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Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


1

Synchroton X-Ray Studies of Liquid-Vapor Interfaces  

Science Journals Connector (OSTI)

The variation of density across the liquid-vapor interface from essentially zero density far out in the vapor phase to a homogeneous density deep in the liquid phase can be determined by X-ray reflectivity mea...

J. Als-Nielsen

1988-01-01T23:59:59.000Z

2

X-ray reflectivity measurements of liquid/solid interfaces under high hydrostatic pressure conditions  

Science Journals Connector (OSTI)

A high hydrostatic pressure cell for X-ray reflectivity measurements at the solid/liquid interface is presented.

Wirkert, F.J.

2013-11-02T23:59:59.000Z

3

A novel X-ray diffractometer for studies of liquid-liquid interfaces  

Science Journals Connector (OSTI)

A dedicated liquid surface diffractometer employing a tilting double-crystal monochromator in Bragg geometry has been designed. This diffractometer allows reflectivity and grazing-incidence scattering measurements of an immobile mechanical completely decoupled liquid sample from 6.4 to 29.4 keV.

Murphy, B.M.

2013-11-29T23:59:59.000Z

4

X-rays at Solid-Liquid Surfaces  

SciTech Connect (OSTI)

Solid-liquid interfaces play an important role in many areas of current and future technologies, and in our biosphere. They play a key role in the development of nanofluidics and nanotribology, which sensitively depend on our knowledge of the microscopic structures and phenomena at the solid-liquid interface. The detailed understanding of how a fluid meets a wall is also a theoretical challenge. In particular, the phenomena at repulsive walls are of interest, since they affect many different phenomena, such as water-repellent surfaces or the role of the hydrophobic interaction in protein folding. Recent x-ray reflectivity studies of various solid-liquid interfaces have disclosed rather intriguiing phenomena, which will be discussed in this lecture: premelting of ice in contact with silica; liquid Pb in contact with Si; water in contact with hydrophobic surfaces. These experiments, carried out with high-energy x-ray microbeams, reveal detailed insight into the liquid density profile closest to the wall. A detailed insight into atomistic phenomena at solid-liquid interfaces is also a prerequisite in the microscopic control of electrochemical reactions at interfaces. Recent x-ray studies show the enormous future potential of such non-destructive analytical tools for the in situ observation of (electro-)chemical surface reactions. This lecture will review recent x-ray experiments on solid-liquid interfaces.

Dosch, Helmut (Max Planck Institute for Metals Research) [Max Planck Institute for Metals Research

2007-05-02T23:59:59.000Z

5

High intensity x-ray source using liquid gallium target  

DOE Patents [OSTI]

A high intensity x-ray source that uses a flowing stream of liquid gallium as a target with the electron beam impinging directly on the liquid metal.

Smither, Robert K. (Hinsdale, IL); Knapp, Gordon S. (Cupertino, CA); Westbrook, Edwin M. (Chicago, IL); Forster, George A. (Westmont, IL)

1990-01-01T23:59:59.000Z

6

X-ray resonant magnetic scattering from structurally and magnetically rough interfaces in multilayered systems. I. Specular reflectivity  

E-Print Network [OSTI]

X-ray resonant magnetic scattering from structurally and magnetically rough interfaces formulation of x-ray resonant magnetic scattering from rough surfaces and interfaces is given for specular/Fe multilayer. DOI: 10.1103/PhysRevB.68.224409 PACS number s : 75.70.Cn, 61.10.Kw I. INTRODUCTION X-ray

Haskel, Daniel

7

X-ray studies of the phases and phase transitions of liquid crystals  

Science Journals Connector (OSTI)

Recent X-ray diffraction studies of liquid crystals are reviewed. The topics are twist grain-boundary phases, antiferroelectric phases studied using resonant diffraction and smectic phases within gel structures.

Clegg, P.S.

2004-12-22T23:59:59.000Z

8

Soft X-ray emission spectroscopy of liquids and lithium batterymaterials  

SciTech Connect (OSTI)

Lithium ion insertion into electrode materials is commonly used in rechargeable battery technology. The insertion implies changes in both the crystal structure and the electronic structure of the electrode material. Side-reactions may occur on the surface of the electrode which is exposed to the electrolyte and form a solid electrolyte interface (SEI). The understanding of these processes is of great importance for improving battery performance. The chemical and physical properties of water and alcohols are complicated by the presence of strong hydrogen bonding. Various experimental techniques have been used to study geometrical structures and different models have been proposed to view the details of how these liquids are geometrically organized by hydrogen bonding. However, very little is known about the electronic structure of these liquids, mainly due to the lack of suitable experimental tools. In this thesis examples of studies of lithium battery electrodes and liquid systems using soft x-ray emission spectroscopy will be presented. Monochromatized synchrotron radiation has been used to accomplish selective excitation, in terms of energy and polarization. The electronic structure of graphite electrodes has been studied, before and after lithium intercalation. Changes in the electronic structure upon lithiation due to transfer of electrons into the graphite {pi}-bands have been observed. Transfer of electrons in to the 3d states of transition metal oxides upon lithiation have been studied, through low energy excitations as dd- and charge transfer-excitations. A SEI was detected on cycled graphite electrodes. By the use of selective excitation different carbon sites were probed in the SEI. The local electronic structure of water, methanol and mixtures of the two have been examined using a special liquid cell, to separate the liquid from the vacuum in the experimental chamber. Results from the study of liquid water showed a strong influence on the 3a1 molecular orbital and orbital mixing between water molecules upon hydrogen bonding. Apart from the four-hydrogen-bonding structure in water, a structure where one hydrogen bond is broken could be separated and identified. The soft x-ray emission study of methanol showed the existence of ring and chain formations in the liquid phase and the dominating structures are formed of 6 and 8 molecules. Upon mixing of the two liquids, a segregation at the molecular level was found and the formation of new structures, which could explain the unexpected low increase of the entropy.

Augustsson, Andreas

2004-10-27T23:59:59.000Z

9

Ultrafast conversions between hydrogen bonded structures in liquid water observed by femtosecond x-ray spectroscopy  

SciTech Connect (OSTI)

We present the first femtosecond soft x-ray spectroscopy in liquids, enabling the observation of changes in hydrogen bond structures in water via core-hole excitation. The oxygen K-edge of vibrationally excited water is probed with femtosecond soft x-ray pulses, exploiting the relation between different water structures and distinct x-ray spectral features. After excitation of the intramolecular OH stretching vibration, characteristic x-ray absorption changes monitor the conversion of strongly hydrogen-bonded water structures to more disordered structures with weaker hydrogen-bonding described by a single subpicosecond time constant. The latter describes the thermalization time of vibrational excitations and defines the characteristic maximum rate with which nonequilibrium populations of more strongly hydrogen-bonded water structures convert to less-bonded ones. On short time scales, the relaxation of vibrational excitations leads to a transient high-pressure state and a transient absorption spectrum different from that of statically heated water.

Wen, Haidan; Huse, Nils; Schoenlein, Robert W.; Lindenberg, Aaron M.

2010-05-01T23:59:59.000Z

10

A microfocus x-ray source based on a nonmetal liquid-jet anode  

SciTech Connect (OSTI)

We demonstrate stable operation of a nonmetallic anode in an electron-impact x-ray source. A high-brightness electron beam is focused on a {approx}70 m/s speed, {approx}10 {mu}m diameter methanol jet producing stable x-ray emission with peak spectral brightness at {approx}5.4x10{sup 5} photons/(sx{mu}m{sup 2}xsrx0.1%BW). The jet is fully evaporated in the interaction point. The shape of a simulated spectrum using Monte Carlo methods shows good agreement with experimental data, and the theoretical brightness values give an upper limit for the achievable x-ray emission from jets with very high velocities. Using this anode concept, all compounds and elements found in liquid form are potentially usable for x-ray generation.

Tuohimaa, T.; Ewald, J.; Schlie, M.; Hertz, H. M.; Vogt, U. [Biomedical and X-ray Physics, Department of Applied Physics, KTH Royal Institute of Technology/Albanova, SE-10691 Stockholm (Sweden); Fernandez-Varea, J. M. [Facultat de Fisica (ECM), Universitat de Barcelona, Diagonal 647, ES-08028 Barcelona (Spain)

2008-06-09T23:59:59.000Z

11

Off-Specular X-ray and Neutron Reflectometry for the Structural Characterization of Buried Interfaces  

SciTech Connect (OSTI)

Off-specular reflectivity or diffuse scattering is sensitive to lateral compositional variations at surfaces and interfaces. It is particularly well-suited as a means of measuring the form and amplitude of surface roughness, as well as separating contributions from physical roughness and gradients in material density. The roughness and lateral correlation lengths of model rough surfaces were cross-correlated using neutron and x-ray off-specular reflectivity (OSNR and OSXR, respectively), and using power spectral density (PSD) analysis of atomic force microscopy (AFM) data. These experiments highlight the advantages of the technique for the investigation of buried interfaces while illustrating how x-ray and neutron techniques work complementarily to measure interfacial roughness.

Lavery, Kristopher A.; Prabhu, Vivek M.; Lin, Eric K.; Wu, Wen-li [Polymers Division and Center for Neutron Research, National Institute of Standards and Technology, Gaithersburg, MD (United States); Satija, Sushil [Center for Neutron Research, National Institute of Standards and Technology, Gaithersburg, MD (United States); Wormington, Matthew [Bede Scientific Inc., Englewood, CO (United States)

2007-09-26T23:59:59.000Z

12

Verification of universal surface scaling behavior in critical binary liquid mixtures with neutron and x-ray reflectometry.  

E-Print Network [OSTI]

??We have studied two critical binary liquid mixtures in the mixed phase regime with x-ray and neutron reflectometry to verify universal critical scaling at a… (more)

Brown, Matthew D.

2007-01-01T23:59:59.000Z

13

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print The geometric structure of liquid water has been investigated in detail by many techniques, but many details are still under debate, such as the actual number of hydrogen bonds (at a given time) between the various water molecules. Even less is known about the electronic structure. Since it is the intermittent bonding between water molecules that gives liquid water its peculiar characteristics, the electronic structure plays a crucial role in understanding the properties of the liquid state. Consequently, information essential for insight into chemical and biological processes in aqueous environments is lacking. To address this need, researchers from Germany and the U.S. have used soft x-ray spectroscopy at the ALS to gain detailed insight into the electronic structure of liquid water. Their spectra show a strong isotope and a weak temperature effect, and, for the first time, a splitting of the primary emission line in x-ray emission spectra. By making use of the internal "femtosecond clock" of the core-hole lifetime, a detailed picture of the electronic structure can be painted that involves fast dissociation processes of the probed water molecules.

14

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print The geometric structure of liquid water has been investigated in detail by many techniques, but many details are still under debate, such as the actual number of hydrogen bonds (at a given time) between the various water molecules. Even less is known about the electronic structure. Since it is the intermittent bonding between water molecules that gives liquid water its peculiar characteristics, the electronic structure plays a crucial role in understanding the properties of the liquid state. Consequently, information essential for insight into chemical and biological processes in aqueous environments is lacking. To address this need, researchers from Germany and the U.S. have used soft x-ray spectroscopy at the ALS to gain detailed insight into the electronic structure of liquid water. Their spectra show a strong isotope and a weak temperature effect, and, for the first time, a splitting of the primary emission line in x-ray emission spectra. By making use of the internal "femtosecond clock" of the core-hole lifetime, a detailed picture of the electronic structure can be painted that involves fast dissociation processes of the probed water molecules.

15

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print The geometric structure of liquid water has been investigated in detail by many techniques, but many details are still under debate, such as the actual number of hydrogen bonds (at a given time) between the various water molecules. Even less is known about the electronic structure. Since it is the intermittent bonding between water molecules that gives liquid water its peculiar characteristics, the electronic structure plays a crucial role in understanding the properties of the liquid state. Consequently, information essential for insight into chemical and biological processes in aqueous environments is lacking. To address this need, researchers from Germany and the U.S. have used soft x-ray spectroscopy at the ALS to gain detailed insight into the electronic structure of liquid water. Their spectra show a strong isotope and a weak temperature effect, and, for the first time, a splitting of the primary emission line in x-ray emission spectra. By making use of the internal "femtosecond clock" of the core-hole lifetime, a detailed picture of the electronic structure can be painted that involves fast dissociation processes of the probed water molecules.

16

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print The geometric structure of liquid water has been investigated in detail by many techniques, but many details are still under debate, such as the actual number of hydrogen bonds (at a given time) between the various water molecules. Even less is known about the electronic structure. Since it is the intermittent bonding between water molecules that gives liquid water its peculiar characteristics, the electronic structure plays a crucial role in understanding the properties of the liquid state. Consequently, information essential for insight into chemical and biological processes in aqueous environments is lacking. To address this need, researchers from Germany and the U.S. have used soft x-ray spectroscopy at the ALS to gain detailed insight into the electronic structure of liquid water. Their spectra show a strong isotope and a weak temperature effect, and, for the first time, a splitting of the primary emission line in x-ray emission spectra. By making use of the internal "femtosecond clock" of the core-hole lifetime, a detailed picture of the electronic structure can be painted that involves fast dissociation processes of the probed water molecules.

17

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print Isotope and Temperature Effects in Liquid Water Probed by Soft X Rays Print The geometric structure of liquid water has been investigated in detail by many techniques, but many details are still under debate, such as the actual number of hydrogen bonds (at a given time) between the various water molecules. Even less is known about the electronic structure. Since it is the intermittent bonding between water molecules that gives liquid water its peculiar characteristics, the electronic structure plays a crucial role in understanding the properties of the liquid state. Consequently, information essential for insight into chemical and biological processes in aqueous environments is lacking. To address this need, researchers from Germany and the U.S. have used soft x-ray spectroscopy at the ALS to gain detailed insight into the electronic structure of liquid water. Their spectra show a strong isotope and a weak temperature effect, and, for the first time, a splitting of the primary emission line in x-ray emission spectra. By making use of the internal "femtosecond clock" of the core-hole lifetime, a detailed picture of the electronic structure can be painted that involves fast dissociation processes of the probed water molecules.

18

Kinetics of alloy formation at the interfaces in a Ni-Ti multilayer: X-ray and neutron reflectometry study  

Science Journals Connector (OSTI)

Vacuum-deposited Ni/Ti multilayers on annealing at different temperatures exhibit formation of ordered alloy layers at interfaces. We have studied in detail the formation of alloy at interfaces of a Ni/Ti multilayer on annealing at 300?°C and 400?°C using powder x-ray diffraction, x-ray reflectometry, polarized neutron reflectometry, and off-specular x-ray reflectometry techniques. Correlation among structural, magnetic, and morphological properties in as-deposited Ni/Ti multilayer as well as in a sample annealed at 300?°C and 400?°C has been studied. X-ray diffraction technique was used to obtain crystal structure of the sample. Specular x-ray reflectometry and neutron reflectometry were used to determine the growth of alloy layers from density profile, as a function of depth in the sample. From off-specular x-ray reflectivity we found that the in-plane correlation lengths at the interfaces grew with annealing. This is associated with alloy crystallite growth obtained from x-ray reflectometry. Detailed magnetic-moment density profile of as-deposited as well as annealed multilayer sample has been determined by polarized neutron reflectometry measurements, which was used to determine the magnetic nature of the alloy layers. The results show formation of nonmagnetic alloy layers at the interfaces on annealing. From the Bragg-peak intensities of x-ray reflectivity and polarized neutron reflectivity measurements, we have estimated the diffusion lengths after annealing at 300?°C and 400?°C.

Surendra Singh; Saibal Basu; Pramod Bhatt; A. K. Poswal

2009-05-28T23:59:59.000Z

19

Ion Distributions Near a Liquid-Liquid Interface  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Ion Distributions Near a Liquid-Liquid Interface Ion Distributions Near a Liquid-Liquid Interface Researchers from the University of Illinois at Chicago; Northern Illinois University; the University of California, Santa Cruz; and ChemMatCARS (sector 15 at the APS) used x-ray reflectivity from ion distributions at the liquid-liquid interface to provide strong evidence that the interfacial structure of a liquid alters the ion distributions near a charged interface, contrary to earlier theories about ions at charged surfaces. Coulomb's Law describes the interaction between two, otherwise isolated, point charges. If many charges are present in the region between these two charges, the net interaction between them is modified. This is commonly found in real systems, such as a plasma gas of electrons and ionized

20

X-ray fluorescence spectroscopy from ions at charged vapor/water interfaces  

E-Print Network [OSTI]

X-ray fluorescence spectra from monovalent ions (Cs+) that accumulate from dilute solutions to form an ion-rich layer near a charged Langmuir monolayer are presented. For the salt solution without the monolayer, the fluorescence signals below the critical angle are significantly lower than the detection sensitivity and only above the critical angle signals from the bulk are observed. In the presence of a monolayer that provides surface charges, strong fluorescence signals below the critical angle are observed. Ion density accumulated at the interface are determined from the fluorescence. The fluorescent spectra collected as a function of incident x-ray energy near the LIII edge yield the extended absorption spectra from the ions, and are compared to recent independent results. The fluorescence data from divalent Ba2+ with and without monolayer are also presented.

Wei Bu; David Vaknin

2009-05-04T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

A liquid-helium cooled large-area silicon PIN photodiode x-ray detector  

E-Print Network [OSTI]

An x-ray detector using a liquid-helium cooled large-area silicon PIN photodiode has been developed along with a tailor-made charge sensitive preamplifier whose first-stage JFET has been cooled. The operating temperature of the JFET has been varied separately and optimized. The x- and $\\gamma$-ray energy spectra for an \

Yoshizumi Inoue; Shigetaka Moriyama; Hideyuki Hara; Makoto Minowa; Fumio Shimokoshi

1995-04-27T23:59:59.000Z

22

Atomic-scale chemical quantification of oxide interfaces using energy-dispersive X-ray spectroscopy  

SciTech Connect (OSTI)

Atomic-scale quantification of chemical composition across oxide interfaces is important for understanding physical properties of epitaxial oxide nanostructures. Energy-dispersive X-ray spectroscopy (EDS) in an aberration-corrected scanning transmission electron microscope was used to quantify chemical composition across the interface of ferromagnetic La{sub 0.7}Sr{sub 0.3}MnO{sub 3} and antiferromagnetic BiFeO{sub 3} quantum structure. This research demonstrates that chemical composition at atomic columns can be quantified by Gaussian peak-fitting of EDS compositional profiles across the interface. Cation diffusion was observed at both A- and B-sublattice sites; and asymmetric chemical profiles exist across the interface, consistent with the previous studies.

Lu, Ping; Van Benthem, Mark [Sandia National Laboratories, P.O. Box 5800, MS 1411, Albuquerque, New Mexico 87185-1411 (United States)] [Sandia National Laboratories, P.O. Box 5800, MS 1411, Albuquerque, New Mexico 87185-1411 (United States); Xiong, Jie; Jia, Quanxi [Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)] [Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)

2013-04-29T23:59:59.000Z

23

Hort-Range Wetting at Liquid Gallium-Bismuth Alloy Surfaces: X-ray Measurements and Square-Gradient Theory  

SciTech Connect (OSTI)

We present an x-ray reflectivity study of wetting at the free surface of the binary liquid metal alloy gallium-bismuth (Ga-Bi) in the region where the bulk phase separates into Bi-rich and Ga-rich liquid phases. The measurements reveal the evolution of the microscopic structure of the wetting films of the Bi-rich, low-surface-tension phase along several paths in the bulk phase diagram. The wetting of the Ga-rich bulk's surface by a Bi-rich wetting film, the thickness of which is limited by gravity to only 50 Angstroms, creates a Ga-rich/Bi-rich liquid/liquid interface close enough to the free surface to allow its detailed study by x rays. The structure of the interface is determined with Angstromsngstrem resolution, which allows the application of a mean-field square gradient model extended by the inclusion of capillary waves as the dominant thermal fluctuations. The sole free parameter of the gradient model, the influence parameter K, that characterizes the influence of concentration gradients on the interfacial excess energy, is determined from our measurements. This, in turn, allows a calculation of the liquid/liquid interfacial tension, and a separation of the intrinsic and capillary wave contributions to the interfacial structure. In spite of expected deviations from MF behavior, based on the upper critical dimensionality (Du = 3 ) of the bulk, we find that the capillary wave excitations only marginally affect the short-range complete wetting behavior. A critical wetting transition that is sensitive to thermal fluctuations appears to be absent in this binary liquid-metal alloy.

Huber, P.; Shpyrko, O; Pershan, P; Ocko, B; DiMasi, E; Deutsch, M

2009-01-01T23:59:59.000Z

24

Spatially resolved x-ray studies of liquid crystals with strongly developed bond-orientational order  

E-Print Network [OSTI]

We present an x-ray study of freely suspended hexatic films of the liquid crystal 3(10)OBC. Our results reveal spatial inhomogeneities of the bond-orientational (BO) order in the vicinity of the hexatic-smectic phase transition and the formation of large scale hexatic domains at lower temperatures. Deep in the hexatic phase up to 25 successive sixfold BO order parameters have been directly determined by means of angular x-ray cross-correlation analysis (XCCA). Such strongly developed hexatic order allowed us to determine higher order correction terms in the scaling relation predicted by the multicritical scaling theory over a full temperature range of the hexatic phase existence.

I. A. Zaluzhnyy; R. P. Kurta; E. A. Sulyanova; O. Y. Gorobtsov; A. G. Shabalin; A. V. Zozulya; A. P. Menushenkov; M. Sprung; B. I. Ostrovskii; I. A. Vartanyants

2014-12-03T23:59:59.000Z

25

A new Diffractometer for Studies of Liquid-Liquid Interfaces  

SciTech Connect (OSTI)

We have designed a novel, dedicated diffractometer for surface x-ray scattering studies of liquid-liquid and liquid-gas interfaces for the PETRA III High Resolution Diffraction Beamline. Using a double crystal beam-tilter in Bragg geometry this new instrument enables reflectivity and grazing incidence diffraction investigations without moving the sample, which is mechanically decoupled from the rest of the diffractometer. This design minimizes external excitation of surface vibrations, a key prerequisite for studies of liquid interfaces. The instrument operates over the energy range 6.4 keV to 30 keV, the higher energy range being optimal for penetration through liquid sample environments. Vertical momentum transfer up to q{sub z} 2.5 A{sup -1} and lateral q{sub ||} up to 4 A{sup -1}will be available.

Murphy, B. M.; Greve, M.; Runge, B.; Koops, C. T.; Elsen, A.; Stettner, J.; Magnussen, O. M. [IEAP, Christian-Albrechts-Universitaet zu Kiel, D-24098 Kiel (Germany); Seeck, O. H. [PETRA III at DESY, Notkestr. 85, D-22603 Hamburg (Germany)

2010-06-23T23:59:59.000Z

26

A Superconducting Tunnel Junction X-ray Spectrometer without Liquid Cryogens  

SciTech Connect (OSTI)

Superconducting tunnel junctions (STJs) are being developed as X-ray detectors because they combine the high energy resolution of cryogenic detector technologies with the high count rate capabilities of athermal devices. We have built STJ spectrometers for chemical analysis of dilute samples by high-resolution soft X-ray spectroscopy at the synchrotron. The instruments use 36 pixels of 200 {micro}m x 200 {micro}m Nb-Al-AlOx-Al-Nb STJs with 165 nm thick Nb absorber films. They have achieved an energy resolution of {approx}10-20 eV FWHM for X-ray energies below 1 keV, and can be operated at a total count rate of {approx}10{sup 6} counts/s. For increased user-friendliness, we have built a liquid-cryogen-free refrigerator based on a two-stage pulse tube cryocooler in combination with a two-stage adiabatic demagnetization stage. It holds the STJ detector at the end of a 40-cm-long cold finger, and attains the required operating temperature of {approx}0.3 K at the push of a button. We describe the instrument performance and present speciation measurements on Eu dopant activators in the novel scintillator material SrI{sub 2} to illustrate the potential for STJ spectrometers at the synchrotron.

Friedrich, S; Hertrich, T; Drury, O B; Cherepy, N J; Hohne, J

2008-06-15T23:59:59.000Z

27

High energy x-ray scattering studies of the local order in liquid Al  

SciTech Connect (OSTI)

The x-ray structure factors and densities for liquid aluminum from 1123 K to 1273 K have been measured using the beamline electrostatic levitator. Atomic structures as a function of temperature have been constructed from the diffraction data with reverse Monte Carlo simulations. An analysis of the local atomic structures in terms of the Honeycutt-Andersen indices indicates a high degree of icosahedral and distorted icosahedral order, a modest amount of body-centered cubic order, and marginal amounts of face-centered cubic and hexagonal close-packed order.

Mauro, N.A.; Bendert, J.C.; Vogt, A.J.; Gewin, J.M.; Kelton, K.F. (WU)

2012-10-23T23:59:59.000Z

28

Synchrotron X-ray Studies of Super-critical Carbon Dioxide / Reservoir Rock Interfaces  

Broader source: Energy.gov [DOE]

Project obectives: Utilize synchrotron X-ray measurements, to monitor all aspects of atomic to nanoscale structural changes resulting from chemical interactions of scCO2-H2O binary fluids with rocks under environments directly relevant to EGS.

29

Surface structure of liquid Bi and Sn: An x-ray reflectivity study  

SciTech Connect (OSTI)

X-ray reflectivity measurements of the liquid Bi surface are presented and analyzed together with previous liquid Sn results. Published measurements on liquid Ga, In, and K all exhibit a single strong maximum at a wave-vector transfer of the order of the reciprocal of an atomic-diameter, due to surface-induced layering. In contrast, both Sn and Bi exhibit - in addition - a weak broad peak at much smaller wave-vector transfers. This feature is an unambiguous signature of an enhanced electron density in the near-surface region. Possible ways of modeling this enhancement are presented. Once the different surface-roughening effects of thermal capillary waves are accounted for, the surface structure factors of Sn and Bi are remarkably similar. The principal difference between the two is that the depth of the layering below the surface is more than {approx}40% larger for Bi than for Sn. This is considerably larger than the ratio of their covalent radii which is only {approx}10%. No theoretical explanation can be offered at this time for the surface structure difference between Sn and Bi and other elemental liquid metals studied to date: Ga, In, and K.

Pershan, P.S.; Stoltz, S.E.; Shpyrko, Oleg G.; Deutsch, Moshe; Balagurusamy, V.S.K.; Meron, Mati; Lin, Binhua; Streitel, Reinhard; (Bar-Ilan U.); (Harvard); (UCSD); (UC)

2009-03-23T23:59:59.000Z

30

Low-Dimensional Water on Ru(0001)Model System for X-ray Absorption Spectroscopy Studies of Liquid Water  

SciTech Connect (OSTI)

We present an x-ray absorption spectroscopy results for fully broken to a complete H-bond network of water molecules on Ru(0001) by varying the morphology from isolated water molecules via two-dimensional clusters to a fully covered monolayer as probed by scanning tunneling microscopy. The sensitivity of x-ray absorption to the symmetry of H-bonding is further elucidated for the amino (-NH{sub 2}) group in glycine adsorbed on Cu(110) where the E-vector is parallel either to the NH donating an H-bond or to the non-H-bonded NH. The results give further evidence for the interpretation of the various spectral features of liquid water and for the general applicability of x-ray absorption spectroscopy to analyze H-bonded systems.

Nordlund, D

2012-02-14T23:59:59.000Z

31

Low-Dimensional Water on Ru(0001); Model System for X-ray Absorption Spectroscopy Studies of Liquid Water  

SciTech Connect (OSTI)

We present an x-ray absorption spectroscopy results for fully broken to a complete H-bond network of water molecules on Ru(0001) by varying the morphology from isolated water molecules via two-dimensional clusters to a fully covered monolayer as probed by scanning tunneling microscopy. The sensitivity of x-ray absorption to the symmetry of H-bonding is further elucidated for the amino (-NH{sub 2}) group in glycine adsorbed on Cu(110) where the E-vector is parallel either to the NH donating an H-bond or to the non-H-bonded NH. The results give further evidence for the interpretation of the various spectral features of liquid water and for the general applicability of x-ray absorption spectroscopy to analyze H-bonded systems.

Nordlund, D.; Ogasawara, H.; Andersson, K.J.; Tatarkhanov, M.; Salmeron, M.; Pettersson, L. G. M.; Nilsson, A.

2009-05-11T23:59:59.000Z

32

Portable chamber for the study of UHV prepared electrochemical interfaces by hard x-ray diffraction  

SciTech Connect (OSTI)

We report on a new electrochemical cell setup, combined with a portable UHV chamber, for in situ x-ray diffraction using synchrotron radiation. In contrast to more traditional electrochemical sample preparation schemes, atomically clean and well-ordered surfaces are routinely prepared by UHV methods, even in the case of reactive elements or alloys. Samples can be transferred from larger UHV systems into the portable chamber without exposure to ambient air. They can then be studied successively in UHV, in controlled gas atmospheres, and in contact with electrolyte solutions under applied electrochemical potential. The electrochemical setup employs a droplet geometry, which guarantees good electrochemical conditions during in situ x-ray measurements combined with voltammetry. We present first experimental results of Cu deposition on GaAs(001) and on freshly produced nanometric Pd(001) islands on Cu{sub 0.83}Pd{sub 0.17}(001), respectively.

Renner, Frank Uwe; Gruender, Yvonne; Zegenhagen, Joerg [European Synchrotron Radiation Facility, BP 220, 38043 Grenoble (France)

2007-03-15T23:59:59.000Z

33

Magnetism at spinel thin film interfaces probed through soft x-ray spectroscopy techniques  

E-Print Network [OSTI]

Magnetism at spinel thin ?lm interfaces probed through softachievable in bulk form. Magnetism at the interface regionand the origin of the magnetism from multiple magnetic

Chopdekar, R.V.

2010-01-01T23:59:59.000Z

34

Structure and Depletion at Fluorocarbon and Hydrocarbon/Water Liquid/Liquid Interfaces  

Science Journals Connector (OSTI)

The results of x-ray reflectivity studies of two oil/water (liquid/liquid) interfaces are inconsistent with recent predictions of the presence of a vaporlike depletion region at hydrophobic/aqueous interfaces. One of the oils, perfluorohexane, is a fluorocarbon whose superhydrophobic interface with water provides a stringent test for the presence of a depletion layer. The other oil, heptane, is a hydrocarbon and, therefore, is more relevant to the study of biomolecular hydrophobicity. These results are consistent with the subangstrom proximity of water to soft hydrophobic materials.

Kaoru Kashimoto; Jaesung Yoon; Binyang Hou; Chiu-hao Chen; Binhua Lin; Makoto Aratono; Takanori Takiue; Mark L. Schlossman

2008-08-14T23:59:59.000Z

35

From ultra-high vacuum to the electrochemical interface : x-ray scattering studies of model electrocatalysts.  

SciTech Connect (OSTI)

In-situ surface X-ray scattering (SXS) has become a powerful probe of the atomic structure at the metal-electrolyte interface. In this paper we describe an experiment in which a Pt(111) sample is prepared under ultra-high vacuum (UHV) conditions to have a p(2 x 2) oxygen layer adsorbed on the surface. The surface is then studied using SXS under UHV conditions before successive transfer to a bulk water environment and then to the electrochemical environment (0.1 M KOH solution) under an applied electrode potential. The Pt surface structure is examined in detail using crystal truncation rod (CTR) measurements under these different conditions. Finally, some suggestions for future experiments on alloy materials, using the same methodology, are proposed and discussed in relation to previous results.

Lucas, C. A.; Cormack, M.; Gallagher, M. E.; Brownrigg, A.; Thompson, P.; Fowler, B.; Grunder, Y.; Roy, J.; Stamenkovic, V.; Markovic, N. M.; Materials Science Division; Univ. of Liverpool; European Synchrotron Radiation Facility

2008-08-01T23:59:59.000Z

36

X-ray study of the electric double layer at the n-hexane/nanocolloidal silica interface  

E-Print Network [OSTI]

The spatial structure of the transition region between an insulator and an electrolyte solution was studied with x-ray scattering.The electron density profile across the n-hexane/silica sol interface (solutions with 5-nm, 7-nm, and 12-nm colloidal particles) agrees with the theory of the electrical double layer and shows separation of positive and negative charges. The interface consists of three layers, i.e., a compact layer of Na+, a loose monolayer of nanocolloidal particles as part of a thick diffuse layer, and a low-density layer sandwiched between them. Its structure is described by a model in which the potential gradient at the interface reflects the difference in the potentials of "image forces" between the cationic Na+ and anionic nanoparticles and the specific adsorption of surface charge. The density of water in the large electric field (1-10 GV/m) of the transition region and the layering of silica in the diffuse layer is discussed.

Aleksey M. Tikhonov

2006-09-11T23:59:59.000Z

37

A liquid densitometer with improved sensitivity employing X-ray transmission techniques  

E-Print Network [OSTI]

A CKNOWLEDGEMENTS LIST OF FIGURES I. INTRODUCTION II. DETERMINATION OFLIQUID DENSITY WITH RADIOISOTOPES Selection of Technique and Radiation Type 3 Selection of Detection System Theory of Density Determinsiion by Radiation Trensmission... Selection of Radioisotope III. DETECTION OF LOW ENERGY X-RAYS IV. DESIGN OF DENSITOMETER 13 18 Design Criteria Density Measuring Cell V. CALIBRATION'OF THE DENSITOMETER VI. RESULTS VII. SUMMARY AND CONCLUSIONS APPENDIX I. APPENDIX II. APPENDIX...

Reuscher, Jon Arthur

1962-01-01T23:59:59.000Z

38

Dissolution dynamics of the calcite-water interface observed in situ by glancing-incidence X-ray scattering  

SciTech Connect (OSTI)

Glancing-incidence X-ray scattering measurements made at the National Synchrotron Light Source were used to investigate dissolution dynamics in situ at the calcite-water interface. The relation between calcite saturation state and roughness of the calcite (1014) cleavage surface as a function of time was examined during pH titrations of an initially calcite-saturated solution. Systematic variations in roughness were observed as a function of saturation state as pH was titrated to values below that of calcite saturation. Different steady-state values of roughness were evident at fixed values of {Delta}G{sub r}, and these were correlated with the extent of undersaturation. A significant increase in roughness begins to occur with increasing undersaturation at a {Delta}G{sub r} value of approximately {minus}2.0 kcal/mol. The dissolution rate corresponding to this increase is about 1.5 x 10{sup 7} mmol/cm {center_dot} sec. This increase in roughness is attributed to a transition in the principal rate-determining dissolution mechanism, and is consistent with both powder-reaction studies of dissolution kinetics and single-crystal dissolution studies by atomic force microscopy. These data indicate some important potential applications of GIXS in the study of mineral-water interface geochemistry.

Sturchio, N.C.; Chiarello, R.P.

1995-06-02T23:59:59.000Z

39

A Novel Dimer Interface and Conformational Changes Revealed by an X-ray Structure of B. subtilis SecA  

SciTech Connect (OSTI)

The SecA ATPase moves polypeptides post-translationally across the plasma membrane of eubacteria, but the mechanism of transport is still unclear. We describe the crystal structure of a novel dimeric form of Bacillus subtilis SecA. Dimerization of SecA occurs at the prominent groove formed by the nucleotide binding domain 2 (nbd2) and the preprotein cross-linking (ppx) domain. The dimer interface is very large, burying approximately 5400 {angstrom}{sup 2} of solvent accessible surface per monomer. Single cysteine disulfide cross-linking shows the presence of this novel SecA dimer in solution. In addition, other dimers also exist in solution, arguing that they all are in equilibrium with monomeric SecA and supporting the idea that the monomer may be the functional species. Dimerization of SecA causes an {alpha}-helix of one subunit to convert to a short {beta}-strand that participates in {beta}-sheet formation with strands in the other subunit. This conversion of secondary structure elements occurs close to the connection between the nbd1 and ppx domains, a potential site of interaction with translocation substrate. Comparing the different X-ray structures of B. subtilis SecA suggests that small changes in the nucleotide binding domains could be amplified via helix 1 of the helical scaffold domain (hsd) to generate larger movements of the domains involved in polypeptide binding.

Zimmer,J.; Li, W.; Rapoport, T.

2006-01-01T23:59:59.000Z

40

Density Profiles of Liquid/Vapor Interfaces Away from Their Critical Point  

E-Print Network [OSTI]

We examine the applicability of various model profiles for the liquid/vapor interface by X-ray reflectivities on water and ethanol and their mixtures at room temperature. Analysis of the X-ray reflecivities using various density profiles shows an error-function like profile is the most adequate within experimental error. Our finding, together with recent observations from simulation studies on liquid surfaces, strongly suggest that the capillary-wave dynamics shapes the interfacial density profile in terms of the error function.

Wei Bu; Doseok Kim; David Vaknin

2014-03-06T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Structural investigation of liquid acetic acid by neutron scattering, DFT calculations and molecular dynamics simulations. Complementarity to x-ray scattering results  

Science Journals Connector (OSTI)

Abstract Neutron scattering experiments have been performed on fully deuterated liquid acetic acid (AA) at room temperature and atmospheric pressure. The scattering data are analyzed to yield the structure factor SM(Q), the molecular form factor F1(Q) and the pair correlation function g(r). To describe the intermolecular arrangement of the liquid, we have considered two dimers and two trimers, involving the isomer cis, already described in our x-ray scattering study. Neutron scattering data show that the local order of the liquid is well described by linear and ring cis trimers. Complementarity with recent x-ray results is then highlighted. Using four force fields, MD simulations show that x-ray and neutron scattering data are better reproduced by both OPLS-AA1 and OPLS-AA2 potentials.

Sonia Fathi; Salah Bouazizi; Sahbi Trabelsi; Miguel Angel Gonzalez; Mohamed Bahri; Salah Nasr; Marie-Claire Bellissent-Funel

2014-01-01T23:59:59.000Z

42

Atomic scale interface engineering by modulated ion-assisted deposition applied to soft x-ray multilayer optics  

Science Journals Connector (OSTI)

Cr/Sc and Ni/V multilayers, intended as normal incidence soft x-ray mirrors and Brewster angle polarizers, have been synthesized by employing a novel modulated low-energy and...

Eriksson, Fredrik; Ghafoor, Naureen; Schäfers, Franz; Gullikson, Eric M; Aouadi, Samir; Rohde, Susanne; Hultman, Lars; Birch, Jens

2008-01-01T23:59:59.000Z

43

Initial stages of ITO/Si interface formation: In situ x-ray photoelectron spectroscopy measurements upon magnetron sputtering and atomistic modelling using density functional theory  

SciTech Connect (OSTI)

Initial stages of indium tin oxide (ITO) growth on a polished Si substrate upon magnetron sputtering were studied experimentally using in-situ x-ray photoelectron spectroscopy measurements. The presence of pure indium and tin, as well as Si bonded to oxygen at the ITO/Si interface were observed. The experimental observations were compared with several atomistic models of ITO/Si interfaces. A periodic model of the ITO/Si interface was constructed, giving detailed information about the local environment at the interface. Molecular dynamics based on density functional theory was performed, showing how metal-oxygen bonds are broken on behalf of silicon-oxygen bonds. These theoretical results support and provide an explanation for the present as well as previous ex-situ and in-situ experimental observations pointing to the creation of metallic In and Sn along with the growth of SiO{sub x} at the ITO/Si interface.

Løvvik, O. M.; Diplas, S.; Ulyashin, A. [SINTEF Materials and Chemistry, Forskningsveien 1, NO-0314 Oslo (Norway); Romanyuk, A. [University of Basel, Kingelbergstr. 82, CH-4056 Basel (Switzerland)

2014-02-28T23:59:59.000Z

44

X-ray Absorption Spectroscopy of Biologically Relevant Systems  

E-Print Network [OSTI]

308, Messer, B. M. X-ray Absorption Spectroscopy of AqueousSarcosine via X-ray Absorption Spectroscopy 5.1 Introductionwith Carboxylate by X-Ray Absorption Spectroscopy of Liquid

Uejio, Janel Sunayo

2010-01-01T23:59:59.000Z

45

Synchrotron X-ray Studies of Super-critical Carbon Dioxide /...  

Broader source: Energy.gov (indexed) [DOE]

Synchrotron X-ray Studies of Super-critical Carbon Dioxide Reservoir Rock Interfaces Synchrotron X-ray Studies of Super-critical Carbon Dioxide Reservoir Rock Interfaces...

46

Probing photochemical transformations at TiO{sub 2}/Pt and TiO{sub 2}/Ir interfaces using x-ray absorption spectroscopy  

SciTech Connect (OSTI)

Structural transformations at the TiO{sub 2}/Pt and TiO{sub 2}/Ir interfaces during UV-irradiation have been probed by X-ray absorption spectroscopy. Oxidation by the photogenerated holes results in the intercalation of Pt and Ir into the Titania matrix. The structural transformations observed with Pt and Ir nanoparticles anchored on TiO{sub 2} is different than the clustering of gold atoms observed in the TiO{sub 2}/Au system. Implications of such structural transformations on the photocatalytic activity of semiconductor photocatalyts are discussed.

Lahiri, Debdutta; Subramanian, V.; Bunker, Bruce A.; Kamat, Prashant V. [Synchrotron Radiation Section, Physics Group, Bhabha Atomic Research Centre, Mumbai 400085 (India); Department of Chemical Engineering, University of Illinois at Urbana-Champaign, Illinois 61801 (United States); Department of Physics, University of Notre Dame, Indiana 46556 (United States); Radiation Laboratory, University of Notre Dame, Indiana 46556 (United States)

2006-05-28T23:59:59.000Z

47

Setup for in situ investigation of gases and gas/solid interfaces by soft x-ray emission and absorption spectroscopy  

SciTech Connect (OSTI)

We present a novel gas cell designed to study the electronic structure of gases and gas/solid interfaces using soft x-ray emission and absorption spectroscopies. In this cell, the sample gas is separated from the vacuum of the analysis chamber by a thin window membrane, allowing in situ measurements under atmospheric pressure. The temperature of the gas can be regulated from room temperature up to approximately 600?°C. To avoid beam damage, a constant mass flow can be maintained to continuously refresh the gaseous sample. Furthermore, the gas cell provides space for solid-state samples, allowing to study the gas/solid interface for surface catalytic reactions at elevated temperatures. To demonstrate the capabilities of the cell, we have investigated a TiO{sub 2} sample behind a mixture of N{sub 2} and He gas at atmospheric pressure.

Benkert, A., E-mail: andreas.benkert@kit.edu, E-mail: l.weinhardt@kit.edu [Institute for Photon Science and Synchrotron Radiation, Karlsruhe Institute of Technology (KIT), Hermann-v.-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany); Universität Würzburg, Experimentelle Physik VII, Am Hubland, 97074 Würzburg (Germany); Gemeinschaftslabor für Nanoanalytik, Karlsruhe Institute of Technology (KIT), 76021 Karlsruhe (Germany); Blum, M. [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States) [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States); Advanced Light Source, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720 (United States); Meyer, F. [Universität Würzburg, Experimentelle Physik VII, Am Hubland, 97074 Würzburg (Germany)] [Universität Würzburg, Experimentelle Physik VII, Am Hubland, 97074 Würzburg (Germany); Wilks, R. G. [Solar Energy Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Hahn-Meitner-Platz 1, 14109 Berlin (Germany)] [Solar Energy Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Hahn-Meitner-Platz 1, 14109 Berlin (Germany); Yang, W. [Advanced Light Source, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720 (United States)] [Advanced Light Source, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720 (United States); Bär, M. [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States) [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States); Solar Energy Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Hahn-Meitner-Platz 1, 14109 Berlin (Germany); Insitut für Physik und Chemie, Brandenburgische Technische Universität Cottbus-Senftenberg, Konrad-Wachsmann-Allee 1, 03046 Cottbus (Germany); and others

2014-01-15T23:59:59.000Z

48

In situ diagnostic of liquid water distribution in cathode catalyst layer in an operating PEMFC by high-resolution soft X-ray radiography  

Science Journals Connector (OSTI)

To investigate the water transport behavior in the cathode catalyst layer (CCL) of an operating proton exchange membrane fuel cell (PEMFC), we examined transversal liquid water distributions in the CCL by using high-resolution soft X-ray radiography. The liquid water concentration gradient across the CCL was observed at a spatial resolution of 1.5 ?m. More liquid water accumulated in the CCL at the gas diffusion layer side than at the polymer electrolyte membrane side. The effect of accumulated liquid water in the CCL on the charge-transfer resistance was confirmed by electrochemical impedance spectroscopy. Liquid water accumulation in the CCL corresponds to deterioration of charge-transfer in the electrode.

Phengxay Deevanhxay; Takashi Sasabe; Shohji Tsushima; Shuichiro Hirai

2012-01-01T23:59:59.000Z

49

Reduced graphene oxide based silver sulfide hybrid films formed at a liquid/liquid interface  

SciTech Connect (OSTI)

Free-standing, ultra-thin films of silver sulfide and reduced graphene oxide (RGO) based silver sulfide hybrids are prepared at a liquid/liquid interface employing in situ chemical reaction strategy. Ag{sub 2}S and RGO?Ag{sub 2}S hybrid films are characterized by various techniques such as UV-visible and photo luminescence spectroscopy, X-ray diffraction and scanning electron microscopy. The morphology of hybrid films consists of Ag{sub 2}S nanocrystals on RGO surface while Ag{sub 2}S films contains branched network of dendritic structures. RGO?Ag{sub 2}S exhibit interesting optical and electrical properties. The hybrid films absorb in the region 500–650 nm and show emission in the red region. A higher conductance is observed for the hybrid films arising from the RGO component. This simple low cost method can be extended to prepare other RGO based metal sulfides.

Bramhaiah, K., E-mail: jsneena@csmr.res.in; John, Neena S., E-mail: jsneena@csmr.res.in [Centre for Soft Matter Research, P.B. No.1329, Jalahalli, Bangalore-560013 (India)

2014-04-24T23:59:59.000Z

50

Growth sequence and interface formation in the Fe/MgO/Fe(001) tunnel junction analyzed by surface x-ray diffraction  

SciTech Connect (OSTI)

We present a surface x-ray diffraction study of the interface geometric structure in the Fe/MgO/Fe(001) magnetic tunnel junction (MTJ). While the lower MgO/Fe(001) interface is characterized by a substoichiometric FeO{sub x} (x=0.6{+-}0.1) layer in agreement with previous studies, growth of Fe on the MgO spacer and the upper Fe/MgO interface structure strongly depends on the preparation method. If 0.4 monolayers of Fe are initially deposited in ambient oxygen atmosphere (p=10{sup -7} mbar) followed by Fe deposition under ultrahigh-vacuum (UHV) conditions, structural coherence across the trilayer junction is observed. In this case, substoichiometric FeO{sub x} layers are present at both Fe/MgO interfaces corresponding to a symmetric MTJ structure. In contrast, lattice registry is not preserved if Fe deposition is carried out solely under UHV conditions. Our results might have important implications for the preparation of magnetic tunnel junctions optimized to achieve giant tunneling-magnetoresistance amplitudes.

Tusche, C.; Meyerheim, H. L.; Kirschner, J. [Max-Planck-Institut fuer Mikrostrukturphysik, Weinberg 2, D-06120 Halle (Germany); Jedrecy, N. [Institut des NanoSciences de Paris, Universites Paris 6 et 7 et CNRS-UMR 7588, 4 place Jussieu, F-75252 Paris Cedex 05 (France); Renaud, G. [CEA-Grenoble, 17 rue des Martyrs, F-38054 Grenoble (France)

2006-11-15T23:59:59.000Z

51

Ionic Liquid-Enhanced Solid State Electrolyte Interface (SEI...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Liquid-Enhanced Solid State Electrolyte Interface (SEI) for Lithium Sulfur Batteries. Ionic Liquid-Enhanced Solid State Electrolyte Interface (SEI) for Lithium Sulfur Batteries....

52

Hard x-ray photoelectron spectroscopy study on band alignment at poly(3,4-ethylenedioxythiophene):poly(styrenesulfonate)/ZnO interface  

SciTech Connect (OSTI)

We used hard x-ray photoelectron spectroscopy to investigate the interfacial electronic states of a poly(styrenesulfonate) doped poly(3,4-ethylenedioxythiophene) (PEDOT:PSS) contact on a ZnO single crystal. An understanding of the interfacial band structure is useful for putting the organic contact to practical use. We observed upward band bending of the ZnO layer a few nanometers from the interface. The detected ZnO bulk region exhibited a flat band structure, meaning that the PEDOT:PSS does not greatly deplete the ZnO layer. The band bending caused the charge injection barrier formation with the result that the contact exhibited the Schottky property.

Nagata, T.; Hayakawa, R.; Chikyow, T. [International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba 305-0044 (Japan); Oh, S.; Wakayama, Y. [International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba 305-0044 (Japan); Department of Chemistry and Biochemistry, Faculty of Engineering, Kyushu University, 1-1 Namiki, Tsukuba 305-0044 (Japan); Yamashita, Y. [International Center for Materials Nanoarchitectonics, National Institute for Materials Science, 1-1 Namiki, Tsukuba 305-0044 (Japan); NIMS Beamline Station at SPring-8, National Institute for Materials Science, 1-1-1 Koto, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan); Yoshikawa, H.; Kobayashi, K. [NIMS Beamline Station at SPring-8, National Institute for Materials Science, 1-1-1 Koto, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan)

2012-10-22T23:59:59.000Z

53

Quantitative studies on inner interfaces in conical metal joints using hard x-ray inline phase contrast radiography  

SciTech Connect (OSTI)

Quantitative investigation of micrometer and submicrometer gaps between joining metal surfaces is applied to conical plug-socket connections in dental titanium implants. Microgaps of widths well beyond the resolving power of industrial x-ray systems are imaged by synchrotron phase contrast radiography. Furthermore, by using an analytical model for the relatively simple sample geometry and applying it to numerical forward simulations of the optical Fresnel propagation, we show that quantitative measurements of the microgap width down to 0.1 {mu}m are possible. Image data recorded at the BAMline (BESSY-II light source, Germany) are presented, with the resolving power of the imaging system being 4 {mu}m in absorption mode and {approx}14 {mu}m in phase contrast mode (z{sub 2}=0.74 m). Thus, phase contrast radiography, combined with numerical forward simulations, is capable of measuring the widths of gaps that are two orders of magnitude thinner than the conventional detection limit.

Zabler, S. [Institute for Materials Science, Technical University of Berlin, EB 13, Strasse des 17, Juni 135, D-10623 Berlin (Germany); Rack, T.; Nelson, K. [Clinic for Oral and Maxifacial Surgery, Charite University Medicine, Augustenburger Platz 1, D-13353 Berlin (Germany); Rack, A. [European Synchrotron Radiation Facility, 6 rue Jules Horowitz, BP 220, F-38043 Grenoble (France)

2010-10-15T23:59:59.000Z

54

X-ray photoelectron spectroscopy and ultraviolet photoelectron spectroscopy investigation of Al-related dipole at the HfO{sub 2}/Si interface  

SciTech Connect (OSTI)

The presence of an ultrathin oxide layer at the high-k/SiO{sub 2} interface may result in an interfacial dipole related to the specific high-k dielectric used for the gate stacks. 1 nm HfO{sub 2}/x nmAl{sub 2}O{sub 3}/SiO{sub 2}/Si stacks with different x values (x=0, 0.4, 0.8, 1.2) have been prepared by atomic layer deposition. Using photoelectron spectroscopy, an Al-related interfacial dipole in the HfO{sub 2}/Al{sub 2}O{sub 3}/SiO{sub 2} gate stack has been identified. X-ray photoelectron spectroscopy analysis shows that the dipole is correlated with the formation of an interfacial Al-silicate. The dipole is located at the Al-silicate interface between Al{sub 2}O{sub 3} and SiO{sub 2}, and its strength increases with the increase in Al{sub 2}O{sub 3} thickness because of Al silicate growth. Such Al-related interfacial dipole should have potential applications in future positive metal-oxide-semiconductor devices.

Zhu, L. Q.; Barrett, N.; Jegou, P. [Groupe Photoemission, CEA/IRAMIS/SPCSI, F-91191 Gif-sur-Yvette (France); Martin, F.; Leroux, C.; Martinez, E.; Grampeix, H.; Renault, O.; Chabli, A. [CEA-LETI, MINATEC, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France)

2009-01-15T23:59:59.000Z

55

X-ray Method Shows How Frog Embryos Could Help Thwart Disease  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Nanocrystals Grow from Liquid Interface Nanocrystals Grow from Liquid Interface Eleventh Arthur H. Compton Award Announced Borland Awarded ACFA-IPAC'13 Prize for Accelerator Science President Obama at the Advanced Photon Source Von Dreele Receives Hanawalt Award APS News Archives: 2012 | 2011 | 2010 | 2009 2008 | 2007 | 2006 | 2005 2004 | 2003 | 2002 | 2001 2000 Subscribe to APS News rss feed X-ray Method Shows How Frog Embryos Could Help Thwart Disease MAY 20, 2013 Bookmark and Share X-ray phase-contrast tomography: Early frog embryo in cellular resolution (left) and cell and tissue motion captured and visualized using flow analysis (right). Image: Alexey Ershov/KIT From R&D Magazine online: An international team of scientists using a new X-ray method recorded the internal structure and cell movement inside a living frog embryo in greater

56

A highly modular beamline electrostatic levitation facility, optimized for in situ high-energy x-ray scattering studies of equilibrium and supercooled liquids  

SciTech Connect (OSTI)

High-energy x-ray diffraction studies of metallic liquids provide valuable information about structural evolution on the atomic length scale, leading to insights into the origin of the nucleation barrier and the processes of supercooling and glass formation. The containerless processing of the beamline electrostatic levitation (BESL) facility allows coordinated thermophysical and structural studies of equilibrium and supercooled liquids to be made in a contamination-free, high-vacuum ({approx}10{sup -8} Torr) environment. To date, the incorporation of electrostatic levitation facilities into synchrotron beamlines has been difficult due to the large footprint of the apparatus and the difficulties associated with its transportation and implementation. Here, we describe a modular levitation facility that is optimized for diffraction studies of high-temperature liquids at high-energy synchrotron beamlines. The modular approach used in the apparatus design allows it to be easily transported and quickly setup. Unlike most previous electrostatic levitation facilities, BESL can be operated by a single user instead of a user team.

Mauro, N.A.; Kelton, K.F. (WU)

2011-10-27T23:59:59.000Z

57

Chest x-Rays  

Broader source: Energy.gov [DOE]

The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica.

58

X-ray beamsplitter  

DOE Patents [OSTI]

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5--50 pairs of alternate Mo/Si layers with a period of 20--250 A. The support membrane is 10--200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window. 6 figs.

Ceglio, N.M.; Stearns, D.G.; Hawryluk, A.M.; Barbee, T.W. Jr.

1987-08-07T23:59:59.000Z

59

X-ray beamsplitter  

DOE Patents [OSTI]

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

Ceglio, Natale M. (Livermore, CA); Stearns, Daniel S. (Mountain View, CA); Hawryluk, Andrew M. (Modesto, CA); Barbee, Jr., Troy W. (Palo Alto, CA)

1989-01-01T23:59:59.000Z

60

X-ray binaries  

E-Print Network [OSTI]

We review the nuclear astrophysics aspects of accreting neutron stars in X-ray binaries. We summarize open astrophysical questions in light of recent observations and their relation to the underlying nuclear physics. Recent progress in the understanding of the nuclear physics, especially of X-ray bursts, is also discussed.

H. Schatz; K. E. Rehm

2006-08-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

Novel Application of X-ray Computed Tomography:? Determination of Gas/Liquid Contact Area and Liquid Holdup in Structured Packing  

Science Journals Connector (OSTI)

Figure 7 Flow system used with GE X-ray CT scanner:? from left, air?water column, water pump, and cart containing flow meters. ... In Figure 24, the results of experimental holdup measurements on the column used for imaging are compared with SRP data from the hydraulic testing of Mellapak 250Y. ... The two-fluid model proved powerful in the prediction of the column hydraulics under various operational conditions such as atm. ...

Christian W. Green; John Farone; Julie K. Briley; R. Bruce Eldridge; Richard A. Ketcham; Ben Nightingale

2007-07-24T23:59:59.000Z

62

X-ray laser  

DOE Patents [OSTI]

An X-ray laser (10) that lases between the K edges of carbon and oxygen, i.e. between 44 and 23 Angstroms, is provided. The laser comprises a silicon (12) and dysprosium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state nickel-like dysprosium ions (34) are resonantly photo-pumped to their upper X-ray laser state by line emission from hydrogen-like silicon ions (32). The novel X-ray laser should prove especially useful for the microscopy of biological specimens.

Nilsen, Joseph (Livermore, CA)

1991-01-01T23:59:59.000Z

63

Interface for liquid chromatograph-mass spectrometer  

DOE Patents [OSTI]

A moving belt interface for real-time, high-performance liquid chromatograph (HPLC)/mass spectrometer (MS) analysis which strips away the HPLC solvent as it emerges from the end of the HPLC column and leaves a residue suitable for mass-spectral analysis. The interface includes a portable, stand-alone apparatus having a plural stage vacuum station, a continuous ribbon or belt, a drive train magnetically coupled to an external drive motor, a calibrated HPLC delivery system, a heated probe tip and means located adjacent the probe tip for direct ionization of the residue on the belt. The interface is also capable of being readily adapted to fit any mass spectrometer.

Andresen, Brian D. (Pleasanton, CA); Fought, Eric R. (Livermore, CA)

1989-01-01T23:59:59.000Z

64

Interface for liquid chromatograph-mass spectrometer  

DOE Patents [OSTI]

A moving belt interface is described for real-time, high-performance liquid chromatograph (HPLC)/mass spectrometer (MS) analysis which strips away the HPLC solvent as it emerges from the end of the HPLC column and leaves a residue suitable for mass-spectral analysis. The interface includes a portable, stand-alone apparatus having a plural stage vacuum station, a continuous ribbon or belt, a drive train magnetically coupled to an external drive motor, a calibrated HPLC delivery system, a heated probe tip and means located adjacent the probe tip for direct ionization of the residue on the belt. The interface is also capable of being readily adapted to fit any mass spectrometer. 8 figs.

Andresen, B.D.; Fought, E.R.

1989-09-19T23:59:59.000Z

65

X-ray absorption spectroscopy  

E-Print Network [OSTI]

009-9473-8 REVIEW X-ray absorption spectroscopy Junko Yano Æand application of X-ray absorption spectroscopy, bothX-ray absorption near-edge structure (XANES) and extended X-

Yano, Junko; Yachandra, Vittal K.

2009-01-01T23:59:59.000Z

66

X-ray Absorption Spectroscopy  

E-Print Network [OSTI]

type: Review X-ray Absorption Spectroscopy Junko Yano andPhotosystem II; XAS, X-ray absorption spectroscopy; EXAFS,X-ray absorption fine structure; EPR, electron paramagnetic

Yano, Junko

2010-01-01T23:59:59.000Z

67

X-Ray Generators  

Science Journals Connector (OSTI)

There are many types of X-ray generators sold commercially. The following are some of ... that should be considered when selecting a particular generator for a particular purpose. All the companies listed below s...

Reuben Rudman

1972-01-01T23:59:59.000Z

68

X-ray Diffraction Laboratory: Department of Chemistry Texas A & M University  

E-Print Network [OSTI]

X-ray Diffraction Laboratory: Department of Chemistry Texas A & M University Doc. No: SOPUSERFD form that can be accessed by the X-ray diffraction webpage. RESPONSIBILITY: The X-ray Diffraction and suggestions in a timely manner. MATERIALS: · Computer Database · Web interface #12;X-ray Diffraction

Meagher, Mary

69

X-ray beam finder  

DOE Patents [OSTI]

An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

Gilbert, H.W.

1983-06-16T23:59:59.000Z

70

Argonne CNM: X-Ray Microscopy Capabilities  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Microscopy Facilities X-Ray Microscopy Facilities The Hard X-Ray Nanoprobe (HXN) facility provides scanning fluorescence, scanning diffraction, and full-field transmission and tomographic imaging capabilities with a spatial resolution of 30 nm over a spectral range of 6-12 keV. Modes of Operation Full-Field Transmission Imaging and Nanotomography X-ray transmission imaging uses both the absorption and phase shift of the X-ray beam by the sample as contrast mechanisms. Absorption contrast is used to map the sample density. Elemental constituents can be located by using differential edge contrast in this mode. Phase contrast can be highly sensitive to edges and interfaces even when the X-ray absorption is weak. These contrast mechanisms are exploited to image samples rapidly in full-field transmission mode under various environmental conditions, or combined with nanotomography methods to study the three-dimensional structure of complex and amorphous nanomaterials with the HXN.

71

X-ray Spectrometry  

Science Journals Connector (OSTI)

These provide excellent energy resolution for a wide range of X-ray energies, from the optical range up to several kiloelectronvolts. ... The Astro-E2 launched in 2005 was the first mission that contained a low-temperature microcalorimeter-based observatory, and three more low-temperature detector-based observatories are being developed (NeXT, Constellation-X, ZEUS). ...

Imre Szalóki; János Osán; René E. Van Grieken

2006-05-10T23:59:59.000Z

72

Solid and liquid spectroscopic analysis (SALSA) - A soft x-ray spectroscopy end station with a novel flow-through liquid cell  

E-Print Network [OSTI]

ultra-high vacuum (UHV), which seems to be incompatible withof the liquid cell into UHV like any other (dry) solidintegrated into a standard UHV sample manipulator with XYZ-

Blum, M.

2010-01-01T23:59:59.000Z

73

Synchrotron x-ray reflectivity study of oxidation/passivation of copper and silicon.  

SciTech Connect (OSTI)

Synchrotron x-ray-scattering technique studies of copper and silicon electrochemical interfaces are reported. These two examples illustrate the application of synchrotron x-ray techniques for oxidation, passivation, and dissolution of metals and semiconductors.

Chu, Y.; Nagy, Z.; Parkhutik, V.; You, H.

1999-07-21T23:59:59.000Z

74

APS 7-BM Beamline: X-Ray Resources  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Useful Websites Useful Websites X-Ray Interactions with Matter from CRXO at LBNL. Intuitive interface for x-ray transmission and reflectivity for a wide range of materials. X-Ray Data Booklet from LBNL. Slightly outdated in places, but many useful tables of edge energies, fluorescence lines, and crystal lattice spacings. NIST XCOM Database. Powerful database of photoelectric absorption, elastic scattering, and Compton scattering cross-sections for a wide range of materials. X-Ray Server. Maintained by Sergey Stepanov at GMCA at the APS, this website has several powerful calculators for simulating x-ray reflection and diffraction. Software X-Ray Oriented Programs (XOP). This program, written by scientists at the ESRF and APS, is widely used in the synchrotron research community.

75

Beyond hard x-ray photoelectron spectroscopy: Simultaneous combination with x-ray diffraction  

SciTech Connect (OSTI)

Hard x-ray photoelectron spectroscopy (HAXPES) is a powerful and novel emerging technique for the nondestructive determination of electronic properties and chemical composition of bulk, buried interfaces and surfaces. It benefits from the exceptionally large escape depth of high kinetic energy photoelectrons, increasing the information depth up to several tens of nanometers. Complementing HAXPES with an atomic structure sensitive technique (such as x-ray diffraction) opens a new research field with major applications for materials science. At SpLine, the Spanish CRG beamline at the European Synchrotron Radiation Facility, we have developed a novel experimental set-up that combines HAXPES and x-ray diffraction (x-ray reflectivity, surface x-ray diffraction, grazing incidence x-ray diffraction, and reciprocal space maps). Both techniques can be operated simultaneously on the same sample and using the same excitation source. The set-up includes a robust 2S + 3D diffractometer hosting a ultrahigh vacuum chamber equipped with a unique photoelectron spectrometer (few eV < electron kinetic energy < 15 keV), x-ray tube (Mg/Ti), 15 keV electron gun, and auxiliary standard surface facilities (molecular beam epitaxy evaporator, ion gun, low energy electron diffraction, sample heating/cooling system, leak valves, load-lock sample transfer, etc.). This end-station offers the unique possibility of performing simultaneous HAXPES + x-ray diffraction studies. In the present work, we describe the experimental set-up together with two experimental examples that emphasize its outstanding capabilities: (i) nondestructive characterization of the Si/Ge and HfO{sub 2}/SiO{sub 2} interfaces on Ge-based CMOS devices, and (ii) strain study on La{sub 0.7}Ca{sub 0.3}MnO{sub 3} ultrathin films grown on SrTiO{sub 3}(001) substrate.

Rubio-Zuazo, Juan; Castro, German R. [SpLine, Spanish CRG beamline at the European Synchrotron Radiation Facility, B.P. 220, F-38043 Grenoble (France) and ICMM-CSIC Cantoblanco, E-28049 Madrid (Spain)

2013-05-15T23:59:59.000Z

76

Tunable X-ray source  

DOE Patents [OSTI]

A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

Boyce, James R. (Williamsburg, VA)

2011-02-08T23:59:59.000Z

77

X-ray Pinhole Camera Measurements  

SciTech Connect (OSTI)

The development of the rod pinch diode [1] has led to high-resolution radiography for dynamic events such as explosive tests. Rod pinch diodes use a small diameter anode rod, which extends through the aperture of a cathode plate. Electrons borne off the aperture surface can self-insulate and pinch onto the tip of the rod, creating an intense, small x-ray source (Primary Pinch). This source has been utilized as the main diagnostic on numerous experiments that include high-value, single-shot events. In such applications there is an emphasis on machine reliability, x-ray reproducibility, and x-ray quality [2]. In tests with the baseline rod pinch diode, we have observed that an additional pinch (Secondary Pinch) occurs at the interface near the anode rod and the rod holder. This suggests that stray electrons exist that are not associated with the Primary Pinch. In this paper we present measurements on both pinches using an x-ray pinhole camera. The camera is placed downstream of the Primary Pinch at an angle of 60° with respect to the diode centerline. This diagnostic will be employed to diagnose x-ray reproducibility and quality. In addition, we will investigate the performance of hybrid diodes relating to the formation of the Primary and Secondary Pinches.

Nelson, D. S. [NSTec; Berninger, M. J. [NSTec; Flores, P. A. [NSTec; Good, D. E. [NSTec; Henderson, D. J. [NSTec; Hogge, K. W. [NSTec; Huber, S. R. [NSTec; Lutz, S. S. [NSTec; Mitchell, S. E. [NSTec; Howe, R. A. [NSTec; Mitton, C. V. [NSTec; Molina, I. [NSTec; Bozman, D. R. [SNL; Cordova, S. R. [SNL; Mitchell, D. R. [SNL; Oliver, B. V. [SNL; Ormond, E. C. [SNL

2013-07-01T23:59:59.000Z

78

X-ray Spectrometry  

Science Journals Connector (OSTI)

The segmented STJ operated at total count rates of above 105 counts/s, and the best-achieved energy resolution of their single STJ was found to be 10 eV for X-ray energies below 1 keV. ... The Mo?Au TES, with an operating temperature of 230 mK, was developed for the Constellation-X mission and the energy resolution of the spectrometer is ?28 eV at 3.3 keV. ...

Imre Szalóki; Szabina B. Török; Jasna Injuk; René E. Van Grieken

2002-05-18T23:59:59.000Z

79

In situ x-ray photoelectron spectroscopy for electrochemical reactions in ordinary solvents  

SciTech Connect (OSTI)

In situ electrochemical X-ray photoelectron spectroscopy (XPS) apparatus, which allows XPS at solid/liquid interfaces under potential control, was constructed utilizing a microcell with an ultra-thin Si membrane, which separates vacuum and a solution. Hard X-rays from a synchrotron source penetrate into the Si membrane surface exposed to the solution. Electrons emitted at the Si/solution interface can pass through the membrane and be analyzed by an analyzer placed in vacuum. Its operation was demonstrated for potential-induced Si oxide growth in water. Effect of potential and time on the thickness of Si and Si oxide layers was quantitatively determined at sub-nanometer resolution.

Masuda, Takuya [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan) [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan); PRESTO, Japan Science and Technology Agency (JST), 4-1-8 Honcho, Kawaguchi, Saitama 333-0012 (Japan); Yoshikawa, Hideki; Kobata, Masaaki; Kobayashi, Keisuke [Synchrotron X-ray Station at SPring-8, National Institute for Materials Science (NIMS), Sayo, Hyogo 679-5148 (Japan)] [Synchrotron X-ray Station at SPring-8, National Institute for Materials Science (NIMS), Sayo, Hyogo 679-5148 (Japan); Noguchi, Hidenori [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan) [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan); PRESTO, Japan Science and Technology Agency (JST), 4-1-8 Honcho, Kawaguchi, Saitama 333-0012 (Japan); Graduate School of Chemical Sciences and Engineering, Hokkaido University, Sapporo, Hokkaido 060-0810 (Japan); International Center for Materials Nanoarchitectonics (WPI-MANA), National Institute for Materials Science (NIMS), Tsukuba, Ibaraki 305-0044 (Japan); Kawasaki, Tadahiro [Graduate School of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya 464-8603 (Japan)] [Graduate School of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya 464-8603 (Japan); Uosaki, Kohei [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan) [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan); Graduate School of Chemical Sciences and Engineering, Hokkaido University, Sapporo, Hokkaido 060-0810 (Japan); International Center for Materials Nanoarchitectonics (WPI-MANA), National Institute for Materials Science (NIMS), Tsukuba, Ibaraki 305-0044 (Japan)

2013-09-09T23:59:59.000Z

80

A combined droplet train and ambient pressure photoemission spectrometer for the investigation of liquid/vapor interfaces  

SciTech Connect (OSTI)

We describe a combined ambient pressure photoelectron spectroscopy/droplet train apparatus for investigating the nature and heterogeneous chemistry of liquid/vapor interfaces. In this instrument a liquid droplet train with typical droplet diameters from 50...150 {micro}m is produced by a vibrating orifice aerosol generator (VOAG). The droplets are irradiated by soft X-rays (100...1500 eV) in front of the entrance aperture of a differentially pumped electrostatic lens system that transfers the emitted electrons into a conventional hemispherical electron analyzer. The photoemission experiments are performed at background pressures of up to several Torr, which allows the study of environmentally important liquid/vapor interfaces, in particular aqueous solutions, under equilibrium conditions. The exposure time of the droplet surface to the background gases prior to the XPS measurement can be varied, which will allow future kinetic measurements of gas uptake on liquid surfaces. As an example, a measurement of the surface composition of a {chi} = 0.21 aqueous methanol solution is presented. The concentration of methanol at the vapor/liquid interface is enhanced by a factor of about 3 over the bulk value, while the expected bulk value is recovered at depths larger than about 1.5 nm.

Starr, David E.; Wong, Ed K.; Worsnop, Douglas R.; Wilson, Kevin R.; Bluhm, Hendrik

2008-05-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


81

Investigations of amino acid-based surfactants at liquid interfaces  

E-Print Network [OSTI]

Herein are presented collective studies of amino acid-based surfactants, also known as lipoamino acids, at liquid interfaces. Chapter III describes an investigation of domain morphology of N-Stearoylglutamic acid (N-SGA) Langmuir monolayers...

Yang, Dengliang

2005-11-01T23:59:59.000Z

82

Enzyme Activity and Biomolecule Templating at Liquid and Solid Interfaces  

SciTech Connect (OSTI)

There are two main components of this research program. The first involves studies of the adsorption and catalytic activity of proteins at fluid-fluid and fluid-solid interfaces; the second employs biological macromolecules as templates at the solid-liquid interface for controlled crystallization of inorganic materials, to provide materials with specific functionality.

Harvey W. Blanch

2004-12-01T23:59:59.000Z

83

X-ray Absorption Spectroscopy  

SciTech Connect (OSTI)

This review gives a brief description of the theory and application of X-ray absorption spectroscopy, both X-ray absorption near edge structure (XANES) and extended X-ray absorption fine structure (EXAFS), especially, pertaining to photosynthesis. The advantages and limitations of the methods are discussed. Recent advances in extended EXAFS and polarized EXAFS using oriented membranes and single crystals are explained. Developments in theory in understanding the XANES spectra are described. The application of X-ray absorption spectroscopy to the study of the Mn4Ca cluster in Photosystem II is presented.

Yano, Junko; Yachandra, Vittal K.

2009-07-09T23:59:59.000Z

84

X-ray fluorescence mapping  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

biololgical cells, over the measurement of impurities in solar cells, to the rare earth content of geological materials. A somewhat 'typical' layout for a X-ray fluorescence...

85

Self-Assembly of Microscale Objects at a Liquid/Liquid Interface through Lateral Capillary Forces  

E-Print Network [OSTI]

Self-Assembly of Microscale Objects at a Liquid/Liquid Interface through Lateral Capillary Forces allowed to self-assemble at the perfluorodecalin/water interface. These plates were fabricated from, the designs of hydrophobic edges necessary to generate menisci useful in self-assembly were different for 100

Prentiss, Mara

86

Nanoparticles at liquid interfaces: Rotational dynamics and angular locking  

SciTech Connect (OSTI)

Nanoparticles with different surface morphologies that straddle the interface between two immiscible liquids are studied via molecular dynamics simulations. The methodology employed allows us to compute the interfacial free energy at different angular orientations of the nanoparticle. Due to their atomistic nature, the studied nanoparticles present both microscale and macroscale geometrical features and cannot be accurately modeled as a perfectly smooth body (e.g., spheres and cylinders). Under certain physical conditions, microscale features can produce free energy barriers that are much larger than the thermal energy of the surrounding media. The presence of these energy barriers can effectively “lock” the particle at specific angular orientations with respect to the liquid-liquid interface. This work provides new insights on the rotational dynamics of Brownian particles at liquid interfaces and suggests possible strategies to exploit the effects of microscale features with given geometric characteristics.

Razavi, Sepideh; Kretzschmar, Ilona [Department of Chemical Engineering, City College of City University of New York, New York, New York 10031 (United States)] [Department of Chemical Engineering, City College of City University of New York, New York, New York 10031 (United States); Koplik, Joel [Department of Physics and The Benjamin Levich Institute for Physico-chemical Hydrodynamics, City College of City University of New York, New York, New York 10031 (United States)] [Department of Physics and The Benjamin Levich Institute for Physico-chemical Hydrodynamics, City College of City University of New York, New York, New York 10031 (United States); Colosqui, Carlos E., E-mail: carlos.colosqui@stonybrook.edu [Department of Mechanical Engineering, Stony Brook University, Stony Brook, New York 11794 (United States)

2014-01-07T23:59:59.000Z

87

Reverse Monte Carlo analysis of the local order in liquid Ge{sub 0.15}Te{sub 0.85} alloys combining neutron scattering and x-ray absorption spectroscopy  

SciTech Connect (OSTI)

The structure of liquid Ge{sub 0.15}Te{sub 0.85} alloys that exhibit a density anomaly between 633 K and 733 K at ambient pressure was investigated using x-ray absorption spectroscopy at the Ge K edge. Using a reverse Monte Carlo method to combine the present results with neutron scattering data, we show that the volume contraction is associated with an increase of the first neighbor coordination number around both Ge and Te by about one atom. The coordination number of Ge increases from 3{+-}0.3 to 4.1{+-}0.3. These results support an interpretation of the density anomaly in terms of the same Peierls-like distortion mechanism acting in the liquid state and in the neighboring (pure Te and GeTe compound) phases.

Coulet, Marie-Vanessa; Testemale, Denis; Hazemann, Jean-Louis; Gaspard, Jean-Pierre; Bichara, Christophe [Laboratoire TECSEN, UMR 6122, CNRS-Universite Paul Cezanne, Campus de St Jerome, 13397 Marseille Cedex 20 (France); SNBL/ESRF, 6 rue Jules Horowitz, Boite Postale 220, 38043, Grenoble (France); Laboratoire de Cristallographie, 25 Avenue des Martyrs, Boite Postale 166, 38043 Grenoble (France) and European Synchroton Radiation Facility, 6 rue Jules Horowitz, Boite Postale 220, 38043 Grenoble (France); Physique de la Matiere Condensee, B5, Universite de Liege, B4000 Sart-Tilman (Belgium); Centre de Recherches en Matiere Condensee et Nanosciences-CNRS, Campus de Luminy, Case 913, F13288 Marseille (France)

2005-11-01T23:59:59.000Z

88

X-ray shearing interferometer  

DOE Patents [OSTI]

An x-ray interferometer for analyzing high density plasmas and optically opaque materials includes a point-like x-ray source for providing a broadband x-ray source. The x-rays are directed through a target material and then are reflected by a high-quality ellipsoidally-bent imaging crystal to a diffraction grating disposed at 1.times. magnification. A spherically-bent imaging crystal is employed when the x-rays that are incident on the crystal surface are normal to that surface. The diffraction grating produces multiple beams which interfere with one another to produce an interference pattern which contains information about the target. A detector is disposed at the position of the image of the target produced by the interfering beams.

Koch, Jeffrey A. (Livermore, CA)

2003-07-08T23:59:59.000Z

89

X-Ray Directional Dichroism of a Polar Ferrimagnet  

Science Journals Connector (OSTI)

In a polar ferrimagnet GaFeO3, we have found a novel magneto-optical effect, termed x-ray nonreciprocal directional dichroism (XNDD), that the x-ray absorption at around the K edge of an Fe ion depends on whether the x-ray propagation vector is parallel or antiparallel to the outer product of the magnetization and electric-polarization vectors. The XNDD spectroscopy as demonstrated here can be a useful tool to probe the local magnetism in noncentrosymmetric systems such as magnetic interfaces and nanostructures.

M. Kubota, T. Arima, Y. Kaneko, J. P. He, X. Z. Yu, and Y. Tokura

2004-03-29T23:59:59.000Z

90

Optics for X-Ray Laser and Laser Plasma Soft X-Ray Radiation  

Science Journals Connector (OSTI)

Focusing X-ray grazing incidence optics for X-ray laser and laser plasma soft X-ray radiation has been studied. ... computer code. Parabolic axisymmetric mirror for focusing Princeton X-ray laser beam and ellipso...

L. Pina; A. Inneman; R. Hudec

1996-01-01T23:59:59.000Z

91

Bubble departure in the direct-contact boiling field with a continuous liquid-liquid interface  

SciTech Connect (OSTI)

Behavior of vapor bubbles was experimentally investigated in the boiling field where a volatile liquid layer of per-fluorocarbon PF5050 (boiling point 306K) was directly in contact with an immiscible hot liquid layer of water above it. Heat was supplied to the continuous liquid-liquid interface by the impingement of the downward hot water jet. Vapor bubbles were generated not only from this continuous interface but from a large number of PF5050 droplets floating on it. According to precise observation, incipience of boiling did not occur at the liquid-liquid interface but in the PF5050 liquid close to the interface in both cases of continuous and dispersed interfaces. As a result, the bubbles broke up the thin PF5050 liquid film above them and rose up into the water layer. This bubble departure phenomenon, which does not occur in the ordinary pool boiling field on the solid heating wall, is very important to evaluate the heat transfer performance in the present direct-contact boiling system. For modeling this behavior, sizes of the bubbles were measured at the moment just after they were released into the water pool. Volumes of the bubbles were larger in the case of departing from the continuous liquid-liquid interface than from the droplets. This tendency could be explained by taking into account the buoyancy force acting on unit area of the thin PF5050 liquid film above the bubble before departure, which was one of the most important parameters for the liquid film breakdown. (author)

Kadoguchi, Katsuhiko [Energy Technology Research Institute, National Institute of Advanced Industrial Science and Technology (AIST), 16-1 Onogawa, Tsukuba, Ibaraki 305-8569 (Japan)

2007-01-15T23:59:59.000Z

92

SMB, X-Ray Spectroscopy & Imaging  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Home X-Ray Spectroscopy & Imaging X-Ray Spectroscopy & Imaging SSRL has five hard X-ray Spectroscopy beamlines and three Microfocus Imaging beamlines dedicated to Biological and...

93

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has...

94

X-ray Imaging Workshop  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Imaging and Spectro-microscopy: Imaging and Spectro-microscopy: the Present and the Future Stanford Synchrotron Radiation Laboratory October 8-9, 2002 Organizers: John Miao & Keith Hodgson A workshop on "X-ray Imaging and Spectro-microscopy: the Present and the Future" was held on October 8-9, 2002. This workshop, organized by John Miao (SSRL) and Keith Hodgson (SSRL) provided a forum to discuss the scientific applications of a variety of imaging and spectro-microscopic techniques, including photoemission electron microscopy (PEEM), angle resolved photoemission spectroscopy (ARPES), coherent diffraction imaging, x-ray microscopy, micro-tomography, holographic imaging, and x-ray micro-probe. Twelve invited speakers discussed the important scientific applications of these techniques, and also predicted the future scientific directions with the advance of instrumentation and x-ray sources. The workshop was well attended with over fifty registered attendees.

95

Miniature x-ray source  

DOE Patents [OSTI]

A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

Trebes, James E. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA)

2000-01-01T23:59:59.000Z

96

Center for X-Ray Optics, 1992  

SciTech Connect (OSTI)

This report discusses the following topics: Center for X-Ray Optics; Soft X-Ray Imaging wit Zone Plate Lenses; Biological X-Ray microscopy; Extreme Ultraviolet Lithography for Nanoelectronic Pattern Transfer; Multilayer Reflective Optics; EUV/Soft X-ray Reflectometer; Photoemission Microscopy with Reflective Optics; Spectroscopy with Soft X-Rays; Hard X-Ray Microprobe; Coronary Angiography; and Atomic Scattering Factors.

Not Available

1993-08-01T23:59:59.000Z

97

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking  

E-Print Network [OSTI]

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking Tom Aldcroft SAO/CXC #12;X-ray Stacking 2008 analysis for a sample Stacking ­ mean properties of sample Chandra X-ray data (faint point sources) are photon-limited with low background => stacking in X-rays is very effective #12;X-ray Stacking 2008-Apr-22

Wolfe, Patrick J.

98

Center for X-Ray Optics, 1991  

SciTech Connect (OSTI)

This report discusses: Soft-X-Ray imaging with zone-plate lenses; multilayer reflective optics; and spectroscopy with x-rays.

Not Available

1992-03-01T23:59:59.000Z

99

SMB, X-ray Absorption Spectroscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Absorption Spectroscopy X-ray Absorption Spectroscopy X-ray absorption spectroscopy (XAS) is a well-established technique for simultaneous local geometric and electronic structure...

100

Tokamak x ray diagnostic instrumentation  

SciTech Connect (OSTI)

Three classes of x-ray diagnostic instruments enable measurement of a variety of tokamak physics parameters from different features of the x-ray emission spectrum. (1) The soft x-ray (1 to 50 keV) pulse-height-analysis (PHA) diagnostic measures impurity concentrations from characteristic line intensities and the continuum enhancement, and measures the electron temperature from the continuum slope. (2) The Bragg x-ray crystal spectrometer (XCS) measures the ion temperature and neutral-beam-induced toroidal rotation velocity from the Doppler broadening and wavelength shift, respectively, of spectral lines of medium-Z impurity ions. Impurity charge state distributions, precise wavelengths, and inner-shell excitation and recombination rates can also be studied. X rays are diffracted and focused by a bent crystal onto a position-sensitive detector. The spectral resolving power E/..delta..E is greater than 10/sup 4/ and time resolution is 10 ms. (3) The x-ray imaging system (XIS) measures the spatial structure of rapid fluctuations (0.1 to 100 kHZ) providing information on MHD phenomena, impurity transport rates, toroidal rotation velocity, plasma position, and the electron temperature profile. It uses an array of silicon surface-barrier diodes which view different chords of the plasma through a common slot aperture and operate in current (as opposed to counting) mode. The effectiveness of shields to protect detectors from fusion-neutron radiation effects has been studied both theoretically and experimentally.

Hill, K.W.; Beiersdorfer, P.; Bitter, M.; Fredrickson, E.; Von Goeler, S.; Hsuan, H.; Johnson, L.C.; Liew, S.L.; McGuire, K.; Pare, V.

1987-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

LIQUID AIR INTERFACE CORROSION TESTING FOR FY2010  

SciTech Connect (OSTI)

An experimental study was undertaken to investigate the corrosivity to carbon steel of the liquid-air interface of dilute simulated radioactive waste solutions. Open-circuit potentials were measured on ASTM A537 carbon steel specimens located slightly above, at, and below the liquid-air interface of simulated waste solutions. The 0.12-inch-diameter specimens used in the study were sized to respond to the assumed distinctive chemical environment of the liquid-air interface, where localized corrosion in poorly inhibited solutions may frequently be observed. The practical inhibition of such localized corrosion in liquid radioactive waste storage tanks is based on empirical testing and a model of a liquid-air interface environment that is made more corrosive than the underlying bulk liquid due to chemical changes brought about by absorbed atmospheric carbon dioxide. The chemical changes were assumed to create a more corrosive open-circuit potential in carbon in contact with the liquid-air interface. Arrays of 4 small specimens spaced about 0.3 in. apart were partially immersed so that one specimen contacted the top of the meniscus of the test solution. Two specimens contacted the bulk liquid below the meniscus and one specimen was positioned in the vapor space above the meniscus. Measurements were carried out for up to 16 hours to ensure steady-state had been obtained. The results showed that there was no significant difference in open-circuit potentials between the meniscus-contact specimens and the bulk-liquid-contact specimens. With the measurement technique employed, no difference was detected between the electrochemical conditions of the meniscus versus the bulk liquid. Stable open-circuit potentials were measured on the specimen located in the vapor space above the meniscus, showing that there existed an electrochemical connection through a thin film of solution extending up from the meniscus. This observation supports the Hobbs-Wallace model of the development of the pitting susceptibility of carbon steel in alkaline solutions.

Zapp, P.

2010-12-16T23:59:59.000Z

102

High performance x-ray anti-scatter grid  

DOE Patents [OSTI]

Disclosed are an x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury. 4 Figs.

Logan, C.M.

1995-05-23T23:59:59.000Z

103

E-Print Network 3.0 - air-liquid interface cell Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

film's air-liquid interface has a significant effect on the lung's mechanical... , is the surface tension and is the mean curvature of the air-liquid interface. For the uni-...

104

E-Print Network 3.0 - aux interfaces liquide Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

film's air-liquid interface has a significant effect on the lung's mechanical... , is the surface tension and is the mean curvature of the air-liquid interface. For the uni-...

105

X-ray Emission from Massive Stars  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore be related to the production of X-rays on massive stars. If so, massive stars' X-rays are much different than those found our own Sun and other cooler stars like the Sun that produce X-rays via magnetic activity

Cohen, David

106

X-ray Emission from Massive Stars  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore #12;What is the mechanism by which massive stars produce x-rays? New results from the Chandra X-ray Observatory ­ high-resolution x-ray spectroscopy: measuring Doppler broadening in emission lines Testing

Cohen, David

107

Final Report: Thermal Conductance of Solid-Liquid Interfaces  

SciTech Connect (OSTI)

Research supported by this grant has significantly advanced fundamental understanding of the thermal conductance of solid-liquid interfaces, and the thermal conductivity of nanofluids and nanoscale composite materials. • The thermal conductance of interfaces between carbon nanotubes and a surrounding matrix of organic molecules is exceptionally small and this small value of the interface conductance limits the enhancement in thermal conductivity that can be achieved by loading a fluid or a polymer with nanotubes. • The thermal conductance of interfaces between metal nanoparticles coated with hydrophilic surfactants and water is relatively high and surprisingly independent of the details of the chemical structure of the surfactant. • We extended our experimental methods to enable studies of planar interfaces between surfactant-coated metals and water where the chemical functionalization can be varied between strongly hydrophobic and strongly hydrophilic. The thermal conductance of hydrophobic interfaces establishes an upper-limit of 0.25 nm on the thickness of the vapor-layer that is often proposed to exist at hydrophobic interfaces. • Our high-precision measurements of fluid suspensions show that the thermal conductivity of fluids is not significantly enhanced by loading with a small volume fraction of spherical nanoparticles. These experimental results directly contradict some of the anomalous results in the recent literature and also rule-out proposed mechanisms for the enhanced thermal conductivity of nanofluids that are based on modification of the fluid thermal conductivity by the coupling of fluid motion and the Brownian motion of the nanoparticles.

Cahil, David, G.; Braun, Paul, V.

2006-05-31T23:59:59.000Z

108

Combined sampler robot and high-performance liquid chromatography: a fully automated system for biological small-angle X-ray scattering experiments at the Synchrotron SOLEIL SWING beamline  

Science Journals Connector (OSTI)

A prototype was developed to perform online purification and automatic loading of protein solutions at a small-angle X-ray scattering beamline.

David, G.

2009-09-08T23:59:59.000Z

109

Cooling for a rotating anode X-ray tube  

DOE Patents [OSTI]

A method and apparatus for cooling a rotating anode X-ray tube. An electromagnetic motor is provided to rotate an X-ray anode with cooling passages in the anode. These cooling passages are coupled to a cooling structure located adjacent the electromagnetic motor. A liquid metal fills the passages of the cooling structure and electrical power is provided to the motor to rotate the anode and generate a rotating magnetic field which moves the liquid metal through the cooling passages and cooling structure.

Smither, Robert K. (Hinsdale, IL)

1998-01-01T23:59:59.000Z

110

The Role of Surface X-ray Scattering in Electrocatalysis  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

3 3 N. M. Markovi , LBNL and C. A. Lucas, University of Liverpool Ecological and political realities have moved discussions of, and advances in, fuel cell technology into mainstream public awareness. Electrocatalysis, the science of modifying the overall rates of electrochemical reactions so that selectivity, yield and efficiency are maximized, is the work from which those advances spring. Studies in electrocatalysis have resulted in highly selective multicomponent gas mixture sensors, human blood component sensors, new electrocatalysts for oxidation/reduction of inorganic and organic pollutants in air and water, as well as better electrocatalysts for the fuel cell conversion of renewable and fossil fuels to electrical work. Studies of the mechanisms by which these catalysts operate have been advanced through development of in-situ surface x-ray scattering (SXS) techniques. SXS capabilities at SSRL were recently used to investigate the interface structure of an ultrathin COad (adsorbed carbon monoxide) overlayer on platinum. This work has elevated the macroscopic description of the COad state at the solid-liquid interface to a microscopic level and enabled the relation between the reactivity and the interfacial structure of COad/Pt to be understood.

111

Compact x-ray source and panel  

DOE Patents [OSTI]

A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

Sampayon, Stephen E. (Manteca, CA)

2008-02-12T23:59:59.000Z

112

Ultrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS)  

E-Print Network [OSTI]

: ultrafast x-rays, x-ray absorption spectroscopy, terawatt lasers, ultrafast reaction dynamics, atomic motion atomic motion by scrutinizing the changes in x- ray absorption spectra during reactions. FirstUltrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS) Guangjun

Guo, Ting

113

Focused X-ray source  

DOE Patents [OSTI]

Disclosed is an intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator. 8 figs.

Piestrup, M.A.; Boyers, D.G.; Pincus, C.I.; Maccagno, P.

1990-08-21T23:59:59.000Z

114

Dependence of solid-liquid interface free energy on liquid structure  

SciTech Connect (OSTI)

The Turnbull relation is widely believed to enable prediction of solid–liquid interface (SLI) free energies from measurements of the latent heat and the solid density. Ewing proposed an additional contribution to the SLI free energy to account for variations in liquid structure near the interface. In the present study, molecular dynamics (MD) simulations were performed to investigate whether SLI free energy depends on liquid structure. Analysis of the MD simulation data for 11 fcc metals demonstrated that the Turnbull relation is only a rough approximation for highly ordered liquids, whereas much better agreement is observed with Ewing’s theory. A modification to Ewing’s relation is proposed in this study that was found to provide excellent agreement with MD simulation data.

Wilson, S R [Ames Laboratory; Mendelev, M I [Ames Laboratory

2014-09-01T23:59:59.000Z

115

Microgap x-ray detector  

DOE Patents [OSTI]

An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

Wuest, Craig R. (Danville, CA); Bionta, Richard M. (Livermore, CA); Ables, Elden (Livermore, CA)

1994-01-01T23:59:59.000Z

116

Chest x-Rays | Department of Energy  

Broader source: Energy.gov (indexed) [DOE]

Chest x-Rays Chest x-Rays Chest x-Rays Chest X-ray B-Reading The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica. The B-reading is considered a special reading because doctors who are certified by NIOSH to perform B-readings use a specific protocol to read and record the findings as developed by the International Labour Organization (ILO). The ILO's protocol provides rules for systematically examining the x-ray in a step-by-step method and recording certain abnormalities or changes on the chest x-ray that can be attributable to

117

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs...

118

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities...

119

Producing X-rays at the APS  

ScienceCinema (OSTI)

An introduction and overview of the Advanced Photon Source at Argonne National Laboratory, the technology that produces the brightest X-ray beams in the Western Hemisphere, and the research carried out by scientists using those X-rays.

None

2013-04-19T23:59:59.000Z

120

SMB, X-ray Fluorescence Imaging  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Fluorescence Imaging X-ray Fluorescence Imaging X-ray fluorescence imaging utilizes the high brightness of SPEAR3 and focused beam generated by the uses of K-B optics, capillaries...

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


121

X-Ray Diffraction on NIF  

SciTech Connect (OSTI)

The National Ignition Facility (NIF) is currently a 192 beam, 1.6 MJ laser. NIF Ramp-Compression Experiments have already made the relevant exo-planet pressure range from 1 to 50 Mbar accessible. We Proposed to Study Carbon Phases by X-Ray Diffraction on NIF. Just a few years ago, ultra-high pressure phase diagrams for materials were very 'simple'. New experiments and theories point out surprising and decidedly complex behavior at the highest pressures considered. High pressures phases of aluminum are also predicted to be complex. Recent metadynamics survey of carbon proposed a dynamic pathway among multiple phases. We need to develop diagnostics and techniques to explore this new regime of highly compressed matter science. X-Ray Diffraction - Understand the phase diagram/EOS/strength/texture of materials to 10's of Mbar. Strategy and physics goals: (1) Powder diffraction; (2) Begin with diamond; (3) Continue with metals etc.; (4) Explore phase diagrams; (5) Develop liquid diffraction; and (6) Reduce background/improve resolution.

Eggert, J H; Wark, J

2012-02-15T23:59:59.000Z

122

High intensity line source for x-ray spectrometer calibration  

SciTech Connect (OSTI)

A high intensity electron-impact x-ray source using a one-dimensional Pierce lens has been built for the purpose of calibrating a bent crystal x-ray spectrometer. This source focuses up to 100 mA of 20-keV electrons to a line on a liquid-cooled anode. The line (which can serve as a virtual slit for the spectrometer) measures approximately 800 ..mu.. x 2 cm. The source is portable and therefore adaptable to numerous types of spectrometer applications. One particular application, the calibration of a high resolution (r = 10/sup 4/) time-resolved cyrstal spectrometer, will be discussed in detail.

Thoe, R.S.

1986-06-01T23:59:59.000Z

123

Ethylenediamine at Air/Liquid and Air/Silica Interfaces: Protonation  

E-Print Network [OSTI]

surface and EDA protonated products at air/liquid interfaces. The SFG spectra of EDA adsorbedEthylenediamine at Air/Liquid and Air/Silica Interfaces: Protonation Versus Hydrogen BondingKa (HOSit)) is between the two pKa values of EDA (in the range of 7.56-10.71) at the air/silica interface

124

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St in hot gas about 250 million light years from Earth. (Credit: X-ray: NASA/CXC/SAO/E.Bulbul, et al-Newton has revealed a mysterious X-ray signal in the data. This signal is represented in the circled data

125

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network [OSTI]

2/9/07 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 9, 07] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

126

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St million light years from Earth. (Credit: X-ray: NASA/CXC/Wesleyan Univ./R.Kilgard, et al; Optical: NASA with optical data from the Hubble Space Telescope (red, green, and blue). The X-ray data reveal hundreds

127

X-ray Spectroscopy of Cool Stars  

E-Print Network [OSTI]

High-resolution X-ray spectroscopy has addressed not only various topics in coronal physics of stars, but has also uncovered important features relevant for our understanding of stellar evolution and the stellar environment. I summarize recent progress in coronal X-ray spectroscopy and in particular also discuss new results from studies of X-rays from pre-main sequence stars.

M. Guedel

2006-09-11T23:59:59.000Z

128

X-Ray Physics Evan Berkowitz  

E-Print Network [OSTI]

X-Ray Physics Evan Berkowitz Junior, MIT Department of Physics (Dated: October 25, 2006) We measure a variety of phenomena related to X-Ray absorption and production. We present data which conforms within, as are 22 Na electron-positron annhilation lines. The importance of understanding x-rays is demonstrated

129

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St 200 million light years from Earth. (Credit: X-ray: NASA/CXC/UAH/M.Sun et al; Optical: NASA, ESA, & the Hubble Heritage Team (STScI/AURA) Caption: This composite image from the Chandra X-ray Observatory (blue

130

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network [OSTI]

9/6/09 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 6, 09] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

131

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St. Cambridge, MA 02138 USA http://chandra.harvard.edu Four Supernova Remnants: NASA's Chandra X-ray Observatory's Chandra X-ray Observatory, four newly processed images of supernova remnants dramatically illustrate

132

Soft X-Ray Diffraction Microscopy of a Frozen Hydrated Yeast Cell  

SciTech Connect (OSTI)

We report the first image of an intact, frozen hydrated eukaryotic cell using x-ray diffraction microscopy, or coherent x-ray diffraction imaging. By plunge freezing the specimen in liquid ethane and maintaining it below -170 deg. C, artifacts due to dehydration, ice crystallization, and radiation damage are greatly reduced. In this example, coherent diffraction data using 520 eV x rays were recorded and reconstructed to reveal a budding yeast cell at a resolution better than 25 nm. This demonstration represents an important step towards high resolution imaging of cells in their natural, hydrated state, without limitations imposed by x-ray optics.

Huang Xiaojing; Nelson, Johanna; Lima, Enju; Miao, Huijie; Steinbrener, Jan; Stewart, Andrew; Turner, Joshua J.; Jacobsen, Chris [Department of Physics and Astronomy, Stony Brook University, Stony Brook, New York 11794-3800 (United States); Kirz, Janos [Department of Physics and Astronomy, Stony Brook University, Stony Brook, New York 11794-3800 (United States); Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Marchesini, Stefano; Shapiro, David [Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Neiman, Aaron M. [Department of Biochemistry and Cell Biology, Stony Brook University, Stony Brook, New York 11794-5215 (United States)

2009-11-06T23:59:59.000Z

133

Using Light to Control How X Rays Interact with Matter  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

ultrafast x-ray spectroscopy. ALS femtosecond spectroscopy beamline layout. Femtosecond x-ray and laser pulses derive from a single 800-nm laser oscillator. Femtosecond x rays...

134

Fast microtomography using bright monochromatic x-rays  

SciTech Connect (OSTI)

A fast microtomography system for high-resolution high-speed imaging has been developed using bright monochromatic x-rays at the BL29XU beamline of SPring-8. The shortest scan time for microtomography we attained was 0.25 s in 1.25 {mu}m effective pixel size by combining the bright monochromatic x-rays, a fast rotating sample stage, and a high performance x-ray imaging detector. The feasibility of the tomography system was successfully demonstrated by visualization of rising bubbles in a viscous liquid, an interesting issue in multiphase flow physics. This system also provides a high spatial (a measurable feature size of 300 nm) or a very high temporal (9.8 {mu}s) resolution in radiographs.

Jung, J. W.; Lee, J. S.; Park, S. J.; Chang, S.; Pyo, J. [X-ray Imaging Center, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); Department of Materials Science and Engineering, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); Kwon, N.; Kim, J. [X-ray Imaging Center, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); School of Interdisciplinary Bioscience and Bioengineering, Pohang University of Science and Technology, Pohang 790-784 (Korea, Republic of); Kohmura, Y.; Nishino, Y.; Yamamoto, M.; Ishikawa, T. [RIKEN/SPring-8, 1-1-1 Kouto, Mikazuki-cho, Sayo-gun, Hyogo 679-5148 (Japan); Je, J. H. [X-ray Imaging Center, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); Department of Materials Science and Engineering, Pohang University of Science and Technology, San 31, Hyoja-dong, Pohang 790-784 (Korea, Republic of); School of Interdisciplinary Bioscience and Bioengineering, Pohang University of Science and Technology, Pohang 790-784 (Korea, Republic of); RIKEN/SPring-8, 1-1-1 Kouto, Mikazuki-cho, Sayo-gun, Hyogo 679-5148 (Japan)

2012-09-15T23:59:59.000Z

135

X-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336342  

E-Print Network [OSTI]

X-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336­342 Published online in Wiley InterScience (www.interscience.wiley.com) DOI: 10.1002/xrs.980 Fish otolith trace element maps: new approaches with synchrotron microbeam x-ray of elements as they accrete through a fish's life. We apply synchrotron microbeam x-ray fluorescence methods

Limburg, Karin E.

136

X-ray Pulsations in the Supersoft X-ray Binary CAL 83  

E-Print Network [OSTI]

X-ray data reveal that the supersoft X-ray binary CAL 83 exhibits 38.4 minute pulsations at some epochs. These X-ray variations are similar to those found in some novae and are likely to be caused by nonradial pulsations the white dwarf. This is the first detection of pulsations in a classical supersoft X-ray binary.

P. C. Schmidtke; A. P. Cowley

2005-09-28T23:59:59.000Z

137

The Step Roughening of the Cu(113) Surface: A Grazing Incidence X-Ray Scattering Study  

Science Journals Connector (OSTI)

In conjunction with the development of high brilliance synchrotron sources, the grazing incidence x-ray scattering (GIXS) technique is emerging as an important structural probe for surface and interface studies [...

K. S. Liang; E. B. Sirota; K. L. D’Amico; G. J. Hughes…

1988-01-01T23:59:59.000Z

138

X-ray Spectroscopy of Cooling Cluster  

SciTech Connect (OSTI)

We review the X-ray spectra of the cores of clusters of galaxies. Recent high resolution X-ray spectroscopic observations have demonstrated a severe deficit of emission at the lowest X-ray temperatures as compared to that expected from simple radiative cooling models. The same observations have provided compelling evidence that the gas in the cores is cooling below half the maximum temperature. We review these results, discuss physical models of cooling clusters, and describe the X-ray instrumentation and analysis techniques used to make these observations. We discuss several viable mechanisms designed to cancel or distort the expected process of X-ray cluster cooling.

Peterson, J.R.; /SLAC; Fabian, A.C.; /Cambridge U., Inst. of Astron.

2006-01-17T23:59:59.000Z

139

X-ray transmissive debris shield  

DOE Patents [OSTI]

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, R.B.

1996-05-21T23:59:59.000Z

140

X-ray Spectroscopy of Cooling Clusters  

E-Print Network [OSTI]

We review the X-ray spectra of the cores of clusters of galaxies. Recent high resolution X-ray spectroscopic observations have demonstrated a severe deficit of emission at the lowest X-ray temperatures as compared to that expected from simple radiative cooling models. The same observations have provided compelling evidence that the gas in the cores is cooling below half the maximum temperature. We review these results, discuss physical models of cooling clusters, and describe the X-ray instrumentation and analysis techniques used to make these observations. We discuss several viable mechanisms designed to cancel or distort the expected process of X-ray cluster cooling.

J. R. Peterson; A. C. Fabian

2005-12-21T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

X-ray transmissive debris shield  

DOE Patents [OSTI]

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, Rick B. (Albuquerque, NM)

1996-01-01T23:59:59.000Z

142

Microsoft PowerPoint - S05-05_Zapp_Liquid Air Interface.ppt  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Liquid-Air Interface Corrosion Studies at SRS Liquid-Air Interface Corrosion Studies at SRS EM Waste Processing Technical Exchange 2010 Philip E. Zapp Savannah River National Laboratory November 17, 2010 SRNL-STI-2010-00695 Print Close 2 Liquid-Air Interface Corrosion Studies at SRS SRNL-STI-2010-00695 Introduction Pitting Corrosion in Carbon Steel Waste Tanks Pitting Induced by Dilute Waste Solutions Dilution for feed preparation for vitrification; waste removal Focus: Pitting Susceptibility at Liquid-Air Interface Service Experience Hydroxide Depletion Model Type III tanks under constr. Tank with ventilation & cooling equip. Print Close 3 Liquid-Air Interface Corrosion Studies at SRS SRNL-STI-2010-00695 Background Pitting in carbon steel at and above liquid-air interface in dilute wastes ([Nitrate] < 1 M)

143

X-ray lithography using holographic images  

DOE Patents [OSTI]

A non-contact X-ray projection lithography method for producing a desired X-ray image on a selected surface of an X-ray-sensitive material, such as photoresist material on a wafer, the desired X-ray image having image minimum linewidths as small as 0.063 .mu.m, or even smaller. A hologram and its position are determined that will produce the desired image on the selected surface when the hologram is irradiated with X-rays from a suitably monochromatic X-ray source of a selected wavelength .lambda.. On-axis X-ray transmission through, or off-axis X-ray reflection from, a hologram may be used here, with very different requirements for monochromaticity, flux and brightness of the X-ray source. For reasonable penetration of photoresist materials by X-rays produced by the X-ray source, the wavelength X, is preferably chosen to be no more than 13.5 nm in one embodiment and more preferably is chosen in the range 1-5 nm in the other embodiment. A lower limit on linewidth is set by the linewidth of available microstructure writing devices, such as an electron beam.

Howells, Malcolm R. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1995-01-01T23:59:59.000Z

144

X-ray Observations of Mrk 231  

E-Print Network [OSTI]

This paper presents new X-ray observations of Mrk 231, an active galaxy of particular interest due to its large infrared luminosity and the presence of several blueshifted broad absorption line (BAL) systems, a phenomenon observed in a small fraction of QSOs. A ROSAT HRI image of Mrk 231 is presented, this shows an extended region of soft X-ray emission, covering several tens of kpc, consistent with the extent of the host galaxy. An ASCA observation of Mrk 231 is also presented. Hard X-rays are detected but the data show no significant variability in X-ray flux. The hard X-ray continuum is heavily attenuated and X-ray column estimates range from ~ 2 x 10^{22} - 10^{23} cm^{-2} depending on whether the material is assumed to be neutral or ionized, and on the model assumed for the extended X-ray component. These ASCA data provide only the second hard X-ray spectrum of a BAL AGN presented to date. The broad-band spectral-energy-distribution of the source is discussed. While Mrk 231 is X-ray weak compared to Seyfert 1 galaxies, it has an optical-to-X-ray spectrum typical of a QSO.

T. J. Turner

1998-08-10T23:59:59.000Z

145

X-ray and Neutron Scattering Studies of Methyl Iodide and Hydrogen Confined in Porous Media.  

E-Print Network [OSTI]

??X-ray diffraction was used to study the liquid - solid phase transition and structure of methyl iodide confined in porous GelTech© glass, with 25, 50… (more)

Glanville, Yvonne

2005-01-01T23:59:59.000Z

146

Hard x-ray imaging from explorer  

SciTech Connect (OSTI)

Coded aperture X-ray detectors were applied to obtain large increases in sensitivity as well as angular resolution. A hard X-ray coded aperture detector concept is described which enables very high sensitivity studies persistent hard X-ray sources and gamma ray bursts. Coded aperture imaging is employed so that approx. 2 min source locations can be derived within a 3 deg field of view. Gamma bursts were located initially to within approx. 2 deg and X-ray/hard X-ray spectra and timing, as well as precise locations, derived for possible burst afterglow emission. It is suggested that hard X-ray imaging should be conducted from an Explorer mission where long exposure times are possible.

Grindlay, J.E.; Murray, S.S.

1981-11-01T23:59:59.000Z

147

Development of x-ray photoelectron microscope with an x-ray laser source  

Science Journals Connector (OSTI)

We have constructed an x-ray photoelectron microscopic system with an x-ray laser as an x-ray source. The lasing line is the Li-like Al 3d-4f transition at 15.47 nm where the recombining Al plasma is used as the x-ray laser medium. The beam from the x-ray laser cavity was then focused by using a Schwarzschild mirror coated with Mo/Si multilayers. The x-ray beam size with a diameter less than 0.5 ?m and the estimated photon number of about 2×10 6 ? photons/shot into the spot were achieved.

Tadayuki Ohchi; Naohiro Yamaguchi; Chiemi Fujikawa; Tamio Hara; Katsumi Watanabe; Ibuki Tanaka; Masami Taguchi

2000-01-01T23:59:59.000Z

148

Applications of soft x-ray lasers  

SciTech Connect (OSTI)

The high brightness and short pulse duration of soft x-ray lasers provide unique advantages for novel applications. Imaging of biological specimens using x-ray lasers has been demonstrated by several groups. Other applications to fields such as chemistry, material science, plasma diagnostics, and lithography are beginning to emerge. We review the current status of soft x-ray lasers from the perspective of applications, and present an overview of the applications currently being developed.

Skinner, C.H.

1993-08-01T23:59:59.000Z

149

High speed x-ray beam chopper  

DOE Patents [OSTI]

A fast, economical, and compact x-ray beam chopper with a small mass and a small moment of inertia whose rotation can be synchronized and phase locked to an electronic signal from an x-ray source and be monitored by a light beam is disclosed. X-ray bursts shorter than 2.5 microseconds have been produced with a jitter time of less than 3 ns.

McPherson, Armon (Oswego, IL); Mills, Dennis M. (Naperville, IL)

2002-01-01T23:59:59.000Z

150

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma  

E-Print Network [OSTI]

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma P. L plasmas in which efficient x-ray laser frequency near-doubling is expected for a number of available x-ray of coherent x rays and tunable optical radiation may result in tunable coherent x-ray radiation powerful

Kaplan, Alexander

151

Colloid Coalescence with Focused X Rays  

SciTech Connect (OSTI)

We show direct evidence that focused x rays enable us to merge polymer colloidal particles at room temperature. This phenomenon is ascribed to the photochemical scission of colloids with x rays, reducing the molecular weight, glass transition temperature, surface tension, and viscosity of colloids. The observation of the neck bridge growth with time shows that the x-ray-induced colloid coalescence is analogous to viscoelastic coalescence. This finding suggests a feasible protocol of photonic nanofabrication by sintering or welding of polymers, without thermal damage, using x-ray photonics.

Weon, B. M.; Kim, J. T.; Je, J. H. [X-ray Imaging Center, Department of Materials Science and Engineering, Pohang University of Science and Technology, Pohang, 790-784 (Korea, Republic of); Yi, J. M. [Samsung Advanced Institute of Technology, Yongin, Gyeonggi, 446-712 (Korea, Republic of); Wang, S.; Lee, W.-K. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)

2011-07-01T23:59:59.000Z

152

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE  

E-Print Network [OSTI]

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE USER'S HANDBOOK Version 1.0 (June 1994) prepared by John . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Chapter Two: XRMB History

153

X-ray laser microscope apparatus  

DOE Patents [OSTI]

A microscope consisting of an x-ray contact microscope and an optical microscope. The optical, phase contrast, microscope is used to align a target with respect to a source of soft x-rays. The source of soft x-rays preferably comprises an x-ray laser but could comprise a synchrotron or other pulse source of x-rays. Transparent resist material is used to support the target. The optical microscope is located on the opposite side of the transparent resist material from the target and is employed to align the target with respect to the anticipated soft x-ray laser beam. After alignment with the use of the optical microscope, the target is exposed to the soft x-ray laser beam. The x-ray sensitive transparent resist material whose chemical bonds are altered by the x-ray beam passing through the target mater GOVERNMENT LICENSE RIGHTS This invention was made with government support under Contract No. De-FG02-86ER13609 awarded by the Department of Energy. The Government has certain rights in this invention.

Suckewer, Szymon (Princeton, NJ); DiCicco, Darrell S. (Plainsboro, NJ); Hirschberg, Joseph G. (Coral Gables, FL); Meixler, Lewis D. (East Windsor, NJ); Sathre, Robert (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ)

1990-01-01T23:59:59.000Z

154

Automation in X-Ray Crystallography  

Science Journals Connector (OSTI)

Automation in X-Ray Crystallography ... But in the past few years, automation procedures have been applied to intrinsically superior experimental methods. ...

S.C. ABRAHAMS

1963-06-03T23:59:59.000Z

155

X-Ray Laser Sources for Microscopy  

Science Journals Connector (OSTI)

Progress and prospects in soft X-ray laser development at Princeton are presented. A comparison to plasma and synchrotron sources is made with a...

C. H. Skinner; D. E. Kim; A. Wouters; D. Voorhees; S. Suckewer

1988-01-01T23:59:59.000Z

156

Compound refractive X-ray lens  

DOE Patents [OSTI]

An apparatus and method for focusing X-rays. In one embodiment, his invention is a commercial-grade compound refractive X-ray lens. The commercial-grade compound refractive X-ray lens includes a volume of low-Z material. The volume of low-Z material has a first surface which is adapted to receive X-rays of commercially-applicable power emitted from a commercial-grade X-ray source. The volume of low-Z material also has a second surface from which emerge the X-rays of commercially-applicable power which were received at the first surface. Additionally, the commercial-grade compound refractive X-ray lens includes a plurality of openings which are disposed between the first surface and the second surface. The plurality of openings are oriented such that the X-rays of commercially-applicable power which are received at the first surface, pass through the volume of low-Z material and through the plurality openings. In so doing, the X-rays which emerge from the second surface are refracted to a focal point.

Nygren, David R. (Berkeley, CA); Cahn, Robert (Walnut Creek, CA); Cederstrom, Bjorn (Traellborg, SE); Danielsson, Mats (Stocksund, SE); Vestlund, Jonas (Stockholm, SE)

2000-01-01T23:59:59.000Z

157

X-Ray Science Division (XSD)  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Science Division (XSD) Search Button About Welcome Overview Visiting the APS Mission & Goals Find People Organization Charts Committees Job Openings User Information...

158

THE SWIFT/BAT HARD X-RAY TRANSIENT MONITOR  

SciTech Connect (OSTI)

The Swift/Burst Alert Telescope (BAT) hard X-ray transient monitor provides near real-time coverage of the X-ray sky in the energy range 15-50 keV. The BAT observes 88% of the sky each day with a detection sensitivity of 5.3 mCrab for a full-day observation and a time resolution as fine as 64 s. The three main purposes of the monitor are (1) the discovery of new transient X-ray sources, (2) the detection of outbursts or other changes in the flux of known X-ray sources, and (3) the generation of light curves of more than 900 sources spanning over eight years. The primary interface for the BAT transient monitor is a public Web site. Between 2005 February 12 and 2013 April 30, 245 sources have been detected in the monitor, 146 of them persistent and 99 detected only in outburst. Among these sources, 17 were previously unknown and were discovered in the transient monitor. In this paper, we discuss the methodology and the data processing and filtering for the BAT transient monitor and review its sensitivity and exposure. We provide a summary of the source detections and classify them according to the variability of their light curves. Finally, we review all new BAT monitor discoveries. For the new sources that are previously unpublished, we present basic data analysis and interpretations.

Krimm, H. A.; Holland, S. T.; Corbet, R. H. D.; Pearlman, A. B.; Baumgartner, W. H.; Cummings, J. R. [Center for Research and Exploration in Space Science and Technology (CRESST) and NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Romano, P. [INAF, Istituto di Astrofisica Spaziale e Fisica Cosmica, Via U. La Malfa 153, I-90146 Palermo (Italy); Kennea, J. A. [Department of Astronomy and Astrophysics, Pennsylvania State University, University Park, PA 16802 (United States); Bloom, J. S. [Department of Astronomy, University of California, Berkeley, Berkeley, CA 94720-3411 (United States); Barthelmy, S. D.; Gehrels, N.; Lien, A. Y.; Markwardt, C. B.; Ukwatta, T. N. [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States); Palmer, D. M. [Los Alamos National Laboratory, B244, Los Alamos, NM 87545 (United States); Sakamoto, T. [Department of Physics and Mathematics, College of Science and Engineering, Aoyama Gakuin University, 5-10-1 Fuchinobe, Chuo-ku, Sagamihara-shi, Kanagawa 252-5258 (Japan); Stamatikos, M. [Department of Physics and Center for Cosmology and Astro-Particle Physics, Ohio State University, Columbus, OH 43210 (United States)

2013-11-01T23:59:59.000Z

159

X-ray spectroscopy of neutron star low-mass X-ray binaries  

E-Print Network [OSTI]

In this thesis, I present work spanning a variety of topics relating to neutron star lowmass X-ray binaries (LMXBs) and utilize spectral information from X-ray observations to further our understanding of these sources. ...

Krauss, Miriam Ilana

2007-01-01T23:59:59.000Z

160

Ultraluminous X-ray Sources: The most extreme X-ray binaries  

E-Print Network [OSTI]

1 Ultraluminous X-ray Sources: The most extreme X-ray binaries Luca Zampieri INAF ULXs ­ Lubiana ­ May 11, 2012- LZ #12;6 · X-ray observations of nearby galaxies show a population of pointlike, off-nuclear sources with L >> Ledd for 1 Msun (L>1.0e39 erg/s) UltraLuminous X-ray Sources (e

Â?umer, Slobodan

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

X-ray Diffraction (XRD) 1.0 What is X-ray Diffraction  

E-Print Network [OSTI]

X-ray Diffraction (XRD) · 1.0 What is X-ray Diffraction · 2.0 Basics of Crystallography · 3.0 Production of X-rays · 4.0 Applications of XRD · 5.0 Instrumental Sources of Error · 6.0 Conclusions #12 why the cleavage faces of crystals appear to reflect X-ray beams at certain angles of incidence (theta

Moeck, Peter

162

Aneta Siemiginowska Chandra X-ray Center  

E-Print Network [OSTI]

-ray and gamma-ray · High Energy Sky · Chandra X-ray Observatory · examples of typical X-ray data, · an example of a data analysis process · statistical challenges · what do we learn from the data? #12;What is Astronomy and phenomena do we study and how? Solar System: Sun and sollar wind, planets, moons, asteroids, comets Our

Wolfe, Patrick J.

163

Watershed in X-ray Astronomy  

Science Journals Connector (OSTI)

... extent the article on page 96 of this issue of Nature from the X-ray astronomy group at the Massachusetts Institute of Technology is a record of disappointments. That is ... near the galactic centre. Now that the first satellite to be devoted to X-ray astronomy has been launched, and is apparently working successfully, the MIT article and another from ...

1971-01-08T23:59:59.000Z

164

X-Ray Identification of Element 104  

Science Journals Connector (OSTI)

The daughter x-ray identification technique has been applied to the identification of element 104. The characteristic K-series x rays from the ?-decay daughter isotope, nobelium (Z=102), have been observed in coincidence with ? particles from the decay of 4.5-sec 104257, thus providing an unequivocal determination of the parent atomic number, Z=104.

C. E. Bemis; Jr.; R. J. Silva; D. C. Hensley; O. L. Keller; Jr.; J. R. Tarrant; L. D. Hunt; P. F. Dittner; R. L. Hahn; C. D. Goodman

1973-09-03T23:59:59.000Z

165

Influence of Janus Particle Shape on Their Interfacial Behavior at Liquid–Liquid Interfaces  

Science Journals Connector (OSTI)

(2-4) Over the course of the past few years in particular, Janus particles, named after the double-faced Roman god, have evolved as a very interesting class of very complex internal colloidal structures among micrometer- or nanosized particles(5, 6) and therefore have attracted much attention from both industrial and academic areas due to their potential applications in emulsions,(7, 8) materials engineering,(9, 10) nanoscience,(11) chemical and biological sensors,(12-16) drug delivery, and self-assembly. ... In the following, several theoretical and practical studies have been performed to predict Janus particle behavior at liquid–liquid interfaces after Binks and Fletcher’s calculations of interfacial adsorption capabilities of biphasic Janus spheres predicted an up to 3-fold stronger adsorption as compared to particles of uniform wettability. ...

Thomas M. Ruhland; André H. Gröschel; Nicholas Ballard; Thomas S. Skelhon; Andreas Walther; Axel H. E. Müller; Stefan A. F. Bon

2013-01-12T23:59:59.000Z

166

Quantitative Measurements of X-ray Intensity  

SciTech Connect (OSTI)

This chapter describes the characterization of several X-ray sources and their use in calibrating different types of X-ray cameras at National Security Technologies, LLC (NSTec). The cameras are employed in experimental plasma studies at Lawrence Livermore National Laboratory (LLNL), including the National Ignition Facility (NIF). The sources provide X-rays in the energy range from several hundred eV to 110 keV. The key to this effort is measuring the X-ray beam intensity accurately and traceable to international standards. This is accomplished using photodiodes of several types that are calibrated using radioactive sources and a synchrotron source using methods and materials that are traceable to the U.S. National Institute of Standards and Technology (NIST). The accreditation procedures are described. The chapter begins with an introduction to the fundamental concepts of X-ray physics. The types of X-ray sources that are used for device calibration are described. The next section describes the photodiode types that are used for measuring X-ray intensity: power measuring photodiodes, energy dispersive photodiodes, and cameras comprising photodiodes as pixel elements. Following their description, the methods used to calibrate the primary detectors, the power measuring photodiodes and the energy dispersive photodiodes, as well as the method used to get traceability to international standards are described. The X-ray source beams can then be measured using the primary detectors. The final section then describes the use of the calibrated X-ray beams to calibrate X-ray cameras. Many of the references are web sites that provide databases, explanations of the data and how it was generated, and data calculations for specific cases. Several general reference books related to the major topics are included. Papers expanding some subjects are cited.

Haugh, M. J., Schneider, M.

2011-09-01T23:59:59.000Z

167

Application of X-ray synchrotron microscopy instrumentation in biology  

SciTech Connect (OSTI)

X-ray micro-fluorescence imaging technique has been used as a significant tool in order to investigate minerals contents in some kinds of materials. The aim of this study was to evaluate the elemental distribution of calcium and zinc in bone substitute materials (nano-hydroxyapatite spheres) and cortical bones through X-Ray Micro-fluorescence analysis with the increment of Synchrotron Radiation in order to evaluate the characteristics of the newly formed bone and its interface, the preexisting bone and biomaterials by the arrangement of collagen fibers and its birefringence. The elemental mapping was carried out at Brazilian Synchrotron Light Laboratory, Campinas - Sao Paulo, Brazil working at D09-XRF beam line. Based on this study, the results suggest that hydroxyapatite-based biomaterials are biocompatible, promote osteo-conduction and favored bone repair. (authors)

Gasperini, F. M. [Medical Science Program, Fluminense Federal Univ., Niteroi (Brazil); Pereira, G. R. [Dept. of Metallurgical and Materials Engineering, Federal Univ. of Rio de Janeiro (Brazil); Granjeiro, J. M. [Molecular and Cell Biology Dept., Fluminense Federal Univ., Niteroi, Rio de Janeiro (Brazil); Calasans-Maia, M. D. [Oral Surgery Dept., Fluminense Federal Univ., Niteroi, Rio de Janeiro (Brazil); Rossi, A. M. [Biomaterials Laboratory, Brazilian Center of Physics Research, Rio de Janeiro (Brazil); Perez, C. A. [Brazilian Synchrotron Laboratory, Campinas, Sao Paulo (Brazil); Lopes, R. T.; Lima, I. [Nuclear Engineering Laboratory, Federal Univ. of Rio de Janeiro (Brazil)

2011-07-01T23:59:59.000Z

168

Micro-array collimators for X-rays and neutrons  

SciTech Connect (OSTI)

The authors describe the fabrication techniques of novel, compact optical elements for collimating and/or focusing beams of X-rays or thermal neutrons. These optical elements are solid composite arrays consisting of regular stacks of alternating micro-foils, analogous in action to Soller slit collimators, but up to three orders of magnitude smaller. The arrays are made of alternating metals with suitable refractive indices for reflection and/or absorption of the specific radiation. In one implementation, the arrays are made of stacked micro-foils of transmissive elements (Al, Cu) coated and/or electroplated with absorbing elements (Gd, Cd), which are repeatedly rolled or drawn and restacked to achieve the required collimation parameters. The authors present results of these collimators using both X-rays and neutrons. The performance of the collimating element is limited only by the choice of micro-foil materials and the uniformity of their interfaces.

Cimmino, A.; Allman, B.E.; Klein, A.G. [Univ. of Melbourne, Parkville (Australia). School of Physics; Hamilton, W.A. [Oak Ridge National Lab., TN (United States). Solid State Div.; Anderson, I.S.; Hamelin, B.; Joeghoej, P. [Inst. Laue-Langevin, Grenoble (France); Bastie, P. [Univ. Joseph Fourier-Grenoble, Saint-Martin-d`Heres (France). Lab. de Spectrometrie Physique

1998-08-01T23:59:59.000Z

169

X-ray Practicals Series 1 Advanced Data Reduction  

E-Print Network [OSTI]

X-ray Practicals Series 1 Advanced Data Reduction Instructor J. Reibenspies, Ph. D. Nattamai Bhuvanesh, Ph.D. Version 1.0.0 #12;X-ray Practicals Series 2 #12;X-ray Practicals Series 3 #12;X-ray is good. The y direction is shifting the most, but the shift is ok #12;X-ray Practicals Series 5 Other

Meagher, Mary

170

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

171

X-ray sources in globular clusters  

E-Print Network [OSTI]

The twelve bright (Lx>10(36) erg/s) X-ray sources in the globular clusters have lower luminosities than the brightest sources in the bulge of our galaxy. The dim (Lx<10(35) erg/s) X-ray sources in globular clusters reach higher luminosities than the cataclysmic variables in the disk of our galaxy. The first difference is a statistical fluke, as comparison with M31 indicates. The second difference is explained because the brightest of the dim sources are not cataclysmic variables, but soft X-ray transients in quiescence. This article describes the BeppoSAX, ROSAT and first Chandra observations leading to these conclusions.

Frank Verbunt

2001-11-22T23:59:59.000Z

172

X-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND  

E-Print Network [OSTI]

with the occurrence of solar X-ray flare, when light travel time delay is accounted, suggesting that X-rays fromX-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND ANIL BHARDWAJ Flight center, Greenbelt, MD 20771, USA Scattering of solar X-ray radiation mainly produces the non

Ã?stgaard, Nikolai

173

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art  

E-Print Network [OSTI]

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art diffractometers offering both single crystal and powder X-Ray diffraction. Powder X-Ray Diffraction High resolution data For more details on powder X-Ray analysis contact Dr J Hriljac on 0121 414 4458 or email: j

Birmingham, University of

174

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray Source  

E-Print Network [OSTI]

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray of an intense, tunable, polarized, and quasi-monochromatic X-ray source has been ongoing at Rensselaer Polytechnic Institute since 2001 [1, 2, 3, 4, 5, 6]. This X-ray source, known as Parametric X-rays (PXR

Danon, Yaron

175

Compact X-Ray Light Source Workshop | EMSL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Compact X-Ray Light Source Workshop Compact X-Ray Light Source Workshop Teller R, Terminello L, Thevuthasan T, Moncton D. 2012. "Compact X-Ray Light Source Workshop Report."...

176

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray...

177

E-Print Network 3.0 - air-liquid interface biofilms Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

, B. Purvedorj y , P. Stoodley yz Summary: and the velocity of the ripples at the biofilmbulk liquid interface. wg 5:09 Nm 2 . 21 12; Strain Source... A Viscoelastic Fluid...

178

APS Bending Magnet X-rays and  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Irradiation of Nd-Fe-B Permanent Magnets with Irradiation of Nd-Fe-B Permanent Magnets with APS Bending Magnet X-rays and 60 Co γ-rays J. Alderman and P.K. Job APS Operations Division Advanced Photon Source J. Puhl Ionizing Radiation Division National Institute of Standards and Technology June 2000 Table of Contents Introduction Radiation-Induced Demagnetization of Permanent Magnets Resources Required γ-ray Irradiation Results and Analysis of γ-ray Irradiation X-ray Irradiation Results and Analysis of X-ray Irradiation Summary and Conclusions Acknowledgements References Tables and Figures Introduction The Advanced Photon Source (APS), as well as other third-generation synchrotron light sources, uses permanent magnets in the insertion devices to produce x-rays for scientific

179

X-ray source for mammography  

DOE Patents [OSTI]

An x-ray source utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms.

Logan, Clinton M. (Pleasanton, CA)

1994-01-01T23:59:59.000Z

180

Ultrafast X-Ray Sources and Science  

Science Journals Connector (OSTI)

X-ray science is entering the ultrafast and ultraintense era - spurred by developments in coherent, short-wavelength sources that range from tabletop to accelerator-based. These...

Young, Linda

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

X-ray induced optical reflectivity  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

The change in optical reflectivity induced by intense x-ray pulses can now be used to study ultrafast many body responses in solids in the femtosecond time domain. X-ray absorption creates photoelectrons and core level holes subsequently filled by Auger or fluorescence processes, and these excitations ultimately add conduction and valence band carriers that perturb optical reflectivity.Optical absorption associated with band filling and band gap narrowing is shown to explain the basic features found in recent measurements on an insulator (silicon nitride, Si3N4), a semiconductor(gallium arsenide,GaAs), and a metal (gold,Au), obtained with ?100 fs x-ray pulses at 500-2000 eV and probed with 800 nm laser pulses. In particular GaAs exhibits an abrupt drop in reflectivity, persisting only for a time comparable to the x-ray excitation pulse duration, consistent with prompt band gap narrowing.

Durbin, Stephen M.

2012-01-01T23:59:59.000Z

182

SMB, X-ray Emission Spectroscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Emission Spectroscopy Beam Line 6-2b X-ray Emission Spectroscopy Beam Line 6-2b is an advanced spectroscopy experimental station on the multidisciplinary general user wiggler Beam...

183

X-raying galaxies: A Chandra legacy  

Science Journals Connector (OSTI)

...Astronomy, University of Massachusetts, Amherst, MA 01003 This presentation...stellar x-ray sources in the solar neighborhood (8). The...elements—Meteoritic and solar . Geochim Cosmochim Acta 53...Astronomy, University of Massachusetts, Amherst, MA 01003, USA...

Q. Daniel Wang

2010-01-01T23:59:59.000Z

184

Small Angle X-Ray Scattering Detector  

DOE Patents [OSTI]

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

Hessler, Jan P.

2004-06-15T23:59:59.000Z

185

X-Ray Nanoimaging: Instruments and Methods  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http:spie.orgOP318 August 28-29, 2013; San Diego, California, USA...

186

Femtosecond X-ray protein nanocrystallography  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Femtosecond X-ray protein nanocrystallography Authors: Chapman, H.N., Fromme, P., Barty, A., White, T.A., Kirian, R.A., Aquila, A., Hunter, M.S., Schulz, J., DePonte, D.P.,...

187

X-ray source for mammography  

DOE Patents [OSTI]

An x-ray source is described utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms. 6 figures.

Logan, C.M.

1994-12-20T23:59:59.000Z

188

Probing Ag nanoparticle surface oxidation in contact with (in)organics: an X-ray scattering and fluorescence yield approach  

Science Journals Connector (OSTI)

An advanced characterization approach to spatially resolve the reactions occurring at the interface between silver nanoparticles and a simple aqueous system is presented. Both phase and chemical distributions were obtained from X-ray scattering and fluorescence yield techniques.

Levard, C.

2011-10-06T23:59:59.000Z

189

Using X-Ray Computed Tomography in Pore Structure Characterization...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Using X-Ray Computed Tomography in Pore Structure Characterization for a Berea Sandstone: Resolution Effect. Using X-Ray Computed Tomography in Pore Structure Characterization for...

190

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

191

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

192

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

193

The Constellation X-ray mission  

Science Journals Connector (OSTI)

The Constellation-X mission is a large collecting area X-ray facility, emphasizing observations at high spectral resolution (E/?E?300–3000) while covering a broad energy band (0.25–40 keV). By increasing the telescope aperture and utilizing efficient spectrometers the mission will achieve a factor of 100 increased sensitivity over current high-resolution X-ray spectroscopy missions. The use of focussing optics across the 10–40 keV band will provide a similar factor of 100 increased sensitivity in this band. Key technologies under development for the mission include lightweight high throughput X-ray optics, multilayer coatings to enhance the hard X-ray performance of X-ray optics, micro-calorimeter spectrometer arrays with 2 eV resolution, low-power and low-weight CCD arrays, lightweight gratings and hard X-ray detectors. When observations commence towards the end of the next decade, Constellation-X will address many pressing questions concerning the extremes of gravity and the evolution of the Universe.

N.E White; H Tananbaum

1999-01-01T23:59:59.000Z

194

X-Ray Observations of Radio Galaxies  

E-Print Network [OSTI]

We review some of the ways that X-ray observations provide unique information on radio galaxies. Thermal bremsstrahlung X-ray emission provides detailed data on ambient densities and temperatures. These parameters in turn can be used for pressure balance calculations and can demonstrate how the ambient gas affects radio source structure. Additionally, many signatures of the interaction of radio jets and lobes with the hot gas are found in high resolution X-ray maps. Non-thermal X-ray emission from knots and hotspots of radio jets can give us constraints on the relativistic electron population for energies greater that that normally sampled in the radio (in the case of synchrotron emission) or can give us an independent estimate of the average magnetic field strength (if inverse Compton emission is the origin of the X-rays). From recent ROSAT HRI observations of 3C 390.3 and 3C 120, we show evidence that X-ray emission from knots and hotspots appears to be associated with regions of large gradients in the radio surface brightness; i.e. at the location of powerful shocks.

D. E. Harris

1998-04-20T23:59:59.000Z

195

Compton backscattered collimated x-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

Ruth, R.D.; Huang, Z.

1998-10-20T23:59:59.000Z

196

Compton backscattered collmated X-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

2000-01-01T23:59:59.000Z

197

Compton backscattered collimated x-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

1998-01-01T23:59:59.000Z

198

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

199

Development of x-ray laminography under an x-ray microscopic condition  

SciTech Connect (OSTI)

An x-ray laminography system under an x-ray microscopic condition was developed to obtain a three-dimensional structure of laterally-extended planar objects which were difficult to observe by x-ray tomography. An x-ray laminography technique was introduced to an x-ray transmission microscope with zone plate optics. Three prototype sample holders were evaluated for x-ray imaging laminography. Layered copper grid sheets were imaged as a laminated sample. Diatomite powder on a silicon nitride membrane was measured to confirm the applicability of this method to non-planar micro-specimens placed on the membrane. The three-dimensional information of diatom shells on the membrane was obtained at a spatial resolution of sub-micron. Images of biological cells on the membrane were also obtained by using a Zernike phase contrast technique.

Hoshino, Masato; Uesugi, Kentaro; Takeuchi, Akihisa; Suzuki, Yoshio; Yagi, Naoto [Japan Synchrotron Radiation Research Institute JASRI/SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)

2011-07-15T23:59:59.000Z

200

X-ray views of neutron star low-mass X-ray binaries  

E-Print Network [OSTI]

A neutron star low-mass X-ray binary is a binary stellar system with a neutron star and a low-mass companion star rotating around each other. In this system the neutron star accretes mass from the companion, and as this matter falls into the deep potential well of the neutron star, the gravitational potential energy is released primarily in the X-ray wavelengths. Such a source was first discovered in X-rays in 1962, and this discovery formally gave birth to the "X-ray astronomy". In the subsequent decades, our knowledge of these sources has increased enormously by the observations with several X-ray space missions. Here we give a brief overview of our current understanding of the X-ray observational aspects of these systems.

Sudip Bhattacharyya

2010-02-24T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

Two-dimensional Electron Liquid State at Oxide Interfaces J. Mannhart  

E-Print Network [OSTI]

Two-dimensional Electron Liquid State at Oxide Interfaces J. Mannhart Max Planck InstituteAlO3 #12;LaAlO3 - SrTiO3 YBa2Cu3O7 G. Hammerl #12;Interfaces with Standard Semiconductors: Space Charge;Conductance-voltage characteristics It/ Vs Vs were measured using a standard lock-in technique.24 Simulta

Yeh, Nai-Chang

202

Is linear response to x-rays suitable for digital dental x-ray imaging systems? —Theoretical and experimental considerations  

Science Journals Connector (OSTI)

The purpose of this study was to consider theoretically and experimentally the suitability of linear response to x-rays for digital dental x-ray imaging systems.

Keiichi Nishikawa PhD; Mamoru Wakoh DDS; PhD; Kinya Kuroyanagi DDS; PhD

2003-06-01T23:59:59.000Z

203

A mean field approach for computing solid-liquid surface tension for nanoscale interfaces  

E-Print Network [OSTI]

A mean field approach for computing solid-liquid surface tension for nanoscale interfaces Chi are largely determined by the solid-liquid surface tension. This is especially true for nanoscale systems with high surface area to volume ratios. While experimental techniques can only measure surface tension

Nielsen, Steven O.

204

Capillary waves and the inherent density profile for the liquid-vapor interface  

E-Print Network [OSTI]

. This approach in turn allows: (1) identification of an "outermost layer" of particles on the liquid. (2). is a nonmonotonic function of normal distance through the interface. and is expected to reflect the diverging bulk distribution for the system in a state of liquid-vapor phase coexistence. This leads to identification

Stillinger, Frank

205

Molecular orientation in soft matter thin films studied by resonant soft X-ray reflectivity  

SciTech Connect (OSTI)

We present a technique to study depth profiles of molecular orientation in soft matter thin films with nanometer resolution. The method is based on dichroism in resonant soft X-ray reflectivity using linear s- and p-polarization. It combines the chemical sensitivity of Near-Edge X-ray Absorption Fine Structure spectroscopy to specific molecular bonds and their orientation relative to the polarization of the incident beam with the precise depth profiling capability of X-ray reflectivity. We demonstrate these capabilities on side chain liquid crystalline polymer thin films with soft X-ray reflectivity data at the carbon K edge. Optical constants of the anisotropic refractive index ellipsoid were obtained from a quantitative analysis using the Berreman formalism. For films up to 50 nm thickness we find that the degree of orientation of the long axis exhibits no depth variation and isindependent of the film thickness.

Mezger, Markus; Jerome, Blandine; Kortright, Jeffrey B.; Valvidares, Manuel; Gullikson, Eric; Giglia, Angelo; Mahne, Nicola; Nannarone, Stefano

2011-01-12T23:59:59.000Z

206

Nonlinear X-ray Compton Scattering  

E-Print Network [OSTI]

X-ray scattering is a weak linear probe of matter. It is primarily sensitive to the position of electrons and their momentum distribution. Elastic X-ray scattering forms the basis of atomic structural determination while inelastic Compton scattering is often used as a spectroscopic probe of both single-particle excitations and collective modes. X-ray free-electron lasers (XFELs) are unique tools for studying matter on its natural time and length scales due to their bright and coherent ultrashort pulses. However, in the focus of an XFEL the assumption of a weak linear probe breaks down, and nonlinear light-matter interactions can become ubiquitous. The field can be sufficiently high that even non-resonant multiphoton interactions at hard X-rays wavelengths become relevant. Here we report the observation of one of the most fundamental nonlinear X-ray-matter interactions, the simultaneous Compton scattering of two identical photons producing a single photon at nearly twice the photon energy. We measure scattered...

Fuchs, Matthias; Chen, Jian; Ghimire, Shambhu; Shwartz, Sharon; Kozina, Michael; Jiang, Mason; Henighan, Thomas; Bray, Crystal; Ndabashimiye, Georges; Bucksbaum, P H; Feng, Yiping; Herrmann, Sven; Carini, Gabriella; Pines, Jack; Hart, Philip; Kenney, Christopher; Guillet, Serge; Boutet, Sebastien; Williams, Garth; Messerschmidt, Marc; Seibert, Marvin; Moeller, Stefan; Hastings, Jerome B; Reis, David A

2015-01-01T23:59:59.000Z

207

X-ray lithography using holographic images  

DOE Patents [OSTI]

Methods for forming X-ray images having 0.25 {micro}m minimum line widths on X-ray sensitive material are presented. A holographic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required. 15 figs.

Howells, M.S.; Jacobsen, C.

1997-03-18T23:59:59.000Z

208

Oscillations During Thermonuclear X-ray Bursts  

E-Print Network [OSTI]

High amplitude, nearly coherent X-ray brightness oscillations during thermonuclear X-ray bursts were discovered with the Rossi X-ray Timing Explorer (RXTE) in early 1996. Spectral and timing evidence strongly supports the conclusion that these oscillations are caused by rotational modulation of the burst emission and that they reveal the spin frequency of neutron stars in low mass X-ray binaries, a long sought goal of X-ray astronomy. Studies carried out over the past year have led to the discovery of burst oscillations in four new sources, bringing to ten the number with confirmed burst oscillations. I review the status of our knowledge of these oscillations and indicate how they can be used to probe the physics of neutron stars. For a few burst oscillation sources it has been proposed that the strongest and most ubiquitous frequency is actually the first overtone of the spin frequency and hence that two nearly antipodal hot spots are present on the neutron star. This inference has important implications for both the physics of thermonuclear burning as well as the mass - radius relation for neutron stars, so its confirmation is crucial. I discuss recent attempts to confirm this hypothesis for 4U 1636-53, the source for which a signal at the putative fundamental (290 Hz) has been claimed.

Tod E. Strohmayer

2001-01-12T23:59:59.000Z

209

X-ray lithography using holographic images  

DOE Patents [OSTI]

Methods for forming X-ray images having 0.25 .mu.m minimum line widths on X-ray sensitive material are presented. A holgraphic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required.

Howells, Malcolm S. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1997-01-01T23:59:59.000Z

210

Predicted X-ray backgrounds for the International X-ray Observatory  

E-Print Network [OSTI]

The background that will be observed by IXO's X-ray detectors naturally separates into two components: (1) a Cosmic X-ray Background (CXB), primarily due to unresolved point sources at high energies (E>2 keV), along with ...

Bautz, Marshall W.

211

Reflection soft X-ray microscope and method  

DOE Patents [OSTI]

A reflection soft X-ray microscope is provided by generating soft X-ray beams, condensing the X-ray beams to strike a surface of an object at a predetermined angle, and focusing the X-ray beams reflected from the surface onto a detector, for recording an image of the surface or near surface features of the object under observation.

Suckewer, Szymon (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ); Rosser, Roy (Princeton, NJ)

1993-01-01T23:59:59.000Z

212

Differential phase contrast X-ray imaging system and components  

DOE Patents [OSTI]

A differential phase contrast X-ray imaging system includes an X-ray illumination system, a beam splitter arranged in an optical path of the X-ray illumination system, and a detection system arranged in an optical path to detect X-rays after passing through the beam splitter.

Stutman, Daniel; Finkenthal, Michael

2014-07-01T23:59:59.000Z

213

X-ray variability in M87  

E-Print Network [OSTI]

We present the evidence for X-ray variability from the core and from knot A in the M87 jet based on data from two observations with the Einstein Observatory High Resolution Imager (HRI) and three observations with the ROSAT HRI. The core intensity showed a 16% increase in 17 months ('79-'80); a 12% increase in the 3 years '92 to '95; and a 17% drop in the last half of 1995. The intensity of knot A appears to have decreased by 16% between 92Jun and 95Dec. Although the core variability is consistent with general expectations for AGN nuclei, the changes in knot A provide constraints on the x-ray emission process and geometry. Thus we predict that the x-ray morphology of knot A will differ significantly from the radio and optical structure.

D. E. Harris; J. A. Biretta; W. Junor

1996-12-05T23:59:59.000Z

214

Displaced Vertices from X-ray Lines  

E-Print Network [OSTI]

We present a simple model of weak-scale thermal dark matter that gives rise to X-ray lines. Dark matter consists of two nearly degenerate states near the weak scale, which are populated thermally in the early universe via co-annihilation with slightly heavier states that are charged under the Standard Model. The X-ray line arises from the decay of the heavier dark matter component into the lighter one via a radiative dipole transition, at a rate that is slow compared to the age of the universe. The model predicts observable signatures at the LHC in the form of exotic events with missing energy and displaced leptons and jets. As an application, we show how this model can explain the recently observed 3.55 keV X-ray line.

Adam Falkowski; Yonit Hochberg; Joshua T. Ruderman

2014-09-09T23:59:59.000Z

215

SSRL School on Synchrotron X-ray Spectroscopy Techniques in Environmental  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Home Home Agenda Location Visitor Information Transportation Tourism & Dining SSRL School on Synchrotron X-ray Spectroscopy Techniques in Environmental and Materials Sciences: Theory and Application June 2-5, 2009 Group photo of the attendees at the SSRL School on X-ray Spectropscopy Techniques in Environmental and Materials Sciences: Theory and Application held June 2-5, 2009 at the Stanford Synchrotron Radiation Lightsource. » View photos from XAS 2009 Overview: Modern synchrotron radiation based X-ray absorption spectroscopy (SR-XAS) techniques offer the ability to probe local molecular scale physical and electronic structures that govern key properties of technological and environmental materials and molecular complexes. The high collimation, intensity, and tunability of SR allow the investigation of a wide range of materials, including thin films and interfaces, nanoparticles, amorphous materials, solutions, hydrated and disordered bacteriogenic minerals, soils, interfaces, and dissolved species.

216

X-ray focal spot locating apparatus and method  

DOE Patents [OSTI]

An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

Gilbert, Hubert W. (Cedar Crest, NM)

1985-07-30T23:59:59.000Z

217

X-ray Science Division: Groups  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Division: Groups Division: Groups Atomic, Molecular and Optical Physics (AMO) Primary Contact: Stephen Southworth Work focuses on understanding how strong optical and x-ray fields interact with matter, with an emphasis on photonic control of electronic, atomic and molecular motion. Chemical and Materials Science (CMS) Primary Contact: Randy Winans Research Disciplines: Chemistry, Materials Science Detectors (DET) Primary Contact: Antonino Miceli GMCA Structural Biology Facility (MX) Primary Contact: Robert Fischetti Research Disciplines: Biology, Life Sciences Imaging (IMG) Primary Contact: Francesco DeCarlo Research Disciplines: Materials Science, Biology, Physics, Life Sciences Inelastic X-ray & Nuclear Resonant Scattering (IXN) Primary Contact: Thomas Gog Research Disciplines: Condensed Matter Physics, Geophysics, Materials

218

Cosmology with X-ray Cluster Baryons  

SciTech Connect (OSTI)

X-ray cluster measurements interpreted with a universal baryon/gas mass fraction can theoretically serve as a cosmological distance probe. We examine issues of cosmological sensitivity for current (e.g., Chandra X-ray Observatory, XMM-Newton) and next generation (e.g., Con-X, XEUS) observations, along with systematic uncertainties and biases. To give competitive next generation constraints on dark energy, we find that systematics will need to be controlled to better than 1percent and any evolution in f_gas (and other cluster gas properties) must be calibrated so the residual uncertainty is weaker than (1+z)0.03.

Linder, Eric V.

2007-04-10T23:59:59.000Z

219

Phase recovery for x-ray crystallography  

Science Journals Connector (OSTI)

For many years people have believed that in conventional x-ray crystallography one can only record the diffraction intensities but not the phases. In order to obtain the atomic arrangements, one usually has to guess a structure and then fit the intensity data by refining its parameters. Here, we show that the phases are in fact hidden in the intensity data, and can be directly recovered from the peak profiles. This method is demonstrated by the normal two-beam x-ray diffraction of a noncentrosymmetric crystal, and nontrivial phases are recovered from the intensity data alone.

G. Xu, G. E. Zhou, and X. Y. Zhang

1999-04-01T23:59:59.000Z

220

Time-resolved x-ray diagnostics  

SciTech Connect (OSTI)

Techniques for time-resolved x-ray diagnostics will be reviewed with emphasis on systems utilizing x-ray diodes or scintillators. System design concerns for high-bandwidth (> 1 GHz) diagnostics will be emphasized. The limitations of a coaxial cable system and a technique for equalizing to improve bandwidth of such a system will be reviewed. Characteristics of new multi-GHz amplifiers will be presented. An example of a complete operational system on the Los Alamos Helios laser will be presented which has a bandwidth near 3 GHz over 38 m of coax. The system includes the cable, an amplifier, an oscilloscope, and a digital camera readout.

Lyons, P.B.

1981-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

2D X-ray scanner and its uses in laboratory reservoir characterization measurements  

SciTech Connect (OSTI)

X-ray techniques are used in petroleum laboratories for a variety of reservoir characterization measurements. This paper describes the configuration of a 2D X-ray scanner and many of the ways in which it simplifies and improves accuracy`s of laboratory measurements. Linear X-ray scanners are most often used to provide descriptions of fluid saturations within core plugs during flow tests. We configured our linear scanner for both horizontal and vertical movement. Samples can be scanned horizontally, vertically, or according to horizontal and vertical grids. X-ray measurements are fast, allowing measurements of two- and three-phase fluid saturations during both steady- and unsteady-state flow processes. Rock samples can be scanned while they are subjected to stress, pore pressure, and temperature conditions simulating those of a petroleum reservoir. Many types of measurements are possible by selecting appropriate X-ray power settings, dopes, filters, and collimator configurations. The scanner has been used for a variety of applications besides fluid saturation measurements. It is useful for measuring porosity distributions in rocks, concentrations of X-ray dopes within flow streams during tracer tests, gap widths in fracture flow cells, fluid interface levels in PVT cells and fluid separators, and other features and phenomena.

Maloney, D.; Doggett, K.

1997-08-01T23:59:59.000Z

222

Sharper Focusing of Hard X-rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Sharper Focusing of Hard X-rays FROM: Physics News Update Number 773 #1, April 12, 2006, by Phil Schewe and Ben Stein Note: This text has been slightly modified from the original. Sharper focusing of hard x-rays has been achieved with a device developed at Argonne National Lab. Because of their high energy, x-rays are hard to focus: they can be reflected from a surface but only at a glancing angle (less than a tenth of a degree); they can be refracted but the index of refraction is very close to 1, so that making efficient lenses becomes a problem; and they can be diffracted, but the relatively thick, variable pitch grating required for focusing is tricky to achieve. The Argonne device is of the diffraction type, and it consists of a stack of alternating layers of metal and silicon, made by depositing progressively thicker layers. When the x-rays fall on such a structure, nearly edge-on, what they see is a grating (called a linear zone plate) consisting of a sort of bar-code pattern.

223

Radioactive Thulium for X-Rays  

Science Journals Connector (OSTI)

Radioactive power from thulium makes Argonne x-ray unit a potential for medical and industrial use ... Active component of the instrument is a tiny particle (one-fifth gram) of thulium-170 which has been made radioactive in a heavy water nuclear reactor at Arco, Idaho. ...

1954-05-03T23:59:59.000Z

224

X-ray spectroscopy of manganese clusters  

SciTech Connect (OSTI)

Much of this thesis represents the groundwork necessary in order to probe Mn clusters more productively than with conventional Mn K-edge XAS and is presented in Part 1. Part 2 contains the application of x-ray techniques to Mn metalloproteins and includes a prognosis at the end of each chapter. Individual Mn oxidation states are more readily distinguishable in Mn L-edge spectra. An empirical mixed valence simulation routine for determining the average Mn oxidation state has been developed. The first Mn L-edge spectra of a metalloprotein were measured and interpreted. The energy of Mn K{beta} emission is strongly correlated with average Mn oxidation state. K{beta} results support oxidation states of Mn(III){sub 2}(IV){sub 2} for the S{sub 1} state of Photosystem II chemical chemically reduced preparations contain predominantly Mn(II). A strength and limitation of XAS is that it probes all of the species of a particular element in a sample. It would often be advantageous to selectively probe different forms of the same element. The first demonstration that chemical shifts in x-ray fluorescence energies can be used to obtain oxidation state-selective x-ray absorption spectra is presented. Spin-dependent spectra can also be used to obtain a more simplified picture of local structure. The first spin-polarized extended x-ray absorption fine structure using Mn K{beta} fluorescence detection is shown.

Grush, M.M. [Univ. of California, Davis, CA (United States). Dept. of Applied Science; [Lawrence Berkeley National Lab., CA (United States). Energy and Environment Div.

1996-06-01T23:59:59.000Z

225

Multiple wavelength X-ray monochromators  

DOE Patents [OSTI]

An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focusing the separate first and second output x-ray radiation wavelengths into separate focal points. 3 figs.

Steinmeyer, P.A.

1992-11-17T23:59:59.000Z

226

Soft x-ray laser microscope  

SciTech Connect (OSTI)

The program consisted of two phases (Phase I and Phase II). The goal of the Phase I (first year program) was to design and construct the Soft X-ray Laser Contact Microscope. Such microscope was constructed and adapted to PPL's 18.2nm soft X-ray Laser (SXL), which in turn was modified and prepared for microscopy experiments. Investigation of the photoresist response to 18.2nm laser radiation and transmissivity of 0.1m thick silicion-nitride (Si[sub 3]N[sub 4]) windows were important initial works. The goal of the first year of Phase II was to construct X-ray contact microscope in combination with existing optical phase microscope, already used by biologists. In the second year of Phase II study of dehydrated Horeseshoe Crab and Hela cancer cells were performed with COXRALM. Also during Phase II, the Imaging X-Ray Laser Microscope (IXRALM) was designed and constructed. This paper describes the development of each of the microscopes and their application for research.

Suckewer, P.I.

1990-10-01T23:59:59.000Z

227

Small Angle X-Ray Scattering Detector  

DOE Patents [OSTI]

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., q.sub.max /q.sub.min.congruent.100.

Hessler, Jan P. (Downers Grove, IL)

2004-06-15T23:59:59.000Z

228

SLAC All Access: X-ray Microscope  

ScienceCinema (OSTI)

SLAC physicists Johanna Nelson and Yijin Liu give a brief overview of the X-ray microscope at the Stanford Synchrotron Radiation Lightsource (SSRL) that is helping improve rechargeable-battery technology by letting researchers peek into the inner workings of batteries as they operate.

Nelson, Johanna; Liu, Yijin

2014-06-13T23:59:59.000Z

229

Molecular Structure and Ordering of Phospholipids at a Liquid-Liquid Interface  

E-Print Network [OSTI]

stretching region of several different phosphocholines adsorbed to the D2O- carbon tetrachloride interface the molecular structure of phosphocholine monolayers adsorbed to the interface between D2O and carbon tetrachloride. Monolayers form from breakup at the interface of aqueous phase phosphocholine vesicles

Richmond, Geraldine L.

230

Ultrahigh vacuum sample mount for x-ray photoelectron spectroscopy up to very high temperature (150-1400 K)  

SciTech Connect (OSTI)

Spectroscopic studies are rarely performed at very high temperature, especially when combined with light from a synchrotron source. Demanding conditions of maintaining ultrahigh vacuum (UHV) during heating, together with the typically brief access to beam time at multiuser synchrotron end stations, may contribute to some of the reasons for the difficulty of such experiments. Consequently, a large number of materials with interesting properties and industrial applications at high temperature remain unexplored. The authors describe here a simple portable sample mount assembly that can be easily utilized at a beamline, with potential utility for a variety of spectroscopic measurements requiring elevated temperatures and an UHV environment. In the specific application described here, the authors use a resistive cartridge heater interfaced with a standard manipulator previously designed for cooling by liquid nitrogen with an UHV chamber and a cylindrical mirror analyzer for x-ray photoemission spectroscopy (XPS) [also known as electron spectroscopy for chemical analysis (ESCA)] at the Synchrotron Radiation Center in Stoughton, WI. The heater cartridge required only modest power to reach target temperatures using an open-loop temperature control. Finally, the authors describe the measurements of XPS (ESCA) and total-electron yield x-ray absorption spectroscopy on nanopowders and on single crystals grown by them. They emphasize the simplicity of the setup, which they believe would be of interest to groups performing measurements at large facilities, where access and time are both limited.

Williamsen, Mark S.; Ray, Shishir K.; Zou Ying; Dudek, John A.; Sen, Somaditya; Bissen, Mark; Kretsch, Laura; Palkar, Vaijayanti R.; Onellion, Marshall F.; Guptasarma, Prasenjit [Department of Physics, University of Wisconsin-Milwaukee, 1900 E. Kenwood Blvd., Milwaukee, Wisconsin 53211 (United States); Synchrotron Radiation Center, 3731 Schneider Dr., Stoughton, Wisconsin 53589 (United States); Department of Electrical Engineering, Indian Institute of Technology Bombay, Mumbai 400076 (India); Department of Physics, University of Wisconsin--Madison, 1150 University Ave., Madison, Wisconsin 53706 (United States); Department of Physics, University of Wisconsin-Milwaukee, 1900 E. Kenwood Blvd., Milwaukee, Wisconsin 53211 (United States)

2011-05-15T23:59:59.000Z

231

Electron accumulation layer at n?Si/non?liquid electrolyte interfaces  

Science Journals Connector (OSTI)

n?Si/non?liquid electrolyteinterfaces have been realized in order to obtain electron accumulation layers of very high concentration at various temperatures. The interface has been characterized by using standard electrochemical measurements and the two?dimensional electron gas has been studied by transconductance and infrared optical absorption measurements. These interfaces are found to exhibit densities as high as 4×101 3 electrons?cm? 2. These results are compared with available data on analogous n?Si/organic?solvent electrolyteinterfaces.

H. Benisty; Ph. Colomban; J.?N. Chazalviel

1987-01-01T23:59:59.000Z

232

Microsoft PowerPoint - S05-07_Varona_Solid-Liquid Waste Interface.pptx  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Liquid Interface Monitor Liquid Interface Monitor (SLIM) Jose Varona D. Roelant, A. Awwad, D. McDaniel Florida International University's Applied Research Center EM Waste Processing Technical Exchange November 17, 2010 Print Close Disclaimer This presentation was prepared as an account of work sponsored by an agency of the United States government (Department of Energy, Office of Environmental Management, under Grant No. DE-FG01-05EW07033). Neither the United States government nor any agency thereof, nor any of their employees, nor any of its contractors, subcontractors, nor their employees makes any warranty, express or implied, or assumes any legal liability or responsibility for the accuracy, completeness,

233

Dual harmonic Kelvin probe force microscopy at the graphene–liquid interface  

SciTech Connect (OSTI)

Kelvin probe force microscopy (KPFM) is a powerful technique for the determination of the contact potential difference (CPD) between an atomic force microscope tip and a sample under ambient and vacuum conditions. However, for many energy storage and conversion systems, including graphene-based electrochemical capacitors, understanding electrochemical phenomena at the solid–liquid interface is paramount. Despite the vast potential to provide fundamental insight for energy storage materials at the nanoscale, KPFM has found limited applicability in liquid environments to date. Here, using dual harmonic (DH)-KPFM, we demonstrate CPD imaging of graphene in liquid. We find good agreement with measurements performed in air, highlighting the potential of DH-KPFM to probe electrochemistry at the graphene–liquid interface.

Collins, Liam; Rodriguez, Brian J., E-mail: brian.rodriguez@ucd.ie [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Conway Institute of Biomolecular and Biomedical Research, University College Dublin, Belfield, Dublin 4 (Ireland); Kilpatrick, Jason I.; Weber, Stefan A. L. [Conway Institute of Biomolecular and Biomedical Research, University College Dublin, Belfield, Dublin 4 (Ireland); Vlassiouk, Ivan V. [Energy and Transportation Science Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831 (United States); Tselev, Alexander; Jesse, Stephen; Kalinin, Sergei V. [Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831 (United States)

2014-03-31T23:59:59.000Z

234

Synchrotron x-ray fluorescence and extended x-ray absorption fine structure analysis  

SciTech Connect (OSTI)

The advent of dedicated synchrotron radiation sources has led to a significant increase in activity in many areas of science dealing with the interaction of x-rays with matter. Synchrotron radiation provides intense, linearly polarized, naturally collimated, continuously tunable photon beams, which are used to determine not only the elemental composition of a complex, polyatomic, dilute material but also the chemical form of the elements with improved accuracy. Examples of the application of synchrotron radiation include experiments in synchrotron x-ray fluorescence (SXRF) analysis and extended x-ray absorption fine structure (EXAFS) analysis. New synchrotron radiation x-ray microprobes for elemental analysis in the parts per billion range are under construction at several laboratories. 76 references, 24 figures.

Chen, J.R.; Gordon, B.M.; Hanson, A.L.; Jones, K.W.; Kraner, H.W.; Chao, E.C.T.; Minkin, J.A.

1984-01-01T23:59:59.000Z

235

X-ray imaging crystal spectrometer for extended X-ray sources  

DOE Patents [OSTI]

Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

Bitter, Manfred L. (Princeton, NJ); Fraenkel, Ben (Jerusalem, IL); Gorman, James L. (Bordentown, NJ); Hill, Kenneth W. (Lawrenceville, NJ); Roquemore, A. Lane (Cranbury, NJ); Stodiek, Wolfgang (Princeton, NJ); von Goeler, Schweickhard E. (Princeton, NJ)

2001-01-01T23:59:59.000Z

236

Rise Time Measurement for Ultrafast X-Ray Pulses  

DOE Patents [OSTI]

A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

Celliers, Peter M.; Weber, Franz A.; Moon, Stephen J.

2005-04-05T23:59:59.000Z

237

X-ray microscopy using grazing-incidence reflection optics  

SciTech Connect (OSTI)

The Kirkpatrick-Baez microscopes are described along with their role as the workhorse of the x-ray imaging devices. This role is being extended with the development of a 22X magnification Kirkpatrick-Baez x-ray microscope with multilayer x-ray mirrors. These mirrors can operate at large angles, high x-ray energies, and have a narrow, well defined x-ray energy bandpass. This will make them useful for numerous experiments. However, where a large solid angle is needed, the Woelter microscope will still be necessary and the technology needed to build them will be useful for many other types of x-ray optics.

Price, R.H.

1981-08-06T23:59:59.000Z

238

X-RAY POINT-SOURCE POPULATIONS CONSTITUTING THE GALACTIC RIDGE X-RAY EMISSION  

SciTech Connect (OSTI)

Apparently diffuse X-ray emission has been known to exist along the central quarter of the Galactic Plane since the beginning of X-ray astronomy; this is referred to as the Galactic Ridge X-ray emission (GRXE). Recent deep X-ray observations have shown that numerous X-ray point sources account for a large fraction of the GRXE in the hard band (2-8 keV). However, the nature of these sources is poorly understood. Using the deepest X-ray observations made in the Chandra bulge field, we present the result of a coherent photometric and spectroscopic analysis of individual X-ray point sources for the purpose of constraining their nature and deriving their fractional contributions to the hard-band continuum and Fe K line emission of the GRXE. Based on the X-ray color-color diagram, we divided the point sources into three groups: A (hard), B (soft and broad spectrum), and C (soft and peaked spectrum). The group A sources are further decomposed spectrally into thermal and non-thermal sources with different fractions in different flux ranges. From their X-ray properties, we speculate that the group A non-thermal sources are mostly active galactic nuclei and the thermal sources are mostly white dwarf (WD) binaries such as magnetic and non-magnetic cataclysmic variables (CVs), pre-CVs, and symbiotic stars, whereas the group B and C sources are X-ray active stars in flares and quiescence, respectively. In the log N-log S curve of the 2-8 keV band, the group A non-thermal sources are dominant above Almost-Equal-To 10{sup -14} erg cm{sup -2} s{sup -1}, which is gradually taken over by Galactic sources in the fainter flux ranges. The Fe K{alpha} emission is mostly from the group A thermal (WD binaries) and the group B (X-ray active stars) sources.

Morihana, Kumiko [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan)] [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Tsujimoto, Masahiro; Ebisawa, Ken [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan)] [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan); Yoshida, Tessei, E-mail: morihana@crab.riken.jp [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)] [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)

2013-03-20T23:59:59.000Z

239

Giant and switchable surface activity of liquid metal via surface oxidation  

Science Journals Connector (OSTI)

...recent developments . Adv Colloid Interface Sci 159 ( 2 ): 198 – 212 . 27 Ladd C So J-H Muth J Dickey MD ( 2013 ) 3D printing of free standing liquid metal microstructures . Adv Mater 25 ( 36 ): 5081 – 5085 . 28 Regan MJ ( 1997 ) X-ray reflectivity...

Mohammad Rashed Khan; Collin B. Eaker; Edmond F. Bowden; Michael D. Dickey

2014-01-01T23:59:59.000Z

240

Cu-Bi as a Model System For Liquid Phase Sintered Thermal Interface Management Materials  

E-Print Network [OSTI]

relates electrical resistivity to thermal conductivity for materials where electrons are principleCu-Bi as a Model System For Liquid Phase Sintered Thermal Interface Management Materials P to produce composite materials. A high melting phase (HMP) and low melting phase (LMP) are mixed

Collins, Gary S.

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
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We encourage you to perform a real-time search of NLEBeta
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241

ARTICLE IN PRESS Modeling hydrogen sulfide emissions across the gas liquid interface  

E-Print Network [OSTI]

production methods in the US have led to the emergence of large- scale commeARTICLE IN PRESS Modeling hydrogen sulfide emissions across the gas­ liquid interface-film theory Hydrogen sulfide Process-based model Lagoon flux Mass transfer a b s t r a c t Hydrogen sulfide (H

Aneja, Viney P.

242

Lattice Boltzmann method for modeling liquid-vapor interface configurations in porous media  

E-Print Network [OSTI]

Lattice Boltzmann method for modeling liquid-vapor interface configurations in porous media Michael; published 13 January 2004. [1] The lattice Boltzmann method (LBM) has emerged as a powerful tool: Modeling; 3230 Mathematical Geophysics: Numerical solutions; KEYWORDS: Lattice Boltzmann Citation: Sukop, M

Sukop, Mike

243

X-rays Illuminate Ancient Archimedes Text  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Related Links: Related Links: May 2005 Headlines TIP Article Press Release Walters Art Museum SSRL Home Page SLAC Home Page Stanford Home Page Tuesday, 31 May 2005 X-rays Illuminate Ancient Archimedes Text (contact: Uwe Bergmann, bergmann@slac.stanford.edu) Archimedes Figure Image provided by Will Noel, The Walters Art Museum An early transcription of Archimedes' mathematical theories has been brought to light through the probing of high-intensity x-rays at SSRL's BL6-2. The text contains part of the Method of Mechanical Theorems, one of Archimedes' most important works, which was probably copied out by a scribe in the tenth century. The parchment on which it was written was later scraped down and reused as pages in a twelfth century prayer book, producing a document known as a palimpsest (which comes from the Greek,

244

HIGH BRILLIANCE X-RAY SCATTERING FOR  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

BRILLIANCE X-RAY SCATTERING FOR BRILLIANCE X-RAY SCATTERING FOR LIFE SCIENCES (LIX) Group Leader: Lin Yang Proposal Team: O. Bilsel 1 , B. Hsiao 2 , H. Huang 3 , T. Irving 4 , A. Menzel 5 , L. Pollack 6 , C. Riekel 7 , J. Rubert 8 , H. Tsuruta 9 , L. Yang 10 1 University of Massachusetts, 2 Stony Brook University, 3 Rice University, 4 IIT, 5SLS, 6 Cornell University, 7 European Synchrotron Radiation Facility, 8 NEU, 9 Stanford Synchrotron Radiation Lightsource, 10 Brookhaven National Laboratory TECHNIQUES AND CAPABILITIES APPLICATIONS ADDITIONAL INFORMATION * Energy range 2-20keV using undulator source. Simultaneous SAXS/WAXS to cover 0.003-3Å -1 at 12keV with 1 micron spot size * Time-resolved solution scattering with resolution of (1) microseconds to milliseconds using continuous-flow mixing (5µm x 10µm spot size) and (2) milliseconds using stopped-

245

Element 104 identified by characteristic x rays  

Science Journals Connector (OSTI)

A research team at the Oak Ridge National Laboratory has recently announced that they have conclusively identified the 257 isotope of element 104. This new work shows promise of shedding light on the controversy between Albert Ghiorso and Georgi N. Flerov the leaders respectively of the groups at Lawrence Berkeley Laboratory and the Joint Institute for Nuclear Research Dubna. The isotope 104 X 257 decays by alpha emission to 102 No 253 with a half?life of 4.3 seconds. The Oak Ridge group observed the K?series x rays from nobelium in coincidence with the alpha particles from 104 X 257 ; the observation of x?ray spectra has never been reported previously by the Berkeley or Dubna workers according to Curtis E. Bemis Jr spokesman for the group.

Ronald J. Cohn

1973-01-01T23:59:59.000Z

246

X-ray radiography for container inspection  

DOE Patents [OSTI]

Arrangements of X-ray inspection systems are described for inspecting high-z materials in voluminous objects such as containers. Inspection methods may involve generating a radiographic image based on detected attenuation corresponding to a pulsed beams of radiation transmitted through a voluminous object. The pulsed beams of radiation are generated by a high-energy source and transmitted substantially downward along an incident angle, of approximately 1.degree. to 30.degree., to a vertical axis extending through the voluminous object. The generated radiographic image may be analyzed to detect on localized high attenuation representative of high-z materials and to discriminate high-z materials from lower and intermediate-z materials on the basis of the high density and greater attenuation of high-z material for higher energy (3-10 MeV) X-rays, and the compact nature of threatening masses of fissionable materials.

Katz, Jonathan I. (Clayton, MO); Morris, Christopher L. (Los Alamos, NM)

2011-06-07T23:59:59.000Z

247

Sample holder for X-ray diffractometry  

DOE Patents [OSTI]

A sample holder for use with X-ray diffractometers with the capability to rotate the sample, as well as to adjust the position of the sample in the x, y, and z directions. Adjustment in the x direction is accomplished through loosening set screws, moving a platform, and retightening the set screws. Motion translators are used for adjustment in the y and z directions. An electric motor rotates the sample, and receives power from the diffractometer.

Hesch, Victor L. (Los Alamos, NM)

1992-01-01T23:59:59.000Z

248

Columbia University X-Ray Measurements  

E-Print Network [OSTI]

V-720 keV · NaI 2x2x2" detector views an energy range of 1 keV-3 MeV Store signal in the tree. computer configuration. Plasmas were created using multi-frequency ECRH, and we find that most of the plasma energy is stored in the fast electrons. The energy spectrum of the x-ray emission below 740 keV is measured

249

Silicon Absolute X-Ray Detectors  

SciTech Connect (OSTI)

The responsivity of silicon photodiodes having no loss in the entrance window, measured using synchrotron radiation in the 1.75 to 60 keV range, was compared to the responsivity calculated using the silicon thickness measured using near-infrared light. The measured and calculated responsivities agree with an average difference of 1.3%. This enables their use as absolute x-ray detectors.

Seely, John F. [Naval Research Laboratory, Washington, D.C. 20375 (United States); Korde, Raj; Sprunck, Jacob [International Radiation Detectors, Inc., Torrance, CA 90505-5243 (United States); Medjoubi, Kadda; Hustache, Stephanie [Synchrotron SOLEIL, L'Orme des Merisiers, Saint-Aubin, BP 48, 91192 Gif-sur-Yvette CEDEX (France)

2010-06-23T23:59:59.000Z

250

Ultrashort x-ray backlighters and applications  

SciTech Connect (OSTI)

Previously, using ultrashort laser pulses focused onto solid targets, we have experimentally studied a controllable ultrafast broadband radiation source in the extreme ultraviolet for time-resolved dynamical studies in ultrafast science [J. Workman, A. Maksimchuk, X. Llu, U. Ellenberger, J. S. Coe, C.-Y. Chien, and D. Umstadter, ``Control of Bright Picosecond X-Ray Emission from Intense Sub- Picosecond Laser-Plasma Interactions,`` Phys. Rev. Lett. 75, 2324 (1995)]. Once armed with a bright ultrafast broadband continuum x-ray source and appropriate detectors, we used the source as a backlighter to study a remotely produced plasma. The application of the source to a problem relevant to high-density matter completes the triad: creating and controlling, efficiently detecting, and applying the source. This work represented the first use of an ultrafast laser- produced x-ray source as a time-resolving probe in an application relevant to atomic, plasma and high-energy-density matter physics. Using the x-ray source as a backlighter, we adopted a pump-probe geometry to investigate the dynamic changes in electronic structure of a thin metallic film as it is perturbed by an ultrashort laser pulse. Because the laser deposits its energy in a skin depth of about 100 {Angstrom} before expansion occurs, up to gigabar pressure shock waves lasting picosecond in duration have been predicted to form in these novel plasmas. This raises the possibility of studying high- energy-density matter relevant to inertial confinement fusion (ICF) and astrophysics in small-scale laboratory experiments. In the past, time-resolved measurements of K-edge shifts in plasmas driven by nanosecond pulses have been used to infer conditions in highly compressed materials. In this study, we used 100-fs laser pulses to impulsively drive shocks into a sample (an untamped 1000 {Angstrom} aluminum film on 2000 {Angstrom} of parylene-n), measuring L-edge shifts.

Umstadter, D., University of Michigan

1997-08-01T23:59:59.000Z

251

X-ray holography at Lawrence Livermore National Laboratory  

SciTech Connect (OSTI)

The x-ray holography program at the Lawrence Livermore National Laboratory has two principal goals: (1) the development of x-ray diffraction techniques for DNA sequence analysis and (2) the development of x-ray laser holography for structural analysis of intact biological cells and organelles. DNA sequence analysis will be accomplished by applying x-ray diffraction techniques to determine the ensemble average of the sequence of labels along the individual elements of crystalline DNA. X-ray laser holographic imaging will be accomplished by applying three dimensional x-ray holography to elucidate the structure of few hundred angstrom objects such as 300 {Angstrom} chromatin fibers, nuclear pores and nucleic acid replication complexes in living cells. Existing laboratory x-ray lasers will be utilized to produce flash x-ray holograms of the biological structures.

Trebes, J.; Annese, C.; Birdsall, D.; Brase, J.; Gray, J.; Lane, S.; London, R.; Matthews, D.; Peters, D.; Pinkel, D.; Stone, G.; Rapp, D.; Rosen, M.; Weier, U.; Yorkey, T.

1990-10-11T23:59:59.000Z

252

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing...

253

X-ray diffraction study of zirconia pillared clays  

Science Journals Connector (OSTI)

X-ray powder diffraction (XRPD) and X-ray radial electronic distribution density (RED) of initial and zirconia-pillared interlayered clays (Zr-PILC) were studied. After pillaring, the basal ... under air to 17.7 ...

D.A. Zyuzin; E.M. Moroz; T.G. Kuznetsova…

2004-01-01T23:59:59.000Z

254

Development of a Schwarzschild-type x-ray microscope  

Science Journals Connector (OSTI)

A Schwarzschild-type x-ray microscope has been designed, constructed, and tested. Ni/C multilayers were used as the x-ray mirrors, with a thickness (2d) of 7 nm and 30 layer pairs. The...

Kado, M; Yamashita, K; Ohtani, M; Tanaka, K A; Kodama, R; Kitamoto, S; Yamanaka, T; Nakai, S

1991-01-01T23:59:59.000Z

255

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in...

256

A Record Run for the APS X-ray Source  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

2004 | 2003 | 2002 | 2001 2000 Subscribe to APS News rss feed A Record Run for the APS X-ray Source FEBRUARY 23, 2012 Bookmark and Share The APS storage ring. X-ray beams and...

257

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscop...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Refinement Friday, September 28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray...

258

TENDER ENERGY X-RAY ABSORPTION  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

TENDER ENERGY X-RAY ABSORPTION TENDER ENERGY X-RAY ABSORPTION SPECTROSCOPY (TES) Project Team: S. Bare 1,2 , J. Brandes 3 , T. Buonassisi 4 , J. Chen 5,2 , M. Croft 6 , E. DiMasi 7 , A. Frenkel 8,2 , D. Hesterberg 9 , S. Hulbert 7,2 , S. Khalid 7 , S. Myneni 10 , P. Northrup 7,11 , E.T. Rasbury 11 , B. Ravel 12 , R. Reeder 11 , J. Rodriguez 7,2 , D. Sparks 5,13 , V. Stojanoff 7 , G. Waychunas 14 1 UOP LLC, 2 Synchrotron Catalysis Consortium, 3 Skidaway Inst. of Oceanography, 4 MIT Laboratory for Photovoltaics Research, 5 Univ. of Delaware, 6 Rutgers Univ., 7 Brookhaven National Lab, 8 Yeshiva Univ., 9 North Carolina State Univ., 10 Princeton Univ., 11 Stony Brook Univ., 12 NIST, 13 Delaware Environmental Inst., 14 Lawrence Berkeley National Lab TECHNIQUES: High performance and in-situ X-ray absorption spectroscopy and spatially-resolved XAS of

259

The X-ray Telescope of CAST  

E-Print Network [OSTI]

The Cern Axion Solar Telescope (CAST) is in operation and taking data since 2003. The main objective of the CAST experiment is to search for a hypothetical pseudoscalar boson, the axion, which might be produced in the core of the sun. The basic physics process CAST is based on is the time inverted Primakoff effect, by which an axion can be converted into a detectable photon in an external electromagnetic field. The resulting X-ray photons are expected to be thermally distributed between 1 and 7 keV. The most sensitive detector system of CAST is a pn-CCD detector combined with a Wolter I type X-ray mirror system. With the X-ray telescope of CAST a background reduction of more than 2 orders off magnitude is achieved, such that for the first time the axion photon coupling constant g_agg can be probed beyond the best astrophysical constraints g_agg < 1 x 10^-10 GeV^-1.

M. Kuster; H. Bräuninger; S. Cébrian; M. Davenport; C. Elefteriadis; J. Englhauser; H. Fischer; J. Franz; P. Friedrich; R. Hartmann; F. H. Heinsius; D. H. H. Hoffmann; G. Hoffmeister; J. N. Joux; D. Kang; K. Königsmann; R. Kotthaus; T. Papaevangelou; C. Lasseur; A. Lippitsch; G. Lutz; J. Morales; A. Rodríguez; L. Strüder; J. Vogel; K. Zioutas

2007-05-10T23:59:59.000Z

260

CHEMICAL APPLICATIONS OF INELASTIC X-RAY SCATTERING  

SciTech Connect (OSTI)

Inelastic x-ray scattering (IXS), complementary to other more established inelastic scattering probes, such as light scattering, electron scattering, and neutron scattering, is becoming an important experimental technique in the study of elementary excitations in condensed matters. Over the past decade, IXS with total energy resolution of few meV has been achieved, and is being used routinely in the study of phonon dispersions in solids and liquids as well as dynamics in disordered and biological systems. In the study of electronic excitations, IXS with total energy resolution on the order of 100 meV to 1 eV is gaining wider applications also. For example, IXS has been used to study collective excitations of valence electrons, single electron excitations of valence electrons, as well as core electron excitations. In comparison with the alternative scattering techniques mentioned above, IXS has several advantages. First, IXS probes the full momentum transfer range of the dielectric response of the sample, whereas light scattering is limited to very small momentum transfers, and electron scattering suffers the effects of multiple scattering at large momentum transfers. Second, since IXS measures the bulk properties of the sample it is not surface sensitive, therefore it does not require special preparation of the sample. The greater flexibility in sample conditions and environments makes IXS an ideal probe in the study of liquids and samples under extreme temperature, pressure, and magnetic field. Third, the tunability of synchrotron radiation sources enables IXS to exploit element specificity and resonant enhancement of scattering cross sections. Fourth, IXS is unique in the study of dynamics of liquids and amorphous solids because it can probe the particular region of energy-momentum transfer phase space, which is inaccessible to inelastic neutron scattering. On the other hand, the main disadvantages of IXS are the small cross sections and the strong absorption of x-rays in high Z elements.

HAYASHI,H.; UDAGAWA,Y.; GILLET,J.M.; CALIEBE,W.A.; KAO,C.C.

2001-08-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

SSRL School 2007 on Hard X-ray Scattering Techniques in MES  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

May 15-17, 2007 SSRL School on Hard X-ray Scattering Techniques in Materials and Environmental Sciences Group photo taken at the SSRL School on Hard X-ray Scattering Techniques in Materials and Environmental Sciences. A large, printable version of this group image is available via clicking on the image. Overview: Modern synchrotron-based X-ray scattering (SR-XRS) techniques offer the ability to probe nano- and atomic-scale structures and order/disorder relationships that critically govern the properties of advanced technological and environmental materials. The high collimation, intensity, and tunability of SR allow the investigation of a wide range of materials, including thin films and interfaces, nanoparticles, amorphous materials, solutions, hydrated and disordered bacteriogenic minerals,

262

In Situ X-Ray Probing Reveals Fingerprints of Surface Platinum Oxide  

SciTech Connect (OSTI)

In situ x-ray absorption spectroscopy (XAS) at the Pt L{sub 3} edge is a useful probe for Pt-O interactions at polymer electrolyte membrane fuel cell (PEMFC) cathodes. We show that XAS using the high energy resolution fluorescence detection (HERFD) mode, applied to a well-defined monolayer Pt/Rh(111) sample where the bulk penetrating hard x-rays probe only surface Pt atoms, provides a unique sensitivity to structure and chemical bonding at the Pt-electrolyte interface. Ab initio multiple-scattering calculations using the FEFF8 code and complementary extended x-ray absorption fine structure (EXAFS) results indicate that the commonly observed large increase of the white-line at high electrochemical potentials on PEMFC cathodes originates from platinum oxide formation, whereas previously proposed chemisorbed oxygen-containing species merely give rise to subtle spectral changes.

Friebel, Daniel

2011-08-24T23:59:59.000Z

263

Applications of holography to x-ray imaging  

SciTech Connect (OSTI)

In this paper we consider various applications of holographic techniques to the problem of soft x-ray imaging. We give special attention to imaging biological material using x-rays in the wavelength range 24 to 45A. We describe some experiments on formation and reconstruction of x-ray holograms and propose some ways in which holographic techniques might contribute to the difficult problem of fabricating optical elements for use in the soft x-ray region.

Howells, M.; Iarocci, M.; Kenney, J.; Rarback, H.; Rosser, R.; Yun, W.

1985-03-01T23:59:59.000Z

264

Applications of holography to X-ray imaging  

SciTech Connect (OSTI)

In this paper the authors consider various applications of holographic techniques to the problem of soft x-ray imaging. Special attention is given to imaging biological material using x-rays in the wavelength range 24-45A. The authors describe some experiments on formation and reconstruction of x-ray holograms and propose some ways in which holographic techniques might contribute to the difficult problem of fabricating optical elements for use in the soft x-ray region.

Howells, M.; Iarocci, M.; Kenney, J.; Rarback, H.; Rosser, R.; Yun, W.

1985-01-01T23:59:59.000Z

265

X-ray MicroCT Training Presentation  

E-Print Network [OSTI]

X-ray MicroCT Training Presentation T. Fettah Kosar, PhD Center for Nanoscale Systems Harvard) Model: HMXST225 (max. 225 kV) #12;Overview 3 Introduction to X-ray imaging and Computed Tomography (CT) · What are X-rays and how do we generate and image them? · How do we magnify X-ray images and keep them

266

Modeling of ultrasound transmission through a solid-liquid interface comprising a network of gas pockets  

SciTech Connect (OSTI)

Ultrasonic inspection of sodium-cooled fast reactor requires a good acoustic coupling between the transducer and the liquid sodium. Ultrasonic transmission through a solid surface in contact with liquid sodium can be complex due to the presence of microscopic gas pockets entrapped by the surface roughness. Experiments are run using substrates with controlled roughness consisting of a network of holes and a modeling approach is then developed. In this model, a gas pocket stiffness at a partially solid-liquid interface is defined. This stiffness is then used to calculate the transmission coefficient of ultrasound at the entire interface. The gas pocket stiffness has a static, as well as an inertial component, which depends on the ultrasonic frequency and the radiative mass.

Paumel, K.; Baque, F. [CEA, DEN, Nuclear Technology Department, F-13108 Saint-Paul-lez-Durance (France); Moysan, J.; Corneloup, G. [Laboratoire de Caracterisation Non Destructive, Universite de la Mediterranee, IUT Aix-en-Provence, Avenue Gaston Berger, 13625 Aix-en-Provence (France); Chatain, D. [CNRS, Aix-Marseille Universite, CINAM-UPR3118, Campus de Luminy, Case 913, 13288 Marseille cedex 09 (France)

2011-08-15T23:59:59.000Z

267

Quantitative x-ray imager (abstract)  

SciTech Connect (OSTI)

We report on development of a quantitative x-ray imager (QXI) for the national Inertial Confinement Fusion Program. Included in this development is a study of photocathode response as a function of photon energy, 2--17.5 keV, which is related to diagnostic development on the National Ignition Facility (NIF). The QXI is defined as being a quantative imager due to the repeated characterization. This instrument is systematically checked out, electronically as well as its photocathode x-ray response, both on a direct current and pulsed x-ray sources, before and after its use on a shot campaign. The QXI is a gated x-ray imager1 used for a variety of experiments conducted in the Inertial Confinement Fusion and Radiation Physics Program. The camera was assembled in Los Alamos and has been under development since 1997 and has now become the workhorse framing camera by the program. The electronics were built by Grant Applied Physics of San Fransisco, CA.2 The QXI has been used at the LANL Trident, LLNL Nova, and University of Rochester Laboratory OMEGA laser facilities. The camera consists of a grated microchannel plate (MCP), a phosphor coated fiberoptic faceplate coupled to film for data readout, along with high speed electronic pulsers to drive the x-ray detector. The QXI has both a two-strip and a four-strip detection head and has the ability to individually bias the gain of each of the strips. The timing of the QXI was done at the Trident short pulse laboratory, using 211 nm light. Single strip jitter was looked at as well and determined to be <25 ps. Flatfielding of the photocathode across the MCP was done with the Trident main laser with 150 J on a gold disk with a 1 ns. Spatial resolution was determined to be <5 {mu}m by using the same laser conditions as before and a backlit 1000 lp/in. grid. The QXI has been used on cylindrical implosion work at the Nova Laser Facility, and on direct-drive cylinder mix and indirect-drive high convergence implosion experiments at OMEGA. Its two-strip module has provided the capability to look at point backlighters, as part of technique development for experiments on the NIF. Its next use will be in March 2000 with its off axis viewer nose at Omega, providing a perpendicular view of Rayleigh--Taylor spike dissipation.

Evans, Scott C.; Archuleta, Tom N.; Oertel, John A.; Walsh, Peter J.

2001-01-01T23:59:59.000Z

268

X-ray Microscopy and Imaging: 2-BM  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

BM BM Introduction The 2-BM beamline offers measurement capabilities for x-ray microtomography, x-ray topography and x-ray microdiffraction. X-ray microtomography and x-ray diffraction instruments are installed on separate optical tables for independent operation with fast switch over time. Optically-coupled high-resolution CCD system is used for microtomography and topography with up to 1 micron spatial resolution. X-ray microdiffraction setup consists of KB microfocussing mirrors (~3 micron minimum spot), four-circle Huber diffractometer, high-precision translation sample stage, two orthogonally-mounted video cameras for viewing sample, fluorescence detector (Si-drift diode) and diffraction detector (a scintillation detector or a CCD). Three different levels of monochromaticity are available. Conventional monochromatic x-rays from a double-bounced Si (111) crystal monochromator (DCM, D E/E=1E-4), wide band-pass monochromatic x-rays from a double multilayer monochromator (DMM, D E/E=1~4E-2) and pink beam. The available x-ray range is from 5 keV to 30 keV. The lower limit is due to the x-ray windows and the upper limit is due to the critical angle of the x-ray mirror. Two different coatings (Cr and Pt) for the x-ray mirror allow either 20 keV or 30 keV energy cutoff.

269

Improvement of YOHKOH Hard X-Ray Imaging  

Science Journals Connector (OSTI)

......Figure la shows the X-ray penetration rate through a single, 0.5 mm...index Fig. 1. (a) X-ray penetration rate through a single tung- sten...the K-escape. (b) X-ray penetration rates averaged over the HXT M2 and......

Jun Sato; Takeo Kosugi; Kazuo Makishima

1999-02-01T23:59:59.000Z

270

Small Angle X-ray Scattering (SAXS) Laboratory Learning Experiences  

E-Print Network [OSTI]

.A. & Svergun D.I. (1987). Structure Analysis by Small-Angle X-Ray and Neutron Scattering. NY: Plenum PressSmall Angle X-ray Scattering (SAXS) Laboratory Learning Experiences o - Use of small angle X-ray scattering instrumentation o - Programs that you will use SAXS (BRUKER AXS) PRIMUS (Konarev, Volkov, Koch

Meagher, Mary

271

X-ray Diffraction Laboratory Department of Chemistry  

E-Print Network [OSTI]

X-ray Diffraction Laboratory Department of Chemistry Texas A & M University College Station, Texas Phone : 979-845-9125 www.chem.tamu.edu/xray xray@tamu.edu X-rayDiffractionLaboratory DepartmentofChemistry 3255TAMU CollegeStation,TX77843-3255 Mission The purpose of our laboratory is to provide X-ray

Meagher, Mary

272

X-ray Diffraction Practicals 1 Graphics Programs  

E-Print Network [OSTI]

X-ray Diffraction Practicals 1 Graphics Programs that will read SHELX or CIF files J. Reibenspies, N. Bhuvanesh ver 1.0.0 #12;X-ray Diffraction Practicals 2 Free software. Gretep : Reads SHELX files shelx files or output thermal ellipsoid plots. http://www.umass.edu/microbio/rasmol/ #12;X-ray

Meagher, Mary

273

X-ray Emission from Massive Stars David Cohen  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore University, Oct. 13, 2005 astro.swarthmore.edu/~cohen/ #12;Outline 1. What you need to know: a. X-rays from the Sun - magnetic activity, x-ray spectra b. Hot stars c. Radiation-driven winds and the Doppler shift d

Cohen, David

274

X-Ray Photoelectron Spectroscopy XPS Mark Engelhard  

E-Print Network [OSTI]

X-Ray Photoelectron Spectroscopy XPS Mark Engelhard 1 #12;EMSL XPS Instrumentation 2 Physical Electronics Quantera XPS High Energy Resolution Focused X-ray Beam Capability Catalysis reaction and processing chamber with inert atmosphere glove box connected to a PHI Quantera Scanning X-ray Microprobe

275

X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO)  

DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

The primary interactions of low-energy x-rays within condensed matter, viz. photoabsorption and coherent scattering, are described for photon energies outside the absorption threshold regions by using atomic scattering factors. The atomic scattering factors may be accurately determined from the atomic photoabsorption cross sections using modified Kramers-Kronig dispersion relations. From a synthesis of the currently available experimental data and recent theoretical calculations for photoabsorption, the angle-independent, forward-scattering components of the atomic scattering factors have been thus semiempirically determined and tabulated here for 92 elements and for the region 50-30,000 eV. Atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction. The incoherent scattering contributions that become significant for the light elements at the higher photon energies are similarly determined. The basic x-ray interaction relations that are used in applied x-ray physics are presented here in terms of the atomic scattering factors. The bulk optical constants are also related to the atomic scattering factors. These atomic and optical relations are applied to the detailed calculation of the reflectivity characteristics of a series of practical x-ray mirror, multilayer, and crystal monochromators. Comparisons of the results of this semiempirical,"atom-like", description of x-ray interactions for the low-energy region with those of experiment and ab initio theory are presented.

Henke, B.L.; Gullikson, E.M.; Davis, J.C.

276

Generation of first hard X-ray pulse at Tsinghua Thomson Scattering X-ray Source  

SciTech Connect (OSTI)

Tsinghua Thomson Scattering X-ray Source (TTX) is the first-of-its-kind dedicated hard X-ray source in China based on the Thomson scattering between a terawatt ultrashort laser and relativistic electron beams. In this paper, we report the experimental generation and characterization of the first hard X-ray pulses (51.7 keV) via head-on collision of an 800 nm laser and 46.7 MeV electron beams. The measured yield is 1.0 Multiplication-Sign 10{sup 6} per pulse with an electron bunch charge of 200 pC and laser pulse energy of 300 mJ. The angular intensity distribution and energy spectra of the X-ray pulse are measured with an electron-multiplying charge-coupled device using a CsI scintillator and silicon attenuators. These measurements agree well with theoretical and simulation predictions. An imaging test using the X-ray pulse at the TTX is also presented.

Du Yingchao; Yan Lixin; Hua Jianfei; Du Qiang; Zhang Zhen; Li Renkai; Qian Houjun; Huang Wenhui; Chen Huaibi; Tang Chuanxiang [Accelerator Laboratory, Department of Engineering Physics, Tsinghua University, Beijing 100084 (China); Key Laboratory of Particle and Radiation Imaging, Tsinghua University, Ministry of Education, Beijing 100084 (China); Key Laboratory of High Energy Radiation Imaging Fundamental Science for National Defense, Tsinghua University, Beijing 100084 (China)

2013-05-15T23:59:59.000Z

277

Calibrating X-ray Imaging Devices for Accurate Intensity Measurement  

SciTech Connect (OSTI)

The purpose of the project presented is to develop methods to accurately calibrate X-ray imaging devices. The approach was to develop X-ray source systems suitable for this endeavor and to develop methods to calibrate solid state detectors to measure source intensity. NSTec X-ray sources used for the absolute calibration of cameras are described, as well as the method of calibrating the source by calibrating the detectors. The work resulted in calibration measurements for several types of X-ray cameras. X-ray camera calibration measured efficiency and efficiency variation over the CCD. Camera types calibrated include: CCD, CID, back thinned (back illuminated), front illuminated.

Haugh, M. J.

2011-07-28T23:59:59.000Z

278

Three-dimensional reconstruction of liquid phases in disordered mesopores using in situ small-angle scattering  

Science Journals Connector (OSTI)

In situ synchrotron small-angle X-ray scattering is used to investigate wetting transitions of liquids confined in disordered mesoporous materials. A plurigaussian stochastic model is proposed, which enables one to analyze the data in terms of changing interface areas, contact angle and triple-line length.

Gommes, C.J.

2013-03-14T23:59:59.000Z

279

X-Ray Imaging Crystal Spectrometer for Extended X-Ray Sources  

SciTech Connect (OSTI)

Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokamak fusion experiment to provide spatially and temporally resolved data on plasma parameters such as ion temperature, toroidal and poloidal rotation, electron temperature, impurity ion charge-state distributions, and impurity transport. The imaging properties of these spherically or toroidally curved crystals provide both spectrally and spatially resolved X-ray data from the plasma using only one small spherically or toroidally curved crystal, thus eliminating the requirement for a large array of crystal spectrometers and the need to cross-calibrate the various crystals.

Bitter, Manfred L.; Fraekel, Benjamin; Gorman, James L.; Hill, Kenneth W.; Roquemore, Lane A.; Stodiek, Wolfgang; Goeler, Schweickhard von

1999-05-01T23:59:59.000Z

280

X-Ray Source Based on the Parametric X-Rays  

E-Print Network [OSTI]

Prospects of parametric x-rays (PXR) application for the development of a tuneable quasi-monochromatic x-ray source for medical imaging are discussed. Analysis of basic requirements for electron accelerator shows that it must be relatively low-energy and high-current linac. In comparison with known ultra-relativistic cases, at low energies PXR properties will be modified to a great extent by multiple scattering of the electrons. PXR intensity dependence on target thickness and beam energy are calculated taking multiple scattering into account. It is concluded that PXR source based on real medical accelerators is feasible and can provide x-ray flux needful for obtaining high quality medical images.

Alexander Lobko; Olga Lugovskaya

2005-09-02T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

Interface for the rapid analysis of liquid samples by accelerator mass spectrometry  

DOE Patents [OSTI]

An interface for the analysis of liquid sample having carbon content by an accelerator mass spectrometer including a wire, defects on the wire, a system for moving the wire, a droplet maker for producing droplets of the liquid sample and placing the droplets of the liquid sample on the wire in the defects, a system that converts the carbon content of the droplets of the liquid sample to carbon dioxide gas in a helium stream, and a gas-accepting ion source connected to the accelerator mass spectrometer that receives the carbon dioxide gas of the sample in a helium stream and introduces the carbon dioxide gas of the sample into the accelerator mass spectrometer.

Turteltaub, Kenneth; Ognibene, Ted; Thomas, Avi; Daley, Paul F; Salazar Quintero, Gary A; Bench, Graham

2014-02-04T23:59:59.000Z

282

Apparatus for monitoring X-ray beam alignment  

DOE Patents [OSTI]

A self-contained, hand-held apparatus is provided for minitoring alignment of an X-ray beam in an instrument employing an X-ray source. The apparatus includes a transducer assembly containing a photoresistor for providing a range of electrical signals responsive to a range of X-ray beam intensities from the X-ray beam being aligned. A circuit, powered by a 7.5 VDC power supply and containing an audio frequency pulse generator whose frequency varies with the resistance of the photoresistor, is provided for generating a range of audible sounds. A portion of the audible range corresponds to low X-ray beam intensity. Another portion of the audible range corresponds to high X-ray beam intensity. The transducer assembly may include an a photoresistor, a thin layer of X-ray fluorescent material, and a filter layer transparent to X-rays but opaque to visible light. X-rays from the beam undergoing alignment penetrate the filter layer and excite the layer of fluorescent material. The light emitted from the fluorescent material alters the resistance of the photoresistor which is in the electrical circuit including the audio pulse generator and a speaker. In employing the apparatus, the X-ray beam is aligned to a complete alignment by adjusting the X-ray beam to produce an audible sound of the maximum frequency.

Steinmeyer, Peter A. (Arvada, CO)

1991-10-08T23:59:59.000Z

283

Photon Sciences | Beamlines | HXN: Hard X-ray Nanoprobe  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

HXN: Hard X-ray Nanoprobe HXN: Hard X-ray Nanoprobe Poster | Fact Sheet | Preliminary Design Report Scientific Scope The Hard X-ray Nanoprobe beamline and endstation instruments (HXN) will be designed and constructed to explore new frontiers of hard x-ray microscopy applications with the highest achievable spatial resolution. Currently the available spatial resolution for scientific applications, provided by scanning x-ray microscopes in the hard x-ray regime, is limited to ~50nm, which is still insufficient for probing the nanoscale interfacial structures critical in determining properties and functionalities of material and biological systems. The HXN beamline aims to enable x-ray experiments at spatial resolutions ranging from 10 to 30 nm with an ultimate goal of ~1 nm. Beamline Description

284

Introduction to Neutron and X-Ray Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Scattering Studies of Thin Scattering Studies of Thin Polymer Films Introduction to Neutron and X-Ray Scattering Sunil K. Sinha UCSD/LANL Acknowledgements: Prof. R.Pynn( Indiana U.) Prof. M.Tolan (U. Dortmund) Wilhelm Conrad Röntgen 1845-1923 1895: Discovery of X-Rays 1901 W. C. Röntgen in Physics for the discovery of x-rays. 1914 M. von Laue in Physics for x-ray diffraction from crystals. 1915 W. H. Bragg and W. L. Bragg in Physics for crystal structure determination. 1917 C. G. Barkla in Physics for characteristic radiation of elements. 1924 K. M. G. Siegbahn in Physics for x-ray spectroscopy. 1927 A. H. Compton in Physics for scattering of x-rays by electrons. 1936 P. Debye in Chemistry for diffraction of x-rays and electrons in gases.

285

Hard X-ray tails and cyclotron features in X-ray pulsars  

E-Print Network [OSTI]

We review the physical processes occurring in the magnetosphere of accreting X-ray pulsars, with emphasis on those processes that give rise to observable effects in their high (E>10 keV) energy spectra. In the second part we compare the empirical spectral laws used to fit the observed spectra with theoretical models, at the light of the BeppoSAX results on the broad-band characterization of the X-ray pulsar continuum, and the discovery of new (multiple) cyclotron resonance features.

Mauro Orlandini; Daniele Dal Fiume

2001-07-27T23:59:59.000Z

286

X-ray imaging performance of scintillator-filled silicon pore arrays  

SciTech Connect (OSTI)

The need for fine detail visibility in various applications such as dental imaging, mammography, but also neurology and cardiology, is the driver for intensive efforts in the development of new x-ray detectors. The spatial resolution of current scintillator layers is limited by optical diffusion. This limitation can be overcome by a pixelation, which prevents optical photons from crossing the interface between two neighboring pixels. In this work, an array of pores was etched in a silicon wafer with a pixel pitch of 50 {mu}m. A very high aspect ratio was achieved with wall thicknesses of 4-7 {mu}m and pore depths of about 400 {mu}m. Subsequently, the pores were filled with Tl-doped cesium iodide (CsI:Tl) as a scintillator in a special process, which includes powder melting and solidification of the CsI. From the sample geometry and x-ray absorption measurement the pore fill grade was determined to be 75%. The scintillator-filled samples have a circular active area of 16 mm diameter. They are coupled with an optical sensor binned to the same pixel pitch in order to measure the x-ray imaging performance. The x-ray sensitivity, i.e., the light output per absorbed x-ray dose, is found to be only 2.5%-4.5% of a commercial CsI-layer of similar thickness, thus very low. The efficiency of the pores to transport the generated light to the photodiode is estimated to be in the best case 6.5%. The modulation transfer function is 40% at 4 lp/mm and 10%-20% at 8 lp/mm. It is limited most likely by the optical gap between scintillator and sensor and by K-escape quanta. The detective quantum efficiency (DQE) is determined at different beam qualities and dose settings. The maximum DQE(0) is 0.28, while the x-ray absorption with the given thickness and fill factor is 0.57. High Swank noise is suspected to be the reason, mainly caused by optical scatter inside the CsI-filled pores. The results are compared to Monte Carlo simulations of the photon transport inside the pore array structure. In addition, some x-ray images of technical and anatomical phantoms are shown. This work shows that scintillator-filled pore arrays can provide x-ray imaging with high spatial resolution, but are not suitable in their current state for most of the applications in medical imaging, where increasing the x-ray doses cannot be tolerated.

Simon, Matthias; Engel, Klaus Juergen; Menser, Bernd; Badel, Xavier; Linnros, Jan [Philips Research Europe, Weisshausstr. 2, 52080 Aachen (Germany); Royal Institute of Technology, Electrum 229, 16440 Kista (Sweden)

2008-03-15T23:59:59.000Z

287

The constellation X-ray mission  

Science Journals Connector (OSTI)

The Constellation-X mission is a large collecting area X-ray facility emphasizing observations at high spectral resolution (E/?E?300–3000) while covering a broad energy band (0.25–40 keV). This mission will achieve a factor of 100 increased sensitivity over current capabilities and is optimized to observe the effects of extreme gravity close to black holes and test models for the formation of large scale structure in the Universe. It is apart of NASA’s strategic plan for launch towards the end of the first decade of the 21st century.

N. E. White; H. Tananbaum

2001-01-01T23:59:59.000Z

288

13 - X-ray and Neutron Scattering  

Science Journals Connector (OSTI)

Abstract This chapter describes the use of neutrons and X-rays as probes in the study of structural and dynamic properties of metallic materials. Crystalline materials are characterized by their diffraction peaks related to their average crystallographic structure. In real crystals, locally displaced atoms and chemically (or isotopically for neutrons) different species may lead not only to changes of peak shapes and positions, but also to additional (diffuse) scattering between Bragg peak, including scattering around the primary beam (small-angle scattering). All these features can be used to extract information about the state of a sample, its compositional and structural variations on a scale depending on the scattering, in static and time-resolved kinetic studies. Energy-resolved scattering also offers an insight into solid-state dynamics on a microscopic scale. Some of the most important methods will be described and illustrated by instructive examples. The presentation offers a combined view of neutron and X-ray scattering, with the necessary simplifications dictated by space limitations. The special properties of thermal neutrons and of hard X-rays (now widely available at synchrotron radiation sources), their mutual combination, and combinations with other methods, in particular electron microscopy, offer ample opportunity to better understand and control materials properties. After a brief introduction to scattering from real crystals and some general ideas about long-range strains and Bragg peaks, the vicinity of Bragg peaks (displacement scattering at large scattering angles), the scattering far away from Bragg peaks (chemical heterogeneities, short-range order), and, in greater detail, small-angle scattering (which is not sensitive to the extent of crystallinity, but to nanoscale variations of chemical composition and of magnetization, precipitation) will be described, along with classical and more recent applications related to short-range ordering and precipitation in bulk and nanostructured alloys. Some other fields are only briefly addressed (grazing-incidence studies of surfaces, radiography, absorption spectroscopies, coherent X-rays). The final section offers some information on the influence of defects on lattice dynamics and on (slow) diffusive motion in materials.

Gernot Kostorz

2014-01-01T23:59:59.000Z

289

Determination of interfacial roughness using X-ray scattering  

SciTech Connect (OSTI)

Crystal truncation rod (CTR) scattering is shown to be a powerful technique for determining interfacial roughness non-destructively. By measuring the decay of scattering away from a Bragg reflection in the surface direction an rms roughness of the surface or interface can be extracted. The authors obtain rms roughness values with an accuracy of {+-} 0.1 {angstrom}. Sensitivity to lateral length scale roughness ranges from the wavelength of the x-rays to between 1,000--10,000 {angstrom} depending on the instrument function and the specific truncation rod. The influence of different cleans, as well as the thermal oxidation process, on the Si-SiO{sub 2} interface is investigated. A hot water treatment prior to the thermal oxidation is shown to roughen the Si-SiO{sub 2} interface. CTR scattering results also show a smoothing of the interface as a result of the oxidation process even for as little as 60 {angstrom} of thermal oxidation. Comparison between AFM and CTR scattering gives a consistent picture of the relative roughness of the wafers, although the absolute numbers do not agree. The differences in the absolute values can be explained by the lateral roughness scale that the two techniques measure, indicating that it is at periodicities below {approx} 100 {angstrom} that the increased roughness observed by the x-ray is found. Crystal truncation rods are shown to be perpendicular to the surface and not along the crystallographic axes of a miscut crystal. It is shown that for a crystal terminated by a regular step array both an atomistic and a continuum description of CTR scattering give identical results. Furthermore, the atomistic approach is used to show that a diamond cubic surface with a miscut is inherently rough. Even for a small miscut the tilt of the CTR with respect to the crystallographic axes results in complications for measuring the rod intensity. The authors present schemes for determining the exact position of the CTR in reciprocal space and for measuring the miscut of a single crystal. These methods were applied to the measurement of CTR intensities of silicon(001) wafers with miscuts of 0.1 and 4 degrees.

Munkholm, A.

1997-05-01T23:59:59.000Z

290

RYLLA. [X-ray transport code  

SciTech Connect (OSTI)

This paper describes a computer code, RYLLA, which models the deposition of x-rays into thin metal slabs, and transports the resulting photoelectrons, finding the distribution of electrons leaving the slab from both the front and back surfaces. The slab must be homogeneous, but can contain a mixture of up to 5 different elements. Due to the short electron mean free path at low electron energies, RYLLA should be used only for studying thin slabs, roughly < 100 mg/cm/sup 2/ for low Z metals, and < 10 mg/cm/sup 2/ for high Z metals. X-ray energies should be in the range of 1 to 150 keV, as they are deposited only via photoionization and Compton scattering processes. Following photoionization, a hole exists in the electron cloud of the absorbing atom. This fills either by Auger or fluoresence, resulting in lower energy holes which are also filled. Fluoresence photons are transported and absorbed in the same manner as the primary photons, except that they are isotropically produced. Once all photons have been transported and absorbed, and all holes have been filled, a space- and energy-dependent electron source spectrum has been obtained. This is used in a discrete ordinate expansion solution of the 1-D transport equation, which gives the output electron spectra at the two slab surfaces. This paper discusses both the physics and coding of RYLLA. Examples of user input are given, as are some comparisons with other codes.

Hyde, R.A.

1983-06-08T23:59:59.000Z

291

Development of procedures for refurbishing x-ray optics at the Advanced Light Source  

E-Print Network [OSTI]

Development of procedures for refurbishing x-ray optics atpractical and robust procedures for refurbishing x-ray

Yashchuk, Valeriy V.

2013-01-01T23:59:59.000Z

292

Standard design for National Ignition Facility x-ray streak and framing cameras  

SciTech Connect (OSTI)

The x-ray streak camera and x-ray framing camera for the National Ignition Facility were redesigned to improve electromagnetic pulse hardening, protect high voltage circuits from pressure transients, and maximize the use of common parts and operational software. Both instruments use the same PC104 based controller, interface, power supply, charge coupled device camera, protective hermetically sealed housing, and mechanical interfaces. Communication is over fiber optics with identical facility hardware for both instruments. Each has three triggers that can be either fiber optic or coax. High voltage protection consists of a vacuum sensor to enable the high voltage and pulsed microchannel plate phosphor voltage. In the streak camera, the high voltage is removed after the sweep. Both rely on the hardened aluminum box and a custom power supply to reduce electromagnetic pulse/electromagnetic interference (EMP/EMI) getting into the electronics. In addition, the streak camera has an EMP/EMI shield enclosing the front of the streak tube.

Kimbrough, J. R.; Bell, P. M.; Bradley, D. K.; Holder, J. P.; Kalantar, D. K.; MacPhee, A. G.; Telford, S. [Lawrence Livermore National Laboratory, Livermore, California 94551-0808 (United States)

2010-10-15T23:59:59.000Z

293

A flexible, highly stable electrochemical scanning probe microscope for nanoscale studies at the solid-liquid interface  

E-Print Network [OSTI]

low-noise measurements in ambient, in situ, and electrochemical environments. II. DESIGNA flexible, highly stable electrochemical scanning probe microscope for nanoscale studies at the solid-liquid interface, specifically in electrolyte environments. Quantification of system noise limits

Gimzewski, James

294

Photon Sciences | Beamlines | IXS: Inelastic X-ray Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

IXS: Inelastic X-ray Scattering IXS: Inelastic X-ray Scattering Poster | Fact Sheet | Preliminary Design Report Scientific Scope Many hot topics related to the high frequency dynamics of condensed matter require both a narrower and steeper resolution function and access to a broader dynamic range than what are currently available. This represents a sort of "no man's land" that falls right in the dynamic gap lying between the high frequency spectroscopies, such as inelastic x-ray scattering (IXS), and the low frequency ones. New IXS spectrometers with improved energy and momentum resolutions would be required to fill this gap. To achieve this goal, a new x-ray optics concept for both the monochromatization and energy analysis of x-rays will be implemented at the NSLS-II Inelastic X-ray Scattering beamline. This solution exploits the

295

X-Ray Fluorescence (XRF) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Fluorescence (XRF) X-Ray Fluorescence (XRF) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: X-Ray Fluorescence (XRF) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Lab Analysis Techniques Exploration Sub Group: Rock Lab Analysis Parent Exploration Technique: Rock Lab Analysis Information Provided by Technique Lithology: Bulk and trace element analysis of rocks, minerals, and sediments. Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png X-Ray Fluorescence (XRF): X-Ray Fluorescence is a lab-based technique used for bulk chemical analysis of rock, mineral, sediment, and fluid samples. The technique depends on the fundamental principles of x-ray interactions with solid materials, similar

296

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

297

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

298

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

299

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

300

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

Definition: X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) Jump to: navigation, search Dictionary.png X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) is a laboratory-based technique commonly used for identification of crystalline materials and analysis of unit cell dimensions. One of two primary types of XRD analysis (X-ray powder diffraction and single-crystal XRD) is commonly applied to samples to obtain specific information about the crystalline material under investigation. X-ray powder diffraction is widely used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline substances (typically in less than 20 minutes). A pure, finely ground, and homogenized sample is required for determination of the bulk composition. Additional uses include detailed

302

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

303

X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

X-Ray Diffraction (XRD) X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: X-Ray Diffraction (XRD) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Lab Analysis Techniques Exploration Sub Group: Rock Lab Analysis Parent Exploration Technique: Rock Lab Analysis Information Provided by Technique Lithology: Rapid and unambiguous identification of unknown minerals.[1] Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png X-Ray Diffraction (XRD): X-Ray Diffraction (XRD) is a laboratory-based technique commonly used for identification of crystalline materials and analysis of unit cell dimensions. One of two primary types of XRD analysis (X-ray powder diffraction and single-crystal XRD) is commonly applied to samples to

304

Density gradient free electron collisionally excited X-ray laser  

DOE Patents [OSTI]

An operational X-ray laser (30) is provided that amplifies 3p-3s transition X-ray radiation along an approximately linear path. The X-ray laser (30) is driven by a high power optical laser. The driving line focused optical laser beam (32) illuminates a free-standing thin foil (34) that may be associated with a substrate (36) for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the X-ray laser gain medium. The X-ray laser (30) may be driven by more than one optical laser beam (32, 44). The X-ray laser (30) has been successfully demonstrated to function in a series of experimental tests.

Campbell, Edward M. (Pleasanton, CA); Rosen, Mordecai D. (Berkeley, CA)

1989-01-01T23:59:59.000Z

305

Density gradient free electron collisionally excited x-ray laser  

DOE Patents [OSTI]

An operational x-ray laser is provided that amplifies 3p-3s transition x-ray radiation along an approximately linear path. The x-ray laser is driven by a high power optical laser. The driving line focused optical laser beam illuminates a free-standing thin foil that may be associated with a substrate for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the x-ray laser gain medium. The x-ray laser may be driven by more than one optical laser beam. The x-ray laser has been successfully demonstrated to function in a series of experimental tests.

Campbell, E.M.; Rosen, M.D.

1984-11-29T23:59:59.000Z

306

Formation of microbeam using tabletop soft X-ray laser  

Science Journals Connector (OSTI)

An X-ray microprobe with a sub-micron size beam and high intensity can provide X-ray analyses with a remarkable spatial resolution. We have performed focusing of an X-ray laser output into a sub-micron beam for the first time. In our experiment, an X-ray laser of Li-like Al 3d–4f transition at 15.47 nm was delivered from an unstable cavity consisting of a concave mirror and a flat mirror with a square orifice of 100×100 ?m in size. The beam from the orifice was then focused by using a Schwarzschild mirror coated with a Mo/Si multilayer. An X-ray beam size with a diameter of about 0.45 ?m and an estimated photon number of about 2×106 photons per shot was achieved. Such sources could be well suited for the realization of X-ray microprobes.

Tadayuki Ohchi; Naohiro Yamaguchi; Chiemi Fujikawa; Tamio Hara

1999-01-01T23:59:59.000Z

307

Portable X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

Portable X-Ray Diffraction (XRD) Portable X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Technique: Portable X-Ray Diffraction (XRD) Details Activities (0) Areas (0) Regions (0) NEPA(0) Exploration Technique Information Exploration Group: Field Techniques Exploration Sub Group: Data Collection and Mapping Parent Exploration Technique: Data Collection and Mapping Information Provided by Technique Lithology: Rapid and unambiguous identification of unknown minerals.[1] Stratigraphic/Structural: Hydrological: Thermal: Dictionary.png Portable X-Ray Diffraction (XRD): Portable X-Ray Diffraction (XRD) is a field-based technique that can be used for identification of crystalline materials and analysis of unit cell dimensions. Portable XRD analysis is similar to X-ray powder diffraction,

308

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

309

X-ray Pinhole Camera Measurements  

SciTech Connect (OSTI)

The rod pinch diode is made up of a cathode plate and a small diameter anode rod that extends through the cathode hole. The anode is charged positively. The rod tip is made of a high-z material which is chosen for its bremsstrahlung efficiency. When the diode is pulsed it produces an intense x-ray source used for pulsed radiography. The baseline or reference diode consists of a 0.75 mm diameter Tungsten (W) tapered anode rod which extends 10 mm through a 9 mm diameter 3 mm thick aluminum (Al) aperture. The majority of the current in the electron beam is created on the edges of the cathode aperture and when properly configured, the electrons will self insulate, travel down the extension of the rod, and pinch onto the tip of the rod. In this presentation, performance of hybrid diodes will be compared with the baseline diode.

Nelson, D. S. [NSTec; Berninger, M. J. [NSTec; Flores, P. A. [NSTec; Good, D. E. [NSTec; Henderson, D. J. [NSTec; Hogge, K. W. [NSTec; Huber, S. R. [NSTec; Lutz, S. S. [NSTec; Mitchell, S. E. [NSTec; Howe, R. A. [NSTec; Mitton, C. V. [NSTec; Molina, I. [NSTec; Bozman, D. R. [SNL; Cordova, S. R. [SNL; Mitchell, D. R. [SNL; Oliver, B. V. [SNL; Ormond, E. C. [SNL

2013-06-20T23:59:59.000Z

310

Gray scale x-ray mask  

DOE Patents [OSTI]

The present invention describes a method for fabricating an embossing tool or an x-ray mask tool, providing microstructures that smoothly vary in height from point-to-point in etched substrates, i.e., structure which can vary in all three dimensions. The process uses a lithographic technique to transfer an image pattern in the surface of a silicon wafer by exposing and developing the resist and then etching the silicon substrate. Importantly, the photoresist is variably exposed so that when developed some of the resist layer remains. The remaining undeveloped resist acts as an etchant barrier to the reactive plasma used to etch the silicon substrate and therefore provides the ability etch structures of variable depths.

Morales, Alfredo M. (Livermore, CA); Gonzales, Marcela (Seattle, WA)

2006-03-07T23:59:59.000Z

311

Nonlinear optics with focused x-ray lasers  

SciTech Connect (OSTI)

We have investigated the possibility of focusing x-ray lasers with the use of multilayered mirrors or zone plates. The results indicate that x-ray intensities as high as 10{sup 14} W/cm{sup 2} can be achieved by focusing saturated Ne-like x-ray lasers. These intensities should be adequate for studying nonlinear optical phenomena. 9 refs., 2 figs.

DaSilva, L.B.; Muendel, M.H.; Falcone, R.W.; Fields, D.J.; Kortright, J.B.; MacGowan, B.J.; Matthews, D.L.; Mrowka, S.; Shimkaveg, G.M.; Trebes, J.E.

1990-12-12T23:59:59.000Z

312

Process and device for x-ray system quality assurance  

SciTech Connect (OSTI)

This invention relates to medical radiography test systems, and more particularly to a method and apparatus for providing evaluation of a medical or dental x-ray system consisting of x-ray generator, film and processor on a daily basis and to thereby assure the production of useful radiographs from the system with no need to repeat patient exposure because of problems with the x-ray system.

Van Pelt, W.F.; Peterson, R.W.

1982-11-10T23:59:59.000Z

313

The first X-ray diffraction measurements on Mars  

Science Journals Connector (OSTI)

The X-ray diffraction/X-ray fluorescence instrument CheMin on the Curiosity rover is a shoebox-sized device using transmission geometry and an energy-discriminating CCD detector. The instrument has returned the first X-ray diffraction data for soil and drilled samples from Mars outcrops, revealing a suite of primary basaltic minerals, amorphous components and varied hydrous alteration products including phyllosilicates.

Bish, D.

2014-10-21T23:59:59.000Z

314

On X-Ray Waveguiding in Nanochannels: Channeling Formalism  

E-Print Network [OSTI]

The question on X-ray extreme focusing (smallest reachable spot size) brings us to the idea for using the wave features of X-ray propagation in media. As known, wave features are revealed at propagation in ultra-narrow collimators as well as at glancing reflection from smooth flat and/or strongly curved surfaces. All these phenomena can be described within the general formalism of X-ray channeling.

S. B. Dabagov

2006-11-20T23:59:59.000Z

315

THE GEODESIC X-RAY TRANSFORM WITH FOLD CAUSTICS The ...  

E-Print Network [OSTI]

Aug 28, 2012 ... THE GEODESIC X-RAY TRANSFORM WITH FOLD CAUSTICS. PLAMEN STEFANOV AND GUNTHER UHLMANN. ABSTRACT. We give a ...

2012-08-28T23:59:59.000Z

316

Inelastic X-ray and Nuclear Resonant Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

... Search About User Information News & Events Science & Education Beamlines Divisions Argonne Home > Advanced Photon Source > Inelastic X-ray and Nuclear Resonant Scattering...

317

Advances in X-Ray Diagnostics of Diesel Fuel Sprays  

Broader source: Energy.gov [DOE]

Recent advances in high-speed X-ray imaging has shown several distinct behaviors of commercial fuel injectors that cannot be seen with more conventional techniques.

318

New intraoral x-ray fluorographic imaging for dentistry  

SciTech Connect (OSTI)

A new dental x-ray fluorographic unit has been developed. This unit is composed of small intraoral x-ray tube, a compact x-ray image intensifier, and a high-resolution TV system. The purposes for developing this equipment were to (1) directly observe the tooth during endodontic procedures and (2) reduce x-ray exposure to the patient and the dentist. The radiation exposure can be reduced to about 1/600 the exposure used with conventional dental film. In clinical trials, a satisfactory fluorographic dental image for endodontic treatment was obtained with this new device.

Higashi, T.; Osada, T.; Aoyama, W.; Iguchi, M.; Suzuki, S.; Kanno, M.; Moriya, K.; Yoshimura, M.; Tusuda, M.

1983-06-01T23:59:59.000Z

319

Normal incidence x-ray mirror for chemical microanalysis  

DOE Patents [OSTI]

An x-ray mirror for both electron column instruments and micro x-ray fluorescence instruments for making chemical, microanalysis comprises a non-planar mirror having, for example, a spherical reflecting surface for x-rays comprised of a predetermined number of alternating layers of high atomic number material and low atomic number material contiguously formed on a substrate and whose layers have a thickness which is a multiple of the wavelength being reflected. For electron column instruments, the wavelengths of interest lie above 1.5nm, while for x-ray fluorescence instruments, the range of interest is below 0.2nm. 4 figs.

Carr, M.J.; Romig, A.D. Jr.

1987-08-05T23:59:59.000Z

320

Self-terminating diffraction gates femtosecond X-ray nanocrystallograp...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Self-terminating diffraction gates femtosecond X-ray nanocrystallography measurements Authors: Barty, A., Caleman, C., Aquila, A., Timneanu, N., Lomb, L., White, T. A., Andreasson,...

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

X-ray Diffuse Scattering Measurements of Nucleation Dynamics...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-ray Diffuse Scattering Measurements of Nucleation Dynamics at Femtosecond Resolution Real-time measurement and control of the non-equilibrium properties of materials represents...

322

XRMS: X-Ray Spectroscopy of Magnetic Solids  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

XRMS: X-Ray Spectroscopy of Magnetic Solids October 22-23, 2011 SLAC National Accelerator Laboratory, Menlo Park, CA More information...

323

X-ray absorption fine structure and magnetization characterization...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

characterization of the metallic Co component in Co-doped ZnO thin films . X-ray absorption fine structure and magnetization characterization of the metallic Co...

324

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering Resonant Soft X-Ray Scattering of Tri-Block Copolymers Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Wednesday, 30 May 2012 00:00 In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

325

X-ray laser system, x-ray laser and method  

DOE Patents [OSTI]

Disclosed is an x-ray laser system comprising a laser containing generating means for emitting short wave length radiation, and means external to said laser for energizing said generating means, wherein when the laser is in an operative mode emitting radiation, the radiation has a transverse coherence length to width ratio of from about 0.05 to 1. Also disclosed is a method of adjusting the parameters of the laser to achieve the desired coherence length to laser width ratio.

London, Richard A. (Oakland, CA); Rosen, Mordecai D. (Berkeley, CA); Strauss, Moshe (Omer, IL)

1992-01-01T23:59:59.000Z

326

Constraints on jet X-ray emission in low/hard state X-ray binaries  

E-Print Network [OSTI]

We show that the combination of the similarities between the X-ray properties of low luminosity accreting black holes and accreting neutron stars, combined with the differences in their radio properties argues that the X-rays from these systems are unlikely to be formed in the relativistic jets. Specifically, the spectra of extreme island state neutron stars and low/hard state black holes are known to be indistinguishable, while the power spectra from these systems are known to show only minor differences beyond what would be expected from scaling the characteristic variability frequencies by the mass of the compact object. The spectral and temporal similarities thus imply a common emission mechanism that has only minor deviations from having all key parameters scaling linearly with the mass of the compact object, while we show that this is inconsistent with the observations that the radio powers of neutron stars are typically about 30 times lower than those of black holes at the same X-ray luminosity. We also show that an abrupt luminosity change would be expected when a system makes a spectral state transition from a radiatively inefficient jet dominated accretion flow to a thin disk dominated flow, but that such a change is not seen.

Thomas J. Maccarone

2005-03-31T23:59:59.000Z

327

Isotropic star in low-mass X-ray binaries and X-ray pulsars  

E-Print Network [OSTI]

We present a model for compact stars in the low mass X-ray binaries(LMXBs) and X-ray pulsars using a metric given by John J. Matese and Patrick G. Whitman \\citep{Matese and Whitman1980}. Here the field equations are reduced to a system of two algebraic equations considering the isotropic pressure. Compact star candidates 4U 1820-30(radius=10km) in LMXBs, and Her X-1(radius=7.7km), SAX J 1808.4-3658(SS1)(radius=7.07km) and SAX J 1808.4-3658(SS2)(radius=6.35km) in X-ray pulsars satisfy all the energy conditions, TOV-equation and stability condition. From our model, we have derived mass($M$), central density($\\rho_{0}$), suface density($\\rho_{b}$), central pressure($p_{0}$), surface pressure($p_{b}$) and surface red-shift($Z_{s}$) of the above mentioned stars, which are very much consistant with the observed/reported datas\\citep{N. K. Glendenning1997,Gondek2000}. We have also observe the adiabatic index($\\gamma$>4/3) of the above steller objects.

Mehedi Kalam; Sk. Monowar Hossein; Sajahan Molla

2014-10-01T23:59:59.000Z

328

Femtosecond x-ray absorption spectroscopy with hard x-ray free electron laser  

SciTech Connect (OSTI)

We have developed a method of dispersive x-ray absorption spectroscopy with a hard x-ray free electron laser (XFEL), generated by a self-amplified spontaneous emission (SASE) mechanism. A transmission grating was utilized for splitting SASE-XFEL light, which has a relatively large bandwidth (?E/E ? 5 × 10{sup ?3}), into several branches. Two primary split beams were introduced into a dispersive spectrometer for measuring signal and reference spectra simultaneously. After normalization, we obtained a Zn K-edge absorption spectrum with a photon-energy range of 210 eV, which is in excellent agreement with that measured by a conventional wavelength-scanning method. From the analysis of the difference spectra, the noise ratio was evaluated to be ?3 × 10{sup ?3}, which is sufficiently small to trace minute changes in transient spectra induced by an ultrafast optical laser. This scheme enables us to perform single-shot, high-accuracy x-ray absorption spectroscopy with femtosecond time resolution.

Katayama, Tetsuo; Togashi, Tadashi; Tono, Kensuke; Kameshima, Takashi [Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan)] [Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198 (Japan); Inubushi, Yuichi; Sato, Takahiro; Hatsui, Takaki; Yabashi, Makina [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan)] [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5148 (Japan); Obara, Yuki; Misawa, Kazuhiko [Department of Applied Physics, Tokyo University of Agriculture and Technology, 2-24-16 Naka-cho, Koganei, Tokyo 184-8588 (Japan)] [Department of Applied Physics, Tokyo University of Agriculture and Technology, 2-24-16 Naka-cho, Koganei, Tokyo 184-8588 (Japan); Bhattacharya, Atanu; Kurahashi, Naoya [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan)] [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan); Ogi, Yoshihiro [Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198 (Japan)] [Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198 (Japan); Suzuki, Toshinori [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan) [Department of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa-Oiwakecho, Sakyo-ku, Kyoto 606-8502 (Japan); Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198 (Japan)

2013-09-23T23:59:59.000Z

329

Burning plasmas with ultrashort soft-x-ray flashing  

SciTech Connect (OSTI)

Fast ignition with narrow-band coherent x-ray pulses has been revisited for cryogenic deuterium-tritium (DT) plasma conditions achieved on the OMEGA Laser System. In contrast to using hard-x-rays (hv = 3-6 keV) proposed in the original x-ray fast-ignition proposal, we find that soft-x-ray sources with hv Almost-Equal-To 500 eV photons can be suitable for igniting the dense DT-plasmas achieved on OMEGA. Two-dimensional radiation-hydrodynamics simulations have identified the break-even conditions for realizing such a 'hybrid' ignition scheme (direct-drive compression with soft-x-ray heating) with 50-{mu}m-offset targets: {approx}10 ps soft-x-ray pulse (hv Almost-Equal-To 500 eV) with a total energy of 500-1000 J to be focused into a 10 {mu}m spot-size. A variety of x-ray pulse parameters have also been investigated for optimization. It is noted that an order of magnitude increase in neutron yield has been predicted even with x-ray energy as low as {approx}50 J. Scaling this idea to a 1 MJ large-scale target, a gain above {approx}30 can be reached with the same soft-x-ray pulse at 1.65 kJ energy. Even though such energetic x-ray sources do not currently exist, we hope that the proposed ignition scheme may stimulate efforts on generating powerful soft-x-ray sources in the near future.

Hu, S. X.; Goncharov, V. N.; Skupsky, S. [Laboratory for Laser Energetics, University of Rochester, 250 East River Road, Rochester, New York 14623-1299 (United States)

2012-07-15T23:59:59.000Z

330

Charge transfer effects of ions at the liquid water/vapor interface  

SciTech Connect (OSTI)

Charge transfer (CT), the movement of small amounts of electron density between non-bonded pairs, has been suggested as a driving force for a variety of physical processes. Herein, we examine the effect of CT on ion adsorption to the water liquid-vapor interface. Using a CT force field for molecular dynamics, we construct a potential of mean force (PMF) for Na{sup +}, K{sup +}, Cl{sup ?}, and I{sup ?}. The PMFs were produced with respect to an average interface and an instantaneous interface. An analysis of the PMF relative to the instantaneous surface reveals that the area in which the anions experience a free energy minimum is quite narrow, and the cations feel a steeply repulsive free energy near the interface. CT is seen to have only minor effects on the overall free energy profiles. However, the long-ranged effects of ions are highlighted by the CT model. Due to CT, the water molecules at the surface become charged, even when the ion is over 15 Å away from the surface.

Soniat, Marielle; Rick, Steven W., E-mail: srick@uno.edu [Department of Chemistry, University of New Orleans, New Orleans, Louisiana 70148 (United States)

2014-05-14T23:59:59.000Z

331

Characterization of GaSb/GaAs interfacial misfit arrays using x-ray diffraction  

Science Journals Connector (OSTI)

We report a nondestructive large-area method to characterize dislocation formation at a highly lattice-mismatched interface. The analysis is based on x-ray diffraction and reciprocal space mapping using a standard lab-based diffractometer. We use this technique to identify and analyze a two-dimensional array of 90° misfit dislocations at a GaSb/GaAs interface. The full width at half maximum of the GaSb 004 reciprocal lattice point is shown to decrease with increasing GaSb epilayer thickness as expected from theoretical models. Based on these measurements the variation in the spatial dislocation frequency is calculated to be 1%.

Charles J. Reyner; Jin Wang; Kalyan Nunna; Andrew Lin; Baolai Liang; Mark S. Goorsky; D. L. Huffaker

2011-01-01T23:59:59.000Z

332

Impact of nuclear irradiation on helium bubble nucleation at interfaces in liquid metals coupled to permeation through stainless steels  

E-Print Network [OSTI]

The impact of nucleating gas bubbles in the form of a dispersed gas phase on hydrogen isotope permeation at interfaces between liquid metals, like LLE, and structural materials, like stainless steel, has been studied. Liquid metal to structural material interfaces involving surfaces, may lower the nucleation barrier promoting bubble nucleation at active sites. Hence, hydrogen isotope absorption into gas bubbles modelling and control at interfaces may have a capital importance regarding design, operation and safety. He bubbles as a permeation barrier principle is analysed showing a significant impact on hydrogen isotope permeation, which may have a significant effect on liquid metal systems, e.g., tritium extraction systems. Liquid metals like LLE under nuclear irradiation in, e.g., breeding blankets of a nuclear fusion reactor would generate tritium which is to be extracted and recirculated as fuel. At the same time that tritium is bred, helium is also generated and may precipitate in the form of nano bubbles...

Fradera, Jorge

2013-01-01T23:59:59.000Z

333

Combined energy dispersive EXAFS and x?ray diffraction  

Science Journals Connector (OSTI)

An in situ experiment to measure both x?ray absorption spectroscopy and x?ray diffraction of aurichalcite is described. The experiment uses position sensitive detectors to enable both data sets to be collected while the sample is slowly decomposed in air and then reduced in hydrogen. ?

A. J. Dent; M. P. Wells; R. C. Farrow; C. A. Ramsdale; G. E. Derbyshire; G. N. Greaves; J. W. Couves; J. M. Thomas

1992-01-01T23:59:59.000Z

334

Fresnel and refractive lenses for X-rays  

Science Journals Connector (OSTI)

We present a Gaussian beam analysis of X-ray refractive and Fresnel lenses. The X-ray refractive lens is featured by an intrinsic soft (Gaussian) aperture due to strong absorption of X-rays by materials. We defined a parameter N0, the critical Fresnel number (CFN), to describe this optical property. The values of N0 for all practical materials are below 1000 for photon energies exceeding 30 eV, still lower for high-Z materials. The maximum effective Fresnel number of a lens is determined by its material to be 2N0 and its maximum enhancement of X-ray intensity is limited to (2?N0)2, independent of its shape. We found that the refractive lens is likely to be useful for manipulating nearly diffraction limited beam in the hard X-ray region and its application is severely restricted by available fabrication capabilities today. X-ray Fresnel lenses, both in cylindrical and linear forms, are proposed as superior focusing elements for hard X-rays. Their high efficiency, up to 100% in optimal construction, will enable us to manipulate beams with multiple lenses and obtain higher performance optics. Their design and fabrication are discussed in reference to those of X-ray Fresnel zone plates and micro Fresnel lenses for optoelectronics.

B.X. Yang

1993-01-01T23:59:59.000Z

335

X-ray attenuation properties of stainless steel (u)  

SciTech Connect (OSTI)

Stainless steel vessels are used to enclose solid materials for studying x-ray radiolysis that involves gas release from the materials. Commercially available stainless steel components are easily adapted to form a static or a dynamic condition to monitor the gas evolved from the solid materials during and after the x-ray irradiation. Experimental data published on the x-ray attenuation properties of stainless steel, however, are very scarce, especially over a wide range of x-ray energies. The objective of this work was to obtain experimental data that will be used to determine how a poly-energetic x-ray beam is attenuated by the stainless steel container wall. The data will also be used in conjunction with MCNP (Monte Carlos Nuclear Particle) modeling to develop an accurate method for determining energy absorbed in known solid samples contained in stainless steel vessels. In this study, experiments to measure the attenuation properties of stainless steel were performed for a range of bremsstrahlung x-ray beams with a maximum energy ranging from 150 keV to 10 MeV. Bremsstrahlung x-ray beams of these energies are commonly used in radiography of engineering and weapon components. The weapon surveillance community has a great interest in understanding how the x-rays in radiography affect short-term and long-term properties of weapon materials.

Wang, Lily L [Los Alamos National Laboratory; Berry, Phillip C [Los Alamos National Laboratory

2009-01-01T23:59:59.000Z

336

Shining Soft X-rays on Magnetic Structures  

Science Journals Connector (OSTI)

...2) demonstrate the power of x-ray magneto-optics in a synchroton study of single crystalline FePd layers, which provides...2) demonstrate the power of x-ray magneto-optics in a synchroton study of single crystalline FePd layers, which provides detailed...

Ulrich Hillebrecht

1999-06-25T23:59:59.000Z

337

Human genome sequencing with direct x-ray holographic imaging  

SciTech Connect (OSTI)

Direct holographic imaging of biological materials is widely applicable to the study of the structure, properties and action of genetic material. This particular application involves the sequencing of the human genome where prospective genomic imaging technology is composed of three subtechnologies, name an x-ray holographic camera, suitable chemistry and enzymology for the preparation of tagged DNA samples, and the illuminator in the form of an x-ray laser. We report appropriate x-ray camera, embodied by the instrument developed by MCR, is available and that suitable chemical and enzymatic procedures exist for the preparation of the necessary tagged DNA strands. Concerning the future development of the x-ray illuminator. We find that a practical small scale x-ray light source is indeed feasible. This outcome requires the use of unconventional physical processes in order to achieve the necessary power-compression in the amplifying medium. The understanding of these new physical mechanisms is developing rapidly. Importantly, although the x-ray source does not currently exist, the understanding of these new physical mechanisms is developing rapidly and the research has established the basic scaling laws that will determine the properties of the x-ray illuminator. When this x-ray source becomes available, an extremely rapid and cost effective instrument for 3-D imaging of biological materials can be applied to a wide range of biological structural assays, including the base-pair sequencing of the human genome and many questions regarding its higher levels of organization.

Rhodes, C.K.

1993-06-08T23:59:59.000Z

338

Twelfth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Twelfth National School on Neutron and X-ray Scattering June 12 � June 26, 2010 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

339

National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

National School on Neutron and X-ray Scattering May 30 � June 13, 2009 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

340

National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

15th National School on Neutron and X-ray Scattering August 10 - 24, 2013 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
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341

Fourteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Fourteenth National School on Neutron and X-ray Scattering August 12 - 25, 2012 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

Pennycook, Steve

342

Thirteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Thirteenth National School on Neutron and X-ray Scattering June 11 ­ June 25, 2011 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

343

Neutron and X-ray Scattering Study of Magnetic Manganites  

E-Print Network [OSTI]

Neutron and X-ray Scattering Study of Magnetic Manganites Graeme Eoin Johnstone A Thesis submitted are performed using a variety of neutron scattering and x-ray scattering techniques. The electronic ground for analysing the results of the polarised neutron scattering experiment. There are a large number of people who

Boothroyd, Andrew

344

Sixteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Sixteenth National School on Neutron and X-ray Scattering June 14-28, 2014 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major's Neutron Scattering Science Division. Scientific Directors: Suzanne G.E. te Velthuis, Esen Ercan Alp

Pennycook, Steve

345

Tenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Tenth National School on Neutron and X-ray Scattering September 24 - October 11, 2008 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

346

X-ray spectra transmitted through Compton-thick absorbers  

E-Print Network [OSTI]

X-ray spectra transmitted through matter which is optically thick to Compton scattering are computed by means of Monte Carlo simulations. Applications to the BeppoSAX data of the Seyfert 2 galaxy in Circinus, and to the spectral modeling of the Cosmic X-ray Background, are discussed.

Giorgio Matt; Fulvio Pompilio; Fabio La Franca

1999-04-24T23:59:59.000Z

347

Laser Copper Plasma X-ray Source Debris Characterization  

E-Print Network [OSTI]

Laser Copper Plasma X-ray Source Debris Characterization A Thesis Presented by David Hurley 3, 2007 Vice President for Research and Dean of Graduate studies #12;Abstract Laser copper plasma for x-ray lithography. Copper debris in the form of vapor, ions, dust, and high-speed particles

Huston, Dryver R.

348

Millisecond oscillations during thermonuclear X-ray bursts  

E-Print Network [OSTI]

I analyze 68 oscillation trains detected in a search of 159 thermonuclear bursts from eight neutron star X-ray binaries observed with the Rossi X-ray Timing Explorer. I use all data that were public as of September 2001. ...

Muno, Michael Patrick, 1975-

2002-01-01T23:59:59.000Z

349

X rays following the alpha decay of Pa231  

Science Journals Connector (OSTI)

More detailed information is presented concerning the L and K x-ray spectra due to internal conversion of the electromagnetic transitions following the ? decay of Pa231. Some of the difficulties discussed in Ref. 1 are clarified by the new results.[RADIOACTIVITY Pa231; measured L and K Ac x-ray components, ?? and ?XL coin Ac227 deduced levels, ICC.

A. G. de Pinho; L. T. Auler; A. G. da Silva

1974-05-01T23:59:59.000Z

350

Improving liquid chromatography-mass spectrometry sensitivity using a subambient pressure ionization with nanoelectrospray (SPIN) interface  

SciTech Connect (OSTI)

In this work the Subambient Pressure Ionization with Nanoelectrospray (SPIN) ion source and interface which operates at ~15-30 Torr is demonstrated to be compatible with gradient reversed-phase liquid chromatography-MS applications, exemplified here with the analysis of complex samples (a protein tryptic digest and a whole cell lysate). A low liquid chromatographic flow rate (100-400 nL/min) allowed stable electrospray to be established while avoiding electrical breakdown. Efforts to increase the operating pressure of the SPIN source relative to previously reported designs prevented solvent freezing and enhanced charged cluster/droplet desolvation. A 5-12-fold improvement in sensitivity relative to a conventional atmospheric pressure nanoelectrospray ionization (ESI) source was obtained for detected peptides.

Tang, Keqi; Page, Jason S.; Marginean, Ioan; Kelly, Ryan T.; Smith, Richard D.

2011-04-22T23:59:59.000Z

351

Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Techniques Wednesday, September 5, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Gang Chen Seminar: Structures at atomic scales are traditionally determined through X-ray crystallography that amplifies scattering intensities by introducing spatial periodicity. For amorphous materials and many macromolecules, such as viruses, proteins and biofilms, it is hard to determine structures due to their incapability to crystallize or change of configuration during crystallization. In this talk, I will present the application of X-ray reflectivity and a newly developed fluctuation X-ray scattering technique to study the structures of lipid membranes and randomly oriented nanoparticles. Three different types of domain registrations occurring with

352

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Refinement Friday, September 28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray absorption spectroscopy has become an important tool in understanding the electronic structure of materials. Resonant absorption edges in the soft x-ray regime are especially interesting as they allow the study of the lighter elements, such as in organic or organo-metallic substances, as well as important L-edges of the 3d transition metals important in magnetic and oxide systems. Measurements of soft x-ray absorption spectra are inherently surface sensitive, and are plagued by issues such as extinction (in electron yield measurements) or self absorption (in fluorescence yield

353

Incoherent x-ray scattering in single molecule imaging  

E-Print Network [OSTI]

Imaging of the structure of single proteins or other biomolecules with atomic resolution would be enormously beneficial to structural biology. X-ray free-electron lasers generate highly intense and ultrashort x-ray pulses, providing a route towards imaging of single molecules with atomic resolution. The information on molecular structure is encoded in the coherent x-ray scattering signal. In contrast to crystallography there are no Bragg reflections in single molecule imaging, which means the coherent scattering is not enhanced. Consequently, a background signal from incoherent scattering deteriorates the quality of the coherent scattering signal. This background signal cannot be easily eliminated because the spectrum of incoherently scattered photons cannot be resolved by usual scattering detectors. We present an ab initio study of incoherent x-ray scattering from individual carbon atoms, including the electronic radiation damage caused by a highly intense x-ray pulse. We find that the coherent scattering pa...

Slowik, Jan Malte; Dixit, Gopal; Jurek, Zoltan; Santra, Robin

2014-01-01T23:59:59.000Z

354

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Unexpected Angular Dependence of Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Wednesday, 29 August 2007 00:00 Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and x-ray polarization, but their orientation relative to the crystallographic axes must be taken into account for accurate interpretation of XMLD data. Magnetism and X Rays

355

X-ray Emission from Massive StarsX-ray Emission from Massive Stars David CohenDavid Cohen  

E-Print Network [OSTI]

X-ray Emission from Massive StarsX-ray Emission from Massive Stars David CohenDavid Cohen/s)Velocity (km/s) #12;absorption emission emission occulted emission emission UV telescope side side front back #12;absorption emission emission occulted emission emission UV telescope side side front back #12;The

Cohen, David

356

In R&D, Super X-rays Mark Many Spots  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

A New Gas Loading System for Diamond Anvil Cells at GSECARS A New Gas Loading System for Diamond Anvil Cells at GSECARS Sidorowicz Named "Supervisor of the Year" SESS 2007: The School for Environmental Sciences with Synchrotrons Art and Science A Breakthrough in Interface Science APS News Archives: 2012 | 2011 | 2010 | 2009 2008 | 2007 | 2006 | 2005 2004 | 2003 | 2002 | 2001 2000 Subscribe to APS News rss feed In R&D, Super X-rays Mark Many Spots MARCH 11, 2008 Bookmark and Share Research and Design Magazine "The Advanced Photon Source (APS) at the U.S. Dept. of Energy's Argonne National Laboratory has been kept busy of late." That's the first sentence of R&D Magazine's recent overview of research results from the APS. The article highlights "a new ultrafast synchrotron x-ray full-field phase contrast imaging technique and used it to reveal

357

Method and apparatus for digitally based high speed x-ray spectrometer  

DOE Patents [OSTI]

A high speed, digitally based, signal processing system which accepts input data from a detector-preamplifier and produces a spectral analysis of the x-rays illuminating the detector. The system achieves high throughputs at low cost by dividing the required digital processing steps between a ``hardwired`` processor implemented in combinatorial digital logic, which detects the presence of the x-ray signals in the digitized data stream and extracts filtered estimates of their amplitudes, and a programmable digital signal processing computer, which refines the filtered amplitude estimates and bins them to produce the desired spectral analysis. One set of algorithms allow this hybrid system to match the resolution of analog systems while operating at much higher data rates. A second set of algorithms implemented in the processor allow the system to be self calibrating as well. The same processor also handles the interface to an external control computer. 19 figs.

Warburton, W.K.; Hubbard, B.

1997-11-04T23:59:59.000Z

358

Method and apparatus for digitally based high speed x-ray spectrometer  

DOE Patents [OSTI]

A high speed, digitally based, signal processing system which accepts input data from a detector-preamplifier and produces a spectral analysis of the x-rays illuminating the detector. The system achieves high throughputs at low cost by dividing the required digital processing steps between a "hardwired" processor implemented in combinatorial digital logic, which detects the presence of the x-ray signals in the digitized data stream and extracts filtered estimates of their amplitudes, and a programmable digital signal processing computer, which refines the filtered amplitude estimates and bins them to produce the desired spectral analysis. One set of algorithms allow this hybrid system to match the resolution of analog systems while operating at much higher data rates. A second set of algorithms implemented in the processor allow the system to be self calibrating as well. The same processor also handles the interface to an external control computer.

Warburton, William K. (1300 Mills St., Menlo Park, CA 94025); Hubbard, Bradley (Santa Cruz, CA)

1997-01-01T23:59:59.000Z

359

SURFACE SEGREGATION STUDIES OF SOFC CATHODES: COMBINING SOFT X-RAYS AND ELECTROCHEMICAL IMPEDENCE SPECTROSCOPY  

SciTech Connect (OSTI)

A system to grow heteroepitaxial thin-films of solid oxide fuel cell (SOFC) cathodes on single crystal substrates was developed. The cathode composition investigated was 20% strontium-doped lanthanum manganite (LSM) grown by pulsed laser deposition (PLD) on single crystal (111) yttria-stabilized zirconia (YSZ) substrates. By combining electrochemical impedance spectroscopy (EIS) with x-ray photoemission spectroscopy (XPS) and x-ray absorption spectroscopy XAS measurements, we conclude that electrically driven cation migration away from the two-phase gas-cathode interface results in improved electrochemical performance. Our results provide support to the premise that the removal of surface passivating phases containing Sr2+ and Mn2+, which readily form at elevated temperatures even in O2 atmospheric pressures, is responsible for the improved cathodic performance upon application of a bias.

Miara, Lincoln J.; Piper, L.F.J.; Davis, Jacob N.; Saraf, Laxmikant V.; Kaspar, Tiffany C.; Basu, Soumendra; Smith, K. E.; Pal, Uday B.; Gopalan, Srikanth

2010-12-01T23:59:59.000Z

360

The X-Ray Microcalorimeter Spectrometer for the International X-Ray Observatory  

SciTech Connect (OSTI)

The International X-Ray Observatory (IXO) is under formulation by NASA, ESA and JAXA for deployment in 2022. IXO emerged over the last 18 months as the NASA Constellation-X and ESA/JAXA X-Ray Evolving Universe Spectrometer (XEUS) missions were combined. The driving performance requirements for the X-Ray Microcalorimeter Spectrometer (XMS) are a spectral resolution of 2.5 eV over the central 2'x2' in the 0.3-7.0 keV band, and 10 eV to the edge of the 5'x5' field of view (FOV). The XMS is now based on a microcalorimeter array of Transition-Edge Sensor (TES) thermometers with Au/Bi absorbers and a SQUID MUX readout. One of the concepts studied as part of the mission formulation has a core 40x40 array corresponding to a 2'x2' FOV with 3'' pixels surrounded by an outer, annular 52x52 array of 6'' pixels that extends the field of view to 5.4'x5.4' with better than 10 eV resolution. There are several options for implementing the readout and cooling system of the XMS under study in the US, Europe and Japan. The ADR system will have from two to five stages depending on the performance of the cryocooler. Mechanical coolers with sufficient cooling power at 4K are available now, and {approx}2K coolers are under development. In this paper we give an overview of the XMS instrument, and some of the tradeoffs to be addressed for this observatory instrument.

Kelley, R. L.; Bandler, S. R.; Kilbourne, C. A.; Porter, F. S.; Shirron, P.; Smith, S. J.; Whitehouse, P. [NASA/Goddard Space Flight Center, Greenbelt, MD (United States); Doriese, W. B.; Irwin, K. [National Institute of Standards and Technology, Boulder, CO (United States); Ezoe, Y.; Ishisaki, Y.; Ohashi, T. [Tokyo Metropolitan University, Hachioji, Tokyo (Japan); Fujimoto, R.; Sato, K. [Faculty of Mathematics and Physics, Kanazawa University, Kanazawa (Japan); Gottardi, L.; Hartog, R. den; Herder, J.-W. den; Hoevers, H.; Korte, P. de; Kuur, J. van der [SRON Netherlands Institute for Space Research, Utrecht (Netherlands)] (and others)

2009-12-16T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

SOFT X-RAY EMISSIONS FROM PLANETS, MOONS, AND COMETS A. Bhardwaj(1)  

E-Print Network [OSTI]

SOFT X-RAY EMISSIONS FROM PLANETS, MOONS, AND COMETS A. Bhardwaj(1) , G. R. Gladstone(2) , R. F to radiate in the soft x-ray energy ( the generation of soft x-rays from these objects, whereas in the hard x-ray energy range (>10 keV) x-rays mainly

Johnson, Robert E.

362

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate  

E-Print Network [OSTI]

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate an effect of a partially reversible x-ray-induced increase of diffuse x-ray scattering in both congruent been attributed to x-ray-induced decay of the ferroelectric phase at room temperature. The x-ray

Byer, Robert L.

363

A Hard X-ray View of Accreting X-ray Binary Pulsars  

E-Print Network [OSTI]

The study of the hard (E>10 keV) energy spectra of X-ray binary pulsars can give a wealth of information on the physical processes that occur close to the neutron star surface. Extreme matter regimes are probed, and precious information on how matter and radiation behave and interact in critical conditions can be obtained. We will give an overview on the most recent results obtained by RXTE and BeppoSAX on this class of objects, in order to pass the baton onto just launched experiments, like INTEGRAL, or soon to be launched, like AGILE and ASTRO-E2.

Mauro Orlandini

2004-02-26T23:59:59.000Z

364

Apparatus for generating x-ray holograms  

DOE Patents [OSTI]

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced.

Rhodes, Charles K. (Chicago, IL); Boyer, Keith (Los Alamos, NM); Solem, Johndale C. (Los Alamos, NM); Haddad, Waleed S. (Chicago, IL)

1990-01-01T23:59:59.000Z

365

Apparatus for generating x-ray holograms  

DOE Patents [OSTI]

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced. 7 figs.

Rhodes, C.K.; Boyer, K.; Solem, J.C.; Haddad, W.S.

1990-09-11T23:59:59.000Z

366

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations imposed by lens-based optical systems. Researchers from Stony Brook University, in collaboration with scientists at the ALS and Cornell University, have taken a large step in this direction by using a lensless x-ray diffraction microscope to image a freeze-dried yeast cell to better than 30-nm resolution. Images were made at several angular orientations of the cell.

367

Femtosecond Time-Delay X-ray Holography  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Time-Delay X-ray Holography Time-Delay X-ray Holography X-ray free-electron lasers (XFELs) will produce photon pulses with a unique and desirable combination of properties. Their short X-ray wavelengths allow penetration into materials and the ability to probe structure at and below the nanometer scale. Their ultra-short duration gives information about this structure at the fundamental time-scales of atoms and molecules. The extreme intensity of the pulses will allow this information to be acquired in a single shot, so that these studies can be carried out on non-repeatable processes or on weakly-scattering objects that will be modified by the pulse. A fourth property of XFEL pulses is their high transverse coherence, which brings the promise of decades of innovation in visible optics to the X-ray regime, such as holography, interferometry, and laser-based imaging. Making an effective use of XFEL pulses, however, will benefit from innovations that are new to both X-ray science and coherent optics. One such innovation is the new method of time-delay X-ray holography [i], recently demonstrated at the FLASH FEL at DESY in Hamburg, to measure the evolution of objects irradiated by intense pulses.

368

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi Center 091 Chemistry Bldg. / College Park, MD 20742  

E-Print Network [OSTI]

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi. or advisor confirmation e-mail X-ray Diffractometer that will be used: User Level and Status Smart Apex2X'Pert Pro MRD (Reflectivity & low angles) Xeuss (Small/Wide Angle X-ray Scattering) Submitting user ­ only

Thirumalai, Devarajan

369

Lunar X-ray fluorescence observations by the Chandrayaan-1 X-ray Spectrometer (C1XS): Results from the nearside southern highlands  

E-Print Network [OSTI]

Lunar X-ray fluorescence observations by the Chandrayaan-1 X-ray Spectrometer (C1XS): Results from Spectroscopy a b s t r a c t The Chandrayaan-1 X-ray Spectrometer (C1XS) flown on-board the first Indian lunar mission Chan- drayaan-1, measured X-ray fluorescence spectra during several episodes of solar flares

Wieczorek, Mark

370

National Ignition Facility core x-ray streak camera  

SciTech Connect (OSTI)

The National Ignition Facility (NIF) core x-ray streak camera will be used for laser performance verification experiments as well as a wide range of physics experiments in the areas of high-energy-density science, inertial confinement fusion, and basic science. The x-ray streak camera system is being designed to record time-dependent x-ray emission from NIF targets using an interchangeable family of snouts for measurements such as one-dimensional (1D) spatial imaging or spectroscopy. the NIF core x-ray streak camera will consist of an x-ray-sensitive photocathode that detects x rays with 1D spatial resolution coupled to an electron streak tube to detect a continuous time history of the x rays incident on the photocathode over selected time periods. A charge-coupled-device (CCD) readout will record the signal from the streak tube. The streak tube, CCD, and associated electronics will reside in an electromagnetic interference, and electromagnetic pulse protected, hermetically sealed, temperature-controlled box whose internal pressure is approximately 1 atm. The streak tube itself will penetrate through the wall of the box into the target chamber vacuum. We are working with a goal of a spatial resolution of 15 lp/mm with 50% contrast transfer function at the photocathode and adjustment sweep intervals of 1--50 ns. The camera spectral sensitivity extends from soft x rays to 20 keV x rays, with varying quantum efficiency based on photocathode selection. The system will have remote control, monitoring, and Ethernet communications through an embedded controller. The core streak camera will be compatible with the instrument manipulators at the OMEGA (University of Rochester) and NIF facilities.

Kimbrough, J. R.; Bell, P. M.; Christianson, G. B.; Lee, F. D.; Kalantar, D. H.; Perry, T. S.; Sewall, N. R.; Wootton, A. J.

2001-01-01T23:59:59.000Z

371

The radiation-tolerant x-ray monitor  

SciTech Connect (OSTI)

A vacuum photoelectric detector (monitor) (VPD) designed for plasma tomography, megnetohydrodynamics monitoring, and imaging with the help of thermal x-ray radiation on the ITER facility is described. Laboratory experiments demonstrate that VPD has high sensitivity to thermal x rays and low sensitivity to hard gamma rays and neutrons. The results of tests of a prototype of this monitor on a {sup 60}Co source of gamma rays, on nuclear reactor and its calibration using radiation from an x-ray tube, and tests of its serviceability on the T-10 facility are presented.

Gott, Yu. V.; Stepanenko, M. M. [Nuclear Fusion Institute, Russian Research Center 'Kurchatov Institute', Kurchatov Sq. 1, Moscow 123182 (Russian Federation)

2008-10-15T23:59:59.000Z

372

X-ray backscatter imaging of nuclear materials  

DOE Patents [OSTI]

The energy of an X-ray beam and critical depth are selected to detect structural discontinuities in a material having an atomic number Z of 57 or greater. The critical depth is selected by adjusting the geometry of a collimator that blocks backscattered radiation so that backscattered X-ray originating from a depth less than the critical depth is not detected. Structures of Lanthanides and Actinides, including nuclear fuel rod materials, can be inspected for structural discontinuities such as gaps, cracks, and chipping employing the backscattered X-ray.

Chapman, Jeffrey Allen; Gunning, John E; Hollenbach, Daniel F; Ott, Larry J; Shedlock, Daniel

2014-09-30T23:59:59.000Z

373

Cryogenic X-Ray Diffraction Microscopy for Biological Samples  

Science Journals Connector (OSTI)

X-ray diffraction microscopy (XDM) is well suited for nondestructive, high-resolution biological imaging, especially for thick samples, with the high penetration power of x rays and without limitations imposed by a lens. We developed nonvacuum, cryogenic (cryo-) XDM with hard x rays at 8 keV and report the first frozen-hydrated imaging by XDM. By preserving samples in amorphous ice, the risk of artifacts associated with dehydration or chemical fixation is avoided, ensuring the imaging condition closest to their natural state. The reconstruction shows internal structures of intact D. radiodurans bacteria in their natural contrast.

Enju Lima; Lutz Wiegart; Petra Pernot; Malcolm Howells; Joanna Timmins; Federico Zontone; Anders Madsen

2009-11-05T23:59:59.000Z

374

Cryogenic X-ray Diffraction Microscopy for Biological Samples  

SciTech Connect (OSTI)

X-ray diffraction microscopy (XDM) is well suited for nondestructive, high-resolution biological imaging, especially for thick samples, with the high penetration power of x rays and without limitations imposed by a lens. We developed nonvacuum, cryogenic (cryo-) XDM with hard x rays at 8 keV and report the first frozen-hydrated imaging by XDM. By preserving samples in amorphous ice, the risk of artifacts associated with dehydration or chemical fixation is avoided, ensuring the imaging condition closest to their natural state. The reconstruction shows internal structures of intact D. radiodurans bacteria in their natural contrast.

E Lima; L Wiegart; P Pernot; M Howells; J Timmins; F Zontone; A Madsen

2011-12-31T23:59:59.000Z

375

X-Ray Afterglows from Gamma-Ray Bursts  

Science Journals Connector (OSTI)

We consider possible interpretations of the recently detected X-ray afterglow from the gamma-ray burst source GRB 970228. Cosmological and Galactic models of gamma-ray bursts predict different flux and spectral evolution of X-ray afterglows. We show that models based on adiabatic expansion of relativistic forward shocks require very efficient particle energization or postburst reacceleration during the expansion. Cooling neutron star models predict a very distinctive spectral and flux evolution that can be tested in current X-ray data.

M. Tavani

1997-01-01T23:59:59.000Z

376

Current Problems for X-ray Emission from Radio Jets  

E-Print Network [OSTI]

A list is presented of known extragalactic radio jets which also have associated X-ray emission. The canonical emission processes for the production of X-rays are reviewed and the sources are categorized on the basis of our current understanding. Although it seems clear that the X-ray emission is non-thermal, the two competing processes, synchrotron and inverse Compton emissions, arise from extremely high energy (synchrotron) or extremely low energy (beaming models with IC emission), relativistic electrons. Only synchrotron self-Compton emission from a few hotspots provides information on the `normal' energy range of the electrons responsible for the observed radio emission.

D. E. Harris

2000-12-17T23:59:59.000Z

377

Dynamic model of anisotropic x-ray refraction  

Science Journals Connector (OSTI)

General mechanisms of anisotropic x-ray refraction at the resonance energy are investigated on the basis of dynamic-scattering theory. The deductions show that x rays within the crystals that have anisotropic susceptibility are completely polarized and have two elliptical polarization states. Analytical expressions of the elliptical axes, refractive indices, and absorption coefficients for these two types of polarized waves are obtained in terms of the anisotropic components of the susceptibility tensor. Anisotropic birefringence and dichroism effects associated with the polarization properties of the x-ray waves are also illustrated theoretically.

X. R. Huang, Yong Li, W. J. Liu, and S. S. Jiang

1997-11-01T23:59:59.000Z

378

Characterization of X-ray generator beam profiles.  

SciTech Connect (OSTI)

T to compute the radiography properties of various materials, the flux profiles of X-ray sources must be characterized. This report describes the characterization of X-ray beam profiles from a Kimtron industrial 450 kVp radiography system with a Comet MXC-45 HP/11 bipolar oil-cooled X-ray tube. The empirical method described here uses a detector response function to derive photon flux profiles based on data collected with a small cadmium telluride detector. The flux profiles are then reduced to a simple parametric form that enables computation of beam profiles for arbitrary accelerator energies.

Mitchell, Dean J; Harding, Lee T.; Thoreson, Gregory G.; Theisen, Lisa Anne; Parmeter, John Ethan; Thompson, Kyle Richard

2013-07-01T23:59:59.000Z

379

Spatiotemporal focusing dynamics in plasmas at X-ray wavelength  

SciTech Connect (OSTI)

Using a finite curvature beam, we investigate here the spatiotemporal focusing dynamics of a laser pulse in plasmas at X-ray wavelength. We trace the dependence of curvature parameter on the focusing of laser pulse and recognize that the self-focusing in plasma is more intense for the X-ray laser pulse with curved wavefront than with flat wavefront. The simulation results demonstrate that spatiotemporal focusing dynamics in plasmas can be controlled with the appropriate choice of beam-plasma parameters to explore the high intensity effects in X-ray regime.

Sharma, A., E-mail: a-physics2001@yahoo.com; Tibai, Z. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary)] [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Hebling, J. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary) [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Szentagothai Research Centre, University of Pecs, Pecs-7624 (Hungary); Mishra, S. K. [Institute for Plasma Research, Gandhinagar (India)] [Institute for Plasma Research, Gandhinagar (India)

2014-03-15T23:59:59.000Z

380

Distribution of binding energies of a water molecule in the water liquid-vapor interface  

SciTech Connect (OSTI)

Distributions of binding energies of a water molecule in the water liquid-vapor interface are obtained on the basis of molecular simulation with the SPC/E model of water. These binding energies together with the observed interfacial density profile are used to test a minimally conditioned Gaussian quasi-chemical statistical thermodynamic theory. Binding energy distributions for water molecules in that interfacial region clearly exhibit a composite structure. A minimally conditioned Gaussian quasi-chemical model that is accurate for the free energy of bulk liquid water breaks down for water molecules in the liquid-vapor interfacial region. This breakdown is associated with the fact that this minimally conditioned Gaussian model would be inaccurate for the statistical thermodynamics of a dilute gas. Aggressive conditioning greatly improves the performance of that Gaussian quasi-chemical model. The analogy between the Gaussian quasi-chemical model and dielectric models of hydration free energies suggests that naive dielectric models without the conditioning features of quasi-chemical theory will be unreliable for these interfacial problems. Multi-Gaussian models that address the composite nature of the binding energy distributions observed in the interfacial region might provide a mechanism for correcting dielectric models for practical applications.

Chempath, Shaji [Los Alamos National Laboratory; Pratt, Lawrence R [TULANE UNIV

2008-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

Soft x-ray resist characterization: Studies with a laser plasma x-ray source  

SciTech Connect (OSTI)

Little work has been performed to characterize the exposure sensitivity, contrast, and tone of candidate resists for photon energies between 100--300 eV, the range in which projection soft x-ray lithography will be developed. We report here the characterization of near-edge x-ray absorption fine structure (NEXAFS) spectra, exposure sensitivity, contrast, and post-exposure processing of selected polysilane resists at photon energies close to the Si L{sub 2,3} absorption edge (100 eV). We find absorption resonance features in the NEXAFS spectra which we assign to excitation into Si--Si and Si--C {sigma}* orbitals. Using monochromatized XUV exposures on the Si--Si {sigma}* resonance at 105 eV, followed by solvent dissolution development, we have measured the exposure sensitivity curves of these resists. We find sensitivities in the range of 600--3000 mJ/cm{sup 2} and contrasts in the range from 0.5--1.4, depending on the polysilane side chain. We have also performed exposure sensitivity measurements at 92 eV, below the edge. Sensitivity decreases slightly compared to 105 eV exposures and the saturation depth and contrast both increase, as expected. We find also that exposing resist films to oxygen after XUV exposure, but before development increases the sensitivity markedly. 7 figs.

Kubiak, G.D.; Outka, D.A. (Sandia National Labs., Livermore, CA (USA)); Zeigler, J.M. (Sandia National Labs., Albuquerque, NM (USA))

1990-01-01T23:59:59.000Z

382

Thermonuclear (Type I) X-Ray Bursts Observed by the Rossi X-Ray Timing Explorer  

Science Journals Connector (OSTI)

We have assembled a sample of 1187 thermonuclear (type I) X-ray bursts from observations of 48 accreting neutron stars by the Rossi X-ray Timing Explorer, spanning more than 10 years. The sample contains examples of two of the three theoretical ignition regimes (confirmed via comparisons with numerical models) and likely examples of the third. We present a detailed analysis of the variation of the burst profiles, energetics, recurrence times, presence of photospheric radius expansion, and presence of burst oscillations, as a function of accretion rate. We estimated the distance for 35 sources exhibiting radius-expansion bursts, and found that the peak flux of such bursts varies typically by 13%. We classified sources into two main groups based on the burst properties: (1) both long and short bursts (indicating mixed H/He accretion), and (2) consistently short bursts (primarily He accretion), and we calculated the mean burst rate as a function of accretion rate for the two groups. The decrease in burst rate observed at > 0.06Edd$0.06˙{M}Edd$ --> ( -->2 ? 1037 ergs s?1) is associated with a transition in the persistent spectral state and (as has been suggested previously) may be related to the increasing role of steady He burning. We found many examples of bursts with recurrence times

Duncan K. Galloway; Michael P. Muno; Jacob M. Hartman; Dimitrios Psaltis; Deepto Chakrabarty

2008-01-01T23:59:59.000Z

383

A Laboratory-based Hard X-ray Monochromator for High-Resolution X-ray Emission Spectroscopy and X-ray Absorption Near Edge Structure Measurements  

E-Print Network [OSTI]

We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low poer x-ray (bremsstrahlung) tube source, a spherically-bent crystal analyzer (SBCA), and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of 5 keV to 10 keV while also dmeonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy (XES) comparable to those achived at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure (XANES), the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-powered line-foc...

Seidler, G T; Remesnik, A J; Pacold, J I; Ball, N A; Barry, N; Styczinski, M; Hoidn, O R

2014-01-01T23:59:59.000Z

384

Synchrotron-Radiation Induced X-Ray Emission (SRIXE)  

SciTech Connect (OSTI)

Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change and increase in scientific use can be maintained for the synchrotron x-ray source. A short summary of the present state of the synchrotron radiation-induced x-ray emission (SRIXE) method is presented here. Basically, SRIXE experiments can include any that depend on the detection. of characteristic x-rays produced by the incident x-ray beam born the synchrotron source as they interact with a sample. Thus, experiments done to measure elemental composition, chemical state, crystal, structure, and other sample parameters can be considered in a discussion of SRIXE. It is also clear that the experimentalist may well wish to use a variety of complementary techniques for study of a given sample. For this reason, discussion of computed microtomography (CMT) and x-ray diffraction is included here. It is hoped that this present discussion will serve as a succinct introduction to the basic ideas of SRIXE for those not working in the field and possibly help to stimulate new types of work by those starting in the field as well as by experienced practitioners of the art. The topics covered include short descriptions of (1) the properties of synchrotron radiation, (2) a description of facilities used for its production, (3) collimated microprobe, (4) focused microprobes, (5) continuum and monoenergetic excitation, (6) detection limits, (7) quantitation, (8) applications of SRIXE, (9) computed microtomography (CMT), and (10)chemical speciation using x-ray absorption near-edge structure (XANES) and extended x-ray absorption fine structure (EXAFS). An effort has been made to cite a wide variety of work from different laboratories to show the vital nature of the field.

Jones, Keith W.

1999-09-01T23:59:59.000Z

385

Liquid crystal displays for the evaluation of dental  

Science Journals Connector (OSTI)

We assessed whether dental x-ray images observed on a liquid crystal display (LCD) could be applied to diagnosis. A 13-inch TFT (thin film transistor) display was utilized in this study. Fifty x-ray films of r...

Keiichi Uchida D.D.S.; Masaomi Takizawa Sc.D.; Takurou Wada D.D.S.; Ph.D.…

1999-06-01T23:59:59.000Z

386

E-Print Network 3.0 - airborne lead x-ray Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Pulsars... you'd . . . Active Galactic . . . X-ray binaries Pulsars and relatives Gamma-ray bursts Gravitational... 1 - Type 2 X-ray binaries - Low mass X-ray binaries (LMXBs)...

387

E-Print Network 3.0 - advanced x-ray timing Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND Summary: with the occurrence of solar X-ray flare, when light travel time delay is accounted, suggesting that X-rays...

388

X-RAY ABSORPTION STUDIES OF GRAPHITE INTERCALATES AND METAL-AMMONIA SOLUTION  

E-Print Network [OSTI]

I. INTRODUCTION A. X-Ray Absorption Spectroscopy B. Graphiteacknowledged. The X-Ray absorption data could not have beenI INTRODUCTION X-ray absorption, spectroscopy (XAS) has been

Robertson, A.S.

2010-01-01T23:59:59.000Z

389

AN X-RAY ABSORPTION SPECTROSCOPY STUDY OF MANGANESE CONTAINING COMPOUNDS AND PHOTOSYNTHETIC SPINACH CHLOROPLASTS  

E-Print Network [OSTI]

II. Extended X-ray Absorption Fine Structure (EXAFS) TheoryIII. X-ray Absorption Spectroscopy (XAS) ExperimentIII. EXTENDED X-RAY ABSORPTION FINE STRUCTURE (EXAFS) DATA

Kirby, Jon Allan

2012-01-01T23:59:59.000Z

390

X-ray Absorption Spectroscopy Study of Prototype Chemical Systems: Theory vs. Experiment  

E-Print Network [OSTI]

acids by Near Edge X-ray Absorption Fine Structure (NEXAFS)X-ray Absorption Spectroscopy Study of Prototype ChemicalGlaeser Spring 2010 X-ray Absorption Spectroscopy Study of

Schwartz, Craig Philip

2010-01-01T23:59:59.000Z

391

X-ray absorption spectroscopy at the Ni-K edge in Stackhousia tryonii Bailey hyperaccumulator  

E-Print Network [OSTI]

X-ray absorption spectroscopy at the Ni–K edge inin vivo by micro x-ray absorption spectroscopy (XAS) at theNi–K edge. Both x-ray absorption near edge structure and

Kachenko, A.

2009-01-01T23:59:59.000Z

392

Definition: Portable X-Ray Diffraction (XRD) | Open Energy Information  

Open Energy Info (EERE)

Definition Definition Edit with form History Facebook icon Twitter icon » Definition: Portable X-Ray Diffraction (XRD) Jump to: navigation, search Dictionary.png Portable X-Ray Diffraction (XRD) Portable X-Ray Diffraction (XRD) is a field-based technique that can be used for identification of crystalline materials and analysis of unit cell dimensions. Portable XRD analysis is similar to X-ray powder diffraction, which has traditionally been used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline substances. Portable XRD analysis allows for simpler sample preparation, faster analytical times than traditional methods (less than 2 minutes), and can be performed at the sampling site in the field. A pure, finely ground

393

Plasma debris sputter resistant x-ray mirror  

Science Journals Connector (OSTI)

A diamond-like carbon (DLC) mirror, used as a grazing incident mirror in a plasma x-ray source, exhibits a high resistance to plasma debris sputtering. Good mirror reflectivity at a...

Amano, Sho; Inoue, Tomoaki; Harada, Tetsuo

2013-01-01T23:59:59.000Z

394

New Directions in X-ray Scattering - SSRL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

6, 2006 A summary of the workshop on New Directions in X-ray Scattering On Dec 6th, we held a day long workshop to solicit user input on the new directions that the SSRL...

395

Energy weighted x-ray dark-field imaging  

Science Journals Connector (OSTI)

The dark-field image obtained in grating-based x-ray phase-contrast imaging can provide information about the objects’ microstructures on a scale smaller than the pixel size...

Pelzer, Georg; Zang, Andrea; Anton, Gisela; Bayer, Florian; Horn, Florian; Kraus, Manuel; Rieger, Jens; Ritter, Andre; Wandner, Johannes; Weber, Thomas; Fauler, Alex; Fiederle, Michael; Wong, Winnie S; Campbell, Michael; Meiser, Jan; Meyer, Pascal; Mohr, Jürgen; Michel, Thilo

2014-01-01T23:59:59.000Z

396

Magnetic fields of neutron stars in X-ray binaries  

E-Print Network [OSTI]

A substantial fraction of the known neutron stars resides in X-ray binaries -- systems in which one compact object accretes matter from a companion star. Neutron stars in X-ray binaries have magnetic fields among the highest found in the Universe, spanning at least the range from $\\sim10^8$ to several 10$^{13}$ G. The magnetospheres around these neutron stars have a strong influence on the accretion process, which powers most of their emission. The magnetic field intensity and geometry, are among the main factors responsible for the large variety of spectral and timing properties observed in the X-ray energy range, making these objects unique laboratories to study the matter behavior and the radiation processes in magnetic fields unaccessible on Earth. In this paper we review the main observational aspects related to the presence of magnetic fields in neutron star X-ray binaries and some methods that are used to estimate their strength.

Revnivtsev, Mikhail

2014-01-01T23:59:59.000Z

397

X-ray emission from the terrestrial magnetosheath  

E-Print Network [OSTI]

[1] X-rays are generated throughout the terrestrial magnetosheath as a consequence of charge transfer collisions between heavy solar wind ions and geocoronal neutrals. The solar wind ions resulting from these collisions ...

Robertson, Ina Picket; Cravens, Thomas Edward

2003-04-29T23:59:59.000Z

398

Lensless Imaging of Magnetic Nanostructures by X-ray Spectro...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

co-workers. Their implementation of the technique is an extension of lensless Fourier transform holography to the x-ray regime, which detects the far field diffraction pattern of a...

399

Spectroscopic imaging, diffraction, and holography with x-ray photoemission  

SciTech Connect (OSTI)

X-ray probes are capable of determining the spatial structure of an atom in a specific chemical state, over length scales from about a micron all the way down to atomic resolution. Examples of these probes include photoemission microscopy, energy-dependent photoemission diffraction, photoelectron holography, and X-ray absorption microspectroscopy. Although the method of image formation, chemical-state sensitivity, and length scales can be very different, these X-ray techniques share a common goal of combining a capability for structure determination with chemical-state specificity. This workshop will address recent advances in holographic, diffraction, and direct imaging techniques using X-ray photoemission on both theoretical and experimental fronts. A particular emphasis will be on novel structure determinations with atomic resolution using photoelectrons.

Not Available

1992-02-01T23:59:59.000Z

400

Polarization Entangled Photons at X-Ray Energies  

E-Print Network [OSTI]

We show that polarization entangled photons at x-ray energies can be generated via spontaneous parametric down conversion. Each of the four Bell states can be generated by choosing the angle of incidence and polarization of the pumping beam.

S. Shwartz; S. E. Harris

2010-12-16T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

Towards hard x-ray imaging at GHz frame rate  

SciTech Connect (OSTI)

Gigahertz (GHz) imaging using hard x-rays ( Greater-Than-Or-Equivalent-To 10 keV) can be useful to high-temperature plasma experiments, as well as research and applications using coherent photons from synchrotron radiation and x-ray free electron lasers. GHz framing rate can be achieved by using multiple cameras through multiplexing. The advantages and trade-offs of single-photon detection mode, when no more than one x-ray photon is detected per pixel, are given. Two possible paths towards x-ray imaging at GHz frame rates using a single camera are: (a) avalanche photodiode arrays of high-Z materials and (b) microchannel plate photomultipliers in conjunction with materials with large indices of refraction.

Wang Zhehui; Morris, C. L.; Kapustinsky, J. S.; Kwiatkowski, K.; Luo, S.-N. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)

2012-10-15T23:59:59.000Z

402

Towards hard X-ray imaging at GHz frame rate  

SciTech Connect (OSTI)

Gigahertz (GHz) imaging using hard X-rays ({approx}> 10 keV) can be useful to high-temperature plasma experiments, as well as research using coherent photons from synchrotron radiation and X-ray free electron lasers. GHz framing rate can be achieved by using multiple cameras through multiplexing. The advantages and trade-offs of single-photon detection mode, when no more than one X-ray photon is detected per pixel, are given. Two possible paths towards X-ray imaging at GHz frame rates using a single camera are (a) Avalanche photodiode arrays of high-Z materials and (b) Microchannel plate photomultipliers in conjunction with materials with large indices of refraction.

Wang, Zhehui [Los Alamos National Laboratory; Morris, Christopher [Los Alamos National Laboratory; Luo, Shengnian [Los Alamos National Laboratory; Kwiatkowski, Kris K. [Los Alamos National Laboratory; Kapustinsky, Jon S. [Los Alamos National Laboratory

2012-05-02T23:59:59.000Z

403

Magnetism studies using resonant, coherent, x-ray scattering...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Magnetism studies using resonant, coherent, x-ray scattering Monday, September 10, 2012 - 10:00am SLAC, Bldg. 137, Room 226 Keoki Seu Seminar: With the advent of free electron...

404

Copyright The Discussion Group of X-Ray Analysis,  

E-Print Network [OSTI]

-2900. 3 In Situ Spatial and Time-Resolved Studies of Electrochemical Reactions by Scanning Transmission X the Signal-to-Noise Ratio of X-ray Diffraction Profiles by Smoothed Principal Component Analysis Zeng Ping

Jun, Kawai

405

X-Ray Astronomy to Resonant Theranostics for Cancer Treatment  

E-Print Network [OSTI]

X-Ray Astronomy to Resonant Theranostics for Cancer Treatment Sultana N. Nahar Department-Plasma Theranostics or RNPT, which gives indication for one most efficient way for destruction of malignant cells. 1

Nahar, Sultana Nurun

406

Vitreous carbon mask substrate for X-ray lithography  

DOE Patents [OSTI]

The present invention is directed to the use of vitreous carbon as a substrate material for providing masks for X-ray lithography. The new substrate also enables a small thickness of the mask absorber used to pattern the resist, and this enables improved mask accuracy. An alternative embodiment comprised the use of vitreous carbon as a LIGA substrate wherein the VC wafer blank is etched in a reactive ion plasma after which an X-ray resist is bonded. This surface treatment provides a surface enabling good adhesion of the X-ray photoresist and subsequent nucleation and adhesion of the electrodeposited metal for LIGA mold-making while the VC substrate practically eliminates secondary radiation effects that lead to delamination of the X-ray resist form the substrate, the loss of isolated resist features, and the formation of a resist layer adjacent to the substrate that is insoluble in the developer.

Aigeldinger, Georg (Livermore, CA); Skala, Dawn M. (Fremont, CA); Griffiths, Stewart K. (Livermore, CA); Talin, Albert Alec (Livermore, CA); Losey, Matthew W. (Livermore, CA); Yang, Chu-Yeu Peter (Dublin, CA)

2009-10-27T23:59:59.000Z

407

Optical and X-ray Variability of AGNs  

E-Print Network [OSTI]

I present new comparisons of AGN optical, UV, and X-ray variations. These reveal complex relationships between the different passbands that can change with time in a given object. While there is evidence from several objects that X-ray and optical activity levels are correlated on long timescales, variations on shorter timescales can occur independently. It is proposed that the combination of correlated and uncorrelated short-timescale variability is a consequence of anisotropic high-energy emission. It is also argued that the correlation between X-ray and optical variability on long timescales must be due to a common underlying factor and not to reprocessing of X-ray radiation.

C. Martin Gaskell

2006-12-30T23:59:59.000Z

408

,~ Abstract Submitted to 1997 Denver X-Ray Conference  

E-Print Network [OSTI]

,~ Abstract Submitted to 1997 Denver X-Ray Conference Denver, Colorado -August 4-8, 1997 BNL-.64346 being distributed through the entire volume of the particle needs further investigation. *Work supported

Brookhaven National Laboratory

409

Photon Sciences | Beamlines | SRX: Submicron Resolution X-ray Spectroscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

SRX: Submicron Resolution X-ray Spectroscopy SRX: Submicron Resolution X-ray Spectroscopy Poster | Fact Sheet | Preliminary Design Report Scientific Scope Scientific communities such as environmental sciences, life sciences, and material sciences have identified the need to develop analytical resources to advance the understanding of complex natural and engineered systems that are heterogeneous on the micron to nanometer scale. These needs for high intensity x-ray nanoprobes resulted in the commitment of the NSLS-II Project to build the Submicron Resolution X-ray (SRX) Spectroscopy beamline showing a unique combination of high spectral resolution over a very broad energy range and very high beam intensity in a sub-micrometer spot. NSLS-II will provide one of the best sources in the world for such an instrument.

410

X-ray Raman scattering study of aligned polyfluorene  

E-Print Network [OSTI]

We present a non-resonant inelastic x-ray scattering study at the carbon K-edge on aligned poly[9,9-bis(2-ethylhexyl)-fluorene-2,7-diyl] and show that the x-ray Raman scattering technique can be used as a practical alternative to x-ray absorption measurements. We demonstrate that this novel method can be applied to studies on aligned $\\pi$-conjugated polymers complementing diffraction and optical studies. Combining the experimental data and a very recently proposed theoretical scheme we demonstrate a unique property of x-ray Raman scattering by performing the symmetry decomposition on the density of unoccupied electronic states into $s$- and $p$-type symmetry contributions.

S. Galambosi; M. Knaapila; J. A. Soininen; K. Nyg\\aard; S. Huotari; F. Galbrecht; U. Scherf; A. P. Monkman; K. Hämäläinen

2006-08-29T23:59:59.000Z

411

X-Ray Photoelectron Spectroscopy (XPS) Applied to Soot & What...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Photoelectron Spectroscopy (XPS) Applied to Soot & What It Can Do for You X-Ray Photoelectron Spectroscopy (XPS) Applied to Soot & What It Can Do for You Presentation given at DEER...

412

Gravitational and Relativistic Deflection of X-Ray Superradiance  

E-Print Network [OSTI]

Exploring Einstein's theories of relativity in quantum systems, for example by using atomic clocks at high speeds can deepen our knowledge in physics. However, many challenges still remain on finding novel methods for detecting effects of gravity and of special relativity and their roles in light-matter interaction. Here we introduce a scheme of x-ray quantum optics that allows for a millimeter scale investigation of the relativistic redshift by directly probing a fixed nuclear crystal in Earth's gravitational field with x-rays. Alternatively, a compact rotating crystal can be used to force interacting x-rays to experience inhomogeneous clock tick rates in a crystal. We find that an association of gravitational or special-relativistic time dilation with quantum interference will be manifested by deflections of x-ray photons. Our protocol suggests a new and feasible tabletop solution for probing effects of gravity and special relativity in the quantum world.

Wen-Te Liao; Sven Ahrens

2014-11-27T23:59:59.000Z

413

Pixel detectors for x-ray imaging spectroscopy in space  

Science Journals Connector (OSTI)

Pixelated semiconductor detectors for X-ray imaging spectroscopy are foreseen as key components of the payload of various future space missions exploring the x-ray sky. Located on the platform of the new Spectrum-Roentgen-Gamma satellite, the eROSITA (extended Roentgen Survey with an Imaging Telescope Array) instrument will perform an imaging all-sky survey up to an X-ray energy of 10 keV with unprecedented spectral and angular resolution. The instrument will consist of seven parallel oriented mirror modules each having its own pnCCD camera in the focus. The satellite born X-ray observatory SIMBOL-X will be the first mission to use formation-flying techniques to implement an X-ray telescope with an unprecedented focal length of around 20 m. The detector instrumentation consists of separate high- and low energy detectors, a monolithic 128 ? 128 DEPFET macropixel array and a pixellated CdZTe detector respectively, making energy band between 0.5 to 80 keV accessible. A similar concept is proposed for the next generation X-ray observatory IXO. Finally, the MIXS (Mercury Imaging X-ray Spectrometer) instrument on the European Mercury exploration mission BepiColombo will use DEPFET macropixel arrays together with a small X-ray telescope to perform a spatially resolved planetary XRF analysis of Mercury's crust. Here, the mission concepts and their scientific targets are briefly discussed, and the resulting requirements on the detector devices together with the implementation strategies are shown.

J Treis; R Andritschke; R Hartmann; S Herrmann; P Holl; T Lauf; P Lechner; G Lutz; N Meidinger; M Porro; R H Richter; F Schopper; H Soltau; L Strüder

2009-01-01T23:59:59.000Z

414

The Hard X-ray Sky: Recent Observational Progress  

SciTech Connect (OSTI)

The last fifty years have witnessed the birth, development, and maturation to full potential of hard X-ray astrophysics. The primary force driving the history of the field has been the development of space-based instrumentation optimized for getting the maximum science out of observations of high-energy photons from astrophysical sources. Hard X-ray telescopes are leading research in areas such as galactic diffuse emission, galactic transients, and active galactic nuclei.

Gehrels, Neil [NASA/GSFC/ASD/Code 661, Greenbelt, Md 20071 (United States); Cannizzo, John K. [CRESST/UMBC/NASA/GSFC/ASD/Code 661, Greenbelt, Md 20071 (United States)

2009-05-11T23:59:59.000Z

415

The X-ray background and the evolution of AGN  

E-Print Network [OSTI]

We discuss the constraints on the AGN evolution from the cosmic X-ray background and source counts. A synthesis model to fit the X-ray background is presented. In the model, the spectrum of type 2 AGN has been modeled including Compton down--scattering within the absorbing material. Besides, we introduced a dependence on redshift of the relative number of obscured sources and found a decrease of the fraction of type 2 AGN at redshifts larger than 2.

Fulvio Pompilio; Fabio La Franca; Giorgio Matt

1999-09-23T23:59:59.000Z

416

Sapphire analyzers for high-resolution x-ray spectroscopy.  

SciTech Connect (OSTI)

We present a sapphire (Al{sub 2}O{sub 3}) analyzer for high-resolution X-ray spectroscopy with 31-meV energy resolution. The analyzer is designed for resonant inelastic X-ray scattering (RIXS) measurements at the CuK{sub a} absorption edge near 8990 eV. The performance of the analyzer is demonstrated by measuring phonon excitations in beryllium because of its known dynamical structure and high counting rates.

Yavas, H.; Alp, E.; Sinn, H.; Alatas, A.; Said, A.; Shvydko, Y.; Toellner, T.; Khachatryan, R.; Billinge, S.; Hasan, Z.; Sturhahn, W.; Michigan State Univ.; Princeton Univ.; DESY

2007-11-11T23:59:59.000Z

417

X-ray tube with magnetic electron steering  

DOE Patents [OSTI]

An X-ray tube uses a magnetic field to steer electrons. The magnetic field urges electrons toward the anode, increasing the proportion of electrons emitted from the cathode that reach desired portions of the anode and consequently contribute to X-ray production. The magnetic field also urges electrons reflected from the anode back to the anode, further increasing the efficiency of the tube.

Reed, Kim W. (Albuquerque, NM); Turman, Bobby N. (Albuquerque, NM); Kaye, Ronald J. (Albuquerque, NM); Schneider, Larry X. (Albuquerque, NM)

2000-01-01T23:59:59.000Z

418

Ris-M-2751 X-Ray Energy Dispersive  

E-Print Network [OSTI]

(PHOT) k«V 50 Risø National Laboratory, DK-4000 Roskilde, Denmark October 1988 #12;Ris*-M-2751 X-ray energy is impinging on the sample (Fig. lb). Its wavelength (photon energy) is in the course of measurements changedm ii. S Risø-M-2751 X-Ray Energy Dispersive Diffraction Lecture Notes Bronislaw Buras BaKo 30 40 E

419

A compact scanning soft X-ray microscope  

SciTech Connect (OSTI)

Soft x-ray microscopes operating at wavelengths between 2.3 nm and 4.4 nm are capable of imaging wet biological cells with a resolution many times that of a visible light microscope. Several such soft x-ray microscopes have been constructed. However, with the exception of contact microscopes, all use synchrotrons as the source of soft x-ray radiation and Fresnel zone plates as the focusing optics. These synchrotron based microscopes are very successful but have the disadvantage of limited access. This dissertation reviews the construction and performance of a compact scanning soft x-ray microscope whose size and accessibility is comparable to that of an electron microscope. The microscope uses a high-brightness laser-produced plasma as the soft x-ray source and normal incidence multilayer-coated mirrors in a Schwarzschild configuration as the focusing optics. The microscope operates at a wavelength of 14 nm, has a spatial resolution of 0.5 {mu}m, and has a soft x-ray photon flux through the focus of 10{sup 4}-10{sup 5} s{sup {minus}1} when operated with only 170 mW of average laser power. The complete system, including the laser, fits on a single 4{prime} x 8{prime} optical table. The significant components of the compact microscope are the laser-produced plasma (LPP) source, the multilayer coatings, and the Schwarzschild objective. These components are reviewed, both with regard to their particular use in the current microscope and with regard to extending the microscope performance to higher resolution, higher speed, and operation at shorter wavelengths. Measurements of soft x-ray emission and debris emission from our present LPP source are presented and considerations given for an optimal LPP source. The LPP source was also used as a broadband soft x-ray source for measurement of normal incidence multilayer mirror reflectance in the 10-25 nm spectral region.

Trail, J.A.

1989-01-01T23:59:59.000Z

420

New Directions in X-Ray Light Sources  

ScienceCinema (OSTI)

July 15, 2008 Berkeley Lab lecture: Molecular movies of chemical reactions and material phase transformations need a strobe of x-rays, the penetrating light that reveals how atoms and molecules assemble in chemical and biological systems and complex materials. Roger Falcone, Director of the Advanced Light Source,will discuss a new generation of x ray sources that will enable a new science of atomic dynamics on ultrafast timescales.

Roger Falcone

2010-01-08T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

X-Ray Diffraction Studies of Copper Nanopowder  

E-Print Network [OSTI]

Copper nanopowder preparation and its X-Ray diffraction studies are reported in this paper. Electrolytic cathode deposition method is simple and cheapest process for its preparation. Copper nanopowder has been prepared from aqueous copper sulphate solution. Wide range of experimental conditions has been adopted in this process and its X-Ray diffraction characterizations have been studied. The results confirming copper nanopowder with size below 30 nm. Uniformed size Copper nanopowder preparation, in normal room temperature is importance of this study.

T. Theivasanthi; M. Alagar

2010-03-31T23:59:59.000Z

422

E-Print Network 3.0 - anomalous small-angle x-ray Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

2008Standard Operating Procedure Title: Small Angle X-ray Scattering... approved: December 26 2009 Small Angle X-ray Scattering, Rotating Anode PURPOSE: This Standard...

423

E-Print Network 3.0 - angle x-ray scattering Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

2008Standard Operating Procedure Title: Small Angle X-ray Scattering... approved: December 26 2009 Small Angle X-ray Scattering, Rotating Anode PURPOSE: This Standard...

424

X-RAY ABSORPTION SPECTROSCOPY FOR THE CHEMICAL CHARACTERIZATION OF ATMOSPHERIC AEROSOLS  

E-Print Network [OSTI]

November 11-16 9 1979 X-RAY ABSORPTION SPECTROSCOPY FOR THEUniversity of California. ABSORPTION SPECTROSCOPY FOR THEand x-ray emission and absorption spectroscopy. The first

Jaklevic, J. M.

2011-01-01T23:59:59.000Z

425

Ultrafast X-ray Phase-Enhanced Microimaging for Visualizing Fuel...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Ultrafast X-ray Phase-Enhanced Microimaging for Visualizing Fuel Injection Process and Diesel Sprays Ultrafast X-ray Phase-Enhanced Microimaging for Visualizing Fuel Injection...

426

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental Science Beamline at the Advanced Light Source. Soft X-Ray Microscopy and Spectroscopy at the Molecular...

427

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

428

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

429

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

430

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

431

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

432

Using Light to Control How X Rays Interact with Matter  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Using Light to Control How X Using Light to Control How X Rays Interact with Matter Using Light to Control How X Rays Interact with Matter Print Wednesday, 27 January 2010 00:00 Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow light. However, it has been unclear whether similar optical control schemes could be used to modify how x rays interact with matter. In a dramatic breakthrough demonstration at the ALS, a Berkeley Lab-Argonne National Laboratory group has now used powerful visible-light lasers to render a nominally opaque material transparent to x rays. While x-ray transparency will have immediate applications at x-ray light sources, the important result is that the findings lay a foundation for a broader spectrum of applications.

433

Using Light to Control How X Rays Interact with Matter  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Using Light to Control How X Rays Interact with Matter Print Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow light. However, it has been unclear whether similar optical control schemes could be used to modify how x rays interact with matter. In a dramatic breakthrough demonstration at the ALS, a Berkeley Lab-Argonne National Laboratory group has now used powerful visible-light lasers to render a nominally opaque material transparent to x rays. While x-ray transparency will have immediate applications at x-ray light sources, the important result is that the findings lay a foundation for a broader spectrum of applications.

434

Using Light to Control How X Rays Interact with Matter  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Using Light to Control How X Rays Interact with Matter Print Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow light. However, it has been unclear whether similar optical control schemes could be used to modify how x rays interact with matter. In a dramatic breakthrough demonstration at the ALS, a Berkeley Lab-Argonne National Laboratory group has now used powerful visible-light lasers to render a nominally opaque material transparent to x rays. While x-ray transparency will have immediate applications at x-ray light sources, the important result is that the findings lay a foundation for a broader spectrum of applications.

435

Liquid-Air Interface Corrosion Testing Simulating The Environment Of Hanford Double Shell Tanks  

SciTech Connect (OSTI)

Coupon tests on A537 carbon steel materials were conducted to evaluate the Liquid-Air Interface (LAI) corrosion susceptibility in a series of solutions designed to simulate conditions in the radioactive waste tanks located at the Hanford Nuclear Facility. The new stress corrosion cracking requirements and the impact of ammonia on LAI corrosion were the primary focus. The minimum R value (i.e., molar ratio of nitrite to nitrate) of 0.15 specified by the new stress corrosion cracking requirements was found to be insufficient to prevent pitting corrosion at the LAI. The pH of the test solutions was 10, which was actually less than the required pH 11 defined by the new requirements. These tests examined the effect of the variation of the pH due to hydroxide depletion at the liquid air interface. The pits from the current testing ranged from 0.001 to 0.008 inch in solutions with nitrate concentrations of 0.4 M and 2.0 M. The pitting and general attack that occurred progressed over the four-months. No significant pitting was observed, however, for a solution with a nitrate concentration of 4.5 M. The pitting depths observed in these partial immersion tests in unevaporated condensates ranged from 0.001 to 0.005 inch after 4 months. The deeper pits were in simulants with low R values. Simulants with R values of approximately 0.6 to 0.8 appeared to significantly reduce the degree of attack. Although, the ammonia did not completely eliminate attack at the LAI, the amount of corrosion in an extremely corrosive solution was significantly reduced. Only light general attack (< 1 mil) occurred on the coupon in the vicinity of the LAI. The concentration of ammonia (i.e., 50 ppm or 500 ppm) did not have a strong effect.

Wiersma, B.; Gray, J. R.; Garcia-Diaz, B. L.; Murphy, T. H.; Hicks, K. R.

2014-01-30T23:59:59.000Z

436

X-ray instrumentation for protein crystallography with SR (abstract)  

SciTech Connect (OSTI)

The station is intended for x-ray analysis of single crystals, primarily that of proteins with the beam of synchrotron radiation from the superconducting wiggler of a special storage ring {ital E}=2.0 GeV, {ital I}=0.3 A in the town of Zelenograd (TNK).{sup 1} The dimensions of the radiation source are 2.35{sup 2} {sigma}{sub {ital x}}{center dot}{sigma}{sub {ital z}}=1.5{times}0.05 mm{sup 2}, the brightness for {lambda}=1.5 A is 10{sup 15} photon/(s mm{sup 2} mrad.{sup 2} 0.1% ({Delta}{lambda}/{lambda})). The station comprises the device forming the monochromatized primary beam ({lambda}=0.5--2.2 A, {Delta}{lambda}/{lambda}{sup {minus}3}{similar to}10{sup {minus}4}) that consists of an asymmetric focusing monochromator with triangular-shaped Si or Ge crystal curved as a round cylinder,{sup 2} a segmented mirror of total external reflection placed behind the monochromator on a rotating bench consisting of 8 flat glass 200{times}50{times}25 mm{sup 2} segments that form a surface imitating an elliptical cylinder, three pairs of horizontal and vertical slits, monitor--ionization chamber, four-circle diffractometer with scintillation counter and horizontal main axis placed on the adjustable carriage that can turn about the monochromator axis; position-sensitive proportional chamber with spherical drift space, 512{times}512 elements of space resolution and time resolution of 10{sup 6} photons per second that can be vertically shifted and bent around the holder horizontal axis. The monochromator goniometer as well as the crystal bend and the mirror segments are driven by the multiple-turn potientiometers by the computer and CAMAC interface.

Popov, A.N.; Kheiker, D.M.; Harutunyan, E.G. (Institute of Crystallography of the USSR Academy of Sciences, Leninsky Prospect 59, Moscow, 117333 (USSR))

1992-01-01T23:59:59.000Z

437

Dilation x-ray imager a new/faster gated x-ray imager for the NIF  

SciTech Connect (OSTI)

As the yield on implosion shots increases it is expected that the peak x-ray emission reduces to a duration with a FWHM as short as 20 ps for {approx}7 Multiplication-Sign 10{sup 18} neutron yield. However, the temporal resolution of currently used gated x-ray imagers on the NIF is 40-100 ps. We discuss the benefits of the higher temporal resolution for the NIF and present performance measurements for dilation x-ray imager, which utilizes pulse-dilation technology [T. J. Hilsabeck et al., Rev. Sci. Instrum. 81, 10E317 (2010)] to achieve x-ray imaging with temporal gate times below 10 ps. The measurements were conducted using the COMET laser, which is part of the Jupiter Laser Facility at the Lawrence Livermore National Laboratory.

Nagel, S. R.; Bell, P. M.; Bradley, D. K.; Ayers, M. J.; Barrios, M. A.; Felker, B.; Smith, R. F.; Collins, G. W.; Jones, O. S.; Piston, K.; Raman, K. S. [Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, California 94550 (United States); Hilsabeck, T. J.; Kilkenny, J. D.; Chung, T.; Sammuli, B. [General Atomics, P.O. Box 85608, San Diego, California 92186-5608 (United States); Hares, J. D.; Dymoke-Bradshaw, A. K. L. [Kentech Instruments Ltd., Wallingford, Oxfordshire OX10 (United Kingdom)

2012-10-15T23:59:59.000Z

438

Modeling the high resolution X-ray spectra from the relativistic jets of the X-ray binary SS 433  

E-Print Network [OSTI]

We test the physical model of the relativistic jets in the galactic X-ray binary SS 433 that was proposed by Marshall et al. 2002 (Paper I) using additional observations from the Chandra High Energy Transmission Grating ...

Lopez, Laura Ann, 1982-

2004-01-01T23:59:59.000Z

439

Diffractive imaging at large Fresnel number: Challenge of dynamic mesoscale imaging with hard x rays  

Science Journals Connector (OSTI)

Real materials have structure at both the atomic or crystalline scale as well as at interfaces and defects at the larger scale of grains. There is a need for the study of materials at the “mesoscale,” the scale at which subgranular physical processes and intergranular organization couple to determine microstructure, crucially impacting constitutive response at the engineering macroscale. Diffractive imaging using photons that can penetrate multiple grains of material would be a transformative technique for the study of the performance of materials in dynamic extremes. Thicker samples imply higher energy photons of shorter wavelength, and imaging of multiple grains implies bigger spot sizes. Such imaging requires the use of future planned and proposed hard x-ray free electron lasers (such as the European XFEL) to provide both the spatial coherence transverse to the large spots and the peak brilliance to provide the short illumination times. The result is that the Fresnel number of the system becomes large and is no longer in the Fraunhofer far-field limit. The interrelated issues of diffractive imaging at large Fresnel number are analyzed, including proof that diffractive imaging is possible in this limit and estimates of the signal-to-noise possible. In addition, derivation of the heating rates for brilliant pulses of x rays are presented. The potential and limitations on multiple dynamic images are derived. This paper will present a study of x-ray interactions with materials in this new regime of spatially coherent but relatively large mesoscale spots at very hard energies. It should provide the theory and design background for the experiments and facilities required to control materials in extreme environments, in particular for the next generation of very-hard-x-ray free electron lasers.

John L. Barber; Cris W. Barnes; Richard L. Sandberg; Richard L. Sheffield

2014-05-12T23:59:59.000Z

440

The crystal–liquid interface of a body?centered?cubic?forming substance: Computer simulations of the r ? 6 potential  

E-Print Network [OSTI]

(the bulk density change).27 For the (100) interface this 10--90 width is measured to be about 5.7a (just over 8 lattice planes). The variation of the diffusion constant through the in­ terface was calculated by dividing the z direction into 30 bins..., and were found not to differ measurably. The limiting liquid value of D (0.011 59 ± 0.000 01) was obtained in a separate 686 parti­ cle simulation of the bulk liquid. Note that bulk liquid diffu­ sion constants are known to be somewhat system size depen...

Laird, Brian Bostian; Haymet, A. D. J.

1989-09-01T23:59:59.000Z

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441

Gain dynamics in a soft X-ray laser ampli er perturbed by a strong injected X-ray eld  

SciTech Connect (OSTI)

Seeding soft X-ray plasma ampli ers with high harmonics has been demonstrated to generate high-brightness soft X-ray laser pulses with full spatial and temporal coherence. The interaction between the injected coherent eld and the swept-gain medium has been modelled. However, no exper- iment has been conducted to probe the gain dynamics when perturbed by a strong external seed eld. Here, we report the rst X-ray pump X-ray probe measurement of the nonlinear response of a plasma ampli er perturbed by a strong soft X-ray ultra-short pulse. We injected a sequence of two time-delayed high-harmonic pulses (l518.9 nm) into a collisionally excited nickel-like molybdenum plasma to measure with femto-second resolution the gain depletion induced by the saturated ampli cation of the high-harmonic pump and its subsequent recovery. The measured fast gain recovery in 1.5 1.75 ps con rms the possibility to generate ultra-intense, fully phase-coherent soft X-ray lasers by chirped pulse ampli cation in plasma ampli ers.

Wang, Yong [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Wang, Shoujun [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Oliva, E [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Lu, L [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Berrill, Mark A [ORNL] [ORNL; Yin, Liang [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Nejdl, J [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Luther, Brad [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Proux, C [Laboratoire d’Optique Applique´e, ENSTA, CNRS, Ecole Polytechnique] [Laboratoire d’Optique Applique´e, ENSTA, CNRS, Ecole Polytechnique; Le, T. T. [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Dunn, James [Lawrence Livermore National Laboratory (LLNL)] [Lawrence Livermore National Laboratory (LLNL); Ros, D [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Zeitoun, Philippe [École Polytechnique] [École Polytechnique; Rocca, Jorge [Colorado State University, Fort Collins] [Colorado State University, Fort Collins

2014-01-01T23:59:59.000Z

442

Diffracted X-ray tracking for monitoring intramolecular motion in individual protein molecules using broad band X-ray  

SciTech Connect (OSTI)

Diffracted X-ray tracking (DXT) enables the tilting and twisting motions of single protein molecules to be monitored with micro- to milliradian resolution using a highly brilliant X-ray source with a wide energy bandwidth. We have developed a technique to monitor single molecules using gold nanocrystals attached to individual protein molecules using the BL28B2 beamline at SPring-8. In this paper we present the installation of a single toroidal X-ray mirror at BL28B2 to focus X-rays in an energy range of 10–20 keV (?E/E = 82% for an X-ray with a wide energy bandwidth). With this beamline we tracked diffraction spots from gold nanocrystals over a wide angle range than that using quasi-monochromatic X-rays. Application of the wide angle DXT technique to biological systems enabled us to observe the on-site motions of single protein molecules that have been functionalized in vivo. We further extend the capability of DXT by observing the fractional tilting and twisting motions of inner proteins under various conditions. As a proof of this methodology and to determine instrumental performance the intramolecular motions of a human serum albumin complex with 2-anthracenecarboxylic acid was investigated using the BL28B2 beamline. The random tilting and twisting intramolecular motions are shown to be directly linked to the movement of individual protein molecules in the buffer solution.

Ichiyanagi, Kouhei; Sasaki, Yuji C. [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan) [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan); Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan); Sekiguchi, Hiroshi; Hoshino, Masato; Kajiwara, Kentaro; Senba, Yasunori; Ohashi, Haruhiko; Ohta, Noboru [Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)] [Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan); Hoshisashi, Kentaro; Jae-won, Chang; Tokue, Maki; Matsushita, Yufuku [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan)] [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan); Nishijima, Masaki; Inoue, Yoshihisa [Department of Applied Chemistry and Office for University-Industry Collaboration, Osaka University, 2-1 Yamadaoka, Suita, Osaka 565-0871 (Japan)] [Department of Applied Chemistry and Office for University-Industry Collaboration, Osaka University, 2-1 Yamadaoka, Suita, Osaka 565-0871 (Japan); Yagi, Naoto [Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan) [Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan); Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)

2013-10-15T23:59:59.000Z

443

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and x-ray polarization, but their orientation relative to the crystallographic axes must be taken into account for accurate interpretation of XMLD data. Magnetism and X Rays The ancient Greeks and also the Chinese knew about strange and rare stones with the power to attract iron. Moreover, when freely suspended these objects pointed north-south. Throughout the past, we have used this phenomenon-magnetism-for navigation and more recently for power production and digital information storage, all while trying to explore and understand its origins. In 1986 researchers at a facility similar to the ALS observed for the first time that the absorption of x rays depends not only on the composition of a material-that is, if it contains iron, nickel, or other elements-but also on its magnetism. The effect is unique in that it allows us to distinguish which atomic species magnetism originates from and provides information about their local atomic environment-for example, whether a magnetic species is surrounded by 4 or 6 oxygen atoms. A research team at the ALS has now shown that the relationship between magnetic order and absorption of x rays is even more complex and exciting than has been assumed for the past 20 years, leading to a reassessment of previous results.

444

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and x-ray polarization, but their orientation relative to the crystallographic axes must be taken into account for accurate interpretation of XMLD data. Magnetism and X Rays The ancient Greeks and also the Chinese knew about strange and rare stones with the power to attract iron. Moreover, when freely suspended these objects pointed north-south. Throughout the past, we have used this phenomenon-magnetism-for navigation and more recently for power production and digital information storage, all while trying to explore and understand its origins. In 1986 researchers at a facility similar to the ALS observed for the first time that the absorption of x rays depends not only on the composition of a material-that is, if it contains iron, nickel, or other elements-but also on its magnetism. The effect is unique in that it allows us to distinguish which atomic species magnetism originates from and provides information about their local atomic environment-for example, whether a magnetic species is surrounded by 4 or 6 oxygen atoms. A research team at the ALS has now shown that the relationship between magnetic order and absorption of x rays is even more complex and exciting than has been assumed for the past 20 years, leading to a reassessment of previous results.

445

Interdiffusion in NiMnSb/V/NiMnSb: X-ray and neutron reflectivity investigation of ion beam sputtered trilayer systems  

SciTech Connect (OSTI)

The new trilayer system NiMnSb/V/NiMnSb on MgO(001) was investigated by means of vibrating sample magnetometry (VSM), x-ray, and neutron reflectivity. VSM revealed a coercive field H{sub c}=23 Oe and a hysteresis loop similar to that of an uncoupled ferromagnet. The x-ray and neutron reflectivity data proved that interface roughnesses of 10 {Angstrom} are present. A detailed analysis yielded significant interdiffusion at the NiMnSb/V interfaces which is one possible explanation for the weak magnetoresistance effect measured in similar NiMnSb-based multilayer systems. {copyright} {ital 1999 American Institute of Physics.}

Schlomka, J.; Tolan, M.; Press, W. [Institut fuer Experimentelle und Angewandte Physik, Christian-Albrechts-Universitaet zu Kiel, 24098 Leibnizstrasse 17-19, Kiel (Germany)] [Institut fuer Experimentelle und Angewandte Physik, Christian-Albrechts-Universitaet zu Kiel, 24098 Leibnizstrasse 17-19, Kiel (Germany); Fitzsimmons, M.R. [Manuel Lujan, Jr. Neutron Scattering Center, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)] [Manuel Lujan, Jr. Neutron Scattering Center, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Siebrecht, R. [Institut Laue-Langevin, 38042 Grenoble, Cedex 9 (France)] [Institut Laue-Langevin, 38042 Grenoble, Cedex 9 (France); Schubert, D.W. [GKSS Forschungszentrum, 21502 Geesthacht (Germany)] [GKSS Forschungszentrum, 21502 Geesthacht (Germany); Simon, P. [Max Planck Institut fuer Polymerforschung, 55021 Mainz (Germany)] [Max Planck Institut fuer Polymerforschung, 55021 Mainz (Germany)

1999-11-01T23:59:59.000Z

446

Characteristics of the weld interface in dissimilar austenitic-pearlitic steel welds  

SciTech Connect (OSTI)

The weld interface in dissimilar alloy welds between austenitic and pearlitic steels was observed directly by using scanning and transmission electron microscopy, and energy-dispersive x-ray spectrometry. Two types of weld interface were found in the joints. One was the austenite/martensite-like interface that formed the boundary between the mixed weld metal zone and the partially mixed transitional zone. The other is the martensite-like/ferrite interface that is the true liquid-solid boundary of the joint. These interfaces can exist independently in different joints and can also coexist in one joint, depending on the Cr and Ni contents of the filler metals and alloy in the base metals. The formation mechanism of the weld interface and its effect on the mechanical properties of the welded joint are discussed.

Pan, C.; Zhang, Z. (Wuhan Transportation Univ. (China). Dept. of Marine Mechanical Engineering)

1994-09-01T23:59:59.000Z

447

Multi-manoeuvrable UHV crystal holder (for X-ray spectrometer)  

Science Journals Connector (OSTI)

The design of a multi-manoeuvrable ultrahigh vacuum (UHV) crystal holder for a new soft X-ray spectrometer is described. The holder is capable of adjusting the position of the crystal by 80 mm in the z direction which is normal to the Rowland circumference of the spectrometer and 8 mm in the orthogonal x and y directions. Angular adjustment is allowed within a maximum range of 10 degrees . All adjustments are accurately reproducible and are made from outside the UHV system. The holder also makes provision for cooling of the crystal by a liquid or gas coolant.

S Ottosson

1976-01-01T23:59:59.000Z

448

Neutron and X-Ray Scattering - Argonne National Laboratories, Materials  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Home Home Neutron and X-Ray Scattering Neutron and X-ray Scattering Science Recent advances in neutron and x-ray scattering instrumentation at major DOE facilities such as the Spallation Neutron Source and Advanced Photon Source provide unprecedented insights into complex phenomena in bulk and interfacial materials. The vision of our group is to harness the complementarity of neutrons and x-rays to study how materials respond on a range of length and time scales to phase competition, so that we can learn to control emergent behavior and generate functional properties in energy-related materials. We use neutrons and x-rays to investigate the structure and dynamics of bulk and interfacial materials with properties that are useful for energy applications, such as superconductivity, magnetism and thermoelectricity. Phase competition can generate or enhance such properties, but it is extremely challenging to characterize fluctuations in the competing order, whether in bulk disordered materials, or artificial heterostructures. Our goal is to utilize efficient techniques that we have been developing for measuring nanoscale phase fluctuations, both static and dynamic, to enable the rational design of new materials for energy within MSD.

449

Optics-free x-ray FEL oscillator  

SciTech Connect (OSTI)

There is a need for an Optics-Free FEL Oscillators (OFFELO) to further the advantages of free-electron lasers and turning them in fully coherent light sources. While SASE (Self-Amplified Spontaneous Emission) FELs demonstrated the capability of providing very high gain and short pulses of radiation and scalability to the X-ray range, the spectra of SASE FELs remains rather wide ({approx}0.5%-1%) compared with typical short wavelengths FEL-oscillators (0.01%-0.0003% in OK-4 FEL). Absence of good optics in VUV and X-ray ranges makes traditional oscillator schemes with very high average and peak spectral brightness either very complex or, strictly speaking, impossible. In this paper, we discuss lattice of the X-ray optics-free FEL oscillator and present results of initial computer simulations of the feedback process and the evolution of FEL spectrum in X-ray OFFELO. We also discuss main limiting factors and feasibility of X-ray OFFELO.

Litvinenko, V.N.; Hao, Y.; Kayran, D.; Trbojevic, D.

2011-03-28T23:59:59.000Z

450

NuSTAR Observations of X-Ray Binaries  

E-Print Network [OSTI]

As of 2014 August, the Nuclear Spectroscopic Telescope Array (NuSTAR) had observed ~30 X-ray binaries either as part of the planned program, as targets of opportunity, or for instrument calibration. The main science goals for the observations include probing the inner part of the accretion disk and constraining black hole spins via reflection components, providing the first observations of hard X-ray emission from quiescent Low Mass X-ray Binaries (LMXBs), measuring cyclotron lines from accreting pulsars, and studying type I X-ray bursts from neutron stars. Here, we describe the science objectives in more depth and give an overview of the NuSTAR observations that have been carried out to achieve the objectives. These include observation of four "IGR" High Mass X-ray Binaries (HMXBs) discovered by INTEGRAL. We also summarize the results that have been obtained and their implications. Among the IGR HMXBs, we focus on the discovery of a cyclotron line in the spectrum of IGR J17544-2619.

Tomsick, John A; Fuerst, Felix; Harrison, Fiona; Miyasaka, Hiromasa; Tendulkar, Shriharsh; Bhalerao, Varun; Chakrabarty, Deepto; King, Ashley; Miller, Jon M; Natalucci, Lorenzo; Stern, Daniel

2015-01-01T23:59:59.000Z

451

Method and apparatus for micromachining using hard X-rays  

DOE Patents [OSTI]

An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures. 21 figs.

Siddons, D.P.; Johnson, E.D.; Guckel, H.; Klein, J.L.

1997-10-21T23:59:59.000Z

452

Method and apparatus for micromachining using hard X-rays  

DOE Patents [OSTI]

An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures.

Siddons, David Peter (Shoreham, NY); Johnson, Erik D. (Ridge, NY); Guckel, Henry (Madison, WI); Klein, Jonathan L. (Madison, WI)

1997-10-21T23:59:59.000Z

453

The History of X-ray Free-Electron Lasers  

SciTech Connect (OSTI)

The successful lasing at the SLAC National Accelerator Laboratory of the Linear Coherent Light Source (LCLS), the first X-ray free-electron laser (X-ray FEL), in the wavelength range 1.5 to 15 {angstrom}, pulse duration of 60 to few femtoseconds, number of coherent photons per pulse from 10{sup 13} to 10{sup 11}, is a landmark event in the development of coherent electromagnetic radiation sources. Until now electrons traversing an undulator magnet in a synchrotron radiation storage ring provided the best X-ray sources. The LCLS has set a new standard, with a peak X-ray brightness higher by ten orders of magnitudes and pulse duration shorter by three orders of magnitudes. LCLS opens a new window in the exploration of matter at the atomic and molecular scales of length and time. Taking a motion picture of chemical processes in a few femtoseconds or less, unraveling the structure and dynamics of complex molecular systems, like proteins, are some of the exciting experiments made possible by LCLS and the other X-ray FELs now being built in Europe and Asia. In this paper, we describe the history of the many theoretical, experimental and technological discoveries and innovations, starting from the 1960s and 1970s, leading to the development of LCLS.

Pellegrini, C.; /UCLA /SLAC; ,

2012-06-28T23:59:59.000Z

454

Ultrafast x-ray diffraction of laser-irradiated crystals  

SciTech Connect (OSTI)

An apparatus has been developed for measuring time-dependent x-ray diffraction. X-ray pulses from an Advanced Light Source bend magnet are diffracted by a sagittally-focusing Si(111) crystal and then by a sample crystal, presently InSb(111). Laser pulses with 100 fs duration and a repetition rate of 1 KHz irradiate the sample inducing a phase transition. Two types of detectors are being employed: an x-ray streak camera and an avalanche photodiode. The streak camera is driven by a photoconductive switch and has a 2 ps temporal resolution determined by trigger jitter. The avalanche photodiode has high quantum efficiency and sufficient time resolution to detect single x-ray pulses in ALS two bunch or camshaft operation. A beamline is under construction dedicated for time resolved and micro-diffraction experiments. In the new beamline a toroidal mirror collects 3 mrad horizontally and makes a 1:1 image of the bend magnet source in the x-ray hutch. A laser induced phase transition has been observed in InSb occurring within 70 ps.

Heimann, P.A. [Lawrence Berkeley National Lab., CA (US). Advanced Light Source; Larsson, J. [Univ. of California, Berkeley, CA (US). Physics Dept.; Chang, Z. [Univ. of Michigan, Ann Arbor, MI (US). Center for Ultrafast Optical Science

1997-09-01T23:59:59.000Z

455

Implications of the X-Ray Properties of Pulsar Nebulae  

E-Print Network [OSTI]

A plausible model for the Crab Nebula is one in which a particle dominated, highly relativistic wind from the pulsar passes through a shock front in which the particles attain a power law energy distribution. The electrons and positrons lose energy radiating synchrotron emission. Here, a one zone version of the model is developed and applied to observations of X-ray pulsar nebulae. Efficient conversion of pulsar spin-down power to X-ray luminosity is expected if the observed electrons are in the synchrotron cooling regime and their energy spectrum is similar to that in the Crab Nebula. In this case, the relation between X-ray luminosity and pulsar spin-down power depends only weakly on the model parameters. The dependence is stronger for a steeper particle spectrum, as appears to be present in N157B, and the efficiency of X-ray production can be lower. If the electrons are not in the cooling regime, the X-ray luminosity can be low, as appears to be the case for the compact nebula around the Vela pulsar. Slow cooling is likely to be caused by a sub-equipartition magnetic field in the radiating region. Observations can place constraints on the uncertain physics of relativistic MHD shocks. The model is related to those developed for gamma-ray burst afterglows.

Roger A. Chevalier

2000-06-01T23:59:59.000Z

456

KOTOBUKI-1 apparatus for cryogenic coherent X-ray diffraction imaging  

SciTech Connect (OSTI)

We have developed an experimental apparatus named KOTOBUKI-1 for use in coherent X-ray diffraction imaging experiments of frozen-hydrated non-crystalline particles at cryogenic temperature. For cryogenic specimen stage with small positional fluctuation for a long exposure time of more than several minutes, we here use a cryogenic pot cooled by the evaporation cooling effect for liquid nitrogen. In addition, a loading device is developed to bring specimens stored in liquid nitrogen to the specimen stage in vacuum. The apparatus allows diffraction data collection for frozen-hydrated specimens at 66 K with a positional fluctuation of less than 0.4 ?m and provides an experimental environment to easily exchange specimens from liquid nitrogen storage to the specimen stage. The apparatus was developed and utilized in diffraction data collection of non-crystalline particles with dimensions of ?m from material and biological sciences, such as metal colloid particles and chloroplast, at BL29XU of SPring-8. Recently, it has been applied for single-shot diffraction data collection of non-crystalline particles with dimensions of sub-?m using X-ray free electron laser at BL3 of SACLA.

Nakasako, Masayoshi; Takayama, Yuki; Oroguchi, Tomotaka; Sekiguchi, Yuki; Kobayashi, Amane [Department of Physics, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223-8522 (Japan) [Department of Physics, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223-8522 (Japan); RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Shirahama, Keiya [Department of Physics, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223-8522 (Japan)] [Department of Physics, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223-8522 (Japan); Yamamoto, Masaki; Hikima, Takaaki; Yonekura, Koji; Maki-Yonekura, Saori; Kohmura, Yoshiki; Inubushi, Yuichi [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan)] [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Takahashi, Yukio; Suzuki, Akihiro [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan) [RIKEN SPring-8 Center, 1-1-1 Kouto, Sayo, Hyogo 679-5148 (Japan); Department of Precision Science and Technology, Graduate School of Engineering, Osaka University, 2-1 Yamadaoka, Suita, Osaka 565-0871 (Japan); Matsunaga, Sachihiro; Inui, Yayoi [Department of Applied Biological Science Faculty of Science and Technology, Tokyo University of Science, 2641 Yamazaki, Noda, Chiba 278-8510 (Japan)] [Department of Applied Biological Science Faculty of Science and Technology, Tokyo University of Science, 2641 Yamazaki, Noda, Chiba 278-8510 (Japan); Tono, Kensuke; Kameshima, Takashi; Joti, Yasumasa [Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)] [Japan Synchrotron Radiation Research Institute, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan); Hoshi, Takahiko [Kohzu Precision Co., Ltd., 2-6-15 Kurigi, Aso-ku, Kawasaki, Kanagawa 215-8521 (Japan)] [Kohzu Precision Co., Ltd., 2-6-15 Kurigi, Aso-ku, Kawasaki, Kanagawa 215-8521 (Japan)

2013-09-15T23:59:59.000Z

457

ON THE X-RAY OUTBURSTS OF TRANSIENT ANOMALOUS X-RAY PULSARS AND SOFT GAMMA-RAY REPEATERS  

SciTech Connect (OSTI)

We show that the X-ray outburst light curves of four transient anomalous X-ray pulsars (AXPs) and soft gamma-ray repeaters (SGRs), namely, XTE J1810-197, SGR 0501+4516, SGR 1627-41, and CXOU J164710.2-455216, can be produced by the fallback disk model that was also applied to the outburst light curves of persistent AXPs and SGRs in our earlier work. The model solves the diffusion equation for the relaxation of a disk that has been pushed back by a soft gamma-ray burst. The sets of main disk parameters used for these transient sources are very similar to each other and to those employed in our earlier models of persistent AXPs and SGRs. There is a characteristic difference between the X-ray outburst light curves of transient and persistent sources. This can be explained by the differences in the disk surface density profiles of the transient and persistent sources in quiescence indicated by their quiescent X-ray luminosities. Our results imply that a viscous disk instability operating at a critical temperature in the range of {approx}1300-2800 K is a common property of all fallback disks around AXPs and SGRs. The effect of the instability is more pronounced and starts earlier for the sources with lower quiescent luminosities, which leads to the observable differences in the X-ray enhancement light curves of transient and persistent sources. A single active disk model with the same basic disk parameters can account for the enhancement phases of both transient and persistent AXPs and SGRs. We also present a detailed parameter study to show the effects of disk parameters on the evolution of the X-ray luminosity of AXPs and SGRs in the X-ray enhancement phases.

Cal Latin-Small-Letter-Dotless-I skan, Sirin; Ertan, Uenal [Sabanc Latin-Small-Letter-Dotless-I University, Orhanl Latin-Small-Letter-Dotless-I -Tuzla, Istanbul, 34956 (Turkey)

2012-10-20T23:59:59.000Z

458

X-ray magnetic circular dichroism in (Ge,Mn) compounds: experiments and modeling Samuel Tardif,1, 2,  

E-Print Network [OSTI]

X-ray magnetic circular dichroism in (Ge,Mn) compounds: experiments and modeling Samuel Tardif,1, 2: July 29, 2013) X-ray absorption (XAS) and x-ray magnetic circular dichroism (XMCD) spectra at the L2),6 and x-ray spectroscopy (x-ray absorption spec- troscopy, XAS, and x-ray magnetic circular

459

Crystallization and preliminary X-ray crystallographic study of disproportionating enzyme from potato  

Science Journals Connector (OSTI)

Disproportionating enzyme from potato was crystallized and preliminarily analyzed using X-ray diffraction.

Imamura, K.

2004-12-24T23:59:59.000Z

460

Evolution of Cygnus X-3 through its Radio and X-ray States  

SciTech Connect (OSTI)

Based on X-ray spectra and studies of the long-term correlated behavior between radio and soft X-ray, we present a detailed evolution of Cyg X-3 through its radio and X-ray states. We comment on the nature of the hard X-ray tail and possible Simbol X contribution in constraining the models.

Szostek, A. [Laboratoire d'Astrophysique de Grenoble, CNRS, Universite Joseph Fourier, Grenoble (France); Astronomical Observatory, Jagiellonian University, Krakow (Poland); Zdziarski, A. A. [Centrum Astronomiczne im. M. Kopernika, Warszawa (Poland); McCollough, M. L. [Smithsonian Astrophysical Observatory, Cambridge (United States)

2009-05-11T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Determination of the iron-sulfur distances in rubredoxin by x-ray absorption spectroscopy  

Science Journals Connector (OSTI)

...x-ray flux from the synchrotron radiation at the Stanford Synchroton Radiation Project has been used to study the extended x-ray...x-ray flux from the synchrotron radiation at the Stanford Synchroton Radiation Project has been used to study the extended x-ray...

R G Shulman; P Eisenberger; W E Blumberg; N A Stombaugh

1975-01-01T23:59:59.000Z

462

X-ray Diffraction / MSE 603 Spring 2002 Qun Shen / CHESS qs11@cornell.edu  

E-Print Network [OSTI]

X-ray Diffraction / MSE 603 Spring 2002 Qun Shen / CHESS qs11@cornell.edu 1. X-ray production & basic properties ­ common sources for diffraction experiments ­ synchrotron radiation ­ response to x-rays by an electron ­ refraction index ­ total external reflection & evanescent wave, TXRF 2. X-ray scattering basics

Shen, Qun

463

Soft X-Ray Diffraction Microscopy of a Frozen Hydrated Yeast Cell Xiaojing Huang,1  

E-Print Network [OSTI]

Soft X-Ray Diffraction Microscopy of a Frozen Hydrated Yeast Cell Xiaojing Huang,1 Johanna Nelson,1 eukaryotic cell using x-ray diffraction microscopy, or coherent x-ray diffraction imaging. By plunge freezingV x rays were recorded and reconstructed to reveal a budding yeast cell at a resolution better than 25

Mohseni, Hooman

464

X-ray Spectroscopy of O Supergiant Winds: Shock Physics, Clumping, and Mass-Loss Rates  

E-Print Network [OSTI]

X-ray Spectroscopy of O Supergiant Winds: Shock Physics, Clumping, and Mass-Loss Rates David Cohen Li (Swarthmore '16), Kelley Langhans (Swarthmore '16) #12;Talk Outline Context of O star X-ray emission: wind shocks 1. X-ray constraints on the shocked wind plasma 2. X-ray absorption as a mass

Cohen, David

465

X-ray spectral diagnostics of neon photoionization experiments on the Z-machine  

E-Print Network [OSTI]

X-ray spectral diagnostics of neon photoionization experiments on the Z-machine David H. Cohen on an initial spectroscopic study of low-density, x-ray photoionized neon with x-ray spectroscopy plasma, and to explore issues related to the rapid x-ray photoionization of relatively cold, low

Cohen, David

466

X-ray absorption anisotropy for polychromatic illumination--Crystal views from inside  

E-Print Network [OSTI]

X-ray absorption anisotropy for polychromatic illumination--Crystal views from inside P. Korecki a Keywords: X-ray absorption Real-space imaging X-ray holography Electron channeling Electron backscatter of the fine structure in X-ray absorption anisotropy, which results from incident beam diffraction

Korecki, Pawe³

467

X-ray emission from clusters of galaxies Craig L. Sarazin  

E-Print Network [OSTI]

X-ray emission from clusters of galaxies Craig L. Sarazin Department of Astronomy, University show that they are bright x-ray sources, with luminosities of 1043 45 ergs/sec. It is now established the stars in all the galaxies in the cluster. The x-ray spectra of clusters show strong x-ray line emission

Sarazin, Craig

468

X-ray four-wave mixing in molecules Satoshi Tanaka  

E-Print Network [OSTI]

X-ray four-wave mixing in molecules Satoshi Tanaka Department of Chemistry, University of Rochester radiation intense light sources have opened up a new era in soft x-ray spectroscopy. The dramatic improvements of spectral resolution in x-ray absorption1,2 and x-ray photoemission spectra3 have revealed

Mukamel, Shaul

469

X-Ray: A Tool for Automatic Measurement of Hardware Parameters  

E-Print Network [OSTI]

X-Ray: A Tool for Automatic Measurement of Hardware Parameters Kamen Yotov, Keshav Pingali, Paul and register tiles. In this paper, we describe X-Ray1 , a system for im- plementing micro-benchmarks to measure. Experimen- tal evaluations of X-Ray on traditional workstations, servers and embedded systems show that X-Ray

Pingali, Keshav K.

470

A low-cost X-ray-transparent experimental cell for synchrotron-based X-ray microtomography studies under geological reservoir conditions  

Science Journals Connector (OSTI)

An X-ray-transparent experimental environment that allows time-resolved studies of porous rocks under geological reservoir conditions using high-energy synchrotron X-ray microtomography is presented.

Fusseis, F.

2013-12-05T23:59:59.000Z

471

Detection limits of high temperature superconducting materials on various substrates by energy dispersive X-ray fluorescence and proton induced X-ray emission methods  

Science Journals Connector (OSTI)

Application of energy dispersive X-ray fluorescence (EDXRF) and proton induced X-ray emission (PIXE) methods has been demonstrated for determining the elemental composition of thin film superconducting materia...

M Lal; H N Bajpai; D Joseph; R K Choudhury

1990-04-01T23:59:59.000Z

472

‘Taking X-ray phase contrast imaging into mainstream applications’ and its satellite workshop ‘Real and reciprocal space X-ray imaging’  

Science Journals Connector (OSTI)

...presented Femtosecond X-ray lasers for imaging atomic structure...which he described X-ray laser-induced electronic ordering...characterization of targets for laser fusion experiments. Krist. Tech...1205396109 ) 20 Talbot, HF . 1836 Facts relating to...

2014-01-01T23:59:59.000Z

473

X-ray movies reveal insect flight, muscle motion  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

BioCAT BioCAT X-ray movies reveal insect flight, muscle motion Photo credit: Michael Dickinson Watching flies fly may not seem like high-tech science, but for researchers using the Western Hemisphere's most brilliant X-rays, from the Advanced Photon Source located at the U.S. Department of Energy's Argonne National Laboratory, it not only helps explain how insects fly but also may someday aid in understanding human heart function. The researchers, from the Illinois Institute of Technology (IIT), Caltech and the University of Vermont, merged two distinct technologies, intense X-ray beams and electronic flight simulators, to study how insect muscles can generate such extraordinary levels of power. The results are published in the the January 20,. 2005, issue of the journal Nature.

474

X-ray Microscopy and Imaging (XSD-XMI)  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Imaging (XMI) Imaging (XMI) About XMI Science and Research Beamlines Highlights Software and Tools Intranet Search APS... Argonne Home > Advanced Photon Source > Contacts FAQs Beamlines News Publications APS Email Portal APS Intranet APS Phonebook APS Quick Links for Users APS Safety and Training Welcome to the X-ray Microscopy and Imaging group (XMI)! X-ray Microscopy and Imaging is part of the X-ray Science Division at the Advanced Photon Source. We develop and support a diverse and multidisciplinary user research program at Sectors 2 and 32 of the APS, with the overall goal to image and study materials structures at spatial and temporal resolutions that are most scientifically relevant to the cutting-edge advances in materials, biological, environmental, and biomedical sciences. To achieve this goal, we actively engage in various research activities including

475

Photon Sciences | Beamlines | XPD: X-ray Powder Diffraction  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

XPD: X-ray Powder Diffraction XPD: X-ray Powder Diffraction Poster | Fact Sheet | Preliminary Design Report Scientific Scope XPD is a tunable facility with the ability to collect diffraction data at high x-ray energies (40keV-80keV), offering rapid acquisition (millisecond) and high angular resolution capabilities on the same instrument. XPD addresses future scientific challenges in, for example, hydrogen storage, CO2 sequestration, advanced structural ceramics, catalysis, and materials processing. Such materials of high technological value often are complex, nanostructured and heterogeneous. The scientific grand challenge is to obtain robust and quantitative (micro)structural information, not only in the ground state at ambient conditions, but also in situ or in operando with varying temperature, pressure, magnetic/electric/stress

476

Workshop on Time Domain Science Using X-ray Techniques  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Time-Resolved Beamlines Time-Resolved Beamlines Advisory Committee Workshop Home Workshop Chairs: Lin Chen (Argonne National Laboratory) Steve Milton (Advanced Photon Source) David Reis (University of Michigan) Linda Young (Argonne National Laboratory) Workshop on Time Domain Science Using X-ray Techniques August 29 September 1, 2004, The Abbey, Fontana, Lake Geneva Area, Wisconsin A workshop on "Time Domain Science Using X-ray Techniques" was held from August 29 September 1, 2004 , welcoming both experts and beginners in the field. This is one of the concurrently held workshops in the series on "Future Scientific Directions for the Advanced Photon Source." The goal of the workshop was to identify future directions in scientific research using time resolved x-ray techniques and to address possiblities to produce ps

477

X-RAY FLUORESCENCE MICROPROBE (XFM) TECHNIQUES AND CAPABILITIES  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

RAY FLUORESCENCE MICROPROBE (XFM) RAY FLUORESCENCE MICROPROBE (XFM) TECHNIQUES AND CAPABILITIES APPLICATIONS WORLD-LEADING MICROFOCUSED EXAFS SPECTROSCOPY * XFM is an optimized three-pole wiggler beamline for the characterization of materials in an "as-is" state that are chemically heterogeneous at the micrometer scale via synchrotron induced X-ray fluorescence. * XFM includes instrumentation for microbeam X-ray fluorescence (µXRF), diffraction (µXRD) and fluorescence computed microtomography (FCMT) . However, it is optimized to provide users state-of-the-art microfocused Extended X-ray Absorption Fine Structure (µEXAFS) spectroscopy between 4 to 20 keV. * XFM will trade-off beam size and flux for sample configuration flexibility. This includes more readily achievable stability

478

Portable X-Ray, K-Edge Heavy Metal Detector  

SciTech Connect (OSTI)

The X-Ray, K-Edge Heavy Metal Detection System was designed and built by Ames Laboratory and the Center for Nondestructive Evaluation at Iowa State University. The system uses a C-frame inspection head with an X-ray tube mounted on one side of the frame and an imaging unit and a high purity germanium detector on the other side. the inspection head is portable and can be easily positioned around ventilation ducts and pipes up to 36 inches in diameter. Wide angle and narrow beam X-ray shots are used to identify the type of holdup material and the amount of the contaminant. Precise assay data can be obtained within minutes of the interrogation. A profile of the containerized holdup material and a permanent record of the measurement are immediately available.

Fricke, V.

1999-10-25T23:59:59.000Z

479

Movable anode x-ray source with enhanced anode cooling  

DOE Patents [OSTI]

An x-ray source is disclosed having a cathode and a disc-shaped anode with a peripheral surface at constant radius from the anode axis opposed to the cathode. The anode has stub axle sections rotatably carried in heat conducting bearing plates which are mounted by thermoelectric coolers to bellows which normally bias the bearing plates to a retracted position spaced from opposing anode side faces. The bellows cooperate with the x-ray source mounting structure for forming closed passages for heat transport fluid. Flow of such fluid under pressure expands the bellows and brings the bearing plates into heat conducting contact with the anode side faces. A worm gear is mounted on a shaft and engages serrations in the anode periphery for rotating the anode when flow of coolant is terminated between x-ray emission events. 5 figs.

Bird, C.R.; Rockett, P.D.

1987-08-04T23:59:59.000Z

480

Physical origin of X-ray flares following GRBs  

E-Print Network [OSTI]

One of the major achievements of Swift is the discovery of the erratic X-ray flares harboring nearly half of gamma-ray bursts (GRBs), both for long-duration and short-duration categories, and both for traditional hard GRBs and soft X-ray flashes (XRFs). Here I review the arguments in support of the suggestion that they are powered by reactivation of the GRB central engine, and that the emission site is typically ``internal'', i.e. at a distance within the forward shock front. The curvature effect that characterizes the decaying lightcurve slope during the fading phase of the flares provides an important clue. I will then discuss several suggestions to re-start the GRB central engine and comment on how future observations may help to unveil the physical origin of X-ray flares.

Bing Zhang

2006-02-25T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.