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Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


1

UMTRA ground water sampling techniques: Comparison of the traditional and low flow methods  

SciTech Connect (OSTI)

This report describes the potential changes in water quality data that may occur with the conversion from MBV (multiple bore volume) to LF (low flow) sampling and provides two examples of how such a change might impact Project decisions. The existing scientific literature on LF sampling is reviewed and the new LF data from three UMTRA Uranium Mill Tailings Remedial Action Project sites are evaluated seeking answers to the questions posed above. Several possible approaches, that the UMTRA Project may take to address issues unanswered by the literature are presented and compared, and a recommendation is offered for the future direction of the LF conversion effort.

NONE

1995-07-01T23:59:59.000Z

2

Sampling system and method  

DOE Patents [OSTI]

The present disclosure provides an apparatus and method for coupling conduit segments together. A first pump obtains a sample and transmits it through a first conduit to a reservoir accessible by a second pump. The second pump further conducts the sample from the reservoir through a second conduit.

Decker, David L.; Lyles, Brad F.; Purcell, Richard G.; Hershey, Ronald Lee

2013-04-16T23:59:59.000Z

3

Sampling system and method  

DOE Patents [OSTI]

An apparatus and method for supporting a tubing bundle during installation or removal. The apparatus includes a clamp for securing the tubing bundle to an external wireline. The method includes deploying the tubing bundle and wireline together, The tubing bundle is periodically secured to the wireline using a clamp.

Decker, David L; Lyles, Brad F; Purcell, Richard G; Hershey, Ronald Lee

2014-05-20T23:59:59.000Z

4

Fluid sampling apparatus and method  

DOE Patents [OSTI]

Incorporation of a bellows in a sampling syringe eliminates ingress of contaminants, permits replication of amounts and compression of multiple sample injections, and enables remote sampling for off-site analysis. 3 figs.

Yeamans, D.R.

1998-02-03T23:59:59.000Z

5

Soil sampling kit and a method of sampling therewith  

DOE Patents [OSTI]

A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allow an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds.

Thompson, Cyril V. (Knoxville, TN)

1991-01-01T23:59:59.000Z

6

Soil sampling kit and a method of sampling therewith  

DOE Patents [OSTI]

A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allows an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds. 11 figures.

Thompson, C.V.

1991-02-05T23:59:59.000Z

7

Method and apparatus for data sampling  

DOE Patents [OSTI]

A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium.

Odell, Daniel M. C. (Aiken, SC)

1994-01-01T23:59:59.000Z

8

Method and apparatus for data sampling  

DOE Patents [OSTI]

A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples is described. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium. 6 figures.

Odell, D.M.C.

1994-04-19T23:59:59.000Z

9

ALARA ASSESSMENT OF SETTLER SLUDGE SAMPLING METHODS  

SciTech Connect (OSTI)

The purpose of this assessment is to compare underwater and above water settler sludge sampling methods to determine if the added cost for underwater sampling for the sole purpose of worker dose reductions is justified. Initial planning for sludge sampling included container, settler and knock-out-pot (KOP) sampling. Due to the significantly higher dose consequence of KOP sludge, a decision was made to sample KOP underwater to achieve worker dose reductions. Additionally, initial plans were to utilize the underwater sampling apparatus for settler sludge. Since there are no longer plans to sample KOP sludge, the decision for underwater sampling for settler sludge needs to be revisited. The present sampling plan calls for spending an estimated $2,500,000 to design and construct a new underwater sampling system (per A21 C-PL-001 RevOE). This evaluation will compare and contrast the present method of above water sampling to the underwater method that is planned by the Sludge Treatment Project (STP) and determine if settler samples can be taken using the existing sampling cart (with potentially minor modifications) while maintaining doses to workers As Low As Reasonably Achievable (ALARA) and eliminate the need for costly redesigns, testing and personnel retraining.

NELSEN LA

2009-01-30T23:59:59.000Z

10

Statistical sampling method for releasing decontaminated vehicles  

SciTech Connect (OSTI)

Earth moving vehicles (e.g., dump trucks, belly dumps) commonly haul radiologically contaminated materials from a site being remediated to a disposal site. Traditionally, each vehicle must be surveyed before being released. The logistical difficulties of implementing the traditional approach on a large scale demand that an alternative be devised. A statistical method (MIL-STD-105E, {open_quotes}Sampling Procedures and Tables for Inspection by Attributes{close_quotes}) for assessing product quality from a continuous process was adapted to the vehicle decontamination process. This method produced a sampling scheme that automatically compensates and accommodates fluctuating batch sizes and changing conditions without the need to modify or rectify the sampling scheme in the field. Vehicles are randomly selected (sampled) upon completion of the decontamination process to be surveyed for residual radioactive surface contamination. The frequency of sampling is based on the expected number of vehicles passing through the decontamination process in a given period and the confidence level desired. This process has been successfully used for 1 year at the former uranium mill site in Monticello, Utah (a CERCLA regulated clean-up site). The method forces improvement in the quality of the decontamination process and results in a lower likelihood that vehicles exceeding the surface contamination standards are offered for survey. Implementation of this statistical sampling method on Monticello Projects has resulted in more efficient processing of vehicles through decontamination and radiological release, saved hundreds of hours of processing time, provided a high level of confidence that release limits are met, and improved the radiological cleanliness of vehicles leaving the controlled site.

Lively, J.W.; Ware, J.A. [Rust Geotech, Grand Junction, CO (United States)

1996-06-01T23:59:59.000Z

11

Flow cytometric detection method for DNA samples  

DOE Patents [OSTI]

Disclosed herein are two methods for rapid multiplex analysis to determine the presence and identity of target DNA sequences within a DNA sample. Both methods use reporting DNA sequences, e.g., modified conventional Taqman.RTM. probes, to combine multiplex PCR amplification with microsphere-based hybridization using flow cytometry means of detection. Real-time PCR detection can also be incorporated. The first method uses a cyanine dye, such as, Cy3.TM., as the reporter linked to the 5' end of a reporting DNA sequence. The second method positions a reporter dye, e.g., FAM.TM. on the 3' end of the reporting DNA sequence and a quencher dye, e.g., TAMRA.TM., on the 5' end.

Nasarabadi,Shanavaz (Livermore, CA); Langlois, Richard G. (Livermore, CA); Venkateswaran, Kodumudi S. (Round Rock, TX)

2011-07-05T23:59:59.000Z

12

Flow cytometric detection method for DNA samples  

DOE Patents [OSTI]

Disclosed herein are two methods for rapid multiplex analysis to determine the presence and identity of target DNA sequences within a DNA sample. Both methods use reporting DNA sequences, e.g., modified conventional Taqman.RTM. probes, to combine multiplex PCR amplification with microsphere-based hybridization using flow cytometry means of detection. Real-time PCR detection can also be incorporated. The first method uses a cyanine dye, such as, Cy3.TM., as the reporter linked to the 5' end of a reporting DNA sequence. The second method positions a reporter dye, e.g., FAM, on the 3' end of the reporting DNA sequence and a quencher dye, e.g., TAMRA, on the 5' end.

Nasarabadi, Shanavaz (Livermore, CA); Langlois, Richard G. (Livermore, CA); Venkateswaran, Kodumudi S. (Livermore, CA)

2006-08-01T23:59:59.000Z

13

Well purge and sample apparatus and method  

DOE Patents [OSTI]

The present invention specifically permits purging and/or sampling of a well but only removing, at most, about 25% of the fluid volume compared to conventional methods and, at a minimum, removing none of the fluid volume from the well. The invention is an isolation assembly with a packer, pump and exhaust, that is inserted into the well. The isolation assembly is designed so that only a volume of fluid between the outside diameter of the isolation assembly and the inside diameter of the well over a fluid column height from the bottom of the well to the top of the active portion (lower annulus) is removed. The packer is positioned above the active portion thereby sealing the well and preventing any mixing or contamination of inlet fluid with fluid above the packer. Ports in the wall of the isolation assembly permit purging and sampling of the lower annulus along the height of the active portion. 8 figs.

Schalla, R.; Smith, R.M.; Hall, S.H.; Smart, J.E.; Gustafson, G.S.

1995-10-24T23:59:59.000Z

14

Well purge and sample apparatus and method  

DOE Patents [OSTI]

The present invention specifically permits purging and/or sampling of a well but only removing, at most, about 25% of the fluid volume compared to conventional methods and, at a minimum, removing none of the fluid volume from the well. The invention is an isolation assembly with a packer, pump and exhaust, that is inserted into the well. The isolation assembly is designed so that only a volume of fluid between the outside diameter of the isolation assembly and the inside diameter of the well over a fluid column height from the bottom of the well to the top of the active portion (lower annulus) is removed. The packer is positioned above the active portion thereby sealing the well and preventing any mixing or contamination of inlet fluid with fluid above the packer. Ports in the wall of the isolation assembly permit purging and sampling of the lower annulus along the height of the active portion.

Schalla, Ronald (Kennewick, WA); Smith, Ronald M. (Richland, WA); Hall, Stephen H. (Kennewick, WA); Smart, John E. (Richland, WA); Gustafson, Gregg S. (Redmond, WA)

1995-01-01T23:59:59.000Z

15

Detection and effects of pump low-flow operation  

SciTech Connect (OSTI)

Operating experience and previous studies have shown that a significant cause of pump problems and failures can result from low- flow operation. Operation at low-flow rates can create unstable flows within the pump impeller and casing. This condition can result in an increased radial and axial thrust on the rotor, which in turn causes higher shaft stresses, increased shaft deflection, and potential bearing and mechanical seal problems. Two of the more serious results of low-flow pump operation are cavitation and recirculation. Cavitation is the formation and subsequent collapse of vapor bubbles in any flow that is at an ambient pressure less than the vapor pressure of the liquid medium. It is the collapse of these vapor bubbles against the metal surfaces of the impeller or casing that causes surface pitting, erosion, and deterioration. Pump recirculation more damaging than cavitation. If located at the impeller eye, recirculation damages the inlet areas of the casing. At the impeller tips, recirculation alters the outside diameter of the impeller. If recirculation occurs around impeller shrouds, it damages thrust bearings. Recirculation also erodes impellers, diffusers, and volutes and causes failure of mechanical seals and bearings. This paper reports on a utility pump failure caused by low-flow induced phenomena. ORNL is investigating the results of low-flow pump operations by evaluating the types of measurements and diagnostic techniques that are currently used by licensees to detect pump degradation. A new, enhanced application of motor current and power data analysis has been developed that uses a signal comparison methodology to produce an instability ratio indicative of normal or unstable flow conditions. Examples of this type of low-flow detection technique are presented in this paper along with a brief discussion of the various types of technologies currently being used by licensees to evaluate pump operation and determine possible degradation.

Casada, D.A.; Greene, R.H.

1993-12-01T23:59:59.000Z

16

Methods for characterizing, classifying, and identifying unknowns in samples  

DOE Patents [OSTI]

Disclosed is a method for taking the data generated from an array of responses from a multichannel instrument, and determining the characteristics of a chemical in the sample without the necessity of calibrating or training the instrument with known samples containing the same chemical. The characteristics determined by the method are then used to classify and identify the chemical in the sample. The method can also be used to quantify the concentration of the chemical in the sample.

Grate, Jay W [West Richland, WA; Wise, Barry M [Manson, WA

2002-01-01T23:59:59.000Z

17

CONVERGENCE OF THE GRIDDY GIBBS SAMPLING METHOD ...  

E-Print Network [OSTI]

[2] Jun S. Liu et. al., The Multiple-Try Method and Local Optimization in Metropolis ... [23] Lipniacki T., Hat B., Faeder J.R., Hlavacek W.S, Journal of Theoretical ...

2013-08-17T23:59:59.000Z

18

DOE methods for evaluating environmental and waste management samples.  

SciTech Connect (OSTI)

DOE Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) provides applicable methods in use by. the US Department of Energy (DOE) laboratories for sampling and analyzing constituents of waste and environmental samples. The development of DOE Methods is supported by the Laboratory Management Division (LMD) of the DOE. This document contains chapters and methods that are proposed for use in evaluating components of DOE environmental and waste management samples. DOE Methods is a resource intended to support sampling and analytical activities that will aid in defining the type and breadth of contamination and thus determine the extent of environmental restoration or waste management actions needed, as defined by the DOE, the US Environmental Protection Agency (EPA), or others.

Goheen, S C; McCulloch, M; Thomas, B L; Riley, R G; Sklarew, D S; Mong, G M; Fadeff, S K [eds.; Pacific Northwest Lab., Richland, WA (United States)

1994-04-01T23:59:59.000Z

19

Microfluidic DNA sample preparation method and device  

DOE Patents [OSTI]

Manipulation of DNA molecules in solution has become an essential aspect of genetic analyses used for biomedical assays, the identification of hazardous bacterial agents, and in decoding the human genome. Currently, most of the steps involved in preparing a DNA sample for analysis are performed manually and are time, labor, and equipment intensive. These steps include extraction of the DNA from spores or cells, separation of the DNA from other particles and molecules in the solution (e.g. dust, smoke, cell/spore debris, and proteins), and separation of the DNA itself into strands of specific lengths. Dielectrophoresis (DEP), a phenomenon whereby polarizable particles move in response to a gradient in electric field, can be used to manipulate and separate DNA in an automated fashion, considerably reducing the time and expense involved in DNA analyses, as well as allowing for the miniaturization of DNA analysis instruments. These applications include direct transport of DNA, trapping of DNA to allow for its separation from other particles or molecules in the solution, and the separation of DNA into strands of varying lengths.

Krulevitch, Peter A. (Pleasanton, CA); Miles, Robin R. (Danville, CA); Wang, Xiao-Bo (San Diego, CA); Mariella, Raymond P. (Danville, CA); Gascoyne, Peter R. C. (Bellaire, TX); Balch, Joseph W. (Livermore, CA)

2002-01-01T23:59:59.000Z

20

Method and apparatus for imaging a sample on a device  

DOE Patents [OSTI]

A method and apparatus for imaging a sample are provided. An electromagnetic radiation source generates excitation radiation which is sized by excitation optics to a line. The line is directed at a sample resting on a support and excites a plurality of regions on the sample. Collection optics collect response radiation reflected from the sample I and image the reflected radiation. A detector senses the reflected radiation and is positioned to permit discrimination between radiation reflected from a certain focal plane in the sample and certain other planes within the sample.

Trulson, Mark (Santa Clara, CA); Stern, David (Mountain View, CA); Fiekowsky, Peter (Los Altos, CA); Rava, Richard (Palo Alto, CA); Walton, Ian (Menlo Park, CA); Fodor, Stephen P. A. (Palo Alto, CA)

2001-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

Method for sampling sub-micron particles  

DOE Patents [OSTI]

Apparatus and method steps for collecting sub-micron sized particles include a collection chamber and cryogenic cooling. The cooling is accomplished by coil tubing carrying nitrogen in liquid form, with the liquid nitrogen changing to the gas phase before exiting from the collection chamber in the tubing. Standard filters are used to filter out particles of diameter greater than or equal to 0.3 microns; however the present invention is used to trap particles of less than 0.3 micron in diameter. A blower draws air to said collection chamber through a filter which filters particles with diameters greater than or equal to 0.3 micron. The air is then cryogenically cooled so that moisture and sub-micron sized particles in the air condense into ice on the coil. The coil is then heated so that the ice melts, and the liquid is then drawn off and passed through a Buchner funnel where the liquid is passed through a Nuclepore membrane. A vacuum draws the liquid through the Nuclepore membrane, with the Nuclepore membrane trapping sub-micron sized particles therein. The Nuclepore membrane is then covered on its top and bottom surfaces with sheets of Mylar.RTM. and the assembly is then crushed into a pellet. This effectively traps the sub-micron sized particles for later analysis.

Gay, Don D. (Aiken, SC); McMillan, William G. (Ulmers, SC)

1985-01-01T23:59:59.000Z

22

Transuranic waste characterization sampling and analysis methods manual  

SciTech Connect (OSTI)

The Transuranic Waste Characterization Sampling and Analysis Methods Manual (Methods Manual) provides a unified source of information on the sampling and analytical techniques that enable Department of Energy (DOE) facilities to comply with the requirements established in the current revision of the Transuranic Waste Characterization Quality Assurance Program Plan (QAPP) for the Waste Isolation Pilot Plant (WIPP) Transuranic (TRU) Waste Characterization Program (the Program). This Methods Manual includes all of the testing, sampling, and analytical methodologies accepted by DOE for use in implementing the Program requirements specified in the QAPP.

NONE

1995-05-01T23:59:59.000Z

23

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 1  

E-Print Network [OSTI]

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 1 DIESEL EXHAUST.D. and Megan Arnold University of Minnesota Department of Mechanical Engineering Center for Diesel Research....................................................................................... 3 Diesel aerosol size instrumentation............................................................ 4

Minnesota, University of

24

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 2  

E-Print Network [OSTI]

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 2 AEROSOL DYMAMICS Arnold University of Minnesota Department of Mechanical Engineering Center for Diesel Research................................................................................................. 3 Diesel aerosol composition and structure................................................... 3

Minnesota, University of

25

Reference Potential source Data type Sampling site Type of samples Number of samples Method of source  

E-Print Network [OSTI]

samples for Saharan dust from Libya back trajectory analysis Kandler et al. 2009 PSA NAF-2 Illite NAF-4 Illite/kaolinite ratio Chlorite/kaolinite ratio Carbonate content Libya (here: central

Meskhidze, Nicholas

26

DOE methods for evaluating environmental and waste management samples  

SciTech Connect (OSTI)

DOE Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) is a resource intended to support sampling and analytical activities for the evaluation of environmental and waste management samples from U.S. Department of Energy (DOE) sites. DOE Methods is the result of extensive cooperation from all DOE analytical laboratories. All of these laboratories have contributed key information and provided technical reviews as well as significant moral support leading to the success of this document. DOE Methods is designed to encompass methods for collecting representative samples and for determining the radioisotope activity and organic and inorganic composition of a sample. These determinations will aid in defining the type and breadth of contamination and thus determine the extent of environmental restoration or waste management actions needed, as defined by the DOE, the U.S. Environmental Protection Agency, or others. The development of DOE Methods is supported by the Analytical Services Division of DOE. Unique methods or methods consolidated from similar procedures in the DOE Procedures Database are selected for potential inclusion in this document. Initial selection is based largely on DOE needs and procedure applicability and completeness. Methods appearing in this document are one of two types, {open_quotes}Draft{close_quotes} or {open_quotes}Verified{close_quotes}. {open_quotes}Draft{close_quotes} methods that have been reviewed internally and show potential for eventual verification are included in this document, but they have not been reviewed externally, and their precision and bias may not be known. {open_quotes}Verified{close_quotes} methods in DOE Methods have been reviewed by volunteers from various DOE sites and private corporations. These methods have delineated measures of precision and accuracy.

Goheen, S.C.; McCulloch, M.; Thomas, B.L.; Riley, R.G.; Sklarew, D.S.; Mong, G.M.; Fadeff, S.K. [eds.

1994-10-01T23:59:59.000Z

27

Soil separator and sampler and method of sampling  

DOE Patents [OSTI]

A soil sampler includes a fluidized bed for receiving a soil sample. The fluidized bed may be in communication with a vacuum for drawing air through the fluidized bed and suspending particulate matter of the soil sample in the air. In a method of sampling, the air may be drawn across a filter, separating the particulate matter. Optionally, a baffle or a cyclone may be included within the fluidized bed for disentrainment, or dedusting, so only the finest particulate matter, including asbestos, will be trapped on the filter. The filter may be removable, and may be tested to determine the content of asbestos and other hazardous particulate matter in the soil sample.

O'Brien, Barry H. (Idaho Falls, ID) [Idaho Falls, ID; Ritter, Paul D. (Idaho Falls, ID) [Idaho Falls, ID

2010-02-16T23:59:59.000Z

28

Method and apparatus for imaging a sample on a device  

DOE Patents [OSTI]

The present invention provides methods and systems for detecting a labeled marker on a sample located on a support. The imaging system comprises a body for immobilizing the support, an excitation radiation source and excitation optics to generate and direct the excitation radiation at the sample. In response, labeled material on the sample emits radiation which has a wavelength that is different from the excitation wavelength, which radiation is collected by collection optics and imaged onto a detector which generates an image of the sample.

Trulson, Mark (Santa Clara, CA); Stern, David (Mountain View, CA); Fiekowsky, Peter (Los Altos, CA); Rava, Richard (Palo Alto, CA); Walton, Ian (Menlo Park, CA); Fodor, Stephen P. A. (Palo Alto, CA)

1996-01-01T23:59:59.000Z

29

RAPID METHOD FOR DETERMINATION OF RADIOSTRONTIUM IN EMERGENCY MILK SAMPLES  

SciTech Connect (OSTI)

A new rapid separation method for radiostrontium in emergency milk samples was developed at the Savannah River Site (SRS) Environmental Bioassay Laboratory (Aiken, SC, USA) that will allow rapid separation and measurement of Sr-90 within 8 hours. The new method uses calcium phosphate precipitation, nitric acid dissolution of the precipitate to coagulate residual fat/proteins and a rapid strontium separation using Sr Resin (Eichrom Technologies, Darien, IL, USA) with vacuum-assisted flow rates. The method is much faster than previous method that use calcination or cation exchange pretreatment, has excellent chemical recovery, and effectively removes beta interferences. When a 100 ml sample aliquot is used, the method has a detection limit of 0.5 Bq/L, well below generic emergency action levels.

Maxwell, S.; Culligan, B.

2008-07-17T23:59:59.000Z

30

Fluidics platform and method for sample preparation and analysis  

DOE Patents [OSTI]

Herein provided are fluidics platform and method for sample preparation and analysis. The fluidics platform is capable of analyzing DNA from blood samples using amplification assays such as polymerase-chain-reaction assays and loop-mediated-isothermal-amplification assays. The fluidics platform can also be used for other types of assays and analyzes. In some embodiments, a sample in a sealed tube can be inserted directly. The following isolation, detection, and analyzes can be performed without a user's intervention. The disclosed platform may also comprises a sample preparation system with a magnetic actuator, a heater, and an air-drying mechanism, and fluid manipulation processes for extraction, washing, elution, assay assembly, assay detection, and cleaning after reactions and between samples.

Benner, W. Henry; Dzenitis, John M.; Bennet, William J.; Baker, Brian R.

2014-08-19T23:59:59.000Z

31

Self-contained cryogenic gas sampling apparatus and method  

DOE Patents [OSTI]

Apparatus for obtaining a whole gas sample, is composed of: a sample vessel having an inlet for receiving a gas sample; a controllable valve mounted for controllably opening and closing the inlet; a valve control coupled to the valve for opening and closing the valve at selected times; a portable power source connected for supplying operating power to the valve control; and a cryogenic coolant in thermal communication with the vessel for cooling the interior of the vessel to cryogenic temperatures. A method is described for obtaining an air sample using the apparatus described above, by: placing the apparatus at a location at which the sample is to be obtained; operating the valve control to open the valve at a selected time and close the valve at a selected subsequent time; and between the selected times maintaining the vessel at a cryogenic temperature by heat exchange with the coolant. 3 figs.

McManus, G.J.; Motes, B.G.; Bird, S.K.; Kotter, D.K.

1996-03-26T23:59:59.000Z

32

E-Print Network 3.0 - atomic absorption method Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

method Search Powered by Explorit Topic List Advanced Search Sample search results for: atomic absorption method...

33

E-Print Network 3.0 - atomic absorption methods Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

methods Search Powered by Explorit Topic List Advanced Search Sample search results for: atomic absorption methods...

34

Method and apparatus for sampling low-yield wells  

DOE Patents [OSTI]

An apparatus and method for collecting a sample from a low-yield well or perched aquifer includes a pump and a controller responsive to water level sensors for filling a sample reservoir. The controller activates the pump to fill the reservoir when the water level in the well reaches a high level as indicated by the sensor. The controller deactivates the pump when the water level reaches a lower level as indicated by the sensors. The pump continuously activates and deactivates the pump until the sample reservoir is filled with a desired volume, as indicated by a reservoir sensor. At the beginning of each activation cycle, the controller optionally can select to purge an initial quantity of water prior to filling the sample reservoir. The reservoir can be substantially devoid of air and the pump is a low volumetric flow rate pump. Both the pump and the reservoir can be located either inside or outside the well.

Last, George V. (Richland, WA); Lanigan, David C. (Kennewick, WA)

2003-04-15T23:59:59.000Z

35

SAMPLING METHODS: A LIST OF SOURCES M.1 Introduction  

E-Print Network [OSTI]

for sampling methods are available through online literature databases; Federal, State, and university libraries; the internet; and other sources. M.2 List of Sources Department of Energy (DOE). 1987, Safety, and Health, Office of Environmental Audit, Washington, D.C. ! General Description of Document

36

Radiochemistry methods in DOE methods for evaluating environmental and waste management samples  

SciTech Connect (OSTI)

Current standard sources of radiochemistry methods are often inappropriate for use in evaluating US Department of Energy environmental and waste management (DOE/EW) samples. Examples of current sources include EPA, ASTM, Standard Methods for the Examination of Water and Wastewater and HASL-300. Applicability of these methods is limited to specific matrices (usually water), radiation levels (usually environmental levels), and analytes (limited number). Radiochemistry methods in DOE Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) attempt to fill the applicability gap that exists between standard methods and those needed for DOE/EM activities. The Radiochemistry chapter in DOE Methods includes an ``analysis and reporting`` guidance section as well as radiochemistry methods. A basis for identifying the DOE/EM radiochemistry needs is discussed. Within this needs framework, the applicability of standard methods and targeted new methods is identified. Sources of new methods (consolidated methods from DOE laboratories and submissions from individuals) and the methods review process will be discussed. The processes involved in generating consolidated methods add editing individually submitted methods will be compared. DOE Methods is a living document and continues to expand by adding various kinds of methods. Radiochemistry methods are highlighted in this paper. DOE Methods is intended to be a resource for methods applicable to DOE/EM problems. Although it is intended to support DOE, the guidance and methods are not necessarily exclusive to DOE. The document is available at no cost through the Laboratory Management Division of DOE, Office of Technology Development.

Fadeff, S.K.; Goheen, S.C.

1994-08-01T23:59:59.000Z

37

Method of isolating an oilfield flowline sample for analysis without shearing the sample  

SciTech Connect (OSTI)

This patent describes a method for isolating an oil field production flowline sample for analysis without shearing the sample. It comprises: placing an isolation chamber in fluid communication with a sampling port of an oilfield production flowline. The isolation chamber comprising a closed vessel, a first entry port into the vessel, and a first exit port out of the vessel controlled by a first valve. The sampling port is controlled by a valve; opening a sampling port valve while the first valve is closed to permit pressure within the isolation chamber to equalize the pressure within the first entry port and the flowline; opening the first valve to permit oilfield production to pass from the flowline through the sampling port and the first entry port into the isolation chamber and out of the first valve; closing the first valve; closing the sampling port valve; allowing the oilfield production fluid contained within the isolation chamber to separate for a period of time, and removing a sample of fluid from the isolation chamber for examination.

Brickhouse, P.E.

1990-03-06T23:59:59.000Z

38

Transuranic waste characterization sampling and analysis methods manual. Revision 1  

SciTech Connect (OSTI)

This Methods Manual provides a unified source of information on the sampling and analytical techniques that enable Department of Energy (DOE) facilities to comply with the requirements established in the current revision of the Transuranic Waste Characterization Quality Assurance Program Plan (QAPP) for the Waste Isolation Pilot Plant (WIPP) Transuranic (TRU) Waste Characterization Program (the Program) and the WIPP Waste Analysis Plan. This Methods Manual includes all of the testing, sampling, and analytical methodologies accepted by DOE for use in implementing the Program requirements specified in the QAPP and the WIPP Waste Analysis Plan. The procedures in this Methods Manual are comprehensive and detailed and are designed to provide the necessary guidance for the preparation of site-specific procedures. With some analytical methods, such as Gas Chromatography/Mass Spectrometry, the Methods Manual procedures may be used directly. With other methods, such as nondestructive characterization, the Methods Manual provides guidance rather than a step-by-step procedure. Sites must meet all of the specified quality control requirements of the applicable procedure. Each DOE site must document the details of the procedures it will use and demonstrate the efficacy of such procedures to the Manager, National TRU Program Waste Characterization, during Waste Characterization and Certification audits.

Suermann, J.F.

1996-04-01T23:59:59.000Z

39

Radiochemistry methods in DOE Methods for Evaluating Environmental and Waste Management Samples: Addressing new challenges  

SciTech Connect (OSTI)

Radiochemistry methods in Department of Energy Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) add to the repertoire of other standard methods in support of U.S. Department of Energy environmental restoration and waste management (DOE/EM) radiochemical characterization activities. Current standard sources of radiochemistry methods are not always applicable for evaluating DOE/EM samples. Examples of current sources include those provided by the US Environmental Protection Agency, the American Society for Testing and Materials, Standard Methods for the Examination of Water and Wastewater, and Environmental Measurements Laboratory Procedures Manual (HASL-300). The applicability of these methods is generally limited to specific matrices (usually water), low-level radioactive samples, and a limited number of analytes. DOE Methods complements these current standard methods by addressing the complexities of EM characterization needs. The process for determining DOE/EM radiochemistry characterization needs is discussed. In this context of DOE/EM needs, the applicability of other sources of standard radiochemistry methods is defined, and gaps in methodology are identified. Current methods in DOE Methods and the EM characterization needs they address are discussed. Sources of new methods and the methods incorporation process are discussed. The means for individuals to participate in (1) identification of DOE/EM needs, (2) the methods incorporation process, and (3) submission of new methods are identified.

Fadeff, S.K.; Goheen, S.C.; Riley, R.G. [Pacific Northwest Lab., Richland, WA (United States)] [and others

1994-12-31T23:59:59.000Z

40

RAPID SEPARATION METHOD FOR ACTINIDES IN EMERGENCY SOIL SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of actinides in soil and sediment samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used for samples up to 2 grams in emergency response situations. The actinides in soil method utilizes a rapid sodium hydroxide fusion method, a lanthanum fluoride soil matrix removal step, and a streamlined column separation process with stacked TEVA, TRU and DGA Resin cartridges. Lanthanum was separated rapidly and effectively from Am and Cm on DGA Resin. Vacuum box technology and rapid flow rates are used to reduce analytical time. Alpha sources are prepared using cerium fluoride microprecipitation for counting by alpha spectrometry. The method showed high chemical recoveries and effective removal of interferences. This new procedure was applied to emergency soil samples received in the NRIP Emergency Response exercise administered by the National Institute for Standards and Technology (NIST) in April, 2009. The actinides in soil results were reported within 4-5 hours with excellent quality.

Maxwell, S.; Culligan, B.; Noyes, G.

2009-11-09T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Determination of Adenosine Triphosphate on Marine Particulates: Synthesis of Methods for Use on OTEC Samples  

E-Print Network [OSTI]

OF METHODS FOR USE ON OTEC SAMPLES. Anthony T. Jones Eric 0.OF METHODS FOR USE ON OTEC SAMPLES. ABSTRACT Adenosine

Jones, Anthony T.; Hartwig, Eric O.

1982-01-01T23:59:59.000Z

42

RAPID SEPARATION METHOD FOR ACTINIDES IN EMERGENCY AIR FILTER SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of actinides and strontium in air filter samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used in emergency response situations. The actinides and strontium in air filter method utilizes a rapid acid digestion method and a streamlined column separation process with stacked TEVA, TRU and Sr Resin cartridges. Vacuum box technology and rapid flow rates are used to reduce analytical time. Alpha emitters are prepared using cerium fluoride microprecipitation for counting by alpha spectrometry. The purified {sup 90}Sr fractions are mounted directly on planchets and counted by gas flow proportional counting. The method showed high chemical recoveries and effective removal of interferences. This new procedure was applied to emergency air filter samples received in the NRIP Emergency Response exercise administered by the National Institute for Standards and Technology (NIST) in April, 2009. The actinide and {sup 90}Sr in air filter results were reported in {approx}4 hours with excellent quality.

Maxwell, S.; Noyes, G.; Culligan, B.

2010-02-03T23:59:59.000Z

43

Well fluid isolation and sample apparatus and method  

DOE Patents [OSTI]

The present invention specifically permits purging and/or sampling of a well but only removing, at most, about 25% of the fluid volume compared to conventional methods and, at a minimum, removing none of the fluid volume from the well. The invention is an isolation assembly that is inserted into the well. The isolation assembly is designed so that only a volume of fluid between the outside diameter of the isolation assembly and the inside diameter of the well over a fluid column height from the bottom of the well to the top of the active portion (lower annulus) is removed. A seal may be positioned above the active portion thereby sealing the well and preventing any mixing or contamination of inlet fluid with fluid above the packer. Purged well fluid is stored in a riser above the packer. Ports in the wall of the isolation assembly permit purging and sampling of the lower annulus along the height of the active portion.

Schalla, Ronald (Kennewick, WA); Smith, Ronald M. (Richland, WA); Hall, Stephen H. (Kennewick, WA); Smart, John E. (Richland, WA)

1995-01-01T23:59:59.000Z

44

Drum plug piercing and sampling device and method  

DOE Patents [OSTI]

An apparatus and method for piercing a drum plug of a drum in order to sample and/or vent gases that may accumulate in a space of the drum is provided. The drum is not damaged and can be reused since the pierced drum plug can be subsequently replaced. The apparatus includes a frame that is configured for engagement with the drum. A cylinder actuated by a fluid is mounted to the frame. A piercer is placed into communication with the cylinder so that actuation of the cylinder causes the piercer to move in a linear direction so that the piercer may puncture the drum plug of the drum.

Counts, Kevin T. (Aiken, SC)

2011-04-26T23:59:59.000Z

45

The Descriptive Experience Sampling method Russell T. Hurlburt & Sarah A. Akhter  

E-Print Network [OSTI]

's [Phenomenol Cogn Sci, this issue] second- person interview method. Key words Descriptive Experience Sampling

Ahmad, Sajjad

46

Method for testing earth samples for contamination by organic contaminants  

DOE Patents [OSTI]

Provided is a method for testing earth samples for contamination by organic contaminants, and particularly for aromatic compounds such as those found in diesel fuel and other heavy fuel oils, kerosene, creosote, coal oil, tars and asphalts. A drying step is provided in which a drying agent is contacted with either the earth sample or a liquid extract phase to reduce to possibility of false indications of contamination that could occur when humic material is present in the earth sample. This is particularly a problem when using relatively safe, non-toxic and inexpensive polar solvents such as isopropyl alcohol since the humic material tends to be very soluble in those solvents when water is present. Also provided is an ultraviolet spectroscopic measuring technique for obtaining an indication as to whether a liquid extract phase contains aromatic organic contaminants. In one embodiment, the liquid extract phase is subjected to a narrow and discrete band of radiation including a desired wave length and the ability of the liquid extract phase to absorb that wavelength of ultraviolet radiation is measured to provide an indication of the presence of aromatic organic contaminants.

Schabron, John F. (Laramie, WY)

1996-01-01T23:59:59.000Z

47

Method for testing earth samples for contamination by organic contaminants  

DOE Patents [OSTI]

Provided is a method for testing earth samples for contamination by organic contaminants, and particularly for aromatic compounds such as those found in diesel fuel and other heavy fuel oils, kerosene, creosote, coal oil, tars and asphalts. A drying step is provided in which a drying agent is contacted with either the earth sample or a liquid extract phase to reduce to possibility of false indications of contamination that could occur when humic material is present in the earth sample. This is particularly a problem when using relatively safe, non-toxic and inexpensive polar solvents such as isopropyl alcohol since the humic material tends to be very soluble in those solvents when water is present. Also provided is an ultraviolet spectroscopic measuring technique for obtaining an indication as to whether a liquid extract phase contains aromatic organic contaminants. In one embodiment, the liquid extract phase is subjected to a narrow and discrete band of radiation including a desired wave length and the ability of the liquid extract phase to absorb that wavelength of ultraviolet radiation is measured to provide an indication of the presence of aromatic organic contaminants. 2 figs.

Schabron, J.F.

1996-10-01T23:59:59.000Z

48

A comparison of methods for representing sparsely sampled random quantities.  

SciTech Connect (OSTI)

This report discusses the treatment of uncertainties stemming from relatively few samples of random quantities. The importance of this topic extends beyond experimental data uncertainty to situations involving uncertainty in model calibration, validation, and prediction. With very sparse data samples it is not practical to have a goal of accurately estimating the underlying probability density function (PDF). Rather, a pragmatic goal is that the uncertainty representation should be conservative so as to bound a specified percentile range of the actual PDF, say the range between 0.025 and .975 percentiles, with reasonable reliability. A second, opposing objective is that the representation not be overly conservative; that it minimally over-estimate the desired percentile range of the actual PDF. The presence of the two opposing objectives makes the sparse-data uncertainty representation problem interesting and difficult. In this report, five uncertainty representation techniques are characterized for their performance on twenty-one test problems (over thousands of trials for each problem) according to these two opposing objectives and other performance measures. Two of the methods, statistical Tolerance Intervals and a kernel density approach specifically developed for handling sparse data, exhibit significantly better overall performance than the others.

Romero, Vicente Jose; Swiler, Laura Painton; Urbina, Angel; Mullins, Joshua

2013-09-01T23:59:59.000Z

49

E-Print Network 3.0 - assurance sampling method Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

for NRDA followed standard operating procedure (SOP), water sampling plans, Summary: procedures, and NOAA's Analytical Quality Assurance Project Plan (QAPP). Samples were sent to...

50

E-Print Network 3.0 - air-cooled low-flow torch Sample Search...  

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22 Electrical discharges in theElectrical discharges in the Reverse Vortex FlowReverse Vortex Flow Summary: Numerical Simulation for 3.5kW Microwave Plasma Stabilization with...

51

Installation of a Low Flow Unit at the Abiquiu Hydroelectric Facility  

SciTech Connect (OSTI)

Final Technical Report for the Recovery Act Project for the Installation of a Low Flow Unit at the Abiquiu Hydroelectric Facility. The Abiquiu hydroelectric facility existed with two each 6.9 MW vertical flow Francis turbine-generators. This project installed a new 3.1 MW horizontal flow low flow turbine-generator. The total plant flow range to capture energy and generate power increased from between 250 and 1,300 cfs to between 75 and 1,550 cfs. Fifty full time equivalent (FTE) construction jobs were created for this project - 50% (or 25 FTE) were credited to ARRA funding due to the ARRA 50% project cost match. The Abiquiu facility has increased capacity, increased efficiency and provides for an improved aquatic environment owing to installed dissolved oxygen capabilities during traditional low flow periods in the Rio Chama. A new powerhouse addition was constructed to house the new turbine-generator equipment.

Jack Q. Richardson

2012-06-28T23:59:59.000Z

52

Field Sampling Report -Water 2005 SFEI PRISM-Methods Development  

E-Print Network [OSTI]

of aquatic toxicity by Pacific Eco-Risk (PER) (2 twenty-liter carboys). 2.2 Personnel The personnel and work transferred remaining samples to AMS in Livermore April 18, 2005 0800-1200 Mr. Salop shipped remaining samples

53

[DOE method for evaluating environmental and waste management samples: Revision 1, Addendum 1  

SciTech Connect (OSTI)

The US Dapartment of Energy`s (DOE`s) environmental and waste management (EM) sampling and analysis activities require that large numbers of samples be analyzed for materials characterization, environmental surveillance, and site-remediation programs. The present document, DOE Methods for Evaluating Environmental and Waste Management Samples (DOE Methods), is a supplemental resource for analyzing many of these samples.

Goheen, S.C.

1995-04-01T23:59:59.000Z

54

E-Print Network 3.0 - activity optimization method Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

optimization method Search Powered by Explorit Topic List Advanced Search Sample search results for: activity optimization method Page: << < 1 2 3 4 5 > >> 1 Optimization 1-1...

55

E-Print Network 3.0 - advanced analysis methods Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

methods Search Powered by Explorit Topic List Advanced Search Sample search results for: advanced analysis methods Page: << < 1 2 3 4 5 > >> 1 Problems in real analysis: advanced...

56

E-Print Network 3.0 - advanced computational methods Sample Search...  

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methods Search Powered by Explorit Topic List Advanced Search Sample search results for: advanced computational methods Page: << < 1 2 3 4 5 > >> 1 Architecture Architecture...

57

E-Print Network 3.0 - advanced statistical methods Sample Search...  

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statistical methods Search Powered by Explorit Topic List Advanced Search Sample search results for: advanced statistical methods Page: << < 1 2 3 4 5 > >> 1 STAT 665365:...

58

Line search methods with variable sample size for unconstrained ...  

E-Print Network [OSTI]

Jun 27, 2011 ... Key words: stochastic optimization, line search, simulations, sample average ...... Utility of agent i for alternative j is given by. Ui,j = Vi,j + ?i,j,.

2011-06-27T23:59:59.000Z

59

Method for preconcentrating a sample for subsequent analysis  

DOE Patents [OSTI]

A system for analysis of trace concentration of contaminants in air includes a portable liquid chromatograph and a preconcentrator for the contaminants to be analyzed. The preconcentrator includes a sample bag having an inlet valve and an outlet valve for collecting an air sample. When the sample is collected the sample bag is connected in series with a sorbing apparatus in a recirculation loop. The sorbing apparatus has an inner gas-permeable container containing a sorbent material and an outer gas-impermeable container. The sample is circulated through the outer container and around the inner container for trapping and preconcentrating the contaminants in the sorbent material. The sorbent material may be a liquid having the same composition as the mobile phase of the chromatograph for direct injection thereinto. Alternatively, the sorbent material may be a porous, solid body, to which mobile phase liquid is added after preconcentration of the contaminants for dissolving the contaminants, the liquid solution then being withdrawn for injection into the chromatograph.

Zaromb, Solomon (Hinsdale, IL)

1990-01-01T23:59:59.000Z

60

Analytical instrument with apparatus and method for sample concentrating  

DOE Patents [OSTI]

A system for analysis of trace concentrations of contaminants in air includes a portable liquid chromatograph and a preconcentrator for the contaminants to be analyzed. The preconcentrator includes a sample bag having an inlet valve and an outlet valve for collecting an air sample. When the sample is collected the sample bag is connected in series with a sorbing apparatus in a recirculation loop. The sorbing apparatus has an inner gas-permeable container containing a sorbent material and an outer gas-impermeable container. The sample is circulated through the outer container and around the inner container for trapping and preconcentrating the contaminants in the sorbent material. The sorbent material may be a liquid having the same composition as the mobile phase of the chromatograph for direct injection thereinto. Alternatively, the sorbent material may be a porous, solid body, to which mobile phase liquid is added after preconcentration of the contaminants for dissolving the contaminants, the liquid solution then being withdrawn for injection into the chromatograph.

Zaromb, S.

1986-08-04T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

Nature Methods Minimalistic encapsulated proteomic sample processing applied to copy number  

E-Print Network [OSTI]

Nature Methods Minimalistic encapsulated proteomic sample processing applied to copy number Supplementary Figure 1 Comparison of SILAC-based ratios using different sample processing conditions steps of the iST sample preparation workflow. It further shows how to troubleshoot the method in case

Cai, Long

62

Statistical Methods and Tools for Hanford Staged Feed Tank Sampling  

SciTech Connect (OSTI)

This report summarizes work conducted by Pacific Northwest National Laboratory to technically evaluate the current approach to staged feed sampling of high-level waste (HLW) sludge to meet waste acceptance criteria (WAC) for transfer from tank farms to the Hanford Waste Treatment and Immobilization Plant (WTP). The current sampling and analysis approach is detailed in the document titled Initial Data Quality Objectives for WTP Feed Acceptance Criteria, 24590-WTP-RPT-MGT-11-014, Revision 0 (Arakali et al. 2011). The goal of this current work is to evaluate and provide recommendations to support a defensible, technical and statistical basis for the staged feed sampling approach that meets WAC data quality objectives (DQOs).

Fountain, Matthew S.; Brigantic, Robert T.; Peterson, Reid A.

2013-10-01T23:59:59.000Z

63

{sup 222}Rn in water: A comparison of two sample collection methods and two sample transport methods, and the determination of temporal variation in North Carolina ground water  

SciTech Connect (OSTI)

Objectives of this field experiment were: (1) determine whether there was a statistically significant difference between the radon concentrations of samples collected by EPA`s standard method, using a syringe, and an alternative, slow-flow method; (2) determine whether there was a statistically significant difference between the measured radon concentrations of samples mailed vs samples not mailed; and (3) determine whether there was a temporal variation of water radon concentration over a 7-month period. The field experiment was conducted at 9 sites, 5 private wells, and 4 public wells, at various locations in North Carolina. Results showed that a syringe is not necessary for sample collection, there was generally no significant radon loss due to mailing samples, and there was statistically significant evidence of temporal variations in water radon concentrations.

Hightower, J.H. III [North Carolina Univ., Chapel Hill, NC (United States). Dept. of Environmental Sciences and Engineering] [North Carolina Univ., Chapel Hill, NC (United States). Dept. of Environmental Sciences and Engineering

1994-12-31T23:59:59.000Z

64

E-Print Network 3.0 - algebraic methods applied Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Sample search results for: algebraic methods applied Page: << < 1 2 3 4 5 > >> 1 Mathematics > Journal of Pure and Applied Algebra July -September 2007 Summary: Mathematics >...

65

E-Print Network 3.0 - analytical methods validation Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

continuous calibration verification for analytical instruments use of method blanks... procedures, and NOAA's Analytical Quality Assurance Project Plan (QAPP). Samples were sent...

66

E-Print Network 3.0 - analytical method validation Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

continuous calibration verification for analytical instruments use of method blanks... procedures, and NOAA's Analytical Quality Assurance Project Plan (QAPP). Samples were sent...

67

E-Print Network 3.0 - analytical methods flambagem Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

continuous calibration verification for analytical instruments use of method blanks... procedures, and NOAA's Analytical Quality Assurance Project Plan (QAPP). Samples were sent...

68

E-Print Network 3.0 - advanced methods algorithms Sample Search...  

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algorithms Search Powered by Explorit Topic List Advanced Search Sample search results for: advanced methods algorithms Page: << < 1 2 3 4 5 > >> 1 Boston University Fall 2010 ECE...

69

E-Print Network 3.0 - analytical chemistry methods Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Powered by Explorit Topic List Advanced Search Sample search results for: analytical chemistry methods Page: << < 1 2 3 4 5 > >> 1 Department of Chemistry Three Year Projection...

70

A DOE manual: DOE methods for evaluating environmental and waste management samples  

SciTech Connect (OSTI)

DOE Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) is a guidance/methods document supporting environmental restoration (ER) and waste management (WM) (collectively referred to as EM) sampling and analysis activities at US Department of Energy (DOE) sites. DOE Methods is intended to supplement existing guidance documents (e.g., the US Environmental Protection Agency`s Test Methods for Evaluating Solid Waste, SW-846), which apply to low-level or non-radioactive samples, and the complexities of waste and environmental samples encountered at DOE sites. The document contains quality assurance (QA), quality control (QC), safety, sampling, organic analysis, inorganic analysis, and radio-analytical guidance as well as sampling and analytical methods. It is updated every six months (April and October) with additional methods. As of April 1994, DOE methods contained 3 sampling and 39 analytical methods. It is anticipated that between 10 and 20 new methods will be added in October 1994. All methods are either peer reviewed and contain performance data, or are included as draft methods.

Goheen, S.C.; Fadeff, S.K.; Sklarew, D.S.; McCulloch, M.; Mong, G.M.; Riley, R.G.; Thomas, B.L.

1994-08-01T23:59:59.000Z

71

Method and apparatus for processing a test sample to concentrate an analyte in the sample from a solvent in the sample  

DOE Patents [OSTI]

A method of processing a test sample to concentrate an analyte in the sample from a solvent in the sample includes: (a) boiling the test sample containing the analyte and solvent in a boiling chamber to a temperature greater than or equal to the solvent boiling temperature and less than the analyte boiling temperature to form a rising sample vapor mixture; (b) passing the sample vapor mixture from the boiling chamber to an elongated primary separation tube, the separation tube having internal sidewalls and a longitudinal axis, the longitudinal axis being angled between vertical and horizontal and thus having an upper region and a lower region; (c) collecting the physically transported liquid analyte on the internal sidewalls of the separation tube; and (d) flowing the collected analyte along the angled internal sidewalls of the separation tube to and pass the separation tube lower region. The invention also includes passing a turbulence inducing wave through a vapor mixture to separate physically transported liquid second material from vaporized first material. Apparatus is also disclosed for effecting separations. Further disclosed is a fluidically powered liquid test sample withdrawal apparatus for withdrawing a liquid test sample from a test sample container and for cleaning the test sample container. 8 figs.

Turner, T.D.; Beller, L.S.; Clark, M.L.; Klingler, K.M.

1997-10-14T23:59:59.000Z

72

High-throughput liquid-absorption preconcentrator sampling methods  

DOE Patents [OSTI]

A system for detecting trace concentrations of an analyte in air includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container comprising a wettable material. The wettable material is continuously wetted with an analyte-sorbing liquid which flows from one part of the container to a lower end. Sampled air flows through the container in contact with the wetted material with a swirling motion which results in efficient transfer of analyte vapors or aerosol particles to the sorbing liquid and preconcentration of traces of analyte in the liquid. The preconcentrated traces of analyte may be either detected within the container or removed therefrom for injection into a separate detection means or for subsequent analysis. 12 figs.

Zaromb, S.

1994-07-12T23:59:59.000Z

73

On the accuracy and resolution of powersum-based sampling methods  

E-Print Network [OSTI]

Recently, several sampling methods suitable for signals that are sums of Diracs have been proposed. Though they are implemented through different acquisition architectures, these methods all rely on estimating the parameters ...

Kusuma, J.

74

E-Print Network 3.0 - ad hoc methods Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

methods Search Powered by Explorit Topic List Advanced Search Sample search results for: ad hoc methods Page: << < 1 2 3 4 5 > >> 1 Ad Hoc Synchronization Considered Harmful Weiwei...

75

E-Print Network 3.0 - assess duration methods Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

duration methods Search Powered by Explorit Topic List Advanced Search Sample search results for: assess duration methods Page: << < 1 2 3 4 5 > >> 1 The U.S. Army Corps of...

76

Universal nucleic acids sample preparation method for cells, spores and their mixture  

DOE Patents [OSTI]

The present invention relates to a method for extracting nucleic acids from biological samples. More specifically the invention relates to a universal method for extracting nucleic acids from unidentified biological samples. An advantage of the presently invented method is its ability to effectively and efficiently extract nucleic acids from a variety of different cell types including but not limited to prokaryotic or eukaryotic cells and/or recalcitrant organisms (i.e. spores). Unlike prior art methods which are focused on extracting nucleic acids from vegetative cell or spores, the present invention effectively extracts nucleic acids from spores, multiple cell types or mixtures thereof using a single method. Important that the invented method has demonstrated an ability to extract nucleic acids from spores and vegetative bacterial cells with similar levels effectiveness. The invented method employs a multi-step protocol which erodes the cell structure of the biological sample, isolates, labels, fragments nucleic acids and purifies labeled samples from the excess of dye.

Bavykin, Sergei (Darien, IL)

2011-01-18T23:59:59.000Z

77

Chemical composition of esophageal-fistula forage samples as influenced by drying method, salivary leaching and sample preparation  

E-Print Network [OSTI]

in partial fulfillment of the requirement for the degree of YASTER OF' SCI"'NCE, De"ember 1g76 CHEJJICAL COY!POSITION OF ESOPHAGEAL-FISTULA FORAGF SA(vPLES AS INFLUENCED BY DRYING I'METHOD, SALIVARY LEACHING AND SAMPLE PREPARATION A Thesis RAFAEL... ARISTIDES ACOS A-GONZALEZ Approved as to style and content by! (Cha rman o Committee) ((iced of Department) ( I'~iamb r ) Yemb r ) Dcc: mb~+~g~n'jrr ABSTRACT Chemical Composition of Esophageal-Fistula Forage Samples as Influenced by Drying Nethod...

Acosta-Gonzalez, Rafael Aristides

1976-01-01T23:59:59.000Z

78

RAPID FUSION METHOD FOR DETERMINATION OF PLUTONIUM ISOTOPES IN LARGE RICE SAMPLES  

SciTech Connect (OSTI)

A new rapid fusion method for the determination of plutonium in large rice samples has been developed at the Savannah River National Laboratory (Aiken, SC, USA) that can be used to determine very low levels of plutonium isotopes in rice. The recent accident at Fukushima Nuclear Power Plant in March, 2011 reinforces the need to have rapid, reliable radiochemical analyses for radionuclides in environmental and food samples. Public concern regarding foods, particularly foods such as rice in Japan, highlights the need for analytical techniques that will allow very large sample aliquots of rice to be used for analysis so that very low levels of plutonium isotopes may be detected. The new method to determine plutonium isotopes in large rice samples utilizes a furnace ashing step, a rapid sodium hydroxide fusion method, a lanthanum fluoride matrix removal step, and a column separation process with TEVA Resin? cartridges. The method can be applied to rice sample aliquots as large as 5 kg. Plutonium isotopes can be determined using alpha spectrometry or inductively-coupled plasma mass spectrometry (ICP-MS). The method showed high chemical recoveries and effective removal of interferences. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory plutonium particles are effectively digested. The MDA for a 5 kg rice sample using alpha spectrometry is 7E-5 mBq g{sup -1}. The method can easily be adapted for use by ICP-MS to allow detection of plutonium isotopic ratios.

Maxwell, S.

2013-03-01T23:59:59.000Z

79

INVESTIGATION OF THE TOTAL ORGANIC HALOGEN ANALYTICAL METHOD AT THE WASTE SAMPLING CHARACTERIZATION FACILITY (WSCF)  

SciTech Connect (OSTI)

Total organic halogen (TOX) is used as a parameter to screen groundwater samples at the Hanford Site. Trending is done for each groundwater well, and changes in TOX and other screening parameters can lead to costly changes in the monitoring protocol. The Waste Sampling and Characterization Facility (WSCF) analyzes groundwater samples for TOX using the United States Environmental Protection Agency (EPA) SW-846 method 9020B (EPA 1996a). Samples from the Soil and Groundwater Remediation Project (S&GRP) are submitted to the WSCF for analysis without information regarding the source of the sample; each sample is in essence a 'blind' sample to the laboratory. Feedback from the S&GRP indicated that some of the WSCF-generated TOX data from groundwater wells had a number of outlier values based on the historical trends (Anastos 2008a). Additionally, analysts at WSCF observed inconsistent TOX results among field sample replicates. Therefore, the WSCF lab performed an investigation of the TOX analysis to determine the cause of the outlier data points. Two causes were found that contributed to generating out-of-trend TOX data: (1) The presence of inorganic chloride in the groundwater samples: at inorganic chloride concentrations greater than about 10 parts per million (ppm), apparent TOX values increase with increasing chloride concentration. A parallel observation is the increase in apparent breakthrough of TOX from the first to the second activated-carbon adsorption tubes with increasing inorganic chloride concentration. (2) During the sample preparation step, excessive purging of the adsorption tubes with oxygen pressurization gas after sample loading may cause channeling in the activated-carbon bed. This channeling leads to poor removal of inorganic chloride during the subsequent wash step with aqueous potassium nitrate. The presence of this residual inorganic chloride then produces erroneously high TOX values. Changes in sample preparation were studied to more effectively remove inorganic chloride from the activated carbon adsorption tubes. With the TOX sample preparation equipment and TOX analyzers at WSCF, the nitrate wash recommended by EPA SW-846 method 9020B was found to be inadequate to remove inorganic chloride interference. Increasing the nitrate wash concentration from 10 grams per liter (g/L) to 100 g/L potassium nitrate and increasing the nitrate wash volume from 3 milliliters (mL) to 10 mL effectively removed the inorganic chloride up to at least 100 ppm chloride in the sample matrix. Excessive purging of the adsorption tubes during sample preparation was eliminated. These changes in sample preparation have been incorporated in the analytical procedure. The results using the revised sample preparation procedure show better agreement of TOX values both for replicate analyses of single samples and for the analysis of replicate samples acquired from the same groundwater well. Furthermore, less apparent column breakthrough now occurs with the revised procedure. One additional modification made to sample preparation was to discontinue the treatment of groundwater samples with sodium bisulfite. Sodium bisulfite is used to remove inorganic chlorine from the sample; inorganic chlorine is not expected to be a constituent in these groundwater samples. Several other factors were also investigated as possible sources of anomalous TOX results: (1) Instrument instability: examination of the history of results for TOX laboratory control samples and initial calibration verification standards indicate good long-term precision for the method and instrument. Determination of a method detection limit of 2.3 ppb in a deionized water matrix indicates the method and instrumentation have good stability and repeatability. (2) Non-linear instrument response: the instrument is shown to have good linear response from zero to 200 parts per billion (ppb) TOX. This concentration range encompasses the majority of samples received at WSCF for TOX analysis. (3) Improper sample preservation: ion-chromatographic analysis of several samples wit

DOUGLAS JG; MEZNARICH HD, PHD; OLSEN JR; ROSS GA; STAUFFER M

2008-09-30T23:59:59.000Z

80

Method and apparatus for measuring the NMR spectrum of an orientationally disordered sample  

DOE Patents [OSTI]

An improved NMR probe and method are described which substantially improve the resolution of NMR measurements made on powdered or amorphous or otherwise oreintationally disordered samples. The apparatus mechanically varies the orientation of the sample such that the time average of two or more sets of spherical harmonic functions is zero.

Pines, Alexander (Berkeley, CA); Samoson, Ago (Tallinn, SU)

1990-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


81

Passive sampling methods to determine household and personal care product use  

E-Print Network [OSTI]

Passive sampling methods to determine household and personal care product use DEBORAH H. BENNETTa, cleaning products, passive sampling, SUPERB, longitudinal. Introduction Personal care and household care products, such as cleaning products and pesticides, are frequently used in most house- holds although

Leistikow, Bruce N.

82

Sample preparation method for glass welding by ultrashort laser pulses yields higher seam strength  

SciTech Connect (OSTI)

Glass welding by ultrashort laser pulses allows joining without the need of an absorber or a preheating and postheating process. However, cracks generated during the welding process substantially impair the joining strength of the welding seams. In this paper a sample preparation method is described that prevents the formation of cracks. The measured joining strength of samples prepared by this method is substantially higher than previously reported values.

Cvecek, K.; Miyamoto, I.; Strauss, J.; Wolf, M.; Frick, T.; Schmidt, M.

2011-05-01T23:59:59.000Z

83

INVESTIGATION OF THE TOTAL ORGANIC HALOGEN ANALYTICAL METHOD AT THE WASTE SAMPLING AND CHARACTERIZATION FACILITY  

SciTech Connect (OSTI)

Total organic halogen (TOX) is used as a parameter to screen groundwater samples at the Hanford Site. Trending is done for each groundwater well, and changes in TOX and other screening parameters can lead to costly changes in the monitoring protocol. The Waste Sampling and Characterization Facility (WSCF) analyzes groundwater samples for TOX using the United States Environmental Protection Agency (EPA) SW-S46 method 9020B (EPA 1996a). Samples from the Soil and Groundwater Remediation Project (SGRP) are submitted to the WSCF for analysis without information regarding the source of the sample; each sample is in essence a ''blind'' sample to the laboratory. Feedback from the SGRP indicated that some of the WSCF-generated TOX data from groundwater wells had a number of outlier values based on the historical trends (Anastos 200Sa). Additionally, analysts at WSCF observed inconsistent TOX results among field sample replicates. Therefore, the WSCF lab performed an investigation of the TOX analysis to determine the cause of the outlier data points. Two causes were found that contributed to generating out-of-trend TOX data: (1) The presence of inorganic chloride in the groundwater samples: at inorganic chloride concentrations greater than about 10 parts per million (ppm), apparent TOX values increase with increasing chloride concentration. A parallel observation is the increase in apparent breakthrough of TOX from the first to the second activated-carbon adsorption tubes with increasing inorganic chloride concentration. (2) During the sample preparation step, excessive purging of the adsorption tubes with oxygen pressurization gas after sample loading may cause channeling in the activated carbon bed. This channeling leads to poor removal of inorganic chloride during the subsequent wash step with aqueous potassium nitrate. The presence of this residual inorganic chloride then produces erroneously high TOX values. Changes in sample preparation were studied to more effectively remove inorganic chloride from the activated-carbon adsorption tubes. With the TOX sample preparation equipment and TOX analyzers at WSCF, the nitrate wash recommended by EPA SW-846 method 9020B was found to be inadequate to remove inorganic chloride interference. Increasing the nitrate wash concentration from 10 grams per liter (g/L) to 100 giL potassium nitrate and increasing the nitrate wash volume from 3 milliliters (mL) to 10 mL effectively removed the inorganic chloride up to at least 100 ppm chloride in the sample matrix. Excessive purging of the adsorption tubes during sample preparation was eliminated. These changes in sample preparation have been incorporated in the analytical procedure. The results using the revised sample preparation procedure show better agreement of TOX values both for replicate analyses of single samples and for the analysis of replicate samples acquired from the same groundwater well. Furthermore, less apparent adsorption tube breakthrough now occurs with the revised procedure. One additional modification made to sample preparation was to discontinue the treatment of groundwater samples with sodium bisulfite. Sodium bisulfite is used to remove inorganic chlorine from the sample; inorganic chlorine is not expected to be a constituent in these groundwater samples. Several other factors were also investigated as possible sources of anomalous TOX results: (1) Instrument instability: examination of the history of results for TOX laboratory control samples and initial calibration verification standards indicate good long-term precision for the method and instrument. Determination of a method detection limit of 2.3 ppb in a deionized water matrix indicates the method and instrumentation have good stability and repeatability. (2) Non-linear instrument response: the instrument is shown to have good linear response from zero to 200 parts per billion (ppb) TOX. This concentration range encompasses the majority of samples received at WSCF for TOX analysis. Linear response was checked using both non-volatile TOX species (trichlorophenol) an

JG DOUGLAS; HK MEZNARICH, PHD; JR OLSEN; GA ROSS PHD; M STAUFFER

2009-02-13T23:59:59.000Z

84

Method for determining the octane rating of gasoline samples by observing corresponding acoustic resonances therein  

DOE Patents [OSTI]

A method is described for determining the octane rating of gasoline samples by observing corresponding acoustic resonances therein. A direct correlation between the octane rating of gasoline and the frequency of corresponding acoustic resonances therein has been experimentally observed. Therefore, the octane rating of a gasoline sample can be directly determined through speed of sound measurements instead of by the cumbersome process of quantifying the knocking quality of the gasoline. Various receptacle geometries and construction materials may be employed. Moreover, it is anticipated that the measurements can be performed on flowing samples in pipes, thereby rendering the present method useful in refineries and distilleries. 3 figs.

Sinha, D.N.; Anthony, B.W.

1997-02-25T23:59:59.000Z

85

Method for determining the octane rating of gasoline samples by observing corresponding acoustic resonances therein  

DOE Patents [OSTI]

A method for determining the octane rating of gasoline samples by observing corresponding acoustic resonances therein. A direct correlation between the octane rating of gasoline and the frequency of corresponding acoustic resonances therein has been experimentally observed. Therefore, the octane rating of a gasoline sample can be directly determined through speed of sound measurements instead of by the cumbersome process of quantifying the knocking quality of the gasoline. Various receptacle geometries and construction materials may be employed. Moreover, it is anticipated that the measurements can be performed on flowing samples in pipes, thereby rendering the present method useful in refineries and distilleries.

Sinha, Dipen N. (Los Alamos, NM); Anthony, Brian W. (Clearfield, PA)

1997-01-01T23:59:59.000Z

86

Systems and methods for laser assisted sample transfer to solution for chemical analysis  

SciTech Connect (OSTI)

Systems and methods are described for laser ablation of an analyte from a specimen and capturing of the analyte in a dispensed solvent to form a testing solution. A solvent dispensing and extraction system can form a liquid microjunction with the specimen. The solvent dispensing and extraction system can include a surface sampling probe. The laser beam can be directed through the surface sampling probe. The surface sampling probe can also serve as an atomic force microscopy probe. The surface sampling probe can form a seal with the specimen. The testing solution including the analyte can then be analyzed using an analytical instrument or undergo further processing.

Van Berkel, Gary J.; Kertesz, Vilmos; Ovchinnikova, Olga S.

2014-06-03T23:59:59.000Z

87

Systems and methods for laser assisted sample transfer to solution for chemical analysis  

DOE Patents [OSTI]

Systems and methods are described for laser ablation of an analyte from a specimen and capturing of the analyte in a dispensed solvent to form a testing solution. A solvent dispensing and extraction system can form a liquid microjunction with the specimen. The solvent dispensing and extraction system can include a surface sampling probe. The laser beam can be directed through the surface sampling probe. The surface sampling probe can also serve as an atomic force microscopy probe. The surface sampling probe can form a seal with the specimen. The testing solution including the analyte can then be analyzed using an analytical instrument or undergo further processing.

Van Berkel, Gary J; Kertesz, Vilmos; Ovchinnikova, Olga S

2013-08-27T23:59:59.000Z

88

Method for Operating a Sensor to Differentiate Between Analytes in a Sample  

DOE Patents [OSTI]

Disclosed is a method for operating a sensor to differentiate between first and second analytes in a sample. The method comprises the steps of determining a input profile for the sensor which will enhance the difference in the output profiles of the sensor as between the first analyte and the second analyte; determining a first analyte output profile as observed when the input profile is applied to the sensor; determining a second analyte output profile as observed when the temperature profile is applied to the sensor; introducing the sensor to the sample while applying the temperature profile to the sensor, thereby obtaining a sample output profile; and evaluating the sample output profile as against the first and second analyte output profiles to thereby determine which of the analytes is present in the sample.

Kunt, Tekin; Cavicchi, Richard E.; Semancik, Stephen; McAvoy, Thomas J.

1998-07-28T23:59:59.000Z

89

Comparison of vapor sampling system (VSS) and in situ vapor sampling (ISVS) methods on Tanks C-107, BY-108, and S-102  

SciTech Connect (OSTI)

The objective of this report is to evaluate the equivalency of two methods used to sample nonradioactive gases and vapors in the Hanford Site high-level waste tank headspaces. In addition to the comparison of the two sampling methods, the effects of an in-line fine particle filter on sampling results are also examined to determine whether results are adversely affected by its presence. This report discusses data from a January 1996 sampling.

Huckaby, J.L.; Edwards, J.A.; Evans, J.C. [and others

1996-05-01T23:59:59.000Z

90

RAPID METHOD FOR DETERMINATION OF {sup 228}Ra IN WATER SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of {sup 228}Ra in natural water samples has been developed at the SRNL/EBL (Savannah River National Lab/ Environmental Bioassay Laboratory) that can be used for emergency response or routine samples. While gamma spectrometry can be employed with sufficient detection limits to determine {sup 228}Ra in solid samples (via {sup 228}Ac) , radiochemical methods that employ gas flow proportional counting techniques typically provide lower MDA (Minimal Detectable Activity) levels for the determination of {sup 228}Ra in water samples. Most radiochemical methods for {sup 228}Ra collect and purify {sup 228}Ra and allow for {sup 228}Ac daughter ingrowth for ~36 hours. In this new SRNL/EBL approach, {sup 228}Ac is collected and purified from the water sample without waiting to eliminate this delay. The sample preparation requires only about 4 hours so that {sup 228}Ra assay results on water samples can be achieved in < 6 hours. The method uses a rapid calcium carbonate precipitation enhanced with a small amount of phosphate added to enhance chemical yields (typically >90%), followed by rapid cation exchange removal of calcium. Lead, bismuth, uranium, thorium and protactinium isotopes are also removed by the cation exchange separation. {sup 228}Ac is eluted from the cation resin directly onto a DGA Resin cartridge attached to the bottom of the cation column to purify {sup 228}Ac. DGA Resin also removes lead and bismuth isotopes, along with Sr isotopes and {sup 90}Y. La is used to determine {sup 228}Ac chemical yield via ICP-MS, but {sup 133}Ba can also be used instead if ICP-MS assay is not available. Unlike some older methods, no lead or strontium holdback carriers or continual readjustment of sample pH is required.

Maxwell, S.

2012-09-05T23:59:59.000Z

91

Multimodal nested sampling: an efficient and robust alternative to MCMC methods for astronomical data analysis  

E-Print Network [OSTI]

In performing a Bayesian analysis of astronomical data, two difficult problems often emerge. First, in estimating the parameters of some model for the data, the resulting posterior distribution may be multimodal or exhibit pronounced (curving) degeneracies, which can cause problems for traditional MCMC sampling methods. Second, in selecting between a set of competing models, calculation of the Bayesian evidence for each model is computationally expensive. The nested sampling method introduced by Skilling (2004), has greatly reduced the computational expense of calculating evidences and also produces posterior inferences as a by-product. This method has been applied successfully in cosmological applications by Mukherjee et al. (2006), but their implementation was efficient only for unimodal distributions without pronounced degeneracies. Shaw et al. (2007), recently introduced a clustered nested sampling method which is significantly more efficient in sampling from multimodal posteriors and also determines the expectation and variance of the final evidence from a single run of the algorithm, hence providing a further increase in efficiency. In this paper, we build on the work of Shaw et al. and present three new methods for sampling and evidence evaluation from distributions that may contain multiple modes and significant degeneracies; we also present an even more efficient technique for estimating the uncertainty on the evaluated evidence. These methods lead to a further substantial improvement in sampling efficiency and robustness, and are applied to toy problems to demonstrate the accuracy and economy of the evidence calculation and parameter estimation. Finally, we discuss the use of these methods in performing Bayesian object detection in astronomical datasets.

Farhan Feroz; M. P. Hobson

2007-07-23T23:59:59.000Z

92

Method for the concentration and separation of actinides from biological and environmental samples  

DOE Patents [OSTI]

A method and apparatus for the quantitative recover of actinide values from biological and environmental sample by passing appropriately prepared samples in a mineral acid solution through a separation column of a dialkyl(phenyl)-N,N-dialylcarbamoylmethylphosphine oxide dissolved in tri-n-butyl phosphate on an inert substrate which selectively extracts the actinide values. The actinide values can be eluted either as a group or individually and their presence quantitatively detected by alpha counting. 3 figs.

Horwitz, E.P.; Dietz, M.L.

1989-05-30T23:59:59.000Z

93

Apparatus and method for maintaining multi-component sample gas constituents in vapor phase during sample extraction and cooling  

DOE Patents [OSTI]

A dilution apparatus for diluting a gas sample. The apparatus includes a sample gas conduit having a sample gas inlet end and a diluted sample gas outlet end, and a sample gas flow restricting orifice disposed proximate the sample gas inlet end connected with the sample gas conduit and providing fluid communication between the exterior and the interior of the sample gas conduit. A diluted sample gas conduit is provided within the sample gas conduit having a mixing end with a mixing space inlet opening disposed proximate the sample gas inlet end, thereby forming an annular space between the sample gas conduit and the diluted sample gas conduit. The mixing end of the diluted sample gas conduit is disposed at a distance from the sample gas flow restricting orifice. A dilution gas source connected with the sample gas inlet end of the sample gas conduit is provided for introducing a dilution gas into the annular space, and a filter is provided for filtering the sample gas. The apparatus is particularly suited for diluting heated sample gases containing one or more condensable components.

Felix, Larry Gordon; Farthing, William Earl; Irvin, James Hodges; Snyder, Todd Robert

2010-05-11T23:59:59.000Z

94

Potential Effect of Climate Change on Design-Period Low Flows in the Mid-Atlantic Mary E. Schoen1  

E-Print Network [OSTI]

(TMDLs) of primary pollutants. Stepwise linear regression is used for predicting the future low change in low flow and the resulting change in TMDL of a point-source primary pollutant are estimated in precipitation and air temperature. For example, increases in air temperature may induce a shift in aquatic biota

95

Risk Assessment of Scramjet Unstart Using Adjoint-Based Sampling Methods  

E-Print Network [OSTI]

Risk Assessment of Scramjet Unstart Using Adjoint-Based Sampling Methods Qiqi Wang Massachusetts it to approximate the unstart probability of a supersonic combustion ramjet (scramjet) engine under changes for approximately 10 s in 2004. The X-43 waspoweredby asupersonic combustionramjet (scramjet) engine, in which air

Alonso, Juan J.

96

Risk Assessment of Scramjet Unstart Using Adjoint-Based Sampling Methods  

E-Print Network [OSTI]

Risk Assessment of Scramjet Unstart Using Adjoint-Based Sampling Methods Qiqi Wang Massachusetts in a SCRamjet engine under uncertain conditions that are characterized by various Gaussian and non (SCRamjet) engine, in which air at supersonic speed is mixed with hydrogen in the combustion chamber

Wang, Qiqi

97

Evaluation of surface sampling method performance for Bacillus Spores on clean and dirty outdoor surfaces.  

SciTech Connect (OSTI)

Recovery of Bacillus atrophaeous spores from grime-treated and clean surfaces was measured in a controlled chamber study to assess sampling method performance. Outdoor surfaces investigated by wipe and vacuum sampling methods included stainless steel, glass, marble and concrete. Bacillus atrophaeous spores were used as a surrogate for Bacillus anthracis spores in this study designed to assess whether grime-coated surfaces significantly affected surface sampling method performance when compared to clean surfaces. A series of chamber tests were carried out in which known amounts of spores were allowed to gravitationally settle onto both clean and dirty surfaces. Reference coupons were co-located with test coupons in all chamber experiments to provide a quantitative measure of initial surface concentrations of spores on all surfaces, thereby allowing sampling recovery calculations. Results from these tests, carried out under both low and high humidity conditions, show that spore recovery from grime-coated surfaces is the same as or better than spore recovery from clean surfaces. Statistically significant differences between method performance for grime-coated and clean surfaces were observed in only about half of the chamber tests conducted.

Wilson, Mollye C.; Einfeld, Wayne; Boucher, Raymond M.; Brown, Gary Stephen; Tezak, Matthew Stephen

2011-06-01T23:59:59.000Z

98

Characterization of Brazilian peat samples by applying a multi-method F. Girardelloa  

E-Print Network [OSTI]

1 Characterization of Brazilian peat samples by applying a multi-method approach F. Girardelloa , R Peat is a mixture of compounds formed by the decomposition of plant residues and mineral materials heterogeneity and natural variety, the physical and chemical properties of peat can vary widely within

Paris-Sud XI, Université de

99

The Balance-Sample Size Frontier in Matching Methods for Causal Inference  

E-Print Network [OSTI]

The Balance-Sample Size Frontier in Matching Methods for Causal Inference Gary King Christopher defining and showing how to calculate the matching frontier as the set of matching solutions with maximum solutions from the frontier for analysis in one step without iteration. The main difficulty in this strategy

100

The Balance-Sample Size Frontier in Matching Methods for Causal Inference1  

E-Print Network [OSTI]

The Balance-Sample Size Frontier in Matching Methods for Causal Inference1 Gary King2 Institute: easier & more powerful · Estimate the (n-imbalance) "matching frontier" 2 / 55 #12;Overview · Problem-hoc checks · Solution: easier & more powerful · Estimate the (n-imbalance) "matching frontier" · Imbalance

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

WATER-QUALITY CONDITIONS DURING LOW FLOW IN THE LOWER YOUGHIOGHENY RIVER BASIN, PENNSYLVANIA, OCTOBER 5-7, 1998  

SciTech Connect (OSTI)

In October 1998, a chemical synoptic survey was conducted by the U.S. Geological Survey, in cooperation with the U.S. Department of Energy, National Energy Technology Laboratory, in the Lower Youghiogheny River Basin in Pennsylvania to give a snap-shot of present (1998) water quality during low-flow conditions. Water samples from 38 sites--12 mainstem sites, 22 tributaries, and 4 mine discharges that discharge directly to the Youghiogheny River--were used to identify sources of contaminants from mining operations. Specific conductance, water temperature, pH, and dissolved oxygen were measured in the field at each site and concentrations of major ions and trace elements were measured in the laboratory. Unaccounted for gains and losses in streamflow were measured during the study. Unaccounted for losses in streamflow might be attributed to water loss through streambed fractures. Extensive mine tunnels are present in the basin and loss of water to these tunnels seems likely. Unaccounted for gains in streamflow may be from unmeasured tributaries or surface seeps, but most of the gains are suspected to come from artesian flow through fractures in the streambed from underground mine pools. Influent flows of rust-colored water were noted in some river sections. The pH values for all the samples collected during this survey were above 5.8, and most (33 of 38 samples) were above 7.0. Samples from the four mine-discharge sites also had pH values between 6.3 and 6.7. The lowest pH (5.8) was in a tributary, Galley Run. All 38 sampling sites had net alkalinity. The alkalinity load in the Youghiogheny River increased between Connellsville and McKeesport from 35 to 79 tons per day. Above Smithton, the measured alkalinity load in the Lower Youghiogheny River agreed well with the estimated alkalinity load. Below Smithton, measured alkalinity loads in the Lower Youghiogheny River are greater than calculated loads, resulting in unaccounted for gains in alkalinity. These gains are believed to be from seeps in the streambed. Approximately one-third of the load of total alkalinity in the Youghiogheny River at McKeesport is attributed to Sewickley Creek, which contributes 14 tons per day. Sulfate concentrations in the Youghiogheny River steadily increase from 33 milligrams per liter at Connellsville to 77 milligrams per liter near McKeesport. The measured concentrations of sulfate exceeded Pennsylvania water-quality standards at four tributary sites (Galley Run, Hickman Run, Sewickley Creek, and Gillespie Run) and all four mine-discharge sites but not at any main-stem sites. A large increase in sulfate load between West Newton and Sutersville can be attributed almost entirely to the contribution from Sewickley Creek (49 tons per day). Approximately 25 percent of the load measured between Connellsville and McKeesport is unaccounted for. These gains are believed to be from seeps in the streambed from underground mine pools. Similar patterns also were observed for loads of sodium, calcium, and magnesium. Unmeasured inputs from mine rainage are believed to be the source of these loads. Elevated concentrations (above background levels) of chemicals associated with drainage from coal-mining operations were measured in samples from tributaries, especially from Galley Run, Gillespie Run, and Sewickley Creek, and from the mine-discharge sites. The synoptic survey conducted for this study was successful in identifying generalized reaches of the Youghiogheny River where unaccounted for loads of constituents associated with mining activities are entering the river. However, the survey was not able to pinpoint the location of these loads. Remote-sensing techniques, such as thermal infrared imaging by the National Energy Technology Laboratory, could be useful for determining the precise locations of these inputs.

James I. Sams, III, Karl T. Schroeder; Terry E. Ackman; J. Kent Crawford; Kim L. Otto

2001-01-01T23:59:59.000Z

102

Simple method for highlighting the temperature distribution into a liquid sample heated by microwave power field  

SciTech Connect (OSTI)

Microwave induced heating is widely used in medical treatments, scientific and industrial applications. The temperature field inside a microwave heated sample is often inhomogenous, therefore multiple temperature sensors are required for an accurate result. Nowadays, non-contact (Infra Red thermography or microwave radiometry) or direct contact temperature measurement methods (expensive and sophisticated fiber optic temperature sensors transparent to microwave radiation) are mainly used. IR thermography gives only the surface temperature and can not be used for measuring temperature distributions in cross sections of a sample. In this paper we present a very simple experimental method for temperature distribution highlighting inside a cross section of a liquid sample, heated by a microwave radiation through a coaxial applicator. The method proposed is able to offer qualitative information about the heating distribution, using a temperature sensitive liquid crystal sheet. Inhomogeneities as smaller as 1°-2°C produced by the symmetry irregularities of the microwave applicator can be easily detected by visual inspection or by computer assisted color to temperature conversion. Therefore, the microwave applicator is tuned and verified with described method until the temperature inhomogeneities are solved.

Surducan, V.; Surducan, E.; Dadarlat, D. [National Institute for Research and Development of Isotopic and Molecular Technologies, 65-103 Donath Street, Cluj-Napoca (Romania)] [National Institute for Research and Development of Isotopic and Molecular Technologies, 65-103 Donath Street, Cluj-Napoca (Romania)

2013-11-13T23:59:59.000Z

103

RAPID METHOD FOR PLUTONIUM, AMERICIUM AND CURIUM IN VERY LARGE SOIL SAMPLES  

SciTech Connect (OSTI)

The analysis of actinides in environmental soil and sediment samples is very important for environmental monitoring. There is a need to measure actinide isotopes with very low detection limits. A new, rapid actinide separation method has been developed and implemented that allows the measurement of plutonium, americium and curium isotopes in very large soil samples (100-200 g) with high chemical recoveries and effective removal of matrix interferences. This method uses stacked TEVA Resin{reg_sign}, TRU Resin{reg_sign} and DGA-Resin{reg_sign} cartridges from Eichrom Technologies (Darien, IL, USA) that allows the rapid separation of plutonium (Pu), americium (Am), and curium (Cm) using a single multistage column combined with alpha spectrometry. The method combines an acid leach step and innovative matrix removal using cerium fluoride precipitation to remove the difficult soil matrix. This method is unique in that it provides high tracer recoveries and effective removal of interferences with small extraction chromatography columns instead of large ion exchange resin columns that generate large amounts of acid waste. By using vacuum box cartridge technology with rapid flow rates, sample preparation time is minimized.

Maxwell, S

2007-01-08T23:59:59.000Z

104

Survey of sampling-based methods for uncertainty and sensitivity analysis.  

SciTech Connect (OSTI)

Sampling-based methods for uncertainty and sensitivity analysis are reviewed. The following topics are considered: (1) Definition of probability distributions to characterize epistemic uncertainty in analysis inputs, (2) Generation of samples from uncertain analysis inputs, (3) Propagation of sampled inputs through an analysis, (4) Presentation of uncertainty analysis results, and (5) Determination of sensitivity analysis results. Special attention is given to the determination of sensitivity analysis results, with brief descriptions and illustrations given for the following procedures/techniques: examination of scatterplots, correlation analysis, regression analysis, partial correlation analysis, rank transformations, statistical tests for patterns based on gridding, entropy tests for patterns based on gridding, nonparametric regression analysis, squared rank differences/rank correlation coefficient test, two dimensional Kolmogorov-Smirnov test, tests for patterns based on distance measures, top down coefficient of concordance, and variance decomposition.

Johnson, Jay Dean; Helton, Jon Craig; Sallaberry, Cedric J. PhD. (.; .); Storlie, Curt B. (Colorado State University, Fort Collins, CO)

2006-06-01T23:59:59.000Z

105

System and method for laser assisted sample transfer to solution for chemical analysis  

DOE Patents [OSTI]

A system and method for laser desorption of an analyte from a specimen and capturing of the analyte in a suspended solvent to form a testing solution are described. The method can include providing a specimen supported by a desorption region of a specimen stage and desorbing an analyte from a target site of the specimen with a laser beam centered at a radiation wavelength (.lamda.). The desorption region is transparent to the radiation wavelength (.lamda.) and the sampling probe and a laser source emitting the laser beam are on opposite sides of a primary surface of the specimen stage. The system can also be arranged where the laser source and the sampling probe are on the same side of a primary surface of the specimen stage. The testing solution can then be analyzed using an analytical instrument or undergo further processing.

Van Berkel, Gary J; Kertesz, Vilmos

2014-01-28T23:59:59.000Z

106

Stochastic sampling method with MCNPX for nuclear data uncertainty propagation in criticality safety applications  

SciTech Connect (OSTI)

In the domain of criticality safety, the efficient propagation of uncertainty in nuclear data to uncertainty in k{sub eff} is an important area of current research. In this paper, a method based on stochastic sampling is presented for uncertainty propagation in MCNPX calculations. To that aim, the nuclear data (i.e. cross sections) are assumed to have a multivariate normal distribution and simple random sampling is performed following this presumed probability distribution. A verification of the developed stochastic sampling procedure with MCNPX is then conducted using the {sup 239}Pu Jezebel experiment as well as the PB-2 BWR and TMI-1 PWR pin cell models from the Uncertainty Analysis in Modeling (UAM) exercises. For the Jezebel case, it is found that the developed stochastic sampling approach predicts similar k{sub eff} uncertainties compared to conventional sensitivity and uncertainty methods. For the UAM models, slightly lower uncertainties are obtained when comparing to existing preliminary results. Further details of these verification studies are discussed and directions for future work are outlined. (authors)

Zhu, T.; Vasiliev, A.; Wieselquist, W.; Ferroukhi, H. [Paul Scherrer Institut, 5232 Villigen (Switzerland)

2012-07-01T23:59:59.000Z

107

A general few-projection method for tomographic reconstruction of samples consisting of several distinct materials  

SciTech Connect (OSTI)

We present a method for tomographic reconstruction of objects containing several distinct materials, which is capable of accurately reconstructing a sample from vastly fewer angular projections than required by conventional algorithms. The algorithm is more general than many previous discrete tomography methods, as: (i) a priori knowledge of the exact number of materials is not required; (ii) the linear attenuation coefficient of each constituent material may assume a small range of a priori unknown values. We present reconstructions from an experimental x-ray computed tomography scan of cortical bone acquired at the SPring-8 synchrotron.

Myers, Glenn R. [Department of Applied Mathematics, Australian National University, Canberra ACT 0200 (Australia); Thomas, C. David L.; Clement, John G. [Melbourne Dental School, University of Melbourne, Melbourne 3010 (Australia); Paganin, David M. [School of Physics, Monash University, Clayton 3800 (Australia); CSIRO Materials Science and Engineering, PB 33, Clayton South, 3169 (Australia); Gureyev, Timur E. [CSIRO Materials Science and Engineering, PB 33, Clayton South, 3169 (Australia)

2010-01-11T23:59:59.000Z

108

Surge Block Method for Controlling Well Clogging and Sampling Sediment during Bioremediation  

SciTech Connect (OSTI)

A surge block treatment method (i.e. inserting a solid rod plunger with a flat seal that closely fits the casing interior into a well and stocking it up and down) was performed for the rehabilitation of wells clogged with biomass and for the collection of time series sediment samples during in situ bioremediation tests for U(VI) immobilization at a the U.S. Department of Energy site in Oak Ridge, TN. The clogging caused by biomass growth had been controlled by using routine surge block treatment for18 times over a nearly four year test period. The treatment frequency was dependent of the dosage of electron donor injection and microbial community developed in the subsurface. Hydraulic tests showed that the apparent aquifer transmissivity at a clogged well with an inner diameter (ID) of 10.16 cm was increased by 8 13 times after the rehabilitation, indicating the effectiveness of the rehabilitation. Simultaneously with the rehabilitation, the surge block method was successfully used for collecting time series sediment samples composed of fine particles (clay and silt) from wells with ID 1.9 10.16 cm for the analysis of mineralogical and geochemical composition and microbial community during the same period. Our results demonstrated that the surge block method provided a cost-effective approach for both well rehabilitation and frequent solid sampling at the same location.

Wu, Wei-min [Stanford University] [Stanford University; Watson, David B [ORNL] [ORNL; Luo, Jian [Stanford University] [Stanford University; Carley, Jack M [ORNL] [ORNL; Mehlhorn, Tonia L [ORNL] [ORNL; Kitanidis, Peter K. [Stanford University] [Stanford University; Jardine, Philip [University of Tennessee, Knoxville (UTK)] [University of Tennessee, Knoxville (UTK); Criddle, Craig [Stanford University] [Stanford University

2013-01-01T23:59:59.000Z

109

Method and apparatus for automated processing and aliquoting of whole blood samples for analysis in a centrifugal fast analyzer  

DOE Patents [OSTI]

A rotor and disc assembly for use in a centrifugal fast analyzer. The assembly is designed to process multiple samples of whole blood followed by aliquoting of the resultant serum into precisely measured samples for subsequent chemical analysis. The assembly requires minimal operator involvement with no mechanical pipetting. The system comprises: (1) a whole blood sample disc; (2) a serum sample disc; (3) a sample preparation rotor; and (4) an analytical rotor. The blood sample disc and serum sample disc are designed with a plurality of precision bore capillary tubes arranged in a spoked array. Samples of blood are loaded into the blood sample disc by capillary action and centrifugally discharged into cavities of the sample preparation rotor where separation of serum and solids is accomplished. The serum is loaded into the capillaries of the serum sample disc by capillary action and subsequently centrifugally expelled into cuvettes of the analyticaly rotor for conventional methods. 5 figs.

Burtis, C.A.; Johnson, W.F.; Walker, W.A.

1985-08-05T23:59:59.000Z

110

Method Evaluation And Field Sample Measurements For The Rate Of Movement Of The Oxidation Front In Saltstone  

SciTech Connect (OSTI)

The objective of this work was to develop and evaluate a series of methods and validate their capability to measure differences in oxidized versus reduced saltstone. Validated methods were then applied to samples cured under field conditions to simulate Performance Assessment (PA) needs for the Saltstone Disposal Facility (SDF). Four analytical approaches were evaluated using laboratory-cured saltstone samples. These methods were X-ray absorption spectroscopy (XAS), diffuse reflectance spectroscopy (DRS), chemical redox indicators, and thin-section leaching methods. XAS and thin-section leaching methods were validated as viable methods for studying oxidation movement in saltstone. Each method used samples that were spiked with chromium (Cr) as a tracer for oxidation of the saltstone. The two methods were subsequently applied to field-cured samples containing chromium to characterize the oxidation state of chromium as a function of distance from the exposed air/cementitious material surface.

Almond, P. M. [Savannah River Site (SRS), Aiken, SC (United States); Kaplan, D. I. [Savannah River Site (SRS), Aiken, SC (United States); Langton, C. A. [Savannah River Site (SRS), Aiken, SC (United States); Stefanko, D. B. [Savannah River Site (SRS), Aiken, SC (United States); Spencer, W. A. [Savannah River Site (SRS), Aiken, SC (United States); Hatfield, A. [Clemson University, Clemson, SC (United States); Arai, Y. [Clemson University, Clemson, SC (United States)

2012-08-23T23:59:59.000Z

111

Sampling, preservation, and analytical methods research plan - liquid redox sulfur recovery technologies: Stretford process. Topical report  

SciTech Connect (OSTI)

GRI has developed a sampling, preservation, and analytical (SPandA) methods research plan for developing and validating analytical methodologies for liquid redox sulfur recovery processes (e.g., Stretford process). The document describes the technical approach which will be used to direct research activities to develop SPandA methodologies to analyze gaseous, aqueous, and solid process streams from the Stretford sulfur recovery process. The primary emphasis is on developing and validating methodologies for analyzing vanadium (IV) and vanadium (V), anthraquinone disulphonic acids (ADA), polysulfide-sulfur, sulfide-sulfur, thiosulfate, sulfate, thiocyanate, total soluble sulfur, alkalinity, pH, total dissolved solids, total suspended solids, and dissolved oxygen in aqueous process streams. The document includes descriptions of the process streams and chemical species, selection of candidate analytical methods, and technical approach for methods development and validation.

Trofe, T.W.

1986-11-01T23:59:59.000Z

112

Uncertainties in Air Exchange using Continuous-Injection, Long-Term Sampling Tracer-Gas Methods  

SciTech Connect (OSTI)

The PerFluorocarbon Tracer (PFT) method is a low-cost approach commonly used for measuring air exchange in buildings using tracer gases. It is a specific application of the more general Continuous-Injection, Long-Term Sampling (CILTS) method. The technique is widely used but there has been little work on understanding the uncertainties (both precision and bias) associated with its use, particularly given that it is typically deployed by untrained or lightly trained people to minimize experimental costs. In this article we will conduct a first-principles error analysis to estimate the uncertainties and then compare that analysis to CILTS measurements that were over-sampled, through the use of multiple tracers and emitter and sampler distribution patterns, in three houses. We find that the CILTS method can have an overall uncertainty of 10-15percent in ideal circumstances, but that even in highly controlled field experiments done by trained experimenters expected uncertainties are about 20percent. In addition, there are many field conditions (such as open windows) where CILTS is not likely to provide any quantitative data. Even avoiding the worst situations of assumption violations CILTS should be considered as having a something like a ?factor of two? uncertainty for the broad field trials that it is typically used in. We provide guidance on how to deploy CILTS and design the experiment to minimize uncertainties.

Sherman, Max H.; Walker, Iain S.; Lunden, Melissa M.

2013-12-01T23:59:59.000Z

113

A quantitative method to detect explosives and selected semivolatiles in soil samples by Fourier transform infrared spectroscopy  

SciTech Connect (OSTI)

This paper describes a novel Fourier transform infrared (FTIR) spectroscopic method that can be used to rapidly screen soil samples from potentially hazardous waste sites. Samples are heated in a thermal desorption unit and the resultant vapors are collected and analyzed in a long-path gas cell mounted in a FTIR. Laboratory analysis of a soil sample by FTIR takes approximately 10 minutes. This method has been developed to identify and quantify microgram concentrations of explosives in soil samples and is directly applicable to the detection of selected volatile organics, semivolatile organics, and pesticides.

Clapper-Gowdy, M.; Dermirgian, J. [Argonne National Lab., IL (United States); Robitaille, G. [Army Environmental Center, Aberdeen Proving Ground, MD (United States)

1995-06-01T23:59:59.000Z

114

Method and apparatus for maintaining multi-component sample gas constituents in vapor phase during sample extraction and cooling  

DOE Patents [OSTI]

An apparatus and method for diluting and cooling that is extracted from high temperature and/or high pressure industrial processes. Through a feedback process, a specialized, CFD-modeled dilution cooler is employed along with real-time estimations of the point at which condensation will occur within the dilution cooler to define a level of dilution and diluted gas temperature that results in a gas that can be conveyed to standard gas analyzers that contains no condensed hydrocarbon compounds or condensed moisture.

Farthing, William Earl (Pinson, AL) [Pinson, AL; Felix, Larry Gordon (Pelham, AL) [Pelham, AL; Snyder, Todd Robert (Birmingham, AL) [Birmingham, AL

2008-02-12T23:59:59.000Z

115

Method and apparatus maintaining multi-component sample gas constituents in vapor phase during sample extraction and cooling  

DOE Patents [OSTI]

An apparatus and method for diluting and cooling that is extracted from high temperature and/or high pressure industrial processes. Through a feedback process, a specialized, CFD-modeled dilution cooler is employed along with real-time estimations of the point at which condensation will occur within the dilution cooler to define a level of dilution and diluted gas temperature that results in a gas that can be conveyed to standard gas analyzers that contains no condensed hydrocarbon compounds or condensed moisture.

Farthing, William Earl (Pinson, AL); Felix, Larry Gordon (Pelham, AL); Snyder, Todd Robert (Birmingham, AL)

2009-12-15T23:59:59.000Z

116

Mixed convection and high-pressure low-flow steam cooling data from a 64-rod bundle  

SciTech Connect (OSTI)

Heat transfer data were obtained from low flow steam cooling experiments in a partially uncovered 64-rod bundle. These tests indicated that free convection effects were superimposed on the laminar and turbulent forced convection heat transfer. This paper describes the influence of buoyancy on laminar and turbulent forced convection heat transfer coefficients. Mechanisms due to buoyancy which alter the local heat transfer are summarized. Criteria indicating the importance of buoyancy on laminar and turbulent upflow in a vertical pipe were developed and compared to other criteria found in the literature. These criteria were used to determine the steam cooling data with significant buoyancy influence. Data with buoyancy influence were compared to mixed convection correlations and to a numerical study for rod bundles.

Sozer, A.

1984-01-01T23:59:59.000Z

117

Flow through in situ reactors with suction lysimeter sampling capability and methods of using  

DOE Patents [OSTI]

An in situ reactor for use in a geological strata includes a liner defining a centrally disposed passageway and a sampling conduit received within the passageway. The sampling conduit may be used to receive a geological speciment derived from geological strata therein and a lysimeter is disposed within the sampling conduit in communication with the geological specimen. Fluid may be added to the geological specimen through the passageway defined by the liner, between an inside surface of the liner and an outside surface of the sampling conduit. A distal portion of the sampling conduit may be in fluid communication with the passageway.

Radtke, Corey W. (Idaho Falls, ID) [Idaho Falls, ID; Blackwelder, D. Brad (Blackfoot, ID) [Blackfoot, ID; Hubbell, Joel M. (Idaho Falls, ID) [Idaho Falls, ID

2009-11-17T23:59:59.000Z

118

A comb-sampling method for enhanced mass analysis in linear electrostatic ion traps  

SciTech Connect (OSTI)

In this paper an algorithm for extracting spectral information from signals containing a series of narrow periodic impulses is presented. Such signals can typically be acquired by pickup detectors from the image-charge of ion bunches oscillating in a linear electrostatic ion trap, where frequency analysis provides a scheme for high-resolution mass spectrometry. To provide an improved technique for such frequency analysis, we introduce the CHIMERA algorithm (Comb-sampling for High-resolution IMpulse-train frequency ExtRAaction). This algorithm utilizes a comb function to generate frequency coefficients, rather than using sinusoids via a Fourier transform, since the comb provides a superior match to the data. This new technique is developed theoretically, applied to synthetic data, and then used to perform high resolution mass spectrometry on real data from an ion trap. If the ions are generated at a localized point in time and space, and the data is simultaneously acquired with multiple pickup rings, the method is shown to be a significant improvement on Fourier analysis. The mass spectra generated typically have an order of magnitude higher resolution compared with that obtained from fundamental Fourier frequencies, and are absent of large contributions from harmonic frequency components.

Greenwood, J. B.; Kelly, O.; Calvert, C. R.; Duffy, M. J.; King, R. B.; Belshaw, L.; Graham, L.; Alexander, J. D.; Williams, I. D. [Centre for Plasma Physics, School of Mathematics and Physics, Queen's University Belfast, Belfast BT7 1NN (United Kingdom); Bryan, W. A. [Department of Physics, Swansea University, Swansea SA2 8PP (United Kingdom); Turcu, I. C. E.; Cacho, C. M.; Springate, E. [Central Laser Facility, STFC Rutherford Appleton Laboratory, Didcot, Oxfordshire OX11 0QX (United Kingdom)

2011-04-15T23:59:59.000Z

119

Tensiometer, drive probe for use with environmental testing equipment, and methods of inserting environmental testing equipment into a sample  

DOE Patents [OSTI]

A method of inserting a tensiometer into a sample, comprises providing a drive probe configured to be engaged by direct push equipment; supporting a porous member from the drive probe; and driving the drive probe into the sample using a cone penetrometer. A tensiometer comprises a drive probe configured to be engaged by direct push equipment or a cone penetrometer; a porous member supported by the drive probe; and a pressure sensor in pressure sensing relation to the porous member.

Hubbell, Joel M.; Sisson, James B.

2005-07-26T23:59:59.000Z

120

E-Print Network 3.0 - assay elisa method Sample Search Results  

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Biology and Medicine 11 An enzyme-linked immunosorbent assay for the determination of dioxins in contaminated sediment and soil samples Summary: -microwell enzyme-linked...

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121

E-Print Network 3.0 - arsine evolution methods Sample Search...  

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and Methods Subjects. Subjects were residents of six counties in western Nevada and Kings County... of Human Subjects. Laboratory Methods. The urinary concentrations were...

122

E-Print Network 3.0 - acceleration measurement method Sample...  

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method Page: << < 1 2 3 4 5 > >> 1 HybridOS: Runtime Support for Reconfigurable Accelerators Summary: and evaluated four methods for accessing the data buffers required by...

123

E-Print Network 3.0 - algorithm based method Sample Search Results  

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search results for: algorithm based method Page: << < 1 2 3 4 5 > >> 1 NUMERICAL OPTIMIZATION MAD 5420-02 Summary: method and algorithm Quadratic fit-polynomial interpolation...

124

E-Print Network 3.0 - analysis methods applied Sample Search...  

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Summary: Methods in Applied Sciences and Engineering (ECCOMAS 2008) June 30 -July 5, 2008 Venice, Italy Manifold... -mail: marino.arroyo@upc.edu Key Words: meshfree methods,...

125

E-Print Network 3.0 - analysis method applied Sample Search Results  

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Summary: Methods in Applied Sciences and Engineering (ECCOMAS 2008) June 30 -July 5, 2008 Venice, Italy Manifold... -mail: marino.arroyo@upc.edu Key Words: meshfree methods,...

126

E-Print Network 3.0 - augmented wave method Sample Search Results  

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turbulent velocities The method to calculate wave energy fluxes carried by longitudinal tube... frequency points n. Another computational parameter, which affects our method of...

127

E-Print Network 3.0 - astm test method Sample Search Results  

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Biodiesel Standards and Testing Methods Alternative Fuels Consortium... Biodiesel production review Key elements in ASTM Specifications and Standard Test Methods ASTM......

128

E-Print Network 3.0 - assay characterization methods Sample Search...  

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partners and the method that yields a suitable signal window and background. Assay design... detection assays, both methods being used for quantitation of second messenger...

129

Uncertainties in Air Exchange using Continuous-Injection, Long-Term Sampling Tracer-Gas Methods  

E-Print Network [OSTI]

Pollutant Control Index: A New Method of Characterizing Ventilation in Commercial Buildings." Proceedings of Indoor Air'

Sherman, Max H.

2014-01-01T23:59:59.000Z

130

METHODS FOR DETERMINING AGITATOR MIXING REQUIREMENTS FOR A MIXING & SAMPLING FACILITY TO FEED WTP (WASTE TREATMENT PLANT)  

SciTech Connect (OSTI)

The following report is a summary of work conducted to evaluate the ability of existing correlative techniques and alternative methods to accurately estimate impeller speed and power requirements for mechanical mixers proposed for use in a mixing and sampling facility (MSF). The proposed facility would accept high level waste sludges from Hanford double-shell tanks and feed uniformly mixed high level waste to the Waste Treatment Plant. Numerous methods are evaluated and discussed, and resulting recommendations provided.

GRIFFIN PW

2009-08-27T23:59:59.000Z

131

VERIFICATION OF THE DEFENSE WASTE PROCESSING FACILITY'S (DWPF) PROCESS DIGESTION METHOD FOR THE SLUDGE BATCH 7A QUALIFICATION SAMPLE  

SciTech Connect (OSTI)

For each sludge batch that is processed in the Defense Waste Processing Facility (DWPF), the Savannah River National Laboratory (SRNL) performs confirmation of the applicability of the digestion method to be used by the DWPF lab for elemental analysis of Sludge Receipt and Adjustment Tank (SRAT) receipt samples and SRAT product process control samples. DWPF SRAT samples are typically dissolved using a room temperature HF-HNO{sub 3} acid dissolution (i.e., DWPF Cold Chem Method, see DWPF Procedure SW4-15.201) and then analyzed by inductively coupled plasma - atomic emission spectroscopy (ICP-AES). This report contains the results and comparison of data generated from performing the Aqua Regia (AR), Sodium peroxide/Hydroxide Fusion (PF) and DWPF Cold Chem (CC) method digestions of Sludge Batch 7a (SB7a) SRAT Receipt and SB7a SRAT Product samples. The SB7a SRAT Receipt and SB7a SRAT Product samples were prepared in the SRNL Shielded Cells, and the SRAT Receipt material is representative of the sludge that constituates the SB7a Batch or qualification composition. This is the sludge in Tank 51 that is to be transferred into Tank 40, which will contain the heel of Sludge Batch 6 (SB6), to form the Sb7a Blend composition.

Click, D.; Edwards, T.; Jones, M.; Wiedenman, B.

2011-03-14T23:59:59.000Z

132

Low flow fume hood  

DOE Patents [OSTI]

A fume hood is provided having an adequate level of safety while reducing the amount of air exhausted from the hood. A displacement flow fume hood works on the principal of a displacement flow which displaces the volume currently present in the hood using a push-pull system. The displacement flow includes a plurality of air supplies which provide fresh air, preferably having laminar flow, to the fume hood. The displacement flow fume hood also includes an air exhaust which pulls air from the work chamber in a minimally turbulent manner. As the displacement flow produces a substantially consistent and minimally turbulent flow in the hood, inconsistent flow patterns associated with contaminant escape from the hood are minimized. The displacement flow fume hood largely reduces the need to exhaust large amounts of air from the hood. It has been shown that exhaust air flow reductions of up to 70% are possible without a decrease in the hood's containment performance. The fume hood also includes a number of structural adaptations which facilitate consistent and minimally turbulent flow within a fume hood.

Bell, Geoffrey C. (Pleasant Hill, CA); Feustel, Helmut E. (Albany, CA); Dickerhoff, Darryl J. (Berkeley, CA)

2002-01-01T23:59:59.000Z

133

E-Print Network 3.0 - advanced control methods Sample Search...  

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network is largely deter- mined by its flow-control: the method used... -the-fly scheduling of existing flow-control methods idles each buffer for a considerable period...

134

E-Print Network 3.0 - automatic spectrophotometric method Sample...  

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Each Summary: to ATP synthesis, can be spectrophotometrically monitored by electrochromic absorption transients... . MATERIALS AND METHODS Cell growth and chromatophore...

135

E-Print Network 3.0 - analytical detection methods Sample Search...  

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materials, and data qualification reporting guidelines. Method detection limits... procedures, and NOAA's Analytical Quality Assurance Project Plan (QAPP). ... Source: NOAA...

136

Recession-based hydrological models for estimating low flows in ungauged catchments in the Himalayas Hydrology and Earth System Sciences, 8(5), 891902 (2004) EGU  

E-Print Network [OSTI]

Recession-based hydrological models for estimating low flows in ungauged catchments in the Himalayas 891 Hydrology and Earth System Sciences, 8(5), 891902 (2004) © EGU Recession-based hydrological.R. Young1 and S.R. Kansakar2 1 Centre for Ecology and Hydrology,Wallingford, Oxfordshire, OX10 8BB, UK 2

Paris-Sud XI, Université de

137

An optimized Line Sampling method for the estimation of the failure probability of nuclear passive systems  

E-Print Network [OSTI]

The quantitative reliability assessment of a thermal-hydraulic (T-H) passive safety system of a nuclear power plant) to operate [5] and, thus, are expected to improve the safety of nuclear power plants because of simplicity long) T-H code simulations that must be performed (one for each sample) for the statistical estimation

Paris-Sud XI, Université de

138

Methods to sample air borne propagules of Aspergillus flavus C.H. Bock1,2,  

E-Print Network [OSTI]

dispersal, spore sampling Abstract Three techniques (cyclone samplers, filter samplers and rotorods) were. Analysis of variance indicated no significant difference between cyclone and filter samplers in quantity of colony forming units caught, but there was a positive correlation between catches of the three separate

Cotty, Peter J.

139

E-Print Network 3.0 - approximate solution method Sample Search...  

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numerical solution of partial differential... , Meshfree Approximation Methods with Matlab, Lecture Notes, IIT, 2005. Other required material... data approximation with radial...

140

E-Print Network 3.0 - artifact reduction methods Sample Search...  

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Technologies and Information Sciences 11 Artifact-based functional comparison of software Rodion M. Podorozhny Summary: and artifacts in their method were classi- fied...

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141

E-Print Network 3.0 - analysis methods today Sample Search Results  

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system Metadata management Context-sensitive warnings Methods to select best sources Spatial... : today's approaches Ethics-related issue 12;Analysis Design Development...

142

E-Print Network 3.0 - argon method Sample Search Results  

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39.95 AMU Synonyms Argon-40 * Argon (ACGIH... -contained breathing apparatus, rubber boots, and heavy rubber gloves. METHODS ... Source: Choi, Kyu Yong - Department of Chemical...

143

E-Print Network 3.0 - accelerated numerical method Sample Search...  

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and Information Sciences 2 HybridOS: Runtime Support for Reconfigurable Accelerators Summary: and evaluated four methods for accessing the data buffers required by...

144

E-Print Network 3.0 - alternative screening method Sample Search...  

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results for: alternative screening method Page: << < 1 2 3 4 5 > >> 1 SIGGRAPH'95 Computer Graphics Proceedings, Annual Conference Series, 1995 Artistic Screening Summary:...

145

E-Print Network 3.0 - analog equation method Sample Search Results  

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times each method was observed, out of the 31 significant analogies... attempted to teach electricity concepts using ... Source: Podolefsky, Noah - Physics Education Research...

146

E-Print Network 3.0 - adaptive methods final Sample Search Results  

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mechanisms. Finally the actors in the process of adaptation will be discussed like the user (adaptable... adaptation methods and tools that are under the control of the user...

147

E-Print Network 3.0 - atom re-evaporation method Sample Search...  

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method Page: << < 1 2 3 4 5 > >> 1 Atomic flux measurement by diode-laser-based atomic absorption spectroscopy Summary: in the absorp- tion profile indicates that barium...

148

E-Print Network 3.0 - arc discharge method Sample Search Results  

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Engineering ; Materials Science 22 Time displacement for a wall-stabilized electric arc in a transverse magnetic field. Summary: -Barrado 7). The simplest method of...

149

E-Print Network 3.0 - air agglomeration method Sample Search...  

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and Nanomedicine Collection: Biology and Medicine 67 Computational Modeling and Optimization of Proton Exchange Membrane Fuel Cells Summary: element method in order to...

150

E-Print Network 3.0 - approximate reasoning methods Sample Search...  

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order... subdomain boundaries is achieved. One such method in this class, the ... Source: Sola, Rolf Haenni - Institut fr Informatik und angewandte Mathematik, Universitt Bern...

151

E-Print Network 3.0 - antigen method histochemical Sample Search...  

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detecting antigen... of immunocytochemical methods for detecting changes in ... Source: Brand, Paul H. - Department of Physiology and Pharmacology, University of Toledo...

152

E-Print Network 3.0 - anatomical landmark method Sample Search...  

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method Page: << < 1 2 3 4 5 > >> 1 Automatic Landmark Tracking and the Optimization of Brain Conformal Mapping Summary: . Objective: Important anatomical features on the cortical...

153

E-Print Network 3.0 - absorption gra method Sample Search Results  

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Resources 5 High Excitation Transfer Efficiency from Energy Relay Dyes in Dye-Sensitized Solar Cells Summary: with higher light absorption, this method cannot be used because the...

154

E-Print Network 3.0 - automatable method extract Sample Search...  

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on Candidate Data for Collocation Extraction Stefan Evert and Hannah Kermes Summary: .de Abstract The paper describes ongoing work on the evaluation of methods for extract- ing...

155

E-Print Network 3.0 - arc plasma method Sample Search Results  

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Arc System Summary: of the most promising directions. The method of plasma pyrolysis and gasification, where at waste processing... -6. High-current electric arcs or electric arc...

156

E-Print Network 3.0 - alternative processing methods Sample Search...  

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various tasks. Because multiple-methods often exist to perform tasks, we can... -First-Search-at-Corel-Using Advanced-Text-Processing sum() max() enables Subtask Relation...

157

E-Print Network 3.0 - adaptive control method Sample Search Results  

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-4. These methods include intelligent control, neural control, adaptive fuzzy control, memory-based control... introduction to the book. A brief discussion on the problem...

158

E-Print Network 3.0 - administration methods based Sample Search...  

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of Medicinal Chemistry, University of Kansas Collection: Chemistry 3 ERNEST ORLANDO LAWRENCE BERKELEY NATIONAL LABORATORY Summary: the methods and assumptions used by...

159

E-Print Network 3.0 - abmr method Sample Search Results  

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de mathmatiques Collection: Mathematics 42 Metastable D-State Spectroscopy Laser Cooling of Barium Summary: other than EDMs . . . . . . . . . . 19 2.4 Experimental Methods...

160

E-Print Network 3.0 - algebraic multigrid methods Sample Search...  

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a multigrid method with fixed-data resolution. Index Terms--Computed tomography, emission tomography, image... restoration 10-15, and image reconstruction 16-22, 13,...

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161

A comparison of diagnostic techniques for detecting salmonella spp in equine fecal samples using culture methods, gel-based pcr, and real-time pcr assays  

E-Print Network [OSTI]

for improved diagnostic methods for detecting Salmonella in equine fecal samples. 120 fecal samples submitted to the Clinical Microbiology Laboratory of the Veterinary Medical Teaching Hospital at Texas A&M University (CML, VMTH, TAMU) were tested...

Smith, Shelle Ann

2007-09-17T23:59:59.000Z

162

E-Print Network 3.0 - agent-based modeling methods Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

and Information Sciences ; Biology and Medicine 5 Tutorial on agent-based modelling and simulation CM Macal1,2 Summary: of disciplines (Section 3), and identify methods and...

163

E-Print Network 3.0 - advanced methods properties Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

EXCELLENTIA CoLumbIA ENgINEErINg290 Summary: on the nanoscale--one-billionth of a meter. Aron Pinczuk's research projects employ advanced optics methods... --be they...

164

E-Print Network 3.0 - analysis method sam Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

he wouldn't have Summary: applications, the methods are very similar." Sam is also a Political Management graduate student at George... S amuel Nitz (B.S. 2004) says he wouldn't...

165

E-Print Network 3.0 - analysis methods volume Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Volume 12, Issue 1, pp. 29-37. N. Uno, F. Kurauchi, H. Tamura, et al., Using Bus Probe Data for Analysis... . Charpillet, A Road Matching Method for Precise Vehicle Localization...

166

E-Print Network 3.0 - angular gammagamma-correlation method Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

gammagamma-correlation method Page: << < 1 2 3 4 5 > >> 1 TUDE DE QUELQUES SPECTRES GAMMA DE NIVEAUX EXCITS DES NOYAUX LGERS Par MM. S. GORODETZKY, TH. MULLER et M. PORT, ....

167

Development of Analytical Methods Coupled to Microdialysis Sampling for Studying Biomarkers of Oxidative Stress  

E-Print Network [OSTI]

generation would increase in biological systems due to induced oxidative stress. In one investigation, a capillary electrophoresis (CE) method with ultra-violet (UV) detection was developed employing pH-mediated stacking, an on-column preconcentration...

Hoque, Md Ehsanul

2007-12-18T23:59:59.000Z

168

E-Print Network 3.0 - axis factoring method Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Once this is done, we can call the setup method to properly initialize the axis... On: color values start end moveBy scaleFactor minValue maxValue AbstractAxis AxisAxisDecorator...

169

E-Print Network 3.0 - assessment methods vi Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

porous media. Materials and Methods Experimental... Effects of Solid-to-Solution Ratio on Uranium(VI) Adsorption and Its Implications T A O C H E N G... , Wisconsin 53706 U(VI)...

170

Verification Of The Defense Waste Processing Facility's (DWPF) Process Digestion Methods For The Sludge Batch 8 Qualification Sample  

SciTech Connect (OSTI)

This report contains the results and comparison of data generated from inductively coupled plasma – atomic emission spectroscopy (ICP-AES) analysis of Aqua Regia (AR), Sodium Peroxide/Sodium Hydroxide Fusion Dissolution (PF) and Cold Chem (CC) method digestions and Cold Vapor Atomic Absorption analysis of Hg digestions from the DWPF Hg digestion method of Sludge Batch 8 (SB8) Sludge Receipt and Adjustment Tank (SRAT) Receipt and SB8 SRAT Product samples. The SB8 SRAT Receipt and SB8 SRAT Product samples were prepared in the SRNL Shielded Cells, and the SRAT Receipt material is representative of the sludge that constitutes the SB8 Batch or qualification composition. This is the sludge in Tank 51 that is to be transferred into Tank 40, which will contain the heel of Sludge Batch 7b (SB7b), to form the SB8 Blend composition.

Click, D. R.; Edwards, T. B.; Wiedenman, B. J.; Brown, L. W.

2013-03-18T23:59:59.000Z

171

Passive sampling for the monitoring of organic pollutants (PAHs, BTEX) in groundwater. Application to a former  

E-Print Network [OSTI]

Passive sampling for the monitoring of organic pollutants (PAHs, BTEX) in groundwater. Application techniques for groundwater sampling can affect the measurement of chemical composition of water. Sampling devices such as low-flow peristaltic pumps can sample water slowly from wells to obtain representative

Boyer, Edmond

172

A new 'Implicit correlation' method for cross-correlation sampling in MCNPX-PoliMi  

SciTech Connect (OSTI)

Monte Carlo particle transport codes used to accurately model detector response are traditionally run in fully analog mode. Analog simulations of cross-correlation measurements with these codes are extremely time-consuming because the probability of correlated detection is extremely small, approximately equal to the product of the probabilities of a single detection in each detector. The new 'implicit correlation' method described here increases the number of correlation event scores thereby reducing variance and required computation times. The cost of the implicit correlation method is comparable to the cost of simulating single event detection for the lowest absolute detector efficiency in the problem. This method is especially useful in the nuclear non-proliferation and safeguards fields for simulating correlation measurements of shielded special nuclear material. The new method was implemented in MCNPX-PoliMi for neutron-neutron cross-correlations with a Cf-252 spontaneous fission source measured by two detectors of variable stand-offs. The method demonstrated good agreement with analog simulation results for multiple measurement geometries. Small differences between non-analog and analog cross-correlation distributions are attributed to known features of the specific problem simulated that will not be present in practical applications. (authors)

Marcath, M. J.; Larsen, E. W.; Clarke, S. D.; Pozzi, S. A. [Department of Nuclear Engineering and Radiological Sciences, University of Michigan, 2355 Bonisteel Boulevard, Ann Arbor, MI, 48109-2104 (United States)

2013-07-01T23:59:59.000Z

173

Test Method Determination of sample size for step-wise transient thermal tests  

E-Print Network [OSTI]

and thermal diffusivity of materials simultaneously. Owing to its heating mode, the step-wise transient method 95616, USA a r t i c l e i n f o Article history: Received 13 November 2008 Accepted 6 January 2009.elsevier.com/locate/polytest ARTICLE

Pan, Ning

174

Method for measuring the rate of cell reproduction by analysis of nanoliter cell samples  

DOE Patents [OSTI]

A method of detecting cancer using a laser biocavity having a semiconductor laser including a microchannel through which cells in fluid traverse, comprising determining the laser wavelength of the laser biocavity with only fluid in the microchannel; determining the wavelength shift of the biocavity when each cell passes through the microchannel; and determining the percentage of cells in G2 phase from the wavelength shift of the cells; wherein an increased percentage of G2 phase cells is an indication of cancer.

Gourley, Paul L.

2005-04-26T23:59:59.000Z

175

Methods for preparing comparative standards and field samples for neutron activation analysis of soil  

SciTech Connect (OSTI)

One of the more difficult problems associated with comparative neutron activation analysis (CNAA) is the preparation of standards which are tailor-made to the desired irradiation and counting conditions. Frequently, there simply is not a suitable standard available commercially, or the resulting gamma spectrum is convoluted with interferences. In a recent soil analysis project, the need arose for standards which contained about 35 elements. In response, a computer spreadsheet was developed to calculate the appropriate amount of each element so that the resulting gamma spectrum is relatively free of interferences. Incorporated in the program are options for calculating all of the irradiation and counting parameters including activity produced, necessary flux/bombardment time, counting time, and appropriate source-to-detector distance. The result is multi-element standards for CNAA which have optimal concentrations. The program retains ease of use without sacrificing capability. In addition to optimized standard production, a novel soil homogenization technique was developed which is a low cost, highly efficient alternative to commercially available homogenization systems. Comparative neutron activation analysis for large scale projects has been made easier through these advancements. This paper contains details of the design and function of the NAA spreadsheet and innovative sample handling techniques.

Glasgow, D.C.; Dyer, F.F.; Robinson, L.

1994-06-01T23:59:59.000Z

176

System and method for measuring particles in a sample stream of a flow cytometer or the like  

DOE Patents [OSTI]

A system and method for analyzing a particle in a sample stream of a flow cytometer or the like. The system has a light source, such as a laser pointer module, for generating a low powered light beam and a fluidics apparatus which is configured to transport particles in the sample stream at substantially low velocity through the light beam for interrogation. Detectors, such as photomultiplier tubes, are configured to detect optical signals generated in response to the light beam impinging the particles. Signal conditioning circuitry is connected to each of the detectors to condition each detector output into electronic signals for processing and is designed to have a limited frequency response to filter high frequency noise from the detector output signals.

Graves, Steven W. (San Juan Pueblo, NM); Habberset, Robert C. (Santa Fe, NM)

2010-11-16T23:59:59.000Z

177

System and method for measuring particles in a sample stream of a flow cytometer using a low power laser source  

DOE Patents [OSTI]

A system and method for analyzing a particle in a sample stream of a flow cytometer or the like. The system has a light source, such as a laser pointer module, for generating a low powered light beam and a fluidics apparatus which is configured to transport particles in the sample stream at substantially low velocity through the light beam for interrogation. Detectors, such as photomultiplier tubes, are configured to detect optical signals generated in response to the light beam impinging the particles. Signal conditioning circuitry is connected to each of the detectors to condition each detector output into electronic signals for processing and is designed to have a limited frequency response to filter high frequency noise from the detector output signals.

Graves, Steven W; Habbersett, Robert C

2013-10-22T23:59:59.000Z

178

System and method for measuring particles in a sample stream of a flow cytometer using low-power laser source  

DOE Patents [OSTI]

A system and method for analyzing a particle in a sample stream of a flow cytometer or the like. The system has a light source, such as a laser pointer module, for generating a low powered light beam and a fluidics apparatus which is configured to transport particles in the sample stream at substantially low velocity through the light beam for interrogation. Detectors, such as photomultiplier tubes, are configured to detect optical signals generated in response to the light beam impinging the particles. Signal conditioning circuitry is connected to each of the detectors to condition each detector output into electronic signals for processing and is designed to have a limited frequency response to filter high frequency noise from the detector output signals.

Graves, Steven W.; Habbersett, Robert C.

2014-07-01T23:59:59.000Z

179

Method and system for selecting data sampling phase for self timed interface logic  

DOE Patents [OSTI]

An exemplary embodiment of the present invention is a method for transmitting data among processors over a plurality of parallel data lines and a clock signal line. A receiver processor receives both data and a clock signal from a sender processor. At the receiver processor a bit of the data is phased aligned with the transmitted clock signal. The phase aligning includes selecting a data phase from a plurality of data phases in a delay chain and then adjusting the selected data phase to compensate for a round-off error. Additional embodiments include a system and storage medium for transmitting data among processors over a plurality of parallel data lines and a clock signal line.

Hoke, Joseph Michael; Ferraiolo, Frank D.; Lo, Tin-Chee; Yarolin, John Michael

2005-01-04T23:59:59.000Z

180

Sub-micron particle sampler apparatus and method for sampling sub-micron particles  

DOE Patents [OSTI]

Apparatus and method steps for collecting sub-micron sized particles include a collection chamber and cryogenic cooling. The cooling is accomplished by coil tubing carrying nitrogen in liquid form, with the liquid nitrogen changing to the gas phase before exiting from the collection chamber in the tubing. Standard filters are used to filter out particles of diameter greater than or equal to 0.3 microns; however, the present invention is used to trap particles of less than 0.3 micron in diameter. A blower draws air to said collection chamber through a filter which filters particles with diameters greater than or equal to 0.3 micron. The air is then cryogenically cooled so that moisture and sub-micron sized particles in the air condense into ice on the coil. The coil is then heated so that the ice melts, and the liquid is then drawn off and passed through a Buchner funnel where the liquid is passed through a Nuclepore membrane. A vacuum draws the liquid through the Nuclepore membrane, with the Nuclepore membrane trapping sub-micron sized particles therein. The Nuclepore membrane is then covered on its top and bottom surfaces with sheets of Mylar and the assembly is then crushed into a pellet. This effectively traps the sub-micron sized particles for later analysis. 6 figures.

Gay, D.D.; McMillan, W.G.

1984-04-12T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

Supporting Methods Sampling error  

E-Print Network [OSTI]

of 0.79, 0.07, 0.07, 0.07. The chart below gives a sense of the magnitude of these values. 1 #12 each of the selections are shown in order from highest affinity for GTP to lowest. The top line in each

Heller, Eric

182

A high sensitivity fiber optic macro-bend based gas flow rate transducer for low flow rates: Theory, working principle, and static calibration  

SciTech Connect (OSTI)

A novel fiber optic macro-bend based gas flowmeter for low flow rates is presented. Theoretical analysis of the sensor working principle, design, and static calibration were performed. The measuring system consists of: an optical fiber, a light emitting diode (LED), a Quadrant position sensitive Detector (QD), and an analog electronic circuit for signal processing. The fiber tip undergoes a deflection in the flow, acting like a cantilever. The consequent displacement of light spot center is monitored by the QD generating four unbalanced photocurrents which are function of fiber tip position. The analog electronic circuit processes the photocurrents providing voltage signal proportional to light spot position. A circular target was placed on the fiber in order to increase the sensing surface. Sensor, tested in the measurement range up to 10 l min{sup -1}, shows a discrimination threshold of 2 l min{sup -1}, extremely low fluid dynamic resistance (0.17 Pa min l{sup -1}), and high sensitivity, also at low flow rates (i.e., 33 mV min l{sup -1} up to 4 l min{sup -1} and 98 mV min l{sup -1} from 4 l min{sup -1} up to 10 l min{sup -1}). Experimental results agree with the theoretical predictions. The high sensitivity, along with the reduced dimension and negligible pressure drop, makes the proposed transducer suitable for medical applications in neonatal ventilation.

Schena, Emiliano; Saccomandi, Paola; Silvestri, Sergio [Center for Integrated Research, Unit of Measurements and Biomedical Instrumentation, Universita Campus Bio-Medico di Roma, Via Alvaro del Portillo, 21, 00128 Rome (Italy)

2013-02-15T23:59:59.000Z

183

Nuclear Instruments and Methods in Physics Research A 555 (2005) 340346 Calculation of gamma multiplicities in a multiplying sample for the  

E-Print Network [OSTI]

Nuclear Instruments and Methods in Physics Research A 555 (2005) 340­346 Calculation of gamma multiplicities in a multiplying sample for the assay of nuclear materials Imre Pa´ zsita,�, Sara A. Pozzib a Department of Nuclear Engineering, Chalmers University of Technology, Fysikgra¨nd 3, SE-412 96 Go

Pázsit, Imre

184

A method for direct, semi-quantitative analysis of gas phase samples using gas chromatography-inductively coupled plasma-mass spectrometry  

SciTech Connect (OSTI)

A new and complete GC–ICP-MS method is described for direct analysis of trace metals in a gas phase process stream. The proposed method is derived from standard analytical procedures developed for ICP-MS, which are regularly exercised in standard ICP-MS laboratories. In order to implement the method, a series of empirical factors were generated to calibrate detector response with respect to a known concentration of an internal standard analyte. Calibrated responses are ultimately used to determine the concentration of metal analytes in a gas stream using a semi-quantitative algorithm. The method was verified using a traditional gas injection from a GC sampling valve and a standard gas mixture containing either a 1 ppm Xe + Kr mix with helium balance or 100 ppm Xe with helium balance. Data collected for Xe and Kr gas analytes revealed that agreement of 6–20% with the actual concentration can be expected for various experimental conditions. To demonstrate the method using a relevant “unknown” gas mixture, experiments were performed for continuous 4 and 7 hour periods using a Hg-containing sample gas that was co-introduced into the GC sample loop with the xenon gas standard. System performance and detector response to the dilute concentration of the internal standard were pre-determined, which allowed semi-quantitative evaluation of the analyte. The calculated analyte concentrations varied during the course of the 4 hour experiment, particularly during the first hour of the analysis where the actual Hg concentration was under predicted by up to 72%. Calculated concentration improved to within 30–60% for data collected after the first hour of the experiment. Similar results were seen during the 7 hour test with the deviation from the actual concentration being 11–81% during the first hour and then decreasing for the remaining period. The method detection limit (MDL) was determined for the mercury by injecting the sample gas into the system following a period of equilibration. The MDL for Hg was calculated as 6.8 ?g · m{sup ? 3}. This work describes the first complete GC–ICP-MS method to directly analyze gas phase samples, and detailed sample calculations and comparisons to conventional ICP-MS methods are provided.

Carter, Kimberly E.; Gerdes, Kirk

2013-07-01T23:59:59.000Z

185

Apparatus and method for quantitatively evaluating total fissile and total fertile nuclide content in samples. [Patent application  

DOE Patents [OSTI]

Simultaneous photon and neutron interrogation of samples for the quantitative determination of total fissile nuclide and total fertile nuclide material present is made possible by the use of an electron accelerator. Prompt and delayed neutrons produced from resulting induced fission are counted using a single detection system and allow the resolution of the contributions from each interrogating flux leading in turn to the quantitative determination sought. Detection limits for /sup 239/Pu are estimated to be about 3 mg using prompt fission neutrons and about 6 mg using delayed neutrons.

Caldwell, J.T.; Kunz, W.E.; Cates, M.R.; Franks, L.A.

1982-07-07T23:59:59.000Z

186

270 | VOL.9 NO.3 | MARCH2012 | nature methods Key requirements for methylation analysis of large sample sizes  

E-Print Network [OSTI]

). This method eliminates five steps from Illumina's library- construction protocol such that multiplexed and sequenced all at once in a single Illumina HiSeq flowcell. Additionally we designed barcodes to process 384 an analysis pipeline for read mapping and methylation quantification, called bisReadMapper (Supplementary Fig

Cai, Long

187

Apparatus and method for quantitative assay of samples of transuranic waste contained in barrels in the presence of matrix material  

DOE Patents [OSTI]

Apparatus and method for performing corrections for matrix material effects on the neutron measurements generated from analysis of transuranic waste drums using the differential-dieaway technique. By measuring the absorption index and the moderator index for a particular drum, correction factors can be determined for the effects of matrix materials on the ''observed'' quantity of fissile and fertile material present therein in order to determine the actual assays thereof. A barrel flux monitor is introduced into the measurement chamber to accomplish these measurements as a new contribution to the differential-dieaway technology. 9 figs.

Caldwell, J.T.; Herrera, G.C.; Hastings, R.D.; Shunk, E.R.; Kunz, W.E.

1987-08-28T23:59:59.000Z

188

Methods and Materials Sample Collection  

E-Print Network [OSTI]

collections for 7July-4 August 1961 survey. .. PACIFIC OCEAN . $lGH9 . . ~ ...56' 170· tS5- BE RI NG SEA ~ Ala

189

Hazard surveillance for workplace magnetic fields. 1: Walkaround sampling method for measuring ambient field magnitude; 2: Field characteristics from waveform measurements  

SciTech Connect (OSTI)

Recent epidemiologic research has suggested that exposure to extremely low frequency (ELF) magnetic fields (MF) may be associated with leukemia, brain cancer, spontaneous abortions, and Alzheimer`s disease. A walkaround sampling method for measuring ambient ELF-MF levels was developed for use in conducting occupational hazard surveillance. This survey was designed to determine the range of MF levels at different industrial facilities so they could be categorized by MF levels and identified for possible subsequent personal exposure assessments. Industries were selected based on their annual electric power consumption in accordance with the hypothesis that large power consumers would have higher ambient MFs when compared with lower power consumers. Sixty-two facilities within thirteen 2-digit Standard Industrial Classifications (SIC) were selected based on their willingness to participate. A traditional industrial hygiene walkaround survey was conducted to identify MF sources, with a special emphasis on work stations.

Methner, M.M.; Bowman, J.D.

1998-03-01T23:59:59.000Z

190

A study of diesel combustion process under the condition of EGR and high-pressure fuel injection with gas sampling method  

SciTech Connect (OSTI)

It is well known that a high-pressure fuel injection is effective for the reduction in particulates and smoke emissions. Exhaust gas recirculation (EGR) is effective for the reduction in NO{sub x} emission. In this study an experiment aiming to understand more comprehensive combustion under the condition of EGR and high-pressure fuel injection was carried out by using gas sampling method for the purpose of understanding what occurred inside the spray before and after combustion. The number of combustion cycles in this engine can be controlled in order to change EGR conditions by adjusting the residual gas concentration in the cylinder. Main results were: (1) close to the nozzle tip, the sampling gas data showed little reaction which implies that combustion never occurs in this area during the injection period; (2) in the case of high-pressure fuel injection O{sub 2} concentration decreased faster and air dilution was more active and earlier, this may cause the decrease of smoke emissions due to accelerated soot oxidation; (3) in the case of EGR, combustion was poor since oxygen concentration was insufficient, thus, inactivity of oxidation reaction caused reduction in NO{sub x} emission; (4) in the case of increasing the amounts of N{sub 2} gas while keeping the O{sub 2} content constant (same amount as without EGR), NO{sub x} emission decreased without deterioration of smoke emission and Pmi.

Shimazaki, Naoki; Hatanaka, Hirokazu; Yokota, Katsuhiko; Nakahira, Toshio

1996-09-01T23:59:59.000Z

191

A Monte Carlo Investigation of Three Different Estimation Methods in Multilevel Structural Equation Modeling Under Conditions of Data Nonnormality and Varied Sample Sizes  

E-Print Network [OSTI]

various sample sizes and differing estimators (maximum likelihood, generalized least squares, and weighted least squares). The finding revealed that the regression coefficients were estimated with little to no bias among the study design conditions...

Byrd, Jimmy

2010-01-14T23:59:59.000Z

192

Method for determination of .sup.18 O/.sup.16 O and .sup.2 H/.sup.1 H ratios and .sup.3 H (tritium) concentrations of xylem waters and subsurface waters using time series sampling  

DOE Patents [OSTI]

A method for determination of .sup.18 O/.sup.16 O and .sup.2 H/.sup.1 H ratios and .sup.3 H concentrations of xylem and subsurface waters using time series sampling, insulating sampling chambers, and combined .sup.18 O/.sup.16 O, .sup.2 H/.sup.1 H and .sup.3 H concentration data on transpired water. The method involves collecting water samples transpired from living plants and correcting the measured isotopic compositions of oxygen (.sup.18 O/.sup.16 O) and hydrogen (.sup.2 H/.sup.1 H and/or .sup.3 H concentrations) to account for evaporative isotopic fractionation in the leafy material of the plant.

Smith, Brian (1126 Delaware St., Berkeley, CA 94702); Menchaca, Leticia (1126 Delaware St., Berkeley, CA 94702)

1999-01-01T23:59:59.000Z

193

Method and apparatus utilizing ionizing and microwave radiation for saturation determination of water, oil and a gas in a core sample  

DOE Patents [OSTI]

A system for determining the relative permeabilities of gas, water and oil in a core sample has a microwave emitter/detector subsystem and an X-ray emitter/detector subsystem. A core holder positions the core sample between microwave absorbers which prevent diffracted microwaves from reaching a microwave detector where they would reduce the signal-to-noise ratio of the microwave measurements. The microwave emitter/detector subsystem and the X-ray emitter/detector subsystem each have linear calibration characteristics, allowing one subsystem to be calibrated with respect to the other subsystem. The dynamic range of microwave measurements is extended through the use of adjustable attenuators. This also facilitates the use of core samples with wide diameters. The stratification characteristics of the fluids may be observed with a windowed cell separator at the outlet of the core sample. The condensation of heavy hydrocarbon gas and the dynamic characteristics of the fluids are observed with a sight glass at the outlet of the core sample.

Maerefat, Nicida L. (Sugar Land, TX); Parmeswar, Ravi (Marlton, NJ); Brinkmeyer, Alan D. (Tulsa, OK); Honarpour, Mehdi (Bartlesville, OK)

1994-01-01T23:59:59.000Z

194

Method and apparatus utilizing ionizing and microwave radiation for saturation determination of water, oil and a gas in a core sample  

DOE Patents [OSTI]

A system is described for determining the relative permeabilities of gas, water and oil in a core sample has a microwave emitter/detector subsystem and an X-ray emitter/detector subsystem. A core holder positions the core sample between microwave absorbers which prevent diffracted microwaves from reaching a microwave detector where they would reduce the signal-to-noise ratio of the microwave measurements. The microwave emitter/detector subsystem and the X-ray emitter/detector subsystem each have linear calibration characteristics, allowing one subsystem to be calibrated with respect to the other subsystem. The dynamic range of microwave measurements is extended through the use of adjustable attenuators. This also facilitates the use of core samples with wide diameters. The stratification characteristics of the fluids may be observed with a windowed cell separator at the outlet of the core sample. The condensation of heavy hydrocarbon gas and the dynamic characteristics of the fluids are observed with a sight glass at the outlet of the core sample. 11 figs.

Maerefat, N.L.; Parmeswar, R.; Brinkmeyer, A.D.; Honarpour, M.

1994-08-23T23:59:59.000Z

195

Measurement of the top quark mass at CDF using the "neutrino phi weighting" template method on a lepton plus isolated track sample  

E-Print Network [OSTI]

We present a measurement of the top quark mass with tt? dilepton events produced in pp? collisions at the Fermilab Tevatron (?s=1.96??TeV) and collected by the CDF II detector. A sample of 328 events with a charged ...

Choudalakis, Georgios

196

Waste classification sampling plan  

SciTech Connect (OSTI)

The purpose of this sampling is to explain the method used to collect and analyze data necessary to verify and/or determine the radionuclide content of the B-Cell decontamination and decommissioning waste stream so that the correct waste classification for the waste stream can be made, and to collect samples for studies of decontamination methods that could be used to remove fixed contamination present on the waste. The scope of this plan is to establish the technical basis for collecting samples and compiling quantitative data on the radioactive constituents present in waste generated during deactivation activities in B-Cell. Sampling and radioisotopic analysis will be performed on the fixed layers of contamination present on structural material and internal surfaces of process piping and tanks. In addition, dose rate measurements on existing waste material will be performed to determine the fraction of dose rate attributable to both removable and fixed contamination. Samples will also be collected to support studies of decontamination methods that are effective in removing the fixed contamination present on the waste. Sampling performed under this plan will meet criteria established in BNF-2596, Data Quality Objectives for the B-Cell Waste Stream Classification Sampling, J. M. Barnett, May 1998.

Landsman, S.D.

1998-05-27T23:59:59.000Z

197

Sampling box  

DOE Patents [OSTI]

An air sampling box that uses a slidable filter tray and a removable filter cartridge to allow for the easy replacement of a filter which catches radioactive particles is disclosed.

Phillips, Terrance D. (617 Chestnut Ct., Aiken, SC 29803); Johnson, Craig (100 Midland Rd., Oak Ridge, TN 37831-0895)

2000-01-01T23:59:59.000Z

198

MIT extraction method for measuring average subchannel axial velocities in reactor assemblies  

SciTech Connect (OSTI)

The MIT extraction method for obtaining flow split data for individual subchannels is described in detail. An analysis of the method is presented which shows that isokinetic values of the subchannel flow rates are obtained directly even though the method is non-isokinetic. Time saving methods are discussed for obtaining the average value of the interior region flow split parameter. An analysis of the method at low bundle flow rates indicates that there is no inherent low flow rate limitation on the method and suggests a way to obtain laminar flow split data.

Hawley, J.T.; Chiu, C.; Todreas, N.E.

1980-08-01T23:59:59.000Z

199

SAMPLE AVERAGE APPROXIMATION METHOD FOR COMPOUND ...  

E-Print Network [OSTI]

Jun 30, 2013 ... bounds from (10) are much sharper than estimates obtained from (11), ..... X a vector of resources allocated at objects i = 1, ..., n to protect them from the .... and cost functions, IE denotes mathematical expectation over ?. ...... [29] H. Markowitz, Mean-Variance Analysis in Portfolio Choice and Capital Markets, ...

2013-06-30T23:59:59.000Z

200

Selection of Sampling Pumps Used for Groundwater Monitoring at the Hanford Site  

SciTech Connect (OSTI)

The variable frequency drive centrifugal submersible pump, Redi-Flo2a made by Grundfosa, was selected for universal application for Hanford Site groundwater monitoring. Specifications for the selected pump and five other pumps were evaluated against current and future Hanford groundwater monitoring performance requirements, and the Redi-Flo2 was selected as the most versatile and applicable for the range of monitoring conditions. The Redi-Flo2 pump distinguished itself from the other pumps considered because of its wide range in output flow rate and its comparatively moderate maintenance and low capital costs. The Redi-Flo2 pump is able to purge a well at a high flow rate and then supply water for sampling at a low flow rate. Groundwater sampling using a low-volume-purging technique (e.g., low flow, minimal purge, no purge, or micropurgea) is planned in the future, eliminating the need for the pump to supply a high-output flow rate. Under those conditions, the Well Wizard bladder pump, manufactured by QED Environmental Systems, Inc., may be the preferred pump because of the lower capital cost.

Schalla, Ronald; Webber, William D.; Smith, Ronald M.

2001-11-05T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

Principles for Sampling Airborne Radioactivity from Stacks  

SciTech Connect (OSTI)

This book chapter describes the special processes involved in sampling the airborne effluents from nuclear faciities. The title of the book is Radioactive Air Sampling Methods. The abstract for this chapter was cleared as PNNL-SA-45941.

Glissmeyer, John A.

2010-10-18T23:59:59.000Z

202

A New Method For Robust High-Precision Time-Series Photometry From Well-Sampled Images: Application to Archival MMT/Megacam Observations of the Open Cluster M37  

E-Print Network [OSTI]

We introduce new methods for robust high-precision photometry from well-sampled images of a non-crowded field with a strongly varying point-spread function. For this work, we used archival imaging data of the open cluster M37 taken by MMT 6.5m telescope. We find that the archival light curves from the original image subtraction procedure exhibit many unusual outliers, and more than 20% of data get rejected by the simple filtering algorithm adopted by early analysis. In order to achieve better photometric precisions and also to utilize all available data, the entire imaging database was re-analyzed with our time-series photometry technique (Multi-aperture Indexing Photometry) and a set of sophisticated calibration procedures. The merit of this approach is as follows: we find an optimal aperture for each star with a maximum signal-to-noise ratio, and also treat peculiar situations where photometry returns misleading information with more optimal photometric index. We also adopt photometric de-trending based on ...

Chang, S -W; Hartman, J D

2015-01-01T23:59:59.000Z

203

Defining And Characterizing Sample Representativeness For DWPF Melter Feed Samples  

SciTech Connect (OSTI)

Representative sampling is important throughout the Defense Waste Processing Facility (DWPF) process, and the demonstrated success of the DWPF process to achieve glass product quality over the past two decades is a direct result of the quality of information obtained from the process. The objective of this report was to present sampling methods that the Savannah River Site (SRS) used to qualify waste being dispositioned at the DWPF. The goal was to emphasize the methodology, not a list of outcomes from those studies. This methodology includes proven methods for taking representative samples, the use of controlled analytical methods, and data interpretation and reporting that considers the uncertainty of all error sources. Numerous sampling studies were conducted during the development of the DWPF process and still continue to be performed in order to evaluate options for process improvement. Study designs were based on use of statistical tools applicable to the determination of uncertainties associated with the data needs. Successful designs are apt to be repeated, so this report chose only to include prototypic case studies that typify the characteristics of frequently used designs. Case studies have been presented for studying in-tank homogeneity, evaluating the suitability of sampler systems, determining factors that affect mixing and sampling, comparing the final waste glass product chemical composition and durability to that of the glass pour stream sample and other samples from process vessels, and assessing the uniformity of the chemical composition in the waste glass product. Many of these studies efficiently addressed more than one of these areas of concern associated with demonstrating sample representativeness and provide examples of statistical tools in use for DWPF. The time when many of these designs were implemented was in an age when the sampling ideas of Pierre Gy were not as widespread as they are today. Nonetheless, the engineers and statisticians used carefully thought out designs that systematically and economically provided plans for data collection from the DWPF process. Key shared features of the sampling designs used at DWPF and the Gy sampling methodology were the specification of a standard for sample representativeness, an investigation that produced data from the process to study the sampling function, and a decision framework used to assess whether the specification was met based on the data. Without going into detail with regard to the seven errors identified by Pierre Gy, as excellent summaries are readily available such as Pitard [1989] and Smith [2001], SRS engineers understood, for example, that samplers can be biased (Gy?s extraction error), and developed plans to mitigate those biases. Experiments that compared installed samplers with more representative samples obtained directly from the tank may not have resulted in systematically partitioning sampling errors into the now well-known error categories of Gy, but did provide overall information on the suitability of sampling systems. Most of the designs in this report are related to the DWPF vessels, not the large SRS Tank Farm tanks. Samples from the DWPF Slurry Mix Evaporator (SME), which contains the feed to the DWPF melter, are characterized using standardized analytical methods with known uncertainty. The analytical error is combined with the established error from sampling and processing in DWPF to determine the melter feed composition. This composition is used with the known uncertainty of the models in the Product Composition Control System (PCCS) to ensure that the wasteform that is produced is comfortably within the acceptable processing and product performance region. Having the advantage of many years of processing that meets the waste glass product acceptance criteria, the DWPF process has provided a considerable amount of data about itself in addition to the data from many special studies. Demonstrating representative sampling directly from the large Tank Farm tanks is a difficult, if not unsolvable enterprise due to li

Shine, E. P.; Poirier, M. R.

2013-10-29T23:59:59.000Z

204

Acceptance sampling using judgmental and randomly selected samples  

SciTech Connect (OSTI)

We present a Bayesian model for acceptance sampling where the population consists of two groups, each with different levels of risk of containing unacceptable items. Expert opinion, or judgment, may be required to distinguish between the high and low-risk groups. Hence, high-risk items are likely to be identifed (and sampled) using expert judgment, while the remaining low-risk items are sampled randomly. We focus on the situation where all observed samples must be acceptable. Consequently, the objective of the statistical inference is to quantify the probability that a large percentage of the unsampled items in the population are also acceptable. We demonstrate that traditional (frequentist) acceptance sampling and simpler Bayesian formulations of the problem are essentially special cases of the proposed model. We explore the properties of the model in detail, and discuss the conditions necessary to ensure that required samples sizes are non-decreasing function of the population size. The method is applicable to a variety of acceptance sampling problems, and, in particular, to environmental sampling where the objective is to demonstrate the safety of reoccupying a remediated facility that has been contaminated with a lethal agent.

Sego, Landon H.; Shulman, Stanley A.; Anderson, Kevin K.; Wilson, John E.; Pulsipher, Brent A.; Sieber, W. Karl

2010-09-01T23:59:59.000Z

205

STATISTICAL METHODS STATISTICAL METHODS  

E-Print Network [OSTI]

STATISTICAL METHODS 1 STATISTICAL METHODS Arnaud Delorme, Swartz Center for Computational@salk.edu. Keywords: statistical methods, inference, models, clinical, software, bootstrap, resampling, PCA, ICA Abstract: Statistics represents that body of methods by which characteristics of a population are inferred

Delorme, Arnaud

206

Optimization Online - Convergence analysis of sampling-based ...  

E-Print Network [OSTI]

Aug 19, 2014 ... Convergence analysis of sampling-based decomposition methods for risk-averse multistage stochastic convex programs.

Vincent Guigues

2014-08-19T23:59:59.000Z

207

Biomolecular Path Sampling Enabled by Processing in Network Storage  

E-Print Network [OSTI]

parallel biomolec- ular sampling methods such as Folding@home [8] have been successfully mapped to grid

Thain, Douglas

208

ESPC IDIQ Contract Sample  

Broader source: Energy.gov [DOE]

Document displays a sample indefinite delivery, indefinite quantity (IDIQ) energy savings performance contract (ESPC).

209

The Effects of Anchor Length, Test Difficulty, Population Ability Differences, Mixture of Populations and Sample Size on the Psychometric Properties of Levine Observed Score Linear Equating Method for Different Assumptions  

E-Print Network [OSTI]

for 100 samples, anchor 40%, 93 easier test Y and ability N(50%, 18%) 45. Bias (top) and RMSE (bottom) at score level for 100 samples, anchor 40%, 94 more difficult test Y and ability N(50%, 18%) 46. Bias (top... is equity, which states that it must be a matter of indifference to the test taker whether he or she takes X or Y. Although equatability is a prerequisite for equity, it does not imply equity because two tests that measure the same construct can differ...

Carvajal, Jorge E.

2011-02-15T23:59:59.000Z

210

E-Print Network 3.0 - affecting endothelial prostacyclin Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

flow initi- ates and modulates endothelial... Endothelial Cells to Different Types of Fluid Mechanical Shear Stress Abdul I. Barakat* and Deborah K. Lieu... . How low flow,...

211

E-Print Network 3.0 - affect distal blood Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

aggregation at low flow rates increases ... Source: Popel, Aleksander S. - Department of Biomedical Engineering, Johns Hopkins University Collection: Engineering ; Biology and...

212

Rain sampling device  

DOE Patents [OSTI]

The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of the precipitation from the chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device. 11 figures.

Nelson, D.A.; Tomich, S.D.; Glover, D.W.; Allen, E.V.; Hales, J.M.; Dana, M.T.

1991-05-14T23:59:59.000Z

213

Rain sampling device  

DOE Patents [OSTI]

The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of said precipitation from said chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device.

Nelson, Danny A. (Richland, WA); Tomich, Stanley D. (Richland, WA); Glover, Donald W. (Prosser, WA); Allen, Errol V. (Benton City, WA); Hales, Jeremy M. (Kennewick, WA); Dana, Marshall T. (Richland, WA)

1991-01-01T23:59:59.000Z

214

COMPUTER SCIENCE SAMPLE PROGRAM  

E-Print Network [OSTI]

COMPUTER SCIENCE SAMPLE PROGRAM (First Math Course MATH 198) This sample program suggests one way CS 181: Foundations of Computer Science II CS 180: Foundations of Computer Science I CS 191

Gering, Jon C.

215

Bayesian methods in bioinformatics  

E-Print Network [OSTI]

- niques for drawing random samples from the posterior for inference. We show that the approach achieves very competitive performance as compared to other methods. The second part focuses on modeling DNA microarray data. Microarray technology enables us...

Baladandayuthapani, Veerabhadran

2007-04-25T23:59:59.000Z

216

SAMPLING-BASED ROADMAP OF TREES FOR PARALLEL MOTION PLANNING 1 Sampling-Based Roadmap of Trees for Parallel  

E-Print Network [OSTI]

SAMPLING-BASED ROADMAP OF TREES FOR PARALLEL MOTION PLANNING 1 Sampling-Based Roadmap of Trees for multiple query motion planning (Probabilistic Roadmap Method - PRM) with sampling-based tree methods algorithms, roadmap, tree, PRM, EST, RRT, SRT. I. INTRODUCTION HIGH-DIMENSIONAL problems such as those

Chen, Brian Y.

217

Microfluidic-Based Robotic Sampling System for Radioactive Solutions  

SciTech Connect (OSTI)

A novel microfluidic based robotic sampling system has been developed for sampling and analysis of liquid solutions in nuclear processes. This system couples the use of a microfluidic sample chip with a robotic system designed to allow remote, automated sampling of process solutions in-cell and facilitates direct coupling of the microfluidic sample chip with analytical instrumentation. This system provides the capability for near real time analysis, reduces analytical waste, and minimizes the potential for personnel exposure associated with traditional sampling methods. A prototype sampling system was designed, built and tested. System testing demonstrated operability of the microfluidic based sample system and identified system modifications to optimize performance.

Jack D. Law; Julia L. Tripp; Tara E. Smith; Veronica J. Rutledge; Troy G. Garn; John Svoboda; Larry Macaluso

2014-02-01T23:59:59.000Z

218

Sampled data lattice filters  

E-Print Network [OSTI]

SAMPLED DATA LATTICE FILTERS A Thesis by WILLIAM TERRY THRIFT III Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE December 1979 Major Subfect...: Electrical Engineering SAMPLED DATA LATTICE FILTERS A Thesis by WILLIAM TERRY THRIFT III Approved as to style and content by: (Chair an of Committee) (Hea f Department) (Member) (Member) (Member) (Member) December 1979 ABSTRACT Sampled Data...

Thrift, William Terry

1980-01-01T23:59:59.000Z

219

Surface sampling concentration and reaction probe  

DOE Patents [OSTI]

A method of analyzing a chemical composition of a specimen is described. The method can include providing a probe comprising an outer capillary tube and an inner capillary tube disposed co-axially within the outer capillary tube, where the inner and outer capillary tubes define a solvent capillary and a sampling capillary in fluid communication with one another at a distal end of the probe; contacting a target site on a surface of a specimen with a solvent in fluid communication with the probe; maintaining a plug volume proximate a solvent-specimen interface, wherein the plug volume is in fluid communication with the probe; draining plug sampling fluid from the plug volume through the sampling capillary; and analyzing a chemical composition of the plug sampling fluid with an analytical instrument. A system for performing the method is also described.

Van Berkel, Gary J; Elnaggar, Mariam S

2013-07-16T23:59:59.000Z

220

Rehabilitation Services Sample Occupations  

E-Print Network [OSTI]

/Industries Correction Agencies Drug Treatment Centers Addiction Counselor Advocacy Occupations Art Therapist BehavioralRehabilitation Services Sample Occupations Sample Work Settings Child & Day Care Centers Clinics................................ IIB 29-1000 E4 Careers in Counseling and Human Services .........IIB 21-1010 C7 Careers in Health Care

Ronquist, Fredrik

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

Biological sample collector  

DOE Patents [OSTI]

A biological sample collector is adapted to a collect several biological samples in a plurality of filter wells. A biological sample collector may comprise a manifold plate for mounting a filter plate thereon, the filter plate having a plurality of filter wells therein; a hollow slider for engaging and positioning a tube that slides therethrough; and a slide case within which the hollow slider travels to allow the tube to be aligned with a selected filter well of the plurality of filter wells, wherein when the tube is aligned with the selected filter well, the tube is pushed through the hollow slider and into the selected filter well to sealingly engage the selected filter well and to allow the tube to deposit a biological sample onto a filter in the bottom of the selected filter well. The biological sample collector may be portable.

Murphy, Gloria A. (French Camp, CA)

2010-09-07T23:59:59.000Z

222

Adaptive Sampling in Hierarchical Simulation  

SciTech Connect (OSTI)

We propose an adaptive sampling methodology for hierarchical multi-scale simulation. The method utilizes a moving kriging interpolation to significantly reduce the number of evaluations of finer-scale response functions to provide essential constitutive information to a coarser-scale simulation model. The underlying interpolation scheme is unstructured and adaptive to handle the transient nature of a simulation. To handle the dynamic construction and searching of a potentially large set of finer-scale response data, we employ a dynamic metric tree database. We study the performance of our adaptive sampling methodology for a two-level multi-scale model involving a coarse-scale finite element simulation and a finer-scale crystal plasticity based constitutive law.

Knap, J; Barton, N R; Hornung, R D; Arsenlis, A; Becker, R; Jefferson, D R

2007-07-09T23:59:59.000Z

223

anisotropic nmr samples: Topics by E-print Network  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

artifacts. Abbreviations: FFT fast Fourier transform; LP linear prediction; MEM maximum entropy method; SN signal-to-noise ratio unknown authors 24 Cryogenic sample...

224

Water Sample Concentrator  

ScienceCinema (OSTI)

Automated portable device that concentrates and packages a sample of suspected contaminated water for safe, efficient transport to a qualified analytical laboratory. This technology will help safeguard against pathogen contamination or chemical and biolog

Idaho National Laboratory

2010-01-08T23:59:59.000Z

225

Dissolution actuated sample container  

DOE Patents [OSTI]

A sample collection vial and process of using a vial is provided. The sample collection vial has an opening secured by a dissolvable plug. When dissolved, liquids may enter into the interior of the collection vial passing along one or more edges of a dissolvable blocking member. As the blocking member is dissolved, a spring actuated closure is directed towards the opening of the vial which, when engaged, secures the vial contents against loss or contamination.

Nance, Thomas A.; McCoy, Frank T.

2013-03-26T23:59:59.000Z

226

SAMPLING AND ANALYSIS PROTOCOLS  

SciTech Connect (OSTI)

Radiological sampling and analyses are performed to collect data for a variety of specific reasons covering a wide range of projects. These activities include: Effluent monitoring; Environmental surveillance; Emergency response; Routine ambient monitoring; Background assessments; Nuclear license termination; Remediation; Deactivation and decommissioning (D&D); and Waste management. In this chapter, effluent monitoring and environmental surveillance programs at nuclear operating facilities and radiological sampling and analysis plans for remediation and D&D activities will be discussed.

Jannik, T; P Fledderman, P

2007-02-09T23:59:59.000Z

227

Biological tracer method  

DOE Patents [OSTI]

The present invention is a biological tracer method for characterizing the movement of a material through a medium, comprising the steps of: introducing a biological tracer comprising a microorganism having ice nucleating activity into a medium; collecting at least one sample of the medium from a point removed from the introduction point; and analyzing the sample for the presence of the biological tracer. The present invention is also a method for using a biological tracer as a label for material identification by introducing a biological tracer having ice nucleating activity into a material, collecting a sample of a portion of the labelled material and analyzing the sample for the presence of the biological tracer. 2 figs.

Strong-Gunderson, J.M.; Palumbo, A.V.

1998-09-15T23:59:59.000Z

228

Biological tracer method  

DOE Patents [OSTI]

The present invention is a biological tracer method for characterizing the movement of a material through a medium, comprising the steps of: introducing a biological tracer comprising a microorganism having ice nucleating activity into a medium; collecting at least one sample of the medium from a point removed from the introduction point; and analyzing the sample for the presence of the biological tracer. The present invention is also a method for using a biological tracer as a label for material identification by introducing a biological tracer having ice nucleating activity into a material, collecting a sample of a portion of the labelled material and analyzing the sample for the presence of the biological tracer.

Strong-Gunderson, Janet M. (Ten Mile, TN); Palumbo, Anthony V. (Oak Ridge, TN)

1998-01-01T23:59:59.000Z

229

Liquid sampling system  

DOE Patents [OSTI]

A conduit extends from a reservoir through a sampling station and back to the reservoir in a closed loop. A jet ejector in the conduit establishes suction for withdrawing liquid from the reservoir. The conduit has a self-healing septum therein upstream of the jet ejector for receiving one end of a double-ended cannula, the other end of which is received in a serum bottle for sample collection. Gas is introduced into the conduit at a gas bleed between the sample collection bottle and the reservoir. The jet ejector evacuates gas from the conduit and the bottle and aspirates a column of liquid from the reservoir at a high rate. When the withdrawn liquid reaches the jet ejector the rate of flow therethrough reduces substantially and the gas bleed increases the pressure in the conduit for driving liquid into the sample bottle, the gas bleed forming a column of gas behind the withdrawn liquid column and interrupting the withdrawal of liquid from the reservoir. In the case of hazardous and toxic liquids, the sample bottle and the jet ejector may be isolated from the reservoir and may be further isolated from a control station containing remote manipulation means for the sample bottle and control valves for the jet ejector and gas bleed. 5 figs.

Larson, L.L.

1984-09-17T23:59:59.000Z

230

Atmospheric sampling glow discharge ionization source  

DOE Patents [OSTI]

An atmospheric sampling glow discharge ionization source that can be used in combination with an analytical instrument which operates at high vacuum, such as a mass spectrometer. The atmospheric sampling glow discharge ionization source comprises a chamber with at least one pair of electrodes disposed therein, an inlet for a gaseous sample to be analyzed and an outlet communicating with an analyzer which operates at subatmospheric pressure. The ionization chamber is maintained at a pressure below atmospheric pressure, and a voltage difference is applied across the electrodes to induce a glow discharge between the electrodes, so that molecules passing through the inlet are ionized by the glow discharge and directed into the analyzer. The ionization source accepts the sample under atmospheric pressure conditions and processes it directly into the high vacuum instrument, bridging the pressure gap and drawing off unwanted atmospheric gases. The invention also includes a method for analyzing a gaseous sample using the glow discharge ionization source described above. 3 figs.

McLuckey, S.A.; Glish, G.L.

1989-07-18T23:59:59.000Z

231

Vapor spill monitoring method  

DOE Patents [OSTI]

Method for continuous sampling of liquified natural gas effluent from a spill pipe, vaporizing the cold liquified natural gas, and feeding the vaporized gas into an infrared detector to measure the gas composition. The apparatus utilizes a probe having an inner channel for receiving samples of liquified natural gas and a surrounding water jacket through which warm water is flowed to flash vaporize the liquified natural gas.

Bianchini, Gregory M. (Livermore, CA); McRae, Thomas G. (Livermore, CA)

1985-01-01T23:59:59.000Z

232

Rapid determination of actinides in asphalt samples  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

A new rapid method for the determination of actinides in asphalt samples has been developed that can be used in emergency response situations or for routine analysis If a radiological dispersive device (RDD), Improvised Nuclear Device (IND) or a nuclear accident such as the accident at the Fukushima Nuclear Power Plant in March, 2011 occurs, there will be an urgent need for rapid analyses of many different environmental matrices, including asphalt materials, to support dose mitigation and environmental clean up. The new method for the determination of actinides in asphalt utilizes a rapid furnace step to destroy bitumen and organics present in the asphalt and sodium hydroxide fusion to digest the remaining sample. Sample preconcentration steps are used to collect the actinides and a new stacked TRU Resin + DGA Resin column method is employed to separate the actinide isotopes in the asphalt samples. The TRU Resin plus DGA Resin separation approach, which allows sequential separation of plutonium, uranium, americium and curium isotopes in asphalt samples, can be applied to soil samples as well.

Maxwell, Sherrod L.; Culligan, Brian K.; Hutchison, Jay B.

2014-01-12T23:59:59.000Z

233

Vapor port and groundwater sampling well  

DOE Patents [OSTI]

A method and apparatus has been developed for combining groundwater monitoring wells with unsaturated-zone vapor sampling ports. The apparatus allows concurrent monitoring of both the unsaturated and the saturated zone from the same well at contaminated areas. The innovative well design allows for concurrent sampling of groundwater and volatile organic compounds (VOCs) in the vadose (unsaturated) zone from a single well, saving considerable time and money. The sample tubes are banded to the outer well casing during installation of the well casing.

Hubbell, Joel M. (Idaho Falls, ID); Wylie, Allan H. (Idaho Falls, ID)

1996-01-01T23:59:59.000Z

234

Vapor port and groundwater sampling well  

DOE Patents [OSTI]

A method and apparatus have been developed for combining groundwater monitoring wells with unsaturated-zone vapor sampling ports. The apparatus allows concurrent monitoring of both the unsaturated and the saturated zone from the same well at contaminated areas. The innovative well design allows for concurrent sampling of groundwater and volatile organic compounds (VOCs) in the vadose (unsaturated) zone from a single well, saving considerable time and money. The sample tubes are banded to the outer well casing during installation of the well casing. 10 figs.

Hubbell, J.M.; Wylie, A.H.

1996-01-09T23:59:59.000Z

235

Blue Moon sampling, vectorial reaction coordinates, and unbiased constrained dynamics  

E-Print Network [OSTI]

Blue Moon sampling, vectorial reaction coordinates, and unbiased constrained dynamics Giovanni force in terms of a conditional expectation which can be computed by Blue Moon sampling Introduction Fifteen years ago the Blue Moon ensemble method was introduced to sample rare events that occur

Van Den Eijnden, Eric

236

Fluid sampling system  

DOE Patents [OSTI]

An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to be decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank. 4 figs.

Houck, E.D.

1994-10-11T23:59:59.000Z

237

Fluid sampling system  

DOE Patents [OSTI]

An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank.

Houck, Edward D. (Idaho Falls, ID)

1994-01-01T23:59:59.000Z

238

Viscous sludge sample collector  

DOE Patents [OSTI]

A vertical core sample collection system for viscous sludge. A sample tube's upper end has a flange and is attached to a piston. The tube and piston are located in the upper end of a bore in a housing. The bore's lower end leads outside the housing and has an inwardly extending rim. Compressed gas, from a storage cylinder, is quickly introduced into the bore's upper end to rapidly accelerate the piston and tube down the bore. The lower end of the tube has a high sludge entering velocity to obtain a full-length sludge sample without disturbing strata detail. The tube's downward motion is stopped when its upper end flange impacts against the bore's lower end inwardly extending rim.

Beitel, George A [Richland, WA

1983-01-01T23:59:59.000Z

239

Hanford Site Environmental Surveillance Master Sampling Schedule  

SciTech Connect (OSTI)

Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest National Laboratory (PNNL) for the U.S. Department of Energy (DOE). Sampling is conducted to evaluate levels of radioactive and nonradioactive pollutants in the Hanford environs, as required in DOE Order 5400.1, ''General Environmental protection Program,'' and DOE Order 5400.5, ''Radiation Protection of the Public and the Environment.'' The sampling methods are described in the Environmental Monitoring Plan, United States Department of Energy, Richland Operations Office, DOE/RL-91-50, Rev.2, U.S. Department of Energy, Richland, Washington. This document contains the CY1999 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes the sampling location, sample type, and analyses to be performed on the sample. In some cases, samples are scheduled on a rotating basis and may not be collected in 1999 in which case the anticipated year for collection is provided. In addition, a map is included for each media showing approximate sampling locations.

LE Bisping

1999-02-12T23:59:59.000Z

240

Environmental Science: Sample Pathway  

E-Print Network [OSTI]

Environmental Science: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Core GE 100 Intro to Env Science ES 105 Env Earth Science Sophomore Year CGS Core (CGS NS201 will fulfill CAS BI107 & 124) MA 115 Statistics Summer Environmental Internship Junior Year CH 171 Chem for Health Sciences CH

Goldberg, Bennett

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

Calculating Confidence, Uncertainty, and Numbers of Samples When Using Statistical Sampling Approaches to Characterize and Clear Contaminated Areas  

SciTech Connect (OSTI)

This report discusses the methodology, formulas, and inputs needed to make characterization and clearance decisions for Bacillus anthracis-contaminated and uncontaminated (or decontaminated) areas using a statistical sampling approach. Specifically, the report includes the methods and formulas for calculating the • number of samples required to achieve a specified confidence in characterization and clearance decisions • confidence in making characterization and clearance decisions for a specified number of samples for two common statistically based environmental sampling approaches. In particular, the report addresses an issue raised by the Government Accountability Office by providing methods and formulas to calculate the confidence that a decision area is uncontaminated (or successfully decontaminated) if all samples collected according to a statistical sampling approach have negative results. Key to addressing this topic is the probability that an individual sample result is a false negative, which is commonly referred to as the false negative rate (FNR). The two statistical sampling approaches currently discussed in this report are 1) hotspot sampling to detect small isolated contaminated locations during the characterization phase, and 2) combined judgment and random (CJR) sampling during the clearance phase. Typically if contamination is widely distributed in a decision area, it will be detectable via judgment sampling during the characterization phrase. Hotspot sampling is appropriate for characterization situations where contamination is not widely distributed and may not be detected by judgment sampling. CJR sampling is appropriate during the clearance phase when it is desired to augment judgment samples with statistical (random) samples. The hotspot and CJR statistical sampling approaches are discussed in the report for four situations: 1. qualitative data (detect and non-detect) when the FNR = 0 or when using statistical sampling methods that account for FNR > 0 2. qualitative data when the FNR > 0 but statistical sampling methods are used that assume the FNR = 0 3. quantitative data (e.g., contaminant concentrations expressed as CFU/cm2) when the FNR = 0 or when using statistical sampling methods that account for FNR > 0 4. quantitative data when the FNR > 0 but statistical sampling methods are used that assume the FNR = 0. For Situation 2, the hotspot sampling approach provides for stating with Z% confidence that a hotspot of specified shape and size with detectable contamination will be found. Also for Situation 2, the CJR approach provides for stating with X% confidence that at least Y% of the decision area does not contain detectable contamination. Forms of these statements for the other three situations are discussed in Section 2.2. Statistical methods that account for FNR > 0 currently only exist for the hotspot sampling approach with qualitative data (or quantitative data converted to qualitative data). This report documents the current status of methods and formulas for the hotspot and CJR sampling approaches. Limitations of these methods are identified. Extensions of the methods that are applicable when FNR = 0 to account for FNR > 0, or to address other limitations, will be documented in future revisions of this report if future funding supports the development of such extensions. For quantitative data, this report also presents statistical methods and formulas for 1. quantifying the uncertainty in measured sample results 2. estimating the true surface concentration corresponding to a surface sample 3. quantifying the uncertainty of the estimate of the true surface concentration. All of the methods and formulas discussed in the report were applied to example situations to illustrate application of the methods and interpretation of the results.

Piepel, Gregory F.; Matzke, Brett D.; Sego, Landon H.; Amidan, Brett G.

2013-04-27T23:59:59.000Z

242

On sampling fractions and electron shower shapes  

SciTech Connect (OSTI)

We study the usage of various definitions of sampling fractions in understanding electron shower shapes in a sampling multilayer electromagnetic calorimeter. We show that the sampling fractions obtained by the conventional definition (I) of (average observed energy in layer)/(average deposited energy in layer) will not give the best energy resolution for the calorimeter. The reason for this is shown to be the presence of layer by layer correlations in an electromagnetic shower. The best resolution is obtained by minimizing the deviation from the total input energy using a least squares algorithm. The 'sampling fractions' obtained by this method (II) are shown to give the best resolution for overall energy. We further show that the method (II) sampling fractions are obtained by summing the columns of a non-local {lambda} tensor that incorporates the correlations. We establish that the sampling fractions (II) cannot be used to predict the layer by layer energies and that one needs to employ the full {lambda} tensor for this purpose. This effect is again a result of the correlations.

Peryshkin, Alexander; Raja, Rajendran; /Fermilab

2011-12-01T23:59:59.000Z

243

Decoupled Sampling for Graphics Pipelines  

E-Print Network [OSTI]

We propose a generalized approach to decoupling shading from visibility sampling in graphics pipelines, which we call decoupled sampling. Decoupled sampling enables stochastic supersampling of motion and defocus blur at ...

Ragan-Kelley, Jonathan Millar

244

Sample introducing apparatus and sample modules for mass spectrometer  

DOE Patents [OSTI]

An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus.

Thompson, Cyril V. (Knoxville, TN); Wise, Marcus B. (Kingston, TN)

1993-01-01T23:59:59.000Z

245

Sample introducing apparatus and sample modules for mass spectrometer  

DOE Patents [OSTI]

An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus. 5 figures.

Thompson, C.V.; Wise, M.B.

1993-12-21T23:59:59.000Z

246

History matching and uncertainty quantificiation using sampling method  

E-Print Network [OSTI]

approach to uncertainty quantification for the nonlinear inverse problems. First, we propose a two-stage MCMC approach using sensitivities for quantifying uncertainty in history matching geological models. In the first stage, we compute the acceptance...

Ma, Xianlin

2009-05-15T23:59:59.000Z

247

Method and apparatus for optimized sampling of volatilizable target substances  

DOE Patents [OSTI]

An apparatus for capturing, from gases such as soil gas, target analytes. Target analytes may include emanations from explosive materials or from residues of explosive materials. The apparatus employs principles of sorption common to solid phase microextraction, and is best used in conjunction with analysis means such as a gas chromatograph. To sorb target analytes, the apparatus functions using various sorptive structures to capture target analyte. Depending upon the embodiment, those structures may include a capillary tube including an interior surface on which sorptive material (similar to that on the surface of a SPME fiber) is supported (along with means for moving gases through the capillary tube so that the gases come into close proximity to the sorptive material). In one disclosed embodiment, at least one such sorptive structure is associated with an enclosure including an opening in communication with the surface of a soil region potentially contaminated with buried explosive material such as unexploded ordnance. Emanations from explosive materials can pass into and accumulate in the enclosure where they are sorbed by the sorptive structures. Also disclosed is the use of heating means such as microwave horns to drive target analytes into the soil gas from solid and liquid phase components of the soil.

Lindgren, Eric R.; Phelan, James M.

2004-10-12T23:59:59.000Z

248

Method and apparatus for optimized sampling of volatilizable target substances  

DOE Patents [OSTI]

An apparatus for capturing, from gases such as soil gas, target analytes. Target analytes may include emanations from explosive materials or from residues of explosive materials. The apparatus employs principles of sorption common to solid phase microextraction, and is best used in conjunction with analysis means such as a gas chromatograph. To sorb target analytes, the apparatus functions using various sorptive structures to capture target analyte. Depending upon the embodiment, those structures may include 1) a conventional solid-phase microextraction (SPME) fiber, 2) a SPME fiber suspended in a capillary tube (with means provided for moving gases through the capillary tube so that the gases come into close proximity to the suspended fiber), and 3) a capillary tube including an interior surface on which sorptive material (similar to that on the surface of a SPME fiber) is supported (along with means for moving gases through the capillary tube so that the gases come into close proximity to the sorptive material). In one disclosed embodiment, at least one such sorptive structure is associated with an enclosure including an opening in communication with the surface of a soil region potentially contaminated with buried explosive material such as unexploded ordnance. Emanations from explosive materials can pass into and accumulate in the enclosure where they are sorbed by the sorptive structures. Also disclosed is the use of heating means such as microwave horns to drive target analytes into the soil gas from solid and liquid phase components of the soil.

Lindgren, Eric R. (Albuquerque, NM); Phelan, James M. (Bosque Farms, NM)

2002-01-01T23:59:59.000Z

249

Tissue sampling methods and standards for vertebrate genomics  

E-Print Network [OSTI]

The recent rise in speed and efficiency of new sequencing technologies have facilitated high-throughput sequencing, assembly and analyses of genomes, advancing ongoing efforts to analyze genetic sequences across major vertebrate groups. Standardized...

Wong, Pamela B. Y.; Wiley, Edward O.; Johnson, Warren E.; Ryder, Oliver A.; O'Brien, Stephen; Haussler, David; Koepfli, Klaus-Peter; Houk, Marlys L.; Perelman, Polina; Mastromonaco, Gabriela; Bentley, Andrew C.; Venkatesh, Byrappa; Zhang, Ya-ping; Murphy, Robert W.; G10KCOS

2012-07-12T23:59:59.000Z

250

A comparison of sample-based Stochastic Optimal Control methods  

E-Print Network [OSTI]

Feb 10, 2010 ... Abstract: In this paper, we compare the performance of two ... algorithm and the optimal strategy, as a performance indicator for the two models.

Pierre Girardeau

2010-02-10T23:59:59.000Z

251

Validation of a personal sampling method for 2-ethylhexyl acrylate  

E-Print Network [OSTI]

in copolymer applications. Copolymers with low priced, hard monomers such as vinyl acetat, e, vinyl chloride, methyl methacrylate, and acrylonitrile are used to produce commercial paint latexes, paper and paper board coatings, nonwoven fabric adhesives... present a significant toxicological hazard. The chemical and physi- cal properties of EHA are presented in Table l. Uses of EHA The acrylic monomer esters are versatile raw materials. They 5 have both vinyl and ester functionality and are useful...

Albert, David Lynn

2012-06-07T23:59:59.000Z

252

A method of measuring velocity of sound in soil samples  

E-Print Network [OSTI]

was required to reduce re- ceiver hum. Batteries and amplifier were completely en- closed in a metal case, and the unit was shoclc mounted to prevent, mic ophonics. 'iwo stages of amplification were required to provide sufficient output. Miniature type 1Th... of surplus Navy sonar units were first used as transmitting and receiving transducers. Each of these consisted of a four-crystal mosaic, and was tuned to 3Q kc. When air was used as a medium, an. oscillator signal fed into the transmitter produced a...

Matzen, Walter T

1950-01-01T23:59:59.000Z

253

Sample Size Selection in Optimization Methods for Machine Learning  

E-Print Network [OSTI]

Oct 18, 2011 ... optimization algorithms for machine learning and stochastic ..... stochastic nature of the problem, we could try to derive conditions of the sam-.

2011-10-18T23:59:59.000Z

254

A New Partial Sample Average Approximation Method for Chance ...  

E-Print Network [OSTI]

However, when ? is not small enough, e.g., 0.1, then the obtained solution ... In other words, for not small ...... constraints in hydro power reservoir management.

2014-10-13T23:59:59.000Z

255

Method for the chromatographic separation of cations from aqueous samples  

DOE Patents [OSTI]

An extraction chromatographic material is described for extracting metal cations from a liquid stream. The extraction chromatographic material is prepared by adsorbing a diesterified methanediphosphonic acid on an inert particulate support. 7 figs.

Horwitz, E.P.; Chiarizia, R.; Dietz, M.L.

1997-07-29T23:59:59.000Z

256

Method for the chromatographic separation of cations from aqueous samples  

DOE Patents [OSTI]

An extraction chromatographic material is described for extracting metal cations from a liquid stream. The extraction chromatographic material is prepared by adsorbing a diesterified methane-diphosphonic acid on an inert particulate support. 7 figs.

Horwitz, E.P.; Chiarizia, R.; Dietz, M.L.

1998-12-22T23:59:59.000Z

257

Examination of Hydrate Formation Methods: Trying to Create Representative Samples  

E-Print Network [OSTI]

permeability measurements of gas hydrate-bearing sediments,International Conference on Gas Hydrates, edited, p. 1058,2009), Influence of gas hydrate morphology on the seismic

Kneafsey, T.J.

2012-01-01T23:59:59.000Z

258

Soil Separator and Sampler and Method of Sampling - Energy Innovation  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administrationcontroller systemsBiSite CulturalDepartment ofat HomeAssurance: DOE NSoftwareSoil

259

The Sample Average Approximation Method Applied to Stochastic ...  

E-Print Network [OSTI]

in this section were observed on 350MHz and 450MHz Sun Sparc workstations. ... approach is to generate instances from the TSP library [27] as follows.

2001-08-06T23:59:59.000Z

260

Monte Carlo Sampling-Based Methods for Stochastic Optimization  

E-Print Network [OSTI]

with the goal of introducing the topic to students and researchers and ..... failed to acknowledge in these pages. ... There are of course many topics that are.

2014-01-22T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

Analysis of large soil samples for actinides  

SciTech Connect (OSTI)

A method of analyzing relatively large soil samples for actinides by employing a separation process that includes cerium fluoride precipitation for removing the soil matrix and precipitates plutonium, americium, and curium with cerium and hydrofluoric acid followed by separating these actinides using chromatography cartridges.

Maxwell, III; Sherrod L. (Aiken, SC)

2009-03-24T23:59:59.000Z

262

Particle Size Distribution of Gypseous Samples  

E-Print Network [OSTI]

to conditions in the field. In order to understand the true characterization of the soil and the gypsum particles, the entire soil sample should be analyzed. Four different approaches to the BaCl2 method presented in the literature (Hesse, 1976, Matar...

Arnett, Morgan P.

2010-01-16T23:59:59.000Z

263

Sample holder with optical features  

DOE Patents [OSTI]

A sample holder for holding a sample to be observed for research purposes, particularly in a transmission electron microscope (TEM), generally includes an external alignment part for directing a light beam in a predetermined beam direction, a sample holder body in optical communication with the external alignment part and a sample support member disposed at a distal end of the sample holder body opposite the external alignment part for holding a sample to be analyzed. The sample holder body defines an internal conduit for the light beam and the sample support member includes a light beam positioner for directing the light beam between the sample holder body and the sample held by the sample support member.

Milas, Mirko; Zhu, Yimei; Rameau, Jonathan David

2013-07-30T23:59:59.000Z

264

Sampling in human cognition  

E-Print Network [OSTI]

Bayesian Decision Theory describes optimal methods for combining sparse, noisy data with prior knowledge to build models of an uncertain world and to use those models to plan actions and make novel decisions. Bayesian ...

Vul, Edward

2010-01-01T23:59:59.000Z

265

RAPID DETERMINATION OF RADIOSTRONTIUM IN SEAWATER SAMPLES  

SciTech Connect (OSTI)

A new method for the determination of radiostrontium in seawater samples has been developed at the Savannah River National Laboratory (SRNL) that allows rapid preconcentration and separation of strontium and yttrium isotopes in seawater samples for measurement. The new SRNL method employs a novel and effective pre-concentration step that utilizes a blend of calcium phosphate with iron hydroxide to collect both strontium and yttrium rapidly from the seawater matrix with enhanced chemical yields. The pre-concentration steps, in combination with rapid Sr Resin and DGA Resin cartridge separation options using vacuum box technology, allow seawater samples up to 10 liters to be analyzed. The total {sup 89}Sr + {sup 90}Sr activity may be determined by gas flow proportional counting and recounted after ingrowth of {sup 90}Y to differentiate {sup 89}Sr from {sup 90}Sr. Gas flow proportional counting provides a lower method detection limit than liquid scintillation or Cerenkov counting and allows simultaneous counting of samples. Simultaneous counting allows for longer count times and lower method detection limits without handling very large aliquots of seawater. Seawater samples up to 6 liters may be analyzed using Sr Resin for {sup 89}Sr and {sup 90}Sr with a Minimum Detectable Activity (MDA) of 1-10 mBq/L, depending on count times. Seawater samples up to 10 liters may be analyzed for {sup 90}Sr using a DGA Resin method via collection and purification of {sup 90}Y only. If {sup 89}Sr and other fission products are present, then {sup 91}Y (beta energy 1.55 MeV, 58.5 day half-life) is also likely to be present. {sup 91}Y interferes with attempts to collect {sup 90}Y directly from the seawater sample without initial purification of Sr isotopes first and {sup 90}Y ingrowth. The DGA Resin option can be used to determine {sup 90}Sr, and if {sup 91}Y is also present, an ingrowth option with using DGA Resin again to collect {sup 90}Y can be performed. An MDA for {sup 90}Sr of <1 mBq/L for an 8 hour count may be obtained using 10 liter seawater sample aliquots.

Maxwell, S.

2013-01-16T23:59:59.000Z

266

E-Print Network 3.0 - advanced micro-sample methods Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

of Science and Technology Collection: Computer Technologies and Information Sciences ; Environmental Sciences and Ecology 4 Architecture Architecture Summary: and functionality...

267

Sample Environment Plans and Progress  

E-Print Network [OSTI]

Sample Environment Plans and Progress at the SNS & HFIR SNS HFIR User Group Meeting American Conference on Neutron Scattering Ottawa, Canada June 26 ­ 30, 2010 Lou Santodonato Sample Environment Group our sample environment capabilities Feedback SHUG meetings User surveys Sample Environment Steering

Pennycook, Steve

268

Cleaning method and apparatus  

DOE Patents [OSTI]

A method of very thoroughly and quikcly cleaning a guaze electrode used in chemical analyses is given, as well as an automobile cleaning apparatus which makes use of the method. The method generates very little waste solution, and this is very important in analyzing radioactive materials, especially in aqueous solutions. The cleaning apparatus can be used in a larger, fully automated controlled potential coulometric apparatus. About 99.98% of a 5 mg plutonium sample was removed in less than 3 minutes, using only about 60 ml of rinse solution and two main rinse steps.

Jackson, D.D.; Hollen, R.M.

1981-02-27T23:59:59.000Z

269

Stack sampling apparatus  

SciTech Connect (OSTI)

An apparatus for obtaining samples from a structure includes a support member, at least one stabilizing member, and at least one moveable member. The stabilizing member has a first portion coupled to the support member and a second portion configured to engage with the structure to restrict relative movement between the support member and the structure. The stabilizing member is radially expandable from a first configuration where the second portion does not engage with a surface of the structure to a second configuration where the second portion engages with the surface of the structure.

Lind, Randall F; Lloyd, Peter D; Love, Lonnie J; Noakes, Mark W; Pin, Francois G; Richardson, Bradley S; Rowe, John C

2014-09-16T23:59:59.000Z

270

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado, Disposal

271

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,

272

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,and

273

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOld

274

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOld

275

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOldOld

276

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction,

277

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction,Groundwater and

278

Sample Changes and Issues  

Annual Energy Outlook 2013 [U.S. Energy Information Administration (EIA)]

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) " ,"ClickPipelines AboutDecemberSteamYear Jan FebThousand Cubic Feet)Year JanC.9.3. Receipts8.160Sample

279

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling at

280

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling at4

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling

282

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C. 20545 OCT 28Sacandaga SiteSep NovWater Sampling

283

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C. 20545 OCT 28Sacandaga SiteSep NovWaterSampling

284

RADON 131 7. ANALYTICAL METHODS  

E-Print Network [OSTI]

The purpose of this chapter is to describe the analytical methods that are available for detecting, measuring, and/or monitoring radon and its progeny. The intent is not to provide an exhaustive list of analytical methods. Rather, the intention is to identify well-established methods that are used as the standard methods of analysis. Many of the analytical methods used for environmental samples are the methods approved by federal agencies and organizations such as EPA and the National Institute for Occupational Safety and Health (NIOSH). Other methods presented in this chapter are those that are approved by groups such as the Association of Official Analytical Chemists (AOAC) and the American Public Health Association (APHA). Additionally, analytical methods are included that modify previously used methods to obtain lower detection limits and/or to improve accuracy and precision. 7.1 BIOLOGICAL MATERIALS Table 7-1 lists various methods used to detect radon progeny in biological samples. Since the half-life of radon is short, its measurement in biological samples, such as serum, urine, blood, etc., is not practical. Measurements of the longer lived radon progeny 210 Pb and 210 Po in biological samples may be used as an indication of radon exposure; however, ingestion of these isotopes from food and drinking water or direct exposure from other environmental media are considered the primary sources of exposure for these

unknown authors

285

Sample storage/disposal study  

SciTech Connect (OSTI)

Radioactive waste from defense operations has accumulated at the Hanford Site`s underground waste tanks since the late 1940`s. Each tank must be analyzed to determine whether it presents any harm to the workers at the Hanford Site, the public or the environment. Analyses of the waste aids in the decision making process in preparation of future tank waste stabilization procedures. Characterization of the 177 waste tanks on the Hanford Site will produce a large amount of archived material. This also brings up concerns as to how the excess waste tank sample material from 325 and 222-S Analytical Laboratories will be handled. Methods to archive and/or dispose of the waste have been implemented into the 222-S and 325 Laboratory procedures. As the amount of waste characterized from laboratory analysis grows, an examination of whether the waste disposal system will be able to compensate for this increase in the amount of waste needs to be examined. Therefore, the need to find the safest, most economically sound method of waste storage/disposal is important.

Valenzuela, B.D.

1994-09-29T23:59:59.000Z

286

Fluid sampling tool  

DOE Patents [OSTI]

A fluid sampling tool is described for sampling fluid from a container. The tool has a fluid collecting portion which is drilled into the container wall, thereby affixing it to the wall. The tool may have a fluid extracting section which withdraws fluid collected by the fluid collecting section. The fluid collecting section has a fluted shank with an end configured to drill a hole into a container wall. The shank has a threaded portion for tapping the borehole. The shank is threadably engaged to a cylindrical housing having an inner axial passageway sealed at one end by a septum. A flexible member having a cylindrical portion and a bulbous portion is provided. The housing can be slid into an inner axial passageway in the cylindrical portion and sealed to the flexible member. The bulbous portion has an outer lip defining an opening. The housing is clamped into the chuck of a drill, the lip of the bulbous section is pressed against a container wall until the shank touches the wall, and the user operates the drill. Wall shavings (kerf) are confined in a chamber formed in the bulbous section as it folds when the shank advances inside the container. After sufficient advancement of the shank, an o-ring makes a seal with the container wall. 6 figs.

Garcia, A.R.; Johnston, R.G.; Martinez, R.K.

1999-05-25T23:59:59.000Z

287

Nuclear methods in environmental and energy research  

SciTech Connect (OSTI)

A total of 75 papers were presented on nuclear methods for analysis of environmental and biological samples. Sessions were devoted to software and mathematical methods; nuclear methods in atmospheric and water research; nuclear and atomic methodology; nuclear methods in biology and medicine; and nuclear methods in energy research.

Vogt, J R [ed.

1980-01-01T23:59:59.000Z

288

Prospecting by sampling and analysis of airborne particulates and gases  

DOE Patents [OSTI]

A method is claimed for prospecting by sampling airborne particulates or gases at a ground position and recording wind direction values at the time of sampling. The samples are subsequently analyzed to determine the concentrations of a desired material or the ratios of the desired material to other identifiable materials in the collected samples. By comparing the measured concentrations or ratios to expected background data in the vicinity sampled, one can select recorded wind directions indicative of the upwind position of the land-based source of the desired material.

Sehmel, G.A.

1984-05-01T23:59:59.000Z

289

Performance evaluation soil samples utilizing encapsulation technology  

DOE Patents [OSTI]

Performance evaluation soil samples and method of their preparation uses encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration. 1 fig.

Dahlgran, J.R.

1999-08-17T23:59:59.000Z

290

Performance evaluation soil samples utilizing encapsulation technology  

DOE Patents [OSTI]

Performance evaluation soil samples and method of their preparation using encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration.

Dahlgran, James R. (Idaho Falls, ID)

1999-01-01T23:59:59.000Z

291

Sample LATEXArticle Glenn Murray  

E-Print Network [OSTI]

Test") in Listing 1, with a reference line 4 to the correct line number. This is good for annotating text, but requires a label{} in the code listing; the input method lets the code be updated outside line breaks and a caption on top. Listing 2: Here is another listing.§ ¤ 1 2

292

Fluid sampling tool  

DOE Patents [OSTI]

The invention includes a rotatable tool for collecting fluid through the wall of a container. The tool includes a fluid collection section with a cylindrical shank having an end portion for drilling a hole in the container wall when the tool is rotated, and a threaded portion for tapping the hole in the container wall. A passageway in the shank in communication with at least one radial inlet hole in the drilling end and an opening at the end of the shank is adapted to receive fluid from the container. The tool also includes a cylindrical chamber affixed to the end of the shank opposite to the drilling portion thereof for receiving and storing fluid passing through the passageway. The tool also includes a flexible, deformable gasket that provides a fluid-tight chamber to confine kerf generated during the drilling and tapping of the hole. The invention also includes a fluid extractor section for extracting fluid samples from the fluid collecting section.

Johnston, Roger G. (Los Alamos, NM); Garcia, Anthony R. E. (Espanola, NM); Martinez, Ronald K. (Santa Cruz, NM)

2001-09-25T23:59:59.000Z

293

Specified assurance level sampling procedure  

SciTech Connect (OSTI)

In the nuclear industry design specifications for certain quality characteristics require that the final product be inspected by a sampling plan which can demonstrate product conformance to stated assurance levels. The Specified Assurance Level (SAL) Sampling Procedure has been developed to permit the direct selection of attribute sampling plans which can meet commonly used assurance levels. The SAL procedure contains sampling plans which yield the minimum sample size at stated assurance levels. The SAL procedure also provides sampling plans with acceptance numbers ranging from 0 to 10, thus, making available to the user a wide choice of plans all designed to comply with a stated assurance level.

Willner, O.

1980-11-01T23:59:59.000Z

294

Recent results of the investigation of a micro-fluidic sampling chip and sampling system for hot cell aqueous processing streams  

SciTech Connect (OSTI)

A Fuel Cycle Research and Development project has investigated an innovative sampling method that could evolve into the next generation sampling and analysis system for metallic elements present in aqueous processing streams. Initially sampling technologies were evaluated and micro-fluidic sampling chip technology was selected and tested. A conceptual design for a fully automated microcapillary-based system was completed and a robotic automated sampling system was fabricated. The mechanical and sampling operation of the completed sampling system was investigated. Different sampling volumes have been tested. It appears that the 10 ?l volume has produced data that had much smaller relative standard deviations than the 2 ?l volume. In addition, the production of a less expensive, mass produced sampling chip was investigated to avoid chip reuse thus increasing sampling reproducibility/accuracy. The micro-fluidic-based robotic sampling system's mechanical elements were tested to ensure analytical reproducibility and the optimum robotic handling of micro-fluidic sampling chips. (authors)

Tripp, J.; Smith, T.; Law, J. [Idaho National Laboratory: P.O. Box 1625, Idaho Falls, ID 83415 (United States)

2013-07-01T23:59:59.000Z

295

Radioactive sample effects on EDXRF spectra  

SciTech Connect (OSTI)

Energy dispersive X-ray fluorescence (EDXRF) is a rapid, straightforward method to determine sample elemental composition. A spectrum can be collected in a few minutes or less, and elemental content can be determined easily if there is adequate energy resolution. Radioactive alpha emitters, however, emit X-rays during the alpha decay process that complicate spectral interpretation. This is particularly noticeable when using a portable instrument where the detector is located in close proximity to the instrument analysis window held against the sample. A portable EDXRF instrument was used to collect spectra from specimens containing plutonium-239 (a moderate alpha emitter) and americium-241 (a heavy alpha emitter). These specimens were then analyzed with a wavelength dispersive XRF (WDXRF) instrument to demonstrate the differences to which sample radiation-induced X-ray emission affects the detectors on these two types of XRF instruments.

Worley, Christopher G [Los Alamos National Laboratory

2008-01-01T23:59:59.000Z

296

DWPF SMECT PVV SAMPLE CHARACTERIZATION AND REMEDIATION  

SciTech Connect (OSTI)

On April 2, 2013, a solid sample of material collected from the Defense Waste Processing Facility’s Process Vessel Vent (PVV) jumper for the Slurry Mix Evaporator Condensate Tank (SMECT) was received at the Savannah River National Laboratory (SRNL). DWPF has experienced pressure spikes within the SMECT and other process vessels which have resulted in processing delays while a vacuum was re-established. Work on this sample was requested in a Technical Assistance Request (TAR). This document reports the results of chemical and physical property measurements made on the sample, as well as insights into the possible impact to the material using DWPF’s proposed remediation methods. DWPF was interested in what the facility could expect when the material was exposed to either 8M nitric acid or 90% formic acid, the two materials they have the ability to flush through the PVV line in addition to process water once the line is capped off during a facility outage.

Bannochie, C.; Crawford, C.

2013-06-18T23:59:59.000Z

297

Improved mesh based photon sampling techniques for neutron activation analysis  

SciTech Connect (OSTI)

The design of fusion power systems requires analysis of neutron activation of large, complex volumes, and the resulting particles emitted from these volumes. Structured mesh-based discretization of these problems allows for improved modeling in these activation analysis problems. Finer discretization of these problems results in large computational costs, which drives the investigation of more efficient methods. Within an ad hoc subroutine of the Monte Carlo transport code MCNP, we implement sampling of voxels and photon energies for volumetric sources using the alias method. The alias method enables efficient sampling of a discrete probability distribution, and operates in 0(1) time, whereas the simpler direct discrete method requires 0(log(n)) time. By using the alias method, voxel sampling becomes a viable alternative to sampling space with the 0(1) approach of uniformly sampling the problem volume. Additionally, with voxel sampling it is straightforward to introduce biasing of volumetric sources, and we implement this biasing of voxels as an additional variance reduction technique that can be applied. We verify our implementation and compare the alias method, with and without biasing, to direct discrete sampling of voxels, and to uniform sampling. We study the behavior of source biasing in a second set of tests and find trends between improvements and source shape, material, and material density. Overall, however, the magnitude of improvements from source biasing appears to be limited. Future work will benefit from the implementation of efficient voxel sampling - particularly with conformal unstructured meshes where the uniform sampling approach cannot be applied. (authors)

Relson, E.; Wilson, P. P. H.; Biondo, E. D. [University of Wisconsin-Madison, 1500 Engineering Drive, Madison, WI 53706 (United States)

2013-07-01T23:59:59.000Z

298

Sampling for Bacteria in Wells  

E-Print Network [OSTI]

This publication will instruct you on the proper procedures for collecting a sample from a water well for bacteriological analysis....

Lesikar, Bruce J.

2001-11-15T23:59:59.000Z

299

Sample Residential Program Term Sheet  

Broader source: Energy.gov (indexed) [DOE]

Goal DRAFT U.S. DOE Sample Residential Program Term Sheet - DRAFT Introduction is seeking to develop an energy...

300

Correlation methods  

SciTech Connect (OSTI)

Correlation methods have been developed to provide a quick and relatively simple technique for estimating the performance of passive solar systems. The correlations are done with respect to data generated from simulation models. The techniques and accuracies are described. Both the Solar Load Ratio and Un-Utilizability methods are described. The advantages and limitations of correlation methods as design tools are discussed.

Balcomb, J.D.

1981-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

B-Cell waste classification sampling and analysis plan  

SciTech Connect (OSTI)

This report documents the methods used to collect and analyze samples to obtain data necessary to verify and/or determine the radionuclide content of the 324 Facility B-Cell decontamination and decommissioning waste stream.

HOBART, R.L.

1999-09-22T23:59:59.000Z

302

Embed and Project: Discrete Sampling with Universal Hashing  

E-Print Network [OSTI]

Embed and Project: Discrete Sampling with Universal Hashing Stefano Ermon, Carla P. Gomes Dept Markov Chain Monte Carlo (MCMC) methods. MCMC techniques are a specialized form of local search that only

Bejerano, Gill

303

Probe for high resolution NMR with sample reorientation  

DOE Patents [OSTI]

An improved NMR probe and method are described which substantially improve the resolution of NMR measurements made on powdered or amorphous or otherwise orientationally disordered samples. The apparatus mechanically varies the orientation of the sample such that the time average of two or more sets of spherical harmonic functions are zero.

Pines, Alexander (Berkeley, CA); Samoson, Ago (Tallinn, SU)

1990-01-01T23:59:59.000Z

304

Probe for high resolution NMR with sample reorientation  

DOE Patents [OSTI]

An improved NMR probe and method are described which substantially improve the resolution of NMR measurements made on powdered or amorphous or otherwise orientationally disordered samples. The apparatus mechanically varies the orientation of the sample such that the time average of two or more sets of spherical harmonic functions are zero. 8 figs.

Pines, A.; Samoson, A.

1990-02-06T23:59:59.000Z

305

Asymmetric Nested Lattice Samples Peter Z. G. Qian1  

E-Print Network [OSTI]

Asymmetric Nested Lattice Samples Peter Z. G. Qian1 , Mingyao Ai2,3 , Youngdeok Hwang1 and Heng Su4-filling designs, called asymmetric nested lattice samples. As a stepping-stone to the proposed approach, we introduce two methods for generating asymmetric nested orthogonal arrays. We then present two elaborate

Qian, Peter Z. G.

306

384 Power plant waste water sampling and analysis plan  

SciTech Connect (OSTI)

This document presents the 384 Power House Sampling and Analysis Plan. The Plan describes sampling methods, locations, frequency, analytes, and stream descriptions. The effluent streams from 384, were characterized in 1989, in support of the Stream Specific Report (WHC-EP-0342, Addendum 1).

Hagerty, K.J.; Knotek, H.M.

1995-01-01T23:59:59.000Z

307

Efficient Sampling of Protein Folding Pathways using HMMSTR and Probabilistic Roadmaps  

E-Print Network [OSTI]

of the samples to minimize van der Waals collisions (VDW), radius of gyration (RG) and hydrogen bond energy (HBEEfficient Sampling of Protein Folding Pathways using HMMSTR and Probabilistic Roadmaps *Yogesh A methods have used the knowledge of the true structure to sample conformational space. Our method uses only

Bystroff, Chris

308

Method and apparatus for measuring nuclear magnetic properties  

DOE Patents [OSTI]

A method for studying the chemical and structural characteristics of materials is disclosed. The method includes placement of a sample material in a high strength polarizing magnetic field to order the sample nuclei. The condition used to order the sample is then removed abruptly and the ordering of the sample allowed to evolve for a time interval. At the end of the time interval, the ordering of the sample is measured by conventional nuclear magnetic resonance techniques. 5 figs.

Weitekamp, D.P.; Bielecki, A.; Zax, D.B.; Zilm, K.W.; Pines, A.

1987-12-01T23:59:59.000Z

309

Post-Award Deliverables Sample (Second Part of Sample Deliverables...  

Broader source: Energy.gov (indexed) [DOE]

Task Orders (IDIQ Attachment. J-4) Sample Statement of Work - Standard Service Offerings for Contractor-Identified Project ESPC TASK ORDER REQUEST FOR PROPOSAL (TO RFP) TEMPLATE...

310

E-Print Network 3.0 - apparent specific volume Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

of Z .sampling technique, specifically small- bottles and Zlarge-volume in situ pumps and large-volume... in samples collected using small- and large-volume methods: the...

311

Application of conditional sampling for measuring ecosystem-scale carbon dioxide exchange in coastal wetlands  

E-Print Network [OSTI]

and seasonal carbon cycles in these ecosystems as well as the response of these systems to environmental change. One convenient method for continuously measuring CER in remote ecosystems is tower-based conditional sampling. With conditional sampling, CER...

Cobos, Douglas Russell

2012-06-07T23:59:59.000Z

312

E-Print Network 3.0 - analytical methods methods Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

of Marine Benthic Ecology and Evolution, Collection: Biology and Medicine ; Environmental Sciences and Ecology 12 Multicriteria analysis problems Multicriteria analysis problem may...

313

Adaptive Sampling for Environmental Robotics  

E-Print Network [OSTI]

186, 2003. S. Thrun, “Robotics Mapping: A survey”, Exploringtechnique to environmental robotics applications includingSampling for Environmental Robotics Mohammad Rahimi †,‡‡ ,

Mohammad Rahimi; Richard Pon; Deborah Estrin; William J. Kaiser; Mani Srivastava; Gaurav S. Sukhatme

2003-01-01T23:59:59.000Z

314

Sample Residential Program Term Sheet  

Broader source: Energy.gov [DOE]

A sample for defining and elaborating on the specifics of a clean energy loan program. Author: U.S. Department of Energy

315

Homeowner Soil Sample Information Form  

E-Print Network [OSTI]

Homeowners should submit this form with their soil samples when requesting a soil test from the Texas A&M Soil Testing Laboratory....

Provin, Tony

2007-04-11T23:59:59.000Z

316

Elimination of ``memory`` from sample handling and inlet system of a mass spectrometer  

DOE Patents [OSTI]

This paper describes a method for preparing the sample handling and inlet system of a mass spectrometer for analysis of a subsequent sample following analysis of a previous sample comprising the flushing of the system interior with supercritical CO{sub 2} and venting the interior. The method eliminates the effect of system ``memory`` on the subsequent analysis, especially following persistent samples such as xenon and krypton.

Chastgner, P.

1991-05-08T23:59:59.000Z

317

Monte Carlo stratified source-sampling  

SciTech Connect (OSTI)

In 1995, at a conference on criticality safety, a special session was devoted to the Monte Carlo {open_quotes}eigenvalue of the world{close_quotes} problem. Argonne presented a paper, at that session, in which the anomalies originally observed in that problem were reproduced in a much simplified model-problem configuration, and removed by a version of stratified source-sampling. The original test-problem was treated by a special code designed specifically for that purpose. Recently ANL started work on a method for dealing with more realistic eigenvalue of the world configurations, and has been incorporating this method into VIM. The original method has been modified to take into account real-world statistical noise sources not included in the model problem. This paper constitutes a status report on work still in progress.

Blomquist, R.N.; Gelbard, E.M.

1997-09-01T23:59:59.000Z

318

Enhanced AFCI Sampling, Analysis, and Safeguards Technology Review  

SciTech Connect (OSTI)

The focus of this study includes the investigation of sampling technologies used in industry and their potential application to nuclear fuel processing. The goal is to identify innovative sampling methods using state of the art techniques that could evolve into the next generation sampling and analysis system for metallic elements. Sampling and analysis of nuclear fuel recycling plant processes is required both to monitor the operations and ensure Safeguards and Security goals are met. In addition, environmental regulations lead to additional samples and analysis to meet licensing requirements. The volume of samples taken by conventional means, can restrain productivity while results samples are analyzed, require process holding tanks that are sized to meet analytical issues rather than process issues (and that create a larger facility footprint), or, in some cases, simply overwhelm analytical laboratory capabilities. These issues only grow when process flowsheets propose new separations systems and new byproduct material for transmutation purposes. Novel means of streamlining both sampling and analysis are being evaluated to increase the efficiency while meeting all requirements for information. This report addresses just a part of the effort to develop and study novel methods by focusing on the sampling and analysis of aqueous samples for metallic elements. It presents an overview of the sampling requirements, including frequency, sensitivity, accuracy, and programmatic drivers, to demonstrate the magnitude of the task. The sampling and analysis system needed for metallic element measurements is then discussed, and novel options being applied to other industrial analytical needs are presented. Inductively coupled mass spectrometry instruments are the most versatile for metallic element analyses and are thus chosen as the focus for the study. Candidate novel means of process sampling, as well as modifications that are necessary to couple such instruments to introduce these samples, are discussed. A suggested path forward based on an automated microchip capillary based sampling system interfaced to the analysis spectrometer is presented. The ability to obtain micro liter volume samples coupled with remote automated means of sample tracking and transport to the instrument would greatly improve analytical efficiency while reducing both personnel exposure and radioactive waste. Application of this sampling technique to new types of mass spectrometers for selective elemental isotopic analysis could also provide significant improvements in safeguards and security analyses.

John Svoboda

2009-09-01T23:59:59.000Z

319

Database Sampling with Functional Dependencies  

E-Print Network [OSTI]

Database Sampling with Functional Dependencies Jes´us Bisbal, Jane Grimson Department of Computer there is a need to prototype the database which the applications will use when in operation. A prototype database can be built by sampling data from an existing database. Including relevant semantic information when

Riera, Jesús Bisbal

320

Sample push-out fixture  

DOE Patents [OSTI]

This invention generally relates to the remote removal of pelletized samples from cylindrical containment capsules. V-blocks are used to receive the samples and provide guidance to push out rods. Stainless steel liners fit into the v-channels on the v-blocks which permits them to be remotely removed and replaced or cleaned to prevent cross contamination between capsules and samples. A capsule holder securely holds the capsule while allowing manual up/down and in/out movement to align each sample hole with the v-blocks. Both end sections contain identical v-blocks; one that guides the drive out screw and rods or manual push out rods and the other to receive the samples as they are driven out of the capsule.

Biernat, John L. (Scotia, NY)

2002-11-05T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

Methods for making nucleotide probes for sequencing and synthesis  

DOE Patents [OSTI]

Compositions and methods for making a plurality of probes for analyzing a plurality of nucleic acid samples are provided. Compositions and methods for analyzing a plurality of nucleic acid samples to obtain sequence information in each nucleic acid sample are also provided.

Church, George M; Zhang, Kun; Chou, Joseph

2014-07-08T23:59:59.000Z

322

MERCURY AND LEAD SAMPLING AT MINNESOTA POWER'S BOSWELL ENERGY CENTER  

SciTech Connect (OSTI)

At the request of the Minnesota Power, Inc., the Energy & Environmental Research Center (EERC) sampled for lead at the stack (or duct directly leading to the stack) for three units at the Boswell Energy Center. All sampling was done in triplicate using U.S. Environmental Protection Agency (EPA) Method 12, with sampling procedures following EPA Methods 1 through 4. During the test program, lead sampling was done using EPA Method 12 in the duct at the outlet of the baghouse serving Unit 2 and the duct at the outlet of the wet particulate scrubber serving Unit 3. For Unit 4, lead sampling was done at the stack. The specific objective for the project was to determine the concentration of lead in the flue gas being emitted into the atmosphere from the Boswell Energy Center. The test program was performed during the period of May 8 through 11, 2000. This report presents the test data, sample calculations, and results, and a discussion of the lead sampling performed at the Boswell Energy Center. The detailed test data and test results, raw test data, process data, laboratory reports, and equipment calibration records are provided in Appendices A, B, and C.

Dennis L. Laudal

2000-08-01T23:59:59.000Z

323

E-Print Network 3.0 - artery infusion chemotherapy Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

infusion chemotherapy Search Powered by Explorit Topic List Advanced Search Sample search results for: artery infusion chemotherapy Page: << < 1 2 3 4 5 > >> 1 Optical method for...

324

E-Print Network 3.0 - asteroid collision risk Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

and of the Summary: ; methods to estimate risk of asteroid collisions with the Earth. 12;... planets sample and of the selection effects involved in asteroid discoveries;...

325

E-Print Network 3.0 - a-exposed atlantic cod Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

326

E-Print Network 3.0 - atlantic cod pineal Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

327

E-Print Network 3.0 - atlantic cod piscidin Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

328

E-Print Network 3.0 - anodic stripping square Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Search Sample search results for: anodic stripping square Page: << < 1 2 3 4 5 > >> 1 Nuclear Instruments and Methods in Physics Research A 554 (2005) 291299 Characteristics of...

329

E-Print Network 3.0 - anterolateral talar facet Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

an initial sample of extant hominoids. We use the tibial and talar components of the ankle joint... - etry and morphology. Methods utilized include: digitization of joint facets...

330

E-Print Network 3.0 - ankle magnetic resonance Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Search Powered by Explorit Topic List Advanced Search Sample search results for: ankle magnetic resonance Page: << < 1 2 3 4 5 > >> 1 Evaluation of Methods That Locate the...

331

E-Print Network 3.0 - actinides phosphinic resins Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Databases and Resources 11 Development of an Automatic Method for Americium and Plutonium Separation and Summary: tetravalent and hexavalent actinides present in the real sample,...

332

E-Print Network 3.0 - airborne ultrasound technology Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

ultrasound technology Search Powered by Explorit Topic List Advanced Search Sample search results for: airborne ultrasound technology Page: << < 1 2 3 4 5 > >> 1 Non-contact Method...

333

Sample rotating turntable kit for infrared spectrometers  

DOE Patents [OSTI]

An infrared spectrometer sample rotating turntable kit has a rotatable sample cup containing the sample. The infrared spectrometer has an infrared spectrometer probe for analyzing the sample and the rotatable sample cup is adapted to receive the infrared spectrometer probe. A reflectance standard is located in the rotatable sample cup. A sleeve is positioned proximate the sample cup and adapted to receive the probe. A rotator rotates the rotatable sample cup. A battery is connected to the rotator.

Eckels, Joel Del (Livermore, CA); Klunder, Gregory L. (Oakland, CA)

2008-03-04T23:59:59.000Z

334

Estimating Methods  

Broader source: Directives, Delegations, and Requirements [Office of Management (MA)]

Based on the project's scope, the purpose of the estimate, and the availability of estimating resources, the estimator can choose one or a combination of techniques when estimating an activity or project. Estimating methods, estimating indirect and direct costs, and other estimating considerations are discussed in this chapter.

1997-03-28T23:59:59.000Z

335

Characterization methods  

SciTech Connect (OSTI)

Methods discussed in this compilation of notes and diagrams are Raman spectroscopy, scanning electron microscopy, transmission electron microscopy, and other surface analysis techniques (auger electron spectroscopy, x-ray photoelectron spectroscopy, electron energy loss spectroscopy, and scanning tunnelling microscopy). A comparative evaluation of different techniques is performed. In-vacuo and in-situ analyses are described.

Glass, J.T. [North Carolina State Univ., Raleigh (United States)

1993-01-01T23:59:59.000Z

336

RAPID DETERMINATION OF {sup 210} PO IN WATER SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that can be used for emergency response or routine water analyses. If a radiological dispersive device (RDD) event or a radiological attack associated with drinking water supplies occurs, there will be an urgent need for rapid analyses of water samples, including drinking water, ground water and other water effluents. Current analytical methods for the assay of {sup 210}Po in water samples have typically involved spontaneous auto-deposition of {sup 210}Po onto silver or other metal disks followed by counting by alpha spectrometry. The auto-deposition times range from 90 minutes to 24 hours or more, at times with yields that may be less than desirable. If sample interferences are present, decreased yields and degraded alpha spectrums can occur due to unpredictable thickening in the deposited layer. Separation methods have focused on the use of Sr Resin?, often in combination with 210Pb analysis. A new rapid method for {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that utilizes a rapid calcium phosphate co-precipitation method, separation using DGA Resin? (N,N,N?,N? tetraoctyldiglycolamide extractant-coated resin, Eichrom Technologies or Triskem-International), followed by rapid microprecipitation of {sup 210}Po using bismuth phosphate for counting by alpha spectrometry. This new method can be performed quickly with excellent removal of interferences, high chemical yields and very good alpha peak resolution, eliminating any potential problems with the alpha source preparation for emergency or routine samples. A rapid sequential separation method to separate {sup 210} Po and actinide isotopes was also developed. This new approach, rapid separation with DGA Resin plus microprecipitation for alpha source preparation, is a significant advance in radiochemistry for the rapid determination of {sup 210}Po.

Maxwell, S.

2013-05-22T23:59:59.000Z

337

Sample Business Plan Framework 3  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

338

Sample Business Plan Framework 2  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

339

Sample Business Plan Framework 4  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

340

Sample Business Plan Framework 1  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Sampling based on local bandwidth  

E-Print Network [OSTI]

The sampling of continuous-time signals based on local bandwidth is considered in this thesis. In an intuitive sense, local bandwidth refers to the rate at which a signal varies locally. One would expect that signals should ...

Wei, Dennis

2007-01-01T23:59:59.000Z

342

Depth-discrete sampling port  

DOE Patents [OSTI]

A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

Pemberton, Bradley E. (Aiken, SC); May, Christopher P. (Columbia, MD); Rossabi, Joseph (Aiken, SC); Riha, Brian D. (Augusta, GA); Nichols, Ralph L. (North Augusta, SC)

1999-01-01T23:59:59.000Z

343

Depth-discrete sampling port  

DOE Patents [OSTI]

A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

Pemberton, Bradley E. (Aiken, SC); May, Christopher P. (Columbia, MD); Rossabi, Joseph (Aiken, SC); Riha, Brian D. (Augusta, GA); Nichols, Ralph L. (North Augusta, SC)

1998-07-07T23:59:59.000Z

344

Case depth verification of hardened samples with Barkhausen noise sweeps  

SciTech Connect (OSTI)

An interesting topic of recent Barkhausen noise (BN) method studies is the application of the method to case depth evaluation of hardened components. The utilization of BN method for this purpose is based on the difference in the magnetic properties between the hardened case and the soft core. Thus, the detection of case depth with BN can be achieved. The measurements typically have been carried out by using low magnetizing frequencies which have deeper penetration to the ferromagnetic samples than the conventional BN measurement. However, the penetration depth is limited due to eddy current damping of the signal. We introduce here a newly found sweep measurement concept for the case depth evaluation. In this study sweep measurements were carried out with various magnetizing frequencies and magnetizing voltages to detect the effect of different frequency and voltage and their correspondence to the actual case depth values verified from destructive characterization. Also a BN measurement device that has an implemented sweep analysis option was utilised. The samples were either induction or case-hardened samples and sample geometry contained both rod samples and gear axle samples with different case depth values. Samples were also further characterized with Xray diffraction to study the residual stress state of the surface. The detailed data processing revealed that also other calculated features than the maximum slope division of the 1st derivative of the BN signal could hold the information about the case depth value of the samples. The sweep method was able to arrange the axles into correct order according to the case depth value even though the axles were used.

Santa-aho, Suvi; Vippola, Minnamari; Lepistö, Toivo [Tampere University of Technology, Department of Materials Science, P.O. Box 589, 33101 Tampere (Finland); Hakanen, Merja [Stresstech Oy, Tikkutehtaantie 1, 40800 Vaajakoski (Finland); Sorsa, Aki; Leiviskä, Kauko [University of Oulu, Control Engineering Laboratory, P.O. Box 4300, FIN-90014 University of Oulu (Finland)

2014-02-18T23:59:59.000Z

345

Determination of actinides in urine and fecal samples  

DOE Patents [OSTI]

A method of determining the radioactivity of specific actinides that are carried in urine or fecal sample material is disclosed. The samples are ashed in a muffle furnace, dissolved in an acid, and then treated in a series of steps of reduction, oxidation, dissolution, and precipitation, including a unique step of passing a solution through a chloride form anion exchange resin for separation of uranium and plutonium from americium.

McKibbin, Terry T. (Larimer County, CO)

1993-01-01T23:59:59.000Z

346

Determination of actinides in urine and fecal samples  

DOE Patents [OSTI]

A method of determining the radioactivity of specific actinides that are carried in urine or fecal sample material is disclosed. The samples are ashed in a muffle furnace, dissolved in an acid, and then treated in a series of steps of reduction, oxidation, dissolution, and precipitation, including a unique step of passing a solution through a chloride form anion exchange resin for separation of uranium and plutonium from americium.

McKibbin, T.T.

1993-03-02T23:59:59.000Z

347

Ion sensing method  

DOE Patents [OSTI]

The present invention allows the determination of trace levels of ionic substances in a sample solution (ions, metal ions, and other electrically charged molecules) by coupling a separation method, such as liquid chromatography, with ion selective electrodes (ISE) prepared so as to allow detection at activities below 10.sup.-6 M. The separation method distributes constituent molecules into fractions due to unique chemical and physical properties, such as charge, hydrophobicity, specific binding interactions, or movement in an electrical field. The separated fractions are detected by means of the ISE(s). These ISEs can be used singly or in an array. Accordingly, modifications in the ISEs are used to permit detection of low activities, specifically, below 10.sup.-6 M, by using low activities of the primary analyte (the molecular species which is specifically detected) in the inner filling solution of the ISE. Arrays constructed in various ways allow flow-through sensing for multiple ions.

Smith, Richard Harding; Martin, Glenn Brian

2004-05-18T23:59:59.000Z

348

Characterization of various bitumen samples from tar sands  

SciTech Connect (OSTI)

The authors have investigated twenty three bitumen samples obtained using different separation methods such as: ultracentrifugation, Dean-Stark extraction, solvent extraction employing vigorous agitation, hot water separation and the Solvent Extraction Spherical Agglomeration technique. These samples were extracted from oil sand feedstocks of different grades, Suncor sludge pond tailings and mineral agglomerates obtained form the Solvent Extraction Spherical Agglomeration process. All of the bitumen samples were examined on a comparative basis using various analytical techniques. These included: fractionation into asphaltenes and maltenes: elemental analyses; molecular weight determination using vapour pressure osmometry and gel permeation chromatography, infrared, proton and /sup 13/C nuclear magnetic resonance spectroscopy. Proton /sup 13/C n.m.r. spectroscopic data were used to determine the distribution of various types of hydrogens and carbons in the samples. These data were also used to derive various molecular parameters in order to investigate average molecular structures of different bitumen samples and some of their asphaltene fractions.

Majid, A.; Bornais, J.; Hutchison, R.A. (National Research Council of Canada, Ottawa, ON (Canada). Div. of Chemistry)

1989-01-01T23:59:59.000Z

349

Freeze chromatography method and apparatus  

DOE Patents [OSTI]

A freeze chromatography method and apparatus are provided which enable separation of the solutes contained in a sample. The apparatus includes an annular column construction comprising cylindrical inner and outer surfaces defining an annular passage therebetween. One of the surfaces is heated and the other cooled while passing an eluent through the annular passageway so that the eluent in contact with the cooled surface freezes and forms a frozen eluent layer thereon. A mixture of solutes dissolved in eluent is passed through the annular passageway in contact with the frozen layer so that the sample solutes in the mixture will tend to migrate either toward or away the frozen layer. The rate at which the mixture flows through the annular passageway is controlled so that the distribution of the sample solutes approaches that at equilibrium and thus a separation between the sample solutes occurs. 3 figs.

Scott, C.D.

1987-04-16T23:59:59.000Z

350

The IRAS Revised Bright Galaxy Sample (RBGS)  

E-Print Network [OSTI]

IRAS flux densities, redshifts, and infrared luminosities are reported for all sources identified in the IRAS Revised Bright Galaxy Sample (RBGS), a complete flux-limited survey of all extragalactic objects with total 60 micron flux density greater than 5.24 Jy, covering the entire sky surveyed by IRAS at Galactic latitude |b| > 5 degrees. The RBGS includes 629 objects, with a median (mean) sample redshift of 0.0082 (0.0126) and a maximum redshift of 0.0876. The RBGS supersedes the previous two-part IRAS Bright Galaxy Samples, which were compiled before the final ("Pass 3") calibration of the IRAS Level 1 Archive in May 1990. The RBGS also makes use of more accurate and consistent automated methods to measure the flux of objects with extended emission. Basic properties of the RBGS sources are summarized, including estimated total infrared luminosities, as well as updates to cross-identifications with sources from optical galaxy catalogs established using the NASA/IPAC Extragalactic Database (NED). In addition...

Sanders, D B; Kim, D C; Surace, J A; Soifer, B T

2003-01-01T23:59:59.000Z

351

RAPID DETERMINATION OF RA-226 IN ENVIRONMENTAL SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of {sup 226}Ra in environmental samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used for emergency response or routine sample analyses. The need for rapid analyses in the event of a Radiological Dispersive Device or Improvised Nuclear Device event is well-known. In addition, the recent accident at Fukushima Nuclear Power Plant in March, 2011 reinforces the need to have rapid analyses for radionuclides in environmental samples in the event of a nuclear accident. {sup 226}Ra (T1/2 = 1,620 years) is one of the most toxic of the long-lived alpha-emitters present in the environment due to its long life and its tendency to concentrate in bones, which increases the internal radiation dose of individuals. The new method to determine {sup 226}Ra in environmental samples utilizes a rapid sodium hydroxide fusion method for solid samples, calcium carbonate precipitation to preconcentrate Ra, and rapid column separation steps to remove interferences. The column separation process uses cation exchange resin to remove large amounts of calcium, Sr Resin to remove barium and Ln Resin as a final purification step to remove {sup 225}Ac and potential interferences. The purified {sup 226}Ra sample test sources are prepared using barium sulfate microprecipitation in the presence of isopropanol for counting by alpha spectrometry. The method showed good chemical recoveries and effective removal of interferences. The determination of {sup 226}Ra in environmental samples can be performed in less than 16 h for vegetation, concrete, brick, soil, and air filter samples with excellent quality for emergency or routine analyses. The sample preparation work takes less than 6 h. {sup 225}Ra (T1/2 = 14.9 day) tracer is used and the {sup 225}Ra progeny {sup 217}At is used to determine chemical yield via alpha spectrometry. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory radium particles are effectively digested. The preconcentration and column separation steps can also be applied to aqueous samples with good results.

Maxwell, S.

2012-01-03T23:59:59.000Z

352

High throughput analysis of samples in flowing liquid  

DOE Patents [OSTI]

Apparatus and method enable imaging multiple fluorescent sample particles in a single flow channel. A flow channel defines a flow direction for samples in a flow stream and has a viewing plane perpendicular to the flow direction. A laser beam is formed as a ribbon having a width effective to cover the viewing plane. Imaging optics are arranged to view the viewing plane to form an image of the fluorescent sample particles in the flow stream, and a camera records the image formed by the imaging optics.

Ambrose, W. Patrick (Los Alamos, NM); Grace, W. Kevin (Los Alamos, NM); Goodwin, Peter M. (Los Alamos, NM); Jett, James H. (Los Alamos, NM); Orden, Alan Van (Fort Collins, CO); Keller, Richard A. (White Rock, NM)

2001-01-01T23:59:59.000Z

353

Waste minimization in analytical chemistry through innovative sample preparation techniques.  

SciTech Connect (OSTI)

Because toxic solvents and other hazardous materials are commonly used in analytical methods, characterization procedures result in significant and costly amount of waste. We are developing alternative analytical methods in the radiological and organic areas to reduce the volume or form of the hazardous waste produced during sample analysis. For the radiological area, we have examined high-pressure, closed-vessel microwave digestion as a way to minimize waste from sample preparation operations. Heated solutions of strong mineral acids can be avoided for sample digestion by using the microwave approach. Because reactivity increases with pressure, we examined the use of less hazardous solvents to leach selected contaminants from soil for subsequent analysis. We demonstrated the feasibility of this approach by extracting plutonium from a NET reference material using citric and tartaric acids with microwave digestion. Analytical results were comparable to traditional digestion methods, while hazardous waste was reduced by a factor often. We also evaluated the suitability of other natural acids, determined the extraction performance on a wider variety of soil types, and examined the extraction efficiency of other contaminants. For the organic area, we examined ways to minimize the wastes associated with the determination of polychlorinated biphenyls (PCBs) in environmental samples. Conventional methods for analyzing semivolatile organic compounds are labor intensive and require copious amounts of hazardous solvents. For soil and sediment samples, we have a method to analyze PCBs that is based on microscale extraction using benign solvents (e.g., water or hexane). The extraction is performed at elevated temperatures in stainless steel cells containing the sample and solvent. Gas chromatography-mass spectrometry (GC/MS) was used to quantitate the analytes in the isolated extract. More recently, we developed a method utilizing solid-phase microextraction (SPME) for natural water samples. In this SPME technique, a fused-silica fiber coated with a polymeric film is exposed to the sample, extraction is allowed to take place, and then the analytes are thermally desorbed for GC analysis. Unlike liquid-liquid extraction or solid-phase extraction, SPME consumes all of the extracted sample in the analysis, significantly reducing the required sample volume.

Smith, L. L.

1998-05-28T23:59:59.000Z

354

High-Throughput Mode Liquid Microjunction Surface Sampling Probe  

SciTech Connect (OSTI)

A simple and automated spot sampling operation mode for a liquid microjunction surface sampling probe/electrospray ionization mass spectrometry (LMJ-SSP/ESI-MS) system is reported. Prior manual and automated spot sampling methods with this probe relied on a careful, relatively slow alignment of the probe and surface distance (<20 m spacing) to form the probe-to-surface liquid microjunction critical to successful surface sampling. Moreover, sampling multiple spots required retraction of the surface from the probe and a repeat of this careful probe-to-surface distance alignment at the next sampling position. With the method described here, the probe was not positioned as close to the surface, the exact probeto-surface positioning was found to be less critical (spanning distances from about 100-300 m), and this distance was not altered during the sampling of an entire array of sample spots. With the probe positioned within the appropriate distance from the surface, the liquid microjunction was formed by letting the liquid from the sampling end of the probe extend out from the probe to the surface. This was accomplished by reducing the selfaspiration liquid flow rate of the probe to a value less than the volume flow rate pumped into the probe. When the self-aspiration rate of the probe was subsequently increased, analytes on the surface that dissolved at the liquid microjunction were aspirated back into the probe with the liquid that created the liquid microjunction and electrosprayed. Presented here are the basics of this new sampling mode, as well as data that illustrate the potential analytical capabilities of the device to conduct highthroughput quantitative analysis.

Van Berkel, Gary J [ORNL; Kertesz, Vilmos [ORNL; King, Richard C. [PharmaCadence

2009-01-01T23:59:59.000Z

355

Enhanced Sampling and Analysis, Selection of Technology for Testing  

SciTech Connect (OSTI)

The focus of this study includes the investigation of sampling technologies used in industry and their potential application to nuclear fuel processing. The goal is to identify innovative sampling methods using state of the art techniques that could evolve into the next generation sampling and analysis system for metallic elements. This report details the progress made in the first half of FY 2010 and includes a further consideration of the research focus and goals for this year. Our sampling options and focus for the next generation sampling method are presented along with the criteria used for choosing our path forward. We have decided to pursue the option of evaluating the feasibility of microcapillary based chips to remotely collect, transfer, track and supply microliters of sample solutions to analytical equipment in support of aqueous processes for used nuclear fuel cycles. Microchip vendors have been screened and a choice made for the development of a suitable microchip design followed by production of samples for evaluation by ANL, LANL, and INL on an independent basis.

Svoboda, John; Meikrantz, David

2010-02-01T23:59:59.000Z

356

Sampling for Beryllium Surface Contamination using Wet, Dry and Alcohol Wipe Sampling  

SciTech Connect (OSTI)

This research project was conducted at the National Nuclear Security Administration's Kansas City Plant, operated by Honeywell Federal Manufacturing and Technologies, in conjunction with the Safety Sciences Department of Central Missouri State University, to compare relative removal efficiencies of three wipe sampling techniques currently used at Department of Energy facilities. Efficiencies of removal of beryllium contamination from typical painted surfaces were tested by wipe sampling with dry Whatman 42 filter paper, with water-moistened (Ghost Wipe) materials, and by methanol-moistened wipes. Test plates were prepared using 100 mm X 15 mm Pyrex Petri dishes with interior surfaces spray painted with a bond coat primer. To achieve uniform deposition over the test plate surface, 10 ml aliquots of solution containing 1 beryllium and 0.1 ml of metal working fluid were transferred to the test plates and subsequently evaporated. Metal working fluid was added to simulate the slight oiliness common on surfaces in metal working shops where fugitive oil mist accumulates over time. Sixteen test plates for each wipe method (dry, water, and methanol) were processed and sampled using a modification of wiping patterns recommended by OSHA Method 125G. Laboratory and statistical analysis showed that methanol-moistened wipe sampling removed significantly more (about twice as much) beryllium/oil-film surface contamination as water-moistened wipes (p< 0.001), which removed significantly more (about twice as much) residue as dry wipes (p <0.001). Evidence for beryllium sensitization via skin exposure argues in favor of wipe sampling with wetting agents that provide enhanced residue removal efficiency.

Kerr, Kent

2004-12-17T23:59:59.000Z

357

Wood elastic characterization from a single sample by resonant ultrasound spectroscopy  

E-Print Network [OSTI]

Wood elastic characterization from a single sample by resonant ultrasound spectroscopy R. Longoa materials such as wood using only one sample. To do so, two complementary methods are used. First, the wood: Resonant ultrasound spectroscopy, spherical and cubic samples, wood, elastic constants 1. Introduction Wood

Paris-Sud XI, Université de

358

JOINT STOCHASTIC SAMPLING FOR RNA SECONDARY STRUCTURE PREDICTION Arif Ozgun Harmanci1  

E-Print Network [OSTI]

sequence [5]. Stochastic sampling operates by sam- pling the set of possible secondary structures of an RNAJOINT STOCHASTIC SAMPLING FOR RNA SECONDARY STRUCTURE PREDICTION Arif Ozgun Harmanci1 , Gaurav improvements over methods that operate on single sequences (See [4] for a review). Stochastic sampling has

Sharma, Gaurav

359

Investigations in the Monte-Carlo sampling for interconnected power systems reliability evaluation  

E-Print Network [OSTI]

. The new approach keeps track of the probability of the unclassified states to keep the error under a specified fraction of the loss of load probability. There are two methods to select a sample state from a set, uniform sampling and proportional sampling...

Feng, Chun

1993-01-01T23:59:59.000Z

360

Image portion identification methods, image parsing methods, image parsing systems, and articles of manufacture  

DOE Patents [OSTI]

Image portion identification methods, image parsing methods, image parsing systems, and articles of manufacture are described. According to one embodiment, an image portion identification method includes accessing data regarding an image depicting a plurality of biological substrates corresponding to at least one biological sample and indicating presence of at least one biological indicator within the biological sample and, using processing circuitry, automatically identifying a portion of the image depicting one of the biological substrates but not others of the biological substrates.

Lassahn, Gordon D.; Lancaster, Gregory D.; Apel, William A.; Thompson, Vicki S.

2013-01-08T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

Project evaluation : a practical asset pricing method  

E-Print Network [OSTI]

This paper presents a practical approach to project evaluation using techniques of modern financial economics, with a sample application to oil development under a complex tax system. The method overcomes shortcomings of ...

Jacoby, Henry D.

1992-01-01T23:59:59.000Z

362

Inertial impaction air sampling device  

DOE Patents [OSTI]

An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

Dewhurst, K.H.

1987-12-10T23:59:59.000Z

363

Spent nuclear fuel sampling strategy  

SciTech Connect (OSTI)

This report proposes a strategy for sampling the spent nuclear fuel (SNF) stored in the 105-K Basins (105-K East and 105-K West). This strategy will support decisions concerning the path forward SNF disposition efforts in the following areas: (1) SNF isolation activities such as repackaging/overpacking to a newly constructed staging facility; (2) conditioning processes for fuel stabilization; and (3) interim storage options. This strategy was developed without following the Data Quality Objective (DQO) methodology. It is, however, intended to augment the SNF project DQOS. The SNF sampling is derived by evaluating the current storage condition of the SNF and the factors that effected SNF corrosion/degradation.

Bergmann, D.W.

1995-02-08T23:59:59.000Z

364

Inertial impaction air sampling device  

DOE Patents [OSTI]

An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry.

Dewhurst, Katharine H. (13150 Wenonah SE. Apt. 727, Albuquerque, NM 87123)

1990-01-01T23:59:59.000Z

365

Inertial impaction air sampling device  

DOE Patents [OSTI]

An inertial impactor is designed which is to be used in an air sampling device for collection of respirable size particles in ambient air. The device may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

Dewhurst, K.H.

1990-05-22T23:59:59.000Z

366

Sample Licensing Agreements | Partnerships | ORNL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 -the Mid-Infrared0 ResourceAwardsSafeguards and SecuritySafety Salt LakeSampleSample

367

RAPID SEPARATION OF ACTINIDES AND RADIOSTRONTIUM IN VEGETATION SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of actinides and radiostrontium in vegetation samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used in emergency response situations or for routine analysis. The actinides in vegetation method utilizes a rapid sodium hydroxide fusion method, a lanthanum fluoride matrix removal step, and a streamlined column separation process with stacked TEVA, TRU and DGA Resin cartridges. Lanthanum was separated rapidly and effectively from Am and Cm on DGA Resin. Alpha emitters are prepared using rare earth microprecipitation for counting by alpha spectrometry. The purified {sup 90}Sr fractions are mounted directly on planchets and counted by gas flow proportional counting. The method showed high chemical recoveries and effective removal of interferences. The actinide and {sup 90}Sr in vegetation sample analysis can be performed in less than 8 h with excellent quality for emergency samples. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory actinide particles or vegetation residue after furnace heating is effectively digested.

Maxwell, S.

2010-06-01T23:59:59.000Z

368

Offline solid phase microextraction sampling system  

DOE Patents [OSTI]

An offline solid phase microextraction (SPME) sampling apparatus for enabling SPME samples to be taken a number of times from a previously collected fluid sample (e.g. sample atmosphere) stored in a fused silica lined bottle which keeps volatile organics in the fluid sample stable for weeks at a time. The offline SPME sampling apparatus has a hollow body surrounding a sampling chamber, with multiple ports through which a portion of a previously collected fluid sample may be (a) released into the sampling chamber, (b) SPME sampled to collect analytes for subsequent GC analysis, and (c) flushed/purged using a fluidically connected vacuum source and purging fluid source to prepare the sampling chamber for additional SPME samplings of the same original fluid sample, such as may have been collected in situ from a headspace.

Harvey, Chris A. (French Camp, CA)

2008-12-16T23:59:59.000Z

369

A Sensitive Determination of Iodine Species, Including Organoiodine, for Freshwater and Seawater Samples Using High Performance Liquid Chromatography and Spectrophotometric Detection  

E-Print Network [OSTI]

, with minimal sample preparation, compared to existing methods. The method has been successfully applied to determine iodide, iodate as the difference of total inorganic iodide and iodide after reduction of the sample, and organic iodine as the difference...

Schwehr, K. A.; Santschi, P. H.

370

Tensiometer methods  

DOE Patents [OSTI]

A method for collecting data regarding a matric potential of a media includes providing a tensiometer having a stainless steel tensiometer casing, the stainless steel tensiometer casing comprising a tip portion which includes a wetted porous stainless steel membrane through which a matric potential of a media is sensed; driving the tensiometer into the media using an insertion tube comprising a plurality of probe casing which are selectively coupled to form the insertion tube as the tensiometer is progressively driven deeper into the media, wherein the wetted porous stainless steel membrane is in contact with the media; and sensing the matric potential the media exerts on the wetted porous stainless steel membrane by a pressure sensor in fluid hydraulic connection with the porous stainless steel membrane. A tensiometer includes a stainless steel casing.

Grover, Blair K.; Hubbell, Joel M.; Sisson, James B.; Casper, William L.

2005-12-20T23:59:59.000Z

371

Casting methods  

DOE Patents [OSTI]

A casting device includes a covered crucible having a top opening and a bottom orifice, a lid covering the top opening, a stopper rod sealing the bottom orifice, and a reusable mold having at least one chamber, a top end of the chamber being open to and positioned below the bottom orifice and a vacuum tap into the chamber being below the top end of the chamber. A casting method includes charging a crucible with a solid material and covering the crucible, heating the crucible, melting the material, evacuating a chamber of a mold to less than 1 atm absolute through a vacuum tap into the chamber, draining the melted material into the evacuated chamber, solidifying the material in the chamber, and removing the solidified material from the chamber without damaging the chamber.

Marsden, Kenneth C.; Meyer, Mitchell K.; Grover, Blair K.; Fielding, Randall S.; Wolfensberger, Billy W.

2012-12-18T23:59:59.000Z

372

Waste tank characterization sampling limits  

SciTech Connect (OSTI)

This document is a result of the Plant Implementation Team Investigation into delayed reporting of the exotherm in Tank 241-T-111 waste samples. The corrective actions identified are to have immediate notification of appropriate Tank Farm Operations Shift Management if analyses with potential safety impact exceed established levels. A procedure, WHC-IP-0842 Section 12.18, ``TWRS Approved Sampling and Data Analysis by Designated Laboratories`` (WHC 1994), has been established to require all tank waste sampling (including core, auger and supernate) and tank vapor samples be performed using this document. This document establishes levels for specified analysis that require notification of the appropriate shift manager. The following categories provide numerical values for analysis that may indicate that a tank is either outside the operating specification or should be evaluated for inclusion on a Watch List. The information given is intended to translate an operating limit such as heat load, expressed in Btu/hour, to an analysis related limit, in this case cesium-137 and strontium-90 concentrations. By using the values provided as safety flags, the analytical laboratory personnel can notify a shift manager that a tank is in potential violation of an operating limit or that a tank should be considered for inclusion on a Watch List. The shift manager can then take appropriate interim measures until a final determination is made by engineering personnel.

Tusler, L.A.

1994-09-02T23:59:59.000Z

373

Sample Internship Posting Department Name  

E-Print Network [OSTI]

Sample Internship Posting Department Name: Internship Title: Location: Description of Organization are examples from other internship postings Interns will: · Analyze potential investments · Shadow team members(s) in ________ is desirable For a list of majors see http://admissions.vanderbilt.edu/major Internship Period: The following

Bordenstein, Seth

374

Environmental surveillance master sampling schedule  

SciTech Connect (OSTI)

This document contains the planned 1994 schedules for routine collection of samples for the Surface Environmental Surveillance Project (SESP), Drinking Water Project, and Ground-Water Surveillance Project. Samples are routinely collected for the SESP and analyzed to determine the quality of air, surface water, soil, sediment, wildlife, vegetation, foodstuffs, and farm products at Hanford Site and surrounding communities. The responsibility for monitoring the onsite drinking water falls outside the scope of the SESP. The Hanford Environmental Health Foundation is responsible for monitoring the nonradiological parameters as defined in the National Drinking Water Standards while PNL conducts the radiological monitoring of the onsite drinking water. PNL conducts the drinking water monitoring project concurrent with the SESP to promote efficiency and consistency, utilize the expertise developed over the years, and reduce costs associated with management, procedure development, data management, quality control and reporting. The ground-water sampling schedule identifies ground-water sampling events used by PNL for environmental surveillance of the Hanford Site.

Bisping, L.E.

1994-02-01T23:59:59.000Z

375

Environmental Analysis & Policy: Sample Pathway  

E-Print Network [OSTI]

Environmental Analysis & Policy: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Sustainable Development OR Spring GE 425 U.S. Environmental Policy (Senior) GE 309 Intermediate Env Analysis (Fall) EAP Elective Summer Environmental Internship Senior Year GE 420 Env Policy Analysis 4 th Semester

Goldberg, Bennett

376

AUTOMATING GROUNDWATER SAMPLING AT HANFORD  

SciTech Connect (OSTI)

Until this past October, Fluor Hanford managed Hanford's integrated groundwater program for the U.S. Department of Energy (DOE). With the new contract awards at the Site, however, the CH2M HILL Plateau Remediation Company (CHPRC) has assumed responsibility for the groundwater-monitoring programs at the 586-square-mile reservation in southeastern Washington State. These programs are regulated by the Resource Conservation and Recovery Act (RCRA) and the Comprehensive Environmental Response Compensation and Liability Act (CERCLA). The purpose of monitoring is to track existing groundwater contamination from past practices, as well as other potential contamination that might originate from RCRA treatment, storage, and disposal (TSD) facilities. An integral part of the groundwater-monitoring program involves taking samples of the groundwater and measuring the water levels in wells scattered across the site. More than 1,200 wells are sampled each year. Historically, field personnel or 'samplers' have been issued pre-printed forms that have information about the well(s) for a particular sampling evolution. This information is taken from the Hanford Well Information System (HWIS) and the Hanford Environmental Information System (HEIS)--official electronic databases. The samplers used these hardcopy forms to document the groundwater samples and well water-levels. After recording the entries in the field, the samplers turned the forms in at the end of the day and the collected information was posted onto a spreadsheet that was then printed and included in a log book. The log book was then used to make manual entries of the new information into the software application(s) for the HEIS and HWIS databases. This is a pilot project for automating this tedious process by providing an electronic tool for automating water-level measurements and groundwater field-sampling activities. The automation will eliminate the manual forms and associated data entry, improve the accuracy of the information recorded, and enhance the efficiency and sampling capacity of field personnel. The goal of the effort is to eliminate 100 percent of the manual input to the database(s) and replace the management of paperwork by the field and clerical personnel with an almost entirely electronic process. These activities will include the following: scheduling the activities of the field teams, electronically recording water-level measurements, electronically logging and filing Groundwater Sampling Reports (GSR), and transferring field forms into the site-wide Integrated Document Management System (IDMS).

CONNELL CW; HILDEBRAND RD; CONLEY SF; CUNNINGHAM DE

2009-01-16T23:59:59.000Z

377

Rapid Determination Of Radiostrontium In Large Soil Samples  

SciTech Connect (OSTI)

A new method for the determination of radiostrontium in large soil samples has been developed at the Savannah River Environmental Laboratory (Aiken, SC, USA) that allows rapid preconcentration and separation of strontium in large soil samples for the measurement of strontium isotopes by gas flow proportional counting. The need for rapid analyses in the event of a Radiological Dispersive Device (RDD) or Improvised Nuclear Device (IND) event is well-known. In addition, the recent accident at Fukushima Nuclear Power Plant in March, 2011 reinforces the need to have rapid analyses for radionuclides in environmental samples in the event of a nuclear accident. The method employs a novel pre-concentration step that utilizes an iron hydroxide precipitation (enhanced with calcium phosphate) followed by a final calcium fluoride precipitation to remove silicates and other matrix components. The pre-concentration steps, in combination with a rapid Sr Resin separation using vacuum box technology, allow very large soil samples to be analyzed for {sup 89,90}Sr using gas flow proportional counting with a lower method detection limit. The calcium fluoride precipitation eliminates column flow problems typically associated with large amounts of silicates in large soil samples.

Maxwell, Sherrod L.; Culligan, Brian K.; Shaw, Patrick J.

2012-05-24T23:59:59.000Z

378

Hanford Site Environmental Surveillance Master Sampling Schedule  

SciTech Connect (OSTI)

This document contains the CY2000 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes sampling locations, sample types, and analyses to be performed.

Bisping, Lynn E.

2000-01-27T23:59:59.000Z

379

Apparatus and method for radioactive waste screening  

DOE Patents [OSTI]

An apparatus and method relating to screening radioactive waste are disclosed for ensuring that at least one calculated parameter for the measurement data of a sample falls within a range between an upper limit and a lower limit prior to the sample being packaged for disposal. The apparatus includes a radiation detector configured for detecting radioactivity and radionuclide content of the of the sample of radioactive waste and generating measurement data in response thereto, and a collimator including at least one aperture to direct a field of view of the radiation detector. The method includes measuring a radioactive content of a sample, and calculating one or more parameters from the radioactive content of the sample.

Akers, Douglas W.; Roybal, Lyle G.; Salomon, Hopi; Williams, Charles Leroy

2012-09-04T23:59:59.000Z

380

System and method for assaying radiation  

SciTech Connect (OSTI)

A system for assaying radiation includes a sample holder configured to hold a liquid scintillation solution. A photomultiplier receives light from the liquid scintillation solution and generates a signal reflective of the light. A control circuit biases the photomultiplier and receives the signal from the photomultiplier reflective of the light. A light impermeable casing surrounds the sample holder, photomultiplier, and control circuit. A method for assaying radiation includes placing a sample in a liquid scintillation solution, placing the liquid scintillation solution in a sample holder, and placing the sample holder inside a light impermeable casing. The method further includes positioning a photomultiplier inside the light impermeable casing and supplying power to a control circuit inside the light impermeable casing.

DiPrete, David P; Whiteside, Tad; Pak, Donald J; DiPrete, Cecilia C

2013-11-12T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

Tank farm backlog soil sample analysis plan  

SciTech Connect (OSTI)

This document describes the measures to collect samples, perform testing on samples, and make decisions to obtain a Contained- in Determination for tank farms backlog soil.

Ahlers, J.D., Westinghouse Hanford

1996-07-17T23:59:59.000Z

382

Rapid Screening of Complex Chemical Samples via Capillary Array Analysis  

SciTech Connect (OSTI)

This report is a summary of the results of a two-year Laboratory-Directed Research and Development (LDRD) project that developed instrumentation and methods for capillary array analysis. During the course of this project, a new capillary array electrochromatography instrument was developed to perform eight simultaneous separations and provide complementary chromatographic information from each column on a single sample.

D. S. Anex; D. W. Neyer

1998-11-01T23:59:59.000Z

383

Blocking Gibbs Sampling in Very Large Probabilistic Expert Systems  

E-Print Network [OSTI]

of Chicago 1118E 58th St. Chicago IL 60637 kong@galton.uchicago.edu U#11;e Kj#26;rul#11; Aalborg University converges much faster than plain Gibbs sampling for very complex problems. Keywords: probabilistic expert one shall be referred to as plain Gibbs. The evaluation of our blocking-Gibbs method is conducted

384

Refractor Importance Sampling Haohai Yu and Robert A. van Engelen  

E-Print Network [OSTI]

al., 1995] properties that make these meth- ods more attractive compared to exact methods. Stochastic Chain Monte Carlo (MCMC) forms another important group of stochastic sampling algorithms. Examples., 1996, MacKay, 1998, Pearl, 1987, Chavez and Cooper, 1990]. Stratified sam- pling [Bouckaert, 1994

van Engelen, Robert A.

385

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING FINAL REPORT  

E-Print Network [OSTI]

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS FINAL REPORT Prepared by David B. Kittelson of Mechanical Engineering Center for Diesel Research Minneapolis, MN January 14, 1999 #12;01/14/99 Page 2 TABLE ................................................................................................................5 DIESEL ENGINE TECHNOLOGY AND EMISSION REGULATIONS .............................7 PHYSICAL

Minnesota, University of

386

SAMPLING FROM LARGE MATRICES: AN APPROACH THROUGH GEOMETRIC FUNCTIONAL ANALYSIS  

E-Print Network [OSTI]

on the best known sample complexity for an approximation algorithm for MAX-2CSP problems. We use methods Decompositions, and approximations to MAX-2CSP problems. 1.1. The spectral norm: low rank approximations and SVD a small random submatrix of A. Solving this problem is essential for development of fast Monte

Vershynin, Roman

387

Anthrax Sampling and Decontamination: Technology Trade-Offs  

SciTech Connect (OSTI)

The goal of this project was to answer the following questions concerning response to a future anthrax release (or suspected release) in a building: 1. Based on past experience, what rules of thumb can be determined concerning: (a) the amount of sampling that may be needed to determine the extent of contamination within a given building; (b) what portions of a building should be sampled; (c) the cost per square foot to decontaminate a given type of building using a given method; (d) the time required to prepare for, and perform, decontamination; (e) the effectiveness of a given decontamination method in a given type of building? 2. Based on past experience, what resources will be spent on evaluating the extent of contamination, performing decontamination, and assessing the effectiveness of the decontamination in abuilding of a given type and size? 3. What are the trade-offs between cost, time, and effectiveness for the various sampling plans, sampling methods, and decontamination methods that have been used in the past?

Price, Phillip N.; Hamachi, Kristina; McWilliams, Jennifer; Sohn, Michael D.

2008-09-12T23:59:59.000Z

388

DNA-based methods of geochemical prospecting  

DOE Patents [OSTI]

The present invention relates to methods for performing surveys of the genetic diversity of a population. The invention also relates to methods for performing genetic analyses of a population. The invention further relates to methods for the creation of databases comprising the survey information and the databases created by these methods. The invention also relates to methods for analyzing the information to correlate the presence of nucleic acid markers with desired parameters in a sample. These methods have application in the fields of geochemical exploration, agriculture, bioremediation, environmental analysis, clinical microbiology, forensic science and medicine.

Ashby, Matthew (Mill Valley, CA)

2011-12-06T23:59:59.000Z

389

WRAP Module 1 sampling strategy and waste characterization alternatives study  

SciTech Connect (OSTI)

The Waste Receiving and Processing Module 1 Facility is designed to examine, process, certify, and ship drums and boxes of solid wastes that have a surface dose equivalent of less than 200 mrem/h. These wastes will include low-level and transuranic wastes that are retrievably stored in the 200 Area burial grounds and facilities in addition to newly generated wastes. Certification of retrievably stored wastes processing in WRAP 1 is required to meet the waste acceptance criteria for onsite treatment and disposal of low-level waste and mixed low-level waste and the Waste Isolation Pilot Plant Waste Acceptance Criteria for the disposal of TRU waste. In addition, these wastes will need to be certified for packaging in TRUPACT-II shipping containers. Characterization of the retrievably stored waste is needed to support the certification process. Characterization data will be obtained from historical records, process knowledge, nondestructive examination nondestructive assay, visual inspection of the waste, head-gas sampling, and analysis of samples taken from the waste containers. Sample characterization refers to the method or methods that are used to test waste samples for specific analytes. The focus of this study is the sample characterization needed to accurately identify the hazardous and radioactive constituents present in the retrieved wastes that will be processed in WRAP 1. In addition, some sampling and characterization will be required to support NDA calculations and to provide an over-check for the characterization of newly generated wastes. This study results in the baseline definition of WRAP 1 sampling and analysis requirements and identifies alternative methods to meet these requirements in an efficient and economical manner.

Bergeson, C.L.

1994-09-30T23:59:59.000Z

390

New Methods and Tools  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

* Concentrate samples around such boundaries p failure p df ()d System success System failure Limit Surface Sampling region - Dynamic Event Trees (DETs): *...

391

Environmental surveillance master sampling schedule  

SciTech Connect (OSTI)

Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the US Department of Energy (DOE). This document contains the planned schedule for routine sample collection for the Surface Environmental Surveillance Project (SESP) and Ground-Water Monitoring Project. Samples for radiological analyses include Air-Particulate Filter, gases and vapor; Water/Columbia River, Onsite Pond, Spring, Irrigation, and Drinking; Foodstuffs/Animal Products including Whole Milk, Poultry and Eggs, and Beef; Foodstuffs/Produce including Leafy Vegetables, Vegetables, and Fruit; Foodstuffs/Farm Products including Wine, Wheat and Alfalfa; Wildlife; Soil; Vegetation; and Sediment. Direct Radiation Measurements include Terrestrial Locations, Columbia River Shoreline Locations, and Onsite Roadway, Railway and Aerial, Radiation Surveys.

Bisping, L E

1992-01-01T23:59:59.000Z

392

Standard practice for bulk sampling of liquid uranium hexafluoride  

E-Print Network [OSTI]

1.1 This practice covers methods for withdrawing representative samples of liquid uranium hexafluoride (UF6) from bulk quantities of the material. Such samples are used for determining compliance with the applicable commercial specification, for example Specification C787 and Specification C996. 1.2 It is assumed that the bulk liquid UF6 being sampled comprises a single quality and quantity of material. This practice does not address any special additional arrangements that might be required for taking proportional or composite samples, or when the sampled bulk material is being added to UF6 residues already in a container (“heels recycle”). 1.3 The number of samples to be taken, their nominal sample weight, and their disposition shall be agreed upon between the parties. 1.4 The scope of this practice does not include provisions for preventing criticality incidents. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of th...

American Society for Testing and Materials. Philadelphia

2001-01-01T23:59:59.000Z

393

Rock Sampling | Open Energy Information  

Open Energy Info (EERE)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data CenterFranconia, Virginia:FAQ < RAPID Jump to: navigation, searchVirginia BlueRiverwoods,Rock Sampling Details Activities (18) Areas

394

INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING DISTRIBUTION, AND POPULATION  

E-Print Network [OSTI]

INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING Keywords: Parametric test, sample, population, sampling distributions Parametric tests are frequently parametric tests, nor hold beliefs that are consistent with that framework. The parametric test framework

Yu, Alex

395

Voltammetric analysis apparatus and method  

DOE Patents [OSTI]

An apparatus and method is described for electrochemical analysis of elements in solution. An auxiliary electrode, a reference electrode, and five working electrodes are positioned in a container containing a sample solution. The working electrodes are spaced apart evenly from each other and the auxiliary electrode to minimize any inter-electrode interference that may occur during analysis. An electric potential is applied between the auxiliary electrode and each of the working electrodes. Simultaneous measurements taken of the current flow through each of the working electrodes for each given potential in a potential range are used for identifying chemical elements present in the sample solution and their respective concentrations. Multiple working electrodes enable a more positive identification to be made by providing unique data characteristic of chemical elements present in the sample solution.

Almon, A.C.

1993-06-08T23:59:59.000Z

396

Generalized Multicoincidence Analysis Methods  

SciTech Connect (OSTI)

The ability to conduct automated trace radionuclide analysis at or near the sample collection point would provide a valuable tool for emergency response, nuclear forensics and environmental monitoring. Pacific Northwest National Laboratory is developing systems for this purpose based on dual gamma-ray spectrometers, e.g. NaI(TI) or HPGe, combined with thin organic scintillator sensors to detect light charged particles. Translating the coincident signatures recorded by these systems, which include , and , into the concentration of detectable radionuclides in the sample requires generalized multicoincidence analysis tools. The development and validation of the Coincidence Lookup Library, which currently contains the probabilities of single and coincidence signatures from more than 420 isotopes, is described. Also discussed is a method to calculate the probability of observing a coincidence signature which incorporates true coincidence summing effects. These effects are particularly important for high-geometric-efficiency detection systems. Finally, a process for validating the integrated analysis software package is demonstrated using GEANT 4 simulations of the prototype detector systems.

Warren, Glen A.; Smith, Leon E.; Aalseth, Craig E.; Ellis, J. E.; Valsan, Andrei B.; Mengesha, Wondwosen

2005-10-01T23:59:59.000Z

397

Method for immunodiagnostic detection of dioxins at low concentrations  

DOE Patents [OSTI]

A method is described for the use of monoclonal antibodies in a sensitive immunoassay for halogenated dioxins and dibenzofurans in industrial samples which contain impurities. Appropriate sample preparation and selective enzyme amplification of the immunoassay sensitivity permits detection of dioxin contaminants in industrial or environmental samples at concentrations in the range of a few parts per trillion.

Vanderlaan, Martin (Danville, CA); Stanker, Larry H. (Livermore, CA); Watkins, Bruce E. (Livermore, CA); Petrovic, Peter (Hochheim am Main, DE); Gorbach, Siegbert (Eppstein/Ts., DE)

1995-01-01T23:59:59.000Z

398

Gnie mcanique Implementing the Quotient Method Controller  

E-Print Network [OSTI]

of this project was to apply this method on a Ball-on-a- Wheel system. This system consists of a ball rolling the ball-on-a-wheel system it is important to have a sufficiently fast sampling rate. Normal webcamsSECTION DE Génie mécanique Implementing the Quotient Method Controller on the Ball-on-a-Wheel

Lausanne, Ecole Polytechnique Fédérale de

399

GASOLINE VEHICLE EXHAUST PARTICLE SAMPLING STUDY  

SciTech Connect (OSTI)

The University of Minnesota collaborated with the Paul Scherrer Institute, the University of Wisconsin (UWI) and Ricardo, Inc to physically and chemically characterize the exhaust plume from recruited gasoline spark ignition (SI) vehicles. The project objectives were: (1) Measure representative particle size distributions from a set of on-road SI vehicles and compare these data to similar data collected on a small subset of light-duty gasoline vehicles tested on a chassis dynamometer with a dilution tunnel using the Unified Drive Cycle, at both room temperature (cold start) and 0 C (cold-cold start). (2) Compare data collected from SI vehicles to similar data collected from Diesel engines during the Coordinating Research Council E-43 project. (3) Characterize on-road aerosol during mixed midweek traffic and Sunday midday periods and determine fleet-specific emission rates. (4) Characterize bulk- and size-segregated chemical composition of the particulate matter (PM) emitted in the exhaust from the gasoline vehicles. Particle number concentrations and size distributions are strongly influenced by dilution and sampling conditions. Laboratory methods were evaluated to dilute SI exhaust in a way that would produce size distributions that were similar to those measured during laboratory experiments. Size fractionated samples were collected for chemical analysis using a nano-microorifice uniform deposit impactor (nano-MOUDI). In addition, bulk samples were collected and analyzed. A mixture of low, mid and high mileage vehicles were recruited for testing during the study. Under steady highway cruise conditions a significant particle signature above background was not measured, but during hard accelerations number size distributions for the test fleet were similar to modern heavy-duty Diesel vehicles. Number emissions were much higher at high speed and during cold-cold starts. Fuel specific number emissions range from 1012 to 3 x 1016 particles/kg fuel. A simple relationship between number and mass emissions was not observed. Data were collected on-road to compare weekday with weekend air quality around the Twin Cities area. This portion of the study resulted in the development of a method to apportion the Diesel and SI contribution to on-road aerosol.

Kittelson, D; Watts, W; Johnson, J; Zarling, D Schauer,J Kasper, K; Baltensperger, U; Burtscher, H

2003-08-24T23:59:59.000Z

400

Improving predictability of time series using maximum entropy methods  

E-Print Network [OSTI]

We discuss how maximum entropy methods may be applied to the reconstruction of Markov processes underlying empirical time series and compare this approach to usual frequency sampling. It is shown that, at least in low dimension, there exists a subset of the space of stochastic matrices for which the MaxEnt method is more efficient than sampling, in the sense that shorter historical samples have to be considered to reach the same accuracy. Considering short samples is of particular interest when modelling smoothly non-stationary processes, for then it provides, under some conditions, a powerful forecasting tool. The method is illustrated for a discretized empirical series of exchange rates.

Gregor Chliamovitch; Alexandre Dupuis; Bastien Chopard; Anton Golub

2014-11-28T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

Improving predictability of time series using maximum entropy methods  

E-Print Network [OSTI]

We discuss how maximum entropy methods may be applied to the reconstruction of Markov processes underlying empirical time series and compare this approach to usual frequency sampling. It is shown that, at least in low dimension, there exists a subset of the space of stochastic matrices for which the MaxEnt method is more efficient than sampling, in the sense that shorter historical samples have to be considered to reach the same accuracy. Considering short samples is of particular interest when modelling smoothly non-stationary processes, for then it provides, under some conditions, a powerful forecasting tool. The method is illustrated for a discretized empirical series of exchange rates.

Chliamovitch, Gregor; Chopard, Bastien; Golub, Anton

2014-01-01T23:59:59.000Z

402

Optimal sampling efficiency in Monte Carlo sampling with an approximate potential  

SciTech Connect (OSTI)

Building on the work of Iftimie et al., Boltzmann sampling of an approximate potential (the 'reference' system) is used to build a Markov chain in the isothermal-isobaric ensemble. At the endpoints of the chain, the energy is evaluated at a higher level of approximation (the 'full' system) and a composite move encompassing all of the intervening steps is accepted on the basis of a modified Metropolis criterion. For reference system chains of sufficient length, consecutive full energies are statistically decorrelated and thus far fewer are required to build ensemble averages with a given variance. Without modifying the original algorithm, however, the maximum reference chain length is too short to decorrelate full configurations without dramatically lowering the acceptance probability of the composite move. This difficulty stems from the fact that the reference and full potentials sample different statistical distributions. By manipulating the thermodynamic variables characterizing the reference system (pressure and temperature, in this case), we maximize the average acceptance probability of composite moves, lengthening significantly the random walk between consecutive full energy evaluations. In this manner, the number of full energy evaluations needed to precisely characterize equilibrium properties is dramatically reduced. The method is applied to a model fluid, but implications for sampling high-dimensional systems with ab initio or density functional theory (DFT) potentials are discussed.

Coe, Joshua D [Los Alamos National Laboratory; Shaw, M Sam [Los Alamos National Laboratory; Sewell, Thomas D [U MISSOURI

2009-01-01T23:59:59.000Z

403

Sample introduction apparatus for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

Van den Engh, Ger (Seattle, WA)

1998-01-01T23:59:59.000Z

404

Sample introduction system for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

Engh, G. van den

1997-02-11T23:59:59.000Z

405

Sample introduction system for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

Van den Engh, Ger (Seattle, WA)

1997-01-01T23:59:59.000Z

406

Sample introduction apparatus for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

Van den Engh, G.

1998-03-10T23:59:59.000Z

407

Synchronized sampling improves fault location  

SciTech Connect (OSTI)

Transmission line faults must be located accurately to allow maintenance crews to arrive at the scene and repair the faulted section as soon as possible. Rugged terrain and geographical layout cause some sections of power transmission lines to be difficult to reach. In the past, a variety of fault location algorithms were introduced as either an add-on feature in protective relays or stand-alone implementation in fault locators. In both cases, the measurements of current and voltages were taken at one terminal of a transmission line only. Under such conditions, it may become difficult to determine the fault location accurately, since data from other transmission line ends are required for more precise computations. In the absence of data from the other end, existing algorithms have accuracy problems under several circumstances, such as varying switching and loading conditions, fault infeed from the other end, and random value of fault resistance. Most of the one-end algorithms were based on estimation of voltage and current phasors. The need to estimate phasors introduces additional difficulty in high-speed tripping situations where the algorithms may not be fast enough in determining fault location accurately before the current signals disappear due to the relay operation and breaker opening. This article introduces a unique concept of high-speed fault location that can be implemented either as a simple add-on to the digital fault recorders (DFRs) or as a stand-alone new relaying function. This advanced concept is based on the use of voltage and current samples that are synchronously taken at both ends of a transmission line. This sampling technique can be made readily available in some new DFR designs incorporating receivers for accurate sampling clock synchronization using the satellite Global Positioning System (GPS).

Kezunovic, M. [Texas A and M Univ., College Station, TX (United States)] [Texas A and M Univ., College Station, TX (United States); Perunicic, B. [Lamar Univ., Beaumont, TX (United States)] [Lamar Univ., Beaumont, TX (United States)

1995-04-01T23:59:59.000Z

408

Licensing Guide and Sample License  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample6, 2011 LawrenceE CAnalytical InstrumentationEnergy

409

Sample Environments at Sector 30  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 -the Mid-Infrared0 ResourceAwardsSafeguards and SecuritySafety Salt LakeSample

410

Use of passive sampling devices to determine soil contaminant concentrations  

SciTech Connect (OSTI)

The effective remediation of contaminated sites requires accurate identification of chemical distributions. A rapid sampling method using passive sampling devices (PSDs) can provide a thorough site assessment. We have been pursuing their application in terrestrial systems and have found that they increase the ease and speed of analysis, decrease solvent usage and overall cost, and minimize the transport of contaminated soils. Time and cost savings allow a higher sampling frequency than is generally the case using traditional methods. PSDs have been used in the field in soils of varying physical properties and have been successful in estimating soil concentrations ranging from 1 {mu}g/kg (parts per billion) to greater than 200 mg/kg (parts per million). They were also helpful in identifying hot spots within the sites. Passive sampling devices show extreme promise as an analytical tool to rapidly characterize contaminant distributions in soil. There are substantial time and cost savings in laboratory personnel and supplies. By selectively excluding common interferences that require sample cleanup, PSDs can be retrieved from the field and processed rapidly (one technician can process approximately 90 PSDs in an 8-h work day). The results of our studies indicate that PSDs can be used to accurately estimate soil contaminant concentrations and provide lower detection limits. Further, time and cost savings will allow a more thorough and detailed characterization of contaminant distributions. 13 refs., 4 figs., 2 tabs.

Johnson, K.A. [Clemson Univ., Pendleton, SC (United States); [Washington State Univ., Richland, WA (United States); Hooper, M.J. [Clemson Univ., Pendleton, SC (United States); Weisskopf, C.P. [Washington State Univ., Richland, WA (United States)

1996-12-31T23:59:59.000Z

411

Pulse measurement apparatus and method  

DOE Patents [OSTI]

An embodiment of the invention is directed to a pulse measuring system that measures a characteristic of an input pulse under test, particularly the pulse shape of a single-shot, nano-second duration, high shape-contrast optical or electrical pulse. An exemplary system includes a multi-stage, passive pulse replicator, wherein each successive stage introduces a fixed time delay to the input pulse under test, a repetitively-gated electronic sampling apparatus that acquires the pulse train including an entire waveform of each replica pulse, a processor that temporally aligns the replicated pulses, and an averager that temporally averages the replicated pulses to generate the pulse shape of the pulse under test. An embodiment of the invention is directed to a method for measuring an optical or an electrical pulse shape. The method includes the steps of passively replicating the pulse under test with a known time delay, temporally stacking the pulses, and temporally averaging the stacked pulses. An embodiment of the invention is directed to a method for increasing the dynamic range of a pulse measurement by a repetitively-gated electronic sampling device having a rated dynamic range capability, beyond the rated dynamic range of the sampling device; e.g., enhancing the dynamic range of an oscilloscope. The embodied technique can improve the SNR from about 300:1 to 1000:1. A dynamic range enhancement of four to seven bits may be achieved.

Marciante, John R. (Webster, NY); Donaldson, William R. (Pittsford, NY); Roides, Richard G. (Scottsville, NY)

2011-10-25T23:59:59.000Z

412

TRU waste-sampling program  

SciTech Connect (OSTI)

As part of a TRU waste-sampling program, Los Alamos National Laboratory retrieved and examined 44 drums of /sup 238/Pu- and /sup 239/Pu-contaminated waste. The drums ranged in age from 8 months to 9 years. The majority of drums were tested for pressure, and gas samples withdrawn from the drums were analyzed by a mass spectrometer. Real-time radiography and visual examination were used to determine both void volumes and waste content. Drum walls were measured for deterioration, and selected drum contents were reassayed for comparison with original assays and WIPP criteria. Each drum tested at atmospheric pressure. Mass spectrometry revealed no problem with /sup 239/Pu-contaminated waste, but three 8-month-old drums of /sup 238/Pu-contaminated waste contained a potentially hazardous gas mixture. Void volumes fell within the 81 to 97% range. Measurements of drum walls showed no significant corrosion or deterioration. All reassayed contents were within WIPP waste acceptance criteria. Five of the drums opened and examined (15%) could not be certified as packaged. Three contained free liquids, one had corrosive materials, and one had too much unstabilized particulate. Eleven drums had the wrong (or not the most appropriate) waste code. In many cases, disposal volumes had been inefficiently used. 2 refs., 23 figs., 7 tabs.

Warren, J.L.; Zerwekh, A.

1985-08-01T23:59:59.000Z

413

Method of absorbance correction in a spectroscopic heating value sensor  

SciTech Connect (OSTI)

A method and apparatus for absorbance correction in a spectroscopic heating value sensor in which a reference light intensity measurement is made on a non-absorbing reference fluid, a light intensity measurement is made on a sample fluid, and a measured light absorbance of the sample fluid is determined. A corrective light intensity measurement at a non-absorbing wavelength of the sample fluid is made on the sample fluid from which an absorbance correction factor is determined. The absorbance correction factor is then applied to the measured light absorbance of the sample fluid to arrive at a true or accurate absorbance for the sample fluid.

Saveliev, Alexei; Jangale, Vilas Vyankatrao; Zelepouga, Sergeui; Pratapas, John

2013-09-17T23:59:59.000Z

414

May 2013 Groundwater and Surface Water Sampling at the Rio Blanco, Colorado, Site (Data Validation Package)  

SciTech Connect (OSTI)

Annual sampling was conducted at the Rio Blanco, Colorado, site for the Long-Term Hydrologic Monitoring Program May 14-16, 2013, to monitor groundwater and surface water for potential radionuclide contamination. Sampling and analyses were conducted as specified in Sampling and Analysis Plan for the U.S. Department of Energy Office of Legacy Management Sites (LMS/PRO/S04351, continually updated). A duplicate sample was collected from location CER #1 Black Sulphur. Samples were analyzed for gamma-emitting radionuclides by high-resolution gamma spectrometry and for tritium using the conventional and enrichment methods.

None

2013-10-01T23:59:59.000Z

415

Analysis with electron microscope of multielement samples using pure element standards  

DOE Patents [OSTI]

This disclosure describes a method and modified analytical electron microscope for determining the concentration of elements in a multielement sample by exposing samples with differing thicknesses for each element to a beam of electrons. Simultaneously the electron dosage and x-ray intensities are measured for each sample of element to determine a ''K/sub AB/'' value to be used in the equation (I/sub A/I/sub B/) = K/sub AB/ (C/sub A//C/sub B/), where I is intensity and C is concentration for elements A and B. The multielement sample is exposed to determine the concentrations of the elements in the sample.

King, W.E.

1986-01-06T23:59:59.000Z

416

Determination of Oebalus pugnax (Hemiptera : Pentatomidae) spatial pattern in rice and development of visual sampling methods and population sampling plans  

E-Print Network [OSTI]

of two polyvinyl chloride (PVC) pipes in the form of a T,stick” made of a 1 m long PVC pipe (2 cm diameter) was usedstick” made of a 1.5 m long PVC pipe (2 cm diameter) was

Espino, L.; Way, M. O.; Wilson, L. T.

2008-01-01T23:59:59.000Z

417

Fluid sampling system for a nuclear reactor  

DOE Patents [OSTI]

A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump. 1 fig.

Lau, L.K.; Alper, N.I.

1994-11-22T23:59:59.000Z

418

Fluid sampling system for a nuclear reactor  

DOE Patents [OSTI]

A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump.

Lau, Louis K. (Monroeville, PA); Alper, Naum I. (Monroeville, PA)

1994-01-01T23:59:59.000Z

419

System and method for assaying a radionuclide  

DOE Patents [OSTI]

A system for assaying a radionuclide includes a liquid scintillation detector, an analyzer connected to the liquid scintillation detector, and a delay circuit connected to the analyzer. A gamma detector and a multi-channel analyzer are connected to the delay circuit and the gamma detector. The multi-channel analyzer produces a signal reflective of the radionuclide in the sample. A method for assaying a radionuclide includes selecting a sample, detecting alpha or beta emissions from the sample with a liquid scintillation detector, producing a first signal reflective of the alpha or beta emissions, and delaying the first signal a predetermined time. The method further includes detecting gamma emissions from the sample, producing a second signal reflective of the gamma emissions, and combining the delayed first signal with the second signal to produce a third signal reflective of the radionuclide.

Cadieux, James R; King, III, George S; Fugate, Glenn A

2014-12-23T23:59:59.000Z

420

Apparatus and method for detecting full-capture radiation events  

DOE Patents [OSTI]

An apparatus and method for sampling the output signal of a radiation detector and distinguishing full-capture radiation events from Compton scattering events. The output signal of a radiation detector is continuously sampled. The samples are converted to digital values and input to a discriminator where samples that are representative of events are identified. The discriminator transfers only event samples, that is, samples representing full-capture events and Compton events, to a signal processor where the samples are saved in a three-dimensional count matrix with time (from the time of onset of the pulse) on the first axis, sample pulse current amplitude on the second axis, and number of samples on the third axis. The stored data are analyzed to separate the Compton events from full-capture events, and the energy of the full-capture events is determined without having determined the energies of any of the individual radiation detector events.

Odell, Daniel M. C. (Aiken, SC)

1994-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

Apparatus and method for detecting full-capture radiation events  

DOE Patents [OSTI]

An apparatus and method are disclosed for sampling the output signal of a radiation detector and distinguishing full-capture radiation events from Compton scattering events. The output signal of a radiation detector is continuously sampled. The samples are converted to digital values and input to a discriminator where samples that are representative of events are identified. The discriminator transfers only event samples, that is, samples representing full-capture events and Compton events, to a signal processor where the samples are saved in a three-dimensional count matrix with time (from the time of onset of the pulse) on the first axis, sample pulse current amplitude on the second axis, and number of samples on the third axis. The stored data are analyzed to separate the Compton events from full-capture events, and the energy of the full-capture events is determined without having determined the energies of any of the individual radiation detector events. 4 figs.

Odell, D.M.C.

1994-10-11T23:59:59.000Z

422

A field sampling strategy for semivariogram inference of fractures in rock outcrops  

SciTech Connect (OSTI)

The stochastic continuum (SC) representation is one common approach for simulating the effects of fracture heterogeneity in groundwater flow and transport models. These SC reservoir models are generally developed using geostatistical methods (e.g., kriging or sequential simulation) that rely on the model semivariogram to describe the spatial variability of each continuum. Although a number of strategies for sampling spatial distributions have been published in the literature, little attention has been paid to the optimization of sampling in resource- or access-limited environments. Here we present a strategy for estimating the minimum sample spacing needed to define the spatial distribution of fractures on a vertical outcrop of basalt, located in the Box Canyon, east Snake River Plain, Idaho. We used fracture maps of similar basalts from the published literature to test experimentally the effects of different sample spacings on the resulting semivariogram model. Our final field sampling strategy was based on the lowest sample density that reproduced the semivariogram of the exhaustively sampled fracture map. Application of the derived sampling strategy to an outcrop in our field area gave excellent results, and illustrates the utility of this type of sample optimization. The method will work for developing a sampling plan for any intensive property, provided prior information for a similar domain is available; for example, fracture maps or ortho-rectified photographs from analogous rock types could be used to plan for sampling of a fractured rock outcrop.

Ryan M. Pollyea; Jerry P. Fairley; Robert K. Podgorney; Travis L. Mcling

2013-10-01T23:59:59.000Z

423

Methods and apparatus for measurement of a dimensional characteristic and methods of predictive modeling related thereto  

DOE Patents [OSTI]

A method of optically determining a change in magnitude of at least one dimensional characteristic of a sample in response to a selected chamber environment. A magnitude of at least one dimension of the at least one sample may be optically determined subsequent to altering the at least one environmental condition within the chamber. A maximum change in dimension of the at least one sample may be predicted. A dimensional measurement apparatus for indicating a change in at least one dimension of at least one sample. The dimensional measurement apparatus may include a housing with a chamber configured for accommodating pressure changes and an optical perception device for measuring a dimension of at least one sample disposed in the chamber. Methods of simulating injection of a gas into a subterranean formation, injecting gas into a subterranean formation, and producing methane from a coal bed are also disclosed.

Robertson, Eric P (Idaho Falls, ID); Christiansen, Richard L. (Littleton, CO)

2007-05-29T23:59:59.000Z

424

Methods for measurement of a dimensional characteristic and methods of predictive modeling related thereto  

DOE Patents [OSTI]

A method of optically determining a change in magnitude of at least one dimensional characteristic of a sample in response to a selected chamber environment. A magnitude of at least one dimension of the at least one sample may be optically determined subsequent to altering the at least one environmental condition within the chamber. A maximum change in dimension of the at least one sample may be predicted. A dimensional measurement apparatus for indicating a change in at least one dimension of at least one sample. The dimensional measurement apparatus may include a housing with a chamber configured for accommodating pressure changes and an optical perception device for measuring a dimension of at least one sample disposed in the chamber. Methods of simulating injection of a gas into a subterranean formation, injecting gas into a subterranean formation, and producing methane from a coal bed are also disclosed.

Robertson, Eric P (Idaho Falls, ID); Christiansen, Richard L. (Littleton, CO)

2007-10-23T23:59:59.000Z

425

Development of a model to predict flow oscillations in low-flow sodium boiling  

E-Print Network [OSTI]

An experimental and analytical program has been carried out in order to better understand the cause and effect of flow oscillations in boiling sodium systems. These oscillations have been noted in previous experiments with ...

Levin, Alan Edward

1980-01-01T23:59:59.000Z

426

Wind power application for low flow irrigation from the Edwards-Trinity aquifer of West Texas  

E-Print Network [OSTI]

Attempts were made to reduce the cost of energy for irrigation in West Texas. To do this two wind turbines of 10 kW size were installed in Garden City and Stiles, Texas to pump water. The turbines were installed on 30 m towers. The pumping water...

Molla, Saiful Islam

1997-01-01T23:59:59.000Z

427

Low-Flow Liquid Desiccant Air Conditioning: General Guidance and Site Considerations  

SciTech Connect (OSTI)

Dehumidification or latent cooling in buildings is an area of growing interest that has been identified as needing more research and improved technologies for higher performance. Heating, ventilating, and air-conditioning (HVAC) systems typically expend excessive energy by using overcool-and-reheat strategies to dehumidify buildings. These systems first overcool ventilation air to remove moisture and then reheat the air to meet comfort requirements. Another common strategy incorporates solid desiccant rotors that remove moisture from the air more efficiently; however, these systems increase fan energy consumption because of the high airside pressure drop of solid desiccant rotors and can add heat of absorption to the ventilation air. Alternatively, liquid desiccant air-conditioning (LDAC) technology provides an innovative dehumidification solution that: (1) eliminates the need for overcooling and reheating from traditional cooling systems; and (2) avoids the increased fan energy and air heating from solid desiccant rotor systems.

Kozubal, E.; Herrmann, L.; Deru, M.; Clark, J.

2014-09-01T23:59:59.000Z

428

Low-Flow Liquid Desiccant Air-Conditioning: Demonstrated Performance and Cost Implications  

SciTech Connect (OSTI)

Cooling loads must be dramatically reduced when designing net-zero energy buildings or other highly efficient facilities. Advances in this area have focused primarily on reducing a building's sensible cooling loads by improving the envelope, integrating properly sized daylighting systems, adding exterior solar shading devices, and reducing internal heat gains. As sensible loads decrease, however, latent loads remain relatively constant, and thus become a greater fraction of the overall cooling requirement in highly efficient building designs, particularly in humid climates. This shift toward latent cooling is a challenge for heating, ventilation, and air-conditioning (HVAC) systems. Traditional systems typically dehumidify by first overcooling air below the dew-point temperature and then reheating it to an appropriate supply temperature, which requires an excessive amount of energy. Another dehumidification strategy incorporates solid desiccant rotors that remove water from air more efficiently; however, these systems are large and increase fan energy consumption due to the increased airside pressure drop of solid desiccant rotors. A third dehumidification strategy involves high flow liquid desiccant systems. These systems require a high maintenance separator to protect the air distribution system from corrosive desiccant droplet carryover and so are more commonly used in industrial applications and rarely in commercial buildings. Both solid desiccant systems and most high-flow liquid desiccant systems (if not internally cooled) add sensible energy which must later be removed to the air stream during dehumidification, through the release of sensible heat during the sorption process.

Kozubal, E.; Herrmann, L.; Deru, M.; Clark, J.; Lowenstein, A.

2014-09-01T23:59:59.000Z

429

High Speed Pumps Are No Longer Limited to Low Flow Applications  

E-Print Network [OSTI]

Historically, the high-speed centrifugal pump was developed prior to World War II for rocket engine fuel pump applications for its advantages of light weight, compactness and dry running capability. Industrial derivatives were introduced in the 60’s...

Burke, P. Y.

430

May 2011 Groundwater and Surface Water Sampling at the Rio Blanco, Colorado, Site (Data Validation Package)  

SciTech Connect (OSTI)

Annual sampling was conducted at the Rio Blanco, Colorado, site for the Long-Term Hydrologic Monitoring Program May 16-17, 2011, to monitor groundwater and surface water for potential radionuclide contamination. Sampling and analyses were conducted as specified in Sampling and Analysis Plan for the U.S. Department of Energy Office of Legacy Management Sites (LMS/PRO/S04351, continually updated). A duplicate sample was collected from location Johnson Artesian WL. Samples were analyzed by the U.S. Environmental Protection Agency (EPA) Radiation&Indoor Environments National Laboratory in Las Vegas, Nevada. Samples were analyzed for gamma-emitting radionuclides by high-resolution gamma spectrometry, and for tritium using the conventional method. Tritium was not measured using the enrichment method because the EPA laboratory no longer offers that service. Results of this monitoring at the Rio Blanco site demonstrate that groundwater and surface water outside the boundaries have not been affected by project-related contaminants.

None

2011-12-01T23:59:59.000Z

431

Sample Residential Program Term Sheet | Department of Energy  

Broader source: Energy.gov (indexed) [DOE]

Sample Residential Program Term Sheet Sample Residential Program Term Sheet A sample for defining and elaborating on the specifics of a clean energy loan program. Sample...

432

GICHD Mine Dog Testing Project - Soil Sample Results No.3  

SciTech Connect (OSTI)

A mine dog evaluation project initiated by the Geneva International Center for Humanitarian Demining is evaluating the capability and reliability of mine detection dogs. The performance of field-operational mine detection dogs will be measured in test minefields in Afghanistan and Bosnia containing actual, but unfused landmines. Repeated performance testing over two years through various seasonal weather conditions will provide data simulating near real world conditions. Soil samples will be obtained adjacent to the buried targets repeatedly over the course of the test. Chemical analysis results from these soil samples will be used to evaluate correlations between mine dog detection performance and seasonal weather conditions. This report documents the analytical chemical methods and results from the third batch of soils received. This batch contained samples from Kharga, Afghanistan collected in October 2002.

PHELAN, JAMES M.; BARNETT, JAMES L.; BENDER, SUSAN FAE ANN; ARCHULETA, LUISA M.

2003-03-01T23:59:59.000Z

433

GICHD mine dog testing project - soil sample results #4.  

SciTech Connect (OSTI)

A mine dog evaluation project initiated by the Geneva International Center for Humanitarian Demining is evaluating the capability and reliability of mine detection dogs. The performance of field-operational mine detection dogs will be measured in test minefields in Afghanistan and Bosnia containing actual, but unfused landmines. Repeated performance testing over two years through various seasonal weather conditions will provide data simulating near real world conditions. Soil samples will be obtained adjacent to the buried targets repeatedly over the course of the test. Chemical analysis results from these soil samples will be used to evaluate correlations between mine dog detection performance and seasonal weather conditions. This report documents the analytical chemical methods and results from the fourth batch of soils received. This batch contained samples from Kharga, Afghanistan collected in April 2003 and Sarajevo, Bosnia collected in May 2003.

Barnett, James L.; Phelan, James M.; Archuleta, Luisa M.; Wood, Tyson B.; Donovan, Kelly L.; Bender, Susan Fae Ann

2003-08-01T23:59:59.000Z

434

Sampling probe for microarray read out using electrospray mass spectrometry  

DOE Patents [OSTI]

An automated electrospray based sampling system and method for analysis obtains samples from surface array spots having analytes. The system includes at least one probe, the probe including an inlet for flowing at least one eluting solvent to respective ones of a plurality of spots and an outlet for directing the analyte away from the spots. An automatic positioning system is provided for translating the probe relative to the spots to permit sampling of any spot. An electrospray ion source having an input fluidicly connected to the probe receives the analyte and generates ions from the analyte. The ion source provides the generated ions to a structure for analysis to identify the analyte, preferably being a mass spectrometer. The probe can be a surface contact probe, where the probe forms an enclosing seal along the periphery of the array spot surface.

Van Berkel, Gary J.

2004-10-12T23:59:59.000Z

435

Concentric micro-nebulizer for direct sample insertion  

DOE Patents [OSTI]

A concentric micro-nebulizer and method for introducing liquid samples into a plasma established in a plasma torch including a first tube connected to a source of plasma gas. The concentric micro-nebulizer has inner and outer concentric tubes extending upwardly within the torch for connection to a source of nebulizer gas and to a source of liquid solvent and to a source of sample liquid. The inner tube is connected to the source of liquid solvent and to the source of sample liquid and the outer tube is connected to the source of nebulizer gas. The outer tube has an orifice positioned slightly below the plasma when it is established, with the inner and outer tubes forming an annulus therebetween with the annular spacing between the tubes at said orifice being less than about 0.05mm. The dead volume of the inner tube is less than about 5 microliters.

Fassel, V.A.; Rice, G.W.; Lawrence, K.E.

1984-03-06T23:59:59.000Z

436

An introduction to boson-sampling  

E-Print Network [OSTI]

Boson-sampling is a simplified model for quantum computing that may hold the key to implementing the first ever post-classical quantum computer. Boson-sampling is a non-universal quantum computer that is significantly more straightforward to build than any universal quantum computer proposed so far. We begin this chapter by motivating boson-sampling and discussing the history of linear optics quantum computing. We then summarize the boson-sampling formalism, discuss what a sampling problem is, explain why boson-sampling is easier than linear optics quantum computing, and discuss the Extended Church-Turing thesis. Next, sampling with other classes of quantum optical states is analyzed. Finally, we discuss the feasibility of building a boson-sampling device using existing technology.

Bryan T. Gard; Keith R. Motes; Jonathan P. Olson; Peter P. Rohde; Jonathan P. Dowling

2014-06-26T23:59:59.000Z

437

General Sample Submission Form University of Utah  

E-Print Network [OSTI]

in all applicable information as completely as possible Sample Information Sample ID / Description/MS/MS (FTMS) ______ Maldi/FTMS ______ Maldi/ToF ______ ESI/MS ______ ESI/FTMS _____ Location and Staff MS file

Hill, Chris

438

Long-Term Hydrologic Monitoring Program Sampling and Analysis Results for 2009  

SciTech Connect (OSTI)

The U.S. Department of Energy (DOE) Office of Legacy Management conducted annual sampling at the Rulison, Colorado, Site for the Long-Term Hydrologic Monitoring Program (LTHMP) on May 11 and 12, 2009. Samples were analyzed by the U.S. Environmental Protection Agency (EPA) Radiation&Indoor Environments National Laboratory in Las Vegas, Nevada. Samples were analyzed for gamma-emitting radionuclides by high-resolution gamma spectroscopy and for tritium using the conventional and enriched methods.

None

2010-01-21T23:59:59.000Z

439

Long-Term Hydrologic Monitoring Program Sampling and Analysis Results for 2010  

SciTech Connect (OSTI)

The U.S. Department of Energy (DOE) Office of Legacy Management conducted annual sampling at the Rulison, Colorado, Site for the Long-Term Hydrologic Monitoring Program (LTHMP) on May 10 and 11, 2010. The U.S. Environmental Protection Agency (EPA) Radiation and Indoor Environments National Laboratory in Las Vegas, Nevada, analyzed the samples. Samples were analyzed for gamma-emitting radionuclides by high-resolution gamma spectroscopy and for tritium using the conventional and enriched methods.

None

2011-01-10T23:59:59.000Z

440

Long-Term Hydrologic Monitoring Program Sampling and Analysis Results for 2008  

SciTech Connect (OSTI)

The U.S. Department of Energy (DOE) Office of Legacy Management conducted annual sampling at the Rulison, Colorado site, for the Long-Term Hydrologic Monitoring Program (LTHMP) on May 12, and 13, 2008. Samples were analyzed by the U.S. Environmental Protection Agency (EPA) Radiation&Indoor Environments National Laboratory in Las Vegas, Nevada. Samples were analyzed for gamma-emitting radionuclides by high-resolution gamma spectroscopy and tritium using the conventional and enriched methods

None

2008-12-15T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


441

Rio Blanco, Colorado, Long-Term Hydrologic Monitoring Program Sampling and Analysis Results for 2009  

SciTech Connect (OSTI)

The U.S. Department of Energy (DOE) Office of Legacy Management conducted annual sampling at the Rio Blanco, Colorado, Site, for the Long-Term Hydrologic Monitoring Program (LTHMP) on May 13 and 14, 2009. Samples were analyzed by the U.S. Environmental Protection Agency (EPA) Radiation&Indoor Environments National Laboratory in Las Vegas, Nevada. Samples were analyzed for gamma-emitting radionuclides by high-resolution gamma spectroscopy and tritium using the conventional and enriched methods.

None

2009-12-21T23:59:59.000Z

442

Apparatus and method for measuring electrostatic polarization  

DOE Patents [OSTI]

An apparatus and method for measuring the electric properties of solid matter which provides data for determining the polarizability of the electron distributions contained therein is disclosed. A sample of the solid to be studied is placed between the plates of a capacitor where it acts as a dielectric. The sample is excited by the interaction of electromagnetic radiation with an atomic species contained in the sample. The voltage induced across the capacitor is then measured as a function of time with the aid of a high Q circuit tuned to a frequency related to the frequency of the applied electromagnetic energy.

Hahn, Erwin L. (Berkeley, CA); Clarke, John (Berkeley, CA); Sloater, Tycho (Urbana, IL); Hilbert, Claude (Austin, TX); Heaney, Michael B. (Berkeley, CA)

1989-01-01T23:59:59.000Z

443

Sample holder for X-ray diffractometry  

DOE Patents [OSTI]

A sample holder for use with X-ray diffractometers with the capability to rotate the sample, as well as to adjust the position of the sample in the x, y, and z directions. Adjustment in the x direction is accomplished through loosening set screws, moving a platform, and retightening the set screws. Motion translators are used for adjustment in the y and z directions. An electric motor rotates the sample, and receives power from the diffractometer.

Hesch, Victor L. (Los Alamos, NM)

1992-01-01T23:59:59.000Z

444

E-Print Network 3.0 - air pollution sampling Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

sampling Search Powered by Explorit Topic List Advanced Search Sample search results for: air pollution sampling Page: << < 1 2 3 4 5 > >> 1 griculture is in the spotlight as a...

445

E-Print Network 3.0 - analysis science modeling Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

science modeling Search Powered by Explorit Topic List Advanced Search Sample search results for: analysis science modeling Page: << < 1 2 3 4 5 > >> 1 FROM MODELS TO METHODS TO...

446

E-Print Network 3.0 - arterial infusion chemotherapy Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Powered by Explorit Topic List Advanced Search Sample search results for: arterial infusion chemotherapy Page: << < 1 2 3 4 5 > >> 1 Optical method for real-time monitoring of...

447

E-Print Network 3.0 - alternative readout schemes Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Search Sample search results for: alternative readout schemes Page: << < 1 2 3 4 5 > >> 1 Nuclear Instruments and Methods in Physics Research A 505 (2003) 215218 A study of a...

448

E-Print Network 3.0 - adherent cvd diamond Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Search Sample search results for: adherent cvd diamond Page: << < 1 2 3 4 5 > >> 1 Thin Film Diamond by Chemical Vapour Deposition Methods M. N. R. Ashfold, P. W. May, and C. A....

449

E-Print Network 3.0 - apparently balanced translocation Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Sample search results for: apparently balanced translocation Page: << < 1 2 3 4 5 > >> 1 ATP-dependent Translocation of Proteins along Single-stranded DNA: Models and Methods of...

450

E-Print Network 3.0 - analysis computer rsac Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Powered by Explorit Topic List Advanced Search Sample search results for: analysis computer rsac Page: << < 1 2 3 4 5 > >> 1 A Note on the Restarted CG Method and Reduced Space...

451

Speed Training: Improving the Rate of Backpropagation Learning through Stochastic Sample Presentation  

E-Print Network [OSTI]

Speed Training: Improving the Rate of Backpropagation Learning through Stochastic Sample. However, using complex neural networks to learn very large training sets is often problematic, imposing prohibitive time constraints on the training process. We present four practical methods for dramatically

Martinez, Tony R.

452

E-Print Network 3.0 - asymmetric b-factory note Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

index of the aerogel samples ranged from 1.012 to 1... of this report. 2 Silica Aerogels for KEK B-Factory The production method of ... Source: BELLE Collaboration...

453

E-Print Network 3.0 - absorption spectrophotometry fi-faas Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

method 7060A) Arsenic concentrations in the plants were relatively low... furnace atomic absorption spectrophotometry. . The samples will also be analyzed to pH using a pH...

454

September 2007 Visual Sample Plan Version 5.08.1 8.0 References  

E-Print Network [OSTI]

. Statistical Methods for Nuclear Material Management, NUREG/CR-4604, U.S. Nuclear Regulatory Commission Laboratory, Richland, Washington. Gilbert, R. O. 2003. Results of QA Testing of the Visual Sample Plan (VSP

455

E-Print Network 3.0 - alkali ion beams Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

beams Search Powered by Explorit Topic List Advanced Search Sample search results for: alkali ion beams Page: << < 1 2 3 4 5 > >> 1 METHOD FOR EFFICIENCY AND TIME RESPONSE...

456

E-Print Network 3.0 - area modular baf2 Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

using the modified Shiraki method... by illuminating the MQW sample surface with a near-infrared IR diode laser with emission at 976 nm. A modular FTIR... incident on...

457

Nano-DESI Source for OA Samples Analyses. EMSL Research and Capability Development Proposals  

E-Print Network [OSTI]

Nano-DESI Source for OA Samples Analyses. EMSL Research and Capability Development Proposals Electrospray Ionization (nano-DESI) method developed as part of this project and other atmospheric ionization

458

System demonstration of an optically-sampled, wavelength-demultiplexed photonic analog-to-digital converter  

E-Print Network [OSTI]

The performance of electronic analog-to-digital converters (ADCs) at high sampling rates is fundamentally limited by the timing jitter of electronic clocks. To circumvent this limitation, one method is to exploit the ...

Peng, Michael Yung

2011-01-01T23:59:59.000Z

459

Estimating the Partition Function of Graphical Models Using Langevin Importance Sampling  

E-Print Network [OSTI]

equation and estimates the partition function using all the samples generated during the random walk at all long time for MCMC sampling to reach the detailed balance equilib- rium. Further, no simple methods, inspired by the obser- vation that if a liquid material cools very quickly, the material will solidify

Xu, Jinbo

460

Energy-Efficient Sampling Schedules for Body Area Vishwa Goudar and Miodrag Potkonjak  

E-Print Network [OSTI]

Energy-Efficient Sampling Schedules for Body Area Networks Vishwa Goudar and Miodrag Potkonjak a novel sampling method to overcome the tradeoff between sensing fidelity and energy-efficiency considerations in the design and deployment of WSNs, energy-efficiency has been identified as the most important

Potkonjak, Miodrag

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Microfluidic Wheatstone bridge for rapid sample analysis Melikhan Tanyeri,a  

E-Print Network [OSTI]

Microfluidic Wheatstone bridge for rapid sample analysis Melikhan Tanyeri,a Mikhil Ranka,a Natawan20604d We developed a microfluidic analogue of the classic Wheatstone bridge circuit for automated, real, the microfluidic Wheatstone bridge represents a new and versatile method for on-chip flow control and sample

Schroeder, Charles

462

EN-012 Ecology September 2003 Using Line Intersect Sampling for Coarse Woody Debris  

E-Print Network [OSTI]

EN-012 Ecology September 2003 Using Line Intersect Sampling for Coarse Woody Debris: Practitioners, coarse woody debris, CWD, piece length, forest ecology, sampling methods, survey design, field to adjust pile volume to wood volume (Little 1982; Hardy 1996). Extension Note Research Disciplines: Ecology

463

Course Number: 7/8129 Course Title: Environmental Sampling and Analysis  

E-Print Network [OSTI]

for measuring environmental chemical and biological contaminants. We will primarily examine sampling1 Course Number: 7/8129 Course Title: Environmental Sampling and Analysis The University of Memphis and analytical methods used to measure airborne contaminants in the general environments as well as the workplace

Dasgupta, Dipankar

464

E-Print Network 3.0 - air samples collected Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Collection NASA's Stardust sample return capsule successfully landed at the Summary: Aerogel: Stardust Collection Material 12;NASA's Stardust sample return capsule...

465

E-Print Network 3.0 - adaptive sampling strategy Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

ray tracing, Whitted Whi80 proposed an adaptive sampling strategy which first... (Eds.) Adaptive Sampling for Geometry-aware Reconstruction Filters Pablo Bauszat1 and Martin...

466

ISOLOK VALVE ACCEPTANCE TESTING FOR DWPF SME SAMPLING PROCESS  

SciTech Connect (OSTI)

Evaluation of the Defense Waste Processing Facility (DWPF) Chemical Process Cell (CPC) cycle time identified several opportunities to improve the CPC processing time. Of the opportunities, a focus area related to optimizing the equipment and efficiency of the sample turnaround time for DWPF Analytical Laboratory was identified. The Mechanical Systems & Custom Equipment Development (MS&CED) Section of the Savannah River National Laboratory (SRNL) evaluated the possibility of using an Isolok{reg_sign} sampling valve as an alternative to the Hydragard{reg_sign} valve for taking process samples. Previous viability testing was conducted with favorable results using the Isolok sampler and reported in SRNL-STI-2010-00749 (1). This task has the potential to improve operability, reduce maintenance time and decrease CPC cycle time. This report summarizes the results from acceptance testing which was requested in Task Technical Request (TTR) HLW-DWPF-TTR-2010-0036 (2) and which was conducted as outlined in Task Technical and Quality Assurance Plan (TTQAP) SRNL-RP-2011-00145 (3). The Isolok to be tested is the same model which was tested, qualified, and installed in the Sludge Receipt Adjustment Tank (SRAT) sample system. RW-0333P QA requirements apply to this task. This task was to qualify the Isolok sampler for use in the DWPF Slurry Mix Evaporator (SME) sampling process. The Hydragard, which is the current baseline sampling method, was used for comparison to the Isolok sampling data. The Isolok sampler is an air powered grab sampler used to 'pull' a sample volume from a process line. The operation of the sampler is shown in Figure 1. The image on the left shows the Isolok's spool extended into the process line and the image on the right shows the sampler retracted and then dispensing the liquid into the sampling container. To determine tank homogeneity, a Coliwasa sampler was used to grab samples at a high and low location within the mixing tank. Data from the two locations were compared to determine if the contents of the tank were well mixed. The Coliwasa sampler is a tube with a stopper at the bottom and is designed to obtain grab samples from specific locations within the drum contents. A position paper (4) was issued to address the prototypic flow loop issues and simulant selections. A statistically designed plan (5) was issued to address the total number of samples each sampler needed to pull, to provide the random order in which samples were pulled and to group samples for elemental analysis. The TTR required that the Isolok sampler perform as well as the Hydragard sampler during these tests to ensure the acceptability of the Isolok sampler for use in the DWPF sampling cells. Procedure No.L9.4-5015 was used to document the sample parameters and process steps. Completed procedures are located in R&D Engineering job folder 23269.

Edwards, T.; Hera, K.; Coleman, C.; Jones, M.; Wiedenman, B.

2011-12-05T23:59:59.000Z

467

Neural net controlled tag gas sampling system for nuclear reactors  

DOE Patents [OSTI]

A method and system for providing a tag gas identifier to a nuclear fuel rod and analyze escaped tag gas to identify a particular failed nuclear fuel rod. The method and system include disposing a unique tag gas composition into a plenum of a nuclear fuel rod, monitoring gamma ray activity, analyzing gamma ray signals to assess whether a nuclear fuel rod has failed and is emitting tag gas, activating a tag gas sampling and analysis system upon sensing tag gas emission from a failed nuclear rod and evaluating the escaped tag gas to identify the particular failed nuclear fuel rod.

Gross, Kenneth C. (Bolingbrook, IL); Laug, Matthew T. (Idaho Fall, ID); Lambert, John D. B. (Wheaton, IL); Herzog, James P. (Downers Grove, IL)

1997-01-01T23:59:59.000Z

468

Neural net controlled tag gas sampling system for nuclear reactors  

DOE Patents [OSTI]

A method and system are disclosed for providing a tag gas identifier to a nuclear fuel rod and analyze escaped tag gas to identify a particular failed nuclear fuel rod. The method and system include disposing a unique tag gas composition into a plenum of a nuclear fuel rod, monitoring gamma ray activity, analyzing gamma ray signals to assess whether a nuclear fuel rod has failed and is emitting tag gas, activating a tag gas sampling and analysis system upon sensing tag gas emission from a failed nuclear rod and evaluating the escaped tag gas to identify the particular failed nuclear fuel rod. 12 figs.

Gross, K.C.; Laug, M.T.; Lambert, J.B.; Herzog, J.P.

1997-02-11T23:59:59.000Z

469

Ultrasonic Porosity Estimation of Low-Porosity Ceramic Samples  

SciTech Connect (OSTI)

We report on efforts to extend the applicability of an airborne ultrasonic pulse-reflection (UPR) method towards lower porosities. UPR is a method that has been used successfully to estimate porosity and tortuosity of high porosity foams. UPR measures acoustical reflectivity of a target surface at two or more incidence angles. We used ceramic samples to evaluate the feasibility of extending the UPR range into low porosities (<35%). The validity of UPR estimates depends on pore size distribution and probing frequency as predicted by the theoretical boundary conditions of the used equivalent fluid model under the high-frequency approximation.

Eskelinen, J.; Hoffren, H. [Electronics Research Unit, Department of Physical Sciences, University of Helsinki, P.O. Box 64 FIN-00014 (Finland); Kohout, T.; Pesonen, L. J. [Division of Geophysics, Department of Physical Sciences, University of Helsinki, P.O. Box 64 FIN-00014 (Finland); Haeggstroem, E. [Electronics Research Unit, Department of Physical Sciences, University of Helsinki, P.O. Box 64 FIN-00014 (Finland); Helsinki Institute of Physics, PO Box 64, FIN-00014 (Finland)

2007-03-21T23:59:59.000Z

470

Monoclonal antibodies to cyclodiene insecticides and method for detecting the same  

DOE Patents [OSTI]

Methods are described for making specific monoclonal antibodies useful for detection of cyclodienes in foods and environmental samples. Monoclonal antibodies specifically reactive with cyclodienes can detect accumulated pesticides in food, tissue or environmental samples. Extraction and preparation of organic samples for immunoassay in a polar-nonpolar reaction medium permits detection of halogenated organic ring structures at concentrations in samples.

Stanker, Larry H. (Livermore, CA); Vanderlaan, Martin (Danville, CA); Watkins, Bruce E. (Livermore, CA)

1994-01-01T23:59:59.000Z

471

Methods for threshold determination in multiplexed assays  

DOE Patents [OSTI]

Methods for determination of threshold values of signatures comprised in an assay are described. Each signature enables detection of a target. The methods determine a probability density function of negative samples and a corresponding false positive rate curve. A false positive criterion is established and a threshold for that signature is determined as a point at which the false positive rate curve intersects the false positive criterion. A method for quantitative analysis and interpretation of assay results together with a method for determination of a desired limit of detection of a signature in an assay are also described.

Tammero, Lance F. Bentley; Dzenitis, John M; Hindson, Benjamin J

2014-06-24T23:59:59.000Z

472

Rotary Mode Core Sample System availability improvement  

SciTech Connect (OSTI)

The Rotary Mode Core Sample System (RMCSS) is used to obtain stratified samples of the waste deposits in single-shell and double-shell waste tanks at the Hanford Site. The samples are used to characterize the waste in support of ongoing and future waste remediation efforts. Four sampling trucks have been developed to obtain these samples. Truck I was the first in operation and is currently being used to obtain samples where the push mode is appropriate (i.e., no rotation of drill). Truck 2 is similar to truck 1, except for added safety features, and is in operation to obtain samples using either a push mode or rotary drill mode. Trucks 3 and 4 are now being fabricated to be essentially identical to truck 2.

Jenkins, W.W.; Bennett, K.L.; Potter, J.D. [Westinghouse Hanford Co., Richland, WA (United States); Cross, B.T.; Burkes, J.M.; Rogers, A.C. [Southwest Research Institute (United States)

1995-02-28T23:59:59.000Z

473

Sample sizes for confidence limits for reliability.  

SciTech Connect (OSTI)

We recently performed an evaluation of the implications of a reduced stockpile of nuclear weapons for surveillance to support estimates of reliability. We found that one technique developed at Sandia National Laboratories (SNL) under-estimates the required sample size for systems-level testing. For a large population the discrepancy is not important, but for a small population it is important. We found that another technique used by SNL provides the correct required sample size. For systems-level testing of nuclear weapons, samples are selected without replacement, and the hypergeometric probability distribution applies. Both of the SNL techniques focus on samples without defects from sampling without replacement. We generalized the second SNL technique to cases with defects in the sample. We created a computer program in Mathematica to automate the calculation of confidence for reliability. We also evaluated sampling with replacement where the binomial probability distribution applies.

Darby, John L.

2010-02-01T23:59:59.000Z

474

Report on Electrochemcial Corrosion Testing of 241-SY-102 Grab Samples from the 2012 Grab Sampling Campaign  

SciTech Connect (OSTI)

This report describes the results of the electrochemical testing performed on tank 241-SY-102 (SY-102) grab samples that were collected in support of corrosion mitigation. The objective of the work presented here was to determine corrosion resistance of tank SY-102 to the grab samples collected using electrochemical methods up to 50°C as well as to satisfy data quality objectives. Grab samples were collected at multiple elevations from Riser 003. The electrochemical corrosion testing was planned to consist of linear polarization resistance testing (LPR) and cyclic potentiodynamic polarization (CPP) testing at 50°C. The temperature would be lowered to 40 °C and the test repeated if the CPP curve indicated pitting corrosion at 50°C. Ifno pitting was indicated by the CPP curve, then a duplicate scan would be repeated at 50°C to confirm the first result. The testing would be complete if the duplicate CPP scan was consistent with the first. This report contains the CPP results of the testing of grab sample 2SY-12-03 and 2SY-12-03DUP composite sample tested under these conditions. There was no indication of pitting at 50°C, and the duplicate scan was in agreement with the first scan. Since no further testing was required, a third scan with a shorter rest time was performed and is present in this report.

Wyrwas, Richard B.; Lamothe, Margaret E.

2013-05-30T23:59:59.000Z

475

Proper Oil Sampling Intervals and Sample Collection Techniques Gasoline/Diesel/Natural Gas Engines  

E-Print Network [OSTI]

Proper Oil Sampling Intervals and Sample Collection Techniques Gasoline/Diesel/Natural Gas Engines: · Oil samples can be collected during oil changes. Follow manufacturers recommendations on frequency (hours, mileage, etc) of oil changes. · Capture a sample from the draining oil while the oil is still hot

476

Site survey method and apparatus  

DOE Patents [OSTI]

The disclosure of the invention is directed to a site survey ground vehicle based apparatus and method for automatically detecting source materials, such as radioactivity, marking the location of the source materials, such as with paint, and mapping the location of the source materials on a site. The apparatus of the invention is also useful for collecting and analyzing samples. The apparatus includes a ground vehicle, detectors mounted at the front of the ground vehicle, and individual detector supports which follow somewhat irregular terrain to allow consistent and accurate detection, and autolocation equipment. 19 figures.

Oldham, J.G.; Spencer, C.R.; Begley, C.L.; Meyer, H.R.

1991-06-18T23:59:59.000Z

477

Calorimetric system and method  

DOE Patents [OSTI]

Apparatus is described for measuring heat capacity of a sample where a series of measurements are taken in succession comprises a sample holder in which a sample to be measured is disposed, a temperature sensor and sample heater for providing a heat pulse thermally connected to the sample, and an adiabatic heat shield in which the sample holder is positioned and including an electrical heater. An electrical power supply device provides an electrical power output to the sample heater to generate a heat pulse. The electrical power from a power source to the heat shield heater is adjusted by a control device, if necessary, from one measurement to the next in response to a sample temperature-versus-time change determined before and after a previous heat pulse to provide a subsequent sample temperature-versus-time change that is substantially linear before and after the subsequent heat pulse. A temperature sensor is used and operable over a range of temperatures ranging from approximately 3K to 350K depending upon the refrigerant used. The sample optionally can be subjected to dc magnetic fields such as from 0 to 12 Tesla (0 to 120 kOe). 18 figs.

Gschneidner, K.A. Jr.; Pecharsky, V.K.; Moorman, J.O.

1998-09-15T23:59:59.000Z

478

Calorimetric system and method  

DOE Patents [OSTI]

Apparatus for measuring heat capacity of a sample where a series of measurements are taken in succession comprises a sample holder in which a sample to be measured is disposed, a temperature sensor and sample heater for providing a heat pulse thermally connected to the sample, and an adiabatic heat shield in which the sample holder is positioned and including an electrical heater. An electrical power supply device provides an electrical power output to the sample heater to generate a heat pulse. The electrical power from a power source to the heat shield heater is adjusted by a control device, if necessary, from one measurement to the next in response to a sample temperature-versus-time change determined before and after a previous heat pulse to provide a subsequent sample temperature-versus-time change that is substantially linear before and after the subsequent heat pulse. A temperature sensor is used and operable over a range of temperatures ranging from approximately 3K to 350K depending upon the refrigerant used. The sample optionally can be subjected to dc magnetic fields such as from 0 to 12 Tesla (0 to 120 kOe).

Gschneidner, Jr., Karl A. (Ames, IA); Pecharsky, Vitalij K. (Ames, IA); Moorman, Jack O. (Boone, IA)

1998-09-15T23:59:59.000Z

479

ANALYTICAL RESULTS OF MOX COLEMANITE CONCRETE SAMPLES POURED AUGUST 29, 2012  

SciTech Connect (OSTI)

The Mixed Oxide Fuel Fabrication Facility (MFFF) will use colemanite bearing concrete neutron absorber panels credited with attenuating neutron flux in the criticality design analyses and shielding operators from radiation. The Savannah River National Laboratory is tasked with measuring the total density, partial hydrogen density, and partial boron density of the colemanite concrete. Samples poured 8/29/12 were received on 9/20/2012 and analyzed. The average total density of each of the samples measured by the ASTM method C 642 was within the lower bound of 1.88 g/cm{sup 3}. The average partial hydrogen density of samples 8.6.1, 8.7.1, and 8.5.3 as measured using method ASTM E 1311 met the lower bound of 6.04E-02 g/cm{sup 3}. The average measured partial boron density of each sample met the lower bound of 1.65E-01 g/cm{sup 3} measured by the ASTM C 1301 method. The average partial hydrogen density of samples 8.5.1, 8.6.3, and 8.7.3 did not meet the lower bound. The samples, as received, were not wrapped in a moist towel as previous samples and appeared to be somewhat drier. This may explain the lower hydrogen partial density with respect to previous samples.

Cozzi, A.; Best, D.; Reigel, M.

2012-10-30T23:59:59.000Z

480

ANALYTICAL RESULTS OF MOX COLEMANITE CONCRETE SAMPLES POURED AUGUST 29, 2012  

SciTech Connect (OSTI)

The Mixed Oxide Fuel Fabrication Facility (MFFF) will use colemanite bearing concrete neutron absorber panels credited with attenuating neutron flux in the criticality design analyses and shielding operators from radiation. The Savannah River National Laboratory is tasked with measuring the total density, partial hydrogen density, and partial boron density of the colemanite concrete. Samples poured 8/29/12 were received on 9/20/2012 and analyzed. The average total density of each of the samples measured by the ASTM method C 642 was within the lower bound of 1.88 g/cm{sup 3}. The average partial hydrogen density of samples 8.6.1, 8.7.1, and 8.5.3 as measured using method ASTM E 1311 met the lower bound of 6.04E-02 g/cm{sup 3}. The average measured partial boron density of each sample met the lower bound of 1.65E-01 g/cm{sup 3} measured by the ASTM C 1301 method. The average partial hydrogen density of samples 8.5.1, 8.6.3, and 8.7.3 did not meet the lower bound. The samples, as received, were not wrapped in a moist towel as previous samples and appeared to be somewhat drier. This may explain the lower hydrogen partial density with respect to previous samples.

Best, D.; Cozzi, A.; Reigel, M.

2012-12-20T23:59:59.000Z

Note: This page contains sample records for the topic "low-flow sampling method" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


481

Analytical Results For MOX Colemanite Concrete Samples Received On September 4, 2013  

SciTech Connect (OSTI)

The Mixed Oxide Fuel Fabrication Facility (MFFF) will use colemanite bearing concrete neutron absorber panels credited with attenuating neutron flux in the criticality design analyses and shielding operators from radiation. The Savannah River National Laboratory (SRNL) is tasked with measuring the total density, partial hydrogen density, and partial boron density of the colemanite concrete. SRNL received three samples of colemanite concrete for analysis on September 4, 2013. The average total density of each of the samples measured by the ASTM method C 642, the average partial hydrogen density was measured using method ASTM E 1131, and the average partial boron density of each sample was measured according to ASTM C 1301. The lower limits and measured values for the total density, hydrogen partial density, and boron partial density are presented. For all the samples tested, the total density and the boron partial density met or exceeded the specified limit. None of the samples met the lower limit for hydrogen partial density.

Reigel, Marissa M.

2013-09-24T23:59:59.000Z

482

Analytical Results For MOX Colemanite Concrete Samples Received On November, 2013  

SciTech Connect (OSTI)

The Mixed Oxide Fuel Fabrication Facility (MFFF) will use colemanite bearing concrete neutron absorber panels credited with attenuating neutron flux in the criticality design analyses and shielding operators from radiation. The Savannah River National Laboratory (SRNL) is tasked with measuring the total density, partial hydrogen density, and partial boron density of the colemanite concrete. SRNL received two samples of colemanite concrete for analysis on November 21, 2013. The average total density of each of the samples measured by the ASTM method C 642, the average partial hydrogen density was measured using method ASTM E 1131, and the average partial boron density of each sample was measured according to ASTM C 1301. For all the samples tested, the total density and the boron partial density met or exceeded the specified limit. None of the samples met the lower limit for hydrogen partial density.

Reigel, Marissa M.

2013-12-18T23:59:59.000Z

483

ANALYTICAL RESULTS FOR MOX COLEMANITE CONCRETE SAMPLES RECEIVED ON NOVEMBER 21, 2013  

SciTech Connect (OSTI)

The Mixed Oxide Fuel Fabrication Facility (MFFF) will use colemanite bearing concrete neutron absorber panels credited with attenuating neutron flux in the criticality design analyses and shielding operators from radiation. The Savannah River National Laboratory (SRNL) is tasked with measuring the total density, partial hydrogen density, and partial boron density of the colemanite concrete. SRNL received two samples of colemanite concrete for analysis on November 21, 2013. The average total density of each of the samples measured by the ASTM method C 642, the average partial hydrogen density was measured using method ASTM E 1131, and the average partial boron density of each sample was measured according to ASTM C 1301. The lower limits and measured values for the total density, hydrogen partial density, and boron partial density are presented. For all the samples tested, the total density and the boron partial density met or exceeded the specified limit. None of the samples met the lower limit for hydrogen partial density.

Reigel, M.

2014-05-19T23:59:59.000Z

484

ANALYTICAL RESULTS FOR MOX COLEMANITE CONCRETE SAMPLES RECEIVED ON SEPTEMBER 4, 2013  

SciTech Connect (OSTI)

The Mixed Oxide Fuel Fabrication Facility (MFFF) will use colemanite bearing concrete neutron absorber panels credited with attenuating neutron flux in the criticality design analyses and shielding operators from radiation. The Savannah River National Laboratory (SRNL) is tasked with measuring the total density, partial hydrogen density, and partial boron density of the colemanite concrete. SRNL received three samples of colemanite concrete for analysis on September 4, 2013. The average total density of each of the samples measured by the ASTM method C 642, the average partial hydrogen density was measured using method ASTM E 1131, and the average partial boron density of each sample was measured according to ASTM C 1301. The lower limits and measured values for the total density, hydrogen partial density, and boron partial density are presented. For all the samples tested, the total density and the boron partial density met or exceeded the specified limit. None of the samples met the lower limit for hydrogen partial density.

Reigel, M.

2014-05-19T23:59:59.000Z

485

Combustion characteristics of 24 lignite samples  

SciTech Connect (OSTI)

In this study, the combustion characteristics such as thermogravimetric analysis (TGA) and differential thermogravimetric analysis (DTGA), burning profile, ignition temperature, and peak temperature were analyzed for 24 lignite samples from different areas of Turkey. The samples were heated up to 900{sup o}C at a constant rate of 10{sup o} C/min in a 5 mL/min flow of dry air. The burning profiles of the samples studied, combined with proximate, sulfur analysis and calorimetry results, contribute to a clearer identification of lignite samples' structure and a better understanding of the coalification process. The lignite samples have been tested with particle size of 0-0.05 mm. Ignition temperatures of the samples have been determined from their burning profiles.

Sensogut, C.; Ozsen, H.; Demirbas, A. [Selcuk University, Konya (Turkey)

2008-07-01T23:59:59.000Z

486

100 Area Columbia River sediment sampling  

SciTech Connect (OSTI)

Forty-four sediment samples were collected from 28 locations in the Hanford Reach of the Columbia River to assess the presence of metals and man-made radionuclides in the near shore and shoreline settings of the Hanford Site. Three locations were sampled upriver of the Hanford Site plutonium production reactors. Twenty-two locations were sampled near the reactors. Three locations were sampled downstream of the reactors near the Hanford Townsite. Sediment was collected from depths of 0 to 6 in. and between 12 to 24 in. below the surface. Samples containing concentrations of metals exceeding the 95 % upper threshold limit values (DOE-RL 1993b) are considered contaminated. Contamination by arsenic, chromium, copper, lead, and zinc was found. Man-made radionuclides occur in all samples except four collected opposite the Hanford Townsite. Man-made radionuclide concentrations were generally less than 1 pCi/g.

Weiss, S.G. [Westinghouse Hanford Co., Richland, WA (United States)

1993-09-08T23:59:59.000Z

487

Optical method for the determination of grain orientation in films  

DOE Patents [OSTI]

A method for the determination of grain orientation in a film sample is provided comprising the steps of measuring a first transient optical response of the film and determining the contribution to the transient optical response arising from a change in the energy distribution of the electrons in the sample, determining the contribution to the transient optical response arising from a propagating strain pulse within the sample, and determining the contribution to the transient optical response arising from a change in sample temperature of the sample. The grain orientation of the sample may be determined using the contributions to the transient optical response arising from the change in the energy distribution of the electrons, the propagating strain pulse, and the change in sample temperature. Additionally, a method for determination of the thickness of a film sample is provided. The grain orientation of the sample is first determined. The grain orientation, together with the velocity of sound and a propagation time of a strain pulse through the sample are then used to determine the thickness of the film sample.

Maris, Humphrey J. (Barrington, RI)

2001-01-01T23:59:59.000Z

488

Long-Term Hydrologic Monitoring Program Sampling and Analysis Results for 2012 at Rulison, Colorado  

SciTech Connect (OSTI)

The U.S. Department of Energy (DOE) Office of Legacy Management conducted annual sampling at the Rulison, Colorado, site for the Long-Term Hydrologic Monitoring Program (LTHMP) on May 8, 2012. The samples were shipped to GEL Laboratories in Charleston, South Carolina, for analysis. All requested analyses were successfully completed. Samples were analyzed for gamma-emitting radionuclides by high-resolution gamma spectrometry; tritium was analyzed using two methods. The conventional tritium method has a detection limit on the order of 400 pCi/L, and a select set of samples was analyzed for tritium using the enriched method, which has a detection limit on the order of 3 pCi/L.

None

2012-12-06T23:59:59.000Z

489

APPROPRIATE ZOOPLANKTON SAMPLING METHODOLOGY FOR OTEC SITES  

E-Print Network [OSTI]

Thermal Energy Conversion (OTEC) sites. Participants J.Zooplankton Sampling for OTEC Sites t~thodology Edited bywho gave an overview of the OTEC program, and the policies

Commins, M.L.

2014-01-01T23:59:59.000Z

490

PolyChord: nested sampling for cosmology  

E-Print Network [OSTI]

PolyChord is a novel nested sampling algorithm tailored for high dimensional parameter spaces. In addition, it can fully exploit a hierarchy of parameter speeds such as is found in CosmoMC and CAMB. It utilises slice sampling at each iteration to sample within the hard likelihood constraint of nested sampling. It can identify and evolve separate modes of a posterior semi-independently and is parallelised using openMPI. PolyChord is available for download at: http://ccpforge.cse.rl.ac.uk/gf/project/polychord/

Handley, W J; Lasenby, A N

2015-01-01T23:59:59.000Z

491

Method for measuring recovery of catalytic elements from fuel cells  

DOE Patents [OSTI]

A method is provided for measuring the concentration of a catalytic clement in a fuel cell powder. The method includes depositing on a porous substrate at least one layer of a powder mixture comprising the fuel cell powder and an internal standard material, ablating a sample of the powder mixture using a laser, and vaporizing the sample using an inductively coupled plasma. A normalized concentration of catalytic element in the sample is determined by quantifying the intensity of a first signal correlated to the amount of catalytic element in the sample, quantifying the intensity of a second signal correlated to the amount of internal standard material in the sample, and using a ratio of the first signal intensity to the second signal intensity to cancel out the effects of sample size.

Shore, Lawrence (Edison, NJ); Matlin, Ramail (Berkeley, NJ)

2011-03-08T23:59:59.000Z

492

Hanford environmental analytical methods: Methods as of March 1990. Volume 3, Appendix A2-I  

SciTech Connect (OSTI)

This paper from the analytical laboratories at Hanford describes the method used to measure pH of single-shell tank core samples. Sludge or solid samples are mixed with deionized water. The pH electrode used combines both a sensor and reference electrode in one unit. The meter amplifies the input signal from the electrode and displays the pH visually.

Goheen, S.C.; McCulloch, M.; Daniel, J.L.

1993-05-01T23:59:59.000Z

493

Macroscopic Subdivision of Silica Aerogel Collectors for Sample Return Missions  

SciTech Connect (OSTI)

Silica aerogel collector tiles have been employed for the collection of particles in low Earth orbit and, more recently, for the capture of cometary particles by NASA's Stardust mission. Reliable, reproducible methods for cutting these and future collector tiles from sample return missions are necessary to maximize the science output from the extremely valuable embedded particles. We present a means of macroscopic subdivision of collector tiles by generating large-scale cuts over several centimeters in silica aerogel with almost no material loss. The cut surfaces are smooth and optically clear allowing visual location of particles for analysis and extraction. This capability is complementary to the smaller-scale cutting capabilities previously described [Westphal (2004), Ishii (2005a, 2005b)] for removing individual impacts and particulate debris in tiny aerogel extractions. Macroscopic cuts enable division and storage or distribution of portions of aerogel tiles for immediate analysis of samples by certain techniques in situ or further extraction of samples suited for other methods of analysis.

Ishii, H A; Bradley, J P

2005-09-14T23:59:59.000Z

494

Procedures for sampling radium-contaminated soils  

SciTech Connect (OSTI)

Two procedures for sampling the surface layer (0 to 15 centimeters) of radium-contaminated soil are recommended for use in remedial action projects. Both procedures adhere to the philosophy that soil samples should have constant geometry and constant volume in order to ensure uniformity. In the first procedure, a ''cookie cutter'' fashioned from pipe or steel plate, is driven to the desired depth by means of a slide hammer, and the sample extracted as a core or plug. The second procedure requires use of a template to outline the sampling area, from which the sample is obtained using a trowel or spoon. Sampling to the desired depth must then be performed incrementally. Selection of one procedure over the other is governed primarily by soil conditions, the cookie cutter being effective in nongravelly soils, and the template procedure appropriate for use in both gravelly and nongravelly soils. In any event, a minimum sample volume of 1000 cubic centimeters is recommended. The step-by-step procedures are accompanied by a description of the minimum requirements for sample documentation. Transport of the soil samples from the field is then addressed in a discussion of the federal regulations for shipping radioactive materials. Interpretation of those regulations, particularly in light of their application to remedial action soil-sampling programs, is provided in the form of guidance and suggested procedures. Due to the complex nature of the regulations, however, there is no guarantee that our interpretations of them are complete or entirely accurate. Preparation of soil samples for radium-226 analysis by means of gamma-ray spectroscopy is described.

Fleischhauer, H.L.

1985-10-01T23:59:59.000Z

495

Portable tester for determining gas content within a core sample  

DOE Patents [OSTI]

A portable tester is provided for reading and displaying the pressure of a gas released from a rock core sample stored within a sealed container and for taking a sample of the released pressurized gas for chemical analysis thereof for subsequent use in a modified direct method test which determines the volume of gas and specific type of gas contained within the core sample. The portable tester includes a pair of low and high range electrical pressure transducers for detecting a gas pressure; a pair of low and high range display units for displaying the pressure of the detected gas- a selector valve connected to the low and high range pressure transducers, a selector knob for selecting gas flow to one of the flow paths; control valve having an inlet connection to the sealed container, and outlets connected to: a sample gas canister, a second outlet port connected to the selector valve means for reading the pressure of the gas from the sealed container to either the low range or high range pressure transducers, and a connection for venting gas contained within the sealed container to the atmosphere. A battery is electrically connected to and supplies the power for operating the unit. The pressure transducers, display units, selector and control valve means and the battery is mounted to and housed within a protective casing for portable transport and use.

Garcia, Jr., Fred (Donora, PA); Schatzel, Steven J. (Bethel Park, PA)

1998-01-01T23:59:59.000Z

496

Stratified source-sampling techniques for Monte Carlo eigenvalue analysis.  

SciTech Connect (OSTI)

In 1995, at a conference on criticality safety, a special session was devoted to the Monte Carlo ''Eigenvalue of the World'' problem. Argonne presented a paper, at that session, in which the anomalies originally observed in that problem were reproduced in a much simplified model-problem configuration, and removed by a version of stratified source-sampling. In this paper, stratified source-sampling techniques are generalized and applied to three different Eigenvalue of the World configurations which take into account real-world statistical noise sources not included in the model problem, but which differ in the amount of neutronic coupling among the constituents of each configuration. It is concluded that, in Monte Carlo eigenvalue analysis of loosely-coupled arrays, the use of stratified source-sampling reduces the probability of encountering an anomalous result over that if conventional source-sampling methods are used. However, this gain in reliability is substantially less than that observed in the model-problem results.

Mohamed, A.

1998-07-10T23:59:59.000Z

497

Method of photon spectral analysis  

DOE Patents [OSTI]

A spectroscopic method to rapidly measure the presence of plutonium in soils, filters, smears, and glass waste forms by measuring the uranium L-shell x-ray emissions associated with the decay of plutonium. In addition, the technique can simultaneously acquire spectra of samples and automatically analyze them for the amount of americium and [gamma]-ray emitting activation and fission products present. The samples are counted with a large area, thin-window, n-type germanium spectrometer which is equally efficient for the detection of low-energy x-rays (10-2,000 keV), as well as high-energy [gamma] rays (>1 MeV). A 8,192- or 16,384 channel analyzer is used to acquire the entire photon spectrum at one time. A dual-energy, time-tagged pulser, that is injected into the test input of the preamplifier to monitor the energy scale, and detector resolution. The L x-ray portion of each spectrum is analyzed by a linear-least-squares spectral fitting technique. The [gamma]-ray portion of each spectrum is analyzed by a standard Ge [gamma]-ray analysis program. This method can be applied to any analysis involving x- and [gamma]-ray analysis in one spectrum and is especially useful when interferences in the x-ray region can be identified from the [gamma]-ray analysis and accommodated during the x-ray analysis.

Gehrke, R.J.; Putnam, M.H.; Killian, E.W.; Helmer, R.G.; Kynaston, R.L.; Goodwin, S.G.; Johnson, L.O.

1993-04-27T23:59:59.000Z

498

Method of detecting sulfur dioxide  

DOE Patents [OSTI]

(CH.sub.3).sub.3 SiNSO is produced by the reaction of ((CH.sub.3).sub.3 Si).sub.2 NH with SO.sub.2. Also produced in the reaction are ((CH.sub.3).sub.3 Si).sub.2 O and a new solid compound [NH.sub.4 ][(CH.sub.3).sub.3 SiOSO.sub.2 ]. Both (CH.sub.3).sub.3 SiNSO and [NH.sub.4 ][(CH.sub.3).sub.3 SiOSO.sub.2 ] have fluorescent properties. The reaction of the subject invention is used in a method of measuring the concentration of SO.sub.2 pollutants in gases. By the method, a sample of gas is bubbled through a solution of ((CH.sub.3).sub.3 Si).sub.2 NH, whereby any SO.sub.2 present in the gas will react to produce the two fluorescent products. The measured fluorescence of these products can then be used to calculate the concentration of SO.sub.2 in the original gas sample. The solid product [NH.sub.4][(CH.sub.3).sub.3 SiOSO.sub.2 ] may be used as a standard in solid state NMR spectroscopy.

Spicer, Leonard D. (Salt Lake City, UT); Bennett, Dennis W. (Clemson, SC); Davis, Jon F. (Salt Lake City, UT)

1985-01-01T23:59:59.000Z

499

Method of photon spectral analysis  

DOE Patents [OSTI]

A spectroscopic method to rapidly measure the presence of plutonium in soils, filters, smears, and glass waste forms by measuring the uranium L-shell x-ray emissions associated with the decay of plutonium. In addition, the technique can simultaneously acquire spectra of samples and automatically analyze them for the amount of americium and .gamma.-ray emitting activation and fission products present. The samples are counted with a large area, thin-window, n-type germanium spectrometer which is equa