National Library of Energy BETA

Sample records for test specimen surface

  1. Fracture toughness results and preliminary analysis for International Cooperative Test Program on specimens containing surface cracks

    SciTech Connect (OSTI)

    Reuter, W.G.; Elfer, N.C.; Hull, D.A.; Newman, J.C. Jr.; Munz, D.; Panontin, T.L.

    1997-12-31

    Specimens containing surface cracks were tested in either tension or bending to compare the stress intensity factor at failure with plane strain fracture toughness (K{sub Ic}) in an International Cooperative Test Program. The material was heat treated to {sigma}{sub ys} = 1 587 MPa and K{sub Ic} = 54 MPa m{sub 1/2}. Because substantial stable crack growth occurred for some specimens, the test plan was modified to include detecting the onset of crack growth. It is shown that P{sub max} and the original fatigue precrack size cannot be employed to calculate K{sub max} for comparison with K{sub Ic} when significant stable crack growth occurs. However, using P{sub init} (load at which stable crack growth is initiated) and the original fatigue precrack size to calculate K{sub max} or K{sub {phi}=30{degree}} provides a very useful comparison with K{sub Ic}. The influence of variations in fatigue precrack configuration on test results are also discussed.

  2. Baseline Test Specimen Machining Report

    SciTech Connect (OSTI)

    mark Carroll

    2009-08-01

    The Next Generation Nuclear Plant (NGNP) Project is tasked with selecting a high temperature gas reactor technology that will be capable of generating electricity and supplying large amounts of process heat. The NGNP is presently being designed as a helium-cooled high temperature gas reactor (HTGR) with a large graphite core. The graphite baseline characterization project is conducting the research and development (R&D) activities deemed necessary to fully qualify nuclear-grade graphite for use in the NGNP reactor. Establishing nonirradiated thermomechanical and thermophysical properties by characterizing lot-to-lot and billet-to-billet variations (for probabilistic baseline data needs) through extensive data collection and statistical analysis is one of the major fundamental objectives of the project. The reactor core will be made up of stacks of graphite moderator blocks. In order to gain a more comprehensive understanding of the varying characteristics in a wide range of suitable graphites, any of which can be classified as nuclear grade, an experimental program has been initiated to develop an extensive database of the baseline characteristics of numerous candidate graphites. Various factors known to affect the properties of graphite will be investigated, including specimen size, spatial location within a graphite billet, specimen orientation within a billet (either parallel to [P] or transverse to [T] the long axis of the as-produced billet), and billet-to-billet variations within a lot or across different production lots. Because each data point is based on a certain position within a given billet of graphite, particular attention must be paid to the traceability of each specimen and its spatial location and orientation within each billet. The evaluation of these properties is discussed in the Graphite Technology Development Plan (Windes et. al, 2007). One of the key components in the evaluation of these graphite types will be mechanical testing on

  3. Apparatus for automated testing of biological specimens

    DOE Patents [OSTI]

    Layne, Scott P.; Beugelsdijk, Tony J.

    1999-01-01

    An apparatus for performing automated testing of infections biological specimens is disclosed. The apparatus comprise a process controller for translating user commands into test instrument suite commands, and a test instrument suite comprising a means to treat the specimen to manifest an observable result, and a detector for measuring the observable result to generate specimen test results.

  4. Influence of thermal conditioning media on Charpy specimen test temperature

    SciTech Connect (OSTI)

    Nanstad, R.K.; Swain, R.L.; Berggren, R.G.

    1989-01-01

    The Charpy V-notch (CVN) impact test is used extensively for determining the toughness of structural materials. Research programs in many technologies concerned with structural integrity perform such testing to obtain Charpy energy vs temperature curves. American Society for Testing and Materials Method E 23 includes rather strict requirements regarding determination and control of specimen test temperature. It specifies minimum soaking times dependent on the use of liquids or gases as the medium for thermally conditioning the specimen. The method also requires that impact of the specimen occur within 5 s removal from the conditioning medium. It does not, however, provide guidance regarding choice of conditioning media. This investigation was primarily conducted to investigate the changes in specimen temperature which occur when water is used for thermal conditioning. A standard CVN impact specimen of low-alloy steel was instrumented with surface-mounted and embedded thermocouples. Dependent on the media used, the specimen was heated or cooled to selected temperatures in the range {minus}100 to 100{degree}C using cold nitrogen gas, heated air, acetone and dry ice, methanol and dry ice, heated oil, or heated water. After temperature stabilization, the specimen was removed from the conditioning medium while the temperatures were recorded four times per second from all thermocouples using a data acquisition system and a computer. The results show that evaporative cooling causes significant changes in the specimen temperatures when water is used for conditioning. Conditioning in the other media did not result in such significant changes. The results demonstrate that, even within the guidelines of E 23, significant test temperature changes can occur which may substantially affect the Charpy impact test results if water is used for temperature conditioning. 7 refs., 11 figs.

  5. Apparatus and method for fatigue testing of a material specimen...

    Office of Scientific and Technical Information (OSTI)

    fluid environment Citation Details In-Document Search Title: Apparatus and method for fatigue testing of a material specimen in a high-pressure fluid environment The ...

  6. Apparatus for tensile testing plate-type ceramic specimens

    DOE Patents [OSTI]

    Liu, K.C.

    1993-08-24

    Apparatus is described for gripping a plate-type tensile specimen having generally T-shaped end regions in a dynamic tension fatigue testing apparatus comprising an annular housing having an open-ended elongated cavity therein, a plurality of hydraulic piston means supported by the housing in a spaced array about the cavity, and a specimen-supporting plate means overlying the piston means at one end of the elongated cavity and displaceable by said piston means in a longitudinal direction with respect to the longitudinal axis of the cavity, said apparatus for gripping a flat plate-type tensile specimen comprising: a pair of elongated pull rods each having oppositely disposed first and second end regions; a pair of mounting means carried by said plate means with each mounting means for pivotally attaching the first end region of each of said pull rods in a central region of said plate means for supporting said pair of elongated pull rods in a side-by-side relationship along a common longitudinal centerline within said cavity; recess means in the second end region of each of said pull rods in adjacently disposed surface regions thereof with said recess means facing one another and each adapted to receive one side of one of the generally T-shaped end regions of the plate-type tensile specimen; and load-bearing means positionable in each of said recess means and adapted to bear against a shoulder on each side of the generally T-shaped end region of the plate-type tensile specimen when a tensile loading is applied thereon.

  7. Localized surface plasmon assisted contrast microscopy for ultrathin transparent specimens

    SciTech Connect (OSTI)

    Wei, Feifei; Lu, Dylan; Aguinaldo, Ryan; Ma, Yicong; Sinha, Sunil K.; Liu, Zhaowei

    2014-10-20

    We demonstrate a high contrast imaging technique, termed localized surface plasmon assisted contrast microscopy, by combining localized surface plasmon resonances (LSPR) and dark-field microscopy technique. Due to the sensitive response of LSPR to the refractive index of the surrounding media, this technique is capable of converting a small refractive index difference to a change in scattering intensity, resulting in a high-contrast, diffraction limited image of a thin unstained specimen with small, gradual refractive-index variation.

  8. Apparatus for tensile testing plate-type ceramic specimens

    DOE Patents [OSTI]

    Liu, Kenneth C.

    1993-01-01

    Apparatus for tensile testing plate-type ceramic specimens having dogbone- or T-shaped end sections without introducing bending stresses in the specimens during the application of a dynamic tensile loading on the specimens is described. A pair of elongated pull rods disposed in a side-by-side relationship are used to grip the shoulders on each T-shaped end section. The pull rods are pivotally attached to a piston-displaceable, disk-shaped member so as to be longitudinally movable with respect to one another effecting the self-alignment thereof with the shoulders on the T-shaped end sections of the specimen to compensate for shoulders being located in different longitudinal positions.

  9. Electrochemical polishing of thread fastener test specimens of nickel-chromium iron alloys

    DOE Patents [OSTI]

    Kephart, Alan R.

    1991-01-01

    An electrochemical polishing device and method for selective anodic dissolution of the surface of test specimens comprised, for example, of nickel-chromium-iron alloys, which provides for uniform dissolution at the localized sites to remove metal through the use of a coiled wire electrode (cathode) placed in the immediate proximity of the working, surface resulting in a polished and uniform grain boundary.

  10. Thick Concrete Specimen Construction, Testing, and Preliminary Analysis

    SciTech Connect (OSTI)

    Clayton, Dwight A.; Hoegh, Kyle; Khazanovich, Lev

    2015-03-01

    The purpose of the U.S. Department of Energy Office of Nuclear Energy’s Light Water Reactor Sustainability (LWRS) Program is to develop technologies and other solutions that can improve the reliability, sustain the safety, and extend the operating lifetimes of nuclear power plants (NPPs) beyond 60 years. Since many important safety structures in an NPP are constructed of concrete, inspection techniques must be developed and tested to evaluate the internal condition. In-service containment structures generally do not allow for the destructive measures necessary to validate the accuracy of these inspection techniques. This creates a need for comparative testing of the various nondestructive evaluation (NDE) measurement techniques on concrete specimens with known material properties, voids, internal microstructure flaws, and reinforcement locations. A preliminary report detailed some of the challenges associated with thick reinforced concrete sections and prioritized conceptual designs of specimens that could be fabricated to represent NPP concrete structures for using in NDE evaluation comparisons. This led to the construction of the concrete specimen presented in this report, which has sufficient reinforcement density and cross-sectional size to represent an NPP containment wall. Details on how a suitably thick concrete specimen was constructed are presented, including the construction materials, final nominal design schematic, as well as formwork and rigging required to safely meet the desired dimensions of the concrete structure. The report also details the type and methods of forming the concrete specimen as well as information on how the rebar and simulated defects were embedded. Details on how the resulting specimen was transported, safely anchored, and marked to allow access for systematic comparative NDE testing of defects in a representative NPP containment wall concrete specimen are also given. Data collection using the MIRA Ultrasonic NDE equipment and

  11. Metallographic analysis of irradiated RERTR-3 fuel test specimens.

    SciTech Connect (OSTI)

    Meyer, M. K.; Hofman, G. L.; Strain, R. V.; Clark, C. R.; Stuart, J. R.

    2000-11-08

    The RERTR-3 irradiation test was designed to investigate the irradiation behavior of aluminum matrix U-MO alloy dispersion fuels under high-temperature, high-fission-rate conditions. Initial postirradiation examination of RERTR-3 fuel specimens has concentrated on binary U-MO atomized fuels. The rate of matrix aluminum depletion was found to be higher than predictions based on low temperature irradiation data. Wavelength Dispersive X-ray Spectroscopy (WDS) indicates that aluminum is present in the interior of the fuel particles. WDS data is supported by a mass and volume balance calculation performed on the basis of image analysis results. The depletion of matrix aluminum seems to have no detrimental effects on fuel performance under the conditions tested to date.

  12. Load apparatus and method for bolt-loaded compact tension test specimen

    DOE Patents [OSTI]

    Buescher, Jr., Brent J.; Lloyd, W. Randolph; Ward, Michael B.; Epstein, Jonathan S.

    1997-01-01

    A bolt-loaded compact tension test specimen load apparatus includes: a) a body having first and second opposing longitudinal ends, the first end comprising an externally threaded portion sized to be threadedly received within the test specimen threaded opening; b) a longitudinal loading rod having first and second opposing longitudinal ends, the loading rod being slidably received in a longitudinal direction within the body internally through the externally threaded portion and slidably extending longitudinally outward of the body first longitudinal end; c) a force sensitive transducer slidably received within the body and positioned to engage relative to the loading rod second longitudinal end; and d) a loading bolt threadedly received relative to the body, the loading bolt having a bearing end surface and being positioned to bear against the transducer to forcibly sandwich the transducer between the loading bolt and loading rod. Also disclosed is a method of in situ determining applied force during crack propagation in a bolt-loaded compact tension test specimen.

  13. Load apparatus and method for bolt-loaded compact tension test specimen

    DOE Patents [OSTI]

    Buescher, B.J. Jr.; Lloyd, W.R.; Ward, M.B.; Epstein, J.S.

    1997-02-04

    A bolt-loaded compact tension test specimen load apparatus includes: (a) a body having first and second opposing longitudinal ends, the first end comprising an externally threaded portion sized to be threadedly received within the test specimen threaded opening; (b) a longitudinal loading rod having first and second opposing longitudinal ends, the loading rod being slidably received in a longitudinal direction within the body internally through the externally threaded portion and slidably extending longitudinally outward of the body first longitudinal end; (c) a force sensitive transducer slidably received within the body and positioned to engage relative to the loading rod second longitudinal end; and (d) a loading bolt threadedly received relative to the body, the loading bolt having a bearing end surface and being positioned to bear against the transducer to forcibly sandwich the transducer between the loading bolt and loading rod. Also disclosed is a method of in situ determining applied force during crack propagation in a bolt-loaded compact tension test specimen. 6 figs.

  14. Capillary test specimen, system, and methods for in-situ visualization of capillary flow and fillet formation

    DOE Patents [OSTI]

    Hall, Aaron C.; Hosking, F. Michael ,; Reece, Mark

    2003-06-24

    A capillary test specimen, method, and system for visualizing and quantifying capillary flow of liquids under realistic conditions, including polymer underfilling, injection molding, soldering, brazing, and casting. The capillary test specimen simulates complex joint geometries and has an open cross-section to permit easy visual access from the side. A high-speed, high-magnification camera system records the location and shape of the moving liquid front in real-time, in-situ as it flows out of a source cavity, through an open capillary channel between two surfaces having a controlled capillary gap, and into an open fillet cavity, where it subsequently forms a fillet on free surfaces that have been configured to simulate realistic joint geometries. Electric resistance heating rapidly heats the test specimen, without using a furnace. Image-processing software analyzes the recorded images and calculates the velocity of the moving liquid front, fillet contact angles, and shape of the fillet's meniscus, among other parameters.

  15. Improved flywheel materials : characterization of nanofiber modified flywheel test specimen.

    SciTech Connect (OSTI)

    Boyle, Timothy J.; Bell, Nelson Simmons; Ehlen, Mark Andrew; Anderson, Benjamin John; Miller, William Kenneth

    2013-09-01

    As alternative energy generating devices (i.e., solar, wind, etc) are added onto the electrical energy grid (AC grid), irregularities in the available electricity due to natural occurrences (i.e., clouds reducing solar input or wind burst increasing wind powered turbines) will be dramatically increased. Due to their almost instantaneous response, modern flywheel-based energy storage devices can act a mechanical mechanism to regulate the AC grid; however, improved spin speeds will be required to meet the necessary energy levels to balance thesegreen' energy variances. Focusing on composite flywheels, we have investigated methods for improving the spin speeds based on materials needs. The so-called composite flywheels are composed of carbon fiber (C-fiber), glass fiber, and aglue' (resin) to hold them together. For this effort, we have focused on the addition of fillers to the resin in order to improve its properties. Based on the high loads required for standard meso-sized fillers, this project investigated the utility of ceramic nanofillers since they can be added at very low load levels due to their high surface area. The impact that TiO2 nanowires had on the final strength of the flywheel material was determined by athree-point-bend' test. The results of the introduction of nanomaterials demonstrated an increase instrength' of the flywheel's C-fiber-resin moiety, with an upper limit of a 30% increase being reported. An analysis of the economic impact concerning the utilization of the nanowires was undertaken and after accounting for new-technology and additional production costs, return on improved-nanocomposite investment was approximated at 4-6% per year over the 20-year expected service life. Further, it was determined based on the 30% improvement in strength, this change may enable a 20-30% reduction in flywheel energy storage cost (%24/kW-h).

  16. The effect of specimen strength and thickness on cracking susceptibility during the Sigmajig weldability test

    SciTech Connect (OSTI)

    Lippold, J.C.; Shademan, S.S.; Baeslack, W.A. III

    1996-03-01

    The effects of yield strength and specimen thickness on the threshold stress for solidification cracking using the Sigmajig weldability test have been determined for A-286 stainless steel. An increase in test specimen yield strength results in a decrease in the threshold stress for cracking. This decrease is attributed in part to a decrease in the width of the plastically deformed weld zone as the yield strength increases, which enhances strain localization in this region and promotes solidification cracking. Over a range of yield strengths, an increase in specimen thickness generally results in higher threshold stress for cracking, which are attributed to an increased inherent restraint. The relationship between weld pool shape, the solidification grain and the fracture stress during transverse loading has been investigated by performing hot-ductility tests of weld fusion zone specimens. The hot-ductility behavior of specimens produced from welds exhibiting elliptical and teardrop-shaped weld pools is comparable. However, specimens produced from welds that exhibit a teardrop-shaped weld pool fracture along the fusion zone centerline above the nil-ductility temperature, whereas specimens produced from welds that exhibit an elliptical-shaped weld pool fracture in the partially melted zone. A correlation was observed between the fracture stress measured by hot-ductility testing and threshold stresses measured using the Sigmajig test.

  17. Modeling and Testing Miniature Torsion Specimens for SiC Joining Development Studies for Fusion

    SciTech Connect (OSTI)

    Henager, Charles H.; Nguyen, Ba Nghiep; Kurtz, Richard J.; Roosendaal, Timothy J.; Borlaug, Brennan A.; Ferraris, Monica; Ventrella, Andrea; Katoh, Yutai

    2015-08-19

    The international fusion community has designed a miniature torsion specimen for neutron irradiation studies of joined SiC and SiC/SiC composite materials. Miniature torsion joints based on this specimen design were fabricated using displacement reactions between Si and TiC to produce Ti3SiC2 + SiC joints with CVD-SiC and tested in torsion-shear prior to and after neutron irradiation. However, many of these miniature torsion specimens fail out-of-plane within the CVD-SiC specimen body, which makes it problematic to assign a shear strength value to the joints and makes it difficult to compare unirradiated and irradiated joint strengths to determine the effects of the irradiation. Finite element elastic damage and elastic-plastic damage models of miniature torsion joints are developed that indicate shear fracture is likely to occur within the body of the joined sample and cause out-of-plane failures for miniature torsion specimens when a certain modulus and strength ratio between the joint material and the joined material exists. The model results are compared and discussed with regard to unirradiated and irradiated joint test data for a variety of joint materials. The unirradiated data includes Ti3SiC2 + SiC/CVD-SiC joints with tailored joint moduli, and includes steel/epoxy and CVD-SiC/epoxy joints. The implications for joint data based on this sample design are discussed.

  18. COMPARISON OF SHEAR STRENGTH OF CERAMIC JOINTS DETERMINED BY VARIOUS TEST METHODS WITH SMALL SPECIMENS

    SciTech Connect (OSTI)

    Katoh, Yutai; Kiggans Jr, James O; Khalifa, Hesham; Back, Christina A.; Hinoki, Tatsuya; Ferraris, Monica

    2015-01-01

    Four different shear test methods i.e. doubled notched shear test, asymmetrical four point bend test, Iosipescu test, and torsion test, were investigated for their ability to evaluate one standard SiC to SiC ceramic brittle joint while using small size specimens. Double notched shear test showed higher stress concentration at the notch base and a lower nominal shear strength. Both asymmetrical four point bend test and Iosipescu test utilized epoxy jointed metal extensors, which failed during test and caused misalignment and tensile type of failure. Torsion test can deliver true shear loading. However, base material failure was observed for the torsion joint samples in this study. None of the tests can successfully induce true shear failure of the joint because the joint is stronger and tougher than the SiC substrate. Torsion test appears to be promising because of the pure shear loading, less stress concentration, and easy alignment.

  19. Recent Accomplishments in the Irradiation Testing of Engineering-Scale Monolithic Fuel Specimens

    SciTech Connect (OSTI)

    N.E. Woolstenhulme; D.M. Wachs; M.K. Meyer; H.W. Glunz; R.B. Nielson

    2012-10-01

    The US fuel development team is focused on qualification and demonstration of the uranium-molybdenum monolithic fuel including irradiation testing of engineering-scale specimens. The team has recently accomplished the successful irradiation of the first monolithic multi-plate fuel element assembly within the AFIP-7 campaign. The AFIP-6 MKII campaign, while somewhat truncated by hardware challenges, exhibited successful irradiation of a large-scale monolithic specimen under extreme irradiation conditions. The channel gap and ultrasonic data are presented for AFIP-7 and AFIP-6 MKII, respectively. Finally, design concepts are summarized for future irradiations such as the base fuel demonstration and design demonstration experiment campaigns.

  20. Material Open Test Assembly Specimen Retrieval from Hanford's Shielded Material Facility

    SciTech Connect (OSTI)

    Valdez, Patrick LJ; Rinker, Michael W.

    2009-06-14

    Hanford’s 324 Building, the Shielded Material Facility (SMF), was developed to provide containment for research and fabrication development studies on highly radioactive metallic and ceramic nuclear reactor fuels and structural materials. Between 1983 and 1992, the SMF was used in support of the Department of Energy (DOE)-funded Fast Flux Test Facility (FFTF) Materials Open Test Assembly (MOTA) program. In this program, metallurgical specimens were irradiated in FFTF and then sent to SMF for processing and storage in two cabinets. This effort was abruptly ended in early 1990s due to programmatic shifts within the DOE, leaving many specimens unexamined. In recent years, these specimens have become of high value to new DOE programs. Pacific Northwest National Laboratory (PNNL) was tasked with retrieving specimens from one of the cabinets in support of fuel clad and duct development for the Advanced Fuel Cycle Initiative. Cesium contamination of the cell and failure of the overhead crane system utilized for opening the cabinets prevented PNNL from using the built-in hot cell equipment to gain access to the cabinets. PNNL designed and tested a lifting device to fit through a standard 10 inch diameter mechanical manipulator port in the SMF South Cell wall. The tool was successfully deployed in June 2008 with the support of Washington Closure Hanford.

  1. Apparatus and method for fatigue testing of a material specimen in a high-pressure fluid environment

    DOE Patents [OSTI]

    Wang, Jy-An; Feng, Zhili; Anovitz, Lawrence M; Liu, Kenneth C

    2013-06-04

    The invention provides fatigue testing of a material specimen while the specimen is disposed in a high pressure fluid environment. A specimen is placed between receivers in an end cap of a vessel and a piston that is moveable within the vessel. Pressurized fluid is provided to compression and tension chambers defined between the piston and the vessel. When the pressure in the compression chamber is greater than the pressure in the tension chamber, the specimen is subjected to a compression force. When the pressure in the tension chamber is greater than the pressure in the compression chamber, the specimen is subjected to a tension force. While the specimen is subjected to either force, it is also surrounded by the pressurized fluid in the tension chamber. In some examples, the specimen is surrounded by hydrogen.

  2. Manipulator having thermally conductive rotary joint for transferring heat from a test specimen

    DOE Patents [OSTI]

    Haney, Steven J.; Stulen, Richard H.; Toly, Norman F.

    1985-01-01

    A manipulator for rotatably moving a test specimen in an ultra-high vacuum chamber includes a translational unit movable in three mutually perpendicular directions. A manipulator frame is rigidly secured to the translational unit for rotatably supporting a rotary shaft. A first copper disc is rigidly secured to an end of the rotary shaft for rotary movement within the vacuum chamber. A second copper disc is supported upon the first disc. The second disc receives a cryogenic cold head and does not rotate with the first disc. A sapphire plate is interposed between the first and second discs to prevent galling of the copper material while maintaining high thermal conductivity between the first and second discs. A spring is disposed on the shaft to urge the second disc toward the first disc and compressingly engage the interposed sapphire plate. A specimen mount is secured to the first disc for rotation within the vacuum chamber. The specimen maintains high thermal conductivity with the second disc receiving the cryogenic transfer line.

  3. Manipulator having thermally conductive rotary joint for transferring heat from a test specimen

    DOE Patents [OSTI]

    Haney, S.J.; Stulen, R.H.; Toly, N.F.

    1983-05-03

    A manipulator for rotatably moving a test specimen in an ultra-high vacuum chamber includes a translational unit movable in three mutually perpendicular directions. A manipulator frame is rigidly secured to the translational unit for rotatably supporting a rotary shaft. A first copper disc is rigidly secured to an end of the rotary shaft for rotary movement within the vacuum chamber. A second copper disc is supported upon the first disc. The second disc receives a cryogenic cold head and does not rotate with the first disc. The second disc receives a cryogenic cold head and does not rotate with the first disc. A sapphire plate is interposed between the first and second discs to prevent galling of the copper material while maintaining high thermal conductivity between the first and second discs. A spring is disposed on the shaft to urge the second disc toward the first disc and compressingly engage the interposed sapphire plate. A specimen mount is secured to the first disc for rotation within the vacuum chamber. The specimen maintains high thermal conductivity with the second disc receiving the cryogenic transfer line.

  4. Apparatus for pre-stress-straining rod-type specimens in tension for in-situ passive fracture testing

    DOE Patents [OSTI]

    Wang, John Jy-an; Liu, Ken C.; Feng, Zhili

    2013-07-31

    A stress-strain testing apparatus imposes a stress-strain on a specimen while disposed in a controlled environment. Each end of the specimen is fastened to an end cap and a strain gage is attached to the specimen. An adjusting mechanism and a compression element are disposed between the end caps forming a frame for applying forces to the end caps and thereby stress-straining the specimen. The adjusting mechanism may be extended or retracted to increase or decrease the imposed stress-strain on the specimen, and the stress-strain is measured by the strain gage on the specimen while the apparatus is exposed to an environment such as high pressure hydrogen. Strain gages may be placed on the frame to measure stress-strains in the frame that may be caused by the environment.

  5. AFCI Fuel Irradiation Test Plan, Test Specimens AFC-1Æ and AFC-1F

    SciTech Connect (OSTI)

    D. C. Crawford; S. L. Hayes; B. A. Hilton; M. K. Meyer; R. G. Ambrosek; G. S. Chang; D. J. Utterbeck

    2003-11-01

    The U. S. Advanced Fuel Cycle Initiative (AFCI) seeks to develop and demonstrate the technologies needed to transmute the long-lived transuranic actinide isotopes contained in spent nuclear fuel into shorter-lived fission products, thereby dramatically decreasing the volume of material requiring disposition and the long-term radiotoxicity and heat load of high-level waste sent to a geologic repository (DOE, 2003). One important component of the technology development is actinide-bearing transmutation fuel forms containing plutonium, neptunium, americium (and possibly curium) isotopes. There are little irradiation performance data available on non-fertile fuel forms, which would maximize the destruction rate of plutonium, and low-fertile (i.e., uranium-bearing) fuel forms, which would support a sustainable nuclear energy option. Initial scoping level irradiation tests on a variety of candidate fuel forms are needed to establish a transmutation fuel form design and evaluate deployment of transmutation fuels.

  6. Machining Test Specimens from Harvested Zion RPV Segments for Through Wall Attenuation Studies

    SciTech Connect (OSTI)

    Rosseel, Thomas M; Sokolov, Mikhail A; Nanstad, Randy K

    2015-01-01

    The decommissioning of the Zion Units 1 and 2 Nuclear Generating Station (NGS) in Zion, Illinois presents a special opportunity for developing a better understanding of materials degradation and other issues associated with extending the lifetime of existing Nuclear Power Plants (NPPs) beyond 60 years of service. In support of extended service and current operations of the US nuclear reactor fleet, the Oak Ridge National Laboratory (ORNL), through the Department of Energy (DOE), Light Water Reactor Sustainability (LWRS) Program, is coordinating and contracting with Zion Solutions, LLC, a subsidiary of Energy Solutions, the selective procurement of materials, structures, and components from the decommissioned reactors. In this paper, we will discuss the acquisition of segments of the Zion Unit 2 Reactor Pressure Vessel (RPV), the cutting of these segments into sections and blocks from the beltline and upper vertical welds and plate material, the current status of machining those blocks into mechanical (Charpy, compact tension, and tensile) test specimens and coupons for chemical and microstructural (TEM, APT, SANS, and nano indention) characterization, as well as the current test plans and possible collaborative projects. Access to service-irradiated RPV welds and plate sections will allow through wall attenuation studies to be performed, which will be used to assess current radiation damage models (Rosseel et al. (2012) and Rosseel et al. (2015)).

  7. Test surfaces useful for calibration of surface profilometers

    DOE Patents [OSTI]

    Yashchuk, Valeriy V; McKinney, Wayne R; Takacs, Peter Z

    2013-12-31

    The present invention provides for test surfaces and methods for calibration of surface profilometers, including interferometric and atomic force microscopes. Calibration is performed using a specially designed test surface, or the Binary Pseudo-random (BPR) grating (array). Utilizing the BPR grating (array) to measure the power spectral density (PSD) spectrum, the profilometer is calibrated by determining the instrumental modulation transfer.

  8. Method for thinning specimen

    DOE Patents [OSTI]

    Follstaedt, David M.; Moran, Michael P.

    2005-03-15

    A method for thinning (such as in grinding and polishing) a material surface using an instrument means for moving an article with a discontinuous surface with an abrasive material dispersed between the material surface and the discontinuous surface where the discontinuous surface of the moving article provides an efficient means for maintaining contact of the abrasive with the material surface. When used to dimple specimens for microscopy analysis, a wheel with a surface that has been modified to produce a uniform or random discontinuous surface significantly improves the speed of the dimpling process without loss of quality of finish.

  9. NESC VII European project: demonstration of warm pre-stressing effect in biaxial loading conditions - Bending tests on 18MND5 cruciform specimens and their interpretation

    SciTech Connect (OSTI)

    Jacquemoud, C.; Yuritzinn, T.; Marie, S.

    2012-07-01

    In the framework of the NESC VII European project, a large experimental program has been dedicated to characterize the Warm Pre-Stressing (WPS) effect in different testing configurations. One of the CEA (France) contributions to this project is the realization of five point bending tests on large cruciform specimens considering different WPS loading cycles. The five cruciform specimens, sponsored by EDF (France) and IRSN (France), are made of 18MND5 steel. Two of them have been tested on a same LCF (Load-Cool-Fracture) loading cycle and two others on the same LCTF (Load-Cool-Transient-Fracture) loading cycle. The experimental results presented in this paper give a successful demonstration of the WPS effect in biaxial loading conditions either on a LCF or on a LCTF cycle. During the test interpretations, different models have then been tested and compared in order to evaluate their ability to predict the cleavage fracture in the case of different WPS loading cycles. They all provide very conservative predictions whatever loading cycle is concerned. (authors)

  10. Biaxial Creep Specimen Fabrication

    SciTech Connect (OSTI)

    JL Bump; RF Luther

    2006-02-09

    This report documents the results of the weld development and abbreviated weld qualification efforts performed by Pacific Northwest National Laboratory (PNNL) for refractory metal and superalloy biaxial creep specimens. Biaxial creep specimens were to be assembled, electron beam welded, laser-seal welded, and pressurized at PNNL for both in-pile (JOYO reactor, O-arai, Japan) and out-of-pile creep testing. The objective of this test campaign was to evaluate the creep behavior of primary cladding and structural alloys under consideration for the Prometheus space reactor. PNNL successfully developed electron beam weld parameters for six of these materials prior to the termination of the Naval Reactors program effort to deliver a space reactor for Project Prometheus. These materials were FS-85, ASTAR-811C, T-111, Alloy 617, Haynes 230, and Nirnonic PE16. Early termination of the NR space program precluded the development of laser welding parameters for post-pressurization seal weldments.

  11. WAFER TEST CAVITY -Linking Surface Microstructure to RF Performance...

    Office of Scientific and Technical Information (OSTI)

    WAFER TEST CAVITY -Linking Surface Microstructure to RF Performance: a 'Short--Sample Test Facility' for characterizing superconducting materials for SRF cavities. Citation Details ...

  12. Fabrication Control Plan for ORNL RH-LOCA ATF Test Specimens to be Irradiated in the ATR

    SciTech Connect (OSTI)

    Kevin G. Field; Richard Howard; Michael Teague

    2014-06-01

    The purpose of this fabrication plan is (1) to summarize the design of a set of rodlets that will be fabricated and then irradiated in the Advanced Test Reactor (ATR) and (2) provide requirements for fabrication and acceptance criteria for inspections of the Light Water Reactor (LWR) – Accident Tolerant Fuels (ATF) rodlet components. The functional and operational (F&OR) requirements for the ATF program are identified in the ATF Test Plan. The scope of this document only covers fabrication and inspections of rodlet components detailed in drawings 604496 and 604497. It does not cover the assembly of these items to form a completed test irradiation assembly or the inspection of the final assembly, which will be included in a separate INL final test assembly specification/inspection document. The controls support the requirements that the test irradiations must be performed safely and that subsequent examinations must provide valid results.

  13. Determination of Interfacial Mechanical Properties of Ceramic Composites by the Compression of Micro-pillar Test Specimens

    SciTech Connect (OSTI)

    Shih, Chunghao; Katoh, Yutai; Leonard, Keith J; Bei, Hongbin; Lara-Curzio, Edgar

    2013-01-01

    A novel method to determine the fiber-matrix interfacial properties of ceramic matrix composites is proposed and evaluated; where micro- pillar samples containing inclined fiber/matrix interfaces were prepared from a SiC fiber reinforced SiC matrix composites then compression-tested using the nano-indentation technique. This new test method employs a simple geometry and mitigates the uncertainties associated with complex stress state in the conventional single filament push-out method for the determination of interfacial properties. Based on the test results using samples with different interface orientations , the interfacial debond shear strength and the internal friction coefficient are explicitly determined and compared with values obtained by other test methods.

  14. Optimizing surface quality of stainless alloys and using a modified ASTM G 48B procedure for acceptance testing

    SciTech Connect (OSTI)

    Maurer, J.R.

    1999-01-01

    The formation of high-temperature oxide scales and Cr-depleted zones on stainless alloys, such as 6% Mo superaustenitic steels, can significantly reduce their corrosion resistance. Effective methods to remove these layers and restore the surface to an optimized condition are detailed. Also, an acceptance test using a modified ASTM G 48B method at 35 C (95 F) for 72 h with a specimen having a crevice, and special corrosion criteria for failure, are described. Comparison of this test method with one using an uncreviced specimen at lower temperatures and for less time is discussed.

  15. Appendix B Surface Infiltration and Aquifer Test Data

    Office of Legacy Management (LM)

    B Surface Infiltration and Aquifer Test Data This page intentionally left blank ... 1000 1100 1200 1300 1400 TIME (MIN) INF-8 TEST I 300 400 TIME (MIN) INF-8 TEST 2 200 250 ...

  16. Apparatuses for prestressing rod-type specimens in torsion for in-situ passive fracture toughness testing in an extremely high-pressure environment of hydrogen

    DOE Patents [OSTI]

    Wang, Jy-an; Liu, Ken C.; Feng, Zhili

    2012-05-15

    An in-situ specimen fixture particularly adapted for prestressing rod-type SNTT-type specimens comprising a tube and end cap wherein the specimen is secured at one end to the tube, and at the opposite end to the end cap. The end cap is rotatable relative to the tube, and may be fixedly secured for creating a torsional force prestressing the specimen enclosed within the tube.

  17. An improved correlation procedure for subsize and full-size Charpy impact specimen data

    SciTech Connect (OSTI)

    Sokolov, M.A.; Alexander, D.J.

    1997-03-01

    The possibility of using subsize specimens to monitor the properties of reactor pressure vessel steels is receiving increasing attention for light-water reactor plant life extension. This potential results from the possibility of cutting samples of small volume form the internal surface of the pressure vessel for determination of the actual properties of the operating pressure vessel. In addition, plant life extension will require supplemental data that cannot be provided by existing surveillance programs. Testing of subsize specimens manufactured from broken halves of previously tested surveillance Charpy specimens offers an attractive means of extending existing surveillance programs. Using subsize Charpy V-notch-type specimens requires the establishment of a specimen geometry that is adequate to obtain a ductile-to-brittle transition curve similar to that obtained from full-size specimens, and the development of correlations for transition temperature and upper-shelf energy (USE) level between subsize and full-size specimens. Five different geometries of subsize specimens were selected for testing and evaluation. The specimens were made from several types of pressure vessel steels with a wide range of yield strengths, transition temperatures, and USEs. The effects of specimen dimensions, including notch depth, angle, and radius, have been studied. The correlations of transition temperatures determined from different types of subsize specimens and the full-size specimens are presented. A new procedure for transforming data from subsize specimens is developed. The transformed data are in good agreement with data from full-size specimens for materials that have USE levels less than 200 J.

  18. Multiple Irradiation Capsule Experiment (MICE)-3B Irradiation Test of Space Fuel Specimens in the Advanced Test Reactor (ATR) - Close Out Documentation for Naval Reactors (NR) Information

    SciTech Connect (OSTI)

    M. Chen; CM Regan; D. Noe

    2006-01-09

    Few data exist for UO{sub 2} or UN within the notional design space for the Prometheus-1 reactor (low fission rate, high temperature, long duration). As such, basic testing is required to validate predictions (and in some cases determine) performance aspects of these fuels. Therefore, the MICE-3B test of UO{sub 2} pellets was designed to provide data on gas release, unrestrained swelling, and restrained swelling at the upper range of fission rates expected for a space reactor. These data would be compared with model predictions and used to determine adequacy of a space reactor design basis relative to fission gas release and swelling of UO{sub 2} fuel and to assess potential pellet-clad interactions. A primary goal of an irradiation test for UN fuel was to assess performance issues currently associated with this fuel type such as gas release, swelling and transient performance. Information learned from this effort may have enabled use of UN fuel for future applications.

  19. ARM: Surface Radiation Measurement Quality Control testing, including climatologically configurable limits

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Shi, Yan; Riihimaki, Laura

    1994-01-07

    Surface Radiation Measurement Quality Control testing, including climatologically configurable limits

  20. Test probe for surface mounted leadless chip carrier

    DOE Patents [OSTI]

    Meyer, Kerry L.; Topolewski, John

    1989-05-23

    A test probe for a surface mounted leadless chip carrier is disclosed. The probed includes specially designed connector pins which allow size reductions in the probe. A thermoplastic housing provides spring action to ensure good mechanical and electrical contact between the pins and the contact strips of a leadless chip carrier. Other features include flexible wires molded into the housing and two different types of pins alternately placed in the housing. These features allow fabrication of a smaller and simpler test probe.

  1. Specimen illumination apparatus with optical cavity for dark field illumination

    DOE Patents [OSTI]

    Pinkel, Daniel; Sudar, Damir; Albertson, Donna

    1999-01-01

    An illumination apparatus with a specimen slide holder, an illumination source, an optical cavity producing multiple reflection of illumination light to a specimen comprising a first and a second reflective surface arranged to achieve multiple reflections of light to a specimen is provided. The apparatus can further include additional reflective surfaces to achieve the optical cavity, a slide for mounting the specimen, a coverslip which is a reflective component of the optical cavity, one or more prisms for directing light within the optical cavity, antifading solutions for improving the viewing properties of the specimen, an array of materials for analysis, fluorescent components, curved reflective surfaces as components of the optical cavity, specimen detection apparatus, optical detection equipment, computers for analysis of optical images, a plane polarizer, fiberoptics, light transmission apertures, microscopic components, lenses for viewing the specimen, and upper and lower mirrors above and below the specimen slide as components of the optical cavity. Methods of using the apparatus are also provided.

  2. Surface-enhanced Raman medical probes and system for disease diagnosis and drug testing

    DOE Patents [OSTI]

    Vo-Dinh, T.

    1999-01-26

    A probe for a surface-enhanced Raman scattering spectrometer includes a member of optically transmissive material for receiving the excitation radiation from a laser and for carrying the radiation emitted from a specimen to a detector. An end of the member for placing against the specimen has a coating that produces surface enhancement of the specimen during Raman scattering spectroscopic analysis. Specifically the coating is formed by a first layer of microparticles on the member and a metal layer over the first layer. The first layer may form a microstructure surface over which a metal layer is applied. Alternatively the coating may be a material containing microparticles of a metal. An optional layer of a material may be applied to the metal layer to concentrate onto the probe compounds of analytical interest onto the probe. 39 figs.

  3. Surface-enhanced raman medical probes and system for disease diagnosis and drug testing

    DOE Patents [OSTI]

    Vo-Dinh, Tuan

    1999-01-01

    A probe for a surface-enhanced Raman scattering spectrometer includes a member of optically transmissive material for receiving the excitation radiation from a laser and for carrying the radiation emitted from a specimen to a detector. An end of the member for placing against the specimen has a coating that produces surface enhancement of the specimen during Raman scattering spectroscopic analysis. Specifically the coating is formed by a first layer of microparticles on the member and a metal layer over the first layer. The first layer may form a microstructure surface over which a metal layer is applied. Alternatively the coating may be a material containing microparticles of a metal. An optional layer of a material may be applied to the metal layer to concentrate onto the probe compounds of analytical interest onto the probe.

  4. Test probe for surface mounted leadless chip carrier

    DOE Patents [OSTI]

    Meyer, K.L.; Topolewski, J.

    1987-10-02

    A test probe for a surface mounted leadless chip carrier is disclosed. The probe includes specially designed connector pins which allow size reductions in the probe. A thermoplastic housing provides spring action to ensure good mechanical and electrical contact between the pins and the contact strips of a leadless chip carrier. Other features include flexible wires molded into the housing and two different types of pins alternately placed in the housing. These features allow fabrication of a smaller and simpler test probe. 1 fig.

  5. An Experimental Study of Shear-Dominated Failure in the 2013 Sandia Fracture Challenge Specimen

    SciTech Connect (OSTI)

    Corona, Edmundo; Deibler, Lisa Anne; Reedlunn, Benjamin; Ingraham, Mathew Duffy; Williams, Shelley

    2015-04-01

    This report presents an experimental study motivated by results obtained during the 2013 Sandia Fracture Challenge. The challenge involved A286 steel, shear-dominated compression specimens whose load-deflection response contained a load maximum fol- lowed by significant displacement under decreasing load, ending with a catastrophic fracture. Blind numerical simulations deviated from the experiments well before the maximum load and did not predict the failure displacement. A series of new tests were conducted on specimens machined from the original A286 steel stock to learn more about the deformation and failure processes in the specimen and potentially improve future numerical simulations. The study consisted of several uniaxial tension tests to explore anisotropy in the material, and a set of new tests on the compression speci- men. In some compression specimen tests, stereo digital image correlation (DIC) was used to measure the surface strain fields local to the region of interest. In others, the compression specimen was loaded to a given displacement prior to failure, unloaded, sectioned, and imaged under the microscope to determine when material damage first appeared and how it spread. The experiments brought the following observations to light. The tensile tests revealed that the plastic response of the material is anisotropic. DIC during the shear- dominated compression tests showed that all three in-plane surface strain components had maxima in the order of 50% at the maximum load. Sectioning of the specimens revealed no signs of material damage at the point where simulations deviated from the experiments. Cracks and other damage did start to form approximately when the max- imum load was reached, and they grew as the load decreased, eventually culminating in catastrophic failure of the specimens. In addition to the steel specimens, a similar study was carried out for aluminum 7075-T651 specimens. These specimens achieved much lower loads and displacements

  6. Elastic-plastic analysis of the SS-3 tensile specimen

    SciTech Connect (OSTI)

    Majumdar, S.

    1998-09-01

    Tensile tests of most irradiated specimens of vanadium alloys are conducted using the miniature SS-3 specimen which is not ASTM approved. Detailed elastic-plastic finite element analysis of the specimen was conducted to show that, as long as the ultimate to yield strength ratio is less than or equal to 1.25 (which is satisfied by many irradiated materials), the stress-plastic strain curve obtained by using such a specimen is representative of the true material behavior.

  7. STRESS CORROSION CRACKING IN TEAR DROP SPECIMENS

    SciTech Connect (OSTI)

    Lam, P; Philip Zapp, P; Jonathan Duffey, J; Kerry Dunn, K

    2009-05-01

    Laboratory tests were conducted to investigate the stress corrosion cracking (SCC) of 304L stainless steel used to construct the containment vessels for the storage of plutonium-bearing materials. The tear drop corrosion specimens each with an autogenous weld in the center were placed in contact with moist plutonium oxide and chloride salt mixtures. Cracking was found in two of the specimens in the heat affected zone (HAZ) at the apex area. Finite element analysis was performed to simulate the specimen fabrication for determining the internal stress which caused SCC to occur. It was found that the tensile stress at the crack initiation site was about 30% lower than the highest stress which had been shifted to the shoulders of the specimen due to the specimen fabrication process. This finding appears to indicate that the SCC initiation took place in favor of the possibly weaker weld/base metal interface at a sufficiently high level of background stress. The base material, even subject to a higher tensile stress, was not cracked. The relieving of tensile stress due to SCC initiation and growth in the HAZ and the weld might have foreclosed the potential for cracking at the specimen shoulders where higher stress was found.

  8. Strain rate and inertial effects on impact loaded single-edge notch bend specimens

    SciTech Connect (OSTI)

    Vargas, P.M.; Dodds, R.H. Jr.

    1995-12-31

    Many problems in fracture mechanics of ductile metals involve surface breaking defects located in structures subjected to impact or blast. When the severity of impact loads is sufficient to produce large inelastic deformations, the assessment of crack-tip conditions must include the effects of plasticity, strain rate and inertia. This work examines the interaction of impact loading, inelastic material deformation and rate sensitivity with the goal of improving the interpretation of ductile fracture toughness values measured under dynamic loading. The authors focus on shallow and deeply notched bend test specimens, SE(B)s, employed routinely to measure the static fracture toughness of a material. A thorough understanding of the test specimen`s dynamic behavior is a prerequisite to the application of measured fracture properties in structural applications. Three-dimensional, nonlinear dynamic analyses are performed for SE(B) fracture specimens subjected to impact loading. Loading rates obtained in conventional drop tower tests are applied in the analyses. An explicit time integration procedure coupled with an efficient (one-point) element integration scheme is employed to compute the dynamic response of the specimen. Strain-rate sensitivity is introduced via a new, efficient implementation of the Bodner-Partom viscoplastic constitutive model. Material properties for A533B steel are used in the analyses. Static analyses of the SE(B) specimens provide baseline responses for assessment of inertial effects. Similarly, dynamic analyses using a strain-rate insensitive material provide reference responses for the assessment of strain rate effects. Strains at key locations on the specimens and the support reactions are extracted from the analyses to assess the accuracy of static formulas commonly used to estimate applied J values. Inertial effects on the applied J are quantified by examining the acceleration component of J evaluated through a domain integral procedure.

  9. Langasite Surface Acoustic Wave Sensors: Fabrication and Testing

    SciTech Connect (OSTI)

    Zheng, Peng; Greve, David W.; Oppenheim, Irving J.; Chin, Tao-Lun; Malone, Vanessa

    2012-02-01

    We report on the development of harsh-environment surface acoustic wave sensors for wired and wireless operation. Surface acoustic wave devices with an interdigitated transducer emitter and multiple reflectors were fabricated on langasite substrates. Both wired and wireless temperature sensing was demonstrated using radar-mode (pulse) detection. Temperature resolution of better than 0.5C was achieved between 200C and 600C. Oxygen sensing was achieved by depositing a layer of ZnO on the propagation path. Although the ZnO layer caused additional attenuation of the surface wave, oxygen sensing was accomplished at temperatures up to 700C. The results indicate that langasite SAW devices are a potential solution for harsh-environment gas and temperature sensing.

  10. Manufacturing of Plutonium Tensile Specimens

    SciTech Connect (OSTI)

    Knapp, Cameron M

    2012-08-01

    Details workflow conducted to manufacture high density alpha Plutonium tensile specimens to support Los Alamos National Laboratory's science campaigns. Introduces topics including the metallurgical challenge of Plutonium and the use of high performance super-computing to drive design. Addresses the utilization of Abaqus finite element analysis, programmable computer numerical controlled (CNC) machining, as well as glove box ergonomics and safety in order to design a process that will yield high quality Plutonium tensile specimens.

  11. Automatic grinding apparatus to control uniform specimen thicknesses

    DOE Patents [OSTI]

    Bryner, J.S.

    1981-01-07

    This invention is directed to a new and improved grinding apparatus comprisng: (1) a movable grinding surface; (2) a specimen holder; (3) a dislacing means for moving the holder and/or grinding surface toward one another; and (4) at least three means for limiting displacement of the holder to the grinding surface.

  12. Automatic grinding apparatus to control uniform specimen thicknesses

    DOE Patents [OSTI]

    Bryner, Joseph S.

    1982-01-01

    This invention is directed to a new and improved grinding apparatus comprising (1) a movable grinding surface, (2) a specimen holder, (3) a displacing device for moving the holder and/or grinding surface toward one another, and (4) at least three devices for limiting displacement of the holder to the grinding surface.

  13. Effect of specimen size on the fracture toughness of V-4Cr-4Ti

    SciTech Connect (OSTI)

    Kurtz, R.J.; Jones, R.H.; Li, Huaxin

    1996-04-01

    J-R curves were generated using the single specimen unload-compliance technique on four specimens of V-4Cr-4Ti to determine the effect of specimen dimensions on the fracture behavior. Ductile crack initiation and growth was observed in the 6.35 mm thick specimens but not in the 12.70 mm thick specimens. The J-R curves determined from these tests were not valid per ASTM validity criteria so quantitative measures of the resistance to ductile crack initiation and growth were not obtained. These data suggests that standard fracture toughness tests were performed with small-scale DCT specimens may also not be valid.

  14. Liquid salt environment stress-rupture testing

    DOE Patents [OSTI]

    Ren, Weiju; Holcomb, David E.; Muralidharan, Govindarajan; Wilson, Dane F.

    2016-03-22

    Disclosed herein are systems, devices and methods for stress-rupture testing selected materials within a high-temperature liquid salt environment. Exemplary testing systems include a load train for holding a test specimen within a heated inert gas vessel. A thermal break included in the load train can thermally insulate a load cell positioned along the load train within the inert gas vessel. The test specimen can include a cylindrical gage portion having an internal void filled with a molten salt during stress-rupture testing. The gage portion can have an inner surface area to volume ratio of greater than 20 to maximize the corrosive effect of the molten salt on the specimen material during testing. Also disclosed are methods of making a salt ingot for placement within the test specimen.

  15. Experiments and analyses on undermatched interleaf specimens in bending

    SciTech Connect (OSTI)

    Parks, D.M.; Ganti, S.; McClintock, F.A.; Epstein, J.S.; Lloyd, L.R.; Reuter, W.G.

    1995-12-31

    Model weldment fracture specimens have been fabricated, tested, and analyzed using finite elements. The specimens consist of an interleaf of commercially pure titanium diffusion-bonded to a harder alloy titanium. A deep edge crack is introduced symmetrically into the interleaf, and the specimens are loaded in pure bending. Variation of the thickness (2h) of the soft interleaf layer provides insight into effects of weld geometry in strongly undermatched weldments tested in plane strain bending. Ductile crack growth (beyond blunting) initiated at loads giving J {doteq} 95 kJ/m{sup 2} in all specimens. In the thickest interleaf geometries, stable tearing was obtained, but in the thinnest interleaf (2h {doteq} 3mm), crack initiation resulted in a massive pop-in of 5.4 mm across an initial ligament of 12 mm. Finite element studies show that the thinnest interleaf geometry had slightly higher peak stress triaxiality at the beginning of cracking, and that the highest triaxiality extended over a larger region than in the thicker interleaf specimens loaded to the same initiation J-values. More importantly, the blockage of plastic straining above and below the crack tip in the 3 mm interleaf specimen forced higher values of plastic strain to spread forward into the {+-} 45{degree} sector of highest stress triaxiality directly ahead of the crack tip. The higher strains, in conjunction with the slightly higher stress triaxiality, led to the unstable pop-in initiation.

  16. Feasibility of Ground Testing a Moon and Mars Surface Power Reactor in EBR-II

    SciTech Connect (OSTI)

    Sheryl Morton; Carl Baily; Tom Hill; Jim Werner

    2006-02-01

    Ground testing of a surface fission power system would be necessary to verify the design and validate reactor performance to support safe and sustained human exploration of the Moon and Mars. The Idaho National Laboratory (INL) has several facilities that could be adapted to support a ground test. This paper focuses on the feasibility of ground testing at the Experimental Breeder Reactor II (EBR-II) facility and using other INL existing infrastructure to support such a test. This brief study concludes that the INL EBR-II facility and supporting infrastructure are a viable option for ground testing the surface power system. It provides features and attributes that offer advantages to locating and performing ground testing at this site, and it could support the National Aeronautics and Space Administration schedules for human exploration of the Moon. This study used the initial concept examined by the U.S. Department of Energy Inter-laboratory Design and Analysis Support Team for surface power, a lowtemperature, liquid-metal, three-loop Brayton power system. With some facility modification, the EBR-II can safely house a test chamber and perform long-term testing of the space reactor power system. The INL infrastructure is available to receive and provide bonded storage for special nuclear materials. Facilities adjacent to EBR-II can provide the clean room environment needed to assemble and store the test article assembly, disassemble the power system at the conclusion of testing, and perform posttest examination. Capability for waste disposal is also available at the INL.

  17. Stress-corrosion cracking and surface-pitting tests of NiCrFe alloy bolts (LWBR development program)

    SciTech Connect (OSTI)

    Keller, K.L.

    1983-02-01

    Accelerated corrosion tests confirmed the adequate resistance to stress corrosion cracking (SCC) of the specific heats of NiCrFe X-750 and NiCrFe 600 used as bolts in the LWBR. SCC acceleration was achieved by running autoclave corrosion tests at 680/sup 0/F (well above the LWBR core operating temperatures of approximately 525/sup 0/F to 560/sup 0/F). Component stress levels were representative of maximum service stresses. No specimens from heats of either alloy suffered SCC.

  18. Preliminary Correlation Map of Geomorphic Surfaces in North-Central Frenchman Flat, Nevada Test Site

    SciTech Connect (OSTI)

    Bechtel Nevada

    2005-08-01

    This correlation map (scale = 1:12,000) presents the results of a mapping initiative that was part of the comprehensive site characterization required to operate the Area 5 Radioactive Waste Management Site, a low-level radioactive waste disposal facility located in northern Frenchman Flat at the Nevada Test Site. Eight primary map units are recognized for Quaternary surfaces: remnants of six alluvial fan or terrace surfaces, one unit that includes colluvial aprons associated with hill slopes, and one unit for anthropogenically disturbed surfaces. This surficial geology map provides fundamental data on natural processes for reconstruction of the Quaternary history of northern Frenchman Flat, which in turn will aid in the understanding of the natural processes that act to develop the landscape, and the time-frames involved in landscape development. The mapping was conducted using color and color-infrared aerial photographs and field verification of map unit composition and boundaries. Criteria for defining the map unit composition of geomorphic surface units are based on relative geomorphic position, landform morphology, and degree of preservation of surface morphology. The bedrock units identified on this map were derived from previous published mapping efforts and are included for completeness.

  19. Determining mechanical behavior of solid materials using miniature specimens

    DOE Patents [OSTI]

    Manahan, M.P.; Argon, A.S.; Harling, O.K.

    1986-02-04

    A Miniaturized Bend Test (MBT) capable of extracting and determining mechanical behavior information from specimens only so large as to have at least a volume or smallest dimension sufficient to satisfy continuum behavior in all directions is disclosed. The mechanical behavior of the material is determined from the measurements taken during the bending of the specimen and is processed according to the principles of linear or nonlinear material mechanics or both. In a preferred embodiment the determination is carried out by a code which is constructed according to the finite element method, and the specimen used for the determinations is a miniature disk simply supported for central loading at the axis on the center of the disk. 51 figs.

  20. Determining mechanical behavior of solid materials using miniature specimens

    DOE Patents [OSTI]

    Manahan, Michael P.; Argon, Ali S.; Harling, Otto K.

    1986-01-01

    A Miniaturized Bend Test (MBT) capable of extracting and determining mechanical behavior information from specimens only so large as to have at least a volume or smallest dimension sufficient to satisfy continuum behavior in all directions. The mechanical behavior of the material is determined from the measurements taken during the bending of the specimen and is processed according to the principles of linear or nonlinear material mechanics or both. In a preferred embodiment the determination is carried out by a code which is constructed according to the finite element method, and the specimen used for the determinations is a miniature disk simply supported for central loading at the axis on the center of the disk.

  1. Midtemperature solar systems test facility predictions for thermal performance based on test data. Polisolar Model POL solar collector with glass reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-05-01

    Thermal performance predictions based on test data are presented for the Polisolar Model POL solar collector, with glass reflector surfaces, for three output temperatures at five cities in the United States.

  2. Midtemperature solar systems test facility predictions for thermal performance based on test data. Toltec two-axis tracking solar collector with 3M acrylic polyester film reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-06-01

    Thermal performance predictions based on test data are presented for the Toltec solar collector, with acrylic film reflector surface, for three output temperatures at five cities in the United States.

  3. Results of experimental tests and calibrations of the surface neutron moisture measurement probe

    SciTech Connect (OSTI)

    Watson, W.T.; Bussell, J.H., Westinghouse Hanford

    1996-08-13

    The surface neutron moisture probe has been tested both to demonstrate that is is able to operate in the expected in-tank temperature and gamma-ray fields and to provide detector responses to known moisture concentration materials. The probe will properly function in a simultaneous high temperature (80 degrees C) and high gamma radiation field (210 rad/hr)environment. Comparisons between computer model predicted and experimentally measured detector responses to changes in moisture provide a basis for the probe calibration to in-tank moisture concentrations.

  4. Testing and monitoring plan for the permanent isolation surface barrier prototype

    SciTech Connect (OSTI)

    Gee, G.W.; Cadwell, L.L.; Freeman, H.D.; Ligotke, M.W.; Link, S.O.; Romine, R.A.; Walters, W.H. Jr.

    1993-06-01

    This document is a testing and monitoring plan for a prototype barrier to be constructed at the Hanford Site in 1993. The prototype barrier is an aboveground structure engineered to demonstrate the basic features of an earthen cover system, designed to permanently isolate waste from the biosphere. These features include multiple layers of soil and rock materials and a low-permeability asphalt sublayer. The surface of the barrier consists of silt loam soil, vegetated with plants. The barrier sides are reinforced with rock or coarse earthen-fill to protect against wind and water erosion. The sublayers inhibit plant and animal intrusion and percolation of water. A series of tests will be conducted on the prototype over the next several years to evaluate barrier performance under extreme climatic conditions.

  5. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Tests - 2011

    SciTech Connect (OSTI)

    Pawloski, G A

    2011-02-28

    This report evaluates collapse evolution for selected Lawrence Livermore National Laboratory (LLNL) underground nuclear tests at the Nevada National Security Site (NNSS, formerly called the Nevada Test Site). The work is being done at the request of National Security Technologies, LLC (NSTec) and supports the Department of Energy, National Nuclear Security Administration for the Nevada Site Office Borehole Management Program (BMP). The primary objective of this program is to close (plug) weapons program legacy boreholes that are deemed no longer useful. Safety decisions must be made before a crater area, or potential crater area, can be reentered for any work. Our statements on cavity collapse and crater formation are input into their safety decisions. The BMP is an on-going program to address hundreds of boreholes at the NTS. Each year NSTec establishes a list of holes to be addressed. They request the assistance of the Lawrence Livermore National Laboratory and Los Alamos National Laboratory Containment Programs to provide information related to the evolution of collapse history and make statements on completeness of collapse as relates to surface crater stability. These statements do not include the effects of erosion that may modify the collapse craters over time. They also do not address possible radiation dangers that may be present. Subject matter experts from the LLNL Containment Program who had been active in weapons testing activities performed these evaluations. Information used included drilling and hole construction, emplacement and stemming, timing and sequence of the selected test and nearby tests, geology, yield, depth of burial, collapse times, surface crater sizes, cavity and crater volume estimations, ground motion, and radiological release information. Both classified and unclassified data were reviewed. Various amounts of information are available for these tests, depending on their age and other associated activities. Lack of data can hamper

  6. Adhesion and chemical vapor testing of second surface silver/glass solar mirrors

    SciTech Connect (OSTI)

    Dake, L.S.; Lind, M.A.

    1980-09-01

    Second surface silvered glass mirrors supplied by four different commercial manufacturers were evaluated for silver-to-glass adhesion and resistance to chemical vapor attack. The mirrors were chemically silvered on identical substrates of low iron float glass. Experiments were performed in order to assess the viability of using adhesion and chemical attack as screening tests for predicting the relative long-term durability of solar mirrors. The results of these tests will be compared at a future time with the survivability of field mirrors deployed in stationary exposure racks at ten locations throughout the United States. The adhesion tests were performed using a commercially-available thin film tensile pull tester in which a stud bonded to the film is pulled and the yield load recorded. Numerous subtleties regarding the selection of the adhesive used to bond the study and the validity of the testing procedure are discussed. Several different methods of normalizing the results were attempted in an effort to reduce the scatter in the data. The same set of samples were exposed to salt spray, water, HCl, H/sub 2/SO/sub 4/, and HNO/sub 3/ vapors and then ranked according to their performance. Visual comparison of tested samples did not yield consistent results; however, definite trends were observed favoring one of the manufacturers. Some SEM/EDX analysis was performed on these mirrors subject to accelerated degradation in order to compare them to mirrors subject to natural degradation. However, insufficient data has been collected to show that any of the tests performed will accurately predict the relative life expectancy of the mirrors in an outdoor environment.

  7. Midtemperature Solar Systems Test Facility predictions for thermal performance based on test data: Custom Engineering trough with glass reflector surface and Sandia-designed receivers

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-05-01

    Thermal performance predictions based on test data are presented for the Custom Engineering trough and Sandia-designed receivers, with glass reflector surface, for three output temperatures at five cities in the United States. Two experimental receivers were tested, one with an antireflective coating on the glass envelope around the receiver tube and one without the antireflective coating.

  8. Testing, Modeling, and Monitoring to Enable Simpler, Cheaper, Longer-Lived Surface Caps

    SciTech Connect (OSTI)

    Piet, Steven James; Breckenridge, Robert Paul; Burns, Douglas Edward

    2003-02-01

    Society has and will continue to generate hazardous wastes whose risks must be managed. For exceptionally toxic, long-lived, and feared waste, the solution is deep burial, e.g., deep geological disposal at Yucca Mtn. For some waste, recycle or destruction/treatment is possible. The alternative for other wastes is storage at or near the ground level (in someones back yard); most of these storage sites include a surface barrier (cap) to prevent downward water migration. Some of the hazards will persist indefinitely. As society and regulators have demanded additional proof that caps are robust against more threats and for longer time periods, the caps have become increasingly complex and expensive. As in other industries, increased complexity will eventually increase the difficulty in estimating performance, in monitoring system/component performance, and in repairing or upgrading barriers as risks are managed. An approach leading to simpler, less expensive, longer-lived, more manageable caps is needed. Our project, which started in April 2002, aims to catalyze a Barrier Improvement Cycle (iterative learning and application) and thus enable Remediation System Performance Management (doing the right maintenance neither too early nor too late). The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions, improve barrier management, and enable improved solutions for future decisions. We believe it will be possible to develop simpler, longer-lived, less expensive caps that are easier to monitor, manage, and repair. The project is planned to: a) improve the knowledge of degradation mechanisms in times shorter than service life; b) improve modeling of barrier degradation dynamics; c) develop sensor systems to identify early degradation; and d) provide a better basis for developing and testing of new barrier systems. This project combines selected exploratory studies (benchtop and field scale), coupled effects accelerated aging

  9. Testing, Modeling, and Monitoring to Enable Simpler, Cheaper, Longer-lived Surface Caps

    SciTech Connect (OSTI)

    Piet, S. J.; Breckenridge, R. P.; Burns, D. E.

    2003-02-25

    Society has and will continue to generate hazardous wastes whose risks must be managed. For exceptionally toxic, long-lived, and feared waste, the solution is deep burial, e.g., deep geological disposal at Yucca Mtn. For some waste, recycle or destruction/treatment is possible. The alternative for other wastes is storage at or near the ground level (in someone's back yard); most of these storage sites include a surface barrier (cap) to prevent downward water migration. Some of the hazards will persist indefinitely. As society and regulators have demanded additional proof that caps are robust against more threats and for longer time periods, the caps have become increasingly complex and expensive. As in other industries, increased complexity will eventually increase the difficulty in estimating performance, in monitoring system/component performance, and in repairing or upgrading barriers as risks are managed. An approach leading to simpler, less expensive, longer-lived, more manageable caps is needed. Our project, which started in April 2002, aims to catalyze a Barrier Improvement Cycle (iterative learning and application) and thus enable Remediation System Performance Management (doing the right maintenance neither too early nor too late). The knowledge gained and the capabilities built will help verify the adequacy of past remedial decisions, improve barrier management, and enable improved solutions for future decisions. We believe it will be possible to develop simpler, longer-lived, less expensive caps that are easier to monitor, manage, and repair. The project is planned to: (a) improve the knowledge of degradation mechanisms in times shorter than service life; (b) improve modeling of barrier degradation dynamics; (c) develop sensor systems to identify early degradation; and (d) provide a better basis for developing and testing of new barrier systems. This project combines selected exploratory studies (benchtop and field scale), coupled effects accelerated

  10. Effect of surface oxidation on the onset of nucleate boiling in a materials test reactor coolant channel

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Forrest, Eric C.; Don, Sarah M.; Hu, Lin -Wen; Buongiorno, Jacopo; McKrell, Thomas J.

    2016-02-29

    The onset of nucleate boiling (ONB) serves as the thermal-hydraulic operating limit for many research and test reactors. However, boiling incipience under forced convection has not been well-characterized in narrow channel geometries or for oxidized surface conditions. This study presents experimental data for the ONB in vertical upflow of deionized (DI) water in a simulated materials test reactor (MTR) coolant channel. The channel gap thickness and aspect ratio were 1.96 mm and 29:1, respectively. Boiling surface conditions were carefully controlled and characterized, with both heavily oxidized and native oxide surfaces tested. Measurements were performed for mass fluxes ranging from 750more » to 3000 kg/m2s and for subcoolings ranging from 10 to 45°C. ONB was identified using a combination of high-speed visual observation, surface temperature measurements, and channel pressure drop measurements. Surface temperature measurements were found to be most reliable in identifying the ONB. For the nominal (native oxide) surface, results indicate that the correlation of Bergles and Rohsenow, when paired with the appropriate single-phase heat transfer correlation, adequately predicts the ONB heat flux. Furthermore, incipience on the oxidized surface occurred at a higher heat flux and superheat than on the plain surface.« less

  11. Simultaneous specimen and stage cleaning device for analytical electron microscope

    DOE Patents [OSTI]

    Zaluzec, Nestor J.

    1996-01-01

    An improved method and apparatus are provided for cleaning both a specimen stage, a specimen and an interior of an analytical electron microscope (AEM). The apparatus for cleaning a specimen stage and specimen comprising a plasma chamber for containing a gas plasma and an air lock coupled to the plasma chamber for permitting passage of the specimen stage and specimen into the plasma chamber and maintaining an airtight chamber. The specimen stage and specimen are subjected to a reactive plasma gas that is either DC or RF excited. The apparatus can be mounted on the analytical electron microscope (AEM) for cleaning the interior of the microscope.

  12. Shallow Flaws Under Biaxial Loading Conditions, Part II: Application of a Weibull Stress Analysis of the Cruciform Bend Specimen Using a Hydrostatic Stress Criterion

    SciTech Connect (OSTI)

    Bass, B.R.; McAfee, W.J.; Williams, P.T.

    1999-08-01

    Cruciform beam fracture mechanics specimensl have been developed in the Heavy Section Steel Technology (HSST) Program at Oak Ridge National Laboratory (ORNL) to introduce a prototypic, far- field, out-of-plane biaxird bending stress component in the test section that approximates the nonlinear biaxial stresses resulting from pressurized-thernxd-shock or pressure-temperature loading of a nuclear reactor pressure vessel (RPV). Matrices of cruciform beam tests were developed to investigate and quantify the effects of temperature, biaxial loading, and specimen size on fracture initiation toughness of two-dimensional (constant depth), shtdlow, surface flaws. Tests were conducted under biaxial load ratios ranging from uniaxial to equibiaxial. These tests demonstrated that biaxial loading can have a pronounced effect on shallow-flaw fracture toughness in the lower transition temperature region for RPV materials. Two and three- parameter Weibull models have been calibrated using a new scheme (developed at the University of Illinois) that maps toughness data from test specimens with distinctly different levels of crack-tip constraint to a small scale yielding (SSY) Weibull stress space. These models, using the new hydrostatic stress criterion in place of the more commonly used maximum principal stress in the kernel of the OW integral definition, have been shown to correlate the experimentally observed biaxiaI effect in cruciform specimens, thereby providing a scaling mechanism between uniaxial and biaxial loading states.

  13. Specimen loading list for the varying temperature experiment

    SciTech Connect (OSTI)

    Qualls, A.L.; Sitterson, R.G.

    1998-09-01

    The varying temperature experiment HFIR-RB-13J has been assembled and inserted in the reactor. Approximately 5300 specimens were cleaned, inspected, matched, and loaded into four specimen holders. A listing of each specimen loaded into the steady temperature holder, its position in the capsule, and the identification of the corresponding specimen loaded into the varying temperature holder is presented in this report.

  14. Motorized manipulator for positioning a TEM specimen

    DOE Patents [OSTI]

    Schmid, Andreas Karl; Andresen, Nord

    2010-12-14

    The invention relates to a motorized manipulator for positioning a TEM specimen holder with sub-micron resolution parallel to a y-z plane and rotating the specimen holder in the y-z plane, the manipulator comprising a base (2), and attachment means (30) for attaching the specimen holder to the manipulator, characterized in that the manipulator further comprises at least three nano-actuators (3.sup.a, 3.sup.b, 3.sup.c) mounted on the base, each nano-actuator showing a tip (4.sup.a, 4.sup.b, 4.sup.c), the at least three tips defining the y-z plane, each tip capable of moving with respect to the base in the y-z plane; a platform (5) in contact with the tips of the nano-actuators; and clamping means (6) for pressing the platform against the tips of the nano-actuators; as a result of which the nano-actuators can rotate the platform with respect to the base in the y-z plane and translate the platform parallel to the y-z plane.

  15. Interim reclamation report, Basalt Waste Isolation Project Near Surface Test Facility 1990

    SciTech Connect (OSTI)

    Brandt, C.A.; Rickard, W.H. Jr.; Hefty, M.G.; Cadoret, N.A.

    1991-01-01

    This report describes the development of the reclamation project for the Hanford Site Near Surface Test Facility (NSTF), its implementation, and preliminary estimates of its success. The goal of the reclamation project is to return disturbed sites as nearly as practicable to their original conditions using native species. Gable Mountain is dominated by two plant communities: a big sagebrush (Artemisia tridentata) -- Sandberg's bluegrass (Poa sandbergii) community and a stiff sagebrush (Artemisia rigida) -- Sandberg's bluegrass community. Disassembly of the site installations began on March 15, 1988, and the site was returned to original contours by December 12, 1988. Two separate revegetation methods were employed at the NSTF to meet differing site constraints. Vegetative cover and density in the revegetation plots were assessed in April 1989 and again in June 1989 and 1990. It is extremely unlikely that the sand pit, borrow pit, box cuts, generator pad area, or ventilation fan area will reach the reclamation objectives set for these areas within the next 50 years without further intervention. These areas currently support few living plants. Vegetation on revegetated native soils appears to be growing as expected. Vegetation growth on the main waterline is well below the objective. To date, no shrubs have grown on the area, growth of native grasses is well below the objective, and much of the area has been covered with the pit run material, which may not support adequate growth. Without further treatments, the areas without the pit run material will likely revert to a nearly pure cheatgrass condition. 44 refs., 13 figs., 7 tabs.

  16. Investigation of Asphalt Mixture Creep Behavior Using Thin Beam Specimens

    SciTech Connect (OSTI)

    Zofka, Adam; Marasteanu, Mihai; Turos, Mugur

    2008-02-15

    The asphalt pavement layer consists of two or more lifts of compacted asphalt mixture; the top of the layer is also exposed to aging, a factor that significantly affects the mixture properties. The current testing specifications use rather thick specimens that cannot be used to investigate the gradual change in properties with pavement depth. This paper investigates the feasibility of using the 3-point bending test with thin asphalt mixture beams (127x12.7x6.35 mm) to determine the low-temperature creep compliance of the mixtures. Several theoretical and semi-empirical models, from the theory of composites, are reviewed and evaluated using numerical and experimental data. Preliminary results show that this method can be used for low-temperature mixture characterization but several crucial factors need further inspection and interpretation.

  17. True uniaxial compressive strengths of rock or coal specimens are independent of diameter-to-length ratios

    SciTech Connect (OSTI)

    Babcock, C.O.

    1991-01-01

    This paper reports that part of the compressive strength of a test specimen of rock or coal in the laboratory or a pillar in a mine comes from physical property strength and, in part, from the constraint provided by the loading stresses. Much confusion in pillar design comes from assigning the total strength change to geometry, as evidenced by the many pillar design equations with width to height as the primary variable. In tests by the U.S. Bureau of Mines, compressive strengths for cylindrical specimens of limestone, marble, sandstone, and coal were independent of the specimen test geometry when the end friction was removed. A conventional uniaxial compressive strength test between two steel platens is actually a uniaxial force and not a uniaxial stress test. The biaxial or triaxial state of stress for much of the test volume changes with the geometry of the test specimen. By removing the end friction supplied by the steel platens to the specimen, a more nearly uniaxial stress state independent of the specimen geometry is produced in the specimen. Pillar design is a constraint and physical property problem rather than a geometry problem. Roof and floor constraint are major factors in pillar design and strength.

  18. Geomorphic Surface Maps of Northern Frenchman Flat, Nevada Test Site, Southern Nevada

    SciTech Connect (OSTI)

    Bechtel Nevada

    2005-08-01

    Large-scale (1:6000) surficial geology maps of northern Frenchman Flat were developed in 1995 as part of comprehensive site characterization required to operate a low-level radioactive waste disposal facility in that area. Seven surficial geology maps provide fundamental data on natural processes and are the platform needed to reconstruct the Quaternary history of northern Frenchman Flat. Reconstruction of the Quaternary history provides an understanding of the natural processes that act to develop the landscape, and the time-frames involved in landscape development. The mapping was conducted using color and color-infrared aerial photographs and field verification of map unit composition and boundaries. Criteria for defining the map unit composition of geomorphic surface units are based on relative geomorphic position, landform morphology, and degree of preservation of surface morphology. Seven geomorphic surfaces (Units 1 through 7) are recognized, spanning from the early Quaternary to present time.

  19. Radionuclide release from PWR spent fuel specimens with induced cladding defects

    SciTech Connect (OSTI)

    Wilson, C.N.; Oversby, V.M.

    1984-03-01

    Radionuclide releases from pressurized water reactor (PWR) spent fuel rod specimens containing various artificially induced cladding defects were compared by leach testing. The study was conducted in support of the Nevada Nuclear Waste Storage Investigations (NNWSI) Waste Package Task to evaluate the effectiveness of failed cladding as a barrier to radionuclide release. Test description and results are presented. 6 references, 4 figures.

  20. Radionuclide release from PWR spent fuel specimens with induced cladding defects

    SciTech Connect (OSTI)

    Wilson, C.N.; Oversby, V.M.

    1984-03-01

    Radionuclide releases from pressurized water reactor (PWR) spent fuel rod specimens containing various artificially induced cladding defects were compared by leach testing. The study was conducted in support of the Nevada Nuclear Waste Storage Investigations (NNWSI) Waste Package Task to evaluate the effectiveness of failed cladding as a barrier to radionuclide release. Test description and results are presented.

  1. Validation Specimen for Contour Method Extension to Multiple Residual Stress Components

    SciTech Connect (OSTI)

    Pagliaro, Pierluigi; Prime, Michael B; Zuccarello, B; Clausen, Bjorn; Watkins, Thomas R

    2007-01-01

    A new theoretical development of the contour method, that allow the user to measure the three normal residual stress components on cross sections of a generic mechanical part, is presented. To validate such a theoretical development, a residual stress test specimen was properly designed, fabricated and then tested with different experimental techniques.

  2. High-resolution, cryogenic, side-entry type specimen stage

    DOE Patents [OSTI]

    King, Wayne E.; Merkle, Karl L.

    1979-01-01

    A high-resolution, cryogenic side-entry type specimen stage includes a copper block within which a specimen can be positioned in the electron beam of an electron microscope, one end of the copper block constituting a specimen heat exchanger, means for directing a flow of helium at cryogenic temperature into the heat exchanger, and electrical leads running from the specimen to the exterior of the microscope for four point D.C. electrical resistivity measurements.

  3. Radiative cooling test facility and performance evaluation of 4-MIL aluminized polyvinyl fluoride and white-paint surfaces

    SciTech Connect (OSTI)

    Kruskopf, M.S.; Berdahl, P.; Martin, M.; Sakkal, F.; Sobolewski, M.

    1980-11-01

    A test facility designed to measure the amount of radiative cooling a specific material or assembly of materials will produce when exposed to the sky is described. Emphasis is placed upon assemblies which are specifically designed to produce radiative cooling and which therefore offer promise for the reduction of temperatures and/or humidities in occupied spaces. The hardware and software used to operate the facility are documented and the results of the first comprehensive experiments are presented. A microcomputer-based control/data acquisition system was employed to study the performance of two prototype radiator surfaces: 4-mil aluminized polyvinyl fluoride (PVF) and white painted surfaces set below polyethylene windscreens. The cooling rates for materials tested were determined and can be approximated by an equation (given). A computer model developed to simulate the cooling process is presented. (MCW)

  4. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Underground Nuclear Tests - 2011, Part 2

    SciTech Connect (OSTI)

    Pawloski, G A

    2012-01-30

    This report evaluates collapse evolution for selected Lawrence Livermore National Laboratory (LLNL) underground nuclear tests at the Nevada National Security Site (NNSS, formerly called the Nevada Test Site). The work is being done to support several different programs that desire access to the ground surface above expended underground nuclear tests. The programs include: the Borehole Management Program, the Environmental Restoration Program, and the National Center for Nuclear Security Gas-Migration Experiment. Safety decisions must be made before a crater area, or potential crater area, can be reentered for any work. Evaluation of cavity collapse and crater formation is input into the safety decisions. Subject matter experts from the LLNL Containment Program who participated in weapons testing activities perform these evaluations. Information used included drilling and hole construction, emplacement and stemming, timing and sequence of the selected test and nearby tests, geology, yield, depth of burial, collapse times, surface crater sizes, cavity and crater volume estimations, ground motion, and radiological release information. Both classified and unclassified data were reviewed. The evaluations do not include the effects of erosion that may modify the collapse craters over time. They also do not address possible radiation dangers that may be present. Various amounts of information are available for these tests, depending on their age and other associated activities. Lack of data can hamper evaluations and introduce uncertainty. We make no attempt to quantify this uncertainty. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Underground Nuclear Tests - 2011 was published on March 2, 2011. This report, considered Part 2 of work undertaken in calendar year 2011, compiles evaluations requested after the March report. The following unclassified summary statements describe collapse evolution and crater

  5. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Underground Nuclear Tests - 2007

    SciTech Connect (OSTI)

    Roberts, S K; Pawloski, G A; Raschke, K

    2007-04-26

    This report describes evaluation of collapse evolution for selected LLNL underground nuclear tests at the Nevada Test Site (NTS). The work is being done at the request of NSTec and supports the Department of Energy National Nuclear Security Association Nevada Site Office Borehole Management Program (BMP). The primary objective of this program is to close (plug) weapons program legacy boreholes that are deemed no longer useful. Safety decisions must be made before a crater area, or potential crater area, can be reentered for any work. Our statements on cavity collapse and crater formation are input into their safety decisions. The BMP is an on-going program to address hundreds of boreholes at the NTS. Each year NSTec establishes a list of holes to be addressed. They request the assistance of the Lawrence Livermore National Laboratory and Los Alamos National Laboratory Containment Programs to provide information related to the evolution of collapse history and make statements on completeness of collapse as relates to surface crater stability. These statements do not include the effects of erosion that may modify the collapse craters over time. They also do not address possible radiation dangers that may be present. Subject matter experts from the LLNL Containment Program and the Chemical Sciences Division who had been active in weapons testing activities performed these evaluations. Information used included drilling and hole construction, emplacement and stemming, timing and sequence of the selected test and nearby tests, geology, yield, depth of burial, collapse times, surface crater sizes, cavity and crater volume estimations, and ground motion. Both classified and unclassified data were reviewed. Various amounts of information are available for these tests, depending on their age and other associated activities. Lack of data can hamper evaluations and introduce uncertainty. We make no attempt to quantify this uncertainty. The following unclassified summary

  6. Rotary turret and reusable specimen holder for mass spectrometer

    DOE Patents [OSTI]

    Banar, Joseph C.; Perrin, Richard E.; Ostrenga, Raymond A.

    1988-01-01

    A sample holder for use in a mass spectrometer is provided for heating a sample to discharge ions through an electrostatic field which focuses and accelerates the ions for analysis. Individual specimen holders form a plurality of filaments for heating the sample materials for ion emission. Mounting devices hold the plurality of filaments at regular spaced apart angles in a closed configuration adjacent the electrostatic field elements. A substantially solid ceramic turret is provided with a plurality of electrical contacts which engage the individual holder means for energizing the filaments and forming a corresponding plurality of radially facing, axially extending first conductive surfaces. A substantially solid stationary turret bearing member is mounted about the rotating turret with a plurality of radially biased second electrical conductive surfaces, mounted to electrically contact facing ones of the plurality of radially facing first conductive surfaces. The assembly provides a large thermal mass for thermal stability and large electrical contact areas for repeatable, stable power input for heating the sample materials. An improved sample holder is also provided having a ceramic body portion for removably engaging conductive wires. The conductive wires are compatible with a selected filament element and the sample material to be analyzed.

  7. Test Plan to Assess Fire Effects on the Function of an Engineered Surface Barrier

    SciTech Connect (OSTI)

    Ward, Anderson L.; Berlin, Gregory T.; Cammann, Jerry W.; Leary, Kevin D.; Link, Steven O.

    2008-09-29

    Wildfire is a frequent perturbation in shrub steppe ecosystems, altering the flora, fauna, atmosphere, and soil of these systems. Research on the fire effects has focused mostly on natural ecosystems with essentially no attention on engineered systems like surface barriers. The scope of the project is to use a simulated wildfire to induce changes in an engineered surface barrier and document the effects on barrier performance. The main objective is to quantify the effects of burning and the resulting post-fire conditions on alterations in soil physical properties; hydrologic response, particularly the water balance; geochemical properties; and biological properties. A secondary objective is to use the lessons learned to maximize fire protection in the design of long-term monitoring systems based on electronic sensors. A simulated wildfire will be initiated, controlled and monitored at the 200-BP-1 barrier in collaboration with the Hanford Fire Department during the fall of 2008. The north half of the barrier will be divided into nine 12 x 12 m plots, each of which will be randomly assigned a fuel load of 2 kg m-2 or 4 kg m-2. Each plot will be ignited around the perimeter and flames allowed to carry to the centre. Any remaining unburned vegetation will be manually burned off using a drip torch. Progress of the fire and its effects will be monitored using point measurements of thermal, hydrologic, and biotic variables. Three measures of fire intensity will be used to characterize fire behavior: (1) flame height, (2) the maximum temperature at three vertical profile levels, and (3) total duration of elevated temperature at these levels. Pre-burn plant information, including species diversity, plant height, and canopy diameter will be measured on shrubs from the plots to be burned and from control plots at the McGee ranch. General assessments of shrub survival, recovery, and recruitment will be made after the fire. Near-surface soil samples will be collected pre- and

  8. Hot surface ignition system control module with accelerated igniter warm-up test program

    SciTech Connect (OSTI)

    Brown, B.T.

    1986-10-07

    This patent describes a gas burner control system which consists of: a burner; an electrical resistance igniter for igniting the burner; valve means for controlling flow of gas to the burner; and a control module, including a microcomputer, for controlling operation of the igniter and the valve means, the microcomputer being programmed to provide a preselected igniter warm-up time period for enabling the igniter to attain a temperature sufficient to ignite gas, the microcomputer being further programmed to provide a test routine including a program for providing an accelerated igniter warm-up time period which is shorter than the preselected igniter warm-up time period but sufficiently long for enabling the igniter to attain at least the minimum temperature required to ignite gas, the program in the test routine being executed in response to a unique signal effected by the control module and a test device which is external from and detachably connected to the control module.

  9. Apparatus and method for magnetically processing a specimen

    DOE Patents [OSTI]

    Ludtka, Gerard M; Ludtka, Gail M; Wilgen, John B; Kisner, Roger A; Jaramillo, Roger A

    2013-09-03

    An apparatus for magnetically processing a specimen that couples high field strength magnetic fields with the magnetocaloric effect includes a high field strength magnet capable of generating a magnetic field of at least 1 Tesla and a magnetocaloric insert disposed within a bore of the high field strength magnet. A method for magnetically processing a specimen includes positioning a specimen adjacent to a magnetocaloric insert within a bore of a magnet and applying a high field strength magnetic field of at least 1 Tesla to the specimen and to the magnetocaloric insert. The temperature of the specimen changes during the application of the high field strength magnetic field due to the magnetocaloric effect.

  10. Protective structures on the surface of zirconium components of light water reactor cores: Formation, testing, and prototype equipment

    SciTech Connect (OSTI)

    Begrambekov, L. B.; Gordeev, A. A.; Evsin, A. E. Ivanova, S. V.; Kaplevsky, A. S.; Sadovskiy, Ya. A.

    2015-12-15

    The results of tests of plasma treatment of zirconium and deposition of protective yttrium coatings used as the methods of protection of zirconium components of light water reactor cores against hydrogenation are detailed. The amount of hydrogen in the treated sample exposed to superheated steam for 2500 h at temperature T = 400°C and pressure p = 1 atm was five times lower than the corresponding value for the untreated one. The amount of hydrogen in the sample coated with yttrium remained almost unchanged in 4000 h of exposure. A plasma method for rapid testing for hydrogen resistance is proposed. The hydrogenation rate provided by this method is 700 times higher than that in tests with superheated steam. The results of preliminary experiments confirm the possibility of constructing a unit for batch processing of the surfaces of fuel rod claddings.

  11. Evaluation of Cavity Collapse and Surface Crater Formation for Selected Lawrence Livermore National Laboratory Underground Nuclear Tests - 2006

    SciTech Connect (OSTI)

    Pawloski, G A; Raschke, K

    2006-03-16

    This report describes evaluation of collapse evolution for selected LLNL underground nuclear tests at the Nevada Test Site (NTS). The work is being done at the request of Bechtel Nevada and supports the Department of Energy National Nuclear Security Association Nevada Site Office Borehole Management Program (BMP). The primary objective of this program is to close (plug) weapons program legacy boreholes that are deemed no longer useful. Safety decisions must be made before a crater area, or potential crater area, can be reentered for any work. Our statements on cavity collapse and crater formation are input into their safety decisions. The BMP is an on-going program to address hundreds of boreholes at the NTS. Each year Bechtel Nevada establishes a list of holes to be addressed. They request the assistance of the Lawrence Livermore National Laboratory and Los Alamos National Laboratory Containment Programs to provide information related to the evolution of collapse history and make statements on completeness of collapse as relates to surface crater stability. These statements do not include the effects of erosion that may modify the collapse craters over time. They also do not address possible radiation dangers that may be present. Subject matter experts from the LLNL Containment Program and the Chemistry Biology and Nuclear Sciences Division who had been active in weapons testing activities performed these evaluations. Information used included drilling and hole construction, emplacement and stemming, timing and sequence of the selected test and nearby tests, geology, yield, depth of burial, collapse times, surface crater sizes, cavity and crater volume estimations, and ground motion. Both classified and unclassified data were reviewed. Various amounts of information are available for these tests, depending on their age and other associated activities. Lack of data can hamper evaluations and introduce uncertainty. We make no attempt to quantify this uncertainty.

  12. Dissociative chemisorption of methane on metal surfaces: Tests of dynamical assumptions using quantum models and ab initio molecular dynamics

    SciTech Connect (OSTI)

    Jackson, Bret; Nattino, Francesco; Kroes, Geert-Jan

    2014-08-07

    The dissociative chemisorption of methane on metal surfaces is of great practical and fundamental importance. Not only is it the rate-limiting step in the steam reforming of natural gas, the reaction exhibits interesting mode-selective behavior and a strong dependence on the temperature of the metal. We present a quantum model for this reaction on Ni(100) and Ni(111) surfaces based on the reaction path Hamiltonian. The dissociative sticking probabilities computed using this model agree well with available experimental data with regard to variation with incident energy, substrate temperature, and the vibrational state of the incident molecule. We significantly expand the vibrational basis set relative to earlier studies, which allows reaction probabilities to be calculated for doubly excited initial vibrational states, though it does not lead to appreciable changes in the reaction probabilities for singly excited initial states. Sudden models used to treat the center of mass motion parallel to the surface are compared with results from ab initio molecular dynamics and found to be reasonable. Similar comparisons for molecular rotation suggest that our rotationally adiabatic model is incorrect, and that sudden behavior is closer to reality. Such a model is proposed and tested. A model for predicting mode-selective behavior is tested, with mixed results, though we find it is consistent with experimental studies of normal vs. total (kinetic) energy scaling. Models for energy transfer into lattice vibrations are also examined.

  13. Project test plan for runoff and erosion on fine-soil barrier surfaces and rock-covered side slopes

    SciTech Connect (OSTI)

    Walters, W.H.; Hoover, K.A.; Cadwell, L.L.

    1990-06-01

    Pacific Northwest Laboratory (PNL) and Westinghouse Hanford Company are working together to develop protective barriers to isolate near-surface radioactive waste. The purpose of the barriers is to protect defense wastes at the US Department of Energy's (DOE) Hanford Site from infiltration of precipitation, biointrusion, and surficial erosion for up to 10,000 years without the need for long-term monitoring, maintenance, or institutional control. The barriers will be constructed of layered earth and rock material designed to direct surface and groundwater pathways away from the buried waste. To address soil erosion as it applies to barrier design and long-term stability, a task designed to study this problem has been included in the Protective Barriers Program at PNL. The barrier soil-erosion task will investigate the ability of the soil cover and side slopes to resist the erosional and destabilizing processes from externally applied water. The study will include identification and field testing of the dominant processes contributing to erosion and barrier failure. The effects of rock mulches, vegetation cover on the top fine-grained soil surface, as well as the stability of rock armoring on the side slopes, will be evaluated. Some of the testing will include the effects of animal intrusion on barrier erosion, and these will be coordinated with other animal intrusion studies. 6 refs., 4 figs., 1 tab.

  14. A Non-Electrostatic Surface Complexation Approach to Modeling Radionuclide Migration at the Nevada Test Site: II. Aluminosilicates

    SciTech Connect (OSTI)

    Zavarin, M; Bruton, C J

    2004-12-16

    Reliable quantitative prediction of contaminant transport in subsurface environments is critical to evaluating the risks associated with radionuclide migration. As part of the Underground Test Area (UGTA) program, radionuclide transport away from selected underground nuclear tests conducted in the saturated zone at the Nevada Test Site (NTS) is being examined. In the near-field environment, reactive transport simulations must account for changes in water chemistry and mineralogy as a function of time and their effect on radionuclide migration. Unlike the Kd approach, surface complexation reactions, in conjunction with ion exchange and precipitation, can be used to describe radionuclide reactive transport as a function of changing environmental conditions. They provide a more robust basis for describing radionuclide retardation in geochemically dynamic environments. In a companion report (Zavarin and Bruton, 2004), a database of radionuclide surface complexation reactions for calcite and iron oxide minerals was developed. In this report, a second set of reactions is developed: surface complexation (SC) and ion exchange (IE) to aluminosilicate minerals. The most simplified surface complexation model, the one-site non-electrostatic model (NEM), and the Vanselow IE model were used to fit a large number of published sorption data and a reaction constant database was developed. Surface complexation of Am(III), Eu(III), Np(V), Pu(IV), Pu(V), and U(VI) to aluminum oxide, silica, and aluminosilicate minerals was modeled using a generalized approach in which surface complexation to aluminosilicate >SiOH or >AlOH reactive sites was considered equivalent to the reactivity of aluminum oxide and silica reactive sites. Ion exchange was allowed to be mineral-dependent. The generalized NEM approach, in conjunction with Vanselow IE, was able to fit most published sorption data well. Fitting results indicate that surface complexation will dominate over ion exchange at pH >7 for the

  15. INFLUENCE OF SPECIMEN SIZE/TYPE ON THE FRACTURE TOUGHNESS OF FIVE IRRADIATED RPV MATERIALS

    SciTech Connect (OSTI)

    Sokolov, Mikhail A; Lucon, Enrico

    2015-01-01

    The Heavy-Section Steel Irradiation (HSSI) Program had previously irradiated five reactor pressure vessel (RPV) steels/welds at fast neutron fluxes of about 4 to 8 1011 n/cm2/s (>1 MeV) to fluences from 0.5 to 3.4 1019 n/cm2 and at 288 C. The unirradiated fracture toughness tests were performed by Oak Ridge National Laboratory with 12.7-mm and 25.4-mm thick (0.5T and 1T) compact specimens, while the HSSI Program provided tensile and 5 10-mm three-point bend specimens to SCK CEN for irradiation in the in-pile section of the Belgian Reactor BR2 at fluxes >1013 n/cm2/s and subsequent testing by SCK CEN. The BR2 irradiations were conducted at about 2 and 4 1013 n/cm2/s with irradiation temperature between 295 C and 300 C (water temperature), and to fluences between 6 and10 1019 n/cm2. The irradiation-induced shifts of the Master Curve reference temperatures, T0, for most of the materials deviated from the embrittlement correlations much more than expected, motivating the testing of 5 10-mm three-point bend specimens of all five materials in the unirradiated condition to eliminate specimen size and geometry as a variable. Tests of the unirradiated small bend specimens resulted in Master Curve reference temperatures, T0, 25 C to 53 C lower than those from the larger compact specimens, meaning that the irradiation-induced reference temperature shifts, T0, were larger than the initial measurements, resulting in much improved agreement between the measured and predicted fracture toughness shifts.

  16. Fracture of surface cracks loaded in bending

    SciTech Connect (OSTI)

    Chao, Y.J.; Reuter, W.G.

    1997-12-31

    Theoretical background of the constraint effect in brittle fracture of solids is reviewed. Fracture test data from D6-aC, a high strength steel, using three-point-bend (SE(B)) specimens and surface cracked plate (SC(B)) specimens under bending are presented. It is shown that the SE(B) data has an elevated fracture toughness for increasing a/W, i.e., a crack geometry with a larger T/K corresponds to a higher K{sub c} which is consistent with the theoretical prediction. The fundamental fracture properties, i.e., the critical strain and the critical distance, determined from the SE(B) test data are then applied to the interpretation and prediction of the SC(B) test data. Reasonable agreement is achieved for the crack growth initiation site and the load.

  17. Flow Components in a NaK Test Loop Designed to Simulate Conditions in a Nuclear Surface Power Reactor

    SciTech Connect (OSTI)

    Polzin, Kurt A.; Godfroy, Thomas J.

    2008-01-21

    A test loop using NaK as the working fluid is presently in use to study material compatibility effects on various components that comprise a possible nuclear reactor design for use on the lunar surface. A DC electromagnetic (EM) pump has been designed and implemented as a means of actively controlling the NaK flow rate through the system and an EM flow sensor is employed to monitor the developed flow rate. These components allow for the matching of the flow rate conditions in test loops with those that would be found in a full-scale surface-power reactor. The design and operating characteristics of the EM pump and flow sensor are presented. In the EM pump, current is applied to a set of electrodes to produce a Lorentz body force in the fluid. A measurement of the induced voltage (back-EMF) in the flow sensor provides the means of monitoring flow rate. Both components are compact, employing high magnetic field strength neodymium magnets thermally coupled to a water-cooled housing. A vacuum gap limits the heat transferred from the high temperature NaK tube to the magnets and a magnetically-permeable material completes the magnetic circuit. The pump is designed to produce a pressure rise of 34.5 kPa, and the flow sensor's predicted output is roughly 20 mV at the loop's nominal flow rate of 0.114 m{sup 3}/hr.

  18. Corrective Action Plan for Corrective Action Unit 417: Central Nevada Test Area Surface, Nevada

    SciTech Connect (OSTI)

    K. Campbell

    2000-04-01

    This Corrective Action Plan provides methods for implementing the approved corrective action alternative as provided in the Corrective Action Decision Document for the Central Nevada Test Area (CNTA), Corrective Action Unit (CAU) 417 (DOE/NV, 1999). The CNTA is located in the Hot Creek Valley in Nye County, Nevada, approximately 137 kilometers (85 miles) northeast of Tonopah, Nevada. The CNTA consists of three separate land withdrawal areas commonly referred to as UC-1, UC-3, and UC-4, all of which are accessible to the public. CAU 417 consists of 34 Corrective Action Sites (CASs). Results of the investigation activities completed in 1998 are presented in Appendix D of the Corrective Action Decision Document (DOE/NV, 1999). According to the results, the only Constituent of Concern at the CNTA is total petroleum hydrocarbons (TPH). Of the 34 CASs, corrective action was proposed for 16 sites in 13 CASs. In fiscal year 1999, a Phase I Work Plan was prepared for the construction of a cover on the UC-4 Mud Pit C to gather information on cover constructibility and to perform site management activities. With Nevada Division of Environmental Protection concurrence, the Phase I field activities began in August 1999. A multi-layered cover using a Geosynthetic Clay Liner as an infiltration barrier was constructed over the UC-4 Mud Pit. Some TPH impacted material was relocated, concrete monuments were installed at nine sites, signs warning of site conditions were posted at seven sites, and subsidence markers were installed on the UC-4 Mud Pit C cover. Results from the field activities indicated that the UC-4 Mud Pit C cover design was constructable and could be used at the UC-1 Central Mud Pit (CMP). However, because of the size of the UC-1 CMP this design would be extremely costly. An alternative cover design, a vegetated cover, is proposed for the UC-1 CMP.

  19. Midtemperature Solar Systems Test Facility predictions for thermal performance based on test data. Alpha Solarco Model 104 solar collector with 0. 125-inch Schott low-iron glass reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-04-01

    Thermal performance predictions based on test data are presented for the Alpha Solarco Model 104 solar collector, with 0.125-inch Schott low-iron glass reflector surface, for three output temperatures at five cities in the United States.

  20. Evaluation of Cavity Collapse and Surface Crater Formation at the Salut Underground Nuclear Test in U20ak, Nevada National Security Site, and the Impact of Stability of the Ground Surface

    SciTech Connect (OSTI)

    Pawloski, G A

    2012-04-25

    At the request of Jerry Sweeney, the LLNL Containment Program performed a review of nuclear test-related data for the Salut underground nuclear test in U20ak to assist in evaluating this legacy site as a test bed for application technologies for use in On-Site Inspections (OSI) under the Comprehensive Nuclear Test Ban Treaty. Review of the Salut site is complicated because the test experienced a subsurface, rather than surface, collapse. Of particular interest is the stability of the ground surface above the Salut detonation point. Proposed methods for on-site verification include radiological signatures, artifacts from nuclear testing activities, and imaging to identify alteration to the subsurface hydrogeologogy due to the nuclear detonation. Sweeney's proposal requires physical access at or near the ground surface of specific underground nuclear test locations at the Nevada Nuclear Test Site (NNSS, formerly the Nevada Test Site), and focuses on possible activities such as visual observation, multispectral measurements, and shallow, and deep geophysical surveys.

  1. Small Specimen Data from a High Temperature HFIR Irradiation Experiment

    SciTech Connect (OSTI)

    Burchell, Timothy D; McDuffee, Joel Lee; Thoms, Kenneth R

    2014-01-01

    The HTV capsule is a High Flux Isotope Reactor (HFIR) target-rod capsule designed to operate at very high temperatures. The graphite containing section of the capsule (in core) is approximately 18 inches (457.2 mm) long and is separated into eight temperature zones. The specimen diameters within each zone are set to achieve the desired gas gap and hence design temperature (900 C, 1200 C or 1500 C). The capsule has five zones containing 0.400 inch (10.16 mm) diameter specimens, two zones containing 0.350 inch (8.89 mm) diameter specimens and one zone containing 0.300 inch (7.62 mm) diameter specimens. The zones have been distributed within the experiment to optimize the gamma heating from the HFIR core as well as minimize the axial heat flow in the capsule. Consequently, there are two 900 C zones, three 1200 C zones, and three 1500 C zones within the HTV capsule. Each zone contains nine specimens 0.210 0.002 inches (5.334 mm) in length. The capsule will be irradiated to a peak dose of 3.17 displacements per atom. The HTV specimens include samples of the following graphite grades: SGL Carbon s NBG-17 and NBG-18, GrafTech s PCEA, Toyo Tanso s IG-110, Mersen s 2114 and the reference grade H-451 (SGL Carbon). As part of the pre-irradiation program the specimens were characterized using ASTM Standards C559 for bulk density, and ASTM C769 for approximate Young s modulus from the sonic velocity. The probe frequency used for the determination of time of flight of the ultrasonic signal was 2.25 MHz. Marked volume (specimen diameter) effects were noted for both bulk density (increased with increasing specimen volume or diameter) and Dynamic Young s modulus (decreased with increasing specimen volume or diameter). These trends are extended by adding the property vs. diameter data for unirradiated AGC-1 creep specimens (nominally 12.5 mm-diameter x 25.4 mm-length). The relatively large reduction in Dynamic Young s Modulus was surprising given the trend for increasing density

  2. NREL: Measurements and Characterization - Surface Analysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    distributions Analyze a wide range of materials, including photovoltaics, microelectronics, polymers, and biological specimens. Our Surface Analysis group wants to work...

  3. Evaluation of Cavity Collapse and Surface Crater Formation at the Norbo Underground Nuclear Test in U8c, Nevada Nuclear Security Site, and the Impact on Stability of the Ground Surface

    SciTech Connect (OSTI)

    Pawloski, G A

    2012-06-18

    Lawrence Livermore National Laboratory (LLNL) Containment Program performed a review of nuclear test-related data for the Norbo underground nuclear test in U8c to assist in evaluating this legacy site as a test bed for application technologies for use in On-Site Inspections (OSI) under the Comprehensive Nuclear Test Ban Treaty. This request is similar to one made for the Salut site in U8c (Pawloski, 2012b). Review of the Norbo site is complicated because the test first exhibited subsurface collapse, which was not unusual, but it then collapsed to the surface over one year later, which was unusual. Of particular interest is the stability of the ground surface above the Norbo detonation point. Proposed methods for on-site verification include radiological signatures, artifacts from nuclear testing activities, and imaging to identify alteration to the subsurface hydrogeology due to the nuclear detonation. Aviva Sussman from the Los Alamos National Laboratory (LANL) has also proposed work at this site. Both proposals require physical access at or near the ground surface of specific underground nuclear test locations at the Nevada Nuclear Security Site (NNSS), formerly the Nevada Test Site (NTS), and focus on possible activities such as visual observation, multispectral measurements, and shallow and deep geophysical surveys.

  4. Ultra high vacuum heating and rotating specimen stage

    DOE Patents [OSTI]

    Coombs, A.W. III

    1995-05-02

    A heating and rotating specimen stage provides for simultaneous specimen heating and rotating. The stage is ideally suited for operation in ultrahigh vacuum (1{times}10{sup {minus}9} torr or less), but is useful at atmosphere and in pressurized systems as well. A specimen is placed on a specimen holder that is attached to a heater that, in turn, is attached to a top housing. The top housing is rotated relative to a bottom housing and electrically connected thereto by electrically conductive brushes. This stage is made of materials that are compatible with UHV, able to withstand high temperatures, possess low outgassing rates, are gall and seize resistant, and are able to carry substantial electrical loading without overheating. 5 figs.

  5. True uniaxial compressive strengths of rock or coal specimens are independent of diameter-to-length ratios. Report of Investigations/1990

    SciTech Connect (OSTI)

    Babcock, C.O.

    1990-01-01

    Part of the compressive strength of a test specimen of rock or coal in the laboratory or a pillar in a mine comes from physical property strength and, in part, from the constraint provided by the loading stresses. Much confusion in pillar design comes from assigning the total strength change to geometry, as evidenced by the many pillar design equations with width to height as the primary variable. In tests by the U.S. Bureau of Mines, compressive strengths for cylindrical specimens of limestone, marble, sandstone, and coal were independent of the specimen test geometry when the end friction was removed. A conventional uniaxial compressive strength test between two steel platens is actually a uniaxial force and not a uniaxial stress test. The biaxial or triaxial state of stress for much of the test volume changes with the geometry of the test specimen. By removing the end friction supplied by the steel platens to the specimen, a more nearly uniaxial stress state independent of the specimen geometry is produced in the specimen. Pillar design is a constraint and physical property problem rather than a geometry problem. Roof and floor constraint are major factors in pillar design and strength.

  6. Resonance test system

    DOE Patents [OSTI]

    Musial, Walter; White, Darris

    2011-05-31

    An apparatus (10) for applying at least one load to a specimen (12) according to one embodiment of the invention may comprise a mass (18). An actuator (20) mounted to the specimen (12) and operatively associated with the mass (18) moves the mass (18) along a linear displacement path (22) that is perpendicular to a longitudinal axis of the specimen (12). A control system (26) operatively associated with the actuator (20) operates the actuator (20) to reciprocate the mass (18) along the linear displacement path (22) at a reciprocating frequency, the reciprocating frequency being about equal to a resonance frequency of the specimen (12) in a test configuration.

  7. Fracture toughness determination using spiral-grooved cylindrical specimen and pure torsional loading

    DOE Patents [OSTI]

    Wang, Jy-An; Liu, Kenneth C.

    2003-07-08

    A method for determining fracture toughness K.sub.IC of materials ranging from metallic alloys, brittle ceramics and their composites, and weldments. A cylindrical specimen having a helical V-groove with a 45.degree. pitch is subjected to pure torsion. This loading configuration creates a uniform tensile-stress crack-opening mode, and a transverse plane-strain state along the helical groove. The full length of the spiral groove is equivalent to the thickness of a conventional compact-type specimen. K.sub.IC values are determined from the fracture torque and crack length measured from the test specimen using a 3-D finite element program (TOR3D-KIC) developed for the purpose. In addition, a mixed mode (combined tensile and shear stress mode) fracture toughness value can be determined by varying the pitch of the helical groove. Since the key information needed for determining the K.sub.IC value is condensed in the vicinity of the crack tip, the specimen can be significantly miniaturized without the loss of generality.

  8. On the modeling of the Taylor cylinder impact test for orthotropic textured materials: Calculations and experiments

    SciTech Connect (OSTI)

    Maudlin, P.J.; Bingert, J.F.; House, J.W.

    1997-04-01

    Taylor impact tests using specimens cut from a rolled plate of Ta were conducted. The Ta was well-characterized in terms of flow stress and crystallographic texture. A piece-wise yield surface was interrogated from this orthotropic texture, and used in EPIC-95 3D simulations of the Taylor test. Good agreement was realized between the calculations and the post-test geometries in terms of major and minor side profiles and impact-interface footprints.

  9. WAFER TEST CAVITY -Linking Surface Microstructure to RF Performance: a ‘Short-­Sample Test Facility’ for characterizing superconducting materials for SRF cavities.

    SciTech Connect (OSTI)

    Pogue, Nathaniel; Comeaux, Justin; McIntyre, Peter

    2014-05-30

    The Wafer Test cavity was designed to create a short sample test system to determine the properties of the superconducting materials and S-I-S hetero-structures. The project, funded by ARRA, was successful in accomplishing several goals to achieving a high gradient test system for SRF research and development. The project led to the design and construction of the two unique cavities that each severed unique purposes: the Wafer test Cavity and the Sapphire Test cavity. The Sapphire Cavity was constructed first to determine the properties of large single crystal sapphires in an SRF environment. The data obtained from the cavity greatly altered the design of the Wafer Cavity and provided the necessary information to ascertain the Wafer Test cavity’s performance.

  10. Grand Junction Projects Office Remedial Action Project: Feasibility test of real-time radiation monitoring during removal of surface contamination from concrete floors

    SciTech Connect (OSTI)

    Leino, R.; Corle, S.

    1995-10-01

    This feasibility test was conducted to determine if real-time radiation-monitoring instruments could be mounted on decontamination machines during remediation activities to provide useful and immediate feedback to equipment operators. The U.S. Department of Energy (DOE) sponsored this field test under the Grand Junction Projects Office Remedial Action Project (GJPORAP) to identify a more efficient method to remove radiological contamination from concrete floor surfaces. This test demonstrated that project durations and costs may be reduced by combining radiation-monitoring equipment with decontamination machines. The test also demonstrated that a microprocessor-based instrument such as a radiation monitor can withstand the type of vibration that is characteristic of floor scabblers with no apparent damage. Combining radiation-monitoring equipment with a decontamination machine reduces the time and costs required to decontaminate concrete surfaces. These time and cost savings result from the reduction in the number of interim radiological surveys that must be conducted to complete remediation. Real-time radiation monitoring allows equipment operators to accurately monitor contamination during the decontamination process without support from radiological technicians, which also reduces the project duration and costs. The DOE Grand Junction Projects Office recommends more extensive and rigorous testing of this real-time radiation monitoring to include a variety of surfaces and decontamination machines. As opportunities arise, additional testing will be conducted under GJPORAP.

  11. Midtemperature solar systems test facility predictions for thermal performance of the Acurex solar collector with FEK 244 reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1981-01-01

    Thermal performance predictions are presented for the Acurex solar collector, with FEK 244 reflector surface, for three output temperatures at five cities in the United States.

  12. RESULTS OF THE EXAMINATION OF ELECTROCHEMICAL NOISE PROBE SPECIMENS REMOVED FROM TANK 241-AN-107 JUNE 2010

    SciTech Connect (OSTI)

    COOKE GA; WYRWAS RB; DUNCAN JB

    2010-11-11

    An Integrated Multi-function Corrosion Probe (IMCP) was installed in Tank 241-AN-107 on September 20, 2006. A portion of the probe was retrieved on June 8, 2010 and the sections holding the detectors were delivered to the 222-S Laboratory for analysis. The examination and disassembly of the probe sections encountered a number of challenges. However, disassembly and relevant analyses were successfully completed. The following summarizes our observations. Brittle failure of the fiberglass probe in the middle of detector 2 resulted in the recovery of only three vapor space C-rings and six supernatant bullet specimens. The design of the bullets and how they were attached to the probe made the recovery of the components more difficult. The use of glue/epoxy on the bullets and the attachment of the flat bottom of the bullets to the curved surface of the fiberglass probe body meant that weight loss on cleaning and surface area of the specimens could not be determined with acceptable accuracy. Macrophotography of all specimens reveals that corrosion was slight in the vapor space and extremely slight in the supernatant. The one pre-cracked C-ring recovered from the vapor space still had the stress bulge visible on the polished surface, indicating that crack propagation had not occurred in the tank. No photographs were taken of the C-ring before deployment. No further analysis was conducted on this specimen. A detailed discussion and photographic documentation are provided in this report.

  13. Ultrasonic Evaluation of Two Dissimilar Metal Weld Overlay Specimens

    SciTech Connect (OSTI)

    Crawford, Susan L.; Cinson, Anthony D.; Prowant, Matthew S.; Moran, Traci L.; Anderson, Michael T.

    2012-06-30

    Two dissimilar metal weld (DMW) pipe-to-nozzle specimens were implanted with thermal fatigue cracks in the 13% to 90% through-wall depth range. The specimens were ultrasonically evaluated with phased-array probes having center frequencies of 0.8, 1.0, 1.5, and 2.0 megahertz (MHz). An Alloy 82/182 weld overlay (WOL) was applied and the specimens were ultrasonically re-evaluated for flaw detection and characterization. The Post-WOL flaw depths were approximately 10% to 56% through-wall. This study has shown the effectiveness of ultrasonic examinations of Alloy 82/182 overlaid DMW specimens. Phased-array probes with center frequency in the 0.8- to 1.0-MHz range provide a strong coherent signal but the greater ultrasonic wavelength and larger beam spot size prevent the reliable detection of small flaws. These small flaws had nominal through-wall depths of less than 15% and length in the 50-60 mm (2-2.4 in.) range. Flaws in the 19% and greater through-wall depth range were readily detected with all four probes. At the higher frequencies, the reflected signals are less coherent but still provide adequate signal for flaw detection and characterization. A single inspection at 2.0 MHz could provide adequate detection and sizing information but a supplemental inspection at 1.0 or 1.5 MHz is recommended.

  14. Investigation of temperature dependence of fracture toughness in high-dose HT9 steel using small-specimen reuse technique

    SciTech Connect (OSTI)

    Baek, Jong-Hyuk; Byun, Thak Sang; Maloy, Stuart A.; Toloczko, Mychailo B.

    2014-01-01

    The temperature dependence of fracture toughness in HT9 steel irradiated to 3145 dpa at 380503 degrees*C was investigated using miniature three-point bend (TPB) fracture specimens. A miniature-specimen reuse technique has been established: the tested halves of subsize Charpy impact specimens with dimensions of 27 mm *3mm* 4 mm were reused for this fracture test campaign by cutting a notch with a diamond-saw in the middle of each half, and by fatigue-precracking to generate a sharp crack tip. It was confirmed that the fracture toughness of HT9 steel in the dose range depends more strongly on the irradiation temperature than the irradiation dose. At an irradiation temperature <430 *degreesC, the fracture toughness of irradiated HT9 increased with the test temperature, reached an upper shelf of 180200 MPa*m^.5 at 350450 degrees*C, and then decreased with the test temperature. At an irradiation temperature >430 degrees*C, the fracture toughness was nearly unchanged up to about 450 *degreesC and decreased slowly with test temperatures in a higher temperature range. Such a rather monotonic test temperature dependence after high-temperature irradiation is similar to that observed for an archive material generally showing a higher degree of toughness. A brittle fracture without stable crack growth occurred in only a few specimens with relatively lower irradiation and test temperatures. In this discussion, these TPB fracture toughness data are compared with previously published data from 12.7 mm diameter disc compact tension (DCT) specimens.

  15. Streamlined Approach for Environmental Restoration Plan for Corrective Action Unit 484: Surface Debris, Waste Sites, and Burn Area, Tonopah Test Range, Nevada

    SciTech Connect (OSTI)

    Bechel Nevada

    2004-05-01

    This Streamlined Approach for Environmental Restoration plan details the activities necessary to close Corrective Action Unit (CAU) 484: Surface Debris, Waste Sites, and Burn Area (Tonopah Test Range). CAU 484 consists of sites located at the Tonopah Test Range, Nevada, and is currently listed in Appendix III of the Federal Facility Agreement and Consent Order. CAU 484 consists of the following six Corrective Action Sites: (1) CAS RG-52-007-TAML, Davis Gun Penetrator Test; (2) CAS TA-52-001-TANL, NEDS Detonation Area; (3) CAS TA-52-004-TAAL, Metal Particle Dispersion Test; (4) CAS TA-52-005-TAAL, Joint Test Assembly DU Sites; (5) CAS TA-52-006-TAPL, Depleted Uranium Site; and (6) CAS TA-54-001-TANL, Containment Tank and Steel Structure

  16. Method for non-destructive testing

    DOE Patents [OSTI]

    Akers, Douglas W.

    2011-08-30

    Non-destructive testing method may include providing a source material that emits positrons in response to bombardment of the source material with photons. The source material is exposed to photons. The source material is positioned adjacent the specimen, the specimen being exposed to at least some of the positrons emitted by the source material. Annihilation gamma rays emitted by the specimen are detected.

  17. Room-temperature fracture in V-(4-5)Cr-(4-5)Ti tensile specimens irradiated in Fusion-1 BOR-60 experiment

    SciTech Connect (OSTI)

    Gazda, J.; Meshii, M.; Tsai, H.

    1998-09-01

    Specimens of V-(4-5)Cr-(4-5)Ti alloys were irradiated to {approx}18 dpa at 320 C in the Fusion-1 capsule inserted into the BOR-60 reactor. Tensile tests at 23 C indicated dramatic yield strength increase (>300%), lack of work hardening, and minimal (<1%) total elongations. SEM analysis of fracture and side surfaces were conducted to determine reduction in are and the mode of fracture. The reduction of area was negligible. All but one specimen failed by a combination of ductile shear deformation and cleavage crack growth. Transgranular cleavage cracks were initiated by stress concentrations at the tips of the shear bands. In side-view observations, evidence was found of slip bands typically associated with dislocation channeling. No differences due to pre-irradiation heat treatment and heat-to-heat composition variations were detected. The only deviation from this behavior was found in V-4Cr-4Ti-B alloy, which failed in the grip portion by complete cleavage cracking.

  18. Analysis of the toxicity in Rocky Flats Plant surface water through a correlation between the whole effluent toxicity test and the Microtox assay

    SciTech Connect (OSTI)

    Ford, S.M.; Wolaver, H.A.; Figueroa, L.A.

    1992-07-01

    Results were correlated from the Microtox assay and the whole effluent acute toxicity test for effluents from the (1) wastewater treatment plant (WWTP) and (2) terminal ponds located at the Rocky Flats Plant. Literature reviews indicate that Photobacterium phosphoreum (Microtox assay) may be used as screening test for the reaction of Ceriodaphnia dubia and Pimephales promelas to toxins present in effluents. This study indicates that the Microtox is less sensitive to toxins present in the WWTP effluent than other test organisms (Ceriodaphnia dubia and Pimephales promelas). Toxicity appears to be from unionized ammonia. Ten months of data reveal that the surface water effluents which leave Rocky Flats boundaries are non-toxic when judged by all three test organisms.

  19. Analysis of the toxicity in Rocky Flats Plant surface water through a correlation between the whole effluent toxicity test and the Microtox assay

    SciTech Connect (OSTI)

    Ford, S.M.; Wolaver, H.A. ); Figueroa, L.A. )

    1992-01-01

    Results were correlated from the Microtox assay and the whole effluent acute toxicity test for effluents from the (1) wastewater treatment plant (WWTP) and (2) terminal ponds located at the Rocky Flats Plant. Literature reviews indicate that Photobacterium phosphoreum (Microtox assay) may be used as screening test for the reaction of Ceriodaphnia dubia and Pimephales promelas to toxins present in effluents. This study indicates that the Microtox is less sensitive to toxins present in the WWTP effluent than other test organisms (Ceriodaphnia dubia and Pimephales promelas). Toxicity appears to be from unionized ammonia. Ten months of data reveal that the surface water effluents which leave Rocky Flats boundaries are non-toxic when judged by all three test organisms.

  20. Measurement of surface tension and viscosity by open capillary techniques

    DOE Patents [OSTI]

    Rye,Robert R. , Yost,Frederick G.

    1998-01-01

    An open-channel capillary is provided, having preferably a v-shaped groove in a flat wettable surface. The groove has timing marks and a source marker in which the specimen to be tested is deposited. The time of passage between the timing marks is recorded, and the ratio of surface tension .gamma. to viscosity .mu. is determined from the equation given below: ##EQU1## where h.sub.0 is the groove depth, .alpha. is the groove angle, .theta. is the liquid/solid contact angle, and t is the flow time. It has been shown by the

  1. CHARPY IMPACT TEST RESULTS ON FIVE MAERIALS AND NIST VERIFICATION...

    Office of Scientific and Technical Information (OSTI)

    CHARPY IMPACT TEST RESULTS ON FIVE MAERIALS AND NIST VERIFICATION SPECIMENS USING ... Randy K, Nanstad' and Mikbail A. Sokolov' cHARPY IMPACT' TEST RESULTS ON FIVE MATERIALS ...

  2. Thermal spray and cold spray analysis of density, porosity, and tensile Specimens for use with LIGA applications

    SciTech Connect (OSTI)

    DECKER,MERLIN K.; SMITH,MARK F.

    2000-02-01

    This analysis provides a preliminary investigation into using Twin-Wire Arc Thermal Spray and Cold Spray as material deposition processes for LIGA applications. These spray material processes were studied to make an initial determination of their potential as alternatives to producing mechanical parts via the electroplating process. Three materials, UltraMachinable{reg_sign} Stainless Steel, BondArc{reg_sign}, and aluminum, were sprayed using Thermal Spray. Only aluminum was sprayed using the Cold Spray process. Following the spray procedure, the test specimens were released from a copper mold and then tested. Three tests, density, tensile strength, and porosity, were performed on the specimens to determine the spray effect on material properties. Twin-Wire Arc Thermal Spray did not demonstrate adequate deposition properties and does not appear to be a good process candidate for LIGA. However, Cold Spray yielded better density results and warrants further investigation to analyze the minimum feature size produced by the process.

  3. Sweet Lake Geopressured-geothermal Project, Magma Gulf-Technadril/DOE Amoco Fee. Volume II. Surface installations reservoir testing. Annual report, February 28, 1981-February 10, 1982

    SciTech Connect (OSTI)

    Hoffman, K.S.

    1984-01-01

    The Magma Gulf-Technadril/Department of Energy Amoco Fee No. 1 (production) and salt water disposal wells were drilled in the period from August, 1980 to February 1981. Surface facilities were designed and constructed during March-June 1981. Flow testing began in June 1981 and continued until February, 1982. The Miogypsinoides interval contains seven discrete sands in the test well. These sands have been numbered 1 to 7, beginning at the top of the sequence. Data from wireline logs and core samples suggested that the first zone to be perforated should be Sand 5. Because of its high porosity and permeability, Sand 5 was thought to contain almost 50% of the total hydraulic capacity of the well. Flow testing of Sand 5 was performed in three stages, each of which is fully described in this report. Phase I was designed as an initial clean-up flow and a reservoir confirmation test. Phase II consisted of the reservoir limit determination test and lasted 17 days. Boundaries were confirmed which suggest that the Sweet Lake reservoir is fairly narrow, with boundaries on three sides, but is open in one direction with no closure for at least 4-1/4 miles. These boundaries approximate the shape of the graben in which the test well was drilled, but may or may not be directly related to the major faults forming the graben. Phase III testing was planned to be a long-term test at commercial design rates. Although Sand 5 alone would not support such rates, long-term production was demonstrated. Additional research not supported by DOE funding was also performed during the period covered by this report. This research, consisting of mud logging, micropaleontology, organic geochemistry, core analysis, and rock mechanics, is summarized in this report.

  4. Mechanical characterization of an additively manufactured Inconel 718 theta-shaped specimen

    SciTech Connect (OSTI)

    Cakmak, Ercan; Watkins, Thomas R.; Bunn, Jeffrey R.; Cornwell, Paris A.; Wang, Yanli; Dehoff, Ryan R.; Babu, Sudarsanam Suresh; Sochalski-Kolbus, Lindsay M.

    2015-11-20

    Two sets of “theta”-shaped specimens were additively manufactured with Inconel 718 powders using an electron beam melting technique with two distinct scan strategies. Light optical microscopy, mechanical testing coupled with a digital image correlation (DIC) technique, finite element modeling, and neutron diffraction with in situ loading characterizations were conducted. The cross-members of the specimens were the focus. Light optical micrographs revealed that different microstructures were formed with different scan strategies. Ex situ mechanical testing revealed each build to be stable under load until ductility was observed on the cross-members before failure. The elastic moduli were determined by forming a correlation between the elastic tensile stresses determined from FEM, and the elastic strains obtained from DIC. The lattice strains were mapped with neutron diffraction during in situ elastic loading; and a good correlation between the average axial lattice strains on the cross-member and those determined from the DIC analysis was found. Lastly, the spatially resolved stresses in the elastic deformation regime are derived from the lattice strains and increased with applied load, showing a consistent distribution along the cross-member.

  5. Mechanical characterization of an additively manufactured Inconel 718 theta-shaped specimen

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Cakmak, Ercan; Watkins, Thomas R.; Bunn, Jeffrey R.; Cornwell, Paris A.; Wang, Yanli; Dehoff, Ryan R.; Babu, Sudarsanam Suresh; Sochalski-Kolbus, Lindsay M.

    2015-11-20

    Two sets of “theta”-shaped specimens were additively manufactured with Inconel 718 powders using an electron beam melting technique with two distinct scan strategies. Light optical microscopy, mechanical testing coupled with a digital image correlation (DIC) technique, finite element modeling, and neutron diffraction with in situ loading characterizations were conducted. The cross-members of the specimens were the focus. Light optical micrographs revealed that different microstructures were formed with different scan strategies. Ex situ mechanical testing revealed each build to be stable under load until ductility was observed on the cross-members before failure. The elastic moduli were determined by forming a correlationmore » between the elastic tensile stresses determined from FEM, and the elastic strains obtained from DIC. The lattice strains were mapped with neutron diffraction during in situ elastic loading; and a good correlation between the average axial lattice strains on the cross-member and those determined from the DIC analysis was found. Lastly, the spatially resolved stresses in the elastic deformation regime are derived from the lattice strains and increased with applied load, showing a consistent distribution along the cross-member.« less

  6. Combined UHV/high-pressure catalysis setup for depth-resolved near-surface spectroscopic characterization and catalytic testing of model catalysts

    SciTech Connect (OSTI)

    Mayr, Lukas; Kltzer, Bernhard; Penner, Simon; Rameshan, Raffael; Department of Inorganic Chemistry, Fritz Haber Institute of the Max Planck Society, Faradayweg 4-6, 14195 Berlin ; Rameshan, Christoph; Institute of Materials Chemistry, Vienna University of Technology, Getreidemarkt 9/BC/01, 1060 Vienna

    2014-05-15

    An ultra-high vacuum (UHV) setup for real and inverse model catalyst preparation, depth-resolved near-surface spectroscopic characterization, and quantification of catalytic activity and selectivity under technologically relevant conditions is described. Due to the all-quartz reactor attached directly to the UHV-chamber, transfer of the catalyst for in situ testing without intermediate contact to the ambient is possible. The design of the UHV-compatible re-circulating batch reactor setup allows the study of reaction kinetics under close to technically relevant catalytic conditions up to 1273 K without contact to metallic surfaces except those of the catalyst itself. With the attached differentially pumped exchangeable evaporators and the quartz-microbalance thickness monitoring equipment, a reproducible, versatile, and standardised sample preparation is possible. For three-dimensional near-surface sample characterization, the system is equipped with a hemispherical analyser for X-ray photoelectron spectroscopy (XPS), electron-beam or X-ray-excited Auger-electron spectroscopy, and low-energy ion scattering measurements. Due the dedicated geometry of the X-ray gun (54.7, magic angle) and the rotatable sample holder, depth analysis by angle-resolved XPS measurements can be performed. Thus, by the combination of characterisation methods with different information depths, a detailed three-dimensional picture of the electronic and geometric structure of the model catalyst can be obtained. To demonstrate the capability of the described system, comparative results for depth-resolved sample characterization and catalytic testing in methanol steam reforming on PdGa and PdZn near-surface intermetallic phases are shown.

  7. Corrective Action Investigation plan for Corrective Action Unit 546: Injection Well and Surface Releases, Nevada Test Site, Nevada, Revision 0

    SciTech Connect (OSTI)

    Alfred Wickline

    2008-03-01

    Corrective Action Unit (CAU) 546 is located in Areas 6 and 9 of the Nevada Test Site, which is approximately 65 miles northwest of Las Vegas, Nevada. Corrective Action Unit 546 is comprised of two Corrective Action Sites (CASs) listed below: •06-23-02, U-6a/Russet Testing Area •09-20-01, Injection Well These sites are being investigated because existing information on the nature and extent of potential contamination is insufficient to evaluate and recommend corrective action alternatives. Additional information will be obtained by conducting a corrective action investigation (CAI) before evaluating corrective action alternatives and selecting the appropriate corrective action for each CAS. The results of the field investigation will support a defensible evaluation of viable corrective action alternatives that will be presented in the Corrective Action Decision Document. The sites will be investigated based on the data quality objectives (DQOs) developed on November 8, 2007, by representatives of the Nevada Division of Environmental Protection and U.S. Department of Energy (DOE), National Nuclear Security Administration Nevada Site Office. The DQO process has been used to identify and define the type, amount, and quality of data needed to develop and evaluate appropriate corrective actions for CAU 546.

  8. Effects of extreme pressure additive chemistry on rolling element bearing surface durability

    SciTech Connect (OSTI)

    Evans, Ryan D.; Nixon, H. P.; Darragh, Craig V.; Howe, Jane Y; Coffey, Dorothy W

    2007-01-01

    Lubricant additives have been known to affect rolling element bearing surface durability for many years. Tapered roller bearings were used in fatigue testing of lubricants formulated with gear oil type additive systems. These systems have sulfur- and phosphoruscontaining compounds used for gear protection as well as bearing lubrication. Several variations of a commercially available base additive formulation were tested having modified sulfur components. The variations represent a range of ''active'' extreme pressure (EP) chemistries. The bearing fatigue test results were compared with respect to EP formulation and test conditions. Inner ring near-surface material in selected test bearings was evaluated on two scales: the micrometer scale using optical metallography and the nanometer scale using transmission electron microscopy (TEM). Focused-ion beam (FIB) techniques were used for TEM specimen preparation. Imaging and chemical analysis of the bearing samples revealed near-surface material and tribofilm characteristics. These results are discussed with respect to the relative fatigue lives.

  9. 2015 Accomplishments-Tritium aging studies on stainless steel. Effects of hydrogen isotopes, crack orientation, and specimen geometry on fracture toughness

    SciTech Connect (OSTI)

    Morgan, Michael J.

    2016-01-01

    This study reports on the effects of hydrogen isotopes, crack orientation, and specimen geometry on the fracture toughness of stainless steels. Fracture toughness variability was investigated for Type 21-6-9 stainless steel using the 7K0004 forging. Fracture toughness specimens were cut from the forging in two different geometric configurations: arc shape and disc shape. The fracture toughness properties were measured at ambient temperature before and after exposure to hydrogen gas and compared to prior studies. There are three main conclusions that can be drawn from the results. First, the fracture toughness properties of actual reservoir forgings and contemporary heats of steel are much higher than those measured in earlier studies that used heats of steel from the 1980s and 1990s and forward extruded forgings which were designed to simulate reservoir microstructures. This is true for as-forged heats as well as forged heats exposed to hydrogen gas. Secondly, the study confirms the well-known observation that cracks oriented parallel to the forging grain flow will propagate easier than those oriented perpendicular to the grain flow. However, what was not known, but is shown here, is that this effect is more pronounced, particularly after hydrogen exposures, when the forging is given a larger upset. In brick forgings, which have a relatively low amount of upset, the fracture toughness variation with specimen orientation is less than 5%; whereas, in cup forgings, the fracture toughness is about 20% lower than that forging to show how specimen geometry affects fracture toughness values. The American Society for Testing Materials (ASTM) specifies minimum specimen section sizes for valid fracture toughness values. However, sub-size specimens have long been used to study tritium effects because of the physical limitation of diffusing hydrogen isotopes into stainless steel at mild temperatures so as to not disturb the underlying forged microstructure. This study shows

  10. A new tribological test for candidate brush seal materials evaluation

    SciTech Connect (OSTI)

    Fellenstein, J.A.; DellaCorte, C.

    1994-10-01

    A new tribological test for candidate brush seal materials evaluation has been developed. The sliding contact between the brush seal wires and their mating counterface journal is simulated by testing a small tuft of wire against the outside diameter of a high speed rotating shaft. The test configuration is similar to a standard block on ring geometry. The new tester provides the capability to measure both the friction and wear of candidate wire and counterface materials under controlled loading conditions in the gram to kilogram range. A wide test condition latitude of speeds (1 to 27 m/s), temperatures (25 to 700C), and loads (0.5 to 10 N) enables the simulation of many of the important tribological parameters found in turbine engine brush seals. This paper describes the new test rig and specimen configuration and presents initial data for candidate seal materials comparing tuft test results and wear surface morphology to field tested seal components.

  11. Use of instrumented Charpy tests to determine onset of upper-shelf energy

    SciTech Connect (OSTI)

    Canonico, D.A.; Stelzman, W.J., Berggren, R.G.; Nanstad, R.K.

    1981-05-01

    Identifying the onset of C/sub v/ upper-shelf toughness is of paramount importance to the continued integrity of a pressure vessel. Most in-service surveillance programs require that the C/sub v/ upper-shelf toughness be determined. This is particularly true for the surveillance programs for nuclear pressure vessels. In the nuclear systems the change in C/sub v/ upper-shelf energy due to irradiation must frequently be determined with a limited number of surveillance specimens. Currently, fracture appearance is the criterion used to assure that the tests are being conducted in the C/sub v/ upper-shelf temperature range. This procedure is satisfactory when a number of specimens are available and accessible for interpretation. This is not always the case; irradiated specimens must be remotely tested and interpreted. Examining a specimen remotely may result in an erroneous interpretation of the fracture surface. To avoid this possibility we have developed a procedure, using an instrumented Charpy impact tester, that by linear extrapolation can identify the onset of the C/sub v/ upper-shelf toughness regime with as few as two specimens. This paper discusses the development of the procedure and its application.

  12. Corrective Action Investigation Plan for Corrective Action Unit 556: Dry Wells and Surface Release Points Nevada Test Site, Nevada (Draft), Revision 0

    SciTech Connect (OSTI)

    Grant Evenson

    2007-02-01

    Corrective Action Unit  (CAU) 556, Dry Wells and Surface Release Points, is located in Areas 6 and 25 of the Nevada Test Site, 65 miles northwest of Las Vegas, Nevada. Corrective Action Unit 556 is comprised of four corrective action sites (CASs) listed below: •06-20-04, National Cementers Dry Well •06-99-09, Birdwell Test Hole •25-60-03, E-MAD Stormwater Discharge and Piping •25-64-01, Vehicle Washdown and Drainage Pit These sites are being investigated because existing information on the nature and extent of potential contamination is insufficient to evaluate and recommend corrective action alternatives. Additional information will be obtained by conducting a corrective action investigation before evaluating corrective action alternatives and selecting the appropriate corrective action for each CAS. The results of the field investigation will support a defensible evaluation of viable corrective action alternatives that will be presented in the Corrective Action Decision Document.

  13. Critical heat flux test apparatus

    DOE Patents [OSTI]

    Welsh, Robert E.; Doman, Marvin J.; Wilson, Edward C.

    1992-01-01

    An apparatus for testing, in situ, highly irradiated specimens at high temperature transients is provided. A specimen, which has a thermocouple device attached thereto, is manipulated into test position in a sealed quartz heating tube by a robot. An induction coil around a heating portion of the tube is powered by a radio frequency generator to heat the specimen. Sensors are connected to monitor the temperatures of the specimen and the induction coil. A quench chamber is located below the heating portion to permit rapid cooling of the specimen which is moved into this quench chamber once it is heated to a critical temperature. A vacuum pump is connected to the apparatus to collect any released fission gases which are analyzed at a remote location.

  14. Specimen coordinate automated measuring machine/fiducial automated measuring machine

    DOE Patents [OSTI]

    Hedglen, Robert E.; Jacket, Howard S.; Schwartz, Allan I.

    1991-01-01

    The Specimen coordinate Automated Measuring Machine (SCAMM) and the Fiducial Automated Measuring Machine (FAMM) is a computer controlled metrology system capable of measuring length, width, and thickness, and of locating fiducial marks. SCAMM and FAMM have many similarities in their designs, and they can be converted from one to the other without taking them out of the hot cell. Both have means for: supporting a plurality of samples and a standard; controlling the movement of the samples in the +/- X and Y directions; determining the coordinates of the sample; compensating for temperature effects; and verifying the accuracy of the measurements and repeating as necessary. SCAMM and FAMM are designed to be used in hot cells.

  15. Specimen Machining for the Study of the Effect of Swelling on CGR in PWR Environment.

    SciTech Connect (OSTI)

    Teysseyre, Sebastien Paul

    2015-06-01

    This report describes the preparation of ten specimens to be used for the study of the effect of swelling on the propagation of irradiation assisted stress corrosion cracking cracks. Four compact tension specimens, four microscopy plates and two tensile specimens were machined from a AISI 304 material that was irradiated up to 33 dpa. The specimens had been machined such as to represent the behavior of materials with 3.7%swelling and <2% swelling.

  16. Synthesis, Development, and Testing of High-Surface-Area Polymer-Based Adsorbents for the Selective Recovery of Uranium from Seawater

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Oyola, Yatsandra; Janke, Christopher J.; Dai, Sheng

    2016-02-29

    The ocean contains uranium with an approximate concentration of 3.34 ppb, which can serve as an incredible supply source to sustain nuclear energy in the United States. Unfortunately, technology currently available to recover uranium from seawater is not efficient enough and mining uranium on land is still more economical. For this study, we have developed polymer-based adsorbents with high uranium adsorption capacities by grafting amidoxime onto high-surface-area polyethylene (PE) fibers. Various process conditions have been screened, in combination with developing a rapid testing protocol (<24 h), to optimize the process. These adsorbents are synthesized through radiation-induced grafting of acrylonitrile (AN)more » and methacrylic acid (MAA) onto PE fibers, followed by the conversion of nitriles to amidoximes and basic conditioning. In addition, the uranium adsorption capacity, measured in units of gU/kgads, is greatly increased by reducing the diameter of the PE fiber or changing its morphology. An increase in the surface area of the PE polymer fiber allows for more grafting sites that are positioned in more-accessible locations, thereby increasing access to grafted molecules that would normally be located in the interior of a fiber with a larger diameter. Polymer fibers with hollow morphologies are able to adsorb beyond 1 order of magnitude more uranium from simulated seawater than current commercially available adsorbents. Finally, several high-surface-area fibers were tested in natural seawater and were able to extract 5–7 times more uranium than any adsorbent reported to date.« less

  17. Sorption testing and generalized composite surface complexation models for determining uranium sorption parameters at a proposed in-situ recovery site

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Johnson, Raymond H.; Truax, Ryan A.; Lankford, David A.; Stone, James J.

    2016-02-03

    Solid-phase iron concentrations and generalized composite surface complexation models were used to evaluate procedures in determining uranium sorption on oxidized aquifer material at a proposed U in situ recovery (ISR) site. At the proposed Dewey Burdock ISR site in South Dakota, USA, oxidized aquifer material occurs downgradient of the U ore zones. Solid-phase Fe concentrations did not explain our batch sorption test results,though total extracted Fe appeared to be positively correlated with overall measured U sorption. Batch sorption test results were used to develop generalized composite surface complexation models that incorporated the full genericsorption potential of each sample, without detailedmore » mineralogiccharacterization. The resultant models provide U sorption parameters (site densities and equilibrium constants) for reactive transport modeling. The generalized composite surface complexation sorption models were calibrated to batch sorption data from three oxidized core samples using inverse modeling, and gave larger sorption parameters than just U sorption on the measured solidphase Fe. These larger sorption parameters can significantly influence reactive transport modeling, potentially increasing U attenuation. Because of the limited number of calibration points, inverse modeling required the reduction of estimated parameters by fixing two parameters. The best-fit models used fixed values for equilibrium constants, with the sorption site densities being estimated by the inversion process. While these inverse routines did provide best-fit sorption parameters, local minima and correlated parameters might require further evaluation. Despite our limited number of proxy samples, the procedures presented provide a valuable methodology to consider for sites where metal sorption parameters are required. Furthermore, these sorption parameters can be used in reactive transport modeling to assess downgradient metal attenuation, especially when no other

  18. Apparatus for testing for infection by a retrovirus

    DOE Patents [OSTI]

    Layne, Scott P.; Beugelsdijk, Tony J.

    1999-01-01

    An apparatus for testing specimens for infection by a retrovirus is described. The apparatus comprises a process controller including a communications module for translating user commands into test instrument suite commands and a means for communicating specimen test results to a user. The apparatus further comprises a test instrument suite including a means for treating the specimen to manifest an observable result and a detector for measuring the observable result.

  19. J-integral for a semi-elliptical surface crack at a bimaterial interface

    SciTech Connect (OSTI)

    Sharobeam, M.H.; Landes, J.D.

    1995-12-31

    Surface cracks are common defects in welded, bonded, and composite structures. The elastic-plastic fracture of these defects may be analyzed using the J-integral. The authors have recently developed a new approach to evaluate the J-integral for semi-elliptical surface cracks in panels made of homogeneous materials and subject to remote tension. This approach, which is based on load separation, allows the evaluation of J for such a three-dimensional geometry using a single specimen test record. It is analogous to the single specimen technique in two-dimensional geometries. In this article, the authors extend their study to surface cracks at bimaterial interfaces. A three-dimensional finite element model is developed to model such a crack. The J-integral is evaluated along the crack front using the virtual crack extension method. The elastic-plastic fracture behavior of the crack is studied. Load separation is also examined and the new single specimen approach for surface cracks in single material panels is extended to those at bimaterial interfaces. The study also includes a comparison between the results of surface cracks in single material panels and those at bimaterial interfaces.

  20. Mixed Stream Test Rig Winter FY-2011 Report

    SciTech Connect (OSTI)

    Chalres Park; Tedd Lister; Kevin DeWall

    2011-04-01

    This report describes the data and analysis of the initial testing campaign of the Mixed Stream Test Rig (MISTER) at Idaho National Laboratory (INL). It describes the test specimen selection, physical configuration of the test equipment, operations methodology, and data and analysis of specimens exposed in two environments designed to represent those expected for high temperature steam electrolysis (HTSE).

  1. Apparatus for X-ray diffraction microscopy and tomography of cryo specimens

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Beetz, T.; Howells, M. R.; Jacobsen, C.; Kao, C. -C.; Kirz, J.; Lima, E.; Mentes, T. O.; Miao, H.; Sanchez-Hanke, C.; Sayre, D.; et al

    2005-03-14

    An apparatus for diffraction microscopy of biological and materials science specimens is described. In this system, a coherent soft X-ray beam is selected with a pinhole, and the illuminated specimen is followed by an adjustable beamstop and CCD camera to record diffraction data from non-crystalline specimens. In addition, a Fresnel zone plate can be inserted to allow for direct imaging. The system makes use of a cryogenic specimen holder with cryotransfer capabilities to allow frozen hydrated specimens to be loaded. The specimen can be tilted over a range of ± 80 ° degrees for three-dimensional imaging; this is done bymore » computer-controlled motors, enabling automated alignment of the specimen through a tilt series. The system is now in use for experiments in soft X-ray diffraction microscopy.« less

  2. Post-Closure Inspection and Monitoring Report for Corrective Action Unit 417: Central Nevada Test Area Surface, Hot Creek Valley, Nevada

    SciTech Connect (OSTI)

    2009-10-01

    This report presents results of data collected during the annual post-closure site inspection conducted at the Central Nevada Test Area, surface Corrective Action Unit (CAU) 417 in June 2009. The annual post-closure site inspection included inspections of the UC-1, UC-3, and UC-4 sites in accordance with the Post-Closure Monitoring Plan provided in the CAU 417 Closure Report (NNSA/NV 2001). The annual inspection conducted at the UC-1 Central Mud Pit (CMP) indicated that the site and soil cover were in good condition. Three new fractures were identified in the soil cover and were filled with bentonite chips during the inspection. The vegetation on the soil cover was adequate but showed signs of the area's ongoing drought. No issues were identified with the CMP fence, gate, or subsidence monuments. No issues were identified with the warning signs and monuments at the other two UC-1 locations

  3. Optical caliper with compensation for specimen deflection and method

    DOE Patents [OSTI]

    Bernacki, Bruce E.

    1997-01-01

    An optical non-contact profilometry system and method provided by an optical caliper with matched optical sensors that are arranged conjugate to each other so that the surface profile and thickness of an article can be measured without using a fixed reference surface and while permitting the article to deflect in space within the acquisition range of the optical sensors. The output signals from the two optical sensors are algebraically added to compensate for any such deflection of the article and provide a so compensated signal, the balance and sign of which provides a measurement of the actual thickness of the article at the optical sensors.

  4. Optical caliper with compensation for specimen deflection and method

    DOE Patents [OSTI]

    Bernacki, B.E.

    1997-12-09

    An optical non-contact profilometry system and method provided by an optical caliper with matched optical sensors that are arranged conjugate to each other so that the surface profile and thickness of an article can be measured without using a fixed reference surface and while permitting the article to deflect in space within the acquisition range of the optical sensors. The output signals from the two optical sensors are algebraically added to compensate for any such deflection of the article and provide a so compensated signal, the balance and sign of which provides a measurement of the actual thickness of the article at the optical sensors. 2 figs.

  5. Development of Advanced Surface Enhancement Technology for Decreasing Wear and Corrosion of Equipment Used for Mineral Processing

    SciTech Connect (OSTI)

    Daniel Tao; R. Honaker; B. K. Parekh

    2007-09-20

    Equipment wear is a major concern in the mineral processing industry, which dramatically increases the maintenance cost and adversely affects plant operation efficiency. In this research, novel surface treatment technologies, High Density Infrared (HDI) and Laser Surface Engineering (LSE) surface coating processes were developed for the surface enhancement of selected mineral and coal processing equipment. Microstructural and mechanical properties of the coated specimens were characterized. Laboratory-simulated wear tests were conducted to evaluate the tribological performance of the coated components. Test results indicate that the wear resistance of ASTM A36 (raw coal screen section) and can be significantly increased by applying HDI and LSE coating processes. Field testing has been performed using a LSE-treated screen panel and it showed a significant improvement of the service life.

  6. Coaxial test fixture

    DOE Patents [OSTI]

    Praeg, Walter F.

    1986-01-01

    An assembly is provided for testing one or more contact material samples in a vacuum environment. The samples are positioned as an inner conductive cylinder assembly which is mounted for reciprocal vertical motion as well as deflection from a vertical axis. An outer conductive cylinder is coaxially positioned around the inner cylinder and test specimen to provide a vacuum enclosure therefor. A power source needed to drive test currents through the test specimens is connected to the bottom of each conductive cylinder, through two specially formed conductive plates. The plates are similar in form, having a plurality of equal resistance current paths connecting the power source to a central connecting ring. The connecting rings are secured to the bottom of the inner conductive assembly and the outer cylinder, respectively. A hydraulic actuator is also connected to the bottom of the inner conductor assembly to adjust the pressure applied to the test specimens during testing. The test assembly controls magnetic forces such that the current distribution through the test samples is symmetrical and that contact pressure is not reduced or otherwise disturbed.

  7. Analysis of structure and deformation behavior of AISI 316L tensile specimens from the second operational target module at the Spallation Neutron Source

    SciTech Connect (OSTI)

    Gussev, Maxim N.; McClintock, David A.; Garner, Frank

    2015-08-05

    In an earlier publication, tensile testing was performed on specimens removed from the first two operational targets of the Spallation Neutron Source (SNS). There were several anomalous features in the results. First, some specimens had very large elongations (up to 57%) while others had significantly smaller values. Second, there was a larger than the usual amount of data scatter in the elongation results. Third, the stress-strain diagrams of nominally similar specimens spanned a wide range of behavior ranging from expected irradiation-induced hardening to varying levels of force drop after yield point and indirect signs of "traveling deformation wave" behavior associated with strain-induced martensite formation. To investigate the cause(s) of such variable tensile behavior, several specimens from Target 2, spanning the range of observed tensile behavior, were chosen for detailed microstructural examination using electron backscattering analysis (EBSD). It was also shown that the steel employed in the construction of the target contained an unexpected bimodal grain size distribution, containing very large out-of-specification grains surrounded by necklaces of grains of within-specification sizes. The large grains were frequently comparable to the width of the gauge section of the tensile specimen. Moreover, the propensity to form martensite during deformation was shown to be accelerated by radiation but also to be very sensitive to the relative orientation of the grains with respect to the tensile axis. Specimens having large grains in the gauge that were most favorably oriented for production of martensite strongly exhibited the traveling deformation wave phenomenon, while those specimens with less favorably oriented grains had lesser or no degree of the wave effect, thereby accounting for the larger than expected data scatter.

  8. Analysis of structure and deformation behavior of AISI 316L tensile specimens from the second operational target module at the Spallation Neutron Source

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Gussev, Maxim N.; McClintock, David A.; Garner, Frank

    2015-08-05

    In an earlier publication, tensile testing was performed on specimens removed from the first two operational targets of the Spallation Neutron Source (SNS). There were several anomalous features in the results. First, some specimens had very large elongations (up to 57%) while others had significantly smaller values. Second, there was a larger than the usual amount of data scatter in the elongation results. Third, the stress-strain diagrams of nominally similar specimens spanned a wide range of behavior ranging from expected irradiation-induced hardening to varying levels of force drop after yield point and indirect signs of "traveling deformation wave" behavior associatedmore » with strain-induced martensite formation. To investigate the cause(s) of such variable tensile behavior, several specimens from Target 2, spanning the range of observed tensile behavior, were chosen for detailed microstructural examination using electron backscattering analysis (EBSD). It was also shown that the steel employed in the construction of the target contained an unexpected bimodal grain size distribution, containing very large out-of-specification grains surrounded by necklaces of grains of within-specification sizes. The large grains were frequently comparable to the width of the gauge section of the tensile specimen. Moreover, the propensity to form martensite during deformation was shown to be accelerated by radiation but also to be very sensitive to the relative orientation of the grains with respect to the tensile axis. Specimens having large grains in the gauge that were most favorably oriented for production of martensite strongly exhibited the traveling deformation wave phenomenon, while those specimens with less favorably oriented grains had lesser or no degree of the wave effect, thereby accounting for the larger than expected data scatter.« less

  9. Design, Construction, and Initial Test of High Spatial Resolution Thermometry Arrays for Detection of Surface Temperature Profiles on SRF Cavities in Super Fluid Helium

    SciTech Connect (OSTI)

    Ari Palczewski, Rongli Geng, Grigory Eremeev

    2011-07-01

    We designed and built two high resolution (0.6-0.55mm special resolution [1.1-1.2mm separation]) thermometry arrays prototypes out of the Allen Bradley 90-120 ohm 1/8 watt resistor to measure surface temperature profiles on SRF cavities. One array was designed to be physically flexible and conform to any location on a SRF cavity; the other was modeled after the common G-10/stycast 2850 thermometer and designed to fit on the equator of an ILC (Tesla 1.3GHz) SRF cavity. We will discuss the advantages and disadvantages of each array and their construction. In addition we will present a case study of the arrays performance on a real SRF cavity TB9NR001. TB9NR001 presented a unique opportunity to test the performance of each array as it contained a dual (4mm separation) cat eye defect which conventional methods such as OST (Oscillating Superleak second-sound Transducers) and full coverage thermometry mapping were unable to distinguish between. We will discuss the new arrays ability to distinguish between the two defects and their preheating performance.

  10. Post-Closure Inspection and Monitoring Report for Corrective Action Unit 417: Central Nevada Test Area Surface, Hot Creek Valley, Nevada

    SciTech Connect (OSTI)

    2009-01-01

    This report presents data collected during the annual post-closure site inspection conducted at the Central Nevada Test Area Surface Corrective Action Unit (CAU) 417 in May of 2008. The annual post-closure site inspection included inspections of the UC-1, UC-3, and UC-4 sites in accordance with the Post-Closure Monitoring Plan provided in the CAU 417 Closure Report (NNSA/NV 2001). The annual inspection conducted at the UC-1 Central Mud Pit (CMP) indicated that the site and soil cover were in good condition. Three new cracks or fractures were observed in the soil cover during the annual inspection and were immediately filled with bentonite chips. The vegetation on the soil cover was adequate, but showed signs of the area's ongoing drought. No issues were identified with the CMP fence, gate, or subsidence monuments. No issues were identified with the warning signs and monuments at the other two UC-1 locations. The annual subsidence survey was conducted at UC-1 CMP and UC-4 Mud Pit C in August 2008. The results of the subsidence surveys indicate that the covers are performing as expected, and no unusual subsidence was observed.

  11. Post-Closure Inspection and Monitoring Report for Corrective Action Unit 417: Central Nevada Test Area Surface, Hot Creek Valley, Nevada

    SciTech Connect (OSTI)

    2013-03-01

    This report presents results of data collected during the annual post-closure site inspections conducted at the Central Nevada Test Area surface Corrective Action Unit (CAU) 417 in May 2011 and July 2012. The annual post-closure site inspections included inspections of the UC-1, UC-3, and UC-4 sites in accordance with the Post-Closure Monitoring Plan provided in the CAU 417 Closure Report (NNSA/NV 2001). The annual inspections conducted at the UC-1 Central Mud Pit (CMP) indicated that the site and soil cover were in good condition. No new fractures or extension of existing fractures were observed and no issues with the fence or gate were identified. The vegetation on the cover continues to look healthy, but the biennial vegetation survey conducted during the 2012 inspection indicated that the total foliar cover was slightly higher in 2009 than in 2012. This may be indicative of a decrease in precipitation observed during the 2-year monitoring period. The precipitation totaled 9.9 inches from July 1, 2010, through June 30, 2011, and 5 inches from July 1, 2011, through June 30, 2012. This decrease in precipitation is also evident in the soil moisture data obtained from the time domain reflectometry sensors. Soil moisture content data show that the UC-1 cover is performing as designed, and evapotranspiration is effectively removing water from the cover.

  12. A versatile elevated-pressure reactor combined with an ultrahigh vacuum surface setup for efficient testing of model and powder catalysts under clean gas-phase conditions

    SciTech Connect (OSTI)

    Morfin, Franck; Piccolo, Laurent

    2013-09-15

    A small-volume reaction cell for catalytic or photocatalytic testing of solid materials at pressures up to 1000 Torr has been coupled to a surface-science setup used for standard sample preparation and characterization under ultrahigh vacuum (UHV). The reactor and sample holder designs allow easy sample transfer from/to the UHV chamber, and investigation of both planar and small amounts of powder catalysts under the same conditions. The sample is heated with an infrared laser beam and its temperature is measured with a compact pyrometer. Combined in a regulation loop, this system ensures fast and accurate temperature control as well as clean heating. The reaction products are automatically sampled and analyzed by mass spectrometry and/or gas chromatography (GC). Unlike previous systems, our GC apparatus does not use a recirculation loop and allows working in clean conditions at pressures as low as 1 Torr while detecting partial pressures smaller than 10{sup ?4} Torr. The efficiency and versatility of the reactor are demonstrated in the study of two catalytic systems: butadiene hydrogenation on Pd(100) and CO oxidation over an AuRh/TiO{sub 2} powder catalyst.

  13. Corrective Action Decision Document/ Closure Report for Corrective Action Unit 556: Dry Wells and Surface Release Points, Nevada Test Site, Nevada with Errata Sheet, Revision 0

    SciTech Connect (OSTI)

    Grant Evenson

    2008-09-01

    This Corrective Action Decision Document (CADD)/Closure Report (CR) has been prepared for Corrective Action Unit 556, Dry Wells and Surface Release Points, located at the Nevada Test Site, Nevada, in accordance with the Federal Facility Agreement and Consent Order (FFACO, 1996; as amended February 2008). Corrective Action Unit (CAU) 556 is comprised of four corrective action sites (CASs): • 06-20-04, National Cementers Dry Well • 06-99-09, Birdwell Test Hole • 25-60-03, E-MAD Stormwater Discharge and Piping • 25-64-01, Vehicle Washdown and Drainage Pit The purpose of this CADD/CR is to provide justification and documentation supporting the recommendation for closure of CAU 556 with no further corrective action. To achieve this, corrective action investigation (CAI) activities began on February 7 and were completed on June 19, 2008, as set forth in the Corrective Action Investigation Plan for Corrective Action Unit 556: Dry Wells and Surface Release Points, Nevada Test Site, Nevada (NNSA/NSO, 2007). The purpose of the CAI was to fulfill the following data needs as defined during the data quality objective (DQO) process: • Determine whether contaminants of concern (COCs) are present. • If COCs are present, determine their nature and extent. • Provide sufficient information and data to complete appropriate corrective actions. The CAU 556 data were evaluated based on the data quality assessment process, which demonstrated the quality and acceptability of the data for use in fulfilling the DQO data needs. Analytes detected during the CAI were evaluated against appropriate final action levels (FALs) to identify the COCs for each CAS. The results of the CAI identified COCs at one of the four CASs in CAU 556 that required the completion of a corrective action. Assessment of the data generated from investigation activities conducted at CAU 556 revealed the following: • Corrective Action Sites 06-20-04, 06-99-09, and 25-64-01 do not contain contamination at

  14. Development testing of the chemical analysis automation polychlorinated biphenyl standard analysis method during surface soils sampling at the David Witherspoon 1630 site

    SciTech Connect (OSTI)

    Hunt, M.A.; Klatt, L.N.; Thompson, D.H.

    1998-02-01

    The Chemical Analysis Automation (CAA) project is developing standardized, software-driven, site-deployable robotic laboratory systems with the objective of lowering the per-sample analysis cost, decreasing sample turnaround time, and minimizing human exposure to hazardous and radioactive materials associated with DOE remediation projects. The first integrated system developed by the CAA project is designed to determine polychlorinated biphenyls (PCB) content in soil matrices. A demonstration and development testing of this system was conducted in conjuction with surface soil characterization activities at the David Witherspoon 1630 Site in Knoxville, Tennessee. The PCB system consists of five hardware standard laboratory modules (SLMs), one software SLM, the task sequence controller (TSC), and the human-computer interface (HCI). Four of the hardware SLMs included a four-channel Soxhlet extractor, a high-volume concentrator, a column cleanup, and a gas chromatograph. These SLMs performed the sample preparation and measurement steps within the total analysis protocol. The fifth hardware module was a robot that transports samples between the SLMs and the required consumable supplies to the SLMs. The software SLM is an automated data interpretation module that receives raw data from the gas chromatograph SLM and analyzes the data to yield the analyte information. The TSC is a software system that provides the scheduling, management of system resources, and the coordination of all SLM activities. The HCI is a graphical user interface that presents the automated laboratory to the analyst in terms of the analytical procedures and methods. Human control of the automated laboratory is accomplished via the HCI. Sample information required for processing by the automated laboratory is entered through the HCI. Information related to the sample and the system status is presented to the analyst via graphical icons.

  15. Midtemperature Solar Systems Test Facility predictions for thermal performance of the Suntec solar collector with heat-formed glass reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1980-11-01

    Thermal performance predictions are presented for the Suntec solar collector, with heat-formed glass reflector surface, for three output temperatures at five cities in the United States.

  16. Sensitivity Test Analysis

    Energy Science and Technology Software Center (OSTI)

    1992-02-20

    SENSIT,MUSIG,COMSEN is a set of three related programs for sensitivity test analysis. SENSIT conducts sensitivity tests. These tests are also known as threshold tests, LD50 tests, gap tests, drop weight tests, etc. SENSIT interactively instructs the experimenter on the proper level at which to stress the next specimen, based on the results of previous responses. MUSIG analyzes the results of a sensitivity test to determine the mean and standard deviation of the underlying population bymore » computing maximum likelihood estimates of these parameters. MUSIG also computes likelihood ratio joint confidence regions and individual confidence intervals. COMSEN compares the results of two sensitivity tests to see if the underlying populations are significantly different. COMSEN provides an unbiased method of distinguishing between statistical variation of the estimates of the parameters of the population and true population difference.« less

  17. Cyclic crack resistance of an anticorrosion surfacing steel joint

    SciTech Connect (OSTI)

    Zuezdin, Y.I.; Andrusiv, B.N.; Nikiforchin, G.N.; Timofeev, B.T.; Zima, Y.V.

    1986-03-01

    An investigation was made of the cyclic crack resistance of the austenitic surfacing - 15Kh2MFA steel transition zone taking into consideration the fatigue crack geometry, the fracture mechanism, and the effect of crack closure. Microstructural analysis showed significant heterogeneity of the surfacing-base metal transition zone. An analysis of the base metal showed that in the area of low-fatigue crack growth rates, there is a significant spread in the experimental data obtained in tests of three specimens. Under steady service conditions, an increased loading asymmetry sharply accelerates failure of the alloy as the result of growth only of the subsurfacing crack, which is partically insensitive to the direction of crack development and to structural changes in the transition zone materials.

  18. Post-Closure Inspection and Monitoring Report for Corrective Action Unit 417: Central Nevada Test Area Surface, Hot Creek Valley, Nevada, for Calendar Year 2007

    SciTech Connect (OSTI)

    2008-09-01

    This report presents data collected during the annual post-closure site inspection conducted at the Central Nevada Test Area Surface Corrective Action Unit (CAU) 417 in May 2007. The annual post-closure site inspection included inspections of the UC-1, UC-3, and UC-4 sites in accordance with the Post-Closure Monitoring Plan provided in the CAU 417 Closure Report (NNSA/NV 2001). The annual inspection conducted at the UC-1 Central Mud Pit (CMP) indicated the site and soil cover were in good condition. No new cracks or fractures were observed in the soil cover during the annual inspection. A crack on the west portion of the cover was observed during the last quarterly inspection in December 2006. This crack was filled with bentonite as part of the maintenance activities conducted in February 2007 and will be monitored during subsequent annual inspections. The vegetation on the soil cover was adequate but showing signs of the area's ongoing drought. No issues were identified with the CMP fence, gate, or subsidence monuments. New DOE Office of Legacy Management signs with updated emergency phone numbers were installed as part of this annual inspection, no issues were identified with the warning signs and monuments at the other two UC-1 locations. The annual subsidence survey was conducted at UC-1 CMP and UC-4 Mud Pit C as part of the maintenance activities conducted in February 2007. The results of the subsidence surveys indicate that the covers are performing as expected, and no unusual subsidence was observed. A vegetation survey of the UC-1 CMP cover and adjacent areas was conducted as part of the annual inspection in May 2007. The vegetation survey indicated that revegetation continues to be successful, although stressed due to the area's prevailing drought conditions. The vegetation should continue to be monitored to document any changes in the plant community and to identify conditions that could potentially require remedial action to maintain a viable vegetation

  19. Face compression yield strength of the copper-Inconel composite specimen

    SciTech Connect (OSTI)

    Horie, T.

    1987-05-01

    A new equation for the face compression yield strength of copper-Inconel composite material has been derived. Elastic-plastic finite element analyses were also made for composite specimens with various aspect ratios to examine the edge effect of the specimen. According to the results of both the new equation and the analyses, the face compression yield strength of the composite should be decreased by about 25% from the value obtained with Becker's equation.

  20. Status of lithium-filled specimen subcapsules for the HFIR-MFE-RB10J experiment

    SciTech Connect (OSTI)

    Robertson, J.P.; Howell, M.; Lenox, K.E.

    1998-09-01

    The HFIR-MFE-RB-10J experiment will be irradiated in a Removable Beryllium position in the HFIR for 10 reactor cycles, accumulating approximately 5 dpa in steel. The upper region of the capsule contains two lithium-filled subcapsules containing vanadium specimens. This report describes the techniques developed to achieve a satisfactory lithium fill with a specimen occupancy of 26% in each subcapsule.

  1. Midtemperature Solar Systems Test Facility predictions for thermal performance of the Solar Kinetics T-700 solar collector with FEK 244 reflector surface

    SciTech Connect (OSTI)

    Harrison, T.D.

    1980-11-01

    Thermal performance predictions are presented for the Solar Kinetics T-700 solar collector, with FEK 244 reflector surface, for three output temperatures at five cities in the United States.

  2. Charpy impact test results on five materials and NIST verification...

    Office of Scientific and Technical Information (OSTI)

    test results on five materials and NIST verification specimens using instrumented 2-mm and 8-mm strikers Citation Details In-Document Search Title: Charpy impact test results on ...

  3. Non-destructive testing method and apparatus

    DOE Patents [OSTI]

    Akers, Douglas W.

    2011-10-04

    Non-destructive testing apparatus may comprise a photon source and a source material that emits positrons in response to bombardment of the source material with photons. The source material is positionable adjacent the photon source and a specimen so that when the source material is positioned adjacent the photon source it is exposed to photons produced thereby. When the source material is positioned adjacent the specimen, the specimen is exposed to at least some of the positrons emitted by the source material. A detector system positioned adjacent the specimen detects annihilation gamma rays emitted by the specimen. Another embodiment comprises a neutron source and a source material that emits positrons in response to neutron bombardment.

  4. Computer program for predicting surface subsidence resulting from pressure depletion in geopressured wells: subsidence prediction for the DOW test well No. 1, Parcperdue, Louisiana

    SciTech Connect (OSTI)

    Janssen, J.C.; Carver, D.R.; Bebout, D.G.; Bachman, A.L.

    1981-01-01

    The nucleus-of-strain concept is used to construct a computer program for predicting surface subsidence due to pressure reduction in geopressured reservoirs. Numerical integration allows one to compute the vertical displacement of the ground surface directly above and beyond the aquifer boundaries which results from the pressure reduction in each of the small finite volumes into which the aquifer is partitioned. The program treats depth (measured from the surface to the mean thickness of the aquifer) as a constant. Variation in aquifer thickness is accounted for by linear interpolation from one boundary to its opposite. In this simple model, subsidence is proportional to the pressure reduction (considered constant in this presentation) and to but one physical parameter, Cm(1-..nu..), in which Cm is its coefficient of uniaxial compaction, and ..nu.. is Poisson's ratio.

  5. Results of charpy V-notch impact testing of structural steel...

    Office of Scientific and Technical Information (OSTI)

    MATERIALS SCIENCE; FERRITIC STEELS; PHYSICAL RADIATION EFFECTS; TENSILE PROPERTIES; IRRADIATION; CHARPY TEST A capsule containing Charpy V-notch (CVN) and mini-tensile specimens...

  6. A comparison of several surface finish measurement methods as applied to ground ceramic and metal surfaces

    SciTech Connect (OSTI)

    Blau, P.J.; Martin, R.L.; Riester, L.

    1996-01-01

    Surface finish is one of the most common measures of surface quality of ground ceramics and metal parts and a wide variety of methods and parameters have been developed to measure it. The purpose of this investigation was to compare the surface roughness parameters obtained on the same two specimens from three different types of measuring instruments: a traditional mechanical stylus system, a non-contact laser scanning system, and the atomic force microscope (two different AFM systems were compared). The same surface-ground silicon nitride and Inconel 625 alloy specimens were used for all measurements in this investigation. Significant differences in arithmetic average roughness, root-mean-square roughness, and peak-to-valley roughness were obtained when comparing data from the various topography measuring instruments. Non-contact methods agreed better with the others on the metal specimen than on the ceramic specimen. Reasons for these differences include the effective dimensions and geometry of the probe with respect to the surface topography; the reflectivity of the surface, and the type of filtering scheme Results of this investigation emphasize the importance of rigorously specifying the manner of surface roughness measurement when either reporting roughness data or when requesting that roughness data be provided.

  7. POST CLOSURE INSPECTION AND MONITORING REPORT FOR CORRECTIVE ACTION UNIT 417: CENTRAL NEVADA TEST AREA - SURFACE, HOT CREEK VALLEY, NEVADA; FOR CALENDAR YEAR 2005

    SciTech Connect (OSTI)

    2006-04-01

    Corrective Action Unit (CAU) 417, Central Nevada Test Area - Surface, is located in Hot Creek Valley in northern Nye County, Nevada, and consists of three areas commonly referred to as UC-1, UC-3, and UC-4. CAU 417 consists of 34 Corrective Action Sites (CASs) which were closed in 2000 (U. S. Department of Energy, National Nuclear Security Administration Nevada Operations Office, 2001). Three CASs at UC-1 were closed in place with administrative controls. At CAS 58-09-01, Central Mud Pit (CMP), a vegetated soil cover was constructed over the mud pit. At the remaining two sites CAS 58-09-02, Mud Pit and 58-09-05, Mud Pits (3), aboveground monuments and warning signs were installed to mark the CAS boundaries. Three CASs at UC-3 were closed in place with administrative controls. Aboveground monuments and warning signs were installed to mark the site boundaries at CAS 58-09-06, Mud Pits (5), CAS 58-25-01, Spill and CAS 58-10-01, Shaker Pad Area. Two CASs that consist of five sites at UC-4 were closed in place with administrative controls. At CAS 58-09-03, Mud Pits 9, an engineered soil cover was constructed over Mud Pit C. At the remaining three sites in CAS 58-09-03 and at CAS 58-10-05, Shaker Pad Area, aboveground monuments and warning signs were installed to mark the site boundaries. The remaining 26 CASs at CAU 417 were either clean-closed or closed by taking no further action. Quarterly post-closure inspections are performed at the CASs that were closed in place at UC-I, UC-3, and UC-4. During calendar year 2005, site inspections were performed on March 15, June 16, September 22, and December 7. The inspections conducted at the UC-1 CMP documented that the site was in good condition and continued to show integrity of the cover unit. No new cracks or fractures were observed until the December inspection. A crack on the west portion of the cover showed evidence of lateral expansion; however, it is not at an actionable level. The crack will be sealed by filling with

  8. Analysis of stress intensity factors for a new mechanical-corrosion specimen

    SciTech Connect (OSTI)

    Rassineux, B.; Crouzet, D.; Le Hong, S.

    1996-12-01

    Electricite de France is conducting a research program to determine stress corrosion cracking rates (CSC) in the Alloy 600 steam generators tubes of the PWR primary system. The objective is to correlate the cracking rates with the specimen stress intensity factor K{sub I}. One of the samples selected for the purpose of this study is the longitudinal notched specimen (TEL). This paper presents the analysis of the stress intensity factor and its experimental validation. The stress intensity factor has been evaluated for different loads using 3D finite element calculations with the Hellen-Parks and G(q) methods. Only crack propagation are considered. As an assessment of the method, the numerical simulations are in good agreement with the fatigue crack growth rates measured experimentally for TEL and compact tension (CT) specimens.

  9. Process for measuring low cadmium levels in blood and other biological specimens

    DOE Patents [OSTI]

    Peterson, David P. (Orland Park, IL); Huff, Edmund A. (Lemont, IL); Bhattacharyya, Maryka H. (Naperville, IL)

    1994-01-01

    A process for measuring low levels of cadmium in blood and other biological specimens is provided without interference from high levels of alkali metal contaminants by forming an aqueous solution and without contamination by environmental cadmium absent the proteins from the specimen, selectively removing cadmium from the aqueous solution on an anion exchange resin, thereby removing the alkali metal contaminants, resolubilizing cadmium from the resin to form a second solution and analyzing the second solution for cadmium, the process being carried out in a cadmium-free environment.

  10. Process for measuring low cadmium levels in blood and other biological specimens

    DOE Patents [OSTI]

    Peterson, David P.; Huff, Edmund A.; Bhattacharyya, Maryka H.

    1994-05-03

    A process for measuring low levels of cadmium in blood and other biological specimens is provided without interference from high levels of alkali metal contaminants by forming an aqueous solution and without contamination by environmental cadmium absent the proteins from the specimen, selectively removing cadmium from the aqueous solution on an anion exchange resin, thereby removing the alkali metal contaminants, resolubilizing cadmium from the resin to form a second solution and analyzing the second solution for cadmium, the process being carried out in a cadmium-free environment.

  11. Operation Greenhouse. Scientific Director's report of atomic-weapon tests at Eniwetok, 1951. Annex 4. 2. Measurement of surface-air movements associated with atomic blasts

    SciTech Connect (OSTI)

    Rados, R.M.; Bogert, J.C.; Haig, T.O.

    1985-09-01

    The purpose of this project was to record continuous measurements of the surface winds in the vicinity of an atomic blast immediately prior to the blast, during passage of the shock wave, and immediately after the blast with special regard to the blast-induced afterwind following local dissipation of the shock wave. From the data obtained, it was concluded that following an atomic explosion there are two specific causes of air-mass movement. One is related to the shock phenomenon and the other to the rising fireball. It can also be concluded that the heated-thermopile-type and strain-gage-type anemometers could be developed to yield more complete data on the air-mass movement at ground level following an atomic explosion.

  12. In-Situ Creep Testing Capability for the Advanced Test Reactor

    SciTech Connect (OSTI)

    B. G. Kim; J. L. Rempe; D. L. Knudson; K. G. Condie; B. H. Sencer

    2012-09-01

    An instrumented creep testing capability is being developed for specimens irradiated in Pressurized Water Reactor (PWR) coolant conditions at the Advanced Test Reactor (ATR). The test rig has been developed such that samples will be subjected to stresses ranging from 92 to 350 MPa at temperatures between 290 and 370 C up to at least 2 dpa (displacement per atom). The status of Idaho National Laboratory (INL) efforts to develop the test rig in-situ creep testing capability for the ATR is described. In addition to providing an overview of in-pile creep test capabilities available at other test reactors, this paper reports efforts by INL to evaluate a prototype test rig in an autoclave at INLs High Temperature Test Laboratory (HTTL). Initial data from autoclave tests with 304 stainless steel (304 SS) specimens are reported.

  13. A proposed benchmark for simulation in radiographic testing

    SciTech Connect (OSTI)

    Jaenisch, G.-R.; Deresch, A.; Bellon, C.; Schumm, A.; Guerin, P.

    2014-02-18

    The purpose of this benchmark study is to compare simulation results predicted by various models of radiographic testing, in particular those that are capable of separately predicting primary and scatter radiation for specimens of arbitrary geometry.

  14. Ecosystem feedbacks to climate change in California: Development, testing, and analysis using a coupled regional atmosphere and land-surface model (WRF3-CLM3.5)

    SciTech Connect (OSTI)

    Subin, Z.M.; Riley, W.J.; Kueppers, L.M.; Jin, J.; Christianson, D.S.; Torn, M.S.

    2010-11-01

    A regional atmosphere model [Weather Research and Forecasting model version 3 (WRF3)] and a land surface model [Community Land Model, version 3.5 (CLM3.5)] were coupled to study the interactions between the atmosphere and possible future California land-cover changes. The impact was evaluated on California's climate of changes in natural vegetation under climate change and of intentional afforestation. The ability of WRF3 to simulate California's climate was assessed by comparing simulations by WRF3-CLM3.5 and WRF3-Noah to observations from 1982 to 1991. Using WRF3-CLM3.5, the authors performed six 13-yr experiments using historical and future large-scale climate boundary conditions from the Geophysical Fluid Dynamics Laboratory Climate Model version 2.1 (GFDL CM2.1). The land-cover scenarios included historical and future natural vegetation from the Mapped Atmosphere-Plant-Soil System-Century 1 (MC1) dynamic vegetation model, in addition to a future 8-million-ha California afforestation scenario. Natural vegetation changes alone caused summer daily-mean 2-m air temperature changes of -0.7 to +1 C in regions without persistent snow cover, depending on the location and the type of vegetation change. Vegetation temperature changes were much larger than the 2-m air temperature changes because of the finescale spatial heterogeneity of the imposed vegetation change. Up to 30% of the magnitude of the summer daily-mean 2-m air temperature increase and 70% of the magnitude of the 1600 local time (LT) vegetation temperature increase projected under future climate change were attributable to the climate-driven shift in land cover. The authors projected that afforestation could cause local 0.2-1.2 C reductions in summer daily-mean 2-m air temperature and 2.0-3.7 C reductions in 1600 LT vegetation temperature for snow-free regions, primarily because of increased evapotranspiration. Because some of these temperature changes are of comparable magnitude to those projected under

  15. Microstructural and micromechanical characterization of IN718 theta shaped specimens built with electron beam melting

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Cakmak, Ercan; Kirka, Michael M.; Watkins, Thomas R.; Cooper, Ryan C.; An, Ke; Choo, Hahn; Wu, Wei; Dehoff, Ryan R.; Babu, Sudarsanam S.

    2016-02-23

    Theta-shaped specimens were additively manufactured out of Inconel 718 powders using an electron beam melting technique, as a model complex load bearing structure. We employed two different build strategies; producing two sets of specimens. Microstructural and micro-mechanical characterizations were performed using electron back-scatter, synchrotron x-ray and in-situ neutron diffraction techniques. In particular, the cross-members of the specimens were the focus of the synchrotron x-ray and in-situ neutron diffraction measurements. The build strategies employed resulted in the formation of distinct microstructures and crystallographic textures, signifying the importance of build-parameter manipulation for microstructural optimization. Large strain anisotropy of the different lattice planesmore » was observed during in-situ loading. Texture was concluded to have a distinct effect upon both the axial and transverse strain responses of the cross-members. In particular, the (200), (220) and (420) transverse lattice strains all showed unexpected overlapping trends in both builds. This was related to the strong {200} textures along the build/loading direction, providing agreement between the experimental and calculated results.« less

  16. Chemical Quantification of Atomic-Scale EDS Maps under Thin Specimen Conditions

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Lu, Ping; Romero, Eric; Lee, Shinbuhm; MacManus-Driscoll, Judith L.; Jia, Quanxi

    2014-10-13

    We report our effort to quantify atomic-scale chemical maps obtained by collecting energy-dispersive X-ray spectra (EDS) using scanning transmission electron microscopy (STEM) (STEM-EDS). Under a thin specimen condition and when the EDS scattering potential is localized, the X-ray counts from atomic columns can be properly counted by fitting Gaussian peaks at the atomic columns, and can then be used for site-by-site chemical quantification. The effects of specimen thickness and X-ray energy on the Gaussian peak-width are investigated by using SrTiO3 (STO) as a model specimen. The relationship between the peak-width and spatial-resolution of an EDS map is also studied. Furthermore,more » the method developed by this work is applied to study a Sm-doped STO thin film and antiphase boundaries present within the STO film. We find that Sm atoms occupy both Sr and Ti sites but preferably the Sr sites, and Sm atoms are relatively depleted at the antiphase boundaries likely due to the effect of strain.« less

  17. Chemical Quantification of Atomic-Scale EDS Maps under Thin Specimen Conditions

    SciTech Connect (OSTI)

    Lu, Ping; Romero, Eric; Lee, Shinbuhm; MacManus-Driscoll, Judith L.; Jia, Quanxi

    2014-10-13

    We report our effort to quantify atomic-scale chemical maps obtained by collecting energy-dispersive X-ray spectra (EDS) using scanning transmission electron microscopy (STEM) (STEM-EDS). Under a thin specimen condition and when the EDS scattering potential is localized, the X-ray counts from atomic columns can be properly counted by fitting Gaussian peaks at the atomic columns, and can then be used for site-by-site chemical quantification. The effects of specimen thickness and X-ray energy on the Gaussian peak-width are investigated by using SrTiO3 (STO) as a model specimen. The relationship between the peak-width and spatial-resolution of an EDS map is also studied. Furthermore, the method developed by this work is applied to study a Sm-doped STO thin film and antiphase boundaries present within the STO film. We find that Sm atoms occupy both Sr and Ti sites but preferably the Sr sites, and Sm atoms are relatively depleted at the antiphase boundaries likely due to the effect of strain.

  18. Surface sampling concentration and reaction probe

    DOE Patents [OSTI]

    Van Berkel, Gary J; Elnaggar, Mariam S

    2013-07-16

    A method of analyzing a chemical composition of a specimen is described. The method can include providing a probe comprising an outer capillary tube and an inner capillary tube disposed co-axially within the outer capillary tube, where the inner and outer capillary tubes define a solvent capillary and a sampling capillary in fluid communication with one another at a distal end of the probe; contacting a target site on a surface of a specimen with a solvent in fluid communication with the probe; maintaining a plug volume proximate a solvent-specimen interface, wherein the plug volume is in fluid communication with the probe; draining plug sampling fluid from the plug volume through the sampling capillary; and analyzing a chemical composition of the plug sampling fluid with an analytical instrument. A system for performing the method is also described.

  19. Translaminar fracture toughness test methods and results from interlaboratory tests of carbon/epoxy laminates

    SciTech Connect (OSTI)

    Underwood, J.H.; Kortschot, M.T.; Lloyd, W.R.; Eidinoff, H.L.; Wilson, D.A.; Ashbaugh, N.

    1995-12-31

    Fracture tests were performed with carbon/polymer laminates and analyzed for the purpose of developing translaminar fracture toughness test and analysis procedures. Notched specimens were tested of two types of symmetrical layups--quasi-isotropic [0/45/90] and [0/90]; two carbon fiber/epoxy materials--a relatively brittle T300 fiber/976 epoxy and a tougher AS4 fiber/977-2 epoxy; two laminate thicknesses--2 mm and 4 mm; and three specimen configurations--the standard three-point bend and compact configurations, and an extended compact specimen with arm-height to specimen-width ratio of 1.9. Stress and displacement expressions were obtained for the extended compact specimen, including those for stress intensity factor, K, and crack mouth opening displacement, V, in terms of relative notch length, a/W, and for a/W in terms of V. Relationships for the bending stresses that control self-similar and off-axis cracking for the extended compact specimen were derived.

  20. Solderability test system

    DOE Patents [OSTI]

    Yost, Fred; Hosking, Floyd M.; Jellison, James L.; Short, Bruce; Giversen, Terri; Reed, Jimmy R.

    1998-01-01

    A new test method to quantify capillary flow solderability on a printed wiring board surface finish. The test is based on solder flow from a pad onto narrow strips or lines. A test procedure and video image analysis technique were developed for conducting the test and evaluating the data. Feasibility tests revealed that the wetted distance was sensitive to the ratio of pad radius to line width (l/r), solder volume, and flux predry time.

  1. Solderability test system

    DOE Patents [OSTI]

    Yost, F.; Hosking, F.M.; Jellison, J.L.; Short, B.; Giversen, T.; Reed, J.R.

    1998-10-27

    A new test method to quantify capillary flow solderability on a printed wiring board surface finish. The test is based on solder flow from a pad onto narrow strips or lines. A test procedure and video image analysis technique were developed for conducting the test and evaluating the data. Feasibility tests revealed that the wetted distance was sensitive to the ratio of pad radius to line width (l/r), solder volume, and flux predry time. 11 figs.

  2. Low Temperature Surface Carburization of Stainless Steels

    SciTech Connect (OSTI)

    Collins, Sunniva R; Heuer, Arthur H; Sikka, Vinod K

    2007-12-07

    Thermodynamic modeling to explain the high degree of carbon solubility possible in austenitic grades under the LTCSS process and experimental validation of model results • Corrosion testing to determine the corrosion resistance improvement possible from the LTCSS process • Erosion testing to determine the erosion resistance improvement possible from the LTCSS process • Wear testing to quantify the wear resistance improvement possible from the LTCSS process • Fatigue testing for quantifying the extent of improvement from the LTCSS process • Component treating and testing under simulated and in-line commercial operations XRD verified expanded austenite lattice, with no evidence of carbide precipitation. Carbon concentration profiles via Auger and electron dispersion spectroscopy (EDS) showed carbon levels in excess of 12 at. % in treated, type 316 SS. Scanning electron microscopy (SEM) of pulled-to-failure treated tensile specimens showed slip bands and no de-cohesion of the treated layer, verifying that the layer remains ductile. Compressive stresses in excess of 2 GPa (300 ksi) have been calculated at the surface of the case. Phase diagram (CALPHAD) (ThermoCalc) and Wagner dilute solution thermodynamic models were developed that calculate the solubility of carbon in austenite as a function of alloying content for the process time and temperature. Several commercial alloys have been modeled, and the model has been used to design experimental alloys with enhanced affinity for carbon solubility at treatment temperatures. Four experimental alloys were melted, rolled, and manufactured into test specimens, and the LTCSS treatment indicated successfully enhanced results and validated the predictions based on thermodynamic modeling. Electrochemical polarization curves show a 600 to 800 mV increase in pitting potential in treated (900-1000 mV) versus non-treated (200-300 mV) type 316 in chloride solutions. Treated 316L showed crevice-corrosion behavior similar to that of Ti-6

  3. High-heat-flux testing of irradiated tungsten-based materials for fusion applications using infrared plasma arc lamps

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Sabau, Adrian S.; Ohriner, Evan K.; Kiggans, Jim; Schaich, Charles R.; Ueda, Yoshio; Harper, David C.; Katoh, Yutai; Snead, Lance L.; Byun, Thak S.

    2014-11-01

    Testing of advanced materials and component mock-ups under prototypical fusion high-heat-flux conditions, while historically a mainstay of fusion research, has proved to be quite challenging, especially for irradiated materials. A new high-heat-flux–testing (HHFT) facility based on water-wall plasma arc lamps (PALs) is now introduced for materials and small-component testing. Two PAL systems, utilizing a 12 000°C plasma arc contained in a quartz tube cooled by a spiral water flow over the inside tube surface, provide maximum incident heat fluxes of 4.2 and 27 MW/m2 over areas of 9×12 and 1×10 cm2, respectively. This paper will present the overall design andmore » implementation of a PAL-based irradiated material target station (IMTS). The IMTS is primarily designed for testing the effects of heat flux or thermal cycling on material coupons of interest, such as those for plasma-facing components. Temperature results are shown for thermal cycling under HHFT of tungsten coupon specimens that were neutron irradiated in HFIR. Finally, radiological surveys indicated minimal contamination of the 36×36×18 cm test section, demonstrating the capability of the new facility to handle irradiated specimens at high temperature.« less

  4. High-Heat-Flux Testing of Irradiated Tungsten-Based Materials for Fusion Applications Using Infrared Plasma Arc Lamps

    SciTech Connect (OSTI)

    Sabau, Adrian S.; Ohriner, Evan K.; Kiggans, Jim; Schaich, Charles R.; Ueda, Yoshio; Harper, David C.; Katoh, Yutai; Snead, Lance L.; Byun, Thak S.

    2014-11-01

    Testing of advanced materials and component mock-ups under prototypical fusion high-heat-flux conditions, while historically a mainstay of fusion research, has proved to be quite challenging, especially for irradiated materials. A new high-heat-flux–testing (HHFT) facility based on water-wall plasma arc lamps (PALs) is now introduced for materials and small-component testing. Two PAL systems, utilizing a 12 000°C plasma arc contained in a quartz tube cooled by a spiral water flow over the inside tube surface, provide maximum incident heat fluxes of 4.2 and 27 MW/m2 over areas of 9×12 and 1×10 cm2, respectively. This paper will present the overall design and implementation of a PAL-based irradiated material target station (IMTS). The IMTS is primarily designed for testing the effects of heat flux or thermal cycling on material coupons of interest, such as those for plasma-facing components. Temperature results are shown for thermal cycling under HHFT of tungsten coupon specimens that were neutron irradiated in HFIR. Finally, radiological surveys indicated minimal contamination of the 36-× 36-× 18-cm test section, demonstrating the capability of the new facility to handle irradiated specimens at high temperature.

  5. A system for combined three-dimensional morphological and molecular analysis of thick tissue specimens

    SciTech Connect (OSTI)

    Fernandez-Gonzalez, Rodrigo; Jones, Arthur; Garcia-Rodriguez, Enrique; Yuan Chen, Ping; Idica, Adam; Lockett, Stephen J.; Barcellos-Hoff, Mary Helen; Ortiz-de-Solorzano, Carlos

    2002-04-25

    We present a new system for simultaneous morphological and molecular analysis of thick tissue samples. The system is composed of a computer assisted microscope and a JAVA-based image display, analysis and visualization program that allows acquisition, annotation, meaningful storage, three-dimensional reconstruction and analysis of structures of interest in thick sectioned tissue specimens. We describe the system in detail and illustrate its use by imaging, reconstructing and analyzing two complete tissue blocks which were differently processed and stained. One block was obtained from a ductal carcinoma in situ (DCIS) lumpectomy specimen and stained alternatively with Hematoxilyn and Eosin (H&E), and with a counterstain and fluorescence in situ hybridization (FISH) to the ERB-B2 gene. The second block contained a fully sectioned mammary gland of a mouse, stained for Histology with H&E. We show how the system greatly reduces the amount of interaction required for the acquisition and analysis and is therefore suitable for studies that require morphologically driven, wide scale (e.g., whole gland) analysis of complex tissue samples or cultures.

  6. Ballistic penetration test results for Ductal and ultra-high performance concrete samples.

    SciTech Connect (OSTI)

    Reinhart, William Dodd; Thornhill, Tom Finley, III

    2010-03-01

    This document provides detailed test results of ballistic impact experiments performed on several types of high performance concrete. These tests were performed at the Sandia National Laboratories Shock Thermodynamic Applied Research Facility using a 50 caliber powder gun to study penetration resistance of concrete samples. This document provides test results for ballistic impact experiments performed on two types of concrete samples, (1) Ductal{reg_sign} concrete is a fiber reinforced high performance concrete patented by Lafarge Group and (2) ultra-high performance concrete (UHPC) produced in-house by DoD. These tests were performed as part of a research demonstration project overseen by USACE and ERDC, at the Sandia National Laboratories Shock Thermodynamic Applied Research (STAR) facility. Ballistic penetration tests were performed on a single stage research powder gun of 50 caliber bore using a full metal jacket M33 ball projectile with a nominal velocity of 914 m/s (3000 ft/s). Testing was observed by Beverly DiPaolo from ERDC-GSL. In all, 31 tests were performed to achieve the test objectives which were: (1) recovery of concrete test specimens for post mortem analysis and characterization at outside labs, (2) measurement of projectile impact velocity and post-penetration residual velocity from electronic and radiographic techniques and, (3) high-speed photography of the projectile prior to impact, impact and exit of the rear surface of the concrete construct, and (4) summarize the results.

  7. An investigation of penetrant techniques for detection of machining-induced surface-breaking cracks on monolithic ceramics

    SciTech Connect (OSTI)

    Forster, G.A.; Ellingson, W.A.

    1996-02-01

    The purpose of this effort was to evaluate penetrant methods for their ability to detect surface-breaking cracks in monolithic ceramic materials with an emphasis on detection of cracks generated by machining. There are two basic penetrant types, visible and fluorescent. The visible penetrant method is usually augmented by powder developers and cracks detected can be seen in visible light. Cracks detected by fluorescent penetrant are visible only under ultraviolet light used with or without a developer. The developer is basically a powder that wicks up penetrant from a crack to make it more observable. Although fluorescent penetrants were recommended in the literature survey conducted early in this effort, visible penetrants and two non-standard techniques, a capillary gaseous diffusion method under development at the institute of Chemical Physics in Moscow, and the {open_quotes}statiflux{close_quotes} method which involves use of electrically charged particles, were also investigated. SiAlON ring specimens (1 in. diameter, 3/4 in. wide) which had been subjected to different thermal-shock cycles were used for these tests. The capillary gaseous diffusion method is based on ammonia; the detector is a specially impregnated paper much like litmus paper. As expected, visible dye penetrants offered no detection sensitivity for tight, surface-breaking cracks in ceramics. Although the non-standard statiflux method showed promise on high-crack-density specimens, it was ineffective on limited-crack-density specimens. The fluorescent penetrant method was superior for surface-breaking crack detection, but successful application of this procedure depends greatly on the skill of the user. Two presently available high-sensitivity fluorescent penetrants were then evaluated for detection of microcracks on Si{sub 3}N{sub 4} and SiC from different suppliers. Although 50X optical magnification may be sufficient for many applications, 200X magnification provides excellent delectability.

  8. High-Heat Flux Testing of Irradiated Tungsten based Materials for Fusion Applications using Infrared Plasma Arc Lamps

    SciTech Connect (OSTI)

    Sabau, Adrian S; Ohriner, Evan Keith; Kiggans Jr, James O; Schaich, Charles Ross; Ueda, Yoshio; Harper, David C; Katoh, Yutai; Snead, Lance Lewis; Byun, Thak Sang

    2014-01-01

    Testing of advanced materials and component mock-ups under prototypical fusion high-heat flux conditions, while historically a mainstay of fusion research has proved challenging, especially for irradiated materials. A new high-heat flux testing facility based on water-wall Plasma Arc Lamps (PALs) is now being used for materials and small component testing. Two PAL systems, utilizing a 12,000 C plasma arc contained in a quartz tube cooled by a spiral water flow over the inside tube surface, are currently in use. The first PAL system provides a maximum incident heat flux of 4.2 MW/m2 over an area of 9x12 cm2. The second PAL available at ORNL provides a maximum incident heat flux of 27 MW/m2 over an area of 1x10 cm2. The absorbed heat fluxes into a tungsten target for the two PALs are approximately 1.97 and 12.7 MW/m2, respectively. This paper will present the overall design of the new PAL facilities as well as the design and implementation of the Irradiated Material Target Station (IMTS). The IMTS is primarily designed for testing the effects of heat flux or thermal cycling on material coupons of interested, such as those for plasma facing components. Moreover, IMTS designs are underway to extend the testing of small mock-ups for assessing the combined heating and thermomechanical effects of cooled, irradiated components. For the testing of material coupons , the specimens are placed in a shallow recess within the molybdenum holder that is attached to a water-cooled copper alloy rod. As the measurement of the specimen temperature for PAL is historically challenging since traditional approaches of temperature measurement cannot be employed due to the infrared heating and proximity of the PAL reflector to the specimen that does not allow a direct line of site, experiments for temperature calibration are presented. Finally, results for the high-heat flux testing of tungsten-based materials using the PAL are presented. As a demonstration of the system, results will be

  9. Metallographic autopsies of full-scale ITER prototype cable-in-conduit conductors after full cyclic testing in SULTAN: III. The importance of strand surface roughness in long twist pitch conductors

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Sanabria, Charlie; Lee, Peter J.; Starch, William; Devred, Arnaud; Larbalestier, David C.

    2016-05-31

    As part of the ITER conductor qualification process, 3 m long Cable-in-Conduit Conductors (CICCs) were tested at the SULTAN facility under conditions simulating ITER operation so as to establish the current sharing temperature, Tcs, as a function of multiple full Lorentz force loading cycles. After a comprehensive evaluation of both the Toroidal Field (TF) and the Central Solenoid (CS) conductors, it was found that Tcs degradation was common in long twist pitch TF conductors while short twist pitch CS conductors showed some Tcs increase. However, one kind of TF conductors containing superconducting strand fabricated by the Bochvar Institute of Inorganicmore » Materials (VNIINM) avoided Tcs degradation despite having long twist pitch. In our earlier metallographic autopsies of long and short twist pitch CS conductors, we observed a substantially greater transverse strand movement under Lorentz force loading for long twist pitch conductors, while short twist pitch conductors had negligible transverse movement. With help from the literature, we concluded that the transverse movement was not the source of Tcs degradation but rather an increase of the compressive strain in the Nb3Sn filaments possibly induced by longitudinal movement of the wires. Like all TF conductors this TF VNIINM conductor showed large transverse motions under Lorentz force loading, but Tcs actually increased, as in all short twist pitch CS conductors. We here propose that the high surface roughness of the VNIINM strand may be responsible for the suppression of the compressive strain enhancement (characteristic of long twist pitch conductors). Furthermore, it appears that increasing strand surface roughness could improve the performance of long twist pitch CICCs.« less

  10. Characterization of industrially produced galvannealed coating using cross-sectional specimen in TEM

    SciTech Connect (OSTI)

    Chakraborty, A.; Saha, R.; Ray, R.K.

    2009-08-15

    Galvannealed coated sheet steels are extensively used in the automotive industry due to their inherent advantages, as compared to other zinc based coating, such as excellent spot weldability, good corrosion resistance and better paintability. Despite the above advantages, galvannealed coating suffers from poor formability due to the presence of hard and brittle Fe-Zn intermetallic phases. The formability of the coating depends on the amount and orientation of different Fe-Zn intermetallic phases. The present study deals with the characterization of an industrially produced galvannealed coating using cross-sectional specimen in a Transmission Electron Microscope. From the selected area diffraction patterns obtained in Transmission Electron Microscope, the orientations of the delta phase were calculated.

  11. Superhydrophobic surfaces

    DOE Patents [OSTI]

    Wang, Evelyn N; McCarthy, Matthew; Enright, Ryan; Culver, James N; Gerasopoulos, Konstantinos; Ghodssi, Reza

    2015-03-24

    Surfaces having a hierarchical structure--having features of both microscale and nanoscale dimensions--can exhibit superhydrophobic properties and advantageous condensation and heat transfer properties. The hierarchical surfaces can be fabricated using biological nanostructures, such as viruses as a self-assembled nanoscale template.

  12. Micromachine friction test apparatus

    DOE Patents [OSTI]

    deBoer, Maarten P.; Redmond, James M.; Michalske, Terry A.

    2002-01-01

    A microelectromechanical (MEM) friction test apparatus is disclosed for determining static or dynamic friction in MEM devices. The friction test apparatus, formed by surface micromachining, is based on a friction pad supported at one end of a cantilevered beam, with the friction pad overlying a contact pad formed on the substrate. A first electrostatic actuator can be used to bring a lower surface of the friction pad into contact with an upper surface of the contact pad with a controlled and adjustable force of contact. A second electrostatic actuator can then be used to bend the cantilevered beam, thereby shortening its length and generating a relative motion between the two contacting surfaces. The displacement of the cantilevered beam can be measured optically and used to determine the static or dynamic friction, including frictional losses and the coefficient of friction between the surfaces. The test apparatus can also be used to assess the reliability of rubbing surfaces in MEM devices by producing and measuring wear of those surfaces. Finally, the friction test apparatus, which is small in size, can be used as an in situ process quality tool for improving the fabrication of MEM devices.

  13. Material test machine for tension-compression tests at high temperature

    DOE Patents [OSTI]

    Cioletti, Olisse C.

    1988-01-01

    Apparatus providing a device for testing the properties of material specimens at high temperatures and pressures in controlled water chemistries includes, inter alia, an autoclave housing the specimen which is being tested. The specimen is connected to a pull rod which couples out of the autoclave to an external assembly which includes one or more transducers, a force balance chamber and a piston type actuator. The pull rod feeds through the force balance chamber and is compensated thereby for the pressure conditions existing within the autoclave and tending to eject the pull rod therefrom. The upper end of the push rod is connected to the actuator through elements containing a transducer comprising a linear variable differential transformer (LVDT). The housing and coil assembly of the LVDT is coupled to a tube which runs through a central bore of the pull rod into the autoclave where it is connected to one side of the specimen. The movable core of the LVDT is coupled to a stem which runs through the tube where it is then connected to the other side of the specimen through a coupling member. A transducer in the form of a load cell including one or more strain gages is located on a necked-down portion of the upper part of the pull rod intermediate the LVDT and force balance chamber.

  14. Test chamber for alpha spectrometry

    DOE Patents [OSTI]

    Larsen, Robert P.

    1977-01-01

    Alpha emitters for low-level radiochemical analysis by measurement of alpha spectra are positioned precisely with respect to the location of a surface-barrier detector by means of a chamber having a removable threaded planchet holder. A pedestal on the planchet holder holds a specimen in fixed engagement close to the detector. Insertion of the planchet holder establishes an O-ring seal that permits the chamber to be pumped to a desired vacuum. The detector is protected against accidental contact and resulting damage.

  15. Leach test methodology for the Waste/Rock Interactions Technology Program

    SciTech Connect (OSTI)

    Bradley, D.J.; McVay, G.L.; Coles, D.G.

    1980-05-01

    Experimental leach studies in the WRIT Program have two primary functions. The first is to determine radionuclide release from waste forms in laboratory environments which attempt to simulate repository conditions. The second is to elucidate leach mechanisms which can ultimately be incorporated into nearfield transport models. The tests have been utilized to generate rates of removal of elements from various waste forms and to provide specimens for surface analysis. Correlation between constituents released to the solution and corresponding solid state profiles is invaluable in the development of a leach mechanism. Several tests methods are employed in our studies which simulate various proposed leach incident scenarios. Static tests include low temperature (below 100/sup 0/C) and high temperature (above 100/sup 0/C) hydrothermal tests. These tests reproduce nonflow or low-flow repository conditions and can be used to compare materials and leach solution effects. The dynamic tests include single-pass, continuous-flow(SPCF) and solution-change (IAA)-type tests in which the leach solutions are changed at specific time intervals. These tests simulate repository conditions of higher flow rates and can also be used to compare materials and leach solution effects under dynamic conditions. The modified IAEA test is somewhat simpler to use than the one-pass flow and gives adequate results for comparative purposes. The static leach test models the condition of near-zero flow in a repository and provides information on element readsorption and solubility limits. The SPCF test is used to study the effects of flowing solutions at velocities that may be anticipated for geologic groundwaters within breached repositories. These two testing methods, coupled with the use of autoclaves, constitute the current thrust of WRIT leach testing.

  16. Surface Soil

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Surface Soil Surface Soil We compare local soil samples with samples collected from northern New Mexico locations that are beyond the range of potential influence from normal Laboratory operations. April 12, 2012 Farm soil sampling Two LANL environmental field team members take soil samples from a farm. Contact Environmental Communication & Public Involvement P.O. Box 1663 MS M996 Los Alamos, NM 87545 (505) 667-0216 Email Measurements are compared to samples from the regional sites and

  17. A simulation of the transport and fate of radon-222 derived from thorium-230 low-level waste in the near-surface zone of the Radioactive Waste Management Site in Area 5 of the Nevada Test Site

    SciTech Connect (OSTI)

    Lindstrom, F.T.; Cawlfield, D.E.; Donahue, M.E.; Emer, D.F.; Shott, G.J.

    1993-12-01

    US Department of Energy (DOE) Order 5820.2A (DOE, 1988) requires performance assessments on all new and existing low-level radioactive waste (LLW) disposal sites. An integral part of performance assessment is estimating the fluxes of radioactive gases such as radon-220 and radon-222. Data needs pointed out by mathematical models drive site characterization. They provide a logical means of performing the required flux estimations. Thorium-230 waste, consisting largely of thorium hydroxide and thorium oxides, has been approved for disposal in shallow trenches and pits at the LLW Radioactive Waste Management Site in Area 5 of the Nevada Test Site. A sophisticated gas transport model, CASCADR8 (Lindstrom et al., 1992b), was used to simulate the transport and fate of radon-222 from its source of origin, nine feet below a closure cap of native soil, through the dry alluvial earth, to its point of release into the atmosphere. CASCADR8 is an M-chain gas-phase radionuclide transport and fate model. It has been tailored to the site-specific needs of the dry desert environment of southern Nevada. It is based on the mass balance principle for each radionuclide and uses gas-phase diffusion as well as barometric pressure-induced advection as its main modes of transport. CASCADR8 uses both reversible and irreversible sorption kinetic rules as well as the usual classical Bateman (1910) M-chain decay rules for its kinetic processes. Worst case radon-222 gas-phase concentrations, as well as surface fluxes, were estimated over 40 days. The maximum flux was then used in an exposure assessment model to estimate the total annual dose equivalent received by a person residing in a standard 2500-square-foot house with 10-foot walls. Results are described.

  18. Effects of testing and storage environments on mechanical properties of Ni-plated and bare U-3/4 wt% Ti

    SciTech Connect (OSTI)

    Zehr, S.W.; Johnson, H.R.; Smugeresky, J.E.; Pashman, K.A.; Nagelberg, A.S.

    1980-01-01

    It was found that storage environments with an adequate supply of oxygen can effectively minimize moisture corrosion of bare U-3/4 Ti. In particular, 0.75 cm/sup 3/ of dry air is calculated to protect 1 cm/sup 2/ of U-3/4 Ti for 20 years storage at room temperature. Consideration of the geometric details of U-3/4 Ti alloy specimens and the free volumes of air (and hence O/sub 2/) available can satisfactorily explain discrepancies in corrosion behavior between recent tests and previously reported data. The storage environment at 70/sup 0/C produces a minor strength increase in bare samples with increasing time. Decreases in ductility are observed for testing conditions of low temperature, low strain rate, and/or high humidity. Surface cracks occur under the same conditions conducive to corrosion, i.e., moderate temperatures, low strain rates, and high humidity. Significant increases in strength result under low-temperature and high-strain-rate conditions of tensile testing. Residual chloride contamination may be responsible for the occasional and otherwise unexplained large scatter in ductility for nominally similar specimens and test conditions. Nickel plating is observed to cause a statistically significant decrease in tensile strength, but no effect on the yield strength or ductility was observed and the presence of high explosive during the aging of tensile bars was observed to have no effect on mechanical properties.

  19. Leak test fitting

    DOE Patents [OSTI]

    Pickett, P.T.

    A hollow fitting for use in gas spectrometry leak testing of conduit joints is divided into two generally symmetrical halves along the axis of the conduit. A clip may quickly and easily fasten and unfasten the halves around the conduit joint under test. Each end of the fitting is sealable with a yieldable material, such as a piece of foam rubber. An orifice is provided in a wall of the fitting for the insertion or detection of helium during testing. One half of the fitting also may be employed to test joints mounted against a surface.

  20. Leak test fitting

    DOE Patents [OSTI]

    Pickett, Patrick T.

    1981-01-01

    A hollow fitting for use in gas spectrometry leak testing of conduit joints is divided into two generally symmetrical halves along the axis of the conduit. A clip may quickly and easily fasten and unfasten the halves around the conduit joint under test. Each end of the fitting is sealable with a yieldable material, such as a piece of foam rubber. An orifice is provided in a wall of the fitting for the insertion or detection of helium during testing. One half of the fitting also may be employed to test joints mounted against a surface.

  1. Forklift Test

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Forklift Safety Test Instructions: All Training and Testing Material is for LSU CAMD Users ... A minimum passing score is 80% (8 out of 10) This test can only be taken once in a thirty ...

  2. TEST-HOLE CONSTRUCTION FOR A NEUTRONIC REACTOR

    DOE Patents [OSTI]

    Ohlinger, L.A.; Seitz, F.; Young, G.J.

    1959-02-17

    Test-hole construction is described for a reactor which provides safe and ready access to the neutron flux region for specimen materials which are to be irradiated therein. An elongated tubular thimble adapted to be inserted in the access hole through the wall of the reactor is constructed of aluminum and is provided with a plurality of holes parallel to the axis of the thimble for conveying the test specimens into position for irradiation, and a conduit for the circulation of coolant. A laminated shield formed of alternate layers of steel and pressed wood fiber is disposed lengthwise of the thimble near the outer end thereof.

  3. Stellite 6 Friction Changes Due to Aging and In-Service Testing

    SciTech Connect (OSTI)

    Watkins, John Clifford; DeWall, Kevin George

    2001-07-01

    For the past several years, researchers at the Idaho National Engineering and Environmental Laboratory, under the sponsorship of the U.S. Nuclear Regulatory Commission, have been investigating the ability of motor-operated valves to close or open when subjected to design basis flow and pressure loads. Part of this research addresses the friction that occurs at the interface between the valve disc and the valve body seats during operation of a gate valve. In most gate valves, these surfaces are hardfaced with Stellite 6, a cobalt-based alloy. The nuclear industry has developed methods to analytically predict the thrust needed to operate these valves at specific pressure conditions. To produce accurate valve thrust predictions; the analyst must have a reasonably accurate, though conservative, estimate of the coefficient of friction at the disc-to-seat interface. One of the questions that remains to be answered is whether, and to what extent, aging of the disc and seat surfaces affects the disc-to-seat coefficient of friction. Specifically, does the accumulation of a surface film due to aging of these surfaces increase the coefficient of friction and if so, how much? This paper presents results of specimen tests addressing this issue with emphasis on the following: • The change in the friction coefficient of Stellite 6 as it ages and whether the friction reaches a plateau. • The effect periodic gate valve cycling due to in-service testing has on the friction coefficient. • The results of an independent review of the test methods, processes, and the results of the research to date. • The status of ongoing aging and friction testing.

  4. Corrosion testing using isotopes

    DOE Patents [OSTI]

    Hohorst, Frederick A.

    1995-12-05

    A method for determining the corrosion behavior of a material with respect to a medium in contact with the material by: implanting a substantially chemically inert gas in a matrix so that corrosion experienced by the material causes the inert gas to enter the medium; placing the medium in contact with the material; and measuring the amount of inert gas which enters the medium. A test sample of a material whose resistance to corrosion by a medium is to be tested, composed of: a body of the material, which body has a surface to be contacted by the medium; and a substantially chemically inert gas implanted into the body to a depth below the surface. A test sample of a material whose resistance to corrosion by a medium is to be tested, composed of: a substrate of material which is easily corroded by the medium, the substrate having a surface; a substantially chemically inert gas implanted into the substrate; and a sheet of the material whose resistance to corrosion is to be tested, the sheet being disposed against the surface of the substrate and having a defined thickness.

  5. Corrosion testing using isotopes

    DOE Patents [OSTI]

    Hohorst, F.A.

    1995-12-05

    A method is described for determining the corrosion behavior of a material with respect to a medium in contact with the material by: implanting a substantially chemically inert gas in a matrix so that corrosion experienced by the material causes the inert gas to enter the medium; placing the medium in contact with the material; and measuring the amount of inert gas which enters the medium. A test sample of a material whose resistance to corrosion by a medium is to be tested is described composed of: a body of the material, which body has a surface to be contacted by the medium; and a substantially chemically inert gas implanted into the body to a depth below the surface. A test sample of a material whose resistance to corrosion by a medium is to be tested is described composed of: a substrate of material which is easily corroded by the medium, the substrate having a surface; a substantially chemically inert gas implanted into the substrate; and a sheet of the material whose resistance to corrosion is to be tested, the sheet being disposed against the surface of the substrate and having a defined thickness. 3 figs.

  6. Lustre Tests

    Energy Science and Technology Software Center (OSTI)

    2007-08-31

    Lustre-tests is a package of regression tests for the Lustre file system containing I/O workloads representative of problems discovered on production systems.

  7. Fracture toughness testing of bi-material joints with high strength mis-match

    SciTech Connect (OSTI)

    Kocak, M.; Hornet, P.; Cornec, A.; Schwalbe, K.H.

    1995-12-31

    This paper deals with the influence of strength mis-match on CTOD ({delta}{sub 5}) R-curves obtained from homogeneous and electron beam (EB) welded bimaterial CT and SENB specimens of two aluminum alloys. The R-curves of metal-metal bimaterial specimens are compared with the R-curves of each alloy to determine the effect of strength mismatch on the locally measured CTOD ({delta}{sub 5}) fracture toughness properties. The homogeneous specimens of two different aluminum alloys, namely 2024-FC and 2024-T351 with yield strengths of 80 and 360 MPa respectively, as well as EB welded bi-material 5 mm thick CT and SENB specimens (a/W = 0.15 and 0.5) have been tested at room temperature. The local CTOD ({delta}{sub 5}) fracture toughness measurements on such composite specimen configurations produced generally strength mis-match and geometry independent R-curves.

  8. Borehole SASW testing to evaluate log(G{sub max}) - log({sigma}{prime}) relationships in situ

    SciTech Connect (OSTI)

    Kalinski, M.E.; Stokoe, K.H. II; Young, Y.L.; Roesset, J.M.

    1999-07-01

    A new method is being developed for the in-situ measurement of shear wave velocity, V{sub s}, in the soil surrounding a borehole. The method involves the measurement of axially propagating surface waves inside an uncased borehole using the Spectral-Analysis-of-Surface-Waves (SASW) approach. Testing if performed with instrumentation housed inside an inflatable tool. Inflation pressures applied by the tool are used to vary radial stresses in the soil surrounding the borehole. Surface wave velocities over a range of frequencies are measured at each inflation pressure. These measurements are then theoretically modeled so that the variation in V{sub s} (an hence small-strain shear module, G{sub max}) with distance behind the borehole wall is determined at each pressure. The results of field tests with the borehole SASW tool at two sites composed of unsaturated clayey soil are presented. These results are compared with independent field seismic measurements and with laboratory tests on intact specimens using the torsional resonant column to assess the validity of the new field method.

  9. TRUPACT-I Unit 0 test data analysis. [Puncture bar impacts; free fall of package 12 inches onto unyielding surface; 30-foot free fall drop onto unyielding target; 40-inch drops onto 6-inch diagmeter puncture bar; engulfment in jet fuel fire for 35 minutes

    SciTech Connect (OSTI)

    Romesberg, L.E.; Hudson, M.L.; Osborne, D.M.

    1985-09-01

    TRUPACT-I was tested to evaluate the response of the design to the normal and hypothetical accident conditions specified in applicable regulations. The governing regulations are contained in DOE Order No. 5480.1, Chapter 3 and 10 CFR, Part 71, Refs. 1 and 2. Tests were conducted at Oak Ridge National Laboratory, Oak Ridge, TN, and at Sandia National Laboratories, Albuquerque, NM. Normal condition tests included three 13-pound (1.25 in. diameter) puncture bar impacts onto the exterior surface and free fall of the package 12 inches onto an essentially unyielding surface. Hypothetical accident conditions included in the test sequence were two 30-foot free fall drops of the package onto an essentially unyielding target, four 40-inch drops onto a 6-inch-diameter puncture bar, and engulfment in a JP-4 jet fuel fire for 35 minutes. Instrumentation data traces will be published in Ref. 3 and are not reproduced herein. This report presents an analysis of the available data and an interpretation of the results. The results of the tests are compared to results from numerical analyses and scale model tests which are incorporated in the TRUPACT-I SARP, Ref. 4. 9 refs., 43 figs., 3 tabs.

  10. Explosives screening on a vehicle surface

    DOE Patents [OSTI]

    Parmeter, John E.; Brusseau, Charles A.; Davis, Jerry D.; Linker, Kevin L.; Hannum, David W.

    2005-02-01

    A system for detecting particles on the outer surface of a vehicle has a housing capable of being placed in a test position adjacent to, but not in contact with, a portion of the outer surface of the vehicle. An elongate sealing member is fastened to the housing along a perimeter surrounding the wall, and the elongate sealing member has a contact surface facing away from the wall to contact the outer surface of the vehicle to define a test volume when the wall is in the test position. A gas flow system has at least one gas inlet extending through the wall for providing a gas stream against the surface of the vehicle within the test volume. This gas stream, which preferably is air, dislodges particles from the surface of the vehicle covered by the housing. The gas stream exits the test volume through a gas outlet and particles in the stream are detected.

  11. Surface mining

    SciTech Connect (OSTI)

    Not Available

    1989-06-01

    This paper reports on a GAO study of attorney and expert witness fees awarded as a result of litigation brought under the Surface Mining Control and Reclamation Act. As of March 24, 1989, a total of about $1.4 million had been awarded in attorney fees and expenses - about $1.3 subject to the provisions of the Employee Retirement Income Security Act, a comparison of its features with provisions of ERISA showed that the plan differed from ERISA provisions in areas such as eligibility, funding, and contribution limits.

  12. Analysis of stress-induced Burgers vector anisotropy in pressurized tube specimens of irradiated ferritic-martensitic steel: JLF-1

    SciTech Connect (OSTI)

    Gelles, D.S.; Shibayama, T.

    1998-09-01

    A procedure for determining the Burgers vector anisotropy in irradiated ferritic steels allowing identification of all a<100> and all a/2<111> dislocations in a region of interest is applied to a pressurized tube specimen of JLF-1 irradiated at 430 C to 14.3 {times} 10{sup 22} n/cm{sup 2} (E > 0.1 MeV) or 61 dpa. Analysis of micrographs indicates large anisotropy in Burgers vector populations develop during irradiation creep.

  13. High Strain Rate Tensile Testing of DOP-26 Iridium

    SciTech Connect (OSTI)

    Schneibel, Joachim H; Carmichael Jr, Cecil Albert; George, Easo P

    2007-11-01

    The iridium alloy DOP-26 was developed through the Radioisotope Power Systems Program in the Office of Nuclear Energy of the Department of Energy. It is used for clad vent set cups containing radioactive fuel in radioisotope thermoelectric generator (RTG) heat sources which provide electric power for spacecraft. This report describes mechanical testing results for DOP-26. Specimens were given a vacuum recrystallization anneal of 1 hour at 1375 C and tested in tension in orientations parallel and perpendicular to the rolling direction of the sheet from which they were fabricated. The tests were performed at temperatures ranging from room temperature to 1090 C and strain rates ranging from 1 x 10{sup -3} to 50 s{sup -1}. Room temperature testing was performed in air, while testing at elevated temperatures was performed in a vacuum better than 1 x 10{sup -4} Torr. The yield stress (YS) and the ultimate tensile stress (UTS) decreased with increasing temperature and increased with increasing strain rate. Between 600 and 1090 C, the ductility showed a slight increase with increasing temperature. Within the scatter of the data, the ductility did not depend on the strain rate. The reduction in area (RA), on the other hand, decreased with increasing strain rate. The YS and UTS values did not differ significantly for the longitudinal and transverse specimens. The ductility and RA values of the transverse specimens were marginally lower than those of the longitudinal specimens.

  14. Surface plasmon sensing of gas phase contaminants using optical...

    Office of Scientific and Technical Information (OSTI)

    Sponsoring Org: USDOE Country of Publication: United States Language: English Subject: 72 ... RESONANCE; SENSITIVITY; SIMULATION; TESTING Optical resonance.; Surface Plasmon ...

  15. Net Test

    Energy Science and Technology Software Center (OSTI)

    2001-09-01

    Nettest is a secure, real-time network utility. The nettest framework is designed to incorporate existing and new network tests, and be run as a daemon or an interactive process. Requests for network tests are received via a SSL connection or the user interface and are authorized using a ACL list (in the future authorization using Akenti will also be supported). For tests that require coordination between the two ends of the test, Nettest establishes anmore » SSL connection to accomplish this coordination. A test between two remote computers can be requested via the user interlace if the Nettest daemon is running on both remote machines and the user is authorized. Authorization for the test is through a chain of trust estabtished by the nettest daemons. Nettest is responsible for determining if the test request is authorized, but it does nothing further to secure the test once the test is running. Currently the Nettest framework incorporates lperf-vl.2, a simple ping type test, and a tuned TCP test that uses a given required throughput and ping results to determine the round trip time to set a buffer size (based on the delay bandwidth product) and then performs an iperf TCP throughput test. Additional network test tools can be integrated into the Nettest framework in the future.« less

  16. Assessment of the integrity of spent fuel assemblies used in dry storage demonstrations at the Nevada Test Site

    SciTech Connect (OSTI)

    Johnson, A.B. Jr.; Dobbins, J.C.; Zaloudek, F.R.

    1987-07-01

    This report summarizes the histories of 17 Zircaloy-clad spent fuel assemblies used in dry storage tests and demonstrations at the Engine Maintenance and Disassembly (EMAD) and Climax facilities at the Nevada Test Site (NTS). The 18th assembly was shipped to the Battelle Columbus Laboratory (BCL) and remained there for extensive characterization and as a source of specimens for whole-rod and rod-segment dry storage tests. The report traces the history of the assemblies after discharge from the Turkey Point Unit 3 pressurized-water reactor (1975 and 1977) through shipment (first arrival at EMAD in December 1978), dry storage tests and demonstrations, and shipment by truck cask from EMAD to the Idaho National Engineering Laboratory (INEL) in May/June 1986. The principal objectives of this report are to assess and document the integrity of the fuel during the extensive dry storage activities at NTS and BCL, and to briefly summarize the dry storage technologies and procedures demonstrated in this program. The dry storage tests and demonstrations involved the following concepts and facilities: (1) surface drywells (EMAD); (2) deep drywells (425 m underground in the Climax granite formation); (3) concrete silo (EMAD); (4) air-cooled vault (EMAD); (5) electrically-heated module for fuel assembly thermal calibration and testing (EMAD/FAITM). 20 refs., 43 figs., 9 tabs.

  17. Reversible Bending Fatigue Testing on Zry-4 Surrogate Rods

    SciTech Connect (OSTI)

    Wang, Jy-An John; Wang, Hong; Bevard, Bruce Balkcom; Howard, Rob L

    2014-01-01

    Testing high-burnup spent nuclear fuel (SNF) presents many challenges in areas such as specimen preparation, specimen installation, mechanical loading, load control, measurements, data acquisition, and specimen disposal because these tasks are complicated by the radioactivity of the test specimens. Research and comparison studies conducted at Oak Ridge National Laboratory (ORNL) resulted in a new concept in 2010 for a U-frame testing setup on which to perform hot-cell reversible bending fatigue testing. Subsequently, the three-dimensional finite element analysis and the engineering design of components were completed. In 2013 the ORNL team finalized the upgrade of the U-frame testing setup and the integration of the U-frame setup into a Bose dual linear motor test bench to develop a cyclic integrated reversible-bending fatigue tester (CIRFT). A final check was conducted on the CIRFT test system in August 2013, and the CIRFT was installed in the hot cell in September 2013 to evaluate both the static and dynamic mechanical response of SNF rods under simulated loads. The fatigue responses of Zircaloy-4 (Zry-4) cladding and the role of pellet pellet and pellet clad interactions are critical to SNF vibration integrity, but such data are not available due to the unavailability of an effective testing system. While the deployment of the developed CIRFT test system in a hot cell will provide the opportunity to generate the data, the use of a surrogate rod has proven quite effective in identifying the underlying deformation mechanism of an SNF composite rod under an equivalent loading condition. This paper presents the experimental results of using surrogate rods under CIRFT reversible cyclic loading. Specifically, monotonic and cyclic bending tests were conducted on surrogate rods made of a Zry-4 tube and alumina pellet inserts, both with and without an epoxy bond.

  18. Vehicle brake testing system

    DOE Patents [OSTI]

    Stevens, Samuel S.; Hodgson, Jeffrey W.

    2002-11-19

    This invention relates to a force measuring system capable of measuring forces associated with vehicle braking and of evaluating braking performance. The disclosure concerns an invention which comprises a first row of linearly aligned plates, a force bearing surface extending beneath and beside the plates, vertically oriented links and horizontally oriented links connecting each plate to a force bearing surface, a force measuring device in each link, a transducer coupled to each force measuring device, and a computing device coupled to receive an output signal from the transducer indicative of measured force in each force measuring device. The present invention may be used for testing vehicle brake systems.

  19. Impact of Dynamic Specimen Shape Evolution on the Atom Probe Tomography Results of Doped Epitaxial Oxide Multilayers: Comparison of Experiment and Simulation

    SciTech Connect (OSTI)

    Madaan, Nitesh; Bao, Jie; Nandasiri, Manjula I.; Xu, Zhijie; Thevuthasan, Suntharampillai; Devaraj, Arun

    2015-08-31

    The experimental atom probe tomography results from two different specimen orientations (top-down and side-ways) of a high oxygen ion conducting Samaria-doped-ceria/Scandia-stabilized-zirconia multilayer thin film solid oxide fuel cell electrolyte was correlated with level-set method based field evaporation simulations for the same specimen orientations. This experiment-theory correlation explains the dynamic specimen shape evolution and ion trajectory aberrations that can induce density artifacts in final reconstruction leading to inaccurate estimation of interfacial intermixing. This study highlights the need and importance of correlating experimental results with field evaporation simulations when using atom probe tomography for studying oxide heterostructure interfaces.

  20. Laser heterodyne surface profiler

    DOE Patents [OSTI]

    Sommargren, Gary E. (Livermore, CA)

    1982-01-01

    A method and apparatus is disclosed for testing the deviation of the face of an object from a flat smooth surface using a beam of coherent light of two plane-polarized components, one of a frequency constantly greater than the other by a fixed amount to produce a difference frequency with a constant phase to be used as a reference. The beam also is split into its two components with the separate components directed onto spaced apart points onthe face of the object to be tested for smoothness. The object is rotated on an axis coincident with one component which is directed to the face of the object at the center which constitutes a virtual fixed point. This component also is used as a reference. The other component follows a circular track on the face of the object as the object is rotated. The two components are recombined after reflection to produce a reflected frequency difference of a phase proportional to the difference in path length which is compared with the reference phase to produce a signal proportional to the deviation of the height of the surface along the circular track with respect to the fixed point at the center.

  1. Clip gage attachment for frictionless measurement of displacement during high-temperature mechanical testing

    DOE Patents [OSTI]

    Alexander, D.J.

    1994-01-04

    An attachment for placement between a test specimen and a remote clip gage extensometer providing improved fracture toughness tests of materials at elevated temperature is described. Using a cylindrical tube and axial rod in new relationship, the device transfers the displacement signal of the fracture toughness test specimen directly to a clip gage extensometer located outside the high temperature furnace. Virtually frictionless operation is assured by having the test specimen center one end of the rod in one end of the tube, while the clip gage extensometer arms center the other end of the rod in the other end of the tube. By providing positive control over both ends of both rod and tube, the attachment may be operated in orientations other than vertical. 1 figure.

  2. Clip gage attachment for frictionless measurement of displacement during high-temperature mechanical testing

    DOE Patents [OSTI]

    Alexander, David J.

    1994-01-01

    An attachment for placement between a test specimen and a remote clip gage extensometer providing improved fracture toughness tests of materials at elevated temperature. Using a cylindrical tube and axial rod in new relationship, the device transfers the displacement signal of the fracture toughness test specimen directly to a clip gage extensometer located outside the high temperature furnace. Virtually frictionless operation is assured by having the test specimen center one end of the rod in one end of the tube, while the clip gage extensometer arms center the other end of the rod in the other end of the tube. By providing positive control over both ends of both rod and tube, the attachment may be operated in orientations other than vertical.

  3. Laser heterodyne surface profiler

    DOE Patents [OSTI]

    Sommargren, G.E.

    1980-06-16

    A method and apparatus are disclosed for testing the deviation of the face of an object from a flat smooth surface using a beam of coherent light of two plane-polarized components, one of a frequency constantly greater than the other by a fixed amount to produce a difference frequency with a constant phase to be used as a reference, and splitting the beam into its two components. The separate components are directed onto spaced apart points on the face of the object to be tested for smoothness while the face of the object is rotated on an axis normal to one point, thereby passing the other component over a circular track on the face of the object. The two components are recombined after reflection to produce a reflected frequency difference of a phase proportional to the difference in path length of one component reflected from one point to the other component reflected from the other point. The phase of the reflected frequency difference is compared with the reference phase to produce a signal proportional to the deviation of the height of the surface along the circular track with respect to the fixed point at the center, thereby to produce a signal that is plotted as a profile of the surface along the circular track. The phase detector includes a quarter-wave plate to convert the components of the reference beam into circularly polarized components, a half-wave plate to shift the phase of the circularly polarized components, and a polarizer to produce a signal of a shifted phase for comparison with the phase of the frequency difference of the reflected components detected through a second polarizer. Rotation of the half-wave plate can be used for phase adjustment over a full 360/sup 0/ range.

  4. Crane Test

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Crane Safety Test Instructions: All Training and Testing Material is for LSU CAMD Users ONLY! Please enter your personal information in the spaces below. A minimum passing score is 80% (8 out of 10) This test can only be taken once in a thirty day period. All fields are required to be filled in. Login: Login First Name: Last Name: Phone Number: Contact: 1. The first thing you should do when using the crane is to: a. verify the battery power on the remote control. b. drag the load to the desired

  5. Impact Testing of Stainless Steel Material at Cold Temperatures

    SciTech Connect (OSTI)

    Spencer D. Snow; D. Keith Morton; Robert K. Blandford

    2008-07-01

    Stainless steels are used for the construction of numerous spent nuclear fuel or radioactive material containers that may be subjected to high strains and moderate strain rates during accidental drop events. Mechanical characteristics of these base materials and their welds under dynamic loads in the strain rate range of concern are not well documented. However, a previous paper [1] reported on impact testing and analysis results performed at the Idaho National Laboratory using 304/304L and 316/316L stainless steel base material specimens at room and elevated temperatures. The goal of the work presented herein is to add recently completed impact tensile testing results at -20 degrees F conditions for dual-marked 304/304L and 316/316L stainless steel material specimens (hereafter referred to as 304L and 316L, respectively). Recently completed welded material impact testing at -20 degrees F, room, 300 degrees F, and 600 degrees F is also reported. Utilizing a drop-weight impact test machine and 1/4-inch to 1/2-inch thick dog-bone shaped test specimens, the impact tests achieved strain rates in the 4 to 40 per second range, depending upon the material temperature. Elevated true stress-strain curves for these materials reflecting varying strain rates and temperatures are presented herein.

  6. Experimental Testing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Testing - Sandia Energy Energy Search Icon Sandia Home Locations Contact Us Employee Locator Energy & Climate Secure & Sustainable Energy Future Stationary Power Energy Conversion Efficiency Solar Energy Wind Energy Water Power Supercritical CO2 Geothermal Natural Gas Safety, Security & Resilience of the Energy Infrastructure Energy Storage Nuclear Power & Engineering Grid Modernization Battery Testing Nuclear Energy Defense Waste Management Programs Advanced Nuclear Energy

  7. Mechanical Testing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Testing - Sandia Energy Energy Search Icon Sandia Home Locations Contact Us Employee Locator Energy & Climate Secure & Sustainable Energy Future Stationary Power Energy Conversion Efficiency Solar Energy Wind Energy Water Power Supercritical CO2 Geothermal Natural Gas Safety, Security & Resilience of the Energy Infrastructure Energy Storage Nuclear Power & Engineering Grid Modernization Battery Testing Nuclear Energy Defense Waste Management Programs Advanced Nuclear Energy

  8. ADAPTATION OF CRACK GROWTH DETECTION TECHNIQUES TO US MATERIAL TEST REACTORS

    SciTech Connect (OSTI)

    A. Joseph Palmer; Sebastien P. Teysseyre; Kurt L. Davis; Gordon Kohse; Yakov Ostrovsky; David M. Carpenter; Joy L. Rempe

    2015-04-01

    A key component in evaluating the ability of Light Water Reactors to operate beyond 60 years is characterizing the degradation of materials exposed to radiation and various water chemistries. Of particular concern is the response of reactor materials to Irradiation Assisted Stress Corrosion Cracking (IASCC). Some test reactors outside the United States, such as the Halden Boiling Water Reactor (HBWR), have developed techniques to measure crack growth propagation during irradiation. The basic approach is to use a custom-designed compact loading mechanism to stress the specimen during irradiation, while the crack in the specimen is monitored in-situ using the Direct Current Potential Drop (DCPD) method. In 2012 the US Department of Energy commissioned the Idaho National Laboratory and the MIT Nuclear Reactor Laboratory (MIT NRL) to take the basic concepts developed at the HBWR and adapt them to a test rig capable of conducting in-pile IASCC tests in US Material Test Reactors. The first two and half years of the project consisted of designing and testing the loader mechanism, testing individual components of the in-pile rig and electronic support equipment, and autoclave testing of the rig design prior to insertion in the MIT Reactor. The load was applied to the specimen by means of a scissor like mechanism, actuated by a miniature metal bellows driven by pneumatic pressure and sized to fit within the small in-core irradiation volume. In addition to the loader design, technical challenges included developing robust connections to the specimen for the applied current and voltage measurements, appropriate ceramic insulating materials that can endure the LWR environment, dealing with the high electromagnetic noise environment of a reactor core at full power, and accommodating material property changes in the specimen, due primarily to fast neutron damage, which change the specimen resistance without additional crack growth. The project culminated with an in

  9. Methodology for Mechanical Property Testing of Fuel Cladding Using a Expanded Plug Wedge Test

    SciTech Connect (OSTI)

    Jiang, Hao; Wang, Jy-An John

    2014-01-01

    An expanded plug method was developed earlier for determining the tensile properties of irradiated fuel cladding. This method tests fuel rod cladding ductility by utilizing an expandable plug to radially stretch a small ring of irradiated cladding material. The circumferential or hoop strain is determined from the measured diametrical expansion of the ring. A developed procedure is used to convert the load circumferential strain data from the ring tests into material pseudo-stress-strain curves, from which material properties of the cladding can be extracted. However, several deficiencies existed in this expanded-plug test that can impact the accuracy of test results, such as that the large axial compressive stress resulted from the expansion plug test can potentially induce the shear failure mode of the tested specimen. Moreover, highly nonuniform stress and strain distribution in the deformed clad gage section and significant compressive stresses, induced by bending deformation due to clad bulging effect, will further result in highly nonconservative estimates of the mechanical properties for both strength and ductility of the tested clad. To overcome the aforementioned deficiencies associated with the current expansion plug test, systematic studies have been conducted. By optimizing the specific geometry designs, selecting the appropriate material for the expansion plug, and adding new components into the testing system, a modified expansion plug testing protocol has been developed. A general procedure was also developed to determine the hoop stress in the tested ring specimen. A scaling factor, -factor, was used to convert the ring load Fring into hoop stress , and is written as _ = F_ring/tl , where t is the clad thickness and l is the clad length. The generated stress-strain curve agrees well with the associated tensile test data in both elastic and plastic deformation regions.

  10. Testing and inspecting lens by holographic means

    DOE Patents [OSTI]

    Hildebrand, Bernard P.

    1976-01-01

    Processes for the accurate, rapid and inexpensive testing and inspecting of oncave and convex lens surfaces through holographic means requiring no beamsplitters, mirrors or overpower optics, and wherein a hologram formed in accordance with one aspect of the invention contains the entire interferometer and serves as both a master and illuminating source for both concave and said convex surfaces to be so tested.

  11. Lens testing using total internal reflection holography

    DOE Patents [OSTI]

    Hildebrand, Bernard P.

    1976-12-14

    Accurate, rapid and inexpensive testing and inspecting of lens surfaces tugh holographic means requiring no beamsplitters, mirrors or overpower optics, and wherein a hologram formed in accordance with one aspect of the invention contains the entire interferometer and serves as both a master and illuminating source for both concave and convex surfaces to be so tested.

  12. Materials tests in support of an MHD (magnetohydrodynamic) coal combustor

    SciTech Connect (OSTI)

    Natesan, K.; Wang, D.Y.; Soppet, W.K.

    1989-11-01

    Corrosion tests were conducted to evaluate the compatibility of candidate alloys in simulated fireside and high-temperature, high- pressure waterside environments of slagging magnetohydrodynamic combustors. The fireside tests were conducted with uncoated specimens and specimens covered with deposit layers of slag or a mixture of slag and seed for as long as 750 h at 600 and 800{degree}F. The waterside corrosion tests were conducted at 450{degree}F in a high-pressure autoclave in which water with two different chemistries was used. Detailed results on the scaling kinetics are presented and the data are used to analyze the material options for different locations in the combustor system. 10 refs., 25 figs., 13 tabs.

  13. Rapid heating tensile tests of hydrogen-charged high-energy-rate-forged 316L stainless steel

    SciTech Connect (OSTI)

    Mosley, W.C.

    1989-05-19

    316L stainless steel is a candidate material for construction of equipment that will be exposed to tritium. Proper design of the equipment will require an understanding of how tritium and its decay product helium affect mechanical properties. This memorandum describes results of rapid heating tensile testing of hydrogen-charged specimens of high-energy-rate-forged (HERF) 316L stainless steel. These results provide a data base for comparison with uncharged and tritium-charged-and-aged specimens to distinguish the effects of hydrogen and helium. Details of the experimental equipment and procedures and results for uncharged specimens were reported previously. 3 refs., 10 figs.

  14. Surface rheology and interface stability.

    SciTech Connect (OSTI)

    Yaklin, Melissa A.; Cote, Raymond O.; Moffat, Harry K.; Grillet, Anne Mary; Walker, Lynn; Koehler, Timothy P.; Reichert, Matthew D.; Castaneda, Jaime N.; Mondy, Lisa Ann; Brooks, Carlton, F.

    2010-11-01

    We have developed a mature laboratory at Sandia to measure interfacial rheology, using a combination of home-built, commercially available, and customized commercial tools. An Interfacial Shear Rheometer (KSV ISR-400) was modified and the software improved to increase sensitivity and reliability. Another shear rheometer, a TA Instruments AR-G2, was equipped with a du Nouey ring, bicone geometry, and a double wall ring. These interfacial attachments were compared to each other and to the ISR. The best results with the AR-G2 were obtained with the du Nouey ring. A Micro-Interfacial Rheometer (MIR) was developed in house to obtain the much higher sensitivity given by a smaller probe. However, it was found to be difficult to apply this technique for highly elastic surfaces. Interfaces also exhibit dilatational rheology when the interface changes area, such as occurs when bubbles grow or shrink. To measure this rheological response we developed a Surface Dilatational Rheometer (SDR), in which changes in surface tension with surface area are measured during the oscillation of the volume of a pendant drop or bubble. All instruments were tested with various surfactant solutions to determine the limitations of each. In addition, foaming capability and foam stability were tested and compared with the rheology data. It was found that there was no clear correlation of surface rheology with foaming/defoaming with different types of surfactants, but, within a family of surfactants, rheology could predict the foam stability. Diffusion of surfactants to the interface and the behavior of polyelectrolytes were two subjects studied with the new equipment. Finally, surface rheological terms were added to a finite element Navier-Stokes solver and preliminary testing of the code completed. Recommendations for improved implementation were given. When completed we plan to use the computations to better interpret the experimental data and account for the effects of the underlying bulk

  15. Laser heterodyne surface profiler

    DOE Patents [OSTI]

    Sommargren, Gary E. (Livermore, CA)

    1984-01-01

    Method and apparatus for testing the deviation of the face of an object from a flat smooth surface using a laser beam having two plane-polarized components, one of a frequency greater than the other to produce a difference frequency with a phase to be used as a reference. The beam also is split into its two components which are directed onto spaced apart points on the face of the object. The object is rotated on an axis coincident with one component as a reference. The other component follows a circular track on the face of the object as the object is rotated. The two components are recombined after reflection to produce a difference frequency having a phase that is shifted in an amount that is proportional to the difference in path length as compared to the reference phase to produce an electrical output signal proportional to the deviation of the height of the surface along the circular track. The output signal is generated by means of a phase detector that includes a first photodetector in the path of the recombined components and a second photodetector in the path of the reference phase. The output signal is dependent on the phase difference of the two photodetector signals. A polarizer, a quarter-wave plate and a half-wave plate are in series in the path of the reference phase. Rotation of the half-wave plate can be used for phase adjustment over a full 360.degree. range for initial calibration of the apparatus.

  16. Sweet Surface Area

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Sweet Surface Area Sweet Surface Area Create a delicious root beer float and learn sophisticated science concepts at the same time. Sweet Surface Area Science is all around us, so ...

  17. Microgrid Testing

    SciTech Connect (OSTI)

    Shirazi, M.; Kroposki, B.

    2012-01-01

    With the publication of IEEE 1574.4 Guide for Design, Operation, and Integration of Distributed Resource Island Systems with Electric Power Systems, there is an increasing amount of attention on not only the design and operations of microgrids, but also on the proper operation and testing of these systems. This standard provides alternative approaches and good practices for the design, operation, and integration of microgrids. This includes the ability to separate from and reconnect to part of the utility grid while providing power to the islanded power system. This presentation addresses the industry need to develop standardized testing and evaluation procedures for microgrids in order to assure quality operation in the grid connected and islanded modes of operation.

  18. Progress Letter Report on Bending Fatigue Test System Development for Spent Nuclear Fuel Vibration Integrity Study (Out-of-cell fatigue testing development - Task 2.4)

    SciTech Connect (OSTI)

    Wang, Jy-An John; Wang, Hong; Cox, Thomas S; Baldwin, Charles A; Bevard, Bruce Balkcom

    2013-08-01

    Vibration integrity of high burn-up spent nuclear fuel in transportation remains to be a critical component of US nuclear waste management system. The structural evaluation of package for spent fuel transportation eventually will need to see if the content or spent fuel is in a subcritical condition. However, a system for testing and characterizing such spent fuel is still lacking mainly due to the complication involved with dealing radioactive specimens in a hot cell environment. Apparently, the current state-of-the-art in spent fuel research and development is quite far away from the delivery of reliable mechanical property data for the assessment of spent fuels in the transport package evaluation. Under the sponsorship of US NRC, ORNL has taken the challenge in developing a robust testing system for spent fuel in hot cell. An extensive literature survey was carried out and unique requirements of such testing system were identified. The U-frame setup has come to the top among various designs examined for reverse bending fatigue test of spent fuel rod. The U-frame has many features that deserve mentioned here: Easy to install spent fuel rod in test; Less linkages than in conventional bending test setup such as three-point or four-point bending; Target the failure mode relevant to the fracture of spent fuel rod in transportation by focusing on pure bending; The continuous calibrations and modifications resulted in the third generation (3G) U-frame testing setup. Rigid arms are split along the LBB axis at rod sample ends. For each arm, this results in a large arm body and an end piece. Mating halves of bushings were modified into two V-shaped surfaces on which linear roller bearings (LRB) are embedded. The rod specimen is installed into the test fixture through opening and closing slide end-pieces. The 3G apparently has addressed major issues of setup identified in the previous stage and been proven to be eligible to be further pursued in this project. On the other

  19. Evaluation of test methods for dynamic toughness characterization of duplex stainless steel forgings

    SciTech Connect (OSTI)

    Natishan, M.E.; Tregoning, R.L.

    1995-12-31

    Ferralium is a dual-phase stainless steel which consists of roughly equal amounts of ferrite and austenite. Conventional Charpy V-notch impact tests were performed on specimens taken from several locations in three orientations from a forged Ferralium plate to quantify the materials dynamic fracture performance. The Charpy tests were compared with 2.54 cm thick (1T) single edge bend (SE(B)) specimens that were tested in a drop tower to measure dynamic fracture initiation toughness (K{sub Id}). SE(B) specimens were removed from three plate locations and tested in a single orientation. Charpy and K{sub Id} tests were performed over the entire fracture mode transition temperature range, but the bulk of testing was concentrated at a single temperature {minus}2 C to provide a statistically significant number of tests at a representative point in the ferritic fracture mode transition region. Charpy impact energy varied consistently with both orientation and location within the forged plate even though large scatter was present in the results. This large scatter precluded an accurate assessment of the materials fracture performance within the transition region. The scatter in the drop tower (SE(B)) results was much less and indicated that plate location had a minimal affect on performance. The reduced scatter in the SE(B) specimens is attributed to two factors. First, the microstructure of Ferralium, while macroscopically homogeneous, contains ferritic and austenitic phase sizes that approach the dimensions of the standard Charpy specimen. Second, the Charpy testing technique causes more variation than the standard SE(B) K{sub Id} tests within the transition region.

  20. Long-term materials test program. Quarterly report, January-March 1983

    SciTech Connect (OSTI)

    1984-03-01

    Exposure of gas turbine materials to a PFBC effluent under the Long-Term Materials Test Program has reached 1507 hours. Unprotected nickel and cobalt base blade and vane alloys show susceptibility to hot corrosion at 1500/sup 0/F (gas temperature), 1300/sup 0/F, and 1100/sup 0/F (air-cooled pins). Precious metal aluminide and M (Co,Fe) CrAlY overlay coatings continue to show good resistance to corrosion above 1450/sup 0/F, but are susceptible to varying degrees of pitting attack between 1050 and 1300/sup 0/F. Significant erosion/corrosion degradation of both base alloys and protective coatings/claddings has been observed on airfoil specimens exposed at 1350/sup 0/F, 800 to 900 fps and dust loadings less than 100 ppM for 1085 hours. Corrosion predominately occurred in areas of direct particle impaction; i.e., leading edge and pressure surface, indicating an erosion/corrosion synergism. At gas velocities of 1200 to 1400 fps, a platinum-aluminide coated IN-738 pin experienced a metal recession rate of 8 mils/1000-hours. The PFBC facility continues to show excellent operational reliability, accumulating over 1100 test hours this quarter. The only concern from an operations standpoint is the gradual thinning of the in-bed heat exchanger tubing at a rate of about 5 mils/100 hours off the diameter.

  1. Low Temperature Waste Immobilization Testing Vol. I

    SciTech Connect (OSTI)

    Russell, Renee L.; Schweiger, Michael J.; Westsik, Joseph H.; Hrma, Pavel R.; Smith, D. E.; Gallegos, Autumn B.; Telander, Monty R.; Pitman, Stan G.

    2006-09-14

    The Pacific Northwest National Laboratory (PNNL) is evaluating low-temperature technologies to immobilize mixed radioactive and hazardous waste. Three waste formsalkali-aluminosilicate hydroceramic cement, Ceramicrete phosphate-bonded ceramic, and DuraLith alkali-aluminosilicate geopolymerwere selected through a competitive solicitation for fabrication and characterization of waste-form properties. The three contractors prepared their respective waste forms using simulants of a Hanford secondary waste and Idaho sodium bearing waste provided by PNNL and characterized their waste forms with respect to the Toxicity Characteristic Leaching Procedure (TCLP) and compressive strength. The contractors sent specimens to PNNL, and PNNL then conducted durability (American National Standards Institute/American Nuclear Society [ANSI/ANS] 16.1 Leachability Index [LI] and modified Product Consistency Test [PCT]) and compressive strength testing (both irradiated and as-received samples). This report presents the results of these characterization tests.

  2. Assembly for testing weldability of sheet metal

    DOE Patents [OSTI]

    David, Stan A.; Woodhouse, John J.

    1985-01-01

    A test assembly for determining the weldability of sheet metal includes (1) a base having a flat side surface with an annular groove in the side surface, a counterbore being formed in the outer wall of the groove and the surface portion of the base circumscribed by the inner wall of the groove being substantially coplanar with the bottom of the counterbore, (2) a test disk of sheet metal the periphery of which is positioned in the counterbore and the outer surface of which is coplanar with one side of the base, and (3) a clamp ring overlying the side surface of the base and the edge portion of the test disk and a plurality of clamp screws which extend through the clamp ring for holding the periphery of the test disk against the bottom of the counterbore.

  3. Assembly for testing weldability of sheet metal

    SciTech Connect (OSTI)

    David, S.A.; Woodhouse, J.J.

    1985-02-19

    A test assembly for determining the weldability of sheet metal includes a base having a flat side surface with an annular groove in the side surface, a counterbore being formed in the outer wall of the groove and the surface portion of the base circumscribed by the inner wall of the groove being substantially coplanar with the bottom of the counterbore, a test disk of sheet metal the periphery of which is positioned in the counterbore and the outer surface of which is coplanar with one side of the base, and a clamp ring overlying the side surface of the base and the edge portion of the test disk and a plurality of clamp screws which extend through the clamp ring for holding the periphery of the test disk against the bottom of the counterbore.

  4. Preparation of actinide specimens for the US/UK joint experiment in the Dounreay Prototype Fast Reactor

    SciTech Connect (OSTI)

    Quinby, T C; Adair, H L; Kobisk, E H

    1982-05-01

    A joint research program involving the United States and the United Kingdom was initiated about four years ago for the purpose of studying the fuel behavior of higher actinides using in-core irradiation in the fast reactor at Dounreay, Scotland. Simultaneously, determination of integral cross sections of a wide variety of higher actinide isotopes (physics specimens) was proposed. Coincidental neutron flux and energy spectral measurements were to be made using vanadium encapsulated dosimetry materials in the immediate region of the fuel pellets and physics samples. The higher actinide samples chosen for the fuel study were /sup 241/Am and /sup 244/Cm in the forms of Am/sub 2/O/sub 3/, Cm/sub 2/O/sub 3/, and Am/sub 6/Cm(RE)/sub 7/O/sub 21/, where (RE) represents a mixture of lanthanides. Milligram quantities of actinide oxides of /sup 248/Cm, /sup 246/Cm, /sup 244/Cm, /sup 243/Cm, /sup 243/Am, /sup 241/Am, /sup 244/Pu, /sup 242/Pu, /sup 241/Pu, /sup 240/Pu, /sup 239/Pu, /sup 238/Pu, /sup 237/Np, /sup 238/U, /sup 236/U, /sup 235/U, /sup 234/U, /sup 233/U, /sup 232/Th, /sup 230/Th, and /sup 231/Pa were encapsulated to obtain nuclear cross section and reaction rate data for these materials.

  5. Surface Water Sampling At Chena Geothermal Area (Waring, Et Al...

    Open Energy Info (EERE)

    calcium and magnesium concentrations were measured, with elevated levels of silica and sulfate. Surface fumarole gases were tested with a flame to indicate carbon dioxide...

  6. United States Naval Surface Warfare Center | Open Energy Information

    Open Energy Info (EERE)

    Warfare Center Jump to: navigation, search Hydro | Hydrodynamic Testing Facilities Name United States Naval Surface Warfare Center Address Carderock, 9500 MacArthur Boulevard...

  7. Tension bending ratcheting tests of 304 stainless steel

    SciTech Connect (OSTI)

    Larson, L.D.; Jones, D.P.; Rapp, D.G.

    1996-12-31

    This paper discusses results of an experimental program conducted to investigate the strain ratcheting behavior of 304 stainless steel under various combinations of applied membrane load and displacement controlled cyclic bending strain. Tests were performed on uniaxial specimens at temperatures of 70 F (21 C) and 550 F (288 C). Bending strain, ratchet strain and axial displacement of the specimens were monitored throughout the tests. Membrane stress to monotonic yield stress ratios of 2/3, 1/2, and 1/3 were tested with pseudo-elastic bending stress to yield stress ratios ranging from 1.4 to 10.7. Test output was in the form of plots of cumulative axial membrane strain versus cycles up to the point of shakedown, i.e., the point at which no additional progressive strain was observed. Shakedown was demonstrated in the 500 F tests but not the room temperature tests. The 550 F results are shown in terms of shakedown membrane strain versus equivalent bending stress ratio for each of the tested membrane stress ratios. The cyclic and monotonic stress-strain curves for the test materials are presented to enable the use of various models for predicting the ratcheting and shakedown behavior. The results may be used to develop improved ratcheting and shakedown rules permitting a relaxation of the traditional ratcheting rules in the ASME Boiler and Pressure Vessel Code.

  8. Furball Explosive Breakout Test

    SciTech Connect (OSTI)

    Carroll, Joshua David

    2015-08-05

    For more than 30 years the Onionskin test has been the primary way to study the surface breakout of a detonation wave. Currently the Onionskin test allows for only a small, one dimensional, slice of the explosive in question to be observed. Asymmetrical features are not observable with the Onionskin test and its one dimensional view. As a result, in 2011, preliminary designs for the Hairball and Furball were developed then tested. The Hairball used shorting pins connected to an oscilloscope to determine the arrival time at 24 discrete points. This limited number of data points, caused by the limited number of oscilloscope channels, ultimately led to the Hairball’s demise. Following this, the Furball was developed to increase the number of data points collected. Instead of shorting pins the Furball uses fiber optics imaged by a streak camera to determine the detonation wave arrival time for each point. The original design was able to capture the detonation wave’s arrival time at 205 discrete points with the ability to increase the number of data points if necessary.

  9. Laser heterodyne surface profiler

    DOE Patents [OSTI]

    Sommargren, G.E.

    1984-06-26

    Method and apparatus are disclosed for testing the deviation of the face of an object from a flat smooth surface using a laser beam having two plane-polarized components, one of a frequency greater than the other to produce a difference frequency with a phase to be used as a reference. The beam also is split into its two components which are directed onto spaced apart points on the face of the object. The object is rotated on an axis coincident with one component as a reference. The other component follows a circular track on the face of the object as the object is rotated. The two components are recombined after reflection to produce a difference frequency having a phase that is shifted in an amount that is proportional to the difference in path length as compared to the reference phase to produce an electrical output signal proportional to the deviation of the height of the surface along the circular track. The output signal is generated by means of a phase detector that includes a first photodetector in the path of the recombined components and a second photodetector in the path of the reference phase. The output signal is dependent on the phase difference of the two photodetector signals. A polarizer, a quarter-wave plate and a half-wave plate are in series in the path of the reference phase. Rotation of the half-wave plate can be used for phase adjustment over a full 360[degree] range for initial calibration of the apparatus. 12 figs.

  10. LONG-TERM CORROSION TESTING OF CANDIDATE MATERIALS FOR HIGH-LEVEL RADIOACTIVE WASTE CONTAINMENT

    SciTech Connect (OSTI)

    Estill, J. C.; Doughty, S.; Gdowski, G. E.; Gordon, S.; King, K.; McCright, R. D.; Wang, F.

    1997-10-01

    Preliminary results are presented from the long-term corrosion test program of candidate materials for the high-level radioactive waste packages that would be emplaced in the potential repository at Yucca Mountain, Nevada. The present waste package design is based on a multi-barrier concept having an inner container of a corrosion resistant material and an outer container of a corrosion allowance material. Test specimens have been exposed to simulated bounding environments that may credibly develop in the vicinity of the waste packages. Corrosion rates have been calculated for weight loss and crevice specimens, and U-bend specimens have been examined for evidence of stress corrosion cracking (SCC). Galvanic testing has been started recently and initial results are forthcoming. Pitting characterization of test specimens will be conducted in the coming year. This test program is expected to continue for a minimum of five years so that long-term corrosion data can be determined to support corrosion model development, performance assessment, and waste package design.