow rates that challenge near surface detection techniques and can be scalable to desired retention rates of large scale CO2 storage projects. Preinjection measurements were made to determine background conditions and characterize natural variability at the site. Modeling of CO2 transport and concentration in saturated soil and the vadose zone was also performed to inform decisions about CO2 release rates and sampling strategies. Four releases of CO2 were carried out over the summer field seasons of 2007 and 2008. Transport of CO2 through soil, water, plants, and air was studied using near surface detection techniques. Soil CO2 flux, soil gas concentration, total carbon in soil, water chemistry, plant health, net CO2 flux, atmospheric CO2 concentration, movement of tracers, and stable isotope ratios were among the quantities measured. Even at relatively low fluxes, most techniques were able to detect elevated levels of CO2 in the soil, atmosphere, or water. Plant stress induced by CO2 was detectable above natural seasonal variations.

  4. A study of the variation of the stress concentration due to an inclusion in a tensile specimen

    E-Print Network [OSTI]

    Coppinger, John Timothy

    1967-01-01T23:59:59.000Z

    A S'1'UDY OF TH1. , VARIATION OF THE STRFSS CONCE1&lTRATION DUF. TO AN INCLUSION IN A TENSILE SPECIMEN A Thesis by JOHN TIiviOTIIY COPPINGER Submitted to the Graduate College of the Texas ALM University ir oartial fulfillment... in the Specimen Containing the 5/32 Diameter Inclusion 13 Calculation of the Maximum Principal Stress in th Specimen Containing the 5/1 6 Diamet, er Inclusion 1 4 Calculation of the Maximum Principal Stress in the Specimen Containing the 13/16 Die...

  5. A study of the variation of the stress concentration due to an inclusion in a tensile specimen 

    E-Print Network [OSTI]

    Coppinger, John Timothy

    1967-01-01T23:59:59.000Z

    A S'1'UDY OF TH1. , VARIATION OF THE STRFSS CONCE1&lTRATION DUF. TO AN INCLUSION IN A TENSILE SPECIMEN A Thesis by JOHN TIiviOTIIY COPPINGER Submitted to the Graduate College of the Texas ALM University ir oartial fulfillment... in the Specimen Containing the 5/32 Diameter Inclusion 13 Calculation of the Maximum Principal Stress in th Specimen Containing the 5/1 6 Diamet, er Inclusion 1 4 Calculation of the Maximum Principal Stress in the Specimen Containing the 13/16 Die...

  6. THERMAL PREDICTIONS OF NEW COMPOSITE MATERIAL DURING INPILE TESTING

    SciTech Connect (OSTI)

    Donna Post Guillen; W. David Swank; Heng Ban; Kurt Harris; Adam Zabriskie

    2011-09-01T23:59:59.000Z

    An inpile experiment is currently underway wherein specimens comprised of a newly developed material are being irradiated at Idaho National Laboratory's Advanced Test Reactor (ATR) in conjunction with Utah State University under the auspices of the ATR National Scientific User Facility. This paper provides the thermophysical properties of this new material measured prior to irradiation. After the irradiation campaign is complete, the thermophysical properties of the specimens will be measured and compared to the preirradiation values. A finite-element model was constructed to predict bounding specimen temperatures during irradiation. Results from the thermal hydraulic modeling, including the steady-state temperatures of the specimens within sealed capsules, are presented. After the irradiation campaign is completed, best-estimate thermal predictions will be performed for the individual specimens using the actual as-run irradiation power levels.

  7. Surface sampling concentration and reaction probe

    DOE Patents [OSTI]

    Van Berkel, Gary J; Elnaggar, Mariam S

    2013-07-16T23:59:59.000Z

    A method of analyzing a chemical composition of a specimen is described. The method can include providing a probe comprising an outer capillary tube and an inner capillary tube disposed co-axially within the outer capillary tube, where the inner and outer capillary tubes define a solvent capillary and a sampling capillary in fluid communication with one another at a distal end of the probe; contacting a target site on a surface of a specimen with a solvent in fluid communication with the probe; maintaining a plug volume proximate a solvent-specimen interface, wherein the plug volume is in fluid communication with the probe; draining plug sampling fluid from the plug volume through the sampling capillary; and analyzing a chemical composition of the plug sampling fluid with an analytical instrument. A system for performing the method is also described.

  8. Nickel Alloy Primary Water Bulk Surface and SCC Corrosion Film Analytical Characterization and SCC Mechanistic Implications

    SciTech Connect (OSTI)

    Morton, D.; Lewis, N.; Hanson, M.; Rice, S.; Sanders, P.

    2007-04-18T23:59:59.000Z

    Alloy 600 corrosion coupon tests were performed: (1) to quantify the temperature dependency of general corrosion and (2) to characterize the composition and structure of bulk surface corrosion films for comparison with ongoing primary water SCC (PWSCC) crack tip corrosion film analyses. Results suggest that the thermal activation energy of Alloy 600 corrosion is consistent with the thermal activation energy of nickel alloy PWSCC. Analytical investigations of the structure and composition of Alloy 600 bulk surface corrosion oxides revealed a duplex (inner and outer) oxide layer structure. The outer layer is discontinuous and comprised of relatively large (1 to 3 {micro}m) nickel ferrite crystals and smaller ({approx}0.1 {micro}m) chromium containing nickel ferrite crystals. The inner layer consists of a relatively continuous chromite spinel (major phase) and chromia (Cr{sub 2}O{sub 3} minor phase) which formed through non-selective oxidation. Chromia and dealloyed Alloy 600 (highly Ni enriched metal) were only observed at 337 C (640 F) and only along the boundaries of deformation induced fine grains and subcells. Specimens having deformation free surfaces exhibited continuous uniform inner chromite spinel oxide layers. Specimens with machining induced surface deformation produced non-uniform inner layer oxides (chromite spinel, Cr{sub 2}O{sub 3} and unoxidized material). PWSCC crack tip oxides, in contrast, were fine grain (no duplex structure) and consisted of both chromium rich spinels and ''NiO'' structure oxides. Generally, nickel rich oxides were more abundant under more oxidized conditions (reduced coolant hydrogen) and spinel rich crack tip oxides were favored under more reducing conditions (increased coolant hydrogen). Bulk surface corrosion film thickness did not correlate with observed SCC growth rates. These results suggest that corrosion is not the rate controlling step of PWSCC but rather that PWSCC and corrosion have a common rate controlling sub process (e.g., cation diffusion, oxygen ingress).

  9. Conductivity Profile Determination by Eddy Current for Shot Peened Superalloy Surfaces Toward Residual Stress Assessment

    SciTech Connect (OSTI)

    Shen, Y.; Lo, C. C. H.; Frishman, A. M.; Lee, C.; Nakagawa, N. [Center for Nondestructive Evaluation, Iowa State University, Ames, Iowa 50011 (United States)

    2007-03-21T23:59:59.000Z

    This paper describes an eddy current model-based method for inverting near-surface conductivity deviation profiles of surface treated materials from swept-high frequency eddy current (SHFEC) data. This work forms part of our current research directed towards the development of an electromagnetic nondestructive technique for assessing residual stress of shot-peened superalloy components. The inversion procedure is based on the use of a parameterized function to describe the near-surface conductivity as a function of depth for a shot-peened surface, and the laterally uniform multi-layer theory of Cheng, Dodd and Deeds to calculate the resulting coil impedance deviations. The convergence of the inversion procedure has been tested against synthesized eddy current data. As a demonstration, the conductivity deviation profiles of a series of Inconel 718 specimens, shot peened at various Almen intensities, have been obtained by inversion. Several consistency tests were conducted to examine the reliability of the inverted conductivity profiles. The results show that conductivity deviation profiles can be reliably determined from SHFEC data within the accuracy of the current measurement system.

  10. Results of irradiated cladding tests and clad plate experiments

    SciTech Connect (OSTI)

    Haggag, F.M.; Iskander, S.K.

    1988-01-01T23:59:59.000Z

    Two aspects critical to the fracture behavior of three-wire stainless steel cladding were investigated by the Heavy-Section Steel Technology (HSST) Program: (1) radiation effects on cladding strength and toughness, and (2) the response of mechanically loaded, flawed structures in the presence of cladding (clad plate experiments). Postirradiation testing results show that, in the test temperature range from /minus/125 to 288/degree/C, the yield strength increased, and ductility insignificantly increased, while there was almost no change in ultimate tensile strength. All cladding exhibited ductile-to-brittle transition behavior during Charpy impact testing. Radiation damage decreased the Charpy upper-shelf energy by 15 to 20% and resulted in up to 28/degree/C shifts of the Charpy impact transition temperature. Results of irradiated 12.5-mm-thick compact specimens (0.5TCS) show consistent decreases in the ductile fracture toughness, J/sub Ic/, and the tearing modulus. Results from clad plate tests have shown that (1) a tough surface layer composed of cladding and/or heat-affected zone has arrested running flaws under conditions where unclad plates have ruptured, and (2) the residual load-bearing capacity of clad plates with large subclad flaws significantly exceeded that of an unclad plate. 13 figs., 1 tab.

  11. FRACTURE MECHANICS APPROACH TO ESTIMATE FATIGUE LIVES OF WELDED LAP-SHEAR SPECIMENS

    SciTech Connect (OSTI)

    Lam, P.; Michigan, J.

    2014-04-25T23:59:59.000Z

    A full range of stress intensity factor solutions for a kinked crack is developed as a function of weld width and the sheet thickness. When used with the associated main crack solutions (global stress intensity factors) in terms of the applied load and specimen geometry, the fatigue lives can be estimated for the laser-welded lap-shear specimens. The estimations are in good agreement with the experimental data. A classical solution for an infinitesimal kink is also employed in the approach. However, the life predictions tend to overestimate the actual fatigue lives. The traditional life estimations with the structural stress along with the experimental stress-fatigue life data (S-N curve) are also provided. In this case, the estimations only agree with the experimental data under higher load conditions.

  12. An investigation of penetrant techniques for detection of machining-induced surface-breaking cracks on monolithic ceramics

    SciTech Connect (OSTI)

    Forster, G.A.; Ellingson, W.A.

    1996-02-01T23:59:59.000Z

    The purpose of this effort was to evaluate penetrant methods for their ability to detect surface-breaking cracks in monolithic ceramic materials with an emphasis on detection of cracks generated by machining. There are two basic penetrant types, visible and fluorescent. The visible penetrant method is usually augmented by powder developers and cracks detected can be seen in visible light. Cracks detected by fluorescent penetrant are visible only under ultraviolet light used with or without a developer. The developer is basically a powder that wicks up penetrant from a crack to make it more observable. Although fluorescent penetrants were recommended in the literature survey conducted early in this effort, visible penetrants and two non-standard techniques, a capillary gaseous diffusion method under development at the institute of Chemical Physics in Moscow, and the {open_quotes}statiflux{close_quotes} method which involves use of electrically charged particles, were also investigated. SiAlON ring specimens (1 in. diameter, 3/4 in. wide) which had been subjected to different thermal-shock cycles were used for these tests. The capillary gaseous diffusion method is based on ammonia; the detector is a specially impregnated paper much like litmus paper. As expected, visible dye penetrants offered no detection sensitivity for tight, surface-breaking cracks in ceramics. Although the non-standard statiflux method showed promise on high-crack-density specimens, it was ineffective on limited-crack-density specimens. The fluorescent penetrant method was superior for surface-breaking crack detection, but successful application of this procedure depends greatly on the skill of the user. Two presently available high-sensitivity fluorescent penetrants were then evaluated for detection of microcracks on Si{sub 3}N{sub 4} and SiC from different suppliers. Although 50X optical magnification may be sufficient for many applications, 200X magnification provides excellent delectability.

  13. Results from Nevada Nuclear Waste Storage Investigations (NNWSI) Series 3 spent fuel dissolution tests

    SciTech Connect (OSTI)

    Wilson, C.N.

    1990-06-01T23:59:59.000Z

    The dissolution and radionuclide release behavior of spent fuel in groundwater is being studied by the Yucca Mountain Project (YMP), formerly the Nevada Nuclear Waste Storage Investigations (NNWSI) Project. Specimens prepared from pressurized water reactor fuel rod segments were tested in sealed stainless steel vessels in Nevada Test Site J-13 well water at 85{degree}C and 25{degree}C. The test matrix included three specimens of bare-fuel particles plus cladding hulls, two fuel rod segments with artificially defected cladding and water-tight end fittings, and an undefected fuel rod section with watertight end fittings. Periodic solution samples were taken during test cycles with the sample volumes replenished with fresh J-13 water. Test cycles were periodically terminated and the specimens restarted in fresh J-13 water. The specimens were run for three cycles for a total test duration of 15 months. 22 refs., 32 figs., 26 tabs.

  14. Nano-Continuum Modeling of a Nuclear Glass Specimen Altered for 25 Years

    SciTech Connect (OSTI)

    Steefel, Carl

    2014-01-06T23:59:59.000Z

    The purpose of this contribution is to report on preliminary nano-continuum scale modeling of nuclear waste glass corrosion. The focus of the modeling is an experiment involving a French glass SON68 specimen leached for 25 years in a granitic environment. In this report, we focus on capturing the nano-scale concentration profiles. We use a high resolution continuum model with a constant grid spacing of 1 nanometer to investigate the glass corrosion mechanisms.

  15. Development of Mechanical Systems for Automated Medical Slide Specimen Storage and Retrieval

    E-Print Network [OSTI]

    Wurtz, Joshua James

    2014-05-31T23:59:59.000Z

    different types of fields. It is only natural that automation and robotics would have endless possibilities for application in the medical field [1]. Human tellers were replaced by automated machines at banks and automated switch boards replaced human... ON EXISTING APPLICATIONS OF RELATED MEDICAL AUTOMATION Automation in clinical laboratories got its start in the early 1980’s when robotic technology had advanced enough to be viable for specimen handling [2,4]. Since then many different versions...

  16. Experimental results obtained during fatigue testing of a spot-welded lap-shear structural-joint specimen are

    E-Print Network [OSTI]

    Giurgiutiu, Victor

    in a number of industries. Spot welding is the traditional method of assembly for steel-based automotive and construction of vehicular structures indicate a strong diversification of material usage, with aluminum and polymeric composites projected to play a major role. While aluminum is amenable to both spot welding

  17. BBR Asphalt mixture creep test BBR Asphalt mixture creep size effect

    E-Print Network [OSTI]

    Minnesota, University of

    #12;Outline ØBBR Asphalt mixture creep test ØBBR Asphalt mixture creep size effect ØBBR Asphalt Point Bending Test Low temperature 3-point bending creep tests on specimens with three different sizes mixture strength test ØBBR Asphalt binder strength test #12;Asphalt Pavements ØRecent efforts under NCHRP

  18. Surface Soil

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Surface Soil Surface Soil We compare local soil samples with samples collected from northern New Mexico locations that are beyond the range of potential influence from normal...

  19. Ecosystem feedbacks to climate change in California: Development, testing, and analysis using a coupled regional atmosphere and land-surface model (WRF3-CLM3.5)

    SciTech Connect (OSTI)

    Subin, Z.M.; Riley, W.J.; Kueppers, L.M.; Jin, J.; Christianson, D.S.; Torn, M.S.

    2010-11-01T23:59:59.000Z

    A regional atmosphere model [Weather Research and Forecasting model version 3 (WRF3)] and a land surface model [Community Land Model, version 3.5 (CLM3.5)] were coupled to study the interactions between the atmosphere and possible future California land-cover changes. The impact was evaluated on California's climate of changes in natural vegetation under climate change and of intentional afforestation. The ability of WRF3 to simulate California's climate was assessed by comparing simulations by WRF3-CLM3.5 and WRF3-Noah to observations from 1982 to 1991. Using WRF3-CLM3.5, the authors performed six 13-yr experiments using historical and future large-scale climate boundary conditions from the Geophysical Fluid Dynamics Laboratory Climate Model version 2.1 (GFDL CM2.1). The land-cover scenarios included historical and future natural vegetation from the Mapped Atmosphere-Plant-Soil System-Century 1 (MC1) dynamic vegetation model, in addition to a future 8-million-ha California afforestation scenario. Natural vegetation changes alone caused summer daily-mean 2-m air temperature changes of -0.7 to +1 C in regions without persistent snow cover, depending on the location and the type of vegetation change. Vegetation temperature changes were much larger than the 2-m air temperature changes because of the finescale spatial heterogeneity of the imposed vegetation change. Up to 30% of the magnitude of the summer daily-mean 2-m air temperature increase and 70% of the magnitude of the 1600 local time (LT) vegetation temperature increase projected under future climate change were attributable to the climate-driven shift in land cover. The authors projected that afforestation could cause local 0.2-1.2 C reductions in summer daily-mean 2-m air temperature and 2.0-3.7 C reductions in 1600 LT vegetation temperature for snow-free regions, primarily because of increased evapotranspiration. Because some of these temperature changes are of comparable magnitude to those projected under climate change this century, projections of climate and vegetation change in this region need to consider these climate-vegetation interactions.

  20. Characterization of Min-K TE-1400 Thermal Insulation (Two-Year Gradient Stress Relaxation Testing Update)

    SciTech Connect (OSTI)

    Hemrick, James Gordon [ORNL; Lara-Curzio, Edgar [ORNL; King, James [ORNL

    2009-09-01T23:59:59.000Z

    Min-K 1400TE insulation material was characterized at Oak Ridge National Laboratory for use in structural applications under gradient temperature conditions. A previous report (ORNL/TM-2008/089) discusses the testing and results from the original three year duration of the project. This testing included compression testing to determine the effect of sample size and test specimen geometry on the compressive strength of Min-K, subsequent compression testing on cylindrical specimens to determine loading rates for stress relaxation testing, isothermal stress relaxation testing, and gradient stress relaxation testing. This report presents the results from the continuation of the gradient temperature stress relaxation testing and the resulting updated modeling.

  1. An investigation into the mechanical response of Berea sandstone to the uniaxial-biaxial test

    E-Print Network [OSTI]

    Denton, Meredith Yrette

    1992-01-01T23:59:59.000Z

    during the loading cycle of the test, and under biaxial strain during unloading. Tests were performed without pore fluid, with unpressured pore fluid, and with drained and undrained pressured pore fluid. The stress-strain relationships... from a suite of laboratory tests. Typical testing programs include triaxial compression tests, hydrostatic compression tests, or extension tests; in all of these tests, the specimens are forced to follow a particular stress path. Less common...

  2. Effect of coating time on corrosion behavior of electroless nickel-phosphorus coated powder metallurgy iron specimens

    SciTech Connect (OSTI)

    Singh, D.; Balasubramaniam, R.; Dube, R.K. [Indian Inst. of Tech., Kanpur (India). Dept. of Materials and Metallurgical Engineering

    1995-08-01T23:59:59.000Z

    Powder metallurgy iron specimens with porosities in the range 0% to 2% were electroless coated with nickel-phosphorus alloy from baths containing sodium hypophosphite (NaH{sub 2}PO{sub 2}{center_dot}H{sub 2}O). The effect of coating time on thickness and phosphorus content of the deposit was analyzed. The free corrosion potentials and corrosion rates of the coated specimens were obtained by the Tafel extrapolation method in 1.0 M hydrochloric acid (HCl) solution. Corrosion rates of the coated specimens after heat treatment also were studied. The observed corrosion characteristics were explained by the mixed-potential theory.

  3. Field Notebook and Specimen Catalog, Numbers 1101-1707 [2468] (1935-1936)

    E-Print Network [OSTI]

    Davis, William B.

    2012-04-09T23:59:59.000Z

    Field Uotes of W. B. Davis 1935 California-Idaho pp. 313-454. F 455-509 Field Nos. 110l-i58l j 1582-1707 All specimens from Idaho in M.V.Z. _________ 5S9I - ? . . ' - ' . ? . - - . . ? , i o e ldU ::,'oce II/. W.B. Davis l935 1101....) Feb. 9, 1935. 1105? Peromyscus c. parasiticus (2 ^*^b x 33) 274-140-27-24 1106? Peromyscus t . gilberti (pregnant but embs. too small to measure) 195-92-25-21 Grizzly Peak, l-? mi. EKE Berkeley, Alameda Co., Calif. Feb. 16, 1107

  4. Micromachine friction test apparatus

    DOE Patents [OSTI]

    deBoer, Maarten P. (Albuquerque, NM); Redmond, James M. (Albuquerque, NM); Michalske, Terry A. (Cedar Crest, NM)

    2002-01-01T23:59:59.000Z

    A microelectromechanical (MEM) friction test apparatus is disclosed for determining static or dynamic friction in MEM devices. The friction test apparatus, formed by surface micromachining, is based on a friction pad supported at one end of a cantilevered beam, with the friction pad overlying a contact pad formed on the substrate. A first electrostatic actuator can be used to bring a lower surface of the friction pad into contact with an upper surface of the contact pad with a controlled and adjustable force of contact. A second electrostatic actuator can then be used to bend the cantilevered beam, thereby shortening its length and generating a relative motion between the two contacting surfaces. The displacement of the cantilevered beam can be measured optically and used to determine the static or dynamic friction, including frictional losses and the coefficient of friction between the surfaces. The test apparatus can also be used to assess the reliability of rubbing surfaces in MEM devices by producing and measuring wear of those surfaces. Finally, the friction test apparatus, which is small in size, can be used as an in situ process quality tool for improving the fabrication of MEM devices.

  5. Material test machine for tension-compression tests at high temperature

    DOE Patents [OSTI]

    Cioletti, Olisse C. (Pittsburgh, PA)

    1988-01-01T23:59:59.000Z

    Apparatus providing a device for testing the properties of material specimens at high temperatures and pressures in controlled water chemistries includes, inter alia, an autoclave housing the specimen which is being tested. The specimen is connected to a pull rod which couples out of the autoclave to an external assembly which includes one or more transducers, a force balance chamber and a piston type actuator. The pull rod feeds through the force balance chamber and is compensated thereby for the pressure conditions existing within the autoclave and tending to eject the pull rod therefrom. The upper end of the push rod is connected to the actuator through elements containing a transducer comprising a linear variable differential transformer (LVDT). The housing and coil assembly of the LVDT is coupled to a tube which runs through a central bore of the pull rod into the autoclave where it is connected to one side of the specimen. The movable core of the LVDT is coupled to a stem which runs through the tube where it is then connected to the other side of the specimen through a coupling member. A transducer in the form of a load cell including one or more strain gages is located on a necked-down portion of the upper part of the pull rod intermediate the LVDT and force balance chamber.

  6. cDNA Microarray Analysis of Serially Sampled Cervical Cancer Specimens From Patients Treated With Thermochemoradiotherapy

    SciTech Connect (OSTI)

    Borkamo, Erling Dahl, E-mail: borkamo@gmail.co [Section of Oncology, Institute of Medicine, University of Bergen, Bergen (Norway); Center for Medical Genetics and Molecular Medicine, Haukeland University Hospital, Bergen (Norway); Schem, Baard-Christian [Department of Oncology and Medical Physics, Haukeland University Hospital, Bergen (Norway); Fluge, Oystein; Bruland, Ove [Center for Medical Genetics and Molecular Medicine, Haukeland University Hospital, Bergen (Norway); Department of Oncology and Medical Physics, Haukeland University Hospital, Bergen (Norway); Dahl, Olav; Mella, Olav [Section of Oncology, Institute of Medicine, University of Bergen, Bergen (Norway); Department of Oncology and Medical Physics, Haukeland University Hospital, Bergen (Norway)

    2009-12-01T23:59:59.000Z

    Purpose: To elucidate changes in gene expression after treatment with regional thermochemoradiotherapy in locally advanced squamous cell cervical cancer. Methods and Materials: Tru-Cut biopsy specimens were serially collected from 16 patients. Microarray gene expression levels before and 24 h after the first and second trimodality treatment sessions were compared. Pathway and network analyses were conducted by use of Ingenuity Pathways Analysis (IPA; Ingenuity Systems, Redwood City, CA). Single gene expressions were analyzed by quantitative real-time reverse transcription-polymerase chain reaction. Results: We detected 53 annotated genes that were differentially expressed after trimodality treatment. Central in the three top networks detected by IPA were interferon alfa, interferon beta, and interferon gamma receptor; nuclear factor kappaB; and tumor necrosis factor, respectively. These genes encode proteins that are important in regulation cell signaling, proliferation, gene expression, and immune stimulation. Biological processes over-represented among the 53 genes were fibrosis, tumorigenesis, and immune response. Conclusions: Microarrays showed minor changes in gene expression after thermochemoradiotherapy in locally advanced cervical cancer. We detected 53 differentially expressed genes, mainly involved in fibrosis, tumorigenesis, and immune response. A limitation with the use of serial biopsy specimens was low quality of ribonucleic acid from tumors that respond to highly effective therapy. Another 'key limitation' is timing of the post-treatment biopsy, because 24 h may be too late to adequately assess the impact of hyperthermia on gene expression.

  7. Surface Decontamination of System Components in Uranium Conversion Plant at KAERI

    SciTech Connect (OSTI)

    Choi, W. K.; Kim, K. N.; Won, H. J.; Jung, C. H.; Oh, W. Z.

    2003-02-25T23:59:59.000Z

    A chemical decontamination process using nitric acid solution was selected as in-situ technology for recycle or release with authorization of a large amount of metallic waste including process system components such as tanks, piping, etc., which is generated by dismantling a retired uranium conversion plant at Korea Atomic Energy Research Institute (KAERI). The applicability of nitric acid solution for surface decontamination of metallic wastes contaminated with uranium compounds was evaluated through the basic research on the dissolution of UO2 and ammonium uranyl carbonate (AUC) powder. Decontamination performance was verified by using the specimens contaminated with such uranium compounds as UO2 and AUC taken from the uranium conversion plant. Dissolution rate of UO2 powder is notably enhanced by the addition of H2O2 as an oxidant even in the condition of a low concentration of nitric acid and low temperature compared with those in a nitric acid solution without H2O2. AUC powders dissolve easily in nitric acid solutions until the solution pH attains about 2.5 {approx} 3. Above that solution pH, however, the uranium concentration in the solution is lowered drastically by precipitation as a form of U3(NH3)4O9 . 5H2O. Decontamination performance tests for the specimens contaminated with UO2 and AUC were quite successful with the application of decontamination conditions obtained through the basic studies on the dissolution of UO2 and AUC powders.

  8. Standard test method for creep-fatigue crack growth testing

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2010-01-01T23:59:59.000Z

    1.1 This test method covers the determination of creep-fatigue crack growth properties of nominally homogeneous materials by use of pre-cracked compact type, C(T), test specimens subjected to uniaxial cyclic forces. It concerns fatigue cycling with sufficiently long loading/unloading rates or hold-times, or both, to cause creep deformation at the crack tip and the creep deformation be responsible for enhanced crack growth per loading cycle. It is intended as a guide for creep-fatigue testing performed in support of such activities as materials research and development, mechanical design, process and quality control, product performance, and failure analysis. Therefore, this method requires testing of at least two specimens that yield overlapping crack growth rate data. The cyclic conditions responsible for creep-fatigue deformation and enhanced crack growth vary with material and with temperature for a given material. The effects of environment such as time-dependent oxidation in enhancing the crack growth ra...

  9. MODIFICATION OF SURFACE AND TRIBOLOGICAL PROPERTIES OF DLC FILMS BY ADDING SILVER CONTENT

    E-Print Network [OSTI]

    Zhang, Hanshen S.

    2008-01-01T23:59:59.000Z

    image the coatings’ surface topography. Mechanical tests oflayer. The coatings surface topography was measured by AFMAND DISCUSSION The surface topography measured by AFM is

  10. Effect of numerical parameters on characterizing the hardening behavior of ductile uniaxial tension specimens.

    SciTech Connect (OSTI)

    Cordova, Theresa Elena; Dion, Kristin; Laing, John Robert; Corona, Edmundo; Breivik, Nicole L.; Wellman, Gerald William; Shelton, Timothy R.

    2010-11-01T23:59:59.000Z

    Many problems of practical importance involve ductile materials that undergo very large strains, in many cases to the point of failure. Examples include structures subjected to impact or blast loads, energy absorbing devices subjected to significant crushing, cold-forming manufacturing processes and others. One of the most fundamental pieces of data that is required in the analysis of this kind of problems is the fit of the uniaxial stress-strain curve of the material. A series of experiments where mild steel plates were punctured with a conical indenter provided a motivation to characterize the true stress-strain curve until the point of failure of this material, which displayed significant ductility. The hardening curve was obtained using a finite element model of the tensile specimens that included a geometric imperfection in the form of a small reduction in the specimen width to initiate necking. An automated procedure iteratively adjusted the true stress-strain curve fit used as input until the predicted engineering stress-strain curve matched experimental measurements. Whereas the fitting is relatively trivial prior to reaching the ultimate engineering stress, the fit of the softening part of the engineering stress-stain curve is highly dependent on the finite element parameters such as element formulation and initial geometry. Results by two hexahedral elements are compared. The first is a standard, under-integrated, uniform-strain element with hourglass control. The second is a modified selectively-reduced-integration element. In addition, the effects of element size, aspect ratio and hourglass control characteristics are investigated. The effect of adaptively refining the mesh based on the aspect ratio of the deformed elements is also considered. The results of the study indicate that for the plate puncture problem, characterizing the material with the same element formulation and size as used in the plate models is beneficial. On the other hand, using different element formulations, sizes or initial aspect ratios can lead to unreliable results.

  11. Linseed Oil-Based Concrete Surface Treatment -for Building and Highway Structures in

    E-Print Network [OSTI]

    , Linseed Oil-Based Concrete Surface Treatment -for Building and Highway Structures in Hong Kong Y using jour Canadian linseed oil- based sealants on concrete specimens madejrom G30120 and G45120 Keywords: Unseed Oil, Concrete Surface Treatment, Salt Spray Resistance, Carbonation, Bond Strength, Ultra

  12. Leak test fitting

    DOE Patents [OSTI]

    Pickett, Patrick T. (Kettering, OH)

    1981-01-01T23:59:59.000Z

    A hollow fitting for use in gas spectrometry leak testing of conduit joints is divided into two generally symmetrical halves along the axis of the conduit. A clip may quickly and easily fasten and unfasten the halves around the conduit joint under test. Each end of the fitting is sealable with a yieldable material, such as a piece of foam rubber. An orifice is provided in a wall of the fitting for the insertion or detection of helium during testing. One half of the fitting also may be employed to test joints mounted against a surface.

  13. Creep-rupture and fractographic analysis of candidate Stirling engine superalloys tested in air

    SciTech Connect (OSTI)

    Bhattachryya, S.

    1984-03-01T23:59:59.000Z

    The creep-rupture behavior of six candidate Stirling engine iron-base superalloys was determined in air. The alloys tested included four wrought alloys (A-286, INCOLOY Alloy 800H, N-155, and 19-9DL) and two cast alloys (CRM-6D and XF-818). The wrought alloys were evaluated in the form of sheet; the cast alloy specimens were investment cast to shape. The creep-rupture specimens were tested in air for up to 3000 hours over the temperature range 650/sup 0/ to 925/sup 0/C. Microstructural and fractographic aspects of the ruptured specimens are discussed with a few correlational graphical analyses included for XF-818 and 19-9DL. Tests are continuing in 15 MPa hydrogen, and later these data will be correlated with air data and microstructural analysis of the specimens conducted.

  14. Long term materials test program. Preliminary operations plan

    SciTech Connect (OSTI)

    None

    1980-03-01T23:59:59.000Z

    The Long Term Materials Testing (LTMT) PFB facility has been designed to duplicate the design point condition of the Coal-Fired Combined Cycle (CFCC) reference commercial plant design developed by GE under contract to DOE, including bed temperature (1750/sup 0/F), pressure (10 atm), excess air (20%), and gas residence time (1.8 sec). The test rig has a one foot diameter bed and consumes about 1.6 tons/day of coal and 0.5 tons/day of dolomite sulphur sorbent. Material specimens are contained in two test sections. The low velocity test section houses 132 pin specimens 1/4 dia., sixty of which can be cooled below the gas stream temperature. The nominal exposure environment of 1650/sup 0/F, 10 atm, 27 fps should ensure representative corrosive conditions, without erosion. The control system for the LTMT facility is designed to operate the rig in such a manner that the test specimens are subjected to constant, controlled conditions representative of the actual service environment. The Preliminary Test Plan presented in Section V outlines three phases of PFB testing, plus screening tests for candidate materials. Operating costs have been updated to reflect the preliminary rig design data and current raw material quotes. The projected operating costs have been effected by raw material costs since the time of the original estimate, but the overall cost per hour of test is still very low: $122/test hour.

  15. Corrosion testing using isotopes

    DOE Patents [OSTI]

    Hohorst, F.A.

    1995-12-05T23:59:59.000Z

    A method is described for determining the corrosion behavior of a material with respect to a medium in contact with the material by: implanting a substantially chemically inert gas in a matrix so that corrosion experienced by the material causes the inert gas to enter the medium; placing the medium in contact with the material; and measuring the amount of inert gas which enters the medium. A test sample of a material whose resistance to corrosion by a medium is to be tested is described composed of: a body of the material, which body has a surface to be contacted by the medium; and a substantially chemically inert gas implanted into the body to a depth below the surface. A test sample of a material whose resistance to corrosion by a medium is to be tested is described composed of: a substrate of material which is easily corroded by the medium, the substrate having a surface; a substantially chemically inert gas implanted into the substrate; and a sheet of the material whose resistance to corrosion is to be tested, the sheet being disposed against the surface of the substrate and having a defined thickness. 3 figs.

  16. Corrosion testing using isotopes

    DOE Patents [OSTI]

    Hohorst, Frederick A. (Idaho Falls, ID)

    1995-12-05T23:59:59.000Z

    A method for determining the corrosion behavior of a material with respect to a medium in contact with the material by: implanting a substantially chemically inert gas in a matrix so that corrosion experienced by the material causes the inert gas to enter the medium; placing the medium in contact with the material; and measuring the amount of inert gas which enters the medium. A test sample of a material whose resistance to corrosion by a medium is to be tested, composed of: a body of the material, which body has a surface to be contacted by the medium; and a substantially chemically inert gas implanted into the body to a depth below the surface. A test sample of a material whose resistance to corrosion by a medium is to be tested, composed of: a substrate of material which is easily corroded by the medium, the substrate having a surface; a substantially chemically inert gas implanted into the substrate; and a sheet of the material whose resistance to corrosion is to be tested, the sheet being disposed against the surface of the substrate and having a defined thickness.

  17. Disk-shaped Compact Tension Test for Plain Concrete A. Amirkhanian1

    E-Print Network [OSTI]

    Paulino, Glaucio H.

    Disk-shaped Compact Tension Test for Plain Concrete A. Amirkhanian1 , D. Spring1 , J. Roesler1 , K cracking prediction of concrete pavement systems. The single-edge notched beam test has been used energy in asphalt concrete using the disk-shaped compact tension (DCT) test. The benefit of this specimen

  18. TENSILE AND CREEP BEHAVIOR OF GEOSYNTHETICS USING CONFINED-ACCELERATED TESTS

    E-Print Network [OSTI]

    Zornberg, Jorge G.

    TENSILE AND CREEP BEHAVIOR OF GEOSYNTHETICS USING CONFINED-ACCELERATED TESTS COMPORTEMENT EN tensile and creep standard tests are performed with in-isolation specimens, they may not reproduce the possibly significant effect of soil-geosynthetic interaction. A new creep testing machine was recently

  19. Explosives screening on a vehicle surface

    DOE Patents [OSTI]

    Parmeter, John E.; Brusseau, Charles A.; Davis, Jerry D.; Linker, Kevin L.; Hannum, David W.

    2005-02-01T23:59:59.000Z

    A system for detecting particles on the outer surface of a vehicle has a housing capable of being placed in a test position adjacent to, but not in contact with, a portion of the outer surface of the vehicle. An elongate sealing member is fastened to the housing along a perimeter surrounding the wall, and the elongate sealing member has a contact surface facing away from the wall to contact the outer surface of the vehicle to define a test volume when the wall is in the test position. A gas flow system has at least one gas inlet extending through the wall for providing a gas stream against the surface of the vehicle within the test volume. This gas stream, which preferably is air, dislodges particles from the surface of the vehicle covered by the housing. The gas stream exits the test volume through a gas outlet and particles in the stream are detected.

  20. Fatigue Testing of Abrasive Water Jet Cut Titanium

    SciTech Connect (OSTI)

    Hovanski, Yuri; Dahl, Michael E.; Williford, Ralph E.

    2009-06-08T23:59:59.000Z

    Battelle Memorial Institute as part of its U.S. Department of Energy (USDOE) Contract No. DE-AC05-76RL01830 to operate the Pacific Northwest National Laboratory (PNNL) provides technology assistance to qualifying small businesses in association with a Technology Assistance Program (TAP). Qualifying companies are eligible to receive a set quantity of labor associated with specific technical assistance. Having applied for a TAP agreement to assist with fatigue characterization of Abrasive Water Jet (AWJ) cut titanium specimens, the OMAX Corporation was awarded TAP agreement 09-02. This program was specified to cover dynamic testing and analysis of fatigue specimens cut from titanium alloy Ti-6%Al-4%V via AWJ technologies. In association with the TAP agreement, a best effort agreement was made to characterize fatigue specimens based on test conditions supplied by OMAX.

  1. Mechanical Testing of TR-55 Rubber Thermally Aged Under Tensile Strain

    SciTech Connect (OSTI)

    Small IV, W; Alviso, C T; Wilson, T S; Chinn, S C; Maxwell, R S

    2009-03-10T23:59:59.000Z

    TR-55 rubber specimens were previously subjected to an aging process consisting of the application of a tensile strain of approximately 67%, 100%, 133%, or 167% elongation for 4, 8, 12, or 16 h at either 250 C or room temperature. Control specimens at the same temperatures/durations were not subjected to tensile strain. The specimens were allowed to recover at room temperature without external stimuli for over 100 days before tensile testing. A single dog bone was cut from each specimen and a stress-strain curve was obtained. The elastic modulus of each specimen was calculated. Specimens aged under tensile strain exhibited rubber-like behavior dependent on the aging elongation and duration. This behavior was not evident in the unstrained controls. For the unstrained controls, exposure to 250 C resulted in an increase in modulus relative to the unheated material independent of the heating duration. The tensile strain applied during the aging process caused a reduction in modulus relative to the controls; lower moduli were observed for the shorter aging durations. Slippage of the specimens in the grips prevented determination of ultimate strength, as all specimens either slipped completely out of the grip before failure or failed at the original grip edge after slipping.

  2. Acoustic Emission and Guided Wave Monitoring of Fatigue Crack Growth on a Full Pipe Specimen

    SciTech Connect (OSTI)

    Meyer, Ryan M.; Cumblidge, Stephen E.; Ramuhalli, Pradeep; Watson, Bruce E.; Doctor, Steven R.; Bond, Leonard J.

    2011-05-06T23:59:59.000Z

    Continuous on-line monitoring of active and passive systems, structures and components in nuclear power plants will be critical to extending the lifetimes of nuclear power plants in the US beyond 60 years. Acoustic emission and guided ultrasonic waves are two tools for continuously monitoring passive systems, structures and components within nuclear power plants and are the focus of this study. These tools are used to monitor fatigue damage induced in a SA 312 TP304 stainless steel pipe specimen. The results of acoustic emission monitoring indicate that crack propagation signals were not directly detected. However, acoustic emission monitoring exposed crack formation prior to visual confirmation through the detection of signals caused by crack closure friction. The results of guided ultrasonic wave monitoring indicate that this technology is sensitive to the presence and size of cracks. The sensitivity and complexity of GUW signals is observed to vary with respect to signal frequency and path traveled by the guided ultrasonic wave relative to the crack orientation.

  3. High Strain Rate Tensile Testing of DOP-26 Iridium

    SciTech Connect (OSTI)

    Schneibel, Joachim H [ORNL; Carmichael Jr, Cecil Albert [ORNL; George, Easo P [ORNL

    2007-11-01T23:59:59.000Z

    The iridium alloy DOP-26 was developed through the Radioisotope Power Systems Program in the Office of Nuclear Energy of the Department of Energy. It is used for clad vent set cups containing radioactive fuel in radioisotope thermoelectric generator (RTG) heat sources which provide electric power for spacecraft. This report describes mechanical testing results for DOP-26. Specimens were given a vacuum recrystallization anneal of 1 hour at 1375 C and tested in tension in orientations parallel and perpendicular to the rolling direction of the sheet from which they were fabricated. The tests were performed at temperatures ranging from room temperature to 1090 C and strain rates ranging from 1 x 10{sup -3} to 50 s{sup -1}. Room temperature testing was performed in air, while testing at elevated temperatures was performed in a vacuum better than 1 x 10{sup -4} Torr. The yield stress (YS) and the ultimate tensile stress (UTS) decreased with increasing temperature and increased with increasing strain rate. Between 600 and 1090 C, the ductility showed a slight increase with increasing temperature. Within the scatter of the data, the ductility did not depend on the strain rate. The reduction in area (RA), on the other hand, decreased with increasing strain rate. The YS and UTS values did not differ significantly for the longitudinal and transverse specimens. The ductility and RA values of the transverse specimens were marginally lower than those of the longitudinal specimens.

  4. Programmable surfaces

    E-Print Network [OSTI]

    Sun, Amy (Amy Teh-Yu)

    2012-01-01T23:59:59.000Z

    Robotic vehicles walk on legs, roll on wheels, are pulled by tracks, pushed by propellers, lifted by wings, and steered by rudders. All of these systems share the common character of momentum transport across their surfaces. ...

  5. Inverse problem for the identification of Chaos representa-tions of random fields using experimental vibrational tests

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    to be identified by using an experimental database constituted of vibrational tests related to 100 speci- mens in the frequency band [0-50]kHz. There are 60 sensors measuring accelerations. All the specimens are excited

  6. INFLUENCE OF SPECIMEN DESIGN ON THE DEFORMATION AND FAILURE OF ZIRCALOY CLADDING

    E-Print Network [OSTI]

    Motta, Arthur T.

    In a reactivity-initiated accident (RIA), a control rod ejection or drop causes a sudden increase in reactor power. Currently, there is no consensus as to the exact nature of the loading on the cladding during an RIA considerable interest and effort in supplementing integral RIA tests with separate-effects ring tests

  7. Report Number 1: Metallurgical characterization of the HAZ in A516-70 and evaluation of fracture toughness specimens

    SciTech Connect (OSTI)

    Lundin, C.D.; Zhou, G.; Khan, K.K.

    1995-07-01T23:59:59.000Z

    An extensive study has been conducted on A516 grade 70 steel to investigate the effect of shallow cracks in weldment HAZs. Charpy V-notch (CVN) and crack-tip opening displacement (CTOD) tests were utilized to characterize the fracture toughness behavior of the heat-affected zone (HAZ) of A516-70 SMAW weldments. The test results are explained on the basis of microstructural features in the HAZ and fractographic examination. Optical light microscopy (OLM) and scanning electron microscopy (SEM) were used for these evaluations. A computer-assisted imaging system was also utilized and it proved to be a powerful tool for fracture surface analysis. It was evident from the testing of thermally simulated HAZs of A516-70, that the CGHAZ has the lowest toughness. The need for welding techniques to create actual weld HAZs without an influence from secondary weld passes was addressed during the course of this investigation. A welding procedure was developed which is capable of producing ``singular`` HAZs in actual welds. The ``singular`` HAZ technique produced a non-overlapped continuous HAZ through the full plate thickness. A good correlation was found between thermally simulated HAZ behavior and ``singular`` HAZ behavior in terms of fracture toughness, hardness and microstructure.

  8. RMOTC - Testing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Sale of Equipment and Materials DOE to Sell NPR-3 Testing Tomorrow's Technology Today RMOTC - Testing - From Lab to Industry, Moving Your Ideas Forward RMOTC provides a neutral,...

  9. Phyllosilicates In this lab you will examine specimens of the phyllosilicate or sheet silicate minerals. In regard to

    E-Print Network [OSTI]

    Dundas, Robert G.

    Phyllosilicates In this lab you will examine specimens of the phyllosilicate or sheet silicate, you should simply know that they are hydrous alumino-silicates (Al will substitute for Si) and you- silicate with K, Mg and Fe". Mineral formulae are provided for convenience. Phyllosilicates Serpentine

  10. 6 TRANSPORTATION OF SPECIMENS All samples to be transported should be packaged in heavy-duty containers and should comply

    E-Print Network [OSTI]

    Marsh, Helene

    plastic bags (see Webb 1998). Place samples in a strong insulated container or cardboard box. Addresses-duty containers and should comply with the appropriate local protocol. It is important that all agencies involved with tape and enclosed in sealed plastic bags. Specimens can also be sent wrapped; place tissues in paper

  11. Effect of Specimen Conditioning on Geosynthetic Clay Liner Shear J.S. McCartney & J.G. Zornberg

    E-Print Network [OSTI]

    Zornberg, Jorge G.

    635 Effect of Specimen Conditioning on Geosynthetic Clay Liner Shear Strength J.S. McCartney & J of geosynthetic clay liners (GCLs) must replicate field conditions while still accounting for time and cost to conditioning. 1 INTRODUCTION Geosynthetic clay liners (GCLs) are prefabricated geocomposite materials used

  12. amplification tests naats: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Actuators. Open Access Theses and Dissertations Summary: ??This document outlines the design, development and testing of an adaptive flutter test surface utilizing low net passive...

  13. Charpy impact test results for low activation ferritic alloys irradiated to 30 dpa

    SciTech Connect (OSTI)

    Schubert, L.E.; Hamilton, M.L.; Gelles, D.S. [Pacific Northwest National Laboratory, Richland, WA (United States)

    1996-04-01T23:59:59.000Z

    Miniature specimens of six low activation ferritic alloys have been impact field tested following irradiation at 370{degrees}C to 30 dpa. Comparison of the results with those of control specimens and specimens irradiated to 10 dpa indicates that degradation in the impact behavior appears to have saturated by {approx}10 dpa in at least four of these alloys. The 7.5Cr-2W alloy referred to as GA3X appears most promising for further consideration as a candidate structural material in fusion reactor applications, although the 9Cr-1V alloy may also warrant further investigation.

  14. Reversible Bending Fatigue Testing on Zry-4 Surrogate Rods

    SciTech Connect (OSTI)

    Wang, Jy-An John [ORNL; Wang, Hong [ORNL; Bevard, Bruce Balkcom [ORNL; Howard, Rob L [ORNL

    2014-01-01T23:59:59.000Z

    Testing high-burnup spent nuclear fuel (SNF) presents many challenges in areas such as specimen preparation, specimen installation, mechanical loading, load control, measurements, data acquisition, and specimen disposal because these tasks are complicated by the radioactivity of the test specimens. Research and comparison studies conducted at Oak Ridge National Laboratory (ORNL) resulted in a new concept in 2010 for a U-frame testing setup on which to perform hot-cell reversible bending fatigue testing. Subsequently, the three-dimensional finite element analysis and the engineering design of components were completed. In 2013 the ORNL team finalized the upgrade of the U-frame testing setup and the integration of the U-frame setup into a Bose dual linear motor test bench to develop a cyclic integrated reversible-bending fatigue tester (CIRFT). A final check was conducted on the CIRFT test system in August 2013, and the CIRFT was installed in the hot cell in September 2013 to evaluate both the static and dynamic mechanical response of SNF rods under simulated loads. The fatigue responses of Zircaloy-4 (Zry-4) cladding and the role of pellet pellet and pellet clad interactions are critical to SNF vibration integrity, but such data are not available due to the unavailability of an effective testing system. While the deployment of the developed CIRFT test system in a hot cell will provide the opportunity to generate the data, the use of a surrogate rod has proven quite effective in identifying the underlying deformation mechanism of an SNF composite rod under an equivalent loading condition. This paper presents the experimental results of using surrogate rods under CIRFT reversible cyclic loading. Specifically, monotonic and cyclic bending tests were conducted on surrogate rods made of a Zry-4 tube and alumina pellet inserts, both with and without an epoxy bond.

  15. Structural Testing at the Micro and Nano Scales: Breaking

    E-Print Network [OSTI]

    Ballarini, Roberto

    Structural Testing at the Micro and Nano Scales: Breaking Invisible Specimens With Zero Force). "Nano measurements with micro devices: mechanical properties of hydrated collagen fibrils," J. of the R tangential slots · Fuel swirls in the spin chamber and exits through the orifice in a hollow conical spray

  16. CORROSION PERFORMANCE OF EPOXY-COATED REINFORCEMENTBEAM TESTS

    E-Print Network [OSTI]

    Texas at Austin, University of

    CORROSION PERFORMANCE OF EPOXY-COATED REINFORCEMENT­BEAM TESTS by Khaled Z. Kahhaleh, Enrique Vaca which simulate a highly corrosive environment and under loading conditions producing concrete cracking was intended to produce a very aggressive environment and to accelerate corrosion of the specimens. The state

  17. Comparative surface and nano-tribological characteristics of nanocomposite diamond-like carbon thin films doped by silver

    E-Print Network [OSTI]

    Zhang, Han-Shen

    2008-01-01T23:59:59.000Z

    the average. The surface topography was measured by AFM (evaluation of the surface topography, the centerlineto characterize the surface topography; and mechanical tests

  18. Surface Soil

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level:Energy: Grid Integration Redefining What'sis Taking Over Our InstagramStructure ofIndustrialSupportingAlbedo at theSurface Soil Surface Soil

  19. Effects of variations in rate of temperature rise, curing temperature and size of specimen on selected physical properties of concrete made with type III cement and steam cured at atmospheric pressure

    E-Print Network [OSTI]

    Aldridge, Weldon Wayne

    1958-01-01T23:59:59.000Z

    made with Type III Portland cement, 2. to determine the interrelationships of the physical pro- perties of the steam cured concrete as exhibited by the variation in size of the test specimens, 3. to compare certain physical properties of steam cured... it was believed that Type III Portland cement would respond favorably, to temperatures 1n the higher ranges. Due to this same reasoning the rate of temperature rise was varied between 40 F, 60o F and 80 F per hour. These oombinations of curing temperature...

  20. AiR surface: AiR surface 1

    E-Print Network [OSTI]

    Tanaka, Jiro

    AiR surface: 1 PDA AiR surface 1 1: AiR surface () () 2 [1] [2] 3 AiR surface AiR surface surface surface surface 3.1 surface [3]( 3 ) surface 3.2 surface surface AiR surface 4 AiR surface surface AiR surface: Virtual Touch Panel

  1. Enhancement of La0.6Sr0.4Co0.2Fe0.8O3-? Durability and Surface Electro-catalytic Activity by La0.85Sr0.15MnO3-? Investigated using a New Test Electrode Platform

    SciTech Connect (OSTI)

    Lynch, Matthew; Yang, Lei; Qin, Wentao; Choi, Jongjin; Liu, Mingfei; Blinn, Kevin; Liu, Meilin

    2011-01-01T23:59:59.000Z

    A carefully designed test cell platform with a new electrode structure is utilized to determine the intrinsic surface catalytic properties of an electrode. With this design, the electrocatalytic activity and stability of an La{sub 0.6}Sr{sub 0.4}Co{sub 0.2}Fe{sub 0.8}O{sub 3??} (LSCF) cathode is enhanced by a dense thin La{sub 0.85}Sr{sub 0.15}MnO{sub 3±?} (LSM) coating, suggesting that an efficient electrode architecture has been demonstrated that can make effective use of desirable properties of two different materials: fast ionic and electronic transport in the backbone (LSCF) and facile surface kinetics on the thin-film coating (LSM). Theoretical analyses suggest that the enhanced electrocatalytic activity of LSM-coated LSCF is attributed possibly to surface activation under cathodic polarization due to the promotion of oxygen adsorption and/or dissociation by the surface layer and the dramatically increased oxygen vacancy population in the surface film. Further, the observed time-dependent activation over a few hundreds of hours and durability are likely associated with the formation of a favorable hybrid surface phase intermediate between LSM and LSCF. This efficient electrode architecture was successfully applied to the state-of-the-art LSCF-based cathodes by a simple solution infiltration process, achieving reduced interfacial resistance and improved stability under fuel cell operating conditions.

  2. Test quality

    SciTech Connect (OSTI)

    Hartley, R.S. [EG and G Idaho, Inc., Idaho Falls, ID (United States); Keller, A.E. [Nuclear Regulatory Commission, Washington, DC (United States)

    1992-09-01T23:59:59.000Z

    This document discusses inservice testing of safety-related components at nuclear power plants which is performed under the American Society of Mechanical Engineers Boiler and Pressure Vessel Code (the Code). Subsections IWP and IWV of Section XI of the Code state test method and frequency requirements for pumps and valves respectively. Tests vary greatly in quality and frequency. This paper explores the concept of test quality and its relationship with operational readiness and preventive maintenance. This paper also considers the frequencies of component testing. Test quality is related to a test`s ability to detect degradation that can cause component failure. The quality of the test depends on several factors, including specific parameters measured, system or component conditions, and instrument accuracy. The quality of some currently required tests for check valves, motor-operated valves, and pumps is also discussed. Suggestions are made to improve test quality by measuring different parameters, testing valves under load, and testing positive displacement pumps at high pressure and centrifugal pumps at high flow rate conditions. These suggestions can help to improve the level of assurance of component operational readiness gained from testing.

  3. Materials testing at the Hanna-IV and Hoe Creek-III in situ coal-gasification sites

    SciTech Connect (OSTI)

    Loop, R.B.; LaRue, D.M.

    1981-03-01T23:59:59.000Z

    Candidate structural alloys were exposed to the direct product gas stream during three different in situ coal gasification experiments at two sites. Physical appearance and chemical analysis indicate that the coating on the specimens following exposure is typical of condensed hydrocarbons, coal char, coal ash, and mineral particles from the overburden. Deposits on specimens from one test had a fairly high concentration of sulfur (about 8 w/o) while the others had very low sulfur concentrations (0.313 w/o and 0.014 w/o, respectively). Energy-dispersive x-ray spectra indicate that corrosion occurred principally by oxidation, with some sulfidation. Mean penetration rates expressed in millimetres/year were calculated from weight loss data. No material evaluated showed a truly unacceptable degradation. There was no consistent difference in the amount of material removed from specimens with or without welds. Specimens from one test experienced no consistent difference in material removal between different exposure angles; a consistent difference in material loss and dents from particle impact indicated that erosion may have occurred in the other two tests. There was no indication of carburization, decarburization, or severe localized attack in the form of pitting or intergranular corrosion on any of the specimens examined. Results obtained for the flame-sprayed 316 SS specimens and one of the Alonized specimens indicated that use of these processes may be questionable in this environment.

  4. Test quality

    SciTech Connect (OSTI)

    Hartley, R.S. (EG and G Idaho, Inc., Idaho Falls, ID (United States)); Keller, A.E. (Nuclear Regulatory Commission, Washington, DC (United States))

    1992-01-01T23:59:59.000Z

    This document discusses inservice testing of safety-related components at nuclear power plants which is performed under the American Society of Mechanical Engineers Boiler and Pressure Vessel Code (the Code). Subsections IWP and IWV of Section XI of the Code state test method and frequency requirements for pumps and valves respectively. Tests vary greatly in quality and frequency. This paper explores the concept of test quality and its relationship with operational readiness and preventive maintenance. This paper also considers the frequencies of component testing. Test quality is related to a test's ability to detect degradation that can cause component failure. The quality of the test depends on several factors, including specific parameters measured, system or component conditions, and instrument accuracy. The quality of some currently required tests for check valves, motor-operated valves, and pumps is also discussed. Suggestions are made to improve test quality by measuring different parameters, testing valves under load, and testing positive displacement pumps at high pressure and centrifugal pumps at high flow rate conditions. These suggestions can help to improve the level of assurance of component operational readiness gained from testing.

  5. Test Images

    E-Print Network [OSTI]

    Test Images. I hope to have a set of test images for the course soon. Some images are available now; some will have to wait until I can find another 100-200

  6. Stress corrosion testing of a superplastically deformed aluminum-lithium alloy

    SciTech Connect (OSTI)

    Srinivasan, M.N. [Lamar Univ., Beaumont, TX (United States). Dept. of Mechanical Engineering

    1998-05-01T23:59:59.000Z

    An investigation was conducted to study the stress corrosion cracking (SCC) tendency of a superplastically deformed aluminum-lithium-based alloy (AA X2094 [UNS A92094]) that had been received in a thermomechanically processed form suitable for dynamic recrystallization. Tensile specimens made from sheets of this material were superplastically deformed at a constant true strain rate of 2 {times} 10{sup {minus}4}/s and a temperature of {approximately}500 C. Specimens then were subjected to stress corrosion testing using the slow strain rate tensile testing (SSRT) technique at a constant initial strain rate of 2 {times} 10{sup {minus}6}/s. Effects of different superplastic deformation variables and stress corrosion testing conditions on the stress-strain relationship of the test specimens were studied.

  7. Clip gage attachment for frictionless measurement of displacement during high-temperature mechanical testing

    DOE Patents [OSTI]

    Alexander, D.J.

    1994-01-04T23:59:59.000Z

    An attachment for placement between a test specimen and a remote clip gage extensometer providing improved fracture toughness tests of materials at elevated temperature is described. Using a cylindrical tube and axial rod in new relationship, the device transfers the displacement signal of the fracture toughness test specimen directly to a clip gage extensometer located outside the high temperature furnace. Virtually frictionless operation is assured by having the test specimen center one end of the rod in one end of the tube, while the clip gage extensometer arms center the other end of the rod in the other end of the tube. By providing positive control over both ends of both rod and tube, the attachment may be operated in orientations other than vertical. 1 figure.

  8. Vehicle brake testing system

    DOE Patents [OSTI]

    Stevens, Samuel S. (Harriman, TN); Hodgson, Jeffrey W. (Lenoir City, TN)

    2002-11-19T23:59:59.000Z

    This invention relates to a force measuring system capable of measuring forces associated with vehicle braking and of evaluating braking performance. The disclosure concerns an invention which comprises a first row of linearly aligned plates, a force bearing surface extending beneath and beside the plates, vertically oriented links and horizontally oriented links connecting each plate to a force bearing surface, a force measuring device in each link, a transducer coupled to each force measuring device, and a computing device coupled to receive an output signal from the transducer indicative of measured force in each force measuring device. The present invention may be used for testing vehicle brake systems.

  9. IFP --Oil & Gas Science and Technology --(Script : 1er specimen) --1 --Oil & Gas Science and Technology --rev. IFP, Vol. xx (2009), No X, pp. 00-00

    E-Print Network [OSTI]

    Boyer, Edmond

    2009-01-01T23:59:59.000Z

    IFP -- Oil & Gas Science and Technology -- (Script : 1er specimen) -- 1 -- Oil & Gas Science2010 Author manuscript, published in "Oil & Gas Science and Technology - Rev. IFP, 65, 3 (2010) 435-444" DOI : 10.2516/ogst/2010007 #12;IFP -- Oil & Gas Science and Technology -- (Script : 1er specimen) -- 2

  10. On some Panamerican Cretaceous crabs (Decapoda: Raninoida) 263 Decapod crustacean specimens recently collected from new and previously reported localities of USA, Mexico, and Colombia, as

    E-Print Network [OSTI]

    Bermingham, Eldredge

    specimens recently collected from new and previously reported localities of USA, Mexico, and Colombia Colombia, Oklahoma and Mexico. Specimens of Cenomanocarcinus vanstraeleni from the Turonian of Mexico and Colombia include features not described previously for this species, such as variation in the shape

  11. Pool boiling on nano-finned surfaces

    E-Print Network [OSTI]

    Sriraman, Sharan Ram

    2008-10-10T23:59:59.000Z

    is explored in this study. Experiments are conducted in a cubical test chamber containing fluoroinert coolant (PF5060, Manufacturer: 3M Co.) as the working fluid. Pool boiling experiments are conducted for saturation and subcooled conditions. Three...). .................................................................................................68 Fig. 19. Plots comparing the heat flux through the enhanced test surfaces (qw”) with the heat flux through the bare test surface (qb”) under 10 °C sub-cooling condition for both nulceate and film boiling regimes. Heat flux data...

  12. Analysis of stress-induced Burgers vector anisotropy in pressurized tube specimens of irradiated ferritic-martensitic steel: JLF-1

    SciTech Connect (OSTI)

    Gelles, D.S. [Pacific Northwest National Lab., Richland, WA (United States); Shibayama, T. [Univ. of Hokkaido, Oarai, Ibaraki (Japan). Inst. for Materials Research

    1998-09-01T23:59:59.000Z

    A procedure for determining the Burgers vector anisotropy in irradiated ferritic steels allowing identification of all a<100> and all a/2<111> dislocations in a region of interest is applied to a pressurized tube specimen of JLF-1 irradiated at 430 C to 14.3 {times} 10{sup 22} n/cm{sup 2} (E > 0.1 MeV) or 61 dpa. Analysis of micrographs indicates large anisotropy in Burgers vector populations develop during irradiation creep.

  13. Investigation of stabilization/solidification for treatment of electric arc furnace dust: Dynamic leaching of monolithic specimens

    SciTech Connect (OSTI)

    Laforest, Guylaine [Centre de Recherche sur les Infrastructures en Beton, Departement de Geologie et de Genie Geologique, Universite Laval, Quebec, Qc, G1K 7P4 (Canada)], E-mail: guylaine.laforest.1@ulaval.ca; Duchesne, Josee [Centre de Recherche sur les Infrastructures en Beton, Departement de Geologie et de Genie Geologique, Universite Laval, Quebec, Qc, G1K 7P4 (Canada)

    2007-12-15T23:59:59.000Z

    Diffusion-controlled leaching of heavy metals (Cr, Ni, Pb and Zn) from electric arc furnace dust treated with ground granulated blast furnace slag (GGBFS) and with ordinary Portland cement (OPC) was evaluated. Monolithic specimens were evaluated under dynamic leaching conditions for 84 days with periodic leachant renewal. The influence of leaching time, nature of the leachant, binder type and the water/solid ratio of the monoliths were investigated. Results obtained showed both binders can immobilize heavy metals in the monoliths under dynamic leaching conditions, with cumulative quantity of leached metal under 0.138 mg (Cr). Alkaline leachant increased metal release from specimens and reducing the water/solid ratio of the monolith allowed for a decrease in the cumulative mass of metals leached. Chemical and mineralogical characterizations indicated that the metals were evenly distributed throughout the specimens for both binders. Decalcification was observed on the OPC monolith border following leaching. This decrease in Ca corresponded to an altered zone (20 {mu}m), identified by scanning electron microscopy. The GGBFS sample did not show an altered zone.

  14. Testing and evaluation of damaged tubular jacket braces 

    E-Print Network [OSTI]

    Moehlman, Scott Alan

    1990-01-01T23:59:59.000Z

    . In addition, crack growth at welded connections may also occur due to corrosion. Due to the high costs and dire consequences of catastrophic failure of an offshore platform, there exists the need to assess the structural integrity of platforms... will be presented. Experimental results of pure compression tests on undamaged, steel, tubular columns were reported by Bouwkamp (1975). Three fabricated electric-weld pipes and four seamless pipe were used for this study. The specimens were tested in pure...

  15. Evaluation of energy release rates in unidirectional double cantilevered beam fracture toughness specimens

    E-Print Network [OSTI]

    Weatherby, Joe Randall

    1982-01-01T23:59:59.000Z

    release rate expression. at locat1ons in the plast1c zone. In the general case, there also exists a zone of failing material, with length u, at the crack tip in which stress cannot be represented by a relation such as (3). F1gure 4 shows the relative... to the Iower crack surface can be wr1tten as u L ~ u L u(x, y) = (u - u ) i + (v - v ) 3 Using matrix notation, Irwin's crack closure integral for a two dimen- sional problem can be written as: SS y, v Ql 54 5 S 4 2 x, u 1 2 Sl 03 (a) S3 y, V...

  16. VAPOR SPACE AND LIQUID/AIR INTERFACECORROSION TESTS

    SciTech Connect (OSTI)

    Zapp, P.; Hoffman, E.

    2009-11-09T23:59:59.000Z

    The phenomena of vapor space corrosion and liquid/air interface corrosion of carbon steel in simulated liquid waste environments have been investigated. Initial experiments have explored the hypothesis that vapor space corrosion may be accelerated by the formation of a corrosive electrolyte on the tank wall by a process of evaporation of relatively warmer waste and condensation of the vapor on the relatively cooler tank wall. Results from initial testing do not support the hypothesis of electrolyte transport by evaporation and condensation. The analysis of the condensate collected by a steel specimen suspended over a 40 C simulated waste solution showed no measurable concentrations of the constituents of the simulated solution and a decrease in pH from 14 in the simulant to 5.3 in the condensate. Liquid/air interface corrosion was studied as a galvanic corrosion system, where steel at the interface undergoes accelerated corrosion while steel in contact with bulk waste is protected. The zero-resistance-ammeter technique was used to measure the current flow between steel specimens immersed in solutions simulating (1) the high-pH bulk liquid waste and (2) the expected low-pH meniscus liquid at the liquid/air interface. Open-circuit potential measurements of the steel specimens were not significantly different in the two solutions, with the result that (1) no consistent galvanic current flow occurred and (2) both the meniscus specimen and bulk specimen were subject to pitting corrosion.

  17. A Scaleless Snake: Tests of the Role of Reptilian Scales in Water Loss and Heat Transfer

    E-Print Network [OSTI]

    Bennett, Albert F.

    A Scaleless Snake: Tests of the Role of Reptilian Scales in Water Loss and Heat Transfer Reprinted: Tests of the Role of Reptilian Scales in Water Loss and Heat Transfer A unique specimen of gopher snake of pulmocutaneous water loss and heat transfer, no difference was observed between the scale- less animal

  18. Interlaboratory comparison of the horizontal pipe insulation test apparatus up to 350{degrees}C

    SciTech Connect (OSTI)

    Whitaker, T.E. [Pabco, Fruita, CO (United States); Graves, R.S. [Oak Ridge National Lab., TN (United States); McElroy, D.L. [McElroy (David L.), Knoxville, TN (United States); Smith, D.R. [National Institute of Standards and Technology, Boulder, CO (United States)

    1993-12-01T23:59:59.000Z

    The purpose of this interlaboratory comparison was to provide information for the precision and bias section in the ASTM Standard Test Method C 335, {open_quotes}Steady-State Heat Transfer Properties of Horizontal Pipe Insulation.{close_quotes} (The text describes the ASTM C 335 test method, the specimens tested and the test protocol). The apparent thermal conductivity of two rigid calcium silicate pipe insulation specimens was measured by eight laboratories. Each laboratory measured both specimens at four different temperatures. The test mean temperatures ranged from 35 to 390{degrees}C. The two standard deviation value for the data ranged from 4.5 to 7.7% and the average value was 6.3%. The statement recommended for the precision and bias statement for Section 13.1.4 of ASTM C 335 is: {open_quotes}Tests performed at seven different laboratories using guarded-end horizontal pipe test apparatus and at one laboratory using an unguarded cylindrical screen test apparatus on two specimens of calcium silicate insulation in the range of mean temperatures from 35 to 390{degree}C did not vary by more than 6.3% (two standard deviations) of the average.{close_quotes}

  19. Standard Test Method for Sandwich Corrosion Test

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2009-01-01T23:59:59.000Z

    1.1 This test method defines the procedure for evaluating the corrosivity of aircraft maintenance chemicals, when present between faying surfaces (sandwich) of aluminum alloys commonly used for aircraft structures. This test method is intended to be used in the qualification and approval of compounds employed in aircraft maintenance operations. 1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information. 1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements appear in Section 9.

  20. Standard test method for determining plane-strain crack-arrest fracture toughness, kIa, of ferritic steels

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2010-01-01T23:59:59.000Z

    1.1 This test method employs a side-grooved, crack-line-wedge-loaded specimen to obtain a rapid run-arrest segment of flat-tensile separation with a nearly straight crack front. This test method provides a static analysis determination of the stress intensity factor at a short time after crack arrest. The estimate is denoted Ka. When certain size requirements are met, the test result provides an estimate, termed KIa, of the plane-strain crack-arrest toughness of the material. 1.2 The specimen size requirements, discussed later, provide for in-plane dimensions large enough to allow the specimen to be modeled by linear elastic analysis. For conditions of plane-strain, a minimum specimen thickness is also required. Both requirements depend upon the crack arrest toughness and the yield strength of the material. A range of specimen sizes may therefore be needed, as specified in this test method. 1.3 If the specimen does not exhibit rapid crack propagation and arrest, Ka cannot be determined. 1.4 The values stat...

  1. Thermo-optical modulation of ultrasonic surface waves for NDE Zhongyu Yan, Peter B. Nagy *

    E-Print Network [OSTI]

    Nagy, Peter B.

    Thermo-optical modulation of ultrasonic surface waves for NDE Zhongyu Yan, Peter B. Nagy 45221-0070, USA Abstract The well-known thermo-elastic effect of laser irradiation can be exploited specimens can be readily de- tected by exploiting this optically induced thermo-elastic modulation during

  2. Three key elements necessary for successful testing

    SciTech Connect (OSTI)

    Ehlig-Economides, C.A.; Hegeman, P. (Schlumberger Oilfield Services, Houston, TX (United States)); Clark, G. (Schlumberger Oilfield Services, Aberdeen (United Kingdom))

    1994-07-25T23:59:59.000Z

    Real-time surface readout during data acquisition, downhole shutting, and appropriate pressure gauges are three key elements for successful well tests. These elements are often overlooked in designing and implementing a successful well test. This second in a series of three articles on well testing shows how these elements affected the testing of an example well. Also reviewed are the capabilities of several new testing tools and techniques.

  3. Evaluation of surface sampling method performance for Bacillus Spores on clean and dirty outdoor surfaces.

    SciTech Connect (OSTI)

    Wilson, Mollye C.; Einfeld, Wayne; Boucher, Raymond M.; Brown, Gary Stephen; Tezak, Matthew Stephen

    2011-06-01T23:59:59.000Z

    Recovery of Bacillus atrophaeous spores from grime-treated and clean surfaces was measured in a controlled chamber study to assess sampling method performance. Outdoor surfaces investigated by wipe and vacuum sampling methods included stainless steel, glass, marble and concrete. Bacillus atrophaeous spores were used as a surrogate for Bacillus anthracis spores in this study designed to assess whether grime-coated surfaces significantly affected surface sampling method performance when compared to clean surfaces. A series of chamber tests were carried out in which known amounts of spores were allowed to gravitationally settle onto both clean and dirty surfaces. Reference coupons were co-located with test coupons in all chamber experiments to provide a quantitative measure of initial surface concentrations of spores on all surfaces, thereby allowing sampling recovery calculations. Results from these tests, carried out under both low and high humidity conditions, show that spore recovery from grime-coated surfaces is the same as or better than spore recovery from clean surfaces. Statistically significant differences between method performance for grime-coated and clean surfaces were observed in only about half of the chamber tests conducted.

  4. Separate effects of surface roughness, wettability and porosity on boiling heat transfer and critical heat flux and optimization of boiling surfaces

    E-Print Network [OSTI]

    O'Hanley, Harrison Fagan

    2012-01-01T23:59:59.000Z

    The separate effects of surface wettability, porosity, and roughness on critical heat flux (CHF) and heat transfer coefficient (HTC) were examined using carefully-engineered surfaces. All test surfaces were prepared on ...

  5. SUPER HARD SURFACED POLYMERS

    SciTech Connect (OSTI)

    Mansur, Louis K [ORNL] [ORNL; Bhattacharya, R [UES, Incorporated, Dayton, OH] [UES, Incorporated, Dayton, OH; Blau, Peter Julian [ORNL] [ORNL; Clemons, Art [ORNL] [ORNL; Eberle, Cliff [ORNL] [ORNL; Evans, H B [UES, Incorporated, Dayton, OH] [UES, Incorporated, Dayton, OH; Janke, Christopher James [ORNL] [ORNL; Jolly, Brian C [ORNL] [ORNL; Lee, E H [Consultant, Milpitas, CA] [Consultant, Milpitas, CA; Leonard, Keith J [ORNL] [ORNL; Trejo, Rosa M [ORNL] [ORNL; Rivard, John D [ORNL] [ORNL

    2010-01-01T23:59:59.000Z

    High energy ion beam surface treatments were applied to a selected group of polymers. Of the six materials in the present study, four were thermoplastics (polycarbonate, polyethylene, polyethylene terephthalate, and polystyrene) and two were thermosets (epoxy and polyimide). The particular epoxy evaluated in this work is one of the resins used in formulating fiber reinforced composites for military helicopter blades. Measures of mechanical properties of the near surface regions were obtained by nanoindentation hardness and pin on disk wear. Attempts were also made to measure erosion resistance by particle impact. All materials were hardness tested. Pristine materials were very soft, having values in the range of approximately 0.1 to 0.5 GPa. Ion beam treatment increased hardness by up to 50 times compared to untreated materials. For reference, all materials were hardened to values higher than those typical of stainless steels. Wear tests were carried out on three of the materials, PET, PI and epoxy. On the ion beam treated epoxy no wear could be detected, whereas the untreated material showed significant wear.

  6. Estimation of the electron beam-induced specimen heating and the emitted X-rays spatial resolution by Kossel microdiffraction in a scanning

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    by Kossel microdiffraction in a scanning electron microscope Denis Bouscaud n , Rapha¨el Pesci, Sophie Metz, France Keywords: Kossel microdiffraction Scanning electron microscope Lattice parameter Specimen developed inside a Scanning Electron Micro- scope for crystallographic orientation, strain and stress

  7. Advanced Thermal Simulator Testing: Thermal Analysis and Test Results

    SciTech Connect (OSTI)

    Bragg-Sitton, Shannon M.; Dickens, Ricky; Dixon, David; Reid, Robert; Adams, Mike; Davis, Joe [NASA Marshall Space Flight Center, Nuclear Systems Branch/ER24, MSFC, AL 35812 (United States)

    2008-01-21T23:59:59.000Z

    Work at the NASA Marshall Space Flight Center seeks to develop high fidelity, electrically heated thermal simulators that represent fuel elements in a nuclear reactor design to support non-nuclear testing applicable to the potential development of a space nuclear power or propulsion system. Comparison between the fuel pins and thermal simulators is made at the outer fuel clad surface, which corresponds to the outer sheath surface in the thermal simulator. The thermal simulators that are currently being tested correspond to a liquid metal cooled reactor design that could be applied for Lunar surface power. These simulators are designed to meet the geometric and power requirements of a proposed surface power reactor design, accommodate testing of various axial power profiles, and incorporate imbedded instrumentation. This paper reports the results of thermal simulator analysis and testing in a bare element configuration, which does not incorporate active heat removal, and testing in a water-cooled calorimeter designed to mimic the heat removal that would be experienced in a reactor core.

  8. Pool boiling on nano-finned surfaces

    E-Print Network [OSTI]

    Sriraman, Sharan Ram

    2009-05-15T23:59:59.000Z

    The effect of nano-structured surfaces on pool boiling heat transfer is explored in this study. Experiments are conducted in a cubical test chamber containing fluoroinert coolant (PF5060, Manufacturer: 3M Co.) as the working fluid. Pool boiling...

  9. Test Comparability

    E-Print Network [OSTI]

    Keller, Christine; Shulenburger, David E.

    2010-01-01T23:59:59.000Z

    KU ScholarWorks | http://kuscholarworks.ku.edu Test Comparability 2010 by Christine Keller and David Shulenburger This work has been made available by the University of Kansas Libraries’ Office of Scholarly Communication and Copyright. Please... and Shulenburger, David. “Test comparability,” with Christine Keller in the Letters section of Change, September/October 2010, p. 6. Published version: http://www.changemag.org/Archives/Back%20 Issues/September-October%202010/letters-to-editor.html Terms of Use...

  10. Test Automation Ant JUnit Test Automation

    E-Print Network [OSTI]

    Mousavi, Mohammad

    Test Automation Ant JUnit Test Automation Mohammad Mousavi Eindhoven University of Technology, The Netherlands Software Testing 2012 Mousavi: Test Automation #12;Test Automation Ant JUnit Outline Test Automation Ant JUnit Mousavi: Test Automation #12;Test Automation Ant JUnit Why? Challenges of Manual Testing

  11. Tests for the Expansion of the Universe

    E-Print Network [OSTI]

    Martin Lopez-Corredoira

    2015-01-07T23:59:59.000Z

    Almost all cosmologists accept nowadays that the redshift of the galaxies is due to the expansion of the Universe (cosmological redshift), plus some Doppler effect of peculiar motions, but can we be sure of this fact by means of some other independent cosmological test? Here I will review some recent tests: CMBR temperature versus redshift, time dilation, the Hubble diagram, the Tolman or surface brightness test, the angular size test, the UV surface brightness limit and the Alcock--Paczy\\'nski test. Some tests favour expansion and others favour a static Universe. Almost all the cosmological tests are susceptible to the evolution of galaxies and/or other effects. Tolman or angular size tests need to assume very strong evolution of galaxy sizes to fit the data with the standard cosmology, whereas the Alcock--Paczynski test, an evaluation of the ratio of observed angular size to radial/redshift size, is independent of it.

  12. Tests for the Expansion of the Universe

    E-Print Network [OSTI]

    Lopez-Corredoira, Martin

    2015-01-01T23:59:59.000Z

    Almost all cosmologists accept nowadays that the redshift of the galaxies is due to the expansion of the Universe (cosmological redshift), plus some Doppler effect of peculiar motions, but can we be sure of this fact by means of some other independent cosmological test? Here I will review some recent tests: CMBR temperature versus redshift, time dilation, the Hubble diagram, the Tolman or surface brightness test, the angular size test, the UV surface brightness limit and the Alcock--Paczy\\'nski test. Some tests favour expansion and others favour a static Universe. Almost all the cosmological tests are susceptible to the evolution of galaxies and/or other effects. Tolman or angular size tests need to assume very strong evolution of galaxy sizes to fit the data with the standard cosmology, whereas the Alcock--Paczynski test, an evaluation of the ratio of observed angular size to radial/redshift size, is independent of it.

  13. Progress Letter Report on Bending Fatigue Test System Development for Spent Nuclear Fuel Vibration Integrity Study (Out-of-cell fatigue testing development - Task 2.4)

    SciTech Connect (OSTI)

    Wang, Jy-An John [ORNL; Wang, Hong [ORNL; Cox, Thomas S [ORNL; Baldwin, Charles A [ORNL; Bevard, Bruce Balkcom [ORNL

    2013-08-01T23:59:59.000Z

    Vibration integrity of high burn-up spent nuclear fuel in transportation remains to be a critical component of US nuclear waste management system. The structural evaluation of package for spent fuel transportation eventually will need to see if the content or spent fuel is in a subcritical condition. However, a system for testing and characterizing such spent fuel is still lacking mainly due to the complication involved with dealing radioactive specimens in a hot cell environment. Apparently, the current state-of-the-art in spent fuel research and development is quite far away from the delivery of reliable mechanical property data for the assessment of spent fuels in the transport package evaluation. Under the sponsorship of US NRC, ORNL has taken the challenge in developing a robust testing system for spent fuel in hot cell. An extensive literature survey was carried out and unique requirements of such testing system were identified. The U-frame setup has come to the top among various designs examined for reverse bending fatigue test of spent fuel rod. The U-frame has many features that deserve mentioned here: Easy to install spent fuel rod in test; Less linkages than in conventional bending test setup such as three-point or four-point bending; Target the failure mode relevant to the fracture of spent fuel rod in transportation by focusing on pure bending; The continuous calibrations and modifications resulted in the third generation (3G) U-frame testing setup. Rigid arms are split along the LBB axis at rod sample ends. For each arm, this results in a large arm body and an end piece. Mating halves of bushings were modified into two V-shaped surfaces on which linear roller bearings (LRB) are embedded. The rod specimen is installed into the test fixture through opening and closing slide end-pieces. The 3G apparently has addressed major issues of setup identified in the previous stage and been proven to be eligible to be further pursued in this project. On the other hand, the purchase of universal testing machine or Bose dual LM2 TB was completed and the testing system was delivered to ORNL in August 2012. The preliminary confirmation of the system and on-site training were given by Bose field engineer and regional manager on 8/1-8/2/2012. The calibration of Bose testing system has been performed by ORNL because the integration of ORNL setup into the Bose TestBench occurred after the installation. Major challenge with this process arose from two aspects: 1) the load control involves two load cells, and 2) U-frame setup itself is a non-standard specimen. ORNL has been able to implement the load control through Cycle Indirect along with pinning the U-frame setup. Two meetings with ORNL hot-cell group (November 2012 and January 2013) were held to discuss the potential issues with both epoxy mounting of rigid sleeve and U-frame setup. Many suggestions were provided to make the procedure friendlier to the manipulator in hot cell. Addressing of these suggestions resulted in another cycle of modifications of both vise mold and setup. The initial meeting with ORNL I&C group occurred in November 2012 with regard to the Bose cable modification and design of central panel to integrate the cables and wires. The first round of cable modification and central panel fabrication was completed in February 2012. The testing with the modified cables exhibited substantial noises and the testing system was not shown to be stable. It was believed the cross talk was responsible to the noise, and a central panel with a better grounding and shielding was highly recommended. The central panel has been re-designed and fabricated in March 2013. In the subsequent period, the ORNL made substantial effort to debug the noises with the load cell channel, and to resolve the noises and nonlinearity with RDP LVDTs related to the integration of RDP LVDTs to Bose system. At the same time, ORNL has completed the verification tests of Bose test system, including cycle tests under reversal bending in load control, bending tests under monotonic load, and cycle test

  14. Standard Guide for Conducting Supplemental Surveillance Tests for Nuclear Power Reactor Vessels, E 706 (IH)

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2010-01-01T23:59:59.000Z

    1.1 This guide discusses test procedures that can be used in conjunction with, but not as alternatives to, those required by Practices E185 and E2215 for the surveillance of nuclear reactor vessels. The supplemental mechanical property tests outlined permit the acquisition of additional information on radiation-induced changes in fracture toughness, notch ductility, and yield strength properties of the reactor vessel steels. 1.2 This guide provides recommendations for the preparation of test specimens for irradiation, and identifies special precautions and requirements for reactor surveillance operations and postirradiation test planning. Guidance on data reduction and computational procedures is also given. Reference is made to other ASTM test methods for the physical conduct of specimen tests and for raw data acquisition.

  15. Variations in Charpy impact data evaluated by a round-robin testing program -- A summary

    SciTech Connect (OSTI)

    Lowe, A.L. Jr. [Lowe Associates, Lynchburg, VA (United States)

    1996-12-31T23:59:59.000Z

    A round-robin type test program was designed to quantify some of the variables associated with Charpy impact test data. Each participant tested pre-machined specimens at each of six designated test temperatures. The data were evaluated using several techniques normally used to determine transition region temperatures and upper-shelf energies. These data were interpreted statistically to determine mean values and standard deviations. Variations in data appear to be more a factor of the specimen location within the material than related to test temperature. The variations in the data between the different testing participants were within the limits commonly observed. The expected erosion determining the 30 and 50 ft-lb transition temperatures and the upper-shelf energies were found to be independent of the evaluation technique used.

  16. Surface Energy,Surface Energy, Surface Tension & Shape of CrystalsSurface Tension & Shape of Crystals

    E-Print Network [OSTI]

    Subramaniam, Anandh

    Surface Energy,Surface Energy, Surface Tension & Shape of CrystalsSurface Tension & Shape of shapes of crystals are important: (i) growth shape and (ii) equilibrium shape Surface/interface energy surfaces. The joining of two phases creates an interface. (Two orientations of the same crystalline phase

  17. perature, using a tensile tester and a strain rate of 5 mm min1 samples were tested for each specimen. The results obtained from

    E-Print Network [OSTI]

    Srinivasarao, Mohan

    . Zhang, H. Li, M. Poh, F. Xia, Z. Y. Cheng, H. Xu, C. Huang, Nature 2002, 419, 284. [9] Q. M. Zhang, V. Bharti, X. Zhao, Science 1998, 280, 2101. [10] H. Xu, Z. Y. Cheng, D. Olson, T. Mai, Q. M. Zhang, Appl

  18. Experimental and Numerical Investigation of Pool Boiling Heat Transfer on Engineered Nano-Finned Surfaces

    E-Print Network [OSTI]

    Yang, Hongjoo

    2014-08-10T23:59:59.000Z

    ............................................................................... 69 3.3. Experimental Procedure ................................................................................... 70 3.3.1. Test Surface Assembly ............................................................................. 70 3.3.2. Leakage Test...

  19. Low Temperature Waste Immobilization Testing Vol. I

    SciTech Connect (OSTI)

    Russell, Renee L.; Schweiger, Michael J.; Westsik, Joseph H.; Hrma, Pavel R.; Smith, D. E.; Gallegos, Autumn B.; Telander, Monty R.; Pitman, Stan G.

    2006-09-14T23:59:59.000Z

    The Pacific Northwest National Laboratory (PNNL) is evaluating low-temperature technologies to immobilize mixed radioactive and hazardous waste. Three waste forms—alkali-aluminosilicate hydroceramic cement, “Ceramicrete” phosphate-bonded ceramic, and “DuraLith” alkali-aluminosilicate geopolymer—were selected through a competitive solicitation for fabrication and characterization of waste-form properties. The three contractors prepared their respective waste forms using simulants of a Hanford secondary waste and Idaho sodium bearing waste provided by PNNL and characterized their waste forms with respect to the Toxicity Characteristic Leaching Procedure (TCLP) and compressive strength. The contractors sent specimens to PNNL, and PNNL then conducted durability (American National Standards Institute/American Nuclear Society [ANSI/ANS] 16.1 Leachability Index [LI] and modified Product Consistency Test [PCT]) and compressive strength testing (both irradiated and as-received samples). This report presents the results of these characterization tests.

  20. Round-robin artificial contamination test on high voltage dc insulators

    SciTech Connect (OSTI)

    Naito, K.; Schneider, H.M.

    1995-07-01T23:59:59.000Z

    This paper summarizes the results of a worldwide round-robin test of high voltage dc (HVDC) insulators, which was carried out in six laboratories aiming at standardization of the method for artificial contamination tests on HVDC insulators. Flashover characteristics of three kinds of specimens were evaluated by the clean fog and the salt fog procedures. Sufficient information is now available to allow the preparation of provisional international specifications for artificial contamination testing of HVDC insulators.

  1. Verification Testing Test Driven Development Testing with JUnit Verification

    E-Print Network [OSTI]

    Peters, Dennis

    Verification Testing Test Driven Development Testing with JUnit Verification Any activity should be verified. #12;Verification Testing Test Driven Development Testing with JUnit Approaches to verification 1 Testing 2 Static Analysis · Peer review · Insepction/Walk-through/Structured review · Formal

  2. Surface rheology and interface stability.

    SciTech Connect (OSTI)

    Yaklin, Melissa A.; Cote, Raymond O.; Moffat, Harry K.; Grillet, Anne Mary; Walker, Lynn; Koehler, Timothy P.; Reichert, Matthew D. (Carnegie Mellon University, Pittsburgh, PA); Castaneda, Jaime N.; Mondy, Lisa Ann; Brooks, Carlton, F.

    2010-11-01T23:59:59.000Z

    We have developed a mature laboratory at Sandia to measure interfacial rheology, using a combination of home-built, commercially available, and customized commercial tools. An Interfacial Shear Rheometer (KSV ISR-400) was modified and the software improved to increase sensitivity and reliability. Another shear rheometer, a TA Instruments AR-G2, was equipped with a du Nouey ring, bicone geometry, and a double wall ring. These interfacial attachments were compared to each other and to the ISR. The best results with the AR-G2 were obtained with the du Nouey ring. A Micro-Interfacial Rheometer (MIR) was developed in house to obtain the much higher sensitivity given by a smaller probe. However, it was found to be difficult to apply this technique for highly elastic surfaces. Interfaces also exhibit dilatational rheology when the interface changes area, such as occurs when bubbles grow or shrink. To measure this rheological response we developed a Surface Dilatational Rheometer (SDR), in which changes in surface tension with surface area are measured during the oscillation of the volume of a pendant drop or bubble. All instruments were tested with various surfactant solutions to determine the limitations of each. In addition, foaming capability and foam stability were tested and compared with the rheology data. It was found that there was no clear correlation of surface rheology with foaming/defoaming with different types of surfactants, but, within a family of surfactants, rheology could predict the foam stability. Diffusion of surfactants to the interface and the behavior of polyelectrolytes were two subjects studied with the new equipment. Finally, surface rheological terms were added to a finite element Navier-Stokes solver and preliminary testing of the code completed. Recommendations for improved implementation were given. When completed we plan to use the computations to better interpret the experimental data and account for the effects of the underlying bulk fluid.

  3. Corrosion Test of US Steels in Lead-Bismuth Eutectic (LBE) and Kinetic Modeling of Corrosion in LBE Systems

    E-Print Network [OSTI]

    McDonald, Kirk

    1 Corrosion Test of US Steels in Lead-Bismuth Eutectic (LBE) and Kinetic Modeling of Corrosion Federation Abstract We present the LBE corrosion test results of several US steels, and a preliminary analysis using a kinetic model for corrosion in LBE systems. Tube and rod specimens of austenitic steels

  4. Development of an adaptable coherent x-ray diffraction microscope with the emphasis on imaging hydrated specimens

    SciTech Connect (OSTI)

    Nam, Daewoong [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan) [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Department of Physics, Pohang University of Science and Technology, Pohang 790-784 (Korea, Republic of); Park, Jaehyun; Shimada, Hiroki; Kim, Sangsoo; Kim, Sunam; Kohmura, Yoshiki; Ishikawa, Tetsuya; Song, Changyong [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan)] [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Gallagher-Jones, Marcus [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan) [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Institute of Integrative Biology, University of Liverpool, Liverpool L69 7ZB (United Kingdom)

    2013-11-15T23:59:59.000Z

    This paper describes the development of a versatile coherent x-ray diffraction microscope capable of imaging biological specimens in solution. The microscope is a flexible platform accommodating various conditions, from low vacuum (10{sup ?2} Pa) to helium gas filled ambient pressure. This flexibility greatly expands the application area, from in situ materials science to biology systems in their native state, by significantly relaxing restrictions to the sample environment. The coherent diffraction microscope has been used successfully to image a yeast cell immersed in buffer solution. We believe that the design of this coherent diffraction microscope can be directly adapted to various platforms such as table top soft x-ray laser, synchrotron x-ray sources, and x-ray free electron laser with minor relevant adjustments.

  5. G. M. Koelemay well No. 1, Jefferson County, Texas. Volume I. Completion and testing: testing geopressured geothermal reservoirs in existing wells. Final report

    SciTech Connect (OSTI)

    Not Available

    1980-01-01T23:59:59.000Z

    The acquisition, completion, and testing of a geopressured-geothermal well are described. The following are covered: geology; petrophysics; re-entry and completion operations - test well; drilling and completion operations - disposal well; test objectives; surface testing facilities; pre-test operations; test sequence; test results and analysis; and return of wells and location to operator. (MHR)

  6. Verifying Test Hypotheses -HOL/TestGen Verifying Test Hypotheses -HOL/TestGen

    E-Print Network [OSTI]

    Verifying Test Hypotheses - HOL/TestGen Verifying Test Hypotheses - HOL/TestGen An Experiment in Test and Proof Thomas Malcher January 20, 2014 1 / 20 #12;Verifying Test Hypotheses - HOL/TestGen HOL/TestGen Outline Introduction Test Hypotheses HOL/TestGen - Demo Verifying Test Hypotheses Conclusion 2 / 20 #12

  7. Corrosion testing of a plutonium-loaded lanthanide borosilicate glass made with Frit B.

    SciTech Connect (OSTI)

    Ebert, W. L.; Chemical Engineering

    2006-09-30T23:59:59.000Z

    Laboratory tests were conducted with a lanthanide borosilicate (LaBS) glass made with Frit B and added PuO2 (the glass is referred to herein as Pu LaBS-B glass) to measure the dependence of the glass dissolution rate on pH and temperature. These results are compared with the dependencies used in the Defense HLW Glass Degradation Model that was developed to account for HLW glasses in total system performance assessment (TSPA) calculations for the Yucca Mountain repository to determine if that model can also be used to represent the release of radionuclides from disposed Pu LaBS glass by using either the same parameter values that are used for HLW glasses or parameter values specific for Pu LaBS glass. Tests were conducted by immersing monolithic specimens of Pu LaBS-B glass in six solutions that imposed pH values between about pH 3.5 and pH 11, and then measuring the amounts of glass components released into solution. Tests were conducted at 40, 70, and 90 C for 1, 2, 3, 4, and 5 days at low glass-surface-area-to-solution volume ratios. As intended, these test conditions maintained sufficiently dilute solutions that the impacts of solution feedback effects on the dissolution rates were negligible in most tests. The glass dissolution rates were determined from the concentrations of Si and B measured in the test solutions. The dissolution rates determined from the releases of Si and B were consistent with the 'V' shaped pH dependence that is commonly seen for borosilicate glasses and is included in the Defense HLW Glass Degradation Model. The rate equation in that model (using the coefficients determined for HLW glasses) provides values that are higher than the Pu LaBS-B glass dissolution rates that were measured over the range of pH and temperature values that were studied (i.e., an upper bound). Separate coefficients for the rate expression in acidic and alkaline solutions were also determined from the test results to model Pu LaBS-B glass dissolution directly. The releases of Gd, Hf, and Pu from the glass were also measured. The release of Pu was significantly less than Si at all temperatures and pH values (on a normalized basis). More Gd than Pu or Hf was released from the glass in acidic solutions, but more Pu than Gd or Hf was released in alkaline solutions. Almost all of the released Gd remained in solution in tests conducted in Teflon vessels, whereas about half of the released Pu and Hf became fixed to the Teflon. In tests conducted in Type 304L stainless steel vessels, most of the released Gd, Hf, and Pu became fixed to the steel. The aqueous concentrations of Gd, Hf, and Pu decreased from about 2 x 10{sup -5}, 2 x 10{sup -8}, and 1 x 10{sup -7} M in tests solutions near pH 3.7 to about 1 x 10{sup -9}, 8 x 10{sup -10}, and 1 x 10{sup -8} M in test solutions near pH 10.8, respectively, in the 90 C tests in Teflon vessels (the solutions were not filtered prior to analysis). Vapor hydration tests (VHTs) were conducted at 120 and 200 C with Pu LaBS-B glass and SRL 418 glass, which was made to represent the HLW glass that will be used to macro-encapsulate LaBS glass within the waste form. Some VHTs were conducted with specimens of Pu LaBS-B and SRL 418 glasses that were in contact to study the effect of the solution generated as HLW glass dissolves on the corrosion behavior of Pu LaBS-B glass. Other VHTs were conducted in which the glasses were not in contact. The Pu LaBS-B glass is more durable than the HLW glass under these accelerating test conditions, even when the glasses are in contact. The presence of the SRL 418 glass did not promote the dissolution of the Pu LaBS-B glass significantly. However, Gd, Hf, and Pu were detected in alteration phases formed on the Pu LaBS-B glass surface and in (or on) phases formed by SRL 418 glass degradation, such as analcime. This indicates that Gd, Hf, and Pu were transported from the LaBS glass, through the water film formed on the specimens, and to the SRL 418 glass during the test. The disposition of the PuO{sub 2} inclusion phases as the Pu LaBS-B glass dissolved was not det

  8. Construction and testing of a flue-gas corrosion probe

    SciTech Connect (OSTI)

    Federer, J.I.; McEvers, J.A.

    1990-08-01T23:59:59.000Z

    The selection of suitable materials for industrial, waste-heat- recovery systems requires assessment of corrosion of materials in various flue-gas environments. Such assessments involve exposing candidate materials to high-temperature flue gases and analyzing the effects of the exposure conditions. Because corrosion is related to flue-gas chemical composition and temperature, variations in temperature complicate the determination of corrosion rates and corrosion mechanisms. Conversely, a relatively constant temperature allows a more accurate determination of the effects of exposure conditions. For this reason, controlled-temperature flue-gas corrosion probes were constructed and tested for exposure tests of materials. A prototype probe consisted of a silicon carbide tube specimen, supporting hardware, and instrumentation for controlling temperature by internal heating and cooling. An advanced probe included other tubular specimens. Testing of the probes in an industrial-type furnace at a nominal flue-gas temperature of 1200{degree}C revealed that temperature control was inadequate. The cooling mode imposed a substantial axial-temperature gradient on the specimens; while the heating mode imposed a smaller gradient, the heating capacity was very limited. 10 refs., 10 figs., 2 tabs.

  9. Fracture toughness test results of thermal aged reactor vessel materials

    SciTech Connect (OSTI)

    DeVan, M.J.; Lowe, A.L. Jr. [B and W Nuclear Technologies Inc., Lynchburg, VA (United States). Nuclear Engineering Dept.; Hall, J.B. [Babcock and Wilcox Co., Alliance, OH (United States)

    1996-12-31T23:59:59.000Z

    Thermal-aged surveillance materials consisting of Sa-533, Grade B, Class 1 plate material; SA-508, Class 2 forging material; and 2 Mn-Mo-Ni/Linde 80 weld metals were removed from two commercial reactor pressure vessels. The material from the first reactor vessel received a thermal exposure of approximately 103,000 hours at 282 C, while the material from the second reactor vessel received a thermal exposure of approximately 93,000 hours at 282 C. Tensile and 1/2 T compact fracture toughness specimens were fabricated from these materials and tested. In addition, to examine the effects of annealing, selected thermal-aged and unaged specimens were annealed at 454 C (850 F) and tested. Varying responses in the fracture toughness properties were observed for all materials after exposure to the thermal-aging temperature. The base metal plate had an observed decrease in J-values after its respective aging exposure, while no significant difference in the J-values were observed for the Linde 80 weld metals. No significant difference was seen in the J-data for the aged/annealed materials, but because of the small number of test specimens available, no conclusion could be determined for the response to annealing.

  10. A Practical Test Method for Mode I Fracture Toughness of Adhesive Joints with Dissimilar Substrates

    SciTech Connect (OSTI)

    Boeman, R.G.; Erdman, D.L.; Klett, L.B.; Lomax, R.D.

    1999-09-27T23:59:59.000Z

    A practical test method for determining the mode I fracture toughness of adhesive joints with dissimilar substrates will be discussed. The test method is based on the familiar Double Cantilever Beam (DCB) specimen geometry, but overcomes limitations in existing techniques that preclude their use when testing joints with dissimilar substrates. The test method is applicable to adhesive joints where the two bonded substrates have different flexural rigidities due to geometric and/or material considerations. Two specific features discussed are the use of backing beams to prevent substrate damage and a compliance matching scheme to achieve symmetric loading conditions. The procedure is demonstrated on a modified DCB specimen comprised of SRIM composite and thin-section, e-coat steel substrates bonded with an epoxy adhesive. Results indicate that the test method provides a practical means of characterizing the mode I fracture toughness of joints with dissimilar substrates.

  11. Standard Test Method for Impact Resistance of Monolithic Polycarbonate Sheet by Means of a Falling Weight

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    1995-01-01T23:59:59.000Z

    1.1 This test method covers the determination of the energy required to initiate failure in monolithic polycarbonate sheet material under specified conditions of impact using a free falling weight. 1.2 Two specimen types are defined as follows: 1.2.1 Type A consists of a flat plate test specimen and employs a clamped ring support. 1.2.2 Type B consists of a simply supported three-point loaded beam specimen (Fig. 1) and is recommended for use with material which can not be failed using the Type A specimen. For a maximum drop height of 6.096 m (20 ft) and a maximum drop weight of 22.68 kg (50 lb), virgin polycarbonate greater than 12.70 mm (1/2 in.) thick will probably require use of the Type B specimen. Note 1 - See also ASTM Methods: D 1709, D 2444 and D 3029. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of reg...

  12. Microgrid Testing

    SciTech Connect (OSTI)

    Shirazi, M.; Kroposki, B.

    2012-01-01T23:59:59.000Z

    With the publication of IEEE 1574.4 Guide for Design, Operation, and Integration of Distributed Resource Island Systems with Electric Power Systems, there is an increasing amount of attention on not only the design and operations of microgrids, but also on the proper operation and testing of these systems. This standard provides alternative approaches and good practices for the design, operation, and integration of microgrids. This includes the ability to separate from and reconnect to part of the utility grid while providing power to the islanded power system. This presentation addresses the industry need to develop standardized testing and evaluation procedures for microgrids in order to assure quality operation in the grid connected and islanded modes of operation.

  13. No corrosion caused by coal chlorine found in AFBC pilot scale tests

    SciTech Connect (OSTI)

    Ho, K.; Pan, W.P.; Riley, J.T.; Liu, K.; Smith, S.

    2000-07-01T23:59:59.000Z

    Measurements of deposition and corrosion were made in the freeboard of a 3 m inner diameter pilot scale atmospheric fluidized-bed combustor (AFBC) during seven 1,000-hours tests using coals with chlorine (Cl) contents ranging from 0.026% up to 0.47% and sulfur contents ranging from 0.897{approximately}4.4%. Uncooled coupons of alloys 304, 309, 347 and a cooled tube of A210C medium carbon steel were exposed to the hot flue gases to investigate the effects of different coal compositions on deposition and corrosion behavior, if any. The uncooled coupons were installed at the tope of the freeboard to simulate the superheater tube conditions (1,020--1,100 F surface temperature), while the temperature of the cooled A210C test tube was controlled to match the conditions of the evaporator tubes. Specimens were removed for examination after 250, 500, 750, 1,000 hours of exposure and analyzed for deposit formation and corrosion. No chlorine was found in the corrosion scale or on the metal surfaces after any of the tests. High sulfur contents were found in the outer parts of the deposits, and appeared to be associated with calcium and magnesium suggesting that the fly ash may react further after being deposited on the surface of the metal. It was concluded that the limestone bed in the AFBC not only can capture the sulfur but also can effectively capture chlorine. This effect helps being the Cl in the AFBC flue gas down to a level of <50 ppm which is significantly lower than the 300{approximately}400 ppm expected from combustion of the coal in the absence of limestone. This reduction in chlorine species in the gas phase has possible implications for decreased corrosion problems not only in the freeboard, but also in the cold end of the boiler. No evidence was found in these tests that metal wastage or corrosion was accelerated, either directly or indirectly, by chlorine in the coal.

  14. Reliability Testing of Polysilicon For MEMs Devices

    SciTech Connect (OSTI)

    LaVan, D.A.; Buchheit, T.E.

    1999-04-05T23:59:59.000Z

    Mission critical applications of MEMS devices require knowledge of the distribution in their material properties and long-term reliability of the small-scale structures. This project reports on a new testing program at Sandia to quantify the strength distribution using samples that reflect the dimensions of critical MEMS components. The strength of polysilicon fabricated with Sandia's SUMMiT 4-layer process was successfully measured using samples with gage sections 2.5 {micro}m thick by 1.7 {micro}m wide and lengths of 15 and 25 {micro}m. These tensile specimens have a freely moving pivot on one end that anchors the sample to the silicon die and prevents off axis loading during testing. Each sample is loaded in uniaxial tension by pulling laterally with a flat tipped diamond in a computer-controlled Nanoindenter. The stress-strain curve is calculated using the specimen cross section and gage length dimensions verified by measuring against a standard in the SEM. The first 48 samples had a means strength of 2.24 {+-} 0.35 GPa. Fracture strength measurements grouped into three strength levels, which matched three failure modes observed in post mortem examinations. The seven samples in the highest strength group failed in the gage section (strength of 2.77 {+-} 0.04 GPa), the moderate strength group failed at the gage section fillet and the lowest strength group failed at a dimple in the hub. With this technique, multiple tests can be programmed at one time and performed without operator assistance at a rate of 20-30 per day allowing the collection of significant populations of data. Since the new test geometry has been proven, the project is moving to test the distributions seen from real geometric features typical to MEMS such as the effect of gage length, fracture toughness, bonding between layers, etch holes, dimples and shear of gear teeth.

  15. Linear variable differential transformer (LVDT)-based elongation measurements in Advanced Test Reactor high temperature irradiation testing

    SciTech Connect (OSTI)

    D. L. Knudson; J. L. Rempe

    2012-02-01T23:59:59.000Z

    New materials are being considered for fuel, cladding and structures in next generation and existing nuclear reactors. These materials can undergo significant dimensional and physical changes during high temperature irradiations. Currently, such changes are determined by repeatedly irradiating a specimen for a specified period of time in the Advanced Test Reactor (ATR) and then removing it from the reactor for evaluation. The labor and time to remove, examine and return irradiated samples for each measurement make this approach very expensive. In addition, such techniques provide limited data and may disturb the phenomena of interest. To resolve these issues, an instrumented creep testing capability is being developed for specimens irradiated under pressurized water reactor coolant conditions in the ATR at the Idaho National Laboratory (INL). This paper reports the status of INL efforts to develop this testing capability. In addition to providing an overview of in-pile creep test capabilities available at other test reactors, this paper focuses on efforts to design and evaluate a prototype test rig in an autoclave at INL’s High Temperature Test Laboratory.

  16. Linear variable differential transformer (LVDT)-based elongation measurements in Advanced Test Reactor high temperature irradiation testing

    SciTech Connect (OSTI)

    D. L. Knudson; J. L. Rempe

    2012-02-01T23:59:59.000Z

    New materials are being considered for fuel, cladding, and structures in next generation and existing nuclear reactors. These materials can undergo significant dimensional and physical changes during high temperature irradiations. Currently, such changes are determined by repeatedly irradiating a specimen for a specified period of time in the Advanced Test Reactor (ATR) and then removing it from the reactor for evaluation. The labor and time to remove, examine, and return irradiated samples for each measurement makes this approach very expensive. In addition, such techniques provide limited data and may disturb the phenomena of interest. To resolve these issues, an instrumented creep testing capability is being developed for specimens irradiated in pressurized water reactor (PWR) coolant conditions in the ATR at the Idaho National Laboratory (INL). This paper reports the status of INL efforts to develop this testing capability. In addition to providing an overview of in-pile creep test capabilities available at other test reactors, this paper focuses on efforts to design and evaluate a prototype test rig in an autoclave at INL's High Temperature Test Laboratory (HTTL).

  17. Surface studies on aluminized and thermally oxidized superalloy 690 substrates interacted with simulated nuclear waste and sodium borosilicate melt

    SciTech Connect (OSTI)

    Yusufali, C., E-mail: yusuf@barc.gov.in; Sengupta, P.; Dutta, R. S.; Dey, G. K. [Materials Science Division, Bhabha Atomic Research Centre, Trombay, Mumbai-400085 (India); Kshirsagar, R. J. [High Pressure and Synchrotron Radiation Physics Division, Bhabha Atomic Research Centre, Trombay, Mumbai-400085 (India); Mishra, R. K.; Kaushik, C. P. [Waste Management Division, Bhabha Atomic Research Centre, Trombay, Mumbai-400085 (India)

    2014-04-24T23:59:59.000Z

    Aluminized and thermally oxidized Ni-Cr-Fe based superalloy 690 substrates with Al{sub 2}O{sub 3} layer on top have been exposed in nitrate based environment (simulated high level nuclear liquid waste) at 373 K for 216 hours and sodium borosilicate melt at 1248 K for 192 hours. The surfaces of exposed samples have been characterized by using Electron probe micro-analyzer (EPMA). Elemental X-ray mapping on coated specimen that exposed in simulated nuclear waste solution revealed that the surface is enriched with Ni, Cr and Al. X-ray mapping on surface of the specimen that interacted with sodium borosilicate melt indicated that the surface is composed of Al, Fe, Ni and Cr.

  18. Tensile and impact testing of an HFBR (High Flux Beam Reactor) control rod follower

    SciTech Connect (OSTI)

    Czajkowski, C.J.; Schuster, M.H.; Roberts, T.C.; Milian, L.W.

    1989-08-01T23:59:59.000Z

    The Materials Technology Group of the Department of Nuclear Energy (DNE) at Brookhaven National Laboratory (BNL) undertook a program to machine and test specimens from a control rod follower from the High Flux Beam Reactor (HFBR). Tensile and Charpy impact specimens were machined and tested from non-irradiated aluminum alloys in addition to irradiated 6061-T6 from the HFBR. The tensile test results on irradiated material showed a two-fold increase in tensile strength to a maximum of 100.6 ksi. The impact resistance of the irradiated material showed a six-fold decrease in values (3 in-lb average) compared to similar non-irradiated material. Fracture toughness (K{sub I}) specimens were tested on an unirradiated compositionally and dimensionally similar (to HFBR follower) 6061 T-6 material with K{sub max} values of 24.8 {plus minus} 1.0 Ksi{radical}in (average) being obtained. The report concludes that the specimens produced during the program yielded reproducible and believable results and that proper quality assurance was provided throughout the program. 9 figs., 6 tabs.

  19. Ris-R-1483(EN) Testing procedure for the single fiber

    E-Print Network [OSTI]

    #12;1 Introduction One of the primary objectives in the field of fiber-polymer composites fragmentation test as conducted at the materials research department (AFM) at Risø. The equipment and specimen is the control of the degree of adhesion between the usually more rigid fiber and the relatively ductile polymer

  20. Calibration of Modulation Transfer Function of Surface Profilometers with 1D and 2D Binary Pseudo-random Array Standards

    E-Print Network [OSTI]

    Yashchuk, Valeriy V.

    2009-01-01T23:59:59.000Z

    Grating Standard for Calibration of Surface Profilometers,Calibration of Modulation Transfer Function of Surfaceas a standard test surface for calibration of the modulation

  1. Standard test method for exfoliation corrosion susceptibility in 2XXX and 7XXX Series Aluminum Alloys (EXCO Test)

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2007-01-01T23:59:59.000Z

    1.1 This test method covers a procedure for constant immersion exfoliation corrosion (EXCO) testing of high-strength 2XXX and 7XXX series aluminum alloys. Note 1—This test method was originally developed for research and development purposes; however, it is referenced, in specific material specifications, as applicable for evaluating production material (refer to Section 14 on Precision and Bias). 1.2 This test method applies to all wrought products such as sheet, plate, extrusions, and forgings produced from conventional ingot metallurgy process. 1.3 This test method can be used with any form of specimen or part that can be immersed in the test solution. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  2. A new solid state tritium surface monitor

    SciTech Connect (OSTI)

    Willms, R. S. (Richard Scott); Dogruel, D. (David); Myers, R. (Richard); Farrell, R. (Richard)

    2004-01-01T23:59:59.000Z

    Traditionally the amount of tritium on a surface is determined by swiping the surface with a material such as filter paper and counting the removed tritium by scintillation. While effective, this method can be time consuming, can alter the surface and only measures removable tritium. For a given application each of these considerations may or may not be a disadvantage. A solid state monitor, on the other hand, has the potential to provide rapid analysis, not alter the surface and measure all tritium on a surface. This allure has promoted open wall ion chamber and PIN diode-based tritium surface monitor development, and these techniques have enjoyed certain success. Recently the first tests were performed with an avalanche photodiode (APD) for surface tritium measurement. The tritium surface concentration is determined by placing the APD within a few millimeters of the surface of interest. Beta decay from the surface tritium impacts the APD resulting in amplified current through the diode. Analysis of this signal with a multi-channel analyzer enables counting of beta decay events and determination of the beta energy spectrum. While quite similar in concept to PIN diode based measurements, side-by-side testing showed that the APD provided substantially better counting efficiency. Considerations included count rate, background, sensitivity, stability and effect of ambient light. An important factor in the U.S. for a tritium surface monitor is the ability to measure concentrations down to the 'free release' limit, i.e., the concentration below which items can be removed from radiological control areas. The two limits being used are 10,000 disintegrations per min (dpm)/100 cm{sup 2} and 1,000 dpm/100 cm{sup 2}. Present tests show that the APD is capable of measuring down to 1,000 dpm/100 cm{sup 2} in reasonable count times. Data from this promising technique will be presented in this paper.

  3. Method and Apparatus for Creating a Topography at a Surface

    DOE Patents [OSTI]

    Adams, David P. (Albuquerque, NM); Sinclair, Michael B. (Albuquerque, NM); Mayer, Thomas M. (Albuquerque, NM); Vasile, Michael J. (Albuquerque, NM); Sweatt, William C. (Albuquerque, NM)

    2008-11-11T23:59:59.000Z

    Methods and apparatus whereby an optical interferometer is utilized to monitor and provide feedback control to an integrated energetic particle column, to create desired topographies, including the depth, shape and/or roughness of features, at a surface of a specimen. Energetic particle columns can direct energetic species including, ions, photons and/or neutral particles to a surface to create features having in-plane dimensions on the order of 1 micron, and a height or depth on the order of 1 nanometer. Energetic processes can include subtractive processes such as sputtering, ablation, focused ion beam milling and, additive processes, such as energetic beam induced chemical vapor deposition. The integration of interferometric methods with processing by energetic species offers the ability to create desired topographies at surfaces, including planar and curved shapes.

  4. Impact Tensile Testing of Stainless Steels at Various Temperatures

    SciTech Connect (OSTI)

    D. K. Morton

    2008-03-01T23:59:59.000Z

    Stainless steels are used for the construction of numerous spent nuclear fuel or radioactive material containers that may be subjected to high strains and moderate strain rates during accidental drop events. Mechanical characteristics of these base materials and their welds under dynamic loads in the strain rate range of concern (1 to 300 per second) are not well documented. However, research is being performed at the Idaho National Laboratory to quantify these characteristics. The work presented herein discusses tensile impact testing of dual-marked 304/304L and 316/316L stainless steel material specimens. Both base material and welded material specimens were tested at -20 oF, room temperature, 300 oF, and 600 oF conditions. Utilizing a drop weight impact test machine and 1/4-inch and 1/2-inch thick dog bone-shaped test specimens, a strain rate range of approximately 4 to 40 per second (depending on initial temperature conditions) was achieved. Factors were determined that reflect the amount of increased strain energy the material can absorb due to strain rate effects. Using the factors, elevated true stress-strain curves for these materials at various strain rates and temperatures were generated. By incorporating the strain rate elevated true stress-strain material curves into an inelastic finite element computer program as the defined material input, significant improvement in the accuracy of the computer analyses was attained. However, additional impact testing is necessary to achieve higher strain rates (up to 300 per second) before complete definition of strain rate effects can be made for accidental drop events and other similar energy-limited impulsive loads. This research approach, using impact testing and a total energy analysis methodology to quantify strain rate effects, can be applied to many other materials used in government and industry.

  5. Effect of Land Surface Heterogeneity on Satellite Near-

    E-Print Network [OSTI]

    Walker, Jeff

    in regulating the energy and water balance at the soil surface and it is therefore a crucial variable for many. SMOS will carry an L-band (1.4GHz) microwave radiometer and will provide near-surface soil moisture highly heterogeneous land surface conditions. The principal objectives of this research are to (i) test

  6. LASER CLEANING OF CONTAMINATED PAINTED SURFACES

    SciTech Connect (OSTI)

    Ames A. Grisanti; Charlene R. Crocker; Robert R. Jensen

    1999-11-19T23:59:59.000Z

    Several techniques are available or under development for surface decontamination in nuclear facilities. Each technique has its merits; however, none of them is universally the best choice for all surface decontamination applications. Because of the multitude of factors which influence the environmental and economic aspects of selecting a surface decontamination technique, it is difficult to select the best method in a given situation; an objective basis for comparing techniques is needed. The objective of this project was to develop a software tool for use by personnel selecting a surface decontamination technique. The software incorporates performance data for available surface decontamination techniques. The beta release version of the Surface Decontamination Assistant Software has been completed and has undergone testing at the Energy and Environmental Research Center. Minor modifications to the software were completed, and a final release version of the software is ready to be issued.

  7. Prototype to Test WHY prototype to test

    E-Print Network [OSTI]

    Prinz, Friedrich B.

    Prototype to Test METHOD WHY prototype to test HOW to prototype to test Prototyping to test or design space. The fundamental way you test your prototypes is by letting users experience them and react to them. In creating prototypes to test with users you have the opportunity to examine your solution

  8. SPACE-R thermionic space nuclear power system: Design and technology demonstration. Task 1.5.6, Moderator containment laboratory experiment test plant (CDRL No. 5)

    SciTech Connect (OSTI)

    Not Available

    1993-10-01T23:59:59.000Z

    The preferred moderator being considered for SPACE-R is yttrium hydride encased in beryllium tubes. The baseline beryllium performs a dual function as it acts as a moderator and provides containment for hydrogen. The permeation rate of hydrogen from the hydride through the beryllium shell at the operating temperature is an important factor for the functionality and reliability of the Be-YHx moderator. Hydrogen containment capability of beryllium is comparable to enamel which was used in SNAP and Topaz II reactors. However, limited experimental data base exists for the hydrogen permeation through fabricated beryllium enclosures at high temperature. Permeation of hydrogen in beryllium is strongly affected by surface conditions, thickness of surface oxide, surface and bulk traps, impurity content and microstructure. The objective of this experiment is to determine the permeation rate of hydrogen from yttrium hydride and zirconium hydride through beryllium in the temperature range of 773 K--973 K. In addition, Topaz II type zirconium hydride specimens with and without the proprietary oxide coating canned in stainless steel will be tested to measure the hydrogen permeation rate. The TSET SS-canned ZrHx samples currently at Phillips Laboratory will be used for the latter test with Phillips Laboratory participation at the SPI hydrogen leak test stand. A key technology demonstration of the effectiveness of transferred arc plasma spraying of a 1 mil Molybdenum coating on the Be cladding will be performed. The effectiveness of the Molybdenum coating in preventing any interaction of Be with Stainless Steel in NaK will be assessed and demonstrated.

  9. Single crystal metal wedges for surface acoustic wave propagation

    DOE Patents [OSTI]

    Fisher, Edward S. (Wheaton, IL)

    1982-01-01T23:59:59.000Z

    An ultrasonic testing device has been developed to evaluate flaws and inhomogeneities in the near-surface region of a test material. A metal single crystal wedge is used to generate high frequency Rayleigh surface waves in the test material surface by conversion of a slow velocity, bulk acoustic mode in the wedge into a Rayleigh wave at the metal-wedge test material interface. Particular classes of metals have been found to provide the bulk acoustic modes necessary for production of a surface wave with extremely high frequency and angular collimation. The high frequency allows flaws and inhomogeneities to be examined with greater resolution. The high degree of angular collimation for the outgoing ultrasonic beam permits precision angular location of flaws and inhomogeneities in the test material surface.

  10. Single crystal metal wedges for surface acoustic wave propagation

    DOE Patents [OSTI]

    Fisher, E.S.

    1980-05-09T23:59:59.000Z

    An ultrasonic testing device has been developed to evaluate flaws and inhomogeneities in the near-surface region of a test material. A metal single crystal wedge is used to generate high frequency Rayleigh surface waves in the test material surface by conversion of a slow velocity, bulk acoustic mode in the wedge into a Rayleigh wave at the metal-wedge test material interface. Particular classes of metals have been found to provide the bulk acoustic modes necessary for production of a surface wave with extremely high frequency and angular collimation. The high frequency allows flaws and inhomogeneities to be examined with greater resolution. The high degree of angular collimation for the outgoing ultrasonic beam permits precision angular location of flaws and inhomogeneities in the test material surface.

  11. TESTING AND ANALYSIS OF CAP CONCRETE STRESS AND STRAIN DUE TO SHRINKAGE, CREEP, AND EXPANSION FINAL REPORT

    SciTech Connect (OSTI)

    Guerrero, H.; Restivo, M.

    2011-08-01T23:59:59.000Z

    In-situ decommissioning of Reactors P- and R- at the Savannah River Site will require filling the reactor vessels with a special concrete based on materials such as magnesium phosphate, calcium aluminate or silica fume. Then the reactor vessels will be overlain with an 8 ft. thick layer of Ordinary Portland Cement (OPC) steel reinforced concrete, called the 'Cap Concrete'. The integrity of this protective layer must be assured to last for a sufficiently long period of time to avoid ingress of water into the reactor vessel and possible movement of radioactive contamination into the environment. During drying of this Cap Concrete however, shrinkage strains are set up in the concrete as a result of diffusion and evaporation of water from the top surface. This shrinkage varies with depth in the poured slab due to a non-uniform moisture distribution. This differential shrinkage results in restraint of the upper layers with larger shrinkage by lower layers with lesser displacements. Tensile stresses can develop at the surface from the strain gradients in the bulk slab, which can lead to surface cracking. Further, a mechanism called creep occurs during the curing period or early age produces strains under the action of restraining forces. To investigate the potential for surface cracking, an experimental and analytical program was started under TTQAP SRNL-RP-2009-01184. Slab sections made of Cap Concrete mixture were instrumented with embedded strain gages and relative humidity sensors and tested under controlled environmental conditions of 23 C and relative humidities (RH) of 40% and 80% over a period of 50 days. Calculation methods were also developed for predictions of stress development in the full-scale concrete placement over the reactor vessels. These methods were evaluated by simulating conditions for the test specimens and the calculation results compared to the experimental data. A closely similar test with strain gages was performed by Kim and Lee for a concrete mixture that did not employ humidity sensors and the admixtures used in this program. Yuan and Wan tried to predict the shrinkage strains and stresses in the Kim and Lee experiment, but did not include a creep analysis. Grasley and Lange conducted full restraint load tests on a concrete prism instrumented with humidity sensors over a 7 day curing period. The hypothetical case of full-scale placement of the Cap Concrete was also analyzed using the developed analytical methods. The calculation performed in this report is for scoping purposes only.

  12. The nature thickness pipe element testing method to validate the application of LBB conception

    SciTech Connect (OSTI)

    Vasilchenko, G.S.; Artemyev, V.I.; Merinov, G.N. [and others

    1997-04-01T23:59:59.000Z

    To validate the application of leak before break analysis to the VVER-1000 reactor, a procedure for testing a large-scale specimen on electrohydraulic machinery was developed. Steel pipe with a circular weld and stainless cladding inside was manufactured and large-scale longitudinal cross-sections were cut. The remaining parts of the weld after cut out were used to determination standard tensile mechanical properties, critical temperature of brittlness and for manufacture of compact specimens. Experimental mechanical properties of the weld are summarized.

  13. Double torsion testing and finite element analysis for determining the electric fracture properties of piezoelectric ceramics

    SciTech Connect (OSTI)

    Shindo, Yasuhide; Narita, Fumio; Mikami, Masaru [Department of Materials Processing, Graduate School of Engineering, Tohoku University, Aoba-yama 6-6-02, Sendai 980-8579 (Japan)

    2005-06-01T23:59:59.000Z

    This paper presents the results of an experimental and numerical investigation in electric fracture behavior of composite [Pb(Zr,Ti)O{sub 3}] double torsion (DT) specimens. DT tests were conducted on a commercial piezoelectric ceramic bonded between two metals. Fracture loads under different electric fields were obtained from the experiment. Nonlinear three-dimensional finite element analysis was also employed to calculate the energy release rate for DT specimens based on the exact (permeable) and approximate (impermeable) crack models. The effects of applied electric field and domain switching on the energy release rate are discussed, and the model predictions are compared with the results of the experiments.

  14. Torsion Testing of Diffusion Bonded LIGA Formed Nickel

    SciTech Connect (OSTI)

    Buchheit, T.E.; Christenson, T.R.; Schmale, D.T.

    1999-01-27T23:59:59.000Z

    A test technique has been devised which is suitable for the testing of the bond strength of batch diffusion bonded LIGA or DXRL defined structures. The method uses a torsion tester constructed with the aid of LIGA fabrication and distributed torsion specimens which also make use of the high aspect ratio nature of DXRL based processing. Measurements reveal achieved bond strengths of 130MPa between electroplated nickel with a bond temperature of 450 C at 7 ksi pressure which is a sufficiently low temperature to avoid mechanical strength degradation.

  15. Superheated-steam test of ethylene propylene rubber cables using a simultaneous aging and accident environment

    SciTech Connect (OSTI)

    Bennett, P.R.; St. Clair, S.D.; Gilmore, T.W.

    1986-06-01T23:59:59.000Z

    The superheated-steam test exposed different ethylene propylene rubber (EPR) cables and insulation specimens to simultaneous aging and a 21-day simultaneous accident environment. In addition, some insulation specimens were exposed to five different aging conditions prior to the 21-day simultaneous accident simulation. The purpose of this superheated-steam test (a follow-on to the saturated-steam tests (NUREG/CR-3538)) was to: (1) examine electrical degradation of different configurations of EPR cables; (2) investigate differences between using superheated-steam or saturated-steam at the start of an accident simulation; (3) determine whether the aging technique used in the saturated-steam test induced artificial degradation; and (4) identify the constituents in EPR that affect moisture absorption.

  16. DATE: ____________________ NVLAP LAB CODE: __________________ Test Method

    E-Print Network [OSTI]

    ______ 23/F01 ASTM E84 Surface Burning Characteristics of Building Materials ______ 23/F02 ASTM E906 Heat for Building Construction, (Sec. 14): Racking Load ______ 23/G11 ASTM E72 (Sec. 15) Conducting Strength Tests of Panels for Building Construction (Sec. 15): Racking Load (Wet) ______ 23/G12 ASTM E564 Static Load Test

  17. State DOT: Louisiana State Report Questions on NDT Testing

    E-Print Network [OSTI]

    State DOT: Louisiana State Report Questions on NDT Testing 1. What NDT testing methods for concrete materials, concrete pavements, and overlays are you trying? LADOTD does not test concrete pavements or overlays non-destructively. We do use the surface resistivity meter for non-destructive testing

  18. Testing of Small Graphite Samples for Nuclear Qualification

    SciTech Connect (OSTI)

    Julie Chapman

    2010-11-01T23:59:59.000Z

    Accurately determining the mechanical properties of small irradiated samples is crucial to predicting the behavior of the overal irradiated graphite components within a Very High Temperature Reactor. The sample size allowed in a material test reactor, however, is limited, and this poses some difficulties with respect to mechanical testing. In the case of graphite with a larger grain size, a small sample may exhibit characteristics not representative of the bulk material, leading to inaccuracies in the data. A study to determine a potential size effect on the tensile strength was pursued under the Next Generation Nuclear Plant program. It focuses first on optimizing the tensile testing procedure identified in the American Society for Testing and Materials (ASTM) Standard C 781-08. Once the testing procedure was verified, a size effect was assessed by gradually reducing the diameter of the specimens. By monitoring the material response, a size effect was successfully identified.

  19. Design of the Next Generation Nuclear Plant Graphite Creep Experiments for Irradiation in the Advanced Test Reactor

    SciTech Connect (OSTI)

    S. Blaine Grover

    2009-05-01T23:59:59.000Z

    The United States Department of Energy’s Next Generation Nuclear Plant (NGNP) Program will be irradiating six gas reactor graphite creep experiments in the Advanced Test Reactor (ATR) located at the Idaho National Laboratory (INL). The ATR has a long history of irradiation testing in support of reactor development and the INL has been designated as the new United States Department of Energy’s lead laboratory for nuclear energy development. The ATR is one of the world’s premiere test reactors for performing long term, high flux, and/or large volume irradiation test programs. These graphite irradiations are being accomplished to support development of the next generation reactors in the United States. The graphite experiments will be irradiated over the next six to eight years to support development of a graphite irradiation performance data base on the new nuclear grade graphites now available for use in high temperature gas reactors. The goals of the irradiation experiments are to obtain irradiation performance data at different temperatures and loading conditions to support design of the Next Generation Nuclear Plant Very High Temperature Gas Reactor, as well as other future gas reactors. The experiments will each consist of a single capsule that will contain seven separate stacks of graphite specimens. Six of the specimen stacks will have half of their graphite specimens under a compressive load, while the other half of the specimens will not be subjected to a compressive load during irradiation. The six stacks will be organized into pairs with a different compressive load being applied to the top half of each pair of specimen stacks. The seventh stack will not have a compressive load on the graphite specimens during irradiation. The specimens will be irradiated in an inert sweep gas atmosphere with on-line temperature and compressive load monitoring and control. There will also be the capability of sampling the sweep gas effluent to determine if any oxidation or off-gassing of the specimens occurs during initial start-up of the experiment. The final design phase for the first experiment was completed in September 2008, and the fabrication and assembly of the experiment test train as well as installation and testing of the control and support systems that will monitor and control the experiment during irradiation are being completed in early calendar 2009. The first experiment is scheduled to be ready for insertion in the ATR by April 30, 2009. This paper will discuss the design of the experiment including the test train and the temperature and compressive load monitoring, control, and data collection systems.

  20. Ino-(chain) silicates In this lab you will examine specimens of the inosilicate or chain silicate minerals. You will need to know

    E-Print Network [OSTI]

    Dundas, Robert G.

    Ino- (chain) silicates In this lab you will examine specimens of the inosilicate or chain silicate the elemental constituents. For hornblende, it will be sufficient to know that is a hydrous silicate with very (Single Chain silicates); Pyroxenes come in two categories ­ orthorhombic and monoclinic: 1

  1. Testing and evaluation of grout repaired tubular members

    E-Print Network [OSTI]

    Nunn, John Mansfield

    1992-01-01T23:59:59.000Z

    . 0006 0. 0043 0. 0017 0. 0022 kL/r 97. 3 96. 9 96. 7 77. 4 92. 8 99. 4 97. 1 111. 5 77. 7 F (ksi) 33. 5 33. 4 33. 8 31. 8 31. 8 33. 7 33. 5 26. 0 32. 5 Fu, (ksi) 2. 7 2. 7 2 ' 7 2. 3 2. 3 2. 3 2. 3 2. 3 2. 3 Notes: 1) k.... 110 kl/r 59. 85 50. 03 69. 99 59. 97 50. 24 59. 97 65. 81 Note: (*) indicates the number of specimens tested Table 8. Data from Experimental Research Performed by J. P. Renault and J. P. Quillevere (1990) Specimen No. 5 A 5 B 6 B...

  2. Status of the NGNP graphite creep experiments AGC-1 and AGC-2 irradiated in the advanced test reactor

    SciTech Connect (OSTI)

    S. Blaine Grover

    2014-05-01T23:59:59.000Z

    The United States Department of Energy's Next Generation Nuclear Plant (NGNP) Program will be irradiating six nuclear graphite creep experiments in the Advanced Test Reactor (ATR) located at the Idaho National Laboratory (INL). The graphite experiments will be irradiated over the next six to eight years to support development of a graphite irradiation performance data base on the new nuclear grade graphites now available for use in high temperature gas reactors. The goals of the irradiation experiments are to obtain irradiation performance data, including irradiation creep, at different temperatures and loading conditions to support design of the next generation nuclear plant (NGNP) very high temperature gas reactor, as well as other future gas reactors. The experiments will each consist of a single capsule that will contain six peripheral stacks of graphite specimens, with half of the graphite specimens in each stack under a compressive load, while the other half of the specimens will not be subjected to a compressive load during irradiation. The six peripheral stacks will have three different compressive loads applied to the top half of three diametrically opposite pairs of specimen stacks, while a seventh stack will not have a compressive load. The specimens will be irradiated in an inert sweep gas atmosphere with on-line temperature and compressive load monitoring and control. There will also be sampling the sweep gas effluent to determine if any oxidation or off-gassing of the specimens occurs during irradiation of the experiment.

  3. MECHANICAL TEST LAB CAPABILITIES

    E-Print Network [OSTI]

    MECHANICAL TEST LAB CAPABILITIES · Static and cyclic testing (ASTM and non-standard) · Impact drop testing · Slow-cycle fatigue testing · High temperature testing to 2500°F · ASTM/ Boeing/ SACMA standard testing · Ability to design and fabricate non-standard test fixtures and perform non-standard tests

  4. Surface effects of underground nuclear explosions

    SciTech Connect (OSTI)

    Allen, B.M.; Drellack, S.L. Jr.; Townsend, M.J.

    1997-06-01T23:59:59.000Z

    The effects of nuclear explosions have been observed and studied since the first nuclear test (code named Trinity) on July 16, 1945. Since that first detonation, 1,053 nuclear tests have been conducted by the US, most of which were sited underground at the Nevada Test Site (NTS). The effects of underground nuclear explosions (UNEs) on their surroundings have long been the object of much interest and study, especially for containment, engineering, and treaty verification purposes. One aspect of these explosion-induced phenomena is the disruption or alteration of the near-surface environment, also known as surface effects. This report was prepared at the request of the Los Alamos National Laboratory (LANL), to bring together, correlate, and preserve information and techniques used in the recognition and documentation of surface effects of UNEs. This report has several main sections, including pertinent background information (Section 2.0), descriptions of the different types of surface effects (Section 3.0), discussion of their application and limitations (Section 4.0), an extensive bibliography and glossary (Section 6.0 and Appendix A), and procedures used to document geologic surface effects at the NTS (Appendix C). Because a majority of US surface-effects experience is from the NTS, an overview of pertinent NTS-specific information also is provided in Appendix B. It is not within the scope of this report to explore new relationships among test parameters, physiographic setting, and the types or degree of manifestation of surface effects, but rather to compile, summarize, and capture surface-effects observations and interpretations, as well as documentation procedures and the rationale behind them.

  5. Orion Flight Test Exploration Flight Test-1

    E-Print Network [OSTI]

    Waliser, Duane E.

    Orion Flight Test Exploration Flight Test-1 PRESS KIT/December 2014 www.nasa.gov NP-2014-11-020-JSC National Aeronautics and Space Administration #12;#12;Orion Flight Test December 2014 Contents Section Page ........................................................................................... 28 i #12;Orion Flight Test ii December 2014 #12;Orion Flight Test December 2014 Flight Overview

  6. Test Preparation Options Free Test Prep Websites

    E-Print Network [OSTI]

    Stowell, Michael

    Test Preparation Options Free Test Prep Websites ACT: http: http://www.collegeboard.com/student/testing/sat/prep_one/test.html http://www.number2.com://testprep.princetonreview.com/CourseSearch/Search.aspx?itemCode=17&productType=F&rid=1&zip=803 02 Test Prep Classes Front Range Community College: Classes

  7. Test and Test Equipment Joshua Lottich

    E-Print Network [OSTI]

    Patel, Chintan

    Test and Test Equipment Joshua Lottich CMPE 640 11/23/05 #12;Testing Verifies that manufactured chip meets design specifications. Cannot test for every potential defect. Modeling defects as faults allows for passing and failing of chips. Ideal test would capture all defects and pass only chips

  8. Adaptation of Crack Growth Detection Techniques to US Material Test Reactors

    SciTech Connect (OSTI)

    A. Joseph Palmer; Sebastien P. Teysseyre; Kurt L. Davis; Joy L. Rempe; Gordon Kohse; Yakov Ostrovsky; David M. Carpenter

    2014-04-01T23:59:59.000Z

    A key component in evaluating the ability of Light Water Reactors to operate beyond 60 years is characterizing the degradation of materials exposed to radiation and various water chemistries. Of particular concern is the response of reactor materials to Irradiation Assisted Stress Corrosion Cracking (IASCC). Some materials testing reactors (MTRs) outside the U.S., such as the Halden Boiling Water Reactor (HBWR), have deployed a technique to measure crack growth propagation during irradiation. This technique incorporates a compact loading mechanism to stress the specimen during irradiation. A crack in the specimen is monitored using the Direct Current Potential Drop (DCPD) method. A project is underway to develop and demonstrate the performance of a similar type of test rig for use in U.S. MTRs. The first year of this three year project was devoted to designing, analyzing, fabricating, and bench top testing a mechanism capable of applying a controlled stress to specimens while they are irradiated in a pressurized water loop (simulating PWR reactor conditions). During the second year, the mechanism will be tested in autoclaves containing high pressure, high temperature water with representative water chemistries. In addition, necessary documentation and safety reviews for testing in a reactor environment will be completed. In the third year, the assembly will be tested in the Massachusetts Institute of Technology Reactor (MITR) and Post Irradiation Examinations (PIE) will be performed.

  9. Leaching action of EJ-13 water on unirradiated UO{sub 2} surfaces under unsaturated conditions at 90{degree}C: Interim report

    SciTech Connect (OSTI)

    Wronkiewicz, D.J.; Bates, J.K.; Gerding, T.J.; Veleckis, E.; Tani, B.S.

    1991-07-01T23:59:59.000Z

    A set of experiments, based on the application of the Unsaturated Test method to the reaction of UO{sub 2} with EJ-13 water, has been conducted over a period of 182.5 weeks. One half of the experiments have been terminated, while one half are still ongoing. Solutions that have dripped from UO{sub 2} specimens have been analyzed for all experiments, while the reacted UO{sub 2} surfaces have been examined for only the terminated experiments. A pulse of uranium release from the UO{sub 2} solid, in conjunction with the formation of dehydrated schoepite on the surface of the UO{sub 2}, was observed during the 39- to 96-week period. Thereafter, the uranium release decreased and a second set of secondary phases was observed. The latter phases incorporate cations from the EJ-13 water and include boltwoodite, uranophane, sklodowskite, compreignacite, and schoepite. The experiments are being continued to monitor for additional changes in solution composition and secondary phase formation, and have now reached the 319-week period. 9 refs., 17 figs., 25 tabs.

  10. In-situ Creep Testing Capability Development for Advanced Test Reactor

    SciTech Connect (OSTI)

    B. G. Kim; J. L. Rempe; D. L. Knudson; K. G. Condie; B. H. Sencer

    2010-08-01T23:59:59.000Z

    Creep is the slow, time-dependent strain that occurs in a material under a constant strees (or load) at high temperature. High temperature is a relative term, dependent on the materials being evaluated. A typical creep curve is shown in Figure 1-1. In a creep test, a constant load is applied to a tensile specimen maintained at a constant temperature. Strain is then measured over a period of time. The slope of the curve, identified in the figure below, is the strain rate of the test during Stage II or the creep rate of the material. Primary creep, Stage I, is a period of decreasing creep rate due to work hardening of the material. Primary creep is a period of primarily transient creep. During this period, deformation takes place and the resistance to creep increases until Stage II, Secondary creep. Stage II creep is a period with a roughly constant creep rate. Stage II is referred to as steady-state creep because a balance is achieved between the work hardening and annealing (thermal softening) processes. Tertiary creep, Stage III, occurs when there is a reduction in cross sectional area due to necking or effective reduction in area due to internal void formation; that is, the creep rate increases due to necking of the specimen and the associated increase in local stress.

  11. To cite this version: Pastor, Marie-Laetitia and Garnier, Christian and Pescay, Christophe Comparison of two non destructive tests in carbon/epoxy

    E-Print Network [OSTI]

    Mailhes, Corinne

    Comparison of two non destructive tests in carbon/epoxy composites. (2010) Journal of Materials Science to the applied method. 2. Materials #12;The specimens are carried out from 8 woven plies carbon/epoxy composite administrator: staff-oatao@listes-diff.inp-toulouse.fr #12;Comparison of two Nondestructive Tests in Carbon

  12. Fluorinated silica microchannel surfaces

    DOE Patents [OSTI]

    Kirby, Brian J.; Shepodd, Timothy Jon

    2005-03-15T23:59:59.000Z

    A method for surface modification of microchannels and capillaries. The method produces a chemically inert surface having a lowered surface free energy and improved frictional properties by attaching a fluorinated alkane group to the surface. The coating is produced by hydrolysis of a silane agent that is functionalized with either alkoxy or chloro ligands and an uncharged C.sub.3 -C.sub.10 fluorinated alkane chain. It has been found that the extent of surface coverage can be controlled by controlling the contact time from a minimum of about 2 minutes to a maximum of 120 minutes for complete surface coverage.

  13. Surface preparation for high purity alumina ceramics enabling direct brazing in hydrogen atmospheres

    DOE Patents [OSTI]

    Cadden, Charles H. (Danville, CA); Yang, Nancy Yuan Chi (Lafayette, CA); Hosking, Floyd M. (Albuquerque, NM)

    2001-01-01T23:59:59.000Z

    The present invention relates to a method for preparing the surface of a high purity alumina ceramic or sapphire specimen that enables direct brazing in a hydrogen atmosphere using an active braze alloy. The present invention also relates to a method for directly brazing a high purity alumina ceramic or sapphire specimen to a ceramic or metal member using this method of surface preparation, and to articles produced by this brazing method. The presence of silicon, in the form of a SiO.sub.2 -containing surface layer, can more than double the tensile bond strength in alumina ceramic joints brazed in a hydrogen atmosphere using an active Au-16Ni-0.75 Mo-1.75V filler metal. A thin silicon coating applied by PVD processing can, after air firing, produce a semi-continuous coverage of the alumina surface with a SiO.sub.2 film. Room temperature tensile strength was found to be proportional to the fraction of air fired surface covered by silicon-containing films. Similarly, the ratio of substrate fracture versus interface separation was also related to the amount of surface silicon present prior to brazing. This process can replace the need to perform a "moly-manganese" metallization step.

  14. TEST SYSTEM FOR EVALUATING SPENT NUCLEAR FUEL BENDING STIFFNESS AND VIBRATION INTEGRITY

    SciTech Connect (OSTI)

    Wang, Jy-An John [ORNL] [ORNL; Wang, Hong [ORNL] [ORNL; Bevard, Bruce Balkcom [ORNL] [ORNL; Howard, Rob L [ORNL] [ORNL; Flanagan, Michelle [U.S. Nuclear Regulatory Commission] [U.S. Nuclear Regulatory Commission

    2013-01-01T23:59:59.000Z

    Transportation packages for spent nuclear fuel (SNF) must meet safety requirements specified by federal regulations. For normal conditions of transport, vibration loads incident to transport must be considered. This is particularly relevant for high-burnup fuel (>45 GWd/MTU). As the burnup of the fuel increases, a number of changes occur that may affect the performance of the fuel and cladding in storage and during transportation. The mechanical properties of high-burnup de-fueled cladding have been previously studied by subjecting defueled cladding tubes to longitudinal (axial) tensile tests, ring-stretch tests, ring-compression tests, and biaxial tube burst tests. The objective of this study is to investigate the mechanical properties and behavior of both the cladding and the fuel in it under vibration/cyclic loads similar to the sustained vibration loads experienced during normal transport. The vibration loads to SNF rods during transportation can be characterized by dynamic, cyclic, bending loads. The transient vibration signals in a specified transport environment can be analyzed, and frequency, amplitude and phase components can be identified. The methodology being implemented is a novel approach to study the vibration integrity of actual SNF rod segments through testing and evaluating the fatigue performance of SNF rods at defined frequencies. Oak Ridge National Laboratory (ORNL) has developed a bending fatigue system to evaluate the response of the SNF rods to vibration loads. A three-point deflection measurement technique using linear variable differential transformers is used to characterize the bending rod curvature, and electromagnetic force linear motors are used as the driving system for mechanical loading. ORNL plans to use the test system in a hot cell for SNF vibration testing on high burnup, irradiated fuel to evaluate the pellet-clad interaction and bonding on the effective lifetime of fuel-clad structure bending fatigue performance. Technical challenges include pure bending implementation, remote installation and detachment of the SNF test specimen, test specimen deformation measurement, and identification of a driving system suitable for use in a hot cell. Surrogate test specimens have been used to calibrate the test setup and conduct systematic cyclic tests. The calibration and systematic cyclic tests have been used to identify test protocol issues prior to implementation in the hot cell. In addition, cyclic hardening in unidirectional bending and softening in reverse bending were observed in the surrogate test specimens. The interface bonding between the surrogate clad and pellets was found to impact the bending response of the surrogate rods; confirming this behavior in the actual spent fuel segments will be an important aspect of the hot cell test implementation,

  15. Appendix B Surface Infiltration and Aquifer Test Data

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA group currentBradleyTableSelling7111A Lithologic and Monitor Well Completion

  16. Fresnel versus Kummer surfaces

    E-Print Network [OSTI]

    Peinke, Joachim

    Fresnel versus Kummer surfaces Alberto Favaro & Friedrich W. Hehl Outline Linear media Linear media-you. Fresnel versus Kummer surfaces: geometrical optics in dispersionless linear (meta)materials and vacuum, 19­23 November 2012 Email: favaro@thp.uni-koeln.de #12;Fresnel versus Kummer surfaces Alberto Favaro

  17. SURFACE TENSION DRIVEN CONVECTION

    E-Print Network [OSTI]

    Wang, Shouhong

    SURFACE TENSION DRIVEN CONVECTION DIJKSTRA, SENGUL, WANG INTRODUCTION LINEAR THEORY MAIN THEOREMS CONCLUDING REMARKS DYNAMIC TRANSITIONS OF SURFACE TENSION DRIVEN CONVECTION H.Dijkstra T. Sengul S. Wang #12;SURFACE TENSION DRIVEN CONVECTION DIJKSTRA, SENGUL, WANG INTRODUCTION LINEAR THEORY MAIN THEOREMS

  18. Standard guide for conducting exfoliation corrosion tests in aluminum alloys

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    1992-01-01T23:59:59.000Z

    1.1 This guide differs from the usual ASTM standard in that it does not address a specific test. Rather, it is an introductory guide for new users of other standard exfoliation test methods, (see Terminology G 15 for definition of exfoliation). 1.2 This guide covers aspects of specimen preparation, exposure, inspection, and evaluation for conducting exfoliation tests on aluminum alloys in both laboratory accelerated environments and in natural, outdoor atmospheres. The intent is to clarify any gaps in existent test methods. 1.3 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only. 1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  19. Design and Testing of Prototypic Elements Containing Monolithic Fuel

    SciTech Connect (OSTI)

    N.E. Woolstenhulme; M.K. Meyer; D.M. Wachs

    2011-10-01T23:59:59.000Z

    The US fuel development team has performed numerous irradiation tests on small to medium sized specimens containing low enriched uranium fuel designs. The team is now focused on qualification and demonstration of the uranium-molybdenum Base Monolithic Design and has entered the next generation of testing with the design and irradiation of prototypic elements which contain this fuel. The designs of fuel elements containing monolithic fuel, such as AFIP-7 (which is currently under irradiation) and RERTR-FE (which is currently under fabrication), are appropriate progressions relative to the technology life cycle. The culmination of this testing program will occur with the design, fabrication, and irradiation of demonstration products to include the base fuel demonstration and design demonstration experiments. Future plans show that design, fabrication, and testing activities will apply the rigor needed for a demonstration campaign.

  20. SHAPE CONTROL OF REPRESENTATIVE TURNED SURFACE G.P. PETROPOULOS*, N.M. VAXEVANIDIS**, C.N. PANDAZARAS*, A. T. ANTONIADIS***

    E-Print Network [OSTI]

    Aristomenis, Antoniadis

    is to investigate into the topography (roughness and waviness) of turned surfaces processed under cutting factors simulation models. Specimens of Ck60 steel were turned for cutting factors properly selected to achieve were, as follows: I) built-up edge: cutting speed v = 25 m/min, feed f = 0.32 mm/rev, depth of cut

  1. Past Test One

    E-Print Network [OSTI]

    MA 366: Introduction to Di?'erential Equations. Fall 2001, Test One. Instructor: Yip o This test booklet has FIVE QUESTIONS, totaling 50 points for the whole test.

  2. Advanced Vehicle Testing & Evaluation

    Broader source: Energy.gov (indexed) [DOE]

    Vehicle Accelerated Reliability Test Battery Electric Vehicle Fast Charge Test Battery Energy Storage Performance Test For DC Fast Charge Demand Reduction...

  3. TEST STATION SALE OF PERFORMANCE TESTED BULLS

    E-Print Network [OSTI]

    Tennessee, University of

    in the test had to meet minimum performance requirements. Those were: CREEP NON-CREEP Adj 205 day wt. 560 520AS-B428 U T BULL TEST STATION SALE OF PERFORMANCE TESTED BULLS THURSDAY, MARCH 8, 2012 12:00 NOON IN GREENEVILLE AND KNOXVILLE LIVESTOCK CENTER http://animalscience.ag.utk.edu/ (For video) #12;UT BULL TEST

  4. Surface cleanliness measurement procedure

    DOE Patents [OSTI]

    Schroder, Mark Stewart (Hendersonville, NC); Woodmansee, Donald Ernest (Simpsonville, SC); Beadie, Douglas Frank (Greenville, SC)

    2002-01-01T23:59:59.000Z

    A procedure and tools for quantifying surface cleanliness are described. Cleanliness of a target surface is quantified by wiping a prescribed area of the surface with a flexible, bright white cloth swatch, preferably mounted on a special tool. The cloth picks up a substantial amount of any particulate surface contamination. The amount of contamination is determined by measuring the reflectivity loss of the cloth before and after wiping on the contaminated system and comparing that loss to a previous calibration with similar contamination. In the alternative, a visual comparison of the contaminated cloth to a contamination key provides an indication of the surface cleanliness.

  5. Tribological interaction between polytetrafluoroethylene and silicon oxide surfaces

    SciTech Connect (OSTI)

    Uçar, A.; Çopuro?lu, M.; Suzer, S., E-mail: suzer@fen.bilkent.edu.tr [Department of Chemistry, Bilkent University, 06800 Ankara (Turkey); Baykara, M. Z. [Department of Mechanical Engineering, Bilkent University, 06800 Ankara (Turkey); Ar?kan, O. [Department of Electrical and Electronics Engineering, Bilkent University, 06800 Ankara (Turkey)

    2014-10-28T23:59:59.000Z

    We investigated the tribological interaction between polytetrafluoroethylene (PTFE) and silicon oxide surfaces. A simple rig was designed to bring about a friction between the surfaces via sliding a piece of PTFE on a thermally oxidized silicon wafer specimen. A very mild inclination (?0.5°) along the sliding motion was also employed in order to monitor the tribological interaction in a gradual manner as a function of increasing contact force. Additionally, some patterns were sketched on the silicon oxide surface using the PTFE tip to investigate changes produced in the hydrophobicity of the surface, where the approximate water contact angle was 45° before the transfer. The nature of the transferred materials was characterized by X-ray photoelectron spectroscopy (XPS) and scanning electron microscopy (SEM). XPS results revealed that PTFE was faithfully transferred onto the silicon oxide surface upon even at the slightest contact and SEM images demonstrated that stable morphological changes could be imparted onto the surface. The minimum apparent contact pressure to realize the PTFE transfer is estimated as 5 kPa, much lower than reported previously. Stability of the patterns imparted towards many chemical washing processes lead us to postulate that the interaction is most likely to be chemical. Contact angle measurements, which were carried out to characterize and monitor the hydrophobicity of the silicon oxide surface, showed that upon PTFE transfer the hydrophobicity of the SiO{sub 2} surface could be significantly enhanced, which might also depend upon the pattern sketched onto the surface. Contact angle values above 100° were obtained.

  6. Inverse Finite Element Modelling and Identification of Constitutive Parameters of UHS Steel Based on Gleeble Tensile Tests at High Temperature

    E-Print Network [OSTI]

    Boyer, Edmond

    identification method - associating a direct finite element model of Gleeble tests and an optimization module1 Inverse Finite Element Modelling and Identification of Constitutive Parameters of UHS Steel Based-2 ) hc heat transfer coefficient at interface between specimen and grips (W m-2 K) hth_eff effective

  7. Advanced Vehicle Testing - Beginning-of-Test Battery Testing...

    Broader source: Energy.gov (indexed) [DOE]

    2.5 V Thermal Mgmt.: Passive, Vacuum-Sealed Unit Pack Weight: 294 kg BATTERY LABORATORY TEST RESULTS SUMMARY Vehicle Mileage and Testing Date Vehicle Odometer: 6,696 mi Date of...

  8. Creep rupture testing of alloy 617 and A508/533 base metals and weldments.

    SciTech Connect (OSTI)

    Natesan, K.; Li, M.; Soppet, W.K.; Rink, D.L. (Nuclear Engineering Division)

    2012-01-17T23:59:59.000Z

    The NGNP, which is an advanced HTGR concept with emphasis on both electricity and hydrogen production, involves helium as the coolant and a closed-cycle gas turbine for power generation with a core outlet/gas turbine inlet temperature of 750-1000 C. Alloy 617 is a prime candidate for VHTR structural components such as reactor internals, piping, and heat exchangers in view of its resistance to oxidation and elevated temperature strength. However, lack of adequate data on the performance of the alloy in welded condition prompted to initiate a creep test program at Argonne National Laboratory. In addition, Testing has been initiated to evaluate the creep rupture properties of the pressure vessel steel A508/533 in air and in helium environments. The program, which began in December 2009, was certified for quality assurance NQA-1 requirements during January and February 2010. Specimens were designed and fabricated during March and the tests were initiated in April 2010. During the past year, several creep tests were conducted in air on Alloy 617 base metal and weldment specimens at temperatures of 750, 850, and 950 C. Idaho National Laboratory, using gas tungsten arc welding method with Alloy 617 weld wire, fabricated the weldment specimens. Eight tests were conducted on Alloy 617 base metal specimens and nine were on Alloy 617 weldments. The creep rupture times for the base alloy and weldment tests were up to {approx}3900 and {approx}4500 h, respectively. The results showed that the creep rupture lives of weld specimens are much longer than those for the base alloy, when tested under identical test conditions. The test results also showed that the creep strain at fracture is in the range of 7-18% for weldment samples and were much lower than those for the base alloy, under similar test conditions. In general, the weldment specimens showed more of a flat or constant creep rate region than the base metal specimens. The base alloy and the weldment exhibited tertiary creep after 50-60% of the rupture life, irrespective of test temperature in the range of 750-950 C. The results showed that the stress dependence of the creep rate followed a power law for both base alloy and weldments. The data also showed that the stress exponent for creep is the same and one can infer that the same mechanism is operative in both base metal and weldments in the temperature range of the current study. SEM fractography analysis indicated that both base metal and weldment showed combined fracture modes consisting of dimple rupture and intergranular cracking. Intergranular cracking was more evident in the weldment specimens, which is consistent with the observation of lower creep ductility in the weldment than in the base metal.

  9. A review of the fossil record of spiders (Araneae) with special reference to Africa, and description of a new specimen from the Triassic Molteno Formation of South Africa

    E-Print Network [OSTI]

    Selden, Paul A.; Anderson, H.M.; Anderson, J.M.

    2009-06-01T23:59:59.000Z

    species in Dominican amber and alive on the island of Hispaniola respectively (Penney 2008). In spite of specimens having been available in gem shops relatively cheaply throughout the world, few descriptions of African copal spiders appeared until recently... amber was really a fake in Madagascan copal. Holl’s one-sentence description and figure (pl. 8, fig. 68a) suggests it almost certainly belongs to an ant-mimicing salticid genus such as Myrmarachne (which occurs in Madagascan copal), although the figure...

  10. Bull Test ID 1118 2013 Florida Bull Test

    E-Print Network [OSTI]

    Jawitz, James W.

    Bull Test ID 1118 2013 Florida Bull Test #12;Bull Test ID 1119 2013 Florida Bull Test #12;Bull Test ID 1120 2013 Florida Bull Test #12;Bull Test ID 1121 2013 Florida Bull Test #12;Bull Test ID 1122 2013 Florida Bull Test #12;Bull Test ID 1123 2013 Florida Bull Test #12;Bull Test ID 1124 2013 Florida

  11. Bull Test ID 1181 2013 Florida Bull Test

    E-Print Network [OSTI]

    Jawitz, James W.

    Bull Test ID 1181 2013 Florida Bull Test #12;Bull Test ID 1182 2013 Florida Bull Test #12;Bull Test ID 1183 2013 Florida Bull Test #12;Bull Test ID 1184 2013 Florida Bull Test #12;Bull Test ID 1185 2013 Florida Bull Test #12;Bull Test ID 1186 2013 Florida Bull Test #12;Bull Test ID 1187 2013 Florida

  12. Bull Test ID 1098 2013 Florida Bull Test

    E-Print Network [OSTI]

    Jawitz, James W.

    Bull Test ID 1098 2013 Florida Bull Test #12;Bull Test ID 1099 2013 Florida Bull Test #12;Bull Test ID 1100 2013 Florida Bull Test #12;Bull Test ID 1101 2013 Florida Bull Test #12;Bull Test ID 1102 2013 Florida Bull Test #12;Bull Test ID 1103 2013 Florida Bull Test #12;Bull Test ID 1104 2013 Florida

  13. Bull Test ID 1160 2013 Florida Bull Test

    E-Print Network [OSTI]

    Jawitz, James W.

    Bull Test ID 1160 2013 Florida Bull Test #12;Bull Test ID 1161 2013 Florida Bull Test #12;Bull Test ID 1162 2013 Florida Bull Test #12;Bull Test ID 1163 2013 Florida Bull Test #12;Bull Test ID 1164 2013 Florida Bull Test #12;Bull Test ID 1165 2013 Florida Bull Test #12;Bull Test ID 1166 2013 Florida

  14. Bull Test ID 1077 2013 Florida Bull Test

    E-Print Network [OSTI]

    Jawitz, James W.

    14th Annual Florida Bull Test #12;Bull Test ID 1077 2013 Florida Bull Test #12;Bull Test ID 1078 2013 Florida Bull Test #12;Bull Test ID 1079 2013 Florida Bull Test #12;Bull Test ID 1080 2013 Florida Bull Test #12;Bull Test ID 1081 2013 Florida Bull Test #12;Bull Test ID 1082 2013 Florida Bull Test #12

  15. Bull Test ID 1140 2013 Florida Bull Test

    E-Print Network [OSTI]

    Jawitz, James W.

    Bull Test ID 1140 2013 Florida Bull Test #12;Bull Test ID 1141 2013 Florida Bull Test #12;Bull Test ID 1142 2013 Florida Bull Test #12;Bull Test ID 1143 2013 Florida Bull Test #12;Bull Test ID 1144 2013 Florida Bull Test #12;Bull Test ID 1145 2013 Florida Bull Test #12;Bull Test ID 1146 2013 Florida

  16. Pressure Change Measurement Leak Testing Errors

    SciTech Connect (OSTI)

    Pryor, Jeff M [ORNL] [ORNL; Walker, William C [ORNL] [ORNL

    2014-01-01T23:59:59.000Z

    A pressure change test is a common leak testing method used in construction and Non-Destructive Examination (NDE). The test is known as being a fast, simple, and easy to apply evaluation method. While this method may be fairly quick to conduct and require simple instrumentation, the engineering behind this type of test is more complex than is apparent on the surface. This paper intends to discuss some of the more common errors made during the application of a pressure change test and give the test engineer insight into how to correctly compensate for these factors. The principals discussed here apply to ideal gases such as air or other monoatomic or diatomic gasses; however these same principals can be applied to polyatomic gasses or liquid flow rate with altered formula specific to those types of tests using the same methodology.

  17. Concolic Testing Koushik Sen

    E-Print Network [OSTI]

    Sen, Koushik

    Concolic testing automates test input generation by com­ bining the concrete and symbolic (concolic) execution of the code under test. Traditional test input generation tech­ niques use either (1) concrete test inputs from these constraints. In contrast, concolic testing tightly couples both concrete

  18. Concolic Testing Koushik Sen

    E-Print Network [OSTI]

    Sen, Koushik

    Concolic testing automates test input generation by com- bining the concrete and symbolic (concolic) execution of the code under test. Traditional test input generation tech- niques use either (1) concrete test inputs from these constraints. In contrast, concolic testing tightly couples both concrete

  19. DNA ELECTROPHORESIS AT SURFACES

    SciTech Connect (OSTI)

    RAFAILOVICH, MIRIAM; SOKOLOV, JONATHAN; GERSAPPE, DILIP

    2003-09-01T23:59:59.000Z

    During this year we performed two major projects: I. We developed a detailed theoretical model which complements our experiments on surface DNA electrophoresis. We found that it was possible to enhance the separation of DNA chains by imposing a chemical nanoscale pattern on the surface. This approach utilized the surface interaction effect of the DNA chains with the substrate and is a refinement to our previous method in which DNA chains were separated on homogeneous flat surfaces. By introducing the nano-patterns on the surface, the conformational changes of DNA chains of different lengths can be amplified, which results in the different friction strengths with the substrate surface. Our results also show that, when compared to the DNA electrophoresis performed on homogeneous flat surfaces, nanopatterned surfaces offer a larger window in choosing different surface interactions to achieve separation. II. In collaboration with a large international manufacturer of skin care products we also embarked on a project involving photo toxicity of titanium dioxide nanoparticles, which are a key ingredient in sunscreen and cosmetic lotions. The results clearly implicated the nanoparticles in catalyzing damage to chromosomal DNA. We then used this knowledge to develop a polymer/anti-oxidant coating which prevented the photocatalytic reaction on DNA while still retaining the UV absorptive properties of the nanoparticles. The standard gel electrophoresis was not sufficient in determining the extent of the DNA damage. The conclusions of this study were based predominantly on analysis obtained with the surface electrophoresis method.

  20. Comparison of glass surfaces as a countertop material to existing surfaces

    SciTech Connect (OSTI)

    Turo, Laura A.; Winschell, Abigail E.

    2011-09-01T23:59:59.000Z

    Gleen Glass, a small production glass company that creates countertops, was selected for the Technology Assistance Program through Pacific Northwest National Laboratory. Gleen Glass was seeking material property analysis comparing glass as a countertop material to current surfaces (i.e. marble, granite and engineered stone). With samples provided from Gleen Glass, testing was done on granite, marble, and 3 different glass surfaces ('Journey,' 'Pebble,' and 'Gleen'). Results showed the glass surfaces have a lower density, lower water absorption, and are stronger in compressive and flexural tests as compared to granite and marble. Thermal shock tests showed the glass failed when objects with a high thermal mass are placed directly on them, whereas marble and granite did not fracture under these conditions.

  1. Charpy impact test results of four low activation ferritic alloys irradiated at 370{degrees}C to 15 DPA

    SciTech Connect (OSTI)

    Schubert, L.E.; Hamilton, M.L.; Gelles, D.S. [Pacific Northwest National Lab., Richland, WA (United States)

    1996-10-01T23:59:59.000Z

    Miniature CVN specimens of four low activation ferritic alloys have been impact tested following irradiation at 370{degrees}C to 15 dpa. Comparison of the results with those of control specimens indicates that degradation in the impact behavior occurs in each of these four alloys. The 9Cr-2W alloy referred to as GA3X and the similar alloy F82H with 7.8Cr-2W appear most promising for further consideration as candidate structural materials in fusion energy system applications. These two alloys exhibit a small DBTT shift to higher temperatures but show increased absorbed energy on the upper shelf.

  2. Electrode holder useful in a corrosion testing device

    DOE Patents [OSTI]

    Murphy, R.J. Jr.; Jamison, D.E.

    1986-08-19T23:59:59.000Z

    The present invention is directed to an apparatus and method for holding one or more test electrodes of precisely known exposed surface area. The present invention is particularly useful in a device for determining the corrosion properties of the materials from which the test electrodes have been formed. The present invention relates to a device and method for holding the described electrodes wherein the exposed surface area of the electrodes is only infinitesimally decreased. Further, in the present invention the exposed, electrically conductive surface area of the contact devices is small relative to the test electrode surface area. The holder of the present invention conveniently comprises a device for contacting and engaging each test electrode at two point contacts infinitesimally small in relation to the exposed surface area of the electrodes. 4 figs.

  3. Boiling Heat Transfer on Superhydrophilic, Superhydrophobic, and Superbiphilic Surfaces

    E-Print Network [OSTI]

    Betz, Amy Rachel; Kim, Chang-Jin 'CJ'; Attinger, Daniel

    2012-01-01T23:59:59.000Z

    With recent advances in micro- and nanofabrication, superhydrophilic and superhydrophobic surfaces have been developed. The statics and dynamics of fluids on these surfaces have been well characterized. However, few investigations have been made into the potential of these surfaces to control and enhance other transport phenomena. In this article, we characterize pool boiling on surfaces with wettabilities varied from superhydrophobic to superhydrophilic, and provide nucleation measurements. The most interesting result of our measurements is that the largest heat transfer coefficients are reached not on surfaces with spatially uniform wettability, but on biphilic surfaces, which juxtapose hydrophilic and hydrophobic regions. We develop an analytical model that describes how biphilic surfaces effectively manage the vapor and liquid transport, delaying critical heat flux and maximizing the heat transfer coefficient. Finally, we manufacture and test the first superbiphilic surfaces (juxtaposing superhydrophobic ...

  4. Surface nonlinear optics

    SciTech Connect (OSTI)

    Shen, Y.R.; Chen, C.K.; de Castro, A.R.B.

    1980-01-01T23:59:59.000Z

    Surface electromagnetic waves are waves propagating along the interface of two media. Their existence was predicted by Sommerfield in 1909. In recent years, interesting applications have been found in the study of overlayers and molecular adsorption on surfaces, in probing of phase transitions, and in measurements of refractive indices. In the laboratory, the nonlinear interaction of surface electromagnetic waves were studied. The preliminary results of this recent venture in this area are presented.

  5. Surface modification to waveguides

    DOE Patents [OSTI]

    Timberlake, J.R.; Ruzic, D.N.; Moore, R.L.; Cohen, S.A.; Manos, D.M.

    1982-06-16T23:59:59.000Z

    A method is described for treating the interior surfaces of a waveguide to improve power transmission comprising the steps of mechanically polishing to remove surface protrusions; electropolishing to remove embedded particles; ultrasonically cleaning to remove any residue; coating the interior waveguide surfaces with an alkyd resin solution or electrophoretically depositing carbon lamp black suspended in an alkyd resin solution to form a 1..mu.. to 5..mu.. thick film; vacuum pyrolyzing the film to form a uniform adherent carbon coating.

  6. Running surface couplings

    E-Print Network [OSTI]

    S. D. Odintsov; A. Wipf

    1995-06-19T23:59:59.000Z

    We discuss the renormalization group improved effective action and running surface couplings in curved spacetime with boundary. Using scalar self-interacting theory as an example, we study the influence of the boundary effects to effective equations of motion in spherical cap and the relevance of surface running couplings to quantum cosmology and symmetry breaking phenomenon. Running surface couplings in the asymptotically free SU(2) gauge theory are found.

  7. Terahertz surface plasmon polaritons on a semiconductor surface structured with

    E-Print Network [OSTI]

    Murphy, Thomas E.

    Terahertz surface plasmon polaritons on a semiconductor surface structured with periodic V-doped silicon surface, using anisotropic wet-etching of crystalline silicon, thereby forming a plasmonic surfaces. © 2013 Optical Society of America OCIS codes: (240.6680) Surface plasmons; (240.6690) Surface

  8. Fatigue Testing of Metallurgically-Bonded EBR-II Superheater Tubes

    SciTech Connect (OSTI)

    Terry C. Totemeier

    2006-12-01T23:59:59.000Z

    Fatigue crack growth tests were performed on 2¼Cr-1Mo steel specimens machined from ex-service Experimental Breeder Reactor – II (EBR-II) superheater duplex tubes. The tubes had been metallurgically bonded with a 100 µm thick Ni interlayer; the specimens incorporated this bond layer. Tests were performed at room temperature in air and at 400°C in air and humid Ar; cracks were grown at varied levels of constant ?K. Crack growth tests at a range of ?K were also performed on specimens machined from the shell of the superheater. In all conditions the presence of the Ni interlayer was found to result in a net retardation of growth as the crack passed through the interlayer. The mechanism of retardation was identified as a disruption of crack planarity and uniformity after passing through the porous interlayer. Full crack arrest was only observed in a single test performed at near-threshold ?K level (12 MPa?m) at 400°C. In this case the crack tip was blunted by oxidation of the base steel at the steel-interlayer interface.

  9. NCMS PWB Surface Finishes Team project summary

    SciTech Connect (OSTI)

    Kokas, J.; DeSantis, C. [United Technologies Corp., Farmington, CT (United States). Hamilton Standard Div.; Wenger, G. [AT and T, New York, NY (United States)] [and others

    1996-04-01T23:59:59.000Z

    The NCMS PWB Surface Finishes Consortium is just about at the end of the five year program. Dozens of projects related to surface finishes and PWB solder-ability were performed by the team throughout the program, and many of them are listed in this paper. They are listed with a cross reference to where and when a technical paper was presented describing the results of the research. However, due to time and space constraints, this paper can summarize the details of only three of the major research projects accomplished by the team. The first project described is an ``Evaluation of PWB Surface Finishes.`` It describes the solderability, reliability, and wire bondability of numerous surface finishes. The second project outlined is an ``Evaluation of PWB Solderability Test Methods.`` The third project outlined is the ``Development and Evaluation of Organic Solderability Preservatives.``

  10. Accelerated Stress Testing, Qualification Testing, HAST, Field...

    Office of Environmental Management (EM)

    stress tests beyond the qualification test levels, which are necessary to predict PV module wear-out. The commercial success of PVs is ultimately based on the long-term...

  11. Reconstructing Surfaces and Functions on Surfaces from

    E-Print Network [OSTI]

    Texas at Austin, University of

    part is a common problem in Reverse Engineering. The part might be scannedwith a device like the laser-engineeringprocesses are nowadays commonplace in the manufacturing industry. For example, a company that manufactures mechanical object and measure the location of points on its surface. Mechanical probes, used in the manufacturing

  12. Method and device for tensile testing of cable bundles

    DOE Patents [OSTI]

    Robertson, Lawrence M; Ardelean, Emil V; Goodding, James C; Babuska, Vit

    2012-10-16T23:59:59.000Z

    A standard tensile test device is improved to accurately measure the mechanical properties of stranded cables, ropes, and other composite structures wherein a witness is attached to the top and bottom mounting blocks holding the cable under test. The witness is comprised of two parts: a top and a bottom rod of similar diameter with the bottom rod having a smaller diameter stem on its upper end and the top rod having a hollow opening in its lower end into which the stem fits forming a witness joint. A small gap is present between the top rod and the larger diameter portion of the bottom rod. A standard extensometer is attached to the top and bottom rods of the witness spanning this small witness gap. When a force is applied to separate the mounting blocks, the gap in the witness expands the same length that the entire test specimen is stretched.

  13. New downhole steam generator tested

    SciTech Connect (OSTI)

    Bleakley, W.B.

    1981-07-01T23:59:59.000Z

    Completion of 2 field tests of a new-model down-hole steam generator paves the way for further evaluation and development of a system destined to increase California's heavy oil production. Current air pollution restrictions there prevent installation of conventional steam generators in several areas of interest to oil operators. The current series of tests, conducted by Chemical Oil Recovery Co. (CORCO) of Bakersfield, California, follows an earlier prototype operation conducted by Sandia National Laboratories in conjunction with the US Department of Energy. The CORCO tests were conducted on the surface with the generator's output going into Tenneco Oil Exploration and Production Co.'s overland-Riokern Well No. 80, located in the Kern River field 4 miles north of Bakersfield. The first test was concluded with just under 1000 bbl of steam injected, less than planned due to a higher-than-expected injection pressure. The unit operated at less than 25% capacity because of the air compressor limitation. Compressor output was only 285 psi, not enough to inject the desired volumes into the reservoir. Test data shows that injection amounted to 150 bpd of 90 to 95% quality steam at 225-psi wellhead pressure. After injection, the well was shut in for 3 days to allow soaking, then put on production. Initial production was 40 bopd at 175 F.

  14. THERMAL TESTING OF PROTOTYPE GENERAL PURPOSE FISSILE PACKAGES USING A FURNACE

    SciTech Connect (OSTI)

    Smith, A; Lawrence Gelder, L; Paul Blanton, P

    2007-02-16T23:59:59.000Z

    The 9977/9978 General Purpose Fissile Package (GPFP) was designed by SRNL to replace the DOT 6M Specification Package and ship Plutonium and Uranium metals and oxides. Urethane foam was used for the overpack to ensure the package would withstand the 10CFR71.73(c)(2) crush test, which is a severe test for drum-type packages. In addition, it was necessary to confirm that the urethane foam configuration provided adequate thermal protection for the containment vessel during the subsequent 10CFR71.73(c)(4) thermal test. Development tests were performed on early prototype test specimens of different diameter overpacks and a range of urethane foam densities. The thermal test was performed using an industrial furnace. Test results were used to optimize the selection of package diameter and foam density, and provided the basis for design enhancements incorporated into the final package design.

  15. Butyl rubber O-ring seals: Revision of test procedures for stockpile materials

    SciTech Connect (OSTI)

    Domeier, L.A.; Wagter, K.R.

    1996-12-01T23:59:59.000Z

    Extensive testing showed little correlation between test slab and O-ring performance. New procedures, comparable to those used with the traditional test slabs, were defined for hardness, compression set, and tensile property testing on sacrificial O-ring specimens. Changes in target performance values were made as needed and were, in one case, tightened to reflect the O-ring performance data. An additional study was carried out on O-ring and slab performance vs cure cycle and showed little sensitivity of material performance to large changes in curing time. Aging and spectra of certain materials indicated that two sets of test slabs from current vendor were accidently made from EPDM rather than butyl rubber. Random testing found no O-rings made from EPDM. As a result, and additional spectroscope test will be added to the product acceptance procedures to verify the type of rubber compound used.

  16. Hydraulic conductivity testing of geosynthetic clay liners (GCLs) using the constant volume method

    SciTech Connect (OSTI)

    Wang, X.; Benson, C.H.

    1999-12-01T23:59:59.000Z

    Hydraulic conductivity tests were conducted using open and constant-volume permeation systems on specimens from a geosynthetic clay liner (GCL). Two constant volume (CV) systems were employed: the falling-head constant-volume (FHCV) system and the constant-head constant-volume (CHCV) system. A conventional burette system using pressurized air was employed for the open system (OS) tests. The test results show that hydraulic conductivity tests can be conducted 30 or more times faster with the FHCV and CHCV systems than with an open system. Typically the permeation portion of the FHCV and CHCV tests can be conducted in one-half day. Slightly lower hydraulic conductivities are measured with the CV systems due to the slightly higher effective stress applied during testing with these systems. The CHCV system has several advantages over the FHCV system, including minimizing initial transient behavior, constant applied effective stress during testing, and simpler calculations.

  17. Concrete Pavement Surface Characteristics

    E-Print Network [OSTI]

    , Broom, Belt, Carpet) Shot Peened Exposed Aggregate Porous (Pervious) Concrete Milled HMA and SurfaceImproving Concrete Pavement Surface Characteristics Pooled Fund TPF-5(139) National Concrete do with this knowledge? #12;Better Design and Construction Practices for Texturing Concrete Pavement

  18. Initial field testing definition of subsurface sealing and backfilling tests in unsaturated tuff; Yucca Mountain Site Characterization Project

    SciTech Connect (OSTI)

    Fernandez, J.A. [Sandia National Labs., Albuquerque, NM (United States); Case, J.B.; Tyburski, J.R. [I. T. Corp., Albuquerque, NM (United States)

    1993-05-01T23:59:59.000Z

    This report contains an initial definition of the field tests proposed for the Yucca Mountain Project repository sealing program. The tests are intended to resolve various performance and emplacement concerns. Examples of concerns to be addressed include achieving selected hydrologic and structural requirements for seals, removing portions of the shaft liner, excavating keyways, emplacing cementitious and earthen seals, reducing the impact of fines on the hydraulic conductivity of fractures, efficient grouting of fracture zones, sealing of exploratory boreholes, and controlling the flow of water by using engineered designs. Ten discrete tests are proposed to address these and other concerns. These tests are divided into two groups: Seal component tests and performance confirmation tests. The seal component tests are thorough small-scale in situ tests, the intermediate-scale borehole seal tests, the fracture grouting tests, the surface backfill tests, and the grouted rock mass tests. The seal system tests are the seepage control tests, the backfill tests, the bulkhead test in the Calico Hills unit, the large-scale shaft seal and shaft fill tests, and the remote borehole sealing tests. The tests are proposed to be performed in six discrete areas, including welded and non-welded environments, primarily located outside the potential repository area. The final selection of sealing tests will depend on the nature of the geologic and hydrologic conditions encountered during the development of the Exploratory Studies Facility and detailed numerical analyses. Tests are likely to be performed both before and after License Application.

  19. HEATER TEST PLANNING FOR THE NEAR SURFACE TEST FACILITY AT THE HANFORD RESERVATION

    E-Print Network [OSTI]

    DuBois, A.

    2010-01-01T23:59:59.000Z

    to the radioactive decay heat of the waste are of crucialused to simulate heat generation from radioactive waste, theheat loads t - be expected from canisters of nuclear waste.

  20. HEATER TEST PLANNING FOR THE NEAR SURFACE TEST FACILITY AT THE HANFORD RESERVATION

    E-Print Network [OSTI]

    DuBois, A.

    2010-01-01T23:59:59.000Z

    m from the central heater, distinct steps can be recognizedof sequential step loading, the secondary heaters will beof the central heater is best described as a series of step

  1. Single atom sputtering events: direct observation of near-surface depleted zones in ion-irradiated tungsten

    SciTech Connect (OSTI)

    Current, M. I.; Wei, C. Y.; Seidman, D. N.

    1980-03-01T23:59:59.000Z

    The three-dimensional spatial arrangement of vacancies contained in depleted zones (DZs), of ion-irradiated tungsten specimens, was determined with atomic resolution by the field-ion microscope (FIM) technique. These DZs were detected in the near-surface region of specimens which had been irradiated in situ at less than or equal to15 K with 20 keV W/sup +/, 30 keV W/sup +/, Kr/sup +/, Cu/sup +/, or Ar/sup +/ ions. The values of the ion dose employed were small (less than or equal to 10/sup 13/ ions cm/sup -2/); therefore, each DZ analyzed was the result of the impact of a single projectile ion. At the irradiation temperature (less than or equal to 15/sup 0/K) both the self-intersitital atoms and vacancies were immobile, so that the primary state of radiation damage was preserved. The following properties of each DZ were determined: the total number of vacancies; the number of vacancies in the near-surface region; the spatial extent - that is, the dimensions required to determine a volume; the average vacancy concentration; the average vacancy concentration associated with the non-surface region; the first-nearest neighbor cluster distribution for the vacancies in the near-surface region; the radial distribution function of all the vacancies; the distribution of vacancies as a function of depth normal to the irradiated surface; and the sputtering yield. Most of the above properties of the near-surface DZs had similar values to those of the DZs detected in the bulk of the FIM specimens. The total number of vacancies detected in the near-surface region wasapproximately consistent with theoretical estimates of the average sputtering yield. The sputtering yield of individual DZs exhibited significant fluctuations from the measured average sputtering yield.

  2. RMOTC - Testing - Geothermal

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Geothermal Testing Notice: As of July 1st, 2014, Testing at RMOTC has officially completed. We would like to thank all of our testing partners and everyone who helped make the...

  3. Test Herrera Report Template

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    development are described in detail in the following section. The model was run in six test sites: Test Site 1 is along the Cowlitz River (Segment 3); Test Site 2 includes the...

  4. ZiaTest

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ZiaTest ZiaTest Description This test executes a new proposed standard benchmark method for MPI startup that is intended to provide a realistic assessment of both launch and wireup...

  5. Directed random testing

    E-Print Network [OSTI]

    Pacheco, Carlos, Ph.D. Massachusetts Institute of Technology

    2009-01-01T23:59:59.000Z

    Random testing can quickly generate many tests, is easy to implement, scales to large software applications, and reveals software errors. But it tends to generate many tests that are illegal or that exercise the same parts ...

  6. LANSCE | Materials Test Station

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Research Facility Training Office Contact Administrative nav background Materials Test Station dotline Testing New Reactor Fuels that Reduce Radioactive Waste Mission Used...

  7. Capillary flow solderability test for printed wiring boards

    SciTech Connect (OSTI)

    Hosking, F.M.; Yost, F.G.; Hernandez, C.L.; Sackinger, S.J.

    1994-04-01T23:59:59.000Z

    This report describes a new technique for evaluating capillary flow solderability on printed circuit boards. The test involves the flow of molten solder from a pad onto different-sized conductor lines. It simulates the spreading dynamics of either plated-through-hole (PTH) or surface mount technology (SMT) soldering. A standard procedure has been developed for the test. Preliminary experiments were conducted and the results demonstrate test feasibility. Test procedures and results are presented in this report.

  8. Vendor System Vulnerability Testing Test Plan

    SciTech Connect (OSTI)

    James R. Davidson

    2005-01-01T23:59:59.000Z

    The Idaho National Laboratory (INL) prepared this generic test plan to provide clients (vendors, end users, program sponsors, etc.) with a sense of the scope and depth of vulnerability testing performed at the INL’s Supervisory Control and Data Acquisition (SCADA) Test Bed and to serve as an example of such a plan. Although this test plan specifically addresses vulnerability testing of systems applied to the energy sector (electric/power transmission and distribution and oil and gas systems), it is generic enough to be applied to control systems used in other critical infrastructures such as the transportation sector, water/waste water sector, or hazardous chemical production facilities. The SCADA Test Bed is established at the INL as a testing environment to evaluate the security vulnerabilities of SCADA systems, energy management systems (EMS), and distributed control systems. It now supports multiple programs sponsored by the U.S. Department of Energy, the U.S. Department of Homeland Security, other government agencies, and private sector clients. This particular test plan applies to testing conducted on a SCADA/EMS provided by a vendor. Before performing detailed vulnerability testing of a SCADA/EMS, an as delivered baseline examination of the system is conducted, to establish a starting point for all-subsequent testing. The series of baseline tests document factory delivered defaults, system configuration, and potential configuration changes to aid in the development of a security plan for in depth vulnerability testing. The baseline test document is provided to the System Provider,a who evaluates the baseline report and provides recommendations to the system configuration to enhance the security profile of the baseline system. Vulnerability testing is then conducted at the SCADA Test Bed, which provides an in-depth security analysis of the Vendor’s system.b a. The term System Provider replaces the name of the company/organization providing the system being evaluated. This can be the system manufacturer, a system user, or a third party organization such as a government agency. b. The term Vendor (or Vendor’s) System replaces the name of the specific SCADA/EMS being tested.

  9. Testing for Toxic Algae By Tadd Barrow

    E-Print Network [OSTI]

    Nebraska-Lincoln, University of

    Testing for Toxic Algae By Tadd Barrow UNL Extension Educator, Water Quality Algae is a microscopic plant that occurs in all water. However, only certain conditions bring algae to the surface, making it toxic to animals, especially humans and dogs. Toxic algae often are naturally occurring from high

  10. Surface alloying of immiscible metals induced by surface state shift

    E-Print Network [OSTI]

    Che, Jingguang

    , and topography; Silver; Gold; Copper; Tungsten; Molybdenum 1. Introduction Surface alloying has been a subjectSurface alloying of immiscible metals induced by surface state shift X.K. Shu, P. Jiang, J.G. Che) surface to form the substitutional surface alloys, despite the fact that they do not like to form alloy

  11. Enhanced surface hydrophobicity by coupling of surface polarity and topography

    E-Print Network [OSTI]

    Enhanced surface hydrophobicity by coupling of surface polarity and topography Nicolas organization and contact angle. We show that when the topography and polarity of the surface act in concert- ciated that the topography of a surface is important in deter- mining the degree of surface

  12. Entropy and surfaceness

    E-Print Network [OSTI]

    Casper, James Kyle

    1997-01-01T23:59:59.000Z

    The layer of the Earth's atmosphere which contains clouds and weather systems is a thin thermoregulatory surface. It maintains an exact energy budget between the Earth and the Sun. Recent work in theoretical physics is ...

  13. SURFACE NONLINEAR OPTICS

    E-Print Network [OSTI]

    Shen, Y.R.

    2010-01-01T23:59:59.000Z

    B. de Castro, and Y. R. Shen, Optics Lett. i, 393 See, for3, 1980 SURFACE NONLINEAR OPTICS Y.R. Shen, C.K. Chen, andde Janiero SURFRACE NONLINEAR OPTICS Y. R. Shen, C. K. Chen,

  14. Asteroid Surface Geophysics

    E-Print Network [OSTI]

    Murdoch, Naomi; Schwartz, Stephen R; Miyamoto, Hideaki

    2015-01-01T23:59:59.000Z

    The regolith-covered surfaces of asteroids preserve records of geophysical processes that have occurred both at their surfaces and sometimes also in their interiors. As a result of the unique micro-gravity environment that these bodies posses, a complex and varied geophysics has given birth to fascinating features that we are just now beginning to understand. The processes that formed such features were first hypothesised through detailed spacecraft observations and have been further studied using theoretical, numerical and experimental methods that often combine several scientific disciplines. These multiple approaches are now merging towards a further understanding of the geophysical states of the surfaces of asteroids. In this chapter we provide a concise summary of what the scientific community has learned so far about the surfaces of these small planetary bodies and the processes that have shaped them. We also discuss the state of the art in terms of experimental techniques and numerical simulations that...

  15. Surface wave interferometry 

    E-Print Network [OSTI]

    Halliday, David Fraser

    2009-01-01T23:59:59.000Z

    This thesis concerns the application of seismic interferometry to surface waves. Seismic interferometry is the process by which the wavefield between two recording locations is estimated, resulting in new recordings at ...

  16. Hydrogeologic investigations at the Nevada Test Site

    SciTech Connect (OSTI)

    Hawkins, W L [Los Alamos National Lab., NM (United States)] [Los Alamos National Lab., NM (United States); Trudeau, D A [Geological Survey, Las Vegas, NV (United States)] [Geological Survey, Las Vegas, NV (United States); Drellack, S L [Raytheon Services Nevada, Inc., Mercury, NV (United States)] [Raytheon Services Nevada, Inc., Mercury, NV (United States)

    1992-01-01T23:59:59.000Z

    The Nevada Test Site was established in 1950 as a continental area for testing nuclear devices and, since 1963, all nuclear detonations there have been underground. Most tests are conducted in vertical shafts with a small percentage conducted in tunnels. The majority of detonation points are above the water table, primarily in volcanic rocks or alluvium. In the testing areas the water table is 450--700 m below the surface. Pre- and post- event geologic investigations are conducted for each test location and long-term studies assess the impact of underground testing on a more regional scale. Studies in progress have not identified any impact on the regional ground water system from testing, but some local effects have been recognized. In some areas where several large tests have been conducted below the water table, water levels hundreds of meters above the regional water table have been measured and radioactivity has been discovered associated with fractures in a few holes. Flow-through and straddle packer testing has revealed unexpectedly high hydraulic pressures at depth. Recently, a multiple completion monitoring well installed to study three zones has confirmed the existence of a significant upward hydraulic gradient. These observations of local pressurization and fracture flow are being further explored to determine the influence of underground nuclear testing on the regional hydrogeologic system.

  17. Immunoassay and antibody microarray analysis of the HUPO Plasma Proteome Project reference specimens: Systematic variation between sample types and calibration of mass spectrometry data

    SciTech Connect (OSTI)

    Haab, Brian B.; Geierstanger, Bernhard H.; Michailidis, George; Vitzthum, Frank; Forrester, Sara; Okon, Ryan; Saviranta, Petri; Brinker, Achim; Sorette, Martin; Perlee, Lorah; Suresh, Shubha; Drwal, Garry; Adkins, Joshua N.; Omenn, Gilbert S.

    2005-08-01T23:59:59.000Z

    Four different immunoassay and antibody microarray methods performed at four different sites were used to measure the levels of a broad range of proteins (N = 323 assays; 39, 88, 168, and 28 assays at the respective sites; 237 unique analytes) in the human serum and plasma reference specimens distributed by the Plasma Proteome Project (PPP) of the HUPO. The methods provided a means to (1) assess the level of systematic variation in protein abundances associated with blood preparation methods (serum, citrate-anticoagulated-plasma, EDTA-anticoagulated-plasma, or heparin-anticoagulated-plasma) and (2) evaluate the dependence on concentration of MS-based protein identifications from data sets using the HUPO specimens. Some proteins, particularly cytokines, had highly variable concentrations between the different sample preparations, suggesting specific effects of certain anticoagulants on the stability or availability of these proteins. The linkage of antibody-based measurements from 66 different analytes with the combined MS/MS data from 18 different laboratories showed that protein detection and the quality of MS data increased with analyte concentration. The conclusions from these initial analyses are that the optimal blood preparation method is variable between analytes and that the discovery of blood proteins by MS can be extended to concentrations below the ng/mL range under certain circumstances. Continued developments in antibody-based methods will further advance the scientific goals of the PPP.

  18. Accelerated Laboratory Tests Using Simultaneous UV, Temperature...

    Broader source: Energy.gov (indexed) [DOE]

    ,nm nm * High UV Radiant Exposure (8400 W UV) * 95% exposure uniformity * Visible and infrared radiation mostly removed * Temperature and relative humidity around specimens...

  19. Dynamometer Testing (Fact Sheet)

    SciTech Connect (OSTI)

    Not Available

    2010-11-01T23:59:59.000Z

    This fact sheet describes the dynamometer and its testing capabilities at the National Wind Technology Center.

  20. Experimental investigation of a thermionic converter with developed surface electrodes

    SciTech Connect (OSTI)

    Luke, James R.; El-Genk, Mohamed S.; Adrian, John M. [Institute for Space and Nuclear Power Studies/Chemical and Nuclear Engineering Department University of New Mexico, Albuquerque, New Mexico 87131 (United States)

    1997-01-10T23:59:59.000Z

    A thermionic converter with developed planar electrode surfaces is designed and tested. One of the electrodes has concentric circular grooves cut into its surface, while the other electrode surface is smooth. The grooves are 0.5 mm deep and 0.5 mm wide, having lands that are 1.0 mm wide. The experimental setup is flexible so that either the smooth or developed surface electrode can be operated as the emitter, with the other operating as the collector. The I-V characteristics and power output are compared for the two electrode arrangements.

  1. Experimental investigation of a thermionic converter with developed surface electrodes

    SciTech Connect (OSTI)

    Luke, J.R.; El-Genk, M.S.; Adrian, J.M. [Institute for Space and Nuclear Power Studies/Chemical and Nuclear Engineering Department University of New Mexico, Albuquerque, New Mexico87131 (United States)

    1997-01-01T23:59:59.000Z

    A thermionic converter with developed planar electrode surfaces is designed and tested. One of the electrodes has concentric circular grooves cut into its surface, while the other electrode surface is smooth. The grooves are 0.5 mm deep and 0.5 mm wide, having lands that are 1.0 mm wide. The experimental setup is flexible so that either the smooth or developed surface electrode can be operated as the emitter, with the other operating as the collector. The I-V characteristics and power output are compared for the two electrode arrangements. {copyright} {ital 1997 American Institute of Physics.}

  2. Improved LWR Cladding Performance by EPD Surface Modification Technique

    SciTech Connect (OSTI)

    Corradini, Michael; Sridharan, Kumar

    2012-11-26T23:59:59.000Z

    This project will utilize the electro-phoretic deposition technique (EPD) in conjunction with nanofluids to deposit oxide coatings on prototypic zirconium alloy cladding surfaces. After demonstrating that this surface modification is reproducible and robust, the team will subject the modified surface to boiling and corrosion tests to characterize the improved nucleate boiling behavior and superior corrosion performance. The scope of work consists of the following three tasks: The first task will employ the EPD surface modification technique to coat the surface of a prototypic set of zirconium alloy cladding tube materials (e.g. Zircaloy and advanced alloys such as M5) with a micron-thick layer of zirconium oxide nanoparticles. The team will characterize the modified surface for uniformity using optical microscopy and scanning-electron microscopy, and for robustness using standard hardness measurements. After zirconium alloy cladding samples have been prepared and characterized using the EPD technique, the team will begin a set of boiling experiments to measure the heat transfer coefficient and critical heat flux (CHF) limit for each prepared sample and its control sample. This work will provide a relative comparison of the heat transfer performance for each alloy and the surface modification technique employed. As the boiling heat transfer experiments begin, the team will also begin corrosion tests for these zirconium alloy samples using a water corrosion test loop that can mimic light water reactor (LWR) operational environments. They will perform extended corrosion tests on the surface-modified zirconium alloy samples and control samples to examine the robustness of the modified surface, as well as the effect on surface oxidation

  3. Surface Water Management Areas (Virginia)

    Broader source: Energy.gov [DOE]

    This legislation establishes surface water management areas, geographically defined surface water areas in which the State Water Control Board has deemed the levels or supply of surface water to be...

  4. Surface Water Quality Standards (Kansas)

    Broader source: Energy.gov [DOE]

    This act states regulations for the quality of surface water in the state. It also states designated uses of classified surface waters, surface water quality criteria and an antidegradation policy...

  5. Check for peroxides every 6 months. opened test 1 test 2 test 3

    E-Print Network [OSTI]

    Pawlowski, Wojtek

    Check for peroxides every 6 months. opened test 1 test 2 test 3 date initials Check for peroxides every 6 months. opened test 1 test 2 test 3 date initials Check for peroxides every 6 months. Test strips can be obtained from EH&S, 5-8200 opened test 1 test 2 test 3 date initials Check for peroxides

  6. Modeling of thermomechanical conditions in Sigmajig weldability test

    SciTech Connect (OSTI)

    Feng, Z.; Zacharia, T.; David, S.A. [Oak Ridge National Lab., TN (United States). Metals and Ceramics Div.

    1995-08-01T23:59:59.000Z

    A finite element model has been developed to evaluate quantitatively the thermomechanical conditions for weld metal solidification cracking of a nickel based superalloy single-crystal in a laboratory weldability test, namely, the Sigmajig test. The effects of weld pool solidification on the thermal and mechanical behaviors of the specimen were considered. Stress-temperature-location diagrams were constructed to reveal the complex local stress development at the trailing edge of the weld pool. The calculated local stress in the solidification temperature range is used to explain the experimentally observed initiation of solidification cracking of the single-crystal under different welding and loading conditions, based on the material resistance versus the mechanical driving force.

  7. Automatic Test Factoring for Java

    E-Print Network [OSTI]

    Saff, David

    2005-06-08T23:59:59.000Z

    Test factoring creates fast, focused unit tests from slow system-widetests; each new unit test exercises only a subset of the functionalityexercised by the system test. Augmenting a test suite with factoredunit tests ...

  8. Entry/Exit Port testing, test report

    SciTech Connect (OSTI)

    Winkelman, R.H.

    1993-05-01T23:59:59.000Z

    The Waste Receiving and Processing Module I (WRAP-1) facility must have the ability to allow 55-gallon drums to enter and exit glovebox enclosures. An Entry/Exit Port (Appendix 1, Figure 1), designed by United Engineers and Constructors (UE&C), is one method chosen for drum transfer. The Entry/Exit Port is to be used for entry of 55-gallon drums into both process entry gloveboxes, exit of 55-gallon drum waste pucks from the low-level waste (LLW) glovebox, and loadout of waste from the restricted waste management glovebox. The Entry/Exit Port relies on capture velocity air flow and a neoprene seal to provide alpha confinement when the Port is in the open and closed positions, respectively. Since the glovebox is in a slight vacuum, air flow is directed into the glovebox through the space between the overpack drum and glovebox floor. The air flow is to direct any airborne contamination into the glovebox. A neoprene seal is used to seal the Port door to the glovebox floor, thus maintaining confinement in the closed position. Entry/Exit Port testing took place February 17, 1993, through April 14, 1993, in the 305 building of Westinghouse Hanford Company. Testing was performed in accordance with the Entry/Exit Port Testing Test Plan, document number WHC-SD-WO26-TP-005. A prototype Entry/Exit Port built at the Hanford Site was tested using fluorescent paint pigment and smoke candles as simulant contaminants. This test report is an interim test report. Further developmental testing is required to test modifications made to the Port as the original design of the Port did not provide complete confinement during all stages of operation.

  9. Large Magnetization at Carbon Surfaces

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Large Magnetization at Carbon Surfaces Large Magnetization at Carbon Surfaces Print Wednesday, 31 August 2011 00:00 From organic matter to pencil lead, carbon is a versatile...

  10. Tools for Surface Analysis | EMSL

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    surface analysis - Because of the importance of clear and unambiguous communications, ISO definitions and concepts related to surface chemical analysis are now freely available....

  11. Status of the NGNP Graphite Creep Experiments AGC-1 and AGC-2 Irradiated in the Advanced Test Reactor

    SciTech Connect (OSTI)

    Blaine Grover

    2012-10-01T23:59:59.000Z

    The United States Department of Energy’s Next Generation Nuclear Plant (NGNP) Program will be irradiating six nuclear graphite creep experiments in the Advanced Test Reactor (ATR) located at the Idaho National Laboratory (INL). The graphite experiments will be irradiated over the next six to eight years to support development of a graphite irradiation performance data base on the new nuclear grade graphites now available for use in high temperature gas reactors. The goals of the irradiation experiments are to obtain irradiation performance data, including irradiation creep, at different temperatures and loading conditions to support design of the Next Generation Nuclear Plant (NGNP) Very High Temperature Gas Reactor, as well as other future gas reactors. The experiments will each consist of a single capsule that will contain six peripheral stacks of graphite specimens, with half of the graphite specimens in each stack under a compressive load, while the other half of the specimens will not be subjected to a compressive load during irradiation. The six peripheral stacks will have different compressive loads applied to the top half of each pair of specimen stacks, while a seventh stack will not have a compressive load. The specimens will be irradiated in an inert sweep gas atmosphere with on-line temperature and compressive load monitoring and control. There will also be sampling the sweep gas effluent to determine if any oxidation or off-gassing of the specimens occurs during irradiation of the experiment. The first experiment, AGC-1, started its irradiation in September 2009, and the irradiation was completed in January 2011. The second experiment, AGC-2, started its irradiation in April 2011 and completed its irradiation in May 2012. This paper will briefly discuss the design of the experiment and control systems, and then present the irradiation results for each experiment to date.

  12. Lectures 9: Surface Plasmon Polaritons Surface Plasmon Polaritons (SPPs)

    E-Print Network [OSTI]

    Lectures 9: Surface Plasmon Polaritons #12;Surface Plasmon Polaritons (SPPs) Introduction and basic properties Standard textbook: - Heinz Raether, Surface Plasmons on Smooth and Rough Surfaces and on Gratings Springer Tracts in Modern Physics, Vol. 111, Springer Berlin 1988 Overview articles on Plasmonics: - A

  13. Compliant layer chucking surface

    DOE Patents [OSTI]

    Blaedel, Kenneth L. (Dublin, CA); Spence, Paul A. (Pleasanton, CA); Thompson, Samuel L. (Pleasanton, CA)

    2004-12-28T23:59:59.000Z

    A method and apparatus are described wherein a thin layer of complaint material is deposited on the surface of a chuck to mitigate the deformation that an entrapped particle might cause in the part, such as a mask or a wafer, that is clamped to the chuck. The harder particle will embed into the softer layer as the clamping pressure is applied. The material composing the thin layer could be a metal or a polymer for vacuum or electrostatic chucks. It may be deposited in various patterns to affect an interrupted surface, such as that of a "pin" chuck, thereby reducing the probability of entrapping a particle.

  14. Surface Plasmon Resonance Imaging Using a High Numerical Aperture Microscope Objective

    E-Print Network [OSTI]

    Zare, Richard N.

    Surface Plasmon Resonance Imaging Using a High Numerical Aperture Microscope Objective Bo Huang-5080 We designed, constructed, and tested a surface plasmon resonance (SPR) microscope using a high, combined with various methods to shorten the surface plasmon propaga- tion length, achieves diffraction

  15. Development of the Flux-Adjusting Surface Data Assimilation System for Mesoscale Models

    E-Print Network [OSTI]

    Niyogi, Dev

    Development of the Flux-Adjusting Surface Data Assimilation System for Mesoscale Models KIRAN and temperature and for surface air temperature and water vapor mixing ratio for mesoscale models. In the FASDAS-field variables. The FASDAS is coupled to a land surface submodel in a three-dimensional mesoscale model and tests

  16. Effective Darcy-scale contact angles in porous media imbibing solutions of various surface tensions

    E-Print Network [OSTI]

    Selker, John

    Effective Darcy-scale contact angles in porous media imbibing solutions of various surface tensions was to develop and test a methodology to determine whether these surface tension effects predictably alter of 25° for the NaNO3 solution solely on the basis of surface tension contrast. The results of this study

  17. X-ray phase contrast imaging of biological specimens with femtosecond pulses of betatron radiation from a compact laser plasma wakefield accelerator

    SciTech Connect (OSTI)

    Kneip, S. [Blackett Laboratory, Imperial College London, London SW7 2AZ (United Kingdom); Center for Ultrafast Optical Science, University of Michigan, Ann Arbor 48109 (United States); McGuffey, C.; Dollar, F.; Chvykov, V.; Kalintchenko, G.; Krushelnick, K.; Maksimchuk, A.; Mangles, S. P. D.; Matsuoka, T.; Schumaker, W.; Thomas, A. G. R.; Yanovsky, V. [Center for Ultrafast Optical Science, University of Michigan, Ann Arbor 48109 (United States); Bloom, M. S.; Najmudin, Z.; Palmer, C. A. J.; Schreiber, J. [Blackett Laboratory, Imperial College London, London SW7 2AZ (United Kingdom)

    2011-08-29T23:59:59.000Z

    We show that x-rays from a recently demonstrated table top source of bright, ultrafast, coherent synchrotron radiation [Kneip et al., Nat. Phys. 6, 980 (2010)] can be applied to phase contrast imaging of biological specimens. Our scheme is based on focusing a high power short pulse laser in a tenuous gas jet, setting up a plasma wakefield accelerator that accelerates and wiggles electrons analogously to a conventional synchrotron, but on the centimeter rather than tens of meter scale. We use the scheme to record absorption and phase contrast images of a tetra fish, damselfly and yellow jacket, in particular highlighting the contrast enhancement achievable with the simple propagation technique of phase contrast imaging. Coherence and ultrafast pulse duration will allow for the study of various aspects of biomechanics.

  18. BENCAP, LLC: CAPSULE VELOCITY TEST

    SciTech Connect (OSTI)

    Meidinger, Brian

    2005-09-07T23:59:59.000Z

    Ben Cap, LLC, has a technology that utilizes bebtonite to plug wells. The bentonite is encapsulated in a cardboard capsule, droped down to the bottom of the well where it is allowed to hydrate, causing the bentonite to expand and plug the well. This method of plugging a well is accepted in some, but not all states. This technology can save a significant amount of money when compared to cementing methods currently used to plug and abandon wells. The test objective was to obtain the terminal velocity of the capsule delivery system as it drops through a column of water in a wellbore. Once the terminal velocity is known, the bentonite swelling action can be timed not to begin swelling until it reaches the bottom of the well bore. The results of the test showed that an average speed of 8.93 plus or minus 0.12 ft/sec was achieved by the capsule as it was falling through a column of water. Plotting the data revealed a very linear function with the capsules achieving terminal velocity shortly after being released. The interference of the capsule impacting the casing was not readily apparent in any of the runs, but a siginal sampling anomaly was present in one run. Because the anomaly was so brief and not present in any of the other runs, no solid conclusions could be drawn. Additional testing would be required to determine the effects of capsules impacting a fluid level that is not at surface.

  19. I/O Test

    E-Print Network [OSTI]

    Beeler, Michael

    1967-10-01T23:59:59.000Z

    IO TEST is intended as a hardware testing and debugging aid for use with the PDP-6 and its associated input multiplexer (analog to digital converter) and output multiplexer (digital to analog converter). While all characters ...

  20. MA 266 Practice Test

    E-Print Network [OSTI]

    2015-02-26T23:59:59.000Z

    Test 1: March 4, 2015. INSTRUCTIONS in the Test. 1. Do not open this exam booklet until told to do so. 2. There are 6 or 7 problems - one per page. 3. Show all ...

  1. Practice test 2

    E-Print Network [OSTI]

    2015-04-12T23:59:59.000Z

    Spring 2015. Test 2: April 15, 2015. INSTRUCTIONS in the Test. 1. Do not open this exam booklet until told to do so. 2. There are 6 or 7 problems - one per page.

  2. area treatability test: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    treatability test First Page Previous Page 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 Next Page Last Page Topic Index 1 Testing Surface Area Pravesh Kothari...

  3. area tonopah test: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    area tonopah test First Page Previous Page 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 Next Page Last Page Topic Index 1 Testing Surface Area Pravesh Kothari...

  4. Coaxial test fixture

    DOE Patents [OSTI]

    Praeg, W.F.

    1984-03-30T23:59:59.000Z

    This invention pertains to arrangements for performing electrical tests on contact material samples, and in particular for testing contact material test samples in an evacuated environment under high current loads. Frequently, it is desirable in developing high-current separable contact material, to have at least a preliminary analysis of selected candidate conductor materials. Testing of material samples will hopefully identify materials unsuitable for high current electrical contact without requiring incorporation of the materials into a completed and oftentimes complex structure.

  5. Blade Testing Trends (Presentation)

    SciTech Connect (OSTI)

    Desmond, M.

    2014-08-01T23:59:59.000Z

    As an invited guest speaker, Michael Desmond presented on NREL's NWTC structural testing methods and capabilities at the 2014 Sandia Blade Workshop held on August 26-28, 2014 in Albuquerque, NM. Although dynamometer and field testing capabilities were mentioned, the presentation focused primarily on wind turbine blade testing, including descriptions and capabilities for accredited certification testing, historical methodology and technology deployment, and current research and development activities.

  6. Articles about Testing

    Broader source: Energy.gov [DOE]

    Stories about testing facilities, capabilities, and certification featured by the U.S. Department of Energy (DOE) Wind Program.

  7. Decontaminating metal surfaces

    DOE Patents [OSTI]

    Childs, E.L.

    1984-01-23T23:59:59.000Z

    Radioactively contaminated surfaces can be electrolytically decontaminated with greatly increased efficiencies by using electrolytes containing higher than heretofore conventional amounts of nitrate, e.g., >600 g/1 of NaNO/sub 3/, or by using nitrate-containing electrolytes which are acidic, e.g., of a pH < 6.

  8. Soil Testing and Research

    E-Print Network [OSTI]

    Ciocan-Fontanine, Ionut

    Soil Testing and Research Analytical Laboratory Copyright © 2014 University of Minnesota Soil Testing and Research Analytical Laboratory Department of Soil, Water and Climate College of Food payable to the University of Minnesota We also accept the following credit cards: Soil Testing

  9. Gas Test Loop Booster Fuel Hydraulic Testing

    SciTech Connect (OSTI)

    Gas Test Loop Hydraulic Testing Staff

    2006-09-01T23:59:59.000Z

    The Gas Test Loop (GTL) project is for the design of an adaptation to the Advanced Test Reactor (ATR) to create a fast-flux test space where fuels and materials for advanced reactor concepts can undergo irradiation testing. Incident to that design, it was found necessary to make use of special booster fuel to enhance the neutron flux in the reactor lobe in which the Gas Test Loop will be installed. Because the booster fuel is of a different composition and configuration from standard ATR fuel, it is necessary to qualify the booster fuel for use in the ATR. Part of that qualification is the determination that required thermal hydraulic criteria will be met under routine operation and under selected accident scenarios. The Hydraulic Testing task in the GTL project facilitates that determination by measuring flow coefficients (pressure drops) over various regions of the booster fuel over a range of primary coolant flow rates. A high-fidelity model of the NW lobe of the ATR with associated flow baffle, in-pile-tube, and below-core flow channels was designed, constructed and located in the Idaho State University Thermal Fluids Laboratory. A circulation loop was designed and constructed by the university to provide reactor-relevant water flow rates to the test system. Models of the four booster fuel elements required for GTL operation were fabricated from aluminum (no uranium or means of heating) and placed in the flow channel. One of these was instrumented with Pitot tubes to measure flow velocities in the channels between the three booster fuel plates and between the innermost and outermost plates and the side walls of the flow annulus. Flow coefficients in the range of 4 to 6.5 were determined from the measurements made for the upper and middle parts of the booster fuel elements. The flow coefficient for the lower end of the booster fuel and the sub-core flow channel was lower at 2.3.

  10. Smart, passive sun facing surfaces

    DOE Patents [OSTI]

    Hively, L.M.

    1996-04-30T23:59:59.000Z

    An article adapted for selectively utilizing solar radiation comprises an absorptive surface and a reflective surface, the absorptive surface and the reflective surface oriented to absorb solar radiation when the sun is in a relatively low position, and to reflect solar radiation when the sun is in a relatively high position. 17 figs.

  11. Smart, passive sun facing surfaces

    DOE Patents [OSTI]

    Hively, Lee M. (Knoxville, TN)

    1996-01-01T23:59:59.000Z

    An article adapted for selectively utilizing solar radiation comprises an absorptive surface and a reflective surface, the absorptive surface and the reflective surface oriented to absorb solar radiation when the sun is in a relatively low position, and to reflect solar radiation when the sun is in a relatively high position.

  12. Free Boundaries and Minimal Surfaces

    E-Print Network [OSTI]

    2015-05-22T23:59:59.000Z

    Freeboundariesariseastheinterfacebetweenmaterialsinwhichthematerialsretain some energy. In contrast, the interface represented by a minimal surface lives in.

  13. Surface decontamination compositions and methods

    DOE Patents [OSTI]

    Wright; Karen E. (Idaho Falls, ID); Cooper, David C. (Idaho Falls, ID); Peterman, Dean R. (Idaho Falls, ID); Demmer, Ricky L. (Idaho Falls, ID); Tripp, Julia L. (Pocatello, ID); Hull, Laurence C. (Idaho Falls, ID)

    2011-03-29T23:59:59.000Z

    Clay-based compositions capable of absorbing contaminants from surfaces or objects having surface faces may be applied to a surface and later removed, the removed clay-based compositions absorbing at least a portion of the contaminant from the surface or object to which it was applied.

  14. A stochastic Monte Carlo computer simulation of the drop-weight test for the determination of nil-ductility transition temperature 

    E-Print Network [OSTI]

    Lambert, Michael Andrew

    1990-01-01T23:59:59.000Z

    . . . . . Page 2. Elements of the Charpy V-notch test. . 3. Elements of the drop-weight NDIT test. . . . . . . 13 4. Generalized fracture analysis diagram (FAD). . . . . . . . . 18 5. Schematic of the one-pass and two-pass crack starter bead welding... of the six forgings. . . 24. Variation in Vicker's microhardness (VHN) with distance from the fusion boundary between the specimen and crack-starter weld bead . . 91 CHAPTER I OVERVIEW OF FRACTURE MECHANICS The drop-weight nil-ductility transition...

  15. Comparison of Three Primary Surface Recuperator Alloys

    SciTech Connect (OSTI)

    Matthews, Wendy [Capstone Turbines; More, Karren Leslie [ORNL; Walker, Larry R [ORNL

    2010-01-01T23:59:59.000Z

    Extensive work performed by Capstone Turbine Corporation, Oak Ridge National Laboratory, and various others has shown that the traditional primary surface recuperator alloy, type 347 stainless steel, is unsuitable for applications above 650 C ({approx}1200 F). Numerous studies have shown that the presence of water vapor greatly accelerates the oxidation rate of type 347 stainless steel at temperatures above 650 C ({approx}1200 F). Water vapor is present as a product of combustion in the microturbine exhaust, making it necessary to find replacement alloys for type 347 stainless steel that will meet the long life requirements of microturbine primary surface recuperators. It has been well established over the past few years that alloys with higher chromium and nickel contents than type 347 stainless steel have much greater oxidation resistance in the microturbine environment. One such alloy that has replaced type 347 stainless steel in primary surface recuperators is Haynes Alloy HR-120 (Haynes and HR-120 are trademarks of Haynes International, Inc.), a solid-solution-strengthened alloy with nominally 33 wt % Fe, 37 wt % Ni and 25 wt % Cr. Unfortunately, while HR-120 is significantly more oxidation resistant in the microturbine environment, it is also a much more expensive alloy. In the interest of cost reduction, other candidate primary surface recuperator alloys are being investigated as possible alternatives to type 347 stainless steel. An initial rainbow recuperator test has been performed at Capstone to compare the oxidation resistance of type 347 stainless steel, HR-120, and the Allegheny Ludlum austenitic alloy AL 20-25+Nb (AL 20-25+Nb is a trademark of ATI Properties, Inc. and is licensed to Allegheny Ludlum Corporation). Evaluation of surface oxide scale formation and associated alloy depletion and other compositional changes has been carried out at Oak Ridge National Laboratory. The results of this initial rainbow test will be presented and discussed in this paper.

  16. Rulison Site Surface Closure Report

    SciTech Connect (OSTI)

    NONE

    1998-07-01T23:59:59.000Z

    This Closure Report provides documentation for closure of the Rulison Site surface and summarizes the data from groundwater monitoring conducted quarterly in 1996 and 1997. The quarterly groundwater monitoring was conducted to demonstrate that no contaminants are migrating from the pond after completion of the pond remediation activities. The Rulison Site is located in the North 1/2 of the Southwest 1/4 of Section 25, Township 7 South, Range 95 West of the 6` Principal Meridian, Garfield County, Colorado, approximately 19 kilometers (km) (12 miles [mi]) southwest of Rifle, Colorado, and approximately 65 km (40 mi) northeast of Grand Junction, Colorado (Figure I - 1). The site is situated on the north slope of Battlement Mesa on the upper reaches of Battlement Creek at an elevation of approximately 2,500 meters (m) (8,200 feet [ft]). The valley is open to the north-northwest and is bounded on the other three sides by steep mountain slopes that rise to elevations above 2,927 m (9,600 ft). Project Rulison was a joint U.S. Atomic Energy Commission (AEC) and Austral Oil Company (Austral) experiment. It was conducted under the AEC`s Plowshare Program to evaluate the feasibility of using a nuclear device to stimulate natural gas production in low- permeability, gas-producing geologic formations. The experiment consisted of detonating a 40-kiloton nuclear device at a depth of 2, 568 m (8,426 ft) below ground surface on September 10, 1969, followed by natural gas production testing in 1970 and 1971 (AEC, 1973).

  17. Pendulum detector testing device

    DOE Patents [OSTI]

    Gonsalves, John M. (Modesto, CA)

    1997-01-01T23:59:59.000Z

    A detector testing device which provides consistent, cost-effective, repeatable results. The testing device is primarily constructed of PVC plastic and other non-metallic materials. Sensitivity of a walk-through detector system can be checked by: 1) providing a standard test object simulating the mass, size and material content of a weapon or other contraband, 2) suspending the test object in successive positions, such as head, waist and ankle levels, simulating where the contraband might be concealed on a person walking through the detector system; and 3) swinging the suspended object through each of the positions, while operating the detector system and observing its response. The test object is retained in a holder in which the orientation of the test device or target can be readily changed, to properly complete the testing requirements.

  18. Pendulum detector testing device

    DOE Patents [OSTI]

    Gonsalves, J.M.

    1997-09-30T23:59:59.000Z

    A detector testing device is described which provides consistent, cost-effective, repeatable results. The testing device is primarily constructed of PVC plastic and other non-metallic materials. Sensitivity of a walk-through detector system can be checked by: (1) providing a standard test object simulating the mass, size and material content of a weapon or other contraband, (2) suspending the test object in successive positions, such as head, waist and ankle levels, simulating where the contraband might be concealed on a person walking through the detector system; and (3) swinging the suspended object through each of the positions, while operating the detector system and observing its response. The test object is retained in a holder in which the orientation of the test device or target can be readily changed, to properly complete the testing requirements. 5 figs.

  19. OTEC-1 Power System Test Program: test plan for first deployment

    SciTech Connect (OSTI)

    None

    1980-03-01T23:59:59.000Z

    This report describes in detail all tests planned for the first eight-month deployment of OTEC-1, a test facility constructed by the US Department of Energy in order to test heat exchangers for closed-cycle power plants using ocean thermal energy. Tests to be performed during the first-deployment period are aimed primarily at determining (1) the effectiveness of countermeasures in preventing biofouling of the heat exchanters, (2) the extent of environmental impacts associated with operation of an OTEC facility, and (3) the performance of a 1-MWe, titanium shell-and-tube evaporator and condenser pair. The condenser to be tested has plain tubes, and the evaporator employs the Linde High Flux surface on the working-fluid (ammonia) side to enhance the heat-transfer rate. This plan provides a statement of the objectives and priorities of the test program, describes the test equipment, gives a detailed account of all tests to be performed and the test schedule, and discusses provisions for management of the test program.

  20. Surface Characterization of Stainless Steel Part by Eddy Current

    SciTech Connect (OSTI)

    Andersen, Eric S.; Hockey, Ronald L.; Prince, James M.; Good, Morris S.

    2003-10-01T23:59:59.000Z

    The Pacific Northwest National Laboratory (PNNL) has nearly a 40 year history of research and development in the field of nondestructive evaluation (NDE). One area of NDE expertise at PNNL is electromagnetic testing which includes a field of eddy current testing (ET). One benefit is that ET can typically be performed at high speeds, and as a result has found many applications in process monitoring and poduction lines. ET has been used in the nuclear, aerospace, and automotive industries for many years. Et technology lends itself well to the detection of near-surface or surface breaking defects such as surface scratches. This paper provides an overview of theory regarding the usage of ET, selected application studies performed by PNNL, a safety analysis, and a wrtie up pertaining to the operations of ET to detect surface scratches.

  1. STRUCTURES AND MATERIALS TEST LABORATORY

    E-Print Network [OSTI]

    Russell, Jeffrey S.

    of the test program described here was to measure the shrinkage and creep characteristics of SCC mixes used. Creep tests ................................................. 4 3. Other tests ........................... 13 Shrinkage Test Results ................................... 16 Creep test Results

  2. Frictional properties between fine grained limestone, dolomite and sandstone along precut surfaces

    E-Print Network [OSTI]

    Iwasaki, Takeshi

    1970-01-01T23:59:59.000Z

    shear surface; w, wet surface; c, clean surface. Table 1. Coefficients of friction of rocks and Minerals (cited from Jaeger and Cook, 1969). EXPERIMENTAL PROCEDURE Triaxial compression experiments were conducted on dry, copper-jacketed samples in a...) and Handin (1969) suggested that it reflected the brittle-ductile transition of the tested rocks. The cohesive shear strength is zero across a precut surface, so in the brittle state Coulomb's cri- terion predicts that coefficient of sliding friction...

  3. Pocked surface neutron detector

    DOE Patents [OSTI]

    McGregor, Douglas (Whitmore Lake, MI); Klann, Raymond (Bolingbrook, IL)

    2003-04-08T23:59:59.000Z

    The detection efficiency, or sensitivity, of a neutron detector material such as of Si, SiC, amorphous Si, GaAs, or diamond is substantially increased by forming one or more cavities, or holes, in its surface. A neutron reactive material such as of elemental, or any compound of, .sup.10 B, .sup.6 Li, .sup.6 LiF, U, or Gd is deposited on the surface of the detector material so as to be disposed within the cavities therein. The portions of the neutron reactive material extending into the detector material substantially increase the probability of an energetic neutron reaction product in the form of a charged particle being directed into and detected by the neutron detector material.

  4. Laser surface cleaning

    SciTech Connect (OSTI)

    Crivella, E.C.; Freiwald, J.; Freiwald, D.A.

    1996-12-31T23:59:59.000Z

    Decontamination of contaminated metal and material recycle, two of 31 priority needs identified by the D&D focus group, are the most promising applications for laser ablation within the DOE complex. F2 Associates has developed a robotic laser ablation system that is capable of high contamination rates, waste volume reduction, surface pore cleaning, and real-time characterization of materials. It is being demonstrated that this system will be the most cost-effective technology for metal decontamination and material recycle.

  5. Surface profiling interferometer

    DOE Patents [OSTI]

    Takacs, Peter Z. (P.O. Box 385, Upton, NY 11973); Qian, Shi-Nan (Hefei Synchrotron Radiation Laboratory, University of Science and, Hefei, Anhui, CN)

    1989-01-01T23:59:59.000Z

    The design of a long-trace surface profiler for the non-contact measurement of surface profile, slope error and curvature on cylindrical synchrotron radiation (SR) mirrors. The optical system is based upon the concept of a pencil-beam interferometer with an inherent large depth-of-field. The key feature of the optical system is the zero-path-difference beam splitter, which separates the laser beam into two colinear, variable-separation probe beams. A linear array detector is used to record the interference fringe in the image, and analysis of the fringe location as a function of scan position allows one to reconstruct the surface profile. The optical head is mounted on an air bearing slide with the capability to measure long aspheric optics, typical of those encountered in SR applications. A novel feature of the optical system is the use of a transverse "outrigger" beam which provides information on the relative alignment of the scan axis to the cylinder optic symmetry axis.

  6. Surface forces: Surface roughness in theory and experiment

    SciTech Connect (OSTI)

    Parsons, Drew F., E-mail: Drew.Parsons@anu.edu.au; Walsh, Rick B.; Craig, Vincent S. J. [Department of Applied Mathematics, Research School of Physical Sciences and Engineering, Australian National University, Canberra, ACT 0200 (Australia)] [Department of Applied Mathematics, Research School of Physical Sciences and Engineering, Australian National University, Canberra, ACT 0200 (Australia)

    2014-04-28T23:59:59.000Z

    A method of incorporating surface roughness into theoretical calculations of surface forces is presented. The model contains two chief elements. First, surface roughness is represented as a probability distribution of surface heights around an average surface height. A roughness-averaged force is determined by taking an average of the classic flat-surface force, weighing all possible separation distances against the probability distributions of surface heights. Second the model adds a repulsive contact force due to the elastic contact of asperities. We derive a simple analytic expression for the contact force. The general impact of roughness is to amplify the long range behaviour of noncontact (DLVO) forces. The impact of the elastic contact force is to provide a repulsive wall which is felt at a separation between surfaces that scales with the root-mean-square (RMS) roughness of the surfaces. The model therefore provides a means of distinguishing between “true zero,” where the separation between the average centres of each surface is zero, and “apparent zero,” defined by the onset of the repulsive contact wall. A normal distribution may be assumed for the surface probability distribution, characterised by the RMS roughness measured by atomic force microscopy (AFM). Alternatively the probability distribution may be defined by the histogram of heights measured by AFM. Both methods of treating surface roughness are compared against the classic smooth surface calculation and experimental AFM measurement.

  7. High temperature pressurized high frequency testing rig and test method

    DOE Patents [OSTI]

    De La Cruz, Jose; Lacey, Paul

    2003-04-15T23:59:59.000Z

    An apparatus is described which permits the lubricity of fuel compositions at or near temperatures and pressures experienced by compression ignition fuel injector components during operation in a running engine. The apparatus consists of means to apply a measured force between two surfaces and oscillate them at high frequency while wetted with a sample of the fuel composition heated to an operator selected temperature. Provision is made to permit operation at or near the flash point of the fuel compositions. Additionally a method of using the subject apparatus to simulate ASTM Testing Method D6079 is disclosed, said method involving using the disclosed apparatus to contact the faces of prepared workpieces under a measured load, sealing the workface contact point into the disclosed apparatus while immersing said contact point between said workfaces in a lubricating media to be tested, pressurizing and heating the chamber and thereby the fluid and workfaces therewithin, using the disclosed apparatus to impart a differential linear motion between the workpieces at their contact point until a measurable scar is imparted to at least one workpiece workface, and then evaluating the workface scar.

  8. DEVELOPMENT OF BURN TEST SPECIFICATIONS FOR FIRE PROTECTION MATERIALS IN RAM PACKAGES

    SciTech Connect (OSTI)

    Gupta, N.

    2010-03-03T23:59:59.000Z

    The regulations in 10 CFR 71 require that the radioactive material (RAM) packages must be able to withstand specific fire conditions given in 10 CFR 71.73 during Hypothetical Accident Conditions (HAC). This requirement is normally satisfied by extensive testing of full scale test specimens under required test conditions. Since fire test planning and execution is expensive and only provides a single snapshot into a package performance, every effort is made to minimize testing and supplement tests with results from computational thermal models. However, the accuracy of such thermal models depends heavily on the thermal properties of the fire insulating materials that are rarely available at the regulatory fire temperatures. To the best of authors knowledge no test standards exist that could be used to test the insulating materials and derive their thermal properties for the RAM package design. This paper presents a review of the existing industry fire testing standards and proposes testing methods that could serve as a standardized specification for testing fire insulating materials for use in RAM packages.

  9. Summary of Test Results for the Interagency Field Test &Evaluation...

    Broader source: Energy.gov (indexed) [DOE]

    Summary of Test Results for the Interagency Field Test &Evaluation of Wind Turbine - Radar Interference Mitigation Technologies Summary of Test Results for the Interagency Field...

  10. MITG Test Plan

    SciTech Connect (OSTI)

    Eck, Marshall B.

    1981-08-01T23:59:59.000Z

    The plan presented is for the testing of a prototypical slice of the Modular Isotopic Thermoelectric Generator (MITG). Cross Reference T48-1.

  11. RMOTC - Testing - Carbon Management

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    several years of site characterization and baseline studies necessary to advance CO2 injection tests that could yield important EOR and storage findings. Numerous...

  12. Optimum Statistical Test Procedure

    E-Print Network [OSTI]

    Rajesh Singh; Jayant Singh; Florentin Smarandache

    2009-04-10T23:59:59.000Z

    In this paper we obtain a test which minimizes the sum of the two error probabilities irrespective of whether $\\sigma^2$ is known or unknown.

  13. OMB MPI Tests

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    MPI Tests Description The Ohio MicroBenchmark suite is a collection of independent MPI message passing performance microbenchmarks developed and written at The Ohio State...

  14. Test 1 Solutions

    E-Print Network [OSTI]

    Microsoft account

    2015-03-03T23:59:59.000Z

    Mar 1, 2015 ... Test 1. Spring 2015. February 18, 2015. 1. (30 points) Christian has started to work today at Spears Corporation. Today is Christian's 42nd.

  15. RMOTC - Testing - Environmental

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    oilfield activities and facilities offers opportunities for testing new technologies for environmental protection and restoration in a real-world environment. Examples include pit...

  16. Solutions to Test 1

    E-Print Network [OSTI]

    Owner

    2014-03-06T23:59:59.000Z

    Math 373. Spring 2013. Test 1. February 12, 2013. 1. Tracy is receiving an annuity immediate with quarterly payments of 250 for 10 years. Tracy invests each ...

  17. Solutions to Test 1

    E-Print Network [OSTI]

    Microsoft account

    2015-01-14T23:59:59.000Z

    Jan 14, 2015 ... TEST 1. MATH 373. Fall 2014. October 7, 2014. 1. Ralph's Retail Stores have borrowed 100,000. Ralph's will repay the loan with annual ...

  18. Battery Safety Testing

    Broader source: Energy.gov (indexed) [DOE]

    Battery Safety Testing Christopher J. Orendorff, Leigh Anna M. Steele, Josh Lamb, and Scott Spangler Sandia National Laboratories 2014 Energy Storage Annual Merit Review...

  19. RMOTC - Testing - Alternative Energies

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    click here. RMOTC provides the opportunity for its partners to field test the latest alternative energy and environmental management technologies which have specific and...

  20. Accelerator Test Facility

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Test Facility Vitaly Yakimenko October 6-7, 2010 ATF User meeting DOE HE, S. Vigdor, ALD - (Contact) T. Ludlam Chair, Physics Department V. Yakimenko Director ATF, Accelerator...

  1. ACCELERATOR TEST FACILITY

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    LABORATORY PHYSICS DEPARTMENT Effective: 04012004 Page 1 of 2 Subject: Accelerator Test Facility - Linear Accelerator General Systems Guide Prepared by: Michael Zarcone...

  2. RMOTC - Library - Test Reports

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Test Reports All non-proprietary project reports that are approved for release are posted here. Many of RMOTC's projects have protection extended through a Cooperative Research and...

  3. Flexibility in Testing Configurations

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Technologies Laboratory and the National Solar Thermal Test Facility to advance the reliability, interconnectivity, and availability of solar technologies in the nation's...

  4. Solutions to Test 1

    E-Print Network [OSTI]

    jeffb_000

    2014-03-04T23:59:59.000Z

    STAT 479. Spring 2014. Test 1. February 18, 2014. 1. You are given the following empirical distribution of losses: 300 500 700 800 1000 1400. An insurance ...

  5. Enhancement of Topological Insulators Surface Conduction

    E-Print Network [OSTI]

    Yu, Xinxin

    2012-01-01T23:59:59.000Z

    Enhancement of Topological Insulators Surface Conduction AEnhancement of Topological Insulators Surface Conduction byTopological Insulator

  6. Near-Surface Engineered Environmental Barrier Integrity

    SciTech Connect (OSTI)

    Piet, S.J.; Breckenridge, R.P.

    2002-05-15T23:59:59.000Z

    The INEEL Environmental Systems Research and Analysis (ESRA) program has launched a new R and D project on Near-Surface Engineered Environmental Barrier Integrity to increase knowledge and capabilities for using engineering and ecological components to improve the integrity of near-surface barriers used to confine contaminants from the public and the environment. The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions and enable improved solutions for future cleanup decisions. The research is planned to (a) improve the knowledge of degradation mechanisms (weathering, biological, geological, chemical, radiological, and catastrophic) in times shorter than service life, (b) improve modeling of barrier degradation dynamics, (c) develop sensor systems to identify degradation prior to failure, and (d) provide a better basis for developing and testing of new barrier systems to increase reliability and reduce the risk of failure. Our project combine s selected exploratory studies (benchtop and field scale), coupled effects accelerated aging testing and the meso-scale, testing of new monitoring concepts, and modeling of dynamic systems. The performance of evapo-transpiration, capillary, and grout-based barriers will be examined.

  7. Near-Surface Engineered Environmental Barrier Integrity

    SciTech Connect (OSTI)

    Piet, Steven James; Breckenridge, Robert Paul; Beller, John Michael; Geesey, Gill Gregroy; Glenn, David Frankie; Jacobson, Jacob Jordan; Martian, Pete; Matthern, Gretchen Elise; Mattson, Earl Douglas; Porro, Indrek; Southworth, Finis Hio; Steffler, Eric Darwin; Stormberg, Angelica Isabel; Stormberg, Gregory John; Versteeg, Roelof Jan; White, Gregory J

    2002-08-01T23:59:59.000Z

    The INEEL Environmental Systems Research and Analysis (ESRA) program has launched a new R&D project on Near-Surface Engineered Environmental Barrier Integrity to increase knowledge and capabilities for using engineering and ecological components to improve the integrity of near-surface barriers used to confine contaminants from the public and the environment. The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions and enable improved solutions for future cleanup decisions. The research is planned to (a) improve the knowledge of degradation mechanisms (weathering, biological, geological, chemical, radiological, and catastrophic) in times shorter than service life, (b) improve modeling of barrier degradation dynamics, (c) develop sensor systems to identify degradation prior to failure, and (d) provide a better basis for developing and testing of new barrier systems to increase reliability and reduce the risk of failure. Our project combines selected exploratory studies (benchtop and field scale), coupled effects accelerated aging testing and the meso-scale, testing of new monitoring concepts, and modeling of dynamic systems. The performance of evapo- transpiration, capillary, and grout-based barriers will be examined.

  8. Sources for Pu in near surface air

    SciTech Connect (OSTI)

    Hartmann, G.; Thom, C.; Baechmann, K.

    1989-01-01T23:59:59.000Z

    This paper provides evidence that most of the Pu in the near surface air today is due to resuspension. Vertical and particle size distribution in near surface air over a period of three years were measured. The seasonal variations of Pu in air and the influence of meteorological parameters on these variations are shown. Samples were taken before the Chernobyl accident in an area where only Pu fallout from the atmospheric nuclear tests of the early sixties occurs. The comparison of the behavior of Pu with other trace elements, which were also measured, showed similar behavior of Pu and elements like Ca, Ti and Fe in near surface air. This confirms that most Pu is resuspended because the main source for these elements in air is the soil surface. Resuspension factors and resuspension rate are estimated for all measured elements. A resuspension factor of 0.8 X 10(-8) m-1 and a resuspension rate of 0.09 X 10(-9) s-1 is calculated for Pu.

  9. surface science ELSEVIER Surface Science384 (1997) 192 200

    E-Print Network [OSTI]

    surface science ELSEVIER Surface Science384 (1997) 192 200 An ab initio Hartree-Fock study Laboratory, Daresbury, Warrington, WA4 4AD, UK Received 3June 1996;acceptedfor publication 27 March 1997 arrangement is found consisting of localisedspinson the surface titanium atoms. © 1997Elsevier

  10. Animal Health Diagnostic Center Test and Fee Schedule Test Name Test Fee Discipline Test Days Lag** Samples Container Coolant Comments

    E-Print Network [OSTI]

    Keinan, Alon

    Animal Health Diagnostic Center Test and Fee Schedule Test Name Test Fee Discipline Test Days Lag** Samples Container Coolant Comments Equine Tests Equine Tests Acid Fast Stain (for bacteria) M-F 1-2 days 1 4 hours for equine. For more information, see Equine Cushing's Tests or AppendixC. For Equine only

  11. Surface tension and contact with soft elastic solids

    E-Print Network [OSTI]

    Robert W. Style; Callen Hyland; Rostislav Boltyanskiy; John S. Wettlaufer; Eric R. Dufresne

    2013-10-11T23:59:59.000Z

    Johnson-Kendall-Robert (JKR) theory is the basis of modern contact mechanics. It describes how two deformable objects adhere together, driven by adhesion energy and opposed by elasticity. However, it does not include solid surface tension, which also opposes adhesion by acting to flatten the surface of soft solids. We tested JKR theory to see if solid surface tension affects indentation behaviour. Using confocal microscopy, we characterised the indentation of glass particles into soft, silicone substrates. While JKR theory held for particles larger than a critical, elastocapillary lengthscale, it failed for smaller particles. Instead, adhesion of small particles mimicked the adsorption of particles at a fluid interface, with a size-independent contact angle between the undeformed surface and the particle given by a generalised version of Young's law. A simple theory quantitatively captures this behaviour, and explains how solid surface tension dominates elasticity for small-scale indentation of soft materials.

  12. Testing of the structural evaluation test unit

    SciTech Connect (OSTI)

    Ammerman, D.J.; Bobbe, J.G.

    1995-12-31T23:59:59.000Z

    In the evaluation of the safety of radioactive material transportation it is important to consider the response of Type B packages to environments more severe than that prescribed by the hypothetical accident sequence in Title 10 Part 71 of the Code of Federal Regulations (NRC 1995). The impact event in this sequence is a 9-meter drop onto an essentially unyielding target, resulting in an impact velocity of 13.4 m/s. The behavior of 9 packages when subjected to impacts more severe than this is not well known. It is the purpose of this program to evaluate the structural response of a test package to these environments. Several types of structural response are considered. Of primary importance is the behavior of the package containment boundary, including the bolted closure and 0-rings. Other areas of concern are loss of shielding capability due to lead slump and the deceleration loading of package contents, that may cause damage to them. This type of information is essential for conducting accurate risk assessments on the transportation of radioactive materials. Currently very conservative estimates of the loss of package protection are used in these assessments. This paper will summarize the results of a regulatory impact test and three extra-regulatory impact tests on a sample package.

  13. Understanding and Evaluating Extended Surfaces

    E-Print Network [OSTI]

    Ganapathy, V.

    Extended surfaces are widely used in heat transfer equipment in power and process plants. While various types of extended surfaces are used in the industry, this paper will limit the discussions to the widely used configurations in heat recovery...

  14. Reactor Testing and Qualification: Prioritized High-level Criticality Testing Needs

    SciTech Connect (OSTI)

    S. Bragg-Sitton; J. Bess; J. Werner; G. Harms; S. Bailey

    2011-09-01T23:59:59.000Z

    Researchers at the Idaho National Laboratory (INL) were tasked with reviewing possible criticality testing needs to support development of the fission surface power system reactor design. Reactor physics testing can provide significant information to aid in development of technologies associated with small, fast spectrum reactors that could be applied for non-terrestrial power systems, leading to eventual system qualification. Several studies have been conducted in recent years to assess the data and analyses required to design and build a space fission power system with high confidence that the system will perform as designed [Marcille, 2004a, 2004b; Weaver, 2007; Parry et al., 2008]. This report will provide a summary of previous critical tests and physics measurements that are potentially applicable to the current reactor design (both those that have been benchmarked and those not yet benchmarked), summarize recent studies of potential nuclear testing needs for space reactor development and their applicability to the current baseline fission surface power (FSP) system design, and provide an overview of a suite of tests (separate effects, sub-critical or critical) that could fill in the information database to improve the accuracy of physics modeling efforts as the FSP design is refined. Some recommendations for tasks that could be completed in the near term are also included. Specific recommendations on critical test configurations will be reserved until after the sensitivity analyses being conducted by Los Alamos National Laboratory (LANL) are completed (due August 2011).

  15. Stability at the surface

    SciTech Connect (OSTI)

    Chambers, Scott A.

    2014-12-05T23:59:59.000Z

    Metal oxides are ubiquitous as minerals in the terrestrial environment, as well as in a variety of technologically important structures such as electronic devices and heterogeneous catalysts. Within these various contexts, interfaces between oxides and gases, liquids and solids drive many critically important phenomena ranging from the uptake of contaminants in groundwater by redox-active minerals to the switching of the millions of transistors found in every cell phone and computer. Function is tied to structure. Therefore, fundamental understanding of the structure of oxide surfaces and interfaces is of crucial importance to the comprehension of a plethora of phenomena involving this broad class of materials.

  16. The Fuel Accident Condition Simulator (FACS) furnace system for high temperature performance testing of VHTR fuel

    SciTech Connect (OSTI)

    Paul A. Demkowicz; David V. Laug; Dawn M. Scates; Edward L. Reber; Lyle G. Roybal; John B. Walter; Jason M. Harp; Robert N. Morris

    2012-10-01T23:59:59.000Z

    The AGR-1 irradiation of TRISO-coated particle fuel specimens was recently completed and represents the most successful such irradiation in US history, reaching peak burnups of greater than 19% FIMA with zero failures out of 300,000 particles. An extensive post-irradiation examination (PIE) campaign will be conducted on the AGR-1 fuel in order to characterize the irradiated fuel properties, assess the in-pile fuel performance in terms of coating integrity and fission metals release, and determine the fission product retention behavior during high temperature safety testing. A new furnace system has been designed, built, and tested to perform high temperature accident tests. The Fuel Accident Condition Simulator furnace system is designed to heat fuel specimens at temperatures up to 2000 degrees C in helium while monitoring the release of volatile fission metals (e.g. Cs, Ag, Sr, and Eu), iodine, and fission gases (Kr, Xe). Fission gases released from the fuel to the sweep gas are monitored in real time using dual cryogenic traps fitted with high purity germanium detectors. Condensable fission products are collected on a plate attached to a water-cooled cold finger that can be exchanged periodically without interrupting the test. Analysis of fission products on the condensation plates involves dry gamma counting followed by chemical analysis of selected isotopes. This paper will describe design and operational details of the Fuel Accident Condition Simulator furnace system and the associated fission gas monitoring system, as well as preliminary system calibration results.

  17. RESULTS OF FIELD TESTING DOE

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    FIELD TESTING AT THE DEPARTMENT OF ENERGY, ROCKY MOUNTAIN OILFIELD TESTING CENTER May through September of 2011 RMOTC is an energy testing center that partners with industry to...

  18. Drop-in capsule testing of plutonium-based fuels in the Advanced Test Reactor

    SciTech Connect (OSTI)

    Chang, G.S.; Ryskamp, J.M.; Terry, W.K.; Ambrosek, R.G.; Palmer, A.J.; Roesener, R.A.

    1996-09-01T23:59:59.000Z

    The most attractive way to dispose of weapons-grade plutonium (WGPu) is to use it as fuel in existing light water reactors (LWRs) in the form of mixed oxide (MOX) fuel - i.e., plutonia (PuO[sub 2]) mixed with urania (UO[sub 2]). Before U.S. reactors could be used for this purpose, their operating licenses would have to be amended. Numerous technical issues must be resolved before LWR operating licenses can be amended to allow the use of MOX fuel. The proposed weapons-grade MOX fuel is unusual, even relative to ongoing foreign experience with reactor-grade MOX power reactor fuel. Some demonstration of the in- reactor thermal, mechanical, and fission gas release behavior of the prototype fuel will most likely be required in a limited number of test reactor irradiations. The application to license operation with MOX fuel must be amply supported by experimental data. The Advanced Test Reactor (ATR) at the Idaho National Engineering Laboratory (INEL) is capable of playing a key role in the irradiation, development, and licensing of these new fuel types. The ATR is a 250- MW (thermal) LWR designed to study the effects of intense radiation on reactor fuels and materials. For 25 years, the primary role of the ATR has been to serve in experimental investigations for the development of advanced nuclear fuels. Both large- and small-volume test positions in the ATR could be used for MOX fuel irradiation. The ATR would be a nearly ideal test bed for developing data needed to support applications to license LWRs for operation with MOX fuel made from weapons-grade plutonium. Furthermore, these data can be obtained more quickly by using ATR instead of testing in a commercial LWR. Our previous work in this area has demonstrated that it is technically feasible to perform MOX fuel testing in the ATR. This report documents our analyses of sealed drop-in capsules containing plutonium-based test specimens placed in various ATR positions.

  19. Advanced Test Reactor Tour

    SciTech Connect (OSTI)

    Miley, Don

    2011-01-01T23:59:59.000Z

    The Advanced Test Reactor at Idaho National Laboratory is the foremost nuclear materials test reactor in the world. This virtual tour describes the reactor, how experiments are conducted, and how spent nuclear fuel is handled and stored. For more information about INL research, visit http://www.facebook.com/idahonationallaboratory.

  20. Advanced Test Reactor Tour

    ScienceCinema (OSTI)

    Miley, Don

    2013-05-28T23:59:59.000Z

    The Advanced Test Reactor at Idaho National Laboratory is the foremost nuclear materials test reactor in the world. This virtual tour describes the reactor, how experiments are conducted, and how spent nuclear fuel is handled and stored. For more information about INL research, visit http://www.facebook.com/idahonationallaboratory.

  1. Cooperative Testing and Analysis

    E-Print Network [OSTI]

    Xie, Tao

    Cooperative Testing and Analysis: Tao Xie Peking University, China (2011-2012) North Carolina State Account for even half the total cost of software development [Beizer 90] Automated testing reduces manual to the user to get her help? Tool Human How does the user help the tool based on the info? Iterations

  2. Tests for Convergence Clubs

    E-Print Network [OSTI]

    Corrado, Luisa; Weeks, Melvyn

    2011-01-26T23:59:59.000Z

    In many applications common in testing for convergence the number of cross-sectional units is large and the number of time periods are few. In these situations tests which are founded upon an omnibus null hypothesis are characterised by a number...

  3. Chemical enhancement of surface deposition

    DOE Patents [OSTI]

    Patch, Keith D. (Lexington, MA); Morgan, Dean T. (Sudbury, MA)

    1997-07-29T23:59:59.000Z

    A method and apparatus for increasing the deposition of ions onto a surface, such as the adsorption of uranium ions on the detecting surface of a radionuclide detector. The method includes the step of exposing the surface to a complexing agent, such as a phosphate ion solution, which has an affinity for the dissolved species to be deposited on the surface. This provides, for example, enhanced sensitivity of the radionuclide detector.

  4. Method for lubricating contacting surfaces

    DOE Patents [OSTI]

    Dugger, Michael T. (Tijeras, NM); Ohlhausen, James A. (Albuquerque, NM); Asay, David B. (Boalsburg, PA); Kim, Seong H. (State College, PA)

    2011-12-06T23:59:59.000Z

    A method is provided for tribological lubrication of sliding contact surfaces, where two surfaces are in contact and in motion relative to each other, operating in a vapor-phase environment containing at least one alcohol compound at a concentration sufficiently high to provide one monolayer of coverage on at least one of the surfaces, where the alcohol compound continuously reacts at the surface to provide lubrication.

  5. Chemical enhancement of surface deposition

    DOE Patents [OSTI]

    Patch, K.D.; Morgan, D.T.

    1997-07-29T23:59:59.000Z

    A method and apparatus are disclosed for increasing the deposition of ions onto a surface, such as the adsorption of uranium ions on the detecting surface of a radionuclide detector. The method includes the step of exposing the surface to a complexing agent, such as a phosphate ion solution, which has an affinity for the dissolved species to be deposited on the surface. This provides, for example, enhanced sensitivity of the radionuclide detector. 16 figs.

  6. Dynamic Testing of Gasifier Refractory

    SciTech Connect (OSTI)

    Michael D. Mann; John P. Hurley

    2002-09-27T23:59:59.000Z

    As DOE continues to advance new power systems, materials issues are often pivotal in determining the ultimate efficiency that can be reached in the system. Refractory performance in slagging gasification represents one of these issues. The University of North Dakota (UND) Chemical Engineering Department in conjunction with the UND Energy & Environmental Research Center (EERC) have initiated a program to thoroughly examine the combined chemical (reaction and phase change) and physical (erosion) effects experienced by a variety of refractory materials during both normal operation and thermal cycling under slagging coal gasification conditions. The goal of this work is to devise a mechanism of refractory loss under these conditions. The focus of the proposed work is to test the corrosion resistance of commercially available refractories to flowing coal slag, and propose the mechanisms of corrosion for the conditions studied. Corrosion is the degradation of material surfaces or grain boundaries by chemical reactions with melts, liquids, or gases, causing loss of material and consequently a decrease in strength of the structure. In order to develop methods of reducing corrosion, the microstructure that is attacked must be identified along with the mechanism and rates of attack. Once these are identified, methods for reducing corrosion rates can be developed. The work will take advantage of equipment and experimental techniques developed at the EERC under funding from several DOE programs. The controlled-atmospheric dynamic corrodent application furnace (CADCAF) will be utilized to simulate refractory/slag interactions under dynamic conditions that more realistically simulate the environment in a slagging coal gasifier than any of the static tests used previously by refractory manufacturers and researchers. To date, efforts have focused on final shakedown of the CADCAF and obtaining representative samples of slag and refractory for testing.

  7. Nanomechanical testing system

    DOE Patents [OSTI]

    Vodnick, David James; Dwivedi, Arpit; Keranen, Lucas Paul; Okerlund, Michael David; Schmitz, Roger William; Warren, Oden Lee; Young, Christopher David

    2014-07-08T23:59:59.000Z

    An automated testing system includes systems and methods to facilitate inline production testing of samples at a micro (multiple microns) or less scale with a mechanical testing instrument. In an example, the system includes a probe changing assembly for coupling and decoupling a probe of the instrument. The probe changing assembly includes a probe change unit configured to grasp one of a plurality of probes in a probe magazine and couple one of the probes with an instrument probe receptacle. An actuator is coupled with the probe change unit, and the actuator is configured to move and align the probe change unit with the probe magazine and the instrument probe receptacle. In another example, the automated testing system includes a multiple degree of freedom stage for aligning a sample testing location with the instrument. The stage includes a sample stage and a stage actuator assembly including translational and rotational actuators.

  8. Air gun test evaluation

    SciTech Connect (OSTI)

    Carleton, J.J. II; Fox, L.; Rudy, C.R.

    1992-01-15T23:59:59.000Z

    A mechanical shock testing apparatus is used for testing the response of components subject to large accelerations in hostile environments. The test acceleration is provided by the impact of a bullet against a plate on which the component to be tested is mounted. This report describes a series of experiments that were performed to determine the dependence of the air gun test apparatus performance on incremental changes in the hardware configurations, changes in the pressure used to drive the bullet, and different accelerometers. The effect of variation of these experimental factors on the measured acceleration was determined using a Taguchi screening experimental design. Experimental settings were determined that can be used to operate the tester with a measured output within acceleration specifications.

  9. Cylinder Test Specification

    SciTech Connect (OSTI)

    Richard Catanach; Larry Hill; Herbert Harry; Ernest Aragon; Don Murk

    1999-10-01T23:59:59.000Z

    The purpose of the cylinder testis two-fold: (1) to characterize the metal-pushing ability of an explosive relative to that of other explosives as evaluated by the E{sub 19} cylinder energy and the G{sub 19} Gurney energy and (2) to help establish the explosive product equation-of-state (historically, the Jones-Wilkins-Lee (JWL) equation). This specification details the material requirements and procedures necessary to assemble and fire a typical Los Alamos National Laboratory (LANL) cylinder test. Strict adherence to the cylinder. material properties, machining tolerances, material heat-treatment and etching processes, and high explosive machining tolerances is essential for test-to-test consistency and to maximize radial wall expansions. Assembly and setup of the cylinder test require precise attention to detail, especially when placing intricate pin wires on the cylinder wall. The cylinder test is typically fired outdoors and at ambient temperature.

  10. TENSILE TESTING OF CARBON STEEL IN HIGH PRESSURE HYDROGEN

    SciTech Connect (OSTI)

    Duncan, A; Thad Adams, T; Ps Lam, P

    2007-05-02T23:59:59.000Z

    An infrastructure of new and existing pipelines and systems will be required to carry and to deliver hydrogen as an alternative energy source under the hydrogen economy. Carbon and low alloy steels of moderate strength are currently used in hydrogen delivery systems as well as in the existing natural gas systems. It is critical to understand the material response of these standard pipeline materials when they are subjected to pressurized hydrogen environments. The methods and results from a testing program to quantify hydrogen effects on mechanical properties of carbon steel pipeline and pipeline weld materials are provided. Tensile properties of one type of steel (A106 Grade B) in base metal, welded and heat affected zone conditions were tested at room temperature in air and high pressure (10.34 MPa or 1500 psig) hydrogen. A general reduction in the materials ability to plastically deform was noted in this material when specimens were tested in hydrogen. Furthermore, the primary mode of fracture was changed from ductile rupture in air to cleavage with secondary tearing in hydrogen. The mechanical test results will be applied in future analyses to evaluate service life of the pipelines. The results are also envisioned to be part of the bases for construction codes and structural integrity demonstrations for hydrogen service pipeline and vessels.

  11. Topological Surface States of Antimony

    E-Print Network [OSTI]

    Petta, Jason

    of the sample and keeping the tunneling current constant, one can obtain a topography of the surface (it~ | | ~ a) Topography of Cu(111) surface b) FT of the g-map c) Sketch of Brillouin Zone L. Petersen et alTopological Surface States of Antimony Masih Mehdizadeh 10.08.2012 #12;Outline Introduction

  12. 1, 351383, 2007 Greenland surface

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    TCD 1, 351­383, 2007 Greenland surface mass balance at the end of this century G. Krinner and N-resolution simulations of the surface mass balance of Greenland at the end of this century G. Krinner and N. Julien LGGE Correspondence to: G. Krinner (krinner@ujf-grenoble.fr) 351 #12;TCD 1, 351­383, 2007 Greenland surface mass

  13. 6, 1205712120, 2006 Surface tension

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    ACPD 6, 12057­12120, 2006 Surface tension: measurement, modelling and cloud activation D. O a Creative Commons License. Atmospheric Chemistry and Physics Discussions Surface tensions of multi­12120, 2006 Surface tension: measurement, modelling and cloud activation D. O. Topping et al. Title Page

  14. Testing of a Transport Cask for Research Reactor Spent Fuel - 13003

    SciTech Connect (OSTI)

    Mourao, Rogerio P.; Leite da Silva, Luiz [Centro de Desenvolvimento da Tecnologia Nuclear, Belo Horizonte (Brazil)] [Centro de Desenvolvimento da Tecnologia Nuclear, Belo Horizonte (Brazil); Miranda, Carlos A.; Mattar Neto, Miguel [Instituto de Pesquisas Energeticas e Nucleares, Sao Paulo (Brazil)] [Instituto de Pesquisas Energeticas e Nucleares, Sao Paulo (Brazil); Quintana, Jose F.A.; Saliba, Roberto O. [Comision Nacional de Energia Atomica, Bariloche (Argentina)] [Comision Nacional de Energia Atomica, Bariloche (Argentina); Novara, Oscar E. [Comision Nacional de Energia Atomica, Buenos Aires (Argentina)] [Comision Nacional de Energia Atomica, Buenos Aires (Argentina)

    2013-07-01T23:59:59.000Z

    Since the beginning of the last decade three Latin American countries that operate research reactors - Argentina, Brazil and Chile - have been joining efforts to improve the regional capability in the management of spent fuel elements from the TRIGA and MTR reactors operated in the region. A main drive in this initiative, sponsored by the International Atomic Energy Agency, is the fact that no definite solution regarding the back end of the research reactor fuel cycle has been taken by any of the participating country. However, any long-term solution - either disposition in a repository or storage away from reactor - will involve at some stage the transportation of the spent fuel through public roads. Therefore, a licensed cask that provides adequate shielding, assurance of subcriticality, and conformance to internationally accepted safety, security and safeguards regimes is considered a strategic part of any future solution to be adopted at a regional level. As a step in this direction, a packaging for the transport of irradiated fuel for MTR and TRIGA research reactors was designed by the tri-national team and a half-scale model equipped with the MTR version of the internal basket was constructed in Argentina and Brazil and tested in Brazil. Three test campaigns have been carried out so far, covering both normal conditions of transportation and hypothetical accident conditions. After failing the tests in the first two test series, the specimen successfully underwent the last test sequence. A second specimen, incorporating the structural improvements in view of the previous tests results, will be tested in the near future. Numerical simulations of the free drop and thermal tests are being carried out in parallel, in order to validate the computational modeling that is going to be used as a support for the package certification. (authors)

  15. Influence of Heat Treatment on Mercury Cavitation Resistance of Surface Hardened 316LN Stainless Steel

    SciTech Connect (OSTI)

    Pawel, Steven J [ORNL; Hsu, Julia [Massachusetts Institute of Technology (MIT)

    2010-11-01T23:59:59.000Z

    The cavitation-erosion resistance of carburized 316LN stainless steel was significantly degraded but not destroyed by heat treatment in the temperature range 500-800 C. The heat treatments caused rejection of some carbon from the carburized layer into an amorphous film that formed on each specimen surface. Further, the heat treatments encouraged carbide precipitation and reduced hardness within the carburized layer, but the overall change did not reduce surface hardness fully to the level of untreated material. Heat treatments as short as 10 min at 650 C substantially reduced cavitation-erosion resistance in mercury, while heat treatments at 500 and 800 C were found to be somewhat less detrimental. Overall, the results suggest that modest thermal excursions perhaps the result of a weld made at some distance to the carburized material or a brief stress relief treatment will not render the hardened layer completely ineffective but should be avoided to the greatest extent possible.

  16. Edit Test Options Page 1 Edit Test Options

    E-Print Network [OSTI]

    Xu, Shouhuai

    Edit Test Options Page 1 Edit Test Options Format Test Information 1. Enter a Name for the Test. 2. Choose a color for the title text of the Test. (Optional) 3. Enter a Description in the Text Box. The description is visible to Students before they click on the link to take the Test. (Optional) 4. If you want

  17. Advancing Toward Test Automation through Effective Manual Testing

    E-Print Network [OSTI]

    . This paper will walk through a best practice scenario for using Manual Tester to more naturally organize test Automation through Effective Manual Testing Bob Levy, Lead Product Manager ­ Functional Test Dennis ElenburgAdvancing Toward Test Automation through Effective Manual Testing May 2005 Advancing Toward Test

  18. Development of a pilot-scale kinetic extruder feeder system and test program. Phase I report

    SciTech Connect (OSTI)

    None

    1982-03-01T23:59:59.000Z

    This report describes the work done under Phase I, the moisture tolerance testing of the Kinetic Extruder. The following coals were used in the test program: Western Bituminous (Utah), Eastern Bituminous (Pennsylvania), North Dakota Lignite, Sub-Bituminous (Montana), and Eastern Bituminous coal mixed with 20-percent Limestone. The coals were initially tested at the as-received moisture level and subsequently tested after surface moisture was added by water spray. Test results and recommendations for future research and development work are presented.

  19. Investigation of IAQ-Relevant Surface Chemistry and Emissions on HVAC Filter Materials

    SciTech Connect (OSTI)

    Destaillats, Hugo; Fisk, William J.

    2010-02-01T23:59:59.000Z

    Chemical reactions involving ozone of outdoor origin and indoor materials are known to be significant sources of formaldehyde and other irritant gas-phase oxidation products in the indoor environment. HVAC filters are exposed to particularly high ozone concentrations--close to outdoor levels. In this study, we investigated chemical processes taking place on the surface of filters that included fiberglass, polyester, cotton/polyester blend and synthetic (e.g., polyolefin) filter media. Ozone reactions were studied on unused filter media, and on filters that were deployed for 3 months in two different locations: at the Lawrence Berkeley National Laboratory and at the Port of Oakland. Specimens from each filter were exposed to ozone under controlled conditions in a laboratory flow tube at a constant flow of dry or humidified air (50percent relative humidity). Ozone was generated with a UV source upstream of the flow tube, and monitored using a photometric detector. Ozone breakthrough curves were recorded for each sample exposed to ~;;150 ppbv O3 for periods of ~;;1000 min, from which we estimated their uptake rate. Most experiments were performed at 1.3 L/min (corresponding to a face velocity of 0.013 m/s), except for a few tests performed at a higher airflow rate, to obtain a face velocity of 0.093 m/s, slightly closer to HVAC operation conditions. Formaldehyde and acetaldehyde, two oxidation byproducts, were collected downstream of the filter and quantified. Emissions of these volatile aldehydes were consistently higher under humidified air than under dry conditions, at which levels were near the limit of detection. Our results confirm that there are significant reactions of ozone as air containing ozone flows through HVAC filters, particularly when the filters are loaded with particles and the air is humidified. The amount of ozone reacted was not clearly related to the types of filter media, e.g., fiberglass versus synthetic. Specific fiberglass filters that were coated with an impaction oil showed significantly higher formaldehyde emissions than most other samples. Those emissions were magnified in the presence of particles (i.e., in used filters), and were observed even in the absence of ozone, which suggests that hydrolysis of filter binder or tackifier additives may be the reason for those high emissions. Mass balance calculations indicate that the emission rates of formaldehyde and acetaldehyde from the filters are generally not large enough to substantially increase indoor formaldehyde or acetaldehyde concentrations.

  20. Tools for measuring surface cleanliness

    DOE Patents [OSTI]

    Schroder, Mark Stewart (Hendersonville, NC); Woodmansee, Donald Ernest (Simpsonville, SC); Beadie, Douglas Frank (Greenville, SC)

    2002-01-01T23:59:59.000Z

    A procedure and tools for quantifying surface cleanliness are described. Cleanliness of a target surface is quantified by wiping a prescribed area of the surface with a flexible, bright white cloth swatch, preferably mounted on a special tool. The cloth picks up a substantial amount of any particulate surface contamination. The amount of contamination is determined by measuring the reflectivity loss of the cloth before and after wiping on the contaminated system and comparing that loss to a previous calibration with similar contamination. In the alternative, a visual comparison of the contaminated cloth to a contamination key provides an indication of the surface cleanliness.