National Library of Energy BETA

Sample records for mil thou dol

  1. VPP Interagency Agreement Between DOE and DOL

    Broader source: Energy.gov [DOE]

    The purpose of thia agreement ie for the U. S. Department Of Labor's (DOL) Occupational Safety and Health Administration (OSHA) Directorate of Federal-State Operation8 (FSO) to provide aeeistance to the U. S. Department of Energy’s (DOE) Office of Occupational safety (EH-31) in the development bf the DOE Voluntary Protection Program (DOE-WP) at Government-~ned-or-LeaBed Contractor-Operated (GOCO) facilities.

  2. DOL: Role in EEOICPA – Part B and Part E

    Broader source: Energy.gov [DOE]

    DOL is tasked with administering the EEOICPA, both Parts B and E. Part B covers current and former workers who have been diagnosed with cancer, chronic beryllium disease, beryllium sensitivity, or...

  3. 1 mil gold bond wire study.

    SciTech Connect (OSTI)

    Huff, Johnathon; McLean, Michael B.; Jenkins, Mark W.; Rutherford, Brian Milne

    2013-05-01

    In microcircuit fabrication, the diameter and length of a bond wire have been shown to both affect the current versus fusing time ratio of a bond wire as well as the gap length of the fused wire. This study investigated the impact of current level on the time-to-open and gap length of 1 mil by 60 mil gold bond wires. During the experiments, constant current was provided for a control set of bond wires for 250ms, 410ms and until the wire fused; non-destructively pull-tested wires for 250ms; and notched wires. The key findings were that as the current increases, the gap length increases and 73% of the bond wires will fuse at 1.8A, and 100% of the wires fuse at 1.9A within 60ms. Due to the limited scope of experiments and limited data analyzed, further investigation is encouraged to confirm these observations.

  4. Experimentally Determined Coordinates for Three MILS Hydrophones Near Ascension Island

    SciTech Connect (OSTI)

    Harben, P. E.; Hollfelder, J. R.; Rodgers, A. J.

    1999-11-19

    We conducted an airgun survey in the waters of Ascension Island in May 1999 to determine new locations and depths for three Missile Impact Location System (MILS) hydrophones (ASC23, ASC24, and ASC26) currently in use by the Prototype International Data Center (PIDC) and the National Data Center (NDC). The nominal and new locations are summarized in Table 1. Although not rigorous, errors in the new locations and depths are conservatively estimated to be less than 100 m. The hydrophones are either on or near the ocean bottom in all three cases. The new depths are consistent with the following: Direct-phase airgun arrivals; Bathymetry determined along the track of the ship used for this airgun survey; Reflected phases from the airgun data; and Depths given in the original hydrophone installation report.

  5. Bivalent metal-based MIL-53 analogues: Synthesis, properties and application

    SciTech Connect (OSTI)

    Liu, Yongxin; Liu, Dan; Wang, Cheng

    2015-03-15

    Trivalent metal-based MIL-53 (Al{sup 3+}, Cr{sup 3+}, Fe{sup 3+}, In{sup 3+}) compounds are interesting metal–organic frameworks (MOFs) with breathing effect and are promising gas sorption materials. Replacing bridging μ{sub 2}-OH group by neutral ligands such as pyridine N-oxide and its derivatives (PNOs), the trivalent metal-based MIL-53 analogous structures could be extended to bivalent metal systems. The introduction of PNOs and bivalent metal elements endows the frameworks with new structural features and physical and chemical properties. This minireview summarizes the recent development of bivalent metal-based MIL-53 analogues (Mn{sup 2+}, Co{sup 2+}, Ni{sup 2+}), typically, focusing on the synthetic strategies and potential applications based on our own works and literatures. We present the synthetic strategy to achieve structures evolution from single-ligand-walled to double-ligand-walled channel. Properties and application of these new materials in a wide range of potential areas are discussed including thermal stability, gas adsorption, magnetism and liquid-phase separation. Promising directions of this research field are also highlighted. - Graphical abstract: The recent development of bivalent metal-based MIL-53 analogues (Mn{sup 2+}, Co{sup 2+}, Ni{sup 2+}) on their synthetic strategies, properties and potential applications was reviewed. - Highlights: • Structure features of bivalent metal-based MIL-53 analogues are illustrated. • Important properties and application are presented. • Host–guest interactions are main impetus for liquid-phase separation. • Promising directions of bivalent metal-based MIL-53 analogues are highlighted.

  6. Experimental evidence of negative linear compressibility in the MIL-53 metal–organic framework family

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Serra-Crespo, Pablo; Dikhtiarenko, Alla; Stavitski, Eli; Juan-Alcañiz, Jana; Kapteijn, Freek; Coudert, François-Xavier; Gascon, Jorge

    2014-03-24

    Here we report a series of powder X-ray diffraction experiments performed on the soft porous crystals MIL-53(Al) and NH2-MIL-53(Al) in a diamond anvil cell under different pressurization media. Systematic refinements of the obtained powder patterns demonstrate that these materials expand along a specific direction while undergoing total volume reduction under an increasing hydrostatic pressure. The results confirm for the first time the negative linear compressibility behaviour of this family of materials, recently predicted from quantum chemical calculations.

  7. Experimental Evidence of Negative Linear Compressibility in the MIL-53 Metal-Organic Framework Family

    SciTech Connect (OSTI)

    Serra-Crespo, Pablo; Dikhtiarenko, Alla; Stavitski, Eli; Juan-Alcaniz, Jana; Kapeteijn, Freek; Coudert, Francois-Xavier; Gascon, Jorge

    2014-03-24

    Here, we report a series of powder X-ray diffraction experiments performed on the soft porous crystals MIL-53(Al) and NH2-MIL-53(Al) in a diamond anvil cell under different pressurization media. Systematic refinements of the obtained powder patterns demonstrate that these materials expand along a specific direction while undergoing total volume reduction under an increasing hydrostatic pressure. Our results confirm for the first time the negative linear compressibility behaviour of this family of materials, recently predicted from quantum chemical calculations.

  8. Experimental Evidence of Negative Linear Compressibility in the MIL-53 Metal-organic Framework Family

    SciTech Connect (OSTI)

    Serra-Crespo, Pablo; Dikhtiarenko, Alla; Stavitski, Eli; Juan-Alcaniz, Jana; Kapteijn, Freek; Coudert, Francois-Xavier; Gascon, Jorge

    2014-03-24

    Here we report a series of powder X-ray diffraction experiments performed on the soft porous crystals MIL-53(Al) and NH2-MIL-53(Al) in a diamond anvil cell under different pressurization media. Systematic refinements of the obtained powder patterns demonstrate that these materials expand along a specific direction while undergoing total volume reduction under an increasing hydrostatic pressure. Our results confirm for the first time the negative linear compressibility behaviour of this family of materials, recently predicted from quantum chemical calculations.

  9. MIL-L-87177 and CLT:X-10 Lubricants Improve Electrical Connector Fretting Corrosion Behavior

    SciTech Connect (OSTI)

    AUKLAND,NEIL R.; HANLON,JAMES T.

    1999-10-12

    We have conducted a fretting research project using MIL-L-87177 and CLT: X-10 lubricants on Nano-miniature connectors. When they were fretted without lubricant, individual connectors first exceeded our 0.5 ohm failure criteria from 2,341 to 45,238 fretting cycles. With additional fretting, their contact resistance increased to more than 100,000 ohms. Unmodified MIL-L-87177 lubricant delayed the onset of first failure to between 430,000 and over 20,000,000 fretting cycles. MIL-L-87177 modified by addition of Teflon powder delayed first failure to beyond 5 million fretting cycles. Best results were obtained when Teflon was used and also when both the straight and modified lubricants were poured into and then out of the connector. CLT: X-10 lubricant delayed the onset of first failure to beyond 55 million cycles in one test where a failure was actually observed and to beyond 20 million cycles in another that was terminated without failure. CLT: X-10 recovered an unlubricated connector driven deeply into failure, with six failed pins recovering immediately and four more recovering during an additional 420 thousand fretting cycles. MIL-L-87177 was not able to recover a connector under similar conditions.

  10. MIL-L-87177 Lubricant Bulletproofs Connectors Against Chemical and Fretting Corrosion

    SciTech Connect (OSTI)

    HANLON, JAMES T.; DE MARQUIS, VIRGINIA K.; TAYLOR, RONALD DEAN

    2002-05-01

    Electrical connectors corrode. Even our best SA and MC connectors finished with 50 to 100 microinches of gold over 50 to 100 microinches of nickel corrode. This work started because some, but not all, lots of connectors held in KC stores for a decade had been destroyed by pore corrosion (chemical corrosion). We have identified a MIL-L-87177 lubricant that absolutely stops chemical corrosion on SA connectors, even in the most severe environments. For commercial connectors which typically have thinner plating thicknesses, not only does the lubricant significantly retard effects of chemical corrosion, but also it greatly prolongs the fretting life. This report highlights the initial development history and use of the lubricant at Bell Labs and AT&T, and the Battelle studies and the USAF experience that lead to its deployment to stop dangerous connector corrosion on the F-16. We report the Sandia, HFM&T and Battelle development work, connector qualification, and material compatibility studies that demonstrate its usefulness and safety on JTA and WR systems. We will be applying MIL-L-87177 Connector Lubricant to all new connectors that go into KC stores. We recommend that it be applied to connectors on newly built cables and equipment as well as material that recycles through manufacturing locations from the field.

  11. Radiative cooling test facility and performance evaluation of 4-MIL aluminized polyvinyl fluoride and white-paint surfaces

    SciTech Connect (OSTI)

    Kruskopf, M.S.; Berdahl, P.; Martin, M.; Sakkal, F.; Sobolewski, M.

    1980-11-01

    A test facility designed to measure the amount of radiative cooling a specific material or assembly of materials will produce when exposed to the sky is described. Emphasis is placed upon assemblies which are specifically designed to produce radiative cooling and which therefore offer promise for the reduction of temperatures and/or humidities in occupied spaces. The hardware and software used to operate the facility are documented and the results of the first comprehensive experiments are presented. A microcomputer-based control/data acquisition system was employed to study the performance of two prototype radiator surfaces: 4-mil aluminized polyvinyl fluoride (PVF) and white painted surfaces set below polyethylene windscreens. The cooling rates for materials tested were determined and can be approximated by an equation (given). A computer model developed to simulate the cooling process is presented. (MCW)

  12. DOL: Office of the Ombudsman for EEOICPA

    Broader source: Energy.gov [DOE]

    The Office of the Ombudsman for the Energy Employees Occupational Illness Compensation Program is an independent office within the Department of Labor that provides assistance and information to...

  13. Property:Incentive/PVNPFitDolKWh | Open Energy Information

    Open Energy Info (EERE)

    Energy (Wisconsin Power and Light) - Advanced Renewables Tariff (Wisconsin) + 0.25 + C CPS Energy - Solartricity Producer Program (Texas) + 0.27 + N NC GreenPower Production...

  14. Property:Incentive/PVResFitDolKWh | Open Energy Information

    Open Energy Info (EERE)

    Energy (Wisconsin Power and Light) - Advanced Renewables Tariff (Wisconsin) + 0.25 + C CPS Energy - Solartricity Producer Program (Texas) + 0.27 + N NC GreenPower Production...

  15. Property:Incentive/PVComFitDolKWh | Open Energy Information

    Open Energy Info (EERE)

    Energy (Wisconsin Power and Light) - Advanced Renewables Tariff (Wisconsin) + 0.25 + C CPS Energy - Solartricity Producer Program (Texas) + 0.27 + N NC GreenPower Production...

  16. U.S. DOL @ - Employment Standards Administration Office of Workers...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    The FECA also provides for the payment of benefits to dependents if me injury or disease ... Payment for chiropractic services is limited to treatment consisting of manual ...

  17. Microsoft PowerPoint - SWDRegional 5-Yr MIL and Ranking Process...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ... Main Unit Bus andor Cable- Assess each units bus andor cable system separately. Lubricating and Insulating Oil System- Assess the pumps, purifiers, tanks, valves, piping, etc. as ...

  18. http://www.nellis.af.mil/library/factsheets/factsheet_print.asp

    National Nuclear Security Administration (NNSA)

    ... With the onset of the Korean War, the mission of LVAFB changed from an advanced single- engine school to one of training jet fighter pilots for the then Far East Air Forces. In ...

  19. https://www.justice.gov/opa/pr/lockheed-martin-agrees-pay-5-mil

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Monday, February 29, 2016 JUSTICE NEWS Department of Justice Office of Public Affairs Lockheed Martin Agrees to Pay $5 Million to Settle Alleged Violations of the False Claims Act and the Resource Conservation and Recovery Act Lockheed Martin Corporation and subsidiaries Lockheed Martin Energy Systems and Lockheed Martin Utility Services (collectively, Lockheed Martin) have agreed to pay the United States $5 million to resolve allegations that they violated the Resource Conservation and Recovery

  20. NIOSH comments to DOL on the Occupational Safety and Health Administration proposed rule on hazardous waste operations and emergency response by R. A. Lemen, December 1987

    SciTech Connect (OSTI)

    Not Available

    1987-12-01

    The testimony concerns the views of NIOSH regarding the safety or workers engaged in hazardous waste operations and emergency response. NIOSH suggests the following requirements: adequate worker training before the worker begins handling hazardous wastes; the use of site control zones and a thorough site evaluation prior to the beginning work at the site; the use of handling techniques that limit the potential for human exposure to hazardous substances; and medical surveillance of all workers potentially exposed to hazardous substances. Suggested modifications to the proposed OSHA regulation are attached and deal with the following areas: scope, application and definitions for the work; contractors and subcontractors; site characterization and analysis; site control; training; medical examinations and consultations; recordkeeping; engineering controls; personal protective equipment; informational programs; shipping and transport; decontamination; procedures for handling emergency incidents; specialist employees; and sanitation at temporary workplaces.

  1. NIOSH comments to DOL on the Occupational Safety and Health Administration proposed rule on occupational exposure to lead by R. A. Lemen, September 1, 1987

    SciTech Connect (OSTI)

    Not Available

    1987-09-01

    The testimony concerns the view of NIOSH regarding the OSHA proposed rule on occupational exposure to lead. Data in reports of air and blood analysis for lead suggest that there are highly variable concentrations of lead in air that range from more than 900 micrograms/cubic meter to levels less than the detection limits of the methods used. Blood concentrations also varied from those typical of concentrations found in the general population to levels substantially in excess of occupational standards of 60 microg/dl. A walk through survey report on air and blood lead concentrations is underway in a brass foundry. The National Occupational Exposure Survey, conducted by NIOSH, has been used to estimate the number of workers in the nine industry sectors requested by OSHA. Microfiche copies of three control technology reports on lead exposure and control in nonferrous foundries and secondary copper smelting were submitted. NIOSH is also submitting a final control technology report on a low energy battery shredder designed to reduce lead emissions.

  2. Buildings and Energy in the 1980's (TABLES)

    U.S. Energy Information Administration (EIA) Indexed Site

    in Residential Buildings, 1984 End Uses RSE Row Fac- tors All End Uses Space Heating Water Heating Air Conditioning Appliances Building Characteristics Buildings (thou- sand)...

  3. Buildings and Energy in the 1980's (TABLES)

    U.S. Energy Information Administration (EIA) Indexed Site

    in Residential Buildings, 1987 End Uses RSE Row Fac- tors All End Uses Space Heating Water Heating Air Conditioning Appliances Building Characteristics Buildings (thou- sand)...

  4. ARQ2003.03.pgm

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ... demonstration hydrogen-producing nuclear power plant. Ultimately however, to achieve the goals of Power for the Twenty-First Cen- tury, reprocessing must handle tens of thou- ...

  5. Buildings and Energy in the 1980's (TABLES)

    U.S. Energy Information Administration (EIA) Indexed Site

    1982 End Uses RSE Row Fac- tors All End Uses Space Heating Water Heating Air Conditioning Appliances Building Characteristics Buildings (thou- sand) Consump- tion...

  6. Buildings and Energy in the 1980's (TABLES)

    U.S. Energy Information Administration (EIA) Indexed Site

    1980 End Uses RSE Row Fac- tors All End Uses Space Heating Water Heating Air Conditioning Appliances Building Characteristics Buildings (thou- sand) Consump- tion...

  7. Buildings and Energy in the 1980's (TABLES)

    U.S. Energy Information Administration (EIA) Indexed Site

    1981 End Uses RSE Row Fac- tors All End Uses Space Heating Water Heating Air Conditioning Appliances Building Characteristics Buildings (thou- sand) Consump- tion...

  8. NIOSH comments to DOL on the Mine Safety and Health Administration's advance notice of proposed rulemaking on notification, investigation, reports and records of accidents, injuries, illnesses, employment and coal production in mines by R. W. Niemeier, February 24, 1989

    SciTech Connect (OSTI)

    Not Available

    1989-02-24

    The testimony concerns the position of NIOSH regarding the existing reporting system of the Mine Safety and Health Administration (MSHA). NIOSH opposes any reduction in the present reporting requirements at this time. NIOSH is presently involved with the Bureau of Labor Statistics (BLS) to upgrade the BLS data gathering system on occupational injuries in general industry. NIOSH addresses five specific areas related to the proposed rulemaking including injury reporting, illness or disease reporting, accident investigation and reporting, employment and coal production reporting, and the MSHA Form 7000-1. In reviewing the current reporting system and data generated by it, NIOSH concludes that the reported injury data are among the best available from any United States governmental regulatory agency. The illness data could be improved by providing more specific disease categories. Minor changes in the Form 7000-1 would provide more easily correlated data. The reliability and detail of the MSHA's data benefit both the operator and the miner by providing for safety and health regulations that are protective to the miner and specific to the problem.

  9. Memorandum of Understanding between the U.S. Department of Labor...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    This Memorandum of Understanding (MOU) serves to set forth the authorities, responsibilities, and procedures by which the Department of Labor (DOL) and the Department of Energy ...

  10. September 16, 2008; HSS/Union Working Group Meeting, Former Worker...

    Broader source: Energy.gov (indexed) [DOE]

    ... of Labor's Division of Energy Employees Occupational Illness Compensation (DEEOIC). ... located in the suburbs of Denver. * DOL DEEOIC representatives reported that Rocky Flats ...

  11. Federal Acquisition Regulation Federal Acquisition Circular 2005...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    6 Summary of Rules FAC 2005-76 Item Subject FAR Case I Equal Employment and Affirmative ... amends the FAR to implement two DOL final rules issued on September 24, 2013 relating to ...

  12. Office of Worker Screening and Compensation Support

    Broader source: Energy.gov [DOE]

    The Office of Worker Screening and Compensation Programs implement the Former Worker Medical Surveillance Program and supports the Department of Labor (DOL) in the implementation of the Energy Employees Occupational Illness Compensation Program Act (EEOICPA).

  13. PRIVACY IMPACT ASSESSMENT: INL Energy Employees' Occupational

    Energy Savers [EERE]

    ... DOL District Claims Office, by the National Institute of Occupational Safety & Health (NIOSH), by the Department of Energy (DOE)-Chicago Office or by the DOE-Grand Junction Office. ...

  14. PRIVACY IMPACT ASSESSMENT: Visitor Dosimeter Badge Tracking

    Energy Savers [EERE]

    ... DOL District Claims Office, by the National Institute of Occupational Safety & Health (NIOSH), by the Department of Energy (DOE)-Chicago Office or by the DOE-Grand Junction Office. ...

  15. Memorandum of Understanding Between the U.S. Department of Labor...

    Broader source: Energy.gov (indexed) [DOE]

    ... To accomplish this goal, DOL will search relevant in- house ... time is of the essence in terms of providing information to ... or enter into any contract or other obligations. ...

  16. National Nanotechnology Initiative's Signature Initiative Sustainable...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    NSF NIH OMB OSTP DHS NRC FDA CPSC ITC USPTO NIOSH DOCBIS USDAFS DOEd DOL DOD DOE NASA ... Agencies involved: DOD, DOE, EPA, ICDNI, NASA, NIH, NIOSH, NIST, NSF, OSHA, USDAFS ...

  17. A Desk Guide to the Davis-Bacon Act

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    ... Request (6) Questions Referred to DOL Sec. 3-2 Payment of DBA Wages and Benefits 23 a. ... Guide 06-16-2010 e. Payment of Piecework Rates, Salaries, or Other-Than Hourly Rates 25 f. ...

  18. A DESK GUIDE TO THE DAVIS-BACON ACT

    Broader source: Energy.gov (indexed) [DOE]

    ... Request (6) Questions Referred to DOL Sec. 3-2 Payment of DBA Wages and Benefits 24 a. ... Payment of Piecework Rates, Salaries, or Other-Than Hourly Rates 26 f. Payment of DBA ...

  19. Memorandum of Understanding between the U.S. Department of Labor and the U.S. Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE)

    January 2011 Memorandum of Understanding between DOL and DOE regarding the authorities, responsibilities and procedures to conduct mandated activities relating to the Energy Employees Occupational Illness Compensation Program Act of 2000.

  20. MEMORANDUM TO: Honorable Patricia Hoffman, Assistant Secretary...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    materials produced by these projects should be made available through a web portal. ... of Department of Labor (DoL), National Science Foundation (NSF) and the Office of EERE ...

  1. Tri-fold - Agencies Assisting with EEOICPA and the Former worker Program |

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Department of Energy Tri-fold - Agencies Assisting with EEOICPA and the Former worker Program Tri-fold - Agencies Assisting with EEOICPA and the Former worker Program March 2015 Agencies Assisting with EEOICPA and the Former Worker Program The Joint Outreach Task Group (JOTG) includes representatives from DOE, Department of Labor (DOL), the National Institute for Occupational Safety and Health (NIOSH), the Offices of the Ombudsman for DOL and NIOSH, and the DOE-funded FWP projects. The JOTG

  2. Joint Outreach Task Group Former Workers Screening Program | Department of

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Energy Former Workers Screening Program Joint Outreach Task Group Former Workers Screening Program The Joint Outreach Task Group (JOTG) includes representatives from DOE, Department of Labor (DOL), the National Institute for Occupational Safety and Health (NIOSH), the Offices of the Ombudsman for DOL and NIOSH, and the DOE-funded FWP projects. The JOTG was established in 2009 under the premise that agencies/programs with common goals can work together by combining resources and coordinating

  3. Energy Employees Occupational Illness Compensation Program Act (EEOICPA)

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Program | Department of Energy Energy Employees Occupational Illness Compensation Program Act (EEOICPA) Program Energy Employees Occupational Illness Compensation Program Act (EEOICPA) Program EEOICPA Program The U.S. Department of Labor (DOL) administers the EEOICPA Program. For information on how to submit an EEOICPA claim, please go to: U.S. Department of Labor, Division of Energy Employees Occupational Illness Compensation DOE's role is to provide requested record information to DOL.

  4. Alternative Fuels Data Center

    Alternative Fuels and Advanced Vehicles Data Center [Office of Energy Efficiency and Renewable Energy (EERE)]

    Measurement Effective November 1, 2015, the Oklahoma Department of Labor (DOL) must standardize compressed natural gas (CNG) and liquefied natural gas (LNG) measurements for retail motor vehicle fuel, unless the National Conference on Weights and Measures has established equivalent measures. Until the DOL standardizes measurements, a gasoline gallon equivalent is equal to 5.66 pounds (lbs.) of CNG and a diesel gallon equivalent is equal to 6.06 lbs. of LNG. (Reference House Bill 1283, 2015, and

  5. Microsoft Word - FUSRAP Wayne NJ.rtf

    Office of Legacy Management (LM)

    ... 26 Federal Plaza, New York, NY 10278 tel: 212-264-0120 mailto: allen.d.roos@usace.army.mil, web: http:www.nan.usace.army.mil US Army Corps of Engineers New York District

  6. URGSIM

    Energy Science and Technology Software Center (OSTI)

    002557IBMPC00 Upper Rio Grande Simulation Model (URGSIM) http://www.spa.usace.army.mil/urgwom/recent.asp

  7. Table HC1.2.1. Living Space Characteristics by

    U.S. Energy Information Administration (EIA) Indexed Site

    Space Characteristics by" " Total, Heated, and Cooled Floorspace, 2005" ,,,"Total Square Footage" ,"Housing Units",,"Total1",,"Heated",,"Cooled" "Living Space Characteristics","Mil...

  8. On the Thermodynamics of Framework Breathing: A Free Energy Model...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ...jp311601q Abstract: When adsorbing guest molecules, the porous metal-organic framework MIL-53(Cr) may vary its cell parameters drastically while retaining its crystallinity. ...

  9. JCESR Presents to the Illinois General Assembly | JCESR

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of Chemistry, University of Illinois at Chicago View presentation Mil Oven, Chief Marketing Officer, Navitas Systems View presentation Samir Mayekar, Chief Executive...

  10. Tax Credits, Rebates & Savings | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    tax abatement for photovoltaic (PV) system expenditures made on buildings located in cities with a population of 1 mil... Eligibility: Commercial, Industrial, Nonprofit,...

  11. Microsoft Word - 07 Texas Water Plan.doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    monthly regional meetings * TWAA (Texas Water Allocation Assessment) * www.swf.usace.army.mil ("(at bottom) Additional Related Material", "Texas Water Allocation Assessment ...

  12. "PART 1: ENERGY/WATER CONSUMPTION AND COST DATA"

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Adjustment Data Report for Fiscal Years Prior to 2008" ,,,"FY","20XX" "Agency:","Department of X",,,"Prepared by:" "Date:",,,,"Phone:" "PART 1: ENERGY/WATER CONSUMPTION AND COST DATA" "1-1. NECPA/E.O. 13423 Goal Subject Buildings" "Energy Type","Consumption Units","Annual Consumption","Annual Cost (Thou. $)","Unit Cost ($)",,"Site-Delivered Btu

  13. LA--12O48-MS DE91

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    -12O48-MS DE91 010299 I ~ I i Tm Thou.mwl Yews of Solitude? 0)1 llzfuhwh!lll Illfrlwiml i)ffo fhc Wmtefsolfltiwl Pilot Project Rqwsitory GrL~gor!/B L')/fo)"(i* Craig W. Kirhood** HmwjOfwf7y Marfit~/. Pmquak!!i+ ~~~~n~~~~L..Al...s.Me. M.xico 87541 L A N L % D I O T D I U E Table of Contents Preface . . . . . . . . . . . . . . . . . . . . . . . . . . .. .. .. .. .. .. .. D O . . . . . . . . . . . ...ooOO.OO..OOOOO"OO".OO """"."" 'ti 1. Introduction . .

  14. Alternative Fuels Data Center

    Alternative Fuels and Advanced Vehicles Data Center [Office of Energy Efficiency and Renewable Energy (EERE)]

    Alternative Fuels Technician Certificates The Department of Labor (DOL) will issue a certificate to any person who has successfully passed the appropriate alternative fuels equipment, alternative fuels compression, or electric vehicle technician examination as provided in the Alternative Fuels Technician Certification Act. A certification fee applies. For companies, partnerships, or corporations involved in the business of installing, servicing, repairing, modifying, or renovating equipment used

  15. DOE: Support Implementation of EEOICPA | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Support Implementation of EEOICPA DOE: Support Implementation of EEOICPA Addthis Description DOE's primary role in the EEOICPA is to provide records to DOL, NIOSH and DOJ, to support claim processing, dose reconstruction and ultimately claim adjudication. The worker records provided by DOE play a vital role in the EEOICPA claims process

  16. NIOSH: Ombudsman to NIOSH for EEOICPA - Part B | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Ombudsman to NIOSH for EEOICPA - Part B NIOSH: Ombudsman to NIOSH for EEOICPA - Part B Addthis Description The NIOSH Ombudsman directly assists both claimants and petitioners. The Ombudsman reviews a claimants' entire case file (DOL initial case file, dose reconstruction report and medical records) and assists petitioners in compiling materials, information and documentation needed to file an SEC petition

  17. Notice of Intent to Revise DOE O 341.1, Federal Employee Health Services

    Broader source: Directives, Delegations, and Requirements [Office of Management (MA)]

    To change Bonneville Power Administration's status to being covered by the order, institutionalize a current requirement to use the Department of Labor's (DOL's) "encomp" process to file a workers' compensation claim, and make minor updates, e.g., for organizational titles and internet links.

  18. IEED Tribal Energy Development to Build Tribal Energy Development Capacity

    Broader source: Energy.gov [DOE]

    The Assistant Secretary - Indian Affairs for the U.S. Department of the Interior, through the Office of Indian Energy and Economic Development, is soliciting grant proposals from Indian tribes to build tribal capacity for energy resource development or management under the Department of the Interior's (DOl's) Tribal Energy Development Capacity (TEDC) grant program.

  19. Notice of Intent to Revise DOE O 341.1, Federal Employee Health Services

    Broader source: Directives, Delegations, and Requirements [Office of Management (MA)]

    2015-11-23

    To change Bonneville Power Administration's status to being covered by the order, institutionalize a current requirement to use the Department of Labor's (DOL's) "encomp" process to file a workers' compensation claim, and make minor updates, e.g., for organizational titles and internet links.

  20. Insights on proximity effect and multiphoton induced luminescence from gold nanospheres in far field optical microscopy

    SciTech Connect (OSTI)

    Borglin, Johan; Guldbrand, Stina; Evenbratt, Hanne; Kirejev, Vladimir; Ericson, Marica B.; Grönbeck, Henrik

    2015-12-07

    Gold nanoparticles can be visualized in far-field multiphoton laser-scanning microscopy (MPM) based on the phenomena of multiphoton induced luminescence (MIL). This is of interest for biomedical applications, e.g., for cancer diagnostics, as MPM allows for working in the near-infrared (NIR) optical window of tissue. It is well known that the aggregation of particles causes a redshift of the plasmon resonance, but its implications for MIL applying far-field MPM should be further exploited. Here, we explore MIL from 10 nm gold nanospheres that are chemically deposited on glass substrates in controlled coverage gradients using MPM operating in NIR range. The substrates enable studies of MIL as a function of inter-particle distance and clustering. It was shown that MIL was only detected from areas on the substrates where the particle spacing was less than one particle diameter, or where the particles have aggregated. The results are interpreted in the context that the underlying physical phenomenon of MIL is a sequential two-photon absorption process, where the first event is driven by the plasmon resonance. It is evident that gold nanospheres in this size range have to be closely spaced or clustered to exhibit detectable MIL using far-field MPM operating in the NIR region.

  1. Experimental Evidence Supported by Simulations of a Very High H{sub 2} Diffusion in Metal Organic Framework Materials

    SciTech Connect (OSTI)

    Salles, F.; Maurin, G.; Jobic, H.; Koza, M. M.; Llewellyn, P. L.; Devic, T.; Serre, C.; Ferey, G.

    2008-06-20

    Quasielastic neutron scattering measurements are combined with molecular dynamics simulations to extract the self-diffusion coefficient of hydrogen in the metal organic frameworks MIL-47(V) and MIL-53(Cr). We find that the diffusivity of hydrogen at low loading is about 2 orders of magnitude higher than in zeolites. Such a high mobility has never been experimentally observed before in any nanoporous materials, although it was predicted in carbon nanotubes. Either 1D or 3D diffusion mechanisms are elucidated depending on the chemical features of the MIL framework.

  2. Army Energy Security Considerations

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    ARMY Energy Security Considerations Don Juhasz, PE, CEM HQDA, OACSIM, DAIM-FDF Telephone: (703)-601-0374 E-mail: don.juhasz@hqda.army.mil FUEL CELL OPPORTUNITIES 26 April 2007 1 of 10 Don Juhasz DAIM-FDF (703) 601-0374 (DSN 329) / don.juhasz@hqda.army.mil 5 April 2007 Army Energy * * * * FOREIGN OIL 2 of 10 Don Juhasz DAIM-FDF (703) 601-0374 (DSN 329) / don.juhasz@hqda.army.mil 5 April 2007 World Energy Situation OIL & GAS LIQUIDS 38% Rise in NTV Fuel Use 35% of DoD utilities 21% of Fed

  3. Demonstration Assessment of Light-Emitting Diode Parking Structure Lighting at U.S. Department of Labor Headquarters

    SciTech Connect (OSTI)

    Kinzey, Bruce R.; Myer, Michael

    2013-03-01

    This report documents a solid-state lighting (SSL) technology demonstration at the parking structure of the U.S. Department of Labor (DOL) Headquarters in Washington, DC, in which light-emitting diode (LED) luminaires were substituted for the incumbent high-pressure sodium (HPS) luminaires and evaluated for relative light quantity and performance. The demonstration results show energy savings of 52% from the initial conversion of HPS to the LED product. These savings were increased to 88% by using occupancy sensor controls that were ultimately set to reduce power to 10% of high state operation after a time delay of 2.5 minutes. Because of the relatively high cost of the LED luminaires at their time of purchase for this project (2010), the simple payback periods were 6.5 years and 4.9 years for retrofit and new construction scenarios, respectively. Staff at DOL Headquarters reported high satisfaction with the operation of the LED product.

  4. Overview FS old.pdf

    Office of Environmental Management (EM)

    Energy Other EEOICP Links and Previous Federal Register Notices Other EEOICP Links and Previous Federal Register Notices Other EEOICP Links MOU between DOL and DOE MOU between HSS and DOE Tri-fold: Agencies Assisting with EEOIPA and the Former Worker Program Deputy Secretary Memo Regarnding Energy Emplyees Occupational Illness Compensation Program Act Interviews of Current and Former Workers Department of Labor Division of Energy Employees Occupational Illness Compensation National Institute

  5. Deputy Secretary Memo Regarding Energy Employees Occupational Illness Compensation Program Act Interviews of Current and Former Workers

    Office of Energy Efficiency and Renewable Energy (EERE)

    The Department embraces its responsibility for and commitment to the health and well-being of the Department of Energy's (DOE) current and former workers, both Federal and contractor employees. Two key programs that advance DO E's commitment to its former and current workers are the Department of Labor (DOL) managed Energy Employees Occupational Illness Compensation Program (EEOICP) and the Former Worker Medical Screening Program.

  6. Sandia National Laboratories: Global Insight, Inc. / Department of Labor

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Facebook Twitter YouTube Flickr RSS Working with Sandia Global Insight, Inc. / Department of Labor Global Insight, Inc. (GII), was created by combining DRI (formerly Data Resources, Inc.) and WEFA (formerly Wharton Econometric Forecasting Associates). Due to copyright/distribution laws being derived from a proprietary service that Sandia pays for, Sandia can no longer provide GII factor information at this website. However, Sandia will continue to supply the DOL and the "combined key

  7. I

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    \ ,~ -'tc;- blank ! I ,- I i I ! f ,. I i..~--~-~*~*-------------.-.-.-.-------------r--------------------------------------~ .2.7. AP::'-!/ . 2.D (( .....--z....,... -;Ill .// -1-:...1- VVk:'.rttc4/( to' ----.J blank ", '1" . ~*.:-1 ... ., Tripp, Larry From: Sent: To: Subject: Attachments: Cone, Elaine M Thursday, April 28, 2011 9:02 AM Tripp, Larry DOL request SKMBT _ C552D11 042807460 (2).pdf larry, This request is for large amounts of data. Our approach for 16 & 17 will be to

  8. Demonstration Assessment of Light-Emitting Diode Parking Structure Lighting

    Office of Scientific and Technical Information (OSTI)

    at U.S. Department of Labor Headquarters (Technical Report) | SciTech Connect Demonstration Assessment of Light-Emitting Diode Parking Structure Lighting at U.S. Department of Labor Headquarters Citation Details In-Document Search Title: Demonstration Assessment of Light-Emitting Diode Parking Structure Lighting at U.S. Department of Labor Headquarters This report documents a solid-state lighting (SSL) technology demonstration at the parking structure of the U.S. Department of Labor (DOL)

  9. Hualapai Tribe - Tribal Utility Development and MAP Wind Assessment

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Tribal Energy Program DOE-BIA Peer Review October 26, 2006 Hualapai Reservation Solar Water Pipeline 1997 to Present * USDA Water Project * Upgraded to provide water to Grand Canyon West Tourism area * Currently being upgraded for increased flow and domestic water quality improvements Earthship Project - 1999 * Funded by DOL Jobs in Recycling program * Built by WIA workers * Solar PV * Water Catchment system Guano Point 2000 * Off Grid 7 kilowatt PV and wind system * Power for lights, kitchen,

  10. Federal financial assistance for hydroelectric power

    SciTech Connect (OSTI)

    Not Available

    1980-09-01

    The Rural Energy Initiative seeks to maximize the effectiveness of Federal programs in developing certain energy resources, including small-scale hydropower. The REI target is to arrange financing for 100 hydro sites by 1981, with about 300 MWe of additional capacity. The REI financial assistance programs for small hydropower development in the US DOE; Economic Development Administration; REA; HUD; Farmers Home Administration; DOI; DOL's CETA programs; and the Community Services Administration are described. (MCW)

  11. Search for: All records | SciTech Connect

    Office of Scientific and Technical Information (OSTI)

    ... E-mail: pandey@mtu.edu, E-mail: shashi.p.karna.civ@mail.mil Phosphorene is emerging as a promising 2D semiconducting material with a direct band gap and high carrier mobility. ...

  12. High compressibility of a flexible metal–organic framework

    SciTech Connect (OSTI)

    Serra-Crespo P.; Stavitski E.; Kapteijn, F.; Gascon, J.

    2012-03-22

    The metal-organic framework NH{sub 2}-MIL-53(In) shows a very high amorphization resistance (>20 GPa) together with a large compressibility (K{sub 0} = 10.9 GPa).

  13. New York City- Property Tax Abatement for Photovoltaic (PV) Equipment Expenditures

    Broader source: Energy.gov [DOE]

    In August 2008 the State of New York enacted legislation allowing a property tax abatement for photovoltaic (PV) system expenditures made on buildings located in cities with a population of 1 mil...

  14. Erin Gill, city of Knoxville sustainability director, on Aug...

    Open Energy Info (EERE)

    Erin Gill, city of Knoxville sustainability director, on Aug. 13, 2014, explains a competition entered by the city with a 5 mil Home WikiSysop's picture Submitted by WikiSysop(15)...

  15. DOE Providing Additional Supercomputing Resources to Study Hurricane...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    ... For more information on the Corps of Engineers, go to http:www.usace.army.mil. Media contact(s): Jeff Sherwood (DOE), (202) 586-5806 Jon Bashor (NERSC), (510) 486-5849 Addthis ...

  16. Safety Functions and Other Features of Remotely Operated Weapon...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    ... B.5 MIL-STD-1472F, "Design Criteria Standard - Human Engineering," U.S. Department of Defense. Note: This standard is mandatory for military purchasers. B.6 "Unmanned Systems ...

  17. Fluorescent Pigments for High-Performance Cool Roofing

    Office of Environmental Management (EM)

    ... Effective solar reflectance (ESR) measurements on final coated substrates were conducted ... Coil and extrusion coatings are applied at dry film thicknesses of ca. 0.8 mils (20 m), ...

  18. Evaluation of the exothermicity of the chemi-ionization reaction...

    Office of Scientific and Technical Information (OSTI)

    Authors: Cox, Richard M ; Kim, JungSoo ; Armentrout, P. B., E-mail: armentrout@chem.utah.edu, E-mail: mheaven@emory.edu, E-mail: albert.viggiano@us.af.mil 1 ; Bartlett, Joshua ; ...

  19. Cybersecurity Online Learning (COL) | Department of Energy

    Energy Savers [EERE]

    You must create a user account using a valid .mil or .gov email address as your User ID. The password you create will work for all future registrations. You must register ...

  20. CX-012460: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Technology for Greenhouse Gas Emission Reduction & Cost Competitiveness of Mil-Spec Jet Fuel Production Using CTL CX(s) Applied: B3.6Date: 41877 Location(s): AlabamaOffices(s): National Energy Technology Laboratory

  1. CX-012462: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Technology for Greenhouse Gas Emission Reduction & Cost Competitiveness of Mil-Spec Jet Fuel Production Using CTL CX(s) Applied: B3.6Date: 41877 Location(s): UtahOffices(s): National Energy Technology Laboratory

  2. ARM - Facility News Article

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    near the ARM North Slope of Alaska (NSA) site in Barrow, to provide measurements of ... that this is mil-spec armored cable," said Mark Ivey, ARM Site Manager for the NSA locale. ...

  3. No FEAR Act | Department of Energy

    Energy Savers [EERE]

    ...Naval Reactors Offices 412-476-7204 Edward.rose@navy.mil TBD SCChicago Office Rufus Smith SCOak Ridge Office 865- 576-4988 Smithrh@oro.doe.gov Judith A. Mead SCHeadquarters ...

  4. Highly Selective Adsorption of Ethylene over Ethane in a MOF Featuring the Combination of Open Metal Site and -Complexation

    SciTech Connect (OSTI)

    Zhang, Yiming; LI, Baiyan; Wu, Zili; Ma, Shengqian

    2015-01-01

    The introduction of the combination of open metal site (OMS) and -complexation into MOF has led to very high ethylene/ethane adsorption selectivity at 318K, as illustrated in the context of MIL-101-Cr-SO3Ag. The interactions with ethylene from both OMS and -complexation in MIL-101-Cr-SO3Ag have been investigated by in situ IR spectroscopic studies and computational calculations, which suggest -complexation contributes dominantly to the high ethylene/ethane adsorption selectivity.

  5. Highly Selective Adsorption of Ethylene over Ethane in a MOF Featuring the Combination of Open Metal Site and -Complexation

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Zhang, Yiming; Li, Baiyan; Wu, Zili; Ma, Shengqian

    2015-01-09

    The introduction of the combination of open metal site (OMS) and -complexation into MOF has led to very high ethylene/ethane adsorption selectivity at 318K, as illustrated in the context of MIL-101-Cr-SO3Ag. The interactions with ethylene from both OMS and -complexation in MIL-101-Cr-SO3Ag have been investigated by in situ IR spectroscopic studies and computational calculations, which suggest -complexation contributes dominantly to the high ethylene/ethane adsorption selectivity.

  6. California National Guard Sustainability Planning, Hydrogen Fuel Goals

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Lt Col Reuben Sendejas/916.361.4339/reuben.r.sendejas@us.army.mil California Army National Guard, Environmental Programs Directorate California National Guard Sustainability Planning, Hydrogen Fuel Goals 27 Oct 08 Lt Col Reuben Sendejas Lt Col Reuben Sendejas/916.361.4339/reuben.r.sendejas@us.army.mil California Army National Guard, Environmental Programs Directorate Sustainability Requires Commitment The Breakfast Analogy 11/11/2008 3 Lt Col Reuben

  7. Corrosion investigation of coatings for surface protection of military hardware

    SciTech Connect (OSTI)

    Lindsey, N.; Vasanth, K.L.

    1996-10-01

    A product improvement program (PIP) for the surface finish of some steel military hardware has been recently initiated by the Navy. Presently the metal cleaning methods, interior and exterior surface finishes and corrosion protection requirements for such hardware are specified in MIL-P-18948. The coated hardware are stored in a warehouse structure for long durations. Because these storage places are not environmentally controlled (that is, no temperature or humidity control) the corrosion protection has not been adequate. The exterior surfaces of the hardware are coated with a corrosion inhibiting alkyd primer coating (TT-P-664) or a rust inhibiting lacquer primer coating (MIL-P-11414) to a thickness of 0.4 to 0.6 mils. The exterior color paint, (MIL-E-52891 or MIL-P11195), is applied to a thickness of 1.5 mils. The investigation of various coatings to replace the present system is an ongoing effort. The coatings have been examined from a corrosion protection vantage point and results have been correlated. The coatings were evaluated by exposing them to natural marine atmosphere and seawater wetdown tests. The coatings were also exposed to a 5.0% sodium chloride solution in a laboratory environmental salt fog chamber for 500 hours. Selected coatings were examined using Electrochemical Impedance Spectroscopy (EIS). The results obtained from field tests, salt fog, and EIS measurements are discussed.

  8. Extrusion of metal oxide superconducting wire, tube or ribbon

    DOE Patents [OSTI]

    Dusek, Joseph T. (Lombard, IL)

    1993-01-01

    A process for extruding a superconducting metal oxide composition YBa.sub.2 Cu.sub.3 O.sub.7-x provides a wire (tube or ribbon) having a cohesive mass and a degree of flexibility together with enhanced electrical properties. Wire diameters in the range of 6-85 mils have been produced with smaller wires on the order of 10 mils in diameter exhibiting enhanced flexibility for forming braided, or multistrand, configurations for greater current carrying capacity. The composition for extrusion contains a polymeric binder to provide a cohesive mass to bind the particles together during the extrusion process with the binder subsequently removed at lower temperatures during sintering. The composition for extrusion further includes a deflocculent, an organic plasticizer and a solvent which also are subsequently removed during sintering. Electrically conductive tubing with an inner diameter of 52 mil and an outer diameter of 87-355 mil has also been produced. Flat ribbons have been produced in the range of 10-125 mil thick by 100-500 mil wide. The superconducting wire, tube or ribbon may include an outer ceramic insulating sheath co-extruded with the wire, tubing or ribbon.

  9. Extrusion of metal oxide superconducting wire, tube or ribbon

    DOE Patents [OSTI]

    Dusek, Joseph T.

    1993-10-05

    A process for extruding a superconducting metal oxide composition YBa.sub.2 Cu.sub.3 O.sub.7-x provides a wire (tube or ribbon) having a cohesive mass and a degree of flexibility together with enhanced electrical properties. Wire diameters in the range of 6-85 mils have been produced with smaller wires on the order of 10 mils in diameter exhibiting enhanced flexibility for forming braided, or multistrand, configurations for greater current carrying capacity. The composition for extrusion contains a polymeric binder to provide a cohesive mass to bind the particles together during the extrusion process with the binder subsequently removed at lower temperatures during sintering. The composition for extrusion further includes a deflocculent, an organic plasticizer and a solvent which also are subsequently removed during sintering. Electrically conductive tubing with an inner diameter of 52 mil and an outer diameter of 87-355 mil has also been produced. Flat ribbons have been produced in the range of 10-125 mil thick by 100-500 mil wide. The superconducting wire, tube or ribbon may include an outer ceramic insulating sheath co-extruded with the wire, tubing or ribbon.

  10. Regulatory Oversight Program, July 1, 1993--March 3, 1997. Volume 2: Appendices

    SciTech Connect (OSTI)

    1997-12-31

    On July, 1993, a Regulatory Oversight (RO) organization was established within the US DOE, Oak Ridge Operations to provide regulatory oversight of the DOE uranium enrichment facilities leased to the United States Enrichment Corporation (USEC). The purpose of the OR program was to ensure continued plant safety, safeguards and security while the plants were transitioned to regulatory oversight by the Nuclear Regulatory Commission (NRC). Volume 2 contains copies of the documents which established the relationship between NRC, DOE, USEC, and DOL (Dept of Labor) required to facilitate regulatory oversight transition.

  11. 1 of 8

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Coverage for: Individual/Family | Plan Type: HDHP Questions: Call 1-877-878-LANL (5265) or visit us at www.bcbsnm.com/coverage. If you aren't clear about any of the underlined terms used in this form, see the Glossary. You can view the Glossary at www.dol.gov/ebsa/pdf/SBCUniformGlossary.pdf or call 1-800-432-0750 to request a copy. This is only a summary. If you want more detail about your coverage and costs, you can get the complete terms in the policy or plan document at

  12. 1 of 8

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Coverage for: Individual/Family | Plan Type: PPO Questions: Call 1-877-878-LANL (5265)or visit us at www.bcbsnm.com/coverage. If you aren't clear about any of the underlined terms used in this form, see the Glossary. You can view the Glossary at www.dol.gov/ebsa/pdf/SBCUniformGlossary.pdf or call 1-877-878-LANL (5265) to request a copy. This is only a summary. If you want more detail about your coverage and costs, you can get the complete terms in the policy or plan document at

  13. 1 of 8

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    National EPO for Retirees with Medicare Coverage Period: 01/01/2016 - 12/31/2016 Summary of Benefits and Coverage: What this Plan Covers & What it Costs Coverage for: Individual/Family | Plan Type: EPO Questions: Call 1-877-878-LANL (5265) or visit us at www.bcbsnm.com/coverage. If you aren't clear about any of the underlined terms used in this form, see the Glossary. You can view the Glossary at www.dol.gov/ebsa/pdf/SBCUniformGlossary.pdf or call 1-877-878-LANL (5265) to request a copy.

  14. 1 of 8

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    PPO Retirees with Medicare Plan Coverage Period: 01/01/2016 - 12/31/2016 Summary of Benefits and Coverage: What this Plan Covers & What it Costs Coverage for: Individual/Family | Plan Type: PPO Questions: Call 1-877-878-LANL (5265) or visit us at www.bcbsnm.com/coverage. If you aren't clear about any of the underlined terms used in this form, see the Glossary. You can view the Glossary at www.dol.gov/ebsa/pdf/SBCUniformGlossary.pdf or call 1-877-878-LANL (5265) to request a copy. This is

  15. SR0107

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    4, 2001 Media Contact: Bill Taylor (803) 725-2889 DOE & DOL Hold Public Meetings For Energy Employees Occupational Illness Compensation Program At Flag Ribbon Art Aiken SC (June 14, 2001) - The U.S. Departments of Labor and Energy will hold two public meetings at 1 p.m. and 7 p.m., Tuesday, June 19 at the North Augusta Community Center, North Augusta, SC, for employees and families who may be eligible for compensation under the Energy Employees Occupational Illness Compensation Program Act.

  16. Contact Us | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Us » Contact Us Contact Us Mailing Address: U.S. Department of Energy Office of Legacy Management 1000 Independence Avenue, SW Washington, DC 20585 Phone: (202) 586-3559 Fax: (202) 586-1540 Email: LM@hq.doe.gov Technical Assistance: LMWebsiteSupport@LM.doe.gov EEOICPA Program The U.S. Department of Labor (DOL) administers the EEOICPA Program. For information on how to submit an EEOICPA claim, please go to: U.S. Department of Labor, Division of Energy Employees Occupational Illness Compensation

  17. Immobilizing Highly Catalytically Active Pt Nanoparticles inside the Pores of Metal-Organic Framework: A Double Solvents Approach

    SciTech Connect (OSTI)

    Aijaz, Arshad; Karkamkar, Abhijeet J.; Choi, Young Joon; Tsumori, Nobuko; Ronnebro, Ewa; Autrey, Thomas; Shioyama, Hiroshi; Xu, Qiang

    2012-08-29

    Ultrafine Pt nanoparticles were successfully immobilized inside the pores of a metal-organic framework MIL-101 without deposition of Pt nanoparticles on the external surfaces of framework by using a 'double solvents' method. The resulting Pt@MIL-101 composites with different Pt loadings represent the first highly active MOF-immobilized metal nanocatalysts for catalytic reactions in all three phases: liquid-phase ammonia borane hydrolysis; solid-phase ammonia borane thermal dehy-drogenation and gas-phase CO oxidation. The observed excellent catalytic performances are at-tributed to the small Pt nanoparticles within the pores of MIL-101. 'We are thankful to AIST and METI for financial support. TA & AK are thankful for support from the US Department of Energy, Office of Basic Energy Sciences, Division of Chemical Sciences, Geosciences & Biosciences. PNNL is operated by Battelle.'

  18. Highly Selective Adsorption of Ethylene over Ethane in a MOF Featuring the Combination of Open Metal Site and -Complexation

    SciTech Connect (OSTI)

    Zhang, Yiming; Li, Baiyan; Wu, Zili; Ma, Shengqian

    2015-01-09

    The introduction of the combination of open metal site (OMS) and -complexation into MOF has led to very high ethylene/ethane adsorption selectivity at 318K, as illustrated in the context of MIL-101-Cr-SO3Ag. The interactions with ethylene from both OMS and -complexation in MIL-101-Cr-SO3Ag have been investigated by in situ IR spectroscopic studies and computational calculations, which suggest -complexation contributes dominantly to the high ethylene/ethane adsorption selectivity.

  19. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Page 1 of 7 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website address: FAR: http://farsite.hill.af.mil/vffara.htm DEAR: http://farsite.hill.af.mil/vfdoea.htm

  20. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Page 1 of 8 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website address: FAR: http://farsite.hill.af.mil/vffara.htm DEAR: http://farsite.hill.af.mil/vfdoea.htm

  1. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Page 1 of 8 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website address: FAR: http://farsite.hill.af.mil/vffara.htm DEAR: http://farsite.hill.af.mil/vfdoea.htm

  2. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    2, 7/14/14) Appendix SFA-1 Page 1 of 3 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website address: FAR: http://farsite.hill.af.mil/vffara.htm DEAR: http://farsite.hill.af.mil/vfdoea.htm

  3. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Page 1 of 8 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website address: FAR: http://farsite.hill.af.mil/vffara.htm DEAR: http://farsite.hill.af.mil/vfdoea.htm

  4. Furniture Rack Corrosion Coupon Surveillance - 2012 Update

    SciTech Connect (OSTI)

    Mickalonis, J. I.; Murphy, T. R.; Berry, C. J.

    2012-10-01

    Under the L Basin corrosion surveillance program furniture rack coupons immersed for 14 years (FY2009 coupons) and 16 years (FY2011 coupons) were analyzed and the results trended with coupons exposed for shorter times. In addition, a section harvested from an actual furniture rack that was immersed for 14 years was analyzed for pitting in the weld and heat-affected-zone (HAZ) regions. The L Basin operations maintained very good water quality over the entire immersion period for these samples. These results for FY2009 and FY2011 coupons showed that the average pit depths for the 6061 and 6063 base metal are 1 and 2 mils, respectively, while those for the weld and HAZ are 3 and 4 mils, respectively. The results for the weld and HAZ regions are similar to coupons removed during the period of FY2003 to FY2007. These similarities indicate that the pit development occurred quickly followed by slow kinetics of increase in pit depth. For the actual furniture rack sample average pits of 5 and 2 mils were measured for the HAZ and weld, respectively. These results demonstrate that pitting corrosion of the aluminum furniture racks used to support the spent fuel occurs in waters of good quality. The corrosion kinetics or pit depth growth rate is much less that 1 mil/year, and would not impact long-term use of this material system for fuel storage racks in L Basin if good water quality is maintained.

  5. Sulfation of metal-organic framework: Opportunities for acid catalysis and proton conductivity

    SciTech Connect (OSTI)

    Goesten, M.G.; Stavitski, E.; Juan-Alcaniz, J.; Ramos-Fernandez, E.V.; Sai Sankar Gupta, K.B.; van Bekkum, H.; Gascon, J. and Kapteijn, F.

    2011-05-24

    A new post-functionalization method for metal-organic frameworks (MOFs) has been developed to introduce acidity for catalysis. Upon treatment with a mixture of triflic anhydride and sulfuric acid, chemically stable MOF structures MIL-101(Cr) and MIL-53(Al) can be sulfated, resulting in a Broensted sulfoxy acid group attached to up to 50% of the aromatic terephthalate linkers of the structure. The sulfated samples have been extensively characterized by solid-state NMR, XANES, and FTIR spectroscopy. The functionalized acidic frameworks show catalytic activity similar to that of acidic polymers like Nafion{reg_sign} display in the esterification of n-butanol with acetic acid (TOF {approx} 1 min{sup -1} {at} 343 K). Water adsorbs strongly up to 4 molecules per sulfoxy acid group, and an additional 2 molecules are taken up at lower temperatures in the 1-D pore channels of S-MIL-53(Al). The high water content and Broensted acidity provide the structure S-MIL-53(Al) a high proton conductivity up to moderate temperatures.

  6. Air Proportional Counter

    DOE Patents [OSTI]

    Simpson, J.A. Jr.

    1950-12-05

    A multiple wire counter utilizing air at atmospheric pressure as the ionizing medium and having a window of a nylon sheet of less than 0.5 mil thickness coated with graphite. The window is permeable to alpha particles so that the counter is well adapted to surveying sources of alpha radiation.

  7. Isotopic evidence for a magmatic contribution to fluids of the geothermal systems of Larderello, Italy, and the Geysers, California

    SciTech Connect (OSTI)

    D'Amore, F.; Bolognesi, L. . Italian National Research Council)

    1994-02-01

    The isotopic composition of steam from the Larderello, Italy, and The Geysers, California, geothermal fields is used to determine the source(s) of the fluid in these two vapor-dominated systems. Previous interpretations suggested the isotopic composition of the two systems was mainly the result of reactions at high temperature between deeply circulating meteoric water and largely sedimentary host rocks. The authors interpret the data for the Larderello and The Geysers fluids as indicating that meteoric water, exchanged with host rocks, mixes with local magnetic water. The isotopic composition of end-member magmatic water at The Geysers is typical of convergent plate boundaries ([delta][sup 18]O = +5 to +11 per mil; [delta]D = [minus]10 to [minus]35 per mil); a local isotopic composition of +11 to +15 per mil [delta][sup 18]O and [minus]15 to [minus]35 per mil [delta]D is suggested for the Larderello magmatic water. The magmatic water derived from the crystallization of underlying magma. Metamorphic waters, derived from dehydration reactions of OH-bearing minerals, may also make a minor contribution to the geothermal fluids.

  8. Buildings Energy Data Book: 5.1 Building Materials/Insulation

    Buildings Energy Data Book [EERE]

    5 Properties of Cool Roofing Materials (1) Asphalt Shingles Shasta White 0.26 0.91 Generic White 0.25 0.91 Generic Grey 0.22 0.91 Light Brown 0.19 0.91 Medium Brown 0.12 0.91 Generic Black 0.05 0.91 White Coatings White Coating (1 coat, 8 mil) 0.80 0.91 White Coating (2 coats, 20 mil) 0.85 0.91 Aluminum Coatings Aluminum 0.61 0.25 Fibered on Black 0.40 0.56 Membranes Gray EPDM (4) 0.23 0.87 White EPDM (4) 0.69 0.87 T-EPDM (4) 0.81 0.92 Light Gravel on Built-Up Roof 0.34 0.90 Metal Roof New, Bare

  9. Final Report For The Erosion And Corrosion Analysis Of Waste Transfer Primary Pipeline Sections From 241-SY Tank Farm

    SciTech Connect (OSTI)

    Page, J. S.; Wyrwas, R. B.; Cooke, G. A.

    2012-10-04

    Three sections of primary transfer pipeline removed from the 241-SY Tank Farm in Hanford's 200 West area, labeled as SN-285, SN-286, and SN-278, were analyzed for the presence and amount of corrosion and erosion on the inside surface of the transfer pipe. All three sections of pipe, ranging in length between 6 and 8 in., were received at the 222-S Laboratory still in the pipe-in-pipe assembly. The annular spaces were filled with urethane foam injected into the pipes for as low as reasonably achievable (ALARA) purposes. The 3-in. primary transfer pipes were first separated from the outer encasement, 6-in. pipes. The pipes were cut into small sections, or coupons, based upon the results of a non-destructive pipe wall thickness measurement which used an ultrasonic transducer. Following removal of the foam, the coupons were subjected to a series of analytical methods utilizing both optical microscopy and scanning electron microscopy to obtain erosion and corrosion information. The ultrasonic transducer analysis of the SN-285 primary pipe did not show any thinned locations in the pipe wall which were outside the expected range for the 3-in. schedule 40 pipe of 216 mils. A coupon was cut from the thinnest area on the pipe, and analysis of the inside surface, which was in contact with the tank waste, revealed a continuous layer of corrosion ~ 100 11m (4 mils) thick under a semi-continuous layer of tank waste residue ~ 20 11m (1 mil) thick. This residue layer was composed of an amorphous phase rich in chromium, magnesium, calcium, and chlorine. Small pits were detected throughout the inside pipe surface with depths up to ~ 50 11m (2 mils). Similarly, the SN-286 primary pipe did not show, by the ultrasonic transducer measurements, any thinned locations in the pipe wall which were outside the expected range for this pipe. Analysis of the coupon cut from the pipe section showed the presence of a tank waste layer containing sodium aluminate and phases rich in iron, calcium

  10. FIRST_Research Perspective_Li

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    1. Structure factor obtained from MD (a) and SAXS (b) at different temperatures: comparison of spatial heterogeneity from snapshots (c) of DILs (top) and MILs (bottom) FIRST Center Research Perspective: Nanoscale Heterogeneity and Dynamics of Room Temperature Ionic Liquids Song Li Vanderbilt University Jianchang Guo, Kee Sung Han, Jose L. Bañuelos, Edward W. Hagaman, Robert W. Shaw Oak Ridge National Laboratory Research Summary: An increase of the alkyl chain length of the cation of room

  11. Resources for Veteran Recruitment | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Resources for Veteran Recruitment Resources for Veteran Recruitment USEFUL WEBSITES FOR VETERAN/MILITARY RECRUITMENT AND HIRING Many of the following websites provide free services for employers looking to hire Veterans and transitioning military service members. WEBSITES - Army Wounded Warrior Program (AW2): http://wtc.army.mil/aw2/index.html - official site for the DoD program for the severely wounded interested in employment. - Clearedjobs.net: http://clearedjobs.net/ - Fee for service,

  12. DOCUMENT RELEASE FORM

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    DNS Policies & Procedures DNS Policies & Procedures DNS Policy Every Federal agency must use only .gov, .mil, or Fed.us domains unless the agency head explicitly determines another domain is necessary for the proper performance of an agency function. Why is this important? Visitors looking for official government information must be confident that is what they are getting. Many websites exist that resemble government websites or that appear to provide "official" government

  13. Department of Energy Acquisition Regulation (DEAR)

    Office of Energy Efficiency and Renewable Energy (EERE)

    To ensure that you are using the most recent version of the Department of Energy Acquisition Regulation (DEAR), use one of the electronic versions at one of the following websites: DOE Procurement - http://management.energy.gov/DEAR.htm; Electronic Code of Federal Regulations - http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?c=ecfr&tpl=/ecfrbrowse/Tit... or Hill Air Force Base - http://farsite.hill.af.mil/vfdoea.htm.

  14. LFS Appendix SFA-1

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Page 1 of 8 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: FAR: http://farsite.hill.af.mil/vffara.htm DEAR:

  15. Rugged calorimeter with a fast rise time

    SciTech Connect (OSTI)

    McMurtry, W.M.; Dolce, S.R.

    1980-01-01

    An intrinsic 1-mil-thick gold foil calorimeter has been developed which rises to 95% of the energy deposited in less than 2 microseconds. This calorimeter is very rugged, and can withstand rough handling without damage. The time constant is long, in the millisecond range, because of its unique construction. Use of this calorimeter has produced 100% data recovery, and agreement with true deposition to less than 10%.

  16. A Tool for Assessing the Text Legibility of Digital Human Machine Interfaces

    SciTech Connect (OSTI)

    Roger Lew; Ronald L. Boring; Thomas A. Ulrich

    2015-08-01

    A tool intended to aid qualified professionals in the assessment of the legibility of text presented on a digital display is described. The assessment of legibility is primarily for the purposes of designing and analyzing human machine interfaces in accordance with NUREG-0700 and MIL-STD 1472G. The tool addresses shortcomings of existing guidelines by providing more accurate metrics of text legibility with greater sensitivity to design alternatives.

  17. US Army Corps of Engineers BUILDING STRONG

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Hydropower 5-year Plan and MIL The Risk Factors CESWD-PDO 22 June 2016 BUILDING STRONG ® Ranking Criteria for Capitalized Work in Plants (Ranking Worksheet) Hydropower Relative Risk Index (1-5)- Primary Ranking *Condition Index *Consequence Rating Criteria *Hydropower Relative Risk Values Availability Risk Public Safety and Health Environmental Concerns Legal Concerns Impact to Other Business Lines Formulate a Condition Index Rank- 1=High Risk; 5= Minimal Risk 2 BUILDING STRONG ® Integration

  18. DNS Policies & Procedures | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    DNS Policies & Procedures DNS Policies & Procedures DNS Policy Every Federal agency must use only .gov, .mil, or Fed.us domains unless the agency head explicitly determines another domain is necessary for the proper performance of an agency function. Why is this important? Visitors looking for official government information must be confident that is what they are getting. Many websites exist that resemble government websites or that appear to provide "official" government

  19. Microsoft Word - AES Appendix SFA-1 (Rev. 8.1, 5-22-15)[1].doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    .1, 5/22/15) Appendix SFA-1 Page 1 of 7 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website addresses: FAR: http://farsite.hill.af.mil/vffara.htm DEAR:

  20. Microsoft Word - CI-OFF Appendix SFA-1 (Rev 2.1, 5-22-15).doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    .1, 5/22/15) Appendix SFA-1 Page 1 of 6 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: * FAR: http://farsite.hill.af.mil/vffara.htm and * DEAR:

  1. Microsoft Word - CI-ON Appendix SFA-1 (Rev 2.1, 5-22-15).doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    .1, 5/22/15) Appendix SFA-1 Page 1 of 6 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: * FAR: http://farsite.hill.af.mil/vffara.htm and * DEAR:

  2. Microsoft Word - CPFFS Appendix SFA-1 (Rev. 7.1, 5-22-15).doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    .1, 5/22/15) Appendix SFA-1 Page 1 of 8 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: FAR: http://farsite.hill.af.mil/vffara.htm DEAR:

  3. Microsoft Word - D-B CONST Appendix SFA-1 (Rev. 3.1, 5-22-15).doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    .1, 5/22/15) Appendix SFA-1 Page 1 of 7 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website address: FAR: http://farsite.hill.af.mil/vffara.htm DEAR:

  4. Microsoft Word - EFS Appendix SFA-1 (Rev. 6.1, 5-22-15).doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    .1, 5/22/15) Appendix SFA-1 Page 1 of 7 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website address: FAR: http://farsite.hill.af.mil/vffara.htm DEAR:

  5. Table Definitions, Sources, and Explanatory Notes

    Gasoline and Diesel Fuel Update (EIA)

    Other Products Definitions Key Terms Definition Aviation Gasoline A complex mixture of relatively volatile hydrocarbons with or without small quantities of additives, blended to form a fuel suitable for use in aviation reciprocating engines. Fuel specifications are provided in ASTM Specification D 910 and Military Specification MIL-G-5572. Note: Data on blending components are not counted in data on finished aviation gasoline. Gas Plant Operator Any firm, including a gas plant owner, which

  6. Table Definitions, Sources, and Explanatory Notes

    Gasoline and Diesel Fuel Update (EIA)

    Petroleum Product Prices by Sales Type Definitions Key Terms Definition Aviation Gasoline (Finished) A complex mixture of relatively volatile hydrocarbons with or without small quantities of additives, blended to form a fuel suitable for use in aviation reciprocating engines. Fuel specifications are provided in ASTM Specification D 910 and Military Specification MIL-G-5572. Note: Data on blending components are not counted in data on finished aviation gasoline. Gas Plant Operator Any firm,

  7. Table Definitions, Sources, and Explanatory Notes

    Gasoline and Diesel Fuel Update (EIA)

    Prices, Sales Volumes & Stocks by State Definitions Key Terms Definition Aviation Gasoline (Finished) A complex mixture of relatively volatile hydrocarbons with or without small quantities of additives, blended to form a fuel suitable for use in aviation reciprocating engines. Fuel specifications are provided in ASTM Specification D 910 and Military Specification MIL-G-5572. Note: Data on blending components are not counted in data on finished aviation gasoline. Gas Plant Operator Any firm,

  8. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: * FAR: http://farsite.hill.af.mil/vffara.htm and * DEAR:

  9. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: * FAR: http://farsite.hill.af.mil/vffara.htm and * DEAR:

  10. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: * FAR: http://farsite.hill.af.mil/vffara.htm and * DEAR:

  11. Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Page 1 of 5 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website addresses: FAR: http://farsite.hill.af.mil/vffara.htm DEAR:

  12. Autonomie: Automotive System Design | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Autonomie: Automotive System Design Autonomie: Automotive System Design Argonne's Autonomie is a MATLAB©-based software environment and framework for automotive control system design, simulation and analysis. Autonomie is capable of Model-in-the-Loop (MIL), Software-in-the-Loop (SIL), Hardware-in-the-Loop (HIL) and Rapid-Control-Prototyping (RCP) Integrating math-based engineering activities through all stages of development Mixing and matching models of different levels of abstraction with

  13. Precision wire feeder for small diameter wire

    DOE Patents [OSTI]

    Brandon, E.D.; Hooper, F.M.; Reichenbach, M.L.

    1992-08-11

    A device for feeding small diameter wire having a diameter less than 0.04 mm (16 mil) to a welding station includes a driving wheel for controllably applying a non-deforming driving force to the wire to move the free end of the wire towards the welding station; and a tension device such as a torque motor for constantly applying a reverse force to the wire in opposition to the driving force to keep the wire taut. 1 figure.

  14. Precision wire feeder for small diameter wire

    DOE Patents [OSTI]

    Brandon, Eldon D.; Hooper, Frederick M.; Reichenbach, Marvin L.

    1992-01-01

    A device for feeding small diameter wire having a diameter less than 0.04 mm (16 mil) to a welding station includes a driving wheel for controllably applying a non-deforming driving force to the wire to move the free end of the wire towards the welding station; and a tension device such as a torque motor for constantly applying a reverse force to the wire in opposition to the driving force to keep the wire taut.

  15. AES Appendix SFA-1

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Appendix SFA-1 Page 1 of 7 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at website addresses: FAR: http://farsite.hill.af.mil/vffara.htm DEAR:

  16. July 28, 2010, AFIRM as a model for technology - focused federal funding

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    RCCC 1 Armed Forces Institute of Regenerative Medicine AFIRM as a model for technology-focused federal funding Prepared by Joachim Kohn, PhD Board of Governors Professor Director (PI), AFIRM-RCCC RCCC 2 AFIRM: Our Mission Marine 1st Sgt. Kasal was wounded in Fallujah, 2004. Courtesy of www.ourmilitary.mil * To develop a comprehensive program in support of the wounded service member, including - Research and development of new therapies and regenerative products - Coordination of innovative

  17. DOE - Office of Legacy Management -- St Louis Airport Site Vicinity

    Office of Legacy Management (LM)

    Properties - 017 Site Vicinity Properties - 017 FUSRAP Considered Sites Site: St. Louis Airport Site Vicinity Properties (017) FUSRAP Active Site. More information at http://www.mvs.usace.army.mil/Home.aspx Designated Name: Berkeley, MO, Site Vicinity Properties Alternate Name: None Location: Berkeley, Missouri Evaluation Year: Added to FUSRAP by Congress in 1984 Site Operations: Contaminated by materials from St Louis Airport site Site Disposition: USACE is actively remediating the site

  18. Hopi Tribe - Utility-Scale Wind Project and Sustainability Program

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Arizona State Map *Hopi is located in Northeastern AZ *Elevations range from 3,900ft to 6,500ft *Geography consists of mesa's/buttes, flat valleys, juniper/pine woodlands, wetlands, etc *Various wildlife species The Hopi Reservation * Consists of Approximately 1.6- mil Acres * Population (Enrolled members) Approximately 12,500 plus * Approximately 7,500 residing on the reservation District #6 Main areas of occupation * 13 separate communities each independent and autonomous from the Tribal

  19. The structure-directed effect of Al-based metal–organic frameworks on fabrication of alumina by thermal treatment

    SciTech Connect (OSTI)

    Liu, Dandan; Dai, Fangna; Tang, Zhe; Liu, Yunqi; Liu, Chenguang

    2015-05-15

    Highlights: • We use Al-MOFs as precursor in the fabrication process of mesoporous alumina by thermal treatment. • The obtained mesoporous alumina has dual pore system and five-fold aluminum. • The aluminum building units in the precursor show structure-directed effect on the formation of alumina. - Abstract: In this work, the block-shaped Al-based metal–organic frameworks (Al-MOFs) MIL-53 have been synthesized by hydrothermal method. To detect the correlation between the structure of Al-MOFs and the formation of alumina, the ligands are eliminated by thermal treatment. MIL-53 and the calcination products were characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM), transmission electron microscopy (TEM), nitrogen adsorption–desorption and solid-state {sup 27}Al nuclear magnetic resonance ({sup 27}Al NMR). It was found that after calcination, the block-shaped Al-MOFs precursor turns into high-crystallinity mesoporous alumina nanosheets, and the thermal treatment product γ-alumina possesses a dual pore system and a large surface area (146 m{sup 2}/g), with five-fold aluminum. During the thermal treatment process, the structure of MIL-53 and its secondary building units have structure-directed effect in the formation of alumina.

  20. Prediction of external corrosion for steel cylinders at the Paducah Gaseous Diffusion Plant: Application of an empirical method

    SciTech Connect (OSTI)

    Lyon, B.F.

    1996-02-01

    During the summer of 1995, ultrasonic wall thickness data were collected for 100 steel cylinders containing depleted uranium (DU) hexafluoride located at Paducah Gaseous Diffusion Plant (PGDP) in Paducah, Kentucky. The cylinders were selected for measurement to assess the condition of the more vulnerable portion of the cylinder inventory at PGDP. The purpose of this report is to apply the method used in Lyon to estimate the effects of corrosion for larger unsampled populations as a function of time. The scope of this report is limited and is not intended to represent the final analyses of available data. Future efforts will include continuing analyses of available data to investigate defensible deviations from the conservative assumptions made to date. For each cylinder population considered, two basic types of analyses were conducted: (1) estimates were made of the number of cylinders as a function of time that will have a minimum wall thickness of either 0 mils (1 mil = 0.00 1 in.) or 250 mils and (2) the current minimum wall thickness distributions across cylinders were estimated for each cylinder population considered. Additional analyses were also performed investigating comparisons of the results for F and G yards with the results presented in Lyon (1995).

  1. A Combined Experimental and Computational Study on the Stability of Nanofluids Containing Metal Organic Frameworks

    SciTech Connect (OSTI)

    Annapureddy, Harsha Vardhan Reddy; Nune, Satish K.; Motkuri, Radha K.; McGrail, B. Peter; Dang, Liem X.

    2015-01-23

    Computational studies on nanofluids composed of metal organic frameworks (MOFs) were performed using molecular modeling techniques. Grand Canonical Monte Carlo (GCMC) simulations were used to study adsorption behavior of 1,1,1,3,3-pentafluoropropane (R-245fa) in a MIL-101 MOF at various temperatures. To understand the stability of the nanofluid composed of MIL-101 particles, we performed molecular dynamics simulations to compute potentials of mean force between hypothetical MIL-101 fragments terminated with two different kinds of modulators in R-245fa and water. Our computed potentials of mean force results indicate that the MOF particles tend to disperse better in water than in R-245fa. The reasons for this observation were analyzed and discussed. Our results agree with experimental results indicating that the employed potential models and modeling approaches provide good description of molecular interactions and the reliabilities. Work performed by LXD was supported by the U.S. Department of Energy (DOE), Office of Basic Energy Sciences, Division of Chemical Sciences, Geosciences, and Biosciences. Work performed by HVRA, SKN, RKM, and PBM was supported by the Office of Energy Efficiency and Renewable Energy, Geothermal Technologies Program. Pacific Northwest National Laboratory is a multiprogram national laboratory operated for DOE by Battelle.

  2. Computational screening of large molecule adsorption by metal-organic frameworks.

    SciTech Connect (OSTI)

    Allendorf, Mark D.; Greathouse, Jeffery A.

    2010-04-01

    Grand canonical Monte Carlo simulations were performed to investigate trends in low-pressure adsorption of a broad range of organic molecules by a set of metal-organic frameworks (MOFs). The organic analytes considered here are relevant to applications in chemical detection: small aromatics (o-, m-, and p-xylene), polycyclic aromatic hydrocarbons (naphthalene, anthracene, phenanthrene), explosives (TNT and RDX), and chemical warfare agents (GA and VM). The framework materials included several Zn-MOFs (IRMOFs 1-3, 7, 8), a Cr-MOF (CrMIL-53lp), and a Cu-MOF (HKUST-1). Many of the larger organics were significantly adsorbed by the target MOFs at low pressure, which is consistent with the exceptionally high isosteric heats of adsorption (25 kcal/mol - 60 kcal/mol) for this range of analyte. At a higher loading pressure of 101 kPa, the Zn-MOFs show a much higher volumetric uptake than either CrMIL-53-lp or HKUST-1 for all types of analyte. Within the Zn-MOF series, analyte loading is proportional to free volume, and loading decreases with increasing analyte size due to molecular packing effects. CrMIL-53lp showed the highest adsorption energy for all analytes, suggesting that this material may be suitable for low-level detection of organics.

  3. Aging, Loss-of-Coolant Accident (LOCA), and high potential testing of damaged cables

    SciTech Connect (OSTI)

    Vigil, R.A.; Jacobus, M.J.

    1994-04-01

    Experiments were conducted to assess the effects of high potential testing of cables and to assess the survivability of aged and damaged cables under Loss-of-Coolant Accident (LOCA) conditions. High potential testing at 240 Vdc/mil on undamaged cables suggested that no damage was incurred on the selected virgin cables. During aging and LOCA testing, Okonite ethylene propylene rubber (EPR) cables with a bonded jacket experienced unexpected failures. The failures appear to be primarily related to the level of thermal aging and the presence of a bonded jacket that ages more rapidly than the insulation. For Brand Rex crosslinked polyolefin (XLPO) cables, the results suggest that 7 mils of insulation remaining should give the cables a high probability of surviving accident exposure following aging. The voltage necessary to detect when 7 mils of insulation remain on unaged Brand Rex cables is approximately 35 kVdc. This voltage level would almost certainly be unacceptable to a utility for use as a damage assessment tool. However, additional tests indicated that a 35 kvdc voltage application would not damage virgin Brand Rex cables when tested in water. Although two damaged Rockbestos silicone rubber cables also failed during the accident test, no correlation between failures and level of damage was apparent.

  4. Prediction of External Corrosion for Steel Cylinders--2007 Report

    SciTech Connect (OSTI)

    Schmoyer, Richard L

    2008-01-01

    Depleted uranium hexafluoride (DUF{sub 6}) is stored in over 62,000 containment cylinders at the Paducah Gaseous Diffusion Plant (PGDP) in Paducah, Kentucky, and at the Portsmouth Gaseous Diffusion Plant (PORTS) in Portsmouth, Ohio. Over 4,800 of the cylinders at Portsmouth were recently moved there from the East Tennessee Technology Park (ETTP) in Oak Ridge, Tennessee. The cylinders range in age up to 56 years and come in various models, but most are 48-inch diameter 'thin-wall'(312.5 mil) and 'thick-wall' (625 mil) cylinders and 30-inch diameter '30A' (including '30B') cylinders with 1/2-inch (500 mil) walls. Most of the cylinders are carbon steel, and they are subject to corrosion. The United States Department of Energy (DOE) manages the cylinders to maintain them and the DUF{sub 6} they contain. Cylinder management requirements are specified in the System Requirements Document (LMES 1997a), and the activities to fulfill them are specified in the System Engineering Management Plan (LMES 1997b). This report documents activities that address DUF{sub 6} cylinder management requirements involving measuring and forecasting cylinder wall thicknesses. As part of these activities, ultrasonic thickness (UT) measurements are made on samples of cylinders. For each sampled cylinder, multiple measurements are made in an attempt to find, approximately, the minimum wall thickness. Some cylinders have a skirt, which is an extension of the cylinder wall to protect the head (end) and valve. The head/skirt interface crevice is thought to be particularly vulnerable to corrosion, and for some skirted cylinders, in addition to the main body UT measurements, a separate suite of measurements is also made at the head/skirt interface. The main-body and head/skirt minimum thickness data are used to fit models relating minimum thickness to cylinder age, nominal thicknesses, and cylinder functional groups defined in terms of plant site, storage yard, top or bottom row storage positions, etc

  5. Adsorption and Separation of Light Gases on an Amino-Functionalized MetalOrganic Framework: An Adsorption and In Situ XRD Study

    SciTech Connect (OSTI)

    Couck S.; Stavitski E.; Gobehiya, E.; Kirschhock, C.E.A.; Serra-Crespo, P.; Juan-Alcaniz, J.; Martinez Joaristi, A.; Gascon, J.; Kapteijn, F.; Baron, G. V.; Denayer J.F.M.

    2012-02-29

    The NH{sub 2}-MIL-53(Al) metal-organic framework was studied for its use in the separation of CO{sub 2} from CH{sub 4}, H{sub 2}, N{sub 2} C{sub 2}H{sub 6} and C{sub 3}H{sub 8} mixtures. Isotherms of methane, ethane, propane, hydrogen, nitrogen, and CO{sub 2} were measured. The atypical shape of these isotherms is attributed to the breathing properties of the material, in which a transition from a very narrow pore form to a narrow pore form and from a narrow pore form to a large pore form occurs, depending on the total pressure and the nature of the adsorbate, as demonstrated by in-situ XRD patterns measured during adsorption. Apart from CO{sub 2}, all tested gases interacted weakly with the adsorbent. As a result, they are excluded from adsorption in the narrow pore form of the material at low pressure. CO{sub 2} interacted much more strongly and was adsorbed in significant amounts at low pressure. This gives the material excellent properties to separate CO{sub 2} from other gases. The separation of CO{sub 2} from methane, nitrogen, hydrogen, or a combination of these gases has been demonstrated by breakthrough experiments using pellets of NH{sub 2}-MIL-53(Al). The effect of total pressure (1-30 bar), gas composition, temperature (303-403 K) and contact time has been examined. In all cases, CO{sub 2} was selectively adsorbed, whereas methane, nitrogen, and hydrogen nearly did not adsorb at all. Regeneration of the adsorbent by thermal treatment, inert purge gas stripping, and pressure swing has been demonstrated. The NH{sub 2}-MIL-53(Al) pellets retained their selectivity and capacity for more than two years.

  6. OTVE combustor wall condition monitoring. Final report, November 1986-September 1988

    SciTech Connect (OSTI)

    Szemenyei, B.; Nelson, R.S.; Barkhoudarian, S.

    1989-08-01

    Conventional ultrasonics, eddy current, and electromagnetic acoustic transduction (EMAT) technologies were evaluated to determine their capability of measuring wall thickness/wear of individual cooling channels in test specimens simulating conditions in the throat region of an OTVE combustion chamber liner. Quantitative results are presented for the eddy current technology, which was shown to measure up to the optimum 20-mil wall thickness with near single channel resolution. Additional results demonstrate the capability of the conventional ultrasonics and EMAT technologies to detect a thinning or cracked wall. Recommendations for additional eddy current and EMAT development tests are presented.

  7. Gainache. Lori M From: Conrad, Jill A

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Gainache. Lori M From: Conrad, Jill A Setit:Friday, February 15, 2013 LOS PM TO: Alex Nazara-i Lale)(nazarali@ctuir~org), Alyssa Buck (Abuc k1gcrpLjd.Org), HNRTC Smith, Anthory; 'Rambi Rodriquez (ba mbirod riquez@ctu i .rg.)Y; 'Barbara Harper (barbaraharer@ctuir.com)'; HNRTC - Landeen, Dan, Dana Mil ler (drn1er@yrenr.com). Darla lackson (darlaijnezperce-org); Dave Rowland (b)(6) davidb@nezperce.org; Doreen Dogsleep {ddoogs een@ynerwm ~corn); HNRTC - Bohnee, Gabriel; 'George Klin~ger (gedrgek

  8. fy13 | netl.doe.gov

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    3 Archive Fiscal Year 2013 Solicitations POSTED DATE SOLICITATION/ FUNDING OPPORTUNITY ANNOUNCEMENT NUMBER SOLICITATION/FUNDING OPPORTUNITY ANNOUNCEMENT SUBJECT TITLE CLOSING DATE(S) DOE CONTACT 08/30/13 Request for Information R&D Aimed at Green House Gas (GHG) Emissions Reductions and Cost Competitiveness for Mil-Spec Jet Fuel Production Using Coal-to-Liquid (CTL) Fuel Technologies 09/30/13 A. Lopez 5/30/13 DE-FOA-0000805 Opportunity Notice for Parties Interested in Partnering with NETL

  9. Reliability analysis for LEB ring magnet power system in SSC

    SciTech Connect (OSTI)

    Smedley, K.

    1991-11-01

    The LEB ring magnet power system contains six subsystems, supervisory control, power supplies, regulation, DC bus, resonant cells, and fault sensing network. The system availability of the total LEB RMPS is required to be 0.999. The work in this paper is to allocate the overall LEB RMPS reliability requirement into reliability requirements for each of the subsystems and lower-tier items. The Feasibility-of-Objective technique combining with engineering experience is the key for the allocation. MIL-HDBK-217F is used to derate SCR components. 7 refs., 5 figs.

  10. Rulison Open

    Office of Legacy Management (LM)

    Control number -R-57 has been assigned t o t h i s report i n the Rulison Open his repon has been r e p i r d d d e c d y from the best mil.blc mpy. Available from the Sixvice; U. S. Department o f Commerce, Price: Papa m . 0 0 g . 9 . . Microfic DISCLAIMER Portions of this document may be illegible in electronic image products. Images are produced from the best available original document. r- r? I I ; i 1 1 j j I, L.-, j TABLE O F CONTENTS ',--.> r\ '-1 I >.\, i Subject 1 1 Page No. I L

  11. Measurements of prompt radiation induced conductivity of Kapton.

    SciTech Connect (OSTI)

    Preston, Eric F.; Zarick, Thomas Andrew; Sheridan, Timothy J.; Hartman, E. Frederick; Stringer, Thomas Arthur

    2010-10-01

    We performed measurements of the prompt radiation induced conductivity in thin samples of Kapton (polyimide) at the Little Mountain Medusa LINAC facility in Ogden, UT. Three mil samples were irradiated with a 0.5 {mu}s pulse of 20 MeV electrons, yielding dose rates of 1E9 to 1E10 rad/s. We applied variable potentials up to 2 kV across the samples and measured the prompt conduction current. Analysis rendered prompt conductivity coefficients between 6E-17 and 2E-16 mhos/m per rad/s, depending on the dose rate and the pulse width.

  12. Window for radiation detectors and the like

    DOE Patents [OSTI]

    Sparks, C.J. Jr.; Ogle, J.C.

    1975-10-28

    An improved x- and gamma-radiation and particle transparent window for the environment-controlling enclosure of various types of radiation and particle detectors is provided by a special graphite foil of a thickness of from about 0.1 to 1 mil. The graphite must have very parallel hexagonal planes with a mosaic spread no greater than 5$sup 0$ to have the necessary strength in thin sections to support one atmosphere or more of pressure. Such graphite is formed by hot- pressing and annealing pyrolytically deposited graphite and thereafter stripping off layers of sufficient thickness to form the window.

  13. Measurements of prompt radiation induced conductivity in Teflon (PTFE).

    SciTech Connect (OSTI)

    Hartman, E. Frederick; Zarick, Thomas Andrew; Sheridan, Timothy J.; Preston, E.

    2013-05-01

    We performed measurements of the prompt radiation induced conductivity (RIC) in thin samples of Teflon (PTFE) at the Little Mountain Medusa LINAC facility in Ogden, UT. Three mil (76.2 microns) samples were irradiated with a 0.5 %CE%BCs pulse of 20 MeV electrons, yielding dose rates of 1E9 to 1E11 rad/s. We applied variable potentials up to 2 kV across the samples and measured the prompt conduction current. Details of the experimental apparatus and analysis are reported in this report on prompt RIC in Teflon.

  14. High resolution collimator system for X-ray detector

    DOE Patents [OSTI]

    Eberhard, Jeffrey W.; Cain, Dallas E.

    1987-01-01

    High resolution in an X-ray computerized tomography (CT) inspection system is achieved by using a collimator/detector combination to limit the beam width of the X-ray beam incident on a detector element to the desired resolution width. In a detector such as a high pressure Xenon detector array, a narrow tapered collimator is provided above a wide detector element. The collimator slits have any desired width, as small as a few mils at the top, the slit width is easily controlled, and they are fabricated on standard machines. The slit length determines the slice thickness of the CT image.

  15. Microsoft Word - VECCHIO, Ken - ABSTRACT.docx

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    a Customer Accesses Green Button Data on PGE.com Step 1: Log in to pge.com account with username and password. Step 2: Click on "My Usage" tab. Step 3: Select "Download My Data" Step 4: Select "Export usage for specific days" then choose your date range and click "Export"

    K en V ecchio Founding C hair, D epartment o f N anoEngineering, U C S an D iego Synthetic M ultifunctional M aterials: Metallic---Intermetallic L aminate ( MIL) C omposites Title: S

  16. Technical evaluation of the noise and isolation testing of the reactor protection system for the Davis Besse Nuclear Power Station, Unit 1

    SciTech Connect (OSTI)

    Selan, J.C.

    1980-01-01

    This report documents the technical evaluation of the noise and isolation testing of the reactor protection system (RPS) for the Davis Besse Nuclear Power Station, Unit 1. The testing was performed in accordance to Section 4.6.11, Susceptibility, of MIL-N-19900B, and NRC approved plant test methods. Analysis of the test results shows that the reactor protection system did not degrade below acceptable levels when subjected to electromagnetic, electrostatic, isolation and noise level tests, nor was the system's ability to perform its Class 1E protective functions affected.

  17. Paint selection for coating radioactive-waste drums

    SciTech Connect (OSTI)

    Briggs, J.L.

    1980-07-01

    It is concluded that although the white epoxy Paint Sample E is suitable for coating waste drums, the additional pretreated costs of grit blasting prior to paint application would preclude adoption of that paint system. The specified 10.0-mil coating thickness of that coating would also incur higher costs. The Vorac epoxy-phenolic base paint (buff or yellow) was the only other paint that exhibited suitable corrosion and impact resistance required for coating the waste drums. In addition, that paint does not require a grit-blasted substrate or other costly pretreatment prior to coating.

  18. CPFF Appendix

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , 7/14/14) Cost Plus Fixed-Fee Services Appendix SFA-1 Page 1 of 8 Appendix SFA-1 FAR & DEAR Clauses Incorporated By Reference (a) The Federal Acquisition Regulation (FAR) and the Department of Energy Acquisition Regulation (DEAR) clauses which are incorporated by reference herein shall have the same force and effect as if printed in full text. (b) Full text of the referenced clauses may be accessed electronically at the following website addresses: FAR: http://farsite.hill.af.mil/vffara.htm

  19. METHOD FOR COATING GRAPHITE WITH NIOBIUM CARBIDE

    DOE Patents [OSTI]

    Kane, J.S.; Carpenter, J.H.; Krikorian, O.H.

    1962-01-16

    A method is given for coating graphite with a hard, tenacious layer of niobium carbide up to 30 mils or more thick. The method makes use of the discovery that niobium metal, if degassed and heated rapidly below the carburization temperature in contact with graphite, spreads, wets, and penetrates the graphite without carburization. The method includes the obvious steps of physically contacting niobium powders or other physical forms of niobium with graphite, degassing the assembly below the niobium melting point, e.g., 1400 deg C, heating to about 2200 to 2400 deg C within about 15 minutes while outgassing at a high volume throughput, and thereafter carburizing the niobium. (AEC)

  20. DOE Energy Exchange

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    DOE Energy Exchange Ms. Amanda Simpson 11 August 2015 www.oei.army.mil UNCLASSIFIED Assistant Secretary of the Army (Installations, Energy & Environment) Acts of Man Acts of Nature Securing the Homeland High-voltage power lines with grid connection to Redstone Arsenal devastated by tornado on April 26, 2011. (TVA) The scene of a shooting and oil spill at a San Jose PG&E substation on April 16, 2013 (CBS) Enhancing Energy Security Office of Energy Initiatives UNCLASSIFIED 2 Army

  1. PROP re-refined oil engine test performance

    SciTech Connect (OSTI)

    Linnard, R.E.

    1980-11-01

    Using conventional, commercially-available nonproprietary (to Phillips) additive treatments, engine test programs have successfully demonstrated Phillips Re-refined Oil Process (PROP) oils' compliance with the performance requirements of MIL-L-46152A and API Services SE/CC. This paper reports on the engine testing experience with PROP refined oils as produced in a full-scale 2 MM GPY PROP plant operating with Buyer-collected used oil feedstocks. Comment is also made on the status of the first two PROP plants, one built for the state of North Carolina and the other for Mohawk Oil Company, Ltd., Vancouver B.C., Canada.

  2. Hot rolling of thick uranium molybdenum alloys

    SciTech Connect (OSTI)

    DeMint, Amy L.; Gooch, Jack G.

    2015-11-17

    Disclosed herein are processes for hot rolling billets of uranium that have been alloyed with about ten weight percent molybdenum to produce cold-rollable sheets that are about one hundred mils thick. In certain embodiments, the billets have a thickness of about 7/8 inch or greater. Disclosed processes typically involve a rolling schedule that includes a light rolling pass and at least one medium rolling pass. Processes may also include reheating the rolling stock and using one or more heavy rolling passes, and may include an annealing step.

  3. ANL-FF-262i

    Office of Legacy Management (LM)

    , v-W&, ANL-FF-262i This document consists of 1 page, No.>f 7 copies. SeriesA. -,-- 22 February 1952 TO; B. Blumenthal Metallurgy From: H, Luetzow Metallurgy Re: HIGH PURITY CRANIUM TO BE ROLLID TO FOIL M r, E. Creutz of the Carnegie Institute of Technology has requested ten square inches of uranium foil 0.1 mil to 1 nil thick., The possibility of pro- ducing foil of this thickness from our foundry's graphite-melted uranium is remote because of the metalIs high carbon content. High purity

  4. Contents A

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    9 June/July 2004 Atlas Pulse Ready to Beat by Kirsten Kellogg In a June ceremony at the Nevada Test Site, the Atlas pulse power machine was welcomed into a family of above-ground capabilities to sup- port the NNSA Stockpile Stewardship Program. The dedication marked the end of a $20.7 mil- lion effort to bring Atlas to the test site from LANL. "Atlas is part of our effort to use means other than nuclear testing to answer questions about the conditions of our stockpile," said Everet

  5. Crowdsourcing Software Announcement | GE Global Research

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    GE, MIT Build Crowdsourcing Software Platform Click to email this to a friend (Opens in new window) Share on Facebook (Opens in new window) Click to share (Opens in new window) Click to share on LinkedIn (Opens in new window) Click to share on Tumblr (Opens in new window) GE, MIT Build Crowdsourcing Software Platform GE (NYSE: GE), with the Massachusetts Institute of Technology (MIT) and the Defense Advanced Research Agency (DARPA), is embarking on a program "vehicleforge.mil" to

  6. Long-term materials test program. Quarterly report, January-March 1983

    SciTech Connect (OSTI)

    1984-03-01

    Exposure of gas turbine materials to a PFBC effluent under the Long-Term Materials Test Program has reached 1507 hours. Unprotected nickel and cobalt base blade and vane alloys show susceptibility to hot corrosion at 1500/sup 0/F (gas temperature), 1300/sup 0/F, and 1100/sup 0/F (air-cooled pins). Precious metal aluminide and M (Co,Fe) CrAlY overlay coatings continue to show good resistance to corrosion above 1450/sup 0/F, but are susceptible to varying degrees of pitting attack between 1050 and 1300/sup 0/F. Significant erosion/corrosion degradation of both base alloys and protective coatings/claddings has been observed on airfoil specimens exposed at 1350/sup 0/F, 800 to 900 fps and dust loadings less than 100 ppM for 1085 hours. Corrosion predominately occurred in areas of direct particle impaction; i.e., leading edge and pressure surface, indicating an erosion/corrosion synergism. At gas velocities of 1200 to 1400 fps, a platinum-aluminide coated IN-738 pin experienced a metal recession rate of 8 mils/1000-hours. The PFBC facility continues to show excellent operational reliability, accumulating over 1100 test hours this quarter. The only concern from an operations standpoint is the gradual thinning of the in-bed heat exchanger tubing at a rate of about 5 mils/100 hours off the diameter.

  7. Prediction of External Corrosion for Steel Cylinders - 1998 Report

    SciTech Connect (OSTI)

    Lyon, B.F.

    1998-01-01

    The United States Department of Energy (DOE) currently manages the UF, Cylinder Project. The project was formed to maintain and safely manage depleted uranium hexafluoride (UF{sub 6}) stored in approximately 50,000 carbon steel cylinders. The cylinders located at three DOE sites: the K-25 site at Oak Ridge, Tennessee (K-25); the Paducah Gaseous Diffusion Plant in Paducah, Kentucky (PGDP), and the Portsmouth Gaseous Diffusion Plant (PORTS) in Portsmouth, Ohio. The System Requirements Document (SRD) (LMES 1997a) delineates the requirements of the project. The appropriate actions needed to fulfill these requirements are then specified within the System Engineering Management Plan (SEMP) (LMES 1997b). The report presented herein documents activities that in whole or in part satisfy specific requirements and actions stated in the UF{sub 6} Cylinder Project SRD and SEMP with respect to forecasting cylinder conditions. The wall thickness projections made in this report are based on the assumption that the corrosion trends noted will continue. Some activities planned may substantially reduce the rate of corrosion, in which case the results presented here are conservative. The results presented here are intended to supercede and enlarge the scope of those presented previously (Lyon 1995,1996, 1997). In particular, projections are made for thin-walled cylinders (nominal initial thickness 312.5 mils) and thick-walled cylinders (nominal initial thickness 625 mils). In addition, a preliminary analysis is conducted for the minimum thickness at the head/skirt interface for skirted cylinders.

  8. The economic impact of removing chloride from closed-loop wet limestone FGD systems. Volume 1. Final report

    SciTech Connect (OSTI)

    Phillips, J.L.; Horton, W.M.

    1995-01-01

    High chloride concentrations in wet limestone FGD systems increase the corrosion rates of certain materials and decrease SO{sub 2} removal efficiency and limestone utilization. This study revealed four different technologies that could be used to control chloride concentrations in closed-loop wet limestone FGD systems: reverse osmosis, electrodialysis reversal, vapor compression evaporation, and duct injection. This two-volume report describes each option in detail, discusses the basis for selecting the chloride threshold levels along with approximate cost estimates for combined chloride removal and waste disposal options, and presents flow sheets and detailed material balances for the least-cost combined options. The total annualized costs for chloride removal and waste disposal estimated in this study for a 300-MW plant range from 0.8 to 1.3 mils/kWh for controlling chloride at 3000 ppm to prevent corrosion and range from 0.3 to 0.7 mils/kWh for controlling chloride at 15,000 ppm to prevent decreased SO{sub 2} removal. The design coal has a relatively high chloride-to-sulfur ratio; costs for other coals would be lower.

  9. The economic impact of removing chloride from closed-loop wet limestone GFD systems. Volume 2. Final report

    SciTech Connect (OSTI)

    Phillips, J.L.; Horton, W.M.

    1995-01-01

    High chloride concentrations in wet limestone FGD systems increase the corrosion rates of certain materials and decrease SO{sub 2} removal efficiency and limestone utilization. This study revealed four different technologies that could be used to control chloride concentrations in closed-loop wet limestone FGD systems: reverse osmosis, electrodialysis reversal, vapor compression evaporation, and duct injection. This two-volume report describes each option in detail, discusses the basis for selecting the chloride threshold levels along with approximate cost estimates for combined chloride removal and waste disposal options, and presents flow sheets and detailed material balances for the least-cost combined options. The total annualized costs for chloride removal and waste disposal estimated in this study for a 300-MW plant range from 0.8 to 1.3 mils/kWh for controlling chloride at 3000 ppm to prevent corrosion and range from 0.3 to 0.7 mils/kWh for controlling chloride at 15,000 ppm to prevent decreased SO{sub 2} removal. The design coal has a relatively high chloride-to-sulfur ratio; costs for other coals would be lower.

  10. Effect of sulfur isotopic composition of zinc and lead sulfides on the E. M. F. of electrochemical cells

    SciTech Connect (OSTI)

    Lusk, J.; Krouse, H.R.; Batts, B.D.

    1988-03-01

    A new effect is reported in which unexpectedly large voltages are produced by electrochemical cells containing sulfides at natural isotopic abundance levels. Room temperature experiments were undertaken to determine whether electrochemical cells employing silver bromide and silver beta alumina as solid electrolytes would be sufficiently sensitive to detect small variations in sulfur isotopic composition for zinc and lead sulfides. Voltages obtained for silver bromide cells tended to increase progressively over at least 20 days, and increased in a regular fashion with increasing differences in isotopic composition between charges. Voltages exceeding 150 mV were obtained for /sup delta/S/sup 3,4/ differences up to 85 per mil for zinc sulfide, but reached only about 20 mV for lead sulfide. Silver beta alumina cells with opposing zinc and lead sulfide charges yielded larger voltages and E.M.F. minimum corresponding to a +8(/plus minus/2) per mil difference. This value shows reasonable agreement with interpolated 20/degrees/C equilibrium values of between +7.5 to +9.8 obtained from the literature. Matured silver bromide cells with opposed zinc and lead sulfide charges behaved similarly but yielded lower voltages. Silver concentration cells of the opposed type are thus able to detect isotopic equilibrium and this will permit calibration of sulfur isotope thermometers down to unexpectedly low temperatures.

  11. Atmospheric corrosion monitoring at the US Department of Energy`s Oak Ridge K-25 Site

    SciTech Connect (OSTI)

    Rao, M.

    1995-12-31

    Depleted uranium hexafluoride (UF{sub 6}) at the US Department of Energy`s K-25 Site at Oak Ridge, TN has been stored in large steel cylinders which have undergone significant atmospheric corrosion damage over the last 35 years. A detailed experimental program to characterize and monitor the corrosion damage was initiated in 1992. Large amounts of corrosion scale and deep pits are found to cover cylinder surfaces. Ultrasonic wall thickness measurements have shown uniform corrosion losses up to 20 mils (0.5 mm) and pits up to 100 mils (2.5 mm) deep. Electrical resistance corrosion probes, time-of-wetness sensors and thermocouples have been attached to cylinder bodies. Atmospheric conditions are monitored using rain gauges, relative humidity sensors and thermocouples. Long-term (16 years) data are being obtained from mild steel corrosion coupons on test racks as well as attached directly to cylinder surfaces. Corrosion rates have been found to intimately related to the times-of-wetness, both tending to be higher on cylinder tops due to apparent sheltering effects. Data from the various tests are compared, discrepancies are discussed and a pattern of cylinder corrosion as a function of cylinder position and location is described.

  12. Safety evaluation for packaging CPC metal boxes

    SciTech Connect (OSTI)

    Romano, T.

    1995-05-15

    This Safety Evaluation for Packaging (SEP) provides authorization for the use of Container Products Corporation (CPC) metal boxes, as described in this document, for the interarea shipment of radioactive contaminated equipment and debris for storage in the Central Waste Complex (CWC) or T Plant located in the 200 West Area. Authorization is granted until November 30, 1995. The CPC boxes included in this SEP were originally procured as US Department of Transportation (DOT) Specification 7A Type A boxes. A review of the documentation provided by the manufacturer revealed the documentation did not adequately demonstrate compliance to the 4 ft drop test requirement of 49 CFR 173.465(c). Preparation of a SEP is necessary to document the equivalent safety of the onsite shipment in lieu of meeting DOT packaging requirements until adequate documentation is received. The equivalent safety of the shipment is based on the fact that the radioactive contents consist of contaminated equipment and debris which are not dispersible. Each piece is wrapped in two layers of no less than 4 mil plastic prior to being placed in the box which has an additional 10 mil liner. Pointed objects and sharp edges are padded to prevent puncture of the plastic liner and wrapping.

  13. 55-Gallon Drum Attenuation Corrections for Waste Assay Measurements

    SciTech Connect (OSTI)

    Casella, V.R.

    2002-04-03

    The present study shows how the percent attenuation for low-level waste (LLW), carbon-steel 55-gallon drums (44 and 46 mil) and for transuranic (TRU) DOT Type 7A 55-gallon drums (approximately 61 mil) changes with gamma energy from 60 keV to 1400 keV. Attenuation for these drums is in the range of 5 to 15 percent at energies from 400 to 1400 keV and from 15 to 35 percent at energies from 120 to 400 keV. At 60 keV, these drums attenuate 70-80 percent of the gamma rays. Correction factors were determined in order to correct for gamma attenuation of a TRU drum if a calibration is performed with a LLW drum. These correction factors increase the activities of the TRU drum by from 10 percent to 2 percent in the energy range of 165 to 1400 keV, with an increase of about 50 percent at 60 keV. Correction factors for TRU drums and for analyses without a drum were used to adjust the percent yield for frequently measured gamma rays, so that the assay libraries could be modified to provide the drum attenuation corrections.

  14. Thermal reliability and performance improvement of close-coupled catalytic converter

    SciTech Connect (OSTI)

    Hijikata, Toshihiko; Kurachi, Hiroshi; Katsube, Fumio; Honacker, H. van

    1996-09-01

    This paper proposes a high temperature catalytic converter design using a ceramic substrate and intumescent matting. It also describes the improvement of converter performance using an advanced thin wall ceramic substrate. Due to future tightening of emission regulations and improvement of fuel economy, higher exhaust gas temperatures are suggested. Therefore, reduction of thermal reliability of an intumescent mat will be a concern because the catalytic converter will be exposed to high temperatures. For this reason, a new design converter has been developed using a dual cone structure for both the inlet and outlet cones. This minimizes heat conduction through the cone and decreases the temperature affecting the mat area. This design converter, without the use of a heat-shield, reduces the converter surface temperature to 441 C despite a catalyst bed temperature of 1,050 C. The long term durability of the converter is demonstrated by the hot vibration test. Since the new design converter does not need a heat-shield, the catalyst diameter can be enlarged by the width of the air gap used in the current design converter. By using an advanced thin wall ceramic substrate, such as 0.11 mm/620 kcpsm (4 mil/400 cpsi), it is possible to improve emission performance and pressure drop compared with the conventional 0.16 mm/620 kcpsm (6 mil/400 cpsi) ceramic substrate.

  15. Cathodic Protection of the Yaquina Bay Bridge

    SciTech Connect (OSTI)

    Bullard, Sophie J.; Cramer, Stephen D.; Covino, Bernard S., Jr.; Holcomb, Gordon R.; Russell, James H.; Laylor, H.M.; Cryer, C.B.

    2001-02-01

    The Yaquina Bay Bridge in Newport, Oregon, was designed by Conde B. McCullough and built in 1936. The 3,223-foot (982 m) structure is a combination of concrete arch approach spans and a steel through arch over the shipping channel. Cathodic protection is used to prevent corrosion damage to the concrete arches. The Oregon Department of Transportation (Oregon DOT) installed a carbon anode coating (DAC-85) on two of the north approach spans in 1985. This anode was operated at a current density of 6.6 mA/m2(0.6 mA/ft2). No failure of the conductive anode was observed in 1990, five years after application, or in 2000, 15 years after application. Thermal-sprayed zinc anodes 20 mils (0.5 mm) thick were applied to half the south approach spans beginning in 1990. Thermal-sprayed zinc anodes 15 mils (0.4 mm) thick were applied to the remaining spans in 1996. These anodes were operated at a current density of 2.2 mA/m2(0.2 mA/ft2). In 1999, four zones on the approach spans were included in a two-year field trial of humectants to improve zinc anode performance. The humectants LiNO3 and LiBr were applied to two zones; the two adjacent zones were left untreated as controls. The humectants substantially reduced circuit resistance compared to the controls.

  16. Prediction of External Corrosion for Steel Cylinders--2002 Report

    SciTech Connect (OSTI)

    Schmoyer, RLS

    2002-07-31

    The United States Department of Energy (DOE) manages the UF{sub 6} Cylinder Project. The project was formed to maintain and safely manage the depleted uranium hexafluoride (UF{sub 6}) stored in approximately 50,000 carbon steel cylinders. The cylinders are located at three DOE sites: the East Tennessee Technology Park (ETTP) site in Oak Ridge, Tennessee; the Paducah Gaseous Diffusion Plant (PGDP) in Paducah, Kentucky, and the Portsmouth Gaseous Diffusion Plant (PORTS) in Portsmouth, Ohio. The System Requirements Document (SRD) (LMES 1997a) delineates the requirements of the project, and the actions needed to fulfill these requirements are specified in the System Engineering Management Plan (SEMP) (LMES 1997b). This report documents activities that in whole or part satisfy specific requirements and actions stated in the UF{sub 6} Cylinder Project SRD and SEMP with respect to forecasting cylinder conditions. The results presented here supercede those presented by Lyon (1995, 1996, 1997, 1998, 2000), and Schmoyer and Lyon (2001). Many of the wall thickness projections made in this report are conservative, because they are based on the assumption that corrosion trends will continue, despite activities such as improved monitoring, relocations to better storage, painting, and other improvements in storage conditions relative to the conditions at the times most of the wall thickness measurements were made. For thin-wall cylinders (design nominal wall thickness 312.5 mils), the critical minimum wall thicknesses criteria used in this report are 0 (breach), 62.5 mils, and 250 mils (1 mil = 0.001 in.). For thick-wall cylinders (design nominal wall thickness 625 mils), the thickness criteria used in this report are 0, 62.5 mils, and 500 mils. The criteria triples are preliminary boundaries identified within the project that indicate (1) loss of material (UF{sub 6}), (2) safe handling and stacking operations, and (3) standards for off-site transport and contents transfer

  17. Correlation of Process Data and Electrochemical Noise to Assess Kraft Digester Corrosion: Spring Grove Experiment

    SciTech Connect (OSTI)

    Pawel, SJ

    2003-06-18

    Electrochemical noise (ECN) probes were deployed in a carbon steel continuous kraft digester at four locations and at one location in the bottom cone of the associated flash tank. The probes consisted of carbon steel electrodes, representing the vessel construction material, and 309LSi stainless steel overlay electrodes, representing the weld overlay repair in a portion of the vessel. Current and potential noise, the temperature at each probe location, and the value of about 32 process parameters (flow rates, liquor chemistry, etc.) were monitored continuously for a period of almost one year. Historical vessel inspection data and post-test evaluation of the probe components were used to assess/compare ECN corrosion activity with physical changes in wall thickness and corrosion patterns on the digester shell. In addition, attempts were made to correlate ECN activity from each electrode type with process parameters. The results indicate the high general corrosion rates of steel observed just below the extraction screens--on the order of 35 mils/y for the past few years--accelerated further during the period of probe deployment. The maximum wastage of steel (normalized to one full year exposure) was about 85 mils/y at the ring 6N probe just below the extraction screens. Consistent with recent historical observations, the steel corrosion rate at the ring 6S probe--at the same elevation but directly across the digester from ring 6N--was significantly lower at about 50 mils/y. Just prior to probe deployment, the digester shell below the extraction screens was overlaid with 309LSi stainless steel, which was observed to be essentially immune to corrosion at this location. While the ECN probes detected differences in electrochemical behavior between steel probes and between 309LSi probes at rings 6N and 6S, there was only poor quantitative correlation of current sums with actual corrosion rates at these locations. A significant contribution of redox reactions on both steel

  18. Pulsed-field gel electrophoresis and radiation hybrid mapping analyses enable the ordering of eleven DNA loci in Xq22

    SciTech Connect (OSTI)

    O'Reilly, M.A.; Alterman, L.A.; Zijlstra, J.; Malcolm, S.; Levinsky, R.J.; Kinnon, C. )

    1993-02-01

    The Xq22 region of the human X chromosome encompasses the loci of several genes and random DNA markers whose relative positions have not been determined. By a combination of PFGE mapping and the analysis of a selected panel of X chromosome radiation hybrid cell lines, we have constructed physical maps of Xq22 that order a total of 11 polymorphic and nonpolymorphic DNA markers. Ten of these probes have been linked physically into three separate clusters, spanning nearly 6 Mb of DNA in total. The DXS94, DXS147, DXS211, DXS17, and DXS87 loci are all present on a 2.7-Mb MluI fragment; PLP, DXS54, DXS24, and DXS83 are present on MluI fragments spanning over 1.6 Mb; and DXS178 is present on a 1.5-Mb MluI fragment. Mapping with additional enzymes has allowed the further ordering of these loci with respect to each other. Together with these data, analysis of a small set of radiation hybrids has suggested the following overall order of loci with Xq22; centromere-DCS178-DXS94-DXS147-DXS211-DXS17-DXS87-PLP-DXS54-DXS24-DXS83-DOL4A5-telomere. The ordering of these random DNA markers, genes, and disease loci, including the genes responsible for Pelizaeus-Merzbacher disease and Alport syndrome, indicates DNA markers that could be of further use clinically for these diseases. Furthermore, this map should form a basis for the refinement of additional disease-associated loci in this region. 32 refs., 4 figs., 2 tabs.

  19. OTVE turbopump condition monitoring, task E. 5. Final report, October 1988-September 1989

    SciTech Connect (OSTI)

    Coleman, P.T.; Collins, J.J.

    1989-08-01

    Recent work has been carried out on development of isotope wear analysis and optical and eddy current technologies to provide bearing wear measurements and real time monitoring of shaft speed, shaft axial displacement and shaft orbit of the Orbit Transfer Vehicle hydrostatic bearing tester. Results show shaft axial displacement can be optically measured (at the same time as shaft orbital motion and speed) to within 0.3 mils by two fiberoptic deflectometers. Evaluation of eddy current probes showed that, in addition to measuring shaft orbital motion, they can be used to measure shaft speed without having to machine grooves on the shaft surface as is the usual practice for turbomachinery. The interim results of this condition monitoring effort are presented.

  20. H O

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    O I - * , TWl rrporl «lf pnpmd u u iccouni of work fponiortd by fbc Unfad Suirs Gomuncnl. KtHka U» Unllii s u m nor Ih. Vaiui SHIM Atomic EnotT Comminjon, oar cur or tncir cnptoynf. nor Mr of ihtk caatrutott, ubcoRtmuirB, or tlwk cmptorra. milMsuir w n a f r . «prM§orimp&cd.of iMnmauy _ { l i . UBl Ibbililr or raponiiMlitr ror Ui. n e o n , , cum- *** pUUuu or tmfol«B or W larornutloa. ippiniia. proaoct or procac rfiKlowd. or rtprucnu Out iu use would not fafrinf* pririirly owned

  1. Erosion enhanced corrosion in superheaters

    SciTech Connect (OSTI)

    Bakker, W.T.; Mitra, S.M.

    1994-12-31

    Abnormal high metal wastage rates were discovered in the reheater of a boiler at the Williams Station on South Carolina Electric and Gas Company, which had been converted from oil to coal firing in 1983. Originally, liquid coal ash corrosion was suspected as the cause of the accelerated corrosion. To confirm this, test spools of austenitic alloys with varying chromium content were installed in the most corrosion prone areas and exposed for 17,431 hrs. It was found that the metal loss rate, ranged from 15--21 mils/yr was independent of the chromium content of the alloy. Microscopic examination indicated that the high corrosion rate was probably due to alternating oxidizing and reducing conditions, which caused the formation of iron and sulfur rich scales, enhanced by fly ash erosion in areas of high gas velocity.

  2. Method of producing novel silicon carbide articles. [Patent application

    DOE Patents [OSTI]

    Milewski, J.V.

    1982-06-18

    A method of producing articles comprising reaction-bonded silicon carbide (SiC) and graphite (and/or carbon) is given. The process converts the graphite (and/or carbon) in situ to SiC, thus providing the capability of economically obtaining articles made up wholly or partially of SiC having any size and shape in which graphite (and/or carbon) can be found or made. When the produced articles are made of an inner graphite (and/or carbon) substrate to which SiC is reaction bonded, these articles distinguish SiC-coated graphite articles found in the prior art by the feature of a strong bond having a gradual (as opposed to a sharply defined) interface which extends over a distance of mils. A method for forming SiC whisker-reinforced ceramic matrices is also given. The whisker-reinforced articles comprise SiC whiskers which substantially retain their structural integrity.

  3. Free-piston Stirling engine experimental program: Part 2. An evaluation of loss mechanisms

    SciTech Connect (OSTI)

    Moynihan, T.; Berggren, R.; Dochat, G.

    1983-06-01

    A series of experiments is described in which measurements were taken on a free-piston Stirling engine to isolate effects believed to degrade engine performance. The effects examined were: compression-space hysteresis, regenerator losses, displacer seal clearance loss, and displacer appendix gap loss. The experimental data from these experiments are given and represent a valuable resource for validation of Stirling engine analysis methods. The most significant of the above effects was found to be the clearance between the displacer and cylinder wall. Best performance was attained by a close clearance seal of 2 mils. Greater clearances or use of a piston ring degraded performance. Overall efficiency of the engine was raised several points due to this finding.

  4. Measurements of prompt radiation induced conductivity of alumina and sapphire.

    SciTech Connect (OSTI)

    Hartman, E. Frederick; Zarick, Thomas Andrew; Sheridan, Timothy J.; Preston, Eric F.

    2011-04-01

    We performed measurements of the prompt radiation induced conductivity in thin samples of Alumina and Sapphire at the Little Mountain Medusa LINAC facility in Ogden, UT. Five mil thick samples were irradiated with pulses of 20 MeV electrons, yielding dose rates of 1E7 to 1E9 rad/s. We applied variable potentials up to 1 kV across the samples and measured the prompt conduction current. Analysis rendered prompt conductivity coefficients between 1E10 and 1E9 mho/m/(rad/s), depending on the dose rate and the pulse width for Alumina and 1E7 to 6E7 mho/m/(rad/s) for Sapphire.

  5. Development of optimized PPP insulated pipe-cable systems in the commercial voltage range. Final report

    SciTech Connect (OSTI)

    Allam, E.M.; McKean, A.L.

    1992-05-01

    The primary objectives of this project included the development of an alternate domestic source of Paper-Polypropylene-Paper (PPP) laminate and the development of optimized designs for PPP-insulated pipe-type cable systems in the commercial voltage range. The development of a domestic source of PPP laminate was successfully completed. This laminate was utilized throughout the program for fabrication of full-size prototype cables submitted for laboratory qualification tests. Selected cables at rated voltages of 138, 230 and 345kV have been designed, fabricated and subjected to the series of qualification tests leading to full laboratory qualification. An optimized design of 2000 kcmil, 345kV cable insulated with 600 mils of domestic PPP laminate was fabricated and successfully passed all laboratory qualification tests. This cable design was subsequently installed at Waltz Mill to undergo the series of field tests leading to full commercial qualification.

  6. Development of optimized PPP insulated pipe-cable systems in the commercial voltage range

    SciTech Connect (OSTI)

    Allam, E.M.; McKean, A.L. )

    1992-05-01

    The primary objectives of this project included the development of an alternate domestic source of Paper-Polypropylene-Paper (PPP) laminate and the development of optimized designs for PPP-insulated pipe-type cable systems in the commercial voltage range. The development of a domestic source of PPP laminate was successfully completed. This laminate was utilized throughout the program for fabrication of full-size prototype cables submitted for laboratory qualification tests. Selected cables at rated voltages of 138, 230 and 345kV have been designed, fabricated and subjected to the series of qualification tests leading to full laboratory qualification. An optimized design of 2000 kcmil, 345kV cable insulated with 600 mils of domestic PPP laminate was fabricated and successfully passed all laboratory qualification tests. This cable design was subsequently installed at Waltz Mill to undergo the series of field tests leading to full commercial qualification.

  7. Solar cell array interconnects

    DOE Patents [OSTI]

    Carey, P.G.; Thompson, J.B.; Colella, N.J.; Williams, K.A.

    1995-11-14

    Electrical interconnects are disclosed for solar cells or other electronic components using a silver-silicone paste or a lead-tin (Pb-Sn) no-clean fluxless solder cream, whereby the high breakage of thin (<6 mil thick) solar cells using conventional solder interconnect is eliminated. The interconnects of this invention employs copper strips which are secured to the solar cells by a silver-silicone conductive paste which can be used at room temperature, or by a Pb-Sn solder cream which eliminates undesired residue on the active surfaces of the solar cells. Electrical testing using the interconnects of this invention has shown that no degradation of the interconnects developed under high current testing, while providing a very low contact resistance value. 4 figs.

  8. Solar cell array interconnects

    DOE Patents [OSTI]

    Carey, Paul G.; Thompson, Jesse B.; Colella, Nicolas J.; Williams, Kenneth A.

    1995-01-01

    Electrical interconnects for solar cells or other electronic components using a silver-silicone paste or a lead-tin (Pb-Sn) no-clean fluxless solder cream, whereby the high breakage of thin (<6 mil thick) solar cells using conventional solder interconnect is eliminated. The interconnects of this invention employs copper strips which are secured to the solar cells by a silver-silicone conductive paste which can be used at room temperature, or by a Pb-Sn solder cream which eliminates undesired residue on the active surfaces of the solar cells. Electrical testing using the interconnects of this invention has shown that no degradation of the interconnects developed under high current testing, while providing a very low contact resistance value.

  9. Regional

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    3 AÇORIANO ORIENTAL SEGUNDA-FEIRA, 5 DE MARÇO DE 2012 PUB Da Graciosa para a Índia graças à estação atmosférica Carlos está atualmente a trabalhar na estação atmosférica móvel instalada na Índia, a dois mil metros de altitude Estar no lugar certo na hora cer- ta pode mudar radicalmente a vida de uma pessoa. Foi isso que aconteceu ao graciosense Carlos Sousa, de 41 anos, que começou por ser trabalhador daconstrução civil antes de emigrar para os Es- tados Unidos da América. No

  10. The development of compact magnetic quadrupoles for ILSE

    SciTech Connect (OSTI)

    Faltens, A.; Mukherjee, S.; Brady, V.

    1990-08-01

    Magnetic focussing is selected for the 4 MeV to 10 MeV section of the Induction Linac Systems Experiments (ILSE) to study the transport of magnetically focussed spacecharge-dominated beams and to explore the engineering problems in accurate positioning of the magnetic fields in an array of quadrupoles. A prototype development program for such magnets is currently under way. A compact design was selected to decrease the overall accelerator diameter and its cost. The design evolved from a cosine 2{theta} current distribution, corrected for end effects. Current-dominated magnets are used in a pulsed mode to allow higher current densities compared to standard dc water-cooled conductors. The POISSON and MAFCO codes were used in the design of the magnets. The construction of the quadrupoles is aimed at achieving location accuracy of the magnetic center to within 1 mil (2.54 {times} 10{sup {minus}5} m) of the mechanical center.

  11. Active alignment/contact verification system

    DOE Patents [OSTI]

    Greenbaum, William M.

    2000-01-01

    A system involving an active (i.e. electrical) technique for the verification of: 1) close tolerance mechanical alignment between two component, and 2) electrical contact between mating through an elastomeric interface. For example, the two components may be an alumina carrier and a printed circuit board, two mating parts that are extremely small, high density parts and require alignment within a fraction of a mil, as well as a specified interface point of engagement between the parts. The system comprises pairs of conductive structures defined in the surfaces layers of the alumina carrier and the printed circuit board, for example. The first pair of conductive structures relate to item (1) above and permit alignment verification between mating parts. The second pair of conductive structures relate to item (2) above and permit verification of electrical contact between mating parts.

  12. Treasury, Postal Approp's Act (11/19/95) PL 104-52

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    FY 96 Appropriations Chronology (Draft) CR (9/30/95) went through 11/13 PL 104-31 MilCon Approp's Act (10/3/95) PL 104-32 Agriculture Approp's Act (10/21/95) PL 104-37 Energy/Water Approp's Act (11/13/95) PL 104-46 Transportation Approp's Act (11/15/95) PL 104-50 Treasury, Postal Approp's Act (11/19/95) PL 104-52 Legislative Approp's Act (11/19/95) PL 104-53 CR (11/19/95) 11/14 through 11/20 PL 104-54 CR (11/20/95) through 12/15 PL 104-56 Defense Approp's Act (12/1/95) PL 104-61 Approp's for

  13. Method of producing silicon carbide articles

    DOE Patents [OSTI]

    Milewski, John V.

    1985-01-01

    A method of producing articles comprising reaction-bonded silicon carbide (SiC) and graphite (and/or carbon) is given. The process converts the graphite (and/or carbon) in situ to SiC, thus providing the capability of economically obtaining articles made up wholly or partially of SiC having any size and shape in which graphite (and/or carbon) can be found or made. When the produced articles are made of an inner graphite (and/or carbon) substrate to which SiC is reaction bonded, these articles distinguish SiC-coated graphite articles found in the prior art by the feature of a strong bond having a gradual (as opposed to a sharply defined) interface which extends over a distance of mils. A method for forming SiC whisker-reinforced ceramic matrices is also given. The whisker-reinforced articles comprise SiC whiskers which substantially retain their structural integrity.

  14. Fluorocarbon Adsorption in Hierarchical Porous Frameworks

    SciTech Connect (OSTI)

    Motkuri, Radha K.; Annapureddy, Harsha V.; Vijayakumar, M.; Schaef, Herbert T.; Martin, P F.; McGrail, B. Peter; Dang, Liem X.; Krishna, Rajamani; Thallapally, Praveen K.

    2014-07-09

    The adsorption behavior of a series of fluorocarbon derivatives was examined on a set of microporous metal organic framework (MOF) sorbents and another set of hierarchical mesoporous MOFs. The microporous M-DOBDC (M = Ni, Co) showed a saturation uptake capacity for R12 of over 4 mmol/g at a very low relative saturation pressure (P/Po) of 0.02. In contrast, the mesoporous MOF MIL-101 showed an exceptionally high uptake capacity reaching over 14 mmol/g at P/Po of 0.4. Adsorption affinity in terms of mass loading and isosteric heats of adsorption were found to generally correlate with the polarizability of the refrigerant with R12 > R22 > R13 > R14 > methane. These results suggest the possibility of exploiting MOFs for separation of azeotropic mixtures of fluorocarbons and use in eco-friendly fluorocarbon-based adsorption cooling and refrigeration applications.

  15. Process for electrically interconnecting electrodes

    DOE Patents [OSTI]

    Carey, Paul G.; Thompson, Jesse B.; Colella, Nicolas J.; Williams, Kenneth A.

    2002-01-01

    Electrical interconnects for solar cells or other electronic components using a silver-silicone paste or a lead-tin (Pb--Sn) no-clean fluxless solder cream, whereby the high breakage of thin (<6 mil thick) solar cells using conventional solder interconnect is eliminated. The interconnects of this invention employs copper strips which are secured to the solar cells by a silver-silicone conductive paste which can be used at room temperature, or by a Pb--Sn solder cream which eliminates undesired residue on the active surfaces of the solar cells. Electrical testing using the interconnects of this invention has shown that no degradation of the interconnects developed under high current testing, while providing a very low contact resistance value.

  16. Formation mechanism of the secondary building unit in a chromium terephthalate metal-organic framework

    SciTech Connect (OSTI)

    Cantu Cantu, David; McGrail, B. Peter; Glezakou, Vassiliki Alexandra

    2014-09-18

    Based on density functional theory calculations and simulation, a detailed mechanism is presented on the formation of the secondary building unit (SBU) of MIL-101, a chromium terephthalate metal-organic framework (MOF). SBU formation is key to MOF nucleation, the rate-limiting step in the formation process of many MOFs. A series of reactions that lead to the formation of the SBU of MIL-101 is proposed in this work. Initial rate-limiting reactions form the metal cluster with three chromium (III) atoms linked to a central bridging oxygen. Terephthalate linkers play a key role as chromium (III) atoms are joined to linker carboxylate groups prior to the placement of the central bridging oxygen. Multiple linker addition reactions, which follow in different paths due to structural isomers, are limited by the removal of water molecules in the first chromium coordination shell. The least energy path is identified were all linkers on one face of the metal center plane are added first. A simple kinetic model based on transition state theory shows the rate of secondary building unit formation similar to the rate metal-organic framework nucleation. The authors are thankful to Dr. R. Rousseau for a critical reading of the manuscript. This research would not have been possible without the support of the Office of Fossil Energy, U.S. Department of Energy. This research was performed using EMSL, a national scientific user facility sponsored by the Department of Energy's Office of Biological and Environmental Research and the PNNL Institutional Computing (PIC) program located at Pacific Northwest National Laboratory.

  17. The correlation between reactivity and ash mineralogy of coke

    SciTech Connect (OSTI)

    Kerkkonen, O.; Mattila, E.; Heiniemi, R.

    1996-12-31

    Rautaruukki is a modern integrated Finnish steel works having a production of 2.4 mil. t/year of flat products. The total fuel consumption of the two blast furnaces in 1994 was 435 kg/t HM. Coke used was 345 kg/t HM and oil injection was 90 kg/t HM. The coking plant was taken in to operation in 1987 and is the only one in Finland, which means that the coking tradition is very short. Coke production is 0.9 mil. t/year. The coking blends include 70--80% medium volatile coals having a wide range of total dilatation. From time to time disturbances in the operation of the blast furnaces have occurred in spite of the fact that the reactivity of the coke used has remained constant or even decreased. It was thought necessary to investigate the factors affecting coke reactivity, in order to better understand the results of the reactivity test. This paper deals with carbonization tests done in a 7 kg test oven using nine individual coals having volatile-matter contents of 17--36% (dry) and seven blends made from these coals. Coke reactivity with CO{sub 2} at 1100 C (CRI) and coke strength after reaction (CSR) were determined using the test developed by the Nippon Steel Corporation. The influence of coke carbon form, porosity and especially ash mineralogy on the coke reactivity were examined. The effects of some additives; petroleum coke (pet coke), the spillage material from the coke ovens and oxidized coal, on coke quality were also studied. Typical inorganic minerals found in coals were added to one of the high volatile coals, which was then coked to determine the affect of the minerals on the properties of the coke produced.

  18. Development of 230-kV high-pressure, gas-filled, pipe-type cable system: Model test program phase

    SciTech Connect (OSTI)

    Silver, D.A. )

    1990-09-01

    The objective of this project was the development of a 230 kV high-pressure gas-filled (HPGF) pipe-type cable employing paper or laminate of paper-polypropylene-paper (PPP) insulation pressurized with N{sub 2} gas or a blend of 15% SF{sub 6}/85% N{sub 2} gas. Heretofore, HPGF pipe-type cables have been restricted to 138 kV ratings due to technical difficulties in achieving higher voltage ratings. In view of the high cost of manufacturing and testing a large number of full size cables, cable models with 2 mm (80 mils) and 2.5 mm (100 mils) wall thicknesses of insulation enclosed in a test fixture capable of withstanding a test pressure of 2070 kPa (300 psig) and high electrical stresses were employed for dissipation factor versus voltage measurements and for ac and impulse breakdown tests at rated and emergency operating temperatures. In addition, a 36 cm (14 in) full wall cable model enclosed in a pressure vessel was utilized for transient pressure response tests. The results of this investigation attest tot he technical feasibility of the design and manufacture of a 230 kV HPGF pipe-type cable employing paper or PPP insulation pressurized with 100% N{sub 2} gas or a blend of 15% SF{sub 6}/85% N{sub 2} gas for operation under normal and 100 hour emergency conditions at conductor temperatures of 85{degree} and 105{degree}C, respectively. The manufacture of a full size PPP insulated cable pressurized with a blend of 15% SF{sub 6}/85% N{sub 2} gas employing pre-impregnated PPP insulating tapes and an annular conductor based on the design stresses defined in this report is recommended for laboratory evaluation and extended life tests. 11 refs., 45 figs., 11 tabs.

  19. Determining the Radiation Damage Effect on Glovebox Glove Material.

    SciTech Connect (OSTI)

    Cournoyer, M. E.; Balkey, J. J.; Andrade, R.M.

    2005-01-01

    The Nuclear Material Technology (NMT) Division has the largest inventory of glove box gloves at Los Alamos National Laboratory. The minimization of unplanned breaches in the glovebox, e.g., glove failures, is a primary concern in the daily operations in NMT Division facilities, including the Plutonium Facility (PF-4) at TA-55 and Chemical and Metallurgy Research (CMR) Facility. Glovebox gloves in these facilities are exposed to elevated temperatures and exceptionally aggressive radiation environments (particulate {sup 239}Pu and {sup 238}Pu). Predictive models are needed to estimate glovebox glove service lifetimes, i.e. change-out intervals. Towards this aim aging studies have been initiated that correlate changes in mechanical (physical) properties with degradation chemistry. This present work derives glovebox glove change intervals based on previously reported mechanical data of thermally aged hypalon glove samples. Specifications for 30 mil tri-layered hypalon/lead glovebox gloves (TLH) and 15 mil hypalon gloves (HYP) have already been established. The relevant mechanical properties are shown on Table 1. Tensile strength is defined as the maximum load applied in breaking a tensile test piece divided by the original cross-sectional area of the test piece (Also termed maximum stress and ultimate tensile stress). Ultimate elongation is the elongation at time of rupture (Also termed maximum strain). The specification for the tensile test and ultimate elongation are the minimum acceptable values. In addition, the ultimate elongation must not vary 20% from the original value. In order to establish a service lifetimes for glovebox gloves in a thermal environment, the mechanical properties of glovebox glove materials were studied.

  20. Hearing Protection Evaluation for the Combat Arms Earplug at Idaho National Laboratory

    SciTech Connect (OSTI)

    James Lovejoy

    2007-03-01

    The Idaho National Laboratory (INL) is managed by Battelle Energy Alliance, LLC (BEA) for the Department of Energy. The INL Protective Security Forces (Pro Force) are involved in training exercises that generate impulse noise by small arms fire. Force-on-force (FOF) training exercises that simulate real world scenarios require the Pro Force to engage the opposition force (OPFOR) while maintaining situational awareness through verbal communications. The Combat Arms earplug was studied to determine if it provides adequate hearing protection in accordance with the requirements of MIL-STD-1474C/D. The Combat Arms earplug uses a design that allows continuous noise through a critical orifice while effectively attenuating high-energy impulse noise. The earplug attenuates noise on a non linear scale, as the sound increases the attenuation increases. The INL studied the effectiveness of the Combat Arms earplug with a Bruel & Kjaer (B&K) head and torso simulator used with a selection of small arms to create impulse sound pressures. The Combat Arms earplugs were inserted into the B&K head and torso ears, and small arms were then discharged to generate the impulse noise. The INL analysis of the data indicates that the Combat Arms earplug does provide adequate protection, in accordance with MIL-STD-1474C/D, when used to protect against impulse noise generated by small arms fire using blank ammunition. Impulse noise generated by small arms fire ranged from 135160 dB range unfiltered un-weighted. The Combat Arms earplug attenuated the sound pressure 1025 dB depending on the impulse noise pressure. This assessment is consistent with the results of previously published studies on the Combat Arms earplug (see Section 5, References). Based upon these result, the INL intends to use the Combat Arms earplug for FOF training exercises.

  1. Review of corrosion in 10- and 14-ton mild steel depleted UF{sub 6} storage cylinders

    SciTech Connect (OSTI)

    Lykins, M.L.

    1995-08-01

    A literature review was conducted to determine the type, extent and severity of corrosion found in the 10- and 14-ton mild steel depleted UF{sub 6} storage cylinders. Also discussed in this review is corrosion found in the valves and plugs used in the cylinders. Corrosion of the cylinders is a gradual process which occurs slowly over time. Understanding corrosion of the cylinders is an important concern for long term storage of the UF{sub 6} in the cylinder yards, as well as the final disposition of the depleted UF{sub 6} tails inventory in the future. The following conclusions are made from the literature review: (1) The general external corrosion rate of the cylinders is about 1 to 2 mils per year (1 mil = 0.001{double_prime}). The highest general external corrosion rate was over 5 mpy on the 48G type cylinders. (2) General internal corrosion from the depleted UF{sub 6} is negligible under normal storage conditions. Crevice corrosion can occur at the cylinder/saddle interface from the retention of water in this area. Crevice corrosion can occur at the cylinder/skirt interface on the older skirted cylinders due to the lack of water drainage in this area. Crevice corrosion can occur on cylinders that have been in ground contact. Crevice corrosion and galvanic corrosion can occur where the stainless steel I.D. nameplates are attached to the cylinder. The packing nuts on the bronze one-inch valves used in the cylinders are susceptible to stress corrosion cracking (SCC). Mechanical damage from routine handling can lead to a breach in a cylinder with subsequent accelerated corrosion of the mild steel due to attack from HF and other UF{sub 6} hydrolysis by-products.

  2. Evaluation of the Molten Salt Reactor Experiment drain tanks for reuse in salt disposal, Oak Ridge National Laboratory, Oak Ridge, Tennessee

    SciTech Connect (OSTI)

    1998-05-01

    This report was prepared to identify the source documentation used to evaluate the drain tanks in the Molten Salt Reactor Experiment (MSRE) at Oak Ridge National Laboratory (ORNL). The evaluation considered the original quality of the tanks, their service history, and their intended use during the removal of fluoride salts. It also includes recommendations for a quality verification plan. The estimates of corrosion damage to the salt containing system at the MSRE are low enough to lend optimism that the system will be fit for its intended use, which is disposal of the salt by transferring it to transport containers. The expected corrosion to date is estimated between 10 and 50 mil, or 2 to 10% of the shell wall. The expected corrosion rate when the tanks are used to remove the salt at 110 F is estimated to be .025 to 0.1 mil per hour of exposure to HF and molten salt. To provide additional assurance that the estimates of corrosion damage are accurate, cost effective nondestructive examination (NDE) has been recommended. The NDE procedures are compared with industry standards and give a perspective for the extent of additional measures taken in the recommendation. A methodology for establishing the remaining life has been recommended, and work is progressing towards providing an engineering evaluation based upon thickness and design conditions for the future use of the tanks. These extra measures and the code based analysis will serve to define the risk of salt or radioactive gases leaking during processing and transfer of the salt as acceptable.

  3. SAVANNAH RIVER SITE TANK CLEANING: CORROSION RATE FOR ONE VERSUS EIGHT PERCENT OXALIC ACID SOLUTION

    SciTech Connect (OSTI)

    Ketusky, E.; Subramanian, K.

    2011-01-20

    Until recently, the use of oxalic acid for chemically cleaning the Savannah River Site (SRS) radioactive waste tanks focused on using concentrated 4 and 8-wt% solutions. Recent testing and research on applicable dissolution mechanisms have concluded that under appropriate conditions, dilute solutions of oxalic acid (i.e., 1-wt%) may be more effective. Based on the need to maximize cleaning effectiveness, coupled with the need to minimize downstream impacts, SRS is now developing plans for using a 1-wt% oxalic acid solution. A technology gap associated with using a 1-wt% oxalic acid solution was a dearth of suitable corrosion data. Assuming oxalic acid's passivation of carbon steel was proportional to the free oxalate concentration, the general corrosion rate (CR) from a 1-wt% solution may not be bound by those from 8-wt%. Therefore, after developing the test strategy and plan, the corrosion testing was performed. Starting with the envisioned process specific baseline solvent, a 1-wt% oxalic acid solution, with sludge (limited to Purex type sludge-simulant for this initial effort) at 75 C and agitated, the corrosion rate (CR) was determined from the measured weight loss of the exposed coupon. Environmental variations tested were: (a) Inclusion of sludge in the test vessel or assuming a pure oxalic acid solution; (b) acid solution temperature maintained at 75 or 45 C; and (c) agitation of the acid solution or stagnant. Application of select electrochemical testing (EC) explored the impact of each variation on the passivation mechanisms and confirmed the CR. The 1-wt% results were then compared to those from the 8-wt%. The immersion coupons showed that the maximum time averaged CR for a 1-wt% solution with sludge was less than 25-mils/yr for all conditions. For an agitated 8-wt% solution with sludge, the maximum time averaged CR was about 30-mils/yr at 50 C, and 86-mils/yr at 75 C. Both the 1-wt% and the 8-wt% testing demonstrated that if the sludge was removed from

  4. Corrosion Assessment of Candidate Materials for the SHINE Subcritical Assembly Vessel and Components FY14 Report

    SciTech Connect (OSTI)

    Pawel, Steven J.

    2014-10-01

    Laboratory corrosion testing of candidate alloys—including Zr-4 and Zr-2.5Nb representing the target solution vessel, and 316L, 2304, 304L, and 17-4 PH stainless steels representing process piping and balance-of-plant components—was performed in support of the proposed SHINE process to produce 99Mo from low-enriched uranium. The test solutions used depleted uranyl sulfate in various concentrations and incorporated a range of temperatures, excess sulfuric acid concentrations, nitric acid additions (to simulate radiolysis product generation), and iodine additions. Testing involved static immersion of coupons in solution and in the vapor above the solution, and was extended to include planned-interval tests to examine details associated with stainless steel corrosion in environments containing iodine species. A large number of galvanic tests featuring couples between a stainless steel and a zirconium-based alloy were performed, and limited vibratory horn testing was incorporated to explore potential erosion/corrosion features of compatibility. In all cases, corrosion of the zirconium alloys was observed to be minimal, with corrosion rates based on weight loss calculated to be less than 0.1 mil/year with no change in surface roughness. The resulting passive film appeared to be ZrO2 with variations in thickness that influence apparent coloration (toward light brown for thicker films). Galvanic coupling with various stainless steels in selected exposures had no discernable effect on appearance, surface roughness, or corrosion rate. Erosion/corrosion behavior was the same for zirconium alloys in uranyl sulfate solutions and in sodium sulfate solutions adjusted to a similar pH, suggesting there was no negative effect of uranium resulting from fluid dynamic conditions aggressive to the passive film. Corrosion of the candidate stainless steels was similarly modest across the entire range of exposures. However, some sensitivity to corrosion of the stainless steels was

  5. PLUTONIUM-URANIUM EXTRACTION (PUREX) FACILITY ALARACT DEMONSTRATION FOR FILTER HOUSING

    SciTech Connect (OSTI)

    LEBARON GJ

    2008-11-25

    deteriorated galvanized filter faceguards discovered during an internal filter housing inspection met American Society of Mechanical Engineers (ASME) AG-l or Military Specification (MIL) 51068 standards. The filter system was designed and installed prior to the issuance of AG-l, February 1986; however, MIL 51068 did require galvanized faceguards. The faceguards are not necessary for filtration or structural purposes; it is concluded that the system is in compliance with the intent of the applicable standard. Appendix B provides supporting information to address this issue.

  6. A hard X-ray study of a manganese-terpyridine catalyst in a chromium-based Metal Organic Framework

    SciTech Connect (OSTI)

    Ramsey, Alexandra V.

    2015-08-28

    Hydrogen produced from water splitting is a promising source of clean energy. However, a robust catalyst is necessary to carry out the water oxidation step of water splitting. In this study, the catalyst studied was [(terpy)Mn(μ-O)2Mn(terpy)]3+ (MnTD) synthesized in the Metal Organic Framework (MOF) MIL-101(Cr), and the method used for analysis was hard X-ray powder diffraction. The diffraction data was used to detect the presence of MOF in different catalytic stages, and lattice parameters were assigned to the samples containing MOF. Fourier maps were constructed with GSAS II to determine the contents of the MOF as preliminary studies suggested that MnTD may not be present. Results showed that MOF is present before catalysis occurs but disappears by the time 45 minutes of catalysis has ensued. Changes in the MOF’s lattice parameters and location of electron density in the Fourier maps suggest attractions between the MOF and catalyst that may lead to MOF degradation. Fourier maps also revealed limited, if any, amounts of MnTD, even before catalysis occurred. Molecular manganese oxide may be the source of the high rate of water oxidation catalysis in the studied system.

  7. TEST PLAN AND PROCEDURE FOR THE EXAMINATION OF TANK 241-AY-101 MULTI-PROBE CORROSION MONITORING SYSTEM

    SciTech Connect (OSTI)

    WYRWAS RB; PAGE JS; COOKE GS

    2012-04-19

    This test plan describes the methods to be used in the forensic examination of the Multi-probe Corrosion Monitoring System (MPCMS) installed in the double-shell tank 241-AY-101 (AY-101). The probe was designed by Applied Research and Engineering Sciences (ARES) Corporation. The probe contains four sections, each of which can be removed from the tank independently (H-14-107634, AY-101 MPCMS Removable Probe Assembly) and one fixed center assembly. Each removable section contains three types of passive corrosion coupons: bar coupons, round coupons, and stressed C-rings (H-14-l07635, AY-101 MPCMS Details). Photographs and weights of each coupon were recorded and reported on drawing H-14-107634 and in RPP-RPT-40629, 241-AY-101 MPCMS C-Ring Coupon Photographs. The coupons will be the subject of the forensic analyses. The purpose of this examination will be to document the nature and extent of corrosion of the 29 coupons. This documentation will consist of photographs and photomicrographs of the C-rings and round coupons, as well as the weights of the bar and round coupons during corrosion removal. The total weight loss of the cleaned coupons will be used in conjunction with the surface area of each to calculate corrosion rates in mils per year. The bar coupons were presumably placed to investigate the liquid-air-interface. An analysis of the waste level heights in the waste tank will be investigated as part of this examination.

  8. Fluid-Structure Interaction Modeling of High-Aspect Ratio Nuclear Fuel Plates Using COMSOL

    SciTech Connect (OSTI)

    Curtis, Franklin G [ORNL] [ORNL; Ekici, Kivanc [ORNL] [ORNL; Freels, James D [ORNL] [ORNL

    2013-01-01

    The High Flux Isotope Reactor at the Oak Ridge National Lab is in the research stage of converting its fuel from high-enriched uranium to low-enriched uranium. Due to different physical properties of the new fuel and changes to the internal fuel plate design, the current safety basis must be re-evaluated through rigorous computational analyses. One of the areas being explored is the fluid-structure interaction phenomenon due to the interaction of thin fuel plates (50 mils thickness) and the cooling fluid (water). Detailed computational fluid dynamics and fluid-structure interaction simulations have only recently become feasible due to improved numerical algorithms and advancements in computing technology. For many reasons including the already built-in fluid-structure interaction module, COMSOL has been chosen for this complex problem. COMSOL's ability to solve multiphysics problems using a fully-coupled and implicit solution algorithm is crucial in obtaining a stable and accurate solution. Our initial findings show that COMSOL can accurately model such problems due to its ability to closely couple the fluid dynamics and the structural dynamics problems.

  9. Task 2 - Limits for High-Frequency Conducted Susceptibility Testing - CS114 (NRC-HQ-60-14-D-0015)

    SciTech Connect (OSTI)

    Wood, Richard Thomas; Ewing, Paul D.; Moses, Rebecca J.

    2015-09-01

    A principal focus of Task 2 under this project was for ORNL to evaluate the basis for susceptibility testing against high-frequency conducted interference and to establish recommendations to resolve concerns about the severity of test limits for the conducted susceptibility (CS) test, CS114, from MIL-STD-461. The primary concern about the test limit has been characterized by the EPRI EMI Working Group in the following terms: Demonstrating compliance with the CS114 test limits recommended in TR-102323 has proven to be problematic, even for components that have been tested to commercial standards and demonstrated proper operation in industrial applications [6]. Specifically, EPRI notes that the CS114 limits approved in regulatory documents are significantly higher than those invoked by the US military and similar commercial standards in the frequency range below 200 kHz. For this task, ORNL evaluated the original approach to establishing the test limit, EPRI technical findings from a review of the limit, and the regulatory basis through which the currently approved limits were accepted. Based on this analysis, strategies have been developed regarding changes to the CS114 limit that can resolve the technical concerns raised by the industry. Guided by the principles that reasonable assurance of safety must not be compromised but excessive conservatism should be reduced, recommendations on a suitable basis for a revised limit have been developed and can be incorporated into the planned Revision 2 of RG 1.180.

  10. Manufacture of Alumina-Forming Austenitic Stainless Steel Alloys by Conventional Casting and Hot-Working Methods

    SciTech Connect (OSTI)

    Brady, M.P.; Yamamoto, Y.; Magee, J.H. (Carpenter Technol. Corp.)

    2009-03-23

    Oak Ridge National Laboratory (ORNL) and Carpenter Technology Corporation (CarTech) participated in an in-kind cost share cooperative research and development agreement (CRADA) effort under the auspices of the Energy Efficiency and Renewable Energy (EERE) Technology Maturation program to explore the feasibility for scale up of developmental ORNL alumina-forming austenitic (AFA) stainless steels by conventional casting and rolling techniques. CarTech successfully vacuum melted 30lb heats of four AFA alloy compositions in the range of Fe-(20-25)Ni-(12-14)Cr-(3-4)Al-(1-2.5)Nb wt.% base. Conventional hot/cold rolling was used to produce 0.5-inch thick plate and 0.1-inch thick sheet product. ORNL subsequently successfully rolled the 0.1-inch sheet to 4 mil thick foil. Long-term oxidation studies of the plate form material were initiated at 650, 700, and 800 C in air with 10 volume percent water vapor. Preliminary results indicated that the alloys exhibit comparable (good) oxidation resistance to ORNL laboratory scale AFA alloy arc casting previously evaluated. The sheet and foil material will be used in ongoing evaluation efforts for oxidation and creep resistance under related CRADAs with two gas turbine engine manufacturers. This work will be directed to evaluation of AFA alloys for use in gas turbine recuperators to permit higher-temperature operating conditions for improved efficiencies and reduced environmental emissions.

  11. Improvement in Thermal-Ionization Mass Spectrometry (TIMS) using Total Flash Evaporation (TFE) method for lanthanides isotope ratio measurements in transmutation targets

    SciTech Connect (OSTI)

    Mialle, S.; Gourgiotis, A.; Aubert, M.; Stadelmann, G.; Gautier, C.; Isnard, H.

    2011-07-01

    The experiments involved in the PHENIX french nuclear reactor to obtain precise and accurate data on the total capture cross sections of the heavy isotopes and fission products require isotopic ratios measurements with uncertainty of a few per mil. These accurate isotopic ratio measurements are performed with mass spectrometer equipped with multi-collector system. The major difficulty for the analyses of these actinides and fission products is the low quantity of the initial powder enclosed in steel container (3 to 5 mg) and the very low quantities of products formed (several {mu}g) after irradiation. Specific analytical developments are performed by Thermal Ionization Mass Spectrometry (TIMS) to be able to analyse several nanograms of elements with this technique. A specific method of acquisition named Total Flash Evaporation was adapted in this study in the case of lanthanide measurements for quantity deposited on the filament in the order of 2 ng and applied on irradiated fuel. To validate the analytical approach and discuss about the accuracy of the data, the isotopic ratios obtained by TIMS are compared with other mass spectrometric techniques such as Multiple-Collector Inductively Coupled Plasma Mass Spectrometer (MC-ICPMS). (authors)

  12. Development of a silicate-nitrite-borate corrosion inhibitor

    SciTech Connect (OSTI)

    Taylor, P.A.

    1982-11-29

    A corrosion inhibitor consisting of 1000 mg/L nitrite (NO/sub 2//sup -/), 500 mg/L silicate (SiO/sub 2/), 300 mg/L boron as a pH buffer, 50 mg/L of a biocide, and 5 mg/L tolyltriazole in deionized water was developed for use in the machine-cooling water system of the Department of Energy's Gas Centrifuge Enrichment Plant (GCEP) at Portsmouth, Ohio. Corrosion tests in this solution using six different types of metals, including 6061 aluminum, have failed to show any corrosion at the 0.05-..mu../y (0.002-mil/y) detection limit. The use of deionized water for this inhibitor solution is strongly recommended for any system containing aluminum because the presence of 30 mg/L of chloride ions is known to cause pitting in 6061 aluminum. The purity of the corrosion inhibitor can be maintained by using a small mixed-bed demineralizer in the water system. The demineralizer originally loads up with sodium and silicate ions, which then exchange for any contaminating ions-such as calcium, magnesium, or chromate-that might enter the corrosion-inhibitor solution.

  13. The effect of conditioning agents on the corrosive properties of molten urea

    SciTech Connect (OSTI)

    Nichols, D E; Nguyen, D T; Norton, M M; Parker, B R; Daniels, L E

    1991-01-01

    From the process case histories of the failure of several heat exchanger tube bundles, it was revealed that molten urea containing lignosulfonate as a granulation conditioning-hardening agent (Urea LS[trademark]) is corrosive to Types 304 and 316 stainless steel. The results of field and laboratory immersion corrosion tests indicated that the corrosivity of molten urea is strongly dependent on the process temperature rather than the conditioner composition. At temperatures below 295F, molten Urea LS[trademark] is not aggressive to these stainless steels. However, at temperatures above 300F, the corrosion of these stainless steels is extremely severe. The corrosion rate of Types 304, 304L, 316, and 316L is as high as hundreds of mils per year. The corrosion mechanism tends to be more general than localized. The results of the laboratory corrosion test also revealed that among alloying elements, copper is detrimental to corrosion resistance of stainless steel exposed to molten Urea LS[trademark], chromium is the most beneficial, and nickel has only a minor effect. Thus, copper-free and chromium stainless steels have superior corrosion resistance to the molten Urea LS[trademark] at a wide range of temperatures up to 345F.

  14. METHOD OF MAKING TUNGSTEN FILAMENTS

    DOE Patents [OSTI]

    Frazer, J.W.

    1962-12-18

    A method of making tungsten filaments is described in which the tungsten is completely free of isotope impurities in the range of masses 234 to 245 for use in mass spectrometers. The filament comprises a tantalum core generally less than 1 mil in diameter having a coating of potassium-free tantalum-diffused tungsten molecularly bonded thereto. In the preferred process of manufacture a short, thin tantalum filament is first mounted between terminal posts mounted in insulated relation through a backing plate. The tungsten is most conveniently vapor plated onto the tantalum by a tungsten carbonyl vapor decomposition method having a critical step because of the tendency of the tantalum to volatilize at the temperature of operntion of the filament. The preferred recipe comprises volatilizing tantalum by resistance henting until the current drops by about 40%, cutting the voltage back to build up the tungsten, and then gradually building the temperature back up to balance the rate of tungsten deposition with the rate of tantalum volatilization. (AEC)

  15. 11.424 Ghz Stripline Transversal Filter for Sub-Picosecond Bunch Timing Measurements

    SciTech Connect (OSTI)

    Van Winkle, D.; Young, A.; Fox, J.D.; /SLAC

    2010-08-26

    Measurement of time-of-arrival or instantaneous longitudinal position is a fundamental beam diagnostic. We present results from a stripline transversal periodic coupler structure which forms the heart of a sub-ps beam timing detector. This filter structure approximates a sinx/x response in the frequency domain which corresponds to a limited pulse length response in the time domain. These techniques have been used extensively in beam feedback systems at 3 GHz center frequencies with operational single-shot resolutions of 200 fs [1]. We present a new design, based on a 11.424 GHz center frequency, which is intended to offer a factor of four improvement in time resolution. Two-dimensional electromagnetic simulation results are shown, and the design optimization approach leading to the final circuit implementation is illustrated. The prototype circuit has been fabricated on 64mil Rogers 4003 and lab frequency domain and time domain data are compared to the 2-D simulation results. Performance of the prototype circuit is shown with applicability to sub-ps beam measurements in LINAC and FEL applications.

  16. Swine lagoon biogas utilization system

    SciTech Connect (OSTI)

    Gettier, S.W.; Roberts, M.

    1994-12-31

    A project was conceived to design and build a system to recover methane from pig manure with covered anaerobic lagoon technology. Covered lagoon technology lends itself both to new lagoon construction and to retrofit designs on existing anaerobic lagoons. A two cell passive in-ground digester/lagoon system was designed for a 600 sow feeder pig farm. The digester was covered with a flexible fabric cover made of 30 mil XR-5. The biogas has 1,100 ppm hydrogen sulfide. For the first month of operation 473 cubic feet of biogas per hour has been recovered from the digester 24 hours per day. At this gas flow the engine turns an induction generator to produce 17.1 KW per hour. A little over 80% of the farm`s electrical needs are generated with methane from swine manure. On an annual basis there will be 150,000 KWh of electricity produced from 4.3 million cubic feet of biogas.

  17. Ultrasonic Phased Array Evaluation of Control Rod Drive Mechanism (CRDM) Nozzle Interference Fit and Weld Region

    SciTech Connect (OSTI)

    Cinson, Anthony D.; Crawford, Susan L.; MacFarlan, Paul J.; Mathews, Royce; Hanson, Brady D.; Diaz, Aaron A.

    2011-07-31

    Ultrasonic phased array data were collected on a removed-from-service CRDM nozzle specimen to assess a previously reported leak path. First a mock-up CRDM specimen was evaluated that contained two 0.076-mm (3.0-mil) interference fit regions formed from an actual Inconel CRDM tube and two 152.4-mm (6.0-in.) thick carbon steel blocks. One interference fit region has a series of precision crafted electric discharge machining (EDM) notches at various lengths, widths, depths, and spatial separations for establishing probe sensitivity, resolution and calibration. The other interference fit has zones of boric acid (crystal form) spaced periodically between the tube and block to represent an actively leaking CRDM nozzle assembly in the field. Ultrasonic phased-array evaluations were conducted using an immersion 8-element annular 5.0-MHz probe from the tube inner diameter (ID). A variety of focal laws were employed to evaluate the interference fit regions and J grove weld, where applicable. Responses from the mock-up specimen were evaluated to determine detection limits and characterization ability as well as contrast the ultrasonic response differences with the presence of boric acid in the fit region. Nozzle 63, from the North Anna Unit-2 nuclear power plant, was evaluated to assess leakage path(s) and was destructively dismantled to allow a visual verification of the leak path(s).

  18. Near Surface Leakage Monitoring for the Verification and Accounting of Geologic Carbon Sequestration Using a Field Ready {sup 14}C Isotopic Analyzer

    SciTech Connect (OSTI)

    Marino, Bruno

    2014-04-14

    Results for the development of a field ready multi-isotopic analyzer for {sup 12}CO{sub 2}, {sup 13}CO{sub 2} and {sup 14}CO{sub 2} and applications for carbon capture and storage (CCS) containment performance are described. A design goal of the field platform was to provide isotopic data with a high data rate, a standardized reference baseline and acceptable precision (e.g., ~ ±50 per mil D{sup 14}CO{sub 2}) for detection and quantification of fossil-fuel CO{sub 2} CCS leakage scenarios. The instrument platform was not designed to replace high precision accelerator mass spectrometry. An additional goal was to combine project scale isotopic data and associated fluxes with unique financial instruments linking CCS containment performance to a publicly traded security providing project revenue to stakeholders. While the primary goals of the project were attained additional work is needed for the instrument platform and deployment within a full scale CCS site that was not available during the project timeframe.

  19. Oxygen isotope fractionation in the vacuum ultraviolet photodissociation of carbon monoxide: Wavelength, pressure and temperature dependency.

    SciTech Connect (OSTI)

    Chakraborty, Subrata; Davis, Ryan; Ahmed, Musahid; Jackson, Teresa L.; Thiemens, Mark H.

    2012-01-03

    Several absorption bands exist in the VUV region of Carbon monoxide (CO). Emission spectra indicate that these bands are all predissociative. An experimental investigation of CO photodissociation by vacuum ultraviolet photons (90 to 108 nm; ~13 to 11 eV) from the Advanced Light Source Synchrotron and direct measurement of the associated oxygen isotopic composition of the products are presented here. A wavelength dependency of the oxygen isotopic composition in the photodissociation product was observed. Slope values (δ'{sup 18}O/ δ'{sup 17}O) ranging from 0.76 to 1.32 were observed in oxygen three-isotope space (δ'{sup 18}O vs. δ'{sup 17}O) which correlated with increasing synchrotron photon energy, and indicate a dependency of the upper electronic state specific dissociation dynamics (e.g., perturbation and coupling associated with a particular state). An unprecedented magnitude in isotope separation was observed for photodissociation at the 105 and 107 nm synchrotron bands and are found to be associated with accidental predissociation of the vibrational states ({nu} = 0 and 1) of the upper electronic state E{sup 1}Π. For each synchrotron band, a large (few hundred per mil) extent of isotopic fractionation was observed and the range of fractionation is a combination of column density and exposure time. A significant temperature dependency in oxygen isotopic fractionation was observed, indicating a rotational level dependency in the predissociation process.

  20. Advanced Materials for Mercury 50 Gas Turbine Combustion System

    SciTech Connect (OSTI)

    Price, Jeffrey

    2008-09-30

    development, multiple concepts including high thermal resistance thermal barrier coatings (TBC), oxide dispersion strengthened (ODS) alloys, continuous fiber ceramic composites (CFCC), and monolithic ceramics were evaluated before down-selection to the most promising candidate materials for field evaluation. Preliminary, component and sub-scale testing was conducted to determine material properties and demonstrate proof-of-concept. Full-scale rig and engine testing was used to validated engine performance prior to field evaluation at a Qualcomm Inc. cogeneration site located in San Diego, California. To ensure that the CFCC liners with the EBC proposed under this program would meet the target life, field evaluations of ceramic matrix composite liners in Centaur{reg_sign} 50 gas turbine engines, which had previously been conducted under the DOE sponsored Ceramic Stationary Gas Turbine program (DE-AC02-92CE40960), was continued under this program at commercial end-user sites under Program Subtask 1A - Extended CFCC Materials Durability Testing. The goal of these field demonstrations was to demonstrate significant component life, with milestones of 20,000 and 30,000 hours. Solar personnel monitor the condition of the liners at the field demonstration sites through periodic borescope inspections and emissions measurements. This program was highly successful at evaluating advanced materials and down-selecting promising solutions for use in gas turbine combustions systems. The addition of the advanced materials technology has enabled the predicted life of the Mercury 50 combustion system to reach 30,000 hours, which is Solar's typical time before overhaul for production engines. In particular, a 40 mil thick advanced Thermal Barrier Coating (TBC) system was selected over various other TBC systems, ODS liners and CFCC liners for the 4,000-hour field evaluation under the program. This advanced TBC is now production bill-of-material at various thicknesses up to 40 mils for all of

  1. Demonstration of multifunctional DNBM corrosion inhibitors in protective coatings for Naval Air/Weapon Systems. Final report, September 1989-July 1992

    SciTech Connect (OSTI)

    Bailin, L.J.

    1993-12-01

    The corrosion protective properties of multifunctional DNBM salts (quaternary ammonium dichromate, nitrate, borate, and molybdate) have been demonstrated on high-strength steel and aluminum alloys found in prototype aerospace weapon systems. The 100% DNBM mixture added to MIL-P-23377 epoxy-polyamide, minus strontium chromate inhibitor, on bare 7075-T6 aluminum alloy resisted 1000 h ASTM B-117 salt spray. However, the coatings were not resistant to hydraulic fluid immersion at the higher concentrations required for the corrosion inhibition. Microencapsulation of the reactive DNBM mixture was adopted as a means to prevent this susceptibility, as well as the destructive oxidation of the hydroxyl groups in the epoxy resin during cure. In the scale-up operation, approximately 20 gallons of DNBM weighing 64 kg (141 lb) was prepared from the four starting quarternary salts synthesized in a chemical process pilot plant. The salts were mixed by dissolving in toluene. Following removal of solvent, the resultant dark-brown liquid, approximating molasses in viscosity, was microencapsulated by the following method: The DNBM was dispersed to form an oil-in-water emulsion in an aqueous colloidal solution of low-viscosity, high-purity methyl cellulose using a Gifford-Wood homogenizer, followed by spray drying in an Anhydro spray dryer. The maximum practicable payload was 75% DNBM. After spray drying, the capsules Corrosion inhibitors, DNBM, Microencapsulation, Epoxy primers, Protective coatings.

  2. HIP clad nickel base Alloy 625 for deep sour wells

    SciTech Connect (OSTI)

    Uhl, W.K.; Pendley, M.R.

    1984-05-01

    The hot isostatic pressing (HIP) process was used to clad nickel base Alloy 625 to AISI 4130 low alloy steel. The performance of the HIP clad material in the corrosive environment characteristic of deep, sour oil and gas wells was evaluated in laboratory tests. Included in the test program were NACE TM-01-77 sulfide stress cracking tests, chloride stress corrosion cracking tests in boiling MgCl /SUB 2'/ , and pitting and crevice corrosion tests. The HIP clad 625 performed excellently, displaying essentially the same corrosion resistance as wrought 625. Specifically the HIP clad 625 resisted sulfide stress cracking at applied stresses as high as 120% of yield strength and resisted chloride stress corrosion cracking at stresses exceeding 100% of yield. The HIP clad 625 also displayed immunity to pitting and crevice corrosion, with corrosion rates of <0.025 mm/y (1 mil/y). The 4130 base metal, however, was attacked severly in all tests. SEM/EDX analysis of the 625/4130 interface demonstrated that dilution of the cladding by the base metal was essentially eliminated.

  3. Calcination/dissolution testing for Hanford Site tank wastes

    SciTech Connect (OSTI)

    Colby, S.A.; Delegard, C.H.; McLaughlin, D.F.; Danielson, M.J.

    1994-07-01

    Thermal treatment by calcination offers several benefits for the treatment of Hanford Site tank wastes, including the destruction of organics and ferrocyanides and an hydroxide fusion that permits the bulk of the mostly soluble nonradioactive constituents to be easily separated from the insoluble transuranic residue. Critical design parameters were tested, including: (1) calciner equipment design, (2) hydroxide fusion chemistry, and (3) equipment corrosion. A 2 gal/minute pilot plant processed a simulated Tank 101-SY waste and produced a free flowing 700 C molten calcine with an average calciner retention time of 20 minutes and >95% organic, nitrate, and nitrite destruction. Laboratory experiments using actual radioactive tank waste and the simulated waste pilot experiments indicate that 98 wt% of the calcine produced is soluble in water, leaving an insoluble transuranic fraction. All of the Hanford Site tank wastes can benefit from calcination/dissolution processing, contingent upon blending various tank waste types to ensure a target of 70 wt% sodium hydroxide/nitrate/nitrite fluxing agent. Finally, corrosion testing indicates that a jacketed nickel liner cooled to below 400 C would corrode <2 mil/year (0.05 mm/year) from molten calcine attack.

  4. Advanced heat exchanger development for molten salts

    SciTech Connect (OSTI)

    Sabharwall, Piyush; Clark, Denis; Glazoff, Michael; Zheng, Guiqiu; Sridharan, Kumar; Anderson, Mark

    2014-12-01

    This study addresses present work concerned with advanced heat exchanger development for molten salt in nuclear and non nuclear thermal systems. The molten salt systems discussed herein use alloys, such as Hastelloy N and 242, which show corrosion resistance to molten salt at nominal operating temperatures up to 700°C. These alloys were diffusion welded, and the corresponding information is presented. Test specimens were prepared for exposing diffusion welds to molten salt environments. Hastelloy N and 242 were found to be weldable by diffusion welding, with ultimate tensile strengths about 90% of base metal values. Both diffusion welds and sheet material in Hastelloy N were corrosion tested in?58 mol% KF and 42 mol% ZrF4 at 650, 700, and 850°C for 200, 500, and 1,000 hours. Corrosion rates found were similar between welded and nonwelded materials, typically <10 mils per year. For materials of construction, nickel and alloys with dense nickel coatings are effectively inert to corrosion in fluorides, but not so in chlorides. Hence, additional testing of selected alloys for resistance to intergranular corrosion is needed, as is a determination of corrosion rate as a function of contaminant type and alloy composition with respect to chromium and carbon to better define the optimal chromium and carbon composition, independent of galvanic or differential solubility effects. Also presented is the division of the nuclear reactor and high temperature components per ASME standards, along with design requirements for a subcritical Rankine power cycle heat exchanger that has to overcome pressure difference of about 17 MPa.

  5. To study of different level of nitrogen manure and density on yield and yield component of variety of K.S.C 704 in dry region of sistan

    SciTech Connect (OSTI)

    Dahmardeh, M.; Forghani, F.; Khammari, E.

    2008-01-30

    Out of three grain of the world, Corn is one of the best, About 7 to 10 thousand years ago in south of Mexico corn become domesticated. In the year 1995 culfivation of corn in the world was 130 mil/ha, and to Total production of the world of corn is 507 M/Tons. Average yield of corn in the year 1995 Among Producer countries was 7.78 To 7.60 t/ha in fance and united state was state was 2.36 To 2.20 t/ha, but in Brazil and Mexico Production of corn was different. With this regards, special manner has been arranged for the suitable cultivation or suitable density plants in one heactar on cultivation variety of K.S.C 704 corn. Also suitable level of Nitrogen manure, this Protect in climatic condition of Sistan region done, sith complete block design with 3 replication. Experiment has been selected as split plot, the main plot with 4 different concentration level such as (200-250-3500 and 350 Kg/ha) and sub plot density with 3 different level such as 111000,83000 and 66000 plan/ha respectively. From stage growth up to harvesting of corn in this reache having Data for each treat. ment, After harvesting Analysis of variance and companion of Average of each treatment has been done by DunKan method. Results has been shown, Measurment of characteristics (yield component) seed yield effected different density level of manure, with increasing of manure weight of one thousand seed yield and also in high density showed high significant differente amoung each other. These are with suitable climatic condition of sistan region if enough water will be available ed using Amount of 350 ks/ha Nitrogen manure and with density 111000 plants/ha we can product suitable seed yield Biological yield.

  6. Paleoenvironment of the Ogallala (Neogene) Formation in west-central Kansas

    SciTech Connect (OSTI)

    Twiss, P.C.; McCahon, T.J.; Oviatt, C.G. . Geology Dept.)

    1993-02-01

    At Lake Scott (Scott County) in west-central Kansas, the Ogallala Formation unconformably overlies the Niobrara Formation (Cretaceous) and forms the bluffs of the north-trending Ladder Creek valley. Two sections (Devil's Backbone, 23 m thick; Suicide Bluff, 45 m thick) contain fluvial sands that grade upward into probable eolian sands. The lower sections contain poorly cemented, moderately sorted, arkosic sand, some mud gravel, and poorly defined fluvial channels. In the lower part of Devil's Backbone, cross-bedded sand is capped by mud drapes. At Suicide Bluff, beds of cross-bedded and better sorted sand occur high in the section. Paleosols and secondary calcite and opal dominate the sections. Pedogenic calcretes with more than 52% CaCO[sub 3] are especially abundant and range up to morphologic Stage VI. The [delta][sup 13]C and [delta][sup 18]O in the calcretes range from [minus]4.8 to [minus]6.5 and [minus]8.2 to [minus]6.7 per mil (PDB), respectively. Opal-A has replaced most rhizoliths of the Ogallala. Silicified fossil seeds (Celtis sp., Biorbia sp.) and probable fossil mammal burrows also occur in the sections. Rhyolitic tephra, about 10 Ma, occurs 12 m below the calcrete caprock of Suicide Bluff. A massive layer of opal occurs about 8 m above the tephra and below a diatomaceous bed. Siliceous cement occurs throughout each section, possibly originating from opal phytoliths, tephra, and/or diatoms. These sections afford the potential for understanding the stratigraphic succession and paleoclimate during the late Miocene to possibly early Pliocene in the central High Plains region.

  7. [An improved, more reliable and more marketable version of the Automatic Metering System

    SciTech Connect (OSTI)

    Patas, J.E.

    1993-07-01

    Texas Research Institute Austin, Inc. (TRI/Austin) was tasked by Letco International to evaluate its Automatic Metering System (AMS), a proportional controller for heat tracing cable. The original objectives were focused primarily on the reliability of the AMS controller. However, from the time of the original TRI/Austin proposal, the AMS device evolved beyond the prototype level into an established market product with sufficient operational experience and data that product reliability evaluation was not a significant test objective. The goals of this effort have been to determine the relative energy usage of the AMS proportional control compared to existing thermostatic control in a realistic freeze protection installation (low temperature test), to perform an accelerated life test for self limiting heat tracing cables to determine the service life impact of AMS control vs. thermostat control, and to perform a reliability analysis of the AMS device according to the 1986 edition of MIL-HDBK-217E [1] specifications. TRI/Austin designed and constructed a test set-up for conducting the low temperature test and the accelerated life test. A conceptual diagram of the test hardware is shown in Figure 1. The control computer was programmed to monitor and collect data from both tests in parallel, using the relay box and control circuitry fabricated at TRI/Austin. Test data and control commands were transmitted to and from the computer via standard parallel and serial interfaces. The AMS controller and relay box switched the power to the test cables, the commercial freezer, and the ALT chamber.

  8. Radioisotope Thermoelectric Generator Transporation System licensed hardware second certification test series and package shock mount system test

    SciTech Connect (OSTI)

    Ferrell, P.C.; Moody, D.A.

    1995-10-01

    This paper presents a summary of two separate drop test a e performed in support of the Radioisotope Thermoelectric Generator (RTG) Transportation System (RTGTS). The first portion of this paper presents the second series of drop testing required to demonstrate that the RTG package design meets the requirements of Title 10, Code of Federal Regulations, ``Part 71`` (10 CFR 71). Results of the first test series, performed in July 1994, demonstrated that some design changes were necessary. The package design was modified to improve test performance and the design changes were incorporated into the Safety Analysis Report for Packaging (SARP). The second full-size certification test article (CTA-2) incorporated the modified design and was tested at the US Department of Energy`s (DOE) Hanford Site near Richland, Washington. With the successful completion of the test series, and pending DOE Office of Facility Safety Analysis approval of the SARP, a certificate of compliance will be issued for the RTG package allowing its use. The second portion of this paper presents the design and testing of the RTG Package Mount System. The RTG package mount was designed to protect the RTG from excessive vibration during transport, provide shock protection during on/off loading, and provide a mechanism for moving the RTG package with a forklift. Military Standard (MIL-STD) 810E, Transit Drop Procedure (DOE 1989), was used to verify that the shock limiting system limited accelerations in excess of 15 G`s at frequencies below 150 Hz. Results of the package mount drop tests indicate that an impact force of 15 G`s was not exceeded in any test from a free drop height of 457 mm (18 in.).

  9. Thermal-sprayed zinc anodes for cathodic protection of steel-reinforced concrete bridges

    SciTech Connect (OSTI)

    Bullard, Sophie J.; Covino, Bernard S., Jr.; Cramer, Stephen D.; McGill, Galen E.

    1996-01-01

    Thermal-sprayed zinc anodes are being used in Oregon in impressed current cathodic protection (ICCP) systems for reinforced concrete bridges. The U.S. Department of Energy, Albany Research Center, is collaborating with the Oregon Department of Transportation (ODOT) to evaluate the long-term performance and service life of these anodes. Laboratory studies were conducted on concrete slabs coated with 0.5 mm (20 mil) thick, thermal-sprayed zinc anodes. The slabs were electrochemically aged at an accelerated rate using an anode current density of 0.032 A/m2 (3mA/ft2). Half the slabs were preheated before thermal-spraying with zinc; the other half were unheated. Electrochemical aging resulted in the formation at the zinc-concrete interface of a thin, low pH zone (relative to cement paste) consisting primarily of ZnO and Zn(OH)2, and in a second zone of calcium and zinc aluminates and silicates formed by secondary mineralization. Both zones contained elevated concentrations of sulfate and chloride ions. The original bond strength of the zinc coating decreased due to the loss of mechanical bond to the concrete with the initial passage of electrical charge (aging). Additional charge led to an increase in bond strength to a maximum as the result of secondary mineralization of zinc dissolution products with the cement paste. Further charge led to a decrease in bond strength and ultimately coating disbondment as the interfacial reaction zones continued to thicken. This occurred at an effective service life of 27 years at the 0.0022 A/m2 (0.2 mA/ft2) current density typically used by ODOT in ICCP systems for coastal bridges. Zinc coating failure under tensile stress was primarily cohesive within the thickening reaction zones at the zinc-concrete interface. There was no difference between the bond strength of zinc coatings on preheated and unheated concrete surfaces after long service times.

  10. Corrosion studies of carbon steel under impinging jets of simulated slurries of neutralized current acid waste (NCAW) and neutralized cladding removal waste (NCRW)

    SciTech Connect (OSTI)

    Smith, H.D.; Elmore, M.R.

    1992-01-01

    Plans for the disposal of radioactive liquid and solid wastes presently stored in double-shell tanks at the Hanford Site call for retrieval and processing of the waste to create forms suitable for permanent disposal. Waste will be retrieved from a tank using a submerged slurry pump in conjunction with one or more rotating slurry jet mixer pumps. Pacific Northwest Laboratory (PNL) has conducted tests using simulated waste slurries to assess the effects of a impinging slurry jet on the corrosion rate of the tank wall and floor, an action that could potentially compromise the tank's structural integrity. Corrosion processes were investigated on a laboratory scale with a simulated neutralized cladding removal waste (NCRW) slurry and in a subsequent test with simulated neutralized current acid waste (NCAW) slurry. The test slurries simulated the actual NCRW and NCAW both chemically and physically. The tests simulated those conditions expected to exist in the respective double-shell tanks during waste retrieval operations. Results of both tests indicate that, because of the action of the mixer pump slurry jets, the waste retrieval operations proposed for NCAW and NCRW will moderately accelerate corrosion of the tank wall and floor. Based on the corrosion of initially unoxidized test specimens, and the removal of corrosion products from those specimens, the maximum time-averaged corrosion rates of carbon steel in both waste simulants for the length of the test was {approximately}4 mil/yr. The protective oxide layer that exists in each storage tank is expected to inhibit corrosion of the carbon steel.

  11. Corrosion studies of carbon steel under impinging jets of simulated slurries of neutralized current acid waste (NCAW) and neutralized cladding removal waste (NCRW)

    SciTech Connect (OSTI)

    Smith, H.D.; Elmore, M.R.

    1992-01-01

    Plans for the disposal of radioactive liquid and solid wastes presently stored in double-shell tanks at the Hanford Site call for retrieval and processing of the waste to create forms suitable for permanent disposal. Waste will be retrieved from a tank using a submerged slurry pump in conjunction with one or more rotating slurry jet mixer pumps. Pacific Northwest Laboratory (PNL) has conducted tests using simulated waste slurries to assess the effects of a impinging slurry jet on the corrosion rate of the tank wall and floor, an action that could potentially compromise the tank`s structural integrity. Corrosion processes were investigated on a laboratory scale with a simulated neutralized cladding removal waste (NCRW) slurry and in a subsequent test with simulated neutralized current acid waste (NCAW) slurry. The test slurries simulated the actual NCRW and NCAW both chemically and physically. The tests simulated those conditions expected to exist in the respective double-shell tanks during waste retrieval operations. Results of both tests indicate that, because of the action of the mixer pump slurry jets, the waste retrieval operations proposed for NCAW and NCRW will moderately accelerate corrosion of the tank wall and floor. Based on the corrosion of initially unoxidized test specimens, and the removal of corrosion products from those specimens, the maximum time-averaged corrosion rates of carbon steel in both waste simulants for the length of the test was {approximately}4 mil/yr. The protective oxide layer that exists in each storage tank is expected to inhibit corrosion of the carbon steel.

  12. Optimization of a CNG series hybrid concept vehicle

    SciTech Connect (OSTI)

    Aceves, S.M.; Smith, J.R.; Perkins, L.J.; Haney, S.W.; Flowers, D.L.

    1995-09-22

    Compressed Natural Gas (CNG) has favorable characteristics as a vehicular fuel, in terms of fuel economy as well as emissions. Using CNG as a fuel in a series hybrid vehicle has the potential of resulting in very high fuel economy (between 26 and 30 km/liter, 60 to 70 mpg) and very low emissions (substantially lower than Federal Tier II or CARB ULEV). This paper uses a vehicle evaluation code and an optimizer to find a set of vehicle parameters that result in optimum vehicle fuel economy. The vehicle evaluation code used in this analysis estimates vehicle power performance, including engine efficiency and power, generator efficiency, energy storage device efficiency and state-of-charge, and motor and transmission efficiencies. Eight vehicle parameters are selected as free variables for the optimization. The optimum vehicle must also meet two perfect requirements: accelerate to 97 km/h in less than 10 s, and climb an infinitely long hill with a 6% slope at 97 km/h with a 272 kg (600 lb.) payload. The optimizer used in this work was originally developed in the magnetic fusion energy program, and has been used to optimize complex systems, such as magnetic and inertial fusion devices, neutron sources, and mil guns. The optimizer consists of two parts: an optimization package for minimizing non-linear functions of many variables subject to several non-linear equality and/or inequality constraints and a programmable shell that allows interactive configuration and execution of the optimizer. The results of the analysis indicate that the CNG series hybrid vehicle has a high efficiency and low emissions. These results emphasize the advantages of CNG as a near-term alternative fuel for vehicles.

  13. Manufacture of Alumina-Forming Austenitic Steel Alloys by Conventional Casting and Hot-Working Methods

    SciTech Connect (OSTI)

    Brady, M.P.; Yamamoto, Y.; Magee, J.H.

    2009-03-10

    Oak Ridge National Laboratory (ORNL) and Carpenter Technology Corporation (CarTech) participated in an in-kind cost share cooperative research and development agreement (CRADA) effort under the auspices of the Energy Efficiency and Renewable Energy (EERE) Technology Maturation Program to explore the feasibility for scale up of developmental ORNL alumina-forming austenitic (AFA) stainless steels by conventional casting and rolling techniques. CarTech successfully vacuum melted 301b heats of four AFA alloy compositions in the range of Fe-(20-25)Ni-(12-14)Cr-(3-4)Al-(l-2.5)Nb wt.% base. Conventional hot/cold rolling was used to produce 0.5-inch thick plate and 0.1-inch thick sheet product. ORNL subsequently successfully rolled the 0.1-inch sheet to 4 mil thick foil. Long-term oxidation studies of the plate form material were initiated at 650, 700, and 800 C in air with 10 volume percent water vapor. Preliminary results indicated that the alloys exhibit comparable (good) oxidation resistance to ORNL laboratory scale AFA alloy arc casting previously evaluated. The sheet and foil material will be used in ongoing evaluation efforts for oxidation and creep resistance under related CRADAs with two gas turbine engine manufacturers. This work will be directed to evaluation of AFA alloys for use in gas turbine recuperators to permit higher-temperature operating conditions for improved efficiencies and reduced environmental emissions. AFA alloy properties to date have been obtained from small laboratory scale arc-castings made at ORNL. The goal of the ORNL-CarTech CRADA was to establish the viability for producing plate, sheet and foil of the AFA alloys by conventional casting and hot working approaches as a first step towards scale up and commercialization of the AFA alloys. The AFA alloy produced under this effort will then be evaluated in related CRADAs with two gas turbine engine manufacturers for gas turbine recuperator applications.

  14. Preliminary evaluation of alternative waste form solidification processes. Volume I. Identification of the processes.

    SciTech Connect (OSTI)

    Treat, R.L.; Nesbitt, J.F.; Blair, H.T.; Carter, J.G.; Gorton, P.S.; Partain, W.L.; Timmerman, C.L.

    1980-04-01

    This document contains preconceptual design data on 11 processes for the solidification and isolation of nuclear high-level liquid wastes (HLLW). The processes are: in-can glass melting (ICGM) process, joule-heated glass melting (JHGM) process, glass-ceramic (GC) process, marbles-in-lead (MIL) matrix process, supercalcine pellets-in-metal (SCPIM) matrix process, pyrolytic-carbon coated pellets-in-metal (PCCPIM) matrix process, supercalcine hot-isostatic-pressing (SCHIP) process, SYNROC hot-isostatic-pressing (SYNROC HIP) process, titanate process, concrete process, and cermet process. For the purposes of this study, it was assumed that each of the solidification processes is capable of handling similar amounts of HLLW generated in a production-sized fuel reprocessing plant. It was also assumed that each of the processes would be enclosed in a shielded canyon or cells within a waste facility located at the fuel reprocessing plant. Finally, it was assumed that all of the processes would be subject to the same set of regulations, codes and standards. Each of the solidification processes converts waste into forms that may be acceptable for geological disposal. Each process begins with the receipt of HLLW from the fuel reprocessing plant. In this study, it was assumed that the original composition of the HLLW would be the same for each process. The process ends when the different waste forms are enclosed in canisters or containers that are acceptable for interim storage. Overviews of each of the 11 processes and the bases used for their identification are presented in the first part of this report. Each process, including its equipment and its requirements, is covered in more detail in Appendices A through K. Pertinent information on the current state of the art and the research and development required for the implementation of each process are also noted in the appendices.

  15. A Capillary Absorption Spectrometer for Stable Carbon Isotope Ratio (13C/12C) Analysis in Very Small Samples

    SciTech Connect (OSTI)

    Kelly, James F.; Sams, Robert L.; Blake, Thomas A.; Newburn, Matthew K.; Moran, James J.; Alexander, M. L.; Kreuzer, Helen W.

    2012-02-06

    A capillary absorption spectrometer (CAS) suitable for IR laser isotope analysis of small CO{sub 2} samples is presented. The system employs a continuous-wave (cw) quantum cascade laser to study nearly adjacent rovibrational transitions of different isotopologues of CO{sub 2} near 2307 cm{sup -1} (4.34 {mu}m). This initial CAS system can achieve relative isotopic precision of about 10 ppm {sup 13}C, or {approx}1{per_thousand} (per mil in delta notation relative to Vienna Pee Dee Belemnite) with 20-100 picomoles of entrained sample within the hollow waveguide for CO{sub 2} concentrations {approx}400 to 750 ppm. Isotopic analyses of such gas fills in a 1-mm ID hollow waveguide of 0.8 m overall physical path length can be carried out down to {approx}2 Torr. Overall {sup 13}C/{sup 12}C ratios can be calibrated to {approx}2{per_thousand} accuracy with diluted CO{sub 2} standards. A novel, low-cost method to reduce cw-fringing noise resulting from multipath distortions in the hollow waveguide is presented, which allows weak absorbance features to be studied at the few ppm level (peak-to-rms) after 1,000 scans are co-added in {approx}10 sec. The CAS is meant to work directly with converted CO{sub 2} samples from a Laser Ablation-Catalytic-Combustion (LA CC) micro-sampler to provide {sup 13}C/{sup 12}C ratios of small biological isolates with spatial resolutions {approx}50 {mu}m.

  16. Radioisotope Thermoelectric Generator Transportation System licensed hardware second certification test series and package shock mount system test

    SciTech Connect (OSTI)

    Ferrell, P.C.; Moody, D.A.

    1996-03-01

    This paper presents a summary of two separate drop test activities that were performed in support of the Radioisotope Thermoelectric Generator (RTG) Transportation System (RTGTS). The first portion of this paper presents the second series of drop testing required to demonstrate that the RTG package design meets the requirements of {ital Title} 10, {ital Code} {ital of} {ital Federal} {ital Regulations}, {open_quote}{open_quote}Part 71{close_quote}{close_quote} (10 CFR 71). Results of the first test series, performed in July 1994, demonstrated that some design changes were necessary. The package design was modified to improve test performance and the design changes were incorporated into the Safety Analysis Report for Packaging (SARP). The second full-size certification test article (CTA-2) incorporated the modified design and was tested at the U.S. Department of Energy{close_quote}s (DOE) Hanford Site near Richland, Washington. With the successful completion of the test series, and pending DOE Office of Facility Safety Analysis approval of the SARP, a certificate of compliance will be issued for the RTG package allowing its use. The second portion of this paper presents the design and testing of the RTG Package Mount System. The RTG package mount was designed to protect the RTG from excessive vibration during transport, provide shock protection during on/off loading, and provide a mechanism for moving the RTG package with a forklift. Military Standard (MIL-STD) 810E, {ital Transit} {ital Drop} {ital Procedure} (DOE 1989), was used to verify that the shock limiting system limited accelerations in excess of 15 G{close_quote}s at frequencies below 150 Hz. Results of the package mount drop tests indicate that an impact force of 15 G{close_quote}s was not exceeded in any test from a free drop height of 457 mm (18 in.). {copyright} {ital 1996 American Institute of Physics.}

  17. Summary of workshop on materials issues associated with low-NO{sub x} combustion conditions in fossil-fired boilers

    SciTech Connect (OSTI)

    1996-08-01

    It was anticipated by some members of the high-temperature corrosion community that the fitting of low-NO{sub x} burners to coal-fired power plants would lead to an increase in furnace wall corrosion, as a result of the relatively substoichiometric conditions created by the staged combustion process. These expectations were not borne out by initial experience. Recently, however, cases of severe furnace wall corrosion have been reported by some U.S. utility boilers retrofitted with modern low-NO{sub x} burners. There is extensive experience of furnace wall corrosion in utility boilers in the U.K., which indicates that excessive fireside corrosion rates (>200 nm/hr; 34 mil/yr) are experienced when tubes are exposed simultaneously to substoichiometric gaseous environments (CO>3.0 percent) and high radiant heat fluxes. Such conditions may be generated when flame impingement occurs. Where such conditions persist, increases in fuel chlorine content will exacerbate the rate of metal loss. In the absence of either circumstances, corrosion rates are much reduced and little influence of coal chlorine content is anticipated. Although the corrosion is essentially sulfidation caused by H{sub 2}S in the flue gas, the contribution of fuel sulfur in the corrosion experience by U.K. boilers is unresolved, partly because of the relatively small range in sulfur content of coals burned in U.K. utility boilers. The intent of this workshop was three-fold: to better define the problem in terms of the form and rate of attack; to examine what is known about its root causes; and to review the potential for using corrosion-resistant materials as part of the solution.

  18. The role of coal in the economy of the Czech Republic

    SciTech Connect (OSTI)

    Doruska, J.

    1995-12-01

    The Czech Republic ranks among the countries with high total reserves of hard coal and lignite. Therefore coal always had and still has a significant role in covering the power demand of the Czech Republic. Transition of the national economy, based on the principles of the market economy and private ownership, affects among others also behavior of the mining companies. A strong emphasis is also aimed at the environmental aspects concerning both the process of coal mining and the process of its utilization. Within these intentions the power policy of the Czech Republic is formulated. The Czech Republic, which has 10 mil. inhabitants, ranks among the countries with a high share of industry in the process of creating the gross national product. This state has its historical roots as on the present territory of the Czech Republic there had been concentrated a majority of industrial and mining capacities of the Hapsburg Empire. The First World War resulted among others in the decline of the Hapsburg Empire. Within this process Czechoslovak Republic was established (apart from other things the center of democracy in the Central Europe). In that republic the industry had an important position. The industrial potential had been expanded even during the occupation of Czechoslovakia by Nazi Germany in the years 1939 - 1945. After the Second World War when Europe was divided into two political spheres Czechoslovakia became a significant industrial base of so called East Bloc. Such a development and the needs of the Eastern Bloc resulted in the intensive development of the heavy industry on the territory of Czechoslovakia.

  19. Liquid-Air Interface Corrosion Testing Simulating The Environment Of Hanford Double Shell Tanks

    SciTech Connect (OSTI)

    Wiersma, B.; Gray, J. R.; Garcia-Diaz, B. L.; Murphy, T. H.; Hicks, K. R.

    2014-01-30

    Coupon tests on A537 carbon steel materials were conducted to evaluate the Liquid-Air Interface (LAI) corrosion susceptibility in a series of solutions designed to simulate conditions in the radioactive waste tanks located at the Hanford Nuclear Facility. The new stress corrosion cracking requirements and the impact of ammonia on LAI corrosion were the primary focus. The minimum R value (i.e., molar ratio of nitrite to nitrate) of 0.15 specified by the new stress corrosion cracking requirements was found to be insufficient to prevent pitting corrosion at the LAI. The pH of the test solutions was 10, which was actually less than the required pH 11 defined by the new requirements. These tests examined the effect of the variation of the pH due to hydroxide depletion at the liquid air interface. The pits from the current testing ranged from 0.001 to 0.008 inch in solutions with nitrate concentrations of 0.4 M and 2.0 M. The pitting and general attack that occurred progressed over the four-months. No significant pitting was observed, however, for a solution with a nitrate concentration of 4.5 M. The pitting depths observed in these partial immersion tests in unevaporated condensates ranged from 0.001 to 0.005 inch after 4 months. The deeper pits were in simulants with low R values. Simulants with R values of approximately 0.6 to 0.8 appeared to significantly reduce the degree of attack. Although, the ammonia did not completely eliminate attack at the LAI, the amount of corrosion in an extremely corrosive solution was significantly reduced. Only light general attack (< 1 mil) occurred on the coupon in the vicinity of the LAI. The concentration of ammonia (i.e., 50 ppm or 500 ppm) did not have a strong effect.

  20. Corrosion of materials in chemical heat pump working fluids

    SciTech Connect (OSTI)

    DeVan, J.H.; Wolf, J.S.

    1988-11-01

    A series of laboratory tests were conducted to evaluate the performance of type A106B and 2.25Cr-1Mo steels, types 304 and 304L stainless steel, and the nickel-base alloy Monel 400 in chemical heat pump environments based on aqueous nitrate salt mixtures. Autoclave screening tests were initially performed to evaluate the stress corrosion cracking (SCC) properties of the materials at temperatures of 170, 210, and 250/degree/C, respectively. In 2-week tests, one of two heats of A106B exhibited cracking tendencies, but all of the other materials showed no evidence of SCC or significant general corrosion. The cracking tendency of the susceptible steel was associated with an abnormal carbide morphology. A series of 250/degree/C capsule tests, conducted for times of up to 6 months, similarly indicated that neither SCC nor general corrosion was a problem area for these material-environment combinations. General corrosion rates were <0.1 mil/year (mpy). The two materials that performed best, type A106B mild steel and type 304L stainless steel, were tested while being dynamically strained in an 80% nitrate salt/20% water mixture at 250/degree/C. These materials survived the tests with no indication of SCC or other significant corrosion effects. Based on this relatively short-term laboratory test program, type 304L stainless steel and A106B carbon steel can be recommended as candidate classes of structural materials for the nitrate-carrying piping of the chemical heat pump. It is noted that stringent microstructural control may be required in the case of type A106B piping. 2 refs., 14 figs., 7 tabs.

  1. Corrosion and degradation of materials in the Synthane coal-gasification pilot plant

    SciTech Connect (OSTI)

    Yurkewycz, R.; Firestone, R.F.

    1981-09-01

    Corrosion monitoring of materials was conducted in the operating environments of the Synthane coal gasification pilot plant between 1976 and 1978. Metal and refractory specimens were exposed in the gasifier vessel in two test locations (fluidized bed, freeboard). Metal coupons only were exposed in the gasifier char cooler (freeboard) and four test locations in the quench system (vapor and liquid phases). Exposure times under operating conditions were 181 to 782 h. In two gasifier test locations (600 psig, 1284/sup 0/F and 1434/sup 0/F), the performance of nickel-base alloys with >20 wt % Cr, 40 to 46 wt % Ni, and 3 to 9.1 wt % Mo was consistently better than for other test alloys. Equivalent linear corrosion rates for these better alloys were < 20 mpy (782 h) with Montana Rosebud coal as feedstock; however, with Illinois No. 6 coal the linear rates were >20 mpy but <75 mpy (181 h). IN-600 (76.5 wt % Ni, 15.8 wt % Cr) was found unsuitable for gasifier internal application. All refractories tested in the two gasifier test locations (600 psig, 1284/sup 0/F and 1434/sup 0/F), with the exception of silicon nitride, were not greatly affected during either exposure period. The better materials were monolithic refractories with 5 to 30% porosity and 50 to 60% alumina content. Corrosion monitoring of metals in the gasifier char cooler freeboard (600 psig, 800/sup 0/F) showed that Type 304 was more resistant to corrosion attack than Type 410 and carbon steel (A-515).During exposure in the product gas quench system (5 to 600 psig, 200/sup 0/ to 445/sup 0/F), austenitic stainless steels, IN-600, and Type 430 experienced only limited corrosion loss and slight to moderate pitting attack (maximum pit depth <7 mils). Monel 400 and carbon steel specimens incurred unacceptable levels of degradation.

  2. A thermodynamic tank model for studying the effect of higher hydrocarbons on natural gas storage in metal-organic frameworks

    SciTech Connect (OSTI)

    Zhang, HD; Deria, P; Farha, OK; Hupp, JT; Snurr, RQ

    2015-01-01

    Metal-organic frameworks (MOFs) are promising materials for storing natural gas in vehicular applications. Evaluation of these materials has focused on adsorption of pure methane, although commercial natural gas also contains small amounts of higher hydrocarbons such as ethane and propane, which adsorb more strongly than methane. There is, thus, a possibility that these higher hydrocarbons will accumulate in the MOF after multiple operating (adsorption/desorption) cycles, and reduce the storage capacity. To study the net effect of ethane and propane on the performance of an adsorbed natural gas (ANG) tank, we developed a mathematical model based on thermodynamics and mass balance equations that describes the state of the tank at any instant. The required inputs are the pure-component isotherms, and mixture adsorption data are calculated using the Ideal Adsorbed Solution Theory (IAST). We focused on how the "deliverable energy'' provided by the ANG tank to the engine changed over 200 operating cycles for a sample of 120 MOF structures. We found that, with any MOF, the ANG tank performance monotonically declines during early operating cycles until a "cyclic steady state'' is reached. We determined that the best materials when the fuel is 100% methane are not necessarily the best when the fuel includes ethane and propane. Among the materials tested, some top MOFs are MOF-143 > NU-800 > IRMOF-14 > IRMOF-20 > MIL-100 > NU-125 > IRMOF-1 > NU-111. MOF-143 is predicted to deliver 5.43 MJ L-1 of tank to the engine once the cyclic steady state is reached. The model also provided insights that can assist in future work to discover more promising adsorbent materials for natural gas storage.

  3. Reactant gas composition for fuel cell potential control

    DOE Patents [OSTI]

    Bushnell, Calvin L.; Davis, Christopher L.

    1991-01-01

    A fuel cell (10) system in which a nitrogen (N.sub.2) gas is used on the anode section (11) and a nitrogen/oxygen (N.sub.2 /O.sub.2) gaseous mix is used on the cathode section (12) to maintain the cathode at an acceptable voltage potential during adverse conditions occurring particularly during off-power conditions, for example, during power plant shutdown, start-up and hot holds. During power plant shutdown, the cathode section is purged with a gaseous mixture of, for example, one-half percent (0.5%) oxygen (O.sub.2) and ninety-nine and a half percent (99.5%) nitrogen (N.sub.2) supplied from an ejector (21) bleeding in air (24/28) into a high pressure stream (27) of nitrogen (N.sub.2) as the primary or majority gas. Thereafter the fuel gas in the fuel processor (31) and the anode section (11) is purged with nitrogen gas to prevent nickel (Ni) carbonyl from forming from the shift catalyst. A switched dummy electrical load (30) is used to bring the cathode potential down rapidly during the start of the purges. The 0.5%/99.5% O.sub.2 /N.sub.2 mixture maintains the cathode potential between 0.3 and 0.7 volts, and this is sufficient to maintain the cathode potential at 0.3 volts for the case of H.sub.2 diffusing to the cathode through a 2 mil thick electrolyte filled matrix and below 0.8 volts for no diffusion at open circuit conditions. The same high pressure gas source (20) is used via a "T" juncture ("T") to purge the anode section and its associated fuel processor (31).

  4. Surface water processes in the Indonesian Throughflow as documented by a high-resolution coral (Delta)14C record

    SciTech Connect (OSTI)

    Fallon, S J; Guilderson, T P

    2008-04-23

    To explore the seasonal to decadal variability in surface water masses that contribute to the Indonesian Throughflow we have generated a 115-year bi-monthly coral-based radiocarbon time-series from a coral in the Makassar Straits. In the pre-bomb (pre-1955) era from 1890 to 1954, the radiocarbon time series occasionally displays a small seasonal signal (10-15{per_thousand}). After 1954 the radiocarbon record increases rapidly, in response to the increased atmospheric {sup 14}C content caused by nuclear weapons testing. From 1957 to 1986 the record displays clear seasonal variability from 15 to 60{per_thousand} and the post-bomb peak (163 per mil) occurred in 1974. The seasonal cycle of radiocarbon can be attributed to variations of surface waters passing through South Makassar Strait. Southern Makassar is under the influence of the Northwest Monsoon, which is responsible for the high Austral summer radiocarbon (North Pacific waters) and the Southeast Monsoon that flushes back a mixture of low (South Pacific and upwelling altered) radiocarbon water from the Banda Sea. The coral record also shows a significant {sup 14}C peak in 1955 due to bomb {sup 14}C water advected into this region in the form of CaCO{sub 3} particles (this implies that the particles were advected intact and then become entrapped in the coral skeleton--is this what we really mean? Wouldn't even fine particles settle out over the inferred transit time from Bikini to MAK?) or water particles with dissolved labeled CO{sub 2} produced during fallout from the Castle tests in 1954.

  5. A comparative analysis of the cryo-compression and cryo-adsorption hydrogen storage methods

    SciTech Connect (OSTI)

    Petitpas, G; Benard, P; Klebanoff, L E; Xiao, J; Aceves, S M

    2014-07-01

    While conventional low-pressure LH₂ dewars have existed for decades, advanced methods of cryogenic hydrogen storage have recently been developed. These advanced methods are cryo-compression and cryo-adsorption hydrogen storage, which operate best in the temperature range 30–100 K. We present a comparative analysis of both approaches for cryogenic hydrogen storage, examining how pressure and/or sorbent materials are used to effectively increase onboard H₂ density and dormancy. We start by reviewing some basic aspects of LH₂ properties and conventional means of storing it. From there we describe the cryo-compression and cryo-adsorption hydrogen storage methods, and then explore the relationship between them, clarifying the materials science and physics of the two approaches in trying to solve the same hydrogen storage task (~5–8 kg H₂, typical of light duty vehicles). Assuming that the balance of plant and the available volume for the storage system in the vehicle are identical for both approaches, the comparison focuses on how the respective storage capacities, vessel weight and dormancy vary as a function of temperature, pressure and type of cryo-adsorption material (especially, powder MOF-5 and MIL-101). By performing a comparative analysis, we clarify the science of each approach individually, identify the regimes where the attributes of each can be maximized, elucidate the properties of these systems during refueling, and probe the possible benefits of a combined “hybrid” system with both cryo-adsorption and cryo-compression phenomena operating at the same time. In addition the relationships found between onboard H₂ capacity, pressure vessel and/or sorbent mass and dormancy as a function of rated pressure, type of sorbent material and fueling conditions are useful as general designing guidelines in future engineering efforts using these two hydrogen storage approaches.

  6. Oxidation of selected alloys during 25,000 h in superheated steam at 482 and 538/sup 0/C

    SciTech Connect (OSTI)

    Griess, J.C.; Maxwell, W.A.

    1980-03-01

    The corrosion of several ferritic and austenitic materials in flowing superheated steam at 482 and 538/sup 0/C (900 and 1000/sup 0/F) were studied. Results obtained during the first 12,000 h of the test were presented previously. Results obtained during the first 25,000 h are summarized. The test specimens are mounted in a nonrecirculating loop that receives steam from the superheater circuit of a fossil-fired power plant. At both temperatures all materials exhibited parabolic oxidation kinetics during the first year and subsequently have oxidized at low constant rates. The ferritic steels containing 2 1/4 and 9% Cr have oxidized at about the same rates, averaging 4.2 and 8.6 ..mu..m/year (0.17 and 0.34 mils/year) at 482 and 538/sup 0/C, respectively, after the first year. Sandvik HT-9 (11.4% Cr) has corroded at slightly lower rates. Annealed and Cold-worked surfaces of these alloys have exhibited identical behavior. At 482/sup 0/C all materials have retained their corrosion products completely, but at 538/sup 0/C some began experiencing exfoliation after 12,000 h. Data suggest that a high silicon content in the alloy minimizes exfoliation. Cold-worked surfaces of alloy 800 are corroding at lower rates than annealed and pickled ones, but in both cases the rates are very low. Alloy 800 specimens that had been intergranularly corroded before exposure to steam are oxidizing at much higher rates, but intergranular penetration has not progressed. Type 304 stainless steel is corroding nonuniformly, but the attack rates are low at both temperatures. Alloy 617 is corroding at the lowest rate of any material in the loop; even after 25,000 h surface films are thin enough to show interference colors.

  7. Advanced heat exchanger development for molten salts

    SciTech Connect (OSTI)

    Sabharwall, Piyush; Clark, Denis; Glazoff, Michael; Zheng, Guiqiu; Sridharan, Kumar; Anderson, Mark

    2014-12-01

    This study addresses present work concerned with advanced heat exchanger development for molten salt in nuclear and non nuclear thermal systems. The molten salt systems discussed herein use alloys, such as Hastelloy N and 242, which show corrosion resistance to molten salt at nominal operating temperatures up to 700C. These alloys were diffusion welded, and the corresponding information is presented. Test specimens were prepared for exposing diffusion welds to molten salt environments. Hastelloy N and 242 were found to be weldable by diffusion welding, with ultimate tensile strengths about 90% of base metal values. Both diffusion welds and sheet material in Hastelloy N were corrosion tested in?58 mol% KF and 42 mol% ZrF4 at 650, 700, and 850C for 200, 500, and 1,000 hours. Corrosion rates found were similar between welded and nonwelded materials, typically <10 mils per year. For materials of construction, nickel and alloys with dense nickel coatings are effectively inert to corrosion in fluorides, but not so in chlorides. Hence, additional testing of selected alloys for resistance to intergranular corrosion is needed, as is a determination of corrosion rate as a function of contaminant type and alloy composition with respect to chromium and carbon to better define the optimal chromium and carbon composition, independent of galvanic or differential solubility effects. Also presented is the division of the nuclear reactor and high temperature components per ASME standards, along with design requirements for a subcritical Rankine power cycle heat exchanger that has to overcome pressure difference of about 17 MPa.

  8. Advanced heat exchanger development for molten salts

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Sabharwall, Piyush; Clark, Denis; Glazoff, Michael; Zheng, Guiqiu; Sridharan, Kumar; Anderson, Mark

    2014-12-01

    This study addresses present work concerned with advanced heat exchanger development for molten salt in nuclear and non nuclear thermal systems. The molten salt systems discussed herein use alloys, such as Hastelloy N and 242, which show corrosion resistance to molten salt at nominal operating temperatures up to 700°C. These alloys were diffusion welded, and the corresponding information is presented. Test specimens were prepared for exposing diffusion welds to molten salt environments. Hastelloy N and 242 were found to be weldable by diffusion welding, with ultimate tensile strengths about 90% of base metal values. Both diffusion welds and sheet materialmore » in Hastelloy N were corrosion tested in?58 mol% KF and 42 mol% ZrF4 at 650, 700, and 850°C for 200, 500, and 1,000 hours. Corrosion rates found were similar between welded and nonwelded materials, typically <10 mils per year. For materials of construction, nickel and alloys with dense nickel coatings are effectively inert to corrosion in fluorides, but not so in chlorides. Hence, additional testing of selected alloys for resistance to intergranular corrosion is needed, as is a determination of corrosion rate as a function of contaminant type and alloy composition with respect to chromium and carbon to better define the optimal chromium and carbon composition, independent of galvanic or differential solubility effects. Also presented is the division of the nuclear reactor and high temperature components per ASME standards, along with design requirements for a subcritical Rankine power cycle heat exchanger that has to overcome pressure difference of about 17 MPa.« less

  9. Long Term Corrosion/Degradation Test Six Year Results

    SciTech Connect (OSTI)

    M. K. Adler Flitton; C. W. Bishop; M. E. Delwiche; T. S. Yoder

    2004-09-01

    The Subsurface Disposal Area (SDA) of the Radioactive Waste Management Complex (RWMC) located at the Idaho National Engineering and Environmental Laboratory (INEEL) contains neutron-activated metals from non-fuel, nuclear reactor core components. The Long-Term Corrosion/Degradation (LTCD) Test is designed to obtain site-specific corrosion rates to support efforts to more accurately estimate the transfer of activated elements to the environment. The test is using two proven, industry-standard methodsdirect corrosion testing using metal coupons, and monitored corrosion testing using electrical/resistance probesto determine corrosion rates for various metal alloys generally representing the metals of interest buried at the SDA, including Type 304L stainless steel, Type 316L stainless steel, Inconel 718, Beryllium S200F, Aluminum 6061, Zircaloy-4, low-carbon steel, and Ferralium 255. In the direct testing, metal coupons are retrieved for corrosion evaluation after having been buried in SDA backfill soil and exposed to natural SDA environmental conditions for times ranging from one year to as many as 32 years, depending on research needs and funding availability. In the monitored testing, electrical/resistance probes buried in SDA backfill soil will provide corrosion data for the duration of the test or until the probes fail. This report provides an update describing the current status of the test and documents results to date. Data from the one-year and three-year results are also included, for comparison and evaluation of trends. In the six-year results, most metals being tested showed extremely low measurable rates of general corrosion. For Type 304L stainless steel, Type 316L stainless steel, Inconel 718, and Ferralium 255, corrosion rates fell in the range of no reportable to 0.0002 mils per year (MPY). Corrosion rates for Zircaloy-4 ranged from no measurable corrosion to 0.0001 MPY. These rates are two orders of magnitude lower than those specified in the

  10. DEPOSITION TANK CORROSION TESTING FOR ENHANCED CHEMICAL CLEANING POST OXALIC ACID DESTRUCTION

    SciTech Connect (OSTI)

    Mickalonis, J.

    2011-08-29

    An Enhanced Chemical Cleaning (ECC) process is being developed to aid in the high level waste tank closure at the Savannah River Site. The ECC process uses an advanced oxidation process (AOP) to destroy the oxalic acid that is used to remove residual sludge from a waste tank prior to closure. The AOP process treats the dissolved sludge with ozone to decompose the oxalic acid through reactions with hydroxyl radicals. The effluent from this oxalic acid decomposition is to be sent to a Type III waste tank and may be corrosive to these tanks. As part of the hazardous simulant testing that was conducted at the ECC vendor location, corrosion testing was conducted to determine the general corrosion rate for the deposition tank and to assess the susceptibility to localized corrosion, especially pitting. Both of these factors impact the calculation of hydrogen gas generation and the structural integrity of the tanks, which are considered safety class functions. The testing consisted of immersion and electrochemical testing of A537 carbon steel, the material of construction of Type III tanks, and 304L stainless steel, the material of construction for transfer piping. Tests were conducted in solutions removed from the destruction loop of the prototype ECC set up. Hazardous simulants, which were manufactured at SRNL, were used as representative sludges for F-area and H-area waste tanks. Oxalic acid concentrations of 1 and 2.5% were used to dissolve the sludge as a feed to the ECC process. Test solutions included the uninhibited effluent, as well as the effluent treated for corrosion control. The corrosion control options included mixing with an inhibited supernate and the addition of hydroxide. Evaporation of the uninhibited effluent was also tested since it may have a positive impact on reducing corrosion. All corrosion testing was conducted at 50 C. The uninhibited effluent was found to increase the corrosion rate by an order of magnitude from less than 1 mil per year (mpy

  11. New processing technique for DEB powder for thermal batteries

    SciTech Connect (OSTI)

    Szwarc, R.; Walton, R.D.

    1980-06-01

    The purpose of this paper is to explore how material processing influences thermal battery performance, and how battery performance can be improved by changes in processing. This discussion is confined to the class of thermal batteries designed by Sandia Laboratories and built under the supervision of General Electric in St. Petersburg, Florida. The electrochemical system employed is: Ca/LiCl-KCl-CaCrO/sub 4//Fe. These batteries are primary reserve batteries which employ a pelletized cell design. Each cell consists of an electrolyte-depolarizer pellet sandwiched between an anode and a heat pellet. The anode employed may be one of two forms: sheet calcium disc, mechanically attached to an iron or steel backing; or a substrate disc of iron or steel on which 3 to 5 mils of calcium had been evaporated. The depolarizer-electrolyte, commonly referred to as DEB, is composed of CaCrO/sub 4/, LiCl-KCl eutectic and SiO/sub 2/ binder powder, which has been blended and pressed into pellets. The DEB pellet serves as electrolyte and as active cathode when the salt becomes molten upon battery activation. The heat pellet serves the dual purpose of providing the heat necessary to activate the battery and as the cathode current collector. The heat pellet is composed of iron powder and KClO/sub 4/. A battery is made up of one or more stacks of about 12 cells connected in series to produce a voltage of 28 to 32 volts. Since activated life requirements for batteries vary from seconds up to one hour, the battery must be well insulated to conserve the heat produced by the ignition of the heat pellets to maintain the electrolyte in a molten state. This insulation is also important to protect sensitive electronic components in contact with the battery case. Because the electrolyte, particularly LiCl, is hygroscopic, the batteries are hermetically sealed in stainless steel cans, and are manufactured in dryrooms maintained at 3% relative humidity or better.

  12. Assessment of Recuperator Materials for Microturbines

    SciTech Connect (OSTI)

    Omatete, O.O.

    2001-01-30

    Microturbines in production (or nearly in production) use metal recuperators with gas inlet temperatures of less than 700 C to raise their efficiency to about 30%. To increase their efficiencies to greater than 40% (which is the DOE Advanced Microturbine Program goal) will require operating at higher gas inlet temperatures, if the compression ratio remains less than 6. Even at higher compression ratios, the inlet temperature will increase as the efficiency increases, necessitating the use of new materials of construction. The materials requirement for recuperators used in microturbines may be categorized by their maximum operating temperatures: 700, 800, and {approximately}900 C. These limits are based on the materials properties that determine recuperator failure, such as corrosion, oxidation, creep, and strength. Metallic alloys are applicable in the 700 and 800 C limits; ceramics are applicable in the 900 C range. Most of the heat exchangers in the current microturbines are primary surface recuperators (PSR), compact recuperators fabricated in 347 stainless steel by rolling foil that is a few (>5) mil thick into air cells; the metal recuperators are operated at temperatures below 650 C. Preliminary research indicates that the use of 347 stainless steel can be extended to 700 C. However, additional directed research is required to improve the current properties of 347 stainless steel and to evaluate extended demonstrations on recuperators fabricated from it. Beyond 700 C and up to about 800 C, advanced austenitic stainless steels or other alloys or superalloys become applicable. Their properties must be measured in the expected operational environment, and recuperators fabricated from them must be evaluated for an extended period. Temperatures beyond 900 C exceed the limits of metals, and ceramic materials will be needed. The relevant properties of Si{sub 3} N{sub 4} and SiC, (creep, corrosion, and oxidation) have been studied extensively. Prototype ceramic

  13. NDE reliability and probability of detection (POD) evolution and paradigm shift

    SciTech Connect (OSTI)

    Singh, Surendra

    2014-02-18

    The subject of NDE Reliability and POD has gone through multiple phases since its humble beginning in the late 1960s. This was followed by several programs including the important one nicknamed “Have Cracks – Will Travel” or in short “Have Cracks” by Lockheed Georgia Company for US Air Force during 1974–1978. This and other studies ultimately led to a series of developments in the field of reliability and POD starting from the introduction of fracture mechanics and Damaged Tolerant Design (DTD) to statistical framework by Bernes and Hovey in 1981 for POD estimation to MIL-STD HDBK 1823 (1999) and 1823A (2009). During the last decade, various groups and researchers have further studied the reliability and POD using Model Assisted POD (MAPOD), Simulation Assisted POD (SAPOD), and applying Bayesian Statistics. All and each of these developments had one objective, i.e., improving accuracy of life prediction in components that to a large extent depends on the reliability and capability of NDE methods. Therefore, it is essential to have a reliable detection and sizing of large flaws in components. Currently, POD is used for studying reliability and capability of NDE methods, though POD data offers no absolute truth regarding NDE reliability, i.e., system capability, effects of flaw morphology, and quantifying the human factors. Furthermore, reliability and POD have been reported alike in meaning but POD is not NDE reliability. POD is a subset of the reliability that consists of six phases: 1) samples selection using DOE, 2) NDE equipment setup and calibration, 3) System Measurement Evaluation (SME) including Gage Repeatability and Reproducibility (Gage R and R) and Analysis Of Variance (ANOVA), 4) NDE system capability and electronic and physical saturation, 5) acquiring and fitting data to a model, and data analysis, and 6) POD estimation. This paper provides an overview of all major POD milestones for the last several decades and discuss rationale for using

  14. Computational Modeling and Assessment Of Nanocoatings for Ultra Supercritical Boilers

    SciTech Connect (OSTI)

    David W. Gandy; John P. Shingledecker

    2011-04-11

    Forced outages and boiler unavailability in conventional coal-fired fossil power plants is most often caused by fireside corrosion of boiler waterwalls. Industry-wide, the rate of wall thickness corrosion wastage of fireside waterwalls in fossil-fired boilers has been of concern for many years. It is significant that the introduction of nitrogen oxide (NOx) emission controls with staged burners systems has increased reported waterwall wastage rates to as much as 120 mils (3 mm) per year. Moreover, the reducing environment produced by the low-NOx combustion process is the primary cause of accelerated corrosion rates of waterwall tubes made of carbon and low alloy steels. Improved coatings, such as the MCrAl nanocoatings evaluated here (where M is Fe, Ni, and Co), are needed to reduce/eliminate waterwall damage in subcritical, supercritical, and ultra-supercritical (USC) boilers. The first two tasks of this six-task project-jointly sponsored by EPRI and the U.S. Department of Energy (DE-FC26-07NT43096)-have focused on computational modeling of an advanced MCrAl nanocoating system and evaluation of two nanocrystalline (iron and nickel base) coatings, which will significantly improve the corrosion and erosion performance of tubing used in USC boilers. The computational model results showed that about 40 wt.% is required in Fe based nanocrystalline coatings for long-term durability, leading to a coating composition of Fe-25Cr-40Ni-10 wt.% Al. In addition, the long term thermal exposure test results further showed accelerated inward diffusion of Al from the nanocrystalline coatings into the substrate. In order to enhance the durability of these coatings, it is necessary to develop a diffusion barrier interlayer coating such TiN and/or AlN. The third task 'Process Advanced MCrAl Nanocoating Systems' of the six-task project jointly sponsored by the Electric Power Research Institute, EPRI and the U.S. Department of Energy (DE-FC26-07NT43096)- has focused on processing of

  15. EVALUATION OF FLOWSHEET CHANGES FOR THE HIGHLY ENRICHED URANIUM BLENDDOWN PROGRAM

    SciTech Connect (OSTI)

    Crowder, M.; Rudisill, T.; Laurinat, J.; Mickalonis, J.

    2007-10-22

    H Canyon is considering a flowsheet change for Plutonium (Pu) Contaminated Scrap (PuCS) material. The proposed change is to route dissolved PuCS material directly to a uranium (U) storage tank. As a result, the PuCS solution will bypass Head End and First U Cycle, and will be purified by solvent extraction in Second U Cycle. The PuCS solution contains appreciable amounts of boron (B) and fluoride (F{sup -}), which are currently at trace levels in the U storage tank. Though unlikely, if the B concentration in the U storage tank were to reach 1.8 g B/g U, the entire contents of the U storage tank would likely require a second pass through Second U Cycle to provide sufficient decontamination to meet the Tennessee Valley Authority (TVA) Blend Grade Highly Enriched Uranium (HEU) specification for B, which is 30 {micro}g/g U. In addition, Second U Cycle is expected to provide sufficient decontamination of F{sup -} and Pu regardless of the amount of PuCS solution sent to the storage tank. Though aluminum (Al) is not present in the PuCS solution, B can be credited as a complexant of F{sup -}. Both stability constants from the literature and Savannah River National Laboratory (SRNL) corrosion studies were documented to demonstrate that B complexation of F{sup -} in nitric acid solutions is sufficient to prevent excessive corrosion. Though B and Al complex F{sup -} to a similar degree, neither completely eliminates the presence of free F{sup -} in solution. Therefore, a limited amount of corrosion is expected even with complexed F{sup -} solutions. Tanks maintained at ambient temperature are not expected to experience significant corrosion. However, the Low Activity Waste (LAW) evaporators may be subjected to a corrosion rate of about 25 mils per year (mpy) as they reach their highest F{sup -} concentrations. The feed adjustment evaporator would only be subjected to the corrosion rate of about 25 mpy in the latter stages of the PuCS campaign. An issue that must be addressed

  16. A human factors approach towards the design of a new glovebox glove for Los Alamos National Laboratory

    SciTech Connect (OSTI)

    Oka, Jude M.

    2012-08-06

    thumb for better positioning, 45 degrees extension angle for the thumb for better positioning, and various angles for the other fingers to allow a more relaxed and natural fit. 3D modeling was used to implement the anthropometric data listed above onto an existing scanned solid model of a human hand. SolidWorks 2010 3-D modeling package was utilized to manipulate the hand model to represent the anthropometric data researched. The anthropometrics and modifications were reviewed by the University of New Mexico Department of Orthopedics hand surgeons. After all modifications and reviews were completed the model was printed out using stereolithography. The printed out model of the hand was used as a mold to create a prototype glovebox glove. The new mold was taken to Piercan USA to produce a 20mil Polyurethane/Hypalon glovebox glove. The Minnesota Dexterity test and Purdue Pegboard test were used to measure the dexterity of the prototype glovebox glove against a current 15 mil Hypalon LANL glovebox glove. Using the data from the tests a student t test was used to determine if there was a significant difference between the current hypalon glove results and the new prototype glove results. With a 95% confidence level the prototype showed to have a significantly lower mean difference from the current hypalon glovebox glove with the Minnesota Dexterity test. With a 95% confidence level the prototype showed to have a significantly higher mean difference from the current hypalon glovebox glove with the Purdue Pegboard test. A p value method was also performed to confirm the results of the student t test. A survey was also given to glovebox workers to determine if they preferred the new design. The best reaction from glovebox workers was the new thumb position, 73.2% of the sample population agreed with the new thumb position. Developing a new glovebox glove will improve the ergonomics of the hand for work performed, decrease exposure time, decreasing risk of breaching, increasing

  17. Task 4 - EMI/RFI Issues Potentially Impacting Electromagnetic Compatibility of I&C Systems (NRCHQ6014D0015)

    SciTech Connect (OSTI)

    Wood, Richard Thomas; Ewing, Paul D.

    2015-05-01

    The U.S. Nuclear Regulatory Commission’s (NRC’s) regulations in Part 50, “Domestic Licensing of Production and Utilization Facilities,” of Title 10 of the Code of Federal Regulations (10 CFR Part 50) state that structures, systems, and components important to safety in a nuclear power plant are to be designed to accommodate the effects of environmental conditions (i.e., remain functional under all postulated service conditions) and that design control measures such as testing are to be used to check the adequacy of design. Regulatory Guide (RG) 1.180 was developed to provide guidance to licensees and applicants on methods acceptable to the NRC staff for complying with the NRC’s regulations on design, installation, and testing practices for addressing the effects of electromagnetic and radio-frequency interference (EMI/RFI) and power surges on safety-related instrumentation and control (I&C) systems. The first revision of RG 1.180 was issued in January 2000 and a second revision was issued in October 2003*. The second revision differed from the first revision in endorsing Military Standard (MIL-STD)-461E and the International Electrotechnical Commission (IEC) Standard (Std) 61000 series of EMI/RFI test methods, extending the guidance to cover signal line testing, incorporating frequency ranges where portable communications devices are experiencing increasing use, and relaxing the operating envelopes (test levels) when experience and confirmatory research warranted. It also offered exemptions from specific test criteria based on technical considerations such as plant conditions and the intended location of the safety-related I&C equipment. Since the last revision, new requirements have been identified, associated RGs have been created and updated, and additional industry guidance has been developed. Additionally, the operational environment has changed with the increase in wireless communication technology for both personal (smartphone) and industrial

  18. A STRUCTURAL IMPACT ASSESSMENT OF FLAWS DETECTED DURING ULTRASONIC EXAMINATION OF TANK 15

    SciTech Connect (OSTI)

    Wiersma, B; James Elder, J

    2008-08-21

    residual stress zone. None of the three cracks beneath the sludge showed evidence of growth. The impact of the cracks that grew on the future service of Tank 15 was also assessed. Tank 15 is expected to undergo closure activities including sludge waste removal. A bounding loading condition for waste removal of the sludge at the bottom of Tank 15 was considered for this analysis. The analysis showed that the combination of hydrostatic, seismic, pump and weld residual stresses are not expected to drive any of the cracks identified during the Tank 15 UT inspection to instability. Wall thickness mapping for general thinning and pitting was also performed. No significant wall thinning was observed. The average wall thickness values were well above nominal. Two isolated pit-like indications were observed. Both were approximately 30 mils deep. However, the remaining wall thickness was still greater than nominal specified for the original construction plate material. It was recommended that a third examination of selected cracks in Tank 15 be performed in 2014. This examination would provide information to determine whether any additional detectable degradation is occurring in Tank 15 and to supplement the basis for characterization of conditions that are non-aggressive to tank corrosion damage. The in-service inspection program is re-evaluated on a three year periodicity. The Type I and II tanks are not active receipt tanks at present, and are therefore not a part of the In-Service Inspection Program for the Type III Tanks [1]. Changes to the mission for Tank 15 and other Type I and II tanks may be considered by the In-Service Inspection Review Committee (ISIRC) and the program adjusted accordingly.

  19. Prompt Neutron Multiplicity Measurements with Portable Detectors

    SciTech Connect (OSTI)

    S. Mukhopadhyay, R. Wolff, R. Maurer, S. Mitchell, E. X. Smith, P. Guss, J. L. Lacy, L. Sun, A. Athanasiades

    2011-09-01

    Mobile detection of kilogram quantities of special nuclear materials (SNM) during maritime transportation is a challenging problem for the U.S. Department of Homeland Security. Counting neutrons emitted by the SNM and partitioning them from background neutrons of multiple origins is the most effective passive means of detecting the SNM. Unfortunately, neutron detection, counting, and partitioning in a maritime environment is complex due to the presence of spallation neutrons (commonly known as “ship effect”) and to the complicated nature of the neutron scattering in that environment. This work studied the possibilities of building a prototype neutron detector using boron- 10 (10B) as the converter in a novel form factor called “straws” that would address the above problem by examining multiplicity distributions of neutrons originating from a fissioning source. Currently, commercially manufactured fission meters (FM) are available that separate cosmic neutrons from non-cosmic neutrons and quantitatively determine the strength of a fissioning source; however, these FMs use 3He, which is becoming increasingly difficult to procure; also the size and weight of a commercial FM is not conducive to manual neutron detection operations in a maritime environment. The current project may provide a near-term solution to the crisis that has arisen from the global scarcity of 3He by offering a viable alternative to the FM. The prototype detector provides a large-area, efficient, lightweight, more granular neutron responsive detection surface (to facilitate imaging) to ease the application of the new FMs. A novel prototype fission meter is being designed at National Security Technologies, LLC, using a thin uniform coating of 10B as neutron converter (only 1 micron thick) inside a large array of thin (4 mm diameter) copper tubes. The copper tubes are only 2-mil thick, and each holds the stretched anode wire under tension and high voltage. The tubes are filled with