National Library of Energy BETA

Sample records for methods analyte line

  1. Hydrogen Fuel Quality - Focus: Analytical Methods Development...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Fuel Quality - Focus: Analytical Methods Development & Hydrogen Fuel Quality Results Hydrogen Fuel Quality - Focus: Analytical Methods Development & Hydrogen Fuel Quality Results ...

  2. CRUCIBLE LINING METHOD

    DOE Patents [OSTI]

    Bone, W.H.; Schmidt, W.W.

    1958-11-01

    A method is presented for forming refractory liners in cylindrical reaction vessels used for the reductlon of uranium tetrafluoride to metallic uranium. A preliminary form, having positioning lugs attached thereto, is inserted into the reaction vessel and the refractory powder, usually CaO, is put in the annular space between the form and the inner wall of the reaction vessel. A jolting table is used to compact this charge of liner material ln place, and after thls has been done, the preliminary form is removed and the flnal form or plug is lnserted without disturbing the partially completed lining. The remainder of the lining charge is then introduced and compacted by jolting, after which the form is removed.

  3. SASSI Analytical Methods Compared with SHAKE Results | Department...

    Office of Environmental Management (EM)

    Analytical Methods Compared with SHAKE Results SASSI Analytical Methods Compared with SHAKE Results SASSI Analytical Methods Compared with SHAKE Results Structural Mechanics - SRS...

  4. Method of identity analyte-binding peptides

    DOE Patents [OSTI]

    Kauvar, Lawrence M.

    1990-01-01

    A method for affinity chromatography or adsorption of a designated analyte utilizes a paralog as the affinity partner. The immobilized paralog can be used in purification or analysis of the analyte; the paralog can also be used as a substitute for antibody in an immunoassay. The paralog is identified by screening candidate peptide sequences of 4-20 amino acids for specific affinity to the analyte.

  5. Method of identity analyte-binding peptides

    DOE Patents [OSTI]

    Kauvar, L.M.

    1990-10-16

    A method for affinity chromatography or adsorption of a designated analyte utilizes a paralog as the affinity partner. The immobilized paralog can be used in purification or analysis of the analyte; the paralog can also be used as a substitute for antibody in an immunoassay. The paralog is identified by screening candidate peptide sequences of 4--20 amino acids for specific affinity to the analyte. 5 figs.

  6. Method and apparatus for detecting an analyte

    DOE Patents [OSTI]

    Allendorf, Mark D.; Hesketh, Peter J.

    2011-11-29

    We describe the use of coordination polymers (CP) as coatings on microcantilevers for the detection of chemical analytes. CP exhibit changes in unit cell parameters upon adsorption of analytes, which will induce a stress in a static microcantilever upon which a CP layer is deposited. We also describe fabrication methods for depositing CP layers on surfaces.

  7. Biodiesel Analytical Methods: August 2002--January 2004

    SciTech Connect (OSTI)

    Van Gerpen, J.; Shanks, B.; Pruszko, R.; Clements, D.; Knothe, G.

    2004-07-01

    Biodiesel is an alternative fuel for diesel engines that is receiving great attention worldwide. The material contained in this book is intended to provide the reader with information about biodiesel engines and fuels, analytical methods used to measure fuel properties, and specifications for biodiesel quality control.

  8. Statistically qualified neuro-analytic failure detection method and system

    DOE Patents [OSTI]

    Vilim, Richard B.; Garcia, Humberto E.; Chen, Frederick W.

    2002-03-02

    An apparatus and method for monitoring a process involve development and application of a statistically qualified neuro-analytic (SQNA) model to accurately and reliably identify process change. The development of the SQNA model is accomplished in two stages: deterministic model adaption and stochastic model modification of the deterministic model adaptation. Deterministic model adaption involves formulating an analytic model of the process representing known process characteristics, augmenting the analytic model with a neural network that captures unknown process characteristics, and training the resulting neuro-analytic model by adjusting the neural network weights according to a unique scaled equation error minimization technique. Stochastic model modification involves qualifying any remaining uncertainty in the trained neuro-analytic model by formulating a likelihood function, given an error propagation equation, for computing the probability that the neuro-analytic model generates measured process output. Preferably, the developed SQNA model is validated using known sequential probability ratio tests and applied to the process as an on-line monitoring system. Illustrative of the method and apparatus, the method is applied to a peristaltic pump system.

  9. Analytical methods for optical remote sensing

    SciTech Connect (OSTI)

    Spellicy, R.L.

    1997-12-31

    Optical monitoring systems are very powerful because of their ability to see many compounds simultaneously as well as their ability to report results in real time. However, these strengths also present unique problems to analysis of the resulting data and validation of observed results. Today, many FTIR and UV-DOAS systems are in use. Some of these are manned systems supporting short term tests while others are totally unmanned systems which are expected to operate without intervention for weeks or months at a time. The analytical methods needed to support both the diversity of compounds and the diversity of applications is challenging. In this paper, the fundamental concepts of spectral analysis for IR/UV systems are presented. This is followed by examples of specific field data from both short term measurement programs looking at unique sources and long-term unmanned monitoring systems looking at ambient air.

  10. Combined surface analytical methods to characterize degradative...

    Office of Scientific and Technical Information (OSTI)

    a silane monolayer, and local displacement of silane molecules from the Si surface.more We have applied this analytical methodology at the Si coupon level up to MEMS devices. ...

  11. ANALYTICAL METHOD FOR THE VOLUMETRIC DETERMINATION OF MOLYBDENUM...

    Office of Scientific and Technical Information (OSTI)

    THE VOLUMETRIC DETERMINATION OF MOLYBDENUM IN URANIUM- MOLYBDENUM ALLOY Citation Details In-Document Search Title: ANALYTICAL METHOD FOR THE VOLUMETRIC DETERMINATION OF MOLYBDENUM ...

  12. SASSI Analytical Methods Compared with SHAKE Free-Field Results

    Office of Environmental Management (EM)

    Analytical Methods Compared with SHAKE Results Structural Mechanics - SRS October 4, 2011 1 Objective This study presents a methodology for validating SASSI for use with a...

  13. Analytical instruments, ionization sources, and ionization methods

    DOE Patents [OSTI]

    Atkinson, David A.; Mottishaw, Paul

    2006-04-11

    Methods and apparatus for simultaneous vaporization and ionization of a sample in a spectrometer prior to introducing the sample into the drift tube of the analyzer are disclosed. The apparatus includes a vaporization/ionization source having an electrically conductive conduit configured to receive sample particulate which is conveyed to a discharge end of the conduit. Positioned proximate to the discharge end of the conduit is an electrically conductive reference device. The conduit and the reference device act as electrodes and have an electrical potential maintained between them sufficient to cause a corona effect, which will cause at least partial simultaneous ionization and vaporization of the sample particulate. The electrical potential can be maintained to establish a continuous corona, or can be held slightly below the breakdown potential such that arrival of particulate at the point of proximity of the electrodes disrupts the potential, causing arcing and the corona effect. The electrical potential can also be varied to cause periodic arcing between the electrodes such that particulate passing through the arc is simultaneously vaporized and ionized. The invention further includes a spectrometer containing the source. The invention is particularly useful for ion mobility spectrometers and atmospheric pressure ionization mass spectrometers.

  14. Analytical chemistry methods for metallic core components: Revision March 1985

    SciTech Connect (OSTI)

    Not Available

    1985-03-01

    This standard provides analytical chemistry methods for the analysis of alloys used to fabricate core components. These alloys are 302, 308, 316, 316-Ti, and 321 stainless steels and 600 and 718 Inconels and they may include other 300-series stainless steels.

  15. Line-of-sight deposition method

    DOE Patents [OSTI]

    Patten, James W.; McClanahan, Edwin D.; Bayne, Michael A.

    1981-01-01

    A line-of-sight method of depositing a film having substantially 100% of theoretical density on a substrate. A pressure vessel contains a target source having a surface thereof capable of emitting particles therefrom and a substrate with the source surface and the substrate surface positioned such that the source surface is substantially parallel to the direction of the particles impinging upon the substrate surface, the distance between the most remote portion of the substrate surface receiving the particles and the source surface emitting the particles in a direction parallel to the substrate surface being relatively small. The pressure in the vessel is maintained less than about 5 microns to prevent scattering and permit line-of-sight deposition. By this method the angles of incidence of the particles impinging upon the substrate surface are in the range of from about 45.degree. to 90.degree. even when the target surface area is greatly expanded to increase the deposition rate.

  16. Line-of-sight deposition method

    DOE Patents [OSTI]

    Patten, J.W.; McClanahan, E.D.; Bayne, M.A.

    1980-04-16

    A line-of-sight method of depositing a film having substantially 100% of theoretical density on a substrate. A pressure vessel contains a target source having a surface thereof capable of emitting particles therefrom and a substrate with the source surface and the substrate surface positioned such that the source surface is substantially parallel to the direction of the particles impinging upon the substrate surface, the distance between the most remote portion of the substrate surface receiving the particles and the source surface emitting the particles in a direction parallel to the substrate surface being relatively small. The pressure in the vessel is maintained less than about 5 microns to prevent scattering and permit line-of-sight deposition. By this method the angles of incidence of the particles impinging upon the substrate surface are in the range of from about 45/sup 0/ to 90/sup 0/ even when the target surface area is greatly expanded to increase the deposition rate.

  17. Estimating Fuel Cycle Externalities: Analytical Methods and Issues, Report 2

    SciTech Connect (OSTI)

    Barnthouse, L.W.; Cada, G.F.; Cheng, M.-D.; Easterly, C.E.; Kroodsma, R.L.; Lee, R.; Shriner, D.S.; Tolbert, V.R.; Turner, R.S.

    1994-07-01

    that also have not been fully addressed. This document contains two types of papers that seek to fill part of this void. Some of the papers describe analytical methods that can be applied to one of the five steps of the damage function approach. The other papers discuss some of the complex issues that arise in trying to estimate externalities. This report, the second in a series of eight reports, is part of a joint study by the U.S. Department of Energy (DOE) and the Commission of the European Communities (EC)* on the externalities of fuel cycles. Most of the papers in this report were originally written as working papers during the initial phases of this study. The papers provide descriptions of the (non-radiological) atmospheric dispersion modeling that the study uses; reviews much of the relevant literature on ecological and health effects, and on the economic valuation of those impacts; contains several papers on some of the more complex and contentious issues in estimating externalities; and describes a method for depicting the quality of scientific information that a study uses. The analytical methods and issues that this report discusses generally pertain to more than one of the fuel cycles, though not necessarily to all of them. The report is divided into six parts, each one focusing on a different subject area.

  18. Method for bonding a transmission line to a downhole tool

    DOE Patents [OSTI]

    Hall, David R.; Fox, Joe

    2007-11-06

    An apparatus for bonding a transmission line to the central bore of a downhole tool includes a pre-formed interface for bonding a transmission line to the inside diameter of a downhole tool. The pre-formed interface includes a first surface that substantially conforms to the outside contour of a transmission line and a second surface that substantially conforms to the inside diameter of a downhole tool. In another aspect of the invention, a method for bonding a transmission line to the inside diameter of a downhole tool includes positioning a transmission line near the inside wall of a downhole tool and placing a mold near the transmission line and the inside wall. The method further includes injecting a bonding material into the mold and curing the bonding material such that the bonding material bonds the transmission line to the inside wall.

  19. Inertial confinement fusion method producing line source radiation fluence

    DOE Patents [OSTI]

    Rose, Ronald P.

    1984-01-01

    An inertial confinement fusion method in which target pellets are imploded in sequence by laser light beams or other energy beams at an implosion site which is variable between pellet implosions along a line. The effect of the variability in position of the implosion site along a line is to distribute the radiation fluence in surrounding reactor components as a line source of radiation would do, thereby permitting the utilization of cylindrical geometry in the design of the reactor and internal components.

  20. Method for Operating a Sensor to Differentiate Between Analytes in a Sample

    DOE Patents [OSTI]

    Kunt, Tekin; Cavicchi, Richard E; Semancik, Stephen; McAvoy, Thomas J

    1998-07-28

    Disclosed is a method for operating a sensor to differentiate between first and second analytes in a sample. The method comprises the steps of determining a input profile for the sensor which will enhance the difference in the output profiles of the sensor as between the first analyte and the second analyte; determining a first analyte output profile as observed when the input profile is applied to the sensor; determining a second analyte output profile as observed when the temperature profile is applied to the sensor; introducing the sensor to the sample while applying the temperature profile to the sensor, thereby obtaining a sample output profile; and evaluating the sample output profile as against the first and second analyte output profiles to thereby determine which of the analytes is present in the sample.

  1. Sensor, method and system of monitoring transmission lines

    DOE Patents [OSTI]

    Syracuse, Steven J.; Clark, Roy; Halverson, Peter G.; Tesche, Frederick M.; Barlow, Charles V.

    2012-10-02

    An apparatus, method, and system for measuring the magnetic field produced by phase conductors in multi-phase power lines. The magnetic field measurements are used to determine the current load on the conductors. The magnetic fields are sensed by coils placed sufficiently proximate the lines to measure the voltage induced in the coils by the field without touching the lines. The x and y components of the magnetic fields are used to calculate the conductor sag, and then the sag data, along with the field strength data, can be used to calculate the current load on the line and the phase of the current. The sag calculations of this invention are independent of line voltage and line current measurements. The system applies a computerized fitter routine to measured and sampled voltages on the coils to accurately determine the values of parameters associated with the overhead phase conductors.

  2. Methods and apparatus for reducing corrosion in refractory linings

    DOE Patents [OSTI]

    Poeppel, Roger B.; Greenberg, Sherman; Diercks, Dwight R.

    1987-01-01

    Methods and apparatus are provided for reducing corrosion in a refractory lining of a liquid-containing vessel used in direct steelmaking processes. The vessel operates at between about 1600.degree. C. and about 1800.degree. C. and an oxygen partial pressure of about 10.sup.-12 atmospheres, creating slag which is rich in FeO. The refractory lining includes a significant level of chromium oxide (Cr.sub.2 O.sub.3), and has small interconnected pores which may be filled with a gas mixture having a higher total pressure and oxygen partial pressure than the total pressure and oxygen partial pressure associted with the liquid against the lining of the vessel. The gas mixture is forced through the pores of the lining so that the pores are continuously filled with the mixture. In this manner, the gas mixture creates a blanket which increases the oxygen partial pressure at the lining enough to maintain the chromium in the lining in a selected valence state in which the chromium has decreased solubility in the FeO slag, thereby reducing corrosion by the FeO and increasing the useful life of the refractory lining.

  3. Analytical methods for determining the reactivity of pyrochemical salts

    SciTech Connect (OSTI)

    Phillips, A.G.; Stakebake, J.L.

    1994-05-01

    Pyrochemical processes used for the purification of plutonium have generated quantities of residue that contain varying amounts of reactive metals such as potassium, sodium, calcium, and magnesium. These residues are currently considered hazardous and are being managed under RCRA because of the reactivity characteristic. This designation is based solely on process knowledge. Currently there is no approved procedure for determining the reactivity of a solid with water. A method is being developed to rapidly evaluate the reactivity of pyrochemical salts with water by measuring the rate of hydrogen generation. The method was initially tested with a magnesium containing pyrochemical salt. A detection limit of approximately 0.004 g of magnesium was established. A surrogate molten salt extraction residue was also tested. Extrapolation of test data resulted in a hydrogen generation rate of 4.4 mg/(g min).

  4. Analytical methods for removing radiological constituents prior to organic analysis

    SciTech Connect (OSTI)

    Hakonson, K.; Monagle, M.; Cournoyer, M.

    1997-12-31

    Within the Department of Energy (DOE), there is a need to analyze mixed waste materials (i.e. materials that are contaminated with both radiological and hazardous components). As part of the technical support the Organic Analysis Group provides for programs within Los Alamos National Laboratory, methods are under development for radiologically contaminated oil samples being tested for polychlorinated biphenyls and other semivolatile constituents. Radionuclides are removed from oil samples by filtering the samples through a commercials available solid phase extraction cartridge. An aliquot of the eluent is then analyzed to quantitate the residual radioactivity.

  5. Analytical Chemistry Laboratory (ACL) procedure compendium. Volume 4, Organic methods

    SciTech Connect (OSTI)

    Not Available

    1993-08-01

    This interim notice covers the following: extractable organic halides in solids, total organic halides, analysis by gas chromatography/Fourier transform-infrared spectroscopy, hexadecane extracts for volatile organic compounds, GC/MS analysis of VOCs, GC/MS analysis of methanol extracts of cryogenic vapor samples, screening of semivolatile organic extracts, GPC cleanup for semivolatiles, sample preparation for GC/MS for semi-VOCs, analysis for pesticides/PCBs by GC with electron capture detection, sample preparation for pesticides/PCBs in water and soil sediment, report preparation, Florisil column cleanup for pesticide/PCBs, silica gel and acid-base partition cleanup of samples for semi-VOCs, concentrate acid wash cleanup, carbon determination in solids using Coulometrics` CO{sub 2} coulometer, determination of total carbon/total organic carbon/total inorganic carbon in radioactive liquids/soils/sludges by hot persulfate method, analysis of solids for carbonates using Coulometrics` Model 5011 coulometer, and soxhlet extraction.

  6. A semi-analytical method for heat sweep calculations in fractured reservoirs

    SciTech Connect (OSTI)

    Pruess, K.; Wu, Y.S.

    1988-01-01

    An analytical approximation is developed for purely conductive heat transfer from impermeable blocks of rock to fluids sweeping past the rocks in fractures. The method was incorporated into a multi-phase fluid and heat flow simulator. Comparison with exact analytical solutions and with simulations using a multiple interacting continua approach shows very good accuracy, with no increase in computing time compared to porous medium simulations. 14 refs., 3 figs., 5 tabs.

  7. A semi-analytical method for heat sweep calculations in fractured reservoirs

    SciTech Connect (OSTI)

    Pruess, K.; Wu, Y.S.

    1988-01-01

    An analytical approximation is developed for purely conductive heat transfer from impermeable blocks of rock to fluids sweeping past the rocks in fractures. The method was incorporated into a multi-phase fluid and heat flow simulator. Comparison with exact analytical solutions and with simulations using a multiple interacting continua approach shows very good accuracy, with no increase in computing time compared to porous medium simulations.

  8. Flammable gas safety program. Analytical methods development: FY 1994 progress report

    SciTech Connect (OSTI)

    Campbell, J.A.; Clauss, S.; Grant, K.; Hoopes, V.; Lerner, B.; Lucke, R.; Mong, G.; Rau, J.; Wahl, K.; Steele, R.

    1994-09-01

    This report describes the status of developing analytical methods to account for the organic components in Hanford waste tanks, with particular focus on tanks assigned to the Flammable Gas Watch List. The methods that have been developed are illustrated by their application to samples obtained from Tank 241-SY-101 (Tank 101-SY).

  9. Existing technology transfer report: analytical capabilities. Volume 2. Appendix A. [Methods and procedures for analysis

    SciTech Connect (OSTI)

    Tewari, K.C.

    1984-06-01

    This volume contains 10 attachments entitled: Monthly progress reports; Method CHN-4 (Carbon, Hydrogen and Nitrogen analysis by Perkin-Elmer elemental analyses); Method Oxygen-6 (oxygen analyzer); Method Nitrogen-8 (Low level nitrogen analysis by Perkin-Elmer 240 elemental analyzer); Method Sulfur-10 (sulfur analysis by oxidative microcoulometry); Method TGA-3 (thermogravimetric analysis of coal liquefaction products and process solvents); Method DSC-5 (Determination of glass transition temperature by differential scanning calorimetry); Method GC-1 (gas chromatography of Fischer-Tropsch products); Method GC-2 (gas chromatography of distillate products from coal liquefaction); Analytical Method No. 1160 (estimation of OH, NH, NH/sub 2/, concentration in methylene chloride soluble materials from SRC liquids); x-ray diffraction method for determining the orientation tendency in calcined coke; and evaluation of mass spectrometers.

  10. Stand-off transmission lines and method for making same

    DOE Patents [OSTI]

    Tuckerman, D.B.

    1991-05-21

    Standoff transmission lines in an integrated circuit structure are formed by etching away or removing the portion of the dielectric layer separating the microstrip metal lines and the ground plane from the regions that are not under the lines. The microstrip lines can be fabricated by a subtractive process of etching a metal layer, an additive process of direct laser writing fine lines followed by plating up the lines or a subtractive/additive process in which a trench is etched over a nucleation layer and the wire is electrolytically deposited. Microstrip lines supported on freestanding posts of dielectric material surrounded by air gaps are produced. The average dielectric constant between the lines and ground plane is reduced, resulting in higher characteristic impedance, less crosstalk between lines, increased signal propagation velocities, and reduced wafer stress. 16 figures.

  11. Stand-off transmission lines and method for making same

    DOE Patents [OSTI]

    Tuckerman, David B.

    1991-01-01

    Standoff transmission lines in an integrated circuit structure are formed by etching away or removing the portion of the dielectric layer separating the microstrip metal lines and the ground plane from the regions that are not under the lines. The microstrip lines can be fabricated by a subtractive process of etching a metal layer, an additive process of direct laser writing fine lines followed by plating up the lines or a subtractive/additive process in which a trench is etched over a nucleation layer and the wire is electrolytically deposited. Microstrip lines supported on freestanding posts of dielectric material surrounded by air gaps are produced. The average dielectric constant between the lines and ground plane is reduced, resulting in higher characteristic impedance, less crosstalk between lines, increased signal propagation velocities, and reduced wafer stress.

  12. Trigonometric and hyperbolic functions method for constructing analytic solutions to nonlinear plane magnetohydrodynamics equilibrium equations

    SciTech Connect (OSTI)

    Moawad, S. M.

    2015-02-15

    In this paper, we present a solution method for constructing exact analytic solutions to magnetohydrodynamics (MHD) equations. The method is constructed via all the trigonometric and hyperbolic functions. The method is applied to MHD equilibria with mass flow. Applications to a solar system concerned with the properties of coronal mass ejections that affect the heliosphere are presented. Some examples of the constructed solutions which describe magnetic structures of solar eruptions are investigated. Moreover, the constructed method can be applied to a variety classes of elliptic partial differential equations which arise in plasma physics.

  13. SRC-I demonstration plant analytical laboratory methods manual. Final technical report

    SciTech Connect (OSTI)

    Klusaritz, M.L.; Tewari, K.C.; Tiedge, W.F.; Skinner, R.W.; Znaimer, S.

    1983-03-01

    This manual is a compilation of analytical procedures required for operation of a Solvent-Refined Coal (SRC-I) demonstration or commercial plant. Each method reproduced in full includes a detailed procedure, a list of equipment and reagents, safety precautions, and, where possible, a precision statement. Procedures for the laboratory's environmental and industrial hygiene modules are not included. Required American Society for Testing and Materials (ASTM) methods are cited, and ICRC's suggested modifications to these methods for handling coal-derived products are provided.

  14. Method and apparatus for continuous fluid leak monitoring and detection in analytical instruments and instrument systems

    DOE Patents [OSTI]

    Weitz, Karl K.; Moore, Ronald J.

    2010-07-13

    A method and device are disclosed that provide for detection of fluid leaks in analytical instruments and instrument systems. The leak detection device includes a collection tube, a fluid absorbing material, and a circuit that electrically couples to an indicator device. When assembled, the leak detection device detects and monitors for fluid leaks, providing a preselected response in conjunction with the indicator device when contacted by a fluid.

  15. Analytic Methods for Benchmarking Hydrogen and Fuel Cell Technologies (Presentation), NREL (National Renewable Energy Laboratory)

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    NREL/PR-5400-64420 NREL is a national laboratory of the U.S. Department of Energy, Office of Energy Efficiency and Renewable Energy, operated by the Alliance for Sustainable Energy, LLC. Analytic Methods for Benchmarking Hydrogen and Fuel Cell Technologies 227 th ECS Meeting, Chicago, Illinois Marc Melaina, Genevieve Saur, Todd Ramsden, Joshua Eichman May 28, 2015 2 Presentation Overview: Four Metrics Analysis projects focus on low-carbon and economic transportation and stationary fuel cell

  16. Field sampling and selecting on-site analytical methods for explosives in soil

    SciTech Connect (OSTI)

    Crockett, A.B.; Craig, H.D.; Jenkins, T.F.; Sisk, W.E.

    1996-12-01

    A large number of defense-related sites are contaminated with elevated levels of secondary explosives. Levels of contamination range from barely detectable to levels above 10% that need special handling because of the detonation potential. Characterization of explosives-contaminated sites is particularly difficult because of the very heterogeneous distribution of contamination in the environment and within samples. To improve site characterization, several options exist including collecting more samples, providing on-site analytical data to help direct the investigation, compositing samples, improving homogenization of the samples, and extracting larger samples. This publication is intended to provide guidance to Remedial Project Managers regarding field sampling and on-site analytical methods for detecting and quantifying secondary explosive compounds in soils, and is not intended to include discussions of the safety issues associated with sites contaminated with explosive residues.

  17. Sampling and analytical methods development at the HGP-a generator facility

    SciTech Connect (OSTI)

    Thomas, D.M.

    1982-10-01

    During shakedown operations for the HGP-A generator plant sampling and analytical problems were encountered during the process chemistry monitoring effort. Acid-preservation of brine for cation analysis required the use of nitrous oxideacetylene flame for accurate A-A analysis of calcium. Analysis of gases for carbonate and sulfide was by specific ion electrode and alkalinity titration, respectively. Sulfide caused substantial interferences with the alkalinity method and corrections for sulfide were required. Sulfide also interfered with chloride analyses in the steam phase requiring removal of the sulfide by boiling. Analysis of dissolved silica in the brine was complicated by the presence of colloidal silica which produced erratic analytical results. An accurate evaluation of the hydrogen sulfide abatement system was possible only when the hydrogen sulfide concentrations in the treated and untreated steam were compared with a second component in the steam phase that was unaffected by caustic injection.

  18. Off-line compatible electronic cash method and system

    SciTech Connect (OSTI)

    Kravitz, David W.; Gemmell, Peter S.; Brickell, Ernest F.

    1998-01-01

    An off-line electronic cash system having an electronic coin, a bank B, a payee S, and a user U with an account at the bank B as well as a user password z.sub.u,i, has a method for performing an electronic cash transfer. An electronic coin is withdrawn from the bank B by the user U and an electronic record of the electronic coin is stored by the bank B. The coin is paid to the payee S by the user U. The payee S deposits the coin with the bank B. A determination is made that the coin is spent and the record of the coin is deleted by the bank B. A further deposit of the same coin after the record is deleted is determined. Additionally, a determination is made which user U originally withdrew the coin after deleting the record. To perform these operations a key pair is generated by the user, including public and secret signature keys. The public signature key along with a user password z.sub.u,i and a withdrawal amount are sent to the bank B by the user U. In response, the bank B sends a coin to the user U signed by the secret key of the bankindicating the value of the coin and the public key of the user U. The payee S transmits a challenge counter to the user U prior to receiving the coin.

  19. Off-line compatible electronic cash method and system

    DOE Patents [OSTI]

    Kravitz, D.W.; Gemmell, P.S.; Brickell, E.F.

    1998-11-03

    An off-line electronic cash system having an electronic coin, a bank B, a payee S, and a user U with an account at the bank B as well as a user password z{sub u,i}, has a method for performing an electronic cash transfer. An electronic coin is withdrawn from the bank B by the user U and an electronic record of the electronic coin is stored by the bank B. The coin is paid to the payee S by the user U. The payee S deposits the coin with the bank B. A determination is made that the coin is spent and the record of the coin is deleted by the bank B. A further deposit of the same coin after the record is deleted is determined. Additionally, a determination is made which user U originally withdrew the coin after deleting the record. To perform these operations a key pair is generated by the user, including public and secret signature keys. The public signature key along with a user password z{sub u,i} and a withdrawal amount are sent to the bank B by the user U. In response, the bank B sends a coin to the user U signed by the secret key of the bank indicating the value of the coin and the public key of the user U. The payee S transmits a challenge counter to the user U prior to receiving the coin. 16 figs.

  20. Continuous human cell lines and method of making same

    DOE Patents [OSTI]

    Stampfer, M.R.

    1985-07-01

    Substantially genetically stable continuous human cell lines derived from normal human mammary epithelial cells (HMEC) and processes for making and using the same. In a preferred embodiment, the cell lines are derived by treating normal human mammary epithelial tissue with a chemical carcinogen such as benzo(a)pyrene. The novel cell lines serve as useful substrates for elucidating the potential effects of a number of toxins, carcinogens and mutagens as well as of the addition of exogenous genetic material. The autogenic parent cells from which the cell lines are derived serve as convenient control samples for testing. The cell lines are not neoplastically transformed, although they have acquired several properties which distinguish them from their normal progenitors. 2 tabs.

  1. Continuous human cell lines and method of making same

    DOE Patents [OSTI]

    Stampfer, Martha R.

    1989-01-01

    Substantially genetically stable continuous human cell lines derived from normal human mammary epithelial cells (HMEC) and processes for making and using the same. In a preferred embodiment, the cell lines are derived by treating normal human mammary epithelial tissue with a chemical carcinogen such as benzo[a]pyrene. The novel cell lines serve as useful substrates for elucidating the potential effects of a number of toxins, carcinogens and mutagens as well as of the addition of exogenous genetic material. The autogenic parent cells from which the cell lines are derived serve as convenient control samples for testing. The cell lines are not neoplastically transformed, although they have acquired several properties which distinguish them from their normal progenitors.

  2. ASTM sampling methods and analytical validation for lead in paint, dust, soil, and air

    SciTech Connect (OSTI)

    Ashley, K.; Schlecht, P.C.; Song, R.; Feng, A.; DeWalt, G.; McKnight, M.E.

    1996-12-31

    ASTM Subcommittee E06.23 on Abatement/Mitigation of Lead Hazards has developed a number of standards that are concerned with the sampling of leas in environmental media, namely paint, dust, soil and airborne particulate. An ASTM practice for the collection of airborne particulate lead in the workplace has been published. New ASTM standards for the collection of dry paint film samples, surface soil samples, and surface dust wipe samples for subsequent lead analysis have also been promulgated. Other draft standards pertinent to lead sampling are under development. The ASTM standards concerned with lead sample collection are accompanied by separate sample preparation standard practices and a standard analysis method. Sample preparation and analytical methods have been evaluated by interlaboratory testing; such analyses may be used to assess the efficacy of sampling protocols.

  3. Pulsed voltage electrospray ion source and method for preventing analyte electrolysis

    DOE Patents [OSTI]

    Kertesz, Vilmos; Van Berkel, Gary

    2011-12-27

    An electrospray ion source and method of operation includes the application of pulsed voltage to prevent electrolysis of analytes with a low electrochemical potential. The electrospray ion source can include an emitter, a counter electrode, and a power supply. The emitter can include a liquid conduit, a primary working electrode having a liquid contacting surface, and a spray tip, where the liquid conduit and the working electrode are in liquid communication. The counter electrode can be proximate to, but separated from, the spray tip. The power system can supply voltage to the working electrode in the form of a pulse wave, where the pulse wave oscillates between at least an energized voltage and a relaxation voltage. The relaxation duration of the relaxation voltage can range from 1 millisecond to 35 milliseconds. The pulse duration of the energized voltage can be less than 1 millisecond and the frequency of the pulse wave can range from 30 to 800 Hz.

  4. GraphPrints: Towards a Graph Analytic Method for Network Anomaly Detection

    SciTech Connect (OSTI)

    Harshaw, Chris R; Bridges, Robert A; Iannacone, Michael D; Reed, Joel W; Goodall, John R

    2016-01-01

    This paper introduces a novel graph-analytic approach for detecting anomalies in network flow data called \\textit{GraphPrints}. Building on foundational network-mining techniques, our method represents time slices of traffic as a graph, then counts graphlets\\textemdash small induced subgraphs that describe local topology. By performing outlier detection on the sequence of graphlet counts, anomalous intervals of traffic are identified, and furthermore, individual IPs experiencing abnormal behavior are singled-out. Initial testing of GraphPrints is performed on real network data with an implanted anomaly. Evaluation shows false positive rates bounded by 2.84\\% at the time-interval level, and 0.05\\% at the IP-level with 100\\% true positive rates at both.

  5. On-line nondestructive methods for examining fuel particles

    SciTech Connect (OSTI)

    Pardini, A.F.; Bond, L.J.; Good, M.S.; Bunch, K.J.; Sandness, G.A.; Hockey, R.L.; Saurwein, J.J.; Gray, J.N.

    2007-07-01

    Tri-isotropic (TRISO) particle fuels are being considered for use in various advanced nuclear power reactors and about 15 billion of these small ({approx} 1 mm diameter) spheres are needed for a single fuel load. Current quality control methods are manual, often destructive of test specimens, and they are economically impractical for automated application at commercial scale. Replacing these methods with new nondestructive evaluation techniques, automated for higher speed, will make fuel production and reactor operation economically more attractive. This paper reports aspects of a project to develop and demonstrate nondestructive examination methods to detect and reject defective particles. The work explored adapting, developing, and demonstrating innovative nondestructive test methods to cost-effectively assure the quality of large percentages of the fuel particles. (authors)

  6. Ion mobility spectrometer, spectrometer analyte detection and identification verification system, and method

    DOE Patents [OSTI]

    Atkinson, David A.

    2002-01-01

    Methods and apparatus for ion mobility spectrometry and analyte detection and identification verification system are disclosed. The apparatus is configured to be used in an ion mobility spectrometer and includes a plurality of reactant reservoirs configured to contain a plurality of reactants which can be reacted with the sample to form adducts having varying ion mobilities. A carrier fluid, such as air or nitrogen, is used to carry the sample into the spectrometer. The plurality of reactants are configured to be selectively added to the carrier stream by use inlet and outlet manifolds in communication with the reagent reservoirs, the reservoirs being selectively isolatable by valves. The invention further includes a spectrometer having the reagent system described. In the method, a first reactant is used with the sample. Following a positive result, a second reactant is used to determine whether a predicted response occurs. The occurrence of the second predicted response tends to verify the existence of a component of interest within the sample. A third reactant can also be used to provide further verification of the existence of a component of interest. A library can be established of known responses of compounds of interest with various reactants and the results of a specific multi-reactant survey of a sample can be compared against the library to determine whether a component detected in the sample is likely to be a specific component of interest.

  7. Analytical energy gradient for the two-component normalized elimination of the small component method

    SciTech Connect (OSTI)

    Zou, Wenli; Filatov, Michael; Cremer, Dieter

    2015-06-07

    The analytical gradient for the two-component Normalized Elimination of the Small Component (2c-NESC) method is presented. The 2c-NESC is a Dirac-exact method that employs the exact two-component one-electron Hamiltonian and thus leads to exact Dirac spin-orbit (SO) splittings for one-electron atoms. For many-electron atoms and molecules, the effect of the two-electron SO interaction is modeled by a screened nucleus potential using effective nuclear charges as proposed by Boettger [Phys. Rev. B 62, 7809 (2000)]. The effect of spin-orbit coupling (SOC) on molecular geometries is analyzed utilizing the properties of the frontier orbitals and calculated SO couplings. It is shown that bond lengths can either be lengthened or shortened under the impact of SOC where in the first case the influence of low lying excited states with occupied antibonding orbitals plays a role and in the second case the jj-coupling between occupied antibonding and unoccupied bonding orbitals dominates. In general, the effect of SOC on bond lengths is relatively small (≤5% of the scalar relativistic changes in the bond length). However, large effects are found for van der Waals complexes Hg{sub 2} and Cn{sub 2}, which are due to the admixture of more bonding character to the highest occupied spinors.

  8. Solvent effects in time-dependent self-consistent field methods. II. Variational formulations and analytical gradients

    SciTech Connect (OSTI)

    Bjorgaard, J. A.; Velizhanin, K. A.; Tretiak, S.

    2015-08-06

    This study describes variational energy expressions and analytical excited state energy gradients for time-dependent self-consistent field methods with polarizable solvent effects. Linear response, vertical excitation, and state-specific solventmodels are examined. Enforcing a variational ground stateenergy expression in the state-specific model is found to reduce it to the vertical excitation model. Variational excited state energy expressions are then provided for the linear response and vertical excitation models and analytical gradients are formulated. Using semiempiricalmodel chemistry, the variational expressions are verified by numerical and analytical differentiation with respect to a static external electric field. Lastly, analytical gradients are further tested by performing microcanonical excited state molecular dynamics with p-nitroaniline.

  9. Solvent effects in time-dependent self-consistent field methods. II. Variational formulations and analytical gradients

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Bjorgaard, J. A.; Velizhanin, K. A.; Tretiak, S.

    2015-08-06

    This study describes variational energy expressions and analytical excited state energy gradients for time-dependent self-consistent field methods with polarizable solvent effects. Linear response, vertical excitation, and state-specific solventmodels are examined. Enforcing a variational ground stateenergy expression in the state-specific model is found to reduce it to the vertical excitation model. Variational excited state energy expressions are then provided for the linear response and vertical excitation models and analytical gradients are formulated. Using semiempiricalmodel chemistry, the variational expressions are verified by numerical and analytical differentiation with respect to a static external electric field. Lastly, analytical gradients are further tested by performingmore » microcanonical excited state molecular dynamics with p-nitroaniline.« less

  10. Standardization of chemical analytical techniques for pyrolysis bio-oil: history, challenges, and current status of methods

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ferrell, Jack R.; Olarte, Mariefel V.; Christensen, Earl D.; Padmaperuma, Asanga B.; Connatser, Raynella M.; Stankovikj, Filip; Meier, Dietrich; Paasikallio, Ville

    2016-07-05

    Here, we discuss the standardization of analytical techniques for pyrolysis bio-oils, including the current status of methods, and our opinions on future directions. First, the history of past standardization efforts is summarized, and both successful and unsuccessful validation of analytical techniques highlighted. The majority of analytical standardization studies to-date has tested only physical characterization techniques. In this paper, we present results from an international round robin on the validation of chemical characterization techniques for bio-oils. Techniques tested included acid number, carbonyl titrations using two different methods (one at room temperature and one at 80 °C), 31P NMR for determination ofmore » hydroxyl groups, and a quantitative gas chromatography–mass spectrometry (GC-MS) method. Both carbonyl titration and acid number methods have yielded acceptable inter-laboratory variabilities. 31P NMR produced acceptable results for aliphatic and phenolic hydroxyl groups, but not for carboxylic hydroxyl groups. As shown in previous round robins, GC-MS results were more variable. Reliable chemical characterization of bio-oils will enable upgrading research and allow for detailed comparisons of bio-oils produced at different facilities. Reliable analytics are also needed to enable an emerging bioenergy industry, as processing facilities often have different analytical needs and capabilities than research facilities. We feel that correlations in reliable characterizations of bio-oils will help strike a balance between research and industry, and will ultimately help to -determine metrics for bio-oil quality. Lastly, the standardization of additional analytical methods is needed, particularly for upgraded bio-oils.« less

  11. SU-E-T-569: Neutron Shielding Calculation Using Analytical and Multi-Monte Carlo Method for Proton Therapy Facility

    SciTech Connect (OSTI)

    Cho, S; Shin, E H; Kim, J; Ahn, S H; Chung, K; Kim, D-H; Han, Y; Choi, D H

    2015-06-15

    Purpose: To evaluate the shielding wall design to protect patients, staff and member of the general public for secondary neutron using a simply analytic solution, multi-Monte Carlo code MCNPX, ANISN and FLUKA. Methods: An analytical and multi-Monte Carlo method were calculated for proton facility (Sumitomo Heavy Industry Ltd.) at Samsung Medical Center in Korea. The NCRP-144 analytical evaluation methods, which produced conservative estimates on the dose equivalent values for the shielding, were used for analytical evaluations. Then, the radiation transport was simulated with the multi-Monte Carlo code. The neutron dose at evaluation point is got by the value using the production of the simulation value and the neutron dose coefficient introduced in ICRP-74. Results: The evaluation points of accelerator control room and control room entrance are mainly influenced by the point of the proton beam loss. So the neutron dose equivalent of accelerator control room for evaluation point is 0.651, 1.530, 0.912, 0.943 mSv/yr and the entrance of cyclotron room is 0.465, 0.790, 0.522, 0.453 mSv/yr with calculation by the method of NCRP-144 formalism, ANISN, FLUKA and MCNP, respectively. The most of Result of MCNPX and FLUKA using the complicated geometry showed smaller values than Result of ANISN. Conclusion: The neutron shielding for a proton therapy facility has been evaluated by the analytic model and multi-Monte Carlo methods. We confirmed that the setting of shielding was located in well accessible area to people when the proton facility is operated.

  12. METHOD AND APPARATUS FOR THE DETECTION OF LEAKS IN PIPE LINES

    DOE Patents [OSTI]

    Jefferson, S.; Cameron, J.F.

    1961-11-28

    A method is described for detecting leaks in pipe lines carrying fluid. The steps include the following: injecting a radioactive solution into a fluid flowing in the line; flushing the line clear of the radioactive solution; introducing a detector-recorder unit, comprising a radioactivity radiation detector and a recorder which records the detector signal over a time period at a substantially constant speed, into the line in association with a go-devil capable of propelling the detector-recorder unit through the line in the direction of the fluid flow at a substantia1ly constant velocity; placing a series of sources of radioactivity at predetermined distances along the downstream part of the line to make a characteristic signal on the recorder record at intervals corresponding to the location of said sources; recovering the detector-recorder unit at a downstream point along the line; transcribing the recorder record of any radioactivity detected during the travel of the detector- recorder unit in terms of distance along the line. (AEC)

  13. Method and apparatus for selective capture of gas phase analytes using metal .beta.-diketonate polymers

    DOE Patents [OSTI]

    Harvey, Scott D [Kennewick, WA

    2011-06-21

    A process and sensor device are disclosed that employ metal .beta.-diketonate polymers to selectively capture gas-phase explosives and weaponized chemical agents in a sampling area or volume. The metal .beta.-diketonate polymers can be applied to surfaces in various analytical formats for detection of: improvised explosive devices, unexploded ordinance, munitions hidden in cargo holds, explosives, and chemical weapons in public areas.

  14. VALIDATION OF ANALYTICAL METHODS AND INSTRUMENTATION FOR BERYLLIUM MEASUREMENT: REVIEW AND SUMMARY OF AVAILABLE GUIDES, PROCEDURES, AND PROTOCOLS

    SciTech Connect (OSTI)

    Ekechukwu, A

    2009-05-27

    Method validation is the process of evaluating whether an analytical method is acceptable for its intended purpose. For pharmaceutical methods, guidelines from the United States Pharmacopeia (USP), International Conference on Harmonisation (ICH), and the United States Food and Drug Administration (USFDA) provide a framework for performing such valications. In general, methods for regulatory compliance must include studies on specificity, linearity, accuracy, precision, range, detection limit, quantitation limit, and robustness. Elements of these guidelines are readily adapted to the issue of validation for beryllium sampling and analysis. This document provides a listing of available sources which can be used to validate analytical methods and/or instrumentation for beryllium determination. A literature review was conducted of available standard methods and publications used for method validation and/or quality control. A comprehensive listing of the articles, papers and books reviewed is given in the Appendix. Available validation documents and guides are listed therein; each has a brief description of application and use. In the referenced sources, there are varying approches to validation and varying descriptions of the valication process at different stages in method development. This discussion focuses on valication and verification of fully developed methods and instrumentation that have been offered up for use or approval by other laboratories or official consensus bodies such as ASTM International, the International Standards Organization (ISO) and the Association of Official Analytical Chemists (AOAC). This review was conducted as part of a collaborative effort to investigate and improve the state of validation for measuring beryllium in the workplace and the environment. Documents and publications from the United States and Europe are included. Unless otherwise specified, all referenced documents were published in English.

  15. Determination of Carbonyls in Pyrolysis Bio-oils by Potentiometric Titration: Faix Method. Laboratory Analytical Procedure (LAP)

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Carbonyls in Pyrolysis Bio-oils by Potentiometric Titration: Faix Method Laboratory Analytical Procedure (LAP) Issue Date: March 2, 2016 Stuart Black and Jack Ferrell National Renewable Energy Laboratory Mariefel V. Olarte and Asanga B. Padmaperuma Pacific Northwest National Laboratory Technical Report NREL/TP-5100-65888 March 2016 NREL is a national laboratory of the U.S. Department of Energy Office of Energy Efficiency & Renewable Energy Operated by the Alliance for Sustainable Energy, LLC

  16. Research prioritization using the Analytic Hierarchy Process: basic methods. Volume 1

    SciTech Connect (OSTI)

    Vesely, W.E.; Shafaghi, A.; Gary, I. Jr.; Rasmuson, D.M.

    1983-08-01

    This report describes a systematic approach for prioritizing research needs and research programs. The approach is formally called the Analytic Hierarchy Process which was developed by T.L. Saaty and is described in several of his texts referenced in the report. The Analytic Hierarchy Process, or AHP for short, has been applied to a wide variety of prioritization problems and has a good record of success as documented in Saaty's texts. The report develops specific guidelines for constructing the hierarchy and for prioritizing the research programs. Specific examples are given to illustrate the steps in the AHP. As part of the work, a computer code has been developed and the use of the code is described. The code allows the prioritizations to be done in a codified and efficient manner; sensitivity and parametric studies can also be straightforwardly performed to gain a better understanding of the prioritization results. Finally, as an important part of the work, an approach is developed which utilizes probabilistic risk analyses (PRAs) to systematically identify and prioritize research needs and research programs. When utilized in an AHP framework, the PRA's which have been performed to date provide a powerful information source for focusing research on those areas most impacting risk and risk uncertainty.

  17. VALIDATION OF ANALYTICAL METHODS AND INSTRUMENTATION FOR BERYLLIUM MEASUREMENT: REVIEW AND SUMMARY OF AVAILABLE GUIDES, PROCEDURES, AND PROTOCOLS

    SciTech Connect (OSTI)

    Ekechukwu, A.

    2008-12-17

    This document proposes to provide a listing of available sources which can be used to validate analytical methods and/or instrumentation for beryllium determination. A literature review was conducted of available standard methods and publications used for method validation and/or quality control. A comprehensive listing of the articles, papers, and books reviewed is given in Appendix 1. Available validation documents and guides are listed in the appendix; each has a brief description of application and use. In the referenced sources, there are varying approaches to validation and varying descriptions of validation at different stages in method development. This discussion focuses on validation and verification of fully developed methods and instrumentation that have been offered up for use or approval by other laboratories or official consensus bodies such as ASTM International, the International Standards Organization (ISO) and the Association of Official Analytical Chemists (AOAC). This review was conducted as part of a collaborative effort to investigate and improve the state of validation for measuring beryllium in the workplace and the environment. Documents and publications from the United States and Europe are included. Unless otherwise specified, all documents were published in English.

  18. DEVELOPMENT OF ANALYTICAL METHODS FOR DETERMINING SUPPRESSOR CONCENTRATION IN THE MCU NEXT GENERATION SOLVENT (NGS)

    SciTech Connect (OSTI)

    Taylor-Pashow, K.; Fondeur, F.; White, T.; Diprete, D.; Milliken, C.

    2013-07-31

    Savannah River National Laboratory (SRNL) was tasked with identifying and developing at least one, but preferably two methods for quantifying the suppressor in the Next Generation Solvent (NGS) system. The suppressor is a guanidine derivative, N,N',N"-tris(3,7-dimethyloctyl)guanidine (TiDG). A list of 10 possible methods was generated, and screening experiments were performed for 8 of the 10 methods. After completion of the screening experiments, the non-aqueous acid-base titration was determined to be the most promising, and was selected for further development as the primary method. {sup 1}H NMR also showed promising results from the screening experiments, and this method was selected for further development as the secondary method. Other methods, including {sup 36}Cl radiocounting and ion chromatography, also showed promise; however, due to the similarity to the primary method (titration) and the inability to differentiate between TiDG and TOA (tri-n-ocytlamine) in the blended solvent, {sup 1}H NMR was selected over these methods. Analysis of radioactive samples obtained from real waste ESS (extraction, scrub, strip) testing using the titration method showed good results. Based on these results, the titration method was selected as the method of choice for TiDG measurement. {sup 1}H NMR has been selected as the secondary (back-up) method, and additional work is planned to further develop this method and to verify the method using radioactive samples. Procedures for analyzing radioactive samples of both pure NGS and blended solvent were developed and issued for the both methods.

  19. SRC-1 quarterly technical report, April-June 1981. [Review of analytical methods needed in SRC Demonstration plants

    SciTech Connect (OSTI)

    Not Available

    1981-10-01

    Twenty-three papers involving the design, materials and equipment for the SRC-1 demonstration coal liquefaction plant near Newman, Daviess County, Kentucky, have been entered individually into EDB and ERA. A number of the papers deal also with the analytical methodology required for the plant, including a rather detailed evaluation of the accuracy requirements and careful evaluation of several methods such as gas chromatography, mass spectroscopy, nuclear magnetic resonance, etc. Flexibility of design is stressed so that products can be optimized for the market and charged if the market requires different products. (LTN)

  20. 4D Emittance Measurements Using Multiple Wire and Waist Scan Methods in the ATF Extraction Line

    SciTech Connect (OSTI)

    Rimbault, C.; Bambade, P.; Brossard, J.; Alabau, M.; Kuroda, S.; Scarfe, A.; Woodley, M.; /SLAC

    2011-11-02

    Emittance measurements performed in the diagnostic section of the Accelerator Test Facility (ATF) extraction line since 1998 led to vertical emittances three times larger than the expected ones, with a strong dependence on intensity. An experimental program is pursued to investigate potential sources of emittance growth and find possible remedies. This requires efficient and reliable emittance measurement techniques. In the past, several phase-space reconstruction methods developed at SLAC and KEK have been used to estimate the vertical emittance, based on multiple location beam size measurements and dedicated quadrupole scans. These methods have been shown to be very sensitive to measurement errors and other fluctuations in the beam conditions. In this context new emittance measurements have been performed revisiting these methods and newly developed ones with a systematic approach to compare and characterise their performance in the ATF extraction line.

  1. Hanford environmental analytical methods (methods as of March 1990). Appendix A3-O and Appendix A3-I

    SciTech Connect (OSTI)

    Goheen, S.D.; McCulloch, M.; Daniel, J.L.

    1993-05-01

    Information is provided on the techniques employed towards the chemical analysis of volatile, semi-volatile matter, pesticides and PCB`s at the Hanford Reservation. Sample preparation methods are included.

  2. An analytical method to calculate equivalent fields to irregular symmetric and asymmetric photon fields

    SciTech Connect (OSTI)

    Tahmasebi Birgani, Mohamad J.; Chegeni, Nahid; Zabihzadeh, Mansoor; Hamzian, Nima

    2014-04-01

    Equivalent field is frequently used for central axis depth-dose calculations of rectangular- and irregular-shaped photon beams. As most of the proposed models to calculate the equivalent square field are dosimetry based, a simple physical-based method to calculate the equivalent square field size was used as the basis of this study. The table of the sides of the equivalent square or rectangular fields was constructed and then compared with the well-known tables by BJR and Venselaar, et al. with the average relative error percentage of 2.5 ± 2.5% and 1.5 ± 1.5%, respectively. To evaluate the accuracy of this method, the percentage depth doses (PDDs) were measured for some special irregular symmetric and asymmetric treatment fields and their equivalent squares for Siemens Primus Plus linear accelerator for both energies, 6 and 18 MV. The mean relative differences of PDDs measurement for these fields and their equivalent square was approximately 1% or less. As a result, this method can be employed to calculate equivalent field not only for rectangular fields but also for any irregular symmetric or asymmetric field.

  3. Redox control of electric melters with complex feed compositions. Part I: analytical methods and models

    SciTech Connect (OSTI)

    Bickford, D F; Diemer, Jr, R B

    1985-01-01

    The redox state of glass from electric melters with complex feed compositions is determined by balance between gases above the melt, and transition metals and organic compounds in the feed. Part I discusses experimental and computational methods of relating flowrates and other melter operating conditions to the redox state of glass, and composition of the melter offgas. Computerized thermodynamic computational methods are useful in predicting the sequence and products of redox reactions and in assessing individual process variations. Melter redox state can be predicted by combining monitoring of melter operating conditions, redox measurement of fused melter feed samples, and periodic redox measurement of product. Mossbauer spectroscopy, and other methods which measure Fe(II)/Fe(III) in glass, can be used to measure melter redox state. Part II develops preliminary operating limits for the vitrification of High-Level Radioactive Waste. Limits on reducing potential to preclude the accumulation of combustible gases, accumulation of sulfides and selenides, and degradation of melter components are the most critical. Problems associated with excessively oxidizing conditions, such as glass foaming and potential ruthenium volatility, are controlled when sufficient formic acid is added to adjust melter feed rheology.

  4. Methods and computer executable instructions for marking a downhole elongate line and detecting same

    DOE Patents [OSTI]

    Watkins, Arthur D.

    2003-05-13

    Methods and computer executable instructions are provided for making an elongate line (22) with a plurality of marks (30) and detecting those marks (30) to determine a distance of the elongate line (22) in a downhole or a physical integrity thereof. In a preferred embodiment, each mark comprises a plurality of particles (44) having a substantially permanent magnetizing capability adhered to an exterior surface of the elongate line (22) at preselected intervals with an epoxy paint. The particles (44) are arranged at each interval as a plurality of bands (40). Thereafter, the particles are oriented into a magnetic signature for that interval by magnetizing the particles to create a magnetic field substantially normal to the exterior surface. This facilitates detection by a Hall effect probe. The magnetic signatures are stored in a computing configuration and, once a mark is detected, a correlation is made to a unique position on the elongate line by comparison with the stored magnetic signatures. Preferred particles include samarium-cobalt and neodymium-iron-boride.

  5. Analytical Methods for Malachite Green : Completion Report : Malachite Green Analysis in Water.

    SciTech Connect (OSTI)

    Allen, John L.; Gofus, Jane E.; Meinertz, Jeffery R.

    1991-06-01

    Malachite green is a known teratogen and therefore its use is limited to nonfood fish under an Investigational New Animal Drug permit (INAD), number 2573. Although a charcoal adsorption column was developed to remove malachite green from hatchery water, INAD compliance requires that the malachite green residue concentrations in any effluent from hatcheries using the chemical be quantified. Therefore, we developed a method for the analysis of malachite green residues in water. Enrichment of the residues of malachite green in water on a diol column followed by High Performance Liquid Chromatographic (HPLC) analysis gives a minimum sensitivity of less than 10 ppb for the chemical. When combined with post-column oxidation using a lead oxide post-column reactor, the procedure can be used for the simultaneous analysis of malachite green in its leuco form, a decomposition product of the dye, as well as its chromatic form. Recovery of the leuco form is pH dependent and water samples should be adjusted to pH 6 to optimize recovery of this form. Water samples spiked with malachite green were concentrated on a diol column followed by elution with 0.05 M p-toluene sulfonic acid in methanol. The methanol elutes were analyzed by HPLC. Pond water samples spiked with malachite green and leuco malachite green yielded average recoveries of 95.4% for malachite green and 57.3% for leuco malachite green. Tap water samples spiked with the carbinol form of malachite green gave average recoveries of 98.6%. The method is very sensitive and is capable of detecting malachite green residues in water at less than 10 ppb. Fish culturists, who cannot find an effective replacement for malachite green, can utilize the method to ensure that their effluents comply with INAD regulations. 13 refs., 2 figs., 7 tabs.

  6. Analytical Chemistry Laboratory (ACL) procedure compendium. Volume 2, Sample preparation methods

    SciTech Connect (OSTI)

    Not Available

    1993-08-01

    This volume contains the interim change notice for sample preparation methods. Covered are: acid digestion for metals analysis, fusion of Hanford tank waste solids, water leach of sludges/soils/other solids, extraction procedure toxicity (simulate leach in landfill), sample preparation for gamma spectroscopy, acid digestion for radiochemical analysis, leach preparation of solids for free cyanide analysis, aqueous leach of solids for anion analysis, microwave digestion of glasses and slurries for ICP/MS, toxicity characteristic leaching extraction for inorganics, leach/dissolution of activated metal for radiochemical analysis, extraction of single-shell tank (SST) samples for semi-VOC analysis, preparation and cleanup of hydrocarbon- containing samples for VOC and semi-VOC analysis, receiving of waste tank samples in onsite transfer cask, receipt and inspection of SST samples, receipt and extrusion of core samples at 325A shielded facility, cleaning and shipping of waste tank samplers, homogenization of solutions/slurries/sludges, and test sample preparation for bioassay quality control program.

  7. Novel Visual and Analytical Methods in Repurposing Legacy Scientific Code - A Case Study

    SciTech Connect (OSTI)

    Oehmen, Christopher S.; Curtis, Darren S.; Phillips, Aaron R.; Peterson, Elena S.

    2013-07-23

    Scientific computing is dominated by team-authored legacy code that has evolved over decades with the purpose of capturing the evolving understanding of a scientific discipline. Accumulated deprecated code, various optimization techniques, and evolving algorithms lead to convoluted source code that is impractical to reverse engineer using mainstream methods. This prevents codes from being truly repeatable or understandable, which are two of the most essential needs in scientific computing. We refactored a long-standing implementation of a common biosequence alignment algorithm in an effort to reproduce its salient behaviors in usable form. Because of the sheer size and complexity of this code base, we developed custom tools to visualize and manipulate the source code behavior under a variety of conditions. We present a case study of extracting and refactoring the algorithmic core and a novel process of discovery/prototyping/testing using a combination of openly available and custom-built tools. The result is a reduction in code size of over 2 orders of magnitude while reconstructing the key protein alignment function in BLAST

  8. Analytical Chemistry Laboratory (ACL) procedure compendium. Volume 3, Inorganic instrumental methods

    SciTech Connect (OSTI)

    Not Available

    1993-08-01

    The methods cover: C in solutions, F (electrode), elements by atomic emission spectrometry, inorganic anions by ion chromatography, Hg in water/solids/sludges, As, Se, Bi, Pb, data calculations for SST (single shell tank?) samples, Sb, Tl, Ag, Pu, O/M ratio, ignition weight loss, pH value, ammonia (N), Cr(VI), alkalinity, U, C sepn. from soil/sediment/sludge, Pu purif., total N, water, C and S, surface Cl/F, leachable Cl/F, outgassing of Ge detector dewars, gas mixing, gas isotopic analysis, XRF of metals/alloys/compounds, H in Zircaloy, H/O in metals, inpurity extraction, reduced/total Fe in glass, free acid in U/Pu solns, density of solns, Kr/Xe isotopes in FFTF cover gas, H by combustion, MS of Li and Cs isotopes, MS of lanthanide isotopes, GC operation, total Na on filters, XRF spectroscopy QC, multichannel analyzer operation, total cyanide in water/solid/sludge, free cyanide in water/leachate, hydrazine conc., ICP-MS, {sup 99}Tc, U conc./isotopes, microprobe analysis of solids, gas analysis, total cyanide, H/N{sub 2}O in air, and pH in soil.

  9. Method for constructing a lined underground cavity by underreaming, grouting, and boring through the grouting

    DOE Patents [OSTI]

    Johnson, W.H.

    1971-02-02

    A method is described for constructing a lined underground cavity. The process includes the steps of securing a casing in a borehole by grouting, underreaming the casing, filling the underreamed region with additional grouting, and then drilling through and underreaming the added grouting, thereby forming a room having a lining formed of the grouting. By using a structurally strong grouting that is impervious to water, the resulting room is waterproof and is suitable for on-site storage of an atomic device and its associated equipment prior to an underground atomic event. Such cavities also have other uses; for example, the cavities may be made very deep and used for storage of various fluids such as natural gas storage. (5 claims)

  10. Analytical methods for fissionable material determinations in the nuclear fuel cycle. Progress report, October 1, 1978-September 30, 1979

    SciTech Connect (OSTI)

    Waterbury, G.R.

    1980-03-01

    Work continues on the development of dissolution techniques for difficult-to-dissolve nuclear materials, the development of methods and automated instruments for plutonium, uranium, and thorium determinations, and the preparation of plutonium materials for the Safeguards Analytical Laboratory Evaluation (SALE) program and distribution by the National Bureau of Standards (NBS) as standard reference materials (SRMs). We are measuring the loner plutonium isotope half-lives, evaluating the isotope correlation techniques and the chemistry involved in the mass-spectrometric ion-bead techniques, and analyzing the SALE uranium materials. Completed subtasks include evaluations of various Teflon materials to recommend those acceptable for the dissolution apparatus developed at LASL, investigations of laser-enhanced dissolution of refractory materials, determinations of diverse ion effects on the microgram-sensitive method for determining uranium, fabrication of the first automated controlled-potential coulometric analyzer for determining plutonium, preparation of a /sup 244/Pu material for distribution by NBS as a SRM, and determination of the half-life of /sup 239/Pu. Work has been started on a spectrophotometric method for determining microgram quantities of plutonium, a microcomplexometric titration method for determining uranium, the use of new reagents for separations of plutonium, the preparation and packaging of a new lot of high-purity plutonium metal for distribution by NBS as a plutonium chemical SRM, and determination of half-lives of other plutonium isotopes.

  11. Apparatus and method for routing a transmission line through a downhole tool

    DOE Patents [OSTI]

    Hall, David R.; Hall, Jr., H. Tracy; Pixton, David S.; Briscoe, Michael; Reynolds, Jay

    2006-07-04

    A method for routing a transmission line through a tool joint having a primary and secondary shoulder, a central bore, and a longitudinal axis, includes drilling a straight channel, at a positive, nominal angle with respect to the longitudinal axis, through the tool joint from the secondary shoulder to a point proximate the inside wall of the centtral bore. The method further includes milling back, from within the central bore, a second channel to merge with the straight channel, thereby forming a continuous channel from the secondary shoulder to the central bore. In selected embodiments, drilling is accomplished by gun-drilling the straight channel. In other embodiments, the method includes tilting the tool joint before drilling to produce the positive, nominal angle. In selected embodiments, the positive, nominal angle is less than or equal to 15 degrees.

  12. Method and apparatus for magnetic resonance imaging and spectroscopy using microstrip transmission line coils

    DOE Patents [OSTI]

    Zhang, Xiaoliang; Ugurbil, Kamil; Chen, Wei

    2006-04-04

    Apparatus and method for MRI imaging using a coil constructed of microstrip transmission line (MTL coil) are disclosed. In one method, a target is positioned to be imaged within the field of a main magnetic field of a magnet resonance imaging (MRI) system, a MTL coil is positioned proximate the target, and a MRI image is obtained using the main magnet and the MTL coil. In another embodiment, the MRI coil is used for spectroscopy. MRI imaging and spectroscopy coils are formed using microstrip transmission line. These MTL coils have the advantageous property of good performance while occupying a relatively small space, thus allowing MTL coils to be used inside restricted areas more easily than some other prior art coils. In addition, the MTL coils are relatively simple to construct of inexpensive components and thus relatively inexpensive compared to other designs. Further, the MTL coils of the present invention can be readily formed in a wide variety of coil configurations, and used in a wide variety of ways. Further, while the MTL coils of the present invention work well at high field strengths and frequencies, they also work at low frequencies and in low field strengths as well.

  13. Method of forming oriented block copolymer line patterns, block copolymer line patterns formed thereby, and their use to form patterned articles

    DOE Patents [OSTI]

    Russell, Thomas P.; Hong, Sung Woo; Lee, Doug Hyun; Park, Soojin; Xu, Ting

    2015-10-13

    A block copolymer film having a line pattern with a high degree of long-range order is formed by a method that includes forming a block copolymer film on a substrate surface with parallel facets, and annealing the block copolymer film to form an annealed block copolymer film having linear microdomains parallel to the substrate surface and orthogonal to the parallel facets of the substrate. The line-patterned block copolymer films are useful for the fabrication of magnetic storage media, polarizing devices, and arrays of nanowires.

  14. Method of and apparatus for determining the similarity of a biological analyte from a model constructed from known biological fluids

    DOE Patents [OSTI]

    Robinson, Mark R.; Ward, Kenneth J.; Eaton, Robert P.; Haaland, David M.

    1990-01-01

    The characteristics of a biological fluid sample having an analyte are determined from a model constructed from plural known biological fluid samples. The model is a function of the concentration of materials in the known fluid samples as a function of absorption of wideband infrared energy. The wideband infrared energy is coupled to the analyte containing sample so there is differential absorption of the infrared energy as a function of the wavelength of the wideband infrared energy incident on the analyte containing sample. The differential absorption causes intensity variations of the infrared energy incident on the analyte containing sample as a function of sample wavelength of the energy, and concentration of the unknown analyte is determined from the thus-derived intensity variations of the infrared energy as a function of wavelength from the model absorption versus wavelength function.

  15. Method and apparatus for line power monitoring for uninterruptible power supplies

    SciTech Connect (OSTI)

    Baxter, R.V. Jr.; Stich, F.A.

    1993-07-20

    AC line waveform monitoring apparatus is described for detecting AC line power faults and providing a fault signal for control of an uninterruptible power supply comprising: (a) means for sampling an AC line power signal at times synchronized with the cycle of the AC line waveform; (b) means for producing a reference waveform at selected sample times during the period of the AC line signal given previous reference waveform values and a prior cycle wherein a reference waveform value at each sample time comprises a selectively weighted average of value at that sample time in the prior cycle of the AC line signal and the previous reference waveform value at that sample time; (c) an uninterruptible power supply including an auxiliary power supply battery, the uninterruptible power supply receiving the AC line power and normally providing the AC line power to a load and responsive to a fault signal to switch to provide power to the load from the battery; (d) means for comparing the AC line signal waveform with the reference waveform at corresponding times in the reference waveform and the signal waveform and providing the fault signal to the uninterruptible power supply so that it provides power to the load from the battery when a selected difference condition is exceeded.

  16. Method and apparatus for processing a test sample to concentrate an analyte in the sample from a solvent in the sample

    DOE Patents [OSTI]

    Turner, T.D.; Beller, L.S.; Clark, M.L.; Klingler, K.M.

    1997-10-14

    A method of processing a test sample to concentrate an analyte in the sample from a solvent in the sample includes: (a) boiling the test sample containing the analyte and solvent in a boiling chamber to a temperature greater than or equal to the solvent boiling temperature and less than the analyte boiling temperature to form a rising sample vapor mixture; (b) passing the sample vapor mixture from the boiling chamber to an elongated primary separation tube, the separation tube having internal sidewalls and a longitudinal axis, the longitudinal axis being angled between vertical and horizontal and thus having an upper region and a lower region; (c) collecting the physically transported liquid analyte on the internal sidewalls of the separation tube; and (d) flowing the collected analyte along the angled internal sidewalls of the separation tube to and pass the separation tube lower region. The invention also includes passing a turbulence inducing wave through a vapor mixture to separate physically transported liquid second material from vaporized first material. Apparatus is also disclosed for effecting separations. Further disclosed is a fluidically powered liquid test sample withdrawal apparatus for withdrawing a liquid test sample from a test sample container and for cleaning the test sample container. 8 figs.

  17. Method and apparatus for processing a test sample to concentrate an analyte in the sample from a solvent in the sample

    DOE Patents [OSTI]

    Turner, Terry D.; Beller, Laurence S.; Clark, Michael L.; Klingler, Kerry M.

    1997-01-01

    A method of processing a test sample to concentrate an analyte in the sample from a solvent in the sample includes: a) boiling the test sample containing the analyte and solvent in a boiling chamber to a temperature greater than or equal to the solvent boiling temperature and less than the analyte boiling temperature to form a rising sample vapor mixture; b) passing the sample vapor mixture from the boiling chamber to an elongated primary separation tube, the separation tube having internal sidewalls and a longitudinal axis, the longitudinal axis being angled between vertical and horizontal and thus having an upper region and a lower region; c) collecting the physically transported liquid analyte on the internal sidewalls of the separation tube; and d) flowing the collected analyte along the angled internal sidewalls of the separation tube to and pass the separation tube lower region. The invention also includes passing a turbulence inducing wave through a vapor mixture to separate physically transported liquid second material from vaporized first material. Apparatus are also disclosed for effecting separations. Further disclosed is a fluidically powered liquid test sample withdrawal apparatus for withdrawing a liquid test sample from a test sample container and for cleaning the test sample container.

  18. Analytical Services Management System

    Energy Science and Technology Software Center (OSTI)

    2005-03-30

    Analytical Services Management System (ASMS) provides sample management services. Sample management includes sample planning for analytical requests, sample tracking for shipping and receiving by the laboratory, receipt of the analytical data deliverable, processing the deliverable and payment of the laboratory conducting the analyses. ASMS is a web based application that provides the ability to manage these activities at multiple locations for different customers. ASMS provides for the assignment of single to multiple samples for standardmore » chemical and radiochemical analyses. ASMS is a flexible system which allows the users to request analyses by line item code. Line item codes are selected based on the Basic Ordering Agreement (BOA) format for contracting with participating laboratories. ASMS also allows contracting with non-BOA laboratories using a similar line item code contracting format for their services. ASMS allows sample and analysis tracking from sample planning and collection in the field through sample shipment, laboratory sample receipt, laboratory analysis and submittal of the requested analyses, electronic data transfer, and payment of the laboratories for the completed analyses. The software when in operation contains business sensitive material that is used as a principal portion of the Kaiser Analytical Management Services business model. The software version provided is the most recent version, however the copy of the application does not contain business sensitive data from the associated Oracle tables such as contract information or price per line item code.« less

  19. Analytical Services Management System

    SciTech Connect (OSTI)

    Church, Shane; Nigbor, Mike; Hillman, Daniel

    2005-03-30

    Analytical Services Management System (ASMS) provides sample management services. Sample management includes sample planning for analytical requests, sample tracking for shipping and receiving by the laboratory, receipt of the analytical data deliverable, processing the deliverable and payment of the laboratory conducting the analyses. ASMS is a web based application that provides the ability to manage these activities at multiple locations for different customers. ASMS provides for the assignment of single to multiple samples for standard chemical and radiochemical analyses. ASMS is a flexible system which allows the users to request analyses by line item code. Line item codes are selected based on the Basic Ordering Agreement (BOA) format for contracting with participating laboratories. ASMS also allows contracting with non-BOA laboratories using a similar line item code contracting format for their services. ASMS allows sample and analysis tracking from sample planning and collection in the field through sample shipment, laboratory sample receipt, laboratory analysis and submittal of the requested analyses, electronic data transfer, and payment of the laboratories for the completed analyses. The software when in operation contains business sensitive material that is used as a principal portion of the Kaiser Analytical Management Services business model. The software version provided is the most recent version, however the copy of the application does not contain business sensitive data from the associated Oracle tables such as contract information or price per line item code.

  20. Temperature and vital effect controls on Bamboo coral (Isididae) isotopegeochemistry: A test of the "lines method"

    SciTech Connect (OSTI)

    Hill, T M; Spero, H J; Guilderson, T P; LaVigne, M; Clague, D; Macalello, S; Jang, N

    2011-03-01

    Deep-sea bamboo corals hold promise as long-term climatic archives, yet little information exists linking bamboo coral geochemistry to measured environmental parameters. This study focuses on a suite of 10 bamboo corals collected from the Pacific and Atlantic basins (250-2136 m water depth) to investigate coral longevity, growth rates, and isotopic signatures. Calcite samples for stable isotopes and radiocarbon were collected from the base the corals, where the entire history of growth is recorded. In three of the coral specimens, samples were also taken from an upper branch for comparison. Radiocarbon and growth band width analyses indicate that the skeletal calcite precipitates from ambient dissolved inorganic carbon and that the corals live for 150-300 years, with extension rates of 9-128 {micro}m/yr. A linear relationship between coral calcite {delta}{sup 18}O and {delta}{sup 13}C indicates that the isotopic composition is influenced by vital effects ({delta}{sup 18}O:{delta}{sup 13}C slope of 0.17-0.47). As with scleractinian deep-sea corals, the intercept from a linear regression of {delta}{sup 18}O versus {delta}{sup 13}C is a function of temperature, such that a reliable paleotemperature proxy can be obtained, using the 'lines method.' Although the coral calcite {delta}{sup 18}O:{delta}{sup 13}C slope is maintained throughout the coral base ontogeny, the branches and central cores of the bases exhibit {delta}{sup 18}O:{delta}{sup 13}C values that are shifted far from equilibrium. We find that a reliable intercept value can be derived from the {delta}{sup 18}O:{delta}{sup 13}C regression of multiple samples distributed throughout one specimen or from multiple samples within individual growth bands.

  1. Analytical Method for the Detection of Ozone Depleting Chemicals (ODC) in Commercial Products Using a Gas Chromatograph with an Electron Capture Detector (GC-ECD)

    SciTech Connect (OSTI)

    Lee, Richard N.; Dockendorff, Brian P.; Wright, Bob W.

    2008-08-01

    This document describes an analytical procedure that was developed for the trace level detection of residual ozone depleting chemicals (ODC) associated with the manufacture of selected commercial products. To ensure the United States meets it obligation under the Montreal Protocol, Congress enacted legislation in 1989 to impose an excise tax on electronic goods imported into the United States that were produced with banned chemicals. This procedure was developed to technically determine if residual ODC chemicals could be detected on electronic circuit boards. The analytical method utilizes a “purge and trap” technique followed by gas chromatography with electron capture detection to capture and analyze the volatile chemicals associated with the matrix. The method describes the procedure, the hardware, operating conditions, calibration, and quality control measures in sufficient detail to allow the capability to be replicated. This document corresponds to internal Standard Operating Procedure (SOP) EFL-130A, Rev 4.

  2. Data Analytics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    MANTISSA Energy Aware Computing Exascale Computing Partnerships Shifter: User Defined Images Archive APEX Home » R & D » Data Analytics Data Analytics MANTISSA Massive Acceleration of New Techniques In Science with Scalable Algorithms: Scalable Statistics and Machine Learning Algorithms are essential for extracting insights from Big Data. Our interdisciplinary team is trying to address a number of challenging analysis problems from a number of science domains at Lawrence Berkeley National

  3. Method and cell lines for the production of monoclonal antibodies to human glycophorin A

    DOE Patents [OSTI]

    Bigbee, W.L.; Fong, S.S.N.; Jensen, R.H.; Vanderlaan, M.

    Cloned mouse hybridoma cell lines have been established which continuously produce antibodies that differentiate between the M and N forms of human glycophorin A. These antibodies have potential application as human blood group reagents, as markers for terminally differentiated erythroid cells and as immunofluorescent labels of somatically variant human erythrocytes.

  4. ANALYTICAL METHOD FOR MEASURING TOTAL PROTIUM AND TOTAL DEUTERIUM IN A GAS MIXTURE CONTAINING H2, D2,AND HD VIA GAS CHAROMATOGRAPHY

    SciTech Connect (OSTI)

    Sessions, H

    2007-08-07

    The most common analytical method of identifying and quantifying non-radioactive isotopic species of hydrogen is mass spectrometry. A low mass, high resolution mass spectrometer with adequate sensitivity and stability to identify and quantify hydrogen isotopes in the low ppm range is an expensive, complex instrument. A new analytical technique has been developed that measures both total protium (H) and total deuterium (D) in a gas mixture containing H{sub 2}, D{sub 2}, and HD using an inexpensive micro gas chromatograph (GC) with two molecular sieve columns. One column uses D{sub 2} as the carrier gas and the other uses H{sub 2} as the carrier gas. Laboratory tests have shown that when used in this configuration the GC can measure both total protium and total deuterium each with a detection and quantification limit of less than 20 ppm.

  5. Guideline for Evaluating Analytical Chemistry Capabilities and Recommending Upgraded Methods and Instrumentation for Nuclear Material Control and Accountability at Russian Nuclear Facilities

    SciTech Connect (OSTI)

    Russ, G.P.

    1999-10-21

    Analytical chemistry plays a key role in nuclear material control and accounting (MC and A). A large part of Special Nuclear Material (SNM) inventories and virtually all of the highly attractive SNM inventories are based on sampling bulk materials followed by destructive assay (DA) of these materials. These measurements support MC and A in process control, physical inventory verification, evaluation of the effects of process changes, detecting and resolving shipper-receiver differences, and the resolution of inspector-facility differences. When evaluating these important functions, US Project Teams need to carefully assess the existing Russian analytical chemistry capabilities and to specify appropriate upgrades where needed. This evaluation and the specification of upgrades have proven difficult, in part, because of the highly specialized and technical nature of DA and because of the wide variety of methods and applications. In addition, providing a DA capability to a Russian analytical laboratory requires much more than simply supplying new instrumentation. Experience has shown that DA upgrades at Russian analytical facilities require more support equipment than was originally anticipated by US Teams. The purpose of this guidance document is to: (1) recommend criteria for US Projects Teams to use in their evaluation of Russian DA capabilities; (2) provide a basis for selection of appropriate upgrades where capabilities are inadequate to support MC and A goals; and (3) to provide a list of Da methods suitable for MC and A with the following information: performance and applications information, strengths and limitations, and references and information on cost. Criteria for evaluating existing capabilities and determining appropriate upgrades are difficult to define. However, this is the basic information needed by the US project Teams. Section IV addresses these criteria.

  6. Analytical Technology

    SciTech Connect (OSTI)

    Goheen, Steven C.

    2001-07-01

    Characterizing environmental samples has been exhaustively addressed in the literature for most analytes of environmental concern. One of the weak areas of environmental analytical chemistry is that of radionuclides and samples contaminated with radionuclides. The analysis of samples containing high levels of radionuclides can be far more complex than that of non-radioactive samples. This chapter addresses the analysis of samples with a wide range of radioactivity. The other areas of characterization examined in this chapter are the hazardous components of mixed waste, and special analytes often associated with radioactive materials. Characterizing mixed waste is often similar to characterizing waste components in non-radioactive materials. The largest differences are in associated safety precautions to minimize exposure to dangerous levels of radioactivity. One must attempt to keep radiological dose as low as reasonably achievable (ALARA). This chapter outlines recommended procedures to safely and accurately characterize regulated components of radioactive samples.

  7. Bearing Analytics

    Broader source: Energy.gov [DOE]

    Bearing Analytics is a leading-edge equipment monitoring company aimed at pioneering a new era in industrial bearing condition monitoring. Our objective is to consolidate the needs of customers, environment, and manufacturers to improve asset management and energy efficiency capabilities one bearing at a time.

  8. On-line method of determining utilization factor in Hg-196 photochemical separation process

    DOE Patents [OSTI]

    Grossman, Mark W.; Moskowitz, Philip E.

    1992-01-01

    The present invention is directed to a method for determining the utilization factor [U] in a photochemical mercury enrichment process (.sup.196 Hg) by measuring relative .sup.196 Hg densities using absorption spectroscopy.

  9. Using the apparent diffusion coefficient to identifying MGMT promoter methylation status early in glioblastoma: importance of analytical method

    SciTech Connect (OSTI)

    Rundle-Thiele, Dayle; Day, Bryan; Stringer, Brett; Fay, Michael; Martin, Jennifer; Jeffree, Rosalind L; Thomas, Paul; Bell, Christopher; Salvado, Olivier; Gal, Yaniv; Coulthard, Alan; Crozier, Stuart; Rose, Stephen

    2015-06-15

    Accurate knowledge of O{sup 6}-methylguanine methyltransferase (MGMT) gene promoter subtype in patients with glioblastoma (GBM) is important for treatment. However, this test is not always available. Pre-operative diffusion MRI (dMRI) can be used to probe tumour biology using the apparent diffusion coefficient (ADC); however, its ability to act as a surrogate to predict MGMT status has shown mixed results. We investigated whether this was due to variations in the method used to analyse ADC. We undertook a retrospective study of 32 patients with GBM who had MGMT status measured. Matching pre-operative MRI data were used to calculate the ADC within contrast enhancing regions of tumour. The relationship between ADC and MGMT was examined using two published ADC methods. A strong trend between a measure of ‘minimum ADC’ and methylation status was seen. An elevated minimum ADC was more likely in the methylated compared to the unmethylated MGMT group (U = 56, P = 0.0561). In contrast, utilising a two-mixture model histogram approach, a significant reduction in mean measure of the ‘low ADC’ component within the histogram was associated with an MGMT promoter methylation subtype (P < 0.0246). This study shows that within the same patient cohort, the method selected to analyse ADC measures has a significant bearing on the use of that metric as a surrogate marker of MGMT status. Thus for dMRI data to be clinically useful, consistent methods of data analysis need to be established prior to establishing any relationship with genetic or epigenetic profiling.

  10. Methods of use of calcium hexa aluminate refractory linings and/or chemical barriers in high alkali or alkaline environments

    DOE Patents [OSTI]

    McGowan, Kenneth A; Cullen, Robert M; Keiser, James R; Hemrick, James G; Meisner, Roberta A

    2013-10-22

    A method for improving the insulating character/and or penetration resistance of a liner in contact with at least one of an alkali and/or alkaline environments is provided. The method comprises lining a surface that is subject to wear by an alkali environment and/or an alkaline environment with a refractory composition comprising a refractory aggregate consisting essentially of a calcium hexa aluminate clinker having the formula CA.sub.6, wherein C is equal to calcium oxide, wherein A is equal to aluminum oxide, and wherein the hexa aluminate clinker has from zero to less than about fifty weight percent C.sub.12A.sub.7, and wherein greater than 98 weight percent of the calcium hexa aluminate clinker having a particle size ranging from -20 microns to +3 millimeters, for forming a liner of the surface. This method improves the insulating character/and or penetration resistance of the liner.

  11. Method and apparatus for measuring on-line failure of turbine thermal barrier coatings

    DOE Patents [OSTI]

    Zombo, Paul J.; Lemieux, Dennis; Diatzikis, Evangelos

    2010-04-06

    A method of remotely monitoring the radiant energy (6) emitted from a turbine component such as a turbine blade (1) having a low-reflective surface coating (3) which may be undergoing potential degradation is used to determine whether erosion, spallation, delamination, or the like, of the coating (3) is occurring.

  12. Method and apparatus for measuring on-line failure of turbine thermal barrier coatings

    DOE Patents [OSTI]

    Zombo, Paul J.; Lemieux, Dennis; Diatzikis, Evangelos

    2010-04-06

    A method of remotely monitoring the radiant energy (6) emitted from a turbine component such as a turbine blade (1) having a low-reflective surface coating (3) which may be undergoing potential degradation is used to determine whether erosion, spallation, delamination, or the like, of the coating (3) is occurring.

  13. Analytical Chemistry Laboratory, progress report for FY 1993

    SciTech Connect (OSTI)

    Not Available

    1993-12-01

    The purpose of this report is to summarize the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year (FY) 1993 (October 1992 through September 1993). This annual report is the tenth for the ACL and describes continuing effort on projects, work on new projects, and contributions of the ACL staff to various programs at ANL. The Analytical Chemistry Laboratory is a full-cost-recovery service center, with the primary mission of providing a broad range of analytical chemistry support services to the scientific and engineering programs at ANL. The ACL also has research programs in analytical chemistry, conducts instrumental and methods development, and provides analytical services for governmental, educational, and industrial organizations. The ACL handles a wide range of analytical problems. Some routine or standard analyses are done, but it is common for the Argonne programs to generate unique problems that require development or modification of methods and adaption of techniques to obtain useful analytical data. The ACL is administratively within the Chemical Technology Division (CMT), its principal ANL client, but provides technical support for many of the technical divisions and programs at ANL. The ACL has four technical groups--Chemical Analysis, Instrumental Analysis, Organic Analysis, and Environmental Analysis--which together include about 45 technical staff members. Talents and interests of staff members cross the group lines, as do many projects within the ACL.

  14. On-line fast response device and method for measuring dissolved gas in a fluid

    DOE Patents [OSTI]

    Tutu, Narinder Kumar

    2011-01-11

    A method and device for the measurement of dissolved gas within a fluid. The fluid, substantially a liquid, is pumped into a pipe. The flow of the fluid is temporally restricted, creating one or more low pressure regions. A measurement indicative of trapped air is taken before and after the restriction. The amount of dissolved air is calculated from the difference between the first and second measurements. Preferably measurements indicative of trapped air is obtained from one or more pressure transducers, capacitance transducers, or combinations thereof. In the alternative, other methods such as those utilizing x-rays or gamma rays may also be used to detect trapped air. Preferably, the fluid is a hydraulic fluid, whereby dissolved air in the fluid is detected.

  15. Analytical platform evaluation for quantification of ERG in prostate cancer using protein and mRNA detection methods

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    He, Jintang; Schepmoes, Athena A.; Shi, Tujin; Wu, Chaochao; Fillmore, Thomas L.; Gao, Yuqian; Smith, Richard D.; Qian, Weijun; Rodland, Karin D.; Liu, Tao; et al

    2015-01-01

    Background: The established methods for detecting prostate cancer (CaP) are based on tests using PSA (blood), PCA3 (urine), and AMACR (tissue) as biomarkers in patient samples. The demonstration of ERG oncoprotein overexpression due to gene fusion in CaP has thus provided ERG as an additional biomarker. Based on this, we hypothesized that ERG protein quantification methods can be of use in the diagnosis of prostate cancer. Methods: Therefore, an antibody-free assay for ERG3 protein detection was developed based on PRISM (high-pressure high-resolution separations with intelligent selection and multiplexing)-SRM (selected reaction monitoring) mass spectrometry. We utilized TMPRSS2-ERG positive VCaP and TMPRSS2-ERGmore » negative LNCaP cells to simulate three different sample types (cells, tissue, and post-DRE urine sediment). Results: Recombinant ERG3 protein spiked into LNCaP cell lysates could be detected at levels as low as 20 pg by PRISM-SRM analysis. The sensitivity of the PRISM-SRM assay was around approximately 10,000 VCaP cells in a mixed cell population model of VCaP and LNCaP cells. Interestingly, ERG protein could be detected in as few as 600 VCaP cells spiked into female urine. The sensitivity of the in-house enzyme-linked immunosorbent assay (ELISA) was similar to the PRISM-SRM assay, with detection of 30 pg of purified recombinant ERG3 protein and 10,000 VCaP cells. On the other hand, qRT-PCR exhibited a higher sensitivity, as TMPRSS2-ERG transcripts were detected in as few as 100 VCaP cells, in comparison to NanoString methodologies which detected ERG from 10,000 cells. Conclusions: Based on this data, we propose that the detection of both ERG transcriptional products with RNA-based assays, as well as protein products of ERG using PRISM-SRM assays, may be of clinical value in developing diagnostics and prognostics assays for prostate cancer given their sensitivity, specificity, and reproducibility.« less

  16. Analytical platform evaluation for quantification of ERG in prostate cancer using protein and mRNA detection methods

    SciTech Connect (OSTI)

    He, Jintang; Schepmoes, Athena A.; Shi, Tujin; Wu, Chaochao; Fillmore, Thomas L.; Gao, Yuqian; Smith, Richard D.; Qian, Weijun; Rodland, Karin D.; Liu, Tao; Camp, David G.; Rastogi, Anshu; Tan, Shyh-Han; Yan, Wusheng; Mohamed, Ahmed A.; Huang, Wei; Banerjee, Sreedatta; Kagan, Jacob; Srivastava, Sudhir; McLeod, David; Srivastava, Shiv; Petrovics, Gyorgy; Dobi, Albert; Srinivasan, Alagarsamy

    2015-01-01

    Background: The established methods for detecting prostate cancer (CaP) are based on tests using PSA (blood), PCA3 (urine), and AMACR (tissue) as biomarkers in patient samples. The demonstration of ERG oncoprotein overexpression due to gene fusion in CaP has thus provided ERG as an additional biomarker. Based on this, we hypothesized that ERG protein quantification methods can be of use in the diagnosis of prostate cancer. Methods: Therefore, an antibody-free assay for ERG3 protein detection was developed based on PRISM (high-pressure high-resolution separations with intelligent selection and multiplexing)-SRM (selected reaction monitoring) mass spectrometry. We utilized TMPRSS2-ERG positive VCaP and TMPRSS2-ERG negative LNCaP cells to simulate three different sample types (cells, tissue, and post-DRE urine sediment). Results: Recombinant ERG3 protein spiked into LNCaP cell lysates could be detected at levels as low as 20 pg by PRISM-SRM analysis. The sensitivity of the PRISM-SRM assay was around approximately 10,000 VCaP cells in a mixed cell population model of VCaP and LNCaP cells. Interestingly, ERG protein could be detected in as few as 600 VCaP cells spiked into female urine. The sensitivity of the in-house enzyme-linked immunosorbent assay (ELISA) was similar to the PRISM-SRM assay, with detection of 30 pg of purified recombinant ERG3 protein and 10,000 VCaP cells. On the other hand, qRT-PCR exhibited a higher sensitivity, as TMPRSS2-ERG transcripts were detected in as few as 100 VCaP cells, in comparison to NanoString methodologies which detected ERG from 10,000 cells. Conclusions: Based on this data, we propose that the detection of both ERG transcriptional products with RNA-based assays, as well as protein products of ERG using PRISM-SRM assays, may be of clinical value in developing diagnostics and prognostics assays for prostate cancer given their sensitivity, specificity, and reproducibility.

  17. Capillary electrophoresis-fluorescence line narrowing system (CE-FLNS) for on-line structural characterization

    DOE Patents [OSTI]

    Jankowiak, R.J.; Small, G.J.; Shields, P.A.

    1999-04-27

    Capillary electrophoresis (CE) is interfaced with low temperature fluorescence line-narrowing (FLN) spectroscopy for on-line structural characterization of separated molecular analytes. 21 figs.

  18. Capillary electrophoresis-fluorescence line narrowing system (CE-FLNS) for on-line structural characterization

    DOE Patents [OSTI]

    Jankowiak, Ryszard J.; Small, Gerald J.; Shields, Peter A.

    1999-04-27

    Capillary electrophoresis (CE) is interfaced with low temperature fluorescence line-narrowing (FLN) spectroscopy for on-line structural characterization of separated molecular analytes.

  19. Filter for on-line air monitor unaffected by radon progeny and method of using same

    DOE Patents [OSTI]

    Phillips, Terrance D.; Edwards, Howard D.

    1999-01-01

    An apparatus for testing air having contaminants and radon progeny therein. The apparatus includes a sampling box having an inlet for receiving the air and an outlet for discharging the air. The sampling box includes a filter made of a plate of sintered stainless steel. The filter traps the contaminants, yet allows at least a portion of the radon progeny to pass therethrough. A method of testing air having contaminants and radon progeny therein. The method includes providing a testing apparatus that has a sampling box with an inlet for receiving the air and an outlet for discharging the air, and has a sintered stainless steel filter disposed within said sampling box; drawing air from a source into the sampling box using a vacuum pump; passing the air through the filter; monitoring the contaminants trapped by the filter; and providing an alarm when a selected level of contaminants is reached. The filter traps the contaminants, yet allows at least a portion of the radon progeny to pass therethrough.

  20. Testing of the method for water microleakage detection from OH hydroxyl spectral lines at the L-2M stellarator

    SciTech Connect (OSTI)

    Voronov, G. S. Berezhetskii, M. S.; Bondar', Yu. F.; Vafin, I. Yu.; Vasil'kov, D. G.; Voronova, E. V.; Grebenshchikov, S. E.; Grishina, I. A.; Larionova, N. F.; Letunov, A. A.; Logvinenko, V. P.; Meshcheryakov, A. I.; Pleshkov, E. I.; Khol'nov, Yu. V.; Fedyanin, O. I.; Tsygankov, V. A.; Shchepetov, S. V.; Kurnaev, V. A.; Vizgalov, I. V.; Urusov, V. A.; and others

    2013-04-15

    Results are presented from L-2M stellarator experiments on testing a possible method for detection of water microleakages in the cooling system of the first wall and vacuum chamber of ITER. The method consists in the spectroscopic detection of spectral lines of the OH hydroxyl, which forms via the dissociation of water molecules in plasma. Emission in the spectral band of 305-310 nm can be detected even at water leakage rates less than 10{sup -4} Pa m{sup 3}/s. Chemical reactions between water and boron compounds on the vacuum chamber wall delay the detection of leakages up to {approx}2000 s. A similar phenomenon can be expected when a leakage will occur in ITER, where the materials suggested for the first wall (Be, Li) can also chemically react with water.

  1. Method for on-line evaluation of materials using prompt gamma ray analysis

    DOE Patents [OSTI]

    Akers, Douglas W.

    2009-12-08

    A method for evaluating a material specimen comprises: Mounting a neutron source and a detector adjacent the material specimen; bombarding the material specimen with neutrons from the neutron source to create prompt gamma rays within the material specimen, some of the prompt gamma rays being emitted from the material specimen, some of the prompt gamma rays resulting in the formation of positrons within the material specimen by pair production; collecting positron annihilation data by detecting with the detector at least one emitted annihilation gamma ray resulting from the annihilation of a positron; storing the positron annihilation data on a data storage system for later retrieval and processing; and continuing to collect and store positron annihilation data, the continued collected and stored positron annihilation data being indicative of an accumulation of lattice damage over time.

  2. APPLICATION OF COLUMN EXTRACTION METHOD FOR IMPURITIES ANALYSIS ON HB-LINE PLUTONIUM OXIDE IN SUPPORT OF MOX FEED PRODUCT SPECIFICATIONS

    SciTech Connect (OSTI)

    Jones, M.; Diprete, D.; Wiedenman, B.

    2012-03-20

    The current mission at H-Canyon involves the dissolution of an Alternate Feedstocks 2 (AFS-2) inventory that contains plutonium metal. Once dissolved, HB-Line is tasked with purifying the plutonium solution via anion exchange, precipitating the Pu as oxalate, and calcining to form plutonium oxide (PuO{sub 2}). The PuO{sub 2} will provide feed product for the Mixed Oxide (MOX) Fuel Fabrication Facility, and the anion exchange raffinate will be transferred to H-Canyon. The results presented in this report document the potential success of the RE resin column extraction application on highly concentrated Pu samples to meet MOX feed product specifications. The original 'Hearts Cut' sample required a 10000x dilution to limit instrument drift on the ICP-MS method. The instrument dilution factors improved to 125x and 250x for the sample raffinate and sample eluent, respectively. As noted in the introduction, the significantly lower dilutions help to drop the total MRL for the analyte. Although the spike recoveries were half of expected in the eluent for several key elements, they were between 94-98% after Nd tracer correction. It is seen that the lower ICD limit requirements for the rare earths are attainable because of less dilution. Especially important is the extremely low Ga limit at 0.12 {mu}g/g Pu; an ICP-MS method is now available to accomplish this task on the sample raffinate. While B and V meet the column A limits, further development is needed to meet the column B limits. Even though V remained on the RE resin column, an analysis method is ready for investigation on the ICP-MS, but it does not mean that V cannot be measured on the ICP-ES at a low dilution to meet the column B limits. Furthermore, this column method can be applicable for ICP-ES as shown in Table 3-2, in that it trims the sample of Pu, decreasing and sometimes eliminating Pu spectral interferences.

  3. Non-Destructive Evaluation of Slot-Die-Coated Lithium Secondary Battery Electrodes by In-Line Laser Caliper and IR Thermography Methods-Journal Cover Page

    SciTech Connect (OSTI)

    Mohanty, Debasish; Li, Jianlin; Born, Rachael; Maxey, L Curt; Dinwiddie, Ralph Barton; Daniel, Claus; Wood III, David L

    2014-01-01

    Note: This is a cover page for the 'Analytical Methods' journal, which was requested by the journal editor for consideration. The article has already been published and the PTS publication ID is 44000. The acknowledgements are same as mentioned in the PTS publication ID 44000.

  4. Analytical Chemistry Laboratory Progress Report for FY 1994

    SciTech Connect (OSTI)

    Green, D.W.; Boparai, A.S.; Bowers, D.L.

    1994-12-01

    The purpose of this report is to summarize the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year (FY) 1994 (October 1993 through September 1994). This annual report is the eleventh for the ACL and describes continuing effort on projects, work on new projects, and contributions of the ACL staff to various programs at ANL. The Analytical Chemistry Laboratory is a full-cost-recovery service center, with the primary mission of providing a broad range of analytical chemistry support services to the scientific and engineering programs at ANL. The ACL also has a research program in analytical chemistry, conducts instrumental and methods development, and provides analytical services for governmental, educational, and industrial organizations. The ACL handles a wide range of analytical problems. Some routine or standard analyses are done, but it is common for the Argonne programs to generate unique problems that require significant development of methods and adaption of techniques to obtain useful analytical data. The ACL has four technical groups -- Chemical Analysis, Instrumental Analysis, Organic Analysis, and Environmental Analysis -- which together include about 45 technical staff members. Talents and interests of staff members cross the group lines, as do many projects within the ACL. The Chemical Analysis Group uses wet- chemical and instrumental methods for elemental, compositional, and isotopic determinations in solid, liquid, and gaseous samples and provides specialized analytical services. Major instruments in this group include an ion chromatograph (IC), an inductively coupled plasma/atomic emission spectrometer (ICP/AES), spectrophotometers, mass spectrometers (including gas-analysis and thermal-ionization mass spectrometers), emission spectrographs, autotitrators, sulfur and carbon determinators, and a kinetic phosphorescence uranium analyzer.

  5. Industrial Analytics Corporation

    SciTech Connect (OSTI)

    Industrial Analytics Corporation

    2004-01-30

    The lost foam casting process is sensitive to the properties of the EPS patterns used for the casting operation. In this project Industrial Analytics Corporation (IAC) has developed a new low voltage x-ray instrument for x-ray radiography of very low mass EPS patterns. IAC has also developed a transmitted visible light method for characterizing the properties of EPS patterns. The systems developed are also applicable to other low density materials including graphite foams.

  6. Laboratory Analytical Procedures | Bioenergy | NREL

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Laboratory Analytical Procedures NREL develops laboratory analytical procedures (LAPs) to provide validated methods for biofuels and pyrolysis bio-oils research. Biomass Compositional Analysis These lab procedures provide tested and accepted methods for performing analyses commonly used in biofuels research. Bio-Oil Analysis These lab procedures allow for the analysis of raw and upgraded pyrolysis bio-oils. Microalgae Compositional Analysis These lab procedures help scientists and researchers

  7. Data and Analytics Strategy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    and Analytics Strategy --- 1 --- Prabhat Data and Analytics Group Lead February 23, 2015 ... ata S o6ware * Big D ata U sers --- 3 --- Data and Analytics Team --- 4 --- DAS T eam M ...

  8. Functionalized magnetic nanoparticle analyte sensor

    DOE Patents [OSTI]

    Yantasee, Wassana; Warner, Maryin G; Warner, Cynthia L; Addleman, Raymond S; Fryxell, Glen E; Timchalk, Charles; Toloczko, Mychailo B

    2014-03-25

    A method and system for simply and efficiently determining quantities of a preselected material in a particular solution by the placement of at least one superparamagnetic nanoparticle having a specified functionalized organic material connected thereto into a particular sample solution, wherein preselected analytes attach to the functionalized organic groups, these superparamagnetic nanoparticles are then collected at a collection site and analyzed for the presence of a particular analyte.

  9. Analytical Services - Hanford Site

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Contracting Wastren Advantage, Inc. Analytical Services Contracting ORP Contracts and Procurements RL Contracts and Procurements CH2M HILL Plateau Remediation Company Mission Support Alliance Washington Closure Hanford HPM Corporation (HPMC) Wastren Advantage, Inc. Analytical Services HASQARD Focus Group Bechtel National, Inc. Washington River Protection Solutions Analytical Services Email Email Page | Print Print Page | Text Increase Font Size Decrease Font Size Analytical laboratory analyses

  10. Scientific Achievement Analytical Transmission Electron Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Analytical Transmission Electron Microscopy (TEM) method was developed to determine thickness and wrinkles in electron beam sensitive 2-dimensional (2D) MFI nanosheets....

  11. Derivation of general analytic gradient expressions for density-fitted post-Hartree-Fock methods: An efficient implementation for the density-fitted second-order MllerPlesset perturbation theory

    SciTech Connect (OSTI)

    Bozkaya, U?ur

    2014-09-28

    General analytic gradient expressions (with the frozen-core approximation) are presented for density-fitted post-HF methods. An efficient implementation of frozen-core analytic gradients for the second-order MllerPlesset perturbation theory (MP2) with the density-fitting (DF) approximation (applying to both reference and correlation energies), which is denoted as DF-MP2, is reported. The DF-MP2 method is applied to a set of alkanes, conjugated dienes, and noncovalent interaction complexes to compare the computational cost of single point analytic gradients with MP2 with the resolution of the identity approach (RI-MP2) [F. Weigend and M. Hser, Theor. Chem. Acc. 97, 331 (1997); R. A. Distasio, R. P. Steele, Y. M. Rhee, Y. Shao, and M. Head-Gordon, J. Comput. Chem. 28, 839 (2007)]. In the RI-MP2 method, the DF approach is used only for the correlation energy. Our results demonstrate that the DF-MP2 method substantially accelerate the RI-MP2 method for analytic gradient computations due to the reduced input/output (I/O) time. Because in the DF-MP2 method the DF approach is used for both reference and correlation energies, the storage of 4-index electron repulsion integrals (ERIs) are avoided, 3-index ERI tensors are employed instead. Further, as in case of integrals, our gradient equation is completely avoid construction or storage of the 4-index two-particle density matrix (TPDM), instead we use 2- and 3-index TPDMs. Hence, the I/O bottleneck of a gradient computation is significantly overcome. Therefore, the cost of the generalized-Fock matrix (GFM), TPDM, solution of Z-vector equations, the back transformation of TPDM, and integral derivatives are substantially reduced when the DF approach is used for the entire energy expression. Further application results show that the DF approach introduce negligible errors for closed-shell reaction energies and equilibrium bond lengths.

  12. Multimedia Analysis plus Visual Analytics = Multimedia Analytics

    SciTech Connect (OSTI)

    Chinchor, Nancy; Thomas, James J.; Wong, Pak C.; Christel, Michael; Ribarsky, Martin W.

    2010-10-01

    Multimedia analysis has focused on images, video, and to some extent audio and has made progress in single channels excluding text. Visual analytics has focused on the user interaction with data during the analytic process plus the fundamental mathematics and has continued to treat text as did its precursor, information visualization. The general problem we address in this tutorial is the combining of multimedia analysis and visual analytics to deal with multimedia information gathered from different sources, with different goals or objectives, and containing all media types and combinations in common usage.

  13. Actinide Analytical Chemistry

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AAC Actinide Analytical Chemistry We do analyses that range from assay of the major and ... Group Office (505) 667-4087 The Actinide Analytical Chemistry (C-AAC) Group at Los Alamos ...

  14. An analytical coarse-graining method which preserves the free energy, structural correlations, and thermodynamic state of polymer melts from the atomistic to the mesoscale

    SciTech Connect (OSTI)

    McCarty, J.; Clark, A. J.; Copperman, J.; Guenza, M. G.

    2014-05-28

    Structural and thermodynamic consistency of coarse-graining models across multiple length scales is essential for the predictive role of multi-scale modeling and molecular dynamic simulations that use mesoscale descriptions. Our approach is a coarse-grained model based on integral equation theory, which can represent polymer chains at variable levels of chemical details. The model is analytical and depends on molecular and thermodynamic parameters of the system under study, as well as on the direct correlation function in the k ? 0 limit, c{sub 0}. A numerical solution to the PRISM integral equations is used to determine c{sub 0}, by adjusting the value of the effective hard sphere diameter, d{sub HS}, to agree with the predicted equation of state. This single quantity parameterizes the coarse-grained potential, which is used to perform mesoscale simulations that are directly compared with atomistic-level simulations of the same system. We test our coarse-graining formalism by comparing structural correlations, isothermal compressibility, equation of state, Helmholtz and Gibbs free energies, and potential energy and entropy using both united atom and coarse-grained descriptions. We find quantitative agreement between the analytical formalism for the thermodynamic properties, and the results of Molecular Dynamics simulations, independent of the chosen level of representation. In the mesoscale description, the potential energy of the soft-particle interaction becomes a free energy in the coarse-grained coordinates which preserves the excess free energy from an ideal gas across all levels of description. The structural consistency between the united-atom and mesoscale descriptions means the relative entropy between descriptions has been minimized without any variational optimization parameters. The approach is general and applicable to any polymeric system in different thermodynamic conditions.

  15. 100-B/C Target Analyte List Development for Soil

    SciTech Connect (OSTI)

    R.W. Ovink

    2010-03-18

    This report documents the process used to identify source area target analytes in support of the 100-B/C remedial investigation/feasibility study addendum to DOE/RL-2008-46. This report also establishes the analyte exclusion criteria applicable for 100-B/C use and the analytical methods needed to analyze the target analytes.

  16. Savannah River Analytical Laboratories Achieve International Standard

    National Nuclear Security Administration (NNSA)

    Accreditation | National Nuclear Security Administration | (NNSA) Savannah River Analytical Laboratories Achieve International Standard Accreditation Tuesday, September 8, 2015 - 12:55pm Savannah River National Laboratory's F/H Analytical Laboratories have achieved ISO/IEC 17025 accreditation, which represents an independent validation of two analytical methods against a set of world-class specifications. The accreditation was formally awarded by the American Association for Laboratory

  17. POLARIZED LINE FORMATION IN MULTI-DIMENSIONAL MEDIA. II. A FAST METHOD TO SOLVE PROBLEMS WITH PARTIAL FREQUENCY REDISTRIBUTION

    SciTech Connect (OSTI)

    Anusha, L. S.; Nagendra, K. N.; Paletou, F.

    2011-01-10

    In the previous paper of this series, we presented a formulation of the polarized radiative transfer equation for resonance scattering with partial frequency redistribution (PRD) in multi-dimensional media for a two-level atom model with unpolarized ground level, using the irreducible spherical tensors T{sub Q}{sup K}(i, {Omega}) for polarimetry. We also presented a polarized approximate lambda iteration method to solve this equation using the Jacobi iteration scheme. The formal solution used was based on a simple finite volume technique. In this paper, we develop a faster and more efficient method which uses the projection techniques applied to the radiative transfer equation (the Stabilized Preconditioned Bi-Conjugate Gradient method). We now use a more accurate formal solver, namely the well-known two-dimensional (2D) short characteristics method. Using the numerical method developed in Paper I, we can consider only simpler cases of finite 2D slabs due to computational limitations. Using the method developed in this paper, we could compute PRD solutions in 2D media in the more difficult context of semi-infinite 2D slabs also. We present several solutions which may serve as benchmarks in future studies in this area.

  18. Web Analytics and Statistics

    Office of Energy Efficiency and Renewable Energy (EERE)

    EERE uses Google Analytics to capture statistics on its websites. These statistics help website managers measure and report on users, sessions, most visited pages, and more.

  19. Bioanalytical Applications of Fluorescence Line-Narrowing and Non-Line-Narrowing Spectroscopy Interfaced with Capillary Electrophoresis and High-Performance Liquid Chromatography

    SciTech Connect (OSTI)

    Kenneth Paul Roberts

    2002-06-27

    Capillary electrophoresis (CE) and high-performance liquid chromatography (HPLC) are widely used analytical separation techniques with many applications in chemical, biochemical, and biomedical sciences. Conventional analyte identification in these techniques is based on retention/migration times of standards; requiring a high degree of reproducibility, availability of reliable standards, and absence of coelution. From this, several new information-rich detection methods (also known as hyphenated techniques) are being explored that would be capable of providing unambiguous on-line identification of separating analytes in CE and HPLC. As further discussed, a number of such on-line detection methods have shown considerable success, including Raman, nuclear magnetic resonance (NMR), mass spectrometry (MS), and fluorescence line-narrowing spectroscopy (FLNS). In this thesis, the feasibility and potential of combining the highly sensitive and selective laser-based detection method of FLNS with analytical separation techniques are discussed and presented. A summary of previously demonstrated FLNS detection interfaced with chromatography and electrophoresis is given, and recent results from on-line FLNS detection in CE (CE-FLNS), and the new combination of HPLC-FLNS, are shown.

  20. Nucleic acid-coupled colorimetric analyte detectors

    DOE Patents [OSTI]

    Charych, Deborah H.; Jonas, Ulrich

    2001-01-01

    The present invention relates to methods and compositions for the direct detection of analytes and membrane conformational changes through the detection of color changes in biopolymeric materials. In particular, the present invention provide for the direct colorimetric detection of analytes using nucleic acid ligands at surfaces of polydiacetylene liposomes and related molecular layer systems.

  1. Extreme Scale Visual Analytics

    SciTech Connect (OSTI)

    Steed, Chad A; Potok, Thomas E; Pullum, Laura L; Ramanathan, Arvind; Shipman, Galen M; Thornton, Peter E; Potok, Thomas E

    2013-01-01

    Given the scale and complexity of today s data, visual analytics is rapidly becoming a necessity rather than an option for comprehensive exploratory analysis. In this paper, we provide an overview of three applications of visual analytics for addressing the challenges of analyzing climate, text streams, and biosurveilance data. These systems feature varying levels of interaction and high performance computing technology integration to permit exploratory analysis of large and complex data of global significance.

  2. Electric and magnetic field reduction by alternative transmission line options

    SciTech Connect (OSTI)

    Stewart, J.R. ); Dale, S.J. ); Klein, K.W. )

    1991-01-01

    Ground level electric, and more recently magnetic, fields from overhead power transmission lines are increasingly important considerations in right of way specification, with states setting or planning to set edge of right of way limits. Research has been conducted in high phase order power transmission wherein six of twelve phases are used to transmit power in less physical space and with reduced electrical environmental effects than conventional designs. The first magnetic field testing, as reported in this paper, has verified predictive methods for determination of magnetic fields from high phase order lines. Based on these analytical methods, field profiles have been determined for lines of different phase order of comparable power capacity. Potential advantages of high phase order as a means of field mitigation are discussed. 10 refs., 12 figs., 3 tabs.

  3. Chemometrics/on-line measurements

    SciTech Connect (OSTI)

    O'Rourke, P.E. )

    1989-11-01

    The possible future of on-line analytical-quality measurements for improved process control and more timely safeguards measurements is examined in the light of a current project at Savannah River. A measurement system involving a fiber-optic spectrophotometer and the application of mathematical techniques called chemometrics is described.

  4. Renewable Analytics | Open Energy Information

    Open Energy Info (EERE)

    Analytics Jump to: navigation, search Name: Renewable Analytics Place: San Francisco, California Zip: 94104 Product: San francisco-based provider of public market trading...

  5. Web Applications for Data Analytics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Web Applications for Data Web Applications for Data Analytics Description and Overview NERSC is providing, on an experimental basis, web-based applications for data analytics. This ...

  6. Technical Letter Report Assessment of Ultrasonic Phased Array Inspection Method for Welds in Cast Austenitic Stainless Steel Pressurizer Surge Line Piping JCN N6398, Task 1B

    SciTech Connect (OSTI)

    Diaz, Aaron A.; Cinson, Anthony D.; Crawford, Susan L.; Mathews, Royce; Moran, Traci L.; Anderson, Michael T.

    2009-07-28

    Research is being conducted for the U.S. Nuclear Regulatory Commission (NRC) at the Pacific Northwest National Laboratory (PNNL) to assess the effectiveness and reliability of advanced nondestructive examination (NDE) methods for the inspection of light water reactor components. The scope of this research encompasses primary system pressure boundary materials including cast austenitic stainless steels (CASS); dissimilar metal welds; piping with corrosion-resistant cladding; weld overlays, inlays and onlays; and far-side examinations of austenitic piping welds. A primary objective of this work is to evaluate various NDE methods to assess their ability to detect, localize, and size cracks in coarse-grained steel components. In this effort, PNNL supports cooperation with Commissariat à l’Energie Atomique (CEA) to assess reliable inspection of CASS materials. The NRC Project Manager has established a cooperative effort with the Institut de Radioprotection et de Surete Nucleaire (IRSN). CEA, under funding from IRSN, are supporting collaborative efforts with the NRC and PNNL. Regarding its work on the NDE of materials, CEA is providing its modeling software (CIVA) in exchange for PNNL offering expertise and data related to phased-array detection and sizing, acoustic attenuation, and back scattering on CASS materials. This collaboration benefits the NRC because CEA performs research and development on CASS for Électricité de France (EdF). This technical letter report provides a summary of a technical evaluation aimed at assessing the capabilities of phased-array (PA) ultrasonic testing (UT) methods as applied to the inspection of welds in CASS pressurizer (PZR) surge line nuclear reactor piping. A set of thermal fatigue cracks (TFCs) was implanted into three CASS PZR surge-line specimens (pipe-to-elbow welds) that were fabricated using vintage CASS materials formed in the 1970s, and flaw responses from these cracks were used to evaluate detection and sizing

  7. Analytical SFE applied to polymeric materials

    SciTech Connect (OSTI)

    Taylor, L.T.

    1995-12-31

    Polymeric materials afford unique challenges for analytical supercritical fluid extraction. Oligomeric components, monomers, anti-oxidants, finishes, residual solvents and processing additives are some of the analytes of interest. In addition to their marginal solubility in 100% CO{sub 2}, the extraction analyte is many times diffusion limited rather than enthalpically driven which means that exhaustive extractions from polymer matrices may be slow. The presentation will draw upon our experiences in the (a) fractionation of high density polyethylene with supercritical propane-modified CO{sub 2}, (b) coupling of SFE and Fourier Transform Infrared Spectrometry (FT-IR) for analysis of finishes from polyester, nylon, aramid, and polyurethane, and (c) removal of low molecular weight oligomers and additives from polyamides and polystyrene and their identification by on-line supercritical fluid chromatography/FT-IR.

  8. Analyte sensing mediated by adapter/carrier molecules

    DOE Patents [OSTI]

    Bayley, Hagan; Braha, Orit; Gu, LiQun

    2002-07-30

    This invention relates to an improved method and system for sensing of one or more analytes. A host molecule, which serves as an adapter/carrier, is used to facilitate interaction between the analyte and the sensor element. A detectable signal is produced reflecting the identity and concentration of analyte present.

  9. Preconcentration and separation of analytes in microchannels

    DOE Patents [OSTI]

    Hatch, Anson; Singh, Anup K.; Herr, Amy E.; Throckmorton, Daniel J.

    2010-11-09

    Disclosed herein are methods and devices for preconcentrating and separating analytes such as proteins and polynucleotides in microchannels. As disclosed, at least one size-exclusion polymeric element is adjacent to processing area or an assay area in a microchannel which may be porous polymeric element. The size-exclusion polymeric element may be used to manipulate, e.g. concentrate, analytes in a sample prior to assaying in the assay area.

  10. Line Projects

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Grand Coulee Transmission Line Replacement Project Hooper Springs McNary-John Day Montana-to-Washington Transmission System Upgrade Project - M2W Olympia-Grand Coulee No. 1...

  11. Biodiesel Utilization: Update on Recent Analytical Techniques (Presentation)

    SciTech Connect (OSTI)

    Alleman, T. L.; Fouts, L.; Luecke, J.; Thornton, M.; McAlpin, C.

    2009-05-01

    To understand and increase the use of biodiesel, analytical methods need to be shared and compared to ensure that accurate data are gathered on this complex fuel.

  12. Sol-Gel Matrices For Direct Colorimetric Detection Of Analytes

    DOE Patents [OSTI]

    Charych, Deborah H.; Sasaki, Darryl; Yamanaka, Stacey

    2002-11-26

    The present invention relates to methods and compositions for the direct detection of analytes using color changes that occur in immobilized biopolymeric material in response to selective binding of analytes to their surface. In particular, the present invention provides methods and compositions related to the encapsulation of biopolymeric material into metal oxide glass using the sol-gel method.

  13. Sol-gel matrices for direct colorimetric detection of analytes

    DOE Patents [OSTI]

    Charych, Deborah H.; Sasaki, Darryl; Yamanaka, Stacey

    2000-01-01

    The present invention relates to methods and compositions for the direct detection of analytes using color changes that occur in immobilized biopolymeric material in response to selective binding of analytes to their surface. In particular, the present invention provides methods and compositions related to the encapsulation of biopolymeric material into metal oxide glass using the sol-gel method.

  14. Flow line sampler

    DOE Patents [OSTI]

    Nicholls, Colin I.

    1992-07-14

    An on-line product sampling apparatus and method for measuring product samples from a product stream (12) in a flow line (14) having a sampling aperture (11), includes a sampling tube (18) for containing product samples removed from flow line (14). A piston (22) removes product samples from the product stream (12) through the sampling aperture (11) and returns samples to product stream (12). A sensor (20) communicates with sample tube (18), and senses physical properties of samples while the samples are within sample tube (18). In one embodiment, sensor (20) comprises a hydrogen transient nuclear magnetic resonance sensor for measuring physical properties of hydrogen molecules.

  15. Electric Transmission Line Siting Compact

    Office of Environmental Management (EM)

    ... creates a method for states to site multi-state electric transmission lines. Three 4 levels of organization are provided: 5 A state project review panel within each ...

  16. Evaluation methodology for comparing memory and communication of analytic processes in visual analytics

    SciTech Connect (OSTI)

    Ragan, Eric D; Goodall, John R

    2014-01-01

    Provenance tools can help capture and represent the history of analytic processes. In addition to supporting analytic performance, provenance tools can be used to support memory of the process and communication of the steps to others. Objective evaluation methods are needed to evaluate how well provenance tools support analyst s memory and communication of analytic processes. In this paper, we present several methods for the evaluation of process memory, and we discuss the advantages and limitations of each. We discuss methods for determining a baseline process for comparison, and we describe various methods that can be used to elicit process recall, step ordering, and time estimations. Additionally, we discuss methods for conducting quantitative and qualitative analyses of process memory. By organizing possible memory evaluation methods and providing a meta-analysis of the potential benefits and drawbacks of different approaches, this paper can inform study design and encourage objective evaluation of process memory and communication.

  17. Spark Distributed Analytic Framework

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Apache Spark Spark Distributed Analytic Framework Description and Overview Apache Spark(tm) is a fast and general engine for large-scale data processing. How to Use Spark Because of its high memory and I/O bandwidth requirements, we recommend you run your spark jobs on Cori. Follow the steps below to use spark, note that the order of the commands matters. DO NOT load the spark module until you are inside a batch job. Interactive mode Submit an interactive batch job with at least 2 nodes: salloc

  18. Sandia National Laboratories: Data Analytics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Pathfinder Airborne ISR Systems What is SAR? Areas of Expertise Images VideoSAR Publications Facebook Twitter YouTube Flickr RSS Top Areas of Expertise Capabilities Hardware Modes & Frequency Bands of Operation Platforms Missions Tasking, Processing, Exploitation & Dissemination (TPED) Data Analytics Pathfinder Airborne ISR Systems Data Analytics Data Analytics Sandia National Laboratories: Synthetic Apperature Radar (SAR): SAR Hardware PANTHER - Pattern ANalytics To support

  19. Hanford analytical services quality assurance requirements documents

    SciTech Connect (OSTI)

    Hyatt, J.E.

    1997-09-25

    Hanford Analytical Services Quality Assurance Requirements Document (HASQARD) is issued by the Analytical Services, Program of the Waste Management Division, US Department of Energy (US DOE), Richland Operations Office (DOE-RL). The HASQARD establishes quality requirements in response to DOE Order 5700.6C (DOE 1991b). The HASQARD is designed to meet the needs of DOE-RL for maintaining a consistent level of quality for sampling and field and laboratory analytical services provided by contractor and commercial field and laboratory analytical operations. The HASQARD serves as the quality basis for all sampling and field/laboratory analytical services provided to DOE-RL through the Analytical Services Program of the Waste Management Division in support of Hanford Site environmental cleanup efforts. This includes work performed by contractor and commercial laboratories and covers radiological and nonradiological analyses. The HASQARD applies to field sampling, field analysis, and research and development activities that support work conducted under the Hanford Federal Facility Agreement and Consent Order Tri-Party Agreement and regulatory permit applications and applicable permit requirements described in subsections of this volume. The HASQARD applies to work done to support process chemistry analysis (e.g., ongoing site waste treatment and characterization operations) and research and development projects related to Hanford Site environmental cleanup activities. This ensures a uniform quality umbrella to analytical site activities predicated on the concepts contained in the HASQARD. Using HASQARD will ensure data of known quality and technical defensibility of the methods used to obtain that data. The HASQARD is made up of four volumes: Volume 1, Administrative Requirements; Volume 2, Sampling Technical Requirements; Volume 3, Field Analytical Technical Requirements; and Volume 4, Laboratory Technical Requirements. Volume 1 describes the administrative requirements

  20. Development of data sets for the validation of analytical instrumentation

    SciTech Connect (OSTI)

    Ellison, S.L.R.; Cox, M.G.; Forbes, A.B.; Butler, B.P.

    1994-05-01

    Analytical chemistry makes use of a wide range of basic statistical operations, including means; standard deviations; significance tests based on assumed distributions; and linear, polynomial, and multivariate regression. The effects of limited numerical precision, poor choice of algorithm, and extreme dynamic range of these common statistical operations are discussed. The effects of incorrect choice of algorithm on calculations of basic statistical parameters and calibration lines are illustrated by examples. Some approaches to validation of such software are considered. The preparation of reference data sets for testing statistical software is discussed. The use of {open_quote}null space{close_quote} methods for producing reference data sets is described, and an example is given. These data sets have well-characterized properties and can be used to test the accuracy of basic statistical procedures. Specific properties that are controlled include the numerical precision required to represent the sets exactly and the analytically correct answers. A further property of some of the data sets under development is the predictability of the deviation from the expected results from poor choice of algorithm. 6 refs., 6 figs., 6 tabs.

  1. Using analytic continuation for the hadronic vacuum polarization computation

    SciTech Connect (OSTI)

    Feng, Xu; Hashimoto, Shoji; Hotzel, Grit; Jansen, Karl; Petschlies, Marcus; Renner Dru B

    2014-11-01

    We present two examples of applications of the analytic continuation method for computing the hadronic vacuum polarization function in space- and time-like momentum regions. These examples are the Adler function and the leading order hadronic contribution to the muon anomalous magnetic moment. We comment on the feasibility of the analytic continuation method and provide an outlook for possible further applications.

  2. VERDE Analytic Modules

    Energy Science and Technology Software Center (OSTI)

    2008-01-15

    The Verde Analytic Modules permit the user to ingest openly available data feeds about phenomenology (storm tracks, wind, precipitation, earthquake, wildfires, and similar natural and manmade power grid disruptions and forecast power outages, restoration times, customers outaged, and key facilities that will lose power. Damage areas are predicted using historic damage criteria of the affected area. The modules use a cellular automata approach to estimating the distribution circuits assigned to geo-located substations. Population estimates servedmore » within the service areas are located within 1 km grid cells and converted to customer counts by conversion through demographic estimation of households and commercial firms within the population cells. Restoration times are estimated by agent-based simulation of restoration crews working according to utility published prioritization calibrated by historic performance.« less

  3. Analytical Chemistry Laboratory progress report for FY 1991

    SciTech Connect (OSTI)

    Green, D.W.; Heinrich, R.R.; Graczyk, D.G.; Lindahl, P.C.; Boparai, A.S.

    1991-12-01

    The purpose of this report is to summarize the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year 1991 (October 1990 through September 1991). This is the eighth annual report for the ACL. The Analytical Chemistry Laboratory is a full-cost-recovery service center, with the primary mission of providing a broad range of analytical chemistry support services to the scientific and engineering programs at ANL. In addition, the ACL conducts a research program in analytical chemistry, works on instrumental and methods development, and provides analytical services for governmental, educational, and industrial organizations. The ACL handles a wide range of analytical problems, from routine standard analyses to unique problems that require significant development of methods and techniques.

  4. Appendix C, Analytical Data | Department of Energy

    Energy Savers [EERE]

    C, Analytical Data Appendix C, Analytical Data Docket No. EO-05-01: Appendix C, Analytical Data from Final Report: Particulate Emissions Testing, Unit 1, Potomac River Generating ...

  5. Existing technology transfer report: analytical capabilities. Appendix B. Volume 3

    SciTech Connect (OSTI)

    Tewari, K.C.

    1984-06-01

    The overall objective of the on-going analytical efforts was to develop in-house expertise and analytical capability for the analysis of coal and coal-derived products in support of SRC-I process technology. The approach taken and work accomplished involved: identification of test methods and associated equipment; review and implementation of analytical facility plan; evaluation of existing instrumentation; evaluation and purchase of new instruments; training of laboratory personnel; validation or development of analytical methods; development of standard product work-up methods and development of analytical protocol for detailed characterization of SRC-I solid and liquid products. This volume contains Appendix B with the following attachments: solvent separation procedure A; Wilsonville solvent separation procedure, distillation separation procedure; solvent separation modified Wilsonville Procedure W; statistical comparison of 3 solvent separation procedures; methods development for column chromatography, and application of gas chromatography to characterization of a hydrogen donor solvent; and high performance liquid chromatographic procedure.

  6. How to choose an online analytical system

    SciTech Connect (OSTI)

    Crandall, J.A. )

    1995-02-01

    To be competitive, hydrocarbon processing industry (HPI) operators must control their processes and product quality in real time. Using online process analytical systems, operators can collect, condition (if necessary) and analyze stream samples. Test results can be used for process control purposes and quality and environmental reports. Improving product stream data enhances control strategies. Quicker feedback on operating conditions and products yields many cost-effective benefits such as maximized uptime, improved process safety, higher product yields, reduced off-spec material, minimized waste products, etc. Before selecting an analytical method, operators should thoroughly investigate process products and operating conditions and their affects on analyzer hardware and software. Process engineers and operators, plant chemists, maintenance engineers and technicians must be involved from the beginning of the project. The paper describes designing a process analytical system, the components of such a system, and the analyzers.

  7. Deep Sludge Gas Release Event Analytical Evaluation

    SciTech Connect (OSTI)

    Sams, Terry L.

    2013-08-15

    Long Abstract. Full Text. The purpose of the Deep Sludge Gas Release Event Analytical Evaluation (DSGRE-AE) is to evaluate the postulated hypothesis that a hydrogen GRE may occur in Hanford tanks containing waste sludges at levels greater than previously experienced. There is a need to understand gas retention and release hazards in sludge beds which are 200 -300 inches deep. These sludge beds are deeper than historical Hanford sludge waste beds, and are created when waste is retrieved from older single-shell tanks (SST) and transferred to newer double-shell tanks (DST).Retrieval of waste from SSTs reduces the risk to the environment from leakage or potential leakage of waste into the ground from these tanks. However, the possibility of an energetic event (flammable gas accident) in the retrieval receiver DST is worse than slow leakage. Lines of inquiry, therefore, are (1) can sludge waste be stored safely in deep beds; (2) can gas release events (GRE) be prevented by periodically degassing the sludge (e.g., mixer pump); or (3) does the retrieval strategy need to be altered to limit sludge bed height by retrieving into additional DSTs? The scope of this effort is to provide expert advice on whether or not to move forward with the generation of deep beds of sludge through retrieval of C-Farm tanks. Evaluation of possible mitigation methods (e.g., using mixer pumps to release gas, retrieving into an additional DST) are being evaluated by a second team and are not discussed in this report. While available data and engineering judgment indicate that increased gas retention (retained gas fraction) in DST sludge at depths resulting from the completion of SST 241-C Tank Farm retrievals is not expected and, even if gas releases were to occur, they would be small and local, a positive USQ was declared (Occurrence Report EM-RP--WRPS-TANKFARM-2012-0014, "Potential Exists for a Large Spontaneous Gas Release Event in Deep Settled Waste Sludge"). The purpose of this technical

  8. Hanford transuranic analytical capability

    SciTech Connect (OSTI)

    McVey, C.B.

    1995-02-24

    With the current DOE focus on ER/WM programs, an increase in the quantity of waste samples that requires detailed analysis is forecasted. One of the prime areas of growth is the demand for DOE environmental protocol analyses of TRU waste samples. Currently there is no laboratory capacity to support analysis of TRU waste samples in excess of 200 nCi/gm. This study recommends that an interim solution be undertaken to provide these services. By adding two glove boxes in room 11A of 222S the interim waste analytical needs can be met for a period of four to five years or until a front end facility is erected at or near the 222-S facility. The yearly average of samples is projected to be approximately 600 samples. The figure has changed significantly due to budget changes and has been downgraded from 10,000 samples to the 600 level. Until these budget and sample projection changes become firmer, a long term option is not recommended at this time. A revision to this document is recommended by March 1996 to review the long term option and sample projections.

  9. Method For Chemical Sensing Using A Microfabricated Teeter-Totter Resonator

    DOE Patents [OSTI]

    Adkins, Douglas Ray; Heller, Edwin J.; Shul, Randy J.

    2004-11-30

    A method for sensing a chemical analyte in a fluid stream comprises providing a microfabricated teeter-totter resonator that relies upon a Lorentz force to cause oscillation in a paddle, applying a static magnetic field substantially aligned in-plane with the paddle, energizing a current conductor line on a surface of the paddle with an alternating electrical current to generate the Lorentz force, exposing the resonator to the analyte, and detecting the response of the oscillatory motion of the paddle to the chemical analyte. Preferably, a chemically sensitive coating is disposed on at least one surface of the paddle to enhance the sorption of the analyte by the paddle. The concentration of the analyte in a fluid stream can be determined by measuring the change in the resonant frequency or phase of the teeter-totter resonator as the chemical analyte is added to or removed from the paddle.

  10. Ecologic Analytics | Open Energy Information

    Open Energy Info (EERE)

    Analytics Place: Bloomington, Minnesota Zip: 55425 Product: Minnesota-based meter data management company. Coordinates: 42.883574, -90.926122 Show Map Loading map......

  11. Analytical Modeling | Open Energy Information

    Open Energy Info (EERE)

    & Analytical Models Website - University of Washington, Department of Economic Business and Geography Page Area Activity Start Date Activity End Date Reference Material...

  12. Analytical laboratory quality audits

    SciTech Connect (OSTI)

    Kelley, William D.

    2001-06-11

    Analytical Laboratory Quality Audits are designed to improve laboratory performance. The success of the audit, as for many activities, is based on adequate preparation, precise performance, well documented and insightful reporting, and productive follow-up. Adequate preparation starts with definition of the purpose, scope, and authority for the audit and the primary standards against which the laboratory quality program will be tested. The scope and technical processes involved lead to determining the needed audit team resources. Contact is made with the auditee and a formal audit plan is developed, approved and sent to the auditee laboratory management. Review of the auditee's quality manual, key procedures and historical information during preparation leads to better checklist development and more efficient and effective use of the limited time for data gathering during the audit itself. The audit begins with the opening meeting that sets the stage for the interactions between the audit team and the laboratory staff. Arrangements are worked out for the necessary interviews and examination of processes and records. The information developed during the audit is recorded on the checklists. Laboratory management is kept informed of issues during the audit so there are no surprises at the closing meeting. The audit report documents whether the management control systems are effective. In addition to findings of nonconformance, positive reinforcement of exemplary practices provides balance and fairness. Audit closure begins with receipt and evaluation of proposed corrective actions from the nonconformances identified in the audit report. After corrective actions are accepted, their implementation is verified. Upon closure of the corrective actions, the audit is officially closed.

  13. Analytical evaluation of atomic form factors: Application to Rayleigh scattering

    SciTech Connect (OSTI)

    Safari, L.; Santos, J. P.; Amaro, P.; Jnkl, K.; Fratini, F.

    2015-05-15

    Atomic form factors are widely used for the characterization of targets and specimens, from crystallography to biology. By using recent mathematical results, here we derive an analytical expression for the atomic form factor within the independent particle model constructed from nonrelativistic screened hydrogenic wave functions. The range of validity of this analytical expression is checked by comparing the analytically obtained form factors with the ones obtained within the Hartee-Fock method. As an example, we apply our analytical expression for the atomic form factor to evaluate the differential cross section for Rayleigh scattering off neutral atoms.

  14. Existing technology transfer report: analytical capabilities. Volume 1

    SciTech Connect (OSTI)

    Tewari, K.C.

    1984-06-01

    The overall objective of the on-going analytical efforts was to develop in-house expertise and analytical capability for the analysis of coal and coal-derived products in support of SRC-I process technology. The approach taken and work accomplished involved: identification of test methods and associated equipment; review and implementation of analytical facility plan; evaluation of existing instrumentation; evaluation and purchase of new instruments; training of laboratory personnel; validation or development of analytical methods; development of standard product work-up methods; and development of analytical protocol for detailed characterization of SRC-I solid and liquid products. Expertise in analytical chemistry was developed by organizing historical knowledge and assimilating new knowledge as it became available from inside and outside research facilities and the chemical literature. The data were then used to define analytical methods, instrumentation, space, staff needed to create a functional coal analysis laboratory. This report summarizes the direction and progress of the analytical development efforts during the period 1974 to 1980. 2 references, 5 figures.

  15. SUSS PM 5 Analytic Probe

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    SUSS PM 5 Analytic Probe analytic.jpg (63416 bytes) CAMD refurbished a Suss microprobe station to perform resist adhesion test. The apparatus is equipped with a 10 lb. linear motor, two microprobes and a CCD camera for observation. Capabilities: Capable of removing PMMA bonded sheets from Si Fine probing of microstructures Back to Equipment

  16. Analytic solutions of an unclassified artifact /

    SciTech Connect (OSTI)

    Trent, Bruce C.

    2012-03-01

    This report provides the technical detail for analytic solutions for the inner and outer profiles of the unclassified CMM Test Artifact (LANL Part Number 157Y-700373, 5/03/2001) in terms of radius and polar angle. Furthermore, analytic solutions are derived for the legacy Sheffield measurement hardware, also in terms of radius and polar angle, using part coordinates, i.e., relative to the analytic profile solutions obtained. The purpose of this work is to determine the exact solution for the “cosine correction” term inherent to measurement with the Sheffield hardware. The cosine correction is required in order to interpret the actual measurements taken by the hardware in terms of an actual part definition, or “knot-point spline definition,” that typically accompanies a component drawing. Specifically, there are two portions of the problem: first an analytic solution must be obtained for any point on the part, e.g., given the radii and the straight lines that define the part, it is required to find an exact solution for the inner and outer profile for any arbitrary polar angle. Next, the problem of the inspection of this part must be solved, i.e., given an arbitrary sphere (representing the inspection hardware) that comes in contact with the part (inner and outer profiles) at any arbitrary polar angle, it is required to determine the exact location of that intersection. This is trivial for the case of concentric circles. In the present case, however, the spherical portion of the profiles is offset from the defined center of the part, making the analysis nontrivial. Here, a simultaneous solution of the part profiles and the sphere was obtained.

  17. Summative Mass Analysis of Algal Biomass - Integration of Analytical Procedures: Laboratory Analytical Procedure (LAP)

    SciTech Connect (OSTI)

    Laurens, L. M. L.

    2013-12-01

    This procedure guides the integration of laboratory analytical procedures to measure algal biomass constituents in an unambiguous manner and ultimately achieve mass balance closure for algal biomass samples. Many of these methods build on years of research in algal biomass analysis.

  18. NATIONAL LEAD COMPANY OF OHIO HEALTH AND SAFETY DIVISION - ANALYTICAL...

    Office of Legacy Management (LM)

    AND RADIATION DEPT. ANALYTICAL CHEMISTRY SECT10 AMPLE NOS.: - ROUTE TO1 7 c, U NO:, Oil Bo Cl Beta METHOD OC ANALYSIS: Ro rfae*3 r4tSAAQ. 5 PH DYI Th TSS COVNTINO DATA1 -BKGD ...

  19. Insulator-based DEP with impedance measurements for analyte detection

    DOE Patents [OSTI]

    Davalos, Rafael V.; Simmons, Blake A.; Crocker, Robert W.; Cummings, Eric B.

    2010-03-16

    Disclosed herein are microfluidic devices for assaying at least one analyte specie in a sample comprising at least one analyte concentration area in a microchannel having insulating structures on or in at least one wall of the microchannel which provide a nonuniform electric field in the presence of an electric field provided by off-chip electrodes; and a pair of passivated sensing electrodes for impedance detection in a detection area. Also disclosed are assay methods and methods of making.

  20. Analytical Tools | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Information Resources » Analytical Tools Analytical Tools The Bioenergy Technologies Office and its national lab partners provide a variety of online tools to help analyze data and facilitate decision making. This page links to several of them and includes a widget that calculates the potential volume of ethanol produced from biomass feedstocks. Knowledge Discovery Framework (KDF): The Bioenergy Knowledge Discovery Framework (KDF) facilitates informed decision making by providing a means to

  1. An atomic orbital-based formulation of analytical gradients and nonadiabatic coupling vector elements for the state-averaged complete active space self-consistent field method on graphical processing units

    SciTech Connect (OSTI)

    Snyder, James W.; Hohenstein, Edward G.; Luehr, Nathan; Martínez, Todd J.

    2015-10-21

    We recently presented an algorithm for state-averaged complete active space self-consistent field (SA-CASSCF) orbital optimization that capitalizes on sparsity in the atomic orbital basis set to reduce the scaling of computational effort with respect to molecular size. Here, we extend those algorithms to calculate the analytic gradient and nonadiabatic coupling vectors for SA-CASSCF. Combining the low computational scaling with acceleration from graphical processing units allows us to perform SA-CASSCF geometry optimizations for molecules with more than 1000 atoms. The new approach will make minimal energy conical intersection searches and nonadiabatic dynamics routine for molecular systems with O(10{sup 2}) atoms.

  2. Plains and Eastern Clean Line Transmission Line: Comment from...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Plains and Eastern Clean Line Transmission Line: Comment from Mr. Dyer Plains and Eastern Clean Line Transmission Line: Comment from Sheila Beck Plains and Eastern Clean Line ...

  3. Plains and Eastern Clean Line Transmission Line: Comment from...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Plains and Eastern Clean Line Transmission Line: Comment from Change.org Plains and Eastern Clean Line Transmission Line: Comment from Mr. Leftwich Plains and Eastern Clean Line ...

  4. Electrospray ion source with reduced analyte electrochemistry

    DOE Patents [OSTI]

    Kertesz, Vilmos; Van Berkel, Gary J

    2013-07-30

    An electrospray ion (ESI) source and method capable of ionizing an analyte molecule without oxidizing or reducing the analyte of interest. The ESI source can include an emitter having a liquid conduit, a working electrode having a liquid contacting surface, a spray tip, a secondary working electrode, and a charge storage coating covering partially or fully the liquid contacting surface of the working electrode. The liquid conduit, the working electrode and the secondary working electrode can be in liquid communication. The electrospray ion source can also include a counter electrode proximate to, but separated from, said spray tip. The electrospray ion source can also include a power system for applying a voltage difference between the working electrodes and a counter-electrode. The power system can deliver pulsed voltage changes to the working electrodes during operation of said electrospray ion source to minimize the surface potential of the charge storage coating.

  5. Electrospray ion source with reduced analyte electrochemistry

    DOE Patents [OSTI]

    Kertesz, Vilmos [Knoxville, TN; Van Berkel, Gary [Clinton, TN

    2011-08-23

    An electrospray ion (ESI) source and method capable of ionizing an analyte molecule without oxidizing or reducing the analyte of interest. The ESI source can include an emitter having a liquid conduit, a working electrode having a liquid contacting surface, a spray tip, a secondary working electrode, and a charge storage coating covering partially or fully the liquid contacting surface of the working electrode. The liquid conduit, the working electrode and the secondary working electrode can be in liquid communication. The electrospray ion source can also include a counter electrode proximate to, but separated from, said spray tip. The electrospray ion source can also include a power system for applying a voltage difference between the working electrodes and a counter-electrode. The power system can deliver pulsed voltage changes to the working electrodes during operation of said electrospray ion source to minimize the surface potential of the charge storage coating.

  6. Superhydrophobic analyte concentration utilizing colloid-pillar...

    Office of Scientific and Technical Information (OSTI)

    Superhydrophobic analyte concentration utilizing colloid-pillar array SERS substrates Citation Details In-Document Search Title: Superhydrophobic analyte concentration utilizing ...

  7. Analytical Chemistry Laboratory | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Chemistry Laboratory provides a broad range of analytical chemistry support services to the scientific and engineering programs. AnalyticalChemistryLaboratoryfactsheet...

  8. Savannah River Analytical Laboratories Achieve International...

    National Nuclear Security Administration (NNSA)

    Savannah River Analytical Laboratories Achieve International Standard Accreditation Tuesday, September 8, 2015 - 12:55pm Savannah River National Laboratory's FH Analytical ...

  9. Pulse shaping with transmission lines

    DOE Patents [OSTI]

    Wilcox, Russell B.

    1987-01-01

    A method and apparatus for forming shaped voltage pulses uses passive reflection from a transmission line with nonuniform impedance. The impedance of the reflecting line varies with length in accordance with the desired pulse shape. A high voltage input pulse is transmitted to the reflecting line. A reflected pulse is produced having the desired shape and is transmitted by pulse removal means to a load. Light activated photoconductive switches made of silicon can be utilized. The pulse shaper can be used to drive a Pockels cell to produce shaped optical pulses.

  10. Pulse shaping with transmission lines

    DOE Patents [OSTI]

    Wilcox, R.B.

    1985-08-15

    A method and apparatus for forming shaped voltage pulses uses passive reflection from a transmission line with nonuniform impedance. The impedance of the reflecting line varies with length in accordance with the desired pulse shape. A high voltage input pulse is transmitted to the reflecting line. A reflected pulse is produced having the desired shape and is transmitted by pulse removal means to a load. Light activated photoconductive switches made of silicon can be utilized. The pulse shaper can be used to drive a Pockels cell to produce shaped optical pulses.

  11. Portable apparatus for separating sample and detecting target analytes

    DOE Patents [OSTI]

    Renzi, Ronald F.; Wally, Karl; Crocker, Robert W.; Stamps, James F.; Griffiths; Stewart K. ,; Fruetel, Julia A.; Horn, Brent A.; Shokair, Isaac R.; Yee, Daniel D.; VanderNoot, Victoria A.; Wiedenman, Boyd J.; West, Jason A. A.; Ferko, Scott M.

    2008-11-18

    Portable devices and methods for determining the presence of a target analyte using a portable device are provided. The portable device is preferably hand-held. A sample is injected to the portable device. A microfluidic separation is performed within the portable device and at least one separated component detected by a detection module within the portable device, in embodiments of the invention. A target analyte is identified, based on the separated component, and the presence of the target analyte is indicated on an output interface of the portable device, in accordance with embodiments of the invention.

  12. Trace detection of analytes using portable raman systems

    SciTech Connect (OSTI)

    Alam, M. Kathleen; Hotchkiss, Peter J.; Martin, Laura E.; Jones, David Alexander

    2015-11-24

    Apparatuses and methods for in situ detection of a trace amount of an analyte are disclosed herein. In a general embodiment, the present disclosure provides a surface-enhanced Raman spectroscopy (SERS) insert including a passageway therethrough, where the passageway has a SERS surface positioned therein. The SERS surface is configured to adsorb molecules of an analyte of interest. A concentrated sample is caused to flow over the SERS surface. The SERS insert is then provided to a portable Raman spectroscopy system, where it is analyzed for the analyte of interest.

  13. Anonymous Help Line

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Anonymous Help Line Ombuds Anonymous Help Line Committed to the fair and equitable treatment of all employees, contractors, and persons doing business with the Laboratory. Contact...

  14. Line Equipment Operator

    Broader source: Energy.gov [DOE]

    There are several Line Equipment Operator positions located in Washington and Oregon. A successful candidate in this position will perform Line Equipment Operator work operating trucks and all...

  15. A semi-experimental nodal synthesis method for the on-line reconstruction of three-dimensional neutron flux-shapes and reactivity

    SciTech Connect (OSTI)

    Jacqmin, R.P.

    1991-12-10

    The safety and optimal performance of large, commercial, light-water reactors require the knowledge at all time of the neutron-flux distribution in the core. In principle, this information can be obtained by solving the time-dependent neutron diffusion equations. However, this approach is complicated and very expensive. Sufficiently accurate, real-time calculations (time scale of approximately one second) are not yet possible on desktop computers, even with fast-running, nodal kinetics codes. A semi-experimental, nodal synthesis method which avoids the solution of the time-dependent, neutron diffusion equations is described. The essential idea of this method is to approximate instantaneous nodal group-fluxes by a linear combination of K, precomputed, three-dimensional, static expansion-functions. The time-dependent coefficients of the combination are found from the requirement that the reconstructed flux-distribution agree in a least-squares sense with the readings of J ({ge}K) fixed, prompt-responding neutron-detectors. Possible numerical difficulties with the least-squares solution of the ill-conditioned, J-by-K system of equations are brought under complete control by the use of a singular-value-decomposition technique. This procedure amounts to the rearrangement of the original, linear combination of K expansion functions into an equivalent more convenient, linear combination of R ({le}K) orthogonalized modes'' of decreasing magnitude. Exceedingly small modes are zeroed to eliminate any risk of roundoff-error amplification, and to assure consistency with the limited accuracy of the data. Additional modes are zeroed when it is desirable to limit the sensitivity of the results to measurement noise.

  16. A semi-experimental nodal synthesis method for the on-line reconstruction of three-dimensional neutron flux-shapes and reactivity. Final report

    SciTech Connect (OSTI)

    Jacqmin, R.P.

    1991-12-10

    The safety and optimal performance of large, commercial, light-water reactors require the knowledge at all time of the neutron-flux distribution in the core. In principle, this information can be obtained by solving the time-dependent neutron diffusion equations. However, this approach is complicated and very expensive. Sufficiently accurate, real-time calculations (time scale of approximately one second) are not yet possible on desktop computers, even with fast-running, nodal kinetics codes. A semi-experimental, nodal synthesis method which avoids the solution of the time-dependent, neutron diffusion equations is described. The essential idea of this method is to approximate instantaneous nodal group-fluxes by a linear combination of K, precomputed, three-dimensional, static expansion-functions. The time-dependent coefficients of the combination are found from the requirement that the reconstructed flux-distribution agree in a least-squares sense with the readings of J ({ge}K) fixed, prompt-responding neutron-detectors. Possible numerical difficulties with the least-squares solution of the ill-conditioned, J-by-K system of equations are brought under complete control by the use of a singular-value-decomposition technique. This procedure amounts to the rearrangement of the original, linear combination of K expansion functions into an equivalent more convenient, linear combination of R ({le}K) orthogonalized ``modes`` of decreasing magnitude. Exceedingly small modes are zeroed to eliminate any risk of roundoff-error amplification, and to assure consistency with the limited accuracy of the data. Additional modes are zeroed when it is desirable to limit the sensitivity of the results to measurement noise.

  17. Reports of the AAAI 2009 Spring Symposia: Technosocial Predictive Analytics.

    SciTech Connect (OSTI)

    Sanfilippo, Antonio P.

    2009-10-01

    The Technosocial Predictive Analytics AAAI symposium was held at Stanford University, Stanford, CA, March 23-25, 2009. The goal of this symposium was to explore new methods for anticipatory analytical thinking that provide decision advantage through the integration of human and physical models. Special attention was also placed on how to leverage supporting disciplines to (a) facilitate the achievement of knowledge inputs, (b) improve the user experience, and (c) foster social intelligence through collaborative/competitive work.

  18. Ultrasonic analyte concentration and application in flow cytometry

    DOE Patents [OSTI]

    Kaduchak, Gregory; Goddard, Greg; Salzman, Gary; Sinha, Dipen; Martin, John C.; Kwiatkowski, Christopher; Graves, Steven

    2015-07-07

    The present invention includes an apparatus and corresponding method for concentrating analytes within a fluid flowing through a tube using acoustic radiation pressure. The apparatus includes a function generator that outputs a radio frequency electrical signal to a transducer that transforms the radio frequency electric signal to an acoustic signal and couples the acoustic signal to the tube. The acoustic signal is converted within the tube to acoustic pressure that concentrates the analytes within the fluid.

  19. Ultrasonic analyte concentration and application in flow cytometry

    DOE Patents [OSTI]

    Kaduchak, Gregory; Goddard, Greg; Salzman, Gary; Sinha, Dipen; Martin, John C.; Kwiatkowski, Christopher; Graves, Steven

    2014-07-22

    The present invention includes an apparatus and corresponding method for concentrating analytes within a fluid flowing through a tube using acoustic radiation pressure. The apparatus includes a function generator that outputs a radio frequency electrical signal to a transducer that transforms the radio frequency electric signal to an acoustic signal and couples the acoustic signal to the tube. The acoustic signal is converted within the tube to acoustic pressure that concentrates the analytes within the fluid.

  20. Ultrasonic analyte concentration and application in flow cytometry

    DOE Patents [OSTI]

    Kaduchak, Gregory; Goddard, Greg; Salzman, Gary; Sinha, Dipen; Martin, John C.; Kwiatkowski, Christopher; Graves, Steven

    2008-03-11

    The present invention includes an apparatus and corresponding method for concentrating analytes within a fluid flowing through a tube using acoustic radiation pressure. The apparatus includes a function generator that outputs a radio frequency electrical signal to a transducer that transforms the radio frequency electric signal to an acoustic signal and couples the acoustic signal to the tube. The acoustic signal is converted within the tube to acoustic pressure that concentrates the analytes within the fluid.

  1. Analytical Spectroscopy - Energy Innovation Portal

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Industrial Technologies Industrial Technologies Find More Like This Return to Search Analytical Spectroscopy Idaho National Laboratory Contact INL About This Technology Technology Marketing Summary The use of lasers has become increasingly widespread, especially for manufacturing products and material analysis. Recently, laser desorption (LD) techniques for mass spectrometry have attracted attention because it produces intact molecular ions, avoids surface charging issues, and allows tuning of

  2. Method and means for dynamic measurement of rates of adsorption from solutions

    DOE Patents [OSTI]

    Slomka, B.J.; Buttermore, W.H.

    1992-05-05

    A method and apparatus are described for the dynamic measurement of rates of absorption from solutions. The method has the advantage of avoiding the use of solvent normally used to establish a baseline. The method involves pre-evacuating the adsorbent contained in an adsorbent cell and thereafter rapidly contacting the adsorbent with analytical solution, all without prior exposure of adsorbent to pure solvent. The result is a sharp characteristic adsorption line. 5 figs.

  3. Method and means for dynamic measurement of rates of adsorption from solutions

    DOE Patents [OSTI]

    Slomka, Bogdan J.; Buttermore, William H.

    1992-05-05

    A method and apparatus for dynamic measurement of rates of absorption from solutions. The method has the advantage of avoiding the use of solvent normally used to establish a baseline. The method involves pre-evacuating the adsorbent contained in an adsorbent cell and thereafter rapidly contacting the adsorbent with analytical solution, all without prior exposure of adsorbent to pure solvent. The result is a sharp characteristic adsorption line.

  4. TH-C-BRD-01: Analytical Computation of Prompt Gamma Ray Emission and Detection for Proton Range Verification

    SciTech Connect (OSTI)

    Sterpin, E; Vynckier, S; Janssens, G; Smeets, J; Prieels, D

    2014-06-15

    Purpose: A prompt gamma (PG) slit camera prototype demonstrated that on-line range monitoring within 12 mm could be performed by comparing expected and measured PG detection profiles. Monte Carlo (MC) can simulate the expected PG profile but this would result in prohibitive computation time for a complete pencil beam treatment plan. We implemented a much faster method that is based on analytical processing of pre-computed MC data. Methods: The formation of the PG detection signal can be separated into: 1) production of PGs and 2) detection by the camera detectors after PG transport in geometry. For proton energies from 40 to 230 MeV, PG productions in depth were pre-computed by MC (PENH) for 12C, 14N, 16O, 31P and 40Ca. The PG production was then modeled analytically by adding the PG production for each element according to local proton energy and tissue composition.PG transport in the patient/camera geometries and the detector response were modeled by convolving the PG production profile with a transfer function. The latter is interpolated from a database of transfer functions fitted to pre-computed MC data (PENELOPE). The database was generated for a photon source in a cylindrical phantom with various radiuses and a camera placed at various positions.As a benchmark, the analytical model was compared to PENH for a water phantom, a phantom with different slabs (adipose, muscle, lung) and a thoracic CT. Results: Good agreement (within 5%) was observed between the analytical model and PENH for the PG production. Similar accuracy for detecting range shifts was also observed. Speed of around 250 ms per profile was achieved (single CPU) using a non-optimized MatLab implementation. Conclusion: We devised a fast analytical model for generating PG detection profiles. In the test cases considered in this study, similar accuracy than MC was achieved for detecting range shifts. This research is supported by IBA.

  5. Analytical solutions to matrix diffusion problems

    SciTech Connect (OSTI)

    Keklinen, Pekka

    2014-10-06

    We report an analytical method to solve in a few cases of practical interest the equations which have traditionally been proposed for the matrix diffusion problem. In matrix diffusion, elements dissolved in ground water can penetrate the porous rock surronuding the advective flow paths. In the context of radioactive waste repositories this phenomenon provides a mechanism by which the area of rock surface in contact with advecting elements is greatly enhanced, and can thus be an important delay mechanism. The cases solved are relevant for laboratory as well for in situ experiments. Solutions are given as integral representations well suited for easy numerical solution.

  6. Plains and Eastern Clean Line Transmission Line: Comment from...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Clean Line: Arkansas and Oklahoma Plains and Eastern Clean Line Transmission Line: Comment from Block Plains and Eastern Clean Line: Arkansas and Oklahoma Comment submitted on ...

  7. Plains and Eastern Clean Line Transmission Line: Comment from...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Comment from Mr. Garrett Plains and Eastern Clean Line Transmission Line: Comment from Ms. Rutherford Plains and Eastern Clean Line Transmission Line: Comment from Ms. Campbell

  8. Plains and Eastern Clean Line Transmission Line: Comment from...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Comment from Downwind, LLC Plains and Eastern Clean Line Transmission Line: Comment from Sheila Beck Plains and Eastern Clean Line Transmission Line: Comment from Crystal Yarbrough

  9. Plains and Eastern Clean Line Transmission Line: Comment from...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Plains and Eastern Clean Line Transmission Line: Comment from Fallon Sanford Plains and Eastern Clean Line Transmission Line: Comment from Mr. Leftwich Plains and Eastern Clean ...

  10. Plains and Eastern Clean Line Transmission Line: Federal Register...

    Office of Environmental Management (EM)

    Plains and Eastern Clean Line Transmission Line: Federal Register Notice, Volume 80, No. 81 - April 28, 2015 Plains and Eastern Clean Line Transmission Line: Federal Register ...

  11. Nuclear Energy Research Initiative Project No. 02 103 Innovative Low Cost Approaches to Automating QA/QC of Fuel Particle Production Using On Line Nondestructive Methods for Higher Reliability Final Project Report

    SciTech Connect (OSTI)

    Ahmed, Salahuddin; Batishko, Charles R.; Flake, Matthew; Good, Morris S.; Mathews, Royce; Morra, Marino; Panetta, Paul D.; Pardini, Allan F.; Sandness, Gerald A.; Tucker, Brian J.; Weier, Dennis R.; Hockey, Ronald L.; Gray, Joseph N.; Saurwein, John J.; Bond, Leonard J.; Lowden, Richard A.; Miller, James H.

    2006-02-28

    This Nuclear Energy Research Initiative (NERI) project was tasked with exploring, adapting, developing and demonstrating innovative nondestructive test methods to automate nuclear coated particle fuel inspection so as to provide the United States (US) with necessary improved and economical Quality Assurance and Control (QA/QC) that is needed for the fuels for several reactor concepts being proposed for both near term deployment [DOE NE & NERAC, 2001] and Generation IV nuclear systems. Replacing present day QA/QC methods, done manually and in many cases destructively, with higher speed automated nondestructive methods will make fuel production for advanced reactors economically feasible. For successful deployment of next generation reactors that employ particle fuels, or fuels in the form of pebbles based on particles, extremely large numbers of fuel particles will require inspection at throughput rates that do not significantly impact the proposed manufacturing processes. The focus of the project is nondestructive examination (NDE) technologies that can be automated for production speeds and make either: (I) On Process Measurements or (II) In Line Measurements. The inspection technologies selected will enable particle quality qualification as a particle or group of particles passes a sensor. A multiple attribute dependent signature will be measured and used for qualification or process control decisions. A primary task for achieving this objective is to establish standard signatures for both good/acceptable particles and the most problematic types of defects using several nondestructive methods.

  12. SociAL Sensor Analytics: Measuring Phenomenology at Scale

    SciTech Connect (OSTI)

    Corley, Courtney D.; Dowling, Chase P.; Rose, Stuart J.; McKenzie, Taylor K.

    2013-06-04

    The objective of this paper is to present a system for interrogating immense social media streams through analytical methodologies that characterize topics and events critical to tactical and strategic planning. First, we propose a conceptual framework for interpreting social media as a sensor network. Time-series models and topic clustering algorithms are used to implement this concept into a functioning analytical system. Next, we address two scientific challenges: 1) to understand, quantify, and baseline phenomenology of social media at scale, and 2) to develop analytical methodologies to detect and investigate events of interest. This paper then documents computational methods and reports experimental findings that address these challenges. Ultimately, the ability to process billions of social media posts per week over a period of years enables the identification of patterns and predictors of tactical and strategic concerns at an unprecedented rate through SociAL Sensor Analytics (SALSA).

  13. Analyte detection using an active assay

    DOE Patents [OSTI]

    Morozov, Victor; Bailey, Charles L.; Evanskey, Melissa R.

    2010-11-02

    Analytes using an active assay may be detected by introducing an analyte solution containing a plurality of analytes to a lacquered membrane. The lacquered membrane may be a membrane having at least one surface treated with a layer of polymers. The lacquered membrane may be semi-permeable to nonanalytes. The layer of polymers may include cross-linked polymers. A plurality of probe molecules may be arrayed and immobilized on the lacquered membrane. An external force may be applied to the analyte solution to move the analytes towards the lacquered membrane. Movement may cause some or all of the analytes to bind to the lacquered membrane. In cases where probe molecules are presented, some or all of the analytes may bind to probe molecules. The direction of the external force may be reversed to remove unbound or weakly bound analytes. Bound analytes may be detected using known detection types.

  14. Methods Research

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Research Methods Research Methods being developed by MANTISSA Researchers Celeste: Bayesian modeling for astronomical images Randomized Linear Algebra for BioImaging Large-Scale PCA for Climate Efficient Graph Analytics for Genomics Unsupervised Learning for Neuroscience Deep Learning for Object Recognition Deep Learning for Daya Bay Unsupervised Learning in Neuroscience Last edited: 2016-07-18 16:52:3

  15. Nuclear reactor overflow line

    DOE Patents [OSTI]

    Severson, Wayne J.

    1976-01-01

    The overflow line for the reactor vessel of a liquid-metal-cooled nuclear reactor includes means for establishing and maintaining a continuous bleed flow of coolant amounting to 5 to 10% of the total coolant flow through the overflow line to prevent thermal shock to the overflow line when the reactor is restarted following a trip. Preferably a tube is disposed concentrically just inside the overflow line extending from a point just inside the reactor vessel to an overflow tank and a suction line is provided opening into the body of liquid metal in the reactor vessel and into the annulus between the overflow line and the inner tube.

  16. A new approach to analytic, non-perturbative and gauge-invariant QCD

    SciTech Connect (OSTI)

    Fried, H.M.; Grandou, T.; Sheu, Y.-M.

    2012-11-15

    Following a previous calculation of quark scattering in eikonal approximation, this paper presents a new, analytic and rigorous approach to the calculation of QCD phenomena. In this formulation a basic distinction between the conventional 'idealistic' description of QCD and a more 'realistic' description is brought into focus by a non-perturbative, gauge-invariant evaluation of the Schwinger solution for the QCD generating functional in terms of the exact Fradkin representations of Green's functional G{sub c}(x,y|A) and the vacuum functional L[A]. Because quarks exist asymptotically only in bound states, their transverse coordinates can never be measured with arbitrary precision; the non-perturbative neglect of this statement leads to obstructions that are easily corrected by invoking in the basic Lagrangian a probability amplitude which describes such transverse imprecision. The second result of this non-perturbative analysis is the appearance of a new and simplifying output called 'Effective Locality', in which the interactions between quarks by the exchange of a 'gluon bundle'-which 'bundle' contains an infinite number of gluons, including cubic and quartic gluon interactions-display an exact locality property that reduces the several functional integrals of the formulation down to a set of ordinary integrals. It should be emphasized that 'non-perturbative' here refers to the effective summation of all gluons between a pair of quark lines-which may be the same quark line, as in a self-energy graph-but does not (yet) include a summation over all closed-quark loops which are tied by gluon-bundle exchange to the rest of the 'Bundle Diagram'. As an example of the power of these methods we offer as a first analytic calculation the quark-antiquark binding potential of a pion, and the corresponding three-quark binding potential of a nucleon, obtained in a simple way from relevant eikonal scattering approximations. A second calculation, analytic, non-perturbative and

  17. Advanced Analytics | GE Global Research

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    GE Predictivity(tm) Industrial Internet Solutions Click to email this to a friend (Opens in new window) Share on Facebook (Opens in new window) Click to share (Opens in new window) Click to share on LinkedIn (Opens in new window) Click to share on Tumblr (Opens in new window) GE Predictivity(tm) Industrial Internet Solutions As a key player in GE's commitment to advance the Industrial Internet, the GE Software Center is at work helping industrial organizations use data, analytics, data

  18. Data Intensive Architecture for Scalable Cyber Analytics

    SciTech Connect (OSTI)

    Olsen, Bryan K.; Johnson, John R.; Critchlow, Terence J.

    2011-12-19

    Cyber analysts are tasked with the identification and mitigation of network exploits and threats. These compromises are difficult to identify due to the characteristics of cyber communication, the volume of traffic, and the duration of possible attack. In this paper, we describe a prototype implementation designed to provide cyber analysts an environment where they can interactively explore a months worth of cyber security data. This prototype utilized On-Line Analytical Processing (OLAP) techniques to present a data cube to the analysts. The cube provides a summary of the data, allowing trends to be easily identified as well as the ability to easily pull up the original records comprising an event of interest. The cube was built using SQL Server Analysis Services (SSAS), with the interface to the cube provided by Tableau. This software infrastructure was supported by a novel hardware architecture comprising a Netezza TwinFin for the underlying data warehouse and a cube server with a FusionIO drive hosting the data cube. We evaluated this environment on a months worth of artificial, but realistic, data using multiple queries provided by our cyber analysts. As our results indicate, OLAP technology has progressed to the point where it is in a unique position to provide novel insights to cyber analysts, as long as it is supported by an appropriate data intensive architecture.

  19. Analytical Chemistry Laboratory. Progress report for FY 1996

    SciTech Connect (OSTI)

    Green, D.W.; Boparai, A.S.; Bowers, D.L.

    1996-12-01

    The purpose of this report is to summarize the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year (FY) 1996. This annual report is the thirteenth for the ACL. It describes effort on continuing and new projects and contributions of the ACL staff to various programs at ANL. The ACL operates in the ANL system as a full-cost-recovery service center, but has a mission that includes a complementary research and development component: The Analytical Chemistry Laboratory will provide high-quality, cost-effective chemical analysis and related technical support to solve research problems of our clients -- Argonne National Laboratory, the Department of Energy, and others -- and will conduct world-class research and development in analytical chemistry and its applications. Because of the diversity of research and development work at ANL, the ACL handles a wide range of analytical chemistry problems. Some routine or standard analyses are done, but the ACL usually works with commercial laboratories if our clients require high-volume, production-type analyses. It is common for ANL programs to generate unique problems that require significant development of methods and adaption of techniques to obtain useful analytical data. Thus, much of the support work done by the ACL is very similar to our applied analytical chemistry research.

  20. NREL: Measurements and Characterization - Analytical Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Analytical Microscopy Analytical microscopy uses various high-resolution techniques to obtain information about materials on the atomic scale. It is one of the most powerful tools available for understanding a material's basic structure, chemistry, and morphology. We use two complementary types of analytical microscopy - electron microscopy and scanning probe microscopy - together with a variety of state-of-the-art imaging and analytical tools to capture data about photovoltaic (PV) materials

  1. Analytical Resources > Research > The Energy Materials Center...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Differential Electrochemical Mass Spectroscopy (DEMS) Electron Microscopy X-Ray Diffraction Analytical Resources Differential Electrochemical Mass Spectroscopy (DEMS) Electron...

  2. Analytic derivation of an approximate SU(3) symmetry inside the symmetry triangle of the interacting boson approximation model

    SciTech Connect (OSTI)

    Bonatsos, Dennis; Karampagia, S.; Casten, R. F.

    2011-05-15

    Using a contraction of the SU(3) algebra to the algebra of the rigid rotator in the large-boson-number limit of the interacting boson approximation (IBA) model, a line is found inside the symmetry triangle of the IBA, along which the SU(3) symmetry is preserved. The line extends from the SU(3) vertex to near the critical line of the first-order shape/phase transition separating the spherical and prolate deformed phases, and it lies within the Alhassid-Whelan arc of regularity, the unique valley of regularity connecting the SU(3) and U(5) vertices in the midst of chaotic regions. In addition to providing an explanation for the existence of the arc of regularity, the present line represents an example of an analytically determined approximate symmetry in the interior of the symmetry triangle of the IBA. The method is applicable to algebraic models possessing subalgebras amenable to contraction. This condition is equivalent to algebras in which the equilibrium ground state and its rotational band become energetically isolated from intrinsic excitations, as typified by deformed solutions to the IBA for large numbers of valence nucleons.

  3. Graph Analytics for Signature Discovery

    SciTech Connect (OSTI)

    Hogan, Emilie A.; Johnson, John R.; Halappanavar, Mahantesh; Lo, Chaomei

    2013-06-01

    Within large amounts of seemingly unstructured data it can be diffcult to find signatures of events. In our work we transform unstructured data into a graph representation. By doing this we expose underlying structure in the data and can take advantage of existing graph analytics capabilities, as well as develop new capabilities. Currently we focus on applications in cybersecurity and communication domains. Within cybersecurity we aim to find signatures for perpetrators using the pass-the-hash attack, and in communications we look for emails or phone calls going up or down a chain of command. In both of these areas, and in many others, the signature we look for is a path with certain temporal properties. In this paper we discuss our methodology for finding these temporal paths within large graphs.

  4. Multipass optical device and process for gas and analyte determination

    DOE Patents [OSTI]

    Bernacki, Bruce E.

    2011-01-25

    A torus multipass optical device and method are described that provide for trace level determination of gases and gas-phase analytes. The torus device includes an optical cavity defined by at least one ring mirror. The mirror delivers optical power in at least a radial and axial direction and propagates light in a multipass optical path of a predefined path length.

  5. Series Transmission Line Transformer

    DOE Patents [OSTI]

    Buckles, Robert A.; Booth, Rex; Yen, Boris T.

    2004-06-29

    A series transmission line transformer is set forth which includes two or more of impedance matched sets of at least two transmissions lines such as shielded cables, connected in parallel at one end ans series at the other in a cascading fashion. The cables are wound about a magnetic core. The series transmission line transformer (STLT) which can provide for higher impedance ratios and bandwidths, which is scalable, and which is of simpler design and construction.

  6. Simultaneous specimen and stage cleaning device for analytical electron microscope

    DOE Patents [OSTI]

    Zaluzec, Nestor J.

    1996-01-01

    An improved method and apparatus are provided for cleaning both a specimen stage, a specimen and an interior of an analytical electron microscope (AEM). The apparatus for cleaning a specimen stage and specimen comprising a plasma chamber for containing a gas plasma and an air lock coupled to the plasma chamber for permitting passage of the specimen stage and specimen into the plasma chamber and maintaining an airtight chamber. The specimen stage and specimen are subjected to a reactive plasma gas that is either DC or RF excited. The apparatus can be mounted on the analytical electron microscope (AEM) for cleaning the interior of the microscope.

  7. Analytical effective tensor for flow-through composites

    DOE Patents [OSTI]

    Sviercoski, Rosangela De Fatima

    2012-06-19

    A machine, method and computer-usable medium for modeling an average flow of a substance through a composite material. Such a modeling includes an analytical calculation of an effective tensor K.sup.a suitable for use with a variety of media. The analytical calculation corresponds to an approximation to the tensor K, and follows by first computing the diagonal values, and then identifying symmetries of the heterogeneity distribution. Additional calculations include determining the center of mass of the heterogeneous cell and its angle according to a defined Cartesian system, and utilizing this angle into a rotation formula to compute the off-diagonal values and determining its sign.

  8. Transmission Business Line

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Transmission Business Line Non-Federal Financing of Transmission Projects - March 2004 Critical paths on the Northwest transmission grid are congested and the system is near or at...

  9. Plains and Eastern Clean Line Transmission Line: Comment from Marshall

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Hughes | Department of Energy from Marshall Hughes Plains and Eastern Clean Line Transmission Line: Comment from Marshall Hughes Comment submitted on updated Part 2 application. Comment from Marshall Hughes 07-10-15.pdf (14.91 KB) More Documents & Publications Plains and Eastern Clean Line Transmission Line: Comment from Mr. Dyer Plains and Eastern Clean Line Transmission Line: Comment from Sheila Beck Plains and Eastern Clean Line Transmission Line: Comment from Patti McCutchen

  10. Analytical Chemistry Laboratory progress report for FY 1984

    SciTech Connect (OSTI)

    Green, D.W.; Heinrich, R.R.; Jensen, K.J.; Stetter, J.R.

    1985-03-01

    Technical and administrative activities of the Analytical Chemistry Laboratory (ACL) are reported for fiscal year 1984. The ACL is a full-cost-recovery service center, with the primary mission of providing a broad range of technical support services to the scientific and engineering programs at ANL. In addition, ACL conducts a research program in analytical chemistry, works on instrumental and methods development, and provides analytical services for governmental, educational, and industrial organizations. The ACL is administratively within the Chemical Technology Division, the principal user, but provides technical support for all of the technical divisions and programs at ANL. The ACL has three technical groups - Chemical Analysis, Instrumental Analysis, and Organic Analysis. Under technical activities 26 projects are briefly described. Under professional activities, a list is presented for publications and reports, oral presentations, awards and meetings attended. 6 figs., 2 tabs.

  11. Web-based Visual Analytics for Extreme Scale Climate Science

    SciTech Connect (OSTI)

    Steed, Chad A; Evans, Katherine J; Harney, John F; Jewell, Brian C; Shipman, Galen M; Smith, Brian E; Thornton, Peter E; Williams, Dean N.

    2014-01-01

    In this paper, we introduce a Web-based visual analytics framework for democratizing advanced visualization and analysis capabilities pertinent to large-scale earth system simulations. We address significant limitations of present climate data analysis tools such as tightly coupled dependencies, ineffi- cient data movements, complex user interfaces, and static visualizations. Our Web-based visual analytics framework removes critical barriers to the widespread accessibility and adoption of advanced scientific techniques. Using distributed connections to back-end diagnostics, we minimize data movements and leverage HPC platforms. We also mitigate system dependency issues by employing a RESTful interface. Our framework embraces the visual analytics paradigm via new visual navigation techniques for hierarchical parameter spaces, multi-scale representations, and interactive spatio-temporal data mining methods that retain details. Although generalizable to other science domains, the current work focuses on improving exploratory analysis of large-scale Community Land Model (CLM) and Community Atmosphere Model (CAM) simulations.

  12. SRC-I Demonstration Plant Analytical Laboratory. Final technical report

    SciTech Connect (OSTI)

    Hamilton, R.F.; Klusaritz, M.; Maroulis, P.J.; Moyer, J.D.; Parees, D.M.; Skinner, R.W.; Sydlik, E.; Tewari, K.C.; Tiedge, W.F.; Znaimer, S.

    1983-09-01

    This report describes planning and methods development activities to establish an SRC-I Coal Liquefaction Demonstration Plant analytical laboratory. Laboratory requirements are listed and methods qualification/development activities are described for the following areas: microanalytical carbon, hydrogen, chlorine, nitrogen, and sulfur procedures; ash determination; GC/MS and GC/FID analyses; metals analyses; and GC-simulated distillation. 2 references, 64 figures, 108 tables.

  13. Transmission Line Security Monitor

    SciTech Connect (OSTI)

    2011-01-01

    The Transmission Line Security Monitor is a multi-sensor monitor that mounts directly on high-voltage transmission lines to detect, characterize and communicate terrorist activity, human tampering and threatening conditions around support towers. For more information about INL's critical infrastructure protection research, visit http://www.facebook.com/idahonationallaboratory.

  14. Transmission Line Security Monitor

    ScienceCinema (OSTI)

    None

    2013-05-28

    The Transmission Line Security Monitor is a multi-sensor monitor that mounts directly on high-voltage transmission lines to detect, characterize and communicate terrorist activity, human tampering and threatening conditions around support towers. For more information about INL's critical infrastructure protection research, visit http://www.facebook.com/idahonationallaboratory.

  15. ANALYTICAL SOLUTIONS OF SINGULAR ISOTHERMAL QUADRUPOLE LENS

    SciTech Connect (OSTI)

    Chu Zhe; Lin, W. P.; Yang Xiaofeng E-mail: linwp@shao.ac.cn

    2013-06-20

    Using an analytical method, we study the singular isothermal quadrupole (SIQ) lens system, which is the simplest lens model that can produce four images. In this case, the radial mass distribution is in accord with the profile of the singular isothermal sphere lens, and the tangential distribution is given by adding a quadrupole on the monopole component. The basic properties of the SIQ lens have been studied in this Letter, including the deflection potential, deflection angle, magnification, critical curve, caustic, pseudo-caustic, and transition locus. Analytical solutions of the image positions and magnifications for the source on axes are derived. We find that naked cusps will appear when the relative intensity k of quadrupole to monopole is larger than 0.6. According to the magnification invariant theory of the SIQ lens, the sum of the signed magnifications of the four images should be equal to unity, as found by Dalal. However, if a source lies in the naked cusp, the summed magnification of the left three images is smaller than the invariant 1. With this simple lens system, we study the situations where a point source infinitely approaches a cusp or a fold. The sum of the magnifications of the cusp image triplet is usually not equal to 0, and it is usually positive for major cusps while negative for minor cusps. Similarly, the sum of magnifications of the fold image pair is usually not equal to 0 either. Nevertheless, the cusp and fold relations are still equal to 0 in that the sum values are divided by infinite absolute magnifications by definition.

  16. Contained radiological analytical chemistry module

    DOE Patents [OSTI]

    Barney, David M.

    1989-01-01

    A system which provides analytical determination of a plurality of water chemistry parameters with respect to water samples subject to radiological contamination. The system includes a water sample analyzer disposed within a containment and comprising a sampling section for providing predetermined volumes of samples for analysis; a flow control section for controlling the flow through the system; and a gas analysis section for analyzing samples provided by the sampling system. The sampling section includes a controllable multiple port valve for, in one position, metering out sample of a predetermined volume and for, in a second position, delivering the material sample for analysis. The flow control section includes a regulator valve for reducing the pressure in a portion of the system to provide a low pressure region, and measurement devices located in the low pressure region for measuring sample parameters such as pH and conductivity, at low pressure. The gas analysis section which is of independent utility provides for isolating a small water sample and extracting the dissolved gases therefrom into a small expansion volume wherein the gas pressure and thermoconductivity of the extracted gas are measured.

  17. Contained radiological analytical chemistry module

    DOE Patents [OSTI]

    Barney, David M.

    1990-01-01

    A system which provides analytical determination of a plurality of water chemistry parameters with respect to water samples subject to radiological contamination. The system includes a water sample analyzer disposed within a containment and comprising a sampling section for providing predetermined volumes of samples for analysis; a flow control section for controlling the flow through the system; and a gas analysis section for analyzing samples provided by the sampling system. The sampling section includes a controllable multiple port valve for, in one position, metering out sample of a predetermined volume and for, in a second position, delivering the material sample for analysis. The flow control section includes a regulator valve for reducing the pressure in a portion of the system to provide a low pressure region, and measurement devices located in the low pressure region for measuring sample parameters such as pH and conductivity, at low pressure. The gas analysis section which is of independent utility provides for isolating a small water sample and extracting the dissolved gases therefrom into a small expansion volume wherein the gas pressure and thermoconductivity of the extracted gas are measured.

  18. Working with SRNL - Our Facilities - Analytical Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    SRNL personell SRNL personell Working with SRNL Our Facilities - Analytical Laboratories The Savannah River National Laboratory's (SRNL) Analytical Laboratories have supported SRS operations for more than 55 years, providing high quality analytical, radiometric and environmental monitoring data to a range of customers. Since the mid-1950s, the labs have provided a diverse array of scientific and technical services in support of Site missions. The labs perform analyses on a wide range of

  19. Analytical admittance characterization of high mobility channel

    SciTech Connect (OSTI)

    Mammeri, A. M.; Mahi, F. Z.; Varani, L.

    2015-03-30

    In this contribution, we investigate the small-signal admittance of the high electron mobility transistors field-effect channels under a continuation branching of the current between channel and gate by using an analytical model. The analytical approach takes into account the linearization of the 2D Poisson equation and the drift current along the channel. The analytical equations discuss the frequency dependence of the admittance at source and drain terminals on the geometrical transistor parameters.

  20. Analytical instrument with apparatus and method for sample concentrating

    DOE Patents [OSTI]

    Zaromb, S.

    1986-08-04

    A system for analysis of trace concentrations of contaminants in air includes a portable liquid chromatograph and a preconcentrator for the contaminants to be analyzed. The preconcentrator includes a sample bag having an inlet valve and an outlet valve for collecting an air sample. When the sample is collected the sample bag is connected in series with a sorbing apparatus in a recirculation loop. The sorbing apparatus has an inner gas-permeable container containing a sorbent material and an outer gas-impermeable container. The sample is circulated through the outer container and around the inner container for trapping and preconcentrating the contaminants in the sorbent material. The sorbent material may be a liquid having the same composition as the mobile phase of the chromatograph for direct injection thereinto. Alternatively, the sorbent material may be a porous, solid body, to which mobile phase liquid is added after preconcentration of the contaminants for dissolving the contaminants, the liquid solution then being withdrawn for injection into the chromatograph.

  1. Hydrogen Fuel Quality - Focus: Analytical Methods Development & Hydrogen

    Broader source: Energy.gov (indexed) [DOE]

    Presentation for Dec. 17, 2008 hydrogen bimonthly informational call and meeting series for state and regional initiatives. nha_webinar_steve_medwin_pres.pdf (226.04 KB) More Documents & Publications Full Fuel-Cycle Comparison of Forklift Propulsion Systems An Evaluation of the Total Cost of Ownership of Fuel Cell-Powered Material Handling Equipment The Hydrogen Tax Incentive Act of 2008 Energy

    Access the recording and download the presentation slides from the Fuel Cell Technologies

  2. Early test facilities and analytic methods for radiation shielding: Proceedings

    SciTech Connect (OSTI)

    Ingersoll, D.T. ); Ingersoll, J.K. )

    1992-11-01

    This report represents a compilation of eight papers presented at the 1992 American Nuclear Society/European Nuclear Society International Meeting. The meeting is of special significance since it commemorates the fiftieth anniversary of the first controlled nuclear chain reaction. The papers contained in this report were presented in a special session organized by the Radiation Protection and Shielding Division in keeping with the historical theme of the meeting. The paper titles are good indicators of their content and are: (1) The origin of radiation shielding research: The Oak Ridge experience, (2) Shielding research at the hanford site, (3) Aircraft shielding experiments at General Dynamics Fort Worth, 1950-1962, (4) Where have the neutrons gone , a history of the tower shielding facility, (5) History and evolution of buildup factors, (6) Early shielding research at Bettis atomic power laboratory, (7) UK reactor shielding: then and now, (8) A very personal view of the development of radiation shielding theory.

  3. Early Test Facilities and Analytic Methods for Radiation Shielding

    SciTech Connect (OSTI)

    Ingersoll, D.T.

    1992-01-01

    This report represents a compilation of eight papers presented at the 1992 American Nuclear Society/European Nuclear Society International Meeting held in Chicago, Illinois on November 15 20,1992. The meeting is of special significance since it commemorates the 50th anniversary of the first controlled nuclear chain reaction, which occurred, not coincidentally, in Chicago. The papers contained in this report were presented in a special session organized by the Radiation Protection and Shielding Division in keeping with the historical theme of the meeting.

  4. SASSI Analytical Methods Compared with SHAKE Free-Field Results

    Office of Environmental Management (EM)

    4-18019 September, 2015 Conceptual Framework for Developing Resilience Metrics for the Electricity, Oil, and Gas Sectors in the United States Jean-Paul Watson, Ross Guttromson, Cesar Silva-Monroy, Robert Jeffers, Katherine Jones, James Ellison, Charles Rath, Jared Gearhart, Dean Jones, Tom Corbet, Charles Hanley, La Tonya Walker Prepared by Sandia National Laboratories Albuquerque, New Mexico 87185 and Livermore, California 94550 Sandia National Laboratories is a multi-program laboratory managed

  5. Analytical Approaches Towards Understanding Structure-Property...

    Office of Scientific and Technical Information (OSTI)

    Laboratory (LLNL), Livermore, CA Sponsoring Org: USDOE Country of Publication: United States Language: English Subject: 37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY

  6. Size separation of analytes using monomeric surfactants

    DOE Patents [OSTI]

    Yeung, Edward S.; Wei, Wei

    2005-04-12

    A sieving medium for use in the separation of analytes in a sample containing at least one such analyte comprises a monomeric non-ionic surfactant of the of the general formula, B-A, wherein A is a hydrophilic moiety and B is a hydrophobic moiety, present in a solvent at a concentration forming a self-assembled micelle configuration under selected conditions and having an aggregation number providing an equivalent weight capable of effecting the size separation of the sample solution so as to resolve a target analyte(s) in a solution containing the same, the size separation taking place in a chromatography or electrophoresis separation system.

  7. Photovoltaic Degradation Rates -- An Analytical Review: Preprint

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Photovoltaic Degradation Rates - An Analytical Review Dirk C. Jordan and Sarah R. Kurtz To ... Abstract As photovoltaic penetration of the power grid increases, accurate predictions of ...

  8. Analytic Power LLC | Open Energy Information

    Open Energy Info (EERE)

    Power LLC Place: Woburn, Massachusetts Zip: 01801 Region: Greater Boston Area Sector: Hydrogen Product: Fuel cell developer Website: www.analytic-power.com Coordinates:...

  9. Transesterification: Laboratory Analytical Procedure (LAP) Van...

    Office of Scientific and Technical Information (OSTI)

    Wychen, S.; Laurens, L. M. L. 09 BIOMASS FUELS; 59 BASIC BIOLOGICAL SCIENCES BIOMASS; ALGAE; LABORATORY ANALYTICAL PROCEDURES; LAPS; TOTAL LIPIDS; FATTY ACID METHYL ESTERS; FAME;...

  10. New User and Data Analytics Training

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    New User and Data Analytics Training New User and Data Analytics Training February 23, 2015 Monday, Feb. 23 - New User and Data Analytics Training NERSC (Berkeley Lab Building 943), 415 20th Street, Oakland, CA If you plan to attend, please register here. There is no registration fee, but your registration helps us plan the event. To attend remotely via WebEx, please see Remote Setup. Note that the morning session "New User Training" and the afternoon session "Data and Analytics

  11. Analytical theory of coherent synchrotron radiation wakefield...

    Office of Scientific and Technical Information (OSTI)

    Analytical theory of coherent synchrotron radiation wakefield of short bunches shielded by ... Word Cloud More Like This Full Text preview image File size NAView Full Text View Full ...

  12. Analytic Challenges to Valuing Energy Storage

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    analytical task. Market Conditions - Markets are continually evolving, and the long-term value of energy storage is difficult to capture. Niche markets have emerged, but...

  13. Investigation and Analytical Description of Acoustic Production...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Investigation and Analytical Description of Acoustic Production by Magneto-Acoustic Mixing Technology Citation Details In-Document Search This content will become...

  14. Nanomechanical Sensor Detects and Identifies Chemical Analytes...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Nanomechanical Sensor Detects and Identifies Chemical Analytes Oak Ridge National ... It can also quickly identify a potentially harmful chemical. The invention's sensitivity ...

  15. Smart Microfabricated Preconcentrator (and Other Micro Analytical...

    Office of Scientific and Technical Information (OSTI)

    Detection Components&Systems). Citation Details In-Document Search Title: Smart Microfabricated Preconcentrator (and Other Micro Analytical Detection Components&Systems). ...

  16. Computing Criticality of Lines in Power Systems

    SciTech Connect (OSTI)

    Pinar, Ali; Reichert, Adam; Lesieutre, Bernard

    2006-10-13

    We propose a computationally efficient method based onnonlinear optimization to identify critical lines, failure of which cancause severe blackouts. Our method computes criticality measure for alllines at a time, as opposed to detecting a single vulnerability,providing a global view of the system. This information on criticality oflines can be used to identify multiple contingencies by selectivelyexploring multiple combinations of broken lines. The effectiveness of ourmethod is demonstrated on the IEEE 30 and 118 bus systems, where we canvery quickly detect the most critical lines in the system and identifysevere multiple contingencies.

  17. Coiled transmission line pulse generators

    DOE Patents [OSTI]

    McDonald, Kenneth Fox

    2010-11-09

    Methods and apparatus are provided for fabricating and constructing solid dielectric "Coiled Transmission Line" pulse generators in radial or axial coiled geometries. The pour and cure fabrication process enables a wide variety of geometries and form factors. The volume between the conductors is filled with liquid blends of monomers, polymers, oligomers, and/or cross-linkers and dielectric powders; and then cured to form high field strength and high dielectric constant solid dielectric transmission lines that intrinsically produce ideal rectangular high voltage pulses when charged and switched into matched impedance loads. Voltage levels may be increased by Marx and/or Blumlein principles incorporating spark gap or, preferentially, solid state switches (such as optically triggered thyristors) which produce reliable, high repetition rate operation. Moreover, these Marxed pulse generators can be DC charged and do not require additional pulse forming circuitry, pulse forming lines, transformers, or an a high voltage spark gap output switch. The apparatus accommodates a wide range of voltages, impedances, pulse durations, pulse repetition rates, and duty cycles. The resulting mobile or flight platform friendly cylindrical geometric configuration is much more compact, light-weight, and robust than conventional linear geometries, or pulse generators constructed from conventional components. Installing additional circuitry may accommodate optional pulse shape improvements. The Coiled Transmission Lines can also be connected in parallel to decrease the impedance, or in series to increase the pulse length.

  18. Analytical solutions for radiation-driven winds in massive stars. I. The fast regime

    SciTech Connect (OSTI)

    Araya, I.; Cur, M.; Cidale, L. S.

    2014-11-01

    Accurate mass-loss rate estimates are crucial keys in the study of wind properties of massive stars and for testing different evolutionary scenarios. From a theoretical point of view, this implies solving a complex set of differential equations in which the radiation field and the hydrodynamics are strongly coupled. The use of an analytical expression to represent the radiation force and the solution of the equation of motion has many advantages over numerical integrations. Therefore, in this work, we present an analytical expression as a solution of the equation of motion for radiation-driven winds in terms of the force multiplier parameters. This analytical expression is obtained by employing the line acceleration expression given by Villata and the methodology proposed by Mller and Vink. On the other hand, we find useful relationships to determine the parameters for the line acceleration given by Mller and Vink in terms of the force multiplier parameters.

  19. Quality control and statistical process control for nuclear analytical measurements

    SciTech Connect (OSTI)

    Seymour, R.; Sergent, F.; Clark, W.H.C.; Gleason, G.

    1993-12-31

    The same driving forces that are making businesses examine quality control of manufacturing processes are making laboratories reevaluate their quality control programs. Increased regulation (accountability), global competitiveness (profitability), and potential for litigation (defensibility) are the principal driving forces behind the development and implementation of QA/QC programs in the nuclear analytical laboratory. Both manufacturing and scientific quality control can use identical statistical methods, albeit with some differences in the treatment of the measured data. Today, the approaches to QC programs are quite different for most analytical laboratories as compared with manufacturing sciences. This is unfortunate because the statistical process control methods are directly applicable to measurement processes. It is shown that statistical process control methods can provide many benefits for laboratory QC data treatment.

  20. Coherent soliton communication lines

    SciTech Connect (OSTI)

    Yushko, O. V. Redyuk, A. A.; Fedoruk, M. P.; Turitsyn, S. K.

    2014-11-15

    The data transmission in coherent fiber-optical communication lines using solitons with a variable phase is studied. It is shown that nonlinear coherent structures (solitons) can be applied for effective signal transmission over a long distance using amplitude and optical-phase keying of information. The optimum ratio of the pulse width to the bit slot at which the spectral efficiency (transmitted bits per second and hertz) is maximal is determined. It is shown that soliton fiber-optical communication lines can ensure data transmission at a higher spectral efficiency as compared to traditional communication lines and at a high signal-to-noise ratio.

  1. Quantifying construction and demolition waste: An analytical review

    SciTech Connect (OSTI)

    Wu, Zezhou; Yu, Ann T.W.; Shen, Liyin; Liu, Guiwen

    2014-09-15

    Highlights: • Prevailing C and D waste quantification methodologies are identified and compared. • One specific methodology cannot fulfill all waste quantification scenarios. • A relevance tree for appropriate quantification methodology selection is proposed. • More attentions should be paid to civil and infrastructural works. • Classified information is suggested for making an effective waste management plan. - Abstract: Quantifying construction and demolition (C and D) waste generation is regarded as a prerequisite for the implementation of successful waste management. In literature, various methods have been employed to quantify the C and D waste generation at both regional and project levels. However, an integrated review that systemically describes and analyses all the existing methods has yet to be conducted. To bridge this research gap, an analytical review is conducted. Fifty-seven papers are retrieved based on a set of rigorous procedures. The characteristics of the selected papers are classified according to the following criteria - waste generation activity, estimation level and quantification methodology. Six categories of existing C and D waste quantification methodologies are identified, including site visit method, waste generation rate method, lifetime analysis method, classification system accumulation method, variables modelling method and other particular methods. A critical comparison of the identified methods is given according to their characteristics and implementation constraints. Moreover, a decision tree is proposed for aiding the selection of the most appropriate quantification method in different scenarios. Based on the analytical review, limitations of previous studies and recommendations of potential future research directions are further suggested.

  2. Resonance ionization for analytical spectroscopy

    DOE Patents [OSTI]

    Hurst, George S.; Payne, Marvin G.; Wagner, Edward B.

    1976-01-01

    This invention relates to a method for the sensitive and selective analysis of an atomic or molecular component of a gas. According to this method, the desired neutral component is ionized by one or more resonance photon absorptions, and the resultant ions are measured in a sensitive counter. Numerous energy pathways are described for accomplishing the ionization including the use of one or two tunable pulsed dye lasers.

  3. ORISE: Radiochemistry and Environmental Analytical Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Radiochemistry and Environmental Analytical Laboratory ORISE techinican performs a radiochemical analysis To complement our environmental assessment and health physics capabilities, the Oak Ridge Institute for Science and Education (ORISE) maintains a radiochemistry and environmental analytical laboratory that facilitates the analysis of environmental samples and unique matrices. ORISE performs radiochemical analyses exclusively for the U.S. Nuclear Regulatory Commission (NRC), as well as

  4. Microfabricated field calibration assembly for analytical instruments

    DOE Patents [OSTI]

    Robinson, Alex L.; Manginell, Ronald P.; Moorman, Matthew W.; Rodacy, Philip J.; Simonson, Robert J.

    2011-03-29

    A microfabricated field calibration assembly for use in calibrating analytical instruments and sensor systems. The assembly comprises a circuit board comprising one or more resistively heatable microbridge elements, an interface device that enables addressable heating of the microbridge elements, and, in some embodiments, a means for positioning the circuit board within an inlet structure of an analytical instrument or sensor system.

  5. Lineman (Live Line)

    Broader source: Energy.gov [DOE]

    There are several Lineman (Liveline) positions located in Spokane, Washington. A successful candidate in this position will perform construction and maintenance work for live-line on wood and steel...

  6. Maersk Line Equipment guide

    National Nuclear Security Administration (NNSA)

    Maersk Line containers has an average age of less than six years and a stringent maintenance programme ensures they are always ready for service. Each container in our fleet...

  7. Power line detection system

    DOE Patents [OSTI]

    Latorre, Victor R.; Watwood, Donald B.

    1994-01-01

    A short-range, radio frequency (RF) transmitting-receiving system that provides both visual and audio warnings to the pilot of a helicopter or light aircraft of an up-coming power transmission line complex. Small, milliwatt-level narrowband transmitters, powered by the transmission line itself, are installed on top of selected transmission line support towers or within existing warning balls, and provide a continuous RF signal to approaching aircraft. The on-board receiver can be either a separate unit or a portion of the existing avionics, and can also share an existing antenna with another airborne system. Upon receipt of a warning signal, the receiver will trigger a visual and an audio alarm to alert the pilot to the potential power line hazard.

  8. Power line detection system

    DOE Patents [OSTI]

    Latorre, V.R.; Watwood, D.B.

    1994-09-27

    A short-range, radio frequency (RF) transmitting-receiving system that provides both visual and audio warnings to the pilot of a helicopter or light aircraft of an up-coming power transmission line complex. Small, milliwatt-level narrowband transmitters, powered by the transmission line itself, are installed on top of selected transmission line support towers or within existing warning balls, and provide a continuous RF signal to approaching aircraft. The on-board receiver can be either a separate unit or a portion of the existing avionics, and can also share an existing antenna with another airborne system. Upon receipt of a warning signal, the receiver will trigger a visual and an audio alarm to alert the pilot to the potential power line hazard. 4 figs.

  9. Line Extension Alternatives

    Broader source: Energy.gov [DOE]

    The Public Service Board (PSB) of Vermont developed rules regarding utility line extension requests. While the majority of the rules focus on the procedure followed (and associated fees) for the...

  10. Efficient Graph Analytics for Genomics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Design » Types of Homes » Efficient Earth-Sheltered Homes Efficient Earth-Sheltered Homes This house in Tempe, Arizona, uses earth-sheltered construction methods to help decrease cooling costs. | Photo by Pamm McFadden This house in Tempe, Arizona, uses earth-sheltered construction methods to help decrease cooling costs. | Photo by Pamm McFadden If you are looking for a home with energy-efficient features that will provide a comfortable, tranquil, weather-resistant dwelling, an earth-sheltered