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Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


1

Sample heating in near-field scanning optical microscopy  

E-Print Network [OSTI]

Heating near the aperture of aluminumcoated,fiber opticnear-field scanning optical microscopy probes was studied as a function of input and output powers. Using the shear-force feedback method, near-field probes were positioned nanometers above a...

Erickson, Elizabeth S.; Dunn, Robert C.

2005-10-05T23:59:59.000Z

2

Widely tuneable scattering-type scanning near-field optical microscopy using pulsed quantum cascade lasers  

SciTech Connect (OSTI)

We demonstrate the use of a pulsed quantum cascade laser, wavelength tuneable between 6 and 10??m, with a scattering-type scanning near-field optical microscope (s-SNOM). A simple method for calculating the signal-to-noise ratio (SNR) of the s-SNOM measurement is presented. For pulsed lasers, the SNR is shown to be highly dependent on the degree of synchronization between the laser pulse and the sampling circuitry; in measurements on a gold sample, the SNR is 26 with good synchronization and less than 1 without. Simulations and experimental s-SNOM images, with a resolution of 100?nm, corresponding to ?/80, and an acquisition time of less than 90 s, are presented as proof of concept. They show the change in the field profile of plasmon-resonant broadband antennas when they are excited with wavelengths of 7.9 and 9.5??m.

Yoxall, Edward, E-mail: edward.yoxall@imperial.ac.uk; Rahmani, Mohsen; Maier, Stefan A.; Phillips, Chris C. [The Blackett Laboratory, Department of Physics, Imperial College London, London SW7 2AZ (United Kingdom)] [The Blackett Laboratory, Department of Physics, Imperial College London, London SW7 2AZ (United Kingdom); Navarro-Cía, Miguel [Optical and Semiconductor Devices Group, Department of Electrical and Electronic Engineering, Imperial College London, London SW7 2BT (United Kingdom)] [Optical and Semiconductor Devices Group, Department of Electrical and Electronic Engineering, Imperial College London, London SW7 2BT (United Kingdom)

2013-11-18T23:59:59.000Z

3

Single Defect Center Scanning Near-Field Optical Microscopy on Graphene  

E-Print Network [OSTI]

We demonstrate high resolution scanning fluorescence resonance energy transfer 10 microscopy between a single nitrogen-vacancy center as donor and graphene as acceptor. 11 Images with few nanometer resolution of single and multilayer graphene structures were 12 attained. An energy transfer efficiency of 30% at distances of 10nm between a single 13 defect and graphene was measured. Further the energy transfer distance dependence of 14 the nitrogen-vacancy center to graphene was measured to show the predicted d-4 15 dependence. Our studies pave the way towards a diamond defect center based versatile 16 single emitter scanning microscope.

J. Tisler; T. Oeckinghaus; R. Stöhr; R. Kolesov; F. Reinhard; J. Wrachtrup

2013-01-02T23:59:59.000Z

4

Near-field microscopy with a scanning nitrogen-vacancy color center in a diamond nanocrystal: A brief review  

E-Print Network [OSTI]

We review our recent developments of near-field scanning optical microscopy (NSOM) that uses an active tip made of a single fluorescent nanodiamond (ND) grafted onto the apex of a substrate fiber tip. The ND hosting a limited number of nitrogen-vacancy (NV) color centers, such a tip is a scanning quantum source of light. The method for preparing the ND-based tips and their basic properties are summarized. Then we discuss theoretically the concept of spatial resolution that is achievable in this special NSOM configuration and find it to be only limited by the scan height over the imaged system, in contrast with the standard aperture-tip NSOM whose resolution depends critically on both the scan height and aperture diameter. Finally, we describe a scheme we have introduced recently for high-resolution imaging of nanoplasmonic structures with ND-based tips that is capable of approaching the ultimate resolution anticipated by theory.

Drezet, A; Cuche, A; Mollet, O; Berthel, M; Huant, S

2015-01-01T23:59:59.000Z

5

Probing nanoscale photo-oxidation in organic films using spatial hole burning near-field scanning optical microscopy  

E-Print Network [OSTI]

Probing nanoscale photo-oxidation in organic films using spatial hole burning near-field scanning from a stationary NSOM tip to induce photo-oxidation. The reduction in the fluorescence yield resulting photo-oxidation as a function of time, position, and environment free from the limits of far

Buratto, Steve

6

Infrared Scattering Scanning Near-Field Optical Microscopy Using An External Cavity Quantum Cascade Laser For Nanoscale Chemical Imaging And Spectroscopy of Explosive Residues  

SciTech Connect (OSTI)

Infrared scattering scanning near-field optical microscopy (s-SNOM) is an apertureless superfocusing technique that uses the antenna properties of a conducting atomic force microscope (AFM) tip to achieve infrared spatial resolution below the diffraction limit. The instrument can be used either in imaging mode, where a fixed wavelength light source is tuned to a molecular resonance and the AFM raster scans an image, or in spectroscopy mode where the AFM is held stationary over a feature of interest and the light frequency is varied to obtain a spectrum. In either case, a strong, stable, coherent infrared source is required. Here we demonstrate the integration of a broadly tunable external cavity quantum cascade laser (ECQCL) into an s-SNOM and use it to obtain infrared spectra of microcrystals of chemicals adsorbed onto gold substrates. Residues of the explosive compound tetryl was deposited onto gold substrates. s-SNOM experiments were performed in the 1260-1400 cm?1 tuning range of the ECQCL, corresponding to the NO2 symmetric stretch vibrational fingerprint region. Vibrational infrared spectra were collected on individual chemical domains with a collection area of *500nm2 and compared to ensemble averaged far-field reflection-absorption infrared spectroscopy (RAIRS) results.

Craig, Ian M.; Phillips, Mark C.; Taubman, Matthew S.; Josberger, Erik E.; Raschke, Markus Bernd

2013-02-04T23:59:59.000Z

7

Single Molecule Emission Characteristics in Near-Field Microscopy  

Science Journals Connector (OSTI)

In near-field scanning optical microscopy (NSOM), the measured fluorescence lifetime of a single dye molecule can be shortened or lengthened, sensitively dependent on the relative position between the molecule and aluminum coated fiber tip. The modified lifetimes and other emission characteristics are simulated by solving Maxwell equations with the finite-difference time-domain (FDTD) method. The 2D computation reveals insight into the lifetime behaviors and provides guidance for nonperturbative spectroscopic measurements with NSOM. This new methodology is capable of predicting molecular emission properties in front of a metal/dielectric interface of arbitrary geometry.

Randy X. Bian; Robert C. Dunn; X. Sunney Xie; P. T. Leung

1995-12-25T23:59:59.000Z

8

Scanning tip microwave near field microscope  

DOE Patents [OSTI]

A microwave near field microscope has a novel microwave probe structure wherein the probing field of evanescent radiation is emitted from a sharpened metal tip instead of an aperture or gap. This sharpened tip, which is electrically and mechanically connected to a central electrode, extends through and beyond an aperture in an endwall of a microwave resonating device such as a microwave cavity resonator or a microwave stripline resonator. Since the field intensity at the tip increases as the tip sharpens, the total energy which is radiated from the tip and absorbed by the sample increases as the tip sharpens. The result is improved spatial resolution without sacrificing sensitivity.

Xiang, Xiao-Dong (Alameda, CA); Schultz, Peter G. (Oakland, CA); Wei, Tao (Albany, CA)

1998-01-01T23:59:59.000Z

9

A near-field scanning microwave microscope based on a superconducting resonator for low power measurements  

E-Print Network [OSTI]

We report on the design and performance of a cryogenic (300 mK) near-field scanning microwave microscope. It uses a microwave resonator as the near-field sensor, operating at a frequency of 6 GHz and microwave probing amplitudes down to 100 uV, approaching low enough photon population (N~1000) of the resonator such that coherent quantum manipulation becomes feasible. The resonator is made out of a miniaturized distributed fractal superconducting circuit that is integrated with the probing tip, micromachined to be compact enough such that it can be mounted directly on a quartz tuning-fork, and used for parallel operation as an atomic force microscope (AFM). The resonator is magnetically coupled to a transmission line for readout, and to achieve enhanced sensitivity we employ a Pound-Drever-Hall measurement scheme to lock to the resonance frequency. We achieve a well localized near-field around the tip such that the microwave resolution is comparable to the AFM resolution, and a capacitive sensitivity down to 6.4x10^-20 F/rtHz, limited by mechanical noise. We believe that the results presented here are a significant step towards probing quantum systems at the nanoscale using near-field scanning microwave microscopy.

S. E. de Graaf; A. V. Danilov; A. Adamyan; S. E. Kubatkin

2014-04-02T23:59:59.000Z

10

Near-field microwave microscopy of high-? oxides grown on graphene with an organic seeding layer  

SciTech Connect (OSTI)

Near-field scanning microwave microscopy (SMM) is used for non-destructive nanoscale characterization of Al{sub 2}O{sub 3} and HfO{sub 2} films grown on epitaxial graphene on SiC by atomic layer deposition using a self-assembled perylene-3,4,9,10-tetracarboxylic dianhydride seeding layer. SMM allows imaging of buried inhomogeneities in the dielectric layer with a spatial resolution close to 100?nm. The results indicate that, while topographic features on the substrate surface cannot be eliminated as possible sites of defect nucleation, the use of a vertically heterogeneous Al{sub 2}O{sub 3}/HfO{sub 2} stack suppresses formation of large outgrowth defects in the oxide film, ultimately improving lateral uniformity of the dielectric film.

Tselev, Alexander, E-mail: tseleva@ornl.gov; Kalinin, Sergei V. [Oak Ridge National Laboratory, Center for Nanophase Materials Sciences, Oak Ridge, Tennessee 37831 (United States)] [Oak Ridge National Laboratory, Center for Nanophase Materials Sciences, Oak Ridge, Tennessee 37831 (United States); Sangwan, Vinod K.; Jariwala, Deep; Lauhon, Lincoln J. [Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois 60208 (United States)] [Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois 60208 (United States); Marks, Tobin J.; Hersam, Mark C. [Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois 60208 (United States) [Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois 60208 (United States); Department of Chemistry, Northwestern University, Evanston, Illinois 60208 (United States)

2013-12-09T23:59:59.000Z

11

Photothermal imaging scanning microscopy  

DOE Patents [OSTI]

Photothermal Imaging Scanning Microscopy produces a rapid, thermal-based, non-destructive characterization apparatus. Also, a photothermal characterization method of surface and subsurface features includes micron and nanoscale spatial resolution of meter-sized optical materials.

Chinn, Diane (Pleasanton, CA); Stolz, Christopher J. (Lathrop, CA); Wu, Zhouling (Pleasanton, CA); Huber, Robert (Discovery Bay, CA); Weinzapfel, Carolyn (Tracy, CA)

2006-07-11T23:59:59.000Z

12

Fluorescence resonance energy transfer scanning near-field optical microscopy  

Science Journals Connector (OSTI)

...and applications. New York: Wiley Interscience...Fluorescence resonance energy transfer SNOM 919...fluorescence resonance energy transfer source...Electromagnetic theory. New York: McGraw-Hill...hierarchy and directed energy transfer in conjugated...

2004-01-01T23:59:59.000Z

13

A near-field scanning microwave microscope based on a superconducting resonator for low power measurements  

E-Print Network [OSTI]

We report on the design and performance of a cryogenic (300 mK) near-field scanning microwave microscope. It uses a microwave resonator as the near-field sensor, operating at a frequency of 6 GHz and microwave probing amplitudes down to 100 uV, approaching low enough photon population (N~1000) of the resonator such that coherent quantum manipulation becomes feasible. The resonator is made out of a miniaturized distributed fractal superconducting circuit that is integrated with the probing tip, micromachined to be compact enough such that it can be mounted directly on a quartz tuning-fork, and used for parallel operation as an atomic force microscope (AFM). The resonator is magnetically coupled to a transmission line for readout, and to achieve enhanced sensitivity we employ a Pound-Drever-Hall measurement scheme to lock to the resonance frequency. We achieve a well localized near-field around the tip such that the microwave resolution is comparable to the AFM resolution, and a capacitive sensitivity down to 6...

de Graaf, S E; Adamyan, A; Kubatkin, S E

2014-01-01T23:59:59.000Z

14

Imaging of quantum Hall edge states under quasiresonant excitation by a near-field scanning optical microscope  

SciTech Connect (OSTI)

A high resolution mapping of quantum Hall edge states has been performed by locally creating electrons with small excess energies with a near-field scanning optical microscope in a dilution refrigerator. We have observed fine structures parallel to the edge in photovoltage signals, which appear only at low temperature. The observed fine structures near sample edges have been seen to shift inward with increase in magnetic field in accordance with Chklovskii Shklovskii, and Glazman model.

Ito, H.; Shibata, Y.; Mamyoda, S.; Ootuka, Y.; Nomura, S. [Division of Physics, University of Tsukuba, Tennodai, Tsukuba, 305-8571 (Japan); Kashiwaya, S. [National Institute of Advanced Industrial Science and Technology (AIST), Umezono, Tsukuba, 305-8568 (Japan); Yamaguchi, M.; Akazaki, T.; Tamura, H. [NTT Basic Research Laboratories, NTT Corporation, Morinosato-Wakamiya, Atsugi, 243-0198 (Japan)

2013-12-04T23:59:59.000Z

15

Modeling and characterization of a cantilever-based near-field scanning microwave impedance microscope  

Science Journals Connector (OSTI)

This paper presents a detailed modeling and characterization of a microfabricated cantilever-based scanning microwave probe with separated excitation and sensing electrodes. Using finite-element analysis we model the tip-sample interaction as small impedance changes between the tip electrode and the ground at our working frequencies near 1 GHz . The equivalent lumped elements of the cantilever can be determined by transmission line simulation of the matching network which routes the cantilever signals to 50 ? feed lines. In the microwave electronics the background common-mode signal is canceled before the amplifier stage so that high sensitivity (below 1 aF capacitance changes) is obtained. Experimental characterization of the microwavemicroscope was performed on ion-implanted Si wafers and patterned semiconductor samples. Pure electrical or topographical signals can be obtained from different reflection modes of the probe.

K. Lai; W. Kundhikanjana; M. Kelly; Z. X. Shen

2008-01-01T23:59:59.000Z

16

Fast scanning two-photon microscopy  

E-Print Network [OSTI]

Fast scanning two-photon microscopy coupled with the use light activated ion channels provides the basis for fast imaging and stimulation in the characterization of in vivo neural networks. A two-photon microscope capable ...

Chang, Jeremy T

2010-01-01T23:59:59.000Z

17

Scanning Probe Microscopy Studies of Carbon Nanotubes  

E-Print Network [OSTI]

Scanning Probe Microscopy Studies of Carbon Nanotubes Teri Wang Odom1 , Jason H. Hafner1 relationship between Single-Walled Carbon Nanotube (SWNT) atomic structure and electronic properties, (2, properties and application of carbon nanotube probe microscopy tips to ultrahigh resolution and chemically

Odom, Teri W.

18

Atomic Force and Scanning Electron Microscopy of Atmospheric Particles  

E-Print Network [OSTI]

conducted so as to characterize atmospheric aerosols from anthropogenic (pollution) and natural (sea saltAtomic Force and Scanning Electron Microscopy of Atmospheric Particles ZAHAVA BARKAY,1 * AMIT 69978, Israel KEY WORDS atmospheric aerosols; atomic force microscopy; scanning electron microscopy

Shapira, Yoram

19

Scanning near-field optical microscopy based on the heterodyne phase-controlled oscillator method  

E-Print Network [OSTI]

obtained for the case of larger vibration amplitudes of the tip. © 2000 American Institute of Physics. S, the particular mechanical properties of such a ``lever'' prevented the broad use of the force-measurement. The idea behind the method is based on the measurement of the damping of the oscillation of the tip subject

Texas at Austin. University of

20

Etched chalcogenide fibers for near-field infrared scanning microscopy M. A. Unger,a)  

E-Print Network [OSTI]

Electron Laser Center, Stanford, California 94305-4085 Received 12 December 1997; accepted for publication by a sulfur-selenide cladding, which is in turn coated with a polymer such as polyamide. For use in a near cladding surrounding the core, and etching the chalcogenide fiber core to a sharp point. Removal

Palanker, Daniel

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

Surface Plasmon mediated near-field imaging and optical addressing in nanoscience  

E-Print Network [OSTI]

We present an overview of recent progress in plasmonics. We focus our study on the observation and excitation of surface plasmon polaritons (SPPs) with optical near-field microscopy. We discuss in particular recent applications of photon scanning tunnelling microscope (PSTM) for imaging of SPP propagating in metal and dielectric wave guides. We show how near-field scanning optical microscopy (NSOM) can be used to optically and actively address remotely nano-objects such as quantum dots. Additionally we compare results obtained with near-field microscopy to those obtained with other optical far-field methods of analysis such as leakage radiation microscopy (LRM).

Drezet, A; Krenn, J R; Brun, M; Huant, S

2007-01-01T23:59:59.000Z

22

Three-dimensional plastic response in polycrystalline copper via near-field high-energy X-ray diffraction microscopy  

Science Journals Connector (OSTI)

The evolution of the crystallographic orientation field in a polycrystalline sample of copper is mapped in three dimensions as tensile strain is applied. Using forward-modeling analysis of high-energy X-ray diffraction microscopy data, the ability to track intragranular orientation variations is demonstrated.

Li, S.F.

2012-10-25T23:59:59.000Z

23

Sub-Kelvin scanning tunneling microscopy on magnetic molecules.  

E-Print Network [OSTI]

??Magnetic molecules have attracted lots interest. In this work, an ultra-stable and low noise scanning tunneling microscopy operating at 400 mK using He-3 (930 mK… (more)

Zhang, Lei

2012-01-01T23:59:59.000Z

24

Reducing Photobleaching in STED Microscopy with Higher Scanning Speed  

E-Print Network [OSTI]

Photobleaching is a major limitation of super-resolution STED microscopy. We show that the photobleaching rate in STED microscopy is slowed down by scanning with a higher linear speed, enabled by the large field of view in our custom-built resonant-scanning STED microscope. The effect of scanning speed on photobleaching is more remarkable at higher levels of depletion laser irradiance. With a depletion irradiance of 0.4 GW/cm$^2$ (time average), we were able to slow down the photobleaching of the Atto 647N dye by 80% with 8-fold faster scanning. Photobleaching is primarily caused by the depletion light acting upon the excited fluorophores. Experimental data qualitatively agree with a theoretical model. Our results encourage further increasing linear scanning speed for photobleaching reduction in STED microscopy.

Wu, Yong

2014-01-01T23:59:59.000Z

25

Scanning Transmission Electron Microscopy Investigations of Complex Oxides  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Scanning Transmission Electron Microscopy Investigations of Complex Oxides Scanning Transmission Electron Microscopy Investigations of Complex Oxides Monday, May 23, 2011 - 3:30pm SSRL Conference room 137-322 Professor Tom Vogt, NanoCenter & Department of Chemistry, University of South Carolina High-Angle-Annular-Dark-Field/Scanning Transmission Electron Microscopy (HAADF/STEM) is a technique uniquely suited for detailed studies of the structure and composition of complex oxides. The HAADF detector collects electrons which have interact inelastically with the potentials of the atoms in the specimen and therefore resembles the better known Z2 (Z is atomic number) Rutherford scattering. One class of important catalysts consists of bronzes based on pentagonal {Mo6O21} building units; these include Mo5O14 and Mo17O47. In the last 20 years, new materials doped with

26

Characterization of power induced heating and damage in fiber optic probes for near-field scanning optical microscopy  

E-Print Network [OSTI]

polymer sample are measured as a function of probe output power, as was previously reported for pulled NSOM probes. The results reveal that sample heating increases rapidly to ?55–60°C as output powers reach ?50nW. At higher output powers, the sample...

Dickenson, Nicholas E.; Erickson, Elizabeth S.; Mooren, Olivia L.; Dunn, Robert C.

2007-04-07T23:59:59.000Z

27

Laser scanning third-harmonic-generation microscopy in biology  

E-Print Network [OSTI]

. Denk, J. H. Stricker and W. W. Webb, "Two-photon laser scanning fluorescence microscopy," Science 248, 73-76 (1990). 3. S. Maiti, J. B. Shear, R. M. Williams, W. R. Zipfel and W. W. Webb, "Measuring-214 (1996). 6. R. Hellwarth and P. Christensen, "Nonlinear optical microscopic examination of structure

Silberberg, Yaron

28

E-Print Network 3.0 - absorption spectroscopic microscopy Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

version of scanning near-field optical microscopy (SNOM). The tunable infrared radiation... the l 3.5 mm, CH vibrational stretch mode absorption band. ... Source:...

29

E-Print Network 3.0 - appendix a3 near-field Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Despite the rapid growth of near-field optical microscopy in the past... decade, many questions about the imaging properties of near-field microscopes ... Source: Dainty, Chris...

30

Advanced Photon Source | Combining Scanning Probe Microscopy and  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

01.2013 01.2013 Nanoscience Seminar presented at Tokyo University On November 1, 2013, Volker Rose was invited to present the Nanoscience Seminar at the Institute of Solid State Physics (ISSP) of the University of Tokyo. In his seminar he discussed the physical principles of Synchrotron X-ray Scanning Tunneling Microscopy (SXSTM) as well as the recent progress made by his team at the Advanced Photon Source. He was invited by Prof. Yukio Hasegawa, who himself conducts SXSTM experiment at the Photon Factory in Tsukuba, Japan. The ISSP serves as the central laboratory of materials science in Japan equipped with state-of-art facilities. It was relocated to the new campus in Kashiwa of the University of Tokyo in 2000 after the 43 years of activities at the Roppongi campus in downtown Tokyo. Here ISSP is focusing

31

Advanced Photon Source | Combining Scanning Probe Microscopy and  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

27.2013 27.2013 Researchers from NSLS-II visit SXSPM team at Argonne Synchrotron x-ray scanning tunneling microscopy will soon also be developed at the National Synchrotron Light Source (NSLS-II) at Brookhaven National Laboratory (BNL). In order to establish collaboration between the two National Laboratories, Drs. Evgeny Nazaretski and Hui Yan fom BNL visited Argonne to learn more about recent progress made in the SXSPM project. During the 2-day visit the teams discussed mutual scientific goals and strategies to achieve them. NSLS-II will be a new state-of-the-art, medium-energy electron storage ring at BNL designed to deliver high intensity and brightness. Construction of the NSLS-II's ring building began in March 2009. The new facility will begin operating in 2014

32

Advanced Photon Source | Combining Scanning Probe Microscopy and  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

APS APS SXSPM News Researchers from NSLS-II visit SXSPM team at Argonne (November 27, 2013) Cummings presents invited talk at magnetism meeting (November 11, 2013) Invited talk at ACSIN-12 & ICSPM21 in Japan (November 11, 2013) Nanoscience Seminar presented at Tokyo University (November 01, 2013) Scientists study old photos for new solutions to corrosion (October 21, 2013) More News Featured Image Recent Publications Kangkang Wang, Daniel Rosenmann, Martin Holt, Robert Winarski, Saw-Wai Hla, and Volker Rose, "An easy-to-implement filter for separating photo-excited signals from topography in scanning tunneling microscopy", Rev. Sci. Instrum. 84, 063704 (2013). More SXSPM Publications Upcoming Presentations V. Rose, 41st Conference on the Physics and Chemistry of Surfaces and Interfaces (PCSI-41) (Invited Speaker)

33

Combined Scanning Transmission Electron Microscopy Tilt- and Focal Series  

SciTech Connect (OSTI)

In this study, a combined tilt- and focal series is proposed as a new recording scheme for high-angle annular dark-field scanning transmission electron microscopy (STEM) tomography. Three-dimensional (3D) data were acquired by mechanically tilting the specimen, and recording a through-focal series at each tilt direction. The sample was a whole-mount macrophage cell with embedded gold nanoparticles. The tilt focal algebraic reconstruction technique (TF-ART) is introduced as a new algorithm to reconstruct tomograms from such combined tilt- and focal series. The feasibility of TF-ART was demonstrated by 3D reconstruction of the experimental 3D data. The results were compared with a conventional STEM tilt series of a similar sample. The combined tilt- and focal series led to smaller missing wedge artifacts, and a higher axial resolution than obtained for the STEM tilt series, thus improving on one of the main issues of tilt series-based electron tomography.

Dahmen, Tim [German Research Center for Artificial Intelligence (DFKI), Germany] [German Research Center for Artificial Intelligence (DFKI), Germany; Baudoin, Jean-Pierre G [ORNL] [ORNL; Lupini, Andrew R [ORNL] [ORNL; Kubel, Christian [Karlsruhe Institute of Technology, Leopoldshafen, Germany] [Karlsruhe Institute of Technology, Leopoldshafen, Germany; Slusallek, Phillip [German Research Center for Artificial Intelligence (DFKI), Germany] [German Research Center for Artificial Intelligence (DFKI), Germany; De Jonge, Niels [ORNL] [ORNL

2014-01-01T23:59:59.000Z

34

Mapping Magnetic Near-Field Distributions of Plasmonic Nanoantennas  

Science Journals Connector (OSTI)

However, standard far-field optical microscopy methods have insufficient resolution and provide no information about the electromagnetic near-fields. ... The top right panel of Figure 3a illustrates how the charges and magnetic near-field (green circles) at the probe aperture line up with the charge distribution and magnetic near-field of the SPR mode. ... and magnetic field lines and Poynting vector distributions are reconstructed in a vol. ...

Denitza Denkova; Niels Verellen; Alejandro V. Silhanek; Ventsislav K. Valev; Pol Van Dorpe; Victor V. Moshchalkov

2013-03-06T23:59:59.000Z

35

Electron and Scanning Probe Microscopies | U.S. DOE Office of Science (SC)  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Electron and Scanning Probe Microscopies Electron and Scanning Probe Microscopies Materials Sciences and Engineering (MSE) Division MSE Home About Research Areas Energy Frontier Research Centers (EFRCs) DOE Energy Innovation Hubs BES Funding Opportunities The Computational Materials and Chemical Sciences Network (CMCSN) Theoretical Condensed Matter Physics Scientific Highlights Reports and Activities Principal Investigators' Meetings BES Home Research Areas Electron and Scanning Probe Microscopies Print Text Size: A A A RSS Feeds FeedbackShare Page This research area supports basic research in condensed matter physics and materials physics using electron scattering and microscopy and scanning probe techniques. The research includes experiments and theory to understand the atomic, electronic, and magnetic structures of materials.

36

Band excitation method applicable to scanning probe microscopy  

DOE Patents [OSTI]

Methods and apparatus are described for scanning probe microscopy. A method includes generating a band excitation (BE) signal having finite and predefined amplitude and phase spectrum in at least a first predefined frequency band; exciting a probe using the band excitation signal; obtaining data by measuring a response of the probe in at least a second predefined frequency band; and extracting at least one relevant dynamic parameter of the response of the probe in a predefined range including analyzing the obtained data. The BE signal can be synthesized prior to imaging (static band excitation), or adjusted at each pixel or spectroscopy step to accommodate changes in sample properties (adaptive band excitation). An apparatus includes a band excitation signal generator; a probe coupled to the band excitation signal generator; a detector coupled to the probe; and a relevant dynamic parameter extractor component coupled to the detector, the relevant dynamic parameter extractor including a processor that performs a mathematical transform selected from the group consisting of an integral transform and a discrete transform.

Jesse, Stephen; Kalinin, Sergei V

2013-05-28T23:59:59.000Z

37

Bioelectrical SPMs (G. Gomila, UB-IBEC) Bioelectric Scanning Probe Microscopies  

E-Print Network [OSTI]

-ups: Micropippete based electrodes Measurements of cell membrane ion transport on single cells 2. Scanning Ion (SNOM),Scanning Tunneling Microscope (STM), Scanning Ion Conductance Microscope (SICM), Scanning Conductance Microscopy #12;7 Bioelectrical SPMs (G. Gomila, UB-IBEC) Single ion channels recordings Average

Ritort, Felix

38

Laser-Scanning Coherent Anti-Stokes Raman Scattering Microscopy and Applications to Cell Biology  

E-Print Network [OSTI]

Laser-Scanning Coherent Anti-Stokes Raman Scattering Microscopy and Applications to Cell Biology Ji 11747-3157 USA ABSTRACT Laser-scanning coherent anti-Stokes Raman scattering (CARS) microscopy with fast., 1990). Duncan et al. constructed the first CARS microscope by use of two dye laser beams

Xie, Xiaoliang Sunney

39

ACQUISITION AND RECONSTRUCTION OF BRAIN TISSUE USING KNIFE-EDGE SCANNING MICROSCOPY  

E-Print Network [OSTI]

ACQUISITION AND RECONSTRUCTION OF BRAIN TISSUE USING KNIFE- EDGE SCANNING MICROSCOPY A Thesis Science #12;ACQUISITION AND RECONSTRUCTION OF BRAIN TISSUE USING KNIFE- EDGE SCANNING MICROSCOPY A Thesis) ______________________________ ______________________________ Ergun Akleman Valerie Taylor (Member) (Head of Department) December 2003 Major Subject: Computer Science

Keyser, John

40

Scanning probe microscopy with inherent disturbance suppression using micromechanical systems  

E-Print Network [OSTI]

All scanning probe microscopes (SPMs) are affected by disturbances, or mechanical noise, in their environments which can limit their imaging resolution. This thesis introduces a general approach for suppressing out-of-plane ...

Sparks, Andrew William, 1977-

2005-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Instrument Series: Microscopy Aberration-Corrected Scanning/Transmission  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Aberration-Corrected Aberration-Corrected Scanning/Transmission Electron Microscope EMSL's aberration-corrected Titan 80-300(tm) scanning/transmission electron microscope (S/TEM) provides high-resolution imaging with sub-angstrom resolution and spectroscopic capabilities. This state-of-the-art instrument is equipped with a Schottky field-emission electron source, an electron gun monochromator, CEOS hexapole spherical aberration corrector for the probe-forming lens, high-angle annular dark field (HAADF) detector, an X-ray spectrometer (EDS), and a high-resolution Gatan Imaging Filter (GIF). The selection of electron energy between 80 kV and 300 kV enables optimized imaging for a variety of samples, including electron beam sensitive materials. Research Applications

42

Instrument Series: Microscopy Ultra-High Vacuum, Low- Temperature Scanning  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Low- Low- Temperature Scanning Probe Microscope EMSL's ultra-high vacuum, low-temperature scanning probe microscope instrument, or UHV LT SPM, is the preeminent system dedicated to surface chemistry and physics at low temperatures down to 5 K. Operating at low temperatures provides high mechanical stability, superior vacuum conditions, and negligible drift for long-term experiments. With thermal diffusion being entirely suppressed, stable imaging becomes possible even for weakly bound species. The system is primarily used for probing single-site chemical reactivity, while the combination with a hyperthermal molecular beam allows the study of important chemical processes at energies corresponding to the operational temperatures well beyond typical UHV studies. The LT SPM provides

43

Scanning photo-induced impedance microscopy*/an impedance based imaging technique  

E-Print Network [OSTI]

Scanning photo-induced impedance microscopy*/an impedance based imaging technique Steffi Krause a technique, scanning photo-induced impedance micro- scopy (SPIM), suitable for the imaging of the complex Photoelectrochemistry has been used widely to study photo-thermally induced current changes at metal surfaces

Moritz, Werner

44

Video-Rate Scanning Two-Photon Excitation Fluorescence Microscopy and Ratio Imaging with Cameleons  

E-Print Network [OSTI]

Video-Rate Scanning Two-Photon Excitation Fluorescence Microscopy and Ratio Imaging with Cameleons ABSTRACT A video-rate (30 frames/s) scanning two-photon excitation microscope has been successfully tested 690 to 1050 nm, prechirper optics for laser pulse-width compression, resonant galvanometer for video

Tsien, Roger Y.

45

Oxygen driven reconstruction dynamics of Ni,,977... measured by time-lapse scanning tunneling microscopy  

E-Print Network [OSTI]

Oxygen driven reconstruction dynamics of Ni,,977... measured by time-lapse scanning tunneling-lapse scanning tunneling microscopy STM has been used to observe the oxygen induced reconstruction behavior of Ni for the merging of steps in the presence of small amounts of adsorbed oxygen, less than 2% of a monolayer. Point

Sibener, Steven

46

Observation of diamond turned OFHC copper using Scanning Tunneling Microscopy  

SciTech Connect (OSTI)

Diamond turned OFHC copper samples have been observed within the past few months using the Scanning Tunneling Microscope. Initial results have shown evidence of artifacts which may be used to better understand the diamond turning process. The STM`s high resolution capability and three dimensional data representation allows observation and study of surface features unobtainable with conventional profilometry systems. Also, the STM offers a better quantitative means by which to analyze surface structures than the SEM. This paper discusses findings on several diamond turned OFHC copper samples having different cutting conditions. Each sample has been cross referenced using STM and SEM.

Grigg, D.A.; Russell, P.E.; Dow, T.A.

1988-12-01T23:59:59.000Z

47

Scanning Hall probe microscopy of a diluted magnetic semiconductor  

SciTech Connect (OSTI)

We have measured the micromagnetic properties of a diluted magnetic semiconductor as a function of temperature and applied field with a scanning Hall probe microscope built in our laboratory. The design philosophy for this microscope and some details are described. The samples analyzed in this work are Ga{sub 0.94}Mn{sub 0.06}As films grown by molecular beam epitaxy. We find that the magnetic domains are 2-4 mum wide and fairly stable with temperature. Magnetic clusters are observed above T{sub C}, which we ascribe to MnAs defects too small and sparse to be detected by a superconducting quantum interference device magnetometer.

Kweon, Seongsoo [Materials Science and Engineering, University of Texas at Austin, Austin, Texas 78712 (United States); Samarth, Nitin [Physics Department, Penn State University, University Park, Pennsylvania 16802 (United States); Lozanne, Alex de [Materials Science and Engineering, University of Texas at Austin, Austin, Texas 78712 (United States); Department of Physics, University of Texas at Austin, Austin, Texas 78712 (United States)

2009-05-01T23:59:59.000Z

48

Characterization of gold nanoparticle films: Rutherford backscattering spectroscopy, scanning electron microscopy with image analysis, and atomic force microscopy  

SciTech Connect (OSTI)

Gold nanoparticle films are of interest in several branches of science and technology, and accurate sample characterization is needed but technically demanding. We prepared such films by DC magnetron sputtering and recorded their mass thickness by Rutherford backscattering spectroscopy. The geometric thickness d{sub g}—from the substrate to the tops of the nanoparticles—was obtained by scanning electron microscopy (SEM) combined with image analysis as well as by atomic force microscopy (AFM). The various techniques yielded an internally consistent characterization of the films. In particular, very similar results for d{sub g} were obtained by SEM with image analysis and by AFM.

Lansåker, Pia C., E-mail: pia.lansaker@angstrom.uu.se; Niklasson, Gunnar A.; Granqvist, Claes G. [Department of Engineering Sciences, The Ångström Laboratory, Uppsala University, P. O. Box 534, SE-751 21 Uppsala (Sweden); Hallén, Anders [Royal Institute of Technology, KTH-ICT, Elektrum 229, Kista, SE-164 40 Stockholm (Sweden)

2014-10-15T23:59:59.000Z

49

Infrared near-field spectroscopy of trace explosives using an external cavity quantum cascade laser  

SciTech Connect (OSTI)

Utilizing a broadly-tunable external cavity quantum cascade laser for scattering-type scanning near-field optical microscopy (s-SNOM), we measure infrared spectra of explosives particles by probing characteristic nitro-group resonances in the 7.1-7.9 µm wavelength range. Measurements are presented with spectral resolution of 0.25 cm-1, spatial resolution of 25 nm, <100 attomolar sensitivity, and at a rapid acquisition time of 90 s per spectrum. We demonstrate high reproducibility of the acquired s-SNOM spectra with very high signal-to-noise ratios and relative noise of <0.02 in self-homodyne detection.

Craig, Ian M.; Taubman, Matthew S.; Lea, Alan S.; Phillips, Mark C.; Josberger, Erik E.; Raschke, Markus Bernd

2013-12-16T23:59:59.000Z

50

Coal Combustion Fly Ash Characterization: Electron Spectroscopy for Chemical Analysis, Energy Dispersive X-ray Analysis, and Scanning Electron Microscopy  

Science Journals Connector (OSTI)

The surface and bulk properties of five samples of fly ash have been examined by electron spectroscopy for chemical analysis (ESCA), scanning electron microscopy (SEM) and energy...

Rothenberg, S J; Denee, P; Holloway, P

1980-01-01T23:59:59.000Z

51

Predicted scanning tunneling microscopy images of carbon nanotubes with atomic vacancies  

E-Print Network [OSTI]

Predicted scanning tunneling microscopy images of carbon nanotubes with atomic vacancies Arkady V STM images of both metallic and semiconducting single-wall carbon nanotubes with atomic vacancies predict that vacancies should result in the formation of hillock-like features in STM images of metallic

Krasheninnikov, Arkady V.

52

X-ray optics for scanning fluorescence microscopy and other applications  

SciTech Connect (OSTI)

Scanning x-ray fluorescence microscopy is analogous to scanning electron microscopy. Maps of chemical element distribution are produced by scanning with a very small x-ray beam. Goal is to perform such scanning microscopy with resolution in the range of <1 to 10 {mu}m, using standard laboratory x-ray tubes. We are investigating mirror optics in the Kirkpatrick-Baez (K-B) configuration. K-B optics uses two curved mirrors mounted orthogonally along the optical axis. The first mirror provides vertical focus, the second mirror provides horizontal focus. We have used two types of mirrors: synthetic multilayers and crystals. Multilayer mirrors are used with lower energy radiation such as Cu K{alpha}. At higher energies such as Ag K{alpha}, silicon wafers are used in order to increase the incidence angles and thereby the photon collection efficiency. In order to increase the surface area of multilayers which reflects x-rays at the Bragg angle, we have designed mirrors with the spacing between layers graded along the optic axis in order to compensate for the changing angle of incidence. Likewise, to achieve a large reflecting surface with silicon, the wafers are placed on a specially designed lever arm which is bent into a log spiral by applying force at one end. In this way, the same diffracting angle is maintained over the entire surface of the wafer, providing a large solid angle for photon collection.

Ryon, R.W. [Lawrence Livermore National Lab., CA (United States); Warburton, W.K. [X-Ray Instrumentation Associates, Menlo Park, CA (United States)

1992-05-01T23:59:59.000Z

53

Versatile Silicon Photodiode Detector Technology for Scanning Electron Microscopy with High-Efficiency Sub-5 keV Electron Detection  

E-Print Network [OSTI]

Versatile Silicon Photodiode Detector Technology for Scanning Electron Microscopy with High for Scanning Electron Microscopy, based on ultrashallow p+ n boron-layer photodiodes, features nm-thin anodes, closely-packed photodiodes and through-wafer apertures allow flexible configurations for optimal material

Technische Universiteit Delft

54

Synthesis and structure of Al clusters supported on TiO2,,110...: A scanning tunneling microscopy study  

E-Print Network [OSTI]

Synthesis and structure of Al clusters supported on TiO2,,110...: A scanning tunneling microscopy, Texas 77843-3255 Received 14 October 1997; accepted 6 April 1998 Al clusters supported on TiO2(110) have been investigated using scanning tunneling microscopy. Al interacts strongly with the TiO2(110) surface

Goodman, Wayne

55

Visualizing Macromolecular Complexes with In Situ Liquid Scanning Transmission Electron Microscopy  

SciTech Connect (OSTI)

A central focus of biological research is understanding the structure/function relationship of macromolecular protein complexes. Yet conventional transmission electron microscopy techniques are limited to static observations. Here we present the first direct images of purified macromolecular protein complexes using in situ liquid scanning transmission electron microscopy. Our results establish the capability of this technique for visualizing the interface between biology and nanotechnology with high fidelity while also probing the interactions of biomolecules within solution. This method represents an important advancement towards allowing future high-resolution observations of biological processes and conformational dynamics in real-time.

Evans, James E.; Jungjohann, K. L.; Wong, Peony C. K.; Chiu, Po-Lin; Dutrow, Gavin H.; Arslan, Ilke; Browning, Nigel D.

2012-11-01T23:59:59.000Z

56

Study of Interactions Between Microbes and Minerals by Scanning Transmission X-Ray Microscopy (STXM)  

SciTech Connect (OSTI)

Scanning Transmission X-ray Microscopy (STXM) and Transmission Electron Microscopy (TEM) were combined to characterize various samples of geomicrobiological interest down to the nanometer scale. An approach based on energy-filtered imaging was used to examine microbe-mineral interactions and the resulting biominerals, as well as biosignatures in simplified laboratory samples. This approach was then applied to natural samples, including natural biofilms entombed in calcium carbonate precipitates and bioweathered silicates and facilitated location of bacterial cells and provided unique insights about their biogeochemical interactions with minerals at the 30-40 nm scale.

Benzerara, K.; /Paris U., VI-VII, LMCP; Tyliszczak, T.; /LBNL, ALS; Brown, G.E., Jr.; /Stanford U., Geo. Environ. Sci. /SLAC, SSRL

2007-01-03T23:59:59.000Z

57

Near-field radiative heat transfer for structured surfaces  

E-Print Network [OSTI]

We apply an analytical approach for determining the near-field radiative heat transfer between a metallic nanosphere and a planar semi-infinite medium with some given surface structure. This approach is based on a perturbative expansion, and evaluated to first order in the surface profile. With the help of numerical results obtained for some simple model geometries we discuss typical signatures that should be obtainable with a near-field scanning thermal microscope operated in either constant-height or constant-distance mode.

Svend-Age Biehs; Oliver Huth; Felix Rüting

2011-03-15T23:59:59.000Z

58

Electronic structure of wurtzite II-VI compound semiconductor cleavage surfaces studied by scanning tunneling microscopy  

Science Journals Connector (OSTI)

We report atomically resolved scanning tunneling microscopy (STM) images of cleavage surfaces of wurtzite II-VI compound semiconductors. CdSe(112¯0), CdSe(101¯0), and CdS(101¯0) were investigated. The STM images confirm a 1×1 reconstruction for all surfaces. At negative and positive sample voltages the occupied and empty dangling-bond states above anions and cations, respectively, dominate the contrast of the STM images. No states in the band gap were found. The electronic structure of the surface permits the observation of dopant atoms in subsurface layers and thus also cross-sectional scanning tunneling microscopy studies of point defects and heterostructures.

B. Siemens, C. Domke, Ph. Ebert, and K. Urban

1997-11-15T23:59:59.000Z

59

Examination of the cu/si(111) 5×5 structure by scanning tunneling microscopy  

Science Journals Connector (OSTI)

The incommensurate 5×5 Cu/Si(111) structure has been examined by scanning tunneling microscopy. Images show that the surface structure is not well described as a hexagonal copper layer modulated at the Si(111) periodicity. Rather, the surface breaks up into 5×5 subunits which pack at spacings varying from 5 to 7 lattice constants, implying that substrate-adsorbate interactions dominate lateral interactions within the Cu adlayer.

R. J. Wilson; S. Chiang; F. Salvan

1988-12-15T23:59:59.000Z

60

UNDERSTANDING THE EFFECTS OF SURFACTANT ADDITION ON RHEOLOGY USING LASER SCANNING CONFOCAL MICROSCOPY  

SciTech Connect (OSTI)

The effectiveness of three dispersants to modify rheology was examined using rheology measurements and laser scanning confocal microscopy (LSCM) in simulated waste solutions. All of the dispersants lowered the yield stress of the slurries below the baseline samples. The rheology curves were fitted reasonably to a Bingham Plastic model. The three-dimensional LSCM images of simulants showed distinct aggregates were greatly reduced after the addition of dispersants leading to a lowering of the yield stress of the simulated waste slurry solutions.

White, T

2007-05-08T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

Development of a Versatile in Vitro Platform for Studying Biological Systems Using Micro-3D Printing and Scanning Electrochemical Microscopy  

Science Journals Connector (OSTI)

We report a novel strategy for studying a broad range of cellular behaviors in real time by combining two powerful analytical techniques, micro-3D printing and scanning electrochemical microscopy (SECM). This allows one, in microbiological studies, to ...

Jiyeon Kim; Jodi L. Connell; Marvin Whiteley; Allen J. Bard

2014-11-17T23:59:59.000Z

62

Microstructure development in particulate coatings examined with high-resolution cryogenic scanning electron microscopy  

SciTech Connect (OSTI)

The authors used cryogenic scanning electron microscopy to examine the early stages of latex film formation. They visualized the influence of ionic strength and extent of carboxylation in latex-calcium carbonate formulations and in latex-only formulations. Results demonstrated that latex particles deposited on calcium carbonate surfaces creating a suspension of carboxylic acid-stabilized calcium carbonate particles. Images of consolidation fronts showed that variation of ionic strength and extent of carboxylation dramatically changes the way latex particles consolidate and form films.

Sheehan, J.G.; Davis, H.T.; Scriven, L.E. [Univ. of Minnesota, Minneapolis, MN (United States); Takamura, Koichi [BASF Corp., Charlotte, NC (United States)

1993-12-01T23:59:59.000Z

63

Imaging and quantitative data acquisition of biological cell walls with Atomic Force Microscopy and Scanning Acoustic Microscopy  

SciTech Connect (OSTI)

This chapter demonstrates the feasibility of Atomic Force Microscopy (AFM) and High Frequency Scanning Acoustic Microscopy (HF-SAM) as tools to characterize biological tissues. Both the AFM and the SAM have shown to provide imaging (with different resolution) and quantitative elasticity measuring abilities. Plant cell walls with minimal disturbance and under conditions of their native state have been examined with these two kinds of microscopy. After descriptions of both the SAM and AFM, their special features and the typical sample preparation is discussed. The sample preparation is focused here on epidermal peels of onion scales and celery epidermis cells which were sectioned for the AFM to visualize the inner surface (closest to the plasma membrane) of the outer epidermal wall. The nm-wide cellulose microfibrils orientation and multilayer structure were clearly observed. The microfibril orientation and alignment tend to be more organized in older scales compared with younger scales. The onion epidermis cell wall was also used as a test analog to study cell wall elasticity by the AFM nanoindentation and the SAM V(z) feature. The novelty in this work was to demonstrate the capability of these two techniques to analyze isolated, single layered plant cell walls in their natural state. AFM nanoindentation was also used to probe the effects of Ethylenediaminetetraacetic acid (EDTA), and calcium ion treatment to modify pectin networks in cell walls. The results suggest a significant modulus increase in the calcium ion treatment and a slight decrease in EDTA treatment. To complement the AFM measurements, the HF-SAM was used to obtain the V(z) signatures of the onion epidermis. These measurements were focused on documenting the effect of pectinase enzyme treatment. The results indicate a significant change in the V(z) signature curves with time into the enzyme treatment. Thus AFM and HF-SAM open the door to a systematic nondestructive structure and mechanical property study of complex biological cell walls. A unique feature of this approach is that both microscopes allow the biological samples to be examined in their natural fluid (water) environment.

Tittmann, B. R. [Penn State; Xi, X. [Penn State

2014-09-01T23:59:59.000Z

64

Imaging and microanalysis of thin ionomer layers by scanning transmission electron microscopy  

SciTech Connect (OSTI)

Improved conditions for imaging and spectroscopic mapping of thin perfluorosulfonic acid (PFSA) ionomer layers in fuel cell electrodes by scanning transmission electron microscopy (STEM) have been investigated. These conditions are first identified on model systems of Nafion ionomer-coated nanostructured thin films and nanoporous Si. The optimized conditions are then applied in a quantitative study of the ionomer through-layer loading for two typical electrode catalyst coatings using electron energy loss and energy dispersive X-ray spectroscopy in the transmission electron microscope. The e-beam induced damage to the perfluorosulfonic acid (PFSA) ionomer is quantified by following the fluorine mass loss with electron exposure and is then mitigated by a few orders of magnitude using cryogenic specimen cooling and a higher incident electron voltage. Multivariate statistical analysis is also applied to the analysis of spectrum images for data denoising and unbiased separation of independent components related to the catalyst, ionomer, and support.

Cullen, David A [ORNL; Koestner, Roland [General Motors Corporation; Kukreja, Ratan [General Motors Corporation; Minko, Sergiy [Clarkson University, Potsdam, NY; Trotsenko, Oleksandr [Clarkson University, Potsdam, NY; Tokarev, Alexander V [ORNL; Guetaz, Laure [French Atomic Energy Commission (CEA), Grenoble; Meyer III, Harry M [ORNL; Parish, Chad M [ORNL; More, Karren Leslie [ORNL

2014-01-01T23:59:59.000Z

65

Difference of operation mechanisms in SWNTs network FETs studied via scanning gate microscopy  

SciTech Connect (OSTI)

Field effect transistors (FETs) whose channel is composed of a network of single wall carbon nanotubes (SWNTs) have been studied to investigate the mechanism of the device operation via scanning gate microscopy (SGM) at room temperature. We observed different SGM response in networks of SWNTs either synthesized by CoMoCAT process or semiconducting enriched by density gradient ultracentrifuge process. In the former case, SGM response was observed at specific inter-tube junctions suggesting a Schottky junction formed with semiconducting and metallic SWNTs in the network. In contrast, multiple concentric rings in the SGM response are observed within the tubes in a network of the latter SWNTs suggesting a possibility of quantum mechanical transport at room-temperature. Different type of SGM responses are confirmed in the two kinds of SWNTs networks, nevertheless such active positions would likely have an important role in the FET operation mechanism in each network.

Wei, Xiaojun; Matsunaga, Masahiro; Yahagi, Tatsurou; Maeda, Kenji; Ochiai, Yuichi; Aoki, Nobuyuki [Graduate School of Advanced Integration Science, Chiba University, Chiba 263-8522 (Japan); Bird, Jonathan P. [Department of Electrical Engineering, University at Buffalo, the State University of New York, Buffalo, NY 14260-1920 (United States); Ishibashi, Koji [Advanced Device Laboratory, RIKEN, Wako, Saitama 351-0198 (Japan)

2013-12-04T23:59:59.000Z

66

Quantitative determination of local potential values in inhomogeneously doped semiconductors by scanning tunneling microscopy  

Science Journals Connector (OSTI)

Local potential changes arising from nanoscale three-dimensional spatial fluctuations in the dopant distribution in Zn-doped GaAs were investigated quantitatively by scanning tunneling microscopy and spectroscopy at (110) cleavage surfaces. Tunneling spectra measured in areas with different local doping concentration show apparent shifts of the valence band edge and apparent changes of the band gap. A quantitative analysis, combined with band bending and tunnel current simulations, demonstrates that these effects arise from tip-induced band bending that modulates the real potential changes. It is illustrated how exact potential changes between locally high and low doped areas can be determined. It is found that the local potential fluctuations in three-dimensionally doped semiconductors are approximately one order of magnitude smaller that those observed in two-dimensionally doped semiconductors.

P. H. Weidlich, R. E. Dunin-Borkowski, and Ph. Ebert

2011-08-29T23:59:59.000Z

67

Nanoscale chemical imaging using synchrotron x-ray enhanced scanning tunneling microscopy  

SciTech Connect (OSTI)

The combination of synchrotron radiation with scanning tunneling microscopy provides a promising new concept for chemical imaging of nanoscale structures. It employs detection of local x-ray absorption, which directly yields chemical, electronic, and magnetic sensitivity. The study of the tip current in the far field (800 nm tip/sample separation) shows that insulator-coated tips have to be considered in order to reduce the background from stray photoelectron. A picture of the different channels contributing to the x-ray enhanced STM process is proposed. If during electron tunneling the sample is illuminated with monochromatic x-rays, characteristic absorption will arise, and core electrons are excited, which might modulate the conventional tunnel current and facilitate chemical imaging at the nanoscale.

Rose, Volker; Freeland, John W. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)

2010-06-23T23:59:59.000Z

68

Nanoindentation and near-field spectroscopy of single semiconductor quantum dots  

Science Journals Connector (OSTI)

Low-temperature near-field scanning optical microscopy was used to study the dependence of the emission spectra of single self-organized InAs on GaAs, InAs on AlAs and InP on GaInP quantum dots (QDs) on contact pressure exerted by a near-field optical fiber tip (nanoindentation). A large energy shift (up to 150 meV), broadening (up to 10 meV), and intensity increase (up to one order of magnitude) of single QD emission lines have been observed at tip compressions up to 70 nm. Ground state energy shift rates from 0.5 to 3.5 meV/nm have been measured for different aperture types (rounded and flat, metal coated and uncoated) and sizes (50–300 nm) in agreement with numerical calculations using Picus–Bir orbital-strain Hamiltonian. A reduction of the hydrostatic pressure coefficient due to a nonuniform In distribution in self-organized QDs has been observed. Anomalously strong lateral inhomogeneity of the local stress field has been observed.

A. M. Mintairov; K. Sun; J. L. Merz; C. Li; A. S. Vlasov; D. A. Vinokurov; O. V. Kovalenkov; V. Tokranov; S. Oktyabrsky

2004-04-05T23:59:59.000Z

69

Scanning Hall Probe Microscopy of Magnetic Vortices inVery Underdoped yttrium-barium-copper-oxide  

SciTech Connect (OSTI)

Since their discovery by Bednorz and Mueller (1986), high-temperature cuprate superconductors have been the subject of intense experimental research and theoretical work. Despite this large-scale effort, agreement on the mechanism of high-T{sub c} has not been reached. Many theories make their strongest predictions for underdoped superconductors with very low superfluid density n{sub s}/m*. For this dissertation I implemented a scanning Hall probe microscope and used it to study magnetic vortices in newly available single crystals of very underdoped YBa{sub 2}Cu{sub 3}O{sub 6+x} (Liang et al. 1998, 2002). These studies have disproved a promising theory of spin-charge separation, measured the apparent vortex size (an upper bound on the penetration depth {lambda}{sub ab}), and revealed an intriguing phenomenon of ''split'' vortices. Scanning Hall probe microscopy is a non-invasive and direct method for magnetic field imaging. It is one of the few techniques capable of submicron spatial resolution coupled with sub-{Phi}{sub 0} (flux quantum) sensitivity, and it operates over a wide temperature range. Chapter 2 introduces the variable temperature scanning microscope and discusses the scanning Hall probe set-up and scanner characterizations. Chapter 3 details my fabrication of submicron GaAs/AlGaAs Hall probes and discusses noise studies for a range of probe sizes, which suggest that sub-100 nm probes could be made without compromising flux sensitivity. The subsequent chapters detail scanning Hall probe (and SQUID) microscopy studies of very underdoped YBa{sub 2}Cu{sub 3}O{sub 6+x} crystals with T{sub c} {le} 15 K. Chapter 4 describes two experimental tests for visons, essential excitations of a spin-charge separation theory proposed by Senthil and Fisher (2000, 2001b). We searched for predicted hc/e vortices (Wynn et al. 2001) and a vortex memory effect (Bonn et al. 2001) with null results, placing upper bounds on the vison energy inconsistent with the theory. Chapter 5 discusses imaging of isolated vortices as a function of T{sub c}. Vortex images were fit with theoretical magnetic field profiles in order to extract the apparent vortex size. The data for the lowest T{sub c}'s (5 and 6.5 K) show some inhomogeneity and suggest that {lambda}{sub ab} might be larger than predicted by the T{sub c} {proportional_to} n{sub s}(0)/m* relation first suggested by results of Uemura et al. (1989) for underdoped cuprates. Finally, Chapter 6 examines observations of apparent ''partial vortices'' in the crystals. My studies of these features indicate that they are likely split pancake vortex stacks. Qualitatively, these split stacks reveal information about pinning and anisotropy in the samples. Collectively these magnetic imaging studies deepen our knowledge of cuprate superconductivity, especially in the important regime of low superfluid density.

Guikema, Janice Wynn; /SLAC, SSRL

2005-12-02T23:59:59.000Z

70

Near-field microscopy: throwing light on the nanoworld  

Science Journals Connector (OSTI)

...instrumentation methods Nanotechnology instrumentation methods...tial for drug discovery, medicine and nanotechnology, while the development...in the life sciences and nanotechnology, and I believe we are now...

2003-01-01T23:59:59.000Z

71

Near-field diffractive elements Daniel Marks  

E-Print Network [OSTI]

by a near-field diffractive element (NDE) that scatters the high-spatial-frequency components of the field susceptibility r , and the NDE is described by the susceptibilty r . The field obeys the equation 2 U r +k0 2 U r to first order in both the NDE and the sample susceptibilities. It is assumed that the background terms

Bhargava, Rohit

72

Magnetic domain structures of focused ion beam-patterned cobalt films using scanning ion microscopy with polarization analysis  

E-Print Network [OSTI]

Magnetic domain structures of focused ion beam-patterned cobalt films using scanning ion microscopy Studies of magnetic domain distributions in patterned magnetic materials are of pivotal importance in the areas of ultrahigh density magnetic recording, MRAM design, and miniaturized magnetic sensor arrays

Rau, Carl

73

Graphene on Ru(0001) Moire Corrugation Studied by Scanning Tunneling Microscopy on Au/Graphene/Ru(0001) Heterostructures  

E-Print Network [OSTI]

Graphene on Ru(0001) Moire Corrugation Studied by Scanning Tunneling Microscopy on Au/Graphene on graphene/Ru(0001) were used to study the corrugation of the moire structure of graphene/Ru(0001 for the graphene/Ru(0001) moire is of structural nature rather than electronic. STM showed a large value

Ciobanu, Cristian

74

Atomic-Scale Imaging and Spectroscopy for In Situ Liquid Scanning Transmission Electron Microscopy  

SciTech Connect (OSTI)

Observation of growth, synthesis, dynamics and electrochemical reactions in the liquid state is an important yet largely unstudied aspect of nanotechnology. The only techniques that can potentially provide the insights necessary to advance our understanding of these mechanisms is simultaneous atomic-scale imaging and quantitative chemical analysis (through spectroscopy) under environmental conditions in the transmission electron microscope (TEM). In this study we describe the experimental and technical conditions necessary to obtain electron energy loss (EEL) spectra from a nanoparticle in colloidal suspension using aberration corrected scanning transmission electron microscopy (STEM) combined with the environmental liquid stage. At a fluid path length below 400 nm, atomic resolution images can be obtained and simultaneous compositional analysis can be achieved. We show that EEL spectroscopy can be used to quantify the total fluid path length around the nanoparticle, and demonstrate characteristic core-loss signals from the suspended nanoparticles can be resolved and analyzed to provide information on the local interfacial chemistry with the surrounding environment. The combined approach using aberration corrected STEM and EEL spectra with the in situ fluid stage demonstrates a plenary platform for detailed investigations of solution based catalysis and biological research.

Jungjohann, K. L.; Evans, James E.; Aguiar, Jeff; Arslan, Ilke; Browning, Nigel D.

2012-06-04T23:59:59.000Z

75

Scanning tunneling microscopy study of nitrogen incorporated HfO{sub 2}  

SciTech Connect (OSTI)

The impact of nitrogen incorporation on the physical and electrical characteristics of the HfO{sub 2} is examined. X-ray photoelectron spectroscopy shows that nitrogen can be incorporated into the HfO{sub 2} via a two-step thermal anneal--first in ultrahigh vacuum (UHV) and subsequently in N{sub 2}. Following the N{sub 2} anneal, scanning tunneling microscopy in UHV reveals a marked reduction in the low-voltage leakage current under gate injection biasing. From band theory and existing first-principles simulation results, one may consistently attribute this improvement to the passivation of oxygen vacancies in the HfO{sub 2} by nitrogen. Improvement in the breakdown strength of the HfO{sub 2} subjected to ramp-voltage stress (substrate injection) is also observed after the N{sub 2} anneal. The local current-voltage curves acquired concurrently during the ramp-voltage stress exhibit 'space-charge limited conduction', which implies that the observed improvement in breakdown strength may be related to a limitation of the current flow through the gate stack in the high stress voltage regime.

Ong, Y. C.; Ang, D. S.; Pey, K. L.; Li, X. [Nanyang Technological University, School of Electrical and Electronic Engineering, Nanyang Avenue, Singapore 639798 (Singapore); O'Shea, S. J.; Wang, S. J. [Institute of Materials Research and Engineering, A-STAR - Agency for Science, Technology and Research, 3 Research Link, Singapore 11760 (Singapore); Tung, C. H. [Institute of Microelectronics, A-STAR - Agency for Science, Technology and Research, 11 Science Park Road, Singapore Science Park II, Singapore 117685 (Singapore)

2008-09-15T23:59:59.000Z

76

Geochemistry Atomic Force Microscopy | EMSL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

imaging modes: contact, intermittent contact, phase imaging, magnetic force microscopy, electric force microscopy, surface potential microscopy, scanning capacitance microscopy,...

77

SCANNING ELECTRON MICROSCOPY AND X-RAY DIFFRACTION ANALYSIS OF TANK 18 SAMPLES  

SciTech Connect (OSTI)

The F-Area Tank Farm (FTF) Performance Assessment (PA) utilizes waste speciation in the waste release model used in the FTF fate and transport modeling. The waste release modeling associated with the residual plutonium in Tank 18 has been identified as a primary contributor to the Tank 18 dose uncertainty. In order to reduce the uncertainty related to plutonium in Tank 18, a better understanding of the plutonium speciation in the Tank 18 waste (including the oxidation state and stoichiometry) is desired. Savannah River National Laboratory (SRNL) utilized Scanning Electron Microscopy (SEM) and X-ray Diffraction (XRD) to analyze Tank 18 samples to provide information on the speciation of plutonium in the waste material. XRD analysis of the Tank 18 samples did not identify any plutonium mineral phases in the samples. These indicates the crystalline mineral phases of plutonium are below the detection limits of the XRD method or that the plutonium phase(s) lack long range order and are present as amorphous or microcrystalline solids. SEM analysis of the Tank 18 samples did locate particles containing plutonium. The plutonium was found as small particles, usually <1 {micro}m but ranging up to several micrometers in diameter, associated with particles of an iron matrix and at low concentration in other elemental matrices. This suggests the plutonium has an affinity for the iron matrix. Qualitatively, the particles of plutonium found in the SEM analysis do not appear to account for all of the plutonium in the sample based on concentrations determined from the chemical analysis of the Tank 18 samples. This suggests that plutonium is also distributed throughout the solids in low concentrations.

Hay, M.; O'Rourke, P.; Ajo, H.

2012-03-08T23:59:59.000Z

78

Infrared near-field imaging and spectroscopy based on thermal or synchrotron radiation  

SciTech Connect (OSTI)

We demonstrate the coupling of a scattering near-field scanning optical microscope combined with a Fourier transform infrared spectrometer. The set-up operates using either the near-field thermal emission from the sample itself, which is proportional to the electromagnetic local density of states, or with an external infrared synchrotron source, which is broadband and highly brilliant. We perform imaging and spectroscopy measurements with sub-wavelength spatial resolution in the mid-infrared range on surfaces made of silicon carbide and gold and demonstrate the capabilities of the two configurations for super-resolved near-field mid-infrared hyperspectral imaging and that the simple use of a properly chosen bandpass filter on the detector allows one to image the spatial distribution of materials with sub-wavelength resolution by studying the contrast in the near-field images.

Peragut, Florian; De Wilde, Yannick, E-mail: yannick.dewilde@espci.fr [ESPCI ParisTech, PSL Research University, CNRS, Institut Langevin, 1 rue Jussieu, F-75005, Paris (France); Brubach, Jean-Blaise; Roy, Pascale [Société Civile Synchrotron SOLEIL, L'Orme des Merisiers, St-Aubin BP48, 91192 Gif-sur-Yvette Cedex (France)

2014-06-23T23:59:59.000Z

79

Low-temperature scanning tunneling microscopy and transport measurements on adsorbate-induced two-dimensional electron systems  

SciTech Connect (OSTI)

We have performed not only magnetotransport measurements on two-dimensional electron systems (2DESs) formed at the cleaved surfaces of p-InAs but also observations of the surface morphology of the adsorbate atoms, which induced the 2DES at the surfaces of narrow band-gap semiconductors, with use of a scanning tunneling microscopy. The electron density of the 2DESs is compared to the atomic density of the isolated Ag adatoms on InAs surfaces.

Masutomi, Ryuichi; Triyama, Naotaka; Okamoto, Tohru [Department of Physics, University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo 113-0033 (Japan)

2013-12-04T23:59:59.000Z

80

Electronic properties of the Ga vacancy in GaP(110) surfaces determined by scanning tunneling microscopy  

Science Journals Connector (OSTI)

The electronic properties of uncharged Ga monovacancies in GaP(110) surfaces are determined from voltage-dependent scanning tunneling microscopy images. The signatures of localized defect states in the band gap are analyzed and their spatial location is determined. Empty and occupied defect states exist. Depressed dangling bonds in the occupied-state images indicate an inward relaxation of the neighboring P atoms. The results agree with recent theoretical work.

Ph. Ebert and K. Urban

1998-07-15T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


81

Recent advances in electron imaging, image interpretation and applications: environmental scanning electron microscopy  

Science Journals Connector (OSTI)

...A treatment of the physics governing this phenomenon...electron microscopy, the physics of which provides much...Varaprasad, L. H. 1991 Handbook of optical constants...ed.) 1991 CRC handbook of chemistry and physics. Boca Raton, FL...

2003-01-01T23:59:59.000Z

82

Scanning transmission X-ray microscopy probe for in situ mechanism study of graphene-oxide-based resistive random access memory  

Science Journals Connector (OSTI)

An in situ probe for scanning transmission X-ray microscopy has been developed and applied to the study of the bipolar resistive switching mechanism in an Al/graphene oxide/Al resistive random access memory device.

Nho, H.W.

2013-11-28T23:59:59.000Z

83

Scanning-tunneling-microscopy studies of disilane adsorption and pyrolytic growth on Si(100)-(2x1)  

SciTech Connect (OSTI)

Scanning tunneling microscopy has been employed to study the adsorption of disilane (Si{sub 2}H{sub 6}) and pyrolytic growth on Si(100)-(2{times}1) at various temperatures. Room-temperature exposures result in a random distribution of dissociation fragments on the surface. Formation of anisotropic monohydride islands and denuded zones as well as island coarsening is observed at higher temperatures. The results are strikingly similar to those reported for growth by molecular-beam epitaxy using pure Si, even though different surface reactions are involved in these two growth processes.

Lin, D.; Hirschorn, E.S.; Chiang, T. (Department of Physics and Materials Research Laboratory, University of Illinois at Urbana-Champaign, Urbana, Illinois 61801 (United States)); Tsu, R.; Lubben, D.; Greene, J.E. (Department of Materials Science, Coordinated Science Laboratory, University of Illinois at Urbana-Champaign, Urbana, Illinois 61801 (United States) Materials Research Laboratory, University of Illinois at Urbana-Champaign, Urbana, Illinois 61801 (United States))

1992-02-15T23:59:59.000Z

84

Surface [4 + 2] Cycloaddition Reaction of Thymine on Si(111)7×7 Observed by Scanning Tunneling Microscopy  

Science Journals Connector (OSTI)

WATLab and Department of Chemistry, University of Waterloo, Waterloo, Ontario N2L 3G1, Canada ... Simple hydrocarbons(1) with aliphatic chain backbones, alkenes, alkynes, and aromatic molecules without and with heteroatoms(3) have been investigated by a number of experimental methods, including X-ray photoelectron spectroscopy (XPS), low-energy electron diffraction (LEED), high-resolution electron energy loss spectroscopy (HREELS), and scanning tunneling microscopy (STM) as well as computational methods based on density functional theory (DFT), Moller–Plesset perturbation theory (MP2), and semiempirical techniques. ...

A. Chatterjee; L. Zhang; K. T. Leung

2013-06-21T23:59:59.000Z

85

Probing the electronic structure of graphene sheets with various thicknesses by scanning transmission X-ray microscopy  

SciTech Connect (OSTI)

The electronic structure of an aggregation of graphene sheets with various thicknesses was probed by scanning transmission X-ray microscopy. A uniform oxidation of the graphene sheets in the flat area was observed regardless of the thickness, while in the folded area the result could be strongly affected by the geometry. Moreover, thick parts of the aggregation showed strong angle-dependence to the incident X-ray, while thin parts showed less angle-dependence, which might be related to the surface wrinkles and ripples. The electronic structure differences due to the geometry and thickness suggest a complicated situation in the aggregation of graphene sheets.

Bai, Lili; Liu, Jinyin; Zhao, Guanqi; Gao, Jing; Sun, Xuhui, E-mail: xhsun@suda.edu.cn, E-mail: jzhong@suda.edu.cn; Zhong, Jun, E-mail: xhsun@suda.edu.cn, E-mail: jzhong@suda.edu.cn [Soochow University-Western University Centre for Synchrotron Radiation Research, Institute of Functional Nano and Soft Materials Laboratory (FUNSOM) and Collaborative Innovation Center of Suzhou Nano Science and Technology, Soochow University, Suzhou 215123 (China)] [Soochow University-Western University Centre for Synchrotron Radiation Research, Institute of Functional Nano and Soft Materials Laboratory (FUNSOM) and Collaborative Innovation Center of Suzhou Nano Science and Technology, Soochow University, Suzhou 215123 (China)

2013-12-16T23:59:59.000Z

86

Investigating the Optical Properties of Dislocations by Scanning Transmission Electron Microscopy  

E-Print Network [OSTI]

investigation for solid-state lighting and display applications, and dislocations are known to be nonradiative the radiative pathway and contribute to the enormous savings in energy use and greenhouse gas emissions expected with efficient solid-state lighting. CL Studies of Dislocations One of the key advantages of a scanning micro

Pennycook, Steve

87

Method for imaging liquid and dielectric materials with scanning polarization force microscopy  

SciTech Connect (OSTI)

The invention images dielectric polarization forces on surfaces induced by a charged scanning force microscope (SFM) probe tip. On insulators, the major contribution to the surface polarizability at low frequencies is from surface ions. The mobility of these ions depends strongly on the humidity. Using the inventive SFM, liquid films, droplets, and other weakly adsorbed materials have been imaged. 9 figs.

Hu, J.; Ogletree, D.F.; Salmeron, M.; Xiao, X.

1999-03-09T23:59:59.000Z

88

Direct determination of exact charge states of surface point defects using scanning tunneling microscopy: As vacancies on GaAs ,,110...  

E-Print Network [OSTI]

microscopy: As vacancies on GaAs ,,110... Kuo-Jen Chao, Arthur R. Smith, and Chih-Kang Shih* Department of the charge state of surface As vacancies on p-type GaAs 110 using scanning tunneling microscopy. This method utilizes the compensation between the local band bending result- ing from the As vacancy and the p

89

Deformation induced changes in surface properties of polymers investigated by scanning force microscopy  

E-Print Network [OSTI]

In this study the possibility of combining commercial Scanning Force Microscopes (SFM) with stretching devices for the investigation of microscopic surface changes during stepwise elongation is investigated. Different types of stretching devices have been developed either for Scanning Platform-SFM or for Stand Alone-SFM. Their suitability for the investigation of deformation induced surface changes is demonstrated. A uniaxially oriented polypropylene film is stretched vertically to its extrusion direction. The reorientation of its microfibrillar structure is investigated and correlated to macroscopic structural changes determined by taking a force-elongation curve. Microtome cuts of natural rubber filled with 15 PHR carbon black are stretched. Changes in topography, local stiffness and adhesive force are simultaneously reported by using a new imaging method called Pulsed Force Mode (PFM).

Sabine Hild; Armin Rosa; Othmar Marti

2013-12-10T23:59:59.000Z

90

Method and apparatus for differential spectroscopic atomic-imaging using scanning tunneling microscopy  

DOE Patents [OSTI]

A Method and apparatus for differential spectroscopic atomic-imaging is disclosed for spatial resolution and imaging for display not only individual atoms on a sample surface, but also bonding and the specific atomic species in such bond. The apparatus includes a scanning tunneling microscope (STM) that is modified to include photon biasing, preferably a tuneable laser, modulating electronic surface biasing for the sample, and temperature biasing, preferably a vibration-free refrigerated sample mounting stage. Computer control and data processing and visual display components are also included. The method includes modulating the electronic bias voltage with and without selected photon wavelengths and frequency biasing under a stabilizing (usually cold) bias temperature to detect bonding and specific atomic species in the bonds as the STM rasters the sample. This data is processed along with atomic spatial topography data obtained from the STM raster scan to create a real-time visual image of the atoms on the sample surface.

Kazmerski, Lawrence L. (Lakewood, CO)

1990-01-01T23:59:59.000Z

91

Near-field/altered-zone models report  

SciTech Connect (OSTI)

The U.S. Department of Energy is studying Yucca Mountain as the possible site for the first underground repository for permanent disposal of spent fuel from commercial nuclear reactors as well as for other types high-level nuclear waste. Emplacement of high-level radioactive waste, especially commercial spent nuclear fuel (CSNF), in Yucca Mountain will release a large amount of heat into the rock above and below the repository. The heating rate will decrease with time, creating a thermal pulse. Over a period of several thousand years, the rock temperature will rise initially, then drop when the production of decay heat falls below the rate at which heat escapes from the hot zone. Besides raising the rock temperature, much of this heat will vaporize water, which will then condense in cooler regions. The condensate is likely to form a gravity-driven heat pipe above the repository, creating the possibility that water may drain back onto the waste packages (WPs) or that it may ''shed'' through the pillars between emplacement drifts. The long-term importance of these effects has been investigated through the development, testing, and application of thermohydrologic (TH) models. Other effects, such coupled chemical and mechanical processes, may also influence the movement of water above, within, and below the emplacement drifts. A recent report on thermally driven coupled processes (Hardin and Chesnut, 1997) provides a qualitative assessment of the probable significance of these processes for the Yucca Mountain Site Characterization Project (YMSCP) and is the phenomenological framework for the present report. This report describes the conceptual and numerical models that have been developed to predict the thermal, mechanical, hydrologic, and chemical responses to the cumulative heat production of the potential host rock at Yucca Mountain. As proposed, the repository horizon will be situated within the Topopah Spring tuff, in the adjacent middle nonlithophysal and lower lithophysal units. These units are made up of moderately to densely welded, devitrified, fractured tuff. The rock's chemical composition is comparable to that of typical granite, but has textural features and mineralogical characteristics of large-scale, silicic volcanism. Because the repository horizon will be approximately 300 m below the ground surface and 200 m above the water table, the repository will be partially saturated. The welded tuff matrix in the host units is highly impermeable, but water and gas flow readily through fractures. The degree of fracturing in these units is highly variable, and the hydrologic significance of fracturing is an important aspect of site investigation. This report describes the characterization and modeling of a region around the potential repository--the altered zone--a region in which the temperature will be increased significantly by waste-generated heat. Numerical simulation has shown that, depending on the boundary conditions, rock properties, and repository design features incorporated in the models, the altered zone (AZ) may extend from the water table to the ground surface. This report also describes models of the near field, the region comprising the repository emplacement drifts and the surrounding rock, which are critical to the performance of engineered components. Investigations of near-field and altered-zone (NF/AZ) processes support the design of underground repository facilities and engineered barriers and also provide constraint data for probabilistic calculations of waste-isolation performance (i.e., performance assessment). The approach to investigation, which is an iterative process involving hypothesis testing and experimentation, has relied on conceptualizing engineered barriers and on performance analysis. This report is a collection, emphasizing conceptual and numerical models, of the recent results contributed from studies of NF/AZ processes and of quantitative measures of NF/AZ performance. The selection and presentation of contributions are intended to show the iterative development of understand

Hardin, E. L., LLNL

1998-03-01T23:59:59.000Z

92

Spatially resolved quantitative mapping of thermomechanical properties and phase transition temperatures using scanning probe microscopy  

DOE Patents [OSTI]

An approach for the thermomechanical characterization of phase transitions in polymeric materials (polyethyleneterephthalate) by band excitation acoustic force microscopy is developed. This methodology allows the independent measurement of resonance frequency, Q factor, and oscillation amplitude of a tip-surface contact area as a function of tip temperature, from which the thermal evolution of tip-surface spring constant and mechanical dissipation can be extracted. A heating protocol maintained a constant tip-surface contact area and constant contact force, thereby allowing for reproducible measurements and quantitative extraction of material properties including temperature dependence of indentation-based elastic and loss moduli.

Jesse, Stephen; Kalinin, Sergei V; Nikiforov, Maxim P

2013-07-09T23:59:59.000Z

93

Acquisition and reconstruction of brain tissue using knife-edge scanning microscopy  

E-Print Network [OSTI]

. As the sample passes under an individual photon receptor, the light intensity value is summed and passed to the next register. The final output pixel is the sum of the light intensity received by all TDI registers for a single sampled point... wide line is imaged along the leading edge of the knife. Our primary camera of choice is a DALSA CT-F3 High- Speed TDI Line Scan Camera. In order to get a high sensitivity at the speed at which we want to cut, the monochrome camera uses Time Delay...

Mayerich, David Matthew

2004-09-30T23:59:59.000Z

94

IR SNOM - Infrared Near-field Nanoimaging | EMSL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Infrared near-field spectroscopy of trace explosives using an external cavity quantum cascade laser. Utilizing a broadly-tunable external cavity quantum cascade laser for...

95

Infrared near-field spectroscopy of trace explosives using an...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

spectroscopy of trace explosives using an external cavity quantum cascade laser. Infrared near-field spectroscopy of trace explosives using an external cavity quantum...

96

Three-Dimensional Aberration-Corrected Scanning Transmission Electron Microscopy for Biology  

SciTech Connect (OSTI)

Recent instrumental developments have enabled greatly improved resolution of scanning transmission electron microscopes (STEM) through aberration correction. An additional and previously unanticipated advantage of aberration correction is the greatly improved depth sensitivity that has led to the reconstruction of a three-dimensional (3D) image from a focal series. In this chapter the potential of aberration-corrected 3D STEM to provide major improvements in the imaging capabilities for biological samples will be discussed. This chapter contains a brief overview ofthe various high-resolution 3D imaging techniques, a historical perspective of the development of STEM, first estimates of the dose-limited axial and lateral resolution on biological samples and initial experiments on stained thin sections.

De Jonge, Niels [ORNL; Sougrat, Rachid [ORNL; Pennycook, Stephen J [ORNL; Peckys, Diana B [ORNL; Lupini, Andrew R [ORNL

2007-01-01T23:59:59.000Z

97

An easy-to-implement filter for separating photo-excited signals from topography in scanning tunneling microscopy  

SciTech Connect (OSTI)

In order to achieve elemental and chemical sensitivity in scanning tunneling microscopy (STM), synchrotron x-rays have been applied to excite core-level electrons during tunneling. The x-ray photo-excitations result in tip currents that are superimposed onto conventional tunneling currents. While carrying important physical information, the varying x-ray induced currents can destabilize the feedback loop causing it to be unable to maintain a constant tunneling current, sometimes even causing the tip to retract fully or crash. In this paper, we report on an easy-to-implement filter circuit that can separate the x-ray induced currents from conventional tunneling currents, thereby allowing simultaneous measurements of topography and chemical contrasts. The filter and the schematic presented here can also be applied to other variants of light-assisted STM such as laser STM.

Wang Kangkang; Rosenmann, Daniel; Holt, Martin; Winarski, Robert; Hla, Saw-Wai [Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Rose, Volker [Center for Nanoscale Materials, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States); Advanced Photon Source, Argonne National Laboratory, 9700 South Cass Avenue, Argonne, Illinois 60439 (United States)

2013-06-15T23:59:59.000Z

98

Comparison of SOFC Cathode Microstructure Quantified using X-ray Nanotomography and Focused Ion Beam - Scanning Electron Microscopy  

SciTech Connect (OSTI)

X-ray nanotomography and focused ion beam scanning electron microscopy (FIB?SEM) have been applied to investigate the complex 3D microstructure of solid oxide fuel cell (SOFC) electrodes at spatial resolutions of 45 nm and below. The application of near edge differential absorption for x-ray nanotomography and energy selected backscatter detection for FIB–SEM enable elemental mapping within the microstructure. Using these methods, non?destructive 3D x-ray imaging and FIB–SEM serial sectioning have been applied to compare three?dimensional elemental mapping of the LSM, YSZ, and pore phases in the SOFC cathode microstructure. The microstructural characterization of an SOFC cathode is reported based on these measurements. The results presented demonstrate the viability of x-ray nanotomography as a quantitative characterization technique and provide key insights into the SOFC cathode microstructure.

Nelson, George J.; Harris, William H.; Lombardo, Jeffrey J.; Izzo, Jr., John R.; Chiu, W. K. S.; Tanasini, Pietro; cantoni, Marco; Van herle, Jan; Comninellis, Christos; Andrews, Joy C.; Liu, Yijin; Pianetta, Piero; Chu, Yong

2011-01-01T23:59:59.000Z

99

Scanning tunneling microscopy on unpinned GaN(11¯00) surfaces: Invisibility of valence-band states  

Science Journals Connector (OSTI)

We investigated the origins of the tunnel current in scanning tunneling microscopy (STM) and spectroscopy experiments on GaN(11¯00) surfaces. By calculating the tunnel currents in the presence of a tip-induced band bending for unpinned n-type GaN(11¯00) surfaces, we demonstrate that only conduction-band states are observed at positive and negative voltage polarities independent of the doping concentration. Valence-band states remain undetectable because tunneling out of the electron-accumulation zone in conduction-band states dominates by four orders of magnitude. As a result band-gap sizes cannot be determined by STM on unpinned GaN(11¯00) surfaces. Appropriate band-edge positions and gap sizes can be determined on pinned surfaces.

Ph. Ebert, L. Ivanova, and H. Eisele

2009-08-24T23:59:59.000Z

100

Josephson scanning tunneling microscopy -- a local and direct probe of the superconducting order parameter  

SciTech Connect (OSTI)

Direct measurements of the superconducting superfluid on the surface of vacuum-cleaved Bi2Sr2CaCu2O8+delta (BSCCO) samples are reported. These measurements are accomplished via Josephson tunneling into the sample using a novel scanning tunneling microscope (STM) equipped with a superconducting tip. The spatial resolution of the STM of lateral distances less than the superconducting coherence length allows it to reveal local inhomogeneities in the pair wavefunction of the BSCCO. Instrument performance is demonstrated first with Josephson measurements of Pb films followed by the layered superconductor NbSe2. The relevant measurement parameter, the Josephson ICRN product, is discussed within the context of both BCS superconductors and the high transition temperature superconductors. The local relationship between the ICRN product and the quasiparticle density of states (DOS) gap are presented within the context of phase diagrams for BSCCO. Excessive current densities can be produced with these measurements and have been found to alter the local DOS in the BSCCO. Systematic studies of this effect were performed to determine the practical measurement limits for these experiments. Alternative methods for preparation of the BSCCO surface are also discussed.

Kimura, Hikari; Dynes, Robert; Barber Jr., Richard. P.; Ono, S.; Ando, Y.

2009-09-01T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

Advances in experimental technique for quantitative two-dimensional dopant profiling by scanning capacitance microscopy  

Science Journals Connector (OSTI)

Several advances have been made toward the achievement of quantitative two-dimensional dopant and carrier profiling. To improve the dielectric and charge properties of the oxide–silicon interface a method of low temperature heat treatment has been developed which produces an insulating layer with consistent quality and reproducibility. After a standard polishing procedure is applied to cross-sectional samples the samples are heated to 300?°C for 30 min under ultraviolet illumination. This additional surface treatment dramatically improves dielectric layer uniformity scanning capacitancemicroscopy (SCM) signal to noise ratio and C–V curve flat band offset. Examples of the improvement in the surface quality and comparisons of converted SCM data with secondary ion mass spectrometry(SIMS) data are shown. A SCM tip study has also been performed that indicates significant tip depletion problems can occur. It is shown that dopedsilicon tips are often depleted by the applied SCM bias voltage causing errors in the SCM measured profile. Worn metalcoated and silicided silicon tips also can cause similar problems. When these effects are tested for and eliminated excellent agreement can be achieved between quantitative SCM profiles and SIMS data over a five-decade range of dopant density using a proper physical model. The impact of the tip size and shape on SCM spatial accuracy is simulated. A flat tip model gives a good agreement with experimental data. It is found that the dc offset used to compensate the C–V curve flat band shift has a consistently opposite sign on p- and n-type substrates. This corresponds to a positive surface on p-type silicon and to a negative surface on n-type silicon. Rectification of the large capacitance probing voltage is considered as a mechanism responsible for the apparent flat band shift of (0.4–1) V measured on the samples after heating under UV irradiation. To explain the larger flat band shift of (1–5) V tip induced charging of water-related traps is proposed and discussed.

V. V. Zavyalov; J. S. McMurray; C. C. Williams

1999-01-01T23:59:59.000Z

102

Coherent Time-Stretch Transform for Near-Field Spectroscopy  

E-Print Network [OSTI]

losses results in reduction in peak power and loss of sensitivity; a key innovation has been diffraction theoryVthe Fraunhofer limit. We may also consider the temporal near-field regime in analogy

Jalali. Bahram

103

Scanning electron microscopy and electron probe microanalyses of the crystalline components of human and animal dental calculi  

SciTech Connect (OSTI)

A review of the use of scanning electron microscopy (SEM) and electron probe microanalyses in the study of dental calculus showed that such studies provided confirmatory and supplementary data on the morphological features of human dental calculi but gave only limited information on the identity of the crystalline or inorganic components. This study aimed to explore the potential of combined SEM and microanalyses in the identification of the crystalline components of the human and animal dental calculi. Human and animal calculi were analyzed. Identification of the crystalline components were made based on the combined information of the morphology (SEM) and Ca/P molar ratios of the crystals with the morphology and Ca/P molar ratio of synthetic calcium phosphates (brushite or DCPD; octacalcium phosphate, OCP; Mg-substituted whitlockite, beta-TCMP; CO/sub 3/-substituted apatite, (CHA); and calcite. SEM showed similarities in morphological features of human and animal dental calculi but differences in the forms of crystals present. Microanalyses and crystal morphology data suggested the presence of CaCO/sub 3/ (calcite) and CHA in the animal (cat, dog, tiger) and of OCP, beta-TCMP and CHA in human dental calculi. X-ray diffraction and infrared (IR) absorption analyses confirmed these results. This exploratory study demonstrated that by taking into consideration what is known about the crystalline components of human and animal dental calculi, combined SEM and microanalyses can provide qualitative identification.

LeGeros, R.Z.; Orly, I.; LeGeros, J.P.; Gomez, C.; Kazimiroff, J.; Tarpley, T.; Kerebel, B.

1988-03-01T23:59:59.000Z

104

3D Imaging of Porous Media Using Laser Scanning Confocal Microscopy with Application to Microscale Transport Processes  

SciTech Connect (OSTI)

We present advances in the application of laser scanning confocal microscopy (LSCM) to image, reconstruct, and characterize statistically the microgeometry of porous geologic and engineering materials. We discuss technical and practical aspects of this imaging technique, including both its advantages and limitations. Confocal imaging can be used to optically section a material, with sub-micron resolution possible in the lateral and axial planes. The resultant volumetric image data, consisting of fluorescence intensities for typically {approximately}50 million voxels in XYZ space, can be used to reconstruct the three-dimensional structure of the two-phase medium. We present several examples of this application, including studying pore geometry in sandstone, characterizing brittle failure processes in low-porosity rock deformed under triaxial loading conditions in the laboratory, and analyzing the microstructure of porous ceramic insulations. We then describe approaches to extract statistical microgeometric descriptions from volumetric image data, and present results derived from confocal volumetric data sets. Finally, we develop the use of confocal image data to automatically generate a three-dimensional mesh for numerical pore-scale flow simulations.

Fredrich, J.T.

1999-02-10T23:59:59.000Z

105

Atomic-resolution study of polarity reversal in GaSb grown on Si by scanning transmission electron microscopy  

SciTech Connect (OSTI)

The atomic-resolved reversal of the polarity across an antiphase boundary (APB) was observed in GaSb films grown on Si by high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). The investigation of the interface structure at the origin of the APB reveals that coalescence of two domains with Ga-prelayer and Sb-prelayer causes the sublattice reversal. The local strain and lattice rotation distributions of the APB, attributed to the discordant bonding length at the APB with the surrounding GaSb lattice, were further studied using the geometric phase analysis technique. The crystallographic characteristics of the APBs and their interaction with other planar defects were observed with HAADF-STEM. The quantitative agreement between experimental and simulated images confirms the observed polarities in the acquired HAADF-STEM data. The self-annihilation mechanism of the APBs is addressed based on the rotation induced by anti-site bonds and APBs' faceting.

Hosseini Vajargah, S.; Woo, S. Y.; Botton, G. A. [Department of Materials Science and Engineering, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Brockhouse Institute for Material Research, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Canadian Centre for Electron Microscopy, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Ghanad-Tavakoli, S. [Centre for Emerging Device Technologies, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Kleiman, R. N.; Preston, J. S. [Brockhouse Institute for Material Research, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Centre for Emerging Device Technologies, McMaster University, Hamilton, Ontario L8S 4L7 (Canada); Department of Engineering Physics, McMaster University, Hamilton, Ontario L8S 4L7 (Canada)

2012-11-01T23:59:59.000Z

106

Scanning tunneling microscopy study of the Eu-induced Ge(111)-(3×2)?(3×4) reconstruction  

Science Journals Connector (OSTI)

Eu-induced (3×2) reconstruction of the Ge(111) surface has been investigated by scanning tunneling microscopy (STM). The empty-state STM images show the chainlike atomic structure that is similar to those of the metal-induced Si(111)-(3×2) surfaces with an adsorbate coverage of 1?6 monolayer (ML). The filled-state STM images combined with the empty-state images at the low bias voltage reveal that the Ge arrangement of Eu?Ge(111)-(3×2) can be well interpreted in terms of the honeycomb chain-channel (HCC) model with the characteristic Ge?Ge double bond and slightly modified Ge honeycomb chains which are similar to those of the 1?6-ML HCC structure of Si(111)-(3×2). In addition, the Eu?Ge(111)-(3×2) surface is found to have a local ×4 periodicity along Eu chains, which can be explained, based on the analysis of STM line profiles, with two nonequivalent adsorption sites occupied by the Eu atoms in the empty channels of the HCC structure. The structural modifications of the Ge honeycomb chains as well as the origin of the ×2 and ×4 chains of Eu atoms in the HCC structure on the Eu?Ge(111) surface are discussed.

M. Kuzmin; P. Laukkanen; R. E. Perälä; I. J. Väyrynen

2006-03-23T23:59:59.000Z

107

scanning tunneling microscopy | EMSL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

(3-dimercapto-1-propanol, BAL)significantly reduced extracellular polymeric substances (EPS) expression by Brevundimonas diminuta in suspended cultures at levels just below the...

108

Combining In-Situ Buffer-Layer-Assisted-Growth with Scanning Probe Microscopy for Formation and Study of Supported Model Catalysts  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

STM images showing the morphology of BaO film (7 ML-left and STM images showing the morphology of BaO film (7 ML-left and 80 ML-right) formed by the direct evaporation of the BaO. EMSL Research and Capability Development Proposals Combining In Situ Buffer-Layer-Assisted-Growth with Scanning Probe Microscopy for Formation and Study of Supported Model Catalysts Project start date: Spring 2008 EMSL Lead Investigator: Igor Lyubinetsky Microscopy Group, EMSL, PNNL Co-investigators: Yingge Du Spectroscopy and Diffraction Group, EMSL, PNNL Wayne Goodman Department of Chemistry, Texas A&M University, College Station, Texas The objective of the project is to implement in situ advanced buffer-layer-assisted growth (BLAG) technique by combining EMSL's ultra-high vacuum scanning probe microscopy (UHV SPM) and

109

Near-Field Imaging with Sound: An Acoustic STM Model  

Science Journals Connector (OSTI)

The invention of scanning tunneling microscopy(STM) 30 years ago opened up a visual window to the nano-world and sparked off a bunch of new methods for investigating and controlling matter and its transformations at the atomic and molecular level.1 However an adequate theoretical understanding of the method is demanding; STM images can be considered quantum theory condensed into a pictorial representation. A hands-on model is presented for demonstrating the imaging principles in introductory teaching. It uses sound waves and computer visualization to create mappings of acoustic resonators. The macroscopic simile is made possible by quantum-classical analogies between matter and sound waves. Grounding STM in acoustic experience may help to make the underlying quantum concepts such as tunneling less abstract to students.

Manfred Euler

2012-01-01T23:59:59.000Z

110

Direct Observation of Optically Forbidden Energy Transfer between CuCl Quantum Cubes via Near-Field Optical Spectroscopy  

Science Journals Connector (OSTI)

We report, for the first time, evidence of near-field energy transfer among CuCl quantum cubes using an ultrahigh-resolution near-field optical microscopy and spectroscopy in the near UV region at 15 K. The sample was high-density CuCl quantum cubes embedded in a NaCl matrix. Measured spatial distributions of the luminescence intensities from 4.6-nm and 6.3-nm quantum cubes clearly established anticorrelation features. This is thought to be a manifestation of the energy transfer from the lowest state of exciton in 4.6-nm quantum cubes to the first dipole-forbidden excited state of exciton in 6.3-nm quantum cubes, which is attributed to the resonant optical near-field interaction.

Tadashi Kawazoe; Kiyoshi Kobayashi; Jungshik Lim; Yoshihito Narita; Motoichi Ohtsu

2002-01-25T23:59:59.000Z

111

Thermal heat radiation, near-field energy density and near-field radiative heat transfer of coated materials  

E-Print Network [OSTI]

We investigate the thermal radiation and thermal near-field energy density of a metal-coated semi-infinite body for different substrates. We show that the surface polariton coupling within the metal coating leads to an enhancement of the TM-mode part of the thermal near-field energy density when a polar substrate is used. In this case the result obtained for a free standing metal film is retrieved. In contrast, in the case of a metal substrate there is no enhancement in the TM-mode part, as can also be explained within the framework of surface plasmon coupling within the coating. Finally, we discuss the influence of the enhanced thermal energy density on the near-field radiative heat transfer between a simple semi-infinite and a coated semi-infinite body for different material combinations.

Svend-Age Biehs

2011-03-15T23:59:59.000Z

112

Near-Field Analysis of Bright and Dark Modes on Plasmonic Metasurfaces Showing Extraordinary Suppressed Transmission  

E-Print Network [OSTI]

Plasmonic metasurfaces are investigated that consist of a sub wavelength line pattern in an ultrathin (~ 10 nm) silver film, designed for extraordinarily suppressed transmission (EOST) in the visible spectral range. Measurements with a near-field scanning optical microscope (NSOM) demonstrate that far field irradiation creates resonant excitations of antenna like (bright) modes that are localized on the metal ridges. In contrast, bound (dark) surface plasmon polaritons (SPPs) launched from an NSOM tip propagate well across the metasurface, preferentially perpendicular to the grating lines.

Dobmann, Sabine; Ploss, Daniel; Peschel, Ulf

2014-01-01T23:59:59.000Z

113

Real-time monitoring of quorum sensing in 3D-printed bacterial aggregates using scanning electrochemical microscopy  

Science Journals Connector (OSTI)

...manipulating small populations. Micro-3D printing is a lithographic technique capable...cells or small populations. This 3D-printing strategy can organize bacteria...behaviors. Here, we combined micro-3D printing and scanning electrochemical...

Jodi L. Connell; Jiyeon Kim; Jason B. Shear; Allen J. Bard; Marvin Whiteley

2014-01-01T23:59:59.000Z

114

Near-field heat transfer between gold nanoparticle arrays  

SciTech Connect (OSTI)

The radiative heat transfer between gold nanoparticle layers is presented using the coupled dipole method. Gold nanoparticles are modelled as effective electric and magnetic dipoles interacting via electromagnetic fluctuations. The effect of higher-order multipoles is implemented in the expression of electric polarizability to calculate the interactions at short distances. Our findings show that the near-field radiation reduces as the radius of the nanoparticles is increased. Also, the magnetic dipole contribution to the heat exchange becomes more important for larger particles. When one layer is displayed in parallel with respect to the other layer, the near-field heat transfer exhibits oscillatory-like features due to the influence of the individual nanostructures. Further details about the effect of the nanoparticles size are also discussed.

Phan, Anh D., E-mail: anhphan@mail.usf.edu [Department of Physics, University of South Florida, Tampa, Florida 33620 (United States); Institute of Physics, Vietnam Academy of Science and Technology, 10 Dao Tan, Ba Dinh, Hanoi 10000 (Viet Nam); Phan, The-Long, E-mail: ptlong2512@yahoo.com [Department of Physics, Chungbuk National University, Cheongju 361-763 (Korea, Republic of); Woods, Lilia M. [Department of Physics, University of South Florida, Tampa, Florida 33620 (United States)

2013-12-07T23:59:59.000Z

115

Near-field effects of asteroid impacts in deep water  

SciTech Connect (OSTI)

Our previous work has shown that ocean impacts of asteroids below 500 m in diameter do not produce devastating long-distance tsunamis. Nevertheless, a significant portion of the ocean lies close enough to land that near-field effects may prove to be the greatest danger from asteroid impacts in the ocean. Crown splashes and central jets that rise up many kilometres into the atmosphere can produce, upon their collapse, highly non-linear breaking waves that could devastate shorelines within a hundred kilometres of the impact site. We present illustrative calculations, in two and three dimensions, of such impacts for a range of asteroid sizes and impact angles. We find that, as for land impacts, the greatest dangers from oceanic impacts are the short-term near-field, and long-term atmospheric effects.

Gisler, Galen R [Los Alamos National Laboratory; Weaver, Robert P [Los Alamos National Laboratory; Gittings, Micheal L [Los Alamos National Laboratory

2009-01-01T23:59:59.000Z

116

Modulation of near-field heat transfer between two gratings  

E-Print Network [OSTI]

We present a theoretical study of near-field heat transfer between two uniaxial anisotropic planar structures. We investigate how the distance and relative orientation (with respect to their optical axes) between the objects affect the heat flux. In particular, we show that by changing the angle between the optical axes it is possible in certain cases to modulate the net heat flux up to 90% at room temperature, and discuss possible applications of such a strong effect.

Svend-Age Biehs; Felipe S. S. Rosa; Philippe Ben-Abdallah

2011-05-18T23:59:59.000Z

117

Two-dimensional Vortex Behavior in Highly Underdoped YBa2Cu3O6 x Observed by Scanning Hall Probe Microscopy  

SciTech Connect (OSTI)

We report scanning Hall probe microscopy of highly underdoped superconducting YBa{sub 2}Cu{sub 3}O{sub 6+x} with T{sub c} ranging from 5 to 15 K which showed distinct flux bundles with less than one superconducting flux quantum ({Iota}{sub 0}) through the sample surface. The sub-{Iota}{sub 0} features occurred more frequently for lower T{sub c}, were more mobile than conventional vortices, and occurred more readily when the sample was cooled with an in-plane field component. We show that these features are consistent with kinked stacks of pancake vortices.

Guikema, J.W.

2010-02-22T23:59:59.000Z

118

Two-dimensional Vortex Behavior in Highly Underdoped YBa_2Cu_3O_{6+x} Observed byScanning Hall Probe Microscopy  

SciTech Connect (OSTI)

We report scanning Hall probe microscopy of highly underdoped superconducting YBa{sub 2}Cu{sub 3}O{sub 6+z} with T{sub c} ranging from 5 to 15 K which showed distinct flux bundles with less than one superconducting flux quantum ({Phi}{sub 0}) through the sample surface. The sub-{Phi}{sub 0} features occurred more frequently for lower T{sub c}, were more mobile than conventional vortices, and occurred more readily when the sample was cooled with an in-plane field component. We show that these features are consistent with kinked stacks of pancake vortices.

Guikema, J.W.; Bluhm, Hendrik; /Stanford U., Appl. Phys. Dept.; Bonn, D.A.; Liang, Ruixing; Hardy, W.N.; /British Columbia U.; Moler, K.A.; /Stanford U., Appl. Phys. Dept.

2008-04-22T23:59:59.000Z

119

Frustration in the Si(111) ‘‘pseudo 5×5’’ Cu structure directly observed by scanning tunneling microscopy  

Science Journals Connector (OSTI)

Frustration in a surface structure has been observed in real space and time using the scanning tunneling microscope. The frustration is revealed as an instability of an inherent feature in the Si(111) ‘‘pseudo 5×5’’ Cu structure. A possible origin of the frustration is proposed.

K. Mortensen

1991-01-28T23:59:59.000Z

120

Formation of the 5×5 reconstruction on cleaved Si(111) surfaces studied by scanning tunneling microscopy  

Science Journals Connector (OSTI)

The transformation of cleaved Si(111)2×1 surfaces into apparent 1×1, 5×5, and 7×7 structures has been studied with the scanning tunneling microscope. Two reaction paths are identified, one proceeding through a disordered adatom arrangement into the 7×7 structure, and the other proceeding directly from 2×1 into the 5×5 structure. Near a nucleation site (step or domain boundary), the first path is favored due to the abundance of adatoms on the surface, and far from a nucleation site the second path dominates.

R. M. Feenstra and M. A. Lutz

1990-09-15T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
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We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


121

Near-field thermal radiation transfer controlled by plasmons in graphene  

E-Print Network [OSTI]

It is shown that thermally excited plasmon-polariton modes can strongly mediate, enhance, and tune the near-field radiation transfer between two closely separated graphene sheets. The dependence of near-field heat exchange ...

Ilic, Ognjen

122

Scanning tunneling microscopy studies of the surfaces of a-Si:H and a-SiGe:H films  

SciTech Connect (OSTI)

The report contains a detailed description of the experimental complexities encountered in developing scanning tunneling microscope (STM) probing of atomic structure on the surface of freshly-grown hydrogenated-amorphous semiconductors. It also contains a speculative microscopic film-growth model that explains differences between the disorder in CVD grown a-Ge:H versus a-Si:H films. This model is derived from prior results obtained in the chemical analysis of GeH{sub 4} plasmas, combined with surface reaction and thermodynamic considerations. The neutral radical fragments of silane, disilane and germane dissociation in discharges, which dominate the vapor and film-growth reactions, have been deduced from detailed analysis of prior data and are reported. 4 refs., 7 figs.

Gallagher, A.; Ostrom, R.; Tannenbaum, D. (National Inst. of Standards and Technology, Boulder, CO (USA))

1991-06-01T23:59:59.000Z

123

Cryogenic scanning force microscopy of quantum Hall samples: Adiabatic transport originating in anisotropic depletion at contact interfaces  

Science Journals Connector (OSTI)

Anisotropic magnetoresistances and intrinsic adiabatic transport features are generated on quantum Hall samples based on an (Al,Ga)As/GaAs heterostructure with alloyed Au/Ge/Ni contacts. We succeed to probe the microscopic origin of these transport features with a cryogenic scanning force microscope by measuring the local potential distribution within the two-dimensional electron system (2DES). These local measurements reveal the presence of an incompressible strip in front of contacts with insulating properties depending on the orientation of the contact/2DES interface line relatively to the crystal axes of the heterostructure. Such an observation gives another microscopic meaning to the term “nonideal contact” used in context with the Landauer-Büttiker formalism applied to the quantum Hall effect.

F. Dahlem; E. Ahlswede; J. Weis; K. v. Klitzing

2010-09-10T23:59:59.000Z

124

An Investigation of Polymer Diffusion in Hydrogel Laminates Using Near-Field FTIR Microscopy  

E-Print Network [OSTI]

of poly(ethylene glycol) (PEG) free chains across poly(acrylic acid) (PAA) gels was investigated the dispersive spectrometer at the desired frequency. An additive-free polymer sample was placed in the reference

Peppas, Nicholas A.

125

Surface species formed by the adsorption and dissociation of water molecules on Ru(0001) surface containing a small coverage of carbon atoms studied by scanning tunneling microscopy  

SciTech Connect (OSTI)

The adsorption and dissociation of water on a Ru(0001) surface containing a small amount ({le} 3 %) of carbon impurities was studied by scanning tunneling microscopy (STM). Various surface species are formed depending on the temperature. These include molecular H{sub 2}O, H{sub 2}O-C complexes, H, O, OH and CH. Clusters of either pure H{sub 2}O or mixed H{sub 2}O-OH species are also formed. Each of these species produces a characteristic contrast in the STM images and can be identified by experiment and by ab initio total energy calculations coupled with STM image simulations. Manipulation of individual species via excitation of vibrational modes with the tunneling electrons has been used as supporting evidence.

Dept of Materials Science and Engineering UCB; Dept of Applied Science and Technology, UCB; Institut de Ciencia de Materials de Barcelona, Barcelona, Spain; Instituto de Ciencia de Materiales de Madrid, Madrid, Spain; Department of Mechanical Engineering, Yale University; Salmeron, Miquel; Shimizu, Tomoko K.; Mugarza, Aitor; Cerda, Jorge I.; Heyde, Markus; Qi, Yabing; Schwarz, Udo D.; Ogletree, D. Frank; Salmeron, Miquel

2008-04-26T23:59:59.000Z

126

Electronic structures and bonding properties of chlorine-treated nitrogenated carbon nanotubes: X-ray absorption and scanning photoelectron microscopy studies  

SciTech Connect (OSTI)

The electronic and bonding properties of nitrogenated carbon nanotubes (N-CNTs) exposed to chlorine plasma were investigated using C and N K-edge x-ray absorption near-edge structure (XANES) and scanning photoelectron microscopy (SPEM). The C and N K-edge XANES spectra of chlorine-treated N-CNTs consistently reveal the formation of pyridinelike N-CNTs by the observation of 1s{yields}{pi}*(e{sub 2u}) antibonding and 1s{yields}{pi}*(b{sub 2g}) bonding states. The valence-band photoemission spectra obtained from SPEM images indicate that chlorination of the nanotubes enhances the C-N bonding. First-principles calculations of the partial densities of states in conjunction with C K-edge XANES data identify the presence of C-Cl bonding in chlorine treated N-CNTs.

Ray, S. C.; Pao, C. W.; Tsai, H. M.; Chiou, J. W.; Pong, W. F.; Chen, C. W.; Tsai, M.-H.; Papakonstantinou, P.; Chen, L. C.; Chen, K. H.; Graham, W. G. [Department of Physics, Tamkang University, Tamsui 251, Taiwan (China); Department of Materials Science and Engineering, National Taiwan University, Taipei 106, Taiwan (China); Department of Physics, National Sun Yat-Sen University, Kaohsiung 804, Taiwan (China); NRI, School of Electrical and Mechanical Engineering, University of Ulster at Jordanstown, Newtownabbey, County Antrim BT37OQB, Northern Ireland (United Kingdom); Center for Condensed Matter Sciences, National Taiwan University, Taipei 106, Taiwan (China); Institute of Atomic and Molecular Sciences, Academia Sinica, Taipei 106, Taiwan (China); Department of Physics and Astronomy, Queens University of Belfast, Belfast, Antrim BT71NN, Northern Ireland (United Kingdom)

2007-05-07T23:59:59.000Z

127

Contrast stability and "stripe" formation in Scanning Tunnelling Microscopy imaging of highly oriented pyrolytic graphite: The role of STM-tip orientations  

E-Print Network [OSTI]

Highly oriented pyrolytic graphite (HOPG) is an important substrate in many technological applications and is routinely used as a standard in Scanning Tunnelling Microscopy (STM) calibration, which makes the accurate interpretation of the HOPG STM contrast of great fundamental and applicative importance. We demonstrate by STM simulations based on electronic structure obtained from first principles that the relative local orientation of the STM-tip apex with respect to the HOPG substrate has a considerable effect on the HOPG STM contrast. Importantly for experimental STM analysis of HOPG, the simulations indicate that local tip-rotations maintaining a major contribution of the $d_{3z^2-r^2}$ tip-apex state to the STM current affect only the secondary features of the HOPG STM contrast resulting in "stripe" formation and leaving the primary contrast unaltered. Conversely, tip-rotations leading to enhanced contributions from $m\

Mándi, Gábor; Palotás, Krisztián

2014-01-01T23:59:59.000Z

128

A novel mathematical model for controllable near-field electrospinning  

SciTech Connect (OSTI)

Near-field electrospinning (NFES) had better controllability than conventional electrospinning. However, due to the lack of guidance of theoretical model, precise deposition of micro/nano fibers could only accomplished by experience. To analyze the behavior of charged jet in NFES using mathematical model, the momentum balance equation was simplified and a new expression between jet cross-sectional radius and axial position was derived. Using this new expression and mass conservation equation, expressions for jet cross-sectional radius and velocity were derived in terms of axial position and initial jet acceleration in the form of exponential functions. Based on Slender-body theory and Giesekus model, a quadratic equation for initial jet acceleration was acquired. With the proposed model, it was able to accurately predict the diameter and velocity of polymer fibers in NFES, and mathematical analysis rather than experimental methods could be applied to study the effects of the process parameters in NFES. Moreover, the movement velocity of the collector stage can be regulated by mathematical model rather than experience. Therefore, the model proposed in this paper had important guiding significance to precise deposition of polymer fibers.

Ru, Changhai, E-mail: rchhai@gmail.com, E-mail: luojun@shu.edu.cn [College of Automation, Harbin Engineering University, Harbin 150001 (China) [College of Automation, Harbin Engineering University, Harbin 150001 (China); Robotics and Microsystems Center, Soochow University, Suzhou 215021 (China); Chen, Jie; Shao, Zhushuai [Robotics and Microsystems Center, Soochow University, Suzhou 215021 (China)] [Robotics and Microsystems Center, Soochow University, Suzhou 215021 (China); Pang, Ming [College of Automation, Harbin Engineering University, Harbin 150001 (China)] [College of Automation, Harbin Engineering University, Harbin 150001 (China); Luo, Jun, E-mail: rchhai@gmail.com, E-mail: luojun@shu.edu.cn [School of Mechatronics Engineering and Automation, Shanghai University, Shanghai 200072 (China)] [School of Mechatronics Engineering and Automation, Shanghai University, Shanghai 200072 (China)

2014-01-15T23:59:59.000Z

129

Correlation between Charge State of Insulating NaCl Surfaces and Ionic Mobility Induced by Water Adsorption: A Combined Ambient Pressure X-ray Photoelectron Spectroscopy and Scanning Force Microscopy Study  

SciTech Connect (OSTI)

In situ ambient pressure X-ray photoelectron spectroscopy (APPES) and scanning force microscopy were used to characterize the surface discharge induced by water layers grown on (001) surfaces of sodium chloride single crystals. The APPES studies show that both kinetic energy (KE) and full width at half-maximum (FWHM) of the Na 2s and Cl 2p core level peaks, monitored as a function of relative humidity (RH), mimic surface conductivity curves measured using scanning force microscopy. The KE position and FWHM of the core level peaks therefore are directly related to the solvation and diffusion of ions at the NaCl(100) surface upon adsorption of water.

Verdaguer, Albert; Jose Segura, Juan; Fraxedas, Jordi; Bluhm, Hendrik; Salmeron, Miquel

2008-09-03T23:59:59.000Z

130

Near-field modeling in Frenchman Flat, Nevada Test Site  

SciTech Connect (OSTI)

The US Department of Energy (DOE) is investigating the effects of nuclear testing in underground test areas (the UGTA program) at the Nevada Test Site. The principal focus of the UGTA program is to better understand and define subsurface radionuclide migration. The study described in this report focuses on the development of tools for generating maps of hydrogeologic characteristics of subsurface Tertiary volcanic units at the Frenchman Flat corrective Action Unit (CAU). The process includes three steps. The first step involves generation of three-dimensional maps of the geologic structure of subsurface volcanic units using geophysical logs to distinguish between two classes: densely welded tuff and nonwelded tuff. The second step generates three-dimensional maps of hydraulic conductivity utilizing the spatial distribution of the two geologic classes obtained in the first step. Each class is described by a correlation structure based on existing data on hydraulic conductivity, and conditioned on the generated spatial location of each class. The final step demonstrates the use of the maps of hydraulic conductivity for modeling groundwater flow and radionuclide transport in volcanic tuffs from an underground nuclear test at the Frenchman Flat CAU. The results indicate that the majority of groundwater flow through the volcanic section occurs through zones of densely welded tuff where connected fractures provide the transport pathway. Migration rates range between near zero to approximately four m/yr, with a mean rate of 0.68 m/yr. This report presents the results of work under the FY96 Near-Field Modeling task of the UGTA program.

Pohlmann, K.; Shirley, C.; Andricevic, R.

1996-12-01T23:59:59.000Z

131

NEAR-FIELD IMAGING OF OBSTACLES Peijun Li and Yuliang Wang  

E-Print Network [OSTI]

applications in modern science and technology, such as nanotechnology, biology, information storage, and surface chemistry. Using near-field imaging, we

2014-06-30T23:59:59.000Z

132

Scanning tunneling microscopy and spectroscopy of Bi-Sr-Ca-Cu-O 2:2:1:2 high-temperature superconductors  

Science Journals Connector (OSTI)

We have used scanning tunneling microscopy and spectroscopy to investigate the surface-topographic and electronic properties of Bi-Sr-Ca-Cu-O 2:2:1:2 compounds. Even though there are two atoms (Bi and O) per lattice point, only one corrugation maximum per lattice point is observed. Polarity-dependent images show that the corrugations of the images taken at opposite polarities are in phase. We discuss possible explanations for this observation of in-phase corrugations at opposite polarities. Spectroscopic data were obtained at both high and low sample biases. Our data show that the density of surface electronic states near the Fermi level is about 3–4 orders of magnitude smaller than that of a typical metal. These states are only detectable when the stabilization voltage of the tunnel junction is low (<1.5 V). The conductivity near zero bias is extremely nonlinear, consistent with a nonmetallic surface layer. Vacuum resonant tunneling studies show that at these low-bias voltages the tip-to-sample distance is very small (?3–6 Å). This small tip-to-sample distance implies that the conductivity we detect near zero bias might result from the underlying CuO layer. We find evidence of bias-field penetration into the sample, implying that the surface density of states near the Fermi level is too small to screen out the electric field.

C. K. Shih; R. M. Feenstra; G. V. Chandrashekhar

1991-04-01T23:59:59.000Z

133

Absence of spin-flip transition at the Cr(001) surface: A combined spin-polarized scanning tunneling microscopy and neutron scattering study  

SciTech Connect (OSTI)

The spin-density wave (SDW) on Cr(001) has been investigated at temperatures between 20-300 K by means of spin-polarized scanning tunneling microscopy (SP-STM). Although neutron-scattering data measured on the same crystal clearly show a spin-flip transition from a transversal (T)-SDW to a longitudinal (L)-SDW at the expected spin-flip (SF) temperature T{sub SF}=123 K, no change was found on the Cr(001) surface with SP-STM. Throughout the entire temperature range the Cr(001) surface maintains a topological antiferromagnetic order with an in-plane magnetization that inverts between adjacent atomically flat terraces separated by monatomic step edges. The experimental results are interpreted by an absence of a spin-flip transition in the near-surface region probably driven by the surface anisotropy. The continuous connection of the surface T-SDW to the bulk L-SDW is accomplished by the formation of a 90 deg. domain wall just below the surface.

Haenke, T.; Krause, S.; Berbil-Bautista, L.; Bode, M.; Wiesendanger, R.; Wagner, V.; Lott, D.; Schreyer, A. [Institute of Applied Physics and Microstructure Research Center, University of Hamburg, Jungiusstrasse 11, D-20355 Hamburg (Germany); Physikalisch-Technische Bundesanstalt (PTB), Bundesallee 100, D-38116 Braunschweig (Germany); Institut fuer Werkstoffforschung, GKSS Forschungszentrum, Max-Planck-Strasse 1, D-21502 Geesthacht (Germany)

2005-05-01T23:59:59.000Z

134

Influence of Surface Preparation on Scanning Kelvin Probe Microscopy and Electron Backscatter Diffraction Analysis of Cross Sections of CdTe/CdS Solar Cells  

SciTech Connect (OSTI)

Electron backscatter diffraction (EBSD) provides information on the crystallographic structure of a sample, while scanning Kelvin probe microscopy (SKPM) provides information on its electrical properties. The advantage of these techniques is their high spatial resolution, which cannot be attained with any other techniques. However, because these techniques analyze the top layers of the sample, surface or cross section features directly influence the results of the measurements, and sample preparation is a main step in the analysis. In this work we investigated different methods to prepare cross sections of CdTe/CdS solar cells for EBSD and SKPM analyses. We observed that procedures used to prepare surfaces for EBSD are not suitable to prepare cross sections, and we were able to develop a process using polishing and ion-beam milling. This process resulted in very good results and allowed us to reveal important aspects of the cross section of the CdTe films. For SKPM, polishing and a light ion-beam milling resulted in cross sections that provided good data. We were able to observe the depletion region on the CdTe film and the p-n junction as well as the interdiffusion layer between CdTe and CdS. However, preparing good-quality cross sections for SKPM is not a reproducible process, and artifacts are often observed.

Moutinho, H. R.; Dhere, R. G.; Jiang, C. S.; Al-Jassim, M. M.

2011-01-01T23:59:59.000Z

135

Direct comparison between X-ray nanotomography and scanning electron microscopy for the microstructure characterization of a solid oxide fuel cell anode  

SciTech Connect (OSTI)

X-ray computed nanotomography (nano-CT) and scanning electron microscopy (SEM) have been applied to characterize the microstructure of a Solid Oxide Fuel Cell (SOFC) anode. A direct comparison between the results of both methods is conducted on the same region of the microstructure to assess the spatial resolution of the nano-CT microstructure, SEM being taken as a reference. A registration procedure is proposed to find out the position of the SEM image within the nano-CT volume. It involves a second SEM observation, which is taken along an orthogonal direction and gives an estimate reference SEM image position, which is then refined by an automated optimization procedure. This enables an unbiased comparison between the cell porosity morphologies provided by both methods. In the present experiment, nano-CT is shown to underestimate the number of pores smaller than 1 ?m and overestimate the size of the pores larger than 1.5 ?m. - Highlights: ? X-ray computed nanotomography (nano-CT) and SEM are used to characterize an SOFC anode. ? A methodology is proposed to compare the nano-CT and SEM data on the same region. ? The spatial resolution of the nano-CT data is assessed from that comparison.

Quey, R., E-mail: quey@emse.fr [CEA, LETI, MINATEC Campus, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France); École des Mines de Saint-Étienne, CNRS UMR 5307, 158 cours Fauriel, 42023 Saint-Étienne, Cedex 2 (France); Suhonen, H., E-mail: heikki.suhonen@esrf.fr [European Synchrotron Radiation Facility (ESRF), 6 Rue Jules Horowitz BP 220, 38043 Grenoble (France); Laurencin, J., E-mail: jerome.laurencin@cea.fr [CEA-Liten, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France); Cloetens, P., E-mail: peter.cloetens@esrf.fr [European Synchrotron Radiation Facility (ESRF), 6 Rue Jules Horowitz BP 220, 38043 Grenoble (France); Bleuet, P., E-mail: pierre.bleuet@cea.fr [CEA, LETI, MINATEC Campus, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France)

2013-04-15T23:59:59.000Z

136

Elemental relationships in rock varnish as seen with SEM/EDX (scanning electron microscopy/energy dispersive x-ray) elemental line profiling  

SciTech Connect (OSTI)

The heterogeneous nature of rock varnish requires a thorough survey of elemental and mineralogic compositions before relating chemical variability of rock varnish to past geochemical environments. Elemental relationships in rock varnish can be examined using scanning electron microscopy (SEM) in conjunction with an elemental line profiling routine using semi-quantitative, energy dispersive x-ray (EDX) analysis. Results of SEM/EDX analysis suggest: variations in cation concentrations used in varnish cation ratio dating relate more specifically to variations in detritus within the varnish than to element mobility as defined by weathering indices; Mn concentration rather than Mn:Fe ratios may be a more appropriate indicator of paleoclimatic fluctuations; and the Mn-oxide phase existing in varnish is most likely a Ba-enriched phase rather than birnessite. Element line profiling offers great potential for gaining insights into geochemical processes affecting the deposition and diagenesis of rock varnish and for testing hypotheses relating to its chemical variability. 27 refs., 9 figs.

Raymond, R. Jr.; Reneau, S.L.; Harrington, C.D.

1990-01-01T23:59:59.000Z

137

Quantification of Artifacts in Scanning Electron Microscopy Tomography: Improving the Reliability of Calculated Transport Parameters in Energy Applications such as Fuel Cell and Battery Electrodes  

Science Journals Connector (OSTI)

Abstract Focused ion beam and scanning electron microscopy tomography (FIB-SEMt) is commonly used to extract reactant transport relevant parameters from nano-porous materials in energy applications, such as fuel cells or batteries. Here we present an approach to virtually model the errors in FIB-SEMt which are caused by the FIB cutting distance. The errors are evaluated in terms of connectivity, solid volume fraction (SVF), conductivity, diffusivity, as well as mean grain and pore sizes. For state-of-the-art FIB-SEMt experiments, where a hydrogen fuel cell catalyst layer with 60 nm mean grain size and 40 % SVF is sectioned with a cutting distance of 15 nm, the error in our simulation ranges up to 51 % (conductivity), whereas other parameters remain largely unaffected (Laplace diffusivity, 4 %). We further present a method, employing virtual coarsening and back interpolation, to reduce FIB cutting distance errors in all investigated parameters. Both error evaluation and correction are applicable to sphere based porous materials with relevance for the energy conversion and storage sector such as polymer electrolyte membrane fuel cell catalyst layer (PEMFC CL), battery carbon binder domain (CBD) or supercapacitor electrodes.

Matthias Klingele; Roland Zengerle; Simon Thiele

2014-01-01T23:59:59.000Z

138

Electronic and structural properties of the InP(1 0 0)(2 × 4) surface studied by core-level photoemission and scanning tunneling microscopy  

Science Journals Connector (OSTI)

The (2 × 4)-reconstructed InP(1 0 0) surfaces have been investigated by scanning tunneling microscopy (STM) and synchrotron-radiation core-level photoelectron spectroscopy. STM observations show that the ?2 model describes the atomic structure of the InP(1 0 0)(2 × 4) surface in a limited range of the surface-preparation conditions, as predicted theoretically but not previously observed. STM results also support the accuracy of the previously found mixed-dimer structure for the InP(1 0 0)(2 × 4) surface under less P-rich conditions. A study of P 2p core-level photoelectron spectra, measured with different surface-sensitivity conditions, demonstrates that P 2p photoemission from the mixed-dimer InP(1 0 0)(2 × 4) surface consists of at least two surface-core-level-shift (SCLS) components which have kinetic energies approximately 0.4 eV higher and 0.3 eV lower than the bulk emission. On the basis of the surface-sensitivity difference between these SCLSs, they are related to the third-layer and top-layer P sites in the mixed-dimer structure, respectively.

P. Laukkanen; J. Pakarinen; M. Ahola-Tuomi; M. Kuzmin; R.E. Perälä; I.J. Väyrynen; A. Tukiainen; V. Rimpiläinen; M. Pessa; M. Adell; J. Sadowski

2006-01-01T23:59:59.000Z

139

The structures and dynamics of atomic and molecular adsorbates on metal surfaces by scanning tunneling microscopy and low energy electron diffraction  

SciTech Connect (OSTI)

Studies of surface structure and dynamics of atoms and molecules on metal surfaces are presented. My research has focused on understanding the nature of adsorbate-adsorbate and adsorbate-substrate interactions through surface studies of coverage dependency and coadsorption using both scanning tunneling microscopy (STM) and low energy electron diffraction (LEED). The effect of adsorbate coverage on the surface structures of sulfur on Pt(111) and Rh(111) was examined. On Pt(111), sulfur forms p(2x2) at 0.25 ML of sulfur, which transforms into a more compressed ({radical}3x{radical}3)R30{degrees} at 0.33 ML. On both structures, it was found that sulfur adsorbs only in fcc sites. When the coverage of sulfur exceeds 0.33 ML, it formed more complex c({radical}3x7)rect structure with 3 sulfur atoms per unit cell. In this structure, two different adsorption sites for sulfur atoms were observed - two on fcc sites and one on hcp site within the unit cell.

Yoon, Hyungsuk Alexander

1996-12-01T23:59:59.000Z

140

Spectroscopic ellipsometric modeling of a Bi–Te–Se write layer of an optical data storage device as guided by atomic force microscopy, scanning electron microscopy, and X-ray diffraction  

Science Journals Connector (OSTI)

Abstract Conventional magnetic tape is the most widely used medium for archival data storage. However, data stored on it need to be migrated every ca. 5 years. Recently, optical discs that store information for hundreds, or even more than 1000 years, have been introduced to the market. We recently proposed that technology in these optical discs be used to make an optical tape that would show greater permanence than its magnetic counterpart. Here we provide a detailed optical characterization of a sputtered thin film of bismuth, tellurium, and selenium (BTS) that is a proposed data storage layer for these devices. The methodology described herein should be useful in the future development of related materials. Spectroscopic ellipsometry (SE) data are obtained using interference enhancement, and the modeling of this data is guided by results from atomic force microscopy (AFM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-ray reflectivity (XRR). By AFM, ca. 40 nm BTS films show ca. 10 nm roughness. SEM images also suggest considerable roughness in the films and indicate that they are composed of 13.1 ± 5.9 nm grains. XRD confirms that the films are crystalline and predicts a grain size of 17 ± 2 nm. XRD results are consistent with the composition of the films — a mildly oxidized BTS material. Three models of increasing complexity are investigated to explain the SE data. The first model consists of a smooth, homogeneous BTS film. The second model adds a roughness layer to the previous model. The third model also has two layers. The bottom layer is modeled as a mixture of BTS and void using a Bruggeman effective medium approximation. The upper layer is similarly modeled, but with a gradient. The first model was unable to adequately model the SE data. The second model was an improvement — lower MSE (4.4) and good agreement with step height measurements. The third model was even better — very low MSE (2.6) and good agreement with AFM results. The third SE model predicted ca. 90% void at the film surface. XRR modeling of the film agreed well with the predictions from SE. The uniquenesses of the SE models were confirmed.

Hao Wang; Nitesh Madaan; Jacob Bagley; Anubhav Diwan; Yiqun Liu; Robert C. Davis; Barry M. Lunt; Stacey J. Smith; Matthew R. Linford

2014-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

Phonon-Polaritons enhance near field thermal transfer across the phase transition of VO2  

E-Print Network [OSTI]

conductivity contrasts of larger than an order of magnitude exist for switchable materials. Yet the control or very low temperatures. A first effort of rectification of thermal transfer in near field by 40 shown that whereas thermal conductivity and far field heat transfer are difficult to tune, in near field

Paris-Sud XI, Université de

142

EMSL: Capabilities: Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Microscopy Microscopy Additional Information Meet the Microscopy Experts Related EMSL User Projects Microscopy Tools are Applied to all Science Themes Watch the Microscopy capability video on EMSL's YouTube channel and read the transcript. Microscopy brochure Quiet Wing brochure EMSL hosts a variety of sophisticated microscopy instruments, including electron microscopes, optical microscopes, scanning probe microscopes, and computer-controlled microscopes for automated particle analysis. These tools are used to image a range of sample types with nanoscale-and even atomic-resolution with applications to surface, environmental, biogeochemical, atmospheric, and biological science. Each state-of-the-art instrument and customized capability is equipped with features for specific

143

Overcoming the black body limit in plasmonic and graphene near-field thermophotovoltaic systems  

E-Print Network [OSTI]

Near-field thermophotovoltaic (TPV) systems with carefully tailored emitter-PV properties show large promise for a new temperature range (600 – 1200K) solid state energy conversion, where conventional thermoelectric (TE) ...

Ilic, Ognjen

144

Near-Field Nanopatterning and Associated Energy Transport Analysis with Thermoreflectance  

E-Print Network [OSTI]

Laser nano-patterning with near-field optical microscope (NSOM) and the associated energy transport analysis are achieved in this study. Based on combined experimental/theoretical analyses, it is found that laser nano-patterning with a NSOM...

Soni, Alok

2013-05-31T23:59:59.000Z

145

Chiral-field microwave antennas (Chiral microwave near fields for far-field radiation)  

E-Print Network [OSTI]

In a single-element structure we obtain a radiation pattern with a squint due to chiral microwave near fields originated from a magnetostatic-mode ferrite disk. At the magnetostatic resonances, one has strong subwavelength localization of energy of microwave radiation. Magnetostatic oscillations in a thin ferrite disk are characterized by unique topological properties: the Poynting-vector vortices and the field helicity. The chiral-topology near fields allow obtaining unique phase structure distribution for far-field microwave radiation.

Kamenetskii, E O; Shavit, R

2015-01-01T23:59:59.000Z

146

Report on Modeling Coupled Processes in the Near Field of a Clay Repository  

Broader source: Energy.gov (indexed) [DOE]

on Modeling Coupled Processes in the Near Field of a Clay on Modeling Coupled Processes in the Near Field of a Clay Repository Report on Modeling Coupled Processes in the Near Field of a Clay Repository Clay/shale has been considered as potential host rock for geological disposal of high-level radioactive waste throughout the world. Coupled thermal, hydrological, mechanical, and chemical (THMC) processes have a significant impact on the long-term safety of a clay repository. This report documents results from three R&D activities: (1) implementation and validation of constitutive relationships, (2) development of a discrete fracture network (DFN) model for investigating coupled processes in the excavation damaged zone, and (3) development of a THM model for the Full-Scale Emplacement Experiment tests at Mont Terri, Switzerland, for the

147

High energy photoelectron emission from gases using plasmonics enhanced near-fields  

E-Print Network [OSTI]

We study theoretically the photoelectron emission in noble gases using plasmonic enhanced near-fields. We demonstrate that these fields have a great potential to generate high energy electrons by direct mid-infrared laser pulses of the current femtosecond oscillator. Typically, these fields appear in the surroundings of plasmonic nanostructures, having different geometrical shape such as bow-ties, metallic waveguides, metal nanoparticles and nanotips, when illuminated by a short laser pulse. In here, we consider metal nanospheres, in which the spatial decay of the near-field of the isolated nanoparticle can be approximated by an exponential function according to recent attosecond streaking measurements. We establish that the strong nonhomogeneous character of the enhanced near-field plays an important role in the above threshold ionization (ATI) process and leads to a significant extension in the photoelectron spectra. In this work, we employ the time dependent Schr\\"odinger equation in reduced dimensions to ...

Ciappina, M F; Guichard, R; Pérez-Hernández, J A; Roso, L; Arnold, M; Siegel, T; Zaïr, A; Lewenstein, M

2013-01-01T23:59:59.000Z

148

Report on THMC Modeling of the Near Field Evolution of a Generic Clay  

Broader source: Energy.gov (indexed) [DOE]

on THMC Modeling of the Near Field Evolution of a Generic on THMC Modeling of the Near Field Evolution of a Generic Clay Repository: Model Validation and Demonstration Rev 2 Report on THMC Modeling of the Near Field Evolution of a Generic Clay Repository: Model Validation and Demonstration Rev 2 Shale and clay-rich rock formations have been considered as potential host rocks for geological disposal of high-level radioactive waste throughout the world. Coupled thermal, hydrological, mechanical, and chemical (THMC) processes have a significant impact on the long-term safety of a repository in this type of rocks. The validity of the two-part Hooke's model (TPHM), a new constitutive relationship, and associated formulations regarding rock hydraulic/mechanical properties is demonstrated by the consistency between observations from a mine-by test at the Mont Terri site

149

Graphene-assisted near-field radiative heat transfer between corrugated polar materials  

SciTech Connect (OSTI)

Graphene has attracted great attention in nanoelectronics, optics, and energy harvesting. Here, the near-field radiative heat transfer between graphene-covered corrugated silica is investigated based on the exact scattering theory. It is found that graphene can improve the radiative heat flux between silica gratings by more than one order of magnitude and alleviate the performance sensitivity to lateral shift. The underlying mechanism is mainly attributed to the improved photon tunneling of modes away from phonon resonances. Besides, coating with graphene leads to nonlocal radiative transfer that breaks Derjaguin's proximity approximation and enables corrugated silica to outperform bulk silica in near-field radiation.

Liu, X. L.; Zhang, Z. M., E-mail: zhuomin.zhang@me.gatech.edu [G. W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, Georgia 30332 (United States)

2014-06-23T23:59:59.000Z

150

Near-field thermal radiation between hyperbolic metamaterials: Graphite and carbon nanotubes  

SciTech Connect (OSTI)

The near-field radiative heat transfer for two hyperbolic metamaterials, namely, graphite and vertically aligned carbon nanotubes (CNTs), is investigated. Graphite is a naturally existing uniaxial medium, while CNT arrays can be modeled as an effective anisotropic medium. Different hyperbolic modes can be separately supported by these materials in certain infrared regions, resulting in a strong enhancement in near-field heat transfer. It is predicted that the heat flux between two CNT arrays can exceed that between SiC plates at any vacuum gap distance and is about 10 times higher with a 10?nm gap.

Liu, X. L.; Zhang, R. Z.; Zhang, Z. M., E-mail: zhuomin.zhang@me.gatech.edu [G. W. Woodruff School of Mechanical Engineering, Georgia Institute of Technology, Atlanta, Georgia 30332 (United States)

2013-11-18T23:59:59.000Z

151

Particle resuspension in the Columbia River plume near field Emily Y. Spahn,1  

E-Print Network [OSTI]

Particle resuspension in the Columbia River plume near field Emily Y. Spahn,1 Alexander R. Horner are used to investigate the mechanisms of sediment resuspension and entrainment into the plume. An east, the plume is much less stratified during low-discharge conditions, and large resuspension events

152

Curve crossing and negative refraction in simulations of near-field coupled metallic nanoparticle arrays  

E-Print Network [OSTI]

Curve crossing and negative refraction in simulations of near-field coupled metallic nanoparticle-polariton LSPP dispersion on regular arrays of metal nanoparticles in the weak-field and weak-damping limits nanoparticle ar- rays to guide electromagnetic energy of optical frequencies along geometries smaller than

Baer, Roi

153

Graphene-based photovoltaic cells for near-field thermal energy conversion  

E-Print Network [OSTI]

Graphene-based photovoltaic cells for near-field thermal energy conversion Riccardo Messina-Sud 11, 2, Avenue Augustin Fresnel, 91127 Palaiseau Cedex, France. Thermophotovoltaic devices are energy-conversion , IR sensing and spectroscopy11,12 and has paved the way to a new generation of NTPV energy-conversion

Paris-Sud XI, Université de

154

Scanning Josephson Tunneling Microscopy of Single Crystal Bi2Sr2CaCu2O8+delta with a Conventional Superconducting Tip  

SciTech Connect (OSTI)

We have performed both Josephson and quasiparticle tunneling in vacuum tunnel junctions formed between a conventional superconducting scanning tunneling microscope tip and overdoped Bi2Sr2CaCu2O8+ single crystals. A Josephson current is observed with a peak centered at a small finite voltage due to the thermal-fluctuation-dominated superconducting phase dynamics. Josephson measurements at different surface locations yield local values for the Josephson ICRN product. Corresponding energy gap measurements were also performed and a surprising inverse correlation was observed between the local ICRN product and the local energy gap.

Kimura, H.; Barber Jr., R. P.; Ono, S.; Ando, Yoichi; Dynes, Robert C.

2009-10-28T23:59:59.000Z

155

Measuring near-field nanoparticle concentration profiles by correlating surface plasmon resonance reflectance with effective refractive index of nanofluids  

Science Journals Connector (OSTI)

Time-dependent and near-field nanoparticle concentrations are determined by correlating the surface plasmon resonance (SPR) reflectance intensities with the effective refractive...

Kim, Iltai; Kihm, Kenneth D

2010-01-01T23:59:59.000Z

156

End station for nanoscale magnetic materials study: Combination of scanning tunneling microscopy and soft X-ray magnetic circular dichroism spectroscopy  

SciTech Connect (OSTI)

We have constructed an end station for nanoscale magnetic materials study at the soft X-ray beamline HiSOR BL-14 at Hiroshima Synchrotron Radiation Center. An ultrahigh-vacuum scanning tunneling microscope (STM) was installed for an in situ characterization of nanoscale magnetic materials in combination with soft X-ray magnetic circular dichroism (XMCD) spectroscopy experiment. The STM was connected to the XMCD experimental station via damper bellows to isolate it from environmental vibrations, thus achieving efficient spatial resolution for observing Si(111) surface at atomic resolution. We performed an in situ experiment with STM and XMCD spectroscopy on Co nanoclusters on an Au(111) surface and explored its practical application to investigate magnetic properties for well-characterized nanoscale magnetic materials.

Ueno, Tetsuro; Sawada, Masahiro; Namatame, Hirofumi [Hiroshima Synchrotron Radiation Center, Hiroshima University, 2-313 Kagamiyama, Higashi-Hiroshima 739-0046 (Japan); Kishimizu, Yusuke; Kimura, Akio [Graduate School of Science, Hiroshima University, 1-3-1 Kagamiyama, Higashi-Hiroshima 739-8526 (Japan); Taniguchi, Masaki [Hiroshima Synchrotron Radiation Center, Hiroshima University, 2-313 Kagamiyama, Higashi-Hiroshima 739-0046 (Japan); Graduate School of Science, Hiroshima University, 1-3-1 Kagamiyama, Higashi-Hiroshima 739-8526 (Japan)

2012-12-15T23:59:59.000Z

157

Near-Field Radiative Heat Transfer between Metamaterials coated with Silicon Carbide Film  

E-Print Network [OSTI]

In this letter, we study the near-field radiative heat transfer between two metamaterial substrates coated with silicon carbide (SiC) thin films. It is known that metamaterials can enhance the near-field heat transfer over ordinary materials due to excitation of magnetic plasmons associated with s polarization, while strong surface phonon polariton exists for SiC.By careful tuning of the optical properties of metamaterial it is possible to excite electrical and magnetic resonance for the metamaterial and surface phonon polaritons for SiC at different spectral regions, resulting in the enhanced heat transfer. The effect of the SiC film thickness at different vacuum gaps is investigated. Results obtained from this study will be beneficial for application of thin film coatings for energy harvesting.

Basu, Soumyadipta; Wang, Liping

2014-01-01T23:59:59.000Z

158

Novel microwave near-field sensors for material characterization, biology, and nanotechnology  

E-Print Network [OSTI]

The wide range of interesting electromagnetic behavior of contemporary materials requires that experimentalists working in this field master many diverse measurement techniques and have a broad understanding of condensed matter physics and biophysics. Measurement of the electromagnetic response of materials at microwave frequencies is important for both fundamental and practical reasons. In this paper, we propose a novel near-field microwave sensor with application to material characterization, biology, and nanotechnology. The sensor is based on a subwavelength ferrite-disk resonator with magnetic-dipolar-mode (MDM) oscillations. Strong energy concentration and unique topological structures of the near fields originated from the MDM resonators allow effective measuring material parameters in microwaves, both for ordinary structures and objects with chiral properties.

Joffe, R; Shavit, R

2015-01-01T23:59:59.000Z

159

A gap capacitance method for slider flying height measurement in near-field optical disk drives  

Science Journals Connector (OSTI)

In order to overcome the diffraction limit of conventional optical disk drives, and substantially increase data storage capacity and density, near-field optical disk drives remain to be realized. The slider of a flying pickup head in a near-field optical disk drive has to fly at a stable spacing above the disk surface. To sense the slider flying height, a gap capacitance method is developed in this study to measure capacitance variation between the pickup head and disk surface. The capacitance varying with the flying height is modulated by a Colpitts oscillator. Subsequent demodulation accounts for height variation of the flying pickup head. Measurement results of this method are verified by using a laser Doppler interferometer.

J.W. Chen; T.S. Liu

2004-01-01T23:59:59.000Z

160

Nonlinear optical tuning of photonic crystal microcavities by near-field probe  

SciTech Connect (OSTI)

We report on a nonlinear way to control and tune the dielectric environment of photonic crystal microcavities exploiting the local heating induced by near-field laser excitation at different excitation powers. The temperature gradient due to the optical absorption results in an index of refraction gradient which modifies the dielectric surroundings of the cavity and shifts the optical modes. Reversible tuning can be obtained either by changing the excitation power density or by exciting in different points of the photonic crystal microcavity.

Vignolini, Silvia; Zani, Margherita; Riboli, Francesco; Vinattieri, Anna; Wiersma, Diederik S.; Gurioli, Massimo [LENS and Department of Physics, University of Florence, Via Nello Carrara 1, 50019 Sesto Fiorentino (Italy); Intonti, Francesca [LENS and Department of Physics, University of Florence, Via Nello Carrara 1, 50019 Sesto Fiorentino (Italy); CNISM, Unita di Ricerca di Firenze, Via Sansone 1, 50019 Sesto Fiorentino (Italy); Balet, Laurent; Li, Lianhe [Ecole Polytechnique Federale de Lausanne, Institute of Photonics and Quantum Electronics, Station 3, CH-1015 Lausanne (Switzerland); Colocci, Marcello [CNISM, Unita di Ricerca di Firenze, Via Sansone 1, 50019 Sesto Fiorentino (Italy); Francardi, Marco; Gerardino, Annamaria [Institute of Photonics and Nanotechnology, CNR, via del Cineto Romano 42, 00156 Roma (Italy); Fiore, Andrea [COBRA Research Institute, Eindhoven University of Technology, 5600 MB Eindhoven (Netherlands)

2008-07-14T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

Strain relief and AlSb buffer layer morphology in GaSb heteroepitaxial films grown on Si as revealed by high-angle annular dark-field scanning transmission electron microscopy  

SciTech Connect (OSTI)

The interfacial misfit (IMF) dislocation array of an epitaxial GaSb film on a Si substrate has been imaged with high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM). The mismatch strain accommodation through dislocation formation has been investigated using geometric phase analysis (GPA) on HAADF-STEM images with atomic resolution to probe the defects' local strain distribution. These measurements indicate that the lattice parameter of the epitaxial film recovers its bulk value within three unit cells from the interface due to the relaxation through IMF dislocations. The atomic number contrast of the HAADF-STEM images and energy dispersive x-ray spectrometry illustrate the formation of islands of AlSb buffer layer along the interface. The role of the AlSb buffer layer in facilitating the GaSb film growth on Si is further elucidated by investigating the strain field of the islands with the GPA.

Vajargah, S. Hosseini; Couillard, M.; Cui, K. [Department of Material Science and Engineering, McMaster University, 1280 Main St. W., Hamilton, Ontario L8S 4M1 (Canada); Tavakoli, S. Ghanad; Robinson, B.; Kleiman, R. N.; Preston, J. S. [Department of Engineering Physics, McMaster University, Hamilton, Ontario L8S 4M1 (Canada); Botton, G. A. [Department of Material Science and Engineering, McMaster University, 1280 Main St. W., Hamilton, Ontario L8S 4M1 (Canada); Canadian Centre for Electron Microscopy, McMaster University, Hamilton, Ontario L8S 4M1 (Canada)

2011-02-21T23:59:59.000Z

162

Piezoelectric & Optical Set-up to measure an Electrical Field. Application to the Longitudinal Near-Field generated by a  

E-Print Network [OSTI]

influences the longitudinal electrical near-field generated by it. For this application, we designed our set extremity on the longitudinal electrical near-field generated by a coaxial cable. Considering1/12 Piezoelectric & Optical Set-up to measure an Electrical Field. Application to the Longitudinal

Paris-Sud XI, Université de

163

Scanning-tunneling-microscopy investigation of the p(2×2) and c(2×2) overlayers of S on Ni(100)  

Science Journals Connector (OSTI)

The p(2×2) and c(2×2) sulfur overlayers on Ni(100), and the clean Ni(100) surface itself, have been imaged in an ultrahigh-vacuum scanning tunneling microscope, and topographic and spectroscopic information was obtained from all three surfaces. These data are compared to theoretical calculations of the surfaces derived using the Green’s-function method of Pendry, Pretre, and Krutzen, where the sample Green’s function is calculated in a multiple-scattering formalism based on the layer Korringa-Kohn-Rostoker method. Our simple model has proved reasonably successful in predicting the corrugation heights observed on the sulfated nickel surfaces, and confirmed the fact that the difference in height observed between the p(2×2) and the c(2×2) phases is electronic in origin. It is also proposed that the enhanced corrugation observed on the clean nickel surface may in part be attributable to the presence of a magnetic surface state immediately below the Fermi energy. Attempts to model the I-V and dI/dV spectroscopy curves proved less successful but it is believed that this was largely attributable to the approximations used in the present calculation.

A. Partridge; G. J. Tatlock; F. M. Leibsle; C. F. J. Flipse; G. Hörmandinger; J. B. Pendry

1993-09-15T23:59:59.000Z

164

Chemical Imaging Analysis of Environmental Particles Using the Focused Ion Beam/Scanning Electron Microscopy Technique: Microanalysis Insights into Atmospheric Chemistry of Fly Ash  

SciTech Connect (OSTI)

Airborne fly ash from coal combustion may represent a source of bioavailable iron (Fe) in the open ocean. However, few studies have been made focusing on Fe speciation and distribution in coal fly ash. In this study, chemical imaging of fly ash has been performed using a dual-beam FIB/SEM (focused ion beam/scanning electron microscope) system for a better understanding of how simulated atmospheric processing modify the morphology, chemical compositions and element distributions of individual particles. A novel approach has been applied for cross-sectioning of fly ash specimen with a FIB in order to explore element distribution within the interior of individual particles. Our results indicate that simulated atmospheric processing causes disintegration of aluminosilicate glass, a dominant material in fly ash particles. Aluminosilicate-phase Fe in the inner core of fly ash particles is more easily mobilized compared with oxide-phase Fe present as surface aggregates on fly ash spheres. Fe release behavior depends strongly on Fe speciation in aerosol particles. The approach for preparation of cross-sectioned specimen described here opens new opportunities for particle microanalysis, particular with respect to inorganic refractive materials like fly ash and mineral dust.

Chen, Haihan; Grassian, Vicki H.; Saraf, Laxmikant V.; Laskin, Alexander

2013-01-21T23:59:59.000Z

165

Scanning tuneeling microscopy studies of fivefold surfaces of icosahedral Al-Pd-Mn quasicrystals and of thin silver films on those surfaces  

SciTech Connect (OSTI)

The present work in this dissertation mainly focuses on the clean fivefold surfaces of i-Al-Pd-Mn quasicrystals as well as the nucleation and growth of Ag films on these surfaces. In addition, Ag film growth on NiAl(110) has been explored in the frame of this dissertation. First, we have investigated the equilibration of a fivefold surface of icosahedral Al-Pd-Mn quasicrystal at 900-915 K and 925-950 K, using Omicron variable temperature scanning tunneling microscope (STM). Annealing at low temperatures resulted in many voids on some terraces while the others were almost void-free. After annealing at 925-950K, void-rich terraces became much rarer. Our STM images suggest that through growth and coalescence of the voids, a different termination becomes exposed on host terraces. All of these observations in our study indicate that even after the quasicrystalline terrace-step structure appears, it evolves with time and temperature. More specifically, based on the STM observations, we conclude that during the annealing a wide range of energetically similar layers nucleate as surface terminations, however, with increasing temperature (and time) this distribution gets narrower via elimination of the metastable void-rich terraces. Next, we have examined the bulk structural models of icosahedral Al-Pd-Mn quasicrystal in terms of the densities, compositions and interplanar spacings for the fivefold planes that might represent physical surface terminations. In our analyses, we mainly have focused on four deterministic models which have no partial or mixed occupancy but we have made some comparisons with an undeterministic model. We have compared the models with each other and also with the available experimental data including STM, LEED-IV, XPD and LEIS. In all deterministic models, there are two different families of layers (a pair of planes), and the nondeterministic model contains similar group of planes. These two families differ in terms of the chemical decoration of their top planes. Hence, we name them as Pd+(with Pd) and Pd-(without Pd). Based on their planer structure and the step height, it can be said that these two families can be viable surface terminations. However, besides the Pd content, these two sets differ in terms of relative densities of their top planes as well as the gap separating the layer from the nearest atomic plane. The experimental data and other arguments lead to the conclusion that the Pd- family is favored over the Pd+. This has an important implication on the interpretation of local motifs seen in the high resolution STM images. In other words, the dark stars are not formed by cut-Bergmans rather they are formed by cut-Mackays.

Unal, Baris

2008-12-01T23:59:59.000Z

166

Novel Approaches to Soft X-ray Spectroscopy: Scanning TransmissionX-ray Microscopy and Ambient Pressure X-Ray PhotoelectronSpectroscopy  

SciTech Connect (OSTI)

This workshop focused on novel spectroscopies at Beamlines 11.0.2, 5.3.2 and 9.3.2 at the ALS. The workshop brought together users from a wide range of fields to highlight recent experimental and technical developments both in scanning transmission X-ray spectroscopy (STXM) and ambient pressure photoelectron spectroscopy (APPES). The morning session featured talks on experiments involving new developments at the STXM, while the afternoon session was devoted to those using APXPS. In the morning session, Tolek Tyliszczak discussed the improved detector developments at the STXM, such as an avalanche photodiode detector and fluorescence and electron detection, as well as the continued development of in situ cells for heating, gas flow, and electrochemical cells. Of these, only the avalanche photodiode in combination with a novel multichannel photon-counting system is in routine use in time-resolved studies. Bartel Van Waeyenberge (Ghent University) presented results of magnetic imaging with a time resolution of 70-100 ps combined with a lateral resolution of 20-40 nm performed with the STXM (Beamline 11.0.2). As a complement to the time-domain ''pump-and-probe'' measurements, they developed a frequency-domain ''sine-excitation'' technique in order to study specific eigenmodes of these ferromagnetic patterns with high spatial resolution. This new approach was used to study the gyrotropic vortex motions in micron-sized ferromagnetic patterns. Adam Hitchcock (McMaster University) presented the development, in collaboration with Daniel Guay (INRS, Varennes) and Sherry Zhang, of the apparatus and techniques for applying STXM to in-situ studies of electrochemistry, in particular electrochromism in polyaniline. In addition, substantial progress was reported on a joint project to develop substrates and methods for chemically selective lithography of multilayer polymer systems. Selective patterns, such as that displayed in the figure, can now be written efficiently with the bend magnet STXM on Beamline 5.3.2. Yves Acremann (SSRL) discussed time and spatially resolved X-ray magnetic circular dichroism (XMCD) experiments on spin transfer devices at the STXM (Beamline 11.0.2). These elegant experiments explore time resolved measurements of the magnetization dynamics within a 100 x 150 nm sample influenced by a spin-polarized current. This experiment shows that the magnetization in these magnetic nanostructures are not uniform, as they are influenced by the Oersted field of the charge current needed to generate the spin current. The implementation of a novel multichannel photon counting system in combination with an avalanche photon detector decreased the data-acquisition time by a factor of 10, owing to its ability to resolve the structure of multi bunch mode. Gordon E. Brown, Jr. (Stanford University and SSRL) described ''Applications of STXM to Microbial Bioweathering and Biomineralization''. In the interaction of bacteria with ferrihydrite nanoparticles, microenvironments that were very different than the bulk material were observed, showing that bulk thermodynamics may not be useful for predicting micro phases. Gordon also presented work showing that iron nanoparticles are attracted to the negatively charged bacteria and form a coating that reduces iron oxide minerals. The afternoon session started with presentations by Simon Mun and Hendrik Bluhm, who discussed the current status and the future plans for the two APPES end-stations at the ALS, which are located at Beamlines 9.3.2 and 11.0.2, respectively. In both end-stations, samples can be measured in gaseous environments at pressures of up to several Torr, which makes possible the investigation of numerous phenomena, in particular in the fields of atmospheric and environmental science as well as heterogeneous catalysis. Specific examples of the application of APPES were shown in the following presentations. John Hemminger (University of California, Irvine) reported on APPES investigations at Beamlines 9.3.2 and 11.0.2 of the interaction of alkali halide surfaces with water. The m

Bluhm, Hendrik; Gilles, Mary K.; Mun, Simon B.; Tyliszczak, Tolek

2006-02-01T23:59:59.000Z

167

Influence of roughness on near-field heat transfer between two plates  

E-Print Network [OSTI]

The surface roughness correction to the near-field heat transfer between two rough bulk materials is discussed by using second-order perturbation theory. The results allow for estimating the impact of surface roughness to the heat transfer in recent experiments between two plates and between a microsphere and a plate (using the Derjaguin approximation). Furthermore, we show that the proximity approximation for describing rough surfaces is valid for distances much smaller than the correlation length of the surface roughness even if the heat transfer is dominated by the coupling of surface modes.

Svend-Age Biehs; Jean-Jacques Greffet

2011-03-11T23:59:59.000Z

168

Accessing the Optical Magnetic Near-Field through Babinet’s Principle  

Science Journals Connector (OSTI)

For illumination and collection two Schwarzschild type objectives were used (32 × , NA = 0.65), with nominal incidence angle between 18° and 40° at focus. ... The tip-scattered antenna near-field is collected by the same parabolic mirror in a backscattering geometry and filtered by a vertical polarizer before being directed to a MCT detector, where it is detected interferometrically. Demodulation of the signal at the second or higher harmonic of the tip-dither frequency ?AFM using a lock-in amplifier suppresses the far-field background signal. ...

Honghua U. Yang; Robert L. Olmon; Kseniya S. Deryckx; Xiaoji G. Xu; Hans A. Bechtel; Yuancheng Xu; Brian A. Lail; Markus B. Raschke

2014-08-06T23:59:59.000Z

169

Geochemistry of Natural Components in the Near-Field Environment, Yucca Mountain, Nevada  

SciTech Connect (OSTI)

The natural near-field environment in and around the emplacement drifts of the proposed nuclear waste repository at Yucca Mountain, Nevada, includes the host rock, dust, seepage, and pore water. The chemical compositions of these components have been determined for assessing possible chemical and mineralogical reactions that may occur after nuclear waste is emplaced. The rock hosting the proposed repository is relatively uniform as shown by a mean coefficient of variation (CV) of 9 percent for major elements. In contrast, compositional variations of dust (bulk and water-soluble fractions), pore water, and seepage are large with mean CVs ranging from 28 to 64 percent. (authors)

Peterman, Zell E. [Yucca Mountain Project Branch, U.S. Geological Survey, MS 963 Box 25046 Denver Federal Center, 6th and Kipling Sts., Denver, CO, 80225 (United States); Oliver, Thomas A. [c/o U.S. Geological Survey, S.M. Stoller Corporation, MS 421 Box 25046 Denver Federal Center, Denver, CO, 80225 (United States)

2007-07-01T23:59:59.000Z

170

A New Interpretation of the Scanning Tunneling Microscope Image...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

of Graphite. A New Interpretation of the Scanning Tunneling Microscope Image of Graphite. Abstract: In this work, highly-resolved scanning tunneling microscopy images of graphite...

171

Spectrally resolved near-field intensity measurements from gain-guided twin-stripe laser diode arrays. Technical report  

SciTech Connect (OSTI)

Gain-guided twin-stripe laser diodes were observed that exhibit two distinct sets of longitudinal modes, one corresponding to a single near-field intensity profile centered between the stripes and the other to a double-lobe near-field distribution centered under the stripes. A large spectral separation between these two sets of modes was also measured. The double-lobe distribution probably results from a weak index guide, which occurs because of the decrease in the current density between stripes. The spectral separation between these two near-field modes is believed to be due to band filling.

Heflinger, D.G.; Fenner, W.R.

1988-11-01T23:59:59.000Z

172

Tungsten Nanowire Based Hyperbolic Metamaterial Emitters for Near-field Thermophotovoltaic Applications  

E-Print Network [OSTI]

Recently, near-field radiative heat transfer enhancement across nanometer vacuum gaps has been intensively studied between two hyperbolic metamaterials (HMMs) due to unlimited wavevectors and high photonic density of state. In this work, we theoretically analyze the energy conversion performance of a thermophotovoltaic (TPV) cell made of In0.2Ga0.8Sb when paired with a HMM emitter composed of tungsten nanowire arrays embedded in Al2O3 host at nanometer vacuum gaps. Fluctuational electrodynamics integrated with effective medium theory and anisotropic thin-film optics is used to calculate the near-field radiative heat transfer. It is found that the spectral radiative energy is enhanced by the epsilon-near-zero and hyperbolic modes at different polarizations. As a result, the power output from a semi-infinite TPV cell is improved by 1.85 times with the nanowire HMM emitter over that with a plain tungsten emitter at a vacuum gap of 10 nm. Moreover, by using a thin TPV cell with 10 um thickness, the conversion eff...

Chang, Jui-Yung; Wang, Liping

2014-01-01T23:59:59.000Z

173

Spectrally enhancing near-field radiative heat transfer by exciting magnetic polariton in SiC gratings  

E-Print Network [OSTI]

In the present work, we theoretically demonstrate, for the first time, that near field radiative transport between 1D periodic grating microstructures separated by subwavelength vacuum gaps can be significantly enhanced by exciting magnetic resonance or polariton. Fluctuational electrodynamics that incorporates scattering matrix theory with rigorous coupled wave analysis is employed to exactly calculate the near field radiative heat flux between two SiC gratings. Besides the well known coupled surface phonon polaritons (SPhP), an additional spectral radiative heat flux peak, which is due to magnetic polariton, is found within the phonon absorption band of SiC. The mechanisms, behaviors and interplays between magnetic polariton, coupled SPhP, single interface SPhP, and Wood's anomaly in the near field radiative transport are elucidated in detail. The findings will open up a new way to control near field radiative heat transfer by magnetic resonance with micro or nanostructured metamaterials.

Yang, Yue

2015-01-01T23:59:59.000Z

174

Apparatus comprising a tunable nanomechanical near-field grating and method for controlling far-field emission  

DOE Patents [OSTI]

A tunable nanomechanical near-field grating is disclosed which is capable of varying the intensity of a diffraction mode of an optical output signal. The tunable nanomechanical near-field grating includes two sub-gratings each having line-elements with width and thickness less than the operating wavelength of light with which the grating interacts. Lateral apertures in the two sub-gratings are formed from the space between one line-element of the first sub-grating and at least one line-element of the second sub-grating. One of the sub-gratings is capable of motion such that at least one of aperture width and aperture depth changes, causing a perturbation to the near-field intensity distribution of the tunable nanomechanical near-field grating and a corresponding change to the far-field emission of thereof.

Carr, Dustin Wade (Albuquerque, NM); Bogart, Gregory Robert (Corrales, NM)

2007-02-06T23:59:59.000Z

175

katherine henderson Pathology Slide Scanning rev1 Page 1 10/21/14 Scanning in Pathology  

E-Print Network [OSTI]

katherine henderson Pathology Slide Scanning rev1 Page 1 10/21/14 Scanning in Pathology Pathology offers several scanning methods: · Whole slide scans to be used as virtual microscopy ­ Aperio Coolscan for 35mm slides or glass slides with adapter (scans tissue area, not cells) The above scanners

176

Switchable stiffness scanning microscope probe  

E-Print Network [OSTI]

Atomic Force Microscopy (AFM) has rapidly gained widespread utilization as an imaging device and micro/nano-manipulator during recent years. This thesis investigates the new concept of a dual stiffness scanning probe with ...

Mueller-Falcke, Clemens T. (Clemens Tobias)

2005-01-01T23:59:59.000Z

177

High-resolution scanning transmission electron microscopy  

Science Journals Connector (OSTI)

...where, is the brightness of the source and bs/80 is the ratio of the real image of the...im-age (0.61A/a). The quantity bs/80 can be most easily defined in the source...tube can be ac-quired at a reasonable cost and is com-patible with full-color displays...

AV Crewe

1983-07-22T23:59:59.000Z

178

Scanning tunnelling microscopy of carbon nanotubes  

Science Journals Connector (OSTI)

...sheet into a cylinder where the car- bon lattice is joined seamlessly...consist of at least a pair of defective rings, e.g. squares, pentagons...sized (Meunier et al. 1999), defective (Meunier & Lambin 1998, 2000...Blase, X., Devita, A. & Car, R. 1997 Electronic structure...

2004-01-01T23:59:59.000Z

179

Cryogenic UHV installation for scanning tunneling microscopy  

Science Journals Connector (OSTI)

In this work we describe a helium cryostat with an ultrahigh vacuum chamber for placing the STM [H. By means of this installation it is possible to perform sample treatmentin situ (breaking, annealing, ion etchin...

V. S. Edelman; I. N. Khlyustikov

1996-01-01T23:59:59.000Z

180

Near-field heat transfer between a nanoparticle and a rough surface  

E-Print Network [OSTI]

In this work we focus on the surface roughness correction to the near-field radiative heat transfer between a nanoparticle and a material with a rough surface utilizing a direct perturbation theory up to second order in the surface profile. We discuss the different distance regimes for the local density of states above the rough material and the heat flux analytically and numerically. We show that the heat transfer rate is larger than that corresponding to a flat surface at short distances. At larger distances it can become smaller due to surface polariton scattering by the rough surface. For distances much smaller than the correlation length of the surface profile, we show that the results converge to a proximity approximation, whereas in the opposite limit the rough surface can be replaced by an equivalent surface layer.

Svend-Age Biehs; Jean-Jacques Greffet

2011-03-11T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

Acceleration of electrons in the near field of lower hybrid frequency grills  

SciTech Connect (OSTI)

On Tore Supra, during lower hybrid (LH) current drive experiments, localized heat flux deposition is observed on plasma facing components such as the guard limiters of the LH grills or any object which is magnetically connected to the LH launching waveguides : modular low-field side limiters, ion cyclotron heating antennas, inner first wall. Similar observations have been made on the divertor plates and limiters of TdeV. In particular, by alternating the rf powers of the 2 grills of Tore Supra, it was shown that the heat flux on the tiles of the guard limiters is related to the local electric field but not with the convective power. We present here a model of acceleration of electrons in the near field of LH antennas. Results of this model are compared to experimental results.

Goniche, M. [JET Joint Undertaking, Abingdon, Oxfordshire (England); Mailloux, J.; Demers, Y.; Jacquet, P.; Bibet, P.; Froissard, P.; Rey, G.; Surle, F.; Tareb, M. [Centre canadien de fusion magnetique, Varnnes, Quebec, (Canada); Guilhem, D.; Harris, J.H. [Oak Ridge National Lab., TN (United States)

1996-09-01T23:59:59.000Z

182

Graphene-based photovoltaic cells for near-field thermal energy conversion  

E-Print Network [OSTI]

Thermophotovoltaic devices are energy-conversion systems generating an electric current from the thermal photons radiated by a hot body. In far field, the efficiency of these systems is limited by the thermodynamic Schockley-Queisser limit corresponding to the case where the source is a black body. On the other hand, in near field, the heat flux which can be transferred to a photovoltaic cell can be several orders of magnitude larger because of the contribution of evanescent photons. This is particularly true when the source supports surface polaritons. Unfortunately, in the infrared where these systems operate, the mismatch between the surface-mode frequency and the semiconductor gap reduces drastically the potential of this technology. Here we show that graphene-based hybrid photovoltaic cells can significantly enhance the generated power paving the way to a promising technology for an intensive production of electricity from waste heat.

Riccardo Messina; Philippe Ben-Abdallah

2012-07-05T23:59:59.000Z

183

PHaSE | U.S. DOE Office of Science (SC)  

Office of Science (SC) Website

scanning probe microscopy, near-field scanning optical microscopy, surface science, neutron diffraction and scattering, density functional theory (DFT), monte carlo (MC),...

184

Nanomechanical near-field grating apparatus and acceleration sensor formed therefrom  

DOE Patents [OSTI]

A nanomechanical near-field grating device is disclosed which includes two sub-gratings vertically spaced by a distance less than or equal to an operating wavelength. Each sub-grating includes a plurality of line-elements spaced apart by a distance less than or equal to the operating wavelength. A light source (e.g., a VCSEL or LED) can provide light at the operating wavelength for operation of the device. The device can operate as an active grating, with the intensity of a reflected or transmitted portion of the light varying as the relative positions of the sub-gratings are controlled by an actuator. The device can also operate as a passive grating, with the relative positions of the sub-gratings changing in response to an environmentally-induced force due to acceleration, impact, shock, vibration, gravity, etc. Since the device can be adapted to sense an acceleration that is directed laterally or vertically, a plurality of devices can be located on a common substrate to form a multi-axis acceleration sensor.

Carr, Dustin Wade (Albuquerque, NM); Bogart, Gregory Robert (Corrales, NM); Keeler, Bianca E. N. (Albuquerque, NM)

2008-03-04T23:59:59.000Z

185

Scanning evanescent electro-magnetic microscope  

DOE Patents [OSTI]

A novel scanning microscope is described that uses near-field evanescent electromagnetic waves to probe sample properties. The novel microscope is capable of high resolution imaging and quantitative measurements of the electrical properties of the sample. The inventive scanning evanescent wave electromagnetic microscope (SEMM) can map dielectric constant, tangent loss, conductivity, complex electrical impedance, and other electrical parameters of materials. The quantitative map corresponds to the imaged detail. The novel microscope can be used to measure electrical properties of both dielectric and electrically conducting materials.

Xiang, Xiao-Dong (Alameda, CA); Gao, Chen (Alameda, CA)

2001-01-01T23:59:59.000Z

186

PHYSICAL REVIEW B 85, 155422 (2012) Near-field thermal radiation transfer controlled by plasmons in graphene  

E-Print Network [OSTI]

in graphene Ognjen Ilic,1,* Marinko Jablan,2 John D. Joannopoulos,1 Ivan Celanovic,3 Hrvoje Buljan,2 and Marin-field radiation transfer between two closely separated graphene sheets. The dependence of near-field heat exchange interband or intraband processes. We predict maximum transfer at low doping and for plasmons in two graphene

Soljaèiæ, Marin

187

Far field extrapolation from near field interactions and shielding influence investigations based on a FE-PEEC coupling method  

E-Print Network [OSTI]

variable speed drive. The aim is to evaluate the near field interactions between the tracks, which have by the floating potentials tracks. Moreover, due to the frequency and power increases, the compliance to EMC limited by the considered frequency range and/or by the geometry complexity, and/or by the medium

Boyer, Edmond

188

Slide27 | OSTI, US Dept of Energy, Office of Scientific and Technical...  

Office of Scientific and Technical Information (OSTI)

ETDEWEB - Bibliographic Citation image of report downloaded (Investigation of optical nanostructures for photovoltaics with near-field scanning microscopy...

189

Head–disk interface problems in first-surface near-field optical recording with flying optical head  

Science Journals Connector (OSTI)

Near-field recording (NFR) technology using a flying optical head is applied for high density optical data storage. Diamond-like carbon (DLC) film and PFPE lubricant film are coated on utmost NFR disk to reduce the tribological problems. A contamination at the head–disk interface (HDI), especially on a solid immersion lens (SIL) is observed. The contaminants are composed of dust materials from the surroundings and lubricant materials from a disk surface. The contaminants are supposed to be condensed by heat from a writing laser beam at the HDI. To avoid the contamination problem, a cover-layer is coated and a focal plane moved under the cover-layer from the HDI. First-surface near-field recording configuration can be modified by laminating a cover-layer, which enhances the possibility of a practical application with a media removability function.

Jin-Hong Kim

2008-01-01T23:59:59.000Z

190

Seismic Protection of Bridge Structures Using Shape Memory Alloy-Based Isolation Systems against Near-Field Earthquakes  

E-Print Network [OSTI]

SEISMIC PROTECTION OF BRIDGE STRUCTURES USING SHAPE MEMORY ALLOY-BASED ISOLATION SYSTEMS AGAINST NEAR-FIELD EARTHQUAKES A Dissertation by OSMAN ESER OZBULUT Submitted to the Office of Graduate Studies of Texas A&M University... Submitted to the Office of Graduate Studies of Texas A&M University in partial fulfillment of the requirements for the degree of DOCTOR OF PHILOSOPHY Approved by: Chair of Committee, Stefan Hurlebaus Committee Members, Jose Roesset Monique Head...

Ozbulut, Osman Eser

2012-02-14T23:59:59.000Z

191

Electron microscopy and microanalysis Two transmission electron microscopes  

E-Print Network [OSTI]

Electron microscopy and microanalysis Two transmission electron microscopes (TEM) and three scanning electron micro- scopes (SEM) are operated by the De- partment. Attachments for TEM include energy dispersive X-ray spectrometer (EDS), scanning transmission attachment, serial electron energy loss

192

Guided optical modes in randomly textured ZnO thin films imaged by near-field scanning optical K. Bittkau* and R. Carius  

E-Print Network [OSTI]

relevance. In particular, when designing thin-film solar cells and light emitting diodes LEDs , ran- domly

Peinke, Joachim

193

Near?field–far?field transition of a finite line source using incoherent light: A student laboratory experiment  

Science Journals Connector (OSTI)

A simple experiment employing low cost apparatus is presented which demonstrates the falloff of intensity with distance and the transition from the near field to the far field of a line source filament incandescent light bulb. A derivation of the Poynting vector as a function of the distance away from the filament is presented which shows an exact correspondence to the derivation for the electric field from a finite line charge source in electrostatics. The experimental data of power vs distance from the filament show an inverse first power of the distance falloff in the near field with a smooth transition to an inverse square law behavior in the far field in good agreement with the theoretical expression when corrections for the measured angular response of the detector are included. The experiment provides an illustration of the inverse square law falloff of intensity at large distances from the source experience with simple concepts and techniques of optical radiometry and incoherent light sources and the analogy between incoherent light sources and electrostatics in an undergraduate laboratory. An additional short experiment provides an illustration of electrical?to?optical power conversion efficiency and temperature dependent resistance associated with electron–phonon scattering in metals. A derivation of isotropic unpolarized elementary radiators from anisotropic dipole radiation is presented in the Appendix.

Xincheng Yan; Yixin Yu; Louis Shen; Keith H. Wanser

1995-01-01T23:59:59.000Z

194

Spring Semester, Course Title: Scanned Probe Techniques  

E-Print Network [OSTI]

: a fundamental understanding of the theoretical underpinnings behind each scanned probe technique Probe Microscopy: Atomic Scale Engineering by Forces and Currents - Adam Foster and Werner Hofer Applied Scanning Probe Methods (Vol. 1-13) ­ Bharat Bhushan, ed. Springer Handbook of Nanotechnology - Bharat

Sherrill, David

195

Near-field-enhanced, off-resonant laser sintering of semiconductor particles for additive manufacturing of dispersed Au–ZnO-micro/nano hybrid structures  

Science Journals Connector (OSTI)

Off-resonant near-field enhancement by gold nanoparticles adsorbed on crystalline zinc oxide significantly increases the energy efficiency of infrared laser sintering. In detail, ten different gold mass loads ...

Marcus Lau; Ralf G. Niemann; Mathias Bartsch; William O’Neill…

2014-03-01T23:59:59.000Z

196

Optical Microscopy and 4Optical Microscopy and 4 Pi MicroscopyPi Microscopy  

E-Print Network [OSTI]

Optical Microscopy and 4Optical Microscopy and 4 Pi MicroscopyPi Microscopy Carolyn A. SuttonCarolyn A. Sutton PH 464PH 464 #12;OverviewOverview The OpticalThe Optical MicroscopeMicroscopy 4 Pi Microscopy4 Pi Microscopy Optical Microscope for Metallography #12;Optical Microscope: OriginsOptical

La Rosa, Andres H.

197

Electron Microscopy | Center for Functional Nanomaterials  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Electron Microscopy Facility Electron Microscopy Facility Electron Microscopy This facility consists of four top-of-the line transmission electron microscopes, two of which are highly specialized instruments capable of extreme levels of resolution, achieved through spherical aberration correction. The facility is also equipped with extensive sample-preparation capabilities. The scientific interests of the staff focus on understanding the microscopic origin of the physical and chemical behavior of materials, with specific emphasis on in-situ studies of materials in native, functional environments. Capabilities Atomic-resolution imaging of internal materials structure with scanning transmission and transmission electron microscopy Spectroscopic characterization with energy dispersive x-ray

198

Salton Sea Geothermal Field, California, as a near-field natural analog of a radioactive waste repository in salt  

SciTech Connect (OSTI)

Since high concentrations of radionuclides and high temperatures are not normally encountered in salt domes or beds, finding an exact geologic analog of expected near-field conditions in a mined nuclear waste repository in salt will be difficult. The Salton Sea Geothermal Field, however, provides an opportunity to investigate the migration and retardation of naturally occurring U, Th, Ra, Cs, Sr and other elements in hot brines which have been moving through clay-rich sedimentary rocks for up to 100,000 years. The more than thirty deep wells drilled in this field to produce steam for electrical generation penetrate sedimentary rocks containing concentrated brines where temperatures reach 365/sup 0/C at only 2 km depth. The brines are primarily Na, K, Ca chlorides with up to 25% of total dissolved solids; they also contain high concentrations of metals such as Fe, Mn, Li, Zn, and Pb. This report describes the geology, geophysics and geochemistry of this system as a prelude to a study of the mobility of naturally occurring radionuclides and radionuclide analogs within it. The aim of this study is to provide data to assist in validating quantitative models of repository behavior and to use in designing and evaluating waste packages and engineered barriers. 128 references, 33 figures, 13 tables.

Elders, W.A.; Cohen, L.H.

1983-11-01T23:59:59.000Z

199

Frequency-Selective Near-Field Radiative Heat Transfer between Photonic Crystal Slabs: A Computational Approach for Arbitrary Geometries and Materials  

E-Print Network [OSTI]

of energy from a hot to a cold body is well known to be enhanced (even exceeding the black- body limit) whenFrequency-Selective Near-Field Radiative Heat Transfer between Photonic Crystal Slabs of Mathematics, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139, USA 3 Department

Soljaèiæ, Marin

200

Development of a microfluidic device for patterning multiple species by scanning probe lithography  

E-Print Network [OSTI]

Scanning Probe Lithography (SPL) is a versatile nanofabrication platform that leverages microfluidic “ink” delivery systems with Scanning Probe Microscopy (SPM) for generating surface-patterned chemical functionality on the sub-100 nm length scale...

Rivas Cardona, Juan Alberto

2009-06-02T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

Iran Thomas Auditorium, 8600 Transport Measurements by Scanning...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

8600 Transport Measurements by Scanning Probe Microscopy: Possibilities for Graphene Randall M. Feenstra Department of Physics Carnegie Mellon University CNMS D D I I S S C C O O...

202

Advanced Photon Source | Combining Scanning Probe Microscopy and  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

0.21.2013 0.21.2013 Scientists study old photos for new solutions to corrosion Each week, Viewpoints features interviews with guests that have expertise and real-word experience regarding specific issues. The program is aired on over 450 radio stations throughout the country. This weeks featured guests are Volker Rose, Physicist with the Advanced Photon Source and Center for Nanoscale Materials, Argonne National Laboratory, (www.anl.gov). and Edward Vicenzi, Research scientist at the Smithsonian Institution's Museum Conservation Institute, (www.si.edu/mci). Material failure caused by corrosion is dangerous and costs billions of dollars every year. What if you could figure out how to prevent and treat corrosion at the tiniest "nano" level before it has a chance to cause a

203

SCANNING ACOUSTIC MICROSCOPY MODELING FOR MICROMECHANICAL MEASUREMENTS OF COMPLEX SUBSTRATES  

E-Print Network [OSTI]

function of the substrate-fluid interface form the two key problems of effective SAM modeling. In the SAM modeling literature, a variety of approaches have been proposed for evaluating Eq 2.1. The approaches most frequently adopted are founded either... 1973). As seen from Eq 2.1, the evaluation of the reflected pressure field requires the computation of the angular spectrum and reflectance function. In general, these quantities can be computed independently. For angular spectrum calculation we...

Marangos, Orestes

2010-05-31T23:59:59.000Z

204

DISLOCATION IMAGES IN HIGH RESOLUTION SCANNING ELECTRON MICROSCOPY  

E-Print Network [OSTI]

. There are several dislocation images in the back scattered mode which are distinctly of excess/defect contrast observed in the dark field : two seperate conditions cars. be found. There is a set of dislocations having

Paris-Sud XI, Université de

205

Scanning Electron Microscopy in Concrete Petrography Paul E. Stutzman  

E-Print Network [OSTI]

hydroxide, needle-like habit of ettringite, and the sheet-like habit of calcium- silicate I C-S-H, platy-Type II C-S-H, and ettringite needles. Calcium Hydroxide Ettringite Calcium Hydroxide Ettringite Calcium-Silicate-Hydrate 15 µµm 10 µµm #12;#12;Calcium Hydroxide in Concrete 63 Figure 2

Bentz, Dale P.

206

Oscillating String as a Force Sensor in Scanning Force Microscopy  

Science Journals Connector (OSTI)

We present a sensor that uses an oscillating string to detect forces. A cantilever beam serves as a sample stage. The string is attached to the free end of ... the free end of the beam modifies the string tension...

A. Stalder; U. Dürig

1995-01-01T23:59:59.000Z

207

Numerical study of the THM effects on the near-field safety of a hypothetical nuclear waste repository--BMT1 of the DECOVALEX III project. Part 1: Conceptualization  

E-Print Network [OSTI]

Numerical study of the THM effects on the near-field safety of a hypothetical nuclear waste on the safety of a hypothetical nuclear waste repository at the near-field and are presented in three on the safety of nuclear waste repositories. To achieve the second objective, hypothetical benchmark test

Paris-Sud XI, Université de

208

Spectroscopy and atomic force microscopy of biomass  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Spectroscopy Spectroscopy and atomic force microscopy of biomass L. Tetard a,b , A. Passian a,b,n , R.H. Farahi a , U.C. Kalluri c , B.H. Davison c , T. Thundat a,b a Biosciences Division, Oak Ridge National Laboratory, Oak Ridge, TN 37831, USA b Department of Physics, University of Tennessee, Knoxville, TN 37996, USA c Environmental Sciences Division, Oak Ridge National Laboratory, Oak Ridge, TN, USA a r t i c l e i n f o Keywords: Atomic force microscopy Spectroscopy Plant cells Biomass Nanomechanics a b s t r a c t Scanning probe microscopy has emerged as a powerful approach to a broader understanding of the molecular architecture of cell walls, which may shed light on the challenge of efficient cellulosic ethanol production. We have obtained preliminary images of both Populus and switchgrass samples using atomic force microscopy (AFM). The results show distinctive features that are shared by switchgrass

209

SUBMOLECULAR IMAGING OF EPITAXIALLY CRYSTALLIZED HELICAL POLYOLEFINS BY ATOMIC FORCE MICROSCOPY  

E-Print Network [OSTI]

Digital Instruments, Inc., Santa Barbara, Cal. USA. Images were taken with an A­type scan head (max. scan microscopy EM and electron diffraction ED. AFM pictures with high resolution could be obtained when using polypropylene has been determined by electron microscopy EM and electron diffraction ED: chain conformation

Peters, Achim

210

Preparation of TiO2(110)-(1x1) Surface via UHV Cleavage: An scanning...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Preparation of TiO2(110)-(1x1) Surface via UHV Cleavage: An scanning tunneling microscopy study. Preparation of TiO2(110)-(1x1) Surface via UHV Cleavage: An scanning tunneling...

211

High resolution, high speed ultrahigh vacuum microscopy  

SciTech Connect (OSTI)

The history and future of transmission electron microscopy (TEM) is discussed as it refers to the eventual development of instruments and techniques applicable to the real time in situ investigation of surface processes with high resolution. To reach this objective, it was necessary to transform conventional high resolution instruments so that an ultrahigh vacuum (UHV) environment at the sample site was created, that access to the sample by various in situ sample modification procedures was provided, and that in situ sample exchanges with other integrated surface analytical systems became possible. Furthermore, high resolution image acquisition systems had to be developed to take advantage of the high speed imaging capabilities of projection imaging microscopes. These changes to conventional electron microscopy and its uses were slowly realized in a few international laboratories over a period of almost 40 years by a relatively small number of researchers crucially interested in advancing the state of the art of electron microscopy and its applications to diverse areas of interest; often concentrating on the nucleation, growth, and properties of thin films on well defined material surfaces. A part of this review is dedicated to the recognition of the major contributions to surface and thin film science by these pioneers. Finally, some of the important current developments in aberration corrected electron optics and eventual adaptations to in situ UHV microscopy are discussed. As a result of all the path breaking developments that have led to today's highly sophisticated UHV-TEM systems, integrated fundamental studies are now possible that combine many traditional surface science approaches. Combined investigations to date have involved in situ and ex situ surface microscopies such as scanning tunneling microscopy/atomic force microscopy, scanning Auger microscopy, and photoemission electron microscopy, and area-integrating techniques such as x-ray photoelectron spectroscopy, ultraviolet photoelectron spectroscopy, Auger electron spectroscopy, low-energy electron diffraction, temperature programmed desorption, high-resolution electron energy-loss and Fourier-transform infrared spectroscopies, and others. Material systems ranging from atomic layers of metals and semiconductors to biology related depositions are being investigated. In the case of biological materials, however, strict limitations to high-resolution applications are imposed by electron radiation damage considerations.

Poppa, Helmut [National Center for Electron Microscopy, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States)

2004-09-01T23:59:59.000Z

212

A High shear stress segment along the San Andreas Fault: Inferences based on near-field stress direction and stress magnitude observations in the Carrizo Plain Area  

SciTech Connect (OSTI)

Nearly 200 new in-situ determinations of stress directions and stress magnitudes near the Carrizo plain segment of the San Andreas fault indicate a marked change in stress state occurring within 20 km of this principal transform plate boundary. A natural consequence of this stress transition is that if the observed near-field ``fault-oblique`` stress directions are representative of the fault stress state, the Mohr-Coulomb shear stresses resolved on San Andreas sub-parallel planes are substantially greater than previously inferred based on fault-normal compression. Although the directional stress data and near-hydrostatic pore pressures, which exist within 15 km of the fault, support a high shear stress environment near the fault, appealing to elevated pore pressures in the fault zone (Byerlee-Rice Model) merely enhances the likelihood of shear failure. These near-field stress observations raise important questions regarding what previous stress observations have actually been measuring. The ``fault-normal`` stress direction measured out to 70 km from the fault can be interpreted as representing a comparable depth average shear strength of the principal plate boundary. Stress measurements closer to the fault reflect a shallower depth-average representation of the fault zone shear strength. If this is true, only stress observations at fault distances comparable to the seismogenic depth will be representative of the fault zone shear strength. This is consistent with results from dislocation monitoring where there is pronounced shear stress accumulation out to 20 km of the fault as a result of aseismic slip within the lower crust loading the upper locked section. Beyond about 20 km, the shear stress resolved on San Andreas fault-parallel planes becomes negligible. 65 refs., 15 figs.

Castillo, D. A., [Department of Geology and Geophysics, University of Adelaide (Australia); Younker, L.W. [Lawrence Livermore National Lab., CA (United States)

1997-01-30T23:59:59.000Z

213

Probing graphene defects and estimating graphene quality with optical microscopy  

SciTech Connect (OSTI)

We report a simple and accurate method for detecting graphene defects that utilizes the mild, dry annealing of graphene/Cu films in air. In contrast to previously reported techniques, our simple approach with optical microscopy can determine the density and degree of dislocation of defects in a graphene film without inducing water-related damage or functionalization. Scanning electron microscopy, confocal Raman and atomic force microscopy, and X-ray photoelectron spectroscopy analysis were performed to demonstrate that our nondestructive approach to characterizing graphene defects with optimized thermal annealing provides rapid and comprehensive determinations of graphene quality.

Lai, Shen [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Center for Human Interface Nanotechnology (HINT), Suwon 440-746 (Korea, Republic of); Kyu Jang, Sung [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Jae Song, Young, E-mail: yjsong@skku.edu [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Department of Physics, Sungkyunkwan University (SKKU), Suwon 440-746 (Korea, Republic of); Lee, Sungjoo, E-mail: leesj@skku.edu [SKKU Advanced Institute of Nanotechnology (SAINT), Suwon 440-746 (Korea, Republic of); Center for Human Interface Nanotechnology (HINT), Suwon 440-746 (Korea, Republic of); College of Information and Communication Engineering, Sungkyunkwan University (SKKU), Suwon 440-746 (Korea, Republic of)

2014-01-27T23:59:59.000Z

214

Nonlinear vibrational microscopy  

DOE Patents [OSTI]

The present invention is a method and apparatus for microscopic vibrational imaging using coherent Anti-Stokes Raman Scattering or Sum Frequency Generation. Microscopic imaging with a vibrational spectroscopic contrast is achieved by generating signals in a nonlinear optical process and spatially resolved detection of the signals. The spatial resolution is attained by minimizing the spot size of the optical interrogation beams on the sample. Minimizing the spot size relies upon a. directing at least two substantially co-axial laser beams (interrogation beams) through a microscope objective providing a focal spot on the sample; b. collecting a signal beam together with a residual beam from the at least two co-axial laser beams after passing through the sample; c. removing the residual beam; and d. detecting the signal beam thereby creating said pixel. The method has significantly higher spatial resolution then IR microscopy and higher sensitivity than spontaneous Raman microscopy with much lower average excitation powers. CARS and SFG microscopy does not rely on the presence of fluorophores, but retains the resolution and three-dimensional sectioning capability of confocal and two-photon fluorescence microscopy. Complementary to these techniques, CARS and SFG microscopy provides a contrast mechanism based on vibrational spectroscopy. This vibrational contrast mechanism, combined with an unprecedented high sensitivity at a tolerable laser power level, provides a new approach for microscopic investigations of chemical and biological samples.

Holtom, Gary R. (Richland, WA); Xie, Xiaoliang Sunney (Richland, WA); Zumbusch, Andreas (Munchen, DE)

2000-01-01T23:59:59.000Z

215

Materials Applications of Photoelectron Emission Microscopy....  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Applications of Photoelectron Emission Microscopy. Materials Applications of Photoelectron Emission Microscopy. Abstract: Photoelectron emission microscopy (PEEM) is a versatile...

216

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Acknowledgment Acknowledgment EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Acknowledgment Please acknowledge your use of the EMC in your publications and presentations with the following acknowledgment statement: The electron microscopy was accomplished at the Electron Microscopy Center at Argonne National Laboratory, a U.S. Department of Energy Office of Science Laboratory operated under Contract No. DE-AC02-06CH11357 by UChicago Argonne, LLC.

217

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

SAMM SAMM EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Sub-Ångstrom Microscopy and Microanalysis Facility In order to meet the scientific challenges of the future, the EMC has built a new state-of-the-art laboratory space for advanced electron microscopy. The new building has been designed to provide next- generation science with an operating environment that cannot be attained by renovating existing facilities. The EMC staff learned as much as possible from similar efforts around the world, including the SuperSTEM building at Daresbury, the Triebenberg Special Laboratory, the AML at Oak Ridge National Laboratory, the new NIST building, and various facilities for nanoscience.

218

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages

Laboratory Laboratory Electron Microscopy Center Argonne Home > EMC > EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers An Office of Science User Facility The Electron Microscopy Center (EMC) at Argonne National Laboratory develops and maintains unique capabilities for electron beam characterization and applies those capabilities to solve materials problems. The EMC staff carry out research with collaborators and users from Argonne, universities, and other laboratories. The expertise and facilities of the EMC additionally serve a group of national and international researchers. The EMC emphasizes three major areas: materials research, technique and instrumentation development, and operation as a national research facility. Research by EMC personnel includes microscopy based studies in high Tc superconducting materials, irradiation effects in metals and semiconductors, phase transformations, and processing related structure and chemistry of interfaces in thin films.

219

Microscopy. I: A Review  

Science Journals Connector (OSTI)

...indicates the spindle to be an orienting force through which a co-ordinated con tractile...asoT,E. M. and M@&soN,C. W. Handbook of Chemi cal Microscopy. Vol. 1. 1st...498 "586,1950. 164. NAORA, H. Fundamental Studies on the Determination of Desoxypentose-Nucleic...

Robert C. Mellors

1953-02-01T23:59:59.000Z

220

Morphological properties of pillared layered materials investigated by electron microscopy technique  

E-Print Network [OSTI]

Scanning electron microscopy was used to investigate morphological features of a diverse range of pillared layered materials. Pillared layered zirconium phosphates, zirconium polyimine phosphonates and anion exchanger derivatives, zinc...

Navas de Mascianglioli, Margarit

2012-06-07T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

Thermal expansion recovery microscopy: Practical design considerations  

SciTech Connect (OSTI)

A detailed study of relevant parameters for the design and operation of a photothermal microscope technique recently introduced is presented. The technique, named thermal expansion recovery microscopy (ThERM) relies in the measurement of the defocusing introduced by a surface that expands and recovers upon the heating from a modulated source. A new two lens design is presented that can be easily adapted to commercial infinite conjugate microscopes and the sensitivity to misalignment is analyzed. The way to determine the beam size by means of a focus scan and the use of that same scan to verify if a thermoreflectance signal is overlapping with the desired ThERM mechanism are discussed. Finally, a method to cancel the thermoreflectance signal by an adequate choice of a nanometric coating is presented.

Mingolo, N., E-mail: nmingol@fi.uba.ar; Martínez, O. E. [Facultad de Ingeniería, Universidad de Buenos Aires, Paseo Colon 850, 1063 Buenos Aires (Argentina)] [Facultad de Ingeniería, Universidad de Buenos Aires, Paseo Colon 850, 1063 Buenos Aires (Argentina)

2014-01-15T23:59:59.000Z

222

Peer Review of "Analysis and Simulation of Near-Field Wave Motion Data from the Source Physics Experiment Explosions," Antoun, et al, 2011 Monitoring Research Review  

SciTech Connect (OSTI)

The following is primarily a review of 'Analysis and Simulation of Near-Field Wave Motion Data from the Source Physics Experiment Explosions,' Antoun, et al, published by Lawrence Livermore National Laboratory (LLNL) after SPE-1 in 2011 (Ref. 1). However, LLNL analysis of SPE-2 (Ref. 2) will also be discussed. A review by Los Alamos National Laboratory (LANL) personnel of Reference 1 finds both the evidence of the effects of joints on the data and the correlation of calculations with the data weak. This conclusion is made on three separate levels: (1) Fundamental observations made of the various referenced figures taken as presented; (2) Observations made following corrections to errors and omissions to the selected data; and (3) Observations made after considering likely errors in the raw data set. The evidence presented in the referenced papers relies on subjective interpretation of various figures. This is the nature of this technical field of study and, indeed, much of our observation is also subjective.

Steedman, David W. [Los Alamos National Laboratory

2012-06-19T23:59:59.000Z

223

Combining In-Situ Buffer-Layer-Assisted-Growth with Scanning...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

growth (BLAG) technique by combining EMSL's ultra-high vacuum scanning probe microscopy (UHV SPM) and applying the resulting novel tool for formation and structural study of BaO...

224

Characterization of adsorbates by2 transient measurements in Scanning3  

E-Print Network [OSTI]

1 1 Characterization of adsorbates by2 transient measurements in Scanning3 Electrochemical electrochemical microscopy in2 transient mode allows the investigation of adsorbate intermediates at a polarized3 measurement of the electrochemical6 impedance allowed the complex differential capacitance for each adsorbed

Boyer, Edmond

225

Vector generator scan converter  

DOE Patents [OSTI]

High printing speeds for graphics data are achieved with a laser printer by transmitting compressed graphics data from a main processor over an I/O channel to a vector generator scan converter which reconstructs a full graphics image for input to the laser printer through a raster data input port. The vector generator scan converter includes a microprocessor with associated microcode memory containing a microcode instruction set, a working memory for storing compressed data, vector generator hardware for drawing a full graphic image from vector parameters calculated by the microprocessor, image buffer memory for storing the reconstructed graphics image and an output scanner for reading the graphics image data and inputting the data to the printer. The vector generator scan converter eliminates the bottleneck created by the I/O channel for transmitting graphics data from the main processor to the laser printer, and increases printer speed up to thirty fold. 7 figs.

Moore, J.M.; Leighton, J.F.

1988-02-05T23:59:59.000Z

226

Scanning computed confocal imager  

DOE Patents [OSTI]

There is provided a confocal imager comprising a light source emitting a light, with a light modulator in optical communication with the light source for varying the spatial and temporal pattern of the light. A beam splitter receives the scanned light and direct the scanned light onto a target and pass light reflected from the target to a video capturing device for receiving the reflected light and transferring a digital image of the reflected light to a computer for creating a virtual aperture and outputting the digital image. In a transmissive mode of operation the invention omits the beam splitter means and captures light passed through the target.

George, John S. (Los Alamos, NM)

2000-03-14T23:59:59.000Z

227

Los Alamos: MST-MTM: EML: Electron Microscopy Laboratory  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Electron Microscopy Laboratory, MST-6 Electron Microscopy Laboratory, MST-6 MST-6 Home Home In the MSL FEI Tecnai F30 Analytical TEM/STEM JEOL 6300FXV High Resolution SEM JEOL 3000F High Resolution Transmission Electron Microscope Philips XL30 F Scanning Electron Microscope & Orientation Imaging System Phillips CM30 Transmission Electron Microscope In the Sigma Building JEOL 840 EPMA with Wavelength Dispersive Spectroscopy FEI Strata DB235 FIB/SEM FEI XL30 Environmental Scanning Electron Microscope & Orientation Imaging System CONTACTS Bob Field 665.3938 Pat Dickerson 665.3036 Rob Dickerson 667.6337 Rod McCabe 606.1649 The Electron Microscopy Laboratory's Capabilities The Electron Microscopy Laboratory's Capabilities The Electron Microscopy Laboratory (EML) is part of MST-6, the Materials Technology - Metallurgy Group within the Materials Science and Technology Division at Los Alamos National Laboratory. It is a facility dedicated to the characterization of materials primarily through imaging, chemical, and crystallographic analyses of material microstructures with several electron and ion beam instruments. Accessory characterization techniques and equipment include energy dispersive x-ray analysis (EDS), wavelength dispersive x-ray analysis (WDS), electron backscatter diffraction (EBSD) and orientation imaging microscopy (OIM), and electron energy loss spectroscopy (EELS).

228

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

An Office of Science User Facility An Office of Science User Facility The Electron Microscopy Center (EMC) at Argonne National Laboratory develops and maintains unique capabilities for electron beam characterization and applies those capabilities to solve materials problems. The EMC staff carry out research with collaborators and users from Argonne, universities, and other laboratories. The expertise and facilities of the EMC additionally serve a group of national and international researchers. The EMC emphasizes three major areas: materials research, technique and instrumentation development, and operation as a national research facility. Research by EMC personnel includes microscopy based studies in high Tc superconducting materials, irradiation effects in metals and semiconductors, phase transformations, and processing related structure and chemistry of interfaces in thin films.

229

Electron Microscopy Lab  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Facilities » Facilities » Electron Microscopy Lab Electron Microscopy Lab Focusing on the study of microstructures with electron and ion beam instruments, including crystallographic and chemical techniques. April 12, 2012 Transmission electron microscope Rob Dickerson examines a multiphase oxide scale using the FEI Titan 80-300 transmission electron microscope. Contact Rob Dickerson (505) 667-6337 Email Rod McCabe (505) 606-1649 Email Pat Dickerson (505) 665-3036 Email Tom Wynn (505) 665-6861 Email Dedicated to the characterization of materials through imaging, chemical, and crystallographic analyses of material microstructures in support of Basic Energy Science, Laboratory Directed Research and Development, DoD, DOE, Work for Others, nuclear energy, and weapons programs. Go to full website »

230

Dynamic Transmission Electron Microscopy  

SciTech Connect (OSTI)

Dynamic transmission electron microscopy (DTEM) combines the benefits of high spatial resolution electron microscopy with the high temporal resolution of ultrafast lasers. The incorporation of these two components into a single instrument provides a perfect platform for in situ observations of material processes. However, previous DTEM applications have focused on observing structural changes occurring in samples exposed to high vacuum. Therefore, in order to expand the pump-probe experimental regime to more natural environmental conditions, in situ gas and liquid chambers must be coupled with Dynamic TEM. This chapter describes the current and future applications of in situ liquid DTEM to permit time-resolved atomic scale observations in an aqueous environment, Although this chapter focuses mostly on in situ liquid imaging, the same research potential exists for in situ gas experiments and the successful integration of these techniques promises new insights for understanding nanoparticle, catalyst and biological protein dynamics with unprecedented spatiotemporal resolution.

Evans, James E.; Jungjohann, K. L.; Browning, Nigel D.

2012-10-12T23:59:59.000Z

231

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Training Training EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers User Training Prior Training in Electron Microscopy: People who wish to operate TEMs must have at least one college-level course in TEM with a lab component or previous TEM experience. The college course can't be one in which TEM was just one of many topics. For researchers who lack academic training and/or practical experience in electron microscopy, we suggest the short courses in TEM at the Hooke College of Applied Sciences, and the hands-on TEM courses at Northwestern University or the University of Chicago or Northern Illinois University.

232

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Overview Overview The mission of the Electron Microscopy Center (EMC) is to: Conduct materials research using advanced microstructural characterization methods; Maintain unique resources and facilities for scientific research for the both the Argonne National Laboratory and national scientific community. Develop and expand the frontiers of microanalysis by fostering the evolution of synergistic state-of-the-art resources in instrumentation, techniques and scientific expertise; The staff members of the EMC carry out their own research as well as participate in collaborative programs with other scientists at Argonne National Laboratory as well as researchers, educators and students worldwide. The Electron Microscopy Center (EMC) at Argonne National Laboratory develops and maintains unique capabilities for electron beam characterization and applies those capabilities to solve materials problems. The EMC staff perform collaborative research with members of other Divisions at Argonne National Laboratory and with collaborators from universities and other laboratories. The expertise and facilities of the EMC additionally serve a group of national and international researchers. The EMC emphasizes three major areas: materials research, technique and instrumentation development, and operation as a national research facility. Research by EMC personnel includes microscopy based studies in high Tc superconducting materials, irradiation effects in metals and semiconductors, phase transformations, and processing related structure and chemistry of interfaces in thin films.

233

Only critical information was scanned  

Office of Legacy Management (LM)

Only critical information was scanned. Entire document is available upon request - Click here to email a...

234

Functional photoacoustic microscopy  

E-Print Network [OSTI]

-fiber phantom??????????????? 20 11 In vivo PAM imaging of subcutaneous microvasculature in rats after SAFT correction????????????????? 21 12 In vivo PAM imaging of subcutaneous microvasculature in rats based on auto-fit scan????????????????? 22... to demonstrate the depth-independent resolution before (A) and after (B) SAFT correction. The comparison of the MIP images before and after the SAFT correction is given by (C) and (D). In order to have a correct representation of the volumetric...

Zhang, Hao

2009-06-02T23:59:59.000Z

235

Argonne CNM: X-Ray Microscopy Capabilities  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Microscopy Facilities X-Ray Microscopy Facilities The Hard X-Ray Nanoprobe (HXN) facility provides scanning fluorescence, scanning diffraction, and full-field transmission and tomographic imaging capabilities with a spatial resolution of 30 nm over a spectral range of 6-12 keV. Modes of Operation Full-Field Transmission Imaging and Nanotomography X-ray transmission imaging uses both the absorption and phase shift of the X-ray beam by the sample as contrast mechanisms. Absorption contrast is used to map the sample density. Elemental constituents can be located by using differential edge contrast in this mode. Phase contrast can be highly sensitive to edges and interfaces even when the X-ray absorption is weak. These contrast mechanisms are exploited to image samples rapidly in full-field transmission mode under various environmental conditions, or combined with nanotomography methods to study the three-dimensional structure of complex and amorphous nanomaterials with the HXN.

236

Scanning micro-sclerometer  

DOE Patents [OSTI]

A scanning micro-sclerometer measures changes in contact stiffness and correlates these changes to characteristics of a scratch. A known force is applied to a contact junction between two bodies and a technique employing an oscillating force is used to generate the contact stiffness between the two bodies. As the two bodies slide relative to each other, the contact stiffness changes. The change is measured to characterize the scratch.

Oliver, Warren C. (Knoxville, TN); Blau, Peter J. (Oak Ridge, TN)

1994-01-01T23:59:59.000Z

237

Scanning micro-sclerometer  

DOE Patents [OSTI]

A scanning micro-sclerometer measures changes in contact stiffness and correlates these changes to characteristics of a scratch. A known force is applied to a contact junction between two bodies and a technique employing an oscillating force is used to generate the contact stiffness between the two bodies. As the two bodies slide relative to each other, the contact stiffness changes. The change is measured to characterize the scratch. 2 figs.

Oliver, W.C.; Blau, P.J.

1994-11-01T23:59:59.000Z

238

Microbial Impacts to the Near-Field Environment Geochemistry (MING): A Model for Estimating Microbial Communities in Repository Drifts at Yucca Mountain  

SciTech Connect (OSTI)

Geochemical and microbiological modeling was performed to evaluate the potential quantities and impact of microorganisms on the geochemistry of the area adjacent to and within nuclear waste packages in the proposed repository drifts at Yucca Mountain, Nevada. The microbial growth results from the introduction of water, ground support, and waste package materials into the deep unsaturated rock. The simulations, which spanned one million years, were accomplished using a newly developed computer code, Microbial Impacts to the Near-Field Environment Geochemistry (MING). MING uses environmental thresholds for limiting microbial growth to temperatures below 120 C and above relative humidities of 90 percent in repository drifts. Once these thresholds are met, MING expands upon a mass balance and thermodynamic approach proposed by McKinley and others (1997), by using kinetic rates to supply constituents from design materials and constituent fluxes including solubilized rock components into the drift, to perform two separate mass-balance calculations as a function of time. The first (nutrient limit) assesses the available nutrients (C, N, P and S) and calculates how many microorganisms can be produced based on a microorganism stoichiometry of C{sub 160}(H{sub 280}O{sub 80})N{sub 30}P{sub 2}S. The second (energy limit) calculates the energy available from optimally combined redox couples for the temperature, and pH at that time. This optimization maximizes those reactions that produce > 15kJ/mol (limit on useable energy) using an iterative linear optimization technique. The final available energy value is converted to microbial mass at a rate of 1 kg of biomass (dry weight) for every 64 MJ of energy. These two values (nutrient limit and energy limit) are then compared and the smaller value represents the number of microorganisms that can be produced over a specified time. MING can also be adapted to investigate other problems of interest as the model can be used in saturated and unsaturated environments and in laboratory situations to establish microbial growth limitations. Other projected uses include investigations of contaminated locations where monitored natural attenuation or engineered bioremediation could be employed.

D.M. Jolley; T.F. Ehrhorn; J. Horn

2002-03-19T23:59:59.000Z

239

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Submit an EMC Proposal Submit an EMC Proposal EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Submit an EMC Proposal EMC Proposal Submission Deadline Dates for FY2014: November 1, 2013 March 7, 2014 July 11, 2014 Is your proposal a multi-facility proposal? In other words, do you intend to submit proposals to EMC and APS or CNM for your research project? If your answer is "yes," go now to the Proposal Gateway.

240

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

EMC Users Committee EMC Users Committee EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers EMC Users Committee An EMC Users Committee has been organized to enhance communication between the user community and the EMC. While the EMC relies on and encourages strong interaction among its users and between its staff and users, the Users Committee provides an additional formal mechanism for user input into EMC planning and operations to ensure that users' needs and concerns are addressed.

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

End-of-Proposal Report End-of-Proposal Report EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers End-of-Proposal Report In accordance with the User Agreement, please provide the EMC with the following information when your proposal expires (one year after its acceptance date or when the experiments end, whichever is sooner). A research summary/progress report using these two templates:

242

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Becoming a User Becoming a User EMC Home Overview Personnel Resources Highlights Publications Visit EMC Contact Info Information for Users Becoming a User Submit a Proposal End-of-Proposal Report Acknowledgment User Training User Safety User Status Instrument Access User Committee User Meetings Data Storage Policy Visiting the EMC Instrument Calendars Info for EMC Staff SÅMM Facility TEAM Project Microscopy Links Argonne Facilities DOE/BES Facilities DOE/BES BES Electron Beam Microcharacterization Centers Procedure to Become a User at the EMC 1. Summary All users have to fulfill certain requirements before access to the EMC can be granted. The following list provides short descriptions of the requirements. Details can be found on this page and via the relevant links at the left. Register for access to Argonne's scientific user facilities (or update your user registration information).

243

Free motion scanning system  

DOE Patents [OSTI]

The present invention relates to an ultrasonic scanner system and method for the imaging of a part system, the scanner comprising: a probe assembly spaced apart from the surface of the part including at least two tracking signals for emitting radiation and a transmitter for emitting ultrasonic waves onto a surface in order to induce at least a portion of the waves to be reflected from the part, at least one detector for receiving the radiation wherein the detector is positioned to receive the radiation from the tracking signals, an analyzer for recognizing a three-dimensional location of the tracking signals based on the emitted radiation, a differential converter for generating an output signal representative of the waveform of the reflected waves, and a device such as a computer for relating said tracking signal location with the output signal and projecting an image of the resulting data. The scanner and method are particularly useful to acquire ultrasonic inspection data by scanning the probe over a complex part surface in an arbitrary scanning pattern.

Sword, Charles K. (Pleasant Hills, PA)

2000-01-01T23:59:59.000Z

244

Introduction to Photoelectron Emission Microscopy: Principles...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Introduction to Photoelectron Emission Microscopy: Principles and Applications. Introduction to Photoelectron Emission Microscopy: Principles and Applications. Abstract: In the...

245

Chapter 11 - Light sheet microscopy  

Science Journals Connector (OSTI)

Abstract This chapter introduces the concept of light sheet microscopy along with practical advice on how to design and build such an instrument. Selective plane illumination microscopy is presented as an alternative to confocal microscopy due to several superior features such as high-speed full-frame acquisition, minimal phototoxicity, and multiview sample rotation. Based on our experience over the last 10 years, we summarize the key concepts in light sheet microscopy, typical implementations, and successful applications. In particular, sample mounting for long time-lapse imaging and the resulting challenges in data processing are discussed in detail.

Michael Weber; Michaela Mickoleit; Jan Huisken

2014-01-01T23:59:59.000Z

246

Electron Microscopy Center  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

General Information for EMC Users General Information for EMC Users The Electron Microscopy Center (EMC) is an Office of Science User Facility operated for the U.S. Department of Energy Office of Science by Argonne National Laboratory. It is one of three scientific user facilities for electron beam microcharacterization and one of several National User Facilities located at Argonne National Laboratory. As a scientific user facility, the EMC supports user-accessible instruments (Resources) for high spatial resolution microanalysis, field imaging, nanoscale structural characterization, nanoscale fabrication and manipulation, and unique in situ studies of materials under the influence of ion-beam irradiation. These capabilities are used in a diverse variety of research areas to address grand challenge scientific questions encompassing, for example, energy-related studies, biology, astrophysics, archaeology, superconductivity, nanotechnology, environmental engineering, tribology, and ferroelectricity. The research is performed both by users and by EMC staff. While many users work independently, the most challenging research activities require extensive contributions from EMC staff.

247

Rapid scanning mass spectrometer  

SciTech Connect (OSTI)

Mass spectrometers and residual gas analyzers (RGA) are used in a variety of applications for analysis of volatile and semi-volatile materials. Analysis is performed by detecting fragments of gas molecules, based on their mass to charge ratio, which are generated in the mass spectrometer. When used as a detector for a gas chromatograph, they function as a means to quantitatively identify isolated volatile species which have been separated from other species via the gas chromatograph. Vacuum Technology, Inc., (VTI) produces a magnetic sector mass spectrometer/RGA which is used in many industrial and laboratory environments. In order to increase the utility of this instrument, it is desirable to increase the mass scanning speed, thereby increasing the number of applications for which it is suited. This project performed the following three upgrades on the computer interface. (1) A new electrometer was designed and built to process the signal from the detector. This new electrometer is more sensitive, over 10 times faster, and over 100 times more stable than the electrometer it will replace. (2) The controller EPROM was reprogrammed with new firmware. This firmware acts as an operating system for the interface and is used to shuttle communications between the PC and the AEROVAC mass spectrometer. (3) The voltage regulator which causes the ion selector voltage to ramp to allow ions of selected mass to be sequentially detected was redesigned and prototyped. The redesigned voltage regulator can be ramped up or down more than 100 times faster than the existing regulator. These changes were incorporated into a prototype unit and preliminary performance testing conducted. Results indicated that scanning speed was significantly increased over the unmodified version.

Leckey, J.H. [Lockheed Martin Energy Systems, Inc., Oak Ridge, TN (United States); Boeckmann, M.D. [Vacuum Technology, Inc., Oak Ridge, TN (United States)

1996-11-25T23:59:59.000Z

248

Directly correlated transmission electron microscopy and atom...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Directly correlated transmission electron microscopy and atom probe tomography of grain boundary oxidation in a Ni-Al binary Directly correlated transmission electron microscopy...

249

Analytical electron microscopy characterization of uranium-contaminated soils from the Fernald Site, FY1993 report  

SciTech Connect (OSTI)

A combination of optical microscopy, scanning electron microscopy with backscattered electron detection (SEM/BSE), and analytical electron microscopy (AEM) is being used to determine the nature of uranium in soils from the Fernald Environmental Management Project. The information gained from these studies is being used to develop and test remediation technologies. Investigations using SEM have shown that uranium is contained within particles that are typically 1 to 100 {mu}m in diameter. Further analysis with AEM has shown that these uranium-rich regions are made up of discrete uranium-bearing phases. The distribution of these uranium phases was found to be inhomogeneous at the microscopic level.

Buck, E.C.; Cunnane, J.C.; Brown, N.R.; Dietz, N.L.

1994-10-01T23:59:59.000Z

250

Simulating realistic imaging conditions for in situ liquid microscopy  

SciTech Connect (OSTI)

In situ transmission electron microscopy enables the imaging of biological cells, macromolecular protein complexes, nanoparticles, and other systems in a near-native environment. In order to improve interpretation of image contrast features and also predict ideal imaging conditions ahead of time, new virtual electron microscopic techniques are needed. A technique for virtual fluid-stage high-angle annular dark-field scanning transmission electron microscopy with the multislice method is presented that enables the virtual imaging of model fluid-stage systems composed of millions of atoms. The virtual technique is exemplified by simulating images of PbS nanoparticles under different imaging conditions and the results agree with previous experimental findings. General insight is obtained on the influence of the effects of fluid path length, membrane thickness, nanoparticle position, defocus and other microscope parameters on attainable image quality.

Welch, David A.; Faller, Roland; Evans, James E.; Browning, Nigel D.

2013-12-01T23:59:59.000Z

251

Acoustic microscopy for characterization of high?temperature superconducting tape  

Science Journals Connector (OSTI)

Although material scientists constantly discover superconducting compounds with higher critical temperatures (T c ’s) manufacturing of the high?temperature superconductors(HTS) remains a problem and long lengths (>1 mile) have yet to be produced. In an effort to produce long length superconductors manufacturing steps for HTS tape production have been critically looked at to find their effects in producing tape with the desired characteristics. In support of determining superconducting tapecharacteristics acoustic microscopy offers the potential for internal microstructural material characterization. This research will ultimately support in?process monitoring of HTSmanufacturing as part of an advanced sensing system to determine the presence of defects and/or the effects of process variables on the HTS tape. This presentation will overview scanning acoustic microscopy and present images of HTS tape at several frequencies ranging from 50 to 500 MHz. The results clearly demonstrate the feasibility of determining the Ag/ceramic interface location and the general integrity of the constituents.

Chiaki Miyasaka; Chris Cobucci; Bernhard Tittmann

1997-01-01T23:59:59.000Z

252

Partial scan design and test sequence generation based on reduced scan shift method  

Science Journals Connector (OSTI)

This paper presents a partial scan algorithm, calledPARES (PartialscanAlgorithm based onREduced Scan shift), for designing partial scan circuits. PARES is based on the reduced scan shift that has been previously ...

Yoshinobu Higami; Seiji Kajihara; Kozo Kinoshita

253

Dynamic Characterization of Graphene Growth and Etching by Oxygen on Ru(0001) by Photoemission Electron Microscopy  

E-Print Network [OSTI]

Dynamic Characterization of Graphene Growth and Etching by Oxygen on Ru(0001) by Photoemission of graphene on Ru(0001) was investigated by photoemission electron microscopy (PEEM) and scanning tunneling, we show that graphene overlayers with sizes ranging from nanometers to sub-millimeters have been

Bao, Xinhe

254

Characterisation of ‘Hadley’ grains by confocal microscopy  

Science Journals Connector (OSTI)

This work forms part of an exploratory study to investigate the use of fluorescent laser scanning confocal microscopy (LSCM) for imaging pores and voids in hardened mortar and concrete. The study has revealed the suitability of the technique for the characterisation of hollow shell (Hadley) hydration grains (these are grains that contain a void within the original boundary of the cement grain). It was found that Hadley grains could be imaged using fluorescent light techniques, subsequent to their impregnation by epoxy resin doped with a fluorescent dye. Prior to this work, it was not clear whether hollow grains were impregnated due to connections with capillary pores, or if they had been impregnated due to connections with damage caused during surface preparation (i.e. micro-cracks or deep surface scratches). However using the 3D LSCM imaging technique it was observed that connections between Hadley grains and hardened cement paste (HCP) capillary pores did exist, in different forms, at depths well below the surface providing ‘conduits’ along which resin was able to flow and impregnate the hollow grains. Other aspects of imaging Hadley grains are also described, such as the sectioning of ‘tips’ of larger grains often taken as separate smaller pores or grains in 2D images.

M.K. Head; H.S. Wong; N.R. Buenfeld

2006-01-01T23:59:59.000Z

255

Attempt of correlative observation of morphological synaptic connectivity by combining confocal laser-scanning microscope and FIB-SEM for immunohistochemical staining technique  

Science Journals Connector (OSTI)

......University, Uchinada, Japan 2 Department of Morphological Brain Science, Graduate School of Medicine, Kyoto University, Kyoto...B. Serial sec- tion scanning electron microscopy of adult brain tissue using focused ion beam milling. J. Neurosci (2008......

Takahiro Sonomura; Takahiro Furuta; Ikuko Nakatani; Yo Yamamoto; Satoru Honma; Takeshi Kaneko

2014-11-01T23:59:59.000Z

256

Role of bias voltage and tunneling current in the perpendicular displacements of freestanding graphene via scanning  

E-Print Network [OSTI]

graphene via scanning tunneling microscopy Peng Xu, Steven D. Barber, Matthew L. Ackerman, James Kevin measurements of freestanding graphene as a function of applied bias voltage and tunneling current setpoint, the graphene approaches the STM tip, while, on the other hand, when the tunneling current is increased

Thibado, Paul M.

257

Design of a scanning Josephson junction microscope for submicron-resolution magnetic imaging  

SciTech Connect (OSTI)

We describe a magnetic field scanning instrument designed to extend the spatial resolution of scanning superconducting quantum interference device microscopy into the submicron regime. This instrument, the scanning Josephson junction microscope, scans a single Josephson junction across the surface of a sample, detecting the local magnetic field by the modulation of the junction critical current. By using a submicron junction and a scanning tunneling microscope feedback system to maintain close proximity to the surface, magnetic field sensitivity of 10 {mu}G with a spatial resolution of 0.3 {mu}m should be attainable, opening up new opportunities for imaging vortex configurations and core structure in superconductors and magnetic domains in magnetic materials. {copyright} {ital 1999 American Institute of Physics.}

Plourde, B.L.; Van Harlingen, D.J. [Department of Physics, Science and Technology Center for Superconductivity, and Materials Research Laboratory, University of Illinois at Urbana-Champaign, Urbana, Illinois 61801 (United States)] [Department of Physics, Science and Technology Center for Superconductivity, and Materials Research Laboratory, University of Illinois at Urbana-Champaign, Urbana, Illinois 61801 (United States)

1999-11-01T23:59:59.000Z

258

Synchronized monochromator and insertion device energy scans at SLS  

SciTech Connect (OSTI)

Synchronous monochromator and insertion device energy scans were implemented at the Surfaces/Interfaces:Microscopy (SIM) beamline in order to provide the users fast X-ray magnetic dichroism studies (XMCD). A simple software control scheme is proposed based on a fast monochromator run-time energy readback which quickly updates the insertion device requested energy during an on-the-fly X-ray absorption scan (XAS). In this scheme the Plain Grating Monochromator (PGM) motion control, being much slower compared with the insertion device (APPLE-II type undulator), acts as a 'master' controlling the undulator 'slave' energy position. This master-slave software implementation exploits EPICS distributed device control over computer network and allows for a quasi-synchronous motion control combined with data acquisition needed for the XAS or XMCD experiment.

Krempasky, J.; Flechsig, U.; Korhonen, T.; Zimoch, D.; Quitmann, Ch.; Nolting, F. [Paul Scherrer Institut, Villigen, Swiss Light Source, 5235 Villigen PSI (Switzerland)

2010-06-23T23:59:59.000Z

259

Characterization and Theory of Electrocatalysts Based on Scanning Electrochemical Microscopy Screening Methods  

E-Print Network [OSTI]

with results for Pd-Co catalysts. This is based on establishing guidelines for selecting test systems, rapid cell cathode where the oxygen reduction reaction (ORR) occurs and important questions about whether the currently favored electrocatalyst for polymer electrolyte membrane fuel cells (PEMFC), Pt supported on C

Henkelman, Graeme

260

Imaging an ionic liquid adlayer by scanning tunneling microscopy at the solid|vacuum interface  

E-Print Network [OSTI]

of Surface Chemistry and Catalysis, Ulm University, D-89069 Ulm, Germany 2 Institute of Particle Technology, Clausthal University of Technology, D-38678 Clausthal- Zellerfeld, Gemany Abstract The first imaging(pentafluoroethyl)trifluorophosphate ([Py1,4]FAP) was evaporated onto a clean Au(111) surface by a Knudsen-type evaporator and the surface

Pfeifer, Holger

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

Recent Advances in Atomic-Scale Spin-Polarized Scanning Tunneling Microscopy  

E-Print Network [OSTI]

, Faradayweg 4-6 D-14195 Berlin (Dahlem) Germany WALTER R. L. LAMBRECHT Department of Physics, Case Western of atomically clean magnetic surfaces. Several key findings have been obtained. First, both magnetic and non Nanometer scale science and technology has been an area of intense research and development activity within

262

Electrochemical Scanning Tunneling Microscopy:? Adlayer Structure and Reaction at Solid/liquid Interface  

Science Journals Connector (OSTI)

From 2003?2006, he was a postdoctoral fellow and visiting fellow in the Department of Chemistry, Unversity of Alberta and National Institute for Nanotechnology (NINT), National Research Council (NRC), Canada. ... On the other hand, ex situ UHV surface characterization techniques, such as low-energy electron diffraction (LEED), electron energy-loss spectroscopy, and Auger electron spectroscopy have also supplied important information on the structure of the specific adsorption. ... Building up complicated assemblies is one big challenge for the future of bottom-up nanodevice fabrication. ...

Dong Wang; Li-Jun Wan

2007-10-09T23:59:59.000Z

263

Improvement of lateral resolution of scanning photo-induced impedance microscopy (SPIM)  

E-Print Network [OSTI]

in the gate metal into an area not covered by metal Influence of semiconductor donor concentration Ga Control Lock-In-Amp. Z X Y CD-ROM player optics Computer Control Output 1000 2000 3000 4000 1000 2000 3000

Moritz, Werner

264

Soft, entirely photoplastic probes for scanning force microscopy G. Genolet,a)  

E-Print Network [OSTI]

. The stiffness of a cantilever is given by its spring constant k Ewt3 /4l3 where w, t, and l denote the width with integrated tips made with a batch molding technique. II. DESCRIPTION AND FABRICATION OF PHOTOPLASTIC PROBES

Bielefeld, Universität

265

Platelet Adhesion in Rabbit Arteries observed by Scanning and Transmission Electron Microscopy  

Science Journals Connector (OSTI)

... the endothelium is removed from the mid-abdominal aorta of a rabbit, by passing a roughened probe into the lumen, only single platelets or small platelet clumps adhere to the ...

B. L. SHEPPARD; J. E. FRENCH

1970-03-14T23:59:59.000Z

266

SCANNING ELECTRON MICROSCOPY AND PORE CASTING: CHEROKEE AND BUG FIELDS, SAN JUAN COUNTY, UTAH  

SciTech Connect (OSTI)

Over 400 million barrels (64 million m{sup 3}) of oil have been produced from the shallow-shelf carbonate reservoirs in the Pennsylvanian (Desmoinesian) Paradox Formation in the Paradox Basin, Utah and Colorado. With the exception of the giant Greater Aneth field, the other 100 plus oil fields in the basin typically contain 2 to 10 million barrels (0.3-1.6 million m{sup 3}) of original oil in place. Most of these fields are characterized by high initial production rates followed by a very short productive life (primary), and hence premature abandonment. Only 15 to 25 percent of the original oil in place is recoverable during primary production from conventional vertical wells. An extensive and successful horizontal drilling program has been conducted in the giant Greater Aneth field. However, to date, only two horizontal wells have been drilled in small Ismay and Desert Creek fields. The results from these wells were disappointing due to poor understanding of the carbonate facies and diagenetic fabrics that create reservoir heterogeneity. These small fields, and similar fields in the basin, are at high risk of premature abandonment. At least 200 million barrels (31.8 million m{sup 3}) of oil will be left behind in these small fields because current development practices leave compartments of the heterogeneous reservoirs undrained. Through proper geological evaluation of the reservoirs, production may be increased by 20 to 50 percent through the drilling of low-cost single or multilateral horizontal legs from existing vertical development wells. In addition, horizontal drilling from existing wells minimizes surface disturbances and costs for field development, particularly in the environmentally sensitive areas of southeastern Utah and southwestern Colorado.

Thomas C. Chidsey Jr; David E. Eby; Louis H. Taylor

2003-12-01T23:59:59.000Z

267

Aberration-corrected scanning transmission electron microscopy: from atomic imaging and analysis to solving energy problems  

Science Journals Connector (OSTI)

...in solving the pressing energy problems facing us today...Discussion Meeting Issue New possibilities with aberration-corrected...Wang), pp.152-191. New York, NY: Springer. Pennycook...and analysis to solving energy problems. | The new possibilities of aberration-corrected...

2009-01-01T23:59:59.000Z

268

A technique for quantitative and qualitative viewing of aquatic bacteria using scanning electron microscopy  

E-Print Network [OSTI]

microscopic enumeration techniques. Water samples are concentrated on pre-wetted (Triton X-100) Nuclepore filters (0. 2 um pore size) to prov1de a uniform distri- bution of bacteria on the filter surface and vacuum filtered (660 Torr). The filter... is transferred to a petri dish containing filter paper soaked 1n 2% glutaraldehyde and the bacter1a are fixed for one hour. Dehydration 1s performed by transferr1ng the filters through a series of petri dishes conta1ning filter paper saturated with 25, 50, 75...

Dreier, Thomas Michael

2012-06-07T23:59:59.000Z

269

Scanning Tunneling Microscopy Studies of Metal Clusters Supported on Graphene and Silica Thin Film  

E-Print Network [OSTI]

The understanding of nucleation and growth of metals on a planar support at the atomic level is critical for both surface science research and heterogeneous catalysis studies. In this dissertation, two planar substrates, including graphene and ultra...

Zhou, Zihao

2012-10-19T23:59:59.000Z

270

Transparent Metal Films for Detection of Single-Molecule Optical Absorption by Scanning Tunneling Microscopy  

Science Journals Connector (OSTI)

To ensure better contact between the sample holder and the thin films, thick silver contacts are deposited at the sample edge using colloidal silver paint (Ted Pella Inc.). ... Berciaud, S.; Cognet, L.; Poulin, P.; Weisman, R. B.; Lounis, B.Absorption Spectroscopy of Individual Single-Walled Carbon Nanotubes Nano Lett. ...

Lea Nienhaus; Gregory E. Scott; Richard T. Haasch; Sarah Wieghold; Joseph W. Lyding; Martin Gruebele

2014-05-22T23:59:59.000Z

271

Scanning Tunneling Microscopy Study of Molybdenum Disulfide and its Derivatives on Cu(111)  

E-Print Network [OSTI]

during STM measurement to avoid vibrations and all thethe vibrations from the ground during STM measurement. For

Lu, Wenhao

2014-01-01T23:59:59.000Z

272

Electrical Characterization of Transition Metal Silicide Nanostructures Using Variable Temperature Scanning Probe Microscopy.  

E-Print Network [OSTI]

??Cobalt disilicide (CoSi2) islands have been formed on Si(111) and Si(100) through UHV deposition and annealing. Current-voltage (I-V) and temperature-dependent current-voltage (I-V-T) curves have been… (more)

Tedesco, Joseph Leo

2007-01-01T23:59:59.000Z

273

Recent advances in electron imaging, image interpretation and applications: environmental scanning electron microscopy  

Science Journals Connector (OSTI)

...specimens in a more `natural' state. As early...the presence of a gas in the specimen chamber...Ionizing collisions with gas molecules generate...SEs, causing a `cascade' of electrons...turn influencing gas cascade amplification. Add...

2003-01-01T23:59:59.000Z

274

Morphological expressions of antibiotic synergism against Pseudomonas aeruginosa as observed by scanning electron microscopy.  

Science Journals Connector (OSTI)

...spheroplasts; (v) surface holes or pits; (vi) super-elongation...spheroplasts; (v) surface holes or pits; (vi) super-elongation...spheroplasts; (v) surface holes or pits; (vi) super-elongation...isolated from a patient with severe burns. The susceptibility of the...

S J Waisbren; D J Hurley; B A Waisbren

1980-12-01T23:59:59.000Z

275

Imaging Single ZnO Vertical Nanowire Laser Cavities using UV-Laser Scanning Confocal Microscopy  

E-Print Network [OSTI]

emerging in the field of optoelectronics and nanophotonicsemerging in the field of optoelectronics and nanophotonics.

Yang, P.

2009-01-01T23:59:59.000Z

276

Scanning Transmission X-ray Microscopy: Applications in Atmospheric Aerosol Research  

E-Print Network [OSTI]

related to the total atomic absorption cross section, ? A (number. Tabulations of atomic absorption cross sections areC are the mass absorption coefficients and atomic masses for

Moffet, Ryan C.

2011-01-01T23:59:59.000Z

277

Scanning Electron Microscopy of Squid, Loligo peale;: Raw, Cooked, and Frozen Mantle  

E-Print Network [OSTI]

OTWELL and GEORGE G. GIDDINGS W. Steven Otwell is with the Department of Food Science and Human Nutrition, University of Florida, Gainesville, FL 32611. George G. Gid- dings is with the Fundacion Chile, Avda Santa, but cooking caused gross distortions in all mantle tissues. North Carolina, and cleaned for use (skin, head

278

Thermally driven visco-elastic measurement technique via spectral variations in scanning probe microscopy cantilevers  

E-Print Network [OSTI]

Understanding how fluids respond to various deformations is of great importance to a spectrum of disciplines ranging from bio-medical research on joint replacements to sealing technology in industrial machinery. Specifically, ...

Jones, Ryan Edward, 1974-

2004-01-01T23:59:59.000Z

279

Aberration-corrected scanning transmission electron microscopy: from atomic imaging and analysis to solving energy problems  

Science Journals Connector (OSTI)

...fuels, but the conversion efficiency of...into electrical energy is limited by...functionality in energy conversion devices such as...insights into the carrier dynamics in the...ability to study energy conversion processes in materials...

2009-01-01T23:59:59.000Z

280

Evaluation of drilled circuit boards using scanning white light interference microscopy  

E-Print Network [OSTI]

of panels drilled at one time. ~ Head Height (HD) - Height of the drill head in inches over the panel. Head height is indicative of the non-drilling, cool-off time out of the hole. A higher head height takes longer time between holes. . Table 4 shows... 7 Avera e Ra, R, and Rt values Bit Block HT SP CL HD PN R& R, R4 1 3 -1 1 -1 -1 1 45. 0395 3. 33275 2. 2925 -1 -1 1 1 -1 609535 5. 28325 3. 752 10 12 -1 1 -1 1 -1 37. 034 3. 5655 2. 7505 4. 14425 4. 3065 5. 827 1 1 1 60. 2075 1 1 1 -1 1 -1...

Nissen, Kristine Kay

2012-06-07T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

Scanning tunneling microscopy investigation of the TiO2 anatase ,,101... surface Wilhelm Hebenstreit,1  

E-Print Network [OSTI]

of tunneling sites in STM. Titanium dioxide (TiO2) is a versatile material that finds uses as a promoter. Fourfold-coordinated Ti atoms at step edges are preferred adsorption sites and allow the identification

Diebold, Ulrike

282

Study of perineal patterns of four species of Meloidogyne (Nematoda:Heteroderoidea) using scanning electron microscopy  

E-Print Network [OSTI]

Strawberry ~tco ersico culent m Arachis ~ho ea Citrull ~ s )rraris ~tco e sico escule t ~ca sicum fr tescens Arachis ~ho ea ~fa a ia sp. Rutgers Florunner Charleston Gray Rutgers California Wonder Florunner Albritton M. ~ico ~ ta M. java' ice... 75-8 (Race 1) 75-30 (Race 3) 75-30 75-37 73-57 74-19 75-37 75-32 75-2 Tomato Tomato Sweet potato Watermelon Corn Pepper Cotton Tomato Watermelon ~tco ersicon esc lentum ~to ersico esculentum ~iomoea batatas C t ullus ~ul s Zea...

Khan, Zainab Najafali

2012-06-07T23:59:59.000Z

283

Optimizing the environment for sub-0.2 nm scanning transmission electron microscopy  

Science Journals Connector (OSTI)

......where the manufacturer's specifications will be most complete) are...or neoprene greatly damps thermal fluctuations (Fig. 7...with neoprene for improved thermal stability. D. A. Muller...column helps greatly, better insulation of the stage drives and objective......

A Muller; J Grazul

2001-05-01T23:59:59.000Z

284

New views of materials through aberration-corrected scanning transmission electron microscopy  

Science Journals Connector (OSTI)

......analysis to solving energy problems. Phil...eds. (2007) New York: Springer...and electron energy loss spectroscopy...eds. (2011) New York: Springer...for electron energy loss spectroscopy...can now give new insights into......

S. J. Pennycook; M. Varela

2011-08-01T23:59:59.000Z

285

Toward Automated Analysis of Biofilm Architecture: Bias Caused by Extraneous Confocal Laser Scanning Microscopy Images  

Science Journals Connector (OSTI)

...bulk-medium interface boundaries...Zeisss CLSM interface software...spreading, two-dimensional fractal dimension...average and standard deviation...34). Measuring the thickness...of various interface PACVEIRs on the standard deviation...

Robin T. Merod; Jennifer E. Warren; Hope McCaslin; Stefan Wuertz

2007-06-01T23:59:59.000Z

286

Investigation of furan on vicinal Pd(1 1 1) by scanning tunneling microscopy  

E-Print Network [OSTI]

fraction in liquids derived from coal and biomass, with methylated phe- nols and furanic rings constituting, including coal and biomass [1]. Oxygen-containing aromatic heterocompounds form the largest contaminant

Chiang, Shirley

287

Scanning Tunneling Microscopy Study of Molybdenum Disulfide and its Derivatives on Cu(111)  

E-Print Network [OSTI]

principles electronic structure calculations . 27 3.1principles electronic structure calculations The followingFirst-principles electronic structure calculations, Physical

Lu, Wenhao

2014-01-01T23:59:59.000Z

288

Automated detection and time lapse analysis of dendritic spines in laser scanning microscopy images  

E-Print Network [OSTI]

is roughly divided into three related components. First, we focus on an image processing pipeline we have and Repair (now Harvard Neurodiscovery Center). I also would like to thank our collaborators: Bernardo

Miller, Eric

289

Scanning Tunneling Microscopy Study of Molybdenum Disulfide and its Derivatives on Cu(111)  

E-Print Network [OSTI]

in ultra-high vacuum(UHV) conditions are systematicallybuilt ultra high vacuum (UHV) STMs in Bartels group withbuilt ultra high vacuum (UHV) STMs in Bartels group with

Lu, Wenhao

2014-01-01T23:59:59.000Z

290

Internal Image Potential in Semiconductors - Effect on Scanning-Tunneling-Microscopy  

E-Print Network [OSTI]

10 10 m ~ o 0 ~ 410 g (25) j(s)=, f dE,D(E?s ) [No(E, ) No(E, qV)?], ? @ mp where mo is the free-electron mass, No(E, ) and No(E, ?qV) are one-dimensional finite-temperature sup- ply functions for electrons in the semiconductor and metal... correct only for a square barrier. If we define the cumulative current density as a function of energy according to Ej (E?s) =e J dE,'D(E,', s )[Xo(E,') Ko(E,' q?V)], ?0 (27) 0.2- ?0.2 ?0.6 5x10 cm (s=5k) the diff'erential current density per...

HUANG, ZH; WEIMER, M.; Allen, Roland E.

1993-01-01T23:59:59.000Z

291

Dynamic imaging with electron microscopy  

ScienceCinema (OSTI)

Livermore researchers have perfected an electron microscope to study fast-evolving material processes and chemical reactions. By applying engineering, microscopy, and laser expertise to the decades-old technology of electron microscopy, the dynamic transmission electron microscope (DTEM) team has developed a technique that can capture images of phenomena that are both very small and very fast. DTEM uses a precisely timed laser pulse to achieve a short but intense electron beam for imaging. When synchronized with a dynamic event in the microscope's field of view, DTEM allows scientists to record and measure material changes in action. A new movie-mode capability, which earned a 2013 R&D 100 Award from R&D Magazine, uses up to nine laser pulses to sequentially capture fast, irreversible, even one-of-a-kind material changes at the nanometer scale. DTEM projects are advancing basic and applied materials research, including such areas as nanostructure growth, phase transformations, and chemical reactions.

Campbell, Geoffrey; McKeown, Joe; Santala, Melissa

2014-05-30T23:59:59.000Z

292

Dynamic imaging with electron microscopy  

SciTech Connect (OSTI)

Livermore researchers have perfected an electron microscope to study fast-evolving material processes and chemical reactions. By applying engineering, microscopy, and laser expertise to the decades-old technology of electron microscopy, the dynamic transmission electron microscope (DTEM) team has developed a technique that can capture images of phenomena that are both very small and very fast. DTEM uses a precisely timed laser pulse to achieve a short but intense electron beam for imaging. When synchronized with a dynamic event in the microscope's field of view, DTEM allows scientists to record and measure material changes in action. A new movie-mode capability, which earned a 2013 R&D 100 Award from R&D Magazine, uses up to nine laser pulses to sequentially capture fast, irreversible, even one-of-a-kind material changes at the nanometer scale. DTEM projects are advancing basic and applied materials research, including such areas as nanostructure growth, phase transformations, and chemical reactions.

Campbell, Geoffrey; McKeown, Joe; Santala, Melissa

2014-02-20T23:59:59.000Z

293

Scan  

Broader source: Energy.gov (indexed) [DOE]

NAME OF PERSON WITH WHOM TO CONFER TELEPHONE DATE ARCHIVIST OF THE UNITED STATES Sharon Evelin NUMBER 1 301 -903-3455 i 1 - I REQUEST FOR REe?RDS DISPOSITION AUTHORITY NUMBER /dl- Y s + - o + - / TO: NATIONAL ARCH~VES & RECORDS ADMINISTRATION 8601 ADELPHI ROAD COLLEGE PARK, MD 20740-6001 1. FROM (Agency or establ~shment) U.S. DEPARTMENT OF ENERGY MAJOR SUBDIVISION Office of the Chief Information Officer MINOR SUBDIVISION Records Management Division I 1 8. DESCRIPTION OF ITEM AND PROPOSED DISPOSITION 1 9. GRS OR 1 10. A ~ T I O r Date received I Z L U V - ~ NOTIFICATION TO AGENCY In accordance with the provlslons of 44 U.S.C 3303a, the dlsposltlon request, Including amendments, 1 s approved except for Items that may be marked "dlsposltion not approved" or "withdrawn" In column 10.

294

Near-Field Magneto-Optical Microscope  

DOE Patents [OSTI]

A device and method for mapping magnetic fields of a sample at a resolution less than the wavelength of light without altering the magnetic field of the sample is disclosed. A device having a tapered end portion with a magneto-optically active particle positioned at the distal end thereof in communication with a fiber optic for transferring incoming linearly polarized light from a source thereof to the particle and for transferring reflected light from the particle is provided. The fiber optic has a reflective material trapping light within the fiber optic and in communication with a light detector for determining the polarization of light reflected from the particle as a function of the strength and direction of the magnetic field of the sample. Linearly polarized light from the source thereof transferred to the particle positioned proximate the sample is affected by the magnetic field of the sample sensed by the particle such that the difference in polarization of light entering and leaving the particle is due to the magnetic field of the sample. Relative movement between the particle and sample enables mapping.

Vlasko-Vlasov, Vitalii; Welp, Ulrich; and Crabtree, George W.

2005-12-06T23:59:59.000Z

295

Near Field Magneto-Optical Microscope  

DOE Patents [OSTI]

A device and method for mapping magnetic fields of a sample at a resolution less than the wavelength of light without altering the magnetic field of the sample is disclosed. A device having a tapered end portion with a magneto-optically active particle positioned at the distal end thereof in communication with a fiber optic for transferring incoming linearly polarized light from a source thereof to the particle and for transferring reflected light from the particle is provided. The fiber optic has a reflective material trapping light within the fiber optic and in communication with a light detector for determining the polarization of light reflected from the particle as a function of the strength and direction of the magnetic field of the sample. Linearly polarized light from the source thereof transferred to the particle positioned proximate the sample is affected by the magnetic field of the sample sensed by the particle such that the difference in polarization of light entering and leaving the particle is due to the magnetic field of the sample. Relative movement between the particle and sample enables mapping.

Vlasko-Vlasov, Vitalii K. (Downers Grove, IL); Welp, Ulrich (Lisle, IL); Crabtree, George W. (Chicago, IL)

2005-12-06T23:59:59.000Z

296

Convergence analysis in near-field imaging  

E-Print Network [OSTI]

Jul 25, 2014 ... inverse scattering problem is that of determining the nature of the ... A comprehensive review can be found in [7] on diffractive optics tech-.

Gang Bao

2014-07-24T23:59:59.000Z

297

Optimizing and extending light-sculpting microscopy for fast functional imaging in neuroscience  

E-Print Network [OSTI]

A number of questions in systems biology such as understanding how dynamics of neuronal networks are related to brain function require the ability to capture the functional dynamics of large cellular populations at high speed. Recently, this has driven the development of a number of parallel and high speed imaging techniques such as light-sculpting microscopy, which has been used to capture neuronal dynamics at the whole brain and single cell level in small model organism. However, the broader applicability of light-sculpting microscopy is limited by the size of volumes for which high speed imaging can be obtained and scattering in brain tissue. Here, we present strategies for optimizing the present tradeoffs in light-sculpting microscopy. Various scanning modalities in light-sculpting microscopy are theoretically and experimentally evaluated, and strategies to maximize the obtainable volume speeds, and depth penetration in brain tissue using different laser systems are provided. Design-choices, important par...

Rupprecht, Peter; Groessl, Florian; Haubensak, Wulf E; Vaziri, Alipasha

2015-01-01T23:59:59.000Z

298

ARM: W-Band Scanning ARM Cloud Radar (W-SACR) Hemispherical Sky RHI Scans (6 horizon-to-horizon scans at 30-degree azimuth intervals)  

DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

W-Band Scanning ARM Cloud Radar (W-SACR) Hemispherical Sky RHI Scans (6 horizon-to-horizon scans at 30-degree azimuth intervals)

Widener, Kevin; Nelson, Dan; Bharadwaj, Nitin; Lindenmaier, Iosif [Andrei; Johnson, Karen

299

ARM: Ka-Band Scanning ARM Cloud Radar (KASACR) Hemispherical Sky RHI Scan (6 horizon-to-horizon scans at 30-degree azimuth intervals)  

DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

Ka-Band Scanning ARM Cloud Radar (KASACR) Hemispherical Sky RHI Scan (6 horizon-to-horizon scans at 30-degree azimuth intervals)

Bharadwaj, Nitin; Widener, Kevin

300

ARM: X-Band Scanning ARM Cloud Radar (XSACR) Hemispherical Sky RHI Scans (6 horizon-to-horizon scans at 30-degree azimuth intervals)  

DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

X-Band Scanning ARM Cloud Radar (XSACR) Hemispherical Sky RHI Scans (6 horizon-to-horizon scans at 30-degree azimuth intervals)

Widener, Kevin; Nelson, Dan; Bharadwaj, Nitin; Lindenmaier, Iosif [Andrei; Johnson, Karen

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

Hyperspectral Microscopy of Explosives Particles Using an External Cavity Quantum Cascade Laser  

SciTech Connect (OSTI)

Using infrared hyperspectral imaging, we demonstrate microscopy of small particles of the explosives compounds RDX, tetryl, and PETN with near diffraction-limited performance. The custom microscope apparatus includes an external cavity quantum cascade laser illuminator scanned over its tuning range of 9.13-10.53 µm in four seconds, coupled with a microbolometer focal plane array to record infrared transmission images. We use the hyperspectral microscopy technique to study the infrared absorption spectra of individual explosives particles, and demonstrate sub-nanogram detection limits.

Phillips, Mark C.; Bernacki, Bruce E.

2012-12-26T23:59:59.000Z

302

NASA DC-8 Airborne Scanning Lidar System  

Science Journals Connector (OSTI)

A scanning lidar system is being developed for installation on the NASA DC-8 atmospheric research aircraft to support...in-situ aerosol and gas measurements. Design and objectives of the DC-8 scanning lidar are p...

Norman B. Nielsen; Edward E. Uthe…

1997-01-01T23:59:59.000Z

303

Three-dimensional scanning confocal laser microscope  

DOE Patents [OSTI]

A confocal microscope for generating an image of a sample includes a first scanning element for scanning a light beam along a first axis, and a second scanning element for scanning the light beam at a predetermined amplitude along a second axis perpendicular to the first axis. A third scanning element scans the light beam at a predetermined amplitude along a third axis perpendicular to an imaging plane defined by the first and second axes. The second and third scanning element are synchronized to scan at the same frequency. The second and third predetermined amplitudes are percentages of their maximum amplitudes. A selector determines the second and third predetermined amplitudes such that the sum of the percentages is equal to one-hundred percent.

Anderson, R. Rox (Lexington, MA); Webb, Robert H. (Lincoln, MA); Rajadhyaksha, Milind (Charlestown, MA)

1999-01-01T23:59:59.000Z

304

Scan Energy AS | Open Energy Information  

Open Energy Info (EERE)

Scan Energy AS Jump to: navigation, search Name: Scan Energy AS Place: Dybvad, Denmark Zip: DK-9352 Sector: Solar, Wind energy Product: Denmark-based solar and wind power project...

305

The X-ray microscopy beamline UE46-PGM2 at BESSY  

SciTech Connect (OSTI)

The Max Planck Institute for Metal Physics in Stuttgart and the Helmholtz Center Berlin operate a soft X-ray microscopy beamline at the storage ring BESSY II. A collimated PGM serves as monochromator for a scanning X-ray microscope and a full field X-ray microscope at the helical undulator UE46. The selection between both instruments is accomplished via two switchable focusing mirrors. The scanning microscope (SM) is based on the ALS STXM microscope and fabricated by the ACCEL company. The full field microscope (FFM) is currently in operation at the U41-SGM beamline and will be relocated to its final location this year.

Follath, R.; Schmidt, J. S. [Helmholtz-Center Berlin, Albert-Einstein-Strasse 15, 12489 Berlin (Germany); Weigand, M. [Max Planck Institute for Metals Research, Heisenbergstrasse 3, 70569 Stuttgart (Germany); Fauth, K. [University Erlangen, Experimental Physics 4, Am Hubland, 97074 Wuerzburg (Germany)

2010-06-23T23:59:59.000Z

306

Scanning electrochemical microscope characterization of thin film combinatorial libraries for fuel cell electrode applications  

Science Journals Connector (OSTI)

Pt–Ru combinatorial libraries of potential fuel cell anode catalysts are formed by sequential sputter deposition through masks onto Si wafers. Scanning electrochemical microscopy (SECM) is employed for characterization of electrocatalytic activity. Aspects of using a scanning electrochemical microscope for characterization of an array of thin film fuel cell electrode materials are discussed. It is shown that in applying SECM to library characterization, careful attention must be paid to thin film annealing, specimen topography and tip degradation in order to realize meaningful results. Results from a Pt–Ru thin film library reveal the most active members near the 50 Pt/50 Ru composition.

M Black; J Cooper; P McGinn

2005-01-01T23:59:59.000Z

307

Microscopy charges ahead | Argonne National Laboratory  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Microscopy charges ahead By Jared Sagoff * May 28, 2014 Tweet EmailPrint ARGONNE, Ill. - Ferroelectric materials - substances in which there is a slight and reversible shift of...

308

Journal of Magnetism and Magnetic Materials 286 (2005) 324328 Light-free magnetic resonance force microscopy for studies of  

E-Print Network [OSTI]

Journal of Magnetism and Magnetic Materials 286 (2005) 324­328 Light-free magnetic resonance force for Physical Sciences, College Park, MD, USA Available online 4 November 2004 Abstract Magnetic resonance force microscopy is a scanned probe technique capable of three-dimensional magnetic resonance imaging. Its

309

Nonlinear Dark-Field Microscopy Hayk Harutyunyan,  

E-Print Network [OSTI]

/20/2010 Published on Web: 11/16/2010 FIGURE 1. Illustration of the nonlinear dark-field imaging method. Two incidentNonlinear Dark-Field Microscopy Hayk Harutyunyan, Stefano Palomba, Jan Renger, Romain Quidant Dark-field microscopy is a background-free imaging method that provides high sensitivity and a large

Novotny, Lukas

310

Faculty Position in Materials Electron Microscopy  

E-Print Network [OSTI]

Faculty Position in Materials Electron Microscopy at the Ecole Polytechnique Fédérale de Lausanne in electron microscopy of materials within its Institute of Materials. We seek exceptional individuals who community. Top-level applications are invited from candidates at the cutting edge of electron microscopic

Candea, George

311

Multiphoton microscopy with near infrared contrast  

E-Print Network [OSTI]

Multiphoton microscopy with near infrared contrast agents Siavash Yazdanfar,a, * Chulmin Joo,a Chun limited to the visible spectrum. We introduce a paradigm for MPM of near-infrared NIR fluorescent Engineers. DOI: 10.1117/1.3420209 Keywords: two-photon microscopy; ultrafast fiber lasers; near-infrared

Larson-Prior, Linda

312

Imaging - Clearer brain scans ... | ornl.gov  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Imaging - Clearer brain scans ... A clever signal noise reduction strategy developed by a team that includes Oak Ridge National Laboratory's Ben Lawrie could dramatically improve...

313

Differential Scanning Microcalorimetry of Intrinsically Disordered Proteins  

Science Journals Connector (OSTI)

Ultrasensitive differential scanning calorimetry (DSC) is an indispensable thermophysical technique enabling to get direct information on enthalpies accompanying heating/cooling of dilute biopolymer solutions. Th...

Sergei E. Permyakov

2012-01-01T23:59:59.000Z

314

City of College Station's Thermographic Mobile Scan  

E-Print Network [OSTI]

During the first quarter of 1986, the City of College Station conducted a thermographic mobile scan of the entire city. A thermographic mobile scan is a process by which heat loss/heat gain data is accumulated by a vehicle traveling the city...

Shear, C. K.

1986-01-01T23:59:59.000Z

315

Dark Field Microscopy for Analytical Laboratory Courses  

Science Journals Connector (OSTI)

An innovative and inexpensive optical microscopy experiment for a quantitative analysis or an instrumental analysis chemistry course is described. The students have hands-on experience with a dark field microscope and investigate the wavelength dependence ...

Ashley E. Augspurger; Anthony S. Stender; Kyle Marchuk; Thomas J. Greenbowe; Ning Fang

2014-05-01T23:59:59.000Z

316

Photon tunnelling microscopy of polyethylene single crystals  

E-Print Network [OSTI]

Photon tunnelling microscopy of polyethylene single crystals Mohan Srinivasarao* and Richard S:photon tunnellingmicroscopy;single crystals; polyethylene) INTRODUCTION The study of morphology of polymers is an area

Srinivasarao, Mohan

317

Subwavelength optical microscopy in the far field  

E-Print Network [OSTI]

We present a procedure for subwavelength optical microscopy. The identical atoms are distributed on a plane and shined with a standing wave. We rotate the plane to different angles and record the resonant fluorescence spectra in the far field, from...

Sun, Qingqing; Al-Amri, M.; Scully, Marlan O.; Zubairy, M. Suhail.

2011-01-01T23:59:59.000Z

318

The Scanning Theremin Microscope: A Model Scanning Probe Instrument for Hands-On Activities  

Science Journals Connector (OSTI)

(9, 10) However, we decided upon a different approach and worked with scanning probe principles to create a large-scale scanning device, the scanning theremin microscope (SThM). ... The simplest mode of scanning is to move the pantograph to scan the probe across the surface at a fixed height, listening for changes in pitch. ... We present a cascade-based computation scheme that has all of the devices and interconnects required for the one-time computation of an arbitrary logic function. ...

Rebecca C. Quardokus; Natalie A. Wasio; S. Alex Kandel

2013-12-20T23:59:59.000Z

319

Imaging of Fluorine and Boron from Fluorinated Boronophenylalanine in the Same Cell at Organelle Resolution by Correlative Ion Microscopy and Confocal Laser Scanning Microscopy  

Science Journals Connector (OSTI)

...J. A. Quantitative imaging and microlocalization of boron-10 in brain tumors and infiltrating tumor cells by SIMS ion...R. Quantitative subcellular dynamic SIMS imaging of boron-10 and boron-11 isotopes in the same cell delivered by...

Subhash Chandra; George W. Kabalka; Daniel R. Lorey II; Duane R. Smith; Jeffrey A. Coderre

2002-08-01T23:59:59.000Z

320

In-situ Transmission Electron Microscopy and Spectroscopy Studies...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Transmission Electron Microscopy and Spectroscopy Studies of Interfaces in Li-ion Batteries: Challenges and In-situ Transmission Electron Microscopy and Spectroscopy Studies of...

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

Ultra-High Resolution Electron Microscopy for Catalyst Characterizatio...  

Broader source: Energy.gov (indexed) [DOE]

Ultra-High Resolution Electron Microscopy for Catalyst Characterization Ultra-High Resolution Electron Microscopy for Catalyst Characterization 2011 DOE Hydrogen and Fuel Cells...

322

Ultra-high Resolution Electron Microscopy for Catalyst Characterizatio...  

Broader source: Energy.gov (indexed) [DOE]

high Resolution Electron Microscopy for Catalyst Characterization Ultra-high Resolution Electron Microscopy for Catalyst Characterization 2009 DOE Hydrogen Program and Vehicle...

323

Ultra-High Resolution Electron Microscopy for Catalyst Characterizatio...  

Broader source: Energy.gov (indexed) [DOE]

High Resolution Electron Microscopy for Catalyst Characterization Ultra-High Resolution Electron Microscopy for Catalyst Characterization 2010 DOE Vehicle Technologies and Hydrogen...

324

Variable Temperature Scanning Probe Microscope | EMSL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

EMSL's ultra-high vacuum, variable-temperature scanning probe microscope system, or UHV VT SPM, is a state-of-the-art surface science tool comprising multiple complementary...

325

String Scanning in the Icon Programming Language  

Science Journals Connector (OSTI)

...Article String Scanning in the Icon Programming Language R. E. Griswold * Department of Computer Science, The University...general-purpose programming language and describes how they have been introduced in the Icon programming language....

R. E. Griswold

1990-01-01T23:59:59.000Z

326

Transmission Electron Microscope and Scanning Electron Microscopes -  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Facilities > Transmission Electron Facilities > Transmission Electron Microscope and Scanning Electron Microscopes FACILITIES Transmission Electron Microscope and Scanning Electron Microscopes Overview Other Facilities Work with Argonne Contact us For Employees Site Map Help Join us on Facebook Follow us on Twitter NE on Flickr Transmission Electron Microscope and Scanning Electron Microscopes The research activities of the Corrosion and Mechanics of Materials Section are supported by complete metallography/sample preparation rooms equipped with several optical and electron microscopes: a Transmission Electron Microscope and two Scanning Electron Microscopes. Bookmark and Share Transmission electron microscope (TEM) Detail of JEOL 100CXII TEM Figure 1: Detail of JEOL 100CXII TEM. Click on image to view larger image.

327

Atom chip microscopy: A novel probe for strongly correlated materials  

SciTech Connect (OSTI)

Improved measurements of strongly correlated systems will enable the predicative design of the next generation of supermaterials. In this program, we are harnessing recent advances in the quantum manipulation of ultracold atomic gases to expand our ability to probe these technologically important materials in heretofore unexplored regions of temperature, resolution, and sensitivity parameter space. We are working to demonstrate the use of atom chips to enable single-shot, large area detection of magnetic flux at the 10^-7 flux quantum level and below. By harnessing the extreme sensitivity of atomic clocks and Bose-Einstein condensates (BECs) to external perturbations, the cryogenic atom chip technology developed here will provide a magnetic flux detection capability that surpasses other techniques---such as scanning SQUIDs---by a factor of 10--1000. We are testing the utility of this technique by using rubidium BECs to image the magnetic fields emanating from charge transport and magnetic domain percolation in strongly correlated materials as they undergo temperature-tuned metal--to--insulator phase transitions. Cryogenic atom chip microscopy introduces three very important features to the toolbox of high-resolution, strongly correlated material microscopy: simultaneous detection of magnetic and electric fields (down to the sub-single electron charge level); no invasive large magnetic fields or gradients; simultaneous micro- and macroscopic spatial resolution; freedom from 1/f flicker noise at low frequencies; and, perhaps most importantly, the complete decoupling of probe and sample temperatures. The first of these features will play an important role in studying the interplay between magnetic and electric domain structure. The last two are crucial for low frequency magnetic noise detection in, e.g., the cuprate pseudogap region and for precision measurements of transport in the high temperature, technologically relevant regime inaccessible to other techniques based on superconducting scanning probes. In periods 1--3 of this grant, which we now close at the University of Illinois at Urbana-Champaign and restart at Stanford University where our new lab is being built, we have demonstrated the ability to rapidly create Rb BECs and trap them within microns of a surface ina cryostat. Period 4 of this grant, to be performed at Stanford, will demonstrate the feasibility of using atom chips with a BEC to image transport features on a cryogenically cooled surface. Successful demonstration, in future funding cycles, will lead directly to the use of system for studies of transport in exotic and technologically relevant materials such as cuprate superconductors and topological insulators.

Lev, Benjamin L

2011-11-03T23:59:59.000Z

328

Spatial resolution in vector potential photoelectron microscopy  

SciTech Connect (OSTI)

The experimental spatial resolution of vector potential photoelectron microscopy is found to be much higher than expected because of the cancellation of one of the expected contributions to the point spread function. We present a new calculation of the spatial resolution with support from finite element ray tracing, and experimental results.

Browning, R. [R. Browning Consultants, 1 Barnhart Place, Shoreham, New York 11786 (United States)] [R. Browning Consultants, 1 Barnhart Place, Shoreham, New York 11786 (United States)

2014-03-15T23:59:59.000Z

329

Physical sectioning in 3D biological microscopy  

E-Print Network [OSTI]

developed in the Brain Networks Laboratory at Texas A&M University, has been used for the purpose of this study. However, the modes of characterizing chatter and its measurement are equally applicable to all current variants of 3D biological microscopy using...

Guntupalli, Jyothi Swaroop

2008-10-10T23:59:59.000Z

330

Physical sectioning in 3D biological microscopy  

E-Print Network [OSTI]

developed in the Brain Networks Laboratory at Texas A&M University, has been used for the purpose of this study. However, the modes of characterizing chatter and its measurement are equally applicable to all current variants of 3D biological microscopy using...

Guntupalli, Jyothi Swaroop

2009-05-15T23:59:59.000Z

331

Feature Article NEXAFS microscopy and resonant scattering  

E-Print Network [OSTI]

and conven- tional electron, X-ray and neutron scattering. We provide an overview of these synchrotron based and derivative struc- tures, ranging from spectroscopy to mechanical analysis and neutron scattering [9,10]. SomeFeature Article NEXAFS microscopy and resonant scattering: Composition and orientation probed

Hitchcock, Adam P.

332

Argonne CNM Highlight: Light Scattering by Nanoparticles  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Light Scattering by Nanoparticles: Understanding Confinement of Light for Nanophotonics Applications through Near-Field Scanning Optical Microscopy Light Scattering by Nanoparticles: Understanding Confinement of Light for Nanophotonics Applications through Near-Field Scanning Optical Microscopy Schematic of the apertureless near-field optical microscope Schematic of the apertureless near-field optical microscope. The optical scattering from the AFM probe tip provides the subdiffraction-limited optical field information. One of the motivations of nanoscience is to achieve sufficient control over photon propagation in nanostructures so as to effectively replace the electron with the photon in all-optical integrated circuits. The much greater speed and bandwidth of light pulses versus electrons promise new capabilities and size reduction of photon based “electronics.” Arrays of metal nanoparticles are currently considered a leading candidate for photon

333

Variable Temperature Ultra-High Vacuum Scanning Tunneling Microscope...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Vacuum Scanning Tunneling Microscope The Omicron variable temperature ultra-high vacuum (UHV) scanning tunneling microscope (VTSTM) is designed to study the structure of both clean...

334

H2Scan LLC | Open Energy Information  

Open Energy Info (EERE)

H2Scan LLC H2Scan LLC Jump to: navigation, search Name H2Scan LLC Place Valencia, California Zip 91355 Sector Hydro, Hydrogen Product Hydrogen specific sensing systems, uniquely able to detect hydrogen against virtually any background gases. Coordinates 39.468791°, -0.376913° Loading map... {"minzoom":false,"mappingservice":"googlemaps3","type":"ROADMAP","zoom":14,"types":["ROADMAP","SATELLITE","HYBRID","TERRAIN"],"geoservice":"google","maxzoom":false,"width":"600px","height":"350px","centre":false,"title":"","label":"","icon":"","visitedicon":"","lines":[],"polygons":[],"circles":[],"rectangles":[],"copycoords":false,"static":false,"wmsoverlay":"","layers":[],"controls":["pan","zoom","type","scale","streetview"],"zoomstyle":"DEFAULT","typestyle":"DEFAULT","autoinfowindows":false,"kml":[],"gkml":[],"fusiontables":[],"resizable":false,"tilt":0,"kmlrezoom":false,"poi":true,"imageoverlays":[],"markercluster":false,"searchmarkers":"","locations":[{"text":"","title":"","link":null,"lat":39.468791,"lon":-0.376913,"alt":0,"address":"","icon":"","group":"","inlineLabel":"","visitedicon":""}]}

335

WorldScan | Open Energy Information  

Open Energy Info (EERE)

WorldScan WorldScan Jump to: navigation, search LEDSGP green logo.png FIND MORE DIA TOOLS This tool is part of the Development Impacts Assessment (DIA) Toolkit from the LEDS Global Partnership. Tool Summary LAUNCH TOOL Name: WorldScan Agency/Company /Organization: Netherlands Bureau for Economic Policy Analysis (CPB) Sector: Climate, Energy Complexity/Ease of Use: Moderate Website: www.gtap.agecon.purdue.edu/resources/res_display.asp?RecordID=1923 Related Tools Marginal Abatement Cost Tool (MACTool) Greenhouse Gas and Air Pollution Interactions and Synergies (GAINS) Gold Standard Program Model ... further results A recursively dynamic general equilibrium model for the world economy, developed for the analysis of long-term issues in international economics; used both as a tool to construct long-term scenarios and as an instrument

336

Exploration, Registration, and Analysis of High-Throughput 3D Microscopy Data from the Knife-Edge Scanning Microscope  

E-Print Network [OSTI]

connectivity analysis; (2) the size of the uncompressed KESM data exceeds a few terabytes and to compare and combine with other data sets from different imaging modalities, the KESM data must be registered to a standard coordinate space; and (3) quantitative...

Sung, Chul

2014-04-25T23:59:59.000Z

337

Growth of High Aspect Ratio Nanometer-Scale Magnets with Chemical Vapor Deposition and Scanning Tunneling Microscopy  

Science Journals Connector (OSTI)

...50 pA). A contamination coating around a denser Fig. 4...deposit with the contamination coating is thus stable against oxidation...of nanoscale filaments and thin film nucleation and growth theory...Instruments-ARIS 5100 UHV-STM. 13. An optical microscope provides a view...

Andrew D. Kent; Thomas M. Shaw; Stephan von Molnár; David D. Awschalom

1993-11-19T23:59:59.000Z

338

A scanning tunneling microscopy study of atomic-scale clustering in InAsP/InP heterostructures  

E-Print Network [OSTI]

Deer Creek Road, MS 26M-7, Palo Alto, CA 94304. that facilitates population inversion.7 Furthermore, the large conduction-band offset in this material system8 ( Ec

Yu, Edward T.

339

Shearforce-Based Constant-Distance Scanning Electrochemical Microscopy as Fabrication Tool for Needle-Type Carbon-Fiber Nanoelectrodes  

Science Journals Connector (OSTI)

Coating the stems but not the end of the tips of the tapered structures with anodic electrodeposition paint was the strategy for limiting the bare carbon to the foremost end and restricting a feasible voltammetry current response to exactly this section. ... The vibrating carbon fiber tip was fixed in space and the electrochemical cell for the EDP deposition was moved through a stage of three joined stepper motors (SPI Robot Systems, Oppenheim, Germany) with a nominal resolution in x-, y-, and z-direction of 10 nm per microstep. ... Furthermore, electrodeposition paints are com. ...

Emad Mohamed Hussien; Wolfgang Schuhmann; Albert Schulte

2010-06-09T23:59:59.000Z

340

A scanning electron microscopy study of diseased root surfaces conditioned with EDTA gel plus Cetavlon after scaling and root planing  

Science Journals Connector (OSTI)

......analysis The results from the semi-quantitative analysis were evaluated using a nonparametric analysis of variance (Kruskal-Wallis test) followed by a Dunn's post test to compare all pairs of data. Results In control groups 1 and 3, which......

Walter Martins Júnior; Andiara De Rossi; Ricardo Samih Georges Abi Rached; Marcos Antonio Rossi

2011-04-01T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Preparation of TiO2(110)-(1x1) Surface via UHV Cleavage: An scanning tunneling microscopy study  

SciTech Connect (OSTI)

TiO2(110) surface was successfully prepared in-situ by UHV cleaving of a commercial TiO2 crystal.. STM imaging revealed atomically flat more than 1 ?m wide terraces with (110) orientation separated by steps running in [001] direction, with very low kink density. Atomically resolved STM images show periodicity in the [001] and [ ] directions with the unit cell parameters measured to ~3 Å and 6.5 Å respectively which are closed to the expected values of bulk terminated (1x1) surface.

Bondarchuk, Olexsandr; Lyubinetsky, Igor

2007-11-26T23:59:59.000Z

342

In situ crystallization of barium zinc silicate in glass-ceramics studied by hot stage scanning electron microscopy  

Science Journals Connector (OSTI)

......Glasses and glass ceramics with blue, green and red photoluminescence. Phys. Chem...implications for melt inclusion analysis. Am. Mineral. (2006) 91:667-679. doi:10...formation of gold nanoparticles in soda lime silicate glass: suppressed Ostwald ripening......

Christian Bocker; Marlen Michaelis; Christian Rüssel

2012-12-01T23:59:59.000Z

343

Measurement of vibrational spectrum of liquid using monochromated scanning transmission electron microscopy–electron energy loss spectroscopy  

Science Journals Connector (OSTI)

......application to lithium-ion battery and hence has been well studied...Atom-by-atom spectroscopy at graphene edge. Nature (2010) 468...temperature molten salts as lithium battery electrolyte. Electrochim...additive systems as lithium-ion battery ionic liquid electrolytes......

Tomohiro Miyata; Mao Fukuyama; Akihide Hibara; Eiji Okunishi; Masaki Mukai; Teruyasu Mizoguchi

2014-10-01T23:59:59.000Z

344

Three- to two-dimensional transition in electrostatic screening of point charges at semiconductor surfaces studied by scanning tunneling microscopy  

Science Journals Connector (OSTI)

The electrostatic screening of localized electric charges on semiconductor surfaces is investigated quantitatively by statistically analyzing the spatial distribution of thermally formed positively charged anion surface vacancies on GaAs and InP(110) surfaces. Two screening regimes are found: at low vacancy concentrations the vacancy charges are found to be three-dimensionally screened by bulk charge carriers. The corresponding screening length, which increases strongly with decreasing carrier concentration, is best described by the classical bulk screening length evaluated with a surface dielectric constant. With increasing vacancy concentration at given bulk carrier concentration, a three- to two-dimensional screening transition occurs. At high vacancy concentrations, the screening is found to be governed by charge carriers located in a two-dimensional surface vacancy defect band, which is partially filled due to the vacancy-induced surface band bending.

A. Laubsch, K. Urban, and Ph. Ebert

2009-12-14T23:59:59.000Z

345

High-energy-resolution monochromator for aberration-corrected scanning transmission electron microscopy/electron energy-loss spectroscopy  

Science Journals Connector (OSTI)

...equal to the beam current per unit area per unit solid angle per unit energy interval, CFE electron sources with their...Monochromated, spatially resolved electron energy-loss spectroscopic measurements of gold nanoparticles in the plasmon range...

2009-01-01T23:59:59.000Z

346

High-energy-resolution monochromator for aberration-corrected scanning transmission electron microscopy/electron energy-loss spectroscopy  

Science Journals Connector (OSTI)

...R. F. 1996 Electron energy-loss spectroscopy in...microscope, 2nd edn. New York, NYPlenum. Egerton...Transmission electron energy loss spectrometry in materials...energy-gain spectroscopy. New J. Phys. 10, 1367-2630...

2009-01-01T23:59:59.000Z

347

High resolution in situ magneto-optic Kerr effect and scanning tunneling microscopy setup with all optical components in UHV  

E-Print Network [OSTI]

optical components in UHV A. Lehnert, P. Buluschek, N. Weiss, J. Giesecke, M. Treier, S. Rusponi, and H UHV chamber. In addition, sample preparation, growth of nanostructures or films, as well

Brune, Harald

348

Thin Film Morphology Control by Mechanical, Electronic and Chemical Interactions: a Scanning Tunneling Microscopy and Photoelectron Spectroscopy Study  

E-Print Network [OSTI]

17 UHV System and2-6 Schematic diagram of a my UHV-LT STM design in both top? ? . STM Instrumentation UHV System and Cyrostat In many

Sun, Dezheng

2012-01-01T23:59:59.000Z

349

Classification of Multiple Types of Organic Carbon Composition in Atmospheric Particles by Scanning Transmission X-Ray Microscopy Analysis  

E-Print Network [OSTI]

al. , 2005), and biomass combustion (Braun, 2005; Tivanskigenerated from biomass (wood) combustion, however, it is

Takahama, S.

2008-01-01T23:59:59.000Z

350

LIVE SCAN FINGERPRINTING PROCESS AND RESPONSIBILITIES  

E-Print Network [OSTI]

LIVE SCAN FINGERPRINTING PROCESS AND RESPONSIBILITIES HUMAN RESOURCES Workforce Planning | One of recruitment) to your Workforce Planning Analyst. Notify Finalists Department must notify finalists of the Live. Workforce Planning Analyst will make available at the Human Resources reception desk, the appropriate number

Eirinaki, Magdalini

351

Department of Health I. Internal Scan  

E-Print Network [OSTI]

and cholesterol; and working with consumers, health plans and providers to improve the quality of care and other non- institutional settings. CURRRENT PLANS: The Division of Health care Financing has been takingDepartment of Health I. Internal Scan There are a variety of areas that will be impacted

Tipple, Brett

352

Student Charter Scan the QR-code  

E-Print Network [OSTI]

Student Charter 2013/2014 Scan the QR-code to obtain the online version. TechnischeUniversiteitDelft #12;#12;Student Charter 2013/2014 Delft University of Technology This is the English version of the Student Charter of Delft University of Technology, published on the TU Delft website: www

353

Global registration of dynamic range scans for articulated model reconstruction  

Science Journals Connector (OSTI)

We present the articulated global registration algorithm to reconstruct articulated 3D models from dynamic range scan sequences. This new algorithm aligns multiple range scans simultaneously to reconstruct a full 3D model from the geometry of these scans. ... Keywords: Range scanning, animation reconstruction, articulated model, nonrigid registration

Will Chang; Matthias Zwicker

2011-05-01T23:59:59.000Z

354

New Developments in Transmission Electron Microscopy for Nanotechnology**  

E-Print Network [OSTI]

New Developments in Transmission Electron Microscopy for Nanotechnology** By Zhong Lin Wang* 1. Electron Microscopy and Nanotechnology Nanotechnology, as an international initiative for science manufacturing are the foundation of nanotechnology. Tracking the historical background of why nanotechnology

Wang, Zhong L.

355

Quantitative imaging of living cells by deep ultraviolet microscopy  

E-Print Network [OSTI]

Developments in light microscopy over the past three centuries have opened new windows into cell structure and function, yet many questions remain unanswered by current imaging approaches. Deep ultraviolet microscopy ...

Zeskind, Benjamin J

2006-01-01T23:59:59.000Z

356

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray...

357

Tomography and High-Resolution Electron Microscopy Study of Surfaces...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Tomography and High-Resolution Electron Microscopy Study of Surfaces and Porosity in a Plate-Like ?-Al2O3. Tomography and High-Resolution Electron Microscopy Study of...

358

TRANSMISSION ELECTRON MICROSCOPY OF WEAKLY DEFORMED ALKALI HALIDE CRYSTALS  

E-Print Network [OSTI]

377 TRANSMISSION ELECTRON MICROSCOPY OF WEAKLY DEFORMED ALKALI HALIDE CRYSTALS H. STRUNK Max'importance croissante du durcissement de la solution solide. Abstract. 2014 Transmission electron microscopy (TEM Abstracts 7j66 - 7 I' 1. Introduction. - It is only some years ago that transmission electron microscopy

Boyer, Edmond

359

Rapid Scan AERI Observations: Benefits and Analysis  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Rapid Scan AERI Observations: Benefits and Analysis Rapid Scan AERI Observations: Benefits and Analysis W. F. Feltz, D. D. Turner, R. O. Knuteson, and R. G. Dedecker Space Science and Engineering Center Cooperative Institute of Mesoscale Meteorological Studies University of Wisconsin-Madison Madison, Wisconsin D. D. Turner Pacific Northwest National Laboratory Richland, Washington Introduction The U.S. Department of Energy's (DOE's) Atmospheric Radiation Measurement (ARM) Program has funded the development of the atmospheric emitted radiance interferometer (AERI). This has led to a hardened, autonomous system that measures downwelling infrared (IR) radiance at high-spectral resolution. Seven AERI systems have been deployed around the world as part of the ARM Program. The initial goal of these instruments was to characterize the clear-sky IR emission from the atmosphere,

360

Circular zig-zag scan video format  

DOE Patents [OSTI]

A circular, ziz-zag scan for use with vidicon tubes. A sine wave is generated, rectified and its fourth root extracted. The fourth root, and its inverse, are used to generate horizontal ramp and sync signals. The fourth root is also used to generate a vertical sync signal, and the vertical sync signal, along with the horizontal sync signal, are used to generate the vertical ramp signal. Cathode blanking and preamplifier clamp signals are also obtained from the vertical sync signal.

Peterson, C. Glen (Los Alamos, NM); Simmons, Charles M. (Los Alamos, NM)

1992-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

Mapping Ionic Currents and Reactivity on the Nanoscale: Electrochemical Strain Microscopy  

SciTech Connect (OSTI)

Solid-state electrochemical processes in oxides underpin a broad spectrum of energy and information storage devices, ranging from Li-ion and Li-air batteries, to solid oxide fuel cells (SOFC) to electroresistive and memristive systems. These functionalities are controlled by the bias-driven diffusive and electromigration transport of mobile ionic species, as well as intricate a set of electrochemical and defect-controlled reactions at interfaces and in bulk. Despite the wealth of device-level and atomistic studies, little is known on the mesoscopic mechanisms of ion diffusion and electronic transport on the level of grain clusters, individual grains, and extended defects. The development of the capability for probing ion transport on the nanometer scale is a key to deciphering complex interplay between structure, functionality, and performance in these systems. Here we introduce Electrochemical Strain Microscopy, a scanning probe microscopy technique based on strong strain-bias coupling in the systems in which local ion concentrations are changed by electrical fields. The imaging capability, as well as time- and voltage spectroscopies analogous to traditional current based electrochemical characterization methods are developed. The reversible intercalation of Li and mapping electrochemical activity in LiCoO2 is demonstrated, illustrating higher Li diffusivity at non-basal planes and grain boundaries. In Si-anode device structure, the direct mapping of Li diffusion at extended defects and evolution of Li-activity with charge state is explored. The electrical field-dependence of Li mobility is studied to determine the critical bias required for the onset of electrochemical transformation, allowing reaction and diffusion processes in the battery system to be separated at each location. Finally, the applicability of ESM for probing oxygen vacancy diffusion and oxygen reduction/evolution reactions is illustrated, and the high resolution ESM maps are correlated with aberration corrected scanning transmission electron microscopy imaging. The future potential for deciphering mechanisms of electrochemical transformations on an atomically-defined single-defect level is discussed.

Kalinin, S.V. (Center for Nanophase Materials Sciences, ORNL) [Center for Nanophase Materials Sciences, ORNL

2010-10-19T23:59:59.000Z

362

Fast electron microscopy via compressive sensing  

DOE Patents [OSTI]

Various technologies described herein pertain to compressive sensing electron microscopy. A compressive sensing electron microscope includes a multi-beam generator and a detector. The multi-beam generator emits a sequence of electron patterns over time. Each of the electron patterns can include a plurality of electron beams, where the plurality of electron beams is configured to impart a spatially varying electron density on a sample. Further, the spatially varying electron density varies between each of the electron patterns in the sequence. Moreover, the detector collects signals respectively corresponding to interactions between the sample and each of the electron patterns in the sequence.

Larson, Kurt W; Anderson, Hyrum S; Wheeler, Jason W

2014-12-09T23:59:59.000Z

363

High-throughput full-automatic synchrotron-based tomographic microscopy  

SciTech Connect (OSTI)

At the TOMCAT (TOmographic Microscopy and Coherent rAdiology experimenTs) beamline of the Swiss Light Source with an energy range of 8-45 keV and voxel size from 0.37 {micro}m to 7.4 {micro}m, full tomographic datasets are typically acquired in 5 to 10 min. To exploit the speed of the system and enable high-throughput studies to be performed in a fully automatic manner, a package of automation tools has been developed. The samples are automatically exchanged, aligned, moved to the correct region of interest, and scanned. This task is accomplished through the coordination of Python scripts, a robot-based sample-exchange system, sample positioning motors and a CCD camera. The tools are suited for any samples that can be mounted on a standard SEM stub, and require no specific environmental conditions. Up to 60 samples can be analyzed at a time without user intervention. The throughput of the system is dependent on resolution, energy and sample size, but rates of four samples per hour have been achieved with 0.74 {micro}m voxel size at 17.5 keV. The maximum intervention-free scanning time is theoretically unlimited, and in practice experiments have been running unattended as long as 53 h (the average beam time allocation at TOMCAT is 48 h per user). The system is the first fully automated high-throughput tomography station: mounting samples, finding regions of interest, scanning and reconstructing can be performed without user intervention. The system also includes many features which accelerate and simplify the process of tomographic microscopy.

Mader, Kevin; Marone, Federica; Hintermüller, Christoph; Mikuljan, Gordan; Isenegger, Andreas; Stampanoni, Marco (SLS)

2011-08-16T23:59:59.000Z

364

Circular zig-zag scan video format  

DOE Patents [OSTI]

A circular, ziz-zag scan for use with vidicon tubes is disclosed. A sine wave is generated, rectified and its fourth root extracted. The fourth root, and its inverse, are used to generate horizontal ramp and sync signals. The fourth root is also used to generate a vertical sync signal, and the vertical sync signal, along with the horizontal sync signal, are used to generate the vertical ramp signal. Cathode blanking and preamplifier clamp signals are also obtained from the vertical sync signal. 10 figs.

Peterson, C.G.; Simmons, C.M.

1992-06-09T23:59:59.000Z

365

NCEM National Center for Electron Microscopy: Staff  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Staff Staff Scientific Technical / Admin. Postdoctoral and Visitors Uli Dahmen, Head Jane Cavlina / Administrator Abhay Gautam Christian Kisielowski John Turner Helmut Poppa Andrew Minor ChengYu Song Frances Allen Andreas Schmid Marissa Libbee Tamara Radetic Peter Ercius Karen Bustillo Haimei Zheng Jim Ciston Alpha N'Diaye Colin Ophus Gong Chen Burak Ozdol Velimir Radmilovic Sara Kiani Hua Guo Christian Liebscher Josh Kacher Chris Nelson Xiuguang Jin Qian Yu Mary Scott Search the LBNL directory services page for other LBNL staff. Scientific Staff Uli Dahmen udahmen@lbl.gov (510) 486-4627 Ulrich Dahmen is Director of the National Center for Electron Microscopy. His current research interests include embedded nanostructures and interfaces in materials. Embedded nanostructures. Size- and shape-dependence of structural phase

366

A System Level Boundary Scan Controller Board for VME Applications  

Science Journals Connector (OSTI)

In this article an application of boundary scan test at system level is analyzed. The objective is met through the description of the design and implementation options of a VME boundary scan controller board prototype and the corresponding software. ... Keywords: ATPG, IEEE 1149.1 boundary scan test, board level test and system level test

Nuno Cardoso; Carlos Beltrán Almeida; José Carlos Da Silva

2001-06-01T23:59:59.000Z

367

Final Scientific/Technical Report for DE-FG02-07ER64500 Study of Lignocellulosic Material Degradation with CARS Microscopy  

SciTech Connect (OSTI)

The program of research undertaken by our Harvard group, in collaboration with Dr. Ding at the National Renewable Energy Laboratory (NREL) in Golden, CO, seeks to introduce, validate and apply a new analytical technique to study the conversion of lignocellulosic biomass into ethanol. This conversion process has been the subject of intense interest over the past few years because of its potential to provide a clean, renewable source of energy to meet increasing global demand. During the funding period, we have clearly demonstrated visualization of lignin and cellulose using intrinsic vibrational contrast with simulated Raman scattering (SRS) microscopy, developed at Harvard. Our approach offers high spatial resolution and time resolution that is sufficient to capture the kinetics of a pre?treatment process. This is reflected by the publications listed below, as well as the use of SRS microscopy at NREL as a routine analysis tool for research on lignocellulosic biomass. In our original proposal, we envisioned moving to near?field CARS imaging in order to perform chemical mapping at the nanoscale. However, given the dramatic progress made by our group in SRS imaging, we concentrated our efforts on using multi?component SRS (lignin, cellulose, lipid, water, protein, deuterated metabolites, etc.) to quantitatively understand the spatially dispersed kinetics in a variety of plant samples under a variety of conditions. In addition, we built a next generation laser system based on fiber laser technology that allowed rugged and portable instrumentation for SRS microscopy. We also pursued new imaging approaches to improve the acquisition speed of SRS imaging of lignocellulose without sacrificing signal?to?noise ratio. This allowed us to image larger volumes of tissue with higher time resolution to get a more comprehensive picture of the heterogeneity of this chemical process from the submicron up to the centimeter scale.

Xie, Xiaoliang Sunney; Ding, Shi-You

2013-09-30T23:59:59.000Z

368

Scanning ARM Cloud Radars Part I: Operational Sampling Strategies  

SciTech Connect (OSTI)

Probing clouds in three-dimensions has never been done with scanning millimeter-wavelength (cloud) radars in a continuous operating environment. The acquisition of scanning cloud radars by the Atmospheric Radiation Measurement (ARM) program and research institutions around the world generate the need for developing operational scan strategies for cloud radars. Here, the first generation of sampling strategies for the Scanning ARM Cloud Radars (SACRs) is discussed. These scan strategies are designed to address the scientific objectives of the ARM program, however, they introduce an initial framework for operational scanning cloud radars. While the weather community uses scan strategies that are based on a sequence of scans at constant elevations, the SACRs scan strategies are based on a sequence of scans at constant azimuth. This is attributed to the cloud properties that are vastly different for rain and snow shafts that are the primary target of precipitation radars. A “cloud surveillance” scan strategy is introduced (HS-RHI) based on a sequence of horizon-to-horizon Range Height Indicator (RHI) scans that sample the hemispherical sky (HS). The HS-RHI scan strategy is repeated every 30 min to provide a static view of the cloud conditions around the SACR location. Between HS-RHI scan strategies other scan strategies are introduced depending on the cloud conditions. The SACRs are pointing vertically in the case of measurable precipitation at the ground. The radar reflectivities are corrected for water vapor attenuation and non-meteorological detection are removed. A hydrometeor detection mask is introduced based on the difference of cloud and noise statistics is discussed.

Kollias, Pavlos; Bharadwaj, Nitin; Widener, Kevin B.; Jo, Ieng; Johnson, Karen

2014-03-01T23:59:59.000Z

369

In-Situ Electron Microscopy of Electrical Energy Storage Materials...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

of Electrical Energy Storage Materials In-Situ Electron Microscopy of Electrical Energy Storage Materials 2011 DOE Hydrogen and Fuel Cells Program, and Vehicle Technologies...

370

In-Situ Electron Microscopy of Electrical Energy Storage Materials...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

of Electrical Energy Storage Materials In-Situ Electron Microscopy of Electrical Energy Storage Materials 2012 DOE Hydrogen and Fuel Cells Program and Vehicle Technologies...

371

Copy of Bound Original For Scanning  

Office of Legacy Management (LM)

Copy of Bound Original Copy of Bound Original For Scanning Document # 1\1\ i g -b DOE/El/-0005/6 Formerly Utilized IVIEWAEC Site! Remedial Action Progrhn, F@diilogical Survey of the Seaway Industrial Par Tonawanda, New Yor May 197 Final Repel Prepared f U.S. Department of Enerc Assistant Secretary for Environme Division of Environmental Control Technolo Washington, D.C. 205, uric Contract No. W-7405-ENG- - - - Available from: ' : -. National Technical Information Service (NTIS) U.S. Department of Comnerce 5285 Port Royal Road Springfield, Virginia 22161 price: Printed Copy: $ 5.25 Microffche: $ 3.00 PREFACE This series of reports results from a program initiated in 1974 by the Atomic Energy Commission (AEC) for determination of the condition of sites formerly utilized by the Manhattan Engineering District &ED)

372

Damage potential characteristics of near-field earthquake motions  

SciTech Connect (OSTI)

In recent major earthquakes; i.e., 1994 Northridge earthquake in the US and 1995 Great Kansai earthquake in Japan, several close-distance strong ground motions have been obtained, which may be of significant interest to earthquake/structural engineers. The damage potential of those recently obtained ground motions is examined based on the nonlinear response analyses of various SDOF systems. For comparison purposes, the El Centro records from the 1940 Imperial Valley earthquake, as well as a set of artificial motions consistent with the R.G. 1.60 spectrum were also used. The engineering insights regarding the seismic design of structures are discussed based on a series of parametric studies.

Park, Y. [Brookhaven National Lab., Upton, NY (United States); Chokshi, N. [Nuclear Regulatory Commission, Washington, DC (United States)

1997-04-01T23:59:59.000Z

373

Heat Transfer between Two Nanoparticles Through Near Field Interaction  

Science Journals Connector (OSTI)

We introduce a thermal conductance by using the fluctuation-dissipation theorem to analyze the heat transfer between two nanoparticles separated by a submicron distance. Using either a molecular dynamics technique or a model based on the Coulomb interaction between fluctuating dipoles, we derive the thermal conductance. Both models agree for distances larger than a few diameters. For separation distances smaller than the particle diameter, we find a transition regime characterized by a thermal conductance larger than the contact conductance.

Gilberto Domingues; Sebastian Volz; Karl Joulain; Jean-Jacques Greffet

2005-03-02T23:59:59.000Z

374

NEAR-FIELD IMAGING OF INFINITE ROUGH SURFACES 1 ...  

E-Print Network [OSTI]

analytic solution for the direct scattering problem is derived from the method of ... mine the scattered field from the incident field and the differential equation governing the wave .... is the unit outward normal vector on S, given explicitly as ...... the periodicity of the solutions, we modified a simple mesh generator in MATLAB by.

2013-09-03T23:59:59.000Z

375

INVERSE MEDIUM SCATTERING PROBLEMS IN NEAR-FIELD ...  

E-Print Network [OSTI]

measured in the far-field zone as a function of the probe position. In TIRM, the sample is ... to be considered, thus defining an interface between two half-spaces

2007-05-08T23:59:59.000Z

376

Near-Field Imaging of Interior Cavities 1 Introduction  

E-Print Network [OSTI]

[14] NIST Digital Library of Mathematical Functions. http://dlmf.nist.gov/, Release ... [26] F. Zeng, F. Cakoni and J. Sun, An inverse electromagnetic scattering ...

2014-07-04T23:59:59.000Z

377

An electron microscopy study of the microstructure and microarchitecture of the Strombus gigas shell  

SciTech Connect (OSTI)

A scanning and transmission electron microscopy study is presented of the microstructure of the Strombus gigas shell. The hierarchical nature of this crossed-lamellar structure and the defect content of the mineral component are described. The mineral component consists of small single crystal grains of aragonite, the metastable orthorhombic polymorph of CaCO{sub 3}. The habit and morphology of the grains discussed here have not been determined previously. The observed habit and defect structure suggest that the organic matrix exerts a high degree of control over the crystal growth of the mineral phase and is responsible for the long range order in the microarhitecture. Electron beam heating of the mineral component leads to certain phase changes and these are discussed. 15 refs., 6 figs.

Rieke, P.C.; Laraia, V.J. (Pacific Northwest Lab., Richland, WA (USA)); Heuer, A.H. (Case Western Reserve Univ., Cleveland, OH (USA)); Aindow, M. (Ohio State Univ., Columbus, OH (USA))

1989-11-01T23:59:59.000Z

378

Spectral-domain phase microscopy with improved sensitivity using two-dimensional detector arrays  

SciTech Connect (OSTI)

In this work we demonstrate the use of two-dimensional detectors to improve the signal-to-noise ratio (SNR) and sensitivity in spectral-domain phase microscopy for subnanometer accuracy measurements. We show that an increase in SNR can be obtained, from 82 dB to 105 dB, using 150 pixel lines of a low-cost CCD camera as compared to a single line, to compute an averaged axial scan. In optimal mechanical conditions, phase stability as small as 92 {mu}rad, corresponding to 6 pm displacement accuracy, could be obtained. We also experimentally demonstrate the benefit of spatial-averaging in terms of the reduction of signal fading due to an axially moving sample. The applications of the improved system are illustrated by imaging live cells in culture.

Singh, K.; Dion, C.; Ozaki, T. [Centre de Recherche, Hopital Maisonneuve-Rosemont, Montreal, Quebec (Canada); Institut National de la Recherche Scientifique, Energie, Materiaux et Telecommunications, Varennes, Quebec (Canada); Lesk, M. R. [Centre de Recherche, Hopital Maisonneuve-Rosemont, Montreal, Quebec (Canada); Departement d'Ophtalmologie, Universite de Montreal, Montreal, Quebec (Canada); Costantino, S. [Centre de Recherche, Hopital Maisonneuve-Rosemont, Montreal, Quebec (Canada); Departement d'Ophtalmologie, Universite de Montreal, Montreal, Quebec (Canada); Institut de Genie Biomedical, Universite de Montreal, Montreal, Quebec (Canada)

2011-02-15T23:59:59.000Z

379

Hetero-epitaxial EuO interfaces studied by analytic electron microscopy  

SciTech Connect (OSTI)

With nearly complete spin polarization, the ferromagnetic semiconductor europium monoxide could enable next-generation spintronic devices by providing efficient ohmic spin injection into silicon. Spin injection is greatly affected by the quality of the interface between the injector and silicon. Here, we use atomic-resolution scanning transmission electron microscopy in conjunction with electron energy loss spectroscopy to directly image and chemically characterize a series of EuO|Si and EuO|YAlO{sub 3} interfaces fabricated using different growth conditions. We identify the presence of europium silicides and regions of disorder at the EuO|Si interfaces, imperfections that could significantly reduce spin injection efficiencies via spin-flip scattering.

Mundy, Julia A. [School of Applied and Engineering Physics, Cornell University, Ithaca, New York 14853 (United States); Hodash, Daniel; Melville, Alexander; Held, Rainer [Department of Materials Science and Engineering, Cornell University, Ithaca, New York 14853 (United States); Mairoser, Thomas; Schmehl, Andreas [Zentrum für Elektronische Korrelationen und Magnetismus, Universität Augsburg, Universitätsstraße 1, D-86159 Augsburg (Germany); Muller, David A.; Kourkoutis, Lena F. [School of Applied and Engineering Physics, Cornell University, Ithaca, New York 14853 (United States); Kavli Institute at Cornell for Nanoscale Science, Ithaca, New York 14853 (United States); Schlom, Darrell G. [Department of Materials Science and Engineering, Cornell University, Ithaca, New York 14853 (United States); Kavli Institute at Cornell for Nanoscale Science, Ithaca, New York 14853 (United States)

2014-03-03T23:59:59.000Z

380

Gordon Research Conferences  

Science Journals Connector (OSTI)

...properties and applications ofx-ray absorp-tion...Mechanisms of thin-film growth (Pauline...reactor models in CVD"; Eugene Irene...from liquids and thin-film surfaces...Near-field scanning optical microscopy...Low-temperature thin-film oxi-dation...John-son, "Optical spectroscopy...

ALEXANDER M. CRUICKSHANK

1986-03-07T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

Materials Science and Engineering B 120 (2005) 9194 Optical index profile at an antiparallel ferroelectric domain  

E-Print Network [OSTI]

-antisites, NbLi (which are excess Nb atoms at Li locations), and lithium vacancies denoted by VLi. The de- fect ferroelectric domain wall in lithium niobate Sungwon Kim, Venkatraman Gopalan Materials Research Institute-stoichiometric lithium niobate. This is imaged using near-field scanning optical microscopy. A detailed modeling

Gopalan, Venkatraman

382

A Transmission Electron Microscopy Study of Presolar Hibonite  

Science Journals Connector (OSTI)

We report isotopic and microstructural data on five presolar hibonite grains (KH1, KH2, KH6, KH15, and KH21) identified in an acid residue of the Krymka LL3.1 ordinary chondrite. Isotopic measurements by secondary ion mass spectrometry (SIMS) verified a presolar circumstellar origin for the grains. Transmission electron microscopy (TEM) examination of the crystal structure and chemistry of the grains was enabled by in situ sectioning and lift-out with a focused-ion-beam scanning-electron microscope (FIB-SEM). Comparisons of isotopic compositions with models indicate that four of the five grains formed in low-mass stars that evolved through the red giant/asymptotic giant branches (RGBs/AGBs), whereas one grain formed in the ejecta of a Type II supernova. Selected-area electron-diffraction patterns show that all grains are single crystals of hibonite. Some grains contain minor structural perturbations (stacking faults) and small spreads in orientation that can be attributed to a combination of growth defects and mechanical processing by grain-grain collisions. The similar structure of the supernova grain to those from RGB/AGB stars indicates a similarity in the formation conditions. Radiation damage (e.g., point defects), if present, occurs below our detection limit. Of the five grains we studied, only one has the pure hibonite composition of CaAl12O19. All others contain minor amounts of Mg, Si, Ti, and Fe. The microstructural data are generally consistent with theoretical predictions, which constrain the circumstellar condensation temperature to a range of 1480-1743 K, assuming a corresponding total gas pressure between 1 ? 10–6 and 1 ? 10–3 atm. The TEM data were also used to develop a calibration for SIMS determination of Ti contents in oxide grains. Grains with extreme 18O depletions, indicating deep mixing has occurred in their parent AGB stars, are slightly Ti enriched compared with grains from stars without deep mixing, most likely reflecting differences in grain condensation conditions.

Thomas J. Zega; Conel M. O'D. Alexander; Larry R. Nittler; Rhonda M. Stroud

2011-01-01T23:59:59.000Z

383

Refined tip preparation by electrochemical etching and ultrahigh vacuum treatment to obtain atomically sharp tips for scanning tunneling microscope and atomic force microscope  

SciTech Connect (OSTI)

A modification of the common electrochemical etching setup is presented. The described method reproducibly yields sharp tungsten tips for usage in the scanning tunneling microscope and tuning fork atomic force microscope. In situ treatment under ultrahigh vacuum (p {<=}10{sup -10} mbar) conditions for cleaning and fine sharpening with minimal blunting is described. The structure of the microscopic apex of these tips is atomically resolved with field ion microscopy and cross checked with field emission.

Hagedorn, Till; Ouali, Mehdi El; Paul, William; Oliver, David; Miyahara, Yoichi; Gruetter, Peter [Department of Physics, McGill University, 3600 Rue University, Montreal, QC H3A2T8 (Canada)

2011-11-15T23:59:59.000Z

384

Room temperature electron transport properties of single C{sub 60} studied using scanning tunneling microscope and reak junctions.  

SciTech Connect (OSTI)

We report the measurements of the electron transport of an individual C{sub 60} molecule through the combination of two experimental efforts. The nanometer-sized junctions were fabricated using electromigration combined with electron beam lithography and shadow effect evaporation. We performed the scanning tunneling microscopy/spectroscopy measurements of dispersed C{sub 60} molecules which were deposited on a highly ordered pyrolytic graphite substrate. The single electron tunneling through a single C{sub 60} molecule due to the Coulomb blockage effect is observed at room temperature.

Cheng, R.; Carvell, J.; Fradin, F. Y.; Indiana Univ.-Purdue Univ. at Indianapolis

2010-09-15T23:59:59.000Z

385

STUDIES OF DENGUE FEVER VIRUS BY ELECTRON MICROSCOPY  

Science Journals Connector (OSTI)

...MICROSCOPY Reginald L. Reagan A. L. Brueckner Live Stock Sanitary Service Laboratory...MICROSCOPY REGINALD L. REAGAN AND A. L. BRUECKNER Live Stock Sanitary Service Laboratory...material 233 REGINALD L. REAGAN AND A. L. BRUECKNER Figure 1. Dengue fever virus (mouse...

Reginald L. Reagan; A. L. Brueckner

1952-08-01T23:59:59.000Z

386

Slow positron annihilation spectroscopy and electron microscopy of electron beam evaporated cobalt and nickel silicides  

SciTech Connect (OSTI)

Metal silicide thin films on single-crystal silicon substrates are the subject of much research, due to their applications as electrical contacts and interconnects, diffusion barriers, low resistance gates, and field-assisted positron moderators, among others. Defects within the silicide layer and/or at the silicide/silicon interface are detrimental to device performance, since they can act as traps for charge carriers, as well as positrons. Pinholes penetrating the film are another detriment particularly for cobalt silicide films, since they allow electrons to permeate the film, rather than travel ballistically, in addition to greatly increasing surface area for recombination events. A series of epitaxial cobalt and nickel silicide thin films, deposited via electron-beam evaporation and annealed at various temperatures, have been grown on single-crystal silicon (111) substrates, in an effort to establish a relationship between deposition and processing parameters and film quality. The films have been analyzed by transmission and scanning electron microscopy, sputter depth profile Auger, and slow positron annihilation spectroscopy. The latter has been shown to both correlate and complement the traditional electron microscopy results.

Frost, R.L.; DeWald, A.B. (Georgia Institute of Technology, Atlanta, Georgia 30332 (USA)); Zaluzec, M.; Rigsbee, J.M. (University of Illinois, Urbana, Illinois 61801 (USA)); Nielsen, B.; Lynn, K.G. (Brookhaven National Laboratory, Upton, New York 11973 (USA))

1990-07-01T23:59:59.000Z

387

V-119: IBM Security AppScan Enterprise Multiple Vulnerabilities |  

Broader source: Energy.gov (indexed) [DOE]

9: IBM Security AppScan Enterprise Multiple Vulnerabilities 9: IBM Security AppScan Enterprise Multiple Vulnerabilities V-119: IBM Security AppScan Enterprise Multiple Vulnerabilities March 26, 2013 - 12:56am Addthis PROBLEM: IBM Security AppScan Enterprise Multiple Vulnerabilities PLATFORM: IBM Rational AppScan 5.x IBM Rational AppScan 8.x ABSTRACT: IBM has acknowledged multiple vulnerabilities REFERENCE LINKS: IBM Reference #:1626264 Secunia Advisory SA52764 CVE-2008-4033 CVE-2012-4431 CVE-2012-5081 CVE-2013-0473 CVE-2013-0474 CVE-2013-0510 CVE-2013-0511 CVE-2013-0512 CVE-2013-0513 CVE-2013-0532 IMPACT ASSESSMENT: Medium DISCUSSION: 1) The application allows users to perform certain actions via HTTP requests without performing proper validity checks to verify the requests. This can be exploited to e.g. cause a DoS when a logged-in user visits a

388

Positron Emission Tomography (PET) and Positron Scanning  

Office of Scientific and Technical Information (OSTI)

DOE R&D Accomplishments DOE R&D Accomplishments Search All Database Web Pages for Go The Basics Home About What's New FAQ Contact Us Laureates Nobel Laureates Fermi Laureates Nobel Physicists Nobel Chemists Medicine Nobels Explore Insights SC Stories Snapshots R&D Nuggets Database Search Browse Reports Database Help Finding Aids Site Map A - Z Index Menu Synopsis Blog Archive QR Code RSS Archive Tag Cloud Videos Widget XML Bookmark and Share Positron Emission Tomography (PET) and Positron Scanning Resources with Additional Information Positron Emission Tomography (PET) Scanner Courtesy Lawrence Berkeley National Laboratory 'Positron Emission Tomography ... [is a medical imaging technique that] can track chemical reactions in living tissues and merges chemistry with biological imaging. Its strength has been in studies of the brain where there has been significant progress in investigations of drug addiction, aging, mental illness, and neurogenic disorders. Positron Emission Tomography (PET) had its genesis in hot-atom chemical research supported by the Chemical Sciences Division of the Office of Basic Energy Sciences. Through this research it was learned, over many years, how to prepare short-lived positron emitters such as 18F whose half-life is 110 minutes. In 1975, the molecule [18F]fluorodeoxyglucose was successfully synthesized at Brookhaven National Laboratory (BNL) and set the stage for Positron Emission Tomography of the human brain.'

389

Lansce Wire Scanning Diagnostics Device Mechanical Design  

SciTech Connect (OSTI)

The Accelerator Operations & Technology Division at Los Alamos National Laboratory operates a linear particle accelerator which utilizes 110 wire scanning diagnostics devices to gain position and intensity information of the proton beam. In the upcoming LANSCE improvements, 51 of these wire scanners are to be replaced with a new design, up-to-date technology and off-the-shelf components. This document outlines the requirements for the mechanical design of the LANSCE wire scanner and presents the recently developed linac wire scanner prototype. Additionally, this document presents the design modifications that have been implemented into the fabrication and assembly of this first linac wire scanner prototype. Also, this document will present the design for the second, third, and fourth wire scanner prototypes being developed. Prototypes 2 and 3 belong to a different section of the particle accelerator and therefore have slightly different design specifications. Prototype 4 is a modification of a previously used wire scanner in our facility. Lastly, the paper concludes with a plan for future work on the wire scanner development.

Rodriguez Esparza, Sergio [Los Alamos National Laboratory; Batygin, Yuri K. [Los Alamos National Laboratory; Gilpatrick, John D. [Los Alamos National Laboratory; Gruchalla, Michael E. [Los Alamos National Laboratory; Maestas, Alfred J. [Los Alamos National Laboratory; Pillai, Chandra [Los Alamos National Laboratory; Raybun, Joseph L. [Los Alamos National Laboratory; Sattler, F. D. [Los Alamos National Laboratory; Sedillo, James Daniel [Los Alamos National Laboratory; Smith, Brian G. [Los Alamos National Laboratory

2011-01-01T23:59:59.000Z

390

A 3D scanning system for biomedical purposes  

Science Journals Connector (OSTI)

The use of three-dimensional (3D) scanning systems for acquiring the external shape features of biological objects has recently been gaining popularity in the biomedical field. A simple, low cost, 3D scanning system is presented, which employs ... Keywords: 3D geometric modelling, 3D scanning, EFDs, biological objects, biomedical scanners, camera calibration, data acquisition, direct linear transformation, elliptical Fourier descriptors, laser light-sectioning, medical imaging, shape features

B. D. Bradley; A. D. C. Chan; M. J. D. Hayes

2009-06-01T23:59:59.000Z

391

The oxidation of aluminum at high temperature studied by Thermogravimetric Analysis and Differential Scanning Calorimetry.  

SciTech Connect (OSTI)

The oxidation in air of high-purity Al foil was studied as a function of temperature using Thermogravimetric Analysis with Differential Scanning Calorimetry (TGA/DSC). The rate and/or extent of oxidation was found to be a non-linear function of the temperature. Between 650 and 750 %C2%B0C very little oxidation took place; at 850 %C2%B0C oxidation occurred after an induction period, while at 950 %C2%B0C oxidation occurred without an induction period. At oxidation temperatures between 1050 and 1150 %C2%B0C rapid passivation of the surface of the aluminum foil occurred, while at 1250 %C2%B0C and above, an initial rapid mass increase was observed, followed by a more gradual increase in mass. The initial rapid increase was accompanied by a significant exotherm. Cross-sections of oxidized specimens were characterized by scanning electron microscopy (SEM); the observed alumina skin thicknesses correlated qualitatively with the observed mass increases.

Coker, Eric Nicholas

2013-10-01T23:59:59.000Z

392

ProxiScan?: A Novel Camera for Imaging Prostate Cancer  

ScienceCinema (OSTI)

ProxiScan is a compact gamma camera suited for high-resolution imaging of prostate cancer. Developed by Brookhaven National Laboratory and Hybridyne Imaging Technologies, Inc., ProxiScan won a 2009 R&D 100 Award, sponsored by R&D Magazine to recognize t

Ralph James

2010-01-08T23:59:59.000Z

393

Fast 3D Scanning for Biometric Identification and Verification  

E-Print Network [OSTI]

Fast 3D Scanning for Biometric Identification and Verification June 2011 Authors Anselmo., & Chen, A. (2011). Fast 3D Scanning for Biometric Identification and Verification. (Prepared by RTI..................................................10 Summary and Findings for Integration of Imperceptible Structured Lighting and SIS's 3D Snapshot

McShea, Daniel W.

394

Combined low-temperature scanning tunneling/atomic force microscope for atomic resolution imaging and site-specific force spectroscopy  

SciTech Connect (OSTI)

The authors present the design and first results of a low-temperature, ultrahigh vacuum scanning probe microscope enabling atomic resolution imaging in both scanning tunneling microscopy (STM) and noncontact atomic force microscopy (NC-AFM) modes. A tuning-fork-based sensor provides flexibility in selecting probe tip materials, which can be either metallic or nonmetallic. When choosing a conducting tip and sample, simultaneous STM/NC-AFM data acquisition is possible. Noticeable characteristics that distinguish this setup from similar systems providing simultaneous STM/NC-AFM capabilities are its combination of relative compactness (on-top bath cryostat needs no pit), in situ exchange of tip and sample at low temperatures, short turnaround times, modest helium consumption, and unrestricted access from dedicated flanges. The latter permits not only the optical surveillance of the tip during approach but also the direct deposition of molecules or atoms on either tip or sample while they remain cold. Atomic corrugations as low as 1 pm could successfully be resolved. In addition, lateral drifts rates of below 15 pm/h allow long-term data acquisition series and the recording of site-specific spectroscopy maps. Results obtained on Cu(111) and graphite illustrate the microscope's performance.

Schwarz, Udo; Albers, Boris J.; Liebmann, Marcus; Schwendemann, Todd C.; Baykara, Mehmet Z.; Heyde, Markus; Salmeron, Miquel; Altman, Eric I.; Schwarz, Udo D.

2008-02-27T23:59:59.000Z

395

NCEM National Center for Electron Microscopy: Becoming an NCEM User  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

New Research New Research Gallery Microscopy Links Becoming an NCEM User Step 1: Submit a proposal Step 2: Before you begin your research Step 3: Instrument qualification Step 4: Accessing NCEM facilities and performing research Step 1: Submit a proposal Deadlines for new proposals are March 15, June 15, September 15, December 15. Access to NCEM facilities is granted to researchers whose proposals are accepted by the NCEM proposal review committee. NCEM users are expected to have a strong background in transmission electron microscopy, and submitted proposals should include evidence of prior electron microscopy experience by the intended operator. Researchers who do not have sufficient experience in electron microscopy may be able to use NCEM facilities through a collaborative project.

396

Measuring Shear Stress in Microfluidics using Traction Force Microscopy  

Science Journals Connector (OSTI)

Traction force microscopy is a previously-developed method to measure shear forces exerted by biological cells on substrates to which they are adhered (Dembo, 1999). The technique determines the shear stress a...

Bryant Mueller

2011-01-01T23:59:59.000Z

397

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing...

398

Doppler optical coherence microscopy for studies of cochlear mechanics  

E-Print Network [OSTI]

The possibility of measuring subnanometer motions with micron scale spatial resolution in the intact mammalian cochlea using Doppler optical coherence microscopy (DOCM) is demonstrated. A novel DOCM system is described ...

Hong, Stanley S.

399

Fast live simultaneous multiwavelength four-dimensional optical microscopy  

Science Journals Connector (OSTI)

...between excitation power and sensitivity...throughput of both systems. Most modern microscopy systems have excellent...connected to a power source (Bioptechs...Pawley JB ( 2006 ) Handbook of Biological Confocal...image sequence restoration . IEEE T Pattern...

Peter M. Carlton; Jérôme Boulanger; Charles Kervrann; Jean-Baptiste Sibarita; Jean Salamero; Susannah Gordon-Messer; Debra Bressan; James E. Haber; Sebastian Haase; Lin Shao; Lukman Winoto; Atsushi Matsuda; Peter Kner; Satoru Uzawa; Mats Gustafsson; Zvi Kam; David A. Agard; John W. Sedat

2010-01-01T23:59:59.000Z

400

Fluorescence microscopy with diffraction resolution barrier broken by stimulated emission  

Science Journals Connector (OSTI)

...intracavity frequency doubler. This system partly converted the Ti:Sapphire...the focused time-averaged power. The axial...processing. Computational image restoration can in addition improve...light. 1 Pawley J ( 1995 ) Handbook of Biological Confocal Microscopy...

Thomas A. Klar; Stefan Jakobs; Marcus Dyba; Alexander Egner; Stefan W. Hell

2000-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in...

402

Carmichael's Concise Review Microscopy is Only Skin Deep  

E-Print Network [OSTI]

Carmichael's Concise Review Microscopy is Only Skin Deep Stephen W. Carmichael Mayo Clinic. Coming Events 2011 EMAS 2011 May 15­19, 2011 Angers, France www.emas-web.net IUMAS-V May 22­27, 2011

Heller, Eric

403

Toward single cell traction microscopy within 3D collagen matrices  

SciTech Connect (OSTI)

Mechanical interaction between the cell and its extracellular matrix (ECM) regulates cellular behaviors, including proliferation, differentiation, adhesion, and migration. Cells require the three-dimensional (3D) architectural support of the ECM to perform physiologically realistic functions. However, current understanding of cell–ECM and cell–cell mechanical interactions is largely derived from 2D cell traction force microscopy, in which cells are cultured on a flat substrate. 3D cell traction microscopy is emerging for mapping traction fields of single animal cells embedded in either synthetic or natively derived fibrous gels. We discuss here the development of 3D cell traction microscopy, its current limitations, and perspectives on the future of this technology. Emphasis is placed on strategies for applying 3D cell traction microscopy to individual tumor cell migration within collagen gels. - Highlights: • Review of the current state of the art in 3D cell traction force microscopy. • Bulk and micro-characterization of remodelable fibrous collagen gels. • Strategies for performing 3D cell traction microscopy within collagen gels.

Hall, Matthew S. [Department of Biological and Environmental Engineering, Cornell University, Ithaca, NY 14853 (United States); Long, Rong [Department of Mechanical Engineering, University of Alberta, Edmonton, AB, Canada T6G 2G8 (Canada); Feng, Xinzeng [Department of Mechanical and Aerospace Engineering, Cornell University, Ithaca, NY 14853 (United States); Huang, YuLing [Department of Biological and Environmental Engineering, Cornell University, Ithaca, NY 14853 (United States); Hui, Chung-Yuen [Department of Mechanical and Aerospace Engineering, Cornell University, Ithaca, NY 14853 (United States); Wu, Mingming, E-mail: mw272@cornell.edu [Department of Biological and Environmental Engineering, Cornell University, Ithaca, NY 14853 (United States)

2013-10-01T23:59:59.000Z

404

Parameter Scan of an Effective Group Difference Pseudopotential Using Grid Computing 1 Parameter Scan of an Effective Group Difference  

E-Print Network [OSTI]

Parameter Scan of an Effective Group Difference Pseudopotential Using Grid Computing 1 Parameter Scan of an Effective Group Difference Pseudopotential Using Grid Computing Wibke SUDHOLT and Kim K of the actual biology/biochemistry. The ability to invoke modern grid technologies offers the ability to create

Abramson, David

405

Optoacoustic Microscopy for Investigation of Material Nanostructures-Embracing the Ultrasmall, Ultrafast, and the Invisible  

SciTech Connect (OSTI)

The goal of this grant was the development of a new type of scanning acoustic microscope for nanometer resolution ultrasound imaging, based on ultrafast optoacoustics (>GHz). In the microscope, subpicosecond laser pulses was used to generate and detect very high frequency ultrasound with nanometer wavelengths. We report here on the outcome of the 3-year DOE/BES grant which involved the design, multifaceted construction, and proof-of-concept demonstration of an instrument that can be used for quantitative imaging of nanoscale material features – including features that may be buried so as to be inaccessible to conventional lightwave or electron microscopies. The research program has produced a prototype scanning optoacoustic microscope which, in combination with advanced computational modeling, is a system-level new technology (two patents issues) which offer novel means for precision metrology of material nanostructures, particularly those that are of contemporary interest to the frontline micro- and optoelectronics device industry. For accomplishing the ambitious technical goals, the research roadmap was designed and implemented in two phases. In Phase I, we constructed a “non-focusing” optoacoustic microscope instrument (“POAM”), with nanometer vertical (z-) resolution, while limited to approximately 10 micrometer scale lateral recolution. The Phase I version of the instrument which was guided by extensive acoustic and optical numerical modeling of the basic underlying acoustic and optical physics, featured nanometer scale close loop positioning between the optoacoustic transducer element and a nanostructured material sample under investigation. In phase II, we implemented and demonstrated a scanning version of the instrument (“SOAM”) where incident acoustic energy is focused, and scanned on lateral (x-y) spatial scale in the 100 nm range as per the goals of the project. In so doing we developed advanced numerical simulations to provide computational models of the focusing of multi-GHz acoustic waves to the nanometer scale and innovated a series fabrication approaches for a new type of broadband high-frequency acoustic focusing microscope objective by applying methods on nanoimprinting and focused-ion beam techniques. In the following, the Phase I and Phase II instrument development is reported as Section II. The first segment of this section describes the POAM instrument and its development, while including much of the underlying ultrafast acoustic physics which is common to all of our work for this grant. Then, the science and engineering of the SOAM instrument is described, including the methods of fabricating new types of acoustic microlenses. The results section is followed by reports on publications (Section III), Participants (Section IV), and statement of full use of the allocated grant funds (Section V).

Nurmikko, Arto; Humphrey, Maris

2014-07-10T23:59:59.000Z

406

Atomic Force Microscopy and Kelvin Probe Force Microscopy Evidence of Local Structural Inhomogeneity and Nonuniform Dopant Distribution in Conducting Polybithiophene  

Science Journals Connector (OSTI)

Atomic Force Microscopy and Kelvin Probe Force Microscopy Evidence of Local Structural Inhomogeneity and Nonuniform Dopant Distribution in Conducting Polybithiophene ... The fundamental difference between polymer grains and grain peripheral areas demonstrated by KFM was also supported by in situ contact-mode AFM data taken with the as-grown polymer film. ... (1)?Pekker, S.; Janossy, A. In Handbook of Conducting Polymers; Skotheim, T. A., Ed.; Marcel Dekker:? New York, 1986; Vol. ...

Oleg A. Semenikhin; Lei Jiang; Tomokazu Iyoda; Kazuhito Hashimoto; Akira Fujishima

1996-11-28T23:59:59.000Z

407

Induction of DNA Damage by Low Dose PET scans  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Induction of DNA Damage by Low Dose PET scans Induction of DNA Damage by Low Dose PET scans Douglas Boreham McMaster University Abstract This research is focused on assessing the radiation risk associated with positron emission tomography (PET) scans. It has been suggested that low dose medical imaging, such as PET scans, carry an added biological risk because they expose the patient to ionizing radiation. PET scanning is an increasingly used nuclear medicine procedure that requires the administration of isotope 18F-fluorodeoxyglucose (18F-FDG, E=250 keV β and 511 keV γ) and results in an effective dose to the patient ranging from 7-22 mSv. The radiation induced DNA damage associated with a PET scan was studied in 7-9 week old female wild type Trp53 +/+ mice. Mice were given a PET scan with 18F-FDG and the biological response was assessed in bone marrow using

408

Los Alamos: MST: MST-6: EML: Electron Microscopy Laboratory  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Strata DB235 FIB/SEM (Focused Ion Beam/High Reolution Scanning Electron Microscope) Strata DB235 FIB/SEM (Focused Ion Beam/High Reolution Scanning Electron Microscope) FEI Strata DB235 FIB/SEM (Focused Ion Beam/High Reolution Scanning Electron Microscope) This is a versatile field emission scanning electron microscope integrated with a focused ion beam column that is used for sophisticated SEM and TEM sample preparation, micromachining, and ultrahigh resolution SEM imaging. The microscope is also equipped for x-ray microanalysis and crystallographic orientation imaging. Microscope consists of a Hexalens SFEG electron beam column, and a Magnum ion beam column with a gallium liquid metal ion source. Imaging with both secondary electrons and ions. Digital image acquisition. Small, stable, high brightness Schottky based field emission electron source provides 1.5 nm resolution at 30 kV. Three electron beam lens modes - normal imaging, high resolution imaging, and EDS imaging.

409

E-Print Network 3.0 - advanced microscopy techniques Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

microscopy techniques and their practice in relationship to materials structure characterization... of Microscopy", Edited by P.W. Hawkes and J.C.H. Spence, Springer, 2006 (An...

410

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental Science Beamline at the Advanced Light Source. Soft X-Ray Microscopy and Spectroscopy at the Molecular...

411

Surface skeleton generation based on 360-degree profile scan  

E-Print Network [OSTI]

A rapid prototyping method is invented, which works on a specific data structure produced by an optical metrology technique: 360-degree surface profile scanning. A computer algorithm takes an object profile data, restructure ...

Chen, Lujie

412

Information efficiency of line-scan imaging mechanisms  

Science Journals Connector (OSTI)

Information theory is used to formulate a single figure of merit for assessing the performance of line-scan imaging systems as a function of their spatial response (PSF or MTF),...

Huck, F O; Halyo, N; Park, S K

1981-01-01T23:59:59.000Z

413

Dynamic study of tunable stiffness scanning microscope probe  

E-Print Network [OSTI]

This study examines the dynamic characteristics of the in-plane tunable stiffness scanning microscope probe for an atomic force microscope (AFM). The analysis was carried out using finite element analysis (FEA) methods for ...

Vega González, Myraida Angélica

2005-01-01T23:59:59.000Z

414

System Provides Clear Brain Scans of Awake, Unrestrained Mice...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

System Provides Clear Brain Scans of Awake, Unrestrained Mice dynamic imaging of mice Three markers attached to the head of a mouse enable the AwakeSPECT system to obtain detailed,...

415

Achieving sub-10-nm resolution using scanning electron beam lithography  

E-Print Network [OSTI]

Achieving the highest possible resolution using scanning-electron-beam lithography (SEBL) has become an increasingly urgent problem in recent years, as advances in various nanotechnology applications have driven demand for ...

Cord, Bryan M. (Bryan Michael), 1980-

2009-01-01T23:59:59.000Z

416

Multi-atlas segmentation in head and neck CT scans  

E-Print Network [OSTI]

We investigate automating the task of segmenting structures in head and neck CT scans, to minimize time spent on manual contouring of structures of interest. We focus on the brainstem and left and right parotids. To generate ...

Arbisser, Amelia M

2012-01-01T23:59:59.000Z

417

Observing Warm Clouds in 3D Using ARM Scanning Cloud  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Observing Warm Clouds in 3D Using ARM Scanning Cloud Radars and a Novel Ensemble Method For original submission and image(s), see ARM Research Highlights http:www.arm.gov...

418

Construction of an ultra-low temperature scanning tunneling microscope  

Science Journals Connector (OSTI)

We describe designs and specifications of an ultra-low temperature scanning tunneling microscope developed at ... works over a wide temperature range between 90 mK and 300 K with atomic resolution as...

Hiroshi Fukuyama; Hiroki Tan; Tetsuya Handa…

1996-01-01T23:59:59.000Z

419

First Observations of Tracking Clouds Using Scanning ARM Cloud Radars  

Science Journals Connector (OSTI)

Tracking clouds using scanning cloud radars can help to document the temporal evolution of cloud properties well before large-drop formation (weather radar “first echo”). These measurements also complement cloud and precipitation tracking using ...

Paloma Borque; Pavlos Kollias; Scott Giangrande

2014-12-01T23:59:59.000Z

420

Detection of bone disease in dogs by radioisotope scanning  

E-Print Network [OSTI]

, delayed union, and nonunion), osteomyelitis, degenerative arthritis, surgical osteotomy, i'ibrous dysplasia, osteochondromatosie, and growing epiphyses. Radioisotopic scanning has been reported 12 for studying the metabolism of Fluorine-18 in dogs 9..., ( 1962): 95-104. 2. Bauer, G. C. H. , and Smith, E. M. r Sr 85 Sointimetry in Osteoarthritis of the Knee. J . Nucl. Med. , 10, (Mar. , 1969): 109-116. Blau, M. , Nagler, W. , and Bender, M. A. : Fluorine ? 18. A New Isotope for Bone Scanning. J. Nucl...

Morris, Earl Louis

2012-06-07T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

CMOS ROM arrays programmable by laser beam scanning  

E-Print Network [OSTI]

CMOS ROM ARRAYS PROGRAMMABLE BY LASER BEAM SCANNING A Thesis bY JONG JUNE LEE Submitted to the Graduate College of Texas ASM University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE May 1984 Major Subject... : Electrical Engineering CMOS ROM ARRAYS PROGRAMMABLE BY LASER BEAM SCANNING A Thesis by JONGJUNE LEE Approved as to style and content by: Noel R. Strader II (Chairman of Committee) Philli E. Allen (Member) Philip S. Noe (Member) Daniel Colunga...

Lee, Jongjune

2012-06-07T23:59:59.000Z

422

Pencil Beam Scanning System Based On A Cyclotron  

SciTech Connect (OSTI)

Sumitomo Heavy Industries, Ltd. (SHI) has developed a new pencil beam scanning system (PBS) for proton therapy in collaboration with National Cancer Center Hospital East (NCCHE). Taking advantage of the continuous beam from the cyclotron P235, the line scanning method is employed in order to realize continuous irradiation with high dose rate. 3D uniform and sphere field was irradiated and compared with the simulation.

Tachikawa, Toshiki; Nonaka, Hideki; Kumata, Yukio [Sumitomo Heavy Industries, Ltd., 5-2 Soubiraki-cho, Niihama, Ehime 792-8588 (Japan); Nishio, Teiji; Ogino, Takashi [National Cancer Center Hospital East, 6-5-1 Kashiwanoha, Kashiwa, Chiba 277-8577 (Japan)

2011-06-01T23:59:59.000Z

423

LINEAR SCANNING METHOD BASED ON THE SAFT COARRAY  

SciTech Connect (OSTI)

This work presents a method to obtain B-scan images based on linear array scanning and 2R-SAFT. Using this technique some advantages are obtained: the ultrasonic system is very simple; it avoids the grating lobes formation, characteristic in conventional SAFT; and subaperture size and focussing lens (to compensate emission-reception) can be adapted dynamically to every image point. The proposed method has been experimentally tested in the inspection of CFRP samples.

Martin, C. J.; Martinez-Graullera, O.; Romero, D.; Ullate, L. G. [Instituto de Automatica Industrial-CSIC, Carretera de Campo Real, km 0.200, La Poveda, Arganda del Rey, Madrid, E-28500 (Spain); Higuti, R. T. [UNESP-Universidade Estadual Paulista, Dep. Electrical Engineering, Av. Brasil, 56, 15385-000, Ilha Solteira, SP (Brazil)

2010-02-22T23:59:59.000Z

424

Imaging Hydrated Microbial Extracellular Polymers: Comparative Analysis by Electron Microscopy  

SciTech Connect (OSTI)

Microbe-mineral and -metal interactions represent a major intersection between the biosphere and geosphere but require high-resolution imaging and analytical tools for investigating microscale associations. Electron microscopy has been used extensively for geomicrobial investigations and although used bona fide, the traditional methods of sample preparation do not preserve the native morphology of microbiological components, especially extracellular polymers. Herein, we present a direct comparative analysis of microbial interactions using conventional electron microscopy approaches of imaging at room temperature and a suite of cryo-electron microscopy methods providing imaging in the close-to-natural hydrated state. In situ, we observed an irreversible transformation of bacterial extracellular polymers during the traditional dehydration-based sample preparation that resulted in the collapse of hydrated gel-like EPS into filamentous structures. Dehydration-induced polymer collapse can lead to inaccurate spatial relationships and hence could subsequently affect conclusions regarding nature of interactions between microbial extracellular polymers and their environment.

Dohnalkova, Alice; Marshall, Matthew J.; Arey, Bruce W.; Williams, Kenneth H.; Buck, Edgar C.; Fredrickson, Jim K.

2011-02-01T23:59:59.000Z

425

Generative Models for Super-Resolution Single Molecule Microscopy Images of Biological Structures  

E-Print Network [OSTI]

an information bridge between super-resolution microscopy and structural biology by using generative models

Matsuda, Noboru

426

Atom probe field ion microscopy and related topics: A bibliography 1992  

SciTech Connect (OSTI)

This bibliography contains citations of books, conference proceedings, journals, and patents published in 1992 on the following types of microscopy: atom probe field ion microscopy (108 items); field emission microscopy (101 items); and field ion microscopy (48 items). An addendum of 34 items missed in previous bibliographies is included.

Russell, K.F.; Godfrey, R.D.; Miller, M.K.

1993-12-01T23:59:59.000Z

427

Development of a combined interference microscope objective and scanning probe microscope  

Science Journals Connector (OSTI)

A compact sensor head combining optical interference and scanning probe microscopy in a single instrument has been developed. This instrument is able to perform complementary quantitative measurements combining fast nondestructive three-dimensional surface analysis with high lateral resolution imaging. A custom interference microscopesensor head has been designed as the optical microscope objective and integrated within the architecture of a commercial interference microscope. The combined instrument makes available both the acquisition software and the hardware interface of the commercial microscope. The latter is able to function as a phase-shift interferometer or white light interferometer. Furthermore the use of an optical fiber to transmit light from an external laser: (i) removes a major heat source from the measurement environment and (ii) makes aperture correction unnecessary. The lateral resolution of the instrument has been extended by the addition of a previously developed compact scanning probe microscope(SPM) module to the custom interference microscope objective. This SPM unit is based upon piezoresistive cantilever technology. The “piezolevers” are self-sensing and therefore require no additional systems such as optical beam deflection or fiber interferometry to monitor their displacement. The mechanical simplicity of the piezolever SPM unit allows for a small physical size and can thus be added to the custom optical sensor head without violating constraints on the working distance defined by the optics. A major benefit of the system in terms of a quantitative nanometrology is the possibility to perform a traceable and direct calibration of the SPM module. This calibration is achieved practically by measuring an appropriate sample at a common location using both techniques. Results are presented here for the measurement of two calibration standards and a test sample to demonstrate the increased lateral resolution of the instrument.

James W. G. Tyrrell; Claudio Dal Savio; Rolf Krüger-Sehm; Hans-Ulrich Danzebrink

2004-01-01T23:59:59.000Z

428

Ecological and agricultural applications of synchrotron IR microscopy  

E-Print Network [OSTI]

Ecological and agricultural applications of synchrotron IR microscopy T.K. Raab a,*, J.P. Vogel b factors to the fungus Erysiphe cichoracearum, a causative agent of powdery mildew disease. Three genes to pro- liferate when environmental conditions and re- sources are optimum. Cellulose, an abundant

429

Nanoscale Thermotropic Phase Transitions Enhance Photothermal Microscopy Signals  

E-Print Network [OSTI]

the material undergoes a phase transition. Herein, we show that thermotropic phase transitions in 4-Cyano-41 Nanoscale Thermotropic Phase Transitions Enhance Photothermal Microscopy Signals A. Nicholas G-objects in various environments. It uses a photo-induced change in the refractive index of the environment. Taking

Boyer, Edmond

430

Nanometric depth resolution from multi-focal images in microscopy  

Science Journals Connector (OSTI)

...that have been stored in a computer, but it is noted that using...interdisciplinary Bridging the Gaps grant from the UK Engineering and...Physics, SUPA/IIS, School of Engineering and Physical...instrumentation Image Processing, Computer-Assisted methods Microscopy...

2011-01-01T23:59:59.000Z

431

ABSTRACTS IN REPORTS CONCERNING ELECTRON MICROSCOPY PUBLISHED IN JAPAN:  

Science Journals Connector (OSTI)

......Thoracic Lymphatics of Living Rabbits and Sites of Escape of Car- bon Particles from the Vessels: Fumihiko KATO (First Dept...deafness. Using light and elect- ron microscopy he studied the defective organ of Corti in Shaker-1 mouse, one strain of congeni......

ABSTRACTS

1967-01-01T23:59:59.000Z

432

Image processing pipeline for synchrotron-radiation-based tomographic microscopy  

Science Journals Connector (OSTI)

A software environment has been developed for processing and reconstructing online the large amount of data generated at TOMCAT, a synchrotron-radiation-based tomographic microscopy beamline of the Swiss Light Source at Paul Scherrer Institute, Switzerland. It has been designed to minimize user interaction and maximize the reconstruction speed and therefore optimize beam time usage.

Hintermüller, C.

2010-05-14T23:59:59.000Z

433

Detection of protein conformation defects from fluorescence microscopy images  

Science Journals Connector (OSTI)

A diagnostic method for protein conformational diseases (PCD) from microscopy images is proposed when such conformational conflicts involve muscular intranuclear inclusions (INIs) indicative of oculopharyngeal muscular dystrophy (OPMD), one variety of ... Keywords: Computer-aided diagnosis, Histogram, Microscopic images, Pattern classification, Protein conformational diseases, Texture analysis

Peifang Guo; Prabir Bhattacharya

2013-09-01T23:59:59.000Z

434

The StarScan plate measuring machine: overview and calibrations  

E-Print Network [OSTI]

The StarScan machine at the U.S. Naval Observatory (USNO) completed measuring photographic astrograph plates to allow determination of proper motions for the USNO CCD Astrograph Catalog (UCAC) program. All applicable 1940 AGK2 plates, about 2200 Hamburg Zone Astrograph plates, 900 Black Birch (USNO Twin Astrograph) plates, and 300 Lick Astrograph plates have been measured. StarScan comprises of a CCD camera, telecentric lens, air-bearing granite table, stepper motor screws, and Heidenhain scales to operate in a step-stare mode. The repeatability of StarScan measures is about 0.2 micrometer. The CCD mapping as well as the global table coordinate system has been calibrated using a special dot calibration plate and the overall accuracy of StarScan x,y data is derived to be 0.5 micrometer. Application to real photographic plate data shows that position information of at least 0.65 micrometer accuracy can be extracted from course grain 103a-type emulsion astrometric plates. Transformations between "direct" and "reverse" measures of fine grain emulsion plate measures are obtained on the 0.3 micrometer level per well exposed stellar image and coordinate, which is at the limit of the StarScan machine.

Norbert Zacharias; Lars Winter; Ellis Holdenried; Jean-Pierre de Cuyper; Ted Rafferty; Gary Wycoff

2008-06-02T23:59:59.000Z

435

E-Print Network 3.0 - analyzer vertically scanning Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

University, New York, NY 10027 Effects of Scanning Schemes on Laser Tube Bending Four laser... scanning schemes for tube bending, including point-source circumferential ......

436

E-Print Network 3.0 - analytical scanning electron Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Electron Microscope Philips CM20 Analytical Scanning... during formation of the carbide particles. 12;Philips CM20 Analytical Scanning Transmission Electron... at SCSAM ...

437

A CCD Camera with Electron Decelerator for Intermediate Voltage Electron Microscopy  

SciTech Connect (OSTI)

Electron microscopists are increasingly turning to Intermediate Voltage Electron Microscopes (IVEMs) operating at 300 - 400 kV for a wide range of studies. They are also increasingly taking advantage of slow-scan charge coupled device (CCD) cameras, which have become widely used on electron microscopes. Under some conditions CCDs provide an improvement in data quality over photographic film, as well as the many advantages of direct digital readout. However, CCD performance is seriously degraded on IVEMs compared to the more conventional 100 kV microscopes. In order to increase the efficiency and quality of data recording on IVEMs, we have developed a CCD camera system in which the electrons are decelerated to below 100 kV before impacting the camera, resulting in greatly improved performance in both signal quality and resolution compared to other CCDs used in electron microscopy. These improvements will allow high-quality image and diffraction data to be collected directly with the CCD, enabling improvements in data collection for applications including high-resolution electron crystallography, single-particle reconstruction of protein structures, tomographic studies of cell ultrastructure and remote microscope operation. This approach will enable us to use even larger format CCD chips that are being developed with smaller pixels.

Downing, Kenneth H; Downing, Kenneth H.; Mooney, Paul E.

2008-03-17T23:59:59.000Z

438

Fault localization and analysis in semiconductor devices with optical-feedback infrared confocal microscopy  

SciTech Connect (OSTI)

We report on a cost-effective optical setup for characterizing light-emitting semiconductor devices with optical-feedback confocal infrared microscopy and optical beam-induced resistance change.We utilize the focused beam from an infrared laser diode to induce local thermal resistance changes across the surface of a biased integrated circuit (IC) sample. Variations in the multiple current paths are mapped by scanning the IC across the focused beam. The high-contrast current maps allow accurate differentiation of the functional and defective sites, or the isolation of the surface-emittingp-i-n devices in the IC. Optical beam-induced current (OBIC) is not generated since the incident beam energy is lower than the bandgap energy of the p-i-n device. Inhomogeneous current distributions in the IC become apparent without the strong OBIC background. They are located at a diffraction-limited resolution by referencing the current maps against the confocal reflectance image that is simultaneously acquired via optical-feedback detection. Our technique permits the accurate identification of metal and semiconductor sites as well as the classification of different metallic structures according to thickness, composition, or spatial inhomogeneity.

Sarmiento, Raymund; Cemine, Vernon Julius; Tagaca, Imee Rose; Salvador, Arnel; Mar Blanca, Carlo; Saloma, Caesar

2007-11-01T23:59:59.000Z

439

Composition analysis by scanning femtosecond laser ultraprobing (CASFLU).  

DOE Patents [OSTI]

The composition analysis by scanning femtosecond ultraprobing (CASFLU) technology scans a focused train of extremely short-duration, very intense laser pulses across a sample. The partially-ionized plasma ablated by each pulse is spectrometrically analyzed in real time, determining the ablated material's composition. The steering of the scanned beam thus is computer directed to either continue ablative material-removal at the same site or to successively remove nearby material for the same type of composition analysis. This invention has utility in high-speed chemical-elemental, molecular-fragment and isotopic analyses of the microstructure composition of complex objects, e.g., the oxygen isotopic compositions of large populations of single osteons in bone.

Ishikawa, Muriel Y. (Livermore, CA); Wood, Lowell L. (Simi Valley, CA); Campbell, E. Michael (Danveille, CA); Stuart, Brent C. (Livermore, CA); Perry, Michael D. (Livermore, CA)

2002-01-01T23:59:59.000Z

440

The scanning Compton polarimeter for the SLD experiment  

SciTech Connect (OSTI)

For the 1994/95 run of the SLD experiment at SLAC, a Compton polarimeter measured the luminosity-weighted electron beam polarization to be (77.2 {+-} 0.5)%. This excellent accuracy is achieved by measuring the rate asymmetry of Compton-scattered electrons near the kinematic endpoint. The polarimeter takes data continuously while the electron and positron beams are in collision and achieves a statistical precision of better than 1% in a three minute run. To calibrate the polarimeter and demonstrate its accuracy, many scans are frequently done. These include scans of the laser polarization, the detector position with respect to the kinematic edge, and the laser power.

Woods, M.; SLD Collaboration

1996-10-01T23:59:59.000Z

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


441

Biofilm Cohesiveness Measurement Using a Novel Atomic Force Microscopy Methodology  

Science Journals Connector (OSTI)

...functions by characterizing friction and/or wear under repeated scanning with variable loads...our knowledge, concomitant friction and wear processes on biofilms, important for understanding...Bacteriol. 186: 8096-8104. 40 Towler, B. W., C. J. Rupp, A. B. Cunningham...

Francois Ahimou; Michael J. Semmens; Paige J. Novak; Greg Haugstad

2007-03-02T23:59:59.000Z

442

Atomic scale investigations of the thermal and electron induced chemistry of small molecules on platinum(111) as revealed by scanning tunneling microscopy  

SciTech Connect (OSTI)

The work presented here can be divided into two parts: 1) an experimental and analysis section dealing with the investigation of small molecules such as methyl bromide, carbon dioxide, diatomic nitrogen, methane and methane?s photochemical derivative methyl radical adsorbed onto the Pt(111) surface, and 2) A detailed explanation of the current STM and chamber, with included designs and detailed instructions for operation and maintenance of both the STM and chamber. The investigations of the methyl bromide molecule show interesting dipole-dipole interactions on the Pt(111) surface. With a (6 x 3) lattice being described as the full monolayer that was created by overdosing and annealing to 104 K. The (6 x 3) lattice is shown to occupy top sites and three fold hollow sites on the Pt(111) surface giving rise to a very sharp and symmetrically split ?2 RAIRS mode, and the absence of the ?5 mode in RAIRS is indicative that the molecules are all aligned with their C-Br bond parallel to the surface normal. Additional sub-monolayer structures were observed that had components that were not aligned with the surface normal. The submonolayer lattices ranging from a structured 0.12 ML to a random coverages estimated at 0.20 ML, to a shift in the (6 x 3) lattice resulting in a high local line coverage of 0.33 ML. Analysis of the CO2 molecules adsorbed onto the Pt(111) surface shows that there is a preferred high temperature dosing that results in a thermodynamically stable system of a (3 x 3) lattice consisting of both horizontal and vertical molecules. The coverage of the (3 x 3) lattice of vertical molecules is 0.11 ML which can be assigned to the RAIRS peak of 2287 cm-1. The vertical molecules are seen to occupy the hollow sites within the horizontal (3 x 3) lattice. The low temperature dosage of multilayers and annealing, to 78 K, show that the (3 x 3) lattice is compressed into a lattice of (5 x 3) with some of the molecules in the unit cell that are incommensurate with the Pt(111) lattice. However, isolated unit cells of the horizontal (3 x 3) lattices remain after the compression which allows a single vertical CO2 molecule to occupy the hollow site resulting in the characteristic 2277 cm-1 peak in RAIRS. The resulting local coverage of the (5 x 3) lattice is calculated to be 0.40 ML. Methane was found to adsorb onto the Pt(111) lattice in a (?3 x ?3) configuration yielding a coverage of 0.33 ML in perfect agreement with previous coverage assignments. With a full coverage of methane adsorbed onto the crystal surface an ArF excimer laser was used to photodissociate the molecules to create methyl radicals that could be imaged by STM. After photochemical deposition of methyl radicals and annealing the surface to 175 K, the STM was used to image the surface. The methyl radical were estimated to arrange in a (?3 by ?3) lattice same as the methane, and imaged as roughly 0.4 ? high protrusions from the surface with a diameter of 5.5 ?. The last molecule that was studied, was the adsorption of diatomic nitrogen on the Pt(111) surface at a temperature of 25 K. Due to the very low desorption temperature of N2 (i.e. 46 K) and the relatively high temperature of the crystal, only chemisorbed molecules were able to be resolved. The results confirm that diatomic nitrogen binds to the top side of the Pt(111) step edge in agreement with Yates RAIRS studies, and calculations by Norskov. However, there was observed a stable cluster of molecules bound to the lower side of the step edge in a (2 x 2) lattice configuration which has previously unknown before these images and is the most likely source of the photoactivity of nitrogen molecules on the crystal surface. It is the hopes of this author that the experiments described within the dissertation lead to new and better understanding of the role that the microscopic scale structures of adsorbates on the surface play in catalysis. Also that the general information of STM design, construction and tip fabrication will be useful to all students who follow me in working

Schwendemann, Todd Charles

2006-01-01T23:59:59.000Z

443

Three-dimensional observation of SiO2 hollow spheres with a double-shell structure using aberration-corrected scanning confocal electron microscopy  

Science Journals Connector (OSTI)

......microscope. Phil. Trans. R. Soc. A (2009) 367...Szilagyi Z S, Lupini A R, Borisevich A, Sides W H Jr, Pennycook S J. Direct...1063/1.3225103 . 32 McNally J G , Karpova T, Cooper...33 De Jonge N , Sougrat R, Northan B M, Pennycook......

Xiaobin Zhang; Masaki Takeguchi; Ayako Hashimoto; Kazutaka Mitsuishi; Peng Wang; Peter D. Nellist; Angus I. Kirkland; Meguru Tezuka; Masayuki Shimojo

2012-06-01T23:59:59.000Z

444

Scanning tunneling microscopy of the phase transition between H/Si,,100...-,,2 1... and H/Si,,100...-,,3 1...  

E-Print Network [OSTI]

of Western Ontario, London, Ontario, Canada N6A 5B7 Received 19 September 1995 The transition from H/Si 100-energy-electron diffraction LEED on the sur- face provide valuable information on the populations of spe- cific adsorbed

Qin, Xiaorong

445

Electric field and humidity effects on adsorbed water behavior on BaTiO3 ferroelectric domains studied by scanning probe microscopy  

E-Print Network [OSTI]

Electric field and humidity effects on adsorbed water behavior on BaTiO3 ferroelectric domains 2014; published online 28 August 2014) Distribution of the adsorbed water on BaTiO3 ferroelectric, which adsorb on the material surface, cause delayed cracking and fracture of ferroelectric ceramics.15

Volinsky, Alex A.

446

The Origin of the Superstructure in Bi2Sr2CaCu2O8+? as Revealed by Scanning Tunneling Microscopy  

Science Journals Connector (OSTI)

...be identified and understood. Horibe et al. (1) originally reported that 02 trapped in 2000-year-old ice from Camp Century, Green-land, has an 180/160 enrichment given by 8 (180) = 0.61 per mil versus present-day at-mospheric...

M. D. Kirk; J. Nogami; A. A. Baski; D. B. Mitzi; A. Kapitulnik; T. H. Geballe; C. F. Quate

1988-12-23T23:59:59.000Z

447

Molecular Studies of Surfaces under Reaction Conditions; Sum Frequency Generation Vibrational Spectroscopy, Scanning Tunneling Microscopy and Ambient Pressure X-Ray Photoelectron Spectroscopy  

SciTech Connect (OSTI)

Instruments developed in our laboratory permit the atomic and molecular level study of NPs under reaction conditions (SFG, ambient pressure XPS and high pressure STM). These studies indicate continuous restructuring of the metal substrate and the adsorbate molecules, changes of oxidation states with NP size and surface composition variations of bimetallic NPs with changes of reactant molecules.

Somorjai, G.A.

2009-11-11T23:59:59.000Z

448

Structure, Mobility, and Composition of Transition Metal Catalyst Surfaces: High-Pressure Scanning Tunneling Microscopy and Ambient-Pressure X-ray Photoelectron Spectroscopy Studies  

E-Print Network [OSTI]

bimetallic nanoparticle catalysts is studied in Chapter 8.and Pt-based bimetallic nanoparticle catalysts, in order toseek the influence of catalyst surface structure on

Zhu, Zhongwei

2014-01-01T23:59:59.000Z

449

A scanning electron microscopy study of the effects of starvation-feeding schedules on the development of the statoliths of Fundulus heteroclitus L.  

E-Print Network [OSTI]

sensory rudiment becomes hollowed-out secondarily to form the otic vesicle, the rudiment of the labyrinth (Wilson and Mattocks 1897; Balinsky 1965). In mummichogs the otic vesicles appear 66 hours after fertilization (Armstrong and Child 1965; New 1966... 1969). Passage of hydrogen ions through the chorion accelerates with increasing salinity. The pH of the subchorionic fluid of mummichog eggs changes to approxi- mate that of the environment so changes in pH may affect development (Armstrong 1927...

Leitner, Roxanne

1978-01-01T23:59:59.000Z

450

Influence of Surface Preparation on Scanning Kelvin Probe Microscopy and Electron Backscatter Diffraction Analysis of Cross Sections of CdTe/CdS Solar Cells: Preprint  

SciTech Connect (OSTI)

In this work we investigated different methods to prepare cross sections of CdTe/CdS solar cells for EBSD and SKPM analyses. We observed that procedures used to prepare surfaces for EBSD are not suitable to prepare cross sections, and we were able to develop a process using polishing and ion-beam milling. This process resulted in very good results and allowed us to reveal important aspects of the cross section of the CdTe film. For SKPM, polishing and a light ion-beam milling resulted in cross sections that provided good data. We were able to observe the depletion region on the CdTe film and the p-n junction as well as the interdiffusion layer between CdTe and CdS. However, preparing good-quality cross sections for SKPM is not a reproducible process, and artifacts are often observed.

Moutinho, H. R.; Dhere, R. G.; Jiang, C. S.; Al-Jassim, M. M.

2011-06-01T23:59:59.000Z

451

Bridging the pressure gap: In situ atomic-level investigations of model platinum catalyst surfaces under reaction conditions by scanning tunneling microscopy  

SciTech Connect (OSTI)

Results of this thesis show that STM measurements can provide information about the surfaces and their adsorbates. Stability of Pt(110) under high pressures of H2, O2, and CO was studied (Chap. 4). In situ UHV and high vacuum experiments were carried out for sulfur on Pt(111) (Chap.5). STM studies of CO/S/Pt(111) in high CO pressures showed that the Pt substrate undergoes a stacking-fault-domain reconstruction involving periodic transitions from fcc to hcp stacking of top-layer atoms (Chap.6). In Chap.7, the stability of propylene on Pt(111) and the decomposition products were studied in situ with the HPSTM. Finally, in Chap.8, results are presented which show how the Pt tip of the HPSTM was used to locally rehydrogenate and oxidize carbonaceous clusters deposited on the Pt(111) surface; the Pt tip acted as a catalyst after activation by short voltage pulses.

McIntyre, B.J.

1994-05-01T23:59:59.000Z

452

Atomic-Scale Spin-Polarized Scanning Tunneling Microscopy Applied To Mn3N2(010) Haiqiang Yang and Arthur R. Smith  

E-Print Network [OSTI]

and Arthur R. Smith Condensed Matter and Surface Science Program, Department of Physics and Astronomy, Ohio

453

Grain boundary atomic structures and light-element visualization in ceramics: combination of Cs-corrected scanning transmission electron microscopy and first-principles calculations  

Science Journals Connector (OSTI)

......materials for electrolytes in solid oxide fuel cells and catalysis because of their unique...electrochemical processes occurring during the battery use. Figure-13a shows an HAADF-STEM...behavior and capacity fade in lithium ion batteries with LiMn2O4 as the cathode material......

Yuichi Ikuhara

2011-08-01T23:59:59.000Z

454

Investigating the relationship between the superconducting and pseudogap states of the high-temperature superconductor Bi-2201 using scanning tunneling microscopy  

E-Print Network [OSTI]

There is considerable controversy regarding the nature of the relationship between the superconducting and pseudogap states of high-temperature superconductors. Although there exist a large number of theories regarding ...

Boyer, Michael Christopher

2008-01-01T23:59:59.000Z

455

Scanning Josephson Tunneling Microscopy of Single Crystal Bi2Sr2CaCu2O8+delta with a Conventional Superconducting Tip  

E-Print Network [OSTI]

materials in the Josephson junction where, Ic is theYBCO) single crystal Josephson junctions can be explained byfor Pb/I/Pb STM Josephson junctions near zero bias with

Kimura, H.

2010-01-01T23:59:59.000Z

456

Structure, defects, and impurities at the rutile TiO2(011)-(2 1) surface: A scanning tunneling microscopy study  

E-Print Network [OSTI]

Available online 21 July 2006 Abstract The titanium dioxide rutile (011) (equivalent to (101)) surface boundaries 1. Introduction Titanium dioxide is a versatile material that finds appli- cations in a wide range) structure are active adsorption sites. Segregation of calcium impurities from the bulk results in an ordered

Diebold, Ulrike

457

Electrostatically focused addressable field emission array chips (AFEA's) for high-speed massively parallel maskless digital E-beam direct write lithography and scanning electron microscopy  

DOE Patents [OSTI]

Systems and methods are described for addressable field emission array (AFEA) chips. A method of operating an addressable field-emission array, includes: generating a plurality of electron beams from a pluralitly of emitters that compose the addressable field-emission array; and focusing at least one of the plurality of electron beams with an on-chip electrostatic focusing stack. The systems and methods provide advantages including the avoidance of space-charge blow-up.

Thomas, Clarence E. (Knoxville, TN); Baylor, Larry R. (Farragut, TN); Voelkl, Edgar (Oak Ridge, TN); Simpson, Michael L. (Knoxville, TN); Paulus, Michael J. (Knoxville, TN); Lowndes, Douglas H. (Knoxville, TN); Whealton, John H. (Oak Ridge, TN); Whitson, John C. (Clinton, TN); Wilgen, John B. (Oak Ridge, TN)

2002-12-24T23:59:59.000Z

458

Wavefunction Imaging Scanning Tunneling Microscopy K. McElroy, J. Lee, J. E. Hoffman, E.W. Hudson, K. M. Lang, & J. C. Seamus Davis  

E-Print Network [OSTI]

: lab lined with Sonex vacuum lines Ultra Low Vibration lab Design 91114I02 5.5" sq at 1.5", 2.75" 0 256) Nature 411, 920 (2001) Cuprate High-Tc Studies 1. Atomic ­ resolution mK- STM 2. Local state tunneling in GaAs (at TmK) we have demonstrated ....... 128 � -8 -6 -4 -2 0 2 4 6 8 0 5 10 15 20 Differential

Davis, James C.

459

Structure, Mobility, and Composition of Transition Metal Catalyst Surfaces: High-Pressure Scanning Tunneling Microscopy and Ambient-Pressure X-ray Photoelectron Spectroscopy Studies  

E-Print Network [OSTI]

in this thesis, including UHV and AES, are also brieflysurfaces need to be prepared in UHV, since samples will bethan the terraces in UHV, implying the partial reversibility

Zhu, Zhongwei

2014-01-01T23:59:59.000Z

460

Intrinsic current-voltage properties of nanowires with four-probe scanning tunneling microscopy: A conductance transition of ZnO nanowire  

E-Print Network [OSTI]

strain. The ZnO-nanowire samples used in our experiments were synthesized via reduction and oxidation of ZnS powder13 and dispersed on a silicon wafer coated with a 500-nm-thick silicon dioxide layer as insulator. The STM tips were made from a tungsten or gold wire using the stan- dard preparation proce

Liu, Feng

Note: This page contains sample records for the topic "microscopy near-field scanning" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Vacancy migration, adatom motion, a.nd atomic bistability on the GaAs(110) surface studied by scanning tunneling microscopy  

E-Print Network [OSTI]

Vacancy migration, adatom motion, a.nd atomic bistability on the GaAs(110) surface studied temperature are reported. The slow dynamic behavior of vacancies and As adatoms can be resolved within a time scale of about one minute, The vacancies and As adatoms are observed to move preferably along the [110

462

Nanoprobes for Future Generations of Photovoltaics  

SciTech Connect (OSTI)

In this Solar Program Review Meeting, we report on our most recent progress in scanning probe microscopy (SPM) and its application to photovoltaics. We have developed an SPM to be operated in combination with a scanning electron microscope (SEM) JEOL5800. The SPM platform is compatible with a helium closed-circuit cryostat and fully accessible to the optics of the cathodoluminescence (CL) detectors with which the JEOL5800 is equipped. Among the innovative modes of operation that the combination --and synergy-- of SPM and electron microscopy provides, we describe (i) measurements of the lateral electron transport based on scanning tunneling microscopy (STM) and atomic force microscopy (AFM); (ii) scanning tunneling luminescence (STL); (iii) electroluminescence mapping; and (iv) near-field cathodoluminescence.

Romero, M. J.; Jiang, C.-S.; Moutinho, H. R.; Al-Jassim, M. M.

2005-11-01T23:59:59.000Z

463

International Scan on Pedestrian and Bicyclist Safety and Mobility  

E-Print Network [OSTI]

­ Differences in culture and behavior, but these can adapt over time ­ Typical safety evaluations mayInternational Scan on Pedestrian and Bicyclist Safety and Mobility: May 2009 Sponsored by Federal Pedestrian and Bicyclist Safety and Mobility ­ Policy ­ Engineering ­ Education ­ Enforcement · Safe Routes

Bertini, Robert L.

464

Scanning tunneling spectroscopy of suspended single-wall carbon nanotubes  

E-Print Network [OSTI]

Scanning tunneling spectroscopy of suspended single-wall carbon nanotubes B. J. LeRoy,a) S. G-wall carbon nanotubes that are freely suspended over a trench. The nanotubes were grown by chemical vapor on the freestanding portions of the nanotubes. Spatially resolved spectroscopy on the suspended portion of both

Dekker, Cees

465

Surround structured lighting: 3-D scanning with orthographic illumination  

Science Journals Connector (OSTI)

This paper presents a new system for rapidly acquiring complete 3-D surface models using a single orthographic structured light projector, a pair of planar mirrors, and one or more synchronized cameras. Using the mirrors, we project structured light ... Keywords: 3-D reconstruction, Full object scanning, Gray codes, Orthographic projection, Structured lighting

Douglas Lanman; Daniel Crispell; Gabriel Taubin

2009-11-01T23:59:59.000Z

466

Icon Scanning: Towards Next Generation QR Codes Itamar Friedman  

E-Print Network [OSTI]

Icon Scanning: Towards Next Generation QR Codes Itamar Friedman Technion Haifa, Israel itamarf-friendly way to obtain this particular applica- tion could be by taking a snapshot of its corresponding icon be thought of as icons with a binary pattern. In this paper we extend this to App-icons and propose

Zelnik-Manor, Lihi - Zelnik-Manor, Lihi

467

ProScan IITM 1 Table of Contents  

E-Print Network [OSTI]

an Existing Stage 19 4.2 Fitting the ProScan Stage 19 4.3 Cable Connections 20 4.4 USB Operation 20 4.5 Focus only to designated power sources as marked on the product. · Make sure the electrical cord is located manufacturers overstate thei

Gardel, Margaret

468

A Rapid Scanning Inspection Method for Insulated Ferromagnetic Tubing  

E-Print Network [OSTI]

Until the present there has been no effective way to rapidly scan thermally insulated refinery or process piping for corrosion or thin wall. Such defects, if left unattended, can lead to wasteful losses of time, energy and money. To date the most...

Marsh, G. M.; Milewits, M.

1984-01-01T23:59:59.000Z

469

Nmap in the Enterprise: Your Guide to Network Scanning  

Science Journals Connector (OSTI)

Nmap, or Network Mapper, is a free, open source tool that is available under the GNU General Public License as published by the Free Software Foundation. It is most often used by network administrators and IT security professionals to scan corporate ... Keywords: Networking, Security

Angela Orebaugh; Becky Pinkard

2008-02-01T23:59:59.000Z

470

Inverse scattering for rotationally scanned optical coherence tomography  

E-Print Network [OSTI]

Inverse scattering for rotationally scanned optical coherence tomography Daniel L. Marks, Tyler S May 16, 2006; posted May 26, 2006 (Doc. ID 67358) Optical coherence tomography of luminal structures coherence tomography1,2 (OCT), is determined in large part by the degree to which the images provide

Bhargava, Rohit

471

A novel image hash algorithm resistant to print-scan  

Science Journals Connector (OSTI)

With the rapid development of multimedia technology, how to establish the integrity of images has become an unavoidable problem. The transform between a digital image and its hard-copy makes the problem more complex. To simplify the content based authentication, ... Keywords: Image hashing, Perceptual hashing, Print, Radon, Scan, Wavelet

Di Wu; Xuebing Zhou; Xiamu Niu

2009-12-01T23:59:59.000Z

472

3D Scanning for Biometric Identification and Verification  

E-Print Network [OSTI]

June 2010 3D Scanning for Biometric Identification and Verification Project Leads Anselmo Lastra visibility, cannot be controlled. A relatively new biometric, 3D facial recognition, holds great promise performance using 3D shape and texture matched that of the much more mature technologies of high

McShea, Daniel W.

473

Processing data from scanning gauges on industrial web processes  

Science Journals Connector (OSTI)

This paper considers the processing of data collected by scanning gauges from industrial web processes such as metal rolling, coating, paper making and plastic film extrusion. It describes a method based upon the generalised sampling theorem for reconstructing ... Keywords: Cross-directional control, Gauging, Sampling, Two-dimensional systems, Web processes

Stephen Duncan; Peter Wellstead

2004-03-01T23:59:59.000Z

474

X-ray Microscopy and Imaging (XSD-XMI)  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Imaging (XMI) Imaging (XMI) About XMI Science and Research Beamlines Highlights Software and Tools Intranet Search APS... Argonne Home > Advanced Photon Source > Contacts FAQs Beamlines News Publications APS Email Portal APS Intranet APS Phonebook APS Quick Links for Users APS Safety and Training Welcome to the X-ray Microscopy and Imaging group (XMI)! X-ray Microscopy and Imaging is part of the X-ray Science Division at the Advanced Photon Source. We develop and support a diverse and multidisciplinary user research program at Sectors 2 and 32 of the APS, with the overall goal to image and study materials structures at spatial and temporal resolutions that are most scientifically relevant to the cutting-edge advances in materials, biological, environmental, and biomedical sciences. To achieve this goal, we actively engage in various research activities including

475

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

476

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

477

CFN Operations and Safety Awareness (COSA) Checklist Electron Microscopy Facility  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Electron Microscopy Facility Electron Microscopy Facility Building 735 This COSA form must be completed for all experimenters working in the CFN and must be submitted to the CFN User Office for badge access. CFN Safety Awareness Policy: Each user must be instructed in the safe procedures in CFN related activities. CFN Facility Laboratory personnel shall keep readily available all relevant instructions and safety literature. Employee/Guest Name Life/Guest Number Department/Division ES&H Coordinator/Ext. Facility Manager COSA Trainer Guest User Staff USER ADMINISTRATION Checked in at User Administration and has valid BNL ID badge Safety Approval Form (SAF) approved. Training requirements completed (Indicate additional training specified in SAF or ESR in lines provided below):

478

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

479

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

480

NCEM National Center for Electron Microscopy: About NCEM  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

NCEM NCEM The National Center for Electron Microscopy (NCEM) is one of the world's foremost centers for electron microscopy and microcharacterization. It is an Office of Science User Facility operated for the U.S. Department of Energy by Lawrence Berkeley National Laboratory. Located adjacent to the University of California, Berkeley, NCEM was established in 1983 to maintain a forefront research center for electron-optical characterization of materials with state-of-the-art instrumentation and expertise. As a national user facility, NCEM is open to scientists from universities, government and industrial laboratories. The center provides cutting-edge instrumentation, techniques and expertise for advanced electron beam microcharacterization of materials at high spatial

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481

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

482

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

483

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

484

Single molecule microscopy in 3D cell cultures and tissues  

Science Journals Connector (OSTI)

Abstract From the onset of the first microscopic visualization of single fluorescent molecules in living cells at the beginning of this century, to the present, almost routine application of single molecule microscopy, the method has well-proven its ability to contribute unmatched detailed insight into the heterogeneous and dynamic molecular world life is composed of. Except for investigations on bacteria and yeast, almost the entire story of success is based on studies on adherent mammalian 2D cell cultures. However, despite this continuous progress, the technique was not able to keep pace with the move of the cell biology community to adapt 3D cell culture models for basic research, regenerative medicine, or drug development and screening. In this review, we will summarize the progress, which only recently allowed for the application of single molecule microscopy to 3D cell systems and give an overview of the technical advances that led to it. While initially posing a challenge, we finally conclude that relevant 3D cell models will become an integral part of the on-going success of single molecule microscopy.

Florian M. Lauer; Elke Kaemmerer; Tobias Meckel

2014-01-01T23:59:59.000Z

485

Sample mounting and transfer for coupling an ultrahigh vacuum variable temperature beetle scanning tunneling microscope with conventional surface probes  

SciTech Connect (OSTI)

We present a new ultrahigh vacuum (UHV) chamber for surface analysis and microscopy at controlled, variable temperatures. The new instrument allows surface analysis with Auger electron spectroscopy, low energy electron diffraction, quadrupole mass spectrometer, argon ion sputtering gun, and a variable temperature scanning tunneling microscope (VT-STM). In this system, we introduce a novel procedure for transferring a sample off a conventional UHV manipulator and onto a scanning tunneling microscope in the conventional ''beetle'' geometry, without disconnecting the heating or thermocouple wires. The microscope, a modified version of the Besocke beetle microscope, is mounted on a 2.75 in. outer diameter UHV flange and is directly attached to the base of the chamber. The sample is attached to a tripod sample holder that is held by the main manipulator. Under UHV conditions the tripod sample holder can be removed from the main manipulator and placed onto the STM. The VT-STM has the capability of acquiring images between the temperature range of 180--500 K. The performance of the chamber is demonstrated here by producing an ordered array of island vacancy defects on a Pt(111) surface and obtaining STM images of these defects.

Nafisi, Kourosh; Ranau, Werner; Hemminger, John C.

2001-01-01T23:59:59.000Z

486

NCEM National Center for Electron Microscopy: Microscopes and Facilities:  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

0.5 0.5 The TEAM 0.5 microscope is a double-aberration-corrected (scanning) transmission electron microscope (STEM/TEM) capable of producing images with 50 pm resolution. The basic instrument is a modified FEI Titan 80-300 microscope equipped with a special high-brightness Schottky-field emission electron source, a gun monochromator, a high-resolution GIF Tridiem energy-filter, and two CEOS hexapole-type spherical aberration correctors. The illumination aberration corrector corrects coherent axial aberrations up to 4th order, as well as 5th order spherical aberration and six-fold astigmatism. The imaging aberration corrector fully corrects for coherent axial aberrations up to 3rd order and partially compensates for 4th and 5th order aberrations. The microscope has two 2048x2048 slow-scan CCD

487

Atom probe field ion microscopy and related topics: A bibliography 1991  

SciTech Connect (OSTI)

This report contains a bibliography for 1991 on the following topics: Atom probe field ion microscopy; field desorption mass spectrometry; field emission; field ion microscopy; and field emission theory.

Russell, K.F.; Miller, M.K.

1993-01-01T23:59:59.000Z

488

Cellular resolution ex vivo imaging of gastrointestinal tissues with coherence microscopy  

E-Print Network [OSTI]

Optical coherence microscopy (OCM) combines confocal microscopy and optical coherence tomography (OCT) to improve imaging depth and contrast, enabling cellular imaging in human tissues. We aim to investigate OCM for ex ...

Fujimoto, James G.

489

Comparison between direct methods for determination of microbial cell volume: electron microscopy and electronic particle sizing.  

Science Journals Connector (OSTI)

...than those processed for electronic particle sizing, reflecting...Electron Microscopy and Electronic Particle Sizing E. MONTESINOS...ofMicrobiology and Institute for Fundamental Biology, Autonomous University...transmission electron microscopy and electronic particle sizing. Statistically...

E Montesinos; I Esteve; R Guerrero

1983-05-01T23:59:59.000Z

490

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Wednesday, 31 August 2005 00:00...

491

Towards automatic cell identi cation in DIC microscopy , C.A. Glasbey2y  

E-Print Network [OSTI]

1998. Journal of Microscopy, 192, 186-193. #12;a b c Figure 1: DIC microscope images: a Chlorella algal

Stone, J. V.

492

Monte Carlo simulation of gamma ray scanning gauge  

SciTech Connect (OSTI)

A gamma ray scanning gauge was simulated with Monte Carlo to study the properties of gamma scanning gauges and to resolve the counts coming from a {sup 235}U source from those coming from a contaminant ({sup 232}U) whose daughters emit high energy gamma rays. The simulation has been used to infer the amount of the {sup 232}U contaminant in a {sup 235}U source to select the best size for the NaI(Tl) detector crystal to minimize the effect of the contaminant. The results demonstrate that Monte Carlo simulation provides a systematic tool for designing a gauge with desired properties and for estimating properties of the gamma source from measured count rates.

Hartfield, G.L.; Freeman, L.B.; Dei, D.E.; Emert, C.J.; Glickstein, S.S.; Kahler, A.C.; Niedzwecki, P.F.

1990-12-31T23:59:59.000Z

493

Measurement of Semiconductor Surface Potential using the Scanning Electron Microscope  

SciTech Connect (OSTI)

We calibrate the secondary electron signal from a standard scanning electron microscope to voltage, yielding an image of the surface or near-surface potential. Data on both atomically abrupt heterojunction GaInP/GaAs and diffused homojunction Si solar cell devices clearly show the expected variation in potential with position and applied bias, giving depletion widths and locating metallurgical junctions to an accuracy better than 10 nm. In some images, distortion near the p-n junction is observed, seemingly consistent with the effects of lateral electric fields (patch fields). Reducing the tube bias removes this distortion. This approach results in rapid and straightforward collection of near-surface potential data using a standard scanning electron microscope.

Heath, J. T.; Jiang, C. S.; Al-Jassim, M. M.

2012-02-15T23:59:59.000Z

494

Nuclear emission microscopies B.L. Doyle a,*, D.S. Walsh a  

E-Print Network [OSTI]

Nuclear emission microscopies B.L. Doyle a,*, D.S. Walsh a , S.N. Renfrow a,b , G. Vizkelethy a,1 Abstract Alternatives to traditional nuclear microprobe analysis (NMA) emerged two years ago with the invention of ion electron emission microscopy (IEEM). With nuclear emission microscopy (NEM) the ion beam

495

Electron Microscopy of Myosin Molecules from Muscle and Non-Muscle Sources  

Science Journals Connector (OSTI)

...1976 research-article Electron Microscopy of Myosin...Muscle and Non-Muscle Sources A. Elliott G. Offer...give the two heads). Electron microscopy of myosin...muscle and non-muscle sources. | Journal Article...Chickens Microscopy, Electron Muscle Proteins Myosins...

1976-01-01T23:59:59.000Z

496

Metastatic cardiac tumor demonstrated by 201 thallium scan  

SciTech Connect (OSTI)

A patient with bronchogenic carcinoma had an electrocardiogram that was initially thought to be consistent with myocardial infarction and possible left ventricular aneurysm. A heart scan with radioactive 201 thallium showed an area of sharply diminished uptake cold spot; however, subsequent thoracotomy showed that this was caused by local pericardial and myocardial infiltration by tumor. This suggests a role for radioactive 201 thallium in the detection of cardiac metastatic tumors.

Lubell, D.L.; Goldfarb, C.R.

1980-07-01T23:59:59.000Z

497

A novel solid-angle tomosynthesis (SAT) scanning scheme  

SciTech Connect (OSTI)

Purpose: Digital tomosynthesis (DTS) recently gained extensive research interests in both diagnostic and radiation therapy fields. Conventional DTS images are generated by scanning an x-ray source and flat-panel detector pair on opposite sides of an object, with the scanning trajectory on a one-dimensional curve. A novel tomosynthesis method named solid-angle tomosynthesis (SAT) is proposed, where the x-ray source scans on an arbitrary shaped two-dimensional surface. Methods: An iterative algorithm in the form of total variation regulated expectation maximization is developed for SAT image reconstruction. The feasibility and effectiveness of SAT is corroborated by computer simulation studies using three-dimensional (3D) numerical phantoms including a 3D Shepp-Logan phantom and a volumetric CT image set of a human breast. Results: SAT is able to cover more space in Fourier domain more uniformly than conventional DTS. Greater coverage and more isotropy in the frequency domain translate to fewer artifacts and more accurately restored features in the in-plane reconstruction. Conclusions: Comparing with conventional DTS, SAT allows cone-shaped x-ray beams to project from more solid angles, thus provides more coverage in the spatial-frequency domain, resulting in better quality of reconstructed image.

Zhang Jin; Yu, Cedric [Department of Radiation Oncology, University of Maryland School of Medicine, 22 S. Greene Street, Baltimore, Maryland 21201 and Xcision Medical System, LLC, 12707 Chapel Chase Drive, Clarksville, Maryland 21209 (United States)

2010-08-15T23:59:59.000Z

498

Alignment and Aperture Scan at the Fermilab Booster  

SciTech Connect (OSTI)

The Fermilab Booster is currently in the process of an intensity upgrade referred to as the Proton Improvement Plan (PIP). The goal of PIP is to have the Booster provide a proton beam flux of 2 x 10{sup 17} protons/hour. This is almost double the current operation of 1.1 x 10{sup 17} protons/hour. Beam losses in the machine due to the increased flux will create larger integrated doses on aperture limiting components that will need to be mitigated. The Booster accelerates beam from 400 MeV to 8 GeV at a rep rate of 15hz and then extracts beam to the Main Injector. Several percent of the beam is lost within 3 msec after injection in the early part of acceleration. The aperture at injection energy was recently measured using corrector scans. Along with magnet survey data and aperture scan data a plan to realign the magnets in the Booster was developed and implemented in May 2012. The beam studies, analysis of the scan and alignment data, and the result of the magnet moves are presented.

Seiya, K.; Lackey, J.; Marsh, W.; Pellico, W.; Still, D.; Triplet, K.; Waller, A.; /Fermilab

2012-05-01T23:59:59.000Z

499

Cryogenic X-Ray Diffraction Microscopy for Biological Samples  

Science Journals Connector (OSTI)

X-ray diffraction microscopy (XDM) is well suited for nondestructive, high-resolution biological imaging, especially for thick samples, with the high penetration power of x rays and without limitations imposed by a lens. We developed nonvacuum, cryogenic (cryo-) XDM with hard x rays at 8 keV and report the first frozen-hydrated imaging by XDM. By preserving samples in amorphous ice, the risk of artifacts associated with dehydration or chemical fixation is avoided, ensuring the imaging condition closest to their natural state. The reconstruction shows internal structures of intact D. radiodurans bacteria in their natural contrast.

Enju Lima; Lutz Wiegart; Petra Pernot; Malcolm Howells; Joanna Timmins; Federico Zontone; Anders Madsen

2009-11-05T23:59:59.000Z

500

Cryogenic X-ray Diffraction Microscopy for Biological Samples  

SciTech Connect (OSTI)

X-ray diffraction microscopy (XDM) is well suited for nondestructive, high-resolution biological imaging, especially for thick samples, with the high penetration power of x rays and without limitations imposed by a lens. We developed nonvacuum, cryogenic (cryo-) XDM with hard x rays at 8 keV and report the first frozen-hydrated imaging by XDM. By preserving samples in amorphous ice, the risk of artifacts associated with dehydration or chemical fixation is avoided, ensuring the imaging condition closest to their natural state. The reconstruction shows internal structures of intact D. radiodurans bacteria in their natural contrast.

E Lima; L Wiegart; P Pernot; M Howells; J Timmins; F Zontone; A Madsen

2011-12-31T23:59:59.000Z