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1

X-rays at Solid-Liquid Interfaces  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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2

X-rays at Solid-Liquid Surfaces  

SciTech Connect (OSTI)

Solid-liquid interfaces play an important role in many areas of current and future technologies, and in our biosphere. They play a key role in the development of nanofluidics and nanotribology, which sensitively depend on our knowledge of the microscopic structures and phenomena at the solid-liquid interface. The detailed understanding of how a fluid meets a wall is also a theoretical challenge. In particular, the phenomena at repulsive walls are of interest, since they affect many different phenomena, such as water-repellent surfaces or the role of the hydrophobic interaction in protein folding. Recent x-ray reflectivity studies of various solid-liquid interfaces have disclosed rather intriguiing phenomena, which will be discussed in this lecture: premelting of ice in contact with silica; liquid Pb in contact with Si; water in contact with hydrophobic surfaces. These experiments, carried out with high-energy x-ray microbeams, reveal detailed insight into the liquid density profile closest to the wall. A detailed insight into atomistic phenomena at solid-liquid interfaces is also a prerequisite in the microscopic control of electrochemical reactions at interfaces. Recent x-ray studies show the enormous future potential of such non-destructive analytical tools for the in situ observation of (electro-)chemical surface reactions. This lecture will review recent x-ray experiments on solid-liquid interfaces.

Dosch, Helmut (Max Planck Institute for Metals Research) [Max Planck Institute for Metals Research

2007-05-02T23:59:59.000Z

3

X-ray standing waves and surface EXAFS studies of electrochemical interfaces  

SciTech Connect (OSTI)

Because of their penetrative power, X-rays are ideally suited for in-situ studies of interfaces in general and solid/liquid interfaces in particular. The recent advent of powerful X-ray synchrotron sources has made experiments of this type feasible. Synchrotron sources offer a broad spectral range of polarized, highly collimated X-rays with intensities that are 10{sup 3}-10{sup 6} higher than those of conventional sources. Moreover, third-generation synchrotron sources, with their projected increase in brightness on the order of 10{sup 4}, will allow for new types of experiments, including the study of dynamic processes in real time. There are a number of X-ray-based surface-sensitive techniques that can be employed in the study of solid/liquid interfaces, including surface EXAFS, X-ray standing waves (XSW), grazing incidence X-ray diffraction (GIXD), and others. In this Account the authors focus on the use of XSW and surface EXAFS. The authors begin with a brief theoretical description followed by experimental aspects of these techniques. The authors then discuss specific examples with emphasis on the underpotential deposition of copper on platinum in the presence and absence of coadsorbates, the potential dependent distribution of interfacial species, and potential dependent structural changes of a redox-active self-assembling monolayer. 33 refs., 7 figs.

Abruna, H.D.; Bommarito, G.M.; Yee, H.S. [Cornell Univ., Ithaca, NY (United States)

1995-06-01T23:59:59.000Z

4

A new endstation at the Swiss Light Source for ultraviolet photoelectron spectroscopy, X-ray photoelectron spectroscopy, and X-ray absorption spectroscopy measurements of liquid solutions  

SciTech Connect (OSTI)

A new liquid microjet endstation designed for ultraviolet (UPS) and X-ray (XPS) photoelectron, and partial electron yield X-ray absorption (XAS) spectroscopies at the Swiss Light Source is presented. The new endstation, which is based on a Scienta HiPP-2 R4000 electron spectrometer, is the first liquid microjet endstation capable of operating in vacuum and in ambient pressures up to the equilibrium vapor pressure of liquid water at room temperature. In addition, the Scienta HiPP-2 R4000 energy analyzer of this new endstation allows for XPS measurements up to 7000 eV electron kinetic energy that will enable electronic structure measurements of bulk solutions and buried interfaces from liquid microjet samples. The endstation is designed to operate at the soft X-ray SIM beamline and at the tender X-ray Phoenix beamline. The endstation can also be operated using a Scienta 5 K ultraviolet helium lamp for dedicated UPS measurements at the vapor-liquid interface using either He I or He II ? lines. The design concept, first results from UPS, soft X-ray XPS, and partial electron yield XAS measurements, and an outlook to the potential of this endstation are presented.

Brown, Matthew A.; Redondo, Amaia Beloqui; Duyckaerts, Nicolas; Mächler, Jean-Pierre [Institute for Chemical and Bioengineering, ETH Zürich, CH-8093 Zürich (Switzerland)] [Institute for Chemical and Bioengineering, ETH Zürich, CH-8093 Zürich (Switzerland); Jordan, Inga; Wörner, Hans Jakob [Laboratory of Physical Chemistry, ETH Zürich, CH-8093 Zürich (Switzerland)] [Laboratory of Physical Chemistry, ETH Zürich, CH-8093 Zürich (Switzerland); Lee, Ming-Tao; Ammann, Markus; Nolting, Frithjof; Kleibert, Armin; Huthwelker, Thomas; Birrer, Mario; Honegger, Juri; Wetter, Reto [Paul Scherrer Institute, CH-5232 Villigen PSI (Switzerland)] [Paul Scherrer Institute, CH-5232 Villigen PSI (Switzerland); Bokhoven, Jeroen A. van [Institute for Chemical and Bioengineering, ETH Zürich, CH-8093 Zürich (Switzerland) [Institute for Chemical and Bioengineering, ETH Zürich, CH-8093 Zürich (Switzerland); Paul Scherrer Institute, CH-5232 Villigen PSI (Switzerland)

2013-07-15T23:59:59.000Z

5

X-ray resonant magnetic scattering from structurally and magnetically rough interfaces in multilayered systems. I. Specular reflectivity  

E-Print Network [OSTI]

X-ray resonant magnetic scattering from structurally and magnetically rough interfaces formulation of x-ray resonant magnetic scattering from rough surfaces and interfaces is given for specular/Fe multilayer. DOI: 10.1103/PhysRevB.68.224409 PACS number s : 75.70.Cn, 61.10.Kw I. INTRODUCTION X-ray

Haskel, Daniel

6

Ultrafast conversions between hydrogen bonded structures in liquid water observed by femtosecond x-ray spectroscopy  

SciTech Connect (OSTI)

We present the first femtosecond soft x-ray spectroscopy in liquids, enabling the observation of changes in hydrogen bond structures in water via core-hole excitation. The oxygen K-edge of vibrationally excited water is probed with femtosecond soft x-ray pulses, exploiting the relation between different water structures and distinct x-ray spectral features. After excitation of the intramolecular OH stretching vibration, characteristic x-ray absorption changes monitor the conversion of strongly hydrogen-bonded water structures to more disordered structures with weaker hydrogen-bonding described by a single subpicosecond time constant. The latter describes the thermalization time of vibrational excitations and defines the characteristic maximum rate with which nonequilibrium populations of more strongly hydrogen-bonded water structures convert to less-bonded ones. On short time scales, the relaxation of vibrational excitations leads to a transient high-pressure state and a transient absorption spectrum different from that of statically heated water.

Wen, Haidan; Huse, Nils; Schoenlein, Robert W.; Lindenberg, Aaron M.

2010-05-01T23:59:59.000Z

7

A microfocus x-ray source based on a nonmetal liquid-jet anode  

SciTech Connect (OSTI)

We demonstrate stable operation of a nonmetallic anode in an electron-impact x-ray source. A high-brightness electron beam is focused on a {approx}70 m/s speed, {approx}10 {mu}m diameter methanol jet producing stable x-ray emission with peak spectral brightness at {approx}5.4x10{sup 5} photons/(sx{mu}m{sup 2}xsrx0.1%BW). The jet is fully evaporated in the interaction point. The shape of a simulated spectrum using Monte Carlo methods shows good agreement with experimental data, and the theoretical brightness values give an upper limit for the achievable x-ray emission from jets with very high velocities. Using this anode concept, all compounds and elements found in liquid form are potentially usable for x-ray generation.

Tuohimaa, T.; Ewald, J.; Schlie, M.; Hertz, H. M.; Vogt, U. [Biomedical and X-ray Physics, Department of Applied Physics, KTH Royal Institute of Technology/Albanova, SE-10691 Stockholm (Sweden); Fernandez-Varea, J. M. [Facultat de Fisica (ECM), Universitat de Barcelona, Diagonal 647, ES-08028 Barcelona (Spain)

2008-06-09T23:59:59.000Z

8

X-ray fluorescence spectroscopy from ions at charged vapor/water interfaces  

E-Print Network [OSTI]

X-ray fluorescence spectra from monovalent ions (Cs+) that accumulate from dilute solutions to form an ion-rich layer near a charged Langmuir monolayer are presented. For the salt solution without the monolayer, the fluorescence signals below the critical angle are significantly lower than the detection sensitivity and only above the critical angle signals from the bulk are observed. In the presence of a monolayer that provides surface charges, strong fluorescence signals below the critical angle are observed. Ion density accumulated at the interface are determined from the fluorescence. The fluorescent spectra collected as a function of incident x-ray energy near the LIII edge yield the extended absorption spectra from the ions, and are compared to recent independent results. The fluorescence data from divalent Ba2+ with and without monolayer are also presented.

Wei Bu; David Vaknin

2009-05-04T23:59:59.000Z

9

A liquid-helium cooled large-area silicon PIN photodiode x-ray detector  

E-Print Network [OSTI]

An x-ray detector using a liquid-helium cooled large-area silicon PIN photodiode has been developed along with a tailor-made charge sensitive preamplifier whose first-stage JFET has been cooled. The operating temperature of the JFET has been varied separately and optimized. The x- and $\\gamma$-ray energy spectra for an \

Yoshizumi Inoue; Shigetaka Moriyama; Hideyuki Hara; Makoto Minowa; Fumio Shimokoshi

1995-04-27T23:59:59.000Z

10

Hort-Range Wetting at Liquid Gallium-Bismuth Alloy Surfaces: X-ray Measurements and Square-Gradient Theory  

SciTech Connect (OSTI)

We present an x-ray reflectivity study of wetting at the free surface of the binary liquid metal alloy gallium-bismuth (Ga-Bi) in the region where the bulk phase separates into Bi-rich and Ga-rich liquid phases. The measurements reveal the evolution of the microscopic structure of the wetting films of the Bi-rich, low-surface-tension phase along several paths in the bulk phase diagram. The wetting of the Ga-rich bulk's surface by a Bi-rich wetting film, the thickness of which is limited by gravity to only 50 Angstroms, creates a Ga-rich/Bi-rich liquid/liquid interface close enough to the free surface to allow its detailed study by x rays. The structure of the interface is determined with Angstromsngstrem resolution, which allows the application of a mean-field square gradient model extended by the inclusion of capillary waves as the dominant thermal fluctuations. The sole free parameter of the gradient model, the influence parameter K, that characterizes the influence of concentration gradients on the interfacial excess energy, is determined from our measurements. This, in turn, allows a calculation of the liquid/liquid interfacial tension, and a separation of the intrinsic and capillary wave contributions to the interfacial structure. In spite of expected deviations from MF behavior, based on the upper critical dimensionality (Du = 3 ) of the bulk, we find that the capillary wave excitations only marginally affect the short-range complete wetting behavior. A critical wetting transition that is sensitive to thermal fluctuations appears to be absent in this binary liquid-metal alloy.

Huber, P.; Shpyrko, O; Pershan, P; Ocko, B; DiMasi, E; Deutsch, M

2009-01-01T23:59:59.000Z

11

Study of liquid gallium at high pressure using synchrotron x-ray  

SciTech Connect (OSTI)

Liquid gallium has been studied at high pressure up to 2 GPa and ambient temperature in a diamond anvil cell using high energy synchrotron x-ray beam. The total x-ray scattering data of liquid gallium were collected up to Q = 12 A{sup -1} and analyzed using pair distribution functions (PDF). The results indicate that the first nearest neighbor peak and second nearest neighbor (shoulder) peak of PDF in liquid gallium does not change with pressure, whereas the higher order (i.e., third and fourth) nearest neighbor peaks shift towards shorter distance with increasing pressure. Reverse Monte Carlo modeling based on the observed data shows that the coordination number in the liquid gallium increases with pressure from 10.5 at 0.3 GPa to 11.6 at 2 GPa. An atomic arrangement similar to the crystalline phase of Ga(II) with coordination number of 12 is proposed for the locally dense-packed rigid unit in liquid gallium. The volume compression data derived from the structure modeling yield a bulk modulus of 12.1(6) GPa for liquid gallium.

Yu, Tony; Guo Quanzhong; Parise, John [Department of Geosciences, Mineral Physics Institute, Stony Brook University, Stony Brook, New York 11794-2100 (United States); Chen Jiuhua [Department of Geosciences, Mineral Physics Institute, Stony Brook University, Stony Brook, New York 11794-2100 (United States); Department of Mechanical and Materials Engineering, Center for the Study of Matters at Extreme Conditions, Florida International University, Miami, Florida 33199 (United States); Ehm, Lars [Department of Geosciences, Mineral Physics Institute, Stony Brook University, Stony Brook, New York 11794-2100 (United States); National Synchrotron Light Source, Brookhaven National Laboratory, Upton, New York 11973-5000 (United States); Huang Shu [Department of Mechanical and Materials Engineering, Center for the Study of Matters at Extreme Conditions, Florida International University, Miami, Florida 33199 (United States); Luo Shengnian [Physics Division, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)

2012-06-01T23:59:59.000Z

12

Spatially resolved x-ray studies of liquid crystals with strongly developed bond-orientational order  

E-Print Network [OSTI]

We present an x-ray study of freely suspended hexatic films of the liquid crystal 3(10)OBC. Our results reveal spatial inhomogeneities of the bond-orientational (BO) order in the vicinity of the hexatic-smectic phase transition and the formation of large scale hexatic domains at lower temperatures. Deep in the hexatic phase up to 25 successive sixfold BO order parameters have been directly determined by means of angular x-ray cross-correlation analysis (XCCA). Such strongly developed hexatic order allowed us to determine higher order correction terms in the scaling relation predicted by the multicritical scaling theory over a full temperature range of the hexatic phase existence.

I. A. Zaluzhnyy; R. P. Kurta; E. A. Sulyanova; O. Y. Gorobtsov; A. G. Shabalin; A. V. Zozulya; A. P. Menushenkov; M. Sprung; B. I. Ostrovskii; I. A. Vartanyants

2014-12-03T23:59:59.000Z

13

Iron near absorption edge X-ray spectroscopy at aqueous-membrane interfaces  

SciTech Connect (OSTI)

Employing synchrotron X-ray scattering, we systematically determine the absorption near-edge spectra (XANES) of iron in its ferrous (Fe2+) and ferric (Fe3+) states both as ions in aqueous solutions and as they bind to form a single layer to anionic templates that consist of carboxyl or phosphate groups at aqueous/vapor interfaces. While the XANES of bulk iron ions show that the electronic state and coordination of iron complexes in the bulk are isotropic, the interfacial bound ions show a signature of a broken inversion-symmetry environment. The XANES of Fe2+ and Fe3+ in the bulk possess distinct profiles however, upon binding they practically exhibit similar patterns. This indicates that both bound ions settle into a stable electronic and coordination configuration with an effective fractional valence (for example, Fe[2+nu]+, 0 < nu < 1) at charged organic templates. Such two dimensional properties may render interfacial iron, abundant in living organisms, a more efficient and versatile catalytic behavior.

Wang, Wenjie; Kuzmenko, Ivan; Vaknin, David

2014-01-01T23:59:59.000Z

14

Synchrotron X-ray Studies of Super-critical Carbon Dioxide / Reservoir Rock Interfaces  

Broader source: Energy.gov [DOE]

Project obectives: Utilize synchrotron X-ray measurements, to monitor all aspects of atomic to nanoscale structural changes resulting from chemical interactions of scCO2-H2O binary fluids with rocks under environments directly relevant to EGS.

15

X-ray reflectivity and surface roughness  

SciTech Connect (OSTI)

Since the advent of high brightness synchrotron radiation sources there has been a phenomenal growth in the use of x-rays as a probe of surface structure. The technique of x-ray reflectivity is particularly relevant to electrochemists since it is capable of probing the structure normal to an electrode surface in situ. In this paper the theoretical framework for x-ray reflectivity is reviewed and the results from previous non-electrochemistry measurements are summarized. These measurements are from the liquid/air interface (CCl/sub 4/), the metal crystal vacuum interface (Au(100)), and from the liquid/solid interface(liquid crystal/silicon). 34 refs., 5 figs.

Ocko, B.M.

1988-01-01T23:59:59.000Z

16

Surface structure of liquid Bi and Sn: An x-ray reflectivity study  

SciTech Connect (OSTI)

X-ray reflectivity measurements of the liquid Bi surface are presented and analyzed together with previous liquid Sn results. Published measurements on liquid Ga, In, and K all exhibit a single strong maximum at a wave-vector transfer of the order of the reciprocal of an atomic-diameter, due to surface-induced layering. In contrast, both Sn and Bi exhibit - in addition - a weak broad peak at much smaller wave-vector transfers. This feature is an unambiguous signature of an enhanced electron density in the near-surface region. Possible ways of modeling this enhancement are presented. Once the different surface-roughening effects of thermal capillary waves are accounted for, the surface structure factors of Sn and Bi are remarkably similar. The principal difference between the two is that the depth of the layering below the surface is more than {approx}40% larger for Bi than for Sn. This is considerably larger than the ratio of their covalent radii which is only {approx}10%. No theoretical explanation can be offered at this time for the surface structure difference between Sn and Bi and other elemental liquid metals studied to date: Ga, In, and K.

Pershan, P.S.; Stoltz, S.E.; Shpyrko, Oleg G.; Deutsch, Moshe; Balagurusamy, V.S.K.; Meron, Mati; Lin, Binhua; Streitel, Reinhard; (Bar-Ilan U.); (Harvard); (UCSD); (UC)

2009-03-23T23:59:59.000Z

17

Multilayer films with sharp, stable interfaces for use in EUV and soft X-ray application  

DOE Patents [OSTI]

The reflectivity and thermal stability of Mo/Si (molybdenum/silicon) multilayer films, used in soft x-ray and extreme ultraviolet region, is enhanced by deposition of a thin layer of boron carbide (e.g., B.sub.4 C) between alternating layers of Mo and Si. The invention is useful for reflective coatings for soft X-ray and extreme ultraviolet optics, multilayer for masks, coatings for other wavelengths and multilayers for masks that are more thermally stable than pure Mo/Si multilayers

Barbee, Jr., Troy W. (Palo Alto, CA); Bajt, Sasa (Livermore, CA)

2002-01-01T23:59:59.000Z

18

Inelastic x-ray scattering study of supercooled liquid and solid silicon.  

SciTech Connect (OSTI)

Momentum-resolved inelastic x-ray scattering (IXS) technique is one of the powerful methods for the study of dynamical properties of a given system even in extreme conditions like high temperature and high pressure. At the same time, experimental studies of physical and structural properties of liquids have multiplied in recent years with the advent of containerless techniques. These methods reduce the possibility of contamination of specimens and remove external nucleation sites. Therefore, by combining the IXS method with the levitation method, the dynamical properties of stable liquids up to 3000 K and supercooled phase of liquids can be studied. Silicon is a basic material in the semiconductor industry and has been the subject of a large amount of experimental and theoretical studies over a long time. In the crystalline phase at ambient conditions, silicon is a diamond-structured semiconductor, but upon melting it undergoes a semiconductor-to-metal transition accompanied by significant changes in the structure and density. The coordination number increases from 4 in the solid to about 6.5 in the liquid, and liquid density is increased by about 10%. The principal purpose of the present study was to determine silicon's elastic modulus from the measurement of averaged sound speed determined from IXS. The experiments were carried out at the Advanced Photon Source (APS) beamline 3-ID with a high-resolution monochromator consisting of two nested channel-cut crystals and four backscattering analyzer setups in the horizontal scattering plane 6 m from the sample. The requirements for very high energy resolution and the basic principles of such instrumentation are discussed elsewhere as referenced. The levitation apparatus was enclosed in a bell jar specially designed for backscattering geometry with a separation of 10 cm between the sample and the detector. Silicon spheres of 2 to 3 mm in diameter were suspended in an argon gas jet and heated with a 270 W CO{sub 2} laser beam. Temperatures were measured during the experiment with a pyrometer whose operating wavelength was 0.65 {micro}m. The temperature gradient on the sample was estimated to be about +/- 20 K. The energy scans were taken for supercooled-liquid and hot-solid silicon at temperature T=1620 K. Sound velocities were determined from the initial slope of the excitation frequencies. Then, the longitudinal moduli for hotsolid and supercooled-liquid silicon were calculated from L = v{sub L}{sup 2}{rho} using measured velocities. In these calculations, density values were taken from Ohsaka et al. as referenced. Results are presented in Table 1. together with room-temperature, hot-solid single-crystal measurements, and stable-liquid values. Room-temperature longitudinal moduli were calculated from the values of the single-crystal elastic constants. They were measured between 300 K and 870 K. Since there was no phase transition up to temperature 1620 K for hot-solid silicon, it is reasonable to extrapolate these data to 1620 K in order to compare to our results for the hot solid. A significant difference (about 20%) is observed between our measurement and the extrapolated single-crystal value of the longitudinal modulus for solid silicon at temperature 1620K. This reduction of the longitudinal modulus may be an indication of the pre-melting. The factor of more than two change in the elastic modulus between supercooled liquid and hot solid at the same temperature can be attributed to the semiconductor-to-metal transition in silicon associated with melting. Also, the longitudinal modulus of the stable liquid is reported in Table 1. About a 10% difference is observed between the modulus of the supercooled and the stable liquid silicon. This can be interpreted as silicon still maintaining metallic properties with a significant increase in the degree of the directional bonding upon supercooling, as found in the x-ray diffraction and ab initio MD studies. All these results are discussed in reference.

Alatas, A.; Said, A.; Sinn, H.; Alp, E.E.; Kodituwakku, C.N.; Saboungi, M.L.; Price, D.L.; X-Ray Science Division; Western Michigan Univ.; Purdue Univ.; CRMD-CNRS; CRMHT-CNRS

2006-01-01T23:59:59.000Z

19

Magnetism at spinel thin film interfaces probed through soft x-ray spectroscopy techniques  

E-Print Network [OSTI]

Magnetism at spinel thin ?lm interfaces probed through softachievable in bulk form. Magnetism at the interface regionand the origin of the magnetism from multiple magnetic

Chopdekar, R.V.

2010-01-01T23:59:59.000Z

20

Structure and Depletion at Fluoro- and Hydro-carbon/Water Liquid/Liquid Interfaces  

E-Print Network [OSTI]

The results of x-ray reflectivity studies of two oil/water (liquid/liquid) interfaces are inconsistent with recent predictions of the presence of a vapor-like depletion region at hydrophobic/aqueous interfaces. One of the oils, perfluorohexane, is a fluorocarbon whose super-hydrophobic interface with water provides a stringent test for the presence of a depletion layer. The other oil, heptane, is a hydrocarbon and, therefore, is more relevant to the study of biomolecular hydrophobicity. These results are consistent with the sub-angstrom proximity of water to soft hydrophobic materials.

Kaoru Kashimoto; Jaesung Yoon; Binyang Hou; Chiu-hao Chen; Binhua Lin; Makoto Aratono; Takanori Takiue; Mark L. Schlossman

2008-07-18T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

X-ray study of the electric double layer at the n-hexane/nanocolloidal silica interface  

E-Print Network [OSTI]

The spatial structure of the transition region between an insulator and an electrolyte solution was studied with x-ray scattering.The electron density profile across the n-hexane/silica sol interface (solutions with 5-nm, 7-nm, and 12-nm colloidal particles) agrees with the theory of the electrical double layer and shows separation of positive and negative charges. The interface consists of three layers, i.e., a compact layer of Na+, a loose monolayer of nanocolloidal particles as part of a thick diffuse layer, and a low-density layer sandwiched between them. Its structure is described by a model in which the potential gradient at the interface reflects the difference in the potentials of "image forces" between the cationic Na+ and anionic nanoparticles and the specific adsorption of surface charge. The density of water in the large electric field (1-10 GV/m) of the transition region and the layering of silica in the diffuse layer is discussed.

Aleksey M. Tikhonov

2006-09-11T23:59:59.000Z

22

Bone Implant Interface Investigation by Synchrotron Radiation X-Ray Microfluorescence  

SciTech Connect (OSTI)

Zinc is known to play a relevant role in growth and development; it has stimulatory effects on in vitro and in vivo bone formation and an inhibitory effect on in vitro osteoclastic bone resorption. The inorganic component of the bone tissue is nonstoichiometric apatite; changes in the composition of hidroxyapatite are subject of studies in order to improve the tissue response after implantation. The objective of this study was to investigate the effect of 0.5% zinc-containing hydroxyapatite in comparison to hydroxyapatite on osseous repair of rabbit's tibia. Cylinders (2x6 mm) of both materials were produced according to the specification of the International Organization for Standardization. Ethics Commission on Teaching and Research in Animals approved this project (HUAP-195/06). Fifteen White New Zealand rabbits were submitted to general anesthesia and two perforations (2 mm) were made in each tibia for implantation of zinc-containing hydroxyapatite cylinders (left tibia) and hydroxyapatite cylinders (right tibia). After 1, 2 and 4 weeks, the animals were killed and one fragment of each tibia with the cylinder was collected and embedded in a methacrylate-based resin and cut into slices (approx200 {mu}m thickness), parallel to the implant's long axis with a precision diamond saw for Synchrotron Radiation X-ray Microfluorescence investigation. The accomplishment of the standard procedures helped the planning, execution and the comparative analysis of the results. The chemical and physical properties of the biomaterials were modified after its implantation and the incorporation of zinc. Both materials are biocompatible and promote osteoconduction and favored bone repair.

Calasans-Maia, M. [Odondology Department, Fluminense Federal Univeristy, Niteroi 24030-900, RJ (Brazil); Sales, E.; Lopes, R. T. [Nuclear Instrumentation Laboratory-PEN/COPPE, Federal Univeristy of Rio de Janeiro, Rio de Janeiro 21941-914, RJ (Brazil); Granjeiro, J. M. [Department of Cell and Molecular Biology, Fluminense Federal University, Niteroi 24030-900, RJ (Brazil); Lima, I. [Odondology Department, Fluminense Federal Univeristy, Niteroi 24030-900, RJ (Brazil); Department of Mechanical Engineering and Energy, Rio de Janeiro State University, Regional Campus-Polytechnic Institute-Alberto Rangel, s/n, Vila Nova, room 308, 28630-050, Nova Friburgo, RJ (Brazil)

2010-04-06T23:59:59.000Z

23

A liquid densitometer with improved sensitivity employing X-ray transmission techniques  

E-Print Network [OSTI]

A CKNOWLEDGEMENTS LIST OF FIGURES I. INTRODUCTION II. DETERMINATION OFLIQUID DENSITY WITH RADIOISOTOPES Selection of Technique and Radiation Type 3 Selection of Detection System Theory of Density Determinsiion by Radiation Trensmission... Selection of Radioisotope III. DETECTION OF LOW ENERGY X-RAYS IV. DESIGN OF DENSITOMETER 13 18 Design Criteria Density Measuring Cell V. CALIBRATION'OF THE DENSITOMETER VI. RESULTS VII. SUMMARY AND CONCLUSIONS APPENDIX I. APPENDIX II. APPENDIX...

Reuscher, Jon Arthur

1962-01-01T23:59:59.000Z

24

Global molecular structure and interfaces : refining an RNA : RNA complex structure using solution x-ray scattering data.  

SciTech Connect (OSTI)

Determining the global architecture of multicomponent systems is a central problem in understanding biomacromolecular machines. Defining interfaces among components and the global structure of multicomponent systems is a central problem in understanding the biological interactions on a molecular level. We demonstrate that solution X-ray scattering data can be used to precisely determine intermolecular interfaces from just the subunit structures, in the complete absence of intermolecular NMR restraints using an example of a 30 kDa RNA-RNA complex. The backbone root-mean-square deviation (rmsd) between structures that are determined using the scattering data and using intermolecular distance restraints is about 0.4 {angstrom}. Further, we refined the global structure of the complex using scattering data as a global restraint. The rmsd in backbone structures that are determined with and without the scattering data refinement is about 3.2 {angstrom}, suggesting the impact of the refinement to the overall structure. Information about the 'global correctness' of solution RNA structures could not be practically obtained otherwise, due to the molecular nature of the RNA molecules, but could only be defined by the scattering data together by residual dipolar couplings. This method provides a powerful new approach for refining global structures of macromolecular complexes whose subunits are elongated.

Zuo, X.; Wang, J.; Foster, T. R.; Schwieters, C. D.; Tiede, D. M.; Butcher, S. E.; Wang, Y.-X.; Chemical Sciences and Engineering Division; NCI-Frederick; Univ. of Wisconin at Madison; NIH

2008-03-19T23:59:59.000Z

25

Characterization of a Fe/Y{sub 2}O{sub 3} metal/oxide interface using neutron and x-ray scattering  

SciTech Connect (OSTI)

The structure of metal/oxide interfaces is important to the radiation resistance of oxide dispersion-strengthened steels. We find evidence of gradual variations in stoichiometry and magnetization across a Fe/Y{sub 2}O{sub 3} metal/oxide heterophase interface using neutron and x-ray reflectometry. These findings suggest that the Fe/Y{sub 2}O{sub 3} interface is a transitional zone approximately ?64?Å-thick containing mixtures or compounds of Fe, Y, and O. Our results illustrate the complex chemical and magnetic nature of Fe/oxide interfaces and demonstrate the utility of combined neutron and x-ray techniques as tools for characterizing them.

Watkins, E. B.; Majewski, J., E-mail: demkowicz@mit.edu, E-mail: jarek@lanl.gov [Lujan Neutron Scattering Center, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Kashinath, A. [Department of Materials Science and Engineering, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States); Computational Modeling Technology, Aramco Research Center—Boston, Cambridge, Massachusetts 02139 (United States); Wang, P. [Lujan Neutron Scattering Center, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Intel Corporation, Hillsboro, Oregon, 97006 (United States); Baldwin, J. K. [Center for Integrated Nanotechnologies, Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States); Demkowicz, M. J., E-mail: demkowicz@mit.edu, E-mail: jarek@lanl.gov [Department of Materials Science and Engineering, Massachusetts Institute of Technology, Cambridge, Massachusetts 02139 (United States)

2014-07-28T23:59:59.000Z

26

Density Profiles of Liquid/Vapor Interfaces Away from Their Critical Point  

E-Print Network [OSTI]

We examine the applicability of various model profiles for the liquid/vapor interface by X-ray reflectivities on water and ethanol and their mixtures at room temperature. Analysis of the X-ray reflecivities using various density profiles shows an error-function like profile is the most adequate within experimental error. Our finding, together with recent observations from simulation studies on liquid surfaces, strongly suggest that the capillary-wave dynamics shapes the interfacial density profile in terms of the error function.

Wei Bu; Doseok Kim; David Vaknin

2014-04-28T23:59:59.000Z

27

Start | View At a Glance | Author Index 220-1 Kinetics of Rapid Redox Processes at the Mineral/Water Interface Using Quick-Scanning X-Ray Absorption Spectroscopy  

E-Print Network [OSTI]

at the Mineral/Water Interface Using Quick-Scanning X-Ray Absorption Spectroscopy (Q-XAS). See more from-situ synchrotron-based technique, quick scanning X-ray absorption spectroscopy (Q-XAS), at sub-second time scales

Sparks, Donald L.

28

X-ray Absorption Spectroscopy of Biologically Relevant Systems  

E-Print Network [OSTI]

308, Messer, B. M. X-ray Absorption Spectroscopy of AqueousSarcosine via X-ray Absorption Spectroscopy 5.1 Introductionwith Carboxylate by X-Ray Absorption Spectroscopy of Liquid

Uejio, Janel Sunayo

2010-01-01T23:59:59.000Z

29

Initial stages of ITO/Si interface formation: In situ x-ray photoelectron spectroscopy measurements upon magnetron sputtering and atomistic modelling using density functional theory  

SciTech Connect (OSTI)

Initial stages of indium tin oxide (ITO) growth on a polished Si substrate upon magnetron sputtering were studied experimentally using in-situ x-ray photoelectron spectroscopy measurements. The presence of pure indium and tin, as well as Si bonded to oxygen at the ITO/Si interface were observed. The experimental observations were compared with several atomistic models of ITO/Si interfaces. A periodic model of the ITO/Si interface was constructed, giving detailed information about the local environment at the interface. Molecular dynamics based on density functional theory was performed, showing how metal-oxygen bonds are broken on behalf of silicon-oxygen bonds. These theoretical results support and provide an explanation for the present as well as previous ex-situ and in-situ experimental observations pointing to the creation of metallic In and Sn along with the growth of SiO{sub x} at the ITO/Si interface.

Løvvik, O. M.; Diplas, S.; Ulyashin, A. [SINTEF Materials and Chemistry, Forskningsveien 1, NO-0314 Oslo (Norway); Romanyuk, A. [University of Basel, Kingelbergstr. 82, CH-4056 Basel (Switzerland)

2014-02-28T23:59:59.000Z

30

The determination of interfacial structure and phase transitions in Al/Cu and Al/Ni interfaces by means of surface extended x-ray absorption fine structure  

SciTech Connect (OSTI)

Surface extended x-ray absorption fine structure (SEXAFS) was used to investigate the interfacial conditions of Al/Cu and Al/Ni shallow buried interfaces. Previous studies using glancing angle extended x-ray absorption fine structure, x-ray reflectivity, photoemission, and SEXAFS produced conflicting results as to whether or not the interfaces between Al and Cu and Al and Ni were reacted upon room temperature deposition. In this study polycrystalline bilayers of Al/Cu and Al/Ni and trilayers of Al/Cu/Al and Al/Ni/Al were deposited on tantalum foil at room temperature in ultra high vacuum and analyzed to evaluate the reactivity of these systems on a nanometer scale. It become overwhelming apparent that the interfacial phase reactions were a function of the vacuum conditions. Samples deposited with the optimum vacuum conditions showed reaction products upon deposition at room temperature which were characterized by comparisons to standards and by least squares fitting the be CuAl{sub 2} and NiAl{sub 3} respectively. The results of this study that the reacted zone thicknesses were readily dependent on the deposition parameters. For both Al on Cu and Al on Ni as well as the metal on Al conditions 10{Angstrom} reaction zones were observed. These reaction zones were smaller than that observed for bilayers of Al on Cu (30{Angstrom}) and Al on Ni (60{Angstrom}) where deposition rates were much higher and samples were much thicker. The reaction species are evident by SEXAFS, where the previous photoemission studies only indicated that changes had occurred. Improved vacuum conditions as compared to the earlier experiments is primarily the reason reactions on deposition were seen in this study as compared to the earlier SEXAFS studies.

Barrera, E.V. (Rice Univ., Houston, TX (United States). Dept. of Mechanical Engineering and Materials Science); Heald, S.M. (Brookhaven National Lab., Upton, NY (United States))

1991-01-01T23:59:59.000Z

31

The determination of interfacial structure and phase transitions in Al/Cu and Al/Ni interfaces by means of surface extended x-ray absorption fine structure  

SciTech Connect (OSTI)

Surface extended x-ray absorption fine structure (SEXAFS) was used to investigate the interfacial conditions of Al/Cu and Al/Ni shallow buried interfaces. Previous studies using glancing angle extended x-ray absorption fine structure, x-ray reflectivity, photoemission, and SEXAFS produced conflicting results as to whether or not the interfaces between Al and Cu and Al and Ni were reacted upon room temperature deposition. In this study polycrystalline bilayers of Al/Cu and Al/Ni and trilayers of Al/Cu/Al and Al/Ni/Al were deposited on tantalum foil at room temperature in ultra high vacuum and analyzed to evaluate the reactivity of these systems on a nanometer scale. It become overwhelming apparent that the interfacial phase reactions were a function of the vacuum conditions. Samples deposited with the optimum vacuum conditions showed reaction products upon deposition at room temperature which were characterized by comparisons to standards and by least squares fitting the be CuAl{sub 2} and NiAl{sub 3} respectively. The results of this study that the reacted zone thicknesses were readily dependent on the deposition parameters. For both Al on Cu and Al on Ni as well as the metal on Al conditions 10{Angstrom} reaction zones were observed. These reaction zones were smaller than that observed for bilayers of Al on Cu (30{Angstrom}) and Al on Ni (60{Angstrom}) where deposition rates were much higher and samples were much thicker. The reaction species are evident by SEXAFS, where the previous photoemission studies only indicated that changes had occurred. Improved vacuum conditions as compared to the earlier experiments is primarily the reason reactions on deposition were seen in this study as compared to the earlier SEXAFS studies.

Barrera, E.V. [Rice Univ., Houston, TX (United States). Dept. of Mechanical Engineering and Materials Science; Heald, S.M. [Brookhaven National Lab., Upton, NY (United States)

1991-12-31T23:59:59.000Z

32

Setup for in situ investigation of gases and gas/solid interfaces by soft x-ray emission and absorption spectroscopy  

SciTech Connect (OSTI)

We present a novel gas cell designed to study the electronic structure of gases and gas/solid interfaces using soft x-ray emission and absorption spectroscopies. In this cell, the sample gas is separated from the vacuum of the analysis chamber by a thin window membrane, allowing in situ measurements under atmospheric pressure. The temperature of the gas can be regulated from room temperature up to approximately 600?°C. To avoid beam damage, a constant mass flow can be maintained to continuously refresh the gaseous sample. Furthermore, the gas cell provides space for solid-state samples, allowing to study the gas/solid interface for surface catalytic reactions at elevated temperatures. To demonstrate the capabilities of the cell, we have investigated a TiO{sub 2} sample behind a mixture of N{sub 2} and He gas at atmospheric pressure.

Benkert, A., E-mail: andreas.benkert@kit.edu, E-mail: l.weinhardt@kit.edu [Institute for Photon Science and Synchrotron Radiation, Karlsruhe Institute of Technology (KIT), Hermann-v.-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany); Universität Würzburg, Experimentelle Physik VII, Am Hubland, 97074 Würzburg (Germany); Gemeinschaftslabor für Nanoanalytik, Karlsruhe Institute of Technology (KIT), 76021 Karlsruhe (Germany); Blum, M. [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States) [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States); Advanced Light Source, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720 (United States); Meyer, F. [Universität Würzburg, Experimentelle Physik VII, Am Hubland, 97074 Würzburg (Germany)] [Universität Würzburg, Experimentelle Physik VII, Am Hubland, 97074 Würzburg (Germany); Wilks, R. G. [Solar Energy Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Hahn-Meitner-Platz 1, 14109 Berlin (Germany)] [Solar Energy Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Hahn-Meitner-Platz 1, 14109 Berlin (Germany); Yang, W. [Advanced Light Source, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720 (United States)] [Advanced Light Source, Lawrence Berkeley National Laboratory, 1 Cyclotron Road, Berkeley, California 94720 (United States); Bär, M. [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States) [Department of Chemistry, University of Nevada, Las Vegas (UNLV), 4505 Maryland Parkway, Nevada 89154-4003 (United States); Solar Energy Research, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, Hahn-Meitner-Platz 1, 14109 Berlin (Germany); Insitut für Physik und Chemie, Brandenburgische Technische Universität Cottbus-Senftenberg, Konrad-Wachsmann-Allee 1, 03046 Cottbus (Germany); and others

2014-01-15T23:59:59.000Z

33

Reduced graphene oxide based silver sulfide hybrid films formed at a liquid/liquid interface  

SciTech Connect (OSTI)

Free-standing, ultra-thin films of silver sulfide and reduced graphene oxide (RGO) based silver sulfide hybrids are prepared at a liquid/liquid interface employing in situ chemical reaction strategy. Ag{sub 2}S and RGO?Ag{sub 2}S hybrid films are characterized by various techniques such as UV-visible and photo luminescence spectroscopy, X-ray diffraction and scanning electron microscopy. The morphology of hybrid films consists of Ag{sub 2}S nanocrystals on RGO surface while Ag{sub 2}S films contains branched network of dendritic structures. RGO?Ag{sub 2}S exhibit interesting optical and electrical properties. The hybrid films absorb in the region 500–650 nm and show emission in the red region. A higher conductance is observed for the hybrid films arising from the RGO component. This simple low cost method can be extended to prepare other RGO based metal sulfides.

Bramhaiah, K., E-mail: jsneena@csmr.res.in; John, Neena S., E-mail: jsneena@csmr.res.in [Centre for Soft Matter Research, P.B. No.1329, Jalahalli, Bangalore-560013 (India)

2014-04-24T23:59:59.000Z

34

Use of X-Ray Absorption Spectroscopy to Monitor the Kinetics of Metal Sorption Reactions at the Soil/Water Interface  

E-Print Network [OSTI]

Use of X-Ray Absorption Spectroscopy to Monitor the Kinetics of Metal Sorption Reactions on the surface coordination environment of Ni sorbed onto clays and aluminum oxides using X-ray absorption fine

Sparks, Donald L.

35

Ionic Liquid-Enhanced Solid State Electrolyte Interface (SEI...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Liquid-Enhanced Solid State Electrolyte Interface (SEI) for Lithium Sulfur Batteries. Ionic Liquid-Enhanced Solid State Electrolyte Interface (SEI) for Lithium Sulfur Batteries....

36

X-ray scattering studies of structure and dynamics of surfaces and interfaces of polymeric liquids  

E-Print Network [OSTI]

and S. K. Sinha, “Structure and dynamics of thin polymer ?Scattering Studies of Structure and Dynamics of Surfaces andScattering Studies of Structure and Dynamics of Surfaces and

Jiang, Zhang

2007-01-01T23:59:59.000Z

37

X-ray photoelectron spectroscopy and ultraviolet photoelectron spectroscopy investigation of Al-related dipole at the HfO{sub 2}/Si interface  

SciTech Connect (OSTI)

The presence of an ultrathin oxide layer at the high-k/SiO{sub 2} interface may result in an interfacial dipole related to the specific high-k dielectric used for the gate stacks. 1 nm HfO{sub 2}/x nmAl{sub 2}O{sub 3}/SiO{sub 2}/Si stacks with different x values (x=0, 0.4, 0.8, 1.2) have been prepared by atomic layer deposition. Using photoelectron spectroscopy, an Al-related interfacial dipole in the HfO{sub 2}/Al{sub 2}O{sub 3}/SiO{sub 2} gate stack has been identified. X-ray photoelectron spectroscopy analysis shows that the dipole is correlated with the formation of an interfacial Al-silicate. The dipole is located at the Al-silicate interface between Al{sub 2}O{sub 3} and SiO{sub 2}, and its strength increases with the increase in Al{sub 2}O{sub 3} thickness because of Al silicate growth. Such Al-related interfacial dipole should have potential applications in future positive metal-oxide-semiconductor devices.

Zhu, L. Q.; Barrett, N.; Jegou, P. [Groupe Photoemission, CEA/IRAMIS/SPCSI, F-91191 Gif-sur-Yvette (France); Martin, F.; Leroux, C.; Martinez, E.; Grampeix, H.; Renault, O.; Chabli, A. [CEA-LETI, MINATEC, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France)

2009-01-15T23:59:59.000Z

38

X-Ray Data Booklet X-RAY DATA BOOKLET  

E-Print Network [OSTI]

X-Ray Data Booklet X-RAY DATA BOOKLET Center for X-ray Optics and Advanced Light Source Lawrence Berkeley National Laboratory Introduction X-Ray Properties of Elements Electron Binding Energies X-Ray Levels of Few Electron Ions Now Available Order X-Ray Data Booklet http://xdb.lbl.gov/ (1 of 3) [2

Meagher, Mary

39

Small-angle x-ray scattering measurements of the microstructure of liquid helium mixtures adsorbed in aerogel  

SciTech Connect (OSTI)

Small-angle x-ray scattering (SAXS) was used to measure the microstructure of isotopic mixtures of {sup 3}He and {sup 4}He adsorbed into silica aerogels as a function of temperature and {sup 3}He concentration. The SAXS measurements could be well described by the formation of a nearly pure film of {sup 4}He which separates from the bulk mixture onto the aerogel strands and which thickens with decreasing temperature. Previous observations of a superfluid {sup 3}He-rich phase are consistent with superfluidity existing within this film phase. Observed differences between different density aerogels are explained in terms of the depletion of {sup 4}He from the bulk mixture due to film formation.

Lurio, L. B.; Mulders, N.; Paetkau, M.; Chan, M. H. W.; Mochrie, S. G. J. [Department of Physics, Northern Illinois University, DeKalb, Illinois 60115 (United States); Department of Physics, University of Delaware, Newark, Delaware 19716 (United States); Department of Physics and Astronomy, Okanagan College, British Columbia V1Y4X8 (Canada); Department of Physics, Pennsylvania State University, University Park, Pennsylvania 16802 (United States); Department of Physics, Yale University, New Haven, Connecticut 06511 (United States)

2007-07-15T23:59:59.000Z

40

Systems and methods for monitoring a solid-liquid interface  

DOE Patents [OSTI]

Systems and methods are provided for monitoring a solid-liquid interface during a casting process. The systems and methods enable determination of the location of a solid-liquid interface during the casting process.

Stoddard, Nathan G; Lewis, Monte A.; Clark, Roger F

2013-06-11T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Electrochemical flowcell for in-situ investigations by soft x-ray absorption and emission spectroscopy  

SciTech Connect (OSTI)

A new liquid flow-cell designed for electronic structure investigations at the liquid-solid interface by soft X-ray absorption and emission spectroscopy is presented. A thin membrane serves simultaneously as a substrate for the working electrode and solid state samples as well as for separating the liquid from the surrounding vacuum conditions. In combination with counter and reference electrodes this approach allows in-situ studies of electrochemical deposition processes and catalytic reactions at the liquid-solid interface in combination with potentiostatic measurements. As model system in-situ monitoring of the deposition process of Co metal from a 10 mM CoCl{sub 2} aqueous solution by X-ray absorption and emission spectroscopy is presented.

Schwanke, C.; Lange, K. M., E-mail: Kathrin.lange@helmholtz-berlin.de [Helmholtz-Zentrum Berlin für Materialien und Energie, Institute of Solar Fuels, Albert-Einstein-Straße 15, 12489 Berlin (Germany); Golnak, R.; Xiao, J. [Helmholtz-Zentrum Berlin für Materialien und Energie, Institute of Methods for Material Development, Albert-Einstein-Straße 15, 12489 Berlin (Germany)

2014-10-15T23:59:59.000Z

42

Indus-2 X-ray lithography beamline for X-ray optics and material science applications  

SciTech Connect (OSTI)

X-ray lithography is an ideal technique by which high aspect ratio and high spatial resolution micro/nano structures are fabricated using X-rays from synchrotron radiation source. The technique has been used for fabricating optics (X-ray, visible and infrared), sensors and actuators, fluidics and photonics. A beamline for X-ray lithography is operational on Indus-2. The beamline offers wide lithographic window from 1-40keV photon energy and wide beam for producing microstructures in polymers upto size ?100mm × 100mm. X-ray exposures are possible in air, vacuum and He gas environment. The air based exposures enables the X-ray irradiation of resist for lithography and also irradiation of biological and liquid samples.

Dhamgaye, V. P., E-mail: vishal@rrcat.gov.in; Lodha, G. S., E-mail: vishal@rrcat.gov.in [Indus Synchrotrons Utilisation Division, Raja Ramanna Centre for Advanced Technology, Indore-452013 (India)

2014-04-24T23:59:59.000Z

43

X-ray beamsplitter  

DOE Patents [OSTI]

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5--50 pairs of alternate Mo/Si layers with a period of 20--250 A. The support membrane is 10--200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window. 6 figs.

Ceglio, N.M.; Stearns, D.G.; Hawryluk, A.M.; Barbee, T.W. Jr.

1987-08-07T23:59:59.000Z

44

X-ray beamsplitter  

DOE Patents [OSTI]

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

Ceglio, Natale M. (Livermore, CA); Stearns, Daniel S. (Mountain View, CA); Hawryluk, Andrew M. (Modesto, CA); Barbee, Jr., Troy W. (Palo Alto, CA)

1989-01-01T23:59:59.000Z

45

Chest x-Rays  

Broader source: Energy.gov [DOE]

The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica.

46

X-ray binaries  

E-Print Network [OSTI]

We review the nuclear astrophysics aspects of accreting neutron stars in X-ray binaries. We summarize open astrophysical questions in light of recent observations and their relation to the underlying nuclear physics. Recent progress in the understanding of the nuclear physics, especially of X-ray bursts, is also discussed.

H. Schatz; K. E. Rehm

2006-08-01T23:59:59.000Z

47

Macromol. Rapid Commun. 19, 557561 (1998) 557 X-ray microscopy of novel thermoplastic/liquid crystalline  

E-Print Network [OSTI]

for applications such as recycling. Introduction Blending immiscible polymers constitutes a crucial means by which solid-state blending variations12, 13) , to highly incompatible or recycled polymeric materials part In this study, blends of the thermoplastic poly(ethylene ter- ephthalate) (PET) and the liquid

48

Quantification of Liquid Water Saturation in a PEM Fuel Cell Diffusion Medium Using X-ray Microtomography  

E-Print Network [OSTI]

Quantification of Liquid Water Saturation in a PEM Fuel Cell Diffusion Medium Using X understanding of the two-phase flow and flooding occurrence in proton exchange membrane PEM fuel cells. We have as ice formation during cold start of PEM fuel cells. The water present in these porous layers

49

X-ray laser  

DOE Patents [OSTI]

An X-ray laser (10) that lases between the K edges of carbon and oxygen, i.e. between 44 and 23 Angstroms, is provided. The laser comprises a silicon (12) and dysprosium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state nickel-like dysprosium ions (34) are resonantly photo-pumped to their upper X-ray laser state by line emission from hydrogen-like silicon ions (32). The novel X-ray laser should prove especially useful for the microscopy of biological specimens.

Nilsen, Joseph (Livermore, CA)

1991-01-01T23:59:59.000Z

50

Interface for liquid chromatograph-mass spectrometer  

DOE Patents [OSTI]

A moving belt interface for real-time, high-performance liquid chromatograph (HPLC)/mass spectrometer (MS) analysis which strips away the HPLC solvent as it emerges from the end of the HPLC column and leaves a residue suitable for mass-spectral analysis. The interface includes a portable, stand-alone apparatus having a plural stage vacuum station, a continuous ribbon or belt, a drive train magnetically coupled to an external drive motor, a calibrated HPLC delivery system, a heated probe tip and means located adjacent the probe tip for direct ionization of the residue on the belt. The interface is also capable of being readily adapted to fit any mass spectrometer.

Andresen, Brian D. (Pleasanton, CA); Fought, Eric R. (Livermore, CA)

1989-01-01T23:59:59.000Z

51

Interface for liquid chromatograph-mass spectrometer  

DOE Patents [OSTI]

A moving belt interface is described for real-time, high-performance liquid chromatograph (HPLC)/mass spectrometer (MS) analysis which strips away the HPLC solvent as it emerges from the end of the HPLC column and leaves a residue suitable for mass-spectral analysis. The interface includes a portable, stand-alone apparatus having a plural stage vacuum station, a continuous ribbon or belt, a drive train magnetically coupled to an external drive motor, a calibrated HPLC delivery system, a heated probe tip and means located adjacent the probe tip for direct ionization of the residue on the belt. The interface is also capable of being readily adapted to fit any mass spectrometer. 8 figs.

Andresen, B.D.; Fought, E.R.

1989-09-19T23:59:59.000Z

52

X-ray absorption spectroscopy  

E-Print Network [OSTI]

009-9473-8 REVIEW X-ray absorption spectroscopy Junko Yano Æand application of X-ray absorption spectroscopy, bothX-ray absorption near-edge structure (XANES) and extended X-

Yano, Junko; Yachandra, Vittal K.

2009-01-01T23:59:59.000Z

53

X-ray Absorption Spectroscopy  

E-Print Network [OSTI]

type: Review X-ray Absorption Spectroscopy Junko Yano andPhotosystem II; XAS, X-ray absorption spectroscopy; EXAFS,X-ray absorption fine structure; EPR, electron paramagnetic

Yano, Junko

2010-01-01T23:59:59.000Z

54

X-ray Diffraction Laboratory: Department of Chemistry Texas A & M University  

E-Print Network [OSTI]

X-ray Diffraction Laboratory: Department of Chemistry Texas A & M University Doc. No: SOPUSERFD form that can be accessed by the X-ray diffraction webpage. RESPONSIBILITY: The X-ray Diffraction and suggestions in a timely manner. MATERIALS: · Computer Database · Web interface #12;X-ray Diffraction

Meagher, Mary

55

X-ray beam finder  

DOE Patents [OSTI]

An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

Gilbert, H.W.

1983-06-16T23:59:59.000Z

56

The limits of ultrahigh-resolution x-ray mapping: estimating uncertainties in thin-film and interface structures determined by phase retrieval methods  

SciTech Connect (OSTI)

Capturing subtle details at the sub-Angstrom level is key to understanding the structural basis of many intriguing interfacial phenomena in epitaxial thin films and nanostructures. X-ray phase retrieval methods are ideally suited to this task but the usual approaches for determination of uncertainties, based on refining a parametrized model, are not applicable in this case. Here we describe a method to estimate the uncertainties of the system electron density, obtained by phase retrieval, and of parameters of interest obtained from it. The method is based on the bootstrap approach and it can be generally applied to surface x-ray scattering data. Several examples are given which illustrate the method's utility in determining uncertainties arising from random and systematic errors. The approach also provides a quantitative measure of the validity of structural solutions obtained by phase retrieval methods.

Zhou H.; Pindak R.; Clarke, R.; Steinberg, D.NM.; Yacoby, Y.

2012-04-25T23:59:59.000Z

57

Synchrotron x-ray reflectivity study of oxidation/passivation of copper and silicon.  

SciTech Connect (OSTI)

Synchrotron x-ray-scattering technique studies of copper and silicon electrochemical interfaces are reported. These two examples illustrate the application of synchrotron x-ray techniques for oxidation, passivation, and dissolution of metals and semiconductors.

Chu, Y.; Nagy, Z.; Parkhutik, V.; You, H.

1999-07-21T23:59:59.000Z

58

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample6, 2011 LawrenceE C H NLensless X-RayLensless X-Ray

59

The X-ray crystal structure of Shewanella oneidensis OmcA reveals new insight at the microbe-mineral interface  

SciTech Connect (OSTI)

The x-ray crystal structure of Shewanella oneidensis OmcA, an extracellular decaheme cytochrome involved in mineral reduction, was solved to a resolution of 2.7 Å. The four OmcA molecules in the asymmetric unit were arranged so the distance between heme-5 on adjacent OmcA monomers was less than 1 nm, indicative of a transient OmcA dimer capable of intermolecular electron transfer. A previously identified hematite binding motif was identified near heme 10, forming a hydroxylated surface that would bring a heme-10 electron egress site to ~ 1 nm of mineral surface.

Edwards, Marcus; Baiden, Nanakow; Johs, Alexander; Tomanicek, Stephen J.; Liang, Liyuan; Shi, Liang; Fredrickson, Jim K.; Zachara, John M.; Gates, Andrew J.; Butt, Julea N.; Richardson, David; Clarke, Thomas A.

2014-05-21T23:59:59.000Z

60

Fluctuation X-Ray Scattering  

SciTech Connect (OSTI)

The work supported by the grant was aimed at developing novel methods of finding the structures of biomolecules using x-rays from novel sources such as the x-ray free electron laser and modern synchrotrons

Saldin, PI: D. K.; Co-I's: J. C. H. Spence and P. Fromme

2013-01-25T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

Beyond hard x-ray photoelectron spectroscopy: Simultaneous combination with x-ray diffraction  

SciTech Connect (OSTI)

Hard x-ray photoelectron spectroscopy (HAXPES) is a powerful and novel emerging technique for the nondestructive determination of electronic properties and chemical composition of bulk, buried interfaces and surfaces. It benefits from the exceptionally large escape depth of high kinetic energy photoelectrons, increasing the information depth up to several tens of nanometers. Complementing HAXPES with an atomic structure sensitive technique (such as x-ray diffraction) opens a new research field with major applications for materials science. At SpLine, the Spanish CRG beamline at the European Synchrotron Radiation Facility, we have developed a novel experimental set-up that combines HAXPES and x-ray diffraction (x-ray reflectivity, surface x-ray diffraction, grazing incidence x-ray diffraction, and reciprocal space maps). Both techniques can be operated simultaneously on the same sample and using the same excitation source. The set-up includes a robust 2S + 3D diffractometer hosting a ultrahigh vacuum chamber equipped with a unique photoelectron spectrometer (few eV < electron kinetic energy < 15 keV), x-ray tube (Mg/Ti), 15 keV electron gun, and auxiliary standard surface facilities (molecular beam epitaxy evaporator, ion gun, low energy electron diffraction, sample heating/cooling system, leak valves, load-lock sample transfer, etc.). This end-station offers the unique possibility of performing simultaneous HAXPES + x-ray diffraction studies. In the present work, we describe the experimental set-up together with two experimental examples that emphasize its outstanding capabilities: (i) nondestructive characterization of the Si/Ge and HfO{sub 2}/SiO{sub 2} interfaces on Ge-based CMOS devices, and (ii) strain study on La{sub 0.7}Ca{sub 0.3}MnO{sub 3} ultrathin films grown on SrTiO{sub 3}(001) substrate.

Rubio-Zuazo, Juan; Castro, German R. [SpLine, Spanish CRG beamline at the European Synchrotron Radiation Facility, B.P. 220, F-38043 Grenoble (France) and ICMM-CSIC Cantoblanco, E-28049 Madrid (Spain)

2013-05-15T23:59:59.000Z

62

X-ray Pinhole Camera Measurements  

SciTech Connect (OSTI)

The development of the rod pinch diode [1] has led to high-resolution radiography for dynamic events such as explosive tests. Rod pinch diodes use a small diameter anode rod, which extends through the aperture of a cathode plate. Electrons borne off the aperture surface can self-insulate and pinch onto the tip of the rod, creating an intense, small x-ray source (Primary Pinch). This source has been utilized as the main diagnostic on numerous experiments that include high-value, single-shot events. In such applications there is an emphasis on machine reliability, x-ray reproducibility, and x-ray quality [2]. In tests with the baseline rod pinch diode, we have observed that an additional pinch (Secondary Pinch) occurs at the interface near the anode rod and the rod holder. This suggests that stray electrons exist that are not associated with the Primary Pinch. In this paper we present measurements on both pinches using an x-ray pinhole camera. The camera is placed downstream of the Primary Pinch at an angle of 60° with respect to the diode centerline. This diagnostic will be employed to diagnose x-ray reproducibility and quality. In addition, we will investigate the performance of hybrid diodes relating to the formation of the Primary and Secondary Pinches.

Nelson, D. S. [NSTec; Berninger, M. J. [NSTec; Flores, P. A. [NSTec; Good, D. E. [NSTec; Henderson, D. J. [NSTec; Hogge, K. W. [NSTec; Huber, S. R. [NSTec; Lutz, S. S. [NSTec; Mitchell, S. E. [NSTec; Howe, R. A. [NSTec; Mitton, C. V. [NSTec; Molina, I. [NSTec; Bozman, D. R. [SNL; Cordova, S. R. [SNL; Mitchell, D. R. [SNL; Oliver, B. V. [SNL; Ormond, E. C. [SNL

2013-07-01T23:59:59.000Z

63

Tunable X-ray source  

DOE Patents [OSTI]

A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

Boyce, James R. (Williamsburg, VA)

2011-02-08T23:59:59.000Z

64

In situ x-ray photoelectron spectroscopy for electrochemical reactions in ordinary solvents  

SciTech Connect (OSTI)

In situ electrochemical X-ray photoelectron spectroscopy (XPS) apparatus, which allows XPS at solid/liquid interfaces under potential control, was constructed utilizing a microcell with an ultra-thin Si membrane, which separates vacuum and a solution. Hard X-rays from a synchrotron source penetrate into the Si membrane surface exposed to the solution. Electrons emitted at the Si/solution interface can pass through the membrane and be analyzed by an analyzer placed in vacuum. Its operation was demonstrated for potential-induced Si oxide growth in water. Effect of potential and time on the thickness of Si and Si oxide layers was quantitatively determined at sub-nanometer resolution.

Masuda, Takuya [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan) [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan); PRESTO, Japan Science and Technology Agency (JST), 4-1-8 Honcho, Kawaguchi, Saitama 333-0012 (Japan); Yoshikawa, Hideki; Kobata, Masaaki; Kobayashi, Keisuke [Synchrotron X-ray Station at SPring-8, National Institute for Materials Science (NIMS), Sayo, Hyogo 679-5148 (Japan)] [Synchrotron X-ray Station at SPring-8, National Institute for Materials Science (NIMS), Sayo, Hyogo 679-5148 (Japan); Noguchi, Hidenori [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan) [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan); PRESTO, Japan Science and Technology Agency (JST), 4-1-8 Honcho, Kawaguchi, Saitama 333-0012 (Japan); Graduate School of Chemical Sciences and Engineering, Hokkaido University, Sapporo, Hokkaido 060-0810 (Japan); International Center for Materials Nanoarchitectonics (WPI-MANA), National Institute for Materials Science (NIMS), Tsukuba, Ibaraki 305-0044 (Japan); Kawasaki, Tadahiro [Graduate School of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya 464-8603 (Japan)] [Graduate School of Engineering, Nagoya University, Furo-cho, Chikusa, Nagoya 464-8603 (Japan); Uosaki, Kohei [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan) [Global Research Center for Environment and Energy Based on Nanomaterials Science (GREEN), National Institute for Materials Science (NIMS), Tsukuba 305-0044 (Japan); Graduate School of Chemical Sciences and Engineering, Hokkaido University, Sapporo, Hokkaido 060-0810 (Japan); International Center for Materials Nanoarchitectonics (WPI-MANA), National Institute for Materials Science (NIMS), Tsukuba, Ibaraki 305-0044 (Japan)

2013-09-09T23:59:59.000Z

65

X-ray lithography source  

DOE Patents [OSTI]

A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits is disclosed. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and eliminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an excellent moderate-priced X-ray source for lithography. 26 figures.

Piestrup, M.A.; Boyers, D.G.; Pincus, C.

1991-12-31T23:59:59.000Z

66

X-ray lithography source  

DOE Patents [OSTI]

A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and elminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an exellent moderate-priced X-ray source for lithography.

Piestrup, Melvin A. (Woodside, CA); Boyers, David G. (Mountain View, CA); Pincus, Cary (Sunnyvale, CA)

1991-01-01T23:59:59.000Z

67

X-Ray Diagnostics  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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68

A combined droplet train and ambient pressure photoemission spectrometer for the investigation of liquid/vapor interfaces  

SciTech Connect (OSTI)

We describe a combined ambient pressure photoelectron spectroscopy/droplet train apparatus for investigating the nature and heterogeneous chemistry of liquid/vapor interfaces. In this instrument a liquid droplet train with typical droplet diameters from 50...150 {micro}m is produced by a vibrating orifice aerosol generator (VOAG). The droplets are irradiated by soft X-rays (100...1500 eV) in front of the entrance aperture of a differentially pumped electrostatic lens system that transfers the emitted electrons into a conventional hemispherical electron analyzer. The photoemission experiments are performed at background pressures of up to several Torr, which allows the study of environmentally important liquid/vapor interfaces, in particular aqueous solutions, under equilibrium conditions. The exposure time of the droplet surface to the background gases prior to the XPS measurement can be varied, which will allow future kinetic measurements of gas uptake on liquid surfaces. As an example, a measurement of the surface composition of a {chi} = 0.21 aqueous methanol solution is presented. The concentration of methanol at the vapor/liquid interface is enhanced by a factor of about 3 over the bulk value, while the expected bulk value is recovered at depths larger than about 1.5 nm.

Starr, David E.; Wong, Ed K.; Worsnop, Douglas R.; Wilson, Kevin R.; Bluhm, Hendrik

2008-05-01T23:59:59.000Z

69

Liquid/Liquid Interface Polymerized Porphyrin Membranes Displaying Size-Selective Molecular and Ionic Permeability  

E-Print Network [OSTI]

Liquid/Liquid Interface Polymerized Porphyrin Membranes Displaying Size-Selective Molecular: December 5, 2005 Thin polymeric membranes have been formed by liquid/liquid interfacial copolymerization of controllable thickness to be obtained.7 The polymerization of 1 was accomplished by condensation of porphyrin

70

Miniature x-ray source  

DOE Patents [OSTI]

A miniature x-ray source capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature x-ray source comprises a compact vacuum tube assembly containing a cathode, an anode, a high voltage feedthru for delivering high voltage to the anode, a getter for maintaining high vacuum, a connection for an initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is highly x-ray transparent and made, for example, from boron nitride. The compact size and potential for remote operation allows the x-ray source, for example, to be placed adjacent to a material sample undergoing analysis or in proximity to the region to be treated for medical applications.

Trebes, James E. (Livermore, CA); Stone, Gary F. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA); Chornenky, Victor I. (Minnetonka, MN)

2002-01-01T23:59:59.000Z

71

X-ray fluorescence mapping  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

biololgical cells, over the measurement of impurities in solar cells, to the rare earth content of geological materials. A somewhat 'typical' layout for a X-ray fluorescence...

72

Self-Assembly of Microscale Objects at a Liquid/Liquid Interface through Lateral Capillary Forces  

E-Print Network [OSTI]

Self-Assembly of Microscale Objects at a Liquid/Liquid Interface through Lateral Capillary Forces allowed to self-assemble at the perfluorodecalin/water interface. These plates were fabricated from, the designs of hydrophobic edges necessary to generate menisci useful in self-assembly were different for 100

Prentiss, Mara

73

Novel Fluctuations at a Constrained Liquid-Solid Interface  

E-Print Network [OSTI]

We study the interface between a solid trapped within a bath of liquid by a suitably shaped non-uniform external potential. Such a potential may be constructed using lasers, external electric or magnetic fields or a surface template. We study a two dimensional case where a thin strip of solid, created in this way, is surrounded on either side by a bath of liquid with which it can easily exchange particles. Since height fluctuations of the interface cost energy, this interface is constrained to remain flat at all length scales. However, when such a solid is stressed by altering the depth of the potential; beyond a certain limit, it responds by relieving stress by novel interfacial fluctuations which involve addition or deletion of entire lattice layers of the crystal. This ``layering'' transition is a generic feature of the system regardless of the details of the interaction potential. We show how such interfacial fluctuations influence mass, momentum and energy transport across the interface. Tiny momentum impulses produce weak shock waves which travel through the interface and cause the spallation of crystal layers into the liquid. Kinetic and energetic constraints prevent spallation of partial layers from the crystal, a fact which may be of some practical use. We also study heat transport through the liquid-solid interface and obtain the resistances in liquid, solid and interfacial regions (Kapitza resistance) as the solid undergoes such layering transitions. Heat conduction, which shows strong signatures of the structural transformations, can be understood using a free volume calculation.

Abhishek Chaudhuri; Debasish Chaudhuri; Surajit Sengupta

2007-03-19T23:59:59.000Z

74

Nanoparticles at liquid interfaces: Rotational dynamics and angular locking  

SciTech Connect (OSTI)

Nanoparticles with different surface morphologies that straddle the interface between two immiscible liquids are studied via molecular dynamics simulations. The methodology employed allows us to compute the interfacial free energy at different angular orientations of the nanoparticle. Due to their atomistic nature, the studied nanoparticles present both microscale and macroscale geometrical features and cannot be accurately modeled as a perfectly smooth body (e.g., spheres and cylinders). Under certain physical conditions, microscale features can produce free energy barriers that are much larger than the thermal energy of the surrounding media. The presence of these energy barriers can effectively “lock” the particle at specific angular orientations with respect to the liquid-liquid interface. This work provides new insights on the rotational dynamics of Brownian particles at liquid interfaces and suggests possible strategies to exploit the effects of microscale features with given geometric characteristics.

Razavi, Sepideh; Kretzschmar, Ilona [Department of Chemical Engineering, City College of City University of New York, New York, New York 10031 (United States)] [Department of Chemical Engineering, City College of City University of New York, New York, New York 10031 (United States); Koplik, Joel [Department of Physics and The Benjamin Levich Institute for Physico-chemical Hydrodynamics, City College of City University of New York, New York, New York 10031 (United States)] [Department of Physics and The Benjamin Levich Institute for Physico-chemical Hydrodynamics, City College of City University of New York, New York, New York 10031 (United States); Colosqui, Carlos E., E-mail: carlos.colosqui@stonybrook.edu [Department of Mechanical Engineering, Stony Brook University, Stony Brook, New York 11794 (United States)

2014-01-07T23:59:59.000Z

75

X-ray shearing interferometer  

DOE Patents [OSTI]

An x-ray interferometer for analyzing high density plasmas and optically opaque materials includes a point-like x-ray source for providing a broadband x-ray source. The x-rays are directed through a target material and then are reflected by a high-quality ellipsoidally-bent imaging crystal to a diffraction grating disposed at 1.times. magnification. A spherically-bent imaging crystal is employed when the x-rays that are incident on the crystal surface are normal to that surface. The diffraction grating produces multiple beams which interfere with one another to produce an interference pattern which contains information about the target. A detector is disposed at the position of the image of the target produced by the interfering beams.

Koch, Jeffrey A. (Livermore, CA)

2003-07-08T23:59:59.000Z

76

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has...

77

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking  

E-Print Network [OSTI]

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking Tom Aldcroft SAO/CXC #12;X-ray Stacking 2008 analysis for a sample Stacking ­ mean properties of sample Chandra X-ray data (faint point sources) are photon-limited with low background => stacking in X-rays is very effective #12;X-ray Stacking 2008-Apr-22

Wolfe, Patrick J.

78

Miniature x-ray source  

DOE Patents [OSTI]

A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

Trebes, James E. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA)

2000-01-01T23:59:59.000Z

79

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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80

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
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81

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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82

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample6, 2011 LawrenceE C H NLensless X-Ray

83

High performance x-ray anti-scatter grid  

DOE Patents [OSTI]

Disclosed are an x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury. 4 Figs.

Logan, C.M.

1995-05-23T23:59:59.000Z

84

High performance x-ray anti-scatter grid  

DOE Patents [OSTI]

An x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury.

Logan, Clinton M. (Pleasanton, CA)

1995-01-01T23:59:59.000Z

85

E-Print Network 3.0 - aux interfaces solide-liquide Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

at the solid- liquid interface.2,3 The reason is the historical... diffusing, at the solid-liquid ... Source: Granick, Steve - Departments of Physics & Materials Science and...

86

E-Print Network 3.0 - air-liquid interface cell Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

film's air-liquid interface has a significant effect on the lung's mechanical... , is the surface tension and is the mean curvature of the air-liquid interface. For the uni-...

87

E-Print Network 3.0 - aux interfaces liquide Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

film's air-liquid interface has a significant effect on the lung's mechanical... , is the surface tension and is the mean curvature of the air-liquid interface. For the uni-...

88

X-ray Emission from Massive Stars  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore be related to the production of X-rays on massive stars. If so, massive stars' X-rays are much different than those found our own Sun and other cooler stars like the Sun that produce X-rays via magnetic activity

Cohen, David

89

X-ray Emission from Massive Stars  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore #12;What is the mechanism by which massive stars produce x-rays? New results from the Chandra X-ray Observatory ­ high-resolution x-ray spectroscopy: measuring Doppler broadening in emission lines Testing

Cohen, David

90

Cooling for a rotating anode X-ray tube  

DOE Patents [OSTI]

A method and apparatus for cooling a rotating anode X-ray tube. An electromagnetic motor is provided to rotate an X-ray anode with cooling passages in the anode. These cooling passages are coupled to a cooling structure located adjacent the electromagnetic motor. A liquid metal fills the passages of the cooling structure and electrical power is provided to the motor to rotate the anode and generate a rotating magnetic field which moves the liquid metal through the cooling passages and cooling structure.

Smither, Robert K. (Hinsdale, IL)

1998-01-01T23:59:59.000Z

91

Compact x-ray source and panel  

DOE Patents [OSTI]

A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

Sampayon, Stephen E. (Manteca, CA)

2008-02-12T23:59:59.000Z

92

Ultrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS)  

E-Print Network [OSTI]

: ultrafast x-rays, x-ray absorption spectroscopy, terawatt lasers, ultrafast reaction dynamics, atomic motion atomic motion by scrutinizing the changes in x- ray absorption spectra during reactions. FirstUltrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS) Guangjun

Guo, Ting

93

Focused X-ray source  

DOE Patents [OSTI]

Disclosed is an intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator. 8 figs.

Piestrup, M.A.; Boyers, D.G.; Pincus, C.I.; Maccagno, P.

1990-08-21T23:59:59.000Z

94

Dependence of solid-liquid interface free energy on liquid structure  

SciTech Connect (OSTI)

The Turnbull relation is widely believed to enable prediction of solid–liquid interface (SLI) free energies from measurements of the latent heat and the solid density. Ewing proposed an additional contribution to the SLI free energy to account for variations in liquid structure near the interface. In the present study, molecular dynamics (MD) simulations were performed to investigate whether SLI free energy depends on liquid structure. Analysis of the MD simulation data for 11 fcc metals demonstrated that the Turnbull relation is only a rough approximation for highly ordered liquids, whereas much better agreement is observed with Ewing’s theory. A modification to Ewing’s relation is proposed in this study that was found to provide excellent agreement with MD simulation data.

Wilson, S R [Ames Laboratory; Mendelev, M I [Ames Laboratory

2014-09-01T23:59:59.000Z

95

Methods and systems for monitoring a solid-liquid interface  

DOE Patents [OSTI]

Methods and systems are provided for monitoring a solid-liquid interface, including providing a vessel configured to contain an at least partially melted material; detecting radiation reflected from a surface of a liquid portion of the at least partially melted material; providing sound energy to the surface; measuring a disturbance on the surface; calculating at least one frequency associated with the disturbance; and determining a thickness of the liquid portion based on the at least one frequency, wherein the thickness is calculated based on L=(2m-1)v.sub.s/4f, where f is the frequency where the disturbance has an amplitude maximum, v.sub.s is the speed of sound in the material, and m is a positive integer (1, 2, 3, . . . ).

Stoddard, Nathan G. (Gettysburg, PA); Clark, Roger F. (Frederick, MD)

2011-10-04T23:59:59.000Z

96

Sudden structural change at ati air/binary liquid interface: Sum frequency study of the air/acetonitrile-water interface  

E-Print Network [OSTI]

Sudden structural change at ati air/binary liquid interface: Sum frequency study of the air/acetonitrile change in an air/acetonitrile-water interface as the solution composition varies; the abruptness of which and in the polarization of the signal from the acetonitrile molecules in the interface observed using infrared + visible

Eisenthal, Kenneth B.

97

Microgap x-ray detector  

DOE Patents [OSTI]

An x-ray detector is disclosed which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope. 3 figures.

Wuest, C.R.; Bionta, R.M.; Ables, E.

1994-05-03T23:59:59.000Z

98

Microgap x-ray detector  

DOE Patents [OSTI]

An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

Wuest, Craig R. (Danville, CA); Bionta, Richard M. (Livermore, CA); Ables, Elden (Livermore, CA)

1994-01-01T23:59:59.000Z

99

Spectral analysis of X-ray binaries  

E-Print Network [OSTI]

In this thesis, I present work from three separate research projects associated with observations of X-ray binaries. Two of those revolve around spectral characteristics of neutron star low-mass X-ray binaries (NS-LMXBs), ...

Fridriksson, Joel Karl

2011-01-01T23:59:59.000Z

100

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs...

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities...

102

Producing X-rays at the APS  

ScienceCinema (OSTI)

An introduction and overview of the Advanced Photon Source at Argonne National Laboratory, the technology that produces the brightest X-ray beams in the Western Hemisphere, and the research carried out by scientists using those X-rays.

None

2013-04-19T23:59:59.000Z

103

X-Ray Diffraction on NIF  

SciTech Connect (OSTI)

The National Ignition Facility (NIF) is currently a 192 beam, 1.6 MJ laser. NIF Ramp-Compression Experiments have already made the relevant exo-planet pressure range from 1 to 50 Mbar accessible. We Proposed to Study Carbon Phases by X-Ray Diffraction on NIF. Just a few years ago, ultra-high pressure phase diagrams for materials were very 'simple'. New experiments and theories point out surprising and decidedly complex behavior at the highest pressures considered. High pressures phases of aluminum are also predicted to be complex. Recent metadynamics survey of carbon proposed a dynamic pathway among multiple phases. We need to develop diagnostics and techniques to explore this new regime of highly compressed matter science. X-Ray Diffraction - Understand the phase diagram/EOS/strength/texture of materials to 10's of Mbar. Strategy and physics goals: (1) Powder diffraction; (2) Begin with diamond; (3) Continue with metals etc.; (4) Explore phase diagrams; (5) Develop liquid diffraction; and (6) Reduce background/improve resolution.

Eggert, J H; Wark, J

2012-02-15T23:59:59.000Z

104

Phase-sensitive X-ray imager  

DOE Patents [OSTI]

X-ray phase sensitive wave-front sensor techniques are detailed that are capable of measuring the entire two-dimensional x-ray electric field, both the amplitude and phase, with a single measurement. These Hartmann sensing and 2-D Shear interferometry wave-front sensors do not require a temporally coherent source and are therefore compatible with x-ray tubes and also with laser-produced or x-pinch x-ray sources.

Baker, Kevin Louis

2013-01-08T23:59:59.000Z

105

Soft X-Ray Diffraction Microscopy of a Frozen Hydrated Yeast Cell  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

We report the first image of an intact, frozen hydrated eukaryotic cell using x-ray diffraction microscopy, or coherent x-ray diffraction imaging. By plunge freezing the specimen in liquid ethane and maintaining it below -170 degrees C, artifacts due to dehydration, ice crystallization, and radiation damage are greatly reduced. In this example, coherent diffraction data using 520 eV x rays were recorded and reconstructed to reveal a budding yeast cell at a resolution better than 25 nm. This demonstration represents an important step towards high resolution imaging of cells in their natural, hydrated state, without limitations imposed by x-ray optics.

Huang, Xiaojing; Nelson, Johanna; Kirz, Janos; Lima, Enju; Marchesini, Stefano; Miao, Huijie; Neiman, Aaron; Shapiro, David; Steinbrener, Jan; Stewart, Andrew; Turner, Joshua; Jacobsen, Chris

2009-11-01T23:59:59.000Z

106

Ethylenediamine at Air/Liquid and Air/Silica Interfaces: Protonation  

E-Print Network [OSTI]

surface and EDA protonated products at air/liquid interfaces. The SFG spectra of EDA adsorbedEthylenediamine at Air/Liquid and Air/Silica Interfaces: Protonation Versus Hydrogen BondingKa (HOSit)) is between the two pKa values of EDA (in the range of 7.56-10.71) at the air/silica interface

107

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St in hot gas about 250 million light years from Earth. (Credit: X-ray: NASA/CXC/SAO/E.Bulbul, et al-Newton has revealed a mysterious X-ray signal in the data. This signal is represented in the circled data

108

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network [OSTI]

2/9/07 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 9, 07] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

109

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St million light years from Earth. (Credit: X-ray: NASA/CXC/Wesleyan Univ./R.Kilgard, et al; Optical: NASA with optical data from the Hubble Space Telescope (red, green, and blue). The X-ray data reveal hundreds

110

Cryotomography x-ray microscopy state  

DOE Patents [OSTI]

An x-ray microscope stage enables alignment of a sample about a rotation axis to enable three dimensional tomographic imaging of the sample using an x-ray microscope. A heat exchanger assembly provides cooled gas to a sample during x-ray microscopic imaging.

Le Gros, Mark (Berkeley, CA); Larabell, Carolyn A. (Berkeley, CA)

2010-10-26T23:59:59.000Z

111

X-ray Spectroscopy of Cool Stars  

E-Print Network [OSTI]

High-resolution X-ray spectroscopy has addressed not only various topics in coronal physics of stars, but has also uncovered important features relevant for our understanding of stellar evolution and the stellar environment. I summarize recent progress in coronal X-ray spectroscopy and in particular also discuss new results from studies of X-rays from pre-main sequence stars.

M. Guedel

2006-09-11T23:59:59.000Z

112

X-Ray Physics Evan Berkowitz  

E-Print Network [OSTI]

X-Ray Physics Evan Berkowitz Junior, MIT Department of Physics (Dated: October 25, 2006) We measure a variety of phenomena related to X-Ray absorption and production. We present data which conforms within, as are 22 Na electron-positron annhilation lines. The importance of understanding x-rays is demonstrated

113

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St 200 million light years from Earth. (Credit: X-ray: NASA/CXC/UAH/M.Sun et al; Optical: NASA, ESA, & the Hubble Heritage Team (STScI/AURA) Caption: This composite image from the Chandra X-ray Observatory (blue

114

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network [OSTI]

9/6/09 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 6, 09] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

115

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St. Cambridge, MA 02138 USA http://chandra.harvard.edu Four Supernova Remnants: NASA's Chandra X-ray Observatory's Chandra X-ray Observatory, four newly processed images of supernova remnants dramatically illustrate

116

X-ray spectroscopy of low-mass X-ray binaries  

E-Print Network [OSTI]

I present high-resolution X-ray grating spectroscopy of neutron stars in low-mass X-ray binaries (LMXBs) using instruments onboard the Chandra X-ray Observatory and the X-ray Multi-Mirror Mission (XMM-Newton). The first ...

Juett, Adrienne Marie, 1976-

2004-01-01T23:59:59.000Z

117

Extending The Methodology Of X-ray Crystallography To Allow X-ray  

E-Print Network [OSTI]

, the radiation damage. While the radiation damage problem can be mitigated somewhat by using cryogenic techniques resolution without serious radiation damage to the specimens. Although X-ray crystallography becomesExtending The Methodology Of X-ray Crystallography To Allow X-ray Microscopy Without X-ray Optics

Miao, Jianwei "John"

118

X-ray Pulsations in the Supersoft X-ray Binary CAL 83  

E-Print Network [OSTI]

X-ray data reveal that the supersoft X-ray binary CAL 83 exhibits 38.4 minute pulsations at some epochs. These X-ray variations are similar to those found in some novae and are likely to be caused by nonradial pulsations the white dwarf. This is the first detection of pulsations in a classical supersoft X-ray binary.

P. C. Schmidtke; A. P. Cowley

2005-09-28T23:59:59.000Z

119

X-ray Spectroscopy of Cooling Clusters  

E-Print Network [OSTI]

We review the X-ray spectra of the cores of clusters of galaxies. Recent high resolution X-ray spectroscopic observations have demonstrated a severe deficit of emission at the lowest X-ray temperatures as compared to that expected from simple radiative cooling models. The same observations have provided compelling evidence that the gas in the cores is cooling below half the maximum temperature. We review these results, discuss physical models of cooling clusters, and describe the X-ray instrumentation and analysis techniques used to make these observations. We discuss several viable mechanisms designed to cancel or distort the expected process of X-ray cluster cooling.

J. R. Peterson; A. C. Fabian

2005-12-21T23:59:59.000Z

120

X-ray transmissive debris shield  

DOE Patents [OSTI]

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, Rick B. (Albuquerque, NM)

1996-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


121

Synchronization of x-ray pulses to the pump laser in an ultrafast x-ray facility  

E-Print Network [OSTI]

Accurate timing of ultrafast x-ray probe pulses emitted fromOF X-RAY PULSES TO THE PUMP LASER IN AN ULTRAFAST X-RAY

Corlett, J.N.; Barry, W.; Byrd, J.M.; Schoenlein, R.; Zholents, A.

2002-01-01T23:59:59.000Z

122

X-ray lithography using holographic images  

DOE Patents [OSTI]

A non-contact X-ray projection lithography method for producing a desired X-ray image on a selected surface of an X-ray-sensitive material, such as photoresist material on a wafer, the desired X-ray image having image minimum linewidths as small as 0.063 .mu.m, or even smaller. A hologram and its position are determined that will produce the desired image on the selected surface when the hologram is irradiated with X-rays from a suitably monochromatic X-ray source of a selected wavelength .lambda.. On-axis X-ray transmission through, or off-axis X-ray reflection from, a hologram may be used here, with very different requirements for monochromaticity, flux and brightness of the X-ray source. For reasonable penetration of photoresist materials by X-rays produced by the X-ray source, the wavelength X, is preferably chosen to be no more than 13.5 nm in one embodiment and more preferably is chosen in the range 1-5 nm in the other embodiment. A lower limit on linewidth is set by the linewidth of available microstructure writing devices, such as an electron beam.

Howells, Malcolm R. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1995-01-01T23:59:59.000Z

123

Liquid chromatography/Fourier transform IR spectrometry interface flow cell  

DOE Patents [OSTI]

A zero dead volume (ZDV) microbore high performance liquid chromatography (..mu.. HPLC)/Fourier transform infrared (FTIR) interface flow cell includes an IR transparent crystal having a small diameter bore therein through which a sample liquid is passed. The interface flow cell further includes a metal holder in combination with a pair of inner, compressible seals for directly coupling the thus configured spectrometric flow cell to the outlet of a ..mu.. HPLC column end fitting to minimize the transfer volume of the effluents exiting the ..mu.. HPLC column which exhibit excellent flow characteristics due to the essentially unencumbered, open-flow design. The IR beam passes transverse to the sample flow through the circular bore within the IR transparent crystal, which is preferably comprised of potassium bromide (KBr) or calcium fluoride (CaF/sub 2/), so as to minimize interference patterns and vignetting encountered in conventional parallel-plate IR cells. The long IR beam pathlength and lensing effect of the circular cross-section of the sample volume in combination with the refractive index differences between the solvent and the transparent crystal serve to focus the IR beam in enhancing sample detection sensitivity by an order of magnitude.

Johnson, C.C.; Taylor, L.T.

1985-01-04T23:59:59.000Z

124

X-ray Imaging Workshop  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear SecurityTensile Strain Switched FerromagnetismWaste and MaterialsWenjun1of EnergyX-ray Computed TomographyImaging

125

X-ray fluorescence mapping  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear SecurityTensile Strain Switched FerromagnetismWaste and MaterialsWenjun1of EnergyX-rayNew Materialsray

126

X-Ray Science Education  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsrucLasDelivered energy consumption byAbout SRNL Home SRNL main campusMore thanX-Ray Imagingfeed

127

Statement of Work Third Party Algorithm Development and Evaluation of Detection of Liquid Explosives in Dual-Energy Digital Radiographic/TIP Ready X-ray Images - Public Version  

SciTech Connect (OSTI)

The purpose of this statement of work is for third party collaborators to train, validate and have Lawrence Livermore National Security, LLC (LLNS) evaluate algorithms to detect liquid threats in digital radiography (DR)/TIP Ready X-ray (TRX) images that will be provided by LLNS through the Transportation and Security Administration (TSA). LLNS will provide a set of images with threat(s) to determine detection rates and non-threat images from airports to determine false alarm rates. A key including a bounding box showing the locations of the threats and non-threats will be provided for the images. It is expected that the Subcontractor shall use half of the images with their keys for training the algorithms and the other half shall be used for validation (third party evaluation) purposes. The Subcontractor shall not use the key to the second half of the data other than for the validation and reporting of the performance of its algorithm (not for training). The Subcontractor has 45 business days from the receipt of datasets and the Subcontract to: (1) Run their detection/classification algorithms on the data; (2) Deliver a final report describing their performance by generating Receiver Operator Characteristic (ROC) curves using their algorithm; and (3) Deliver a copy of the third party's executable software (already trained and validated by the datasets) to LLNL accompanied by a user manual. LLNS will evaluate the performance of the same algorithm on another separate set of data. LLNS evaluation of the Subcontractor's algorithm will be documented in a final report within 30 days of receiving the executable code. This report will be sent to TSA and the report may be disseminated to the Subcontract at TSA's discretion.

Nekoogar, F; Martz, Jr., H E

2009-09-23T23:59:59.000Z

128

Controlling X-rays With Light  

SciTech Connect (OSTI)

Ultrafast x-ray science is an exciting frontier that promises the visualization of electronic, atomic and molecular dynamics on atomic time and length scales. A largelyunexplored area of ultrafast x-ray science is the use of light to control how x-rays interact with matter. In order to extend control concepts established for long wavelengthprobes to the x-ray regime, the optical control field must drive a coherent electronic response on a timescale comparable to femtosecond core-hole lifetimes. An intense field is required to achieve this rapid response. Here an intense optical control pulse isobserved to efficiently modulate photoelectric absorption for x-rays and to create an ultrafast transparency window. We demonstrate an application of x-ray transparencyrelevant to ultrafast x-ray sources: an all-photonic temporal cross-correlation measurement of a femtosecond x-ray pulse. The ability to control x-ray/matterinteractions with light will create new opportunities at current and next-generation x-ray light sources.

Glover, Ernie; Hertlein, Marcus; Southworth, Steve; Allison, Tom; van Tilborg, Jeroen; Kanter, Elliot; Krassig, B.; Varma, H.; Rude, Bruce; Santra, Robin; Belkacem, Ali; Young, Linda

2010-08-02T23:59:59.000Z

129

X-ray Observations of Mrk 231  

E-Print Network [OSTI]

This paper presents new X-ray observations of Mrk 231, an active galaxy of particular interest due to its large infrared luminosity and the presence of several blueshifted broad absorption line (BAL) systems, a phenomenon observed in a small fraction of QSOs. A ROSAT HRI image of Mrk 231 is presented, this shows an extended region of soft X-ray emission, covering several tens of kpc, consistent with the extent of the host galaxy. An ASCA observation of Mrk 231 is also presented. Hard X-rays are detected but the data show no significant variability in X-ray flux. The hard X-ray continuum is heavily attenuated and X-ray column estimates range from ~ 2 x 10^{22} - 10^{23} cm^{-2} depending on whether the material is assumed to be neutral or ionized, and on the model assumed for the extended X-ray component. These ASCA data provide only the second hard X-ray spectrum of a BAL AGN presented to date. The broad-band spectral-energy-distribution of the source is discussed. While Mrk 231 is X-ray weak compared to Seyfert 1 galaxies, it has an optical-to-X-ray spectrum typical of a QSO.

T. J. Turner

1998-08-10T23:59:59.000Z

130

Techniques for synchronization of X-Ray pulses to the pump laser in an ultrafast X-Ray facility  

E-Print Network [OSTI]

synchronization of ultrafast x-ray pulses produced in theAccurate timing of ultrafast x-ray probe pulses emitted fromOF X-RAY PULSES TO THE PUMP LASER IN AN ULTRAFAST X-RAY

Corlett, J.N.; Doolittle, L.; Schoenlein, R.; Staples, J.; Wilcox, R.; Zholents, A.

2003-01-01T23:59:59.000Z

131

Low energy electron diffraction (LEED) and sum frequency generation (SFG) vibrational spectroscopy studies of solid-vacuum, solid-air and solid-liquid interfaces  

SciTech Connect (OSTI)

Electron based surface probing techniques can provide detailed information about surface structure or chemical composition in vacuum environments. The development of new surface techniques has made possible in situ molecular level studies of solid-gas interfaces and more recently, solid-liquid interfaces. The aim of this dissertation is two-fold. First, by using novel sample preparation, Low Energy Electron Diffraction (LEED) and other traditional ultra high vacuum (UHV) techniques are shown to provide new information on the insulator/vacuum interface. The surface structure of the classic insulator NaCl has been determined using these methods. Second, using sum frequency generation (SFG) surface specific vibrational spectroscopy studies were performed on both the biopolymer/air and electrode/electrolyte interfaces. The surface structure and composition of polyetherurethane-silicone copolymers were determined in air using SFG, atomic force microscopy (AFM), and X-ray photoelectron spectroscopy (XPS). SFG studies of the electrode (platinum, gold and copper)/electrolyte interface were performed as a function of applied potential in an electrochemical cell.

Hoffer, Saskia

2002-08-19T23:59:59.000Z

132

Hard x-ray imaging from explorer  

SciTech Connect (OSTI)

Coded aperture X-ray detectors were applied to obtain large increases in sensitivity as well as angular resolution. A hard X-ray coded aperture detector concept is described which enables very high sensitivity studies persistent hard X-ray sources and gamma ray bursts. Coded aperture imaging is employed so that approx. 2 min source locations can be derived within a 3 deg field of view. Gamma bursts were located initially to within approx. 2 deg and X-ray/hard X-ray spectra and timing, as well as precise locations, derived for possible burst afterglow emission. It is suggested that hard X-ray imaging should be conducted from an Explorer mission where long exposure times are possible.

Grindlay, J.E.; Murray, S.S.

1981-11-01T23:59:59.000Z

133

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma  

E-Print Network [OSTI]

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma P. L plasmas in which efficient x-ray laser frequency near-doubling is expected for a number of available x-ray of coherent x rays and tunable optical radiation may result in tunable coherent x-ray radiation powerful

Kaplan, Alexander

134

High speed x-ray beam chopper  

DOE Patents [OSTI]

A fast, economical, and compact x-ray beam chopper with a small mass and a small moment of inertia whose rotation can be synchronized and phase locked to an electronic signal from an x-ray source and be monitored by a light beam is disclosed. X-ray bursts shorter than 2.5 microseconds have been produced with a jitter time of less than 3 ns.

McPherson, Armon (Oswego, IL); Mills, Dennis M. (Naperville, IL)

2002-01-01T23:59:59.000Z

135

X-ray populations in galaxies  

E-Print Network [OSTI]

Today's sensistive, high resolution Chandra X-ray observations allow the study of many populations of X-ray sources. The traditional astronomical tools of photometric diagrams and luminosity functions are now applied to these populations, and provide the means for classifying the X-ray sources and probing their evolution. While overall stellar mass drives the amount of X-ray binaries in old stellar population, the amount of sources in star-forming galaxies is related to the star formation rate. Shart-lived, luminous, high mass binaries (HNXBs) dominate these young populations.

G. Fabbiano

2005-11-09T23:59:59.000Z

136

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE  

E-Print Network [OSTI]

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE USER'S HANDBOOK Version 1.0 (June 1994) prepared by John . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Chapter Two: XRMB History

137

X-ray laser microscope apparatus  

DOE Patents [OSTI]

A microscope consisting of an x-ray contact microscope and an optical microscope. The optical, phase contrast, microscope is used to align a target with respect to a source of soft x-rays. The source of soft x-rays preferably comprises an x-ray laser but could comprise a synchrotron or other pulse source of x-rays. Transparent resist material is used to support the target. The optical microscope is located on the opposite side of the transparent resist material from the target and is employed to align the target with respect to the anticipated soft x-ray laser beam. After alignment with the use of the optical microscope, the target is exposed to the soft x-ray laser beam. The x-ray sensitive transparent resist material whose chemical bonds are altered by the x-ray beam passing through the target mater GOVERNMENT LICENSE RIGHTS This invention was made with government support under Contract No. De-FG02-86ER13609 awarded by the Department of Energy. The Government has certain rights in this invention.

Suckewer, Szymon (Princeton, NJ); DiCicco, Darrell S. (Plainsboro, NJ); Hirschberg, Joseph G. (Coral Gables, FL); Meixler, Lewis D. (East Windsor, NJ); Sathre, Robert (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ)

1990-01-01T23:59:59.000Z

138

Compound refractive X-ray lens  

DOE Patents [OSTI]

An apparatus and method for focusing X-rays. In one embodiment, his invention is a commercial-grade compound refractive X-ray lens. The commercial-grade compound refractive X-ray lens includes a volume of low-Z material. The volume of low-Z material has a first surface which is adapted to receive X-rays of commercially-applicable power emitted from a commercial-grade X-ray source. The volume of low-Z material also has a second surface from which emerge the X-rays of commercially-applicable power which were received at the first surface. Additionally, the commercial-grade compound refractive X-ray lens includes a plurality of openings which are disposed between the first surface and the second surface. The plurality of openings are oriented such that the X-rays of commercially-applicable power which are received at the first surface, pass through the volume of low-Z material and through the plurality openings. In so doing, the X-rays which emerge from the second surface are refracted to a focal point.

Nygren, David R. (Berkeley, CA); Cahn, Robert (Walnut Creek, CA); Cederstrom, Bjorn (Traellborg, SE); Danielsson, Mats (Stocksund, SE); Vestlund, Jonas (Stockholm, SE)

2000-01-01T23:59:59.000Z

139

X-Ray Science Division (XSD)  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Science Division (XSD) Search Button About Welcome Overview Visiting the APS Mission & Goals Find People Organization Charts Committees Job Openings User Information...

140

X-ray spectroscopy of neutron star low-mass X-ray binaries  

E-Print Network [OSTI]

In this thesis, I present work spanning a variety of topics relating to neutron star lowmass X-ray binaries (LMXBs) and utilize spectral information from X-ray observations to further our understanding of these sources. ...

Krauss, Miriam Ilana

2007-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

Ultraluminous X-ray Sources: The most extreme X-ray binaries  

E-Print Network [OSTI]

1 Ultraluminous X-ray Sources: The most extreme X-ray binaries Luca Zampieri INAF ULXs ­ Lubiana ­ May 11, 2012- LZ #12;6 · X-ray observations of nearby galaxies show a population of pointlike, off-nuclear sources with L >> Ledd for 1 Msun (L>1.0e39 erg/s) UltraLuminous X-ray Sources (e

Â?umer, Slobodan

142

X-ray Diffraction (XRD) 1.0 What is X-ray Diffraction  

E-Print Network [OSTI]

X-ray Diffraction (XRD) · 1.0 What is X-ray Diffraction · 2.0 Basics of Crystallography · 3.0 Production of X-rays · 4.0 Applications of XRD · 5.0 Instrumental Sources of Error · 6.0 Conclusions #12 why the cleavage faces of crystals appear to reflect X-ray beams at certain angles of incidence (theta

Moeck, Peter

143

X-ray source populations in galaxies  

E-Print Network [OSTI]

Today's sensitive, high-resolution X-ray observations allow the study of populations of X-ray sources, in the luminosity range of Galactic X-ray binaries, in galaxies as distant as 20-30 Mpc. The traditional astronomical tools of photometric diagrams and luminosity functions are now applied to these populations, providing a direct probe of the evolved binary component of different stellar populations. The study of the X-ray populations of E and S0 galaxies has revamped the debate on the formation and evolution of low-mass X-ray binaries (LMXBs) and on the role of globular clusters in these processes. While overall stellar mass drives the amount of X-ray binaries in old stellar populations, the amount of sources in star forming galaxies is related to the star formation rate. Short-lived, luminous, high-mass binaries (HMXBs) dominate these young populations. The most luminous sources in these systems are the debated ULXs, which have been suggested to be ~100-1000 Msol black holes, but could alternatively include a number of binaries with stellar mass black holes. Very soft sources have also been discovered in many galaxies and their nature is currently being debated. Observations of the deep X-ray sky, and comparison with deep optical surveys, are providing the first evidence of the X-ray evolution of galaxies.

G. Fabbiano

2005-11-16T23:59:59.000Z

144

Aneta Siemiginowska Chandra X-ray Center  

E-Print Network [OSTI]

-ray and gamma-ray · High Energy Sky · Chandra X-ray Observatory · examples of typical X-ray data, · an example of a data analysis process · statistical challenges · what do we learn from the data? #12;What is Astronomy and phenomena do we study and how? Solar System: Sun and sollar wind, planets, moons, asteroids, comets Our

Wolfe, Patrick J.

145

Phased Contrast X-Ray Imaging  

ScienceCinema (OSTI)

The Pacific Northwest National Laboratory is developing a range of technologies to broaden the field of explosives detection. Phased contrast X-ray imaging, which uses silicon gratings to detect distortions in the X-ray wave front, may be applicable to mail or luggage scanning for explosives; it can also be used in detecting other contraband, small-parts inspection, or materials characterization.

Erin Miller

2012-12-31T23:59:59.000Z

146

Quantitative Measurements of X-ray Intensity  

SciTech Connect (OSTI)

This chapter describes the characterization of several X-ray sources and their use in calibrating different types of X-ray cameras at National Security Technologies, LLC (NSTec). The cameras are employed in experimental plasma studies at Lawrence Livermore National Laboratory (LLNL), including the National Ignition Facility (NIF). The sources provide X-rays in the energy range from several hundred eV to 110 keV. The key to this effort is measuring the X-ray beam intensity accurately and traceable to international standards. This is accomplished using photodiodes of several types that are calibrated using radioactive sources and a synchrotron source using methods and materials that are traceable to the U.S. National Institute of Standards and Technology (NIST). The accreditation procedures are described. The chapter begins with an introduction to the fundamental concepts of X-ray physics. The types of X-ray sources that are used for device calibration are described. The next section describes the photodiode types that are used for measuring X-ray intensity: power measuring photodiodes, energy dispersive photodiodes, and cameras comprising photodiodes as pixel elements. Following their description, the methods used to calibrate the primary detectors, the power measuring photodiodes and the energy dispersive photodiodes, as well as the method used to get traceability to international standards are described. The X-ray source beams can then be measured using the primary detectors. The final section then describes the use of the calibrated X-ray beams to calibrate X-ray cameras. Many of the references are web sites that provide databases, explanations of the data and how it was generated, and data calculations for specific cases. Several general reference books related to the major topics are included. Papers expanding some subjects are cited.

Haugh, M. J., Schneider, M.

2011-09-01T23:59:59.000Z

147

X-ray small-angle scattering from sputtered CeO{sub 2}/C bilayers  

SciTech Connect (OSTI)

Surface and interface morphology of cerium oxide/carbon bilayers used as thin-film catalysts is studied by grazing-incidence small-angle x-ray scattering, scanning electron microscopy, and atomic-force microscopy, and the dependence of the structural parameters on the thicknesses of the constituting layers is investigated. The applicability of x-ray scattering and its advantages over standard analytical methods are discussed.

Haviar, S.; Dubau, M.; Khalakhan, I.; Vorokhta, M.; Matolinova, I.; Matolin, V. [Department of Surface and Plasma Science, Faculty of Mathematics and Physics Charles University, V Holesovickach 2, 180 00, Prague 8 (Czech Republic); Vales, V.; Endres, J.; Holy, V. [Department of Condensed Matter Physics, Faculty of Mathematics and Physics, Charles University, Ke Karlovu 5, 121 16 Prague 2 (Czech Republic); Buljan, M. [Institute Ruder Boskovic, Bijenicka 54, 10000 Zagreb (Croatia); Bernstorff, S. [Sincrotrone ELETTRA, 34149 Basovizza, Trieste (Italy)

2013-01-14T23:59:59.000Z

148

X-ray Practicals Series 1 Advanced Data Reduction  

E-Print Network [OSTI]

X-ray Practicals Series 1 Advanced Data Reduction Instructor J. Reibenspies, Ph. D. Nattamai Bhuvanesh, Ph.D. Version 1.0.0 #12;X-ray Practicals Series 2 #12;X-ray Practicals Series 3 #12;X-ray is good. The y direction is shifting the most, but the shift is ok #12;X-ray Practicals Series 5 Other

Meagher, Mary

149

Anti-contamination device for cryogenic soft X-ray diffraction microscopy  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

Cryogenic microscopy allows one to view frozen hydrated biological and soft matter specimens with good structural preservation and a high degree of stability against radiation damage. We describe a liquid nitrogen-cooled anti-contamination device for cryogenic X-ray diffraction microscopy. The anti-contaminator greatly reduces the buildup of ice layers on the specimen due to condensation of residual water vapor in the experimental vacuum chamber. We show by coherent X-ray diffraction measurements that this leads to fivefold reduction of background scattering, which is important for far-field X-ray diffraction microscopy of biological specimens.

Huang, Xiaojing; Miao, Huijie; Nelson, Johanna; Turner, Joshua; Steinbrener, Jan; Shapiro, David; Kirz, Janos; Jacobsen, Chris

2011-05-01T23:59:59.000Z

150

X-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND  

E-Print Network [OSTI]

with the occurrence of solar X-ray flare, when light travel time delay is accounted, suggesting that X-rays fromX-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND ANIL BHARDWAJ Flight center, Greenbelt, MD 20771, USA Scattering of solar X-ray radiation mainly produces the non

Ã?stgaard, Nikolai

151

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art  

E-Print Network [OSTI]

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art diffractometers offering both single crystal and powder X-Ray diffraction. Powder X-Ray Diffraction High resolution data For more details on powder X-Ray analysis contact Dr J Hriljac on 0121 414 4458 or email: j

Birmingham, University of

152

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray Source  

E-Print Network [OSTI]

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray of an intense, tunable, polarized, and quasi-monochromatic X-ray source has been ongoing at Rensselaer Polytechnic Institute since 2001 [1, 2, 3, 4, 5, 6]. This X-ray source, known as Parametric X-rays (PXR

Danon, Yaron

153

X-Ray Physics in Confinement  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear SecurityTensile Strain Switched FerromagnetismWaste and MaterialsWenjun1of Energy WorldwideX-RayX-RayX-Ray

154

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray...

155

E-Print Network 3.0 - air-liquid interface biofilms Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

, B. Purvedorj y , P. Stoodley yz Summary: and the velocity of the ripples at the biofilmbulk liquid interface. wg 5:09 Nm 2 . 21 12; Strain Source... A Viscoelastic Fluid...

156

Small Angle X-Ray Scattering Detector  

DOE Patents [OSTI]

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

Hessler, Jan P.

2004-06-15T23:59:59.000Z

157

X-ray grid-detector apparatus  

DOE Patents [OSTI]

A hybrid grid-detector apparatus for x-ray systems wherein a microchannel plate structure has an air-interspaced grid portion and a phosphor/optical fluid-filled grid portion. The grids are defined by multiple adjacent channels separated by lead-glass septa. X-rays entering the air-interspaced grid portion at an angle of impingement upon the septa are attenuated, while non-impinging x-rays pass through to the phosphor/fluid filled portion. X-ray energy is converted to luminescent energy in the phosphor/fluid filled portion and the resultant beams of light are directed out of the phosphor/optical fluid filled portion to an imaging device.

Boone, John M. (Folsom, CA); Lane, Stephen M. (Oakland, CA)

1998-01-27T23:59:59.000Z

158

X-ray source for mammography  

DOE Patents [OSTI]

An x-ray source utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms.

Logan, Clinton M. (Pleasanton, CA)

1994-01-01T23:59:59.000Z

159

X-ray induced optical reflectivity  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

The change in optical reflectivity induced by intense x-ray pulses can now be used to study ultrafast many body responses in solids in the femtosecond time domain. X-ray absorption creates photoelectrons and core level holes subsequently filled by Auger or fluorescence processes, and these excitations ultimately add conduction and valence band carriers that perturb optical reflectivity.Optical absorption associated with band filling and band gap narrowing is shown to explain the basic features found in recent measurements on an insulator (silicon nitride, Si3N4), a semiconductor(gallium arsenide,GaAs), and a metal (gold,Au), obtained with ?100 fs x-ray pulses at 500-2000 eV and probed with 800 nm laser pulses. In particular GaAs exhibits an abrupt drop in reflectivity, persisting only for a time comparable to the x-ray excitation pulse duration, consistent with prompt band gap narrowing.

Durbin, Stephen M.

2012-01-01T23:59:59.000Z

160

Columbia University X-Ray Measurements  

E-Print Network [OSTI]

Columbia University X-Ray Measurements of the Levitated Dipole Experiment J. L. Ellsworth, J. Kesner MIT Plasma Science and Fusion Center D.T. Garnier, A.K. Hansen, M.E. Mauel Columbia University

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

X-Ray Nanoimaging: Instruments and Methods  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http:spie.orgOP318 August 28-29, 2013; San Diego, California, USA...

162

X-ray source for mammography  

DOE Patents [OSTI]

An x-ray source is described utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms. 6 figures.

Logan, C.M.

1994-12-20T23:59:59.000Z

163

Principles of X-ray Navigation  

SciTech Connect (OSTI)

X-ray navigation is a new concept in satellite navigation in which orientation, position and time are measured by observing stellar emissions in x-ray wavelengths. X-ray navigation offers the opportunity for a single instrument to be used to measure these parameters autonomously. Furthermore, this concept is not limited to missions in close proximity to the earth. X-ray navigation can be used on a variety of missions from satellites in low earth orbit to spacecraft on interplanetary missions. In 1997 the Unconventional Stellar Aspect Experiment (USA) will be launched as part of the Advanced Research and Global Observation Satellite (ARGOS). USA will provide the first platform for real-time experimentation in the field of x-ray navigation and also serves as an excellent case study for the design and manufacturing of space qualified systems in small, autonomous groups. Current techniques for determining the orientation of a satellite rely on observations of the earth, sun and stars in infrared, visible or ultraviolet wavelengths. It is possible to use x-ray imaging devices to provide arcsecond level measurement of attitude based on star patterns in the x-ray sky. This technique is explored with a simple simulation. Collimated x-ray detectors can be used on spinning satellites to provide a cheap and reliable measure of orientation. This is demonstrated using observations of the Crab Pulsar taken by the high Energy Astronomy Observatory (HEAO-1) in 1977. A single instrument concept is shown to be effective, but dependent on an a priori estimate of the guide star intensity and thus susceptible to errors in that estimate. A star scanner based on a differential measurement from two x-ray detectors eliminates the need for an a priori estimate of the guide star intensity. A first order model and a second order model of the two star scanner concepts are considered. Many of the stars that emit in the x-ray regime are also x-ray pulsars with frequency stability approaching a part in 10{sup 9}. By observing these pulsations, a satellite can keep accurate time autonomously. They have demonstrated the acquisition and tracking of the Crab nebula pulsar by simulating the operation of a phase-locked loop.

Hanson, John Eric; /SLAC

2006-03-17T23:59:59.000Z

164

Hard X-ray Fluorescence Measurements of Heteroepitaxial Solid...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Hard X-ray Fluorescence Measurements of Heteroepitaxial Solid Oxide Fuel Cell Cathode Materials. Hard X-ray Fluorescence Measurements of Heteroepitaxial Solid Oxide Fuel Cell...

165

Using X-Ray Computed Tomography in Pore Structure Characterization...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Using X-Ray Computed Tomography in Pore Structure Characterization for a Berea Sandstone: Resolution Effect. Using X-Ray Computed Tomography in Pore Structure Characterization for...

166

X-ray views of neutron star low-mass X-ray binaries  

E-Print Network [OSTI]

A neutron star low-mass X-ray binary is a binary stellar system with a neutron star and a low-mass companion star rotating around each other. In this system the neutron star accretes mass from the companion, and as this matter falls into the deep potential well of the neutron star, the gravitational potential energy is released primarily in the X-ray wavelengths. Such a source was first discovered in X-rays in 1962, and this discovery formally gave birth to the "X-ray astronomy". In the subsequent decades, our knowledge of these sources has increased enormously by the observations with several X-ray space missions. Here we give a brief overview of our current understanding of the X-ray observational aspects of these systems.

Sudip Bhattacharyya

2010-02-24T23:59:59.000Z

167

X-Ray Observations of Radio Galaxies  

E-Print Network [OSTI]

We review some of the ways that X-ray observations provide unique information on radio galaxies. Thermal bremsstrahlung X-ray emission provides detailed data on ambient densities and temperatures. These parameters in turn can be used for pressure balance calculations and can demonstrate how the ambient gas affects radio source structure. Additionally, many signatures of the interaction of radio jets and lobes with the hot gas are found in high resolution X-ray maps. Non-thermal X-ray emission from knots and hotspots of radio jets can give us constraints on the relativistic electron population for energies greater that that normally sampled in the radio (in the case of synchrotron emission) or can give us an independent estimate of the average magnetic field strength (if inverse Compton emission is the origin of the X-rays). From recent ROSAT HRI observations of 3C 390.3 and 3C 120, we show evidence that X-ray emission from knots and hotspots appears to be associated with regions of large gradients in the radio surface brightness; i.e. at the location of powerful shocks.

D. E. Harris

1998-04-20T23:59:59.000Z

168

Compton backscattered collimated x-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

Ruth, R.D.; Huang, Z.

1998-10-20T23:59:59.000Z

169

Compton backscattered collmated X-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

2000-01-01T23:59:59.000Z

170

Compton backscattered collimated x-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

1998-01-01T23:59:59.000Z

171

Control and ultrasonic actuation of a gas-liquid interface in a microfluidic chip  

E-Print Network [OSTI]

This article describes the design and manufacturing of a microfluidic chip, allowing for the actuation of a gas-liquid interface and of the neighboring fluid. A first way to control the interface motion is to apply a pressure difference across it. In this case, the efficiency of three different micro-geometries at anchoring the interface is compared. Also, the critical pressures needed to move the interface are measured and compared to theoretical result. A second way to control the interface motion is by ultrasonic excitation. When the excitation is weak, the interface exhibits traveling waves, which follow a dispersion equation. At stronger ultrasonic levels, standing waves appear on the interface, with frequencies that are half integer multiple of the excitation frequency. An associated microstreaming flow field observed in the vicinity of the interface is characterized. The meniscus and associated streaming flow have the potential to transport particles and mix reagents.

Jie Xu; Daniel Attinger

2009-12-15T23:59:59.000Z

172

(Electron transfer rates at semiconductor/liquid interfaces)  

SciTech Connect (OSTI)

Work has focused on several aspects of the fundamental chemistry and physics semiconductor/liquid junction behavior. These projects have been directed primarily towards GaAs/liquid contacts, because GaAs/liquid systems provide high energy conversion efficiencies and offer an opportunity to gain mechanistic understanding of the factors that are important to control in an efficient photoelectrochemical energy conversion system.

Lewis, N.S.

1992-01-01T23:59:59.000Z

173

[Electron transfer rates at semiconductor/liquid interfaces]. Progress report  

SciTech Connect (OSTI)

Work has focused on several aspects of the fundamental chemistry and physics semiconductor/liquid junction behavior. These projects have been directed primarily towards GaAs/liquid contacts, because GaAs/liquid systems provide high energy conversion efficiencies and offer an opportunity to gain mechanistic understanding of the factors that are important to control in an efficient photoelectrochemical energy conversion system.

Lewis, N.S.

1992-08-01T23:59:59.000Z

174

Transient x-ray diffraction and its application to materials science and x-ray optics  

SciTech Connect (OSTI)

Time resolved x-ray diffraction and scattering have been applied to the measurement of a wide variety of physical phenomena from chemical reactions to shock wave physics. Interest in this method has heightened in recent years with the advent of versatile, high power, pulsed x-ray sources utilizing laser plasmas, electron beams and other methods. In this article, we will describe some of the fundamentals involved in time resolved x-ray diffraction, review some of the history of its development, and describe some recent progress in the field. In this article we will emphasize the use of laser-plasmas as the x-ray source for transient diffraction.

Hauer, A.A.; Kopp, R.; Cobble, J.; Kyrala, G.; Springer, R. [and others

1997-12-01T23:59:59.000Z

175

IN SITU SURFACE X-RAY SCATTERING STUDIES OF ELECTROSORPTION  

SciTech Connect (OSTI)

A short review of the application of surface x-ray scattering techniques to the electrode/electrolyte interfaces is presented. Recent results on metal, halide, and metal-halide adlayers with three specific systems: Bi on Au(100) and Au(110); Br on Au(100) and Ag(100); and the coadsorption of Tl with Br or I on Au(111), are given as an illustration. Factors affecting ordering of pure metal and halide adlayers and the metal-halide surface compounds are discussed in some detail.

WANG,J.X.; ADZIC,R.R.; OCKO,B.M.

1998-07-01T23:59:59.000Z

176

A mean field approach for computing solid-liquid surface tension for nanoscale interfaces  

E-Print Network [OSTI]

A mean field approach for computing solid-liquid surface tension for nanoscale interfaces Chi are largely determined by the solid-liquid surface tension. This is especially true for nanoscale systems with high surface area to volume ratios. While experimental techniques can only measure surface tension

Nielsen, Steven O.

177

Capillary waves and the inherent density profile for the liquid-vapor interface  

E-Print Network [OSTI]

. This approach in turn allows: (1) identification of an "outermost layer" of particles on the liquid. (2). is a nonmonotonic function of normal distance through the interface. and is expected to reflect the diverging bulk distribution for the system in a state of liquid-vapor phase coexistence. This leads to identification

Stillinger, Frank

178

High-resolution x-ray diffraction microscopy of specifically labeled yeast cells  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

X-ray diffraction microscopy complements other x-ray microscopy methods by being free of lens-imposed radiation dose and resolu- tion limits, and it allows for high-resolution imaging of biological specimens too thick to be viewed by electron microscopy. We report here the highest resolution (11–13 nm) x-ray diffraction micrograph of biological specimens, and a demonstration of mole- cular-specific gold labeling at different depths within cells via through-focus propagation of the reconstructed wavefield. The lec- tin concanavalin A conjugated to colloidal gold particles was used to label the ?-mannan sugar in the cell wall of the yeast Saccharomyces cerevisiae. Cells were plunge-frozen in liquid ethane and freeze-dried, after which they were imaged whole using x-ray diffraction microscopy at 750 eV photon energy.

Nelson, J.; Huang, X.; Steinbrener, J.; Shapiro, D.; Kirz, J.; Marchesini, S.; Neiman, A. M.; Turner, J. J.; Jacobsen, C.

2010-04-20T23:59:59.000Z

179

Oscillations During Thermonuclear X-ray Bursts  

E-Print Network [OSTI]

High amplitude, nearly coherent X-ray brightness oscillations during thermonuclear X-ray bursts were discovered with the Rossi X-ray Timing Explorer (RXTE) in early 1996. Spectral and timing evidence strongly supports the conclusion that these oscillations are caused by rotational modulation of the burst emission and that they reveal the spin frequency of neutron stars in low mass X-ray binaries, a long sought goal of X-ray astronomy. Studies carried out over the past year have led to the discovery of burst oscillations in four new sources, bringing to ten the number with confirmed burst oscillations. I review the status of our knowledge of these oscillations and indicate how they can be used to probe the physics of neutron stars. For a few burst oscillation sources it has been proposed that the strongest and most ubiquitous frequency is actually the first overtone of the spin frequency and hence that two nearly antipodal hot spots are present on the neutron star. This inference has important implications for both the physics of thermonuclear burning as well as the mass- radius relation for neutron stars, so its confirmation is crucial. I discuss recent attempts to confirm this hypothesis for 4U 1636-53, the source for which a signal at the putative fundamental (290 Hz) has been claimed.

Tod E. Strohmayer

2001-01-01T23:59:59.000Z

180

Nonlinear X-ray Compton Scattering  

E-Print Network [OSTI]

X-ray scattering is a weak linear probe of matter. It is primarily sensitive to the position of electrons and their momentum distribution. Elastic X-ray scattering forms the basis of atomic structural determination while inelastic Compton scattering is often used as a spectroscopic probe of both single-particle excitations and collective modes. X-ray free-electron lasers (XFELs) are unique tools for studying matter on its natural time and length scales due to their bright and coherent ultrashort pulses. However, in the focus of an XFEL the assumption of a weak linear probe breaks down, and nonlinear light-matter interactions can become ubiquitous. The field can be sufficiently high that even non-resonant multiphoton interactions at hard X-rays wavelengths become relevant. Here we report the observation of one of the most fundamental nonlinear X-ray-matter interactions, the simultaneous Compton scattering of two identical photons producing a single photon at nearly twice the photon energy. We measure scattered...

Fuchs, Matthias; Chen, Jian; Ghimire, Shambhu; Shwartz, Sharon; Kozina, Michael; Jiang, Mason; Henighan, Thomas; Bray, Crystal; Ndabashimiye, Georges; Bucksbaum, P H; Feng, Yiping; Herrmann, Sven; Carini, Gabriella; Pines, Jack; Hart, Philip; Kenney, Christopher; Guillet, Serge; Boutet, Sebastien; Williams, Garth; Messerschmidt, Marc; Seibert, Marvin; Moeller, Stefan; Hastings, Jerome B; Reis, David A

2015-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

Ultrafast X-Ray Coherent Control  

SciTech Connect (OSTI)

This main purpose of this grant was to develop the nascent #12;eld of ultrafast x-ray science using accelerator-based sources, and originally developed from an idea that a laser could modulate the di#11;racting properties of a x-ray di#11;racting crystal on a fast enough time scale to switch out in time a shorter slice from the already short x-ray pulses from a synchrotron. The research was carried out primarily at the Advanced Photon Source (APS) sector 7 at Argonne National Laboratory and the Sub-Picosecond Pulse Source (SPPS) at SLAC; in anticipation of the Linac Coherent Light Source (LCLS) x-ray free electron laser that became operational in 2009 at SLAC (all National User Facilities operated by BES). The research centered on the generation, control and measurement of atomic-scale dynamics in atomic, molecular optical and condensed matter systems with temporal and spatial resolution . It helped develop the ultrafast physics, techniques and scienti#12;c case for using the unprecedented characteristics of the LCLS. The project has been very successful with results have been disseminated widely and in top journals, have been well cited in the #12;eld, and have laid the foundation for many experiments being performed on the LCLS, the world's #12;rst hard x-ray free electron laser.

Reis, David

2009-05-01T23:59:59.000Z

182

Oscillations During Thermonuclear X-ray Bursts  

E-Print Network [OSTI]

High amplitude, nearly coherent X-ray brightness oscillations during thermonuclear X-ray bursts were discovered with the Rossi X-ray Timing Explorer (RXTE) in early 1996. Spectral and timing evidence strongly supports the conclusion that these oscillations are caused by rotational modulation of the burst emission and that they reveal the spin frequency of neutron stars in low mass X-ray binaries, a long sought goal of X-ray astronomy. Studies carried out over the past year have led to the discovery of burst oscillations in four new sources, bringing to ten the number with confirmed burst oscillations. I review the status of our knowledge of these oscillations and indicate how they can be used to probe the physics of neutron stars. For a few burst oscillation sources it has been proposed that the strongest and most ubiquitous frequency is actually the first overtone of the spin frequency and hence that two nearly antipodal hot spots are present on the neutron star. This inference has important implications for both the physics of thermonuclear burning as well as the mass - radius relation for neutron stars, so its confirmation is crucial. I discuss recent attempts to confirm this hypothesis for 4U 1636-53, the source for which a signal at the putative fundamental (290 Hz) has been claimed.

Tod E. Strohmayer

2001-01-12T23:59:59.000Z

183

X-ray lithography using holographic images  

DOE Patents [OSTI]

Methods for forming X-ray images having 0.25 .mu.m minimum line widths on X-ray sensitive material are presented. A holgraphic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required.

Howells, Malcolm S. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1997-01-01T23:59:59.000Z

184

Reflection soft X-ray microscope and method  

DOE Patents [OSTI]

A reflection soft X-ray microscope is provided by generating soft X-ray beams, condensing the X-ray beams to strike a surface of an object at a predetermined angle, and focusing the X-ray beams reflected from the surface onto a detector, for recording an image of the surface or near surface features of the object under observation.

Suckewer, Szymon (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ); Rosser, Roy (Princeton, NJ)

1993-01-01T23:59:59.000Z

185

Differential phase contrast X-ray imaging system and components  

DOE Patents [OSTI]

A differential phase contrast X-ray imaging system includes an X-ray illumination system, a beam splitter arranged in an optical path of the X-ray illumination system, and a detection system arranged in an optical path to detect X-rays after passing through the beam splitter.

Stutman, Daniel; Finkenthal, Michael

2014-07-01T23:59:59.000Z

186

X-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336342  

E-Print Network [OSTI]

, Chicago, IL 60637, USA 3 Cornell High Energy Synchrotron Source and School of Applied and EngineeringX-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336­342 Published online in Wiley InterScience (www to establish a breakthrough in high-resolution, simultaneous area mapping of multiple trace elements

Limburg, Karin E.

187

In Operando X-ray Diffraction and Transmission X-ray Microscopy of Lithium Sulfur Batteries  

E-Print Network [OSTI]

In Operando X-ray Diffraction and Transmission X-ray Microscopy of Lithium Sulfur Batteries Johanna Information ABSTRACT: Rechargeable lithium-sulfur (Li-S) batteries hold great potential for high of these batteries for commercial use. The two primary obstacles are the solubility of long chain lithium

Cui, Yi

188

X-Ray Data from the X-Ray Data Booklet Online  

DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

The original X-Ray Data Booklet, published in 1985, became a classic reference source. The online version has been significantly revised and updated to reflect today's science. Hundreds of pages of authoritative data provide the x-ray properties of elements, information on synchrotron radiation, scattering processes, optics and detectors, and other related calculations, formulas, and data tables.

Thompson, Albert C.; Attwood, David T.; Gullikson, Eric M.; Howells, Malcolm R.; Kortright, Jeffrey B.; Robinson, Arthur L.; Underwood, James H.; Kim, Kwang-Je; Kirz, Janos; Lindau, Ingolf; Pianetta, Piero; Winick, Herman; Williams, Gwyn P.; Scofield, James H.

189

Predicted X-ray backgrounds for the International X-ray Observatory  

E-Print Network [OSTI]

The background that will be observed by IXO's X-ray detectors naturally separates into two components: (1) a Cosmic X-ray Background (CXB), primarily due to unresolved point sources at high energies (E>2 keV), along with ...

Bautz, Marshall W.

190

X-ray variability in M87  

E-Print Network [OSTI]

We present the evidence for X-ray variability from the core and from knot A in the M87 jet based on data from two observations with the Einstein Observatory High Resolution Imager (HRI) and three observations with the ROSAT HRI. The core intensity showed a 16% increase in 17 months ('79-'80); a 12% increase in the 3 years '92 to '95; and a 17% drop in the last half of 1995. The intensity of knot A appears to have decreased by 16% between 92Jun and 95Dec. Although the core variability is consistent with general expectations for AGN nuclei, the changes in knot A provide constraints on the x-ray emission process and geometry. Thus we predict that the x-ray morphology of knot A will differ significantly from the radio and optical structure.

D. E. Harris; J. A. Biretta; W. Junor

1996-12-05T23:59:59.000Z

191

Combined microstructure x-ray optics  

SciTech Connect (OSTI)

Multilayers are man-made microstructures which vary in depth and are now of sufficient quality to be used as x-ray, soft x-ray and extreme ultraviolet optics. Gratings are man-made in plane microstructures which have been used as optic elements for most of this century. Joining of these two optical microstructures to form combined microstructure optical microstructures to form combined microstructure optical elements has the potential for greatly enhancing both the throughput and the resolution attainable in these spectral ranges. The characteristics of these new optic elements will be presented and compared to experiment with emphasis on the unique properties of these combined microstructures. These results reported are general in nature and not limited to the soft x-ray or extreme ultraviolet spectral domains and also apply to neutrons. 19 refs., 7 figs., 4 tabs.

Barbee, T.W. Jr.

1989-02-01T23:59:59.000Z

192

The X-ray/submillimetre link  

E-Print Network [OSTI]

It is widely believed that most of the cosmic X-ray background (XRB) is produced by a vast, hitherto undetected population of obscured AGN. Deep X-ray surveys with Chandra and XMM will soon test this hypothesis. Similarly, recent sub-mm surveys with SCUBA have revealed an analogous population of exceptionally luminous, dust-enshrouded {\\em star-forming} galaxies at high redshift. There is now growing evidence for an intimate link between these obscured populations. There are currently large uncertainties in the models, but several independent arguments lead to the conclusion that a significant fraction of the SCUBA sources ($10-30% $) will contain quasars. Recent observational studies of SCUBA survey sources appear to confirm these predictions, although the relative roles of AGN and star-forming activity in heating the dust are unclear. Forthcoming surveys combining X-ray and sub-mm observations will provide a very powerful tool for disentangling these processes.

O. Almaini

2000-01-07T23:59:59.000Z

193

X-ray atlas of rheumatic diseases  

SciTech Connect (OSTI)

This atlas comprises instructive X-rays of the various inflammatory rheumatic joint diseases in all stages at the extremities and the spinal column. In addition, the complex pattern of the wide range of arthroses, also known as degenerative rheumatic disease is included. Besides the instructive pointers to X-ray diagnosis, the book is also a guide to differential diagnosis. Hence, this book is actually an X-ray atlas of joint diseases in general. Selected Contents: Introduction: What Does ''Rheumatism'' Actually Mean./Radiographic Methodology in Rheumatic Diseases of the Locomotor System/The Mosaic of Arthritis/Adult Rheumatoid Arthritis/Seronegative Spondylarthritis/Classic Collagen Diseases/Enthesiopathies/Gout-Pseudogout

Dihlmann, W.

1986-01-01T23:59:59.000Z

194

X-ray focal spot locating apparatus and method  

DOE Patents [OSTI]

An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

Gilbert, Hubert W. (Cedar Crest, NM)

1985-07-30T23:59:59.000Z

195

2D X-ray scanner and its uses in laboratory reservoir characterization measurements  

SciTech Connect (OSTI)

X-ray techniques are used in petroleum laboratories for a variety of reservoir characterization measurements. This paper describes the configuration of a 2D X-ray scanner and many of the ways in which it simplifies and improves accuracy`s of laboratory measurements. Linear X-ray scanners are most often used to provide descriptions of fluid saturations within core plugs during flow tests. We configured our linear scanner for both horizontal and vertical movement. Samples can be scanned horizontally, vertically, or according to horizontal and vertical grids. X-ray measurements are fast, allowing measurements of two- and three-phase fluid saturations during both steady- and unsteady-state flow processes. Rock samples can be scanned while they are subjected to stress, pore pressure, and temperature conditions simulating those of a petroleum reservoir. Many types of measurements are possible by selecting appropriate X-ray power settings, dopes, filters, and collimator configurations. The scanner has been used for a variety of applications besides fluid saturation measurements. It is useful for measuring porosity distributions in rocks, concentrations of X-ray dopes within flow streams during tracer tests, gap widths in fracture flow cells, fluid interface levels in PVT cells and fluid separators, and other features and phenomena.

Maloney, D.; Doggett, K.

1997-08-01T23:59:59.000Z

196

Energy resolved X-ray grating interferometry  

SciTech Connect (OSTI)

Although compatible with polychromatic radiation, the sensitivity in X-ray phase contrast imaging with a grating interferometer is strongly dependent on the X-ray spectrum. We used an energy resolving detector to quantitatively investigate the dependency of the noise from the spectral bandwidth and to consequently optimize the system-by selecting the best energy band matching the experimental conditions-with respect to sensitivity maximization and, eventually, dose. Further, since theoretical calculations of the spectrum are usually limited due to non-ideal conditions, an energy resolving detector accurately quantifies the spectral changes induced by the interferometer including flux reduction and beam hardening.

Thuering, T.; Stampanoni, M. [Swiss Light Source, Paul Scherrer Institut, Villigen PSI (Switzerland) [Swiss Light Source, Paul Scherrer Institut, Villigen PSI (Switzerland); Institute for Biomedical Engineering, Swiss Federal Institute of Technology, Zurich (Switzerland); Barber, W. C.; Iwanczyk, J. S. [DxRay, Inc., Northridge, California 91324 (United States)] [DxRay, Inc., Northridge, California 91324 (United States); Seo, Y.; Alhassen, F. [UCSF Physics Research Laboratory, Department of Radiology and Biomedical Imaging, University of California, San Francisco, California 94143 (United States)] [UCSF Physics Research Laboratory, Department of Radiology and Biomedical Imaging, University of California, San Francisco, California 94143 (United States)

2013-05-13T23:59:59.000Z

197

Radiobiological studies using gamma and x rays.  

SciTech Connect (OSTI)

There are approximately 500 self-shielded research irradiators used in various facilities throughout the U.S. These facilities use radioactive sources containing either 137Cs or 60Co for a variety of biological investigations. A report from the National Academy of Sciences[1] described the issues with security of particular radiation sources and the desire for their replacement. The participants in this effort prepared two peer-reviewed publications to document the results of radiobiological studies performed using photons from 320-kV x rays and 137Cs on cell cultures and mice. The effectiveness of X rays was shown to vary with cell type.

Potter, Charles Augustus; Longley, Susan W.; Scott, Bobby R. [Lovelace Respiratory Research Institute, Albuquerque, NM; Lin, Yong [Lovelace Respiratory Research Institute, Albuquerque, NM; Wilder, Julie [Lovelace Respiratory Research Institute, Albuquerque, NM; Hutt, Julie A. [Lovelace Respiratory Research Institute, Albuquerque, NM; Padilla, Mabel T. [Lovelace Respiratory Research Institute, Albuquerque, NM; Gott, Katherine M. [Lovelace Respiratory Research Institute, Albuquerque, NM

2013-02-01T23:59:59.000Z

198

Time-resolved x-ray diagnostics  

SciTech Connect (OSTI)

Techniques for time-resolved x-ray diagnostics will be reviewed with emphasis on systems utilizing x-ray diodes or scintillators. System design concerns for high-bandwidth (> 1 GHz) diagnostics will be emphasized. The limitations of a coaxial cable system and a technique for equalizing to improve bandwidth of such a system will be reviewed. Characteristics of new multi-GHz amplifiers will be presented. An example of a complete operational system on the Los Alamos Helios laser will be presented which has a bandwidth near 3 GHz over 38 m of coax. The system includes the cable, an amplifier, an oscilloscope, and a digital camera readout.

Lyons, P.B.

1981-01-01T23:59:59.000Z

199

Theoretical standards in x-ray spectroscopies  

SciTech Connect (OSTI)

We propose to extend our state-of-the-art, ab initio XAFS (X-ray absorption fine structure) codes, FEFF. Our current work has been highly successful in achieving accurate, user-friendly XAFS standards, exceeding the performance of both tabulated standards and other codes by a considerable margin. We now propose to add the capability to treat more complex materials. This includes multiple-scattering, polarization dependence, an approximate treatment of XANES (x-ray absorption near edge structure), and other improvements. We also plan to adapt FEFF to other spectroscopies, e.g. photoelectron diffraction (PD) and diffraction anomalous fine structure (DAFS).

Not Available

1992-01-01T23:59:59.000Z

200

X-Ray Nanoimaging: Instruments and Methods  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
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201

X-ray Computed Tomography | EMSL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsrucLasDelivered energy consumption byAbout SRNL Home SRNL main campusMore thanX-Ray ImagingfeedX-ray

202

Investigations of amino acid-based surfactants at liquid interfaces  

E-Print Network [OSTI]

at the air/water interface by epifluorescence microscopy. Anisotropic feather-like domains were observed in L-enantiomeric monolayers while symmetric circular domains were found in racemic N-SGA monolayers. At a surface pressure of 30 mN/m the enantiomeric...

Yang, Dengliang

2005-11-01T23:59:59.000Z

203

Small Angle X-Ray Scattering Detector  

DOE Patents [OSTI]

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., q.sub.max /q.sub.min.congruent.100.

Hessler, Jan P. (Downers Grove, IL)

2004-06-15T23:59:59.000Z

204

SLAC All Access: X-ray Microscope  

ScienceCinema (OSTI)

SLAC physicists Johanna Nelson and Yijin Liu give a brief overview of the X-ray microscope at the Stanford Synchrotron Radiation Lightsource (SSRL) that is helping improve rechargeable-battery technology by letting researchers peek into the inner workings of batteries as they operate.

Nelson, Johanna; Liu, Yijin

2014-06-13T23:59:59.000Z

205

X-ray spectroscopy of manganese clusters  

SciTech Connect (OSTI)

Much of this thesis represents the groundwork necessary in order to probe Mn clusters more productively than with conventional Mn K-edge XAS and is presented in Part 1. Part 2 contains the application of x-ray techniques to Mn metalloproteins and includes a prognosis at the end of each chapter. Individual Mn oxidation states are more readily distinguishable in Mn L-edge spectra. An empirical mixed valence simulation routine for determining the average Mn oxidation state has been developed. The first Mn L-edge spectra of a metalloprotein were measured and interpreted. The energy of Mn K{beta} emission is strongly correlated with average Mn oxidation state. K{beta} results support oxidation states of Mn(III){sub 2}(IV){sub 2} for the S{sub 1} state of Photosystem II chemical chemically reduced preparations contain predominantly Mn(II). A strength and limitation of XAS is that it probes all of the species of a particular element in a sample. It would often be advantageous to selectively probe different forms of the same element. The first demonstration that chemical shifts in x-ray fluorescence energies can be used to obtain oxidation state-selective x-ray absorption spectra is presented. Spin-dependent spectra can also be used to obtain a more simplified picture of local structure. The first spin-polarized extended x-ray absorption fine structure using Mn K{beta} fluorescence detection is shown.

Grush, M.M. [Univ. of California, Davis, CA (United States). Dept. of Applied Science; [Lawrence Berkeley National Lab., CA (United States). Energy and Environment Div.

1996-06-01T23:59:59.000Z

206

Multiple wavelength X-ray monochromators  

DOE Patents [OSTI]

An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focusing the separate first and second output x-ray radiation wavelengths into separate focal points. 3 figs.

Steinmeyer, P.A.

1992-11-17T23:59:59.000Z

207

Catalog of supersoft X-ray sources  

E-Print Network [OSTI]

This catalog comprises an up-to-date (December 1999) list of luminous (>10^36 erg/s), binary supersoft X-ray sources. This electronic version (including the accompannying Web-pages) supersedes the printed version of Greiner (1996).

J. Greiner

2000-05-11T23:59:59.000Z

208

Molecular Structure and Ordering of Phospholipids at a Liquid-Liquid Interface  

E-Print Network [OSTI]

stretching region of several different phosphocholines adsorbed to the D2O- carbon tetrachloride interface the molecular structure of phosphocholine monolayers adsorbed to the interface between D2O and carbon tetrachloride. Monolayers form from breakup at the interface of aqueous phase phosphocholine vesicles

Richmond, Geraldine L.

209

Dual harmonic Kelvin probe force microscopy at the graphene–liquid interface  

SciTech Connect (OSTI)

Kelvin probe force microscopy (KPFM) is a powerful technique for the determination of the contact potential difference (CPD) between an atomic force microscope tip and a sample under ambient and vacuum conditions. However, for many energy storage and conversion systems, including graphene-based electrochemical capacitors, understanding electrochemical phenomena at the solid–liquid interface is paramount. Despite the vast potential to provide fundamental insight for energy storage materials at the nanoscale, KPFM has found limited applicability in liquid environments to date. Here, using dual harmonic (DH)-KPFM, we demonstrate CPD imaging of graphene in liquid. We find good agreement with measurements performed in air, highlighting the potential of DH-KPFM to probe electrochemistry at the graphene–liquid interface.

Collins, Liam; Rodriguez, Brian J., E-mail: brian.rodriguez@ucd.ie [School of Physics, University College Dublin, Belfield, Dublin 4 (Ireland); Conway Institute of Biomolecular and Biomedical Research, University College Dublin, Belfield, Dublin 4 (Ireland); Kilpatrick, Jason I.; Weber, Stefan A. L. [Conway Institute of Biomolecular and Biomedical Research, University College Dublin, Belfield, Dublin 4 (Ireland); Vlassiouk, Ivan V. [Energy and Transportation Science Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831 (United States); Tselev, Alexander; Jesse, Stephen; Kalinin, Sergei V. [Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831 (United States)

2014-03-31T23:59:59.000Z

210

X-ray microscopy using grazing-incidence reflections optics  

SciTech Connect (OSTI)

The role of Kirkpatrick-Baez microscopes as the workhorse of the x-ray imaging devices is discussed. This role is being extended with the development of a 22X magnification Kirkpatrick-Baez x-ray microscope with multilayer x-ray mirrors. These mirrors can operate at large angles, high x-ray energies, and have a narrow, well defined x-ray energy bandpass. This will make them useful for numerous experiments. However, where a large solid angle is needed, the Woelter microscope will still be necessary and the technology needed to build them will be useful for many other types of x-ray optics.

Price, R.H.

1983-06-30T23:59:59.000Z

211

X-ray microscopy using grazing-incidence reflection optics  

SciTech Connect (OSTI)

The Kirkpatrick-Baez microscopes are described along with their role as the workhorse of the x-ray imaging devices. This role is being extended with the development of a 22X magnification Kirkpatrick-Baez x-ray microscope with multilayer x-ray mirrors. These mirrors can operate at large angles, high x-ray energies, and have a narrow, well defined x-ray energy bandpass. This will make them useful for numerous experiments. However, where a large solid angle is needed, the Woelter microscope will still be necessary and the technology needed to build them will be useful for many other types of x-ray optics.

Price, R.H.

1981-08-06T23:59:59.000Z

212

Rise Time Measurement for Ultrafast X-Ray Pulses  

DOE Patents [OSTI]

A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

Celliers, Peter M.; Weber, Franz A.; Moon, Stephen J.

2005-04-05T23:59:59.000Z

213

Rise time measurement for ultrafast X-ray pulses  

DOE Patents [OSTI]

A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

Celliers, Peter M. (Berkeley, CA); Weber, Franz A. (Oakland, CA); Moon, Stephen J. (Tracy, CA)

2005-04-05T23:59:59.000Z

214

Is the Calcite-Water Interface Understood? Direct Comparisons...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Is the Calcite-Water Interface Understood? Direct Comparisons of Molecular Dynamics Simulations with Specular X-ray Reflectivity Is the Calcite-Water Interface Understood? Direct...

215

X-ray imaging crystal spectrometer for extended X-ray sources  

DOE Patents [OSTI]

Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

Bitter, Manfred L. (Princeton, NJ); Fraenkel, Ben (Jerusalem, IL); Gorman, James L. (Bordentown, NJ); Hill, Kenneth W. (Lawrenceville, NJ); Roquemore, A. Lane (Cranbury, NJ); Stodiek, Wolfgang (Princeton, NJ); von Goeler, Schweickhard E. (Princeton, NJ)

2001-01-01T23:59:59.000Z

216

X-RAY POINT-SOURCE POPULATIONS CONSTITUTING THE GALACTIC RIDGE X-RAY EMISSION  

SciTech Connect (OSTI)

Apparently diffuse X-ray emission has been known to exist along the central quarter of the Galactic Plane since the beginning of X-ray astronomy; this is referred to as the Galactic Ridge X-ray emission (GRXE). Recent deep X-ray observations have shown that numerous X-ray point sources account for a large fraction of the GRXE in the hard band (2-8 keV). However, the nature of these sources is poorly understood. Using the deepest X-ray observations made in the Chandra bulge field, we present the result of a coherent photometric and spectroscopic analysis of individual X-ray point sources for the purpose of constraining their nature and deriving their fractional contributions to the hard-band continuum and Fe K line emission of the GRXE. Based on the X-ray color-color diagram, we divided the point sources into three groups: A (hard), B (soft and broad spectrum), and C (soft and peaked spectrum). The group A sources are further decomposed spectrally into thermal and non-thermal sources with different fractions in different flux ranges. From their X-ray properties, we speculate that the group A non-thermal sources are mostly active galactic nuclei and the thermal sources are mostly white dwarf (WD) binaries such as magnetic and non-magnetic cataclysmic variables (CVs), pre-CVs, and symbiotic stars, whereas the group B and C sources are X-ray active stars in flares and quiescence, respectively. In the log N-log S curve of the 2-8 keV band, the group A non-thermal sources are dominant above Almost-Equal-To 10{sup -14} erg cm{sup -2} s{sup -1}, which is gradually taken over by Galactic sources in the fainter flux ranges. The Fe K{alpha} emission is mostly from the group A thermal (WD binaries) and the group B (X-ray active stars) sources.

Morihana, Kumiko [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan)] [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Tsujimoto, Masahiro; Ebisawa, Ken [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan)] [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan); Yoshida, Tessei, E-mail: morihana@crab.riken.jp [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)] [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)

2013-03-20T23:59:59.000Z

217

Economizer Based Data Center Liquid Cooling with Advanced Metal Interfaces  

SciTech Connect (OSTI)

A new chiller-less data center liquid cooling system utilizing the outside air environment has been shown to achieve up to 90% reduction in cooling energy compared to traditional chiller based data center cooling systems. The system removes heat from Volume servers inside a Sealed Rack and transports the heat using a liquid loop to an Outdoor Heat Exchanger which rejects the heat to the outdoor ambient environment. The servers in the rack are cooled using a hybrid cooling system by removing the majority of the heat generated by the processors and memory by direct thermal conduction using coldplates and the heat generated by the remaining components using forced air convection to an air- to- liquid heat exchanger inside the Sealed Rack. The anticipated benefits of such energy-centric configurations are significant energy savings at the data center level. When compared to a traditional 10 MW data center, which typically uses 25% of its total data center energy consumption for cooling this technology could potentially enable a cost savings of up to $800,000-$2,200,000/year (assuming electricity costs of 4 to 11 cents per kilowatt-hour) through the reduction in electrical energy usage.

Timothy Chainer

2012-11-30T23:59:59.000Z

218

Cu-Bi as a Model System For Liquid Phase Sintered Thermal Interface Management Materials  

E-Print Network [OSTI]

relates electrical resistivity to thermal conductivity for materials where electrons are principleCu-Bi as a Model System For Liquid Phase Sintered Thermal Interface Management Materials P to produce composite materials. A high melting phase (HMP) and low melting phase (LMP) are mixed

Collins, Gary S.

219

High resolution x-ray microscope  

SciTech Connect (OSTI)

The authors present x-ray images of grid meshes and biological material obtained using a microspot x-ray tube with a multilayer optic and a 92-element parabolic compound refractive lens (CRL) made of a plastic containing only hydrogen and carbon. Images obtained using this apparatus are compared with those using an area source with a spherical lens and a spherical lens with multilayer condenser. The authors found the best image quality using the multilayer condenser with a parabolic lens, compared to images with a spherical lens and without the multilayer optics. The resolution was measured using a 155-element parabolic CRL and a multilayer condenser with the microspot tube. The experiment demonstrates about 1.1 {mu}m resolution.

Gary, C. K.; Park, H.; Lombardo, L. W.; Piestrup, M. A.; Cremer, J. T.; Pantell, R. H.; Dudchik, Y. I. [Adelphi Technology, Inc. 981-B Industrial Road, San Carlos, California 94070 (United States); Department of Electrical Engineering, Stanford University, Stanford, California 94305 (United States); Institute of Applied Physics Problems, Kurchatova 7, Minsk 220064 (Belarus)

2007-04-30T23:59:59.000Z

220

X-ray radiography for container inspection  

DOE Patents [OSTI]

Arrangements of X-ray inspection systems are described for inspecting high-z materials in voluminous objects such as containers. Inspection methods may involve generating a radiographic image based on detected attenuation corresponding to a pulsed beams of radiation transmitted through a voluminous object. The pulsed beams of radiation are generated by a high-energy source and transmitted substantially downward along an incident angle, of approximately 1.degree. to 30.degree., to a vertical axis extending through the voluminous object. The generated radiographic image may be analyzed to detect on localized high attenuation representative of high-z materials and to discriminate high-z materials from lower and intermediate-z materials on the basis of the high density and greater attenuation of high-z material for higher energy (3-10 MeV) X-rays, and the compact nature of threatening masses of fissionable materials.

Katz, Jonathan I. (Clayton, MO); Morris, Christopher L. (Los Alamos, NM)

2011-06-07T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

Biological Imaging by Soft X-Ray Diffraction Microscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in...

222

The X-ray Microcalorimeter Spectrometer onboard of IXO  

E-Print Network [OSTI]

One of the instruments on the International X-ray Observatory (IXO), under study with NASA, ESA and JAXA, is the X-ray Microcalorimeter Spectrometer (XMS). This instrument, which will provide high spectral resolution images, ...

Figueroa-Feliciano, Enectali

223

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscop...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Refinement Friday, September 28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray...

224

Sample holder for X-ray diffractometry  

DOE Patents [OSTI]

A sample holder for use with X-ray diffractometers with the capability to rotate the sample, as well as to adjust the position of the sample in the x, y, and z directions. Adjustment in the x direction is accomplished through loosening set screws, moving a platform, and retightening the set screws. Motion translators are used for adjustment in the y and z directions. An electric motor rotates the sample, and receives power from the diffractometer.

Hesch, Victor L. (Los Alamos, NM)

1992-01-01T23:59:59.000Z

225

Columbia University X-Ray Measurements  

E-Print Network [OSTI]

V-720 keV · NaI 2x2x2" detector views an energy range of 1 keV-3 MeV Store signal in the tree. computer configuration. Plasmas were created using multi-frequency ECRH, and we find that most of the plasma energy is stored in the fast electrons. The energy spectrum of the x-ray emission below 740 keV is measured

226

X-rays from Supernova Remnants  

E-Print Network [OSTI]

A summary of X-ray observations of supernova remnants is presented including the explosion fragment A of the Vela SNR, Tycho, N132D, RX J0852-4622, the Crab Nebula and the 'bulls eye', and SN 1987A, high-lighting the progress made with Chandra and XMM-Newton and touching upon the questions which arise from these observations and which might inspire future research.

B. Aschenbach

2002-08-28T23:59:59.000Z

227

X-ray Free-electron Lasers  

SciTech Connect (OSTI)

In a free-electron laser (FEL) the lasing medium is a high-energy beam of electrons flying with relativistic speed through a periodic magnetic field. The interaction between the synchrotron radiation that is produced and the electrons in the beam induces a periodic bunching of the electrons, greatly increasing the intensity of radiation produced at a particular wavelength. Depending only on a phase match between the electron energy and the magnetic period, the wavelength of the FEL radiation can be continuously tuned within a wide spectral range. The FEL concept can be adapted to produce radiation wavelengths from millimeters to Angstroms, and can in principle produce hard x-ray beams with unprecedented peak brightness, exceeding that of the brightest synchrotron source by ten orders of magnitude or more. This paper focuses on short-wavelength FELs. It reviews the physics and characteristic properties of single-pass FELs, as well as current technical developments aiming for fully coherent x-ray radiation pulses with pulse durations in the 100 fs to 100 as range. First experimental results at wavelengths around 100 nm and examples of scientific applications planned on the new, emerging x-ray FEL facilities are presented.

Feldhaus, J.; /DESY; Arthur, J.; Hastings, J.B.; /SLAC

2007-02-23T23:59:59.000Z

228

The X-ray Telescope of CAST  

E-Print Network [OSTI]

The Cern Axion Solar Telescope (CAST) is in operation and taking data since 2003. The main objective of the CAST experiment is to search for a hypothetical pseudoscalar boson, the axion, which might be produced in the core of the sun. The basic physics process CAST is based on is the time inverted Primakoff effect, by which an axion can be converted into a detectable photon in an external electromagnetic field. The resulting X-ray photons are expected to be thermally distributed between 1 and 7 keV. The most sensitive detector system of CAST is a pn-CCD detector combined with a Wolter I type X-ray mirror system. With the X-ray telescope of CAST a background reduction of more than 2 orders off magnitude is achieved, such that for the first time the axion photon coupling constant g_agg can be probed beyond the best astrophysical constraints g_agg < 1 x 10^-10 GeV^-1.

M. Kuster; H. Bräuninger; S. Cébrian; M. Davenport; C. Elefteriadis; J. Englhauser; H. Fischer; J. Franz; P. Friedrich; R. Hartmann; F. H. Heinsius; D. H. H. Hoffmann; G. Hoffmeister; J. N. Joux; D. Kang; K. Königsmann; R. Kotthaus; T. Papaevangelou; C. Lasseur; A. Lippitsch; G. Lutz; J. Morales; A. Rodríguez; L. Strüder; J. Vogel; K. Zioutas

2007-05-10T23:59:59.000Z

229

X-Ray Searches for Solar Axions  

E-Print Network [OSTI]

Axions generated thermally in the solar core can convert nearly directly to X-rays as they pass through the solar atmosphere via interaction with the magnetic field. The result of this conversion process would be a diffuse centrally-concentrated source of few-keV X-rays at disk center; it would have a known dimension, of order 10% of the solar diameter, and a spectral distribution resembling the blackbody spectrum of the solar core. Its spatial structure in detail would depend on the distribution of mass and field in the solar atmosphere. The brightness of the source depends upon these factors as well as the unknown coupling constant and the unknown mass of the axion; this particle is hypothetical and no firm evidence for its existence has been found yet. We describe the solar magnetic environment as an axion/photon converter and discuss the upper limits obtained by existing and dedicated observations from three solar X-ray observatories: Yohkoh, RHESSI, and Hinode

Hugh S. Hudson; L. W. Acton; E. DeLuca; I. G. Hannah; K. Reardon; K. Van Bibber

2012-01-22T23:59:59.000Z

230

Applications of holography to x-ray imaging  

SciTech Connect (OSTI)

In this paper we consider various applications of holographic techniques to the problem of soft x-ray imaging. We give special attention to imaging biological material using x-rays in the wavelength range 24 to 45A. We describe some experiments on formation and reconstruction of x-ray holograms and propose some ways in which holographic techniques might contribute to the difficult problem of fabricating optical elements for use in the soft x-ray region.

Howells, M.; Iarocci, M.; Kenney, J.; Rarback, H.; Rosser, R.; Yun, W.

1985-03-01T23:59:59.000Z

231

Applications of holography to X-ray imaging  

SciTech Connect (OSTI)

In this paper the authors consider various applications of holographic techniques to the problem of soft x-ray imaging. Special attention is given to imaging biological material using x-rays in the wavelength range 24-45A. The authors describe some experiments on formation and reconstruction of x-ray holograms and propose some ways in which holographic techniques might contribute to the difficult problem of fabricating optical elements for use in the soft x-ray region.

Howells, M.; Iarocci, M.; Kenney, J.; Rarback, H.; Rosser, R.; Yun, W.

1985-01-01T23:59:59.000Z

232

X-ray MicroCT Training Presentation  

E-Print Network [OSTI]

X-ray MicroCT Training Presentation T. Fettah Kosar, PhD Center for Nanoscale Systems Harvard) Model: HMXST225 (max. 225 kV) #12;Overview 3 Introduction to X-ray imaging and Computed Tomography (CT) · What are X-rays and how do we generate and image them? · How do we magnify X-ray images and keep them

233

Anomalous X-ray Diffraction Studies for Photovoltaic Applications  

SciTech Connect (OSTI)

Anomalous X-ray Diffraction (AXRD) has become a useful technique in characterizing bulk and nanomaterials as it provides specific information about the crystal structure of materials. In this project we present the results of AXRD applied to materials for photovoltaic applications: ZnO loaded with Ga and ZnCo{sub 2}O{sub 4} spinel. The X-ray diffraction data collected for various energies were plotted in Origin software. The peaks were fitted using different functions including Pseudo Voigt, Gaussian, and Lorentzian. This fitting provided the integrated intensity data (peaks area values), which when plotted as a function of X-ray energies determined the material structure. For the first analyzed sample, Ga was not incorporated into the ZnO crystal structure. For the ZnCo{sub 2}O{sub 4} spinel Co was found in one or both tetrahedral and octahedral sites. The use of anomalous X-ray diffraction (AXRD) provides element and site specific information for the crystal structure of a material. This technique lets us correlate the structure to the electronic properties of the materials as it allows us to probe precise locations of cations in the spinel structure. What makes it possible is that in AXRD the diffraction pattern is measured at a number of energies near an X-ray absorption edge of an element of interest. The atomic scattering strength of an element varies near its absorption edge and hence the total intensity of the diffraction peak changes by changing the X-ray energy. Thus AXRD provides element specific structural information. This method can be applied to both crystalline and liquid materials. One of the advantages of AXRD in crystallography experiments is its sensitivity to neighboring elements in the periodic tables. This method is also sensitive to specific crystallographic phases and to a specific site in a phase. The main use of AXRD in this study is for transparent conductors (TCs) analysis. TCs are considered to be important materials because of their efficiency and low risk of environmental pollution. These materials are important to solar cells as a result of their remarkable combination of optical and electrical properties, including high electrical conductivity and high optical transparency in the spectrum of visible light. TCs provide a transparent window, which allows sunlight to pass through while also allowing electricity to conduct out of the cell. Spinel materials have the chemical form AB{sub 2}O{sub 4}, and are made of a face-centered cubic (FCC) lattice of oxygen anions and cations in specific interstitial sites. A normal spinel has all A cations on tetrahedral sites and B cations on octahedral sites. In contrast; an inverse spinel has the A and half of the B cations on octahedral sites and the other half of the B cations on tetrahedral sites; a mixed spinel lies between. In the spinel structure, 8 of 64 possible tetrahedral sites and 16 of 32 possible octahedral sites are filled. Normal spinels have particularly high conduction as the linear octahedral chains of B cations likely serve as conduction paths. In this paper we present how the data obtained with AXRD is used to analyze TCs properties as they apply to photovoltaic applications. One of the materials used for this analysis is zinc oxide. It has been loaded with 5% and 10% of Ga, which has an absorption edge of 10367 eV. The peak (100) was measured for the zinc oxide loaded with 10% Ga. In the case of 5% Ga, we measured peaks (100) and (101). With the information provided by the AXRD we can identify if Ga is being incorporated in the ZnO crystal structure. The analysis of 311 plane in the ZnCo{sub 2}O{sub 4} spinel shows if Co is in tetrahedral or octahedral site.

Not Available

2011-06-22T23:59:59.000Z

234

Modeling of ultrasound transmission through a solid-liquid interface comprising a network of gas pockets  

SciTech Connect (OSTI)

Ultrasonic inspection of sodium-cooled fast reactor requires a good acoustic coupling between the transducer and the liquid sodium. Ultrasonic transmission through a solid surface in contact with liquid sodium can be complex due to the presence of microscopic gas pockets entrapped by the surface roughness. Experiments are run using substrates with controlled roughness consisting of a network of holes and a modeling approach is then developed. In this model, a gas pocket stiffness at a partially solid-liquid interface is defined. This stiffness is then used to calculate the transmission coefficient of ultrasound at the entire interface. The gas pocket stiffness has a static, as well as an inertial component, which depends on the ultrasonic frequency and the radiative mass.

Paumel, K.; Baque, F. [CEA, DEN, Nuclear Technology Department, F-13108 Saint-Paul-lez-Durance (France); Moysan, J.; Corneloup, G. [Laboratoire de Caracterisation Non Destructive, Universite de la Mediterranee, IUT Aix-en-Provence, Avenue Gaston Berger, 13625 Aix-en-Provence (France); Chatain, D. [CNRS, Aix-Marseille Universite, CINAM-UPR3118, Campus de Luminy, Case 913, 13288 Marseille cedex 09 (France)

2011-08-15T23:59:59.000Z

235

Detection of Nonthermal Melting by Ultrafast X-ray  

E-Print Network [OSTI]

of super- heating of the interface but limited by the speed of sound. Typically, a layer a few tens, if a solid is heated to or above the melting temperature, nucleation of the liquid phase occurs around), which exceeds the melting temperature within several picoseconds. After nucleation of the liquid phase

Geddes, Cameron Guy Robinson

236

A novel instrument for quantitative nanoanalytics involving complementary X-ray methodologies  

SciTech Connect (OSTI)

A novel ultra-high vacuum instrument for X-ray reflectometry and spectrometry-related techniques for nanoanalytics by means of synchrotron radiation has been constructed and commissioned. This versatile instrument was developed by the Physikalisch-Technische Bundesanstalt, Germany's national metrology institute, and includes a 9-axis manipulator that allows for an independent alignment of the samples with respect to all degrees of freedom. In addition, a rotational and translational movement of several photodiodes as well as a translational movement of an aperture system in and out of the beam is provided. Thus, the new instrument enables various analytical techniques based on energy dispersive X-ray detectors such as reference-free X-ray fluorescence analysis (XRF), total-reflection XRF, grazing-incidence XRF in addition to optional X-ray reflectometry measurements or polarization-dependent X-ray absorption fine structure analyses. With this instrument samples having a size of up to 100 mm Multiplication-Sign 100 mm can be analyzed with respect to their mass deposition, elemental or spatial composition, or the species in order to probe surface contamination, layer composition and thickness, the depth profile of matrix elements or implants, the species of nanolayers, nanoparticles or buried interfaces as well as the molecular orientation of bonds. Selected applications of this advanced ultra-high vacuum instrument demonstrate both its flexibility and capability.

Lubeck, J.; Beckhoff, B.; Fliegauf, R.; Holfelder, I.; Hoenicke, P.; Mueller, M.; Pollakowski, B.; Reinhardt, F.; Weser, J. [Physikalisch-Technische Bundesanstalt, Abbestr. 2-12, 10587 Berlin (Germany)

2013-04-15T23:59:59.000Z

237

Femtosecond laser-electron x-ray source  

DOE Patents [OSTI]

A femtosecond laser-electron X-ray source. A high-brightness relativistic electron injector produces an electron beam pulse train. A system accelerates the electron beam pulse train. The femtosecond laser-electron X-ray source includes a high intra-cavity power, mode-locked laser and an x-ray optics system.

Hartemann, Frederic V.; Baldis, Hector A.; Barty, Chris P.; Gibson, David J.; Rupp, Bernhard

2004-04-20T23:59:59.000Z

238

X-ray Diffraction Laboratory Department of Chemistry  

E-Print Network [OSTI]

X-ray Diffraction Laboratory Department of Chemistry Texas A & M University College Station, Texas Phone : 979-845-9125 www.chem.tamu.edu/xray xray@tamu.edu X-rayDiffractionLaboratory DepartmentofChemistry 3255TAMU CollegeStation,TX77843-3255 Mission The purpose of our laboratory is to provide X-ray

Meagher, Mary

239

X-ray Diffraction Practicals 1 Graphics Programs  

E-Print Network [OSTI]

X-ray Diffraction Practicals 1 Graphics Programs that will read SHELX or CIF files J. Reibenspies, N. Bhuvanesh ver 1.0.0 #12;X-ray Diffraction Practicals 2 Free software. Gretep : Reads SHELX files shelx files or output thermal ellipsoid plots. http://www.umass.edu/microbio/rasmol/ #12;X-ray

Meagher, Mary

240

X-ray Emission from Massive Stars David Cohen  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore University, Oct. 13, 2005 astro.swarthmore.edu/~cohen/ #12;Outline 1. What you need to know: a. X-rays from the Sun - magnetic activity, x-ray spectra b. Hot stars c. Radiation-driven winds and the Doppler shift d

Cohen, David

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

X-Ray Photoelectron Spectroscopy XPS Mark Engelhard  

E-Print Network [OSTI]

X-Ray Photoelectron Spectroscopy XPS Mark Engelhard 1 #12;EMSL XPS Instrumentation 2 Physical Electronics Quantera XPS High Energy Resolution Focused X-ray Beam Capability Catalysis reaction and processing chamber with inert atmosphere glove box connected to a PHI Quantera Scanning X-ray Microprobe

242

HIgh Rate X-ray Fluorescence Detector  

SciTech Connect (OSTI)

The purpose of this project was to develop a compact, modular multi-channel x-ray detector with integrated electronics. This detector, based upon emerging silicon drift detector (SDD) technology, will be capable of high data rate operation superior to the current state of the art offered by high purity germanium (HPGe) detectors, without the need for liquid nitrogen. In addition, by integrating the processing electronics inside the detector housing, the detector performance will be much less affected by the typically noisy electrical environment of a synchrotron hutch, and will also be much more compact than current systems, which can include a detector involving a large LN2 dewar and multiple racks of electronics. The combined detector/processor system is designed to match or exceed the performance and features of currently available detector systems, at a lower cost and with more ease of use due to the small size of the detector. In addition, the detector system is designed to be modular, so a small system might just have one detector module, while a larger system can have many â?? you can start with one detector module, and add more as needs grow and budget allows. The modular nature also serves to simplify repair. In large part, we were successful in achieving our goals. We did develop a very high performance, large area multi-channel SDD detector, packaged with all associated electronics, which is easy to use and requires minimal external support (a simple power supply module and a closed-loop water cooling system). However, we did fall short of some of our stated goals. We had intended to base the detector on modular, large-area detectors from Ketek GmbH in Munich, Germany; however, these were not available in a suitable time frame for this project, so we worked instead with pnDetector GmbH (also located in Munich). They were able to provide a front-end detector module with six 100 m^2 SDD detectors (two monolithic arrays of three elements each) along with associated preamplifiers; these detectors surpassed the performance we expected to get from the Ketek detectors, however they are housed in a sealed module, which does not offer the ease of repair and expandability weâ??d hoped to achieve with the Ketek SDDâ??s. Our packaging efforts were quite successful, as we came up with a very compact way to mount the detector and to house the associated electronics, as well as a very effective way to reliably take out the heat (from the electronics as well as the detectorâ??s Peltier coolers) without risk of condensation and without external airflow or vibration, which could create problems for the target applications. While we were able to design compact processing electronics that fit into the detector assembly, they are still at the prototype stage, and would require a significant redesign to achieve product status. We have not yet tested this detector at a synchrotron facility; we do still plan on working with some close contacts at the nearby Stanford Synchrotron Radiation Laboratory (SSRL) to get some testing with the beam (using existing commercial electronics for readout, as the integrated processor is not ready for use).

Grudberg, Peter Matthew [XIA LLC

2013-04-30T23:59:59.000Z

243

Quantitative x-ray imager (abstract)  

SciTech Connect (OSTI)

We report on development of a quantitative x-ray imager (QXI) for the national Inertial Confinement Fusion Program. Included in this development is a study of photocathode response as a function of photon energy, 2--17.5 keV, which is related to diagnostic development on the National Ignition Facility (NIF). The QXI is defined as being a quantative imager due to the repeated characterization. This instrument is systematically checked out, electronically as well as its photocathode x-ray response, both on a direct current and pulsed x-ray sources, before and after its use on a shot campaign. The QXI is a gated x-ray imager1 used for a variety of experiments conducted in the Inertial Confinement Fusion and Radiation Physics Program. The camera was assembled in Los Alamos and has been under development since 1997 and has now become the workhorse framing camera by the program. The electronics were built by Grant Applied Physics of San Fransisco, CA.2 The QXI has been used at the LANL Trident, LLNL Nova, and University of Rochester Laboratory OMEGA laser facilities. The camera consists of a grated microchannel plate (MCP), a phosphor coated fiberoptic faceplate coupled to film for data readout, along with high speed electronic pulsers to drive the x-ray detector. The QXI has both a two-strip and a four-strip detection head and has the ability to individually bias the gain of each of the strips. The timing of the QXI was done at the Trident short pulse laboratory, using 211 nm light. Single strip jitter was looked at as well and determined to be <25 ps. Flatfielding of the photocathode across the MCP was done with the Trident main laser with 150 J on a gold disk with a 1 ns. Spatial resolution was determined to be <5 {mu}m by using the same laser conditions as before and a backlit 1000 lp/in. grid. The QXI has been used on cylindrical implosion work at the Nova Laser Facility, and on direct-drive cylinder mix and indirect-drive high convergence implosion experiments at OMEGA. Its two-strip module has provided the capability to look at point backlighters, as part of technique development for experiments on the NIF. Its next use will be in March 2000 with its off axis viewer nose at Omega, providing a perpendicular view of Rayleigh--Taylor spike dissipation.

Evans, Scott C.; Archuleta, Tom N.; Oertel, John A.; Walsh, Peter J.

2001-01-01T23:59:59.000Z

244

X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO)  

DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

The primary interactions of low-energy x-rays within condensed matter, viz. photoabsorption and coherent scattering, are described for photon energies outside the absorption threshold regions by using atomic scattering factors. The atomic scattering factors may be accurately determined from the atomic photoabsorption cross sections using modified Kramers-Kronig dispersion relations. From a synthesis of the currently available experimental data and recent theoretical calculations for photoabsorption, the angle-independent, forward-scattering components of the atomic scattering factors have been thus semiempirically determined and tabulated here for 92 elements and for the region 50-30,000 eV. Atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction. The incoherent scattering contributions that become significant for the light elements at the higher photon energies are similarly determined. The basic x-ray interaction relations that are used in applied x-ray physics are presented here in terms of the atomic scattering factors. The bulk optical constants are also related to the atomic scattering factors. These atomic and optical relations are applied to the detailed calculation of the reflectivity characteristics of a series of practical x-ray mirror, multilayer, and crystal monochromators. Comparisons of the results of this semiempirical,"atom-like", description of x-ray interactions for the low-energy region with those of experiment and ab initio theory are presented.

Henke, B.L.; Gullikson, E.M.; Davis, J.C.

245

Calibrating X-ray Imaging Devices for Accurate Intensity Measurement  

SciTech Connect (OSTI)

The purpose of the project presented is to develop methods to accurately calibrate X-ray imaging devices. The approach was to develop X-ray source systems suitable for this endeavor and to develop methods to calibrate solid state detectors to measure source intensity. NSTec X-ray sources used for the absolute calibration of cameras are described, as well as the method of calibrating the source by calibrating the detectors. The work resulted in calibration measurements for several types of X-ray cameras. X-ray camera calibration measured efficiency and efficiency variation over the CCD. Camera types calibrated include: CCD, CID, back thinned (back illuminated), front illuminated.

Haugh, M. J.

2011-07-28T23:59:59.000Z

246

Proceedings of the workshop on X-ray computed microtomography  

SciTech Connect (OSTI)

This report consists of vugraphs from the nine presentations at the conference. Titles of the presentations are: CMT: Applications and Techniques; Computer Microtomography Using X-rays from Third Generation Synchrotron X-ray; Approaches to Soft-X-ray Nanotomography; Diffraction Enhanced Tomography; X-ray Computed Microtomography Applications at the NSLS; XCMT Applications in Forestry and Forest Products; 3DMA: Investigating Three Dimensional Pore Geometry from High Resolution Images; X-ray Computed Microtomography Studies of Volcanic Rock; and 3-D Visualization of Tomographic Volumes.

NONE

1998-02-01T23:59:59.000Z

247

X-Ray Source Based on the Parametric X-Rays  

E-Print Network [OSTI]

Prospects of parametric x-rays (PXR) application for the development of a tuneable quasi-monochromatic x-ray source for medical imaging are discussed. Analysis of basic requirements for electron accelerator shows that it must be relatively low-energy and high-current linac. In comparison with known ultra-relativistic cases, at low energies PXR properties will be modified to a great extent by multiple scattering of the electrons. PXR intensity dependence on target thickness and beam energy are calculated taking multiple scattering into account. It is concluded that PXR source based on real medical accelerators is feasible and can provide x-ray flux needful for obtaining high quality medical images.

Alexander Lobko; Olga Lugovskaya

2005-09-02T23:59:59.000Z

248

Apparatus for monitoring X-ray beam alignment  

DOE Patents [OSTI]

A self-contained, hand-held apparatus is provided for monitoring alignment of an X-ray beam in an instrument employing an X-ray source. The apparatus includes a transducer assembly containing a photoresistor for providing a range of electrical signals responsive to a range of X-ray beam intensities from the X-ray beam being aligned. A circuit, powered by a 7.5 VDC power supply and containing an audio frequency pulse generator whose frequency varies with the resistance of the photoresistor, is provided for generating a range of audible sounds. A portion of the audible range corresponds to low X-ray beam intensity. Another portion of the audible range corresponds to high X-ray beam intensity. The transducer assembly may include an a photoresistor, a thin layer of X-ray fluorescent material, and a filter layer transparent to X-rays but opaque to visible light. X-rays from the beam undergoing alignment penetrate the filter layer and excite the layer of fluorescent material. The light emitted from the fluorescent material alters the resistance of the photoresistor which is in the electrical circuit including the audio pulse generator and a speaker. In employing the apparatus, the X-ray beam is aligned to a complete alignment by adjusting the X-ray beam to produce an audible sound of the maximum frequency. 2 figures.

Steinmeyer, P.A.

1991-10-08T23:59:59.000Z

249

Apparatus for monitoring X-ray beam alignment  

DOE Patents [OSTI]

A self-contained, hand-held apparatus is provided for minitoring alignment of an X-ray beam in an instrument employing an X-ray source. The apparatus includes a transducer assembly containing a photoresistor for providing a range of electrical signals responsive to a range of X-ray beam intensities from the X-ray beam being aligned. A circuit, powered by a 7.5 VDC power supply and containing an audio frequency pulse generator whose frequency varies with the resistance of the photoresistor, is provided for generating a range of audible sounds. A portion of the audible range corresponds to low X-ray beam intensity. Another portion of the audible range corresponds to high X-ray beam intensity. The transducer assembly may include an a photoresistor, a thin layer of X-ray fluorescent material, and a filter layer transparent to X-rays but opaque to visible light. X-rays from the beam undergoing alignment penetrate the filter layer and excite the layer of fluorescent material. The light emitted from the fluorescent material alters the resistance of the photoresistor which is in the electrical circuit including the audio pulse generator and a speaker. In employing the apparatus, the X-ray beam is aligned to a complete alignment by adjusting the X-ray beam to produce an audible sound of the maximum frequency.

Steinmeyer, Peter A. (Arvada, CO)

1991-10-08T23:59:59.000Z

250

Interface for the rapid analysis of liquid samples by accelerator mass spectrometry  

DOE Patents [OSTI]

An interface for the analysis of liquid sample having carbon content by an accelerator mass spectrometer including a wire, defects on the wire, a system for moving the wire, a droplet maker for producing droplets of the liquid sample and placing the droplets of the liquid sample on the wire in the defects, a system that converts the carbon content of the droplets of the liquid sample to carbon dioxide gas in a helium stream, and a gas-accepting ion source connected to the accelerator mass spectrometer that receives the carbon dioxide gas of the sample in a helium stream and introduces the carbon dioxide gas of the sample into the accelerator mass spectrometer.

Turteltaub, Kenneth; Ognibene, Ted; Thomas, Avi; Daley, Paul F; Salazar Quintero, Gary A; Bench, Graham

2014-02-04T23:59:59.000Z

251

X-ray emission properties of galaxies in Abell 3128  

E-Print Network [OSTI]

We use archival Chandra X-ray Observatory data to investigate X-ray emission from early-type galaxies in the rich z=0.06 cluster Abell 3128. By combining the X-ray count-rates from an input list of optically-selected galaxies, we obtain a statistical detection of X-ray flux, unbiased by X-ray selection limits. Using 87 galaxies with reliable Chandra data, X-ray emission is detected for galaxies down to M_B ~ -19.0, with only an upper limit determined for galaxies at M_B ~ -18.3. The ratio of X-ray to optical luminosities is consistent with recent determinations of the low-mass X-ray binary content of nearby elliptical galaxies. Taken individually, in contrast, we detect significant (3sigma) flux for only six galaxies. Of these, one is a foreground galaxy, while two are optically-faint galaxies with X-ray hardness ratios characteristic of active galactic nuclei. The remaining three detected galaxies are amongst the optically-brightest cluster members, and have softer X-ray spectra. Their X-ray flux is higher than that expected from X-ray binaries, by a factor 2-10; the excess suggests these galaxies have retained their hot gaseous haloes. The source with the highest L_X / L_B ratio is of unusual optical morphology with prominent sharp-edged shells. Notwithstanding these few exceptions, the cluster population overall exhibits X-ray properties consistent with their emission being dominated by X-ray binaries. We conclude that in rich cluster environments, interaction with the ambient intra-cluster medium acts to strip most galaxies of their hot halo gas.

Russell J. Smith

2003-07-15T23:59:59.000Z

252

X-ray generation using carbon nanotubes  

E-Print Network [OSTI]

of these sys- tems are illustrated in Figure 2(b) also outlines the principle mode of operation. Here, sealed in an inexpensive and eas- ily fabricated evacuated glass or ceramic envelope, the elec- trons are liberated from a metallic filament, often made... - ment of CNT-based FE sources is provided in [152]. Here we provide a condensed review of the progress, as it pertains to X-ray sources, since then. CNTs have some of the highest attainable aspect ratios, high thermal conductivity, low chemical...

Parmee, Richard J.; Collins, Clare M.; Milne, William I.; Cole, Matthew T.

2015-01-06T23:59:59.000Z

253

SMB, Small Angle X-Ray Scattering  

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254

SMB, X-ray Absorption Spectroscopy  

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255

SMB, X-ray Emission Spectroscopy  

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256

X-ray Microscopy and Imaging: FAQs  

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257

X-rays Illuminate Ancient Archimedes Text  

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258

X-Ray Nanoimaging: Instruments and Methods  

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259

X-Ray Science Division (XSD)  

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260

Gamma Radiation & X-Rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

Femtosecond X-ray protein nanocrystallography  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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262

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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263

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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264

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

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265

The BMW X-ray Cluster Survey  

E-Print Network [OSTI]

We describe the main features of the BMW survey of serendipitous X-ray clusters, based on the still unexploited ROSAT-HRI archival observations. The sky coverage, surface density and first deep optical CCD images of the candidates indicate that this sample can represent an excellent complement to the existing PSPC deep cluster surveys and will provide us with a fully independent probe of the evolution of the cluster abundance, in addition to significantly increasing the number of clusters known at z>0.6.

Alberto Moretti; Luigi Guzzo; Sergio Campana; Stefano Covino; Davide Lazzati; Marcella Longhetti; Emilio Molinari; Maria Rosa Panzera; Gianpiero Tagliaferri; Ian Dell'Antonio

2001-03-21T23:59:59.000Z

266

The BMW X-ray Cluster Survey  

E-Print Network [OSTI]

We describe the main features of the BMW survey of serendipitous X-ray clusters, based on the still unexploited ROSAT-HRI archival observations. The sky coverage, surface density and first deep optical CCD images of the candidates indicate that this sample can represent an excellent complement to the existing PSPC deep cluster surveys and will provide us with a fully independent probe of the evolution of the cluster abundance, in addition to significantly increasing the number of clusters known at z>0.6.

Moretti, A; Campana, S; Covino, S; Lazzati, D; Longhetti, M; Molinari, E; Panzera, M R; Tagliaferri, G; Dell'Antonio, I P; Moretti, Alberto; Guzzo, Luigi; Campana, Sergio; Covino, Stefano; Lazzati, Davide; Longhetti, Marcella; Molinari, Emilio; Panzera, Maria Rosa; Tagliaferri, Gianpiero; Antonio, Ian Dell'

2001-01-01T23:59:59.000Z

267

X-ray reflectivity studies of the metal/solution interphase  

SciTech Connect (OSTI)

We have designed an electrochemical cell that permits x-ray scattering studies in a transmission geometry under in-situ electrochemical control and have performed x-ray specular reflectivity studies of several metal/solution interphases as a function of electrochemical potential. For the copper/solution interphase, we found that the reflectivity changes upon oxidation and reduction, indicating a phase transition between copper and copper oxide at the interphase. We also found that the thickness of the pure copper and the roughness of the interfaces exhibited electrochemical irreversibility that is consistent with the potentials for the oxidation waves in the anodic sweep and the reduction waves in the cathodic sweep of the voltammogram. A standard Fresnel expression for the x-ray specular reflectivity was applied in the data analysis, and a smoothly varying Lorentzian interface profile was used for the individual rough interfaces. Furthermore, an incoherent average was used to include the effect of correlated roughness between a pair of interfaces. Preliminary results are also presented for the silver/solution and platinum/solution interphases. 14 refs., 9 figs., 2 tabs.

You, H.; Nagy, Z.; Melendres, C.A.; Zurawski, D.J.; Chiarello, R.P.; Yonco, R.M.; Kim, H.K.; Maroni, V.A.

1991-09-01T23:59:59.000Z

268

RYLLA. [X-ray transport code  

SciTech Connect (OSTI)

This paper describes a computer code, RYLLA, which models the deposition of x-rays into thin metal slabs, and transports the resulting photoelectrons, finding the distribution of electrons leaving the slab from both the front and back surfaces. The slab must be homogeneous, but can contain a mixture of up to 5 different elements. Due to the short electron mean free path at low electron energies, RYLLA should be used only for studying thin slabs, roughly < 100 mg/cm/sup 2/ for low Z metals, and < 10 mg/cm/sup 2/ for high Z metals. X-ray energies should be in the range of 1 to 150 keV, as they are deposited only via photoionization and Compton scattering processes. Following photoionization, a hole exists in the electron cloud of the absorbing atom. This fills either by Auger or fluoresence, resulting in lower energy holes which are also filled. Fluoresence photons are transported and absorbed in the same manner as the primary photons, except that they are isotropically produced. Once all photons have been transported and absorbed, and all holes have been filled, a space- and energy-dependent electron source spectrum has been obtained. This is used in a discrete ordinate expansion solution of the 1-D transport equation, which gives the output electron spectra at the two slab surfaces. This paper discusses both the physics and coding of RYLLA. Examples of user input are given, as are some comparisons with other codes.

Hyde, R.A.

1983-06-08T23:59:59.000Z

269

Development of procedures for refurbishing x-ray optics at the Advanced Light Source  

E-Print Network [OSTI]

Development of procedures for refurbishing x-ray optics atpractical and robust procedures for refurbishing x-ray

Yashchuk, Valeriy V.

2013-01-01T23:59:59.000Z

270

The variability properties of X-ray steep and X-ray flat quasars  

E-Print Network [OSTI]

We have studied the variability of 6 low redshift, radio quiet `PG' quasars on three timescales (days, weeks, and months) using the ROSAT HRI. The quasars were chosen to lie at the two extreme ends of the ROSAT PSPC spectral index distribution and hence of the H$\\beta$ FWHM distribution. The observation strategy has been carefully designed to provide even sampling on these three basic timescales and to provide a uniform sampling among the quasars We have found clear evidence that the X-ray steep, narrow H_beta, quasars systematically show larger amplitude variations than the X-ray flat broad H_beta quasars on timescales from 2 days to 20 days. On longer timescales we do not find significant differences between steep and flat quasars, although the statistics are poorer. We suggest that the above correlation between variability properties and spectral steepness can be explained in a scenario in which the X-ray steep, narrow line objects are in a higher L/L_Edd state with respect to the X-ray flat, broad line objects. We evaluated the power spectrum of PG1440+356 (the brigthest quasar in our sample) between 2E-7 and 1E-3 Hz, where it goes into the noise. The power spectrum is roughly consistent with a 1/f law between 1E-3 and 2E-6 Hz. Below this frequency it flattens significantly.

Fabrizio Fiore; Ari Laor; Martin Elvis; Fabrizio Nicastro; Emanuele Giallongo

1998-03-20T23:59:59.000Z

271

Standard design for National Ignition Facility x-ray streak and framing cameras  

SciTech Connect (OSTI)

The x-ray streak camera and x-ray framing camera for the National Ignition Facility were redesigned to improve electromagnetic pulse hardening, protect high voltage circuits from pressure transients, and maximize the use of common parts and operational software. Both instruments use the same PC104 based controller, interface, power supply, charge coupled device camera, protective hermetically sealed housing, and mechanical interfaces. Communication is over fiber optics with identical facility hardware for both instruments. Each has three triggers that can be either fiber optic or coax. High voltage protection consists of a vacuum sensor to enable the high voltage and pulsed microchannel plate phosphor voltage. In the streak camera, the high voltage is removed after the sweep. Both rely on the hardened aluminum box and a custom power supply to reduce electromagnetic pulse/electromagnetic interference (EMP/EMI) getting into the electronics. In addition, the streak camera has an EMP/EMI shield enclosing the front of the streak tube.

Kimbrough, J. R.; Bell, P. M.; Bradley, D. K.; Holder, J. P.; Kalantar, D. K.; MacPhee, A. G.; Telford, S. [Lawrence Livermore National Laboratory, Livermore, California 94551-0808 (United States)

2010-10-15T23:59:59.000Z

272

A flexible, highly stable electrochemical scanning probe microscope for nanoscale studies at the solid-liquid interface  

E-Print Network [OSTI]

low-noise measurements in ambient, in situ, and electrochemical environments. II. DESIGNA flexible, highly stable electrochemical scanning probe microscope for nanoscale studies at the solid-liquid interface, specifically in electrolyte environments. Quantification of system noise limits

Gimzewski, James

273

Fabrication process for a gradient index x-ray lens  

DOE Patents [OSTI]

A process for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments m the soft x-ray region.

Bionta, Richard M. (Livermore, CA); Makowiecki, Daniel M. (Livermore, CA); Skulina, Kenneth M. (Livermore, CA)

1995-01-01T23:59:59.000Z

274

Density gradient free electron collisionally excited X-ray laser  

DOE Patents [OSTI]

An operational X-ray laser (30) is provided that amplifies 3p-3s transition X-ray radiation along an approximately linear path. The X-ray laser (30) is driven by a high power optical laser. The driving line focused optical laser beam (32) illuminates a free-standing thin foil (34) that may be associated with a substrate (36) for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the X-ray laser gain medium. The X-ray laser (30) may be driven by more than one optical laser beam (32, 44). The X-ray laser (30) has been successfully demonstrated to function in a series of experimental tests.

Campbell, Edward M. (Pleasanton, CA); Rosen, Mordecai D. (Berkeley, CA)

1989-01-01T23:59:59.000Z

275

Soft x-ray reduction camera for submicron lithography  

DOE Patents [OSTI]

Soft x-ray projection lithography can be performed using x-ray optical components and spherical imaging lenses (mirrors), which form an x-ray reduction camera. The x-ray reduction is capable of projecting a 5x demagnified image of a mask onto a resist coated wafer using 4.5 nm radiation. The diffraction limited resolution of this design is about 135 nm with a depth of field of about 2.8 microns and a field of view of 0.2 cm.sup.2. X-ray reflecting masks (patterned x-ray multilayer mirrors) which are fabricated on thick substrates and can be made relatively distortion free are used, with a laser produced plasma for the source. Higher resolution and/or larger areas are possible by varying the optic figures of the components and source characteristics.

Hawryluk, Andrew M. (2708 Rembrandt Pl., Modesto, CA 95356); Seppala, Lynn G. (7911 Mines Rd., Livermore, CA 94550)

1991-01-01T23:59:59.000Z

276

Soft x-ray reduction camera for submicron lithography  

DOE Patents [OSTI]

Soft x-ray projection lithography can be performed using x-ray optical components and spherical imaging lenses (mirrors), which form an x-ray reduction camera. The x-ray reduction is capable of projecting a 5x demagnified image of a mask onto a resist coated wafer using 4.5 nm radiation. The diffraction limited resolution of this design is about 135 nm with a depth of field of about 2.8 microns and a field of view of 0.2 cm[sup 2]. X-ray reflecting masks (patterned x-ray multilayer mirrors) which are fabricated on thick substrates and can be made relatively distortion free are used, with a laser produced plasma for the source. Higher resolution and/or larger areas are possible by varying the optic figures of the components and source characteristics. 9 figures.

Hawryluk, A.M.; Seppala, L.G.

1991-03-26T23:59:59.000Z

277

Density gradient free electron collisionally excited x-ray laser  

DOE Patents [OSTI]

An operational x-ray laser is provided that amplifies 3p-3s transition x-ray radiation along an approximately linear path. The x-ray laser is driven by a high power optical laser. The driving line focused optical laser beam illuminates a free-standing thin foil that may be associated with a substrate for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the x-ray laser gain medium. The x-ray laser may be driven by more than one optical laser beam. The x-ray laser has been successfully demonstrated to function in a series of experimental tests.

Campbell, E.M.; Rosen, M.D.

1984-11-29T23:59:59.000Z

278

Legacy of the X-Ray Laser Program  

SciTech Connect (OSTI)

The X-Ray Laser Program has evolved from a design effort focusing on developing a Strategic Defense Initiative weapon that protects against Soviet ICBMs to a scientific project that is producing new technologies for industrial and medical research. While the great technical successes and failures of the X-ray laser itself cannot be discussed, this article presents the many significant achievements made as part of the X-ray laser effort that are now being used for other applications at LLNL.

Nilsen, J.

1993-08-06T23:59:59.000Z

279

On X-Ray Waveguiding in Nanochannels: Channeling Formalism  

E-Print Network [OSTI]

The question on X-ray extreme focusing (smallest reachable spot size) brings us to the idea for using the wave features of X-ray propagation in media. As known, wave features are revealed at propagation in ultra-narrow collimators as well as at glancing reflection from smooth flat and/or strongly curved surfaces. All these phenomena can be described within the general formalism of X-ray channeling.

S. B. Dabagov

2006-11-20T23:59:59.000Z

280

X-ray Pinhole Camera Measurements  

SciTech Connect (OSTI)

The rod pinch diode is made up of a cathode plate and a small diameter anode rod that extends through the cathode hole. The anode is charged positively. The rod tip is made of a high-z material which is chosen for its bremsstrahlung efficiency. When the diode is pulsed it produces an intense x-ray source used for pulsed radiography. The baseline or reference diode consists of a 0.75 mm diameter Tungsten (W) tapered anode rod which extends 10 mm through a 9 mm diameter 3 mm thick aluminum (Al) aperture. The majority of the current in the electron beam is created on the edges of the cathode aperture and when properly configured, the electrons will self insulate, travel down the extension of the rod, and pinch onto the tip of the rod. In this presentation, performance of hybrid diodes will be compared with the baseline diode.

Nelson, D. S. [NSTec; Berninger, M. J. [NSTec; Flores, P. A. [NSTec; Good, D. E. [NSTec; Henderson, D. J. [NSTec; Hogge, K. W. [NSTec; Huber, S. R. [NSTec; Lutz, S. S. [NSTec; Mitchell, S. E. [NSTec; Howe, R. A. [NSTec; Mitton, C. V. [NSTec; Molina, I. [NSTec; Bozman, D. R. [SNL; Cordova, S. R. [SNL; Mitchell, D. R. [SNL; Oliver, B. V. [SNL; Ormond, E. C. [SNL

2013-06-20T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

Gray scale x-ray mask  

DOE Patents [OSTI]

The present invention describes a method for fabricating an embossing tool or an x-ray mask tool, providing microstructures that smoothly vary in height from point-to-point in etched substrates, i.e., structure which can vary in all three dimensions. The process uses a lithographic technique to transfer an image pattern in the surface of a silicon wafer by exposing and developing the resist and then etching the silicon substrate. Importantly, the photoresist is variably exposed so that when developed some of the resist layer remains. The remaining undeveloped resist acts as an etchant barrier to the reactive plasma used to etch the silicon substrate and therefore provides the ability etch structures of variable depths.

Morales, Alfredo M. (Livermore, CA); Gonzales, Marcela (Seattle, WA)

2006-03-07T23:59:59.000Z

282

A laser triggered vacuum spark x-ray lithography source  

E-Print Network [OSTI]

ionized state or the physical processes occurring 15 in a high temperature plasma. There are many advantages to the use of the vacuum spark as an x-ray source; the simplicity of the machine is one. The x-ray output is within the range usable for x-ray... spark apparatus ha- been studied here to determine its applicability to x-ray lithography. A capacitor which stored approximately 3 KJ supplied most of the energy for the plasma. A Nd-YAG laser was used to supply electrons and metallic atoms...

Keating, Richard Allen

1987-01-01T23:59:59.000Z

283

Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

axes must be taken into account for accurate interpretation of XMLD data. Magnetism and X Rays The ancient Greeks and also the Chinese knew about strange and rare...

284

Refractive Optics for Hard X-ray Transmission Microscopy  

SciTech Connect (OSTI)

For hard x-ray transmission microscopy at photon energies higher than 15 keV we design refractive condenser and imaging elements to be used with synchrotron light sources as well as with x-ray tube sources. The condenser lenses are optimized for low x-ray attenuation--resulting in apertures greater than 1 mm--and homogeneous intensity distribution on the detector plane, whereas the imaging enables high-resolution (<100 nm) full-field imaging. To obtain high image quality at reasonable exposure times, custom-tailored matched pairs of condenser and imaging lenses are being developed. The imaging lenses (compound refractive lenses, CRLs) are made of SU-8 negative resist by deep x-ray lithography. SU-8 shows high radiation stability. The fabrication technique enables high-quality lens structures regarding surface roughness and arrangement precision with arbitrary 2D geometry. To provide point foci, crossed pairs of lenses are used. Condenser lenses have been made utilizing deep x-ray lithographic patterning of thick SU-8 layers, too, whereas in this case, the aperture is limited due to process restrictions. Thus, in terms of large apertures, condenser lenses made of structured and rolled polyimide film are more attractive. Both condenser types, x-ray mosaic lenses and rolled x-ray prism lenses (RXPLs), are considered to be implemented into a microscope setup. The x-ray optical elements mentioned above are characterized with synchrotron radiation and x-ray laboratory sources, respectively.

Simon, M.; Last, A.; Mohr, J.; Nazmov, V.; Reznikova, E. [Institute for Microstructure Technology, Karlsruhe Institute of Technology Kaiserstrasse 12, 76131 Karlsruhe (Germany); Ahrens, G.; Voigt, A. [Microresist Technology, Koepenikerstrasse 325, 12555 Berlin (Germany)

2011-09-09T23:59:59.000Z

285

X-ray compass for determining device orientation  

DOE Patents [OSTI]

An apparatus and method for determining the orientation of a device with respect to an x-ray source. In one embodiment, the present invention is coupled to a medical device in order to determine the rotational orientation of the medical device with respect to the x-ray source. In such an embodiment, the present invention is comprised of a scintillator portion which is adapted to emit photons upon the absorption of x-rays emitted from the x-ray source. An x-ray blocking portion is coupled to the scintillator portion. The x-ray blocking portion is disposed so as to vary the quantity of x-rays which penetrate the scintillator portion based upon the particular rotational orientation of the medical device with respect to the x-ray source. A photon transport mechanism is also coupled to the scintillator portion. The photon transport mechanism is adapted to pass the photons emitted from the scintillator portion to an electronics portion. By analyzing the quantity of the photons, the electronics portion determines the rotational orientation of the medical device with respect to the x-ray source.

Da Silva, Luiz B. (Danville, CA); Matthews, Dennis L. (Moss Beach, CA); Fitch, Joseph P. (Livermore, CA); Everett, Matthew J. (Pleasanton, CA); Colston, Billy W. (Livermore, CA); Stone, Gary F. (Livermore, CA)

1999-01-01T23:59:59.000Z

286

X-ray compass for determining device orientation  

DOE Patents [OSTI]

An apparatus and method for determining the orientation of a device with respect to an x-ray source are disclosed. In one embodiment, the present invention is coupled to a medical device in order to determine the rotational orientation of the medical device with respect to the x-ray source. In such an embodiment, the present invention is comprised of a scintillator portion which is adapted to emit photons upon the absorption of x-rays emitted from the x-ray source. An x-ray blocking portion is coupled to the scintillator portion. The x-ray blocking portion is disposed so as to vary the quantity of x-rays which penetrate the scintillator portion based upon the particular rotational orientation of the medical device with respect to the x-ray source. A photon transport mechanism is also coupled to the scintillator portion. The photon transport mechanism is adapted to pass the photons emitted from the scintillator portion to an electronics portion. By analyzing the quantity of the photons, the electronics portion determines the rotational orientation of the medical device with respect to the x-ray source. 25 figs.

Da Silva, L.B.; Matthews, D.L.; Fitch, J.P.; Everett, M.J.; Colston, B.W.; Stone, G.F.

1999-06-15T23:59:59.000Z

287

Normal incidence x-ray mirror for chemical microanalysis  

DOE Patents [OSTI]

An x-ray mirror for both electron column instruments and micro x-ray fluorescence instruments for making chemical, microanalysis comprises a non-planar mirror having, for example, a spherical reflecting surface for x-rays comprised of a predetermined number of alternating layers of high atomic number material and low atomic number material contiguously formed on a substrate and whose layers have a thickness which is a multiple of the wavelength being reflected. For electron column instruments, the wavelengths of interest lie above 1.5nm, while for x-ray fluorescence instruments, the range of interest is below 0.2nm. 4 figs.

Carr, M.J.; Romig, A.D. Jr.

1987-08-05T23:59:59.000Z

288

Fuel Injection and Spray Research Using X-Ray Diagnostics  

Broader source: Energy.gov (indexed) [DOE]

collaborations - Explore new capabilities, applications Upgraded x-ray optics in FY2011 - Allows us to resolve finer structures in spray * Old beamline: 150 m x...

289

Using Light to Control How X Rays Interact with Matter  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

pulse, a heretofore difficult challenge. This capability should help to further develop ultrafast x-ray spectroscopy. ALS femtosecond spectroscopy beamline layout. Femtosecond...

290

Geometric classification of open-cell metal foams using X-ray micro-computed tomography  

SciTech Connect (OSTI)

The geometry of foams has long been an area of interest, and a number of idealized geometric descriptions have been proposed. In order to acquire detailed, quantitative, geometric data for aluminum open-cell metal foams, X-ray {mu}CT is employed. The X-ray {mu}CT images are analyzed using specialized software, FoamView Registered-Sign , from which geometric information including strut length and pore shapes are extracted. The X-ray {mu}CT analysis allows comparison of the ideal geometric models to the actual geometric characteristics of the metal foam samples. The results reveal a high variability in ligament length, as well as features supporting the ideal geometry known as the Weaire-Phelan unit cell. The geometric findings provide information useful for improving current models of open-cell metal foam. Applications can range from predicting heat transfer or load failure to predicting liquid retention. Highlights: Black-Right-Pointing-Pointer Aluminum open-cell metal foams are geometrically classified Black-Right-Pointing-Pointer X-ray micro-computed tomography and specialized software are used to gather geometric data Black-Right-Pointing-Pointer The foams are shown to have a high variability in strut length Black-Right-Pointing-Pointer The Weaire-Phelan unit cell is shown to be a better representative of these foams.

Bock, Jessica, E-mail: bock6@illinois.edu; Jacobi, Anthony M., E-mail: a-jacobi@illinois.edu

2013-01-15T23:59:59.000Z

291

X-ray laser system, x-ray laser and method  

DOE Patents [OSTI]

Disclosed is an x-ray laser system comprising a laser containing generating means for emitting short wave length radiation, and means external to said laser for energizing said generating means, wherein when the laser is in an operative mode emitting radiation, the radiation has a transverse coherence length to width ratio of from about 0.05 to 1. Also disclosed is a method of adjusting the parameters of the laser to achieve the desired coherence length to laser width ratio.

London, Richard A. (Oakland, CA); Rosen, Mordecai D. (Berkeley, CA); Strauss, Moshe (Omer, IL)

1992-01-01T23:59:59.000Z

292

Constraints on jet X-ray emission in low/hard state X-ray binaries  

E-Print Network [OSTI]

We show that the combination of the similarities between the X-ray properties of low luminosity accreting black holes and accreting neutron stars, combined with the differences in their radio properties argues that the X-rays from these systems are unlikely to be formed in the relativistic jets. Specifically, the spectra of extreme island state neutron stars and low/hard state black holes are known to be indistinguishable, while the power spectra from these systems are known to show only minor differences beyond what would be expected from scaling the characteristic variability frequencies by the mass of the compact object. The spectral and temporal similarities thus imply a common emission mechanism that has only minor deviations from having all key parameters scaling linearly with the mass of the compact object, while we show that this is inconsistent with the observations that the radio powers of neutron stars are typically about 30 times lower than those of black holes at the same X-ray luminosity. We also show that an abrupt luminosity change would be expected when a system makes a spectral state transition from a radiatively inefficient jet dominated accretion flow to a thin disk dominated flow, but that such a change is not seen.

Thomas J. Maccarone

2005-03-31T23:59:59.000Z

293

Isotropic star in low-mass X-ray binaries and X-ray pulsars  

E-Print Network [OSTI]

We present a model for compact stars in the low mass X-ray binaries(LMXBs) and X-ray pulsars using a metric given by John J. Matese and Patrick G. Whitman \\citep{Matese and Whitman1980}. Here the field equations are reduced to a system of two algebraic equations considering the isotropic pressure. Compact star candidates 4U 1820-30(radius=10km) in LMXBs, and Her X-1(radius=7.7km), SAX J 1808.4-3658(SS1)(radius=7.07km) and SAX J 1808.4-3658(SS2)(radius=6.35km) in X-ray pulsars satisfy all the energy conditions, TOV-equation and stability condition. From our model, we have derived mass($M$), central density($\\rho_{0}$), suface density($\\rho_{b}$), central pressure($p_{0}$), surface pressure($p_{b}$) and surface red-shift($Z_{s}$) of the above mentioned stars, which are very much consistant with the observed/reported datas\\citep{N. K. Glendenning1997,Gondek2000}. We have also observe the adiabatic index($\\gamma$>4/3) of the above steller objects.

Mehedi Kalam; Sk. Monowar Hossein; Sajahan Molla

2014-10-01T23:59:59.000Z

294

Boron Doped diamond films as electron donors in photovoltaics: An X-ray absorption and hard X-ray photoemission study  

SciTech Connect (OSTI)

Highly boron-doped diamond films are investigated for their potential as transparent electron donors in solar cells. Specifically, the valence band offset between a diamond film (as electron donor) and Cu(In,Ga)Se{sub 2} (CIGS) as light absorber is determined by a combination of soft X-ray absorption spectroscopy and hard X-ray photoelectron spectroscopy, which is more depth-penetrating than standard soft X-ray photoelectron spectroscopy. In addition, a theoretical analysis of the valence band is performed, based on GW quasiparticle band calculations. The valence band offset is found to be small: VBO?=?VBM{sub CIGS} – VBM{sub diamond}?=?0.3?eV?±?0.1?eV at the CIGS/Diamond interface and 0.0?eV?±?0.1?eV from CIGS to bulk diamond. These results provide a promising starting point for optimizing the band offset by choosing absorber materials with a slightly lower valence band maximum.

Kapilashrami, M.; Zegkinoglou, I. [Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Department of Physics, University of Wisconsin Madison, Madison, Wisconsin 53706 (United States); Conti, G.; Nemšák, S.; Conlon, C. S.; Fadley, C. S. [Department of Physics, University of California, Davis, California 95616 (United States); Materials Sciences Division, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Törndahl, T.; Fjällström, V. [Ångström Solar Center, Uppsala University, Box 534, SE-751 21 Uppsala (Sweden); Lischner, J. [Department of Physics, University of California, Berkeley, California 94720 (United States); Louie, Steven G. [Materials Sciences Division, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Department of Physics, University of California, Berkeley, California 94720 (United States); Hamers, R. J.; Zhang, L. [Department of Chemistry, University of Wisconsin Madison, Madison, Wisconsin 53706 (United States); Guo, J.-H. [Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States); Himpsel, F. J., E-mail: fhimpsel@wisc.edu [Department of Physics, University of Wisconsin Madison, Madison, Wisconsin 53706 (United States)

2014-10-14T23:59:59.000Z

295

Charge transfer effects of ions at the liquid water/vapor interface  

SciTech Connect (OSTI)

Charge transfer (CT), the movement of small amounts of electron density between non-bonded pairs, has been suggested as a driving force for a variety of physical processes. Herein, we examine the effect of CT on ion adsorption to the water liquid-vapor interface. Using a CT force field for molecular dynamics, we construct a potential of mean force (PMF) for Na{sup +}, K{sup +}, Cl{sup ?}, and I{sup ?}. The PMFs were produced with respect to an average interface and an instantaneous interface. An analysis of the PMF relative to the instantaneous surface reveals that the area in which the anions experience a free energy minimum is quite narrow, and the cations feel a steeply repulsive free energy near the interface. CT is seen to have only minor effects on the overall free energy profiles. However, the long-ranged effects of ions are highlighted by the CT model. Due to CT, the water molecules at the surface become charged, even when the ion is over 15 Å away from the surface.

Soniat, Marielle; Rick, Steven W., E-mail: srick@uno.edu [Department of Chemistry, University of New Orleans, New Orleans, Louisiana 70148 (United States)

2014-05-14T23:59:59.000Z

296

X-ray spectra transmitted through Compton-thick absorbers  

E-Print Network [OSTI]

X-ray spectra transmitted through matter which is optically thick to Compton scattering are computed by means of Monte Carlo simulations. Applications to the BeppoSAX data of the Seyfert 2 galaxy in Circinus, and to the spectral modeling of the Cosmic X-ray Background, are discussed.

Giorgio Matt; Fulvio Pompilio; Fabio La Franca

1999-04-24T23:59:59.000Z

297

Measurement and characterization of x-ray spot size  

SciTech Connect (OSTI)

In planning an x-ray imaging experiment one must have an accurate model of the imaging system to obtain optimum results. The blurring caused by the finite size of the x-ray source is often the least understood element in the system. We have developed experimental and analytical methods permitting accurate measurement and modeling of the x-ray source. The model offers a simple and accurate way to optimize the radiographic geometry for any given experimental requirement (i.e., resolution and dose at detector). Any text on radiography will mention the effects of the finite size of the x-ray source on image quality and how one can minimize this influence by the choice of a small radiographic magnification. The film blur (independent of the source blur) is often treated as a single number and combined with an effective blur dimension for the x-ray source to give a total blur on the film. In this paper, we will develop a treatment of x-ray sources based on the modulation transfer function (MTF). This approach allows us to infer the spatial distribution function of the electron beam that produces the bremsstrahlung x-rays and to predict the performance of an x-ray imaging system if we know the MTF of the detector. This treatment is much more accurate than a single number characterization. 4 refs., 7 figs.

Mueller, K.H.

1989-01-01T23:59:59.000Z

298

High resolution energy-sensitive digital X-ray  

DOE Patents [OSTI]

An apparatus and method for detecting an x-ray and for determining the depth of penetration of an x-ray into a semiconductor strip detector. In one embodiment, a semiconductor strip detector formed of semiconductor material is disposed in an edge-on orientation towards an x-ray source such that x-rays From the x-ray source are incident upon and substantially perpendicular to the front edge of the semiconductor strip detector. The semiconductor strip detector is formed of a plurality of segments. The segments are coupled together in a collinear arrangement such that the semiconductor strip detector has a length great enough such that substantially all of the x-rays incident on the front edge of the semiconductor strip detector interact with the semiconductor material which forms the semiconductor strip detector. A plurality of electrodes are connected to the semiconductor strip detect or such that each one of the of semiconductor strip detector segments has at least one of the of electrodes coupled thereto. A signal processor is also coupled to each one of the electrodes. The present detector detects an interaction within the semiconductor strip detector, between an x-ray and the semiconductor material, and also indicates the depth of penetration of the x-ray into the semiconductor strip detector at the time of the interaction.

Nygren, David R. (Berkeley, CA)

1995-01-01T23:59:59.000Z

299

Human genome sequencing with direct x-ray holographic imaging  

SciTech Connect (OSTI)

Direct holographic imaging of biological materials is widely applicable to the study of the structure, properties and action of genetic material. This particular application involves the sequencing of the human genome where prospective genomic imaging technology is composed of three subtechnologies, name an x-ray holographic camera, suitable chemistry and enzymology for the preparation of tagged DNA samples, and the illuminator in the form of an x-ray laser. We report appropriate x-ray camera, embodied by the instrument developed by MCR, is available and that suitable chemical and enzymatic procedures exist for the preparation of the necessary tagged DNA strands. Concerning the future development of the x-ray illuminator. We find that a practical small scale x-ray light source is indeed feasible. This outcome requires the use of unconventional physical processes in order to achieve the necessary power-compression in the amplifying medium. The understanding of these new physical mechanisms is developing rapidly. Importantly, although the x-ray source does not currently exist, the understanding of these new physical mechanisms is developing rapidly and the research has established the basic scaling laws that will determine the properties of the x-ray illuminator. When this x-ray source becomes available, an extremely rapid and cost effective instrument for 3-D imaging of biological materials can be applied to a wide range of biological structural assays, including the base-pair sequencing of the human genome and many questions regarding its higher levels of organization.

Rhodes, C.K.

1993-06-08T23:59:59.000Z

300

Electromagnetic Application: X-RAY Alawi H. Ba-Surrah  

E-Print Network [OSTI]

, Pulyui published high-quality x-ray images in journals in Paris and London. · Nikola Tesla In April 1887, Nikola Tesla began to investigate X-rays using high voltages and tubes of his own design, as well. The principle behind Tesla's device is called the Bremsstrahlung process, in which a high-energy secondary X

Masoudi, Husain M.

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

Thirteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Thirteenth National School on Neutron and X-ray Scattering June 11 ­ June 25, 2011 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

302

Neutron and X-ray Scattering Study of Magnetic Manganites  

E-Print Network [OSTI]

Neutron and X-ray Scattering Study of Magnetic Manganites Graeme Eoin Johnstone A Thesis submitted are performed using a variety of neutron scattering and x-ray scattering techniques. The electronic ground for analysing the results of the polarised neutron scattering experiment. There are a large number of people who

Boothroyd, Andrew

303

Tenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Tenth National School on Neutron and X-ray Scattering September 24 - October 11, 2008 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

304

Sixteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Sixteenth National School on Neutron and X-ray Scattering June 14-28, 2014 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major's Neutron Scattering Science Division. Scientific Directors: Suzanne G.E. te Velthuis, Esen Ercan Alp

Pennycook, Steve

305

Fourteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Fourteenth National School on Neutron and X-ray Scattering August 12 - 25, 2012 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

Pennycook, Steve

306

National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

15th National School on Neutron and X-ray Scattering August 10 - 24, 2013 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

307

National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

National School on Neutron and X-ray Scattering May 30 ­ June 13, 2009 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

308

Twelfth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Twelfth National School on Neutron and X-ray Scattering June 12 ­ June 26, 2010 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

309

Ultrafast x-rays: radiographing magnetism Project overview  

E-Print Network [OSTI]

, head of the ultrafast magnetism group. Stanford PULSE is a worldwide renowned centre for ultrafast1 Ultrafast x-rays: radiographing magnetism Project overview The main purpose of the proposed, it is now possible to achieve x-ray pulses that are a few femtoseconds long and that are focused within

Haviland, David

310

Laser Copper Plasma X-ray Source Debris Characterization  

E-Print Network [OSTI]

Laser Copper Plasma X-ray Source Debris Characterization A Thesis Presented by David Hurley 3, 2007 Vice President for Research and Dean of Graduate studies #12;Abstract Laser copper plasma for x-ray lithography. Copper debris in the form of vapor, ions, dust, and high-speed particles

Huston, Dryver R.

311

Millisecond oscillations during thermonuclear X-ray bursts  

E-Print Network [OSTI]

I analyze 68 oscillation trains detected in a search of 159 thermonuclear bursts from eight neutron star X-ray binaries observed with the Rossi X-ray Timing Explorer. I use all data that were public as of September 2001. ...

Muno, Michael Patrick, 1975-

2002-01-01T23:59:59.000Z

312

Chandra X-ray Analysis of Galaxy Cluster A168  

E-Print Network [OSTI]

We present Chandra X-ray observations of galaxy cluster A168 (z=0.045). Two X-ray peaks with a projected distance of 676 kpc are found to be located close to two dominant galaxies, respectively. Both peaks are significantly offset from the peak of the number density distribution of galaxies. This suggests that A168 consists of two subclusters, a northern subcluster (A168N) and a southern subcluster (A168S). Further X-ray imaging analysis reveals that (1) the X-ray isophotes surrounding the two X-ray peaks are heavily distorted, (2) an elongated and ontinuous filament connects the two X-ray peaks. These suggest that strong interactions have occurred between the two subclusters. Spectral analysis shows that A168 has a mean temperature of 2.53 +/- 0.09 keV and a mean metallicity of 0.31 +/- 0.04 Z_{solar}. The metallicity is roughly a constant across the cluster but the temperature shows some systematic variations. Most X-ray, optical and radio properties of A168 are consistent with it being an off-axis merger several Gyrs after a core passage, although detailed numerical simulations are required to see whether the observed properties, in particular the significant offset between the optical and X-ray centers, can be reproduced in such a scenario.

Yanbin Yang; Zhiying Huo; Xu Zhou; Suijian Xue; Shude Mao; Jun Ma; Jiansheng Chen

2004-06-29T23:59:59.000Z

313

Trapping energy of a spherical particle on a curved liquid interface  

E-Print Network [OSTI]

We derive the trapping energy of a colloidal particle at a liquid interface with contact angle h and principal curvatures c1 and c2. The boundary conditions at the particle surface are significantly simplified by introducing the shift e of its vertical position. We discuss the undulating contact line and the curvatureinduced lateral forces for a single particle and a pair of nearby particles. The single-particle trapping energy is found to decrease with the square of both the total curvature c1 + c2 and the anisotropy c1 ? c2. In the case of non-uniform curvatures, the resulting lateral force pushes particles toward more strongly curved regions.

Joseph Léandri; Alois Würger

2014-01-29T23:59:59.000Z

314

Determination of the pressure at the gas-liquid interface using acoustic speed measurements  

E-Print Network [OSTI]

. The density can be expressed with the use of the real gas law. This yields BP = ? (g/gc) *dz*P*M/(144*Z*R*T) BP = ? (g/gc) *dz*P*SG*MAIR/(144*Z*R*T) (26) 21 where: SG MAIR specific gravity of gas. (air= 1. 0), Molecular weight of air, 28. 966...DETERMINATION OF THE PRESSURE AT THE GAS-LIQUID INTERFACE USING ACOUSTIC SPEED MEASUREMENTS A Thesis by DAG GUSTAV HEGGELUND Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirements for the degree...

Heggelund, Dag Gustav

1988-01-01T23:59:59.000Z

315

Improving liquid chromatography-mass spectrometry sensitivity using a subambient pressure ionization with nanoelectrospray (SPIN) interface  

SciTech Connect (OSTI)

In this work the Subambient Pressure Ionization with Nanoelectrospray (SPIN) ion source and interface which operates at ~15-30 Torr is demonstrated to be compatible with gradient reversed-phase liquid chromatography-MS applications, exemplified here with the analysis of complex samples (a protein tryptic digest and a whole cell lysate). A low liquid chromatographic flow rate (100-400 nL/min) allowed stable electrospray to be established while avoiding electrical breakdown. Efforts to increase the operating pressure of the SPIN source relative to previously reported designs prevented solvent freezing and enhanced charged cluster/droplet desolvation. A 5-12-fold improvement in sensitivity relative to a conventional atmospheric pressure nanoelectrospray ionization (ESI) source was obtained for detected peptides.

Tang, Keqi; Page, Jason S.; Marginean, Ioan; Kelly, Ryan T.; Smith, Richard D.

2011-04-22T23:59:59.000Z

316

X-Ray Observations of Gamma-Ray Burst Afterglows  

E-Print Network [OSTI]

The discovery by the BeppoSAX satellite of X-ray afterglow emission from the gamma-ray burst which occurred on 28 February 1997 produced a revolution in our knowledge of the gamma-ray burst phenomenon. Along with the discovery of X-ray afterglows, the optical afterglows of gamma-ray bursts were discovered and the distance issue was settled, at least for long $\\gamma$-ray bursts. The 30 year mystery of the gamma-ray burst phenomenon is now on the way to solution. Here I rewiew the observational status of the X-ray afterglow emission, its mean properties (detection rate, continuum spectra, line features, and light curves), and the X-ray constraints on theoretical models of gamma-ray bursters and their progenitors. I also discuss the early onset afterglow emission, the remaining questions, and the role of future X-ray afterglow observations.

Filippo Frontera

2004-06-25T23:59:59.000Z

317

X-ray intensity interferometer for undulator radiation  

SciTech Connect (OSTI)

Intensity interferometry is well established with visible light but has never been demonstrated with x-radiation. We propose to measure the transverse coherence of an x-ray beam, for the first time, using the method of Hanbury Brown and Twiss. The x-ray interferometer consists of an array of slits, a grazing incidence reflective beamsplitter, a pair of fast multichannel plate detectors and a broadband, low-noise correlator circuit. The NSLS X1 or X13 soft x-ray undulator will supply the partially coherent x-rays. We are developing this technique to characterize the coherence properties of x-ray beams from high brilliance insertion devices at third-generation synchrotron light facilities such as the Advanced Photon Source and the Advanced Light Source. 17 refs.

Gluskin, E.; McNulty, I.; Viccaro, P.J. [Argonne National Lab., IL (United States); Howells, M.R. [Lawrence Berkeley Lab., CA (United States)

1991-12-31T23:59:59.000Z

318

X-ray intensity interferometer for undulator radiation  

SciTech Connect (OSTI)

Intensity interferometry is well established with visible light but has never been demonstrated with x-radiation. We propose to measure the transverse coherence of an x-ray beam, for the first time, using the method of Hanbury Brown and Twiss. The x-ray interferometer consists of an array of slits, a grazing incidence reflective beamsplitter, a pair of fast multichannel plate detectors and a broadband, low-noise correlator circuit. The NSLS X1 or X13 soft x-ray undulator will supply the partially coherent x-rays. We are developing this technique to characterize the coherence properties of x-ray beams from high brilliance insertion devices at third-generation synchrotron light facilities such as the Advanced Photon Source and the Advanced Light Source. 17 refs.

Gluskin, E.; McNulty, I.; Viccaro, P.J. (Argonne National Lab., IL (United States)); Howells, M.R. (Lawrence Berkeley Lab., CA (United States))

1991-01-01T23:59:59.000Z

319

Broadband high resolution X-ray spectral analyzer  

DOE Patents [OSTI]

A broad bandwidth high resolution x-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces x-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available x-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for x-ray microanalysis or in research applications such as laboratory and astrophysical x-ray and particle spectroscopy.

Silver, Eric H. (Berkeley, CA); Legros, Mark (Berkeley, CA); Madden, Norm W. (Livermore, CA); Goulding, Fred (Lafayette, CA); Landis, Don (Pinole, CA)

1998-01-01T23:59:59.000Z

320

A refined model for characterizing x-ray multilayers  

SciTech Connect (OSTI)

The ability to quickly and accurately characterize arbitrary multilayers is very valuable for not only can we use the characterizations to predict the reflectivity of a multilayer for any soft x-ray wavelength, we also can generalize the results to apply to other multilayers of the same type. In addition, we can use the characterizations as a means of evaluating various sputtering environments and refining sputtering techniques to obtain better multilayers. In this report we have obtained improved characterizations for sample molybdenum-silicon and vanadium-silicon multilayers. However, we only examined five crystals overall, so the conclusions that we could draw about the structure of general multilayers is limited. Research involving many multilayers manufactured under the same sputtering conditions is clearly in order. In order to best understand multilayer structures it may be necessary to further refine our model, e.g., adopting a Gaussian form for the interface regions. With such improvements we can expect even better agreement with experimental values and continued concurrence with other characterization techniques. 18 refs., 30 figs., 7 tabs.

Oren, A.L.; Henke, B.L.

1987-12-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

X-ray Emission from Massive StarsX-ray Emission from Massive Stars David CohenDavid Cohen  

E-Print Network [OSTI]

X-ray Emission from Massive StarsX-ray Emission from Massive Stars David CohenDavid Cohen/s)Velocity (km/s) #12;absorption emission emission occulted emission emission UV telescope side side front back #12;absorption emission emission occulted emission emission UV telescope side side front back #12;The

Cohen, David

322

Automated high pressure cell for pressure jump x-ray diffraction  

SciTech Connect (OSTI)

A high pressure cell for small and wide-angle x-ray diffraction measurements of soft condensed matter samples has been developed, incorporating a fully automated pressure generating network. The system allows both static and pressure jump measurements in the range of 0.1-500 MPa. Pressure jumps can be performed as quickly as 5 ms, both with increasing and decreasing pressures. Pressure is generated by a motorized high pressure pump, and the system is controlled remotely via a graphical user interface to allow operation by a broad user base, many of whom may have little previous experience of high pressure technology. Samples are loaded through a dedicated port allowing the x-ray windows to remain in place throughout an experiment; this facilitates accurate subtraction of background scattering. The system has been designed specifically for use at beamline I22 at the Diamond Light Source, United Kingdom, and has been fully integrated with the I22 beamline control systems.

Brooks, Nicholas J.; Gauthe, Beatrice L. L. E.; Templer, Richard H.; Ces, Oscar; Seddon, John M. [Department of Chemistry, Imperial College London, South Kensington Campus, London SW7 2AZ (United Kingdom); Terrill, Nick J. [Diamond Light Source, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0DE (United Kingdom); Rogers, Sarah E. [ISIS, Rutherford Appleton Laboratory, Harwell Science and Innovation Campus, Didcot, Oxfordshire OX11 0QX (United Kingdom)

2010-06-15T23:59:59.000Z

323

SURFACE SEGREGATION STUDIES OF SOFC CATHODES: COMBINING SOFT X-RAYS AND ELECTROCHEMICAL IMPEDENCE SPECTROSCOPY  

SciTech Connect (OSTI)

A system to grow heteroepitaxial thin-films of solid oxide fuel cell (SOFC) cathodes on single crystal substrates was developed. The cathode composition investigated was 20% strontium-doped lanthanum manganite (LSM) grown by pulsed laser deposition (PLD) on single crystal (111) yttria-stabilized zirconia (YSZ) substrates. By combining electrochemical impedance spectroscopy (EIS) with x-ray photoemission spectroscopy (XPS) and x-ray absorption spectroscopy XAS measurements, we conclude that electrically driven cation migration away from the two-phase gas-cathode interface results in improved electrochemical performance. Our results provide support to the premise that the removal of surface passivating phases containing Sr2+ and Mn2+, which readily form at elevated temperatures even in O2 atmospheric pressures, is responsible for the improved cathodic performance upon application of a bias.

Miara, Lincoln J.; Piper, L.F.J.; Davis, Jacob N.; Saraf, Laxmikant V.; Kaspar, Tiffany C.; Basu, Soumendra; Smith, K. E.; Pal, Uday B.; Gopalan, Srikanth

2010-12-01T23:59:59.000Z

324

The role of project science in the Chandra X-ray Observatory  

E-Print Network [OSTI]

The Chandra X-ray Observatory, one of NASA's Great Observatories, has an outstanding record of scientific and technical success. This success results from the efforts of a team comprising NASA, its contractors, the Smithsonian Astrophysical Observatory, the instrument groups, and other elements of the scientific community -- including the thousands of scientists who utilize this powerful facility for astrophysical research. We discuss the role of NASA Project Science in the formulation, development, calibration, and operation of the Chandra X-ray Observatory. In addition to serving as an interface between the scientific community and the Project, Project Science performed what we term "science systems engineering". This activity encompasses translation of science requirements into technical requirements and assessment of the scientific impact of programmatic and technical trades. We briefly describe several examples of science systems engineering conducted by Chandra Project Science.

Stephen L. O'Dell; Martin C. Weisskopf

2006-06-16T23:59:59.000Z

325

Method and apparatus for digitally based high speed x-ray spectrometer  

DOE Patents [OSTI]

A high speed, digitally based, signal processing system which accepts input data from a detector-preamplifier and produces a spectral analysis of the x-rays illuminating the detector. The system achieves high throughputs at low cost by dividing the required digital processing steps between a "hardwired" processor implemented in combinatorial digital logic, which detects the presence of the x-ray signals in the digitized data stream and extracts filtered estimates of their amplitudes, and a programmable digital signal processing computer, which refines the filtered amplitude estimates and bins them to produce the desired spectral analysis. One set of algorithms allow this hybrid system to match the resolution of analog systems while operating at much higher data rates. A second set of algorithms implemented in the processor allow the system to be self calibrating as well. The same processor also handles the interface to an external control computer.

Warburton, William K. (1300 Mills St., Menlo Park, CA 94025); Hubbard, Bradley (Santa Cruz, CA)

1997-01-01T23:59:59.000Z

326

AugEX: AUGER ELECTRON AND X-RAY SPECTROMETER ON CHANDRAYAAN-2 ROVER  

E-Print Network [OSTI]

for determining elemental composition which have a space heritage X-Ray Fluorescence (XRF) Particle-induced X-ray fluorescence (XRF) Expected Advantage: cover low Z elements with higher sensitivity than XRF or PIXE. ACHARYA-ray absorption or charged particle bombardment X-ray emission induced by X-ray absorption: XRF X-ray emission

Bapat, Bhas

327

SOFT X-RAY EMISSIONS FROM PLANETS, MOONS, AND COMETS A. Bhardwaj(1)  

E-Print Network [OSTI]

SOFT X-RAY EMISSIONS FROM PLANETS, MOONS, AND COMETS A. Bhardwaj(1) , G. R. Gladstone(2) , R. F to radiate in the soft x-ray energy ( the generation of soft x-rays from these objects, whereas in the hard x-ray energy range (>10 keV) x-rays mainly

Johnson, Robert E.

328

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate  

E-Print Network [OSTI]

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate an effect of a partially reversible x-ray-induced increase of diffuse x-ray scattering in both congruent been attributed to x-ray-induced decay of the ferroelectric phase at room temperature. The x-ray

Byer, Robert L.

329

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi Center 091 Chemistry Bldg. / College Park, MD 20742  

E-Print Network [OSTI]

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi. or advisor confirmation e-mail X-ray Diffractometer that will be used: User Level and Status Smart Apex2X'Pert Pro MRD (Reflectivity & low angles) Xeuss (Small/Wide Angle X-ray Scattering) Submitting user ­ only

Thirumalai, Devarajan

330

Lunar X-ray fluorescence observations by the Chandrayaan-1 X-ray Spectrometer (C1XS): Results from the nearside southern highlands  

E-Print Network [OSTI]

Lunar X-ray fluorescence observations by the Chandrayaan-1 X-ray Spectrometer (C1XS): Results from Spectroscopy a b s t r a c t The Chandrayaan-1 X-ray Spectrometer (C1XS) flown on-board the first Indian lunar mission Chan- drayaan-1, measured X-ray fluorescence spectra during several episodes of solar flares

Wieczorek, Mark

331

Soft-x-ray spectroscopy study of nanoscale materials  

SciTech Connect (OSTI)

The ability to control the particle size and morphology of nanoparticles is of crucial importance nowadays both from a fundamental and industrial point of view considering the tremendous amount of high-tech applications. Controlling the crystallographic structure and the arrangement of atoms along the surface of nanostructured material will determine most of its physical properties. In general, electronic structure ultimately determines the properties of matter. Soft X-ray spectroscopy has some basic features that are important to consider. X-ray is originating from an electronic transition between a localized core state and a valence state. As a core state is involved, elemental selectivity is obtained because the core levels of different elements are well separated in energy, meaning that the involvement of the inner level makes this probe localized to one specific atomic site around which the electronic structure is reflected as a partial density-of-states contribution. The participation of valence electrons gives the method chemical state sensitivity and further, the dipole nature of the transitions gives particular symmetry information. The new generation synchrotron radiation sources producing intensive tunable monochromatized soft X-ray beams have opened up new possibilities for soft X-ray spectroscopy. The introduction of selectively excited soft X-ray emission has opened a new field of study by disclosing many new possibilities of soft X-ray resonant inelastic scattering. In this paper, some recent findings regarding soft X-ray absorption and emission studies of various nanostructured systems are presented.

Guo, J.-H.

2005-07-30T23:59:59.000Z

332

Apparatus for generating x-ray holograms  

DOE Patents [OSTI]

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced.

Rhodes, Charles K. (Chicago, IL); Boyer, Keith (Los Alamos, NM); Solem, Johndale C. (Los Alamos, NM); Haddad, Waleed S. (Chicago, IL)

1990-01-01T23:59:59.000Z

333

Apparatus for generating x-ray holograms  

DOE Patents [OSTI]

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced. 7 figs.

Rhodes, C.K.; Boyer, K.; Solem, J.C.; Haddad, W.S.

1990-09-11T23:59:59.000Z

334

National Ignition Facility core x-ray streak camera  

SciTech Connect (OSTI)

The National Ignition Facility (NIF) core x-ray streak camera will be used for laser performance verification experiments as well as a wide range of physics experiments in the areas of high-energy-density science, inertial confinement fusion, and basic science. The x-ray streak camera system is being designed to record time-dependent x-ray emission from NIF targets using an interchangeable family of snouts for measurements such as one-dimensional (1D) spatial imaging or spectroscopy. the NIF core x-ray streak camera will consist of an x-ray-sensitive photocathode that detects x rays with 1D spatial resolution coupled to an electron streak tube to detect a continuous time history of the x rays incident on the photocathode over selected time periods. A charge-coupled-device (CCD) readout will record the signal from the streak tube. The streak tube, CCD, and associated electronics will reside in an electromagnetic interference, and electromagnetic pulse protected, hermetically sealed, temperature-controlled box whose internal pressure is approximately 1 atm. The streak tube itself will penetrate through the wall of the box into the target chamber vacuum. We are working with a goal of a spatial resolution of 15 lp/mm with 50% contrast transfer function at the photocathode and adjustment sweep intervals of 1--50 ns. The camera spectral sensitivity extends from soft x rays to 20 keV x rays, with varying quantum efficiency based on photocathode selection. The system will have remote control, monitoring, and Ethernet communications through an embedded controller. The core streak camera will be compatible with the instrument manipulators at the OMEGA (University of Rochester) and NIF facilities.

Kimbrough, J. R.; Bell, P. M.; Christianson, G. B.; Lee, F. D.; Kalantar, D. H.; Perry, T. S.; Sewall, N. R.; Wootton, A. J.

2001-01-01T23:59:59.000Z

335

Development of Nanofluidic Cells for Ultrafast X-ray Studies of Water  

SciTech Connect (OSTI)

In order to study the molecular structure and dynamics of liquid water with soft x-ray probes, samples with nanoscale dimensions are needed. This paper describes a simple method for preparing nanofluidic water cells. The idea is to confine a thin layer of water between two silicon nitride windows. The windows are 1 mm x 1 mm and 0.5 mm x 0.5 mm in size and have a thickness of 150 nm. The thickness of the water layer was measured experimentally by probing the infrared spectrum of water in the cells with a Fourier Transform InfraRed (FTIR) apparatus and from soft x-ray static measurements at the Advanced Light Source (ALS) at Lawrence Berkeley National Laboratory. Water layers ranging from 10 nm to more than 2 {micro}m were observed. Evidence for changes in the water structure compared to bulk water is observed in the ultrathin cells.

Irizarry, Melvin E.; /Puerto Rico U., Mayaguez /SLAC

2006-08-23T23:59:59.000Z

336

Gated x-ray detector for the National Ignition Facility  

SciTech Connect (OSTI)

Two new gated x-ray imaging cameras have recently been designed, constructed, and delivered to the National Ignition Facility in Livermore, CA. These gated x-Ray detectors are each designed to fit within an aluminum airbox with a large capacity cooling plane and are fitted with an array of environmental housekeeping sensors. These instruments are significantly different from earlier generations of gated x-ray images due, in part, to an innovative impedance matching scheme, advanced phosphor screens, pulsed phosphor circuits, precision assembly fixturing, unique system monitoring, and complete remote computer control. Preliminary characterization has shown repeatable uniformity between imaging strips, improved spatial resolution, and no detectable impedance reflections.

Oertel, John A.; Aragonez, Robert; Archuleta, Tom; Barnes, Cris; Casper, Larry; Fatherley, Valerie; Heinrichs, Todd; King, Robert; Landers, Doug; Lopez, Frank; Sanchez, Phillip; Sandoval, George; Schrank, Lou; Walsh, Peter; Bell, Perry; Brown, Matt; Costa, Robert; Holder, Joe; Montelongo, Sam; Pederson, Neal [Los Alamos National Laboratory, Los Alamos, New Mexico 87544 (United States); Lawrence Livermore National Laboratory, Livermore, California 94551-0808 (United States); VI Control Systems Ltd., Los Alamos, New Mexico 87544 (United States)

2006-10-15T23:59:59.000Z

337

X-ray afterglows from gamma-ray bursts  

E-Print Network [OSTI]

We consider possible interpretations of the recently detected X- ray afterglow from the gamma-ray burst source GRB 970228. Cosmological and Galactic models of gamma-ray bursts predict different flux and spectral evolution of X-ray afterglows. We show that models based on adiabatic expansion of relativistic forward shocks require very efficient particle energization or post-burst re-acceleration during the expansion. Cooling neutron star models predict a very distinctive spectral and flux evolution that can be tested in current X-ray data.

M. Tavani

1997-03-24T23:59:59.000Z

338

Linear accelerator x-ray sources with high duty cycle  

SciTech Connect (OSTI)

X-ray cargo inspection systems typically use a several-MV pulsed linear accelerator (linac) to produce a bremsstrahlung spectrum of x rays by bombarding a target with electrons. The x rays traverse the cargo and are detected by a detector array. Spectroscopy of the detected x rays is very desirable: if one can determine the spectrum of the transmitted x rays, one can determine the Z of the material they traversed. Even in relatively low-dose modes of operation, thousands of x rays arrive at each detector element during each pulse, unless the x rays are heavily absorbed or scattered by the cargo. For portal or fixed-site systems, dose rates, and therefore x-ray count rates, are even higher. Because of the high x-ray count rate, spectroscopy is impractical in conventional cargo inspection systems, except in certain special cases. For a mobile system, typical pulse durations are a few microseconds, and the number of pulses is on the order of 100 per second, leading to a duty factor of about 0.04%. Clearly, a linear accelerator x-ray source with much higher duty factor would be useful, since then the same number of x rays could be spread out over time, reducing the x-ray count rate. In this paper, we explore the possibility of designing a linear accelerator system, using more or less Conventional Off the Shelf (COTS) components, capable of duty cycles of 1% or greater. A survey was conducted of available linac RF source options and, given the possibilities, calculations were performed for suitable beam centerline designs. Keeping in mind that the size and cost of the accelerator system should be practical for use in a mobile cargo inspection system, only a few options are shown to be reasonably feasible, both requiring the use of klystrons instead of the magnetrons used in conventional systems. An S-Band design appears clearly possible, and there is also a promising X-Band design.

Condron, Cathie; Brown, Craig; Gozani, Tsahi; Langeveld, Willem G. J. [Rapiscan Laboratories, Inc., 520 Almanor Ave. Sunnyvale, CA 94085 (United States); Hernandez, Michael [XScell corp., 2134 Old Middlefield Way, Mountain View, CA 94043 (United States)

2013-04-19T23:59:59.000Z

339

Current Problems for X-ray Emission from Radio Jets  

E-Print Network [OSTI]

A list is presented of known extragalactic radio jets which also have associated X-ray emission. The canonical emission processes for the production of X-rays are reviewed and the sources are categorized on the basis of our current understanding. Although it seems clear that the X-ray emission is non-thermal, the two competing processes, synchrotron and inverse Compton emissions, arise from extremely high energy (synchrotron) or extremely low energy (beaming models with IC emission), relativistic electrons. Only synchrotron self-Compton emission from a few hotspots provides information on the `normal' energy range of the electrons responsible for the observed radio emission.

D. E. Harris

2000-12-17T23:59:59.000Z

340

X-ray backscatter imaging of nuclear materials  

DOE Patents [OSTI]

The energy of an X-ray beam and critical depth are selected to detect structural discontinuities in a material having an atomic number Z of 57 or greater. The critical depth is selected by adjusting the geometry of a collimator that blocks backscattered radiation so that backscattered X-ray originating from a depth less than the critical depth is not detected. Structures of Lanthanides and Actinides, including nuclear fuel rod materials, can be inspected for structural discontinuities such as gaps, cracks, and chipping employing the backscattered X-ray.

Chapman, Jeffrey Allen; Gunning, John E; Hollenbach, Daniel F; Ott, Larry J; Shedlock, Daniel

2014-09-30T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Spatiotemporal focusing dynamics in plasmas at X-ray wavelength  

SciTech Connect (OSTI)

Using a finite curvature beam, we investigate here the spatiotemporal focusing dynamics of a laser pulse in plasmas at X-ray wavelength. We trace the dependence of curvature parameter on the focusing of laser pulse and recognize that the self-focusing in plasma is more intense for the X-ray laser pulse with curved wavefront than with flat wavefront. The simulation results demonstrate that spatiotemporal focusing dynamics in plasmas can be controlled with the appropriate choice of beam-plasma parameters to explore the high intensity effects in X-ray regime.

Sharma, A., E-mail: a-physics2001@yahoo.com; Tibai, Z. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary)] [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Hebling, J. [Institute of Physics, University of Pecs, Pecs–7624 (Hungary) [Institute of Physics, University of Pecs, Pecs–7624 (Hungary); Szentagothai Research Centre, University of Pecs, Pecs-7624 (Hungary); Mishra, S. K. [Institute for Plasma Research, Gandhinagar (India)] [Institute for Plasma Research, Gandhinagar (India)

2014-03-15T23:59:59.000Z

342

X-Ray Microscopy and Imaging: Science and Research  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear SecurityTensile Strain Switched FerromagnetismWaste and MaterialsWenjun1of Energy WorldwideX-RayX-RayX-Ray

343

Characterization of X-ray generator beam profiles.  

SciTech Connect (OSTI)

T to compute the radiography properties of various materials, the flux profiles of X-ray sources must be characterized. This report describes the characterization of X-ray beam profiles from a Kimtron industrial 450 kVp radiography system with a Comet MXC-45 HP/11 bipolar oil-cooled X-ray tube. The empirical method described here uses a detector response function to derive photon flux profiles based on data collected with a small cadmium telluride detector. The flux profiles are then reduced to a simple parametric form that enables computation of beam profiles for arbitrary accelerator energies.

Mitchell, Dean J; Harding, Lee T.; Thoreson, Gregory G.; Theisen, Lisa Anne; Parmeter, John Ethan; Thompson, Kyle Richard

2013-07-01T23:59:59.000Z

344

Synchrotron-Radiation Induced X-Ray Emission (SRIXE)  

SciTech Connect (OSTI)

Elemental analysis using emission of characteristic x rays is a well-established scientific method. The success of this analytical method is highly dependent on the properties of the source used to produce the x rays. X-ray tubes have long existed as a principal excitation source, but electron and proton beams have also been employed extensively. The development of the synchrotron radiation x-ray source that has taken place during the past 40 years has had a major impact on the general field of x-ray analysis. Even tier 40 years, science of x-ray analysis with synchrotron x-ray beams is by no means mature. Improvements being made to existing synchrotron facilities and the design and construction of new facilities promise to accelerate the development of the general scientific use of synchrotron x-ray sources for at least the next ten years. The effective use of the synchrotron source technology depends heavily on the use of high-performance computers for analysis and theoretical interpretation of the experimental data. Fortunately, computer technology has advanced at least as rapidly as the x-ray technology during the past 40 years and should continue to do so during the next decade. The combination of these technologies should bring about dramatic advances in many fields where synchrotron x-ray science is applied. It is interesting also to compare the growth and rate of acceptance of this particular research endeavor to the rates for other technological endeavors. Griibler [1997] cataloged the time required for introduction, diffusion,and acceptance of technological, economic, and social change and found mean values of 40 to 50 years. The introduction of the synchrotron source depends on both technical and non-technical factors, and the time scale at which this seems to be occurring is quite compatible with what is seen for other major innovations such as the railroad or the telegraph. It will be interesting to see how long the present rate of technological change and increase in scientific use can be maintained for the synchrotron x-ray source. A short summary of the present state of the synchrotron radiation-induced x-ray emission (SRIXE) method is presented here. Basically, SRIXE experiments can include any that depend on the detection. of characteristic x-rays produced by the incident x-ray beam born the synchrotron source as they interact with a sample. Thus, experiments done to measure elemental composition, chemical state, crystal, structure, and other sample parameters can be considered in a discussion of SRIXE. It is also clear that the experimentalist may well wish to use a variety of complementary techniques for study of a given sample. For this reason, discussion of computed microtomography (CMT) and x-ray diffraction is included here. It is hoped that this present discussion will serve as a succinct introduction to the basic ideas of SRIXE for those not working in the field and possibly help to stimulate new types of work by those starting in the field as well as by experienced practitioners of the art. The topics covered include short descriptions of (1) the properties of synchrotron radiation, (2) a description of facilities used for its production, (3) collimated microprobe, (4) focused microprobes, (5) continuum and monoenergetic excitation, (6) detection limits, (7) quantitation, (8) applications of SRIXE, (9) computed microtomography (CMT), and (10)chemical speciation using x-ray absorption near-edge structure (XANES) and extended x-ray absorption fine structure (EXAFS). An effort has been made to cite a wide variety of work from different laboratories to show the vital nature of the field.

Jones, Keith W.

1999-09-01T23:59:59.000Z

345

Automated suppression of errors in LTP-II slope measurements with x-ray optics  

E-Print Network [OSTI]

slope measurements with x-ray optics Zulfiqar Ali, Curtis L.with state-of-the-art x-ray optics. Significant suppressionscanning, metrology of x-ray optics, deflectometry Abstract

Ali, Zulfiqar

2011-01-01T23:59:59.000Z

346

X-ray optics metrology limited by random noise, instrumental drifts, and systematic errors  

E-Print Network [OSTI]

X-ray optics metrology limited by random noise, instrumentalUSA Center for X-ray Optics, Lawrence Berkeley Nationaland reflecting x-ray optics suitable for micro- and nano-

Yashchuk, Valeriy V.

2010-01-01T23:59:59.000Z

347

E-Print Network 3.0 - advanced x-ray timing Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND Summary: with the occurrence of solar X-ray flare, when light travel time delay is accounted, suggesting that X-rays...

348

X-RAY ABSORPTION STUDIES OF GRAPHITE INTERCALATES AND METAL-AMMONIA SOLUTION  

E-Print Network [OSTI]

I. INTRODUCTION A. X-Ray Absorption Spectroscopy B. Graphiteacknowledged. The X-Ray absorption data could not have beenI INTRODUCTION X-ray absorption, spectroscopy (XAS) has been

Robertson, A.S.

2010-01-01T23:59:59.000Z

349

AN X-RAY ABSORPTION SPECTROSCOPY STUDY OF MANGANESE CONTAINING COMPOUNDS AND PHOTOSYNTHETIC SPINACH CHLOROPLASTS  

E-Print Network [OSTI]

II. Extended X-ray Absorption Fine Structure (EXAFS) TheoryIII. X-ray Absorption Spectroscopy (XAS) ExperimentIII. EXTENDED X-RAY ABSORPTION FINE STRUCTURE (EXAFS) DATA

Kirby, Jon Allan

2012-01-01T23:59:59.000Z

350

X-ray Absorption Spectroscopy Study of Prototype Chemical Systems: Theory vs. Experiment  

E-Print Network [OSTI]

acids by Near Edge X-ray Absorption Fine Structure (NEXAFS)X-ray Absorption Spectroscopy Study of Prototype ChemicalGlaeser Spring 2010 X-ray Absorption Spectroscopy Study of

Schwartz, Craig Philip

2010-01-01T23:59:59.000Z

351

X-ray absorption spectroscopy at the Ni-K edge in Stackhousia tryonii Bailey hyperaccumulator  

E-Print Network [OSTI]

X-ray absorption spectroscopy at the Ni–K edge inin vivo by micro x-ray absorption spectroscopy (XAS) at theNi–K edge. Both x-ray absorption near edge structure and

Kachenko, A.

2009-01-01T23:59:59.000Z

352

E-Print Network 3.0 - angle x-ray studies Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

4 X-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND Summary: and solar wind, and how planetary and cometary X-rays can be used to study...

353

Beyond 3-D X-ray Imaging: Methodology Development and Applications...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

to the availability of the new generation of X-ray sources and the advanced X-ray optics. The advanced X-ray Optics along with novel methodology has made it possible to...

354

E-Print Network 3.0 - airborne lead x-ray Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Pulsars... you'd . . . Active Galactic . . . X-ray binaries Pulsars and relatives Gamma-ray bursts Gravitational... 1 - Type 2 X-ray binaries - Low mass X-ray binaries (LMXBs)...

355

E-Print Network 3.0 - accreting milli-second x-ray Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

milli-second x-ray Search Powered by Explorit Topic List Advanced Search Sample search results for: accreting milli-second x-ray Page: << < 1 2 3 4 5 > >> 1 X-rays from classical T...

356

Recent Flash X-Ray Injector Modeling  

SciTech Connect (OSTI)

The injector of the Flash X-Ray (FXR) accelerator has a significantly larger than expected beam emittance. A computer modeling effort involving three different injector design codes was undertaken to characterize the FXR injector and determine the cause of the large emittance. There were some variations between the codes, but in general the simulations were consistent and pointed towards a much smaller normalized, rms emittance (36 cm-mr) than what was measured (193 cm-mr) at the exit of the injector using a pepperpot technique. The simulations also indicated that the present diode design was robust with respect to perturbations to the nominal design. Easily detected mechanical alignment/position errors and magnet errors did not lead to appreciable increase in the simulated emittance. The physics of electron emission was not modeled by any of the codes and could be the source of increased emittance. The nominal simulation assumed uniform Child-Langmuir Law emission from the velvet cathode and no shroud emission. Simulations that looked at extreme non-uniform cathode and shroud emission scenarios resulted in doubling of the emittance. An alternative approach was to question the pepperpot measurement. Simulations of the measurement showed that the pepperpot aperture foil could double the emittance with respect to the non-disturbed beam. This leads to a diplomatic explanation of the discrepancy between predicted and measured emittance where the fault is shared. The measured value is too high due to the effect of the diagnostic on the beam and the simulations are too low because of unaccounted cathode and/or shroud emission physics. Fortunately there is a relatively simple experiment that can resolve the emittance discrepancy. If the large measured emittance value is correct, the beam envelope is emittance dominated at modest values of focusing field and beam radius. Measurements of the beam envelope on an imaging foil at the exit of the injector would lead to an accurate value of the emittance. If the emittance was approximately half of the measured value, the beam envelope is slightly space charge dominated, but envelope measurements would set reasonable bounds on the emittance value. For an emittance much less than 100 cm-mr, the envelope measurements would be insensitive to emittance. The outcome of this envelope experiment determines if a redesigned diode is needed or if more sophisticated emittance measurements should be pursued.

Houck, T; Blackfield, D; Burke, J; Chen, Y; Javedani, J; Paul, A C

2004-11-10T23:59:59.000Z

357

Polarization Entangled Photons at X-Ray Energies  

E-Print Network [OSTI]

We show that polarization entangled photons at x-ray energies can be generated via spontaneous parametric down conversion. Each of the four Bell states can be generated by choosing the angle of incidence and polarization of the pumping beam.

S. Shwartz; S. E. Harris

2010-12-16T23:59:59.000Z

358

Towards hard X-ray imaging at GHz frame rate  

SciTech Connect (OSTI)

Gigahertz (GHz) imaging using hard X-rays ({approx}> 10 keV) can be useful to high-temperature plasma experiments, as well as research using coherent photons from synchrotron radiation and X-ray free electron lasers. GHz framing rate can be achieved by using multiple cameras through multiplexing. The advantages and trade-offs of single-photon detection mode, when no more than one X-ray photon is detected per pixel, are given. Two possible paths towards X-ray imaging at GHz frame rates using a single camera are (a) Avalanche photodiode arrays of high-Z materials and (b) Microchannel plate photomultipliers in conjunction with materials with large indices of refraction.

Wang, Zhehui [Los Alamos National Laboratory; Morris, Christopher [Los Alamos National Laboratory; Luo, Shengnian [Los Alamos National Laboratory; Kwiatkowski, Kris K. [Los Alamos National Laboratory; Kapustinsky, Jon S. [Los Alamos National Laboratory

2012-05-02T23:59:59.000Z

359

Towards hard x-ray imaging at GHz frame rate  

SciTech Connect (OSTI)

Gigahertz (GHz) imaging using hard x-rays ( Greater-Than-Or-Equivalent-To 10 keV) can be useful to high-temperature plasma experiments, as well as research and applications using coherent photons from synchrotron radiation and x-ray free electron lasers. GHz framing rate can be achieved by using multiple cameras through multiplexing. The advantages and trade-offs of single-photon detection mode, when no more than one x-ray photon is detected per pixel, are given. Two possible paths towards x-ray imaging at GHz frame rates using a single camera are: (a) avalanche photodiode arrays of high-Z materials and (b) microchannel plate photomultipliers in conjunction with materials with large indices of refraction.

Wang Zhehui; Morris, C. L.; Kapustinsky, J. S.; Kwiatkowski, K.; Luo, S.-N. [Los Alamos National Laboratory, Los Alamos, New Mexico 87545 (United States)

2012-10-15T23:59:59.000Z

360

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

12.0.2.2 Citation: J.J. Turner et al., "X-Ray Diffraction Microscopy of Magnetic Structures," Phys. Rev. Lett. 107, 033904 (2011). Web: http:prl.aps.orgpdfPRLv107i3e033904...

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

Magnetism studies using resonant, coherent, x-ray scattering...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Magnetism studies using resonant, coherent, x-ray scattering Monday, September 10, 2012 - 10:00am SLAC, Bldg. 137, Room 226 Keoki Seu Seminar: With the advent of free electron...

362

Systems and methods for detecting x-rays  

DOE Patents [OSTI]

Systems and methods for detecting x-rays are disclosed herein. One or more x-ray-sensitive scintillators can be configured from a plurality of heavy element nano-sized particles and a plastic material, such as polystyrene. As will be explained in greater detail herein, the heavy element nano-sized particles (e.g., PbWO4) can be compounded into the plastic material with at least one dopant that permits the plastic material to scintillate. X-rays interact with the heavy element nano-sized particles to produce electrons that can deposit energy in the x-ray sensitive scintillator, which in turn can produce light.

Bross, Alan D.; Mellott, Kerry L.; Pla-Dalmau, Anna

2006-05-02T23:59:59.000Z

363

Epoxy replication for Wolter x-ray microscope fabrication  

SciTech Connect (OSTI)

An epoxy replica of a test piece designed to simulate a Wolter x-ray microscope geometry showed no loss of x-ray reflectivity or resolution, compared to the original. The test piece was a diamond-turned cone with 1.5/sup 0/ half angle. A flat was fly-cut on one side, then super- and conventionally polished. The replica was separated at the 1.5/sup 0/-draft angle, simulating a shallow angle Wolter microscope geometry. A test with 8.34 A x rays at 0.9/sup 0/ grazing angle showed a reflectivity of 67% for the replica flat surface, and 70% for the original. No spread of the reflected beam was observed with a 20-arc second wide test beam. This test verifies the epoxy replication technique for production of Wolter x-ray microscopes.

Priedhorsky, W.

1981-01-01T23:59:59.000Z

364

The colours of the X-ray background  

E-Print Network [OSTI]

The recent deep X-ray surveys at both soft (0.5--2 keV) and hard (2--10 keV) energies have greatly extended our knowledge of the X-ray source density and spectral shapes at relatively faint fluxes adding further evidence on the fact that discrete sources, mainly AGNs, are responsible for the X-ray background (XRB) emission over a broad energy range. In addition the first complete optically identified samples of soft X-ray sources are becoming available allowing to test the XRB AGN synthesis models in the light of recent results. In this paper I will briefly compare the model predictions with some new observational data.

A. Comastri

1998-09-07T23:59:59.000Z

365

Vitreous carbon mask substrate for X-ray lithography  

DOE Patents [OSTI]

The present invention is directed to the use of vitreous carbon as a substrate material for providing masks for X-ray lithography. The new substrate also enables a small thickness of the mask absorber used to pattern the resist, and this enables improved mask accuracy. An alternative embodiment comprised the use of vitreous carbon as a LIGA substrate wherein the VC wafer blank is etched in a reactive ion plasma after which an X-ray resist is bonded. This surface treatment provides a surface enabling good adhesion of the X-ray photoresist and subsequent nucleation and adhesion of the electrodeposited metal for LIGA mold-making while the VC substrate practically eliminates secondary radiation effects that lead to delamination of the X-ray resist form the substrate, the loss of isolated resist features, and the formation of a resist layer adjacent to the substrate that is insoluble in the developer.

Aigeldinger, Georg (Livermore, CA); Skala, Dawn M. (Fremont, CA); Griffiths, Stewart K. (Livermore, CA); Talin, Albert Alec (Livermore, CA); Losey, Matthew W. (Livermore, CA); Yang, Chu-Yeu Peter (Dublin, CA)

2009-10-27T23:59:59.000Z

366

Optical and X-ray Variability of AGNs  

E-Print Network [OSTI]

I present new comparisons of AGN optical, UV, and X-ray variations. These reveal complex relationships between the different passbands that can change with time in a given object. While there is evidence from several objects that X-ray and optical activity levels are correlated on long timescales, variations on shorter timescales can occur independently. It is proposed that the combination of correlated and uncorrelated short-timescale variability is a consequence of anisotropic high-energy emission. It is also argued that the correlation between X-ray and optical variability on long timescales must be due to a common underlying factor and not to reprocessing of X-ray radiation.

C. Martin Gaskell

2006-12-30T23:59:59.000Z

367

,~ Abstract Submitted to 1997 Denver X-Ray Conference  

E-Print Network [OSTI]

,~ Abstract Submitted to 1997 Denver X-Ray Conference Denver, Colorado -August 4-8, 1997 BNL-.64346 being distributed through the entire volume of the particle needs further investigation. *Work supported

Brookhaven National Laboratory

368

Nanofabrication of Diffractive X-ray Optics for Synchrotrons...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Nanofabrication of Diffractive X-ray Optics for Synchrotrons and XFELs Wednesday, March 11, 2015 - 3:00pm SLAC, Redtail Hawk Conference Room 108A Speaker: Christian David, Paul...

369

Soft x-ray capabilities for investigating the strongly correlated...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Soft x-ray capabilities for investigating the strongly correlated electron materials Friday, September 14, 2012 - 1:00pm SLAC, Bldg. 137, Room 226 Jun-Sik Lee Seminar One of the...

370

X-ray Raman scattering study of aligned polyfluorene  

E-Print Network [OSTI]

We present a non-resonant inelastic x-ray scattering study at the carbon K-edge on aligned poly[9,9-bis(2-ethylhexyl)-fluorene-2,7-diyl] and show that the x-ray Raman scattering technique can be used as a practical alternative to x-ray absorption measurements. We demonstrate that this novel method can be applied to studies on aligned $\\pi$-conjugated polymers complementing diffraction and optical studies. Combining the experimental data and a very recently proposed theoretical scheme we demonstrate a unique property of x-ray Raman scattering by performing the symmetry decomposition on the density of unoccupied electronic states into $s$- and $p$-type symmetry contributions.

S. Galambosi; M. Knaapila; J. A. Soininen; K. Nyg\\aard; S. Huotari; F. Galbrecht; U. Scherf; A. P. Monkman; K. Hämäläinen

2006-08-29T23:59:59.000Z

371

X-Ray Photoelectron Spectroscopy (XPS) Applied to Soot & What...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Photoelectron Spectroscopy (XPS) Applied to Soot & What It Can Do for You X-Ray Photoelectron Spectroscopy (XPS) Applied to Soot & What It Can Do for You Presentation given at DEER...

372

Gravitational and Relativistic Deflection of X-Ray Superradiance  

E-Print Network [OSTI]

Exploring Einstein's theories of relativity in quantum systems, for example by using atomic clocks at high speeds can deepen our knowledge in physics. However, many challenges still remain on finding novel methods for detecting effects of gravity and of special relativity and their roles in light-matter interaction. Here we introduce a scheme of x-ray quantum optics that allows for a millimeter scale investigation of the relativistic redshift by directly probing a fixed nuclear crystal in Earth's gravitational field with x-rays. Alternatively, a compact rotating crystal can be used to force interacting x-rays to experience inhomogeneous clock tick rates in a crystal. We find that an association of gravitational or special-relativistic time dilation with quantum interference will be manifested by deflections of x-ray photons. Our protocol suggests a new and feasible tabletop solution for probing effects of gravity and special relativity in the quantum world.

Wen-Te Liao; Sven Ahrens

2014-11-27T23:59:59.000Z

373

The X-ray background and the evolution of AGN  

E-Print Network [OSTI]

We discuss the constraints on the AGN evolution from the cosmic X-ray background and source counts. A synthesis model to fit the X-ray background is presented. In the model, the spectrum of type 2 AGN has been modeled including Compton down--scattering within the absorbing material. Besides, we introduced a dependence on redshift of the relative number of obscured sources and found a decrease of the fraction of type 2 AGN at redshifts larger than 2.

Fulvio Pompilio; Fabio La Franca; Giorgio Matt

1999-09-23T23:59:59.000Z

374

Sapphire analyzers for high-resolution x-ray spectroscopy.  

SciTech Connect (OSTI)

We present a sapphire (Al{sub 2}O{sub 3}) analyzer for high-resolution X-ray spectroscopy with 31-meV energy resolution. The analyzer is designed for resonant inelastic X-ray scattering (RIXS) measurements at the CuK{sub a} absorption edge near 8990 eV. The performance of the analyzer is demonstrated by measuring phonon excitations in beryllium because of its known dynamical structure and high counting rates.

Yavas, H.; Alp, E.; Sinn, H.; Alatas, A.; Said, A.; Shvydko, Y.; Toellner, T.; Khachatryan, R.; Billinge, S.; Hasan, Z.; Sturhahn, W.; Michigan State Univ.; Princeton Univ.; DESY

2007-11-11T23:59:59.000Z

375

Ris-M-2751 X-Ray Energy Dispersive  

E-Print Network [OSTI]

(PHOT) k«V 50 Risø National Laboratory, DK-4000 Roskilde, Denmark October 1988 #12;Ris*-M-2751 X-ray energy is impinging on the sample (Fig. lb). Its wavelength (photon energy) is in the course of measurements changedm ii. S Risø-M-2751 X-Ray Energy Dispersive Diffraction Lecture Notes Bronislaw Buras BaKo 30 40 E

376

New Directions in X-Ray Light Sources  

ScienceCinema (OSTI)

July 15, 2008 Berkeley Lab lecture: Molecular movies of chemical reactions and material phase transformations need a strobe of x-rays, the penetrating light that reveals how atoms and molecules assemble in chemical and biological systems and complex materials. Roger Falcone, Director of the Advanced Light Source,will discuss a new generation of x ray sources that will enable a new science of atomic dynamics on ultrafast timescales.

Roger Falcone

2010-01-08T23:59:59.000Z

377

X-Ray Diffraction Studies of Copper Nanopowder  

E-Print Network [OSTI]

Copper nanopowder preparation and its X-Ray diffraction studies are reported in this paper. Electrolytic cathode deposition method is simple and cheapest process for its preparation. Copper nanopowder has been prepared from aqueous copper sulphate solution. Wide range of experimental conditions has been adopted in this process and its X-Ray diffraction characterizations have been studied. The results confirming copper nanopowder with size below 30 nm. Uniformed size Copper nanopowder preparation, in normal room temperature is importance of this study.

T. Theivasanthi; M. Alagar

2010-03-31T23:59:59.000Z

378

X-ray tube with magnetic electron steering  

DOE Patents [OSTI]

An X-ray tube uses a magnetic field to steer electrons. The magnetic field urges electrons toward the anode, increasing the proportion of electrons emitted from the cathode that reach desired portions of the anode and consequently contribute to X-ray production. The magnetic field also urges electrons reflected from the anode back to the anode, further increasing the efficiency of the tube.

Reed, Kim W. (Albuquerque, NM); Turman, Bobby N. (Albuquerque, NM); Kaye, Ronald J. (Albuquerque, NM); Schneider, Larry X. (Albuquerque, NM)

2000-01-01T23:59:59.000Z

379

X-Ray Fluorescence (XRF) Analysis of Obsidian Artifacts from Shoofly Ruin, Central Arizona  

E-Print Network [OSTI]

X-RAY FLUORESCENCE (XRF) ANALYSIS OF OBSIDIAN ARTIFACTS FROM62:426-437. SOUTHWEST XRF PAPER Table 1. X-ray fluorescence

Shackley, M. Steven

1986-01-01T23:59:59.000Z

380

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Soft X-Ray Microscopy and Spectroscopy at the Molecular Environmental Science Beamline at the Advanced Light Source. Soft X-Ray Microscopy and Spectroscopy at the Molecular...

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

How Can X-ray Transient Absorption Spectroscopy Aide Solar Energy...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

are from optimized on structural, energetic and dynamic parameters. Intense X-ray pulses from synchrotrons and X-ray free electrons lasers coupled with ultrafast lasers...

382

X-RAY ABSORPTION SPECTROSCOPY FOR THE CHEMICAL CHARACTERIZATION OF ATMOSPHERIC AEROSOLS  

E-Print Network [OSTI]

November 11-16 9 1979 X-RAY ABSORPTION SPECTROSCOPY FOR THEUniversity of California. ABSORPTION SPECTROSCOPY FOR THEand x-ray emission and absorption spectroscopy. The first

Jaklevic, J. M.

2011-01-01T23:59:59.000Z

383

Ultrafast X-ray Phase-Enhanced Microimaging for Visualizing Fuel...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Ultrafast X-ray Phase-Enhanced Microimaging for Visualizing Fuel Injection Process and Diesel Sprays Ultrafast X-ray Phase-Enhanced Microimaging for Visualizing Fuel Injection...

384

Quiet Sun X-rays as Signature for New Particles  

E-Print Network [OSTI]

We have studied published data from the Yohkoh solar X-ray mission, with the purpose of searching for signals from radiative decays of new, as yet undiscovered massive neutral particles. This search is based on the prediction that solar axions of the Kaluza-Klein type should result in the emission of X-rays from the Sun direction beyond the limb with a characteristic radial distribution. These X-rays should be observed more easily during periods of quiet Sun. An additional signature is the observed emission of hard X-rays by SMM, NEAR and RHESSI. The recent observation made by RHESSI of a continuous emission from the non-flaring Sun of X-rays in the 3 to ~15 keV range fits the generic axion scenario. This work also suggests new analyses of existing data, in order to exclude instrumental effects; it provides the rationale for targeted observations with present and upcoming (solar) X-ray telescopes, which can provide the final answer on the nature of the signals considered here. Such measurements become more promising during the forthcoming solar cycle minimum with an increased number of quiet Sun periods.

K. Zioutas; K. Dennerl; L. DiLella; D. H. H. Hoffmann; J. Jacoby; Th. Papaevangelou

2004-03-08T23:59:59.000Z

385

X-ray absorption in distant type II QSOs  

E-Print Network [OSTI]

We present the results of the X-ray spectral analysis of an XMM-Newton-selected type II QSO sample with z>0.5 and 0.5-10 keV flux of 0.3-33 x 10^{-14} erg/s/cm^2. The distribution of absorbing column densities in type II QSOs is investigated and the dependence of absorption on X-ray luminosity and redshift is studied. We inspected 51 spectroscopically classified type II QSO candidates from the XMM-Newton Marano field survey, the XMM-Newton-2dF wide angle survey (XWAS), and the AXIS survey to set-up a well-defined sample with secure optical type II identifications. Fourteen type II QSOs were classified and an X-ray spectral analysis performed. Since most of our sources have only ~40 X-ray counts (PN-detector), we carefully studied the fit results of the simulated X-ray spectra as a function of fit statistic and binning method. We determined that fitting the spectra with the Cash-statistic and a binning of minimum one count per bin recovers the input values of the simulated X-ray spectra best. Above 100 PN coun...

Krumpe, M; Corral, A; Schwope, A D; Carrera, F J; Barcons, X; Page, M; Mateos, S; Tedds, J A; Watson, M G

2008-01-01T23:59:59.000Z

386

Spectral Formation in X-Ray Pulsar Accretion Columns  

E-Print Network [OSTI]

We present the first self-consistent model for the dynamics and the radiative transfer occurring in bright X-ray pulsar accretion columns, with a special focus on the role of the shock in energizing the emerging X-rays. The pressure inside the accretion column of a luminous X-ray pulsar is dominated by the photons, and consequently the equations describing the coupled radiative-dynamical structure must be solved simultaneously. Spectral formation in these sources is therefore a complex, nonlinear phenomenon. We obtain the analytical solution for the Green's function describing the upscattering of monochromatic radiation injected into the column from the thermal mound located near the base of the flow. The Green's function is convolved with a Planck distribution to model the X-ray spectrum resulting from the reprocessing of blackbody photons produced in the thermal mound. These photons diffuse through the infalling gas and eventually escape out the walls of the column, forming the observed X-ray spectrum. We show that the resulting column-integrated, phase-averaged spectrum has a power-law shape at high energies and a blackbody shape at low energies, in agreement with the observational data for many X-ray pulsars.

Peter A. Becker; Michael T. Wolff

2005-03-03T23:59:59.000Z

387

Liquid-Air Interface Corrosion Testing Simulating The Environment Of Hanford Double Shell Tanks  

SciTech Connect (OSTI)

Coupon tests on A537 carbon steel materials were conducted to evaluate the Liquid-Air Interface (LAI) corrosion susceptibility in a series of solutions designed to simulate conditions in the radioactive waste tanks located at the Hanford Nuclear Facility. The new stress corrosion cracking requirements and the impact of ammonia on LAI corrosion were the primary focus. The minimum R value (i.e., molar ratio of nitrite to nitrate) of 0.15 specified by the new stress corrosion cracking requirements was found to be insufficient to prevent pitting corrosion at the LAI. The pH of the test solutions was 10, which was actually less than the required pH 11 defined by the new requirements. These tests examined the effect of the variation of the pH due to hydroxide depletion at the liquid air interface. The pits from the current testing ranged from 0.001 to 0.008 inch in solutions with nitrate concentrations of 0.4 M and 2.0 M. The pitting and general attack that occurred progressed over the four-months. No significant pitting was observed, however, for a solution with a nitrate concentration of 4.5 M. The pitting depths observed in these partial immersion tests in unevaporated condensates ranged from 0.001 to 0.005 inch after 4 months. The deeper pits were in simulants with low R values. Simulants with R values of approximately 0.6 to 0.8 appeared to significantly reduce the degree of attack. Although, the ammonia did not completely eliminate attack at the LAI, the amount of corrosion in an extremely corrosive solution was significantly reduced. Only light general attack (< 1 mil) occurred on the coupon in the vicinity of the LAI. The concentration of ammonia (i.e., 50 ppm or 500 ppm) did not have a strong effect.

Wiersma, B.; Gray, J. R.; Garcia-Diaz, B. L.; Murphy, T. H.; Hicks, K. R.

2014-01-30T23:59:59.000Z

388

Simultaneous probing of bulk liquid phase and catalytic gas-liquid-solid interface under working conditions using attenuated total reflection infrared spectroscopy  

SciTech Connect (OSTI)

Design and performance of a reactor set-up for attenuated total reflection infrared (ATR-IR) spectroscopy suitable for simultaneous reaction monitoring of bulk liquid and catalytic solid-liquid-gas interfaces under working conditions are presented. As advancement of in situ spectroscopy an operando methodology for gas-liquid-solid reaction monitoring was developed that simultaneously combines catalytic activity and molecular level detection at the catalytically active site of the same sample. Semi-batch reactor conditions are achieved with the analytical set-up by implementing the ATR-IR flow-through cell in a recycle reactor system and integrating a specifically designed gas feeding system coupled with a bubble trap. By the use of only one spectrometer the design of the new ATR-IR reactor cell allows for simultaneous detection of the bulk liquid and the catalytic interface during the working reaction. Holding two internal reflection elements (IRE) the sample compartments of the horizontally movable cell are consecutively flushed with reaction solution and pneumatically actuated, rapid switching of the cell (<1 s) enables to quasi simultaneously follow the heterogeneously catalysed reaction at the catalytic interface on a catalyst-coated IRE and in the bulk liquid on a blank IRE. For a complex heterogeneous reaction, the asymmetric hydrogenation of 2,2,2-trifluoroacetophenone on chirally modified Pt catalyst the elucidation of catalytic activity/enantioselectivity coupled with simultaneous monitoring of the catalytic solid-liquid-gas interface is shown. Both catalytic activity and enantioselectivity are strongly dependent on the experimental conditions. The opportunity to gain improved understanding by coupling measurements of catalytic performance and spectroscopic detection is presented. In addition, the applicability of modulation excitation spectroscopy and phase-sensitive detection are demonstrated.

Meemken, Fabian; Müller, Philipp; Hungerbühler, Konrad; Baiker, Alfons, E-mail: baiker@chem.ethz.ch [Department of Chemistry and Applied Biosciences, Institute for Chemical and Bioengineering, ETH Zürich, Hönggerberg, HCI, CH-8093 Zürich (Switzerland)

2014-08-15T23:59:59.000Z

389

Dilation x-ray imager a new/faster gated x-ray imager for the NIF  

SciTech Connect (OSTI)

As the yield on implosion shots increases it is expected that the peak x-ray emission reduces to a duration with a FWHM as short as 20 ps for {approx}7 Multiplication-Sign 10{sup 18} neutron yield. However, the temporal resolution of currently used gated x-ray imagers on the NIF is 40-100 ps. We discuss the benefits of the higher temporal resolution for the NIF and present performance measurements for dilation x-ray imager, which utilizes pulse-dilation technology [T. J. Hilsabeck et al., Rev. Sci. Instrum. 81, 10E317 (2010)] to achieve x-ray imaging with temporal gate times below 10 ps. The measurements were conducted using the COMET laser, which is part of the Jupiter Laser Facility at the Lawrence Livermore National Laboratory.

Nagel, S. R.; Bell, P. M.; Bradley, D. K.; Ayers, M. J.; Barrios, M. A.; Felker, B.; Smith, R. F.; Collins, G. W.; Jones, O. S.; Piston, K.; Raman, K. S. [Lawrence Livermore National Laboratory, 7000 East Avenue, Livermore, California 94550 (United States); Hilsabeck, T. J.; Kilkenny, J. D.; Chung, T.; Sammuli, B. [General Atomics, P.O. Box 85608, San Diego, California 92186-5608 (United States); Hares, J. D.; Dymoke-Bradshaw, A. K. L. [Kentech Instruments Ltd., Wallingford, Oxfordshire OX10 (United Kingdom)

2012-10-15T23:59:59.000Z

390

Modeling the high resolution X-ray spectra from the relativistic jets of the X-ray binary SS 433  

E-Print Network [OSTI]

We test the physical model of the relativistic jets in the galactic X-ray binary SS 433 that was proposed by Marshall et al. 2002 (Paper I) using additional observations from the Chandra High Energy Transmission Grating ...

Lopez, Laura Ann, 1982-

2004-01-01T23:59:59.000Z

391

54X-rays from Hot Gases Near the SN1979C Black Hole The Chandra X-Ray Observatory  

E-Print Network [OSTI]

is in solar mass units, and R is in kilometers. Problem 1 - Combining these equations using the method-Newton and the German ROSAT observatory revealed a bright source of X-rays that has remained steady for the 12 years, or distribution of X-rays with energy, support the idea that the object in SN 1979C is a black hole being fed

392

The crystal–liquid interface of a body?centered?cubic?forming substance: Computer simulations of the r ? 6 potential  

E-Print Network [OSTI]

(the bulk density change).27 For the (100) interface this 10--90 width is measured to be about 5.7a (just over 8 lattice planes). The variation of the diffusion constant through the in­ terface was calculated by dividing the z direction into 30 bins..., and were found not to differ measurably. The limiting liquid value of D (0.011 59 ± 0.000 01) was obtained in a separate 686 parti­ cle simulation of the bulk liquid. Note that bulk liquid diffu­ sion constants are known to be somewhat system size depen...

Laird, Brian Bostian; Haymet, A. D. J.

1989-09-01T23:59:59.000Z

393

Heat transfer issues in high-heat-load synchrotron x-ray beams  

SciTech Connect (OSTI)

In this paper, a short description of the synchrotron radiation x-ray sources and the associated power loads is given, followed by a brief description of typical synchrotron components and their heat load. It is emphasized that the design goals for most of these components is to limit (a) temperature, (b) stresses, or (c) strains in the system. Each design calls for a different geometry, material selection, and cooling scheme. Cooling schemes that have been utilized so far are primarily single phase and include simple macrochannel cooling, microchannel cooling, contact cooling, pin-post cooling, porous-flow cooling, jet cooling, etc. Water, liquid metals, and various cryogenic coolants have been used. Because the trend in x-ray beam development is towards brighter (i.e., more powerful) beams and assuming that no radical changes in the design of x-ray generating machines occurs in the next few years, it is fair to state that the utilization of various effective cooling schemes and, in particular, two-phase flow (e.g., subcooled boiling) warrants further investigation. This, however, requires a thorough examination of stability and reliability of two-phase flows for high-heat-flux components operating in ultrahigh vacuum with stringent reliability requirements.

Khounsary, A.M.; Mills, D.M.

1994-09-01T23:59:59.000Z

394

X-ray absorption in distant type II QSOs  

E-Print Network [OSTI]

We present the results of the X-ray spectral analysis of an XMM-Newton-selected type II QSO sample with z>0.5 and 0.5-10 keV flux of 0.3-33 x 10^{-14} erg/s/cm^2. The distribution of absorbing column densities in type II QSOs is investigated and the dependence of absorption on X-ray luminosity and redshift is studied. We inspected 51 spectroscopically classified type II QSO candidates from the XMM-Newton Marano field survey, the XMM-Newton-2dF wide angle survey (XWAS), and the AXIS survey to set-up a well-defined sample with secure optical type II identifications. Fourteen type II QSOs were classified and an X-ray spectral analysis performed. Since most of our sources have only ~40 X-ray counts (PN-detector), we carefully studied the fit results of the simulated X-ray spectra as a function of fit statistic and binning method. We determined that fitting the spectra with the Cash-statistic and a binning of minimum one count per bin recovers the input values of the simulated X-ray spectra best. Above 100 PN counts, the free fits of the spectrum's slope and absorbing hydrogen column density are reliable. We find only moderate absorption (N_H=(2-10) x 10^22 cm^-2) and no obvious trends with redshift and intrinsic X-ray luminosity. In a few cases a Compton-thick absorber cannot be excluded. Two type II objects with no X-ray absorption were discovered. We find no evidence for an intrinsic separation between type II AGN and high X-ray luminosity type II QSO in terms of absorption. The stacked X-ray spectrum of our 14 type II QSOs shows no iron K-alpha line. In contrast, the stack of the 8 type II AGN reveals a very prominent iron K-alpha line at an energy of ~ 6.6 keV and an EW ~ 2 keV.

M. Krumpe; G. Lamer; A. Corral; A. D. Schwope; F. J. Carrera; X. Barcons; M. Page; S. Mateos; J. A. Tedds; M. G. Watson

2008-03-10T23:59:59.000Z

395

Gain dynamics in a soft X-ray laser ampli er perturbed by a strong injected X-ray eld  

SciTech Connect (OSTI)

Seeding soft X-ray plasma ampli ers with high harmonics has been demonstrated to generate high-brightness soft X-ray laser pulses with full spatial and temporal coherence. The interaction between the injected coherent eld and the swept-gain medium has been modelled. However, no exper- iment has been conducted to probe the gain dynamics when perturbed by a strong external seed eld. Here, we report the rst X-ray pump X-ray probe measurement of the nonlinear response of a plasma ampli er perturbed by a strong soft X-ray ultra-short pulse. We injected a sequence of two time-delayed high-harmonic pulses (l518.9 nm) into a collisionally excited nickel-like molybdenum plasma to measure with femto-second resolution the gain depletion induced by the saturated ampli cation of the high-harmonic pump and its subsequent recovery. The measured fast gain recovery in 1.5 1.75 ps con rms the possibility to generate ultra-intense, fully phase-coherent soft X-ray lasers by chirped pulse ampli cation in plasma ampli ers.

Wang, Yong [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Wang, Shoujun [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Oliva, E [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Lu, L [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Berrill, Mark A [ORNL] [ORNL; Yin, Liang [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Nejdl, J [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Luther, Brad [Colorado State University, Fort Collins] [Colorado State University, Fort Collins; Proux, C [Laboratoire d’Optique Applique´e, ENSTA, CNRS, Ecole Polytechnique] [Laboratoire d’Optique Applique´e, ENSTA, CNRS, Ecole Polytechnique; Le, T. T. [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Dunn, James [Lawrence Livermore National Laboratory (LLNL)] [Lawrence Livermore National Laboratory (LLNL); Ros, D [Laboratoire de Physique des Gaz et des Gaz et des Plasmas] [Laboratoire de Physique des Gaz et des Gaz et des Plasmas; Zeitoun, Philippe [École Polytechnique] [École Polytechnique; Rocca, Jorge [Colorado State University, Fort Collins] [Colorado State University, Fort Collins

2014-01-01T23:59:59.000Z

396

Characteristics of the weld interface in dissimilar austenitic-pearlitic steel welds  

SciTech Connect (OSTI)

The weld interface in dissimilar alloy welds between austenitic and pearlitic steels was observed directly by using scanning and transmission electron microscopy, and energy-dispersive x-ray spectrometry. Two types of weld interface were found in the joints. One was the austenite/martensite-like interface that formed the boundary between the mixed weld metal zone and the partially mixed transitional zone. The other is the martensite-like/ferrite interface that is the true liquid-solid boundary of the joint. These interfaces can exist independently in different joints and can also coexist in one joint, depending on the Cr and Ni contents of the filler metals and alloy in the base metals. The formation mechanism of the weld interface and its effect on the mechanical properties of the welded joint are discussed.

Pan, C.; Zhang, Z. (Wuhan Transportation Univ. (China). Dept. of Marine Mechanical Engineering)

1994-09-01T23:59:59.000Z

397

Water destruction by X-rays in young stellar objects  

E-Print Network [OSTI]

We study the H2O chemistry in star-forming environments under the influence of a central X-ray source and a central far ultraviolet (FUV) radiation field. The gas-phase water chemistry is modeled as a function of time, hydrogen density and X-ray flux. To cover a wide range of physical environments, densities between n_H = 10^4-10^9 cm^-3 and temperatures between T = 10-1000 K are studied. Three different regimes are found: For T water abundance is of order 10^-7-10^-6 and can be somewhat enhanced or reduced due to X-rays, depending on time and density. For 100 K 10^-3 ergs s-1 cm^-2 (t = 10^4 yrs) and for F_X > 10^-4 ergs s^-1 cm^-2 (t = 10^5 yrs). At higher temperatures (T > 250 K) and hydrogen densities, water can persist with x(H2O) ~ 10^-4 even for high X-ray fluxes. The X-ray and FUV models are applied to envelopes around low-mass Class 0 and I young stellar objects (YSOs). Water is destroyed in both Class 0 and I envelopes on relatively short timescales (t ~ 5000 yrs) for realistic X-ray fluxes, although the effect is less prominent in Class 0 envelopes due to the higher X-ray absorbing densities there. FUV photons from the central source are not effective in destroying water. The average water abundance in Class I sources for L_X > 10^27 ergs s^-1 is predicted to be x(H2O) < 10^-6.

P. Stauber; J. K. Jorgensen; E. F. van Dishoeck; S. D. Doty; A. O. Benz

2006-02-06T23:59:59.000Z

398

Area detector corrections for high quality synchrotron X-ray structure factor measurements  

SciTech Connect (OSTI)

Correction procedures for obtaining accurate X-ray structure factors from large area detectors are considered, including subpanel effects, over excited pixels and careful intensity corrections. Problems associated with data normalization, the use of a pixel response correction from a glass standard and minimization of systematic errors are also discussed. Data from glassy GeSe{sub 2} and liquid water measured with a Perkin Elmer amorphous-Silicon detector are used to demonstrate the effectiveness of these correction procedures. This requires reduction of systematic errors in the measured intensity to around the 0.1% level.

Skinner L. B.; Parise J.; Benmore, C.

2011-10-01T23:59:59.000Z

399

X-ray magnetic circular dichroism in (Ge,Mn) compounds: experiments and modeling Samuel Tardif,1, 2,  

E-Print Network [OSTI]

X-ray magnetic circular dichroism in (Ge,Mn) compounds: experiments and modeling Samuel Tardif,1, 2: July 29, 2013) X-ray absorption (XAS) and x-ray magnetic circular dichroism (XMCD) spectra at the L2),6 and x-ray spectroscopy (x-ray absorption spec- troscopy, XAS, and x-ray magnetic circular

400

NuSTAR Observations of X-Ray Binaries  

E-Print Network [OSTI]

As of 2014 August, the Nuclear Spectroscopic Telescope Array (NuSTAR) had observed ~30 X-ray binaries either as part of the planned program, as targets of opportunity, or for instrument calibration. The main science goals for the observations include probing the inner part of the accretion disk and constraining black hole spins via reflection components, providing the first observations of hard X-ray emission from quiescent Low Mass X-ray Binaries (LMXBs), measuring cyclotron lines from accreting pulsars, and studying type I X-ray bursts from neutron stars. Here, we describe the science objectives in more depth and give an overview of the NuSTAR observations that have been carried out to achieve the objectives. These include observation of four "IGR" High Mass X-ray Binaries (HMXBs) discovered by INTEGRAL. We also summarize the results that have been obtained and their implications. Among the IGR HMXBs, we focus on the discovery of a cyclotron line in the spectrum of IGR J17544-2619.

Tomsick, John A; Fuerst, Felix; Harrison, Fiona; Miyasaka, Hiromasa; Tendulkar, Shriharsh; Bhalerao, Varun; Chakrabarty, Deepto; King, Ashley; Miller, Jon M; Natalucci, Lorenzo; Stern, Daniel

2015-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

Optics-free x-ray FEL oscillator  

SciTech Connect (OSTI)

There is a need for an Optics-Free FEL Oscillators (OFFELO) to further the advantages of free-electron lasers and turning them in fully coherent light sources. While SASE (Self-Amplified Spontaneous Emission) FELs demonstrated the capability of providing very high gain and short pulses of radiation and scalability to the X-ray range, the spectra of SASE FELs remains rather wide ({approx}0.5%-1%) compared with typical short wavelengths FEL-oscillators (0.01%-0.0003% in OK-4 FEL). Absence of good optics in VUV and X-ray ranges makes traditional oscillator schemes with very high average and peak spectral brightness either very complex or, strictly speaking, impossible. In this paper, we discuss lattice of the X-ray optics-free FEL oscillator and present results of initial computer simulations of the feedback process and the evolution of FEL spectrum in X-ray OFFELO. We also discuss main limiting factors and feasibility of X-ray OFFELO.

Litvinenko, V.N.; Hao, Y.; Kayran, D.; Trbojevic, D.

2011-03-28T23:59:59.000Z

402

The History of X-ray Free-Electron Lasers  

SciTech Connect (OSTI)

The successful lasing at the SLAC National Accelerator Laboratory of the Linear Coherent Light Source (LCLS), the first X-ray free-electron laser (X-ray FEL), in the wavelength range 1.5 to 15 {angstrom}, pulse duration of 60 to few femtoseconds, number of coherent photons per pulse from 10{sup 13} to 10{sup 11}, is a landmark event in the development of coherent electromagnetic radiation sources. Until now electrons traversing an undulator magnet in a synchrotron radiation storage ring provided the best X-ray sources. The LCLS has set a new standard, with a peak X-ray brightness higher by ten orders of magnitudes and pulse duration shorter by three orders of magnitudes. LCLS opens a new window in the exploration of matter at the atomic and molecular scales of length and time. Taking a motion picture of chemical processes in a few femtoseconds or less, unraveling the structure and dynamics of complex molecular systems, like proteins, are some of the exciting experiments made possible by LCLS and the other X-ray FELs now being built in Europe and Asia. In this paper, we describe the history of the many theoretical, experimental and technological discoveries and innovations, starting from the 1960s and 1970s, leading to the development of LCLS.

Pellegrini, C.; /UCLA /SLAC; ,

2012-06-28T23:59:59.000Z

403

Method and apparatus for micromachining using hard X-rays  

DOE Patents [OSTI]

An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures.

Siddons, David Peter (Shoreham, NY); Johnson, Erik D. (Ridge, NY); Guckel, Henry (Madison, WI); Klein, Jonathan L. (Madison, WI)

1997-10-21T23:59:59.000Z

404

Method and apparatus for micromachining using hard X-rays  

DOE Patents [OSTI]

An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures. 21 figs.

Siddons, D.P.; Johnson, E.D.; Guckel, H.; Klein, J.L.

1997-10-21T23:59:59.000Z

405

High-energy x-ray production with pyroelectric crystals Jeffrey A. Geuthera  

E-Print Network [OSTI]

High-energy x-ray production with pyroelectric crystals Jeffrey A. Geuthera and Yaron Danon, the usefulness of an x-ray source is determined by its yield and endpoint energy. In x-ray fluorescence, for example, high-energy sources enable the excitation of the K-shell x-ray peaks for high-Z materials as well

Danon, Yaron

406

Tools for a Theoretical X-ray Beamline J. J. Rehr*  

E-Print Network [OSTI]

Tools for a Theoretical X-ray Beamline J. J. Rehr* Department of Physics University of Washington, France 22 October 2010 #12;X-ray Spectroscopy Beamline #12;Tools for a Theoretical X-ray Beamline · GOAL Theoretical X-ray Beamline: 2. Tools for EXAFS and XANES, EELS, XMCD, ... 3. DFT/MD-TOOLS 4. Next generation

Botti, Silvana

407

E-Print Network 3.0 - axial x-ray power Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

for: axial x-ray power Page: << < 1 2 3 4 5 > >> 1 Martin Elvis, X-ray & XUV Active Optics, Soleil, 14-15 Dec 2006 Active X-ray OpticsActive X-ray Optics Summary: 1 Martin...

408

Chemical Shifts in X-ray and Photo-Electron Spectroscopy: A Historical review  

E-Print Network [OSTI]

Chemical Shifts in X-ray and Photo-Electron Spectroscopy: A Historical review Ingvar Lindgren 1 Introduction 2 2 Chemical shift in X-ray spectroscopy 2 2.1 Discovery of the chemical shift in X-ray spectroscopy . . . . . . . . . . . . . 3 2.2 Interpretation of the chemical shift in X-ray spectroscopy

Lindgren, Ingvar

409

X-ray Diffraction / MSE 603 Spring 2002 Qun Shen / CHESS qs11@cornell.edu  

E-Print Network [OSTI]

X-ray Diffraction / MSE 603 Spring 2002 Qun Shen / CHESS qs11@cornell.edu 1. X-ray production & basic properties ­ common sources for diffraction experiments ­ synchrotron radiation ­ response to x-rays by an electron ­ refraction index ­ total external reflection & evanescent wave, TXRF 2. X-ray scattering basics

Shen, Qun

410

X-ray Spectroscopy of O Supergiant Winds: Shock Physics, Clumping, and Mass-Loss Rates  

E-Print Network [OSTI]

X-ray Spectroscopy of O Supergiant Winds: Shock Physics, Clumping, and Mass-Loss Rates David Cohen Li (Swarthmore '16), Kelley Langhans (Swarthmore '16) #12;Talk Outline Context of O star X-ray emission: wind shocks 1. X-ray constraints on the shocked wind plasma 2. X-ray absorption as a mass

Cohen, David

411

X-ray spectral diagnostics of neon photoionization experiments on the Z-machine  

E-Print Network [OSTI]

X-ray spectral diagnostics of neon photoionization experiments on the Z-machine David H. Cohen on an initial spectroscopic study of low-density, x-ray photoionized neon with x-ray spectroscopy plasma, and to explore issues related to the rapid x-ray photoionization of relatively cold, low

Cohen, David

412

X-ray absorption anisotropy for polychromatic illumination--Crystal views from inside  

E-Print Network [OSTI]

X-ray absorption anisotropy for polychromatic illumination--Crystal views from inside P. Korecki a Keywords: X-ray absorption Real-space imaging X-ray holography Electron channeling Electron backscatter of the fine structure in X-ray absorption anisotropy, which results from incident beam diffraction

Korecki, Pawe³

413

X-ray emission from clusters of galaxies Craig L. Sarazin  

E-Print Network [OSTI]

X-ray emission from clusters of galaxies Craig L. Sarazin Department of Astronomy, University show that they are bright x-ray sources, with luminosities of 1043 45 ergs/sec. It is now established the stars in all the galaxies in the cluster. The x-ray spectra of clusters show strong x-ray line emission

Sarazin, Craig

414

X-ray four-wave mixing in molecules Satoshi Tanaka  

E-Print Network [OSTI]

X-ray four-wave mixing in molecules Satoshi Tanaka Department of Chemistry, University of Rochester radiation intense light sources have opened up a new era in soft x-ray spectroscopy. The dramatic improvements of spectral resolution in x-ray absorption1,2 and x-ray photoemission spectra3 have revealed

Mukamel, Shaul

415

X-Ray: A Tool for Automatic Measurement of Hardware Parameters  

E-Print Network [OSTI]

X-Ray: A Tool for Automatic Measurement of Hardware Parameters Kamen Yotov, Keshav Pingali, Paul and register tiles. In this paper, we describe X-Ray1 , a system for im- plementing micro-benchmarks to measure. Experimen- tal evaluations of X-Ray on traditional workstations, servers and embedded systems show that X-Ray

Pingali, Keshav K.

416

Quantification of rapid environmental redox processes with quick-scanning x-ray absorption  

E-Print Network [OSTI]

Quantification of rapid environmental redox processes with quick-scanning x-ray absorption. Here we apply quick-scanning x-ray absorption spectroscopy (Q-XAS), at sub-second time that can be measured using x-ray absorption spectroscopy. arsenic extended x-ray absorption fine structure

Sparks, Donald L.

417

ON THE X-RAY OUTBURSTS OF TRANSIENT ANOMALOUS X-RAY PULSARS AND SOFT GAMMA-RAY REPEATERS  

SciTech Connect (OSTI)

We show that the X-ray outburst light curves of four transient anomalous X-ray pulsars (AXPs) and soft gamma-ray repeaters (SGRs), namely, XTE J1810-197, SGR 0501+4516, SGR 1627-41, and CXOU J164710.2-455216, can be produced by the fallback disk model that was also applied to the outburst light curves of persistent AXPs and SGRs in our earlier work. The model solves the diffusion equation for the relaxation of a disk that has been pushed back by a soft gamma-ray burst. The sets of main disk parameters used for these transient sources are very similar to each other and to those employed in our earlier models of persistent AXPs and SGRs. There is a characteristic difference between the X-ray outburst light curves of transient and persistent sources. This can be explained by the differences in the disk surface density profiles of the transient and persistent sources in quiescence indicated by their quiescent X-ray luminosities. Our results imply that a viscous disk instability operating at a critical temperature in the range of {approx}1300-2800 K is a common property of all fallback disks around AXPs and SGRs. The effect of the instability is more pronounced and starts earlier for the sources with lower quiescent luminosities, which leads to the observable differences in the X-ray enhancement light curves of transient and persistent sources. A single active disk model with the same basic disk parameters can account for the enhancement phases of both transient and persistent AXPs and SGRs. We also present a detailed parameter study to show the effects of disk parameters on the evolution of the X-ray luminosity of AXPs and SGRs in the X-ray enhancement phases.

Cal Latin-Small-Letter-Dotless-I skan, Sirin; Ertan, Uenal [Sabanc Latin-Small-Letter-Dotless-I University, Orhanl Latin-Small-Letter-Dotless-I -Tuzla, Istanbul, 34956 (Turkey)

2012-10-20T23:59:59.000Z

418

X-ray absorption signatures of the molecular environment in water and ice  

E-Print Network [OSTI]

The x-ray absorption spectra of water and ice are calculated with a many-body approach for electron-hole excitations. The experimental features, including the small effects of temperature change in the liquid, are quantitatively reproduced from molecular configurations generated by ab-initio molecular dynamics. The spectral difference between the solid and the liquid is due to two major short range order effects. One, due to breaking of hydrogen bonds, enhances the pre-edge intensity in the liquid. The other, due to a non-bonded molecular fraction in the first coordination shell, affects the main spectral edge in the conversion of ice to water. This effect may not involve hydrogen bond breaking as shown by experiment in high-density amorphous ice.

Wei Chen; Xifan Wu; Roberto Car

2009-09-21T23:59:59.000Z

419

Sum frequency generation study on the orientation of room-temperature ionic liquid at the grapheneionic liquid interface  

E-Print Network [OSTI]

such as dye-sensitized solar cells and super capacitors, room-temperature ionic liquids are considered

Bao, Jiming

420

Quantized hard-x-ray phase vortices nucleated by aberrated nanolenses  

SciTech Connect (OSTI)

Quantized x-ray phase vortices, namely, screw-type topological defects in the wave fronts of a coherent monochromatic scalar x-ray wave field, may be spontaneously nucleated by x-ray lenses. Phase retrieval is used to reconstruct the phase and amplitude of the complex disturbance created by aberrated gold nanolenses illuminated with hard x rays. A nanoscale quantized x-ray vortex-antivortex dipole is observed, manifest both as a pair of opposite-helicity branch points in the Riemann sheets of the multivalued x-ray phase map of the complex x-ray field and in the vorticity of the associated Poynting vector field.

Pavlov, Konstantin M. [School of Science and Technology, University of New England, Armidale, New South Wales 2351 (Australia); School of Physics, Monash University, Victoria 3800 (Australia); Paganin, David M. [School of Physics, Monash University, Victoria 3800 (Australia); Vine, David J. [ARC Centre of Excellence for Coherent X-ray Science, School of Physics, The University of Melbourne, Parkville, Victoria 3010 (Australia); Schmalz, Jelena A. [School of Science and Technology, University of New England, Armidale, New South Wales 2351 (Australia); Suzuki, Yoshio; Uesugi, Kentaro; Takeuchi, Akihisa; Yagi, Naoto [SPring-8/JASRI (Japan Synchrotron Radiation Research Institute), Hyogo 679-5198 (Japan); Kharchenko, Alexander; Blaj, Gabriel [PANalytical B.V., P.O. Box 13, 7600 AA Almelo (Netherlands); Jakubek, Jan [Institute of Experimental and Applied Physics, Czech Technical University in Prague, 166 36 Prague 6 (Czech Republic); Altissimo, Matteo [Melbourne Centre for Nanofabrication, 151 Wellington Road, Clayton, Victoria 3168 (Australia); Materials Science and Engineering, Commonwealth Scientific and Industrial Research Organisation, Clayton South, Victoria 3169 (Australia); Clark, Jesse N. [London Centre for Nanotechnology, University College, Gower St, London WC1E 6BT (United Kingdom)

2011-01-15T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

Theory of angular dispersive imaging hard x-ray spectrographs  

E-Print Network [OSTI]

A spectrograph is an optical instrument that disperses photons of different energies into distinct directions and space locations, and images photon spectra on a position-sensitive detector. Spectrographs consist of collimating, angular dispersive, and focusing optical elements. Bragg reflecting crystals arranged in an asymmetric scattering geometry are used as the dispersing elements. A ray-transfer matrix technique is applied to propagate x-rays through the optical elements. Several optical designs of hard x-ray spectrographs are proposed and their performance is analyzed. Spectrographs with an energy resolution of 0.1 meV and a spectral window of imaging up to a few tens of meVs are shown to be feasible for inelastic x-ray scattering (IXS) spectroscopy applications. In another example, a spectrograph with a 1-meV spectral resolution and 85-meV spectral window of imaging is considered for Cu K-edge resonant IXS (RIXS).

Shvyd'ko, Yuri

2015-01-01T23:59:59.000Z

422

The Large Observatory For X-ray Timing: LOFT  

E-Print Network [OSTI]

LOFT, the Large Observatory for X-ray Timing, is a new space mission concept devoted to observations of Galactic and extra-Galactic sources in the X-ray domain with the main goals of probing gravity theory in the very strong field environment of black holes and other compact objects, and investigating the state of matter at supra-nuclear densities in neutron stars. The instruments on-board LOFT, the Large area detector and the Wide Field Monitor combine for the first time an unprecedented large effective area (~10 m2 at 8 keV) sensitive to X-ray photons mainly in the 2-30 keV energy range and a spectral resolution approaching that of CCD-based telescopes (down to 200 eV at 6 keV). LOFT is currently competing for a launch of opportunity in 2022 together with the other M3 mission candidates of the ESA Cosmic Vision Program.

Bozzo, E

2013-01-01T23:59:59.000Z

423

X-ray microscope assemblies. Final report and metrology report  

SciTech Connect (OSTI)

This is the Final Report and Metrology Report prepared under Lawrence Livermore Laboratory Subcontract 9936205, X-ray Microscope Assemblies. The purpose of this program was to design, fabricate, and perform detailed metrology on an axisymmetric grazing-incidence x-ray microscope (XRMS) to be used as a diagnostic instrument in the Lawrence Livermore Laser Fusion Program. The optical configuration chosen for this device consists of two internally polished surfaces of revolution: an hyperboloid facing the object; and a confocal, co-axial elliposid facing the image. This arrangement is known as the Wolter Type-I configuration. The grazing angle of reflection for both surfaces is approximately 1/sup 0/. The general optical performance goals under this program were to achieve a spatial resolution in the object plane in the soft x-ray region of approximately 1 micron, and to achieve an effective solid collecting angle which is an appreciable fraction of the geometric solid collecting angle.

Zehnpfennig, T.F.

1981-04-13T23:59:59.000Z

424

Imaging X-ray Thomson Scattering Spectrometer Design and Demonstration  

SciTech Connect (OSTI)

In many laboratory astrophysics experiments, intense laser irradiation creates novel material conditions with large, one-dimensional gradients in the temperature, density, and ionization state. X-ray Thomson scattering is a powerful technique for measuring these plasma parameters. However, the scattered signal has previously been measured with little or no spatial resolution, which limits the ability to diagnose inhomogeneous plasmas. We report on the development of a new imaging x-ray Thomson spectrometer (IXTS) for the Omega laser facility. The diffraction of x-rays from a toroidally-curved crystal creates high-resolution images that are spatially resolved along a one-dimensional profile while spectrally dispersing the radiation. This focusing geometry allows for high brightness while localizing noise sources and improving the linearity of the dispersion. Preliminary results are presented from a scattering experiment that used the IXTS to measure the temperature profile of a shocked carbon foam.

Gamboa, E.J. [University of Michigan; Huntington, C.M. [University of Michigan; Trantham, M.R. [University of Michigan; Keiter, P.A [University of Michigan; Drake, R.P. [University of Michigan; Montgomery, David [Los Alamos National Laboratory; Benage, John F. [Los Alamos National Laboratory; Letzring, Samuel A. [Los Alamos National Laboratory

2012-05-04T23:59:59.000Z

425

Quiescent X-ray emission from an evolved brown dwarf ?  

E-Print Network [OSTI]

I report on the X-ray detection of Gl569Bab. During a 25ksec Chandra observation the binary brown dwarf is for the first time spatially separated in X-rays from the flare star primary Gl569A. Companionship to Gl569A constrains the age of the brown dwarf pair to ~300-800 Myr. The observation presented here is only the second X-ray detection of an evolved brown dwarf. About half of the observing time is dominated by a large flare on Gl569Bab, the remainder is characterized by weak and non-variable emission just above the detection limit. This emission -- if not related to the afterglow of the flare -- represents the first detection of a quiescent corona on a brown dwarf, representing an important piece in the puzzle of dynamos in the sub-stellar regime.

B. Stelzer

2004-09-27T23:59:59.000Z

426

Data fusion in neutron and X-ray computed tomography  

SciTech Connect (OSTI)

We present a fusion methodology between neutron and X-ray computed tomography (CT). On the one hand, the inspection by X-ray CT of a wide class of multimaterials in non-destructive testing applications suffers from limited information of object features. On the other hand, neutron imaging can provide complementary data in such a way that the combination of both data sets fully characterizes the object. In this contribution, a novel data fusion procedure, called Fusion Regularized Simultaneous Algebraic Reconstruction Technique, is developed where the X-ray reconstruction is modified to fulfill the available data from the imaging with neutrons. The experiments, which were obtained from an aluminum profile containing a steel screw, and attached carbon fiber plates demonstrate that the image quality in CT can be significantly improved when the proposed fusion method is used.

Schrapp, Michael J. [Siemens AG, Corporate Technology, Otto-Hahn-Ring 6, 81739 Munich (Germany); Physik Department E21, Technische Universität München, James-Franck-Strasse 1, 85747 Garching (Germany); Goldammer, Matthias [Siemens AG, Corporate Technology, Otto-Hahn-Ring 6, 81739 Munich (Germany); Schulz, Michael [Physik Department E21, Technische Universität München, James-Franck-Strasse 1, 85747 Garching (Germany); Heinz Maier-Leibnitz Zentrum (MLZ), Technische Universität München, Lichtenbergstrasse 1, 85747 Garching (Germany); Issani, Siraj; Bhamidipati, Suryanarayana [Siemens AG, Corporate Technology, Bangalore (India); Böni, Peter [Physik Department E21, Technische Universität München, James-Franck-Strasse 1, 85747 Garching (Germany)

2014-10-28T23:59:59.000Z

427

Movable anode x-ray source with enhanced anode cooling  

DOE Patents [OSTI]

An x-ray source is disclosed having a cathode and a disc-shaped anode with a peripheral surface at constant radius from the anode axis opposed to the cathode. The anode has stub axle sections rotatably carried in heat conducting bearing plates which are mounted by thermoelectric coolers to bellows which normally bias the bearing plates to a retracted position spaced from opposing anode side faces. The bellows cooperate with the x-ray source mounting structure for forming closed passages for heat transport fluid. Flow of such fluid under pressure expands the bellows and brings the bearing plates into heat conducting contact with the anode side faces. A worm gear is mounted on a shaft and engages serrations in the anode periphery for rotating the anode when flow of coolant is terminated between x-ray emission events. 5 figs.

Bird, C.R.; Rockett, P.D.

1987-08-04T23:59:59.000Z

428

Eta Car and Its Surroundings: the X-ray Diagnosis  

E-Print Network [OSTI]

X-ray emission from the supermassive star Eta Carinae (\\ec) originates from hot shocked gas produced by current stellar mass loss as well as ejecta from prior eruptive events. Absorption of this emission by cool material allows the determination of the spatial and temporal distribution of this material. Emission from the shocked gas can provide important information about abundances through the study of thermal X-ray line emission. We discuss how studies of the X-ray emission from Eta Car at a variety of temporal, spatial and spectral scales and resolutions have helped refine our knowledge of both the continuous and discrete mass loss from the system, and its interactions with more extended material around the star.

M. F. Corcoran; K. Hamaguchi

2007-03-02T23:59:59.000Z

429

Portable X-Ray, K-Edge Heavy Metal Detector  

SciTech Connect (OSTI)

The X-Ray, K-Edge Heavy Metal Detection System was designed and built by Ames Laboratory and the Center for Nondestructive Evaluation at Iowa State University. The system uses a C-frame inspection head with an X-ray tube mounted on one side of the frame and an imaging unit and a high purity germanium detector on the other side. the inspection head is portable and can be easily positioned around ventilation ducts and pipes up to 36 inches in diameter. Wide angle and narrow beam X-ray shots are used to identify the type of holdup material and the amount of the contaminant. Precise assay data can be obtained within minutes of the interrogation. A profile of the containerized holdup material and a permanent record of the measurement are immediately available.

Fricke, V.

1999-10-25T23:59:59.000Z

430

X-ray radiography with highly charged ions  

DOE Patents [OSTI]

An extremely small (1-250 micron FWHM) beam of slow highly charged ions deexciting on an x-ray production target generates x-ray monochromatic radiation that is passed through a specimen and detected for imaging. The resolution of the x-ray radiograms is improved and such detection is achieved with relatively low dosages of radiation passing through the specimen. An apparatus containing an electron beam ion trap (and modifications thereof) equipped with a focusing column serves as a source of ions that generate radiation projected onto an image detector. Electronic and other detectors are able to detect an increased amount of radiation per pixel than achieved by previous methods and apparati.

Marrs, Roscoe E. (Livermore, CA)

2000-01-01T23:59:59.000Z

431

Biological imaging by soft x-ray diffraction microscopy  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

We have used the method of x-ray diffraction microscopy to image the complex-valued exit wave of an intact and unstained yeast cell. The images of the freeze-dried cell, obtained by using 750-eV x-rays from different angular orientations, portray several of the cell's major internal components to 30-nm resolution. The good agreement among the independently recovered structures demonstrates the accuracy of the imaging technique. To obtain the best possible reconstructions, we have implemented procedures for handling noisy and incomplete diffraction data, and we propose a method for determining the reconstructed resolution. This work represents a previously uncharacterized application of x-ray diffraction microscopy to a specimen of this complexity and provides confidence in the feasibility of the ultimate goal of imaging biological specimens at 10-nm resolution in three dimensions.

Shapiro, D.; Thibault, P.; Beetz, T.; Elser, V.; Howells, M.; Jacobsen, C.; Kirz, J.; Lima, E.; Miao, H.; Neiman, A. M.; Sayre, D.

2005-10-25T23:59:59.000Z

432

Gas Bubbles and Gas Pancakes at Liquid/Solid Interface: A Continuum Theory Incorporated with Molecular Interactions  

E-Print Network [OSTI]

The states of gas accumulated at the liquid-solid interface are analyzed based on the continuum theory where the Hamaker constant is used to describe the long-range interaction at the microscopic scale. The Hamaker constant is always negative, whereas the gas spreading coefficient can be either sign. Despite the complexity of gas, including that the density profile may not be uniform due to absorption on both solid and liquid surfaces, we predict three possible gas states at the liquid-solid interface, i.e. complete wetting, partial wetting and pseudopartial wetting. These possible gas states correspond respectively to a gas pancake (or film) surrounded by a wet solid, a gas bubble with a finite contact angle, and a gas bubble(s) coexisting with a gas pancake. Typical thickness of the gas pancakes is at the nanoscale within the force range of the long-range interaction, whereas the radius of the gas bubbles can be large. The state of gas bubble(s) coexisting with a gas film is predicted theoretically for the first time. Our theoretical results can contribute to the development of a unified picture of gas nucleation at the liquid-solid interface.

Zhaoxia Li; Xuehua Zhang; Lijuan Zhang; Xiaocheng Zeng; Jun Hu; Haiping Fang

2007-10-27T23:59:59.000Z

433

X-RAY BINARY EVOLUTION ACROSS COSMIC TIME  

SciTech Connect (OSTI)

High-redshift galaxies permit the study of the formation and evolution of X-ray binary (XRB) populations on cosmological timescales, probing a wide range of metallicities and star formation rates (SFRs). In this paper, we present results from a large-scale population synthesis study that models the XRB populations from the first galaxies of the universe until today. We use as input to our modeling the Millennium II cosmological simulation and the updated semi-analytic galaxy catalog by Guo et al. to self-consistently account for the star formation history and metallicity evolution of the universe. Our modeling, which is constrained by the observed X-ray properties of local galaxies, gives predictions about the global scaling of emission from XRB populations with properties such as SFR and stellar mass, and the evolution of these relations with redshift. Our simulations show that the X-ray luminosity density (X-ray luminosity per unit volume) from XRBs in our universe today is dominated by low-mass XRBs, and it is only at z {approx}> 2.5 that high-mass XRBs become dominant. We also find that there is a delay of {approx}1.1 Gyr between the peak of X-ray emissivity from low-mass XRBs (at z {approx} 2.1) and the peak of SFR density (at z {approx} 3.1). The peak of the X-ray luminosity from high-mass XRBs (at z {approx} 3.9) happens {approx}0.8 Gyr before the peak of the SFR density, which is due to the metallicity evolution of the universe.

Fragos, T.; Zezas, A. [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States)] [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Lehmer, B.; Tzanavaris, P. [Department of Physics and Astronomy, The Johns Hopkins University, Homewood Campus, Baltimore, MD 21218 (United States)] [Department of Physics and Astronomy, The Johns Hopkins University, Homewood Campus, Baltimore, MD 21218 (United States); Tremmel, M. [Department of Astronomy, University of Washington, Box 351580, U.W., Seattle, WA 98195-1580 (United States)] [Department of Astronomy, University of Washington, Box 351580, U.W., Seattle, WA 98195-1580 (United States); Basu-Zych, A.; Hornschemeier, A.; Jenkins, L.; Ptak, A. [NASA Goddard Space Flight Centre, Code 662, Greenbelt, MD 20771 (United States)] [NASA Goddard Space Flight Centre, Code 662, Greenbelt, MD 20771 (United States); Belczynski, K. [Astronomical Observatory, University of Warsaw, Al. Ujazdowskie 4, 00-478 Warsaw (Poland)] [Astronomical Observatory, University of Warsaw, Al. Ujazdowskie 4, 00-478 Warsaw (Poland); Kalogera, V., E-mail: tfragos@cfa.harvard.edu [Department of Physics and Astronomy, Northwestern University, 2145 Sheridan Road, Evanston, IL 60208 (United States)

2013-02-10T23:59:59.000Z

434

High-resolution X-ray spectroscopy of Theta Car  

E-Print Network [OSTI]

Context : The peculiar hot star Theta Car in the open cluster IC2602 is a blue straggler as well as a single-line binary of short period (2.2d). Aims : Its high-energy properties are not well known, though X-rays can provide useful constraints on the energetic processes at work in binaries as well as in peculiar, single objects. Methods : We present the analysis of a 50ks exposure taken with the XMM-Newton observatory. It provides medium as well as high-resolution spectroscopy. Results : Our high-resolution spectroscopy analysis reveals a very soft spectrum with multiple temperature components (1--6MK) and an X-ray flux slightly below the `canonical' value (log[L_X(0.1-10.)/L_{BOL}] ~ -7). The X-ray lines appear surprisingly narrow and unshifted, reminiscent of those of beta Cru and tau Sco. Their relative intensities confirm the anomalous abundances detected in the optical domain (C strongly depleted, N strongly enriched, O slightly depleted). In addition, the X-ray data favor a slight depletion in neon and iron, but they are less conclusive for the magnesium abundance (solar-like?). While no significant changes occur during the XMM-Newton observation, variability in the X-ray domain is detected on the long-term range. The formation radius of the X-ray emission is loosely constrained to <5 R_sol, which allows for a range of models (wind-shock, corona, magnetic confinement,...) though not all of them can be reconciled with the softness of the spectrum and the narrowness of the lines.

Yael Naze; Gregor Rauw

2008-08-25T23:59:59.000Z

435

Advances in the Detection of As in Environmental Samples Using Low Energy X-ray Fluorescence in a Scanning Transmission X-ray  

E-Print Network [OSTI]

X-ray emission (PIXE),4 or energy dispersive X-ray (EDX) spectrometry in scanning or transmission XAdvances in the Detection of As in Environmental Samples Using Low Energy X-ray Fluorescence at high spatial resolution is needed in many areas of geobiochemistry and environmental science. Scanning

Hitchcock, Adam P.

436

Advances in X-Ray Chemical Analysis, Japan, 45 (2014) ISSN 0911-7806 Report on 10th Chinese X-Ray Spectrometry Conference (CXRSC)  

E-Print Network [OSTI]

and Information Technology), Dr. Yidong Zhao (Institute of High Energy Physics of Chinese Academy of Sciences-Ray Spectrometry Conference (CXRSC) Ying LIU #12;#12;45 345 Report on 10th Chinese X-Ray Spectrometry Conference (CXRSC) Adv. X-Ray. Chem. Anal., Japan 45, pp.345-348 (2014) Report on 10th Chinese X-Ray Spectrometry

Jun, Kawai

437

Probing stellar winds and accretion physics in high-mass X-ray binaries and ultra-luminous X-ray sources with LOFT  

E-Print Network [OSTI]

This is a White Paper in support of the mission concept of the Large Observatory for X-ray Timing (LOFT), proposed as a medium-sized ESA mission. We discuss the potential of LOFT for the study of high-mass X-ray binaries and ultra-luminous X-ray sources. For a summary, we refer to the paper.

Orlandini, M; Zampieri, L; Bozzo, E; Baykal, A; Blay, P; Chernyakova, M; Corbet, R; D'Aì, A; Enoto, T; Ferrigno, C; Finger, M; Klochkov, D; Kreykenbohm, I; Inam, S C; Jenke, P; Masetti, N; Manousakis, A; Mihara, T; Paul, B; Postnov, K; Reig, P; Romano, P; Santangelo, A; Shakura, N; Staubert, R; Torrejón, J M; Walter, R; Wilms, J; Wilson-Hodge, C

2015-01-01T23:59:59.000Z

438

The NIF x-ray spectrometer calibration campaign at Omega  

SciTech Connect (OSTI)

The calibration campaign of the National Ignition Facility X-ray Spectrometer (NXS) was carried out at the OMEGA laser facility. Spherically symmetric, laser-driven, millimeter-scale x-ray sources of K-shell and L-shell emission from various mid-Z elements were designed for the 2–18 keV energy range of the NXS. The absolute spectral brightness was measured by two calibrated spectrometers. We compare the measured performance of the target design to radiation hydrodynamics simulations.

Pérez, F.; Kemp, G. E.; Barrios, M. A.; Pino, J.; Scott, H.; Ayers, S.; Chen, H.; Emig, J.; Colvin, J. D.; Fournier, K. B., E-mail: fournier2@llnl.gov [Lawrence Livermore National Laboratory, P. O. Box 808, Livermore, California 94551 (United States); Regan, S. P.; Bedzyk, M.; Shoup, M. J.; Agliata, A.; Yaakobi, B.; Marshall, F. J.; Hamilton, R. A. [Laboratory for Laser Energetics, University of Rochester, Rochester, New York 14623 (United States); Jaquez, J.; Farrell, M.; Nikroo, A. [General Atomics, P.O. Box 85608, San Diego, California 92186 (United States)

2014-11-15T23:59:59.000Z

439

X-Ray Binary Systems in the Small Magellanic Cloud  

E-Print Network [OSTI]

We present the result of a systematic search for spectrally hard and soft X-ray binary systems in the Small Magellanic Cloud (SMC). This search has been applied to ROSAT PSPC data (0.1-2.4 keV) collected during 9 pointed observations towards this galaxy covering a time span of 2 years from October 91 till October 93. Selection criteria have been defined in order to confine the sample of candidates. Finally 7 spectrally hard and 4 spectrally soft sources were selected from the list as candidates for binaries in the SMC. The sample is luminosity limited (>3.10**35 erg/s). SMC X-1 has been observed during a full binary orbit starting with a low-state covering an X-ray eclipse and emerging into a bright long-duration flare with two short-duration flares separated by 10 hours. The Be type transient SMC X-2 has been redetected with ROSAT. Variability has been found in the sources RX J0051.8-7231 and RX J0052.1-731 already discovered with Einstein. RX J0101.0-7206 has been discovered at the north-eastern boundary of the giant SMC HII region N66 during an X-ray outburst and half a year later during a quiescent phase. A variable source, RX J0049.1-7250, located north-east of the SMC supernova remnant N19 and which may either be an X-ray binary or an AGN turns out to be strongly absorbed. It may be located behind the SMC. If it is an X-ray binary then it radiates at the Eddington limit in the X-ray bright state. Another variable and hard X-ray source RX J0032.9-7348 has been discovered at the south-eastern border of the body of the SMC. A high mass X-ray binary nature is favored for this source. We searched for CAL87 like systems in the SMC catalog and found none. A new candidate supersoft source RX J0103.8-7254 has been detected. We cannot exclude that it is a foreground object.

P. Kahabka; W. Pietsch

1997-06-09T23:59:59.000Z

440

The dominant X-ray wind in massive star binaries  

E-Print Network [OSTI]

We investigate which shocked wind is responsible for the majority of the X-ray emission in colliding wind binaries, an issue where there is some confusion in the literature, and which we show is more complicated than has been assumed. We find that where both winds rapidly cool (typically close binaries), the ratio of the wind speeds is often more important than the momentum ratio, because it controls the energy flux ratio, and the faster wind is generally the dominant emitter. When both winds are largely adiabatic (typically long-period binaries), the slower and denser wind will cool faster and the stronger wind generally dominates the X-ray luminosity.

J. M. Pittard; I. R. Stevens

2002-04-15T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


441

Optimized Volumetric Scanning for X-Ray Array Sources  

SciTech Connect (OSTI)

Non-destructive evaluation (NDE) is the science and technology of determining non-invasively the internal structure of manufactured parts, objects, and materials. NDE application areas include medicine, industrial manufacturing, military, homeland security, and airport luggage screening. X-ray measurement systems are most widely used because of their ability to image through a wide range of material densities (from human tissue in medical applications to the dense materials of weapon components). Traditional x-ray systems involve a single source and detector system that rotate and/or translate about the object under evaluation. At each angular location, the source projects x-rays through the object. The rays undergo attenuation proportional to the density of the object's constitutive material. The detector records a measure of the attenuation. Mathematical algorithms are used to invert the forward attenuated ray projection process to form images of the object. This is known as computed tomography (CT). In recent years, the single-source x-ray NDE systems have been generalized to arrays of x-ray sources. Array sources permit multiple views of the object with fewer rotations and translations of the source/detector system. The spatially diverse nature of x-ray array sources has the potential of reducing data collection time, reducing imaging artifacts, and increasing the resolution of the resultant images. Most of the existing CT algorithms were not derived from array source models with a spatially diverse set of viewing perspectives. Single-source x-ray CT data collection, processing, and imaging methods and algorithms are not applicable when the source location is expanded from one dimension (a rotating and/or translating point source) to two (a rotating and/or translating array). They must be reformulated. The goal of this project is to determine the applicability of x-ray array sources to problems of interest to LLNL and its customers. It is believed array source data collection will be faster while yielding higher resolution reconstructions with fewer artifacts. There are three tasks in the research: (1) Develop forward array source analytic and computational models; (2) Research and develop array source reconstruction algorithms; and (3) Perform experiments.

Lehman, S K; Foudray, A M; Wang, A; Kallman, J S; Martz, H

2009-09-29T23:59:59.000Z

442

Confusion of Diffuse Objects in the X-ray Sky  

E-Print Network [OSTI]

Most of the baryons in the present-day universe are thought to reside in intergalactic space at temperatures of 10^5-10^7 K. X-ray emission from these baryons contributes a modest (~10%) fraction of the ~ 1 keV background whose prominence within the large-scale cosmic web depends on the amount of non-gravitational energy injected into intergalactic space by supernovae and AGNs. Here we show that the virialized regions of groups and clusters cover over a third of the sky, creating a source-confusion problem that may hinder X-ray searches for individual intercluster filaments and contaminate observations of distant groups.

G. Mark Voit; August E. Evrard; Greg L. Bryan

2000-12-08T23:59:59.000Z

443

Bragg x-ray survey spectrometer for ITER  

SciTech Connect (OSTI)

Several potential impurity ions in the ITER plasmas will lead to loss of confined energy through line and continuum emission. For real time monitoring of impurities, a seven channel Bragg x-ray spectrometer (XRCS survey) is considered. This paper presents design and analysis of the spectrometer, including x-ray tracing by the Shadow-XOP code, sensitivity calculations for reference H-mode plasma and neutronics assessment. The XRCS survey performance analysis shows that the ITER measurement requirements of impurity monitoring in 10 ms integration time at the minimum levels for low-Z to high-Z impurity ions can largely be met.

Varshney, S. K.; Jakhar, S. [ITER-India, Institute for Plasma Research, Bhat, Gandhinagar, Gujarat 382428 (India); Barnsley, R. [ITER Organization, Route de Vinon sur Verdon, 13115 Saint Paul Lez Durance (France); O'Mullane, M. G. [Department of Physics, University of Strathclyde, Glasgow G4 0NG (United Kingdom)

2012-10-15T23:59:59.000Z

444

High resolution collimator system for X-ray detector  

DOE Patents [OSTI]

High resolution in an X-ray computerized tomography (CT) inspection system is achieved by using a collimator/detector combination to limit the beam width of the X-ray beam incident on a detector element to the desired resolution width. In a detector such as a high pressure Xenon detector array, a narrow tapered collimator is provided above a wide detector element. The collimator slits have any desired width, as small as a few mils at the top, the slit width is easily controlled, and they are fabricated on standard machines. The slit length determines the slice thickness of the CT image.

Eberhard, Jeffrey W. (Schenectady, NY); Cain, Dallas E. (Scotia, NY)

1987-01-01T23:59:59.000Z

445

High-resolution radio observations of X-ray binaries  

E-Print Network [OSTI]

I present an overview of important results obtained using high-resolution very long baseline interferometry (VLBI) observations of X-ray binary systems. These results derive from both astrometric observations and resolved imaging of sources, from black holes to neutron star and even white dwarf systems. I outline a number of upcoming developments in instrumentation, both new facilities and ongoing upgrades to existing VLBI instruments, and I conclude by identifying a number of important areas of investigation where VLBI will be crucial in advancing our understanding of X-ray binaries.

James Miller-Jones

2008-09-15T23:59:59.000Z

446

X-ray Absorption Measurements on Nickel Cathode of Sodium-beta Alumina batteries: Fe-Ni-CI Chemical Associations  

SciTech Connect (OSTI)

Sections of Na-Al-NiCl2 cathodes from sodium-beta alumina ZEBRA batteries have been characterized with X-ray fluorescence mapping, and XANES measurements to probe the microstructure, elemental correlation, and chemical speciation after voltage cycling. Cycling was performed under identical load conditions at either 240 or 280 °C operating temperature and subsequently quenched in either the charged or discharged state. X-ray fluorescence mapping and XANES measurements were made adjacent to the current collector and ?"-Al2O3 solid electrolyte interfaces to detect possible gradients in chemical properties across the cathode. An FeS additive, introduced during battery synthesis, was found to be present as either Fe metal or an Fe(II) chloride in all cathode samples. X-ray fluorescence mapping reveals an operating temperature and charge-state dependent spatial correlation between Fe, Ni, and Cl concentration. XANES measurements indicate that both Ni and Fe are chemically reactive and shift between metallic and chloride phases in the charged and discharged states, respectively. However the percentage of chemically active Ni and Fe is significantly less in the cell operated at lower temperature. Additionally, the cathode appeared chemically homogeneous at the scale of our X-ray measurements.

Bowden, Mark E.; Alvine, Kyle J.; Fulton, John L.; Lemmon, John P.; Lu, Xiaochuan; Webb-Robertson, Bobbie-Jo M.; Heald, Steve M.; Balasubramanian, Mahalingam; Mortensen, Devon R.; Seidler, Gerald T.; Hess, Nancy J.

2014-02-01T23:59:59.000Z

447

Structure of gas-liquid interface and hydrophobic interface for urea aqueous solution: a computer simulation study  

E-Print Network [OSTI]

near the interfacial areas are analyzed in terms of density, orientation and number of hydrogen bonds. For each kind of interface, systems with four different urea concentrations are included, ranging from 0M to 8M. The results show slight change...

Yu, Meng

2009-05-15T23:59:59.000Z

448

THE X-RAY BINARY POPULATION IN M33. II. X-RAY SPECTRA AND VARIABILITY H.-J. Grimm, J. McDowell, A. Zezas, D.-W. Kim, and G. Fabbiano  

E-Print Network [OSTI]

THE X-RAY BINARY POPULATION IN M33. II. X-RAY SPECTRA AND VARIABILITY H.-J. Grimm, J. McDowell, A the X-ray spectra and X-ray spectral variability of compact X-ray sources for 3 Chandra observations observations shows that X-ray absorption values are consistent with Galactic X-ray binaries and most sources

Kim, Dong-Woo

449

Modification of the TASMIP x-ray spectral model for the simulation of microfocus x-ray sources  

SciTech Connect (OSTI)

Purpose: The availability of accurate and simple models for the estimation of x-ray spectra is of great importance for system simulation, optimization, or inclusion of photon energy information into data processing. There is a variety of publicly available tools for estimation of x-ray spectra in radiology and mammography. However, most of these models cannot be used directly for modeling microfocus x-ray sources due to differences in inherent filtration, energy range and/or anode material. For this reason the authors propose in this work a new model for the simulation of microfocus spectra based on existing models for mammography and radiology, modified to compensate for the effects of inherent filtration and energy range. Methods: The authors used the radiology and mammography versions of an existing empirical model [tungsten anode spectral model interpolating polynomials (TASMIP)] as the basis of the microfocus model. First, the authors estimated the inherent filtration included in the radiology model by comparing the shape of the spectra with spectra from the mammography model. Afterwards, the authors built a unified spectra dataset by combining both models and, finally, they estimated the parameters of the new version of TASMIP for microfocus sources by calibrating against experimental exposure data from a microfocus x-ray source. The model was validated by comparing estimated and experimental exposure and attenuation data for different attenuating materials and x-ray beam peak energy values, using two different x-ray tubes. Results: Inherent filtration for the radiology spectra from TASMIP was found to be equivalent to 1.68 mm Al, as compared to spectra obtained from the mammography model. To match the experimentally measured exposure data the combined dataset required to apply a negative filtration of about 0.21 mm Al and an anode roughness of 0.003 mm W. The validation of the model against real acquired data showed errors in exposure and attenuation in line with those reported for other models for radiology or mammography. Conclusions: A new version of the TASMIP model for the estimation of x-ray spectra in microfocus x-ray sources has been developed and validated experimentally. Similarly to other versions of TASMIP, the estimation of spectra is very simple, involving only the evaluation of polynomial expressions.

Sisniega, A.; Vaquero, J. J., E-mail: juanjose.vaquero@uc3m.es [Departamento de Bioingeniería e Ingeniería Aeroespacial, Universidad Carlos III de Madrid, Madrid ES28911 (Spain); Instituto de Investigación Sanitaria Gregorio Marañón, Madrid ES28007 (Spain); Desco, M. [Departamento de Bioingeniería e Ingeniería Aeroespacial, Universidad Carlos III de Madrid, Madrid ES28911 (Spain) [Departamento de Bioingeniería e Ingeniería Aeroespacial, Universidad Carlos III de Madrid, Madrid ES28911 (Spain); Instituto de Investigación Sanitaria Gregorio Marañón, Madrid ES28007 (Spain); Centro de Investigación Biomédica en Red de Salud Mental (CIBERSAM), Madrid ES28029 (Spain)

2014-01-15T23:59:59.000Z

450

LIQUID CRYSTAL THERMOGRAPHY ON THE FLUID SOLID INTERFACE OF ROTATING SYSTEMS  

E-Print Network [OSTI]

= Aluminum c = centrifugal lc = liquid crystal o = aerodynamic wall friction related p = at constant pressu

Camci, Cengiz

451

Compact X-ray Light Source Workshop Report  

SciTech Connect (OSTI)

This report, produced jointly by EMSL and FCSD, is the result of a workshop held in September 2011 that examined the utility of a compact x-ray light source (CXLS) in addressing many scientific challenges critical to advancing energy science and technology.

Thevuthasan, Suntharampillai; Evans, James E.; Terminello, Louis J.; Koppenaal, David W.; Manke, Kristin L.; Plata, Charity

2012-12-01T23:59:59.000Z

452

Radioactivity and X-rays Applications and health effects  

E-Print Network [OSTI]

as the release of radioactivity from reactor accidents and fallout from nuclear explosions in the atmosphereRadioactivity and X-rays Applications and health effects by Thormod Henriksen #12;Preface ­ 7 Chapter 2. What is radioactivity page 8 ­ 27 Chapter 3. Radioactive decay laws page 28 ­ 35

Sahay, Sundeep

453

The Evolution of Coronal X-ray Emission  

E-Print Network [OSTI]

as a hydrogen burning star. Rocks were present in the solar system at 1 Myr, the giant planets formed within 10 flares, coronal mass ejections etc. interact(ed) with planetary systems. The properties of the early Sun out (i.e. photoionisation/photodissociation can change chemistry, X-ray/EUV radiation can heat upper

454

In-situ mechanical testing during X-ray diffraction  

SciTech Connect (OSTI)

Deforming metals during recording X-ray diffraction patterns is a useful tool to get a deeper understanding of the coupling between microstructure and mechanical behaviour. With the advances in flux, detector speed and focussing techniques at synchrotron facilities, in-situ mechanical testing is now possible during powder diffraction and Laue diffraction. The basic principle is explained together with illustrative examples.

Van Swygenhoven, Helena, E-mail: helena.vanswygenhoven@psi.ch; Van Petegem, Steven

2013-04-15T23:59:59.000Z

455

Crystal defect studies using x-ray diffuse scattering  

SciTech Connect (OSTI)

Microscopic lattice defects such as point (single atom) defects, dislocation loops, and solute precipitates are characterized by local electronic density changes at the defect sites and by distortions of the lattice structure surrounding the defects. The effect of these interruptions of the crystal lattice on the scattering of x-rays is considered in this paper, and examples are presented of the use of the diffuse scattering to study the defects. X-ray studies of self-interstitials in electron irradiated aluminum and copper are discussed in terms of the identification of the interstitial configuration. Methods for detecting the onset of point defect aggregation into dislocation loops are considered and new techniques for the determination of separate size distributions for vacancy loops and interstitial loops are presented. Direct comparisons of dislocation loop measurements by x-rays with existing electron microscopy studies of dislocation loops indicate agreement for larger size loops, but x-ray measurements report higher concentrations in the smaller loop range. Methods for distinguishing between loops and three-dimensional precipitates are discussed and possibilities for detailed studies considered. A comparison of dislocation loop size distributions obtained from integral diffuse scattering measurements with those from TEM show a discrepancy in the smaller sizes similar to that described above.

Larson, B.C.

1980-01-01T23:59:59.000Z

456

Soft x-ray diagnostics for pulsed power machines  

SciTech Connect (OSTI)

A variety of soft x-ray diagnostics are being fielded on the Los Alamos National Laboratory Pegasus and Procyon pulsed power systems and also being fielded on joint US/Russian magnetized target fusion experiments known as MAGO (Magnitoye Obzhatiye). The authors have designed a low-cost modular photoemissive detector designated the XRD-96 that uses commercial 1100 series aluminum for the photocathode. In addition to photocathode detectors a number of designs using solid state silicon photodiodes have been designed and fielded. They also present a soft x-ray time-integrated pinhole camera system that uses standard type TMAX-400 photographic film that obviates the need for expensive and no longer produced zero-overcoat soft x-ray emulsion film. In a typical experiment the desired spectral energy cuts, signal intensity levels, and desired field of view will determine diagnostic geometry and x-ray filters selected. The authors have developed several computer codes to assist in the diagnostic design process and data deconvolution. Examples of the diagnostic design process and data analysis for a typical pulsed power experiment are presented.

Idzorek, G.C.; Coulter, W.L.; Walsh, P.J.; Montoya, R.R.

1995-08-01T23:59:59.000Z

457

Soft x-ray laser microscope. Final report  

SciTech Connect (OSTI)

The program consisted of two phases (Phase I and Phase II). The goal of the Phase I (first year program) was to design and construct the Soft X-ray Laser Contact Microscope. Such microscope was constructed and adapted to PPL`s 18.2nm soft X-ray Laser (SXL), which in turn was modified and prepared for microscopy experiments. Investigation of the photoresist response to 18.2nm laser radiation and transmissivity of 0.1m thick silicion-nitride (Si{sub 3}N{sub 4}) windows were important initial works. The goal of the first year of Phase II was to construct X-ray contact microscope in combination with existing optical phase microscope, already used by biologists. In the second year of Phase II study of dehydrated Horeseshoe Crab and Hela cancer cells were performed with COXRALM. Also during Phase II, the Imaging X-Ray Laser Microscope (IXRALM) was designed and constructed. This paper describes the development of each of the microscopes and their application for research.

Suckewer, P.I.

1990-10-01T23:59:59.000Z

458

Data needs for X-ray astronomy satellites  

SciTech Connect (OSTI)

I review the current status of atomic data for X-ray astronomy satellites. This includes some of the astrophysical issues which can be addressed, current modeling and analysis techniques, computational tools, the limitations imposed by currently available atomic data, and the validity of standard assumptions. I also discuss the future: challenges associated with future missions and goals for atomic data collection.

Kallman, T. [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States)

2013-07-11T23:59:59.000Z

459

Lensless imaging of nanoporous glass with soft X-rays  

DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

Coherent soft X-ray diffraction has been used to image nanoporous glass structure in two dimensions using different methods. The merit of the reconstructions was judged using a new method of Fourier phase correlation with a final, refined image. The porous structure was found to have a much larger average size then previously believed.

Turner, Joshua J.; Nelson, Johanna; Huang, Xiaojing; Steinbrener, Jan; Jacobsen, Chris

2013-06-01T23:59:59.000Z

460

Transient x-ray absorption spectroscopy of hydrated halogen atom  

E-Print Network [OSTI]

Time-resolved x-ray absorption spectroscopy has been used to observe the transient species generated by one-photon detachment of an electron from aqueous bromide. The K-edge spectrum of the short-lived Br(0) atom exhibits a resonant 1s-4p transition...

Elles, Christopher G.; Shkrob, Ilya A.; Crowell, Robert A.; Arms, Dohn A.; Landahl, Eric C.

2008-02-11T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Vanadium-pumped titanium x-ray laser  

DOE Patents [OSTI]

A resonantly photo-pumped x-ray laser is formed of a vanadium and titanium foil combination that is driven by two beams of intense line focused optical laser radiation. Ground state neon-like titanium ions are resonantly photo-pumped by line emission from fluorine-like vanadium ions. 4 figs.

Nilsen, J.

1992-05-26T23:59:59.000Z

462

Vanadium-pumped titanium x-ray laser  

DOE Patents [OSTI]

A resonantly photo-pumped x-ray laser (10) is formed of a vanadium (12) and titanium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state neon-like titanium ions (34) are resonantly photo-pumped by line emission from fluorine-like vanadium ions (32).

Nilsen, Joseph (Livermore, CA)

1992-01-01T23:59:59.000Z

463

X-ray Emission from Thunderstorms and Lightning  

ScienceCinema (OSTI)

How lightning is initiated in the relatively low electric fields inside thunderclouds and how it can then propagate for tens of kilometers through virgin air are two of the great unsolved problems in the atmospheric sciences.  Until very recently it was believed that lightning was entirely a conventional discharge, involving only low-energy (a few eV) electrons.  This picture changed completely a few years ago with the discovery of intense x-ray emission from both natural cloud-to-ground lightning and rocket-triggered lightning.  This energetic emission cannot be produced by a conventional discharge, and so the presence of x-rays strongly implies that runaway breakdown plays a role in lightning processes.  During runaway breakdown, electrons are accelerated through air to nearly the speed of light by strong electric fields.  These runaway electrons then emit bremsstrahlung x-rays and gamma-rays during collisions with air.  Indeed, the x-ray and gamma-ray emission produced by runaway breakdown near the tops of thunderstorms is bright enough to be seen from outer space, 600 km away.  As a result, the physics used for decades to describe thunderstorm electrification and lightning discharges is incomplete and needs to be revisited. 

Joseph Dwyer

2010-01-08T23:59:59.000Z

464

X-ray ferromagnetic resonance spectroscopy and S. Rusponi  

E-Print Network [OSTI]

-coupled multilayers,1,2,11,12 as well as current-induced magnetization excitations in spin-valve structures.13,14 Very at GHz frequencies. XMCD is defined as the dependence of the x-ray absorp- tion coefficient

Brune, Harald

465

Double K-Vacancy Production by X-Ray Photoionization  

E-Print Network [OSTI]

Double K-Vacancy Production by X-Ray Photoionization S. H. Southworth£ , R. W. Dunford£ , E. P Photon Source. Double K-vacancy production in Ne was observed by recording the KK-KLL Auger. For Mo, double K-vacancy production was observed by recording the K fluorescence hypersatellite

466

DEDUCING ELECTRON PROPERTIES FROM HARD X-RAY OBSERVATIONS  

E-Print Network [OSTI]

of the accelerated electron distribution. Keywords: Sun: flares; Sun: X-rays; Sun: acceleration; Sun: energetic distribution 31 4.5 Low-energy cutoffs in the electron distribution 32 4.6 Temperature distribution of thermal-ray emission process(es) in question with the electron distribution function, which is in turn a function

Piana, Michele

467

A mirror for lab-based quasi-monochromatic parallel x-rays  

SciTech Connect (OSTI)

A multilayered parabolic mirror with six W/Al bilayers was designed and fabricated to generate monochromatic parallel x-rays using a lab-based x-ray source. Using this mirror, curved bright bands were obtained in x-ray images as reflected x-rays. The parallelism of the reflected x-rays was investigated using the shape of the bands. The intensity and monochromatic characteristics of the reflected x-rays were evaluated through measurements of the x-ray spectra in the band. High intensity, nearly monochromatic, and parallel x-rays, which can be used for high resolution x-ray microscopes and local radiation therapy systems, were obtained.

Nguyen, Thanhhai; Lu, Xun; Lee, Chang Jun; Jeon, Insu, E-mail: i-jeon@chonnam.ac.kr [School of Mechanical Engineering, Chonnam National University, 300 Yongbong-dong, Buk-gu, Gwangju 500-757 (Korea, Republic of); Jung, Jin-Ho [Pro-optics Co., Ltd., 475 Ami-ri, Bubal-eup, Icheon 467-866 (Korea, Republic of); Jin, Gye-Hwan [Department of Radiology, Nambu University, 76 Chumdan Jungang 1-ro, Gwangsan-gu, Gwangju 506-706 (Korea, Republic of); Kim, Sung Youb [School of Mechanical and Advanced Materials Engineering, Ulsan National Institute of Science and Technology, 100 Banyeon-ri, Eonyang-eup, Ulju-gun, Ulsan 689-798 (Korea, Republic of)

2014-09-15T23:59:59.000Z

468

SUPERLUMINOUS X-RAYS FROM A SUPERLUMINOUS SUPERNOVA  

SciTech Connect (OSTI)

The discovery of a population of superluminous supernovae (SLSNe), with peak luminosities a factor of {approx}100 brighter than normal supernovae (SNe; typically SLSNe have M{sub V} < -21), has shown an unexpected diversity in core-collapse SN properties. Numerous models have been postulated for the nature of these events, including a strong interaction of the shockwave with a dense circumstellar environment, a re-energizing of the outflow via a central engine, or an origin in the catastrophic destruction of the star following a loss of pressure due to pair production in an extremely massive stellar core (so-called pair instability SNe). Here we consider constraints that can be placed on the explosion mechanism of hydrogen-poor SLSNe (SLSNe-I) via X-ray observations, with XMM-Newton, Chandra, and Swift, and show that at least one SLSN-I is likely the brightest X-ray SN ever observed, with L{sub X} {approx} 10{sup 45} erg s{sup -1}, {approx}150 days after its initial discovery. This is a luminosity three orders of magnitude higher than seen in other X-ray SNe powered via circumstellar interactions. Such high X-ray luminosities are sufficient to ionize the ejecta and markedly reduce the optical depth, making it possible to see deep into the ejecta and any source of emission that resides there. Alternatively, an engine could have powered a moderately relativistic jet external to the ejecta, similar to those seen in gamma-ray bursts. If the detection of X-rays does require an engine it implies that these SNe do create compact objects, and that the stars are not completely destroyed in a pair instability event. Future observations will determine which, if any, of these mechanisms are at play in SLSNe.

Levan, A. J.; Wheatley, P. J. [Department of Physics, University of Warwick, Coventry CV4 7AL (United Kingdom); Read, A. M.; Tanvir, N. R. [Department of Physics and Astronomy, University of Leicester, University Road, Leicester LE1 7RH (United Kingdom); Metzger, B. D., E-mail: a.j.levan@warwick.ac.uk [Department of Physics, Columbia University, 538 West 120th Street, 704 Pupin Hall, MC 5255, New York, NY 10027 (United States)

2013-07-10T23:59:59.000Z

469

High resolution, multiple-energy linear sweep detector for x-ray imaging  

DOE Patents [OSTI]

Apparatus is disclosed for generating plural electrical signals in a single scan in response to incident X-rays received from an object. Each electrical signal represents an image of the object at a different range of energies of the incident X-rays. The apparatus comprises a first X-ray detector, a second X-ray detector stacked upstream of the first X-ray detector, and an X-ray absorber stacked upstream of the first X-ray detector. The X-ray absorber provides an energy-dependent absorption of the incident X-rays before they are incident at the first X-ray detector, but provides no absorption of the incident X-rays before they are incident at the second X-ray detector. The first X-ray detector includes a linear array of first pixels, each of which produces an electrical output in response to the incident X-rays in a first range of energies. The first X-ray detector also includes a circuit that generates a first electrical signal in response to the electrical output of each of the first pixels. The second X-ray detector includes a linear array of second pixels, each of which produces an electrical output in response to the incident X-rays in a second range of energies, broader than the first range of energies. The second X-ray detector also includes a circuit that generates a second electrical signal in response to the electrical output of each of the second pixels. 12 figs.

Perez-Mendez, V.; Goodman, C.A.

1996-08-20T23:59:59.000Z

470

High resolution, multiple-energy linear sweep detector for x-ray imaging  

DOE Patents [OSTI]

Apparatus for generating plural electrical signals in a single scan in response to incident X-rays received from an object. Each electrical signal represents an image of the object at a different range of energies of the incident X-rays. The apparatus comprises a first X-ray detector, a second X-ray detector stacked upstream of the first X-ray detector, and an X-ray absorber stacked upstream of the first X-ray detector. The X-ray absorber provides an energy-dependent absorption of the incident X-rays before they are incident at the first X-ray detector, but provides no absorption of the incident X-rays before they are incident at the second X-ray detector. The first X-ray detector includes a linear array of first pixels, each of which produces an electrical output in response to the incident X-rays in a first range of energies. The first X-ray detector also includes a circuit that generates a first electrical signal in response to the electrical output of each of the first pixels. The second X-ray detector includes a linear array of second pixels, each of which produces an electrical output in response to the incident X-rays in a second range of energies, broader than the first range of energies. The second X-ray detector also includes a circuit that generates a second electrical signal in response to the electrical output of each of the second pixels.

Perez-Mendez, Victor (Berkeley, CA); Goodman, Claude A. (Kensington, CA)

1996-01-01T23:59:59.000Z

471

Refractive optical elements and optical system for high energy x-ray microscopy  

SciTech Connect (OSTI)

In material science, X-ray radiation with photon energies above 25 keV is used because of its penetration into high density materials. Research of the inner structure of novel materials, such as electrodes in high power batteries for engines, require X-ray microscopes operating in the hard X-ray energy range. A flexible X-ray microscope for hard X-rays with photon energies higher than 25 keV will be realized at the synchrotron source ANKA in Karlsruhe, Germany. The device will use refractive X-ray lenses as condenser as well as objective lenses.

Simon, M.; Altapova, V.; Baumbach, T.; Kluge, M.; Last, A.; Marschall, F.; Mohr, J.; Nazmov, V.; Vogt, H. [Karlsruhe Institute of Technology, Institute of Microstructure Technology, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany); Karlsruhe Institute of Technology, Laboratory for Applications of Synchrotron Radiation, Engesser Strasse 15, 76131 Karlsruhe (Germany); Karlsruhe Institute of Technology, Institute of Microstructure Technology, Hermann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany)

2012-05-17T23:59:59.000Z

472

Real-time X-ray Diffraction Measurements of Shocked Polycrystalline Tin and Aluminum  

SciTech Connect (OSTI)

A new, fast, single-pulse x-ray diffraction (XRD) diagnostic for determining phase transitions in shocked polycrystalline materials has been developed. The diagnostic consists of a 37-stage Marx bank high-voltage pulse generator coupled to a needle-and-washer electron beam diode via coaxial cable, producing line and bremsstrahlung x-ray emission in a 35-ns pulse. The characteristic K? lines from the selected anodes of silver and molybdenum are used to produce the diffraction patterns, with thin foil filters employed to remove the characteristic K? line emission. The x-ray beam passes through a pinhole collimator and is incident on the sample with an approximately 3-mm by 6-mm spot and 1° full-width-half-maximum (FWHM) angular divergence in a Bragg-reflecting geometry. For the experiments described in this report, the angle between the incident beam and the sample surface was 8.5°. A Debye-Scherrer diffraction image was produced on a phosphor located 76 mm from the polycrystalline sample surface. The phosphor image was coupled to a charge-coupled device (CCD) camera through a coherent fiberoptic bundle. Dynamic single-pulse XRD experiments were conducted with thin foil samples of tin, shock loaded with a 1-mm vitreous carbon back window. Detasheet high explosive with a 2-mm-thick aluminum buffer was used to shock the sample. Analysis of the dynamic shock-loaded tin XRD images revealed a phase transformation of the tin beta phase into an amorphous or liquid state. Identical experiments with shock-loaded aluminum indicated compression of the face-centered-cubic (fcc) aluminum lattice with no phase transformation.

Dane V. Morgan, Don Macy, Gerald Stevens

2008-11-22T23:59:59.000Z

473

Adsorption Trajectories and Free-Energy Separatrices for Colloidal Particles in Contact with a Liquid-Liquid Interface  

E-Print Network [OSTI]

We apply the recently developed triangular tessellation technique as presented in [J. de Graaf et al., Phys. Rev. E 80, 051405 (2009)] to calculate the free energy associated with the adsorption of anisotropic colloidal particles at a flat interface. From the free-energy landscape, we analyze the adsorption process, using a simplified version of Langevin dynamics. The present result is a first step to understand the time-dependent behavior of colloids near interfaces. This study shows a wide range of adsorption trajectories, where the emphasis lies on a strong dependence of the dynamics on the orientation of the colloid at initial contact with the interface. We believe that the observed orientational dependence in our simple model can be recovered in suitable experimental systems.

J. de Graaf; M. Dijkstra; R. van Roij

2010-02-18T23:59:59.000Z

474

Studies of local and intermediate range structure in crystalline and amorphouse materials at high pressure using high-energy x-rays.  

SciTech Connect (OSTI)

The method of high-energy total elastic X-ray scattering to determine the atomic structure of nanocrystalline, highly disordered, and amorphous materials is presented. The current state of the technique, its potential, and limitations are discussed with two successful studies on the pressure induced phase transition in mackinawite (FeS) and the high-pressure behavior of liquid gallium.

Ehm, L.; Antao, M.; Chen, J.; Locke, D. R.; Michel, F. M.; Martin, C. D.; Yu, T.; Lee, P. L.; Chupas, P. J.; Shastri, S. D.; Guo, Q.; Parise, J. B.; Stony Brook Univ.; BNL

2007-06-01T23:59:59.000Z

475

Studies of Local and Intermediate Range Structure in Crystalline and Amorphous Materials at High Pressure Using High-Energy X-rays  

SciTech Connect (OSTI)

The method of high-energy total elastic X-ray scattering to determine the atomic structure of nanocrystalline, highly disordered, and amorphous materials is presented. The current state of the technique, its potential, and limitations are discussed with two successful studies on the pressure induced phase transition in mackinawite (FeS) and the high-pressure behavior of liquid gallium.

Ehm,L.; Antao, S.; Chen, J.; Locke, D.; Michel, F.; Martin, D.; Yu, T.; Parise, J.; Lee, P.; et al.

2007-01-01T23:59:59.000Z

476

Line X-ray emission from Al targets irradiated by high-intensity, variable-length laser pulses  

E-Print Network [OSTI]

Line X-ray emission from Al targets irradiated by high-intensity, variable-length laser pulses J; the scaling rules for the conversion efficiency of the laser radiation into the line X-ray emission are discussed. Keywords: Laser-produced plasma; Line X-ray emission; X-ray sources; X-ray spectroscopy 1

Limpouch, Jiri

477

Analysis of the optical design of the NSLS-II Coherent Hard X-ray beamline  

SciTech Connect (OSTI)

Ultra-low emittance third-generation synchrotron radiation sources such as the NSLS-II offer excellent opportunities for the development of experimental techniques exploiting x-ray coherence. Coherent light scattered by a heterogeneous sample produces a speckle pattern characteristic for the specific arrangement of the scatterers. This may vary over time, and the resultant intensity fluctuations can be measured and analyzed to provide information about the sample dynamics. X-ray photon correlation spectroscopy (XPCS) extends the capability of dynamic light scattering to opaque and turbid samples and extends the measurements of time evolution to nanometer length scales. As a consequence XPCS became crucial in the study of dynamics in systems including, but not being limited to, colloids, polymers, complex fluids, surfaces and interfaces, phase ordering alloys, etc. In this paper we present the conceptual optical design and the theoretical performance of the Coherent Hard X-ray (CHX) beamline at NSLS-II, dedicated to XPCS and other coherent scattering techniques. For the optical design of this beamline, there is a tradeoff between the coherence needed to distinguish individual speckles and the phase acceptance (high intensity) required to measure fast dynamics with an adequate signal-to-noise level. As XPCS is a 'photon hungry' technique, the beamline optimization requires maximizing the signal-to-noise ratio of the measured intensity-intensity autocorrelation function. The degree of coherence, as measured by a two-slit (Young) experiment, is used to characterize the speckle pattern visibilities. The beamline optimization strategy consists of maximization of the on-sample intensity while keeping the degree of coherence within the 0.1-0.5 range. The resulted design deviates substantially from an ad-hoc modification of a hard x-ray beamline for XPCS measurements. The CHX beamline will permit studies of complex systems and measurements of bulk dynamics down to the microsecond time scales. In general, the 10-fold increase in brightness of the NSLS-II, compared to other sources, will allow for measurements of dynamics on time-scales that are two orders of magnitude faster than what is currently possible. We also conclude that the common approximations used in evaluating the transverse coherence length would not be sufficiently accurate for the calculation of the coherent properties of an undulator-based beamline, and a thorough beamline optimization at a low-emittance source such as the NSLS-II requires a realistic wave-front propagation analysis.

Fluerasu A.; Chubar, O.; Kaznatcheev, K.; Baltser, J.; Wiegart, Lutz; Evans-Lutterodt, K.; Carlucci-Dayton, M.; Berman, L.

2011-08-21T23:59:59.000Z

478

Determination of preferential molecular orientation in porphyrin-fullerene dyad ZnDHD6ee monolayers by the X-ray standing-wave method and X-ray reflectometry  

SciTech Connect (OSTI)

Monolayers of porphyrin-fullerene dyad molecules with zinc atoms incorporated into the porphyrin ring (ZnDHD6ee) on the surface of aqueous subphase and on Si substrates have been investigated by the X-ray standing-wave method and X-ray reflectometry. The experiments have been performed under laboratory conditions and on synchrotron radiation sources (KMC-2 station of BESSY II (Berlin) and Langmuir station at the National Research Centre 'Kurchatov Institute'). Depth distributions of Zn atoms and electron density in the monolayer film are calculated. On the basis of the analysis of these distributions, it is concluded that ZnDHD6ee dyad molecules in monolayers have preferential orientation. The data obtained indicate that the molecules in monolayer film retain their orientation when the monolayer is transferred from a liquid subphase surface onto a solid substrate.

Seregin, A. Yu., E-mail: seregin@gmail.com; D'yakova, Yu. A.; Yakunin, S. N.; Makhotkin, I. A. [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)] [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation); Alekseev, A. S. [Russian Academy of Sciences, Prokhorov General Physics Institute (Russian Federation)] [Russian Academy of Sciences, Prokhorov General Physics Institute (Russian Federation); Klechkovskaya, V. V.; Tereschenko, E. Yu. [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)] [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation); Tkachenko, N. V.; Lemmetyinen, H. [Tampere University of Technology (Finland)] [Tampere University of Technology (Finland); Feigin, L. A.; Kovalchuk, M. V. [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)] [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)

2013-11-15T23:59:59.000Z

479

Fiber fed x-ray/gamma ray imaging apparatus  

DOE Patents [OSTI]

X-ray/gamma ray imaging apparatus is disclosed for detecting the position, energy, and intensity of x-ray/gamma ray radiation comprising scintillation means disposed in the path of such radiation and capable of generating photons in response to such radiation; first photodetection means optically bonded to the scintillation means and capable of generating an electrical signal indicative of the intensity, and energy of the radiation detected by the scintillation means; second photodetection means capable of generating an electrical signal indicative of the position of the radiation in the radiation pattern; and means for optically coupling the scintillation means to the second photodetection means. The photodetection means are electrically connected to control and storage means which may also be used to screen out noise by rejecting a signal from one photodetection means not synchronized to a signal from the other photodetection means; and also to screen out signals from scattered radiation. 6 figs.

Hailey, C.J.; Ziock, K.P.

1992-06-02T23:59:59.000Z

480

Segmentation of x-ray images using Probabilistic Relaxation Labeling  

SciTech Connect (OSTI)

Segmentation is a process of separating objects of interest from their background or from other objects in an image. Without a suitable segmentation scheme, it is very difficult to detect contraband in X-rays images. In this paper, a Probabilistic Relaxation Labeling (PRL) segmentation scheme is presented and compared with other segmentation methods. PRL segmentation is an interative algorithm that labels each pixel in an image by cooperative use of two information sources: the pixel probability and the degree of certainty of its probability supported by the neighboring pixels. The practical implementation and results of the PRL segmentation on X-ray baggage images are also discussed and compared with other segmentation methods. 13 refs., 12 figs.

Thai, T.Q.

1991-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "liquid interface x-ray" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


481

Hard X-ray Phase-Contrast Tomographic Nanoimaging  

SciTech Connect (OSTI)

Synchrotron-based full-field tomographic microscopy established itself as a tool for noninvasive investigations. Many beamlines worldwide routinely achieve micrometer spatial resolution while the isotropic 100-nm barrier is reached and trespassed only by few instruments, mainly in the soft x-ray regime. We present an x-ray, full-field microscope with tomographic capabilities operating at 10 keV and with a 3D isotropic resolution of 144 nm recently installed at the TOMCAT beamline of the Swiss Light Source. Custom optical components, including a beam-shaping condenser and phase-shifting dot arrays, were used to obtain an ideal, aperture-matched sample illumination and very sensitive phase-contrast imaging. The instrument has been successfully used for the nondestructive, volumetric investigation of single, unstained cells.

Stampanoni, M. [Paul Scherrer Institut, 5232 Villigen (Switzerland); Institute for Biomedical Engineering, University and ETH Zuerich, 8092 Zuerich (Switzerland); Marone, F.; Vila-Comamala, J.; Gorelick, S.; David, C.; Mokso, R. [Paul Scherrer Institut, 5232 Villigen (Switzerland); Trtik, P.; Jefimovs, K. [EMPA, Swiss Federal Laboratories for Materials Science and Technology, 8600 Duebendorf (Switzerland)

2011-09-09T23:59:59.000Z

482

Water Window Ptychographic Imaging with Characterized Coherent X-rays  

E-Print Network [OSTI]

We report on a ptychographical coherent diffractive imaging experiment in the water window with focused soft X-rays at $500~\\mathrm{eV}$. An X-ray beam with high degree of coherence was selected for ptychography at the P04 beamline of the PETRA III synchrotron radiation source. We measured the beam coherence with the newly developed non-redundant array method. A pinhole $2.6~\\mathrm{\\mu m}$ in size selected the coherent part of the beam and was used for ptychographic measurements of a lithographically manufactured test sample and fossil diatom. The achieved resolution was $53~\\mathrm{nm}$ for the test sample and only limited by the size of the detector. The diatom was imaged at a resolution better than $90~\\mathrm{nm}$.

Rose, Max; Dzhigaev, Dmitry; Gorobtsov, Oleg; Senkbeil, Tobias; von Gundlach, Andreas; Gorniak, Thomas; Shabalin, Anatoly; Viefhaus, Jens; Rosenhahn, Axel; Vartanyants, Ivan

2015-01-01T23:59:59.000Z

483

Superluminous X-rays from a superluminous supernova  

E-Print Network [OSTI]

The discovery of a population of superluminous supernovae (SLSNe), with peak luminosities a factor of ~100 brighter than normal SNe (typically SLSNe have M_V engine, or an origin in the catastrophic destruction of the star following a loss of pressure due to pair production in an extremely massive stellar core (so-called pair instability supernovae). Here we consider constraints that can be placed on the explosion mechanism of Hydrogen-poor SLSNe (SLSNe-I) via X-ray observations, with XMM-Newton, Chandra and Swift, and show that at least one SLSNe-I is likely the brightest X-ray supernovae ever observed, with L_X ~ 10^45 ergs/s, ~150 days after its initial discovery. This is a luminosity 3 orders of magnitude higher than seen in ...

Levan, A J; Metzger, B D; Wheatley, P J; Tanvir, N R

2013-01-01T23:59:59.000Z

484

Dense Plasma X-ray Scattering: Methods and Applications  

SciTech Connect (OSTI)

We have developed accurate x-ray scattering techniques to measure the physical p