National Library of Energy BETA

Sample records for high resolution irradiance

  1. Spatial disaggregation of satellite-derived irradiance using a high-resolution digital elevation model

    SciTech Connect (OSTI)

    Ruiz-Arias, Jose A.; Tovar-Pescador, Joaquin; Cebecauer, Tomas; Suri, Marcel

    2010-09-15

    Downscaling of the Meteosat-derived solar radiation ({proportional_to}5 km grid resolution) is based on decomposing the global irradiance and correcting the systematic bias of its components using the elevation and horizon shadowing that are derived from the SRTM-3 digital elevation model (3 arc sec resolution). The procedure first applies the elevation correction based on the difference between coarse and high spatial resolution. Global irradiance is split into direct, diffuse circumsolar and diffuse isotropic components using statistical models, and then corrections due to terrain shading and sky-view fraction are applied. The effect of reflected irradiance is analysed only in the theoretical section. The method was applied in the eastern Andalusia, Spain, and the validation was carried out for 22 days on April, July and December 2006 comparing 15-min estimates of the satellite-derived solar irradiance and observations from nine ground stations. Overall, the corrections of the satellite estimates in the studied region strongly reduced the mean bias of the estimates for clear and cloudy days from roughly 2.3% to 0.4%. (author)

  2. High resolution data acquisition

    DOE Patents [OSTI]

    Thornton, G.W.; Fuller, K.R.

    1993-04-06

    A high resolution event interval timing system measures short time intervals such as occur in high energy physics or laser ranging. Timing is provided from a clock, pulse train, and analog circuitry for generating a triangular wave synchronously with the pulse train (as seen in diagram on patent). The triangular wave has an amplitude and slope functionally related to the time elapsed during each clock pulse in the train. A converter forms a first digital value of the amplitude and slope of the triangle wave at the start of the event interval and a second digital value of the amplitude and slope of the triangle wave at the end of the event interval. A counter counts the clock pulse train during the interval to form a gross event interval time. A computer then combines the gross event interval time and the first and second digital values to output a high resolution value for the event interval.

  3. High resolution data acquisition

    DOE Patents [OSTI]

    Thornton, Glenn W.; Fuller, Kenneth R.

    1993-01-01

    A high resolution event interval timing system measures short time intervals such as occur in high energy physics or laser ranging. Timing is provided from a clock (38) pulse train (37) and analog circuitry (44) for generating a triangular wave (46) synchronously with the pulse train (37). The triangular wave (46) has an amplitude and slope functionally related to the time elapsed during each clock pulse in the train. A converter (18, 32) forms a first digital value of the amplitude and slope of the triangle wave at the start of the event interval and a second digital value of the amplitude and slope of the triangle wave at the end of the event interval. A counter (26) counts the clock pulse train (37) during the interval to form a gross event interval time. A computer (52) then combines the gross event interval time and the first and second digital values to output a high resolution value for the event interval.

  4. High resolution time interval meter

    DOE Patents [OSTI]

    Martin, A.D.

    1986-05-09

    Method and apparatus are provided for measuring the time interval between two events to a higher resolution than reliability available from conventional circuits and component. An internal clock pulse is provided at a frequency compatible with conventional component operating frequencies for reliable operation. Lumped constant delay circuits are provided for generating outputs at delay intervals corresponding to the desired high resolution. An initiation START pulse is input to generate first high resolution data. A termination STOP pulse is input to generate second high resolution data. Internal counters count at the low frequency internal clock pulse rate between the START and STOP pulses. The first and second high resolution data are logically combined to directly provide high resolution data to one counter and correct the count in the low resolution counter to obtain a high resolution time interval measurement.

  5. High resolution telescope

    DOE Patents [OSTI]

    Massie, Norbert A.; Oster, Yale

    1992-01-01

    A large effective-aperture, low-cost optical telescope with diffraction-limited resolution enables ground-based observation of near-earth space objects. The telescope has a non-redundant, thinned-aperture array in a center-mount, single-structure space frame. It employs speckle interferometric imaging to achieve diffraction-limited resolution. The signal-to-noise ratio problem is mitigated by moving the wavelength of operation to the near-IR, and the image is sensed by a Silicon CCD. The steerable, single-structure array presents a constant pupil. The center-mount, radar-like mount enables low-earth orbit space objects to be tracked as well as increases stiffness of the space frame. In the preferred embodiment, the array has elemental telescopes with subaperture of 2.1 m in a circle-of-nine configuration. The telescope array has an effective aperture of 12 m which provides a diffraction-limited resolution of 0.02 arc seconds. Pathlength matching of the telescope array is maintained by an electro-optical system employing laser metrology. Speckle imaging relaxes pathlength matching tolerance by one order of magnitude as compared to phased arrays. Many features of the telescope contribute to substantial reduction in costs. These include eliminating the conventional protective dome and reducing on-site construction activites. The cost of the telescope scales with the first power of the aperture rather than its third power as in conventional telescopes.

  6. Details of the response of Kodak high resolution plate to x-irradiation for the characterization of ICF targets and components

    SciTech Connect (OSTI)

    Martin, A.J.; Simms, R.J.

    1985-01-01

    Radiographic images are used in the characterization of Internal Confinement Fusion targets and target components. The use of this technique involves consideration of: (1) the continuum and line emission source spectra produced by a tungsten anode, (2) the attenuation of the source spectrum by material in the x-ray path, and (3) the response of the x-ray detector, a Kodak HRP (High Resolution Plate), to the incident x-ray flux. 5 refs., 4 figs.

  7. High resolution digital delay timer

    DOE Patents [OSTI]

    Martin, Albert D.

    1988-01-01

    Method and apparatus are provided for generating an output pulse following a trigger pulse at a time delay interval preset with a resolution which is high relative to a low resolution available from supplied clock pulses. A first lumped constant delay (20) provides a first output signal (24) at predetermined interpolation intervals corresponding to the desired high resolution time interval. Latching circuits (26, 28) latch the high resolution data (24) to form a first synchronizing data set (60). A selected time interval has been preset to internal counters (142, 146, 154) and corrected for circuit propagation delay times having the same order of magnitude as the desired high resolution. Internal system clock pulses (32, 34) count down the counters to generate an internal pulse delayed by an interval which is functionally related to the preset time interval. A second LCD (184) corrects the internal signal with the high resolution time delay. A second internal pulse is then applied to a third LCD (74) to generate a second set of synchronizing data (76) which is complementary with the first set of synchronizing data (60) for presentation to logic circuits (64). The logic circuits (64) further delay the internal output signal (72) to obtain a proper phase relationship of an output signal (80) with the internal pulses (32, 34). The final delayed output signal (80) thereafter enables the output pulse generator (82) to produce the desired output pulse (84) at the preset time delay interval following input of the trigger pulse (10, 12).

  8. Radiometry High Spectral Resolution Fourier

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High Spectral Resolution Fourier Transform Infrared Instruments for the Atmospheric Radiation Measurement Program H. E. Revercomb, W. L. Smith, R. O. Knuteson, F. A. Best, R. G. Dedecker, T. P. Dirkx, R. A. Herbsleb, and J. F. Short University of Wisconsin Madison, Wisconsin H. B. Howell National Oceanic and Atmospheric Administration Systems Design and Applications Branch Madison, Wisconsin D. Murcray and F. Murcray University of Denver Denver, Colorado Accurate and spectrally detailed

  9. High resolution time interval counter

    DOE Patents [OSTI]

    Condreva, K.J.

    1994-07-26

    A high resolution counter circuit measures the time interval between the occurrence of an initial and a subsequent electrical pulse to two nanoseconds resolution using an eight megahertz clock. The circuit includes a main counter for receiving electrical pulses and generating a binary word--a measure of the number of eight megahertz clock pulses occurring between the signals. A pair of first and second pulse stretchers receive the signal and generate a pair of output signals whose widths are approximately sixty-four times the time between the receipt of the signals by the respective pulse stretchers and the receipt by the respective pulse stretchers of a second subsequent clock pulse. Output signals are thereafter supplied to a pair of start and stop counters operable to generate a pair of binary output words representative of the measure of the width of the pulses to a resolution of two nanoseconds. Errors associated with the pulse stretchers are corrected by providing calibration data to both stretcher circuits, and recording start and stop counter values. Stretched initial and subsequent signals are combined with autocalibration data and supplied to an arithmetic logic unit to determine the time interval in nanoseconds between the pair of electrical pulses being measured. 3 figs.

  10. High resolution time interval counter

    DOE Patents [OSTI]

    Condreva, Kenneth J.

    1994-01-01

    A high resolution counter circuit measures the time interval between the occurrence of an initial and a subsequent electrical pulse to two nanoseconds resolution using an eight megahertz clock. The circuit includes a main counter for receiving electrical pulses and generating a binary word--a measure of the number of eight megahertz clock pulses occurring between the signals. A pair of first and second pulse stretchers receive the signal and generate a pair of output signals whose widths are approximately sixty-four times the time between the receipt of the signals by the respective pulse stretchers and the receipt by the respective pulse stretchers of a second subsequent clock pulse. Output signals are thereafter supplied to a pair of start and stop counters operable to generate a pair of binary output words representative of the measure of the width of the pulses to a resolution of two nanoseconds. Errors associated with the pulse stretchers are corrected by providing calibration data to both stretcher circuits, and recording start and stop counter values. Stretched initial and subsequent signals are combined with autocalibration data and supplied to an arithmetic logic unit to determine the time interval in nanoseconds between the pair of electrical pulses being measured.

  11. Afghanistan Pakistan High Resolution Wind Resource - Datasets...

    Open Energy Info (EERE)

    Pakistan High Resolution Wind Resource This shapefile containing 50 meter height data has been validated by NREL and wind energy meteorological consultants. However, the data is...

  12. High resolution scintillation detector with semiconductor readout

    DOE Patents [OSTI]

    Levin, Craig S.; Hoffman, Edward J.

    2000-01-01

    A novel high resolution scintillation detector array for use in radiation imaging such as high resolution Positron Emission Tomography (PET) which comprises one or more parallelepiped crystals with at least one long surface of each crystal being in intimate contact with a semiconductor photodetector such that photons generated within each crystal by gamma radiation passing therethrough is detected by the photodetector paired therewith.

  13. High-Resolution PET Detector. Final report

    SciTech Connect (OSTI)

    Karp, Joel

    2014-03-26

    The objective of this project was to develop an understanding of the limits of performance for a high resolution PET detector using an approach based on continuous scintillation crystals rather than pixelated crystals. The overall goal was to design a high-resolution detector, which requires both high spatial resolution and high sensitivity for 511 keV gammas. Continuous scintillation detectors (Anger cameras) have been used extensively for both single-photon and PET scanners, however, these instruments were based on NaI(Tl) scintillators using relatively large, individual photo-multipliers. In this project we investigated the potential of this type of detector technology to achieve higher spatial resolution through the use of improved scintillator materials and photo-sensors, and modification of the detector surface to optimize the light response function.We achieved an average spatial resolution of 3-mm for a 25-mm thick, LYSO continuous detector using a maximum likelihood position algorithm and shallow slots cut into the entrance surface.

  14. A High Resolution Scale-of-four

    DOE R&D Accomplishments [OSTI]

    Fitch, V.

    1949-08-25

    A high resolution scale-of-four has been developed to be used in conjunction with the nuclear particle detection devices in applications where the counting rate is unusually high. Specifically, it is intended to precede the commercially available medium resolution scaling circuits and so decrease the resolving time of the counting system. The circuit will function reliably on continuously recurring pulses separated by less than 0.1 microseconds. It will resolve two pulses (occurring at a moderate repetition rate) which are spaced at 0.04 microseconds. A five-volt input signal is sufficient to actuate the device.

  15. ELECTRONICS UPGRADE OF HIGH RESOLUTION MASS SPECTROMETERS

    SciTech Connect (OSTI)

    Mcintosh, J; Joe Cordaro, J

    2008-03-10

    High resolution mass spectrometers are specialized systems that allow researchers to determine the exact mass of samples to four significant digits by using magnetic and electronic sector mass analyzers. Many of the systems in use today at research laboratories and universities were designed and built more than two decades ago. The manufacturers of these systems have abandoned the support for some of the mass spectrometers and parts to power and control them have become scarce or obsolete. The Savannah River National Laboratory has been involved in the upgrade of the electronics and software for these legacy machines. The Electronics Upgrade of High Resolution Mass Spectrometers consists of assembling high-end commercial instrumentation from reputable manufacturers with a minimal amount of customization to replace the electronics for the older systems. By taking advantage of advances in instrumentation, precise magnet control can be achieved using high resolution current sources and continuous feedback from a high resolution hall-effect probe. The custom equipment include a precision voltage divider/summing amplifier chassis, high voltage power supply chassis and a chassis for controlling the voltage emission for the mass spectrometer source tube. The upgrade package is versatile enough to interface with valve control, vacuum and other instrumentation. Instrument communication is via a combination of Ethernet and traditional IEEE-488 GPIB protocols. The system software upgrades include precision control, feedback and spectral waveform analysis tools.

  16. Ultra-High Resolution Electron Microscopy for Catalyst Characterizatio...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    High Resolution Electron Microscopy for Catalyst Characterization Ultra-High Resolution Electron Microscopy for Catalyst Characterization 2011 DOE Hydrogen and Fuel Cells Program, ...

  17. Ultra-high Resolution Electron Microscopy for Catalyst Characterizatio...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    high Resolution Electron Microscopy for Catalyst Characterization Ultra-high Resolution Electron Microscopy for Catalyst Characterization 2009 DOE Hydrogen Program and Vehicle ...

  18. High-Resolution Photocurrent Microscopy Using Near-FieldCathodolumine...

    Office of Scientific and Technical Information (OSTI)

    High-Resolution Photocurrent Microscopy Using Near-Field Cathodoluminescence of Quantum Dots. Citation Details In-Document Search Title: High-Resolution Photocurrent Microscopy ...

  19. Supercomputers Fuel Global High-Resolution Climate Models

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Supercomputers Fuel Global High-Resolution Climate Models Supercomputers Fuel Global High-Resolution Climate Models Berkeley Lab Researcher Says Climate Science is Entering New ...

  20. High resolution absorption spectroscopy of exploding wire plasmas...

    Office of Scientific and Technical Information (OSTI)

    Published Article: High resolution absorption spectroscopy of exploding wire plasmas using an x-pinch x-ray source and spherically bent crystal Title: High resolution absorption ...

  1. Ultra-High Resolution Electron Microscopy for Catalyst Characterizatio...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    pm029allard2010p.pdf More Documents & Publications Ultra-High Resolution Electron Microscopy for Catalyst Characterization Ultra-high Resolution Electron Microscopy for Catalyst...

  2. High resolution patterning of silica aerogels

    SciTech Connect (OSTI)

    Bertino, M.F.; Hund, J.F.; Sosa, J.; Zhang, G.; Sotiriou-Leventis, C.; Leventis, N.; Tokuhiro, A.T.; Terry, J. (UMR-MUST); (IIT)

    2008-10-30

    Three-dimensional metallic structures are fabricated with high spatial resolution in silica aerogels. In our method, silica hydrogels are prepared with a standard base-catalyzed route, and exchanged with an aqueous solution typically containing Ag{sup +} ions (1 M) and 2-propanol (0.2 M). The metal ions are reduced photolytically with a table-top ultraviolet lamp, or radiolytically, with a focused X-ray beam. We fabricated dots and lines as small as 30 x 70 {micro}m, protruding for several mm into the bulk of the materials. The hydrogels are eventually supercritically dried to yield aerogels, without any measurable change in the shape and spatial resolution of the lithographed structures. Transmission electron microscopy shows that illuminated regions are composed by Ag clusters with a size of several {micro}m, separated by thin layers of silica.

  3. Experiences with the High Energy Resolution Optics (HERO) update...

    Office of Scientific and Technical Information (OSTI)

    Resolution Optics (HERO) update on a physical electronics 690 auger system. Citation Details In-Document Search Title: Experiences with the High Energy Resolution Optics (HERO) ...

  4. High Resolution Imaging Science Experiment | Open Energy Information

    Open Energy Info (EERE)

    Resolution Imaging Science Experiment Jump to: navigation, search OpenEI Reference LibraryAdd to library Web Site: High Resolution Imaging Science Experiment Author University of...

  5. Ultra-high resolution computed tomography imaging

    DOE Patents [OSTI]

    Paulus, Michael J.; Sari-Sarraf, Hamed; Tobin, Jr., Kenneth William; Gleason, Shaun S.; Thomas, Jr., Clarence E.

    2002-01-01

    A method for ultra-high resolution computed tomography imaging, comprising the steps of: focusing a high energy particle beam, for example x-rays or gamma-rays, onto a target object; acquiring a 2-dimensional projection data set representative of the target object; generating a corrected projection data set by applying a deconvolution algorithm, having an experimentally determined a transfer function, to the 2-dimensional data set; storing the corrected projection data set; incrementally rotating the target object through an angle of approximately 180.degree., and after each the incremental rotation, repeating the radiating, acquiring, generating and storing steps; and, after the rotating step, applying a cone-beam algorithm, for example a modified tomographic reconstruction algorithm, to the corrected projection data sets to generate a 3-dimensional image. The size of the spot focus of the beam is reduced to not greater than approximately 1 micron, and even to not greater than approximately 0.5 microns.

  6. Application of Spatially Resolved High Resolution Crystal Spectrometry...

    Office of Scientific and Technical Information (OSTI)

    Crystal Spectrometry to ICF Plasmas Kenneth W. Hill, et. al. 70 PLASMA PHYSICS AND FUSION TECHNOLOGY High Temperature High Temperature High resolution (3; 10 000) 1D...

  7. Characterization of spatially resolved high resolution x-ray spectrometers

    Office of Scientific and Technical Information (OSTI)

    for high energy density physics and light source experiments (Journal Article) | SciTech Connect Characterization of spatially resolved high resolution x-ray spectrometers for high energy density physics and light source experiments Citation Details In-Document Search Title: Characterization of spatially resolved high resolution x-ray spectrometers for high energy density physics and light source experiments A high resolution 1D imaging x-ray spectrometer concept comprising a spherically

  8. High resolution EUV monochromator/spectrometer

    DOE Patents [OSTI]

    Koike, Masako

    1996-06-18

    This invention is related to a monochromator which employs a spherical mirror, a traveling plane mirror with simultaneous rotation, and a varied spacing plane grating. The divergent beam from the entrance slit is converged by the spherical mirror located at the various positions in the monochromator depending of the inventive system. To provide the meaningful diffraction efficiencies and to reduce unwanted higher order lights, the deviation angle subtending the incidence and diffraction beams for the plane grating is varied with the position of the traveling plane mirror with simultaneous rotation located in the front or back of the plane grating with wavelength scanning. The outgoing beam from the monochromator goes through the fixed exit slit and has same beam direction regardless of the scanning wavelength. The combination of properly designed motions of the plane mirror and novel varied-spacing parameters of the inventive plane grating corrects the aberrations and focuses the monochromatic spectral image on the exit slit, enabling measurements at high spectral resolution. 10 figs.

  9. High resolution EUV monochromator/spectrometer

    DOE Patents [OSTI]

    Koike, Masako

    1996-01-01

    This invention is related to a monochromator which employs a spherical mirror, a traveling plane mirror with simultaneous rotation, and a varied spacing plane grating. The divergent beam from the entrance slit is converged by the spherical mirror located at the various positions in the monochromator depending of the inventive system. To provide the meaningful diffraction efficiencies and to reduce unwanted higher order lights, the deviation angle subtending the incidence and diffraction beams for the plane grating is varied with the position of the traveling plane mirror with simultaneous rotation located in the front or back of the plane grating with wavelength scanning. The outgoing beam from the monochromator goes through the fixed exit slit and has same beam direction regardless of the scanning wavelength. The combination of properly designed motions of the plane mirror and novel varied-spacing parameters of the inventive plane grating corrects the aberrations and focuses the monochromatic spectral image on the exit slit, enabling measurements at high spectral resolution.

  10. High vertical resolution crosswell seismic imaging

    DOE Patents [OSTI]

    Lazaratos, Spyridon K.

    1999-12-07

    A method for producing high vertical resolution seismic images from crosswell data is disclosed. In accordance with one aspect of the disclosure, a set of vertically spaced, generally horizontally extending continuous layers and associated nodes are defined within a region between two boreholes. The specific number of nodes is selected such that the value of a particular characteristic of the subterranean region at each of the nodes is one which can be determined from the seismic data. Once values are established at the nodes, values of the particular characteristic are assigned to positions between the node points of each layer based on the values at node within that layer and without regard to the values at node points within any other layer. A seismic map is produced using the node values and the assigned values therebetween. In accordance with another aspect of the disclosure, an approximate model of the region is established using direct arrival traveltime data. Thereafter, the approximate model is adjusted using reflected arrival data. In accordance with still another aspect of the disclosure, correction is provided for well deviation. An associated technique which provides improvements in ray tracing is also disclosed.

  11. High-resolution ophthalmic imaging system

    DOE Patents [OSTI]

    Olivier, Scot S. (Livermore, CA); Carrano, Carmen J. (Livermore, CA)

    2007-12-04

    A system for providing an improved resolution retina image comprising an imaging camera for capturing a retina image and a computer system operatively connected to the imaging camera, the computer producing short exposures of the retina image and providing speckle processing of the short exposures to provide the improved resolution retina image. The system comprises the steps of capturing a retina image, producing short exposures of the retina image, and speckle processing the short exposures of the retina image to provide the improved resolution retina image.

  12. High resolution, high rate x-ray spectrometer

    DOE Patents [OSTI]

    Goulding, F.S.; Landis, D.A.

    1983-07-14

    It is an object of the invention to provide a pulse processing system for use with detected signals of a wide dynamic range which is capable of very high counting rates, with high throughput, with excellent energy resolution and a high signal-to-noise ratio. It is a further object to provide a pulse processing system wherein the fast channel resolving time is quite short and substantially independent of the energy of the detected signals. Another object is to provide a pulse processing system having a pile-up rejector circuit which will allow the maximum number of non-interfering pulses to be passed to the output. It is also an object of the invention to provide new methods for generating substantially symmetrically triangular pulses for use in both the main and fast channels of a pulse processing system.

  13. Merging high resolution geophysical and geochemical surveys to...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    combine a suite of high resolution geophysical and geochemical techniques to reduce exploration risk by characterizing hydrothermal alteration, fault geometries and relationships. ...

  14. PROJECT PROFILE: High-resolution Investigations of Transport...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    in Thin-Film Photovoltaic Devices PROJECT PROFILE: High-resolution Investigations of Transport Limiting Defects and Interfaces in Thin-Film Photovoltaic Devices Funding ...

  15. Computational Performance of Ultra-High-Resolution Capability...

    Office of Scientific and Technical Information (OSTI)

    Computational Performance of Ultra-High-Resolution Capability in the Community Earth System Model Citation Details In-Document Search Title: Computational Performance of ...

  16. Goodbye, Watts. Hello, Lumens. (High-Resolution EPS Billboard)

    Broader source: Energy.gov [DOE]

    High-resolution EPS of billboard reading, 'Goodbye Watts. Hello Lumens. The new way to shop for light. Energysaver.gov

  17. Goodbye, Watts. Hello, Lumens. (High-Resolution JPG Billboard)

    Broader source: Energy.gov [DOE]

    High-resolution JPG of billboard reading, 'Goodbye Watts. Hello Lumens. The new way to shop for light. Energysaver.gov

  18. NREL GIS Data: Bhutan High Resolution Wind Resource - Datasets...

    Open Energy Info (EERE)

    NREL GIS Data: Bhutan High Resolution Wind Resource This shapefile containing 50 meter height data has been validated by NREL and wind energy meteorological consultants. However,...

  19. High-resolution measurements of the spatial and temporal evolution...

    Office of Scientific and Technical Information (OSTI)

    temporal evolution of megagauss magnetic fields created in intense short-pulse laser-plasma interactions Citation Details In-Document Search Title: High-resolution measurements...

  20. Lanai high-density irradiance sensor network for characterizing solar

    Office of Scientific and Technical Information (OSTI)

    resource variability of MW-scale PV system. (Conference) | SciTech Connect Conference: Lanai high-density irradiance sensor network for characterizing solar resource variability of MW-scale PV system. Citation Details In-Document Search Title: Lanai high-density irradiance sensor network for characterizing solar resource variability of MW-scale PV system. Sandia National Laboratories (Sandia) and SunPower Corporation (SunPower) have completed design and deployment of an autonomous irradiance

  1. Occult Breast Cancer: Scintimammography with High-Resolution...

    Office of Scientific and Technical Information (OSTI)

    Occult Breast Cancer: Scintimammography with High-Resolution Breast-specific Gamma Camera in Women at High Risk for Breast Cancer Citation Details In-Document Search Title: Occult ...

  2. Exploring electronic structure through high-resolution hard x...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Laboratory Modern high brilliance beamlines coupled with recent advances in hard-x-ray optics are establishing high-resolution hard x-ray spectroscopies as a powerful analytical...

  3. A high-resolution imaging x-ray crystal spectrometer for high...

    Office of Scientific and Technical Information (OSTI)

    A high-resolution imaging x-ray crystal spectrometer for high energy density plasmas Citation Details In-Document Search Title: A high-resolution imaging x-ray crystal spectrometer ...

  4. A high-resolution imaging X-ray crystal spectrometer for high...

    Office of Scientific and Technical Information (OSTI)

    A high-resolution imaging X-ray crystal spectrometer for high energy density (HED) plasmas Citation Details In-Document Search Title: A high-resolution imaging X-ray crystal ...

  5. High resolution data base for use with MAP

    SciTech Connect (OSTI)

    Tapley, W.C.; Harris, D.B.

    1987-05-05

    A high resolution cartographic data base of thw World is available from the CIA. We obtained this data, extracted portions of the data, and produced cartographic files of varying resolutions. The resulting data files are of the proper format for use with MAP (2), our in-house cartographic plotting program.

  6. Invited Article: High resolution angle resolved photoemission with tabletop

    Office of Scientific and Technical Information (OSTI)

    11 eV laser (Journal Article) | SciTech Connect Invited Article: High resolution angle resolved photoemission with tabletop 11 eV laser Citation Details In-Document Search Title: Invited Article: High resolution angle resolved photoemission with tabletop 11 eV laser We developed a table-top vacuum ultraviolet (VUV) laser with 113.778 nm wavelength (10.897 eV) and demonstrated its viability as a photon source for high resolution angle-resolved photoemission spectroscopy (ARPES). This

  7. Sector 3 : High Resolution X-ray Scattering | Advanced Photon...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    & workshops IXN Group Useful Links Current APS status ESAF System GUP System X-Ray Science Division My APS Portal Sector 3 : High Resolution X-ray Scattering Sector 3 is...

  8. Phase contrast in high resolution electron microscopy

    DOE Patents [OSTI]

    Rose, H.H.

    1975-09-23

    This patent relates to a device for developing a phase contrast signal for a scanning transmission electron microscope. The lens system of the microscope is operated in a condition of defocus so that predictable alternate concentric regions of high and low electron density exist in the cone of illumination. Two phase detectors are placed beneath the object inside the cone of illumination, with the first detector having the form of a zone plate, each of its rings covering alternate regions of either higher or lower electron density. The second detector is so configured that it covers the regions of electron density not covered by the first detector. Each detector measures the number of electrons incident thereon and the signal developed by the first detector is subtracted from the signal developed by the record detector to provide a phase contrast signal. (auth)

  9. High-Resolution Photocurrent Microscopy Using Near-Field

    Office of Scientific and Technical Information (OSTI)

    Cathodoluminescence of Quantum Dots. (Journal Article) | SciTech Connect High-Resolution Photocurrent Microscopy Using Near-Field Cathodoluminescence of Quantum Dots. Citation Details In-Document Search Title: High-Resolution Photocurrent Microscopy Using Near-Field Cathodoluminescence of Quantum Dots. Abstract not provided. Authors: Talin, Albert Alec Publication Date: 2013-05-01 OSTI Identifier: 1145404 Report Number(s): SAND2013-4169J 453180 DOE Contract Number: DE-AC04-94AL85000 Resource

  10. PROJECT PROFILE: High-resolution Investigations of Transport Limiting

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Defects and Interfaces in Thin-Film Photovoltaic Devices | Department of Energy High-resolution Investigations of Transport Limiting Defects and Interfaces in Thin-Film Photovoltaic Devices PROJECT PROFILE: High-resolution Investigations of Transport Limiting Defects and Interfaces in Thin-Film Photovoltaic Devices Funding Opportunity: SuNLaMP SunShot Subprogram: Photovoltaics Location: National Renewable Energy Laboratory, Golden, CO Amount Awarded: $1,000,000 This project will develop the

  11. Supercomputers Fuel Global High-Resolution Climate Models

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Supercomputers Fuel Global High-Resolution Climate Models Supercomputers Fuel Global High-Resolution Climate Models Berkeley Lab Researcher Says Climate Science is Entering New Golden Age November 12, 2014 Contact: Julie Chao, jchao@lbl.gov, 510.486.6491 wehnerclimate2 Simulated and observed annual maximum 5 day accumulated precipitation over land points, averaged. Observations are calculated from the period 1979 to 1999. Model results are calculated from the period 1979 to 2005. Not long ago,

  12. High resolution amorphous silicon radiation detectors

    DOE Patents [OSTI]

    Street, R.A.; Kaplan, S.N.; Perez-Mendez, V.

    1992-05-26

    A radiation detector employing amorphous Si:H cells in an array with each detector cell having at least three contiguous layers (n-type, intrinsic, p-type), positioned between two electrodes to which a bias voltage is applied. An energy conversion layer atop the silicon cells intercepts incident radiation and converts radiation energy to light energy of a wavelength to which the silicon cells are responsive. A read-out device, positioned proximate to each detector element in an array allows each such element to be interrogated independently to determine whether radiation has been detected in that cell. The energy conversion material may be a layer of luminescent material having a columnar structure. In one embodiment a column of luminescent material detects the passage therethrough of radiation to be detected and directs a light beam signal to an adjacent a-Si:H film so that detection may be confined to one or more such cells in the array. One or both electrodes may have a comb structure, and the teeth of each electrode comb may be interdigitated for capacitance reduction. The amorphous Si:H film may be replaced by an amorphous Si:Ge:H film in which up to 40 percent of the amorphous material is Ge. Two dimensional arrays may be used in X-ray imaging, CT scanning, crystallography, high energy physics beam tracking, nuclear medicine cameras and autoradiography. 18 figs.

  13. High resolution amorphous silicon radiation detectors

    DOE Patents [OSTI]

    Street, Robert A.; Kaplan, Selig N.; Perez-Mendez, Victor

    1992-01-01

    A radiation detector employing amorphous Si:H cells in an array with each detector cell having at least three contiguous layers (n type, intrinsic, p type), positioned between two electrodes to which a bias voltage is applied. An energy conversion layer atop the silicon cells intercepts incident radiation and converts radiation energy to light energy of a wavelength to which the silicon cells are responsive. A read-out device, positioned proximate to each detector element in an array allows each such element to be interrogated independently to determine whether radiation has been detected in that cell. The energy conversion material may be a layer of luminescent material having a columnar structure. In one embodiment a column of luminescent material detects the passage therethrough of radiation to be detected and directs a light beam signal to an adjacent a-Si:H film so that detection may be confined to one or more such cells in the array. One or both electrodes may have a comb structure, and the teeth of each electrode comb may be interdigitated for capacitance reduction. The amorphous Si:H film may be replaced by an amorphous Si:Ge:H film in which up to 40 percent of the amorphous material is Ge. Two dimensional arrays may be used in X-ray imaging, CT scanning, crystallography, high energy physics beam tracking, nuclear medicine cameras and autoradiography.

  14. Performance of a High Resolution Cavity Beam Position Monitor System

    SciTech Connect (OSTI)

    Walston, S; Boogert, S; Chung, C; Fitsos, P; Frisch, J; Gronberg, J; Hayano, H; Honda, Y; Kolomensky, Y; Lyapin, A; Malton, S; May, J; McCormick, D; Meller, R; Miller, D; Orimoto, T; Ross, M; Slater, M; Smith, S; Smith, T; Terunuma, N; Thomson, M; Urakawa, J; Vogel, V; Ward, D; White, G

    2006-12-18

    It has been estimated that an RF cavity Beam Position Monitor (BPM) could provide a position measurement resolution of less than one nanometer. We have developed a high resolution cavity BPM and associated electronics. A triplet comprised of these BPMs was installed in the extraction line of the Accelerator Test Facility (ATF) at the High Energy Accelerator Research Organization (KEK) for testing with its ultra-low emittance beam. The three BPMs were each rigidly mounted inside an alignment frame on six variable-length struts which could be used to move the BPMs in position and angle. We have developed novel methods for extracting the position and tilt information from the BPM signals including a robust calibration algorithm which is immune to beam jitter. To date, we have demonstrated a position resolution of 15.6 nm and a tilt resolution of 2.1 {micro}rad over a dynamic range of approximately {+-} 20 {micro}m.

  15. Performance of a High Resolution Cavity Beam Position Monitor System

    SciTech Connect (OSTI)

    Walston, Sean; Boogert, Stewart; Chung, Carl; Fitsos, Joe; Frisch, Joe; Gronberg, Jeff; Hayano, Hitoshi; Honda, Yosuke; Kolomensky, Yury; Lyapin, Alexey; Malton, Stephen; May, Justin; McCormick, Douglas; Meller, Robert; Miller, David John; Orimoto, Toyoko; Ross, Marc; Slater, Mark; Smith, Steve; Smith, Tonee; Terunuma, Nobuhiro; /Fermilab /UC, Berkeley /LBL, Berkeley /Cambridge U. /Royal Holloway, U. of London /Cornell U., LNS /LLNL, Livermore /University Coll. London /SLAC /Caltech /KEK, Tsukuba

    2007-06-08

    It has been estimated that an RF cavity Beam Position Monitor (BPM) could provide a position measurement resolution of less than one nanometer. We have developed a high resolution cavity BPM and associated electronics. A triplet comprised of these BPMs was installed in the extraction line of the Accelerator Test Facility (ATF) at the High Energy Accelerator Research Organization (KEK) for testing with its ultra-low emittance beam. The three BPMs were each rigidly mounted inside an alignment frame on six variable-length struts which could be used to move the BPMs in position and angle. We have developed novel methods for extracting the position and tilt information from the BPM signals including a robust calibration algorithm which is immune to beam jitter. To date, we have demonstrated a position resolution of 15.6 nm and a tilt resolution of 2.1 {mu}rad over a dynamic range of approximately {+-} 20 {mu}m.

  16. High-dose neutron irradiation performance of dielectric mirrors

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Nimishakavi Anantha Phani Kiran Kumar; Leonard, Keith J.; Jellison, Jr., Gerald Earle; Snead, Lance Lewis

    2015-05-01

    The study presents the high-dose behavior of dielectric mirrors specifically engineered for radiation-tolerance: alternating layers of Al2O3/SiO2 and HfO2/SiO2 were grown on sapphire substrates and exposed to neutron doses of 1 and 4 dpa at 458 10K in the High Flux Isotope Reactor (HFIR). In comparison to previously reported results, these higher doses of 1 and 4 dpa results in a drastic drop in optical reflectance, caused by a failure of the multilayer coating. HfO2/SiO2 mirrors failed completely when exposed to 1 dpa, whereas the reflectance of Al2O3/SiO2 mirrors reduced to 44%, eventually failing at 4 dpa. Transmission electron microscopymore » (TEM) observation of the Al2O3/SiO2 specimens showed SiO2 layer defects which increases size with irradiation dose. The typical size of each defect was 8 nm in 1 dpa and 42 nm in 4 dpa specimens. Buckling type delamination of the interface between the substrate and first layer was typically observed in both 1 and 4 dpa HfO2/SiO2 specimens. Composition changes across the layers were measured in high resolution scanning-TEM mode using energy dispersive spectroscopy. A significant interdiffusion between the film layers was observed in Al2O3/SiO2 mirror, though less evident in HfO2/SiO2 system. Lastly, the ultimate goal of this work is the provide insight into the radiation-induced failure mechanisms of these mirrors.« less

  17. High Dose Neutron Irradiation Performance of Dielectric Mirrors

    SciTech Connect (OSTI)

    Nimishakavi, Anantha Phani Kiran Kumar; Leonard, Keith J; Jellison Jr, Gerald Earle; Snead, Lance Lewis

    2015-01-01

    The study presents the high-dose behavior of dielectric mirrors specifically engineered for radiation-tolerance: alternating layers of Al2O3/SiO2 and HfO2/SiO2 were grown on sapphire substrates and exposed to neutron doses of 1 and 4 dpa at 458 10K in the High Flux Isotope Reactor (HFIR). In comparison to previously reported results, these higher doses of 1 and 4 dpa results in a drastic drop in optical reflectance, caused by a failure of the multilayer coating. HfO2/SiO2 mirrors failed completely when exposed to 1 dpa, whereas the reflectance of Al2O3/SiO2 mirrors reduced to 44%, eventually failing at 4 dpa. Transmission electron microscopy (TEM) observation of the Al2O3/SiO2 specimens showed SiO2 layer defects which increases size with irradiation dose. The typical size of each defect was 8 nm in 1 dpa and 42 nm in 4 dpa specimens. Buckling type delamination of the interface between the substrate and first layer was typically observed in both 1 and 4 dpa HfO2/SiO2 specimens. Composition changes across the layers were measured in high resolution scanning-TEM mode using energy dispersive spectroscopy. A significant interdiffusion between the film layers was observed in Al2O3/SiO2 mirror, though less evident in HfO2/SiO2 system. The ultimate goal of this work is the provide insight into the radiation-induced failure mechanisms of these mirrors.

  18. High-resolution radiography by means of a hodoscope

    DOE Patents [OSTI]

    De Volpi, Alexander

    1978-01-01

    The fast neutron hodoscope, a device that produces neutron radiographs with coarse space resolution in a short time, is modified to produce neutron or gamma radiographs of relatively thick samples and with high space resolution. The modification comprises motorizing a neutron and gamma collimator to permit a controlled scanning pattern, simultaneous collection of data in a number of hodoscope channels over a period of time, and computerized image reconstruction of the data thus gathered.

  19. Lynx: A High-Resolution Synthetic Aperture Radar

    SciTech Connect (OSTI)

    Doerry, A.W.; Hensley, W.H.; Pace, F.; Stence, J.; Tsunoda, S.I.; Walker, B.C.; Woodring, M.

    1999-03-08

    Lynx is a high resolution, synthetic aperture radar (SAR) that has been designed and built by Sandia National Laboratories in collaboration with General Atomics (GA). Although Lynx may be operated on a wide variety of manned and unmanned platforms, it is primarily intended to be fielded on unmanned aerial vehicles. In particular, it may be operated on the Predator, I-GNAT, or Prowler II platforms manufactured by GA Aeronautical Systems, Inc. The Lynx production weight is less than 120 lb. and has a slant range of 30 km (in 4 mm/hr rain). It has operator selectable resolution and is capable of 0.1 m resolution in spotlight mode and 0.3 m resolution in stripmap mode. In ground moving target indicator mode, the minimum detectable velocity is 6 knots with a minimum target cross-section of 10 dBsm. In coherent change detection mode, Lynx makes registered, complex image comparisons either of 0.1 m resolution (minimum) spotlight images or of 0.3 m resolution (minimum) strip images. The Lynx user interface features a view manager that allows it to pan and zoom like a video camera. Lynx was developed under corporate finding from GA and will be manufactured by GA for both military and commercial applications. The Lynx system architecture will be presented and some of its unique features will be described. Imagery at the finest resolutions in both spotlight and strip modes have been obtained and will also be presented.

  20. High resolution absorption spectroscopy of exploding wire plasmas using an

    Office of Scientific and Technical Information (OSTI)

    x-pinch x-ray source and spherically bent crystal (Journal Article) | DOE PAGES Published Article: High resolution absorption spectroscopy of exploding wire plasmas using an x-pinch x-ray source and spherically bent crystal Title: High resolution absorption spectroscopy of exploding wire plasmas using an x-pinch x-ray source and spherically bent crystal Authors: Knapp, P. F. [1] ; Pikuz, S. A. [1] ; Shelkovenko, T. A. [1] ; Hammer, D. A. [1] ; Hansen, S. B. [2] + Show Author Affiliations

  1. High resolution collimator system for X-ray detector

    DOE Patents [OSTI]

    Eberhard, Jeffrey W.; Cain, Dallas E.

    1987-01-01

    High resolution in an X-ray computerized tomography (CT) inspection system is achieved by using a collimator/detector combination to limit the beam width of the X-ray beam incident on a detector element to the desired resolution width. In a detector such as a high pressure Xenon detector array, a narrow tapered collimator is provided above a wide detector element. The collimator slits have any desired width, as small as a few mils at the top, the slit width is easily controlled, and they are fabricated on standard machines. The slit length determines the slice thickness of the CT image.

  2. Transition-Edge Sensor X-Ray Fluorescence (TES-XRF) for High Resolution

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Material Identification | Princeton Plasma Physics Lab Transition-Edge Sensor X-Ray Fluorescence (TES-XRF) for High Resolution Material Identification X-Ray Fluorescence (XRF) is a technique for material identification. A low energy electron gun bombards a thin foil anode to produce a spectrum of x-rays that irradiate a material sample. The interaction of the x-rays through the photoelectric effect induce a cascade of atomic transitions in the sample material that re-emit characteristic

  3. Unsupervised Feature Learning for High-Resolution Satellite Image Classification

    SciTech Connect (OSTI)

    Cheriyadat, Anil M

    2013-01-01

    The rich data provided by high-resolution satellite imagery allow us to directly model geospatial neighborhoods by understanding their spatial and structural patterns. In this paper we explore an unsupervised feature learning approach to model geospatial neighborhoods for classification purposes. While pixel and object based classification approaches are widely used for satellite image analysis, often these approaches exploit the high-fidelity image data in a limited way. In this paper we extract low-level features to characterize the local neighborhood patterns. We exploit the unlabeled feature measurements in a novel way to learn a set of basis functions to derive new features. The derived sparse feature representation obtained by encoding the measured features in terms of the learned basis function set yields superior classification performance. We applied our technique on two challenging image datasets: ORNL dataset representing one-meter spatial resolution satellite imagery representing five land-use categories and, UCMERCED dataset consisting of 21 different categories representing sub-meter resolution overhead imagery. Our results are highly promising and, in the case of UCMERCED dataset we outperform the best results obtained for this dataset. We show that our feature extraction and learning methods are highly effective in developing a detection system that can be used to automatically scan large-scale high-resolution satellite imagery for detecting large-facility.

  4. High-Resolution Simulations of Coal Injection in A Gasifier

    SciTech Connect (OSTI)

    Li, Tingwen; Gel, Aytekin; Syamlal, M; Guenther, Chris; Pannala, Sreekanth

    2010-01-01

    This study demonstrates an approach to effectively combine high- and low-resolution simulations for design studies of industrial coal gasifier. The flow-field data from a 10 million cell full-scale simulation of a commercial-scale gasifier were used to construct a reduced configuration to economically study the coal injection in detail. High-resolution numerical simulations of the coal injection were performed using the open-source code MFIX running on a high performance computing system. Effects of grid resolution and numerical discretization scheme on the predicted behavior of coal injection and gasification kinetics were analyzed. Pronounced differences were predicted in the devolatilization and steam gasification rates because of different discretization schemes, implying that a high-order numerical scheme is required to predict well the unsteady gasification process on an adequately resolved grid. Computational costs for simulations of varying resolutions are presented to illustrate the trade-off between the accuracy of solution and the time-to-solution, an important consideration when engineering simulations are used for the design of commercial-scale units.

  5. HIGH RESOLUTION RESISTIVITY LEAK DETECTION DATA PROCESSING & EVALUATION MEHTODS & REQUIREMENTS

    SciTech Connect (OSTI)

    SCHOFIELD JS

    2007-10-04

    This document has two purposes: {sm_bullet} Describe how data generated by High Resolution REsistivity (HRR) leak detection (LD) systems deployed during single-shell tank (SST) waste retrieval operations are processed and evaluated. {sm_bullet} Provide the basic review requirements for HRR data when Hrr is deployed as a leak detection method during SST waste retrievals.

  6. LES Modeling of High Resolution Satellite Cloud Spatial and Thermal

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Structure at ARM-SGP site: How well can we Simulate Clouds from Space? LES Modeling of High Resolution Satellite Cloud Spatial and Thermal Structure at ARM-SGP site: How well can we Simulate Clouds from Space? Dubey, Manvendra DOE/Los Alamos National Laboratory Chylek, Petr DOE/Los Alamos National Laboratory Reisner, Jon Los Alamos National Laboratory Porch, William Los Alamos National Laboratory Category: Cloud Properties We report high fidelity observations of the spatial and thermal

  7. High resolution transmission spectroscopy as a diagnostic for Jovian exoplanet atmospheres: constraints from theoretical models

    SciTech Connect (OSTI)

    Kempton, Eliza M.-R.; Perna, Rosalba; Heng, Kevin

    2014-11-01

    We present high resolution transmission spectra of giant planet atmospheres from a coupled three-dimensional (3D) atmospheric dynamics and transmission spectrum model that includes Doppler shifts which arise from winds and planetary motion. We model Jovian planets covering more than two orders of magnitude in incident flux, corresponding to planets with 0.9-55 day orbital periods around solar-type stars. The results of our 3D dynamical models reveal certain aspects of high resolution transmission spectra that are not present in simple one-dimensional (1D) models. We find that the hottest planets experience strong substellar to anti-stellar (SSAS) winds, resulting in transmission spectra with net blueshifts of up to 3 km s{sup 1}, whereas less irradiated planets show almost no net Doppler shifts. We find only minor differences between transmission spectra for atmospheres with temperature inversions and those without. Compared to 1D models, peak line strengths are significantly reduced for the hottest atmospheres owing to Doppler broadening from a combination of rotation (which is faster for close-in planets under the assumption of tidal locking) and atmospheric winds. Finally, high resolution transmission spectra may be useful in studying the atmospheres of exoplanets with optically thick clouds since line cores for very strong transitions should remain optically thick to very high altitude. High resolution transmission spectra are an excellent observational test for the validity of 3D atmospheric dynamics models, because they provide a direct probe of wind structures and heat circulation. Ground-based exoplanet spectroscopy is currently on the verge of being able to verify some of our modeling predictions, most notably the dependence of SSAS winds on insolation. We caution that interpretation of high resolution transmission spectra based on 1D atmospheric models may be inadequate, as 3D atmospheric motions can produce a noticeable effect on the absorption signatures.

  8. Broadband high resolution X-ray spectral analyzer

    DOE Patents [OSTI]

    Silver, Eric H.; Legros, Mark; Madden, Norm W.; Goulding, Fred; Landis, Don

    1998-01-01

    A broad bandwidth high resolution x-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces x-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available x-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for x-ray microanalysis or in research applications such as laboratory and astrophysical x-ray and particle spectroscopy.

  9. Broadband high resolution X-ray spectral analyzer

    DOE Patents [OSTI]

    Silver, E.H.; Legros, M.; Madden, N.W.; Goulding, F.; Landis, D.

    1998-07-07

    A broad bandwidth high resolution X-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces X-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available X-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for X-ray microanalysis or in research applications such as laboratory and astrophysical X-ray and particle spectroscopy. 6 figs.

  10. A high-resolution imaging X-ray crystal spectrometer for high...

    Office of Scientific and Technical Information (OSTI)

    for high energy density (HED) plasmas Citation Details In-Document Search Title: A high-resolution imaging X-ray crystal spectrometer for high energy density (HED) plasmas ...

  11. Irradiation Programs and Test Plans to Assess High-Fluence Irradiation Assisted Stress Corrosion Cracking Susceptibility.

    SciTech Connect (OSTI)

    Teysseyre, Sebastien

    2015-03-01

    . Irradiation assisted stress corrosion cracking (IASCC) is a known issue in current reactors. In a 60 year lifetime, reactor core internals may experience fluence levels up to 15 dpa for boiling water reactors (BWR) and 100+ dpa for pressurized water reactors (PWR). To support a safe operation of our fleet of reactors and maintain their economic viability it is important to be able to predict any evolution of material behaviors as reactors age and therefore fluence accumulated by reactor core component increases. For PWR reactors, the difficulty to predict high fluence behavior comes from the fact that there is not a consensus of the mechanism of IASCC and that little data is available. It is however possible to use the current state of knowledge on the evolution of irradiated microstructure and on the processes that influences IASCC to emit hypotheses. This report identifies several potential changes in microstructure and proposes to identify their potential impact of IASCC. The susceptibility of a component to high fluence IASCC is considered to not only depends on the intrinsic IASCC susceptibility of the component due to radiation effects on the material but to also be related to the evolution of the loading history of the material and interaction with the environment as total fluence increases. Single variation type experiments are proposed to be performed with materials that are representative of PWR condition and with materials irradiated in other conditions. To address the lack of IASCC propagation and initiation data generated with material irradiated in PWR condition, it is proposed to investigate the effect of spectrum and flux rate on the evolution of microstructure. A long term irradiation, aimed to generate a well-controlled irradiation history on a set on selected materials is also proposed for consideration. For BWR, the study of available data permitted to identify an area of concern for long term performance of component. The efficiency of hydrogen water chemistry mitigation technology may decrease as fluence increases for high-stress intensity factors. This report describes a program plan to determine the efficiency of hydrogen water chemistry as a function of the stress intensity factor applied and fluence. The use of existing, available, materials and the generation of additional materials via irradiation in a research reactor are considered.

  12. High-resolution electron microscopy of advanced materials

    SciTech Connect (OSTI)

    Mitchell, T.E.; Kung, H.H.; Sickafus, K.E.; Gray, G.T. III; Field, R.D.; Smith, J.F.

    1997-11-01

    This final report chronicles a three-year, Laboratory Directed Research and Development (LDRD) project at Los Alamos National Laboratory (LANL). The High-Resolution Electron Microscopy Facility has doubled in size and tripled in quality since the beginning of the three-year period. The facility now includes a field-emission scanning electron microscope, a 100 kV field-emission scanning transmission electron microscope (FE-STEM), a 300 kV field-emission high-resolution transmission electron microscope (FE-HRTEM), and a 300 kV analytical transmission electron microscope. A new orientation imaging microscope is being installed. X-ray energy dispersive spectrometers for chemical analysis are available on all four microscopes; parallel electron energy loss spectrometers are operational on the FE-STEM and FE-HRTEM. These systems enable evaluation of local atomic bonding, as well as chemical composition in nanometer-scale regions. The FE-HRTEM has a point-to-point resolution of 1.6 {angstrom}, but the resolution can be pushed to its information limit of 1 {angstrom} by computer reconstruction of a focal series of images. HRTEM has been used to image the atomic structure of defects such as dislocations, grain boundaries, and interfaces in a variety of materials from superconductors and ferroelectrics to structural ceramics and intermetallics.

  13. High-resolution ionization detector and array of such detectors

    DOE Patents [OSTI]

    McGregor, Douglas S. (Ypsilanti, MI); Rojeski, Ronald A. (Pleasanton, CA)

    2001-01-16

    A high-resolution ionization detector and an array of such detectors are described which utilize a reference pattern of conductive or semiconductive material to form interaction, pervious and measurement regions in an ionization substrate of, for example, CdZnTe material. The ionization detector is a room temperature semiconductor radiation detector. Various geometries of such a detector and an array of such detectors produce room temperature operated gamma ray spectrometers with relatively high resolution. For example, a 1 cm.sup.3 detector is capable of measuring .sup.137 Cs 662 keV gamma rays with room temperature energy resolution approaching 2% at FWHM. Two major types of such detectors include a parallel strip semiconductor Frisch grid detector and the geometrically weighted trapezoid prism semiconductor Frisch grid detector. The geometrically weighted detector records room temperature (24.degree. C.) energy resolutions of 2.68% FWHM for .sup.137 Cs 662 keV gamma rays and 2.45% FWHM for .sup.60 Co 1.332 MeV gamma rays. The detectors perform well without any electronic pulse rejection, correction or compensation techniques. The devices operate at room temperature with simple commercially available NIM bin electronics and do not require special preamplifiers or cooling stages for good spectroscopic results.

  14. High throughput screening of ligand binding to macromolecules using high resolution powder diffraction

    DOE Patents [OSTI]

    Von Dreele, Robert B.; D'Amico, Kevin

    2006-10-31

    A process is provided for the high throughput screening of binding of ligands to macromolecules using high resolution powder diffraction data including producing a first sample slurry of a selected polycrystalline macromolecule material and a solvent, producing a second sample slurry of a selected polycrystalline macromolecule material, one or more ligands and the solvent, obtaining a high resolution powder diffraction pattern on each of said first sample slurry and the second sample slurry, and, comparing the high resolution powder diffraction pattern of the first sample slurry and the high resolution powder diffraction pattern of the second sample slurry whereby a difference in the high resolution powder diffraction patterns of the first sample slurry and the second sample slurry provides a positive indication for the formation of a complex between the selected polycrystalline macromolecule material and at least one of the one or more ligands.

  15. Towards Ultra-High Resolution Models of Climate and Weather

    SciTech Connect (OSTI)

    Wehner, Michael; Oliker, Leonid; Shalf, John

    2007-01-01

    We present a speculative extrapolation of the performance aspects of an atmospheric general circulation model to ultra-high resolution and describe alternative technological paths to realize integration of such a model in the relatively near future. Due to a superlinear scaling of the computational burden dictated by stability criterion, the solution of the equations of motion dominate the calculation at ultra-high resolutions. From this extrapolation, it is estimated that a credible kilometer scale atmospheric model would require at least a sustained ten petaflop computer to provide scientifically useful climate simulations. Our design study portends an alternate strategy for practical power-efficient implementations of petaflop scale systems. Embedded processor technology could be exploited to tailor a custom machine designed to ultra-high climate model specifications at relatively affordable cost and power considerations. The major conceptual changes required by a kilometer scale climate model are certain to be difficult to implement. Although the hardware, software, and algorithms are all equally critical in conducting ultra-high climate resolution studies, it is likely that the necessary petaflop computing technology will be available in advance of a credible kilometer scale climate model.

  16. High energy resolution, high angular acceptance crystal monochromator

    DOE Patents [OSTI]

    Alp, E.E.; Mooney, T.M.; Toellner, T.

    1996-06-04

    A 4-bounce dispersive crystal monochromator reduces the bandpass of synchrotron radiation to a 10-50 meV range without sacrificing angular acceptance. The monochromator includes the combination of an asymmetrical channel-cut single crystal of lower order reflection and a symmetrical channel-cut single crystal of higher order reflection in a nested geometric configuration. In the disclosed embodiment, a highly asymmetrically cut ({alpha}=20) outer silicon crystal (4 2 2) with low order reflection is combined with a symmetrically cut inner silicon crystal (10 6 4) with high order reflection to condition a hard x-ray component (5--30 keV) of synchrotron radiation down to the {micro}eV-neV level. Each of the crystals is coupled to the combination of a positioning inchworm and angle encoder via a respective rotation stage for accurate relative positioning of the crystals and precise energy tuning of the monochromator. 7 figs.

  17. High energy resolution, high angular acceptance crystal monochromator

    DOE Patents [OSTI]

    Alp, Ercan E.; Mooney, Timothy M.; Toellner, Thomas

    1996-06-04

    A 4-bounce dispersive crystal monochromator reduces the bandpass of synchrotron radiation to a 10-50 meV range without sacrificing angular acceptance. The monochromator includes the combination of an asymmetrical channel-cut single crystal of lower order reflection and a symmetrical channel-cut single crystal of higher order reflection in a nested geometric configuration. In the disclosed embodiment, a highly asymmetrically cut (.alpha.=20) outer silicon crystal (4 2 2) with low order reflection is combined with a symmetrically cut inner silicon crystal (10 6 4) with high order reflection to condition a hard x-ray component (5-30 keV) of synchrotron radiation down to the .mu.eV-neV level. Each of the crystals is coupled to the combination of a positioning inchworm and angle encoder via a respective rotation stage for accurate relative positioning of the crystals and precise energy tuning of the monochromator.

  18. High resolution reservoir geological modelling using outcrop information

    SciTech Connect (OSTI)

    Zhang Changmin; Lin Kexiang; Liu Huaibo

    1997-08-01

    This is China`s first case study of high resolution reservoir geological modelling using outcrop information. The key of the modelling process is to build a prototype model and using the model as a geological knowledge bank. Outcrop information used in geological modelling including seven aspects: (1) Determining the reservoir framework pattern by sedimentary depositional system and facies analysis; (2) Horizontal correlation based on the lower and higher stand duration of the paleo-lake level; (3) Determining the model`s direction based on the paleocurrent statistics; (4) Estimating the sandbody communication by photomosaic and profiles; (6) Estimating reservoir properties distribution within sandbody by lithofacies analysis; and (7) Building the reservoir model in sandbody scale by architectural element analysis and 3-D sampling. A high resolution reservoir geological model of Youshashan oil field has been built by using this method.

  19. Turbine component casting core with high resolution region

    DOE Patents [OSTI]

    Kamel, Ahmed; Merrill, Gary B.

    2014-08-26

    A hollow turbine engine component with complex internal features can include a first region and a second, high resolution region. The first region can be defined by a first ceramic core piece formed by any conventional process, such as by injection molding or transfer molding. The second region can be defined by a second ceramic core piece formed separately by a method effective to produce high resolution features, such as tomo lithographic molding. The first core piece and the second core piece can be joined by interlocking engagement that once subjected to an intermediate thermal heat treatment process thermally deform to form a three dimensional interlocking joint between the first and second core pieces by allowing thermal creep to irreversibly interlock the first and second core pieces together such that the joint becomes physically locked together providing joint stability through thermal processing.

  20. HIGH SPATIAL RESOLUTION OBSERVATIONS OF LOOPS IN THE SOLAR CORONA

    SciTech Connect (OSTI)

    Brooks, David H.; Ugarte-Urra, Ignacio [College of Science, George Mason University, 4400 University Drive, Fairfax, VA 22030 (United States); Warren, Harry P. [Space Science Division, Naval Research Laboratory, Washington, DC 20375 (United States); Winebarger, Amy R. [NASA Marshall Space Flight Center, ZP 13, Huntsville, AL 35812 (United States)

    2013-08-01

    Understanding how the solar corona is structured is of fundamental importance to determine how the Sun's upper atmosphere is heated to high temperatures. Recent spectroscopic studies have suggested that an instrument with a spatial resolution of 200 km or better is necessary to resolve coronal loops. The High Resolution Coronal Imager (Hi-C) achieved this performance on a rocket flight in 2012 July. We use Hi-C data to measure the Gaussian widths of 91 loops observed in the solar corona and find a distribution that peaks at about 270 km. We also use Atmospheric Imaging Assembly data for a subset of these loops and find temperature distributions that are generally very narrow. These observations provide further evidence that loops in the solar corona are often structured at a scale of several hundred kilometers, well above the spatial scale of many proposed physical mechanisms.

  1. LandScan 2013 High Resolution Global Population Data Set

    Energy Science and Technology Software Center (OSTI)

    2014-07-01

    The LandScan data set is a worldwide population database compiled on a 30"x30" latitude/longitude grid. Census counts (at sub-national level) were apportioned to each grid cell based on likelihood coefficients, which are based on land cover, slope, road proximity, high-resolution imagery, and other data sets. The LandScan data set was developed as part of Oak Ridge National Laboratory (ORNL) Global Population Project for estimating ambient populations at risk.

  2. allows researchers to capture high-resolution images

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    allows researchers to capture high-resolution images - Sandia Energy Energy Search Icon Sandia Home Locations Contact Us Employee Locator Energy & Climate Secure & Sustainable Energy Future Stationary Power Energy Conversion Efficiency Solar Energy Wind Energy Water Power Supercritical CO2 Geothermal Natural Gas Safety, Security & Resilience of the Energy Infrastructure Energy Storage Nuclear Power & Engineering Grid Modernization Battery Testing Nuclear Fuel Cycle Defense Waste

  3. Methodology for Clustering High-Resolution Spatiotemporal Solar Resource Data

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Methodology for Clustering High-Resolution Spatiotemporal Solar Resource Data Dan Getman, Anthony Lopez, Trieu Mai, and Mark Dyson National Renewable Energy Laboratory Technical Report NREL/TP-6A20-63148 September 2015 NREL is a national laboratory of the U.S. Department of Energy Office of Energy Efficiency & Renewable Energy Operated by the Alliance for Sustainable Energy, LLC This report is available at no cost from the National Renewable Energy Laboratory (NREL) at

  4. The Astrophysical Plasmadynamic Explorer (APEX): A High Resolution Spectroscopic Observatory

    SciTech Connect (OSTI)

    Kowalski, M P; Cruddace, R G; Wood, K S; Yentis, D J; Gursky, H; Barbee, T W; Goldstein, W H; Kordas, J F; Fritz, G G; Hunter, W R; Barstow, M A; Bannister, N P; Culhane, J L; Lapington, J S

    2002-07-18

    EUVE and the ROSAT WFC have left a tremendous legacy in astrophysics at EUV wavelengths. More recently, Chandra and XMM-Newton have demonstrated at X-ray wavelengths the power of high-resolution astronomical spectroscopy, which allows the identification of weak emission lines, the measurement of Doppler shifts and line profiles, and the detection of narrow absorption features. This leads to a complete understanding of the density, temperature, abundance, magnetic, and dynamic structure of astrophysical plasmas. However, the termination of the EUVE mission has left a gaping hole in spectral coverage at crucial EUV wavelengths ({approx}100-300 {angstrom}), where hot (10{sup 5}-10{sup 8} K) plasmas radiate most strongly and produce critical spectral diagnostics. CHIPS will fill this hole only partially as it is optimized for diffuse emission and has only moderate resolution (R {approx} 150). For discrete sources, we have successfully flown a follow-on instrument to the EUVE spectrometer (A{sub eff} {approx} 1 cm{sup 2}, R {approx} 400), the high-resolution spectrometer J-PEX(A{sub eff} {approx} 3 cm{sup 2}, R {approx} 3000). Here we build on the J-PEX prototype and present a strawman design for an orbiting spectroscopic observatory, APEX, a SMEX-class instrument containing a suite of 8 spectrometers that together achieve both high effective area (A{sub eff} > 20 cm{sup 2}) and high spectral resolution (R {approx} 10,000) over the range 100-300 {angstrom}. We also discuss alternate configurations for shorter and longer wavelengths.

  5. High-resolution, cryogenic, side-entry type specimen stage

    DOE Patents [OSTI]

    King, Wayne E.; Merkle, Karl L.

    1979-01-01

    A high-resolution, cryogenic side-entry type specimen stage includes a copper block within which a specimen can be positioned in the electron beam of an electron microscope, one end of the copper block constituting a specimen heat exchanger, means for directing a flow of helium at cryogenic temperature into the heat exchanger, and electrical leads running from the specimen to the exterior of the microscope for four point D.C. electrical resistivity measurements.

  6. Irradiation performance of AGR-1 high temperature reactor fuel

    SciTech Connect (OSTI)

    Paul A. Demkowicz; John D. Hunn; Robert N. Morris; Charles A. Baldwin; Philip L. Winston; Jason M. Harp; Scott A. Ploger; Tyler Gerczak; Isabella J. van Rooyen; Fred C. Montgomery; Chinthaka M. Silva

    2014-10-01

    The AGR-1 experiment contained 72 low-enriched uranium oxide/uranium carbide TRISO-coated particle fuel compacts in six capsules irradiated to burnups of 11.2 to 19.5% FIMA, with zero TRISO coating failures detected during the irradiation. The irradiation performance of the fuelincluding the extent of fission product release and the evolution of kernel and coating microstructureswas evaluated based on detailed examination of the irradiation capsules, the fuel compacts, and individual particles. Fractional release of 110mAg from the fuel compacts was often significant, with capsule-average values ranging from 0.01 to 0.38. Analysis of silver release from individual compacts indicated that it was primarily dependent on fuel temperature history. Europium and strontium were released in small amounts through intact coatings, but were found to be significantly retained in the outer pyrocrabon and compact matrix. The capsule-average fractional release from the compacts was 110 4 to 510 4 for 154Eu and 810 7 to 310 5 for 90Sr. The average 134Cs release from compacts was <310 6 when all particles maintained intact SiC. An estimated four particles out of 2.98105 experienced partial cesium release due to SiC failure during the irradiation, driving 134Cs release in two capsules to approximately 10 5. Identification and characterization of these particles has provided unprecedented insight into the nature and causes of SiC coating failure in high-quality TRISO fuel. In general, changes in coating morphology were found to be dominated by the behavior of the buffer and inner pyrolytic carbon (IPyC), and infrequently observed SiC layer damage was usually related to cracks in the IPyC. Palladium attack of the SiC layer was relatively minor, except for the particles that released cesium during irradiation, where SiC corrosion was found adjacent to IPyC cracks. Palladium, silver, and uranium were found in the SiC layer of irradiated particles, and characterization of these elements within the SiC microstructure is the subject of ongoing focused study.

  7. Resolution of a High Performance Cavity Beam Positron Monitor System

    SciTech Connect (OSTI)

    Walston, S.; Chung, C.; Fitsos, P.; Gronberg, J.; Ross, M.; Khainovski, O.; Kolomensky, Y.; Loscutoff, P.; Slater, M.; Thomson, M.; Ward, D.; Boogert, S.; Vogel, V.; Meller, R.; Lyapin, A.; Malton, S.; Miller, D.; Frisch, J.; Hinton, S.; May, J.; McCormick, D.; /SLAC /Caltech /KEK, Tsukuba

    2007-07-06

    International Linear Collider (ILC) interaction region beam sizes and component position stability requirements will be as small as a few nanometers. It is important to the ILC design effort to demonstrate that these tolerances can be achieved--ideally using beam-based stability measurements. It has been estimated that RF cavity beam position monitors (BPMs) could provide position measurement resolutions of less than one nanometer and could form the basis of the desired beam-based stability measurement. We have developed a high resolution RF cavity BPM system. A triplet of these BPMs has been installed in the extraction line of the KEK Accelerator Test Facility (ATF) for testing with its ultra-low emittance beam. A metrology system for the three BPMs was recently installed. This system employed optical encoders to measure each BPM's position and orientation relative to a zero-coefficient of thermal expansion carbon fiber frame and has demonstrated that the three BPMs behave as a rigid-body to less than 5 nm. To date, we have demonstrated a BPM resolution of less than 20 nm over a dynamic range of +/- 20 microns.

  8. Resolution of a High Performance Cavity Beam Position Monitor System

    SciTech Connect (OSTI)

    Walston, S; Chung, C; Fitsos, P; Gronberg, J; Ross, M; Khainovski, O; Kolomensky, Y; Loscutoff, P; Slater, M; Thomson, M; Ward, D; Boogert, S; Vogel, V; Meller, R; Lyapin, A; Malton, S; Miller, D; Frisch, J; Hinton, S; May, J; McCormick, D; Smith, S; Smith, T; White, G; Orimoto, T; Hayano, H; Honda, Y; Terunuma, N; Urakawa, J

    2005-09-12

    International Linear Collider (ILC) interaction region beam sizes and component position stability requirements will be as small as a few nanometers. It is important to the ILC design effort to demonstrate that these tolerances can be achieved - ideally using beam-based stability measurements. It has been estimated that RF cavity beam position monitors (BPMs) could provide position measurement resolutions of less than one nanometer and could form the basis of the desired beam-based stability measurement. We have developed a high resolution RF cavity BPM system. A triplet of these BPMs has been installed in the extraction line of the KEK Accelerator Test Facility (ATF) for testing with its ultra-low emittance beam. A metrology system for the three BPMs was recently installed. This system employed optical encoders to measure each BPM's position and orientation relative to a zero-coefficient of thermal expansion carbon fiber frame and has demonstrated that the three BPMs behave as a rigid-body to less than 5 nm. To date, we have demonstrated a BPM resolution of less than 20 nm over a dynamic range of +/- 20 microns.

  9. Designing arrays for modern high-resolution methods

    SciTech Connect (OSTI)

    Dowla, F.U.

    1987-10-01

    A bearing estimation study of seismic wavefields propagating from a strongly heterogeneous media shows that with the high-resolution MUSIC algorithm the bias of the direction estimate can be reduced by adopting a smaller aperture sub-array. Further, on this sub-array, the bias of the MUSIC algorithm is less than those of the MLM and Bartlett methods. On the full array, the performance for the three different methods are comparable. Improvement in bearing estimation in MUSIC with a reduced aperture might be attributed to increased signal coherency in the array. For methods with less resolution, the improved signal coherency in the smaller array is possible being offset by severe loss of resolution and the presence of weak secondary sources. Building upon the characteristics of real seismic wavefields, a design language has been developed to generate, modify, and test other arrays. Eigenstructures of wavefields and arrays have been studied empirically by simulation of a variety of realistic signals. 6 refs., 5 figs.

  10. ON THE IMPACT OF SUPER RESOLUTION WSR-88D DOPPLER RADAR DATA ASSIMILATION ON HIGH RESOLUTION NUMERICAL MODEL FORECASTS

    SciTech Connect (OSTI)

    Chiswell, S

    2009-01-11

    Assimilation of radar velocity and precipitation fields into high-resolution model simulations can improve precipitation forecasts with decreased 'spin-up' time and improve short-term simulation of boundary layer winds (Benjamin, 2004 & 2007; Xiao, 2008) which is critical to improving plume transport forecasts. Accurate description of wind and turbulence fields is essential to useful atmospheric transport and dispersion results, and any improvement in the accuracy of these fields will make consequence assessment more valuable during both routine operation as well as potential emergency situations. During 2008, the United States National Weather Service (NWS) radars implemented a significant upgrade which increased the real-time level II data resolution to 8 times their previous 'legacy' resolution, from 1 km range gate and 1.0 degree azimuthal resolution to 'super resolution' 250 m range gate and 0.5 degree azimuthal resolution (Fig 1). These radar observations provide reflectivity, velocity and returned power spectra measurements at a range of up to 300 km (460 km for reflectivity) at a frequency of 4-5 minutes and yield up to 13.5 million point observations per level in super-resolution mode. The migration of National Weather Service (NWS) WSR-88D radars to super resolution is expected to improve warning lead times by detecting small scale features sooner with increased reliability; however, current operational mesoscale model domains utilize grid spacing several times larger than the legacy data resolution, and therefore the added resolution of radar data is not fully exploited. The assimilation of super resolution reflectivity and velocity data into high resolution numerical weather model forecasts where grid spacing is comparable to the radar data resolution is investigated here to determine the impact of the improved data resolution on model predictions.

  11. Production of high Resoulution Irradiance Data for Central America...

    Open Energy Info (EERE)

    irradiance (GHI) and direct irradiance (DNI) data sets for the countries of Cuba, El Salvador, Guatemala, Honduras and Nicaragua. Much of our initial effort focused on building up...

  12. High Resolution Atmospheric Modeling for Wind Energy Applications

    SciTech Connect (OSTI)

    Simpson, M; Bulaevskaya, V; Glascoe, L; Singer, M

    2010-03-18

    The ability of the WRF atmospheric model to forecast wind speed over the Nysted wind park was investigated as a function of time. It was found that in the time period we considered (August 1-19, 2008), the model is able to predict wind speeds reasonably accurately for 48 hours ahead, but that its forecast skill deteriorates rapidly after 48 hours. In addition, a preliminary analysis was carried out to investigate the impact of vertical grid resolution on the forecast skill. Our preliminary finding is that increasing vertical grid resolution does not have a significant impact on the forecast skill of the WRF model over Nysted wind park during the period we considered. Additional simulations during this period, as well as during other time periods, will be run in order to validate the results presented here. Wind speed is a difficult parameter to forecast due the interaction of large and small length scale forcing. To accurately forecast the wind speed at a given location, the model must correctly forecast the movement and strength of synoptic systems, as well as the local influence of topography / land use on the wind speed. For example, small deviations in the forecast track or strength of a large-scale low pressure system can result in significant forecast errors for local wind speeds. The purpose of this study is to provide a preliminary baseline of a high-resolution limited area model forecast performance against observations from the Nysted wind park. Validating the numerical weather prediction model performance for past forecasts will give a reasonable measure of expected forecast skill over the Nysted wind park. Also, since the Nysted Wind Park is over water and some distance from the influence of terrain, the impact of high vertical grid spacing for wind speed forecast skill will also be investigated.

  13. Modeling Spatial Dependencies in High-Resolution Overhead Imagery

    SciTech Connect (OSTI)

    Cheriyadat, Anil M; Bright, Eddie A; Vatsavai, Raju

    2011-01-01

    Human settlement regions with different physical and socio-economic attributes exhibit unique spatial characteristics that are often illustrated in high-resolution overhead imageries. For example- size, shape and spatial arrangements of man-made structures are key attributes that vary with respect to the socioeconomic profile of the neighborhood. Successfully modeling these attributes is crucial in developing advanced image understanding systems for interpreting complex aerial scenes. In this paper we present three different approaches to model the spatial context in the overhead imagery. First, we show that the frequency domain of the image can be used to model the spatial context [1]. The shape of the spectral energy contours characterize the scene context and can be exploited as global features. Secondly, we explore a discriminative framework based on the Conditional Random Fields (CRF) [2] to model the spatial context in the overhead imagery. The features derived from the edge orientation distribution calculated for a neighborhood and the associated class labels are used as input features to model the spatial context. Our third approach is based on grouping spatially connected pixels based on the low-level edge primitives to form support-regions [3]. The statistical parameters generated from the support-region feature distributions characterize different geospatial neighborhoods. We apply our approaches on high-resolution overhead imageries. We show that proposed approaches characterize the spatial context in overhead imageries.

  14. High resolution A/D conversion based on piecewise conversion at lower resolution

    DOE Patents [OSTI]

    Terwilliger, Steve

    2012-06-05

    Piecewise conversion of an analog input signal is performed utilizing a plurality of relatively lower bit resolution A/D conversions. The results of this piecewise conversion are interpreted to achieve a relatively higher bit resolution A/D conversion without sampling frequency penalty.

  15. High resolution spectroscopic study of BeΛ10

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Gogami, T.; Chen, C.; Kawama, D.; Achenbach, P.; Ahmidouch, A.; Albayrak, I.; Androic, D.; Asaturyan, A.; Asaturyan, R.; Ates, O.; et al

    2016-03-10

    Spectroscopy of amore » $$^{10}_{\\Lambda}$$Be hypernucleus was carried out at JLab Hall C using the $$(e,e^{\\prime}K^{+})$$ reaction. A new magnetic spectrometer system (SPL+HES+HKS), specifically designed for high resolution hypernuclear spectroscopy, was used to obtain an energy spectrum with a resolution of 0.78 MeV (FWHM). The well-calibrated spectrometer system of the present experiment using the $$p(e,e^{\\prime}K^{+})\\Lambda,\\Sigma^{0}$$ reactions allowed us to determine the energy levels, and the binding energy of the ground state peak (mixture of 1$$^{-}$$ and 2$$^{-}$$ states) was obtained to be B$$_{\\Lambda}$$=8.55$$\\pm$$0.07(stat.)$$\\pm$$0.11(sys.) MeV. Furthermore, the result indicates that the ground state energy is shallower than that of an emulsion study by about 0.5 MeV which provides valuable experimental information on charge symmetry breaking effect in the $$\\Lambda N$$ interaction.« less

  16. A high-resolution imaging X-ray crystal spectrometer for high energy

    Office of Scientific and Technical Information (OSTI)

    density (HED) plasmas (Journal Article) | SciTech Connect Journal Article: A high-resolution imaging X-ray crystal spectrometer for high energy density (HED) plasmas Citation Details In-Document Search Title: A high-resolution imaging X-ray crystal spectrometer for high energy density (HED) plasmas Authors: Chen, H ; Bitter, M ; Hill, K W ; Kerr, S ; Magee, E ; Nagel, S R ; Park, J ; Schneider, M B ; Stone, G ; Williams, G J ; Beiersdorfer, P Publication Date: 2014-05-29 OSTI Identifier:

  17. Bright x-ray sources from laser irradiation of foams with high...

    Office of Scientific and Technical Information (OSTI)

    Bright x-ray sources from laser irradiation of foams with high concentration of Ti Citation Details In-Document Search Title: Bright x-ray sources from laser irradiation of foams...

  18. Bright x-ray sources from laser irradiation of foams with high...

    Office of Scientific and Technical Information (OSTI)

    Bright x-ray sources from laser irradiation of foams with high concentration of Ti Citation Details In-Document Search Title: Bright x-ray sources from laser irradiation of foams ...

  19. Compact and mobile high resolution PET brain imager

    DOE Patents [OSTI]

    Majewski, Stanislaw; Proffitt, James

    2011-02-08

    A brain imager includes a compact ring-like static PET imager mounted in a helmet-like structure. When attached to a patient's head, the helmet-like brain imager maintains the relative head-to-imager geometry fixed through the whole imaging procedure. The brain imaging helmet contains radiation sensors and minimal front-end electronics. A flexible mechanical suspension/harness system supports the weight of the helmet thereby allowing for patient to have limited movements of the head during imaging scans. The compact ring-like PET imager enables very high resolution imaging of neurological brain functions, cancer, and effects of trauma using a rather simple mobile scanner with limited space needs for use and storage.

  20. HIGH-RESOLUTION ATMOSPHERIC ENSEMBLE MODELING AT SRNL

    SciTech Connect (OSTI)

    Buckley, R.; Werth, D.; Chiswell, S.; Etherton, B.

    2011-05-10

    The High-Resolution Mid-Atlantic Forecasting Ensemble (HME) is a federated effort to improve operational forecasts related to precipitation, convection and boundary layer evolution, and fire weather utilizing data and computing resources from a diverse group of cooperating institutions in order to create a mesoscale ensemble from independent members. Collaborating organizations involved in the project include universities, National Weather Service offices, and national laboratories, including the Savannah River National Laboratory (SRNL). The ensemble system is produced from an overlapping numerical weather prediction model domain and parameter subsets provided by each contributing member. The coordination, synthesis, and dissemination of the ensemble information are performed by the Renaissance Computing Institute (RENCI) at the University of North Carolina-Chapel Hill. This paper discusses background related to the HME effort, SRNL participation, and example results available from the RENCI website.

  1. A Versatile High-Resolution X-Ray Imager (HRXI) for Laser-Plasma...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: A Versatile High-Resolution X-Ray Imager (HRXI) for Laser-Plasma Experiments on OMEGA Citation Details In-Document Search Title: A Versatile High-Resolution X-Ray ...

  2. High resolution x-ray and gamma ray imaging using diffraction...

    Office of Scientific and Technical Information (OSTI)

    High resolution x-ray and gamma ray imaging using diffraction lenses with mechanically bent crystals Title: High resolution x-ray and gamma ray imaging using diffraction lenses ...

  3. Structure recognition from high resolution images of ceramic composites

    SciTech Connect (OSTI)

    Ushizima, Daniela; Perciano, Talita; Krishnan, Harinarayan; Loring, Burlen; Bale, Hrishikesh; Parkinson, Dilworth; Sethian, James

    2015-01-05

    Fibers provide exceptional strength-to-weight ratio capabilities when woven into ceramic composites, transforming them into materials with exceptional resistance to high temperature, and high strength combined with improved fracture toughness. Microcracks are inevitable when the material is under strain, which can be imaged using synchrotron X-ray computed micro-tomography (mu-CT) for assessment of material mechanical toughness variation. An important part of this analysis is to recognize fibrillar features. This paper presents algorithms for detecting and quantifying composite cracks and fiber breaks from high-resolution image stacks. First, we propose recognition algorithms to identify the different structures of the composite, including matrix cracks and fibers breaks. Second, we introduce our package F3D for fast filtering of large 3D imagery, implemented in OpenCL to take advantage of graphic cards. Results show that our algorithms automatically identify micro-damage and that the GPU-based implementation introduced here takes minutes, being 17x faster than similar tools on a typical image file.

  4. Which Bulb Is Right for You? (High-Resolution EPS Billboard)

    Broader source: Energy.gov [DOE]

    High-resolution EPS of billboard reading, 'Which bulb is right for you? Save energy, save money. Energysaver.gov.'

  5. Which Bulb Is Right for You? (High-Resolution JPG Billboard)

    Broader source: Energy.gov [DOE]

    HIgh-resolution JPG of billboard reading, 'Which bulb is right for you? Save energy, save money. Energysaver.gov.'

  6. Final report: high resolution lensless 3D imaging of nanostructures with coherent x-rays

    SciTech Connect (OSTI)

    Jacobsen, Chris

    2014-12-07

    Final report on the project "High resolution lensless 3D imaging of nanostructures with coherent x-rays"

  7. Delivery of completed irradiation vehicles and the quality assurance document to the High Flux Isotope Reactor for irradiation

    SciTech Connect (OSTI)

    Petrie, Christian M.; McDuffee, Joel Lee; Katoh, Yutai; Terrani, Kurt A.

    2015-10-01

    This report details the initial fabrication and delivery of two Fuel Cycle Research and Development (FCRD) irradiation capsules (ATFSC01 and ATFSC02), with associated quality assurance documentation, to the High Flux Isotope Reactor (HFIR). The capsules and documentation were delivered by September 30, 2015, thus meeting the deadline for milestone M3FT-15OR0202268. These irradiation experiments are testing silicon carbide composite tubes in order to obtain experimental validation of thermo-mechanical models of stress states in SiC cladding irradiated under a prototypic high heat flux. This document contains a copy of the completed capsule fabrication request sheets, which detail all constituent components, pertinent drawings, etc., along with a detailed summary of the capsule assembly process performed by the Thermal Hydraulics and Irradiation Engineering Group (THIEG) in the Reactor and Nuclear Systems Division (RNSD). A complete fabrication package record is maintained by the THIEG and is available upon request.

  8. Cryogenic, high-resolution x-ray detector with high count rate capability

    DOE Patents [OSTI]

    Frank, Matthias; Mears, Carl A.; Labov, Simon E.; Hiller, Larry J.; Barfknecht, Andrew T.

    2003-03-04

    A cryogenic, high-resolution X-ray detector with high count rate capability has been invented. The new X-ray detector is based on superconducting tunnel junctions (STJs), and operates without thermal stabilization at or below 500 mK. The X-ray detector exhibits good resolution (.about.5-20 eV FWHM) for soft X-rays in the keV region, and is capable of counting at count rates of more than 20,000 counts per second (cps). Simple, FET-based charge amplifiers, current amplifiers, or conventional spectroscopy shaping amplifiers can provide the electronic readout of this X-ray detector.

  9. High dose rate intraluminal irradiation in recurrent endobronchial carcinoma

    SciTech Connect (OSTI)

    Seagren, S.L.; Harrell, J.H.; Horn, R.A.

    1985-12-01

    Palliative therapy for previously irradiated patients with symptomatic recurrent endobronchial malignancy is a difficult problem. We have had the opportunity to treat 20 such patients with high dose rate (50-100 rad/min) endobronchial brachytherapy. Eligible patients had received previous high dose thoracic irradiation (TDF greater than or equal to 90), a performance status of greater than or equal to 50, and symptoms caused by a bronchoscopically defined and implantable lesion. The radiation is produced by a small cobalt-60 source (0.7 Ci) remotely afterloaded by cable control. The source is fed into a 4 mm diameter catheter which is placed with bronchoscopic guidance; it may oscillate if necessary to cover the lesion. A dose of 1,000 rad at 1 cm from the source is delivered. We have performed 22 procedures in 20 patients, four following YAG laser debulking. Most had cough, some with hemoptysis. Eight had dyspnea secondary to obstruction and three had obstructive pneumonitis. In 12, symptoms recurred with a mean time to recurrence of 4.3 months (range 1-9 months). Eighteen patients were followed-up and reexamined via bronchoscope 1-2.5 months following the procedure; two were lost to follow-up. All had at least 50 percent clearance of tumor, and six had complete clearance; most regressions were documented on film or videotape. In six, the palliation was durable. The procedure has been well tolerated with no toxicity. We conclude that palliative endobronchial high dose rate brachytherapy is a useful palliative modality in patients with recurrent endobronchial symptomatic carcinoma.

  10. Small UAV-Acquired, High-resolution, Georeferenced Still Imagery

    SciTech Connect (OSTI)

    Ryan Hruska

    2005-09-01

    Currently, small Unmanned Aerial Vehicles (UAVs) are primarily used for capturing and down-linking real-time video. To date, their role as a low-cost airborne platform for capturing high-resolution, georeferenced still imagery has not been fully utilized. On-going work within the Unmanned Vehicle Systems Program at the Idaho National Laboratory (INL) is attempting to exploit this small UAV-acquired, still imagery potential. Initially, a UAV-based still imagery work flow model was developed that includes initial UAV mission planning, sensor selection, UAV/sensor integration, and imagery collection, processing, and analysis. Components to support each stage of the work flow are also being developed. Critical to use of acquired still imagery is the ability to detect changes between images of the same area over time. To enhance the analysts change detection ability, a UAV-specific, GIS-based change detection system called SADI or System for Analyzing Differences in Imagery is under development. This paper will discuss the associated challenges and approaches to collecting still imagery with small UAVs. Additionally, specific components of the developed work flow system will be described and graphically illustrated using varied examples of small UAV-acquired still imagery.

  11. Long Duration Performance of High Temperature Irradiation Resistant Thermocouples

    SciTech Connect (OSTI)

    Rempe, Joy L; Knudson, D. L.; Condie, K. G.; Wilkins, S. C.

    2007-05-01

    Many advanced nuclear reactor designs require new fuel, cladding, and structural materials. Data are needed to characterize the performance of these new materials in high temperature, radiation conditions. However, traditional methods for measuring temperature inpile degrade at temperatures above 1100 ºC. To address this instrumentation need, the Idaho National Laboratory (INL) developed and evaluated the performance of a high temperature irradiation-resistant thermocouple that contains alloys of molybdenum and niobium. To verify the performance of INL’s recommended thermocouple design, a series of high temperature (from 1200 to 1800 ºC) long duration (up to six months) tests has been initiated. This paper summarizes results from the tests that have been completed. Data are presented from 4000 hour tests conducted at 1200 and 1400 ºC that demonstrate the stability of this thermocouple (less than 2% drift). In addition, post test metallographic examinations are discussed which confirm the compatibility of thermocouple materials throughout these long duration, high temperature tests.

  12. High time-resolution photodetectors for PET applications

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ronzhin, Anatoly

    2016-02-01

    This paper describes recent developments aiming at the improvement of the time resolution of photodetectors used in positron emission tomography (PET). Promising photodetector candidates for future PET-time-of-flight (TOF) applications are also discussed.

  13. High resolution PFPE-based molding High resolution PFPE-based molding High resolution PFPE-based molding techniques for nanofabrication of high pattern density sub-20 nm features: A fundamental materials approach

    SciTech Connect (OSTI)

    Williams, Stuart S [University of North Carolina, Chapel Hill; Samulski, Edward [University of North Carolina, Chapel Hill; Lopez, Renee [University of North Carolina, Chapel Hill; Ruiz, Ricardo [Hitachi; DeSimone, Joseph [University of North Carolina, Chapel Hill; Retterer, Scott T [ORNL

    2010-01-01

    ABSTRACT. Described herein is the development and investigation of PFPE-based elastomers for high resolution replica molding applications. The modulus of the elastomeric materials was increased through synthetic and additive approaches while maintaining relatively low surface energies (<25 mN/m). Using practically relevant large area master templates, we show that the resolution of the molds is strongly dependant upon the elastomeric mold modulus. A composite mold approach was used to form flexible molds out of stiff, high modulus materials that allow for replication of sub-20 nm post structures. Sub-100 nm line grating master templates, formed using e-beam lithography, were used to determine the experimental stability of the molding materials. It was observed that as the feature spacing decreased, high modulus composite molds were able to effectively replicate the nano-grating structures without cracking or tear-out defects that typically occur with high modulus elastomers.

  14. Study of fish response using particle image velocimetry and high-speed, high-resolution imaging

    SciTech Connect (OSTI)

    Deng, Z.; Richmond, M. C.; Mueller, R. P.; Gruensch, G. R.

    2004-10-01

    Fish swimming has fascinated both engineers and fish biologists for decades. Digital particle image velocimetry (DPIV) and high-speed, high-resolution digital imaging are recently developed analysis tools that can help engineers and biologists better understand how fish respond to turbulent environments. This report details studies to evaluate DPIV. The studies included a review of existing literature on DPIV, preliminary studies to test the feasibility of using DPIV conducted at our Flow Biology Laboratory in Richland, Washington September through December 2003, and applications of high-speed, high-resolution digital imaging with advanced motion analysis to investigations of fish injury mechanisms in turbulent shear flows and bead trajectories in laboratory physical models. Several conclusions were drawn based on these studies, which are summarized as recommendations for proposed research at the end of this report.

  15. Johann Spectrometer for High Resolution X-ray Spectroscopy

    SciTech Connect (OSTI)

    Machek, Pavel; Froeba, Michael; Welter, Edmund; Caliebe, Wolfgang; Brueggmann, Ulf; Draeger, Guenter

    2007-01-19

    A newly designed vacuum Johann spectrometer with a large focusing analyzer crystal for inelastic x-ray scattering and high resolution fluorescence spectroscopy has been installed at the DORIS III storage ring. Spherically bent crystals with a maximum diameter of 125 mm, and cylindrically bent crystals are employed as dispersive optical elements. Standard radius of curvature of the crystals is 1000 mm, however, the design of the mechanical components also facilitates measurements with smaller and larger bending radii. Up to four crystals are mounted on a revolving crystal changer which enables crystal changes without breaking the vacuum. The spectrometer works at fixed Bragg angle. It is preferably designed for the measurements in non-scanning mode with a broad beam spot, and offers a large flexibility to set the sample to the optimum position inside the Rowland circle. A deep depletion CCD camera is employed as a position sensitive detector to collect the energy-analyzed photons on the circumference of the Rowland circle. The vacuum in the spectrometer tank is typically 10-6 mbar. The sample chamber is separated from the tank either by 25 {mu}m thick Kapton windows, which allows samples to be measured under ambient conditions, or by two gate valves. The spectrometer is currently installed at wiggler beamline W1 whose working range is 4-10.5 keV with typical flux at the sample of 5x1010photons/s/mm2. The capabilities of the spectrometer are illustrated by resonant inelastic experiments on 3d transition metals and rare earth compounds, and by chemical shift measurements on chromium compounds.

  16. High resolution x-ray and gamma ray imaging using diffraction lenses with

    Office of Scientific and Technical Information (OSTI)

    mechanically bent crystals (Patent) | DOEPatents High resolution x-ray and gamma ray imaging using diffraction lenses with mechanically bent crystals Title: High resolution x-ray and gamma ray imaging using diffraction lenses with mechanically bent crystals A method for high spatial resolution imaging of a plurality of sources of x-ray and gamma-ray radiation is provided. High quality mechanically bent diffracting crystals of 0.1 mm radial width are used for focusing the radiation and

  17. Small Specimen Data from a High Temperature HFIR Irradiation Experiment

    SciTech Connect (OSTI)

    Burchell, Timothy D; McDuffee, Joel Lee; Thoms, Kenneth R

    2014-01-01

    The HTV capsule is a High Flux Isotope Reactor (HFIR) target-rod capsule designed to operate at very high temperatures. The graphite containing section of the capsule (in core) is approximately 18 inches (457.2 mm) long and is separated into eight temperature zones. The specimen diameters within each zone are set to achieve the desired gas gap and hence design temperature (900 C, 1200 C or 1500 C). The capsule has five zones containing 0.400 inch (10.16 mm) diameter specimens, two zones containing 0.350 inch (8.89 mm) diameter specimens and one zone containing 0.300 inch (7.62 mm) diameter specimens. The zones have been distributed within the experiment to optimize the gamma heating from the HFIR core as well as minimize the axial heat flow in the capsule. Consequently, there are two 900 C zones, three 1200 C zones, and three 1500 C zones within the HTV capsule. Each zone contains nine specimens 0.210 0.002 inches (5.334 mm) in length. The capsule will be irradiated to a peak dose of 3.17 displacements per atom. The HTV specimens include samples of the following graphite grades: SGL Carbon s NBG-17 and NBG-18, GrafTech s PCEA, Toyo Tanso s IG-110, Mersen s 2114 and the reference grade H-451 (SGL Carbon). As part of the pre-irradiation program the specimens were characterized using ASTM Standards C559 for bulk density, and ASTM C769 for approximate Young s modulus from the sonic velocity. The probe frequency used for the determination of time of flight of the ultrasonic signal was 2.25 MHz. Marked volume (specimen diameter) effects were noted for both bulk density (increased with increasing specimen volume or diameter) and Dynamic Young s modulus (decreased with increasing specimen volume or diameter). These trends are extended by adding the property vs. diameter data for unirradiated AGC-1 creep specimens (nominally 12.5 mm-diameter x 25.4 mm-length). The relatively large reduction in Dynamic Young s Modulus was surprising given the trend for increasing density with increasing volume. The graphite-filler particle size was noted to be influential in the volume dependency data, with finer grained graphites showing the least specimen volume/diameter effect. Here the volume dependency trends are discussed in terms of the graphite s filler-particle size and texture.

  18. Updated flux information for neutron scattering and irradiation facilities at the BNL High Flux Beam Reactor

    SciTech Connect (OSTI)

    Holden, N.E.; Hu, J.P.; Reciniello, R.N.; Sengupta, S.; Greenwood, L.R.; Farrell, K.

    1997-08-01

    The HFBR is a heavy water, D{sub 2}O, cooled and moderated reactor with twenty-eight fuel elements containing a maximum of 9.8 kilograms of {sup 235}U. While most reactors attempt to minimize the escape of neutrons from the core, the HFBR`s D{sub 2}O design allows the thermal neutron flux to peak in the reflector region and maximizes the number of thermal neutrons available to nine horizontal external beams, H-1 to H-9, used for neutron scattering and capture reactions, supporting physics, chemistry and biology experiments. All horizontal beam tubes were built tangential to the direction of the emerging neutrons, except for the H-2 beam tube, which looks directly at the core and has been used for neutron cross section measurements utilizing fast neutrons and for the TRISTAN fission product studies. In recent years, there have been some beam modifications and new instrumentation introduced at the HFBR. A high resolution neutron powder diffractometer instrument is now operating with a resolution of 5 {times} 10{sup {minus}4} at horizontal beam line H-1. To study scattering from liquid surfaces, a neutron reflection spectrometer was introduced on the CNF beam line at H-9. In the past year, a fourth beam line has been added to the CNF line at H-9. The existing beam plug at the H-6 beam line has recently been removed and a new plug, which will feature super mirrored surfaces, is now being installed. Last year, the vertical beam thimble, V-13, a fixed port filled with thirty year old samples used for HFBR material surveillance studies was replaced by a new thimble and charging station at the core edge creating an irradiation facility to substitute for the original V-13. A neutron dosimetry program has begun to measure and calculate the energy dependent neutron and gamma ray flux densities and/or dose rates at horizontal beam lines and vertical irradiation thimbles.

  19. A high-resolution imaging x-ray crystal spectrometer for high energy density plasmas

    SciTech Connect (OSTI)

    Chen, Hui E-mail: bitter@pppl.gov; Magee, E.; Nagel, S. R.; Park, J.; Schneider, M. B.; Stone, G.; Williams, G. J.; Beiersdorfer, P.; Bitter, M. E-mail: bitter@pppl.gov; Hill, K. W.; Kerr, S.

    2014-11-15

    Adapting a concept developed for magnetic confinement fusion experiments, an imaging crystal spectrometer has been designed and tested for HED plasmas. The instrument uses a spherically bent quartz [211] crystal with radius of curvature of 490.8 mm. The instrument was tested at the Titan laser at Lawrence Livermore National Laboratory by irradiating titanium slabs with laser intensities of 10{sup 19}–10{sup 20} W/cm{sup 2}. He-like and Li-like Ti lines were recorded, from which the spectrometer performance was evaluated. This spectrometer provides very high spectral resolving power (E/dE > 7000) while acquiring a one-dimensional image of the source.

  20. Probe for high resolution NMR with sample reorientation

    DOE Patents [OSTI]

    Pines, Alexander; Samoson, Ago

    1990-01-01

    An improved NMR probe and method are described which substantially improve the resolution of NMR measurements made on powdered or amorphous or otherwise orientationally disordered samples. The apparatus mechanically varies the orientation of the sample such that the time average of two or more sets of spherical harmonic functions are zero.

  1. Probe for high resolution NMR with sample reorientation

    DOE Patents [OSTI]

    Pines, A.; Samoson, A.

    1990-02-06

    An improved NMR probe and method are described which substantially improve the resolution of NMR measurements made on powdered or amorphous or otherwise orientationally disordered samples. The apparatus mechanically varies the orientation of the sample such that the time average of two or more sets of spherical harmonic functions are zero. 8 figs.

  2. Experiences with the High Energy Resolution Optics (HERO) update on a

    Office of Scientific and Technical Information (OSTI)

    physical electronics 690 auger system. (Conference) | SciTech Connect Experiences with the High Energy Resolution Optics (HERO) update on a physical electronics 690 auger system. Citation Details In-Document Search Title: Experiences with the High Energy Resolution Optics (HERO) update on a physical electronics 690 auger system. We will present our experiences with the new High Energy Resolution Optics (HERO) upgrade on a Physical Electronics Auger 690 system. This upgrade allows the single

  3. A high-resolution imaging X-ray crystal spectrometer for intense...

    Office of Scientific and Technical Information (OSTI)

    for intense laser plasma interaction experiments Citation Details In-Document Search Title: A high-resolution imaging X-ray crystal spectrometer for intense laser plasma ...

  4. D&D Toolbox Robotic Deployment of High Resolution Laser Imaging...

    Office of Environmental Management (EM)

    PBS SR-0040 The robotically deployed laser surveying system was demonstrated in the ... Robotic Deployment of High Resolution Laser Imaging for Characterization Challenge The ...

  5. A high-resolution imaging X-ray crystal spectrometer for intense...

    Office of Scientific and Technical Information (OSTI)

    intense laser plasma interaction experiments Citation Details In-Document Search Title: A high-resolution imaging X-ray crystal spectrometer for intense laser plasma interaction ...

  6. Characterization of spatially resolved high resolution x-ray...

    Office of Scientific and Technical Information (OSTI)

    spectrometers for high energy density physics and light source experiments Citation ... spectrometers for high energy density physics and light source experiments A high ...

  7. Automated analysis for microcalcifications in high resolution digital mammograms

    DOE Patents [OSTI]

    Mascio, L.N.

    1996-12-17

    A method is disclosed for automatically locating microcalcifications indicating breast cancer. The invention assists mammographers in finding very subtle microcalcifications and in recognizing the pattern formed by all the microcalcifications. It also draws attention to microcalcifications that might be overlooked because a more prominent feature draws attention away from an important object. A new filter has been designed to weed out false positives in one of the steps of the method. Previously, iterative selection threshold was used to separate microcalcifications from the spurious signals resulting from texture or other background. A Selective Erosion or Enhancement (SEE) Filter has been invented to improve this step. Since the algorithm detects areas containing potential calcifications on the mammogram, it can be used to determine which areas need be stored at the highest resolution available, while, in addition, the full mammogram can be reduced to an appropriate resolution for the remaining cancer signs. 8 figs.

  8. Automated analysis for microcalcifications in high resolution digital mammograms

    DOE Patents [OSTI]

    Mascio, Laura N.

    1996-01-01

    A method for automatically locating microcalcifications indicating breast cancer. The invention assists mammographers in finding very subtle microcalcifications and in recognizing the pattern formed by all the microcalcifications. It also draws attention to microcalcifications that might be overlooked because a more prominent feature draws attention away from an important object. A new filter has been designed to weed out false positives in one of the steps of the method. Previously, iterative selection threshold was used to separate microcalcifications from the spurious signals resulting from texture or other background. A Selective Erosion or Enhancement (SEE) Filter has been invented to improve this step. Since the algorithm detects areas containing potential calcifications on the mammogram, it can be used to determine which areas need be stored at the highest resolution available, while, in addition, the full mammogram can be reduced to an appropriate resolution for the remaining cancer signs.

  9. Methodology for Clustering High-Resolution Spatiotemporal Solar Resource Data

    SciTech Connect (OSTI)

    Getman, Dan; Lopez, Anthony; Mai, Trieu; Dyson, Mark

    2015-09-01

    In this report, we introduce a methodology to achieve multiple levels of spatial resolution reduction of solar resource data, with minimal impact on data variability, for use in energy systems modeling. The selection of an appropriate clustering algorithm, parameter selection including cluster size, methods of temporal data segmentation, and methods of cluster evaluation are explored in the context of a repeatable process. In describing this process, we illustrate the steps in creating a reduced resolution, but still viable, dataset to support energy systems modeling, e.g. capacity expansion or production cost modeling. This process is demonstrated through the use of a solar resource dataset; however, the methods are applicable to other resource data represented through spatiotemporal grids, including wind data. In addition to energy modeling, the techniques demonstrated in this paper can be used in a novel top-down approach to assess renewable resources within many other contexts that leverage variability in resource data but require reduction in spatial resolution to accommodate modeling or computing constraints.

  10. Irradiation and Bevacizumab in High-Grade Glioma Retreatment Settings

    SciTech Connect (OSTI)

    Niyazi, Maximilian; Ganswindt, Ute; Schwarz, Silke Birgit [Department of Radiation Oncology, Ludwig-Maximilians-University Munich, Munich (Germany); Kreth, Friedrich-Wilhelm; Tonn, Joerg-Christian [Department of Neurosurgery, Ludwig-Maximilians-University Munich, Munich (Germany); Geisler, Julia; Fougere, Christian la [Department of Nuclear Medicine, Ludwig-Maximilians-University Munich, Munich (Germany); Ertl, Lorenz; Linn, Jennifer [Department of Neuroradiology, Ludwig-Maximilians-University Munich, Munich (Germany); Siefert, Axel [Department of Radiation Oncology, Ludwig-Maximilians-University Munich, Munich (Germany); Belka, Claus, E-mail: claus.belka@med.uni-muenchen.de [Department of Radiation Oncology, Ludwig-Maximilians-University Munich, Munich (Germany)

    2012-01-01

    Purpose: Reirradiation is a treatment option for recurrent high-grade glioma with proven but limited effectiveness. Therapies directed against vascular endothelial growth factor have been shown to exert certain efficacy in combination with chemotherapy and have been safely tested in combination with radiotherapy in a small cohort of patients. To study the feasibility of reirradiation combined with bevacizumab treatment, the toxicity and treatment outcomes of this approach were analyzed retrospectively. Patients and Methods: After previous treatment with standard radiotherapy (with or without temozolomide) patients with recurrent malignant glioma received bevacizumab (10 mg/kg intravenous) on Day 1 and Day 15 during radiotherapy. Maintenance therapy was selected based on individual considerations, and mainly bevacizumab-containing regimens were chosen. Patients received 36 Gy in 18 fractions. Results: The data of the medical charts of the 30 patients were analyzed retrospectively. All were irradiated in a single institution and received either bevacizumab (n = 20), no additional substance (n = 7), or temozolomide (n = 3). Reirradiation was tolerated well, regardless of the added drug. In 1 patient treated with bevacizumab, a wound dehiscence occurred. Overall survival was significantly better in patients receiving bevacizumab (p = 0.03, log-rank test). In a multivariate proportional hazards Cox model, bevacizumab, Karnovsky performance status, and World Health Organization grade at relapse turned out to be the most important predictors for overall survival. Conclusion: Reirradiation with bevacizumab is a feasible and effective treatment for patients with recurrent high-grade gliomas. A randomized trial is warranted to finally answer the question whether bevacizumab adds substantial benefit to a radiotherapeutic retreatment setting.

  11. High-order multilayer coated blazed gratings for high resolution soft x-ray spectroscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Voronov, Dmitriy L.; Goray, Leonid I.; Warwick, Tony; Yashchuk, Valeriy V.; Padmore, Howard A.

    2015-02-17

    A grand challenge in soft x-ray spectroscopy is to drive the resolving power of monochromators and spectrometers from the 104 achieved routinely today to well above 105. This need is driven mainly by the requirements of a new technique that is set to have enormous impact in condensed matter physics, Resonant Inelastic X-ray Scattering (RIXS). Unlike x-ray absorption spectroscopy, RIXS is not limited by an energy resolution dictated by the core-hole lifetime in the excitation process. Using much higher resolving power than used for normal x-ray absorption spectroscopy enables access to the energy scale of soft excitations in matter. Thesemoreexcitations such as magnons and phonons drive the collective phenomena seen in correlated electronic materials such as high temperature superconductors. RIXS opens a new path to study these excitations at a level of detail not formerly possible. However, as the process involves resonant excitation at an energy of around 1 keV, and the energy scale of the excitations one would like to see are at the meV level, to fully utilize the technique requires the development of monochromators and spectrometers with one to two orders of magnitude higher energy resolution than has been conventionally possible. Here we investigate the detailed diffraction characteristics of multilayer blazed gratings. These elements offer potentially revolutionary performance as the dispersive element in ultra-high resolution x-ray spectroscopy. In doing so, we have established a roadmap for the complete optimization of the grating design. Traditionally 1st order gratings are used in the soft x-ray region, but we show that as in the optical domain, one can work in very high spectral orders and thus dramatically improve resolution without significant loss in efficiency.less

  12. On the feasibility of comprehensive high-resolution 3D remote dosimetry

    SciTech Connect (OSTI)

    Juang, Titania; Grant, Ryan; Adamovics, John; Ibbott, Geoffrey; Oldham, Mark

    2014-07-15

    Purpose: This study investigates the feasibility of remote high-resolution 3D dosimetry with the PRESAGE/Optical-CT system. In remote dosimetry, dosimeters are shipped out from a central base institution to a remote institution for irradiation, then shipped back to the base institution for subsequent readout and analysis. Methods: Two nominally identical optical-CT scanners for 3D dosimetry were constructed and placed at the base (Duke University) and remote (Radiological Physics Center) institutions. Two formulations of PRESAGE (SS1, SS2) radiochromic dosimeters were investigated. Higher sensitivity was expected in SS1, which had higher initiator content (0.25% bromotrichloromethane), while greater temporal stability was expected in SS2. Four unirradiated PRESAGE dosimeters (two per formulation, cylindrical dimensions 11 cm diameter, 8.59.5 cm length) were imaged at the base institution, then shipped to the remote institution for planning and irradiation. Each dosimeter was irradiated with the same simple treatment plan: an isocentric 3-field cross arrangement of 4 4 cm open 6 MV beams configured as parallel opposed laterals with an anterior beam. This simple plan was amenable to accurate and repeatable setup, as well as accurate dose modeling by a commissioned treatment planning system (Pinnacle). After irradiation and subsequent (within 1 h) optical-CT readout at the remote institution, the dosimeters were shipped back to the base institution for remote dosimetry readout 3 days postirradiation. Measured on-site and remote relative 3D dose distributions were registered to the Pinnacle dose calculation, which served as the reference distribution for 3D gamma calculations with passing criteria of 5%/2 mm, 3%/3 mm, and 3%/2 mm with a 10% dose threshold. Gamma passing rates, dose profiles, and color-maps were all used to assess and compare the performance of both PRESAGE formulations for remote dosimetry. Results: The best agreements between the Pinnacle plan and dosimeter readout were observed in PRESAGE formulation SS2. Under 3%/3 mm 3D gamma passing criteria, passing rates were 91.5% 3.6% (SS1) and 97.4% 2.2% (SS2) for immediate on-site dosimetry, 96.7% 2.4% (SS1) and 97.6% 0.6% (SS2) for remote dosimetry. These passing rates are well within TG119 recommendations (88%90% passing). Under the more stringent criteria of 3%/2 mm, there is a pronounced difference [8.0 percentage points (pp)] between SS1 formulation passing rates for immediate and remote dosimetry while the SS2 formulation maintains both higher passing rates and consistency between immediate and remote results (differences ? 1.2 pp) at all metrics. Both PRESAGE formulations under study maintained high linearity of dose response (R{sup 2} > 0.996) for 18 Gy over 14 days with response slope consistency within 4.9% (SS1) and 6.6% (SS2), and a relative dose distribution that remained stable over time was demonstrated in the SS2 dosimeters. Conclusions: Remote 3D dosimetry was shown to be feasible with a PRESAGE dosimeter formulation (SS2) that exhibited relative temporal stability and high accuracy when read off-site 3 days postirradiation. Characterization of the SS2 dose response demonstrated linearity (R{sup 2} > 0.998) over 14 days and suggests accurate readout over longer periods of time would be possible. This result provides a foundation for future investigations using remote dosimetry to study the accuracy of advanced radiation treatments. Further work is planned to characterize dosimeter reproducibility and dose response over longer periods of time.

  13. Design and performance of AERHA, a high acceptance high resolution soft x-ray spectrometer

    SciTech Connect (OSTI)

    Chiuzbăian, Sorin G. Hague, Coryn F.; Brignolo, Stefania; Baumier, Cédric; Lüning, Jan; CNRS, UMR 7614, Laboratoire de Chimie Physique-Matière et Rayonnement, 11 rue Pierre et Marie Curie, F-75005 Paris; Synchrotron SOLEIL, L’Orme des Merisiers, Saint-Aubin, B.P. 48, F-91192 Gif-sur-Yvette ; Avila, Antoine; Delaunay, Renaud; Mariot, Jean-Michel; CNRS, UMR 7614, Laboratoire de Chimie Physique-Matière et Rayonnement, 11 rue Pierre et Marie Curie, F-75005 Paris ; Jaouen, Nicolas; Polack, François; Thomasset, Muriel; Lagarde, Bruno; Nicolaou, Alessandro; Sacchi, Maurizio; Sorbonne Universités, UPMC Univ Paris 06, UMR 7588, Institut des NanoSciences de Paris, 4 place Jussieu, F-75252 Paris Cedex 05; CNRS, UMR 7588, Institut des NanoSciences de Paris, 4 place Jussieu, F-75252 Paris Cedex 05

    2014-04-15

    A soft x-ray spectrometer based on the use of an elliptical focusing mirror and a plane varied line spacing grating is described. It achieves both high resolution and high overall efficiency while remaining relatively compact. The instrument is dedicated to resonant inelastic x-ray scattering studies. We set out how this optical arrangement was judged best able to guarantee performance for the 50 − 1000 eV range within achievable fabrication targets. The AERHA (adjustable energy resolution high acceptance) spectrometer operates with an effective angular acceptance between 100 and 250 μsr (energy dependent) and a resolving power well in excess of 5000 according to the Rayleigh criterion. The high angular acceptance is obtained by means of a collecting pre-mirror. Three scattering geometries are available to enable momentum dependent measurements with 135°, 90°, and 50° scattering angles. The instrument operates on the Synchrotron SOLEIL SEXTANTS beamline which serves as a high photon flux 2 × 200 μm{sup 2} focal spot source with full polarization control.

  14. Toroidal magnetic detector for high resolution measurement of muon momenta

    DOE Patents [OSTI]

    Bonanos, Peter (East Brunswick, NJ)

    1992-01-01

    A muon detector system including central and end air-core superconducting toroids and muon detectors enclosing a central calorimeter/detector. Muon detectors are positioned outside of toroids and all muon trajectory measurements are made in a nonmagnetic environment. Internal support for each magnet structure is provided by sheets, located at frequent and regularly spaced azimuthal planes, which interconnect the structural walls of the toroidal magnets. In a preferred embodiment, the shape of the toroidal magnet volume is adjusted to provide constant resolution over a wide range of rapidity.

  15. Toroidal magnetic detector for high resolution measurement of muon momenta

    DOE Patents [OSTI]

    Bonanos, P.

    1992-01-07

    A muon detector system including central and end air-core superconducting toroids and muon detectors enclosing a central calorimeter/detector. Muon detectors are positioned outside of toroids and all muon trajectory measurements are made in a nonmagnetic environment. Internal support for each magnet structure is provided by sheets, located at frequent and regularly spaced azimuthal planes, which interconnect the structural walls of the toroidal magnets. In a preferred embodiment, the shape of the toroidal magnet volume is adjusted to provide constant resolution over a wide range of rapidity. 4 figs.

  16. A High Resolution Hydrometer Phase Classifier Based on Analysis...

    Office of Scientific and Technical Information (OSTI)

    Satellite-based retrievals of cloudmore phase in high latitudes are often hindered by the highly reflecting ice-covered ground and persistent temperature inversions. From the ...

  17. Irradiation response of commercial, high-Tc superconducting tapes: Electromagnetic transport properties

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Gapud, A. A.; Greenwood, N. T.; Alexander, J. A.; Khan, A.; Leonard, K. J.; Aytug, T.; List III, F. A.; Rupich, M. W.; Zhang, Y.

    2015-07-01

    Effects of low dose irradiation on the electrical transport current properties of commercially available high-temperature superconducting, coated-conductor tapes were investigated, in view of potential applications in the irradiative environment of fusion reactors. Three different tapes, each with unique as-grown flux-pinning structures, were irradiated with Au and Ni ions at energies that provide a range of damage effects, with accumulated damage levels near that expected for conductors in a fusion reactor environment. Measurements using transport current determined the pre- and post-irradiation resistivity, critical current density, and pinning force density, yielding critical temperatures, irreversibility lines, and inferred vortex creep rates. Results showmore » that at the irradiation damage levels tested, any detriment to as-grown pre-irradiation properties is modest; indeed in one case already-superior pinning forces are enhanced, leading to higher critical currents.« less

  18. Irradiation of commercial, high-Tc superconducting tape for potential fusion applications: electromagnetic transport properties

    SciTech Connect (OSTI)

    Aytug, Tolga [ORNL; Gapud, Albert A. [University of South Alabama, Mobile; List III, Frederick Alyious [ORNL; Leonard, Keith J [ORNL; Rupich, Marty [American Superconductor Corporation, Westborough, MA; Zhang, Yanwen [ORNL; Greenwood, N T [University of South Alabama, Mobile; Alexander, J A [University of South Alabama, Mobile; Khan, A [University of South Alabama, Mobile

    2015-01-01

    Effects of low dose irradiation on the electrical transport current properties of commercially available high-temperature superconducting, coated-conductor tapes were investigated, in view of potential applications in the irradiative environment of fusion reactors. Three different tapes, each with unique as-grown flux-pinning structures, were irradiated with Au and Ni ions at energies that provide a range of damage effects, with accumulated damage levels near that expected for conductors in a fusion reactor environment. Measurements using transport current determined the pre- and post-irradiation resistivity, critical current density, and pinning force density, yielding critical temperatures, irreversibility lines, and inferred vortex creep rates. Results show that at the irradiation damage levels tested, any detriment to as-grown pre-irradiation properties is modest; indeed in one case already-superior pinning forces are enhanced, leading to higher critical currents.

  19. A versatile high-resolution x-ray imager (HRXI) for laser-plasma...

    Office of Scientific and Technical Information (OSTI)

    x-ray imager (HRXI) devoted to laser-plasma experiments combines two state-of-the-art technologies developed in France: a high-resolution x-ray microscope and a high-speed...

  20. Rhode Island High Resolution Wind Resource - Datasets - OpenEI...

    Open Energy Info (EERE)

    Detailed license and usage information for this dataset Preview Download 50m GIS NREL Rhode Island energy high resoltuion renewable shapefile wind wind data wind...

  1. Beam collimation with polycapillary x-ray optics for high contrast high resolution monochromatic imaging

    SciTech Connect (OSTI)

    Sugiro, Francisca R.; Li Danhong; MacDonald, C.A.

    2004-12-01

    Monochromatic imaging can provide better contrast and resolution than conventional broadband radiography. In broadband systems, low energy photons do not contribute to the image, but are merely absorbed, while high energy photons produce scattering that degrades the image. By tuning to the optimal energy, one can eliminate undesirable lower and higher energies. Monochromatization is achieved by diffraction from a single crystal. A crystal oriented to diffract at a particular energy, in this case the characteristic line energy, diffracts only those photons within a narrow range of angles. The resultant beam from a divergent source is nearly parallel, but not very intense. To increase the intensity, collimation was performed with polycapillary x-ray optics, which can collect radiation from a divergent source and redirect it into a quasi parallel beam. Contrast and resolution measurements were performed with diffracting crystals with both high and low angular acceptance. Testing was first done at 8 keV with an intense copper rotating anode x-ray source, then 17.5 keV measurements were made with a low power molybdenum source. At 8 keV, subject contrast was a factor of five higher than for the polychromatic case. At 17.5 keV, monochromatic contrast was two times greater than the conventional polychromatic contrast. The subject contrasts measured at both energies were in good agreement with theory. An additional factor of two increase in contrast, for a total gain of four, is expected at 17.5 keV from the removal of scatter. Scatter might be simply removed using an air gap, which does not degrade resolution with a parallel beam.

  2. High-resolution retinal imaging using adaptive optics and Fourier-domain optical coherence tomography

    DOE Patents [OSTI]

    Olivier, Scot S.; Werner, John S.; Zawadzki, Robert J.; Laut, Sophie P.; Jones, Steven M.

    2010-09-07

    This invention permits retinal images to be acquired at high speed and with unprecedented resolution in three dimensions (4.times.4.times.6 .mu.m). The instrument achieves high lateral resolution by using adaptive optics to correct optical aberrations of the human eye in real time. High axial resolution and high speed are made possible by the use of Fourier-domain optical coherence tomography. Using this system, we have demonstrated the ability to image microscopic blood vessels and the cone photoreceptor mosaic.

  3. Irradiation performance of fast reactor MOX fuel pins with ferritic/martensitic cladding irradiated to high burnups

    SciTech Connect (OSTI)

    Tomoyuki Uwaba; Masahiro Ito; Kozo Katsuyama; Bruce J. Makenas; David W. Wootan; Jon Carmack

    2011-05-01

    The ACO-3 irradiation test, which attained extremely high burnups of about 232 GWd/t and resisted a high neutron fluence (E > 0.1 MeV) of about 39 × 1026 n/m2 as one of the lead tests of the Core Demonstration Experiment in the Fast Flux Test Facility, demonstrated that the fuel pin cladding made of ferritic/martensitic HT-9 alloy had superior void swelling resistance. The measured diameter profiles of the irradiated ACO-3 fuel pins showed axially extensive incremental strain in the MOX fuel column region and localized incremental strain near the interfaces between the MOX fuel and upper blanket columns. These incremental strains were as low as 1.5% despite the extremely high level of the fast neutron fluence. Evaluation of the pin diametral strain indicated that the incremental strain in the MOX fuel column region was substantially due to cladding void swelling and irradiation creep caused by internal fission gas pressure, while the localized strain near the MOX fuel/upper blanket interface was likely the result of the pellet/cladding mechanical interaction (PCMI) caused by cesium/fuel reactions. The evaluation also suggested that the PCMI was effectively mitigated by a large gap size between the cladding and blanket column.

  4. Irradiation performance of fast reactor MOX fuel pins with ferritic/martensitic cladding irradiated to high burnups

    SciTech Connect (OSTI)

    Uwaba, Tomoyuki; Ito, Masahiro; Mizuno, Tomoyasu; Katsuyama, Kozo; Makenas, Bruce J.; Wootan, David W.; Carmack, Jon

    2011-06-16

    The ACO-3 irradiation test, which attained extremely high burnups of about 232 GWd/t and resisted a high neutron fluence (E > 0.1 MeV) of about 39E26 n/m2 as one of the lead tests of the Core Demonstration Experiment in the Fast Flux Test Facility, demonstrated that the fuel pin cladding made of ferritic/martensitic HT-9 alloy had superior void swelling resistance. The measured diameter profiles of the irradiated ACO-3 fuel pins showed axially extensive incremental strain in the MOX fuel column region and localized incremental strain near the interfaces between the MOX fuel and upper blanket columns. These incremental strains were as low as 1.5% despite the extremely high level of the fast neutron fluence. Evaluation of the pin diametral strain indicated that the incremental strain in the MOX fuel column region was substantially due to cladding void swelling and irradiation creep caused by internal fission gas pressure, while the localized strain near the MOX fuel/upper blanket interface was likely the result of the pellet/cladding mechanical interaction (PCMI) caused by cesium/fuel reactions. The evaluation also suggested that the PCMI was effectively mitigated by a large gap size between the cladding and blanket column.

  5. Device for high spatial resolution chemical analysis of a sample and method of high spatial resolution chemical analysis

    DOE Patents [OSTI]

    Van Berkel, Gary J.

    2015-10-06

    A system and method for analyzing a chemical composition of a specimen are described. The system can include at least one pin; a sampling device configured to contact a liquid with a specimen on the at least one pin to form a testing solution; and a stepper mechanism configured to move the at least one pin and the sampling device relative to one another. The system can also include an analytical instrument for determining a chemical composition of the specimen from the testing solution. In particular, the systems and methods described herein enable chemical analysis of specimens, such as tissue, to be evaluated in a manner that the spatial-resolution is limited by the size of the pins used to obtain tissue samples, not the size of the sampling device used to solubilize the samples coupled to the pins.

  6. Compact high resolution isobar separator for study of exotic decays

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Transverse Gradient Undulator (Journal Article) | SciTech Connect Compact X-ray Free Electron Laser from a Laser-plasma Accelerator using a Transverse Gradient Undulator Citation Details In-Document Search Title: Compact X-ray Free Electron Laser from a Laser-plasma Accelerator using a Transverse Gradient Undulator Compact laser-plasma accelerators can produce high energy electron beams with low emittance, high peak current but a rather large energy spread. The large energy spread hinders

  7. A High Resolution Hydrometer Phase Classifier Based on Analysis of Cloud

    Office of Scientific and Technical Information (OSTI)

    Radar Doppler Spectra. (Conference) | SciTech Connect High Resolution Hydrometer Phase Classifier Based on Analysis of Cloud Radar Doppler Spectra. Citation Details In-Document Search Title: A High Resolution Hydrometer Phase Classifier Based on Analysis of Cloud Radar Doppler Spectra. The lifecycle and radiative properties of clouds are highly sensitive to the phase of their hydrometeors (i.e., liquid or ice). Knowledge of cloud phase is essential for specifying the optical properties of

  8. Exploring electronic structure through high-resolution hard x-ray

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    spectroscopies | Stanford Synchrotron Radiation Lightsource Exploring electronic structure through high-resolution hard x-ray spectroscopies Tuesday, July 23, 2013 - 11:00am SLAC, Conference Room 137-322 Presented by Dimosthenis Sokaras, Stanford Synchrotron Radiation Lightsource, SLAC National Accelerator Laboratory Modern high brilliance beamlines coupled with recent advances in hard-x-ray optics are establishing high-resolution hard x-ray spectroscopies as a powerful analytical tool for

  9. Bright x-ray sources from laser irradiation of foams with high...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Bright x-ray sources from laser irradiation of foams with high concentration of Ti Citation Details In-Document Search Title: Bright x-ray sources from laser ...

  10. A HIGH-RESOLUTION ATLAS OF URANIUM-NEON IN THE H BAND (Journal Article) |

    Office of Scientific and Technical Information (OSTI)

    SciTech Connect A HIGH-RESOLUTION ATLAS OF URANIUM-NEON IN THE H BAND Citation Details In-Document Search Title: A HIGH-RESOLUTION ATLAS OF URANIUM-NEON IN THE H BAND We present a high-resolution (R Almost-Equal-To 50,000) atlas of a uranium-neon (U/Ne) hollow-cathode spectrum in the H band (1454-1638 nm) for the calibration of near-infrared spectrographs. We obtained this U/Ne spectrum simultaneously with a laser-frequency comb spectrum, which we used to provide a first-order calibration to

  11. Objectives and layout of a high-resolution x-ray imaging crystal

    Office of Scientific and Technical Information (OSTI)

    spectrometer for the large helical device (Journal Article) | SciTech Connect Objectives and layout of a high-resolution x-ray imaging crystal spectrometer for the large helical device Citation Details In-Document Search Title: Objectives and layout of a high-resolution x-ray imaging crystal spectrometer for the large helical device A high-resolution x-ray imaging crystal spectrometer, whose concept was tested on NSTX and Alcator C-Mod, is being designed for the large helical device (LHD).

  12. Bright x-ray sources from laser irradiation of foams with high

    Office of Scientific and Technical Information (OSTI)

    concentration of Ti (Journal Article) | SciTech Connect Bright x-ray sources from laser irradiation of foams with high concentration of Ti Citation Details In-Document Search Title: Bright x-ray sources from laser irradiation of foams with high concentration of Ti Low-density foams irradiated by a 20 kJ laser at the Omega laser facility (Laboratory for Laser Energetics, Rochester, NY, USA) are shown to convert more than 5% of the laser energy into 4.6 to 6.0 keV x rays. This record

  13. High Resolution PV Power Modeling for Distribution Circuit Analysis

    SciTech Connect (OSTI)

    Norris, B. L.; Dise, J. H.

    2013-09-01

    NREL has contracted with Clean Power Research to provide 1-minute simulation datasets of PV systems located at three high penetration distribution feeders in the service territory of Southern California Edison (SCE): Porterville, Palmdale, and Fontana, California. The resulting PV simulations will be used to separately model the electrical circuits to determine the impacts of PV on circuit operations.

  14. High resolution PET breast imager with improved detection efficiency

    DOE Patents [OSTI]

    Majewski, Stanislaw

    2010-06-08

    A highly efficient PET breast imager for detecting lesions in the entire breast including those located close to the patient's chest wall. The breast imager includes a ring of imaging modules surrounding the imaged breast. Each imaging module includes a slant imaging light guide inserted between a gamma radiation sensor and a photodetector. The slant light guide permits the gamma radiation sensors to be placed in close proximity to the skin of the chest wall thereby extending the sensitive region of the imager to the base of the breast. Several types of photodetectors are proposed for use in the detector modules, with compact silicon photomultipliers as the preferred choice, due to its high compactness. The geometry of the detector heads and the arrangement of the detector ring significantly reduce dead regions thereby improving detection efficiency for lesions located close to the chest wall.

  15. High-Resolution Residential Feeder Load Characterization and Variability Modelling

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Residential Feeder Load Characterization and Variability Modelling Andrew Pohl, Jay Johnson, Santiago Sena, Robert Broderick, and Jimmy Quiroz Sandia National Laboratories, Albuquerque, NM, 87185, USA Abstract - Data from of a highly instrumented residential feeder in Ota City, Japan was used to determine 1 second load variability for the aggregation of 50, 100, 250, and 500 homes. The load variability is categorized by binning the data into seasons, weekdays vs. weekends, and time of day to

  16. Characterization of spatially resolved high resolution x-ray spectrometers for high energy density physics and light source experiments

    SciTech Connect (OSTI)

    Hill, K. W. Bitter, M.; Delgado-Aparacio, L.; Efthimion, P.; Pablant, N. A.; Lu, J.; Beiersdorfer, P.; Chen, H.; Magee, E.

    2014-11-15

    A high resolution 1D imaging x-ray spectrometer concept comprising a spherically bent crystal and a 2D pixelated detector is being optimized for diagnostics of small sources such as high energy density physics (HEDP) and synchrotron radiation or x-ray free electron laser experiments. This instrument is used on tokamak experiments for Doppler measurements of ion temperature and plasma flow velocity profiles. Laboratory measurements demonstrate a resolving power, E/ΔE of order 10 000 and spatial resolution better than 10 μm. Initial tests of the high resolution instrument on HEDP plasmas are being performed.

  17. High-resolution ab initio three-dimensional x-ray diffraction microscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Chapman, Henry N.; Barty, Anton; Marchesini, Stefano; Noy, Aleksandr; Hau-Riege, Stefan P.; Cui, Congwu; Howells, Malcolm R.; Rosen, Rachel; He, Haifeng; Spence, John C. H.; et al

    2006-01-01

    Coherent x-ray diffraction microscopy is a method of imaging nonperiodic isolated objects at resolutions limited, in principle, by only the wavelength and largest scattering angles recorded. We demonstrate x-ray diffraction imaging with high resolution in all three dimensions, as determined by a quantitative analysis of the reconstructed volume images. These images are retrieved from the three-dimensional diffraction data using no a priori knowledge about the shape or composition of the object, which has never before been demonstrated on a nonperiodic object. We also construct two-dimensional images of thick objects with greatly increased depth of focus (without loss of transverse spatialmore » resolution). These methods can be used to image biological and materials science samples at high resolution with x-ray undulator radiation and establishes the techniques to be used in atomic-resolution ultrafast imaging at x-ray free-electron laser sources.« less

  18. Merging high resolution geophysical and geochemical surveys to reduce exploration risk at Glass Buttes, Oregon

    Broader source: Energy.gov [DOE]

    DOE Geothermal Technologies Peer Review - 2010. The primary objective of this project is to combine a suite of high resolution geophysical and geochemical techniques to reduce exploration risk by characterizing hydrothermal alteration, fault geometries and relationships.

  19. Objectives and Layout of a High-Resolution X-ray Imaging Crystal...

    Office of Scientific and Technical Information (OSTI)

    Imaging Crystal Spectrometer for the Large Helical Device (LHD) Citation Details In-Document Search Title: Objectives and Layout of a High-Resolution X-ray Imaging Crystal ...

  20. Design Parameters and Objectives of a High--Resolution X--ray...

    Office of Scientific and Technical Information (OSTI)

    Crystal Spectrometer for the Large Helical Device (LHD) Citation Details In-Document Search Title: Design Parameters and Objectives of a High--Resolution X--ray Imaging Crystal ...

  1. Layout And Results From The Initial Opeeration Of The High-resolution...

    Office of Scientific and Technical Information (OSTI)

    Layout And Results From The Initial Opeeration Of The High-resolution X-ray Imaging ... The nal hardware design and con guration are detailed along with the calibration ...

  2. Design Parameters and Objectives of a High--Resolution X--ray...

    Office of Scientific and Technical Information (OSTI)

    Technical Report: Design Parameters and Objectives of a High--Resolution X--ray Imaging Crystal Spectrometer for the Large Helical Device (LHD) Citation Details In-Document Search ...

  3. Objectives and Layout of a High-Resolution X-ray Imaging Crystal...

    Office of Scientific and Technical Information (OSTI)

    Technical Report: Objectives and Layout of a High-Resolution X-ray Imaging Crystal Spectrometer for the Large Helical Device (LHD) Citation Details In-Document Search Title: ...

  4. Objectives and layout of a high-resolution x-ray imaging crystal...

    Office of Scientific and Technical Information (OSTI)

    x-ray imaging crystal spectrometer for the large helical device Citation Details In-Document Search Title: Objectives and layout of a high-resolution x-ray imaging ...

  5. Optic for an endoscope/borescope having high resolution and narrow field of view

    DOE Patents [OSTI]

    Stone, Gary F.; Trebes, James E.

    2003-10-28

    An optic having optimized high spatial resolution, minimal nonlinear magnification distortion while at the same time having a limited chromatic focal shift or chromatic aberrations. The optic located at the distal end of an endoscopic inspection tool permits a high resolution, narrow field of view image for medical diagnostic applications, compared to conventional optics for endoscopic instruments which provide a wide field of view, low resolution image. The image coverage is over a narrow (<20 degrees) field of view with very low optical distortion (<5% pin cushion or barrel distortion. The optic is also optimized for best color correction as well as to aid medical diagnostics.

  6. Post-Delivery test report for light duty utility arm high resolution stereoscopic video system (HRSVS)

    SciTech Connect (OSTI)

    Pardini, A.F., Westinghouse Hanford

    1996-05-07

    This report documents the post delivery testing of the High Resolution Stereoscopic Video Camera System (HRSVS) LDUA system,designed for use by the Light Duty Utility Arm (LDUA) project.The post delivery test shows by demonstration that the high resolution stereoscopic video camera system is fully operational to perform the task of aligning the LDUA arm and mast with the entry riser during deployment operations within a Hanford Site waste tank.

  7. High-resolution crystal structure of human protease-activated receptor 1

    Office of Scientific and Technical Information (OSTI)

    (Journal Article) | SciTech Connect High-resolution crystal structure of human protease-activated receptor 1 Citation Details In-Document Search Title: High-resolution crystal structure of human protease-activated receptor 1 Authors: Zhang, Cheng ; Srinivasan, Yoga ; Arlow, Daniel H. ; Fung, Juan Jose ; Palmer, Daniel ; Zheng, Yaowu ; Green, Hillary F. ; Pandey, Anjali ; Dror, Ron O. ; Shaw, David E. ; Weis, William I. ; Coughlin, Shaun R. ; Kobilka, Brian K. [1] ; D.E. Shaw) [2] ;

  8. High-resolution genetic mapping of allelic variants associated with cell

    Office of Scientific and Technical Information (OSTI)

    wall chemistry in Populus (Journal Article) | DOE PAGES Accepted Manuscript: High-resolution genetic mapping of allelic variants associated with cell wall chemistry in Populus « Prev Next » Title: High-resolution genetic mapping of allelic variants associated with cell wall chemistry in Populus We report the identification of six genetic loci and the allelic-variants associated with Populus cell wall phenotypes determined independently using pyrolysis Molecular Beam Mass Spectrometry

  9. Layout And Results From The Initial Opeeration Of The High-resolution X-ray

    Office of Scientific and Technical Information (OSTI)

    Imaging Crystal Spectrometer On The Large Helical Device (Technical Report) | SciTech Connect SciTech Connect Search Results Technical Report: Layout And Results From The Initial Opeeration Of The High-resolution X-ray Imaging Crystal Spectrometer On The Large Helical Device Citation Details In-Document Search Title: Layout And Results From The Initial Opeeration Of The High-resolution X-ray Imaging Crystal Spectrometer On The Large Helical Device First results of ion and electron

  10. A high-resolution imaging X-ray crystal spectrometer for intense laser

    Office of Scientific and Technical Information (OSTI)

    plasma interaction experiments (Conference) | SciTech Connect Conference: A high-resolution imaging X-ray crystal spectrometer for intense laser plasma interaction experiments Citation Details In-Document Search Title: A high-resolution imaging X-ray crystal spectrometer for intense laser plasma interaction experiments Authors: Chen, H ; Bitter, M ; Hazi, A ; Hill, K ; Kerr, S ; Magee, E ; Nagel, S ; Park, J ; Schneider, M ; Stone, G ; Williams, G ; Beiersdorfer, P Publication Date:

  11. Detailed High-Resolution Three-Dimensional Simulations of OMEGA Separated

    Office of Scientific and Technical Information (OSTI)

    Reactants Inertial Confinement Fusion Experiments (Conference) | SciTech Connect Detailed High-Resolution Three-Dimensional Simulations of OMEGA Separated Reactants Inertial Confinement Fusion Experiments Citation Details In-Document Search Title: Detailed High-Resolution Three-Dimensional Simulations of OMEGA Separated Reactants Inertial Confinement Fusion Experiments Authors: Haines, Brian Michael [1] ; Grim, Gary P. [1] ; Fincke, James R. [1] ; Shah, Rahul C. [1] ; Forrest, Chad [2] ;

  12. System for target irradiation in the Iskra-6 high-power laser facility

    SciTech Connect (OSTI)

    Bondarenko, S V; Garanin, Sergey G; Eroshenko, V A; Kochemasov, G G; L'vov, L V; Mochalov, M R

    1999-03-31

    An analysis is made of various systems for direct irradiation of a target enabling achievement of a high degree of the irradiation uniformity. The required departure from uniformity of target irradiation, {delta}I/I {<=} 1% - 2%, may be attained when the number of laser beams is N {>=} 80, the diameter of the waist is approximately equal to the target diameter, and the intensity profile in the waist is Gaussian or super-Gaussian. Various methods of forming the necessary intensity distribution in a transverse cross section of a beam are considered. (interaction of laser radiation with matter. laser plasma)

  13. Irradiation Creep in Graphite

    SciTech Connect (OSTI)

    Ubic, Rick; Butt, Darryl; Windes, William

    2014-03-13

    An understanding of the underlying mechanisms of irradiation creep in graphite material is required to correctly interpret experimental data, explain micromechanical modeling results, and predict whole-core behavior. This project will focus on experimental microscopic data to demonstrate the mechanism of irradiation creep. High-resolution transmission electron microscopy should be able to image both the dislocations in graphite and the irradiation-induced interstitial clusters that pin those dislocations. The team will first prepare and characterize nanoscale samples of virgin nuclear graphite in a transmission electron microscope. Additional samples will be irradiated to varying degrees at the Advanced Test Reactor (ATR) facility and similarly characterized. Researchers will record microstructures and crystal defects and suggest a mechanism for irradiation creep based on the results. In addition, the purchase of a tensile holder for a transmission electron microscope will allow, for the first time, in situ observation of creep behavior on the microstructure and crystallographic defects.

  14. Low-energy D{sup +} and H{sup +} ion irradiation effects on highly oriented pyrolytic graphite

    SciTech Connect (OSTI)

    Kue Park, Jun; Won Lee, Kyu; Hee Han, Jun; Jung Kweon, Jin; Kim, Dowan; Eui Lee, Cheol [Department of Physics and Institute for Nano Science, Korea University, Seoul 136-713 (Korea, Republic of)] [Department of Physics and Institute for Nano Science, Korea University, Seoul 136-713 (Korea, Republic of); Lim, Sun-Taek; Kim, Gon-Ho [Department of Nuclear Engineering, Seoul National University, Seoul 151-744 (Korea, Republic of)] [Department of Nuclear Engineering, Seoul National University, Seoul 151-744 (Korea, Republic of); Noh, S. J.; Kim, H. S. [Department of Applied Physics, Dankook University, Yongin 448-701 (Korea, Republic of)] [Department of Applied Physics, Dankook University, Yongin 448-701 (Korea, Republic of)

    2013-12-07

    We have investigated the low-energy (100 eV) D{sup +} and H{sup +} ion irradiation effects on the structural and chemical properties of highly oriented pyrolytic graphite (HOPG). Structural disorder due to the ion irradiation was identified by the Raman spectroscopy, the D{sup +} irradiation giving rise to greater structural disorder than the H{sup +} irradiation. Only sp{sup 2} bonding was identified in the X-ray photoemission spectroscopy of the D{sup +}-irradiated HOPG, indicating no change in the surface chemical structure. The H{sup +} irradiation, on the other hand, gave rise to sp{sup 3} bonding and ???{sup *} transition, the sp{sup 3} bonding increasing with increasing irradiation dose. It is thus shown that the chemical properties of the HOPG surface may be sensitively modified by the low-energy H{sup +} ion irradiation, but not by the low-energy D{sup +} ion irradiation.

  15. STATUS OF HIGH FLUX ISOTOPE REACTOR IRRADIATION OF SILICON CARBIDE/SILICON CARBIDE JOINTS

    SciTech Connect (OSTI)

    Katoh, Yutai; Koyanagi, Takaaki; Kiggans, Jim; Cetiner, Nesrin; McDuffee, Joel

    2014-09-01

    Development of silicon carbide (SiC) joints that retain adequate structural and functional properties in the anticipated service conditions is a critical milestone toward establishment of advanced SiC composite technology for the accident-tolerant light water reactor (LWR) fuels and core structures. Neutron irradiation is among the most critical factors that define the harsh service condition of LWR fuel during the normal operation. The overarching goal of the present joining and irradiation studies is to establish technologies for joining SiC-based materials for use as the LWR fuel cladding. The purpose of this work is to fabricate SiC joint specimens, characterize those joints in an unirradiated condition, and prepare rabbit capsules for neutron irradiation study on the fabricated specimens in the High Flux Isotope Reactor (HFIR). Torsional shear test specimens of chemically vapor-deposited SiC were prepared by seven different joining methods either at Oak Ridge National Laboratory or by industrial partners. The joint test specimens were characterized for shear strength and microstructures in an unirradiated condition. Rabbit irradiation capsules were designed and fabricated for neutron irradiation of these joint specimens at an LWR-relevant temperature. These rabbit capsules, already started irradiation in HFIR, are scheduled to complete irradiation to an LWR-relevant dose level in early 2015.

  16. Design of a High Resolution and High Flux Beam line for VUV Angle-Resolved Photoemission at UVSOR-II

    SciTech Connect (OSTI)

    Kimura, Shin-ichi; Ito, Takahiro; Nakamura, Eiken; Hosaka, Masahito; Katoh, Masahiro

    2007-01-19

    A high-energy-resolution angle-resolved photoemission beamline in the vacuum-ultraviolet (VUV) region has been designed for a 750 MeV synchrotron light source UVSOR-II. The beamline equips an APPLE-II-type undulator with the horizontally/vertically linear and right/left circular polarizations, a modified Wadsworth-type monochromator and a high-resolution photoelectron analyzer. The monochromator covers the photon energy range of 6 - 40 eV. The energy resolution (hv/{delta}hv) and the photon flux on samples are expected to be 2 x 104 and 1012 photons/sec at 10 eV, 4 x 104 and 5 x 1011 photons/sec at 20 eV, and 6 x 104 and 1011 photons/sec at 40 eV, respectively. The beamline provides the high-resolution angle-resolved photoemission spectroscopy less than 1 meV in the whole VUV energy range.

  17. High Resolution/High Fidelity Seismic Imaging and Parameter Estimation for Geological Structure and Material Characterization

    SciTech Connect (OSTI)

    Ru-Shan Wu; Xiao-Bi Xie

    2008-06-08

    Our proposed work on high resolution/high fidelity seismic imaging focused on three general areas: (1) development of new, more efficient, wave-equation-based propagators and imaging conditions, (2) developments towards amplitude-preserving imaging in the local angle domain, in particular, imaging methods that allow us to estimate the reflection as a function of angle at a layer boundary, and (3) studies of wave inversion for local parameter estimation. In this report we summarize the results and progress we made during the project period. The report is divided into three parts, totaling 10 chapters. The first part is on resolution analysis and its relation to directional illumination analysis. The second part, which is composed of 6 chapters, is on the main theme of our work, the true-reflection imaging. True-reflection imaging is an advanced imaging technology which aims at keeping the image amplitude proportional to the reflection strength of the local reflectors or to obtain the reflection coefficient as function of reflection-angle. There are many factors which may influence the image amplitude, such as geometrical spreading, transmission loss, path absorption, acquisition aperture effect, etc. However, we can group these into two categories: one is the propagator effect (geometric spreading, path losses); the other is the acquisition-aperture effect. We have made significant progress in both categories. We studied the effects of different terms in the true-amplitude one-way propagators, especially the terms including lateral velocity variation of the medium. We also demonstrate the improvements by optimizing the expansion coefficients in different terms. Our research also includes directional illumination analysis for both the one-way propagators and full-wave propagators. We developed the fast acquisition-aperture correction method in the local angle-domain, which is an important element in the true-reflection imaging. Other developments include the super-wide angle one-way propagator and special full-wave reverse-time migration method. Finally, we studied the theoretical basis of true-reflection imaging and bridges imaging and inversion with the theory of diffraction tomography.

  18. High-resolution spectroscopic probes of collisions and half-collisions

    SciTech Connect (OSTI)

    Hall, G.E.

    1993-12-01

    Research in this program explores the dynamics of gas phase collisions and photodissociation by high-resolution laser spectroscopy. Simultaneous state and velocity detection frequently permits a determination of scalar or vector correlations among products. The correlated product distributions are always more informative, and often easier to interpret than the uncorrelated product state distributions. The authors have recently built an apparatus to record transient absorption spectra with 50 nS time resolution and 20 MHz frequency resolution using a single frequency Ti:sapphire laser. The photodissociation of NCCN and C{sub 2}H{sub 5}SCN at 193 nm is discussed.

  19. Developing a bright 17 keV x-ray source for probing high-energy-density states of matter at high spatial resolution

    SciTech Connect (OSTI)

    Huntington, C. M.; Park, H.-S.; Maddox, B. R.; Barrios, M. A.; Benedetti, R.; Braun, D. G.; Landen, O. L.; Wehrenberg, C. E.; Remington, B. A.; Hohenberger, M.; Regan, S. P.

    2015-04-15

    A set of experiments were performed on the National Ignition Facility (NIF) to develop and optimize a bright, 17 keV x-ray backlighter probe using laser-irradiated Nb foils. High-resolution one-dimensional imaging was achieved using a 15 μm wide slit in a Ta substrate to aperture the Nb He{sub α} x-rays onto an open-aperture, time integrated camera. To optimize the x-ray source for imaging applications, the effect of laser pulse shape and spatial profile on the target was investigated. Two laser pulse shapes were used—a “prepulse” shape that included a 3 ns, low-intensity laser foot preceding the high-energy 2 ns square main laser drive, and a pulse without the laser foot. The laser spatial profile was varied by the use of continuous phase plates (CPPs) on a pair of shots compared to beams at best focus, without CPPs. A comprehensive set of common diagnostics allowed for a direct comparison of imaging resolution, total x-ray conversion efficiency, and x-ray spectrum between shots. The use of CPPs was seen to reduce the high-energy tail of the x-ray spectrum, whereas the laser pulse shape had little effect on the high-energy tail. The measured imaging resolution was comparably high for all combinations of laser parameters, but a higher x-ray flux was achieved without phase plates. This increased flux was the result of smaller laser spot sizes, which allowed us to arrange the laser focal spots from multiple beams and produce an x-ray source which was more localized behind the slit aperture. Our experiments are a first demonstration of point-projection geometry imaging at NIF at the energies (>10 keV) necessary for imaging denser, higher-Z targets than have previously been investigated.

  20. Data Driven Approach for High Resolution Population Distribution and Dynamics Models

    SciTech Connect (OSTI)

    Bhaduri, Budhendra L; Bright, Eddie A; Rose, Amy N; Liu, Cheng; Urban, Marie L; Stewart, Robert N

    2014-01-01

    High resolution population distribution data are vital for successfully addressing critical issues ranging from energy and socio-environmental research to public health to human security. Commonly available population data from Census is constrained both in space and time and does not capture population dynamics as functions of space and time. This imposes a significant limitation on the fidelity of event-based simulation models with sensitive space-time resolution. This paper describes ongoing development of high-resolution population distribution and dynamics models, at Oak Ridge National Laboratory, through spatial data integration and modeling with behavioral or activity-based mobility datasets for representing temporal dynamics of population. The model is resolved at 1 km resolution globally and describes the U.S. population for nighttime and daytime at 90m. Integration of such population data provides the opportunity to develop simulations and applications in critical infrastructure management from local to global scales.

  1. Dedicated mobile high resolution prostate PET imager with an insertable transrectal probe

    DOE Patents [OSTI]

    Majewski, Stanislaw; Proffitt, James

    2010-12-28

    A dedicated mobile PET imaging system to image the prostate and surrounding organs. The imaging system includes an outside high resolution PET imager placed close to the patient's torso and an insertable and compact transrectal probe that is placed in close proximity to the prostate and operates in conjunction with the outside imager. The two detector systems are spatially co-registered to each other. The outside imager is mounted on an open rotating gantry to provide torso-wide 3D images of the prostate and surrounding tissue and organs. The insertable probe provides closer imaging, high sensitivity, and very high resolution predominately 2D view of the prostate and immediate surroundings. The probe is operated in conjunction with the outside imager and a fast data acquisition system to provide very high resolution reconstruction of the prostate and surrounding tissue and organs.

  2. High resolution x-ray and gamma ray imaging using diffraction lenses with mechanically bent crystals

    DOE Patents [OSTI]

    Smither, Robert K.

    2008-12-23

    A method for high spatial resolution imaging of a plurality of sources of x-ray and gamma-ray radiation is provided. High quality mechanically bent diffracting crystals of 0.1 mm radial width are used for focusing the radiation and directing the radiation to an array of detectors which is used for analyzing their addition to collect data as to the location of the source of radiation. A computer is used for converting the data to an image. The invention also provides for the use of a multi-component high resolution detector array and for narrow source and detector apertures.

  3. High Specific Activity Sn-117m by Post Irradiation Isotope Separation

    SciTech Connect (OSTI)

    DAuria, John

    2015-04-16

    ElectroMagnetic Isotope Separation (EMIS) is used in the production of enriched stable isotopes. We demonstrated the feasibility of using EMIS to produce medium Specific Activity 117mSm using high purity 116Sn target material irradiated in a high flux reactor.

  4. HIGH-RESOLUTION OBSERVATIONS AND THE PHYSICS OF HIGH-VELOCITY CLOUD A0

    SciTech Connect (OSTI)

    Verschuur, Gerrit L.

    2013-04-01

    The neutral hydrogen structure of high-velocity cloud A0 (at about -180 km s{sup -1}) has been mapped with a 9.'1 resolution. Gaussian decomposition of the profiles is used to separately map families of components defined by similarities in center velocities and line widths. About 70% of the H I gas is in the form of a narrow, twisted filament whose typical line widths are of the order of 24 km s{sup -1}. Many bright features with narrow line widths of the order of 6 km s{sup -1}, clouds, are located in and near the filament. A third category with properties between those of the filament and clouds appears in the data. The clouds are not always co-located with the broader line width filament emission as seen projected on the sky. Under the assumption that magnetic fields underlie the presence of the filament, a theorem is developed for its stability in terms of a toroidal magnetic field generated by the flow of gas along field lines. It is suggested that the axial magnetic field strength may be derived from the excess line width of the H I emission over and above that due to kinetic temperature by invoking the role of Alfven waves that create what is in essence a form of magnetic turbulence. At a distance of 200 pc the axial and the derived toroidal magnetic field strengths in the filament are then about 6 {mu}G while for the clouds they are about 4 {mu}G. The dependence of the derived field strength on distance is discussed.

  5. High Temperature Irradiation Resistant Thermocouple (HTIR-TC)

    ScienceCinema (OSTI)

    None

    2013-05-28

    INL researchers have created a new thermocouple that can resist high temperature and radiation. This device will improve safety and reduce costs associated with unit failures. Learn more about INL research at http://www.facebook.com/idahonationallaboratory

  6. High Temperature Irradiation Resistant Thermocouple (HTIR-TC)

    SciTech Connect (OSTI)

    2011-01-01

    INL researchers have created a new thermocouple that can resist high temperature and radiation. This device will improve safety and reduce costs associated with unit failures. Learn more about INL research at http://www.facebook.com/idahonationallaboratory

  7. Layout and results from the initial operation of the high-resolution x-ray

    Office of Scientific and Technical Information (OSTI)

    imaging crystal spectrometer on the Large Helical Device (Journal Article) | SciTech Connect Layout and results from the initial operation of the high-resolution x-ray imaging crystal spectrometer on the Large Helical Device Citation Details In-Document Search Title: Layout and results from the initial operation of the high-resolution x-ray imaging crystal spectrometer on the Large Helical Device First results of ion and electron temperature profile measurements from the x-ray imaging

  8. A space-based, high-resolution view of notable changes in urban NO x

    Office of Scientific and Technical Information (OSTI)

    pollution around the world (2005-2014) (Journal Article) | SciTech Connect A space-based, high-resolution view of notable changes in urban NO x pollution around the world (2005-2014) Citation Details In-Document Search Title: A space-based, high-resolution view of notable changes in urban NO x pollution around the world (2005-2014) Nitrogen oxides (NOx = NO + NO2) are produced during combustion processes and, thus may serve as a proxy for fossil fuel-based energy usage and coemitted

  9. High-resolution Bent-crystal Spectrometer for the Ultra-soft X-ray Region

    DOE R&D Accomplishments [OSTI]

    Beiersdorfer, P.; von Goeler, S.; Bitter, M.; Hill, K. W.; Hulse, R. A.; Walling, R. S.

    1988-10-01

    A multichannel vacuum Brag-crystal spectrometer has been developed for high-resolution measurements of the line emission from tokamak plasmas in the wavelength region between 4 and 25 angstrom. The spectrometer employs a bent crystal in Johann geometry and a microchannel-plate intensified photodiode array. The instrument is capable of measuring high-resolution spectra (lambda/..delta..lambda approx. 3000) with fast time resolution (4 msec per spectrum) and good spatial resolution (3 cm). The spectral bandwidth is ..delta..lambda/lambda{sub 0} = 8 angstrom. A simple tilt mechanism allows access to different wavelength intervals. In order to illustrate the utility of the new spectrometer, time- and space-resolved measurements of the n = 3 to n = 2 spectrum of selenium from the Princeton Large Torus tokamak plasmas are presented. The data are used to determine the plasma transport parameters and to infer the radial distribution of fluorinelike, neonlike, and sodiumlike ions of selenium in the plasma. The new ultra-soft x-ray spectrometer has thus enabled us to demonstrate the utility of high-resolution L-shell spectroscopy of neonlike ions as a fusion diagnostic.

  10. A High Resolution, Light-Weight, Synthetic Aperture Radar for UAV Application

    SciTech Connect (OSTI)

    Doerry, A.W.; Hensley, W.H.; Stence, J.; Tsunoda, S.I. Pace, F.; Walker, B,C.; Woodring, M.

    1999-05-27

    (U) Sandia National Laboratories in collaboration with General Atomics (GA) has designed and built a high resolution, light-weight, Ku-band Synthetic Aperture Radar (SAR) known as "Lynx". Although Lynx can be operated on a wide variety of manned and unmanned platforms, its design is optimized for use on medium altitude Unmanned Aerial Vehicles (UAVS). In particular, it can be operated on the Predator, I-GNAT, and Prowler II platforms manufactured by GA. (U) The radar production weight is less than 120 lb and operates within a 3 GHz band from 15.2 GHz to 18.2 GHz with a peak output power of 320 W. Operating range is resolution and mode dependent but can exceed 45 km in adverse weather (4 mm/hr rain). Lynx has operator selectable resolution and is capable of 0.1 m resolution in spotlight mode and 0.3 m resolution in stripmap mode, over substantial depression angles (5 to 60 deg) and squint angles (broadside 45 deg). Real-time Motion Compensation is implemented to allow high-quality image formation even during vehicle turns and other maneuvers.

  11. LandScan 2012 High Resolution Global Population DataSet

    Energy Science and Technology Software Center (OSTI)

    2013-09-17

    The LandScan data set is a worldwide population database compiled on a 30"x20" latitude/longitude grid. Census counts at sub-national level were apportioned to each grid cell based on likelihood coefficients, which are based on land cover, slope, road proximity, high-resolution imagery, and other data sets.

  12. Virtually distortion-free imaging system for large field, high resolution lithography

    DOE Patents [OSTI]

    Hawryluk, A.M.; Ceglio, N.M.

    1993-01-05

    Virtually distortion free large field high resolution imaging is performed using an imaging system which contains large field distortion or field curvature. A reticle is imaged in one direction through the optical system to form an encoded mask. The encoded mask is then imaged back through the imaging system onto a wafer positioned at the reticle position.

  13. Final Report: High Spectral Resolution Atmospheric Emitted Radiance Studies with the ARM UAV

    SciTech Connect (OSTI)

    Revercomb, Henry E.

    1999-12-31

    The active participation in the Atmospheric Radiation Measurement (ARM) Unmanned Airborne Vehicle (UAV) science team that was anticipated in the grant proposal was indefinitely delayed after the first year due to a programmatic decision to exclude the high spectral resolution observations from the existing ARM UAV program. However, this report shows that substantial progress toward the science objectives of this grant have made with the help of separate funding from NASA and other agencies. In the four year grant period (including time extensions), a new high spectral resolution instrument has been flown and has successfully demonstrated the ability to obtain measurements of the type needed in the conduct of this grant. In the near term, the third water vapor intensive observing period (WVIOP-3) in October 2000 will provide an opportunity to bring the high spectral resolution observations of upwelling radiance into the ARM program to complement the downwelling radiance observations from the existing ARM AERI instruments. We look forward to a time when the ARM-UAV program is able to extend its scope to include the capability for making these high spectral resolution measurements from a UAV platform.

  14. High spatial resolution X-ray and gamma ray imaging system using diffraction crystals

    DOE Patents [OSTI]

    Smither, Robert K.

    2011-05-17

    A method and a device for high spatial resolution imaging of a plurality of sources of x-ray and gamma-ray radiation are provided. The device comprises a plurality of arrays, with each array comprising a plurality of elements comprising a first collimator, a diffracting crystal, a second collimator, and a detector.

  15. Modeling of Arctic Storms with a Variable High-Resolution General Circulation Model

    SciTech Connect (OSTI)

    Taylor, Mark A.; Roesler, Erika Louise; Bosler, Peter Andrew

    2015-08-01

    The Department of Energy’s (DOE) Biological and Environmental Research project, “Water Cycle and Climate Extremes Modeling” is improving our understanding and modeling of regional details of the Earth’s water cycle. Sandia is using high resolution model behavior to investigate storms in the Arctic.

  16. Real-Time High Resolution Quantitative Imaging by Three Wavelength Digital

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Holography - Energy Innovation Portal Real-Time High Resolution Quantitative Imaging by Three Wavelength Digital Holography Oak Ridge National Laboratory Contact ORNL About This Technology Technology Marketing Summary An optical system capable of reproducing three-dimensional images was invented at ORNL. This system can detect height changes of a few nanometers or less and render clear, single shot images. These types of precise, high speed measurements are important for a variety of

  17. High-resolution Soft-RIXS: Scientific Goals and Technical Challenges |

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Stanford Synchrotron Radiation Lightsource High-resolution Soft-RIXS: Scientific Goals and Technical Challenges Tuesday, November 22, 2011 - 3:30pm SSRL Conference Room 137-322 Giacomo Ghiringhelli, CNR/SPIN and Dipartimento di Fisica, Politecnico di Milano, Italy Visiting scholar at SIMES-Department of physics, Stanford University The interest in resonant inelastic soft x-ray scattering has been recently boosted mainly by results on high Tc superconductors and other cuprates, where orbital

  18. High-resolution x-ray diffraction microscopy of specifically labeled yeast cells

    SciTech Connect (OSTI)

    Nelson, Johanna; Huang, Xiaojing; Steinbrener, Jan; Shapiro, David; Kirz, Janos; Marchesini, Stephano; Neiman, Aaron M.; Turner, Joshua J.; Jacobsen, Chris

    2010-04-20

    X-ray diffraction microscopy complements other x-ray microscopy methods by being free of lens-imposed radiation dose and resolution limits, and it allows for high-resolution imaging of biological specimens too thick to be viewed by electron microscopy. We report here the highest resolution (11-13 nm) x-ray diffraction micrograph of biological specimens, and a demonstration of molecular-specific gold labeling at different depths within cells via through-focus propagation of the reconstructed wavefield. The lectin concanavalin A conjugated to colloidal gold particles was used to label the ?-mannan sugar in the cell wall of the yeast Saccharomyces cerevisiae. Cells were plunge-frozen in liquid ethane and freeze-dried, after which they were imaged whole using x-ray diffraction microscopy at 750 eV photon energy.

  19. High-resolution x-ray diffraction microscopy of specifically labeled yeast cells

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Nelson, Johanna; Huang, Xiaojing; Steinbrener, Jan; Shapiro, David; Kirz, Janos; Marchesini, Stephano; Neiman, Aaron M.; Turner, Joshua J.; Jacobsen, Chris

    2010-04-20

    X-ray diffraction microscopy complements other x-ray microscopy methods by being free of lens-imposed radiation dose and resolution limits, and it allows for high-resolution imaging of biological specimens too thick to be viewed by electron microscopy. We report here the highest resolution (11-13 nm) x-ray diffraction micrograph of biological specimens, and a demonstration of molecular-specific gold labeling at different depths within cells via through-focus propagation of the reconstructed wavefield. The lectin concanavalin A conjugated to colloidal gold particles was used to label the α-mannan sugar in the cell wall of the yeast Saccharomyces cerevisiae. Cells were plunge-frozen in liquid ethane andmore » freeze-dried, after which they were imaged whole using x-ray diffraction microscopy at 750 eV photon energy.« less

  20. SU-E-T-415: An Ionization Chamber Array with High Spatial Resolution for External Beam Radiotherapy

    SciTech Connect (OSTI)

    Togno, M; Wilkens, J; Menichelli, D

    2014-06-01

    Purpose: To characterize an ionization chamber array technology with high spatial resolution and high charge collection efficiency for external beam radiotherapy. Methods: The prototype under test is a linear array of air vented ionization chambers developed by IBA Dosimetry, consisting of 80 pixels with 3.5mm spatial resolution and 4mm{sup 3} sensitive volume. The detector was characterized in a plastic phantom with {sup 60} Co radiation and MV X-rays from an ELEKTA Agility LINAC (with flattened and unflattened beam qualities). Bias voltage was varied in order to evaluate charge collection efficiency. A commercial array of ionization chambers (MatriXX Evolution, IBA Dosimetry) and an amorphous silicon flat panel in direct conversion configuration were used as references. Results: Repeatability (0.4%) and stability under continuous gamma irradiation (0.3%) are very good, in spite of low active volume and sensitivity (?200pC/Gy). Charge collection efficiency is higher than 99% already at 150V with ?2mGy dose per pulse, leading to a 1.1% sensitivity change with dose per pulse in the range 0.09-2mGy (covering all flattened and unflattened applications). Measured dose profiles are in agreement with MatriXX for fields larger than 22cm{sup 2}, in which case the linear array offers a much better characterization of the penumbra region. Down to 11cm{sup 2}, measured profiles are in very good agreement with the flat panel. Conclusion: The array represents a valuable tool for the characterization of treatment fields in which high spatial resolution is required, together with the dosimetric performance of air vented ionization chambers. Such a technology would be particularly valuable in association with advanced treatment modalities such as rotational radiotherapy, stereotactic treatments (even with unflattened beam qualities) and proton therapy, due to the insensitivity of the chambers on dose per pulse. In the future, a two dimensional prototype based on this technology will be developed and tested. This research project has been supported by a Marie Curie Early Initial Training Network Fellowship of the European Community's Seventh Framework Programme under contract number (PITN-GA-2011-289198-.

  1. Laser Doppler field sensor for high resolution flow velocity imaging without camera

    SciTech Connect (OSTI)

    Voigt, Andreas; Bayer, Christian; Shirai, Katsuaki; Buettner, Lars; Czarske, Juergen

    2008-09-20

    In this paper we present a laser sensor for highly spatially resolved flow imaging without using a camera. The sensor is an extension of the principle of laser Doppler anemometry (LDA). Instead of a parallel fringe system, diverging and converging fringes are employed. This method facilitates the determination of the tracer particle position within the measurement volume and leads to an increased spatial and velocity resolution compared to conventional LDA. Using a total number of four fringe systems the flow is resolved in two spatial dimensions and the orthogonal velocity component. Since no camera is used, the resolution of the sensor is not influenced by pixel size effects. A spatial resolution of 4 {mu}m in the x direction and 16 {mu}m in the y direction and a relative velocity resolution of 1x10{sup -3} have been demonstrated up to now. As a first application we present the velocity measurement of an injection nozzle flow. The sensor is also highly suitable for applications in nano- and microfluidics, e.g., for the measurement of flow rates.

  2. High Dose Neutron Irradiation of Hi-Nicalon Type S Silicon Carbide Composites, Part 2. Mechanical and Physical Properties

    SciTech Connect (OSTI)

    Katoh, Yutai; Nozawa, Takashi; Shih, Chunghao Phillip; Ozawa, Kazumi; Koyanagi, Takaaki; Porter, Wallace D; Snead, Lance Lewis

    2015-01-07

    Nuclear-grade silicon carbide (SiC) composite material was examined for mechanical and thermophysical properties following high-dose neutron irradiation in the High Flux Isotope Reactor at a temperature range of 573–1073 K. Likewise, the material was chemical vapor-infiltrated SiC-matrix composite with a two-dimensional satin weave Hi-Nicalon Type S SiC fiber reinforcement and a multilayered pyrocarbon/SiC interphase. Moderate (1073 K) to very severe (573 K) degradation in mechanical properties was found after irradiation to >70 dpa, whereas no evidence was found for progressive evolution in swelling and thermal conductivity. The swelling was found to recover upon annealing beyond the irradiation temperature, indicating the irradiation temperature, but only to a limited extent. Moreover, the observed strength degradation is attributed primarily to fiber damage for all irradiation temperatures, particularly a combination of severe fiber degradation and likely interphase damage at relatively low irradiation temperatures.

  3. High spatial resolution brain functional MRI using submillimeter balanced steady-state free precession acquisition

    SciTech Connect (OSTI)

    Wu, Pei-Hsin; Chung, Hsiao-Wen; Tsai, Ping-Huei; Wu, Ming-Long; Chuang, Tzu-Chao; Shih, Yi-Yu; Huang, Teng-Yi

    2013-12-15

    Purpose: One of the technical advantages of functional magnetic resonance imaging (fMRI) is its precise localization of changes from neuronal activities. While current practice of fMRI acquisition at voxel size around 3 3 3 mm{sup 3} achieves satisfactory results in studies of basic brain functions, higher spatial resolution is required in order to resolve finer cortical structures. This study investigated spatial resolution effects on brain fMRI experiments using balanced steady-state free precession (bSSFP) imaging with 0.37 mm{sup 3} voxel volume at 3.0 T. Methods: In fMRI experiments, full and unilateral visual field 5 Hz flashing checkerboard stimulations were given to healthy subjects. The bSSFP imaging experiments were performed at three different frequency offsets to widen the coverage, with functional activations in the primary visual cortex analyzed using the general linear model. Variations of the spatial resolution were achieved by removing outerk-space data components. Results: Results show that a reduction in voxel volume from 3.44 3.44 2 mm{sup 3} to 0.43 0.43 2 mm{sup 3} has resulted in an increase of the functional activation signals from (7.7 1.7)% to (20.9 2.0)% at 3.0 T, despite of the threefold SNR decreases in the original images, leading to nearly invariant functional contrast-to-noise ratios (fCNR) even at high spatial resolution. Activation signals aligning nicely with gray matter sulci at high spatial resolution would, on the other hand, have possibly been mistaken as noise at low spatial resolution. Conclusions: It is concluded that the bSSFP sequence is a plausible technique for fMRI investigations at submillimeter voxel widths without compromising fCNR. The reduction of partial volume averaging with nonactivated brain tissues to retain fCNR is uniquely suitable for high spatial resolution applications such as the resolving of columnar organization in the brain.

  4. Irradiation dose and temperature dependence of fracture toughness in high dose HT9 steel from the fuel duct of FFTF

    SciTech Connect (OSTI)

    Byun, Thak Sang; Toloczko, M; Maloy, S

    2013-01-01

    Static fracture toughness tests have been performed for high dose HT9 steel using miniature disk compact tension (DCT) specimens to expand the knowledge base for fast reactor core materials. The HT9 steel DCT specimens were from the ACO-3 duct of the Fast Flux Test Facility (FFTF), which achieved high doses in the range of 3 148 dpa at 378 504oC. The static fracture resistance (J-R) tests have been performed in a servohydraulic testing machine in vacuum at selected temperatures including room temperature, 200 C, and each irradiation temperature. Brittle fracture with a low toughness less than 50 MPa m occurred in room temperature tests when irradiation temperature was below 400 C, while ductile fracture with stable crack growth was observed in all tests at higher irradiation temperatures. No fracture toughness less than 100 MPa m was measured when the irradiation temperature was above 430 C. It was shown that the influence of irradiation temperature was dominant in fracture toughness while the irradiation dose has only limited influence over the dose range 3 148 dpa. A post upper-shelf behavior was observed for the non-irradiated and high temperature (>430 C) irradiation cases, which indicates that the ductile-brittle transition temperatures (DBTTs) in those conditions are lower than room temperature. A comparison with the collection of existing data confirmed the dominance of irradiation temperature in the fracture toughness of HT9 steels.

  5. Nanoscale deformation analysis with high-resolution transmission electron microscopy and digital image correlation

    SciTech Connect (OSTI)

    Wang, Xueju; Pan, Zhipeng; Fan, Feifei; Wang, Jiangwei; Liu, Yang; Mao, Scott X.; Zhu, Ting; Xia, Shuman

    2015-09-10

    We present an application of the digital image correlation (DIC) method to high-resolution transmission electron microscopy (HRTEM) images for nanoscale deformation analysis. The combination of DIC and HRTEM offers both the ultrahigh spatial resolution and high displacement detection sensitivity that are not possible with other microscope-based DIC techniques. We demonstrate the accuracy and utility of the HRTEM-DIC technique through displacement and strain analysis on amorphous silicon. Two types of error sources resulting from the transmission electron microscopy (TEM) image noise and electromagnetic-lens distortions are quantitatively investigated via rigid-body translation experiments. The local and global DIC approaches are applied for the analysis of diffusion- and reaction-induced deformation fields in electrochemically lithiated amorphous silicon. As a result, the DIC technique coupled with HRTEM provides a new avenue for the deformation analysis of materials at the nanometer length scales.

  6. Nanoscale deformation analysis with high-resolution transmission electron microscopy and digital image correlation

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Wang, Xueju; Pan, Zhipeng; Fan, Feifei; Wang, Jiangwei; Liu, Yang; Mao, Scott X.; Zhu, Ting; Xia, Shuman

    2015-09-10

    We present an application of the digital image correlation (DIC) method to high-resolution transmission electron microscopy (HRTEM) images for nanoscale deformation analysis. The combination of DIC and HRTEM offers both the ultrahigh spatial resolution and high displacement detection sensitivity that are not possible with other microscope-based DIC techniques. We demonstrate the accuracy and utility of the HRTEM-DIC technique through displacement and strain analysis on amorphous silicon. Two types of error sources resulting from the transmission electron microscopy (TEM) image noise and electromagnetic-lens distortions are quantitatively investigated via rigid-body translation experiments. The local and global DIC approaches are applied for themore » analysis of diffusion- and reaction-induced deformation fields in electrochemically lithiated amorphous silicon. As a result, the DIC technique coupled with HRTEM provides a new avenue for the deformation analysis of materials at the nanometer length scales.« less

  7. High-resolution spectroscopy of jet-cooled CH{sub 5}{sup +}: Progress

    SciTech Connect (OSTI)

    Savage, C.; Dong, F.; Nesbitt, D. J.

    2015-01-22

    Protonated methane (CH{sub 5}{sup +}) is thought to be a highly abundant molecular ion in interstellar medium, as well as a potentially bright ?wave- mm wave emitter that could serve as a tracer for methane. This paper describes progress and first successful efforts to obtain a high resolution, supersonically cooled spectrum of CH{sub 5}{sup +} in the 2900-3100 cm{sup ?1} region, formed in a slit supersonic discharge at low jet temperatures and with sub-Doppler resolution. Short term precision in frequency measurement (< 5 MHz on an hour time scale) is obtained from a thermally controlled optical transfer cavity servoloop locked onto a frequency stabilized HeNe laser. Long term precision (< 20 MHz day-to-day) due to pressure, temperature and humidity dependent index of refraction effects in the optical transfer cavity is also present and discussed.

  8. Superconducting gamma and fast-neutron spectrometers with high energy resolution

    DOE Patents [OSTI]

    Friedrich, Stephan; , Niedermayr, Thomas R.; Labov, Simon E.

    2008-11-04

    Superconducting Gamma-ray and fast-neutron spectrometers with very high energy resolution operated at very low temperatures are provided. The sensor consists of a bulk absorber and a superconducting thermometer weakly coupled to a cold reservoir, and determines the energy of the incident particle from the rise in temperature upon absorption. A superconducting film operated at the transition between its superconducting and its normal state is used as the thermometer, and sensor operation at reservoir temperatures around 0.1 K reduces thermal fluctuations and thus enables very high energy resolution. Depending on the choice of absorber material, the spectrometer can be configured either as a Gamma-spectrometer or as a fast-neutron spectrometer.

  9. LandScan 2014 High-Resolution Global Population Data Set

    Energy Science and Technology Software Center (OSTI)

    2015-01-01

    The LandScan data set is a worldwide population database compiled on a 30" X 30" latitude/longitude grid. Census counts (at sub-national level) were apportioned to each grid cell based on likelihood coefficients, which are based on land cover, slope, road proximity, high-resolution imagery, and other data sets. The LandScan data set was developed as part of Oak Ridge National Laboratory (ORNL) Global Population Project for estimating ambient populations at risk.

  10. The Importance of High Temporal Resolution in Modeling Renewable Energy Penetration Scenarios

    SciTech Connect (OSTI)

    Nicolosi, Marco; Mills, Andrew D; Wiser, Ryan H

    2010-10-08

    Traditionally, modeling investment and dispatch problems in electricity economics has been limited by computation power. Due to this limitation, simplifications are applied. One common practice, for example, is to reduce the temporal resolution of the dispatch by clustering similar load levels. The increase of intermittent electricity from renewable energy sources (RES-E) changes the validity of this assumption. RES-E already cover a certain amount of the total demand. This leaves an increasingly volatile residual demand to be matched by the conventional power market. This paper quantifies differences in investment decisions by applying three different time-resolution residual load patterns in an investment and dispatch power system model. The model optimizes investment decisions in five year steps between today and 2030 with residual load levels for 8760, 288 and 16 time slices per year. The market under consideration is the four zone ERCOT market in Texas. The results show that investment decisions significantly differ across the three scenarios. In particular, investments into base-load technologies are substantially reduced in the high resolution scenario (8760 residual load levels) relative to the scenarios with lower temporal resolution. Additionally, the amount of RES-E curtailment and the market value of RES-E exhibit noteworthy differences.

  11. Application of spatially resolved high resolution crystal spectrometry to inertial confinement fusion plasmas

    SciTech Connect (OSTI)

    Hill, K. W.; Bitter, M.; Delgado-Aparacio, L.; Pablant, N. A.; Beiersdorfer, P.; Schneider, M.; Widmann, K.; Sanchez del Rio, M.; Zhang, L.

    2012-10-15

    High resolution ({lambda}/{Delta}{lambda}{approx} 10 000) 1D imaging x-ray spectroscopy using a spherically bent crystal and a 2D hybrid pixel array detector is used world wide for Doppler measurements of ion-temperature and plasma flow-velocity profiles in magnetic confinement fusion plasmas. Meter sized plasmas are diagnosed with cm spatial resolution and 10 ms time resolution. This concept can also be used as a diagnostic of small sources, such as inertial confinement fusion plasmas and targets on x-ray light source beam lines, with spatial resolution of micrometers, as demonstrated by laboratory experiments using a 250-{mu}m {sup 55}Fe source, and by ray-tracing calculations. Throughput calculations agree with measurements, and predict detector counts in the range 10{sup -8}-10{sup -6} times source x-rays, depending on crystal reflectivity and spectrometer geometry. Results of the lab demonstrations, application of the technique to the National Ignition Facility (NIF), and predictions of performance on NIF will be presented.

  12. Towards Direct Simulation of Future Tropical Cyclone Statistics in a High-Resolution Global Atmospheric Model

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Wehner, Michael F.; Bala, G.; Duffy, Phillip; Mirin, Arthur A.; Romano, Raquel

    2010-01-01

    We present a set of high-resolution global atmospheric general circulation model (AGCM) simulations focusing on the model's ability to represent tropical storms and their statistics. We find that the model produces storms of hurricane strength with realistic dynamical features. We also find that tropical storm statistics are reasonable, both globally and in the north Atlantic, when compared to recent observations. The sensitivity of simulated tropical storm statistics to increases in sea surface temperature (SST) is also investigated, revealing that a credible late 21st century SST increase produced increases in simulated tropical storm numbers and intensities in all ocean basins. Whilemore » this paper supports previous high-resolution model and theoretical findings that the frequency of very intense storms will increase in a warmer climate, it differs notably from previous medium and high-resolution model studies that show a global reduction in total tropical storm frequency. However, we are quick to point out that this particular model finding remains speculative due to a lack of radiative forcing changes in our time-slice experiments as well as a focus on the Northern hemisphere tropical storm seasons.« less

  13. A high spatial resolution Stokes polarimeter for motional Stark effect imaging

    SciTech Connect (OSTI)

    Thorman, Alex; Michael, Clive; Howard, John [Plasma Research Laboratory, Research School of Physics and Engineering, Australian National University, Canberra ACT 0200 (Australia)

    2013-06-15

    We describe an enhanced temporally switched interfero-polarimeter that has been successfully deployed for high spatial resolution motional Stark effect imaging on the KSTAR superconducting tokamak. The system utilizes dual switching ferroelectric liquid crystal waveplates to image the full Stokes vector of elliptically polarized and Doppler-shifted Stark-Zeeman Balmer-alpha emission from high energy neutral beams injected into the magnetized plasma. We describe the optical system and compare its performance against a Mueller matrix model that takes account of non-ideal performance of the switching ferro-electric liquid crystal waveplates and other polarizing components.

  14. Dynamic frequency-domain interferometer for absolute distance measurements with high resolution

    SciTech Connect (OSTI)

    Weng, Jidong; Liu, Shenggang; Ma, Heli; Tao, Tianjiong; Wang, Xiang; Liu, Cangli; Tan, Hua

    2014-11-15

    A unique dynamic frequency-domain interferometer for absolute distance measurement has been developed recently. This paper presents the working principle of the new interferometric system, which uses a photonic crystal fiber to transmit the wide-spectrum light beams and a high-speed streak camera or frame camera to record the interference stripes. Preliminary measurements of harmonic vibrations of a speaker, driven by a radio, and the changes in the tip clearance of a rotating gear wheel show that this new type of interferometer has the ability to perform absolute distance measurements both with high time- and distance-resolution.

  15. High-resolution electron-ion coincidence spectroscopy of ethanol in intense laser fields

    SciTech Connect (OSTI)

    Hatamoto, T.; Pruemper, G.; Okunishi, M.; Ueda, K.; Mathur, D.

    2007-06-15

    High-resolution electron-ion coincidence spectroscopy is used to (i) map correlations between electrons and ions from atomlike ionization of ethanol by intense 400 and 800 nm light pulses and (ii) disentangle the effects of dissociative multiphoton (MPI) and tunneling (TI) ionization. Electron spectra correlated with C{sup n+} (n=1,2,3) exhibit a continuum structure with a high-energy tail due to inelastic collisions involving rescattered electrons following TI, while those correlated with C{sub 2}H{sub n}O{sup +} have structure characteristic of MPI and above-threshold ionization.

  16. Analysis of high-resolution spectra from a hybrid interferometric/dispersive spectrometer

    SciTech Connect (OSTI)

    Ko, Phyllis; Scott, Jill R.; Jovanovic, Igor

    2015-09-05

    To fully take advantage of a low-cost, small footprint hybrid interferometric/dispersive spectrometer, a math- ematical reconstruction technique was developed to accurately capture the high-resolution and relative peak intensities from complex patterns. A Fabry-Perot etalon was coupled to a Czerny-Turner spectrometer, in- creasing spectral resolution by an order of magnitude without the commensurate increase in spectrometer size. Measurement of the industry standard Hg 313.1555/313.1844 nm doublet yielded a ratio of 0.682 with 1.8%error, which agreed well with an independent measurement and literature values. The doublet separation (29 pm), is similar to the U isotope shift (25 pm) at 424.437 nm that is of interest to monitoring nuclear nonpro-liferation activities. Additionally, the technique was applied to a LIBS measurement of the mineral cinnabar (HgS) and resulted in a ratio of 0.681. This reconstruction method could enable significantly smaller, portable high-resolution instruments with isotopic specificity, benefiting a variety of spectroscopic applications.

  17. High-Resolution Structure of the Photosynthetic Mn4Ca Catalyst from X-ray Spectroscopy

    SciTech Connect (OSTI)

    Yachandra, Vittal; Yano, Junko; Kern, Jan; Pushkar, Yulia; Sauer, Kenneth; Glatzel, Pieter; Bergmann, Uwe; Messinger, Johannes; Zouni, Athina; Yachandra, Vittal K.

    2007-08-01

    The application of high-resolution X-ray spectroscopy methods to study the photosynthetic water oxidizing complex, which contains a unique hetero-nuclear catalytic Mn4Ca cluster, are described. Issues of X-ray damage especially at the metal sites in the Mn4Ca cluster are discussed. The structure of the Mn4Ca catalyst at high-resolution which has so far eluded attempts of determination by X-ray diffraction, EXAFS and other spectroscopic techniques has been addressed using polarized EXAFS techniques applied to oriented PS II membrane preparations and PS II single crystals. A review of how the resolution of traditional EXAFS techniques can be improved, using methods such as range-extended EXAFS is presented, and the changes that occur in the structure of the cluster as it advances through the catalytic cycle are described. X-ray absorption and emission techniques (XANES and K? emission) have been used earlier to determine the oxidation states of the Mn4Ca cluster, and in this report we review the use of X-ray resonant Raman spectroscopy to understand the electronic structure of the Mn4Ca cluster as it cycles through the intermediate S-states.

  18. Analysis of high-resolution spectra from a hybrid interferometric/dispersive spectrometer

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ko, Phyllis; Scott, Jill R.; Jovanovic, Igor

    2015-09-05

    To fully take advantage of a low-cost, small footprint hybrid interferometric/dispersive spectrometer, a math- ematical reconstruction technique was developed to accurately capture the high-resolution and relative peak intensities from complex patterns. A Fabry-Perot etalon was coupled to a Czerny-Turner spectrometer, in- creasing spectral resolution by an order of magnitude without the commensurate increase in spectrometer size. Measurement of the industry standard Hg 313.1555/313.1844 nm doublet yielded a ratio of 0.682 with 1.8%error, which agreed well with an independent measurement and literature values. The doublet separation (29 pm), is similar to the U isotope shift (25 pm) at 424.437 nm thatmore » is of interest to monitoring nuclear nonpro-liferation activities. Additionally, the technique was applied to a LIBS measurement of the mineral cinnabar (HgS) and resulted in a ratio of 0.681. This reconstruction method could enable significantly smaller, portable high-resolution instruments with isotopic specificity, benefiting a variety of spectroscopic applications.« less

  19. High-resolution photoelectron spectra of the pyrimidine-type nucleobases

    SciTech Connect (OSTI)

    Fulfer, K. D.; Hardy, D.; Poliakoff, E. D.; Aguilar, A. A.

    2015-06-14

    High-resolution photoelectron spectra of the gas phase pyrimidine-type nucleobases, thymine, uracil, and cytosine, were collected using synchrotron radiation over the photon energy range 17 ≤ hν ≤ 150 eV. These data provide the highest resolution photoelectron spectra of thymine, uracil, and cytosine published to date. By comparing integrated regions of the energy dependent photoelectron spectra of thymine, the ionization potentials of the first four ionic states of thymine were estimated to be 8.8, 9.8, 10.3, and 10.8 eV. The thymine data also show evidence for low energy shape resonances in three of the outermost valence electronic states. Comparing the uracil spectrum with the thymine spectrum, the four outermost valence electronic states of uracil likely begin at binding energies 9.3, 9.9, 10.5, and 11.0 eV. High-resolution spectra indicate only one tautomeric form of cytosine contributes significantly to the spectrum with the four outermost valence electronic states beginning at binding energies 8.9, 9.9, 10.4, and 10.85 eV.

  20. [S IV] IN THE NGC 5253 SUPERNEBULA: IONIZED GAS KINEMATICS AT HIGH RESOLUTION

    SciTech Connect (OSTI)

    Beck, Sara C.; Lacy, John H.; Turner, Jean L.; Kruger, Andrew; Richter, Matt; Crosthwaite, Lucian P.

    2012-08-10

    The nearby dwarf starburst galaxy NGC 5253 hosts a deeply embedded radio-infrared supernebula excited by thousands of O stars. We have observed this source in the 10.5 {mu}m line of S{sup +3} at 3.8 km s{sup -1} spectral and 1.''4 spatial resolution, using the high-resolution spectrometer TEXES on the IRTF. The line profile cannot be fit well by a single Gaussian. The best simple fit describes the gas with two Gaussians, one near the galactic velocity with FWHM 33.6 km s{sup -1} and another of similar strength and FWHM 94 km s{sup -1} centered {approx}20 km s{sup -1} to the blue. This suggests a model for the supernebula in which gas flows toward us out of the molecular cloud, as in a 'blister' or 'champagne flow' or in the H II regions modelled by Zhu.

  1. Short range, ultra-wideband radar with high resolution swept range gate

    DOE Patents [OSTI]

    McEwan, Thomas E.

    1998-05-26

    A radar range finder and hidden object locator is based on ultra-wide band radar with a high resolution swept range gate. The device generates an equivalent time amplitude scan with a typical range of 4 inches to 20 feet, and an analog range resolution as limited by a jitter of on the order of 0.01 inches. A differential sampling receiver is employed to effectively eliminate ringing and other aberrations induced in the receiver by the near proximity of the transmit antenna, so a background subtraction is not needed, simplifying the circuitry while improving performance. Uses of the invention include a replacement of ultrasound devices for fluid level sensing, automotive radar, such as cruise control and parking assistance, hidden object location, such as stud and rebar finding. Also, this technology can be used when positioned over a highway lane to collect vehicle count and speed data for traffic control.

  2. The High-Resolution Lightweight Telescope for the EUV (HiLiTE)

    SciTech Connect (OSTI)

    Martinez-Galarce, D S; Boerner, P; Soufli, R; De Pontieu, B; Katz, N; Title, A; Gullikson, E M; Robinson, J C; Baker, S L

    2008-06-02

    The High-resolution Lightweight Telescope for the EUV (HiLiTE) is a Cassegrain telescope that will be made entirely of Silicon Carbide (SiC), optical substrates and metering structure alike. Using multilayer coatings, this instrument will be tuned to operate at the 465 {angstrom} Ne VII emission line, formed in solar transition region plasma at {approx}500,000 K. HiLiTE will have an aperture of 30 cm, angular resolution of {approx}0.2 arc seconds and operate at a cadence of {approx}5 seconds or less, having a mass that is about 1/4 that of one of the 20 cm aperture telescopes on the Atmospheric Imaging Assembly (AIA) instrument aboard NASA's Solar Dynamics Observatory (SDO). This new instrument technology thus serves as a path finder to a post-AIA, Explorer-class missions.

  3. New developments in high resolution borehole seismology and their applications to reservoir development and management

    SciTech Connect (OSTI)

    Paulsson, B.N.P.

    1997-08-01

    Single-well seismology, Reverse Vertical Seismic Profiles (VSP`s) and Crosswell seismology are three new seismic techniques that we jointly refer to as borehole seismology. Borehole seismic techniques are of great interest because they can obtain much higher resolution images of oil and gas reservoirs than what is obtainable with currently used seismic techniques. The quality of oil and gas reservoir management decisions depend on the knowledge of both the large and the fine scale features in the reservoirs. Borehole seismology is capable of mapping reservoirs with an order of magnitude improvement in resolution compared with currently used technology. In borehole seismology we use a high frequency seismic source in an oil or gas well and record the signal in the same well, in other wells, or on the surface of the earth.

  4. Short range, ultra-wideband radar with high resolution swept range gate

    DOE Patents [OSTI]

    McEwan, T.E.

    1998-05-26

    A radar range finder and hidden object locator is based on ultra-wide band radar with a high resolution swept range gate. The device generates an equivalent time amplitude scan with a typical range of 4 inches to 20 feet, and an analog range resolution as limited by a jitter of on the order of 0.01 inches. A differential sampling receiver is employed to effectively eliminate ringing and other aberrations induced in the receiver by the near proximity of the transmit antenna, so a background subtraction is not needed, simplifying the circuitry while improving performance. Uses of the invention include a replacement of ultrasound devices for fluid level sensing, automotive radar, such as cruise control and parking assistance, hidden object location, such as stud and rebar finding. Also, this technology can be used when positioned over a highway lane to collect vehicle count and speed data for traffic control. 14 figs.

  5. Effects of downscaled high-resolution meteorological data on the PSCF identification of emission sources

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Cheng, Meng -Dawn; Kabela, Erik D.

    2016-04-30

    The Potential Source Contribution Function (PSCF) model has been successfully used for identifying regions of emission source at a long distance in this study, the PSCF model relies on backward trajectories calculated by the Hybrid Single-Particle Lagrangian Integrated Trajectory (HYSPLIT) model. In this study, we investigated the impacts of grid resolution and Planetary Boundary Layer (PBL) parameterization (e.g., turbulent transport of pollutants) on the PSCF analysis. The Mellor-Yamada-Janjic (MYJ) and Yonsei University (YUS) parameterization schemes were selected to model the turbulent transport in the PBL within the Weather Research and Forecasting (WRF version 3.6) model. Two separate domain grid sizesmore » (83 and 27 km) were chosen in the WRF downscaling in generating the wind data for driving the HYSPLIT calculation. The effects of grid size and PBL parameterization are important in incorporating the influ- ence of regional and local meteorological processes such as jet streaks, blocking patterns, Rossby waves, and terrain-induced convection on the transport of pollutants by a wind trajectory. We found high resolution PSCF did discover and locate source areas more precisely than that with lower resolution meteorological inputs. The lack of anticipated improvement could also be because a PBL scheme chosen to produce the WRF data was only a local parameterization and unable to faithfully duplicate the real atmosphere on a global scale. The MYJ scheme was able to replicate PSCF source identification by those using the Reanalysis and discover additional source areas that was not identified by the Reanalysis data. In conclusion, a potential benefit for using high-resolution wind data in the PSCF modeling is that it could discover new source location in addition to those identified by using the Reanalysis data input.« less

  6. Irradiation dose and temperature dependence of fracture toughness in high dose HT9 steel from the fuel duct of FFTF

    SciTech Connect (OSTI)

    Byun, Thak Sang; Toloczko, Mychailo B.; Saleh, Tarik A.; Maloy, Stuart A.

    2013-01-14

    To expand the knowledge base for fast reactor core materials, fracture toughness has been evaluated for high dose HT9 steel using miniature disk compact tension (DCT) specimens. The HT9 steel DCT specimens were machined from the ACO-3 fuel duct of the Fast Flux Test Facility (FFTF), which achieved high doses in the range of 3–148 dpa at 378–504 C. The static fracture resistance (J-R) tests have been performed in a servohydraulic testing machine in vacuum at selected temperatures including room temperature, 200 C, and each irradiation temperature. Brittle fracture with a low toughness less than 50 MPa pm occurred in room temperature tests when irradiation temperature was below 400 C, while ductile fracture with stable crack growth was observed when irradiation temperature was higher. No fracture toughness less than 100 MPa pm was measured when the irradiation temperature was above 430 C. It was shown that the influence of irradiation temperature was dominant in fracture toughness while the irradiation dose has only limited influence over the wide dose range 3–148 dpa. A slow decrease of fracture toughness with test temperature above room temperature was observed for the nonirradiated and high temperature (>430 *C) irradiation cases, which indicates that the ductile–brittle transition temperatures (DBTTs) in those conditions are lower than room temperature. A comparison with the collection of existing data confirmed the dominance of irradiation temperature in the fracture toughness of HT9 steels.

  7. Radiation tolerant nanocrystalline ZrN films under high dose heavy-ion irradiations

    SciTech Connect (OSTI)

    Jiao, L.; Wang, H.; Yu, K. Y.; Chen, D.; Jacob, C.; Shao, L.; Zhang, X.

    2015-04-14

    ZrN, a refractory ceramic material, finds many potential applications in advanced nuclear reactors. However, the grain size dependent radiation response in nanocrystalline (nc) ZrN under high dose heavy ion irradiation has not yet been studied to date. Here, we compare the radiation response of nc-ZrN films (with a respective average grain size of ∼9 and 31 nm) to Fe{sup 2+} ion irradiations up to a damage level of 10 displacements-per-atom (dpa). The ZrN film with the average grain size of 9 nm shows prominently enhanced radiation tolerance as evidenced by suppressed grain growth, alleviated radiation softening, as well as reduced variation in electrical resistivity. In contrast, ZrN with the larger average grain size of 31 nm shows prominent radiation softening and resistivity increase, attributed to the high density of defect cluster formed inside the grains. The influence of grain boundaries on enhanced irradiation tolerance in nc-ZrN is discussed.

  8. High Resolution BPM Upgrade for the ATF Damping Ring at KEK

    SciTech Connect (OSTI)

    Eddy, N.; Briegel, C.; Fellenz, B.; Gianfelice-Wendt, E.; Prieto, P.; Rechenmacher, R.; Semenov, A.; Voy, D.; Wendt, M.; Zhang, D.; Terunuma, N.; /KEK, Tsukuba

    2011-08-17

    A beam position monitor (BPM) upgrade at the KEK Accelerator Test Facility (ATF) damping ring has been accomplished, carried out by a KEK/FNAL/SLAC collaboration under the umbrella of the global ILC R&D effort. The upgrade consists of a high resolution, high reproducibility read-out system, based on analog and digital down-conversion techniques, digital signal processing, and also implements a new automatic gain error correction schema. The technical concept and realization as well as results of beam studies are presented. The next generation of linear colliders require ultra-low vertical emittance of <2 pm-rad. The damping ring at the KEK Accelerator Test Facility (ATF) is designed to demonstrate this mission critical goal. A high resolution beam position monitor (BPM) system for the damping ring is one of the key tools for realizing this goal. The BPM system needs to provide two distnict measurements. First, a very high resolution ({approx}100-200nm) closed-orbit measurement which is averaged over many turns and realized with narrowband filter techniques - 'narrowband mode'. This is needed to monitor and steer the beam along an optimum orbit and to facilitate beam-based alignment to minimize non-linear field effects. Second, is the ability to make turn by turn (TBT) measurements to support optics studies and corrections necessary to achieve the design performance. As the TBT measurement necessitates a wider bandwidth, it is often referred to as 'wideband mode'. The BPM upgrade was initiated as a KEK/SLAC/FNAL collaboration in the frame of the Global Design Initiative of the International Linear Collider. The project was realized and completed using Japan-US funds with Fermilab as the core partner.

  9. Radio frequency phototube and optical clock: High resolution, high rate and highly stable single photon timing technique

    SciTech Connect (OSTI)

    Amur Margaryan

    2011-10-01

    A new timing technique for single photons based on the radio frequency phototube and optical clock or femtosecond optical frequency comb generator is proposed. The technique has a 20 ps resolution for single photons, is capable of operating with MHz frequencies and achieving 10 fs instability level.

  10. PPPL to design a high-resolution diagnostic system for the National

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Ignition Facility | Princeton Plasma Physics Lab to design a high-resolution diagnostic system for the National Ignition Facility By Johm Greenwald November 16, 2015 Tweet Widget Google Plus One Share on Facebook Kenneth Hill and Manfred Bitter inspect an X-ray crystal spectrometer to be used to study OMEGA EP laser-produced plasmas. (Photo by Elle Starkman/Office of Communications) Kenneth Hill and Manfred Bitter inspect an X-ray crystal spectrometer to be used to study OMEGA EP

  11. design a high-resolution diagnostic system for the National Ignition

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Facility | Princeton Plasma Physics Lab design a high-resolution diagnostic system for the National Ignition Facility By John Greenwald November 16, 2015 Tweet Widget Google Plus One Share on Facebook Kenneth Hill and Manfred Bitter inspect an X-ray crystal spectrometer to be used to study OMEGA EP laser-produced plasmas. (Photo by Elle Starkman/Office of Communications) Kenneth Hill and Manfred Bitter inspect an X-ray crystal spectrometer to be used to study OMEGA EP laser-produced plasmas.

  12. High-resolution PET [Positron Emission Tomography] for Medical Science Studies

    DOE R&D Accomplishments [OSTI]

    Budinger, T. F.; Derenzo, S. E.; Huesman, R. H.; Jagust, W. J.; Valk, P. E.

    1989-09-01

    One of the unexpected fruits of basic physics research and the computer revolution is the noninvasive imaging power available to today's physician. Technologies that were strictly the province of research scientists only a decade or two ago now serve as the foundations for such standard diagnostic tools as x-ray computer tomography (CT), magnetic resonance imaging (MRI), magnetic resonance spectroscopy (MRS), ultrasound, single photon emission computed tomography (SPECT), and positron emission tomography (PET). Furthermore, prompted by the needs of both the practicing physician and the clinical researcher, efforts to improve these technologies continue. This booklet endeavors to describe the advantages of achieving high resolution in PET imaging.

  13. High-resolution methods for preserving the sum of mass fractions: improved ?-scheme and an alternative

    SciTech Connect (OSTI)

    Syamlal, Madhava; Benyahia, Sofiane

    2013-11-20

    When high resolution convection schemes are used for discretizing chemical species mass balance equations, the mass fractions are not guaranteed to add to one. We show that a proposed remedy called ?-scheme (Darwish and Moukalled, Comput.Methods Appl.Mech. Engrg. 192 (2003): 1711) will degrade to a diffusive first-order scheme when a chemical species vanishes from the mixture, for example, because of chemical reactions. We propose an improvement to the ?-scheme to overcome this problem. Furthermore, a computationally efficient alternative scheme is proposed and evaluated with several examples, to quantify the improvements in the accuracy and the computational time.

  14. Development of a High Resolution X-Ray Imaging Crystal Spectrometer

    Office of Scientific and Technical Information (OSTI)

    83 PPPL- 4283 Development of a High Resolution X-Ray Imaging Crystal Spectrometer for Measurement of Ion-Temperature and Rotation-Velocity Profiles in Fusion Energy Research Plasmas January 2008 K. W. Hill, M. L. Bitter, Ch. Broennimann, E. F. Eikenberry, A. Ince-Cushman, S. G. Lee, J. E. Rice, S. Scott, and R. Barnsley Princeton Plasma Physics Laboratory Report Disclaimers Full Legal Disclaimer This report was prepared as an account of work sponsored by an agency of the United States

  15. Scientific system for high-resolution measurement of the circumsolar radiation

    SciTech Connect (OSTI)

    Schrott, Simeon Schmidt, Thomas Hornung, Thorsten Nitz, Peter

    2014-09-26

    We developed a camera based system for measurements of the circumsolar radiation with a high angular resolution of 0.1 mrad. Subsequent measurements may be taken at intervals as short as 15 s. In this publication we describe the optical system in detail and discuss some aspects of the measurement method. First results from two days of measurement at Freiburg i. Br., Germany, are presented and compared to data from literature. The good results encourage us to perform longer measurement campaigns in future to better understand the influence of circumsolar radiation on the power yield of concentrating photovoltaic systems.

  16. High Resolution Snapshots for the Complete Reaction Cycle of a Cocaine

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Catalytic Antibody High Resolution Snapshots for the Complete Reaction Cycle of a Cocaine Catalytic Antibody Xueyong Zhu1, Tobin J. Dickerson2,3, Claude J. Rogers2,3, Gunnar F. Kaufmann2,3, Jenny M. Mee2,3, Kathleen M. McKenzie2,3, Kim D. Janda2,3,4,* and Ian A. Wilson1,4,* Departments of Molecular Biology1 and Chemistry2 and Immunology3, and The Skaggs Institute for Chemical Biology4, The Scripps Research Institute, 10550 North Torrey Pines Road, La Jolla, CA 92037, USA. Cocaine is a

  17. Magnetic lens apparatus for a low-voltage high-resolution electron microscope

    DOE Patents [OSTI]

    Crewe, Albert V.

    1996-01-01

    A lens apparatus in which a beam of charged particles of low accelerating voltage is brought to a focus by a magnetic field, the lens being situated behind the target position. The lens comprises an electrically-conducting coil arranged around the axis of the beam and a magnetic pole piece extending along the axis of the beam at least within the space surrounded by the coil. The lens apparatus comprises the sole focusing lens for high-resolution imaging in a low-voltage scanning electron microscope.

  18. High-Resolution Spectroscopy with the Chandra X-ray Observatory

    ScienceCinema (OSTI)

    Canizares, Claude R. [MIT, Cambridge, Massachusetts, United States

    2010-01-08

    The capabilities of the Chandra X-ray Observatory and XMM-Newton for high-resolution spectroscopy have brought tradition plasma diagnostic techniques to the study of cosmic plasma. Observations have probed nearly every class of astronomical object, from young proto-starts through massive O starts and black hole binaries, supernova remnants, active galactic nuclei, and the intergalactic medium. Many of these sources show remarkable rich spectra that reveal new physical information, such as emission measure distributions, elemental abundances, accretion disk and wind signatures, and time variability. This talk will present an overview of the Chandra instrumentaton and selected examples of spectral observations of astrophysical and cosmological importance.

  19. High-resolution imaging and target designation through clouds or smoke

    DOE Patents [OSTI]

    Perry, Michael D.

    2003-01-01

    A method and system of combining gated intensifiers and advances in solid-state, short-pulse laser technology, compact systems capable of producing high resolution (i.e., approximately less than 20 centimeters) optical images through a scattering medium such as dense clouds, fog, smoke, etc. may be achieved from air or ground based platforms. Laser target designation through a scattering medium is also enabled by utilizing a short pulse illumination laser and a relatively minor change to the detectors on laser guided munitions.

  20. High-resolution inverse Raman and resonant-wave-mixing spectroscopy

    SciTech Connect (OSTI)

    Rahn, L.A.

    1993-12-01

    These research activities consist of high-resolution inverse Raman spectroscopy (IRS) and resonant wave-mixing spectroscopy to support the development of nonlinear-optical techniques for temperature and concentration measurements in combustion research. Objectives of this work include development of spectral models of important molecular species needed to perform coherent anti-Stokes Raman spectroscopy (CARS) measurements and the investigation of new nonlinear-optical processes as potential diagnostic techniques. Some of the techniques being investigated include frequency-degenerate and nearly frequency-degenerate resonant four-wave-mixing (DFWM and NDFWM), and resonant multi-wave mixing (RMWM).

  1. Machine Learning Approaches for High-resolution Urban Land Cover Classification: A Comparative Study

    SciTech Connect (OSTI)

    Vatsavai, Raju; Chandola, Varun; Cheriyadat, Anil M; Bright, Eddie A; Bhaduri, Budhendra L; Graesser, Jordan B

    2011-01-01

    The proliferation of several machine learning approaches makes it difficult to identify a suitable classification technique for analyzing high-resolution remote sensing images. In this study, ten classification techniques were compared from five broad machine learning categories. Surprisingly, the performance of simple statistical classification schemes like maximum likelihood and Logistic regression over complex and recent techniques is very close. Given that these two classifiers require little input from the user, they should still be considered for most classification tasks. Multiple classifier systems is a good choice if the resources permit.

  2. Appending High-Resolution Elevation Data to GPS Speed Traces for Vehicle Energy Modeling and Simulation

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Appending High-Resolution Elevation Data to GPS Speed Traces for Vehicle Energy Modeling and Simulation E. Wood, E. Burton, A. Duran, and J. Gonder Technical Report NREL/TP-5400-61109 June 2014 NREL is a national laboratory of the U.S. Department of Energy Office of Energy Efficiency & Renewable Energy Operated by the Alliance for Sustainable Energy, LLC This report is available at no cost from the National Renewable Energy Laboratory (NREL) at www.nrel.gov/publications. Contract No.

  3. High order finite difference methods with subcell resolution for advection equations with stiff source terms

    SciTech Connect (OSTI)

    Wang, Wei; Shu, Chi-Wang; Yee, H.C.; Sjgreen, Bjrn

    2012-01-01

    A new high order finite-difference method utilizing the idea of Harten ENO subcell resolution method is proposed for chemical reactive flows and combustion. In reaction problems, when the reaction time scale is very small, e.g., orders of magnitude smaller than the fluid dynamics time scales, the governing equations will become very stiff. Wrong propagation speed of discontinuity may occur due to the underresolved numerical solution in both space and time. The present proposed method is a modified fractional step method which solves the convection step and reaction step separately. In the convection step, any high order shock-capturing method can be used. In the reaction step, an ODE solver is applied but with the computed flow variables in the shock region modified by the Harten subcell resolution idea. For numerical experiments, a fifth-order finite-difference WENO scheme and its anti-diffusion WENO variant are considered. A wide range of 1D and 2D scalar and Euler system test cases are investigated. Studies indicate that for the considered test cases, the new method maintains high order accuracy in space for smooth flows, and for stiff source terms with discontinuities, it can capture the correct propagation speed of discontinuities in very coarse meshes with reasonable CFL numbers.

  4. A Global Climate Model Agent for High Spatial and Temporal Resolution Data

    SciTech Connect (OSTI)

    Wood, Lynn S.; Daily, Jeffrey A.; Henry, Michael J.; Palmer, Bruce J.; Schuchardt, Karen L.; Dazlich, Donald A.; Heikes, Ross P.; Randall, David

    2015-02-01

    Fine cell granularity in modern climate models can produce terabytes of data in each snapshot, causing significant I/O overhead. To address this issue, a method of reducing the I/O latency of high-resolution climate models by identifying and selectively outputting regions of interest is presented. Working with a Global Cloud Resolving Model and running with up to 10240 processors on a Cray XE6, this method provides significant I/O bandwidth reduction depending on the frequency of writes and size of the region of interest. The implementation challenges of determining global parameters in a strictly core-localized model and properly formatting output files that only contain subsections of the global grid are addressed, as well as the overall bandwidth impact and benefits of the method. The gains in I/O throughput provided by this method allow dual output rates for high-resolution climate models: a low-frequency global snapshot as well as a high-frequency regional snapshot when events of particular interest occur.

  5. Tritium trapping in silicon carbide in contact with solid breeder under high flux isotope reactor irradiation

    SciTech Connect (OSTI)

    H. Katsui; Y. Katoh; A. Hasegawa; M. Shimada; Y. Hatano; T. Hinoki; S. Nogami; T. Tanaka; S. Nagata; T. Shikama

    2013-11-01

    The trapping of tritium in silicon carbide (SiC) injected from ceramic breeding materials was examined via tritium measurements using imaging plate (IP) techniques. Monolithic SiC in contact with ternary lithium oxide (lithium titanate and lithium aluminate) as a ceramic breeder was irradiated in the High Flux Isotope Reactor (HFIR) in Oak Ridge, Tennessee, USA. The distribution of photo-stimulated luminescence (PSL) of tritium in SiC was successfully obtained, which separated the contribution of 14C -rays to the PSL. The tritium incident from ceramic breeders was retained in the vicinity of the SiC surface even after irradiation at 1073 K over the duration of ~3000 h, while trapping of tritium was not observed in the bulk region. The PSL intensity near the SiC surface in contact with lithium titanate was higher than that obtained with lithium aluminate. The amount of the incident tritium and/or the formation of a Li2SiO3 phase on SiC due to the reaction with lithium aluminate under irradiation likely were responsible for this observation.

  6. High resolution transmission electron microscopic in-situ observations of plastic deformation of compressed nanocrystalline gold

    SciTech Connect (OSTI)

    Wang, Guoyong; Lian, Jianshe; Jiang, Qing; Sun, Sheng; Zhang, Tong-Yi

    2014-09-14

    Nanocrystalline (nc) metals possess extremely high strength, while their capability to deform plastically has been debated for decades. Low ductility has hitherto been considered an intrinsic behavior for most nc metals, due to the lack of five independent slip systems actively operating during deformation in each nanograin. Here we report in situ high resolution transmission electron microscopic (HRTEM) observations of deformation process of nc gold under compression, showing the excellent ductility of individual and aggregate nanograins. Compression causes permanent change in the profile of individual nanograins, which is mediated by dislocation slip and grain rotation. The high rate of grain boundary sliding and large extent of widely exited grain rotation may meet the boundary compatibility requirements during plastic deformation. The in situ HRTEM observations suggest that nc gold is not intrinsically brittle under compressive loading.

  7. A new variable-resolution associative memory for high energy physics

    SciTech Connect (OSTI)

    Annovi, A.; Amerio, S.; Beretta, M.; Bossini, E.; Crescioli, F.; Dell'Orso, M.; Giannetti, P.; Hoff, J.; Liu, T.; Magalotti, D.; Piendibene, M.; Sacco, I.; Schoening, A.; Soltveit, H. K.; Stabile, A.; Tripiccione, R.; Liberali, V.; Vitillo, R.; Volpi, G.

    2011-07-01

    We describe an important advancement for the Associative Memory device (AM). The AM is a VLSI processor for pattern recognition based on Content Addressable Memory (CAM) architecture. The AM is optimized for on-line track finding in high-energy physics experiments. Pattern matching is carried out by finding track candidates in coarse resolution 'roads'. A large AM bank stores all trajectories of interest, called 'patterns', for a given detector resolution. The AM extracts roads compatible with a given event during detector read-out. Two important variables characterize the quality of the AM bank: its 'coverage' and the level of fake roads. The coverage, which describes the geometric efficiency of a bank, is defined as the fraction of tracks that match at least one pattern in the bank. Given a certain road size, the coverage of the bank can be increased just adding patterns to the bank, while the number of fakes unfortunately is roughly proportional to the number of patterns in the bank. Moreover, as the luminosity increases, the fake rate increases rapidly because of the increased silicon occupancy. To counter that, we must reduce the width of our roads. If we decrease the road width using the current technology, the system will become very large and extremely expensive. We propose an elegant solution to this problem: the 'variable resolution patterns'. Each pattern and each detector layer within a pattern will be able to use the optimal width, but we will use a 'don't care' feature (inspired from ternary CAMs) to increase the width when that is more appropriate. In other words we can use patterns of variable shape. As a result we reduce the number of fake roads, while keeping the efficiency high and avoiding excessive bank size due to the reduced width. We describe the idea, the implementation in the new AM design and the implementation of the algorithm in the simulation. Finally we show the effectiveness of the 'variable resolution patterns' idea using simulated high occupancy events in the ATLAS detector. (authors)

  8. Study of Fish Response Using Particle Image Velocimetry and High-Speed, High-Resolution Imaging

    SciTech Connect (OSTI)

    Deng, Zhiqun; Richmond, Marshall C.; Guensch, Gregory R.; Mueller, Robert P.

    2004-10-23

    Existing literature of previous particle image velocimetry (PIV) studies of fish swimming has been reviewed. Historically, most of the studies focused on the performance evaluation of freely swimming fish. Technological advances over the last decade, especially the development of digital particle image velocimetry (DPIV) technique, make possible more accurate, quantitative descriptions of the flow patterns adjacent to the fish and in the wake behind the fins and tail, which are imperative to decode the mechanisms of drag reduction and propulsive efficiency. For flows generated by different organisms, the related scales and flow regimes vary significantly. For small Reynolds numbers, viscosity dominates; for very high Reynolds numbers, inertia dominates, and three-dimensional complexity occurs. The majority of previous investigations dealt with the lower end of Reynolds number range. The fish of our interest, such as rainbow trout and spring and fall chinook salmon, fall into the middle range, in which neither viscosity nor inertia is negligible, and three-dimensionality has yet to dominate. Feasibility tests have proven the applicability of PIV to flows around fish. These tests have shown unsteady vortex shedding in the wake, high vorticity region and high stress region, with the highest in the pectoral area. This evident supports the observations by Nietzel et al. (2000) and Deng et al. (2004) that the operculum are most vulnerable to damage from the turbulent shear flow, because they are easily pried open, and the large vorticity and shear stress can lift and tear off scales, rupture or dislodge eyes, and damage gills. In addition, the unsteady behavior of the vortex shedding in the wake implies that injury to fish by the instantaneous flow structures would likely be much higher than the injury level estimated using the average values of the dynamics parameters. Based on existing literature, our technological capability, and relevance and practicability to Department of Energy's Hydropower Program, we identified three major research areas of interest: free swimming, the boundary layer over fish, and kinematic response of fish. We propose that the highest priority is to characterize the kinematic response of fish to different turbulent environments such as high shear/turbulence and hydrodynamic disturbances created by solid structures such as deflector and turbine runner blade; the next priority is to map the boundary layer over swimming fish; the last is to document the behavior of freely swimming fish, focusing on fish of our interest. Grid turbulence and Karman vortex street will be employed to map the boundary layers over fish and investigate the effects of environmental disturbances on the swimming performance of fish, because they are well established and documented in engineering literature and are representative of fish's swimming environments. Extreme conditions characteristic of turbine environments, such as strong shear environment and collision, will be investigated. Through controlled laboratory studies, the fish injury mechanism from different sources will be evaluated in isolation. The major goals are to: gain first-hand knowledge of the biological effects under such extreme hydraulic environments in which fish could lack the capability to overcome the perturbations and be vulnerable to injury; Better understand field results by integrating the laboratory studies with the responses of sensor fish device; More importantly, provide well-defined validation cases and boundary conditions for geometry-based computational fluid-structure interaction modeling in order to simulate the complex hydraulic environments in advanced hydropower systems and their effects on fish, greatly enhancing the potential to use CFD as a bio-hydraulic design alternative.

  9. High-resolution multi-band imaging for validation and characterization of small Kepler planets

    SciTech Connect (OSTI)

    Everett, Mark E.; Silva, David R.; Barclay, Thomas; Howell, Steve B.; Ciardi, David R.; Horch, Elliott P.; Crepp, Justin R.

    2015-02-01

    High-resolution ground-based optical speckle and near-infrared adaptive optics images are taken to search for stars in close angular proximity to host stars of candidate planets identified by the NASA Kepler Mission. Neighboring stars are a potential source of false positive signals. These stars also blend into Kepler light curves, affecting estimated planet properties, and are important for an understanding of planets in multiple star systems. Deep images with high angular resolution help to validate candidate planets by excluding potential background eclipsing binaries as the source of the transit signals. A study of 18 Kepler Object of Interest stars hosting a total of 28 candidate and validated planets is presented. Validation levels are determined for 18 planets against the likelihood of a false positive from a background eclipsing binary. Most of these are validated at the 99% level or higher, including five newly validated planets in two systems: Kepler-430 and Kepler-431. The stellar properties of the candidate host stars are determined by supplementing existing literature values with new spectroscopic characterizations. Close neighbors of seven of these stars are examined using multi-wavelength photometry to determine their nature and influence on the candidate planet properties. Most of the close neighbors appear to be gravitationally bound secondaries, while a few are best explained as closely co-aligned field stars. Revised planet properties are derived for each candidate and validated planet, including cases where the close neighbors are the potential host stars.

  10. Indexing Permafrost Soil Organic Matter Degradation Using High-Resolution Mass Spectrometry

    SciTech Connect (OSTI)

    Mann, Benjamin F.; Chen, Hongmei; Herndon, Elizabeth M.; Chu, Rosalie K.; Tolic, Nikola; Portier, Evan F.; Roy Chowdhury, Taniya; Robinson, Errol W.; Callister, Stephen J.; Wullschleger, Stan D.; Graham, David E.; Liang, Liyuan; Gu, Baohua; Hui, Dafeng

    2015-06-12

    Microbial degradation of soil organic matter (SOM) is a key process for terrestrial carbon cycling, although the molecular details of these transformations remain unclear. This study reports the application of ultrahigh resolution mass spectrometry to profile the molecular composition of SOM and its degradation during a simulated warming experiment. A soil sample, collected near Barrow, Alaska, USA, was subjected to a 40-day incubation under anoxic conditions and analyzed before and after the incubation to determine changes of SOM composition. A CHO index based on molecular C, H, and O data was utilized to codify SOM components according to their observed degradation potentials. Compounds with a CHO index score between –1 and 0 in a water-soluble fraction (WSF) demonstrated high degradation potential, with a highest shift of CHO index occurred in the N-containing group of compounds, while similar stoichiometries in a base-soluble fraction (BSF) did not. Additionally, compared with the classical H:C vs O:C van Krevelen diagram, CHO index allowed for direct visualization of the distribution of heteroatoms such as N in the identified SOM compounds. We demonstrate that CHO index is useful not only in characterizing arctic SOM at the molecular level but also enabling quantitative description of SOM degradation, thereby facilitating incorporation of the high resolution MS datasets to future mechanistic models of SOM degradation and prediction of greenhouse gas emissions.

  11. High-resolution laboratory measurements of coronal lines in the 198-218 å region

    SciTech Connect (OSTI)

    Beiersdorfer, Peter; Träbert, Elmar; Lepson, Jaan K.; Brickhouse, Nancy S.; Golub, Leon

    2014-06-10

    We present high-resolution laboratory measurements of the emission from various ions of C, N, O, F, Ne, S, Ar, Fe, and Ni in the extreme ultraviolet wavelength band centered around the λ211 Fe XIV channel of the Atmospheric Imaging Assembly on the Solar Dynamics Observatory. While all of the strong iron lines in this region are well known, we note many weaker lines of iron that are not yet identified. The high resolution of our measurements also allows us to resolve several lines in Fe XI, Fe XII, and Fe XIII between 200 and 205 Å, whose identities were in question based on a disagreement between different databases. The spectra of the elements other than iron are much less known, and we find a multitude of lines that are not yet in the databases. For example, the CHIANTI database clearly disagrees with the NIST data listings on several of the argon lines we observe and also it contains only about half of the observed sulfur lines.

  12. LENS MODELS OF HERSCHEL-SELECTED GALAXIES FROM HIGH-RESOLUTION NEAR-IR OBSERVATIONS

    SciTech Connect (OSTI)

    Calanog, J. A.; Cooray, A.; Ma, B.; Casey, C. M.; Fu, Hai; Wardlow, J.; Amber, S.; Baker, A. J.; Baes, M.; Bock, J.; Bourne, N.; Dye, S.; Bussmann, R. S.; Chapman, S. C.; Clements, D. L.; Conley, A.; Dannerbauer, H.; Dunne, L.; Eales, S.; and others

    2014-12-20

    We present Keck-Adaptive Optics and Hubble Space Telescope high resolution near-infrared (IR) imaging for 500 ?m bright candidate lensing systems identified by the Herschel Multi-tiered Extragalactic Survey and Herschel Astrophysical Terahertz Large Area Survey. Out of 87 candidates with near-IR imaging, 15 (?17%) display clear near-IR lensing morphologies. We present near-IR lens models to reconstruct and recover basic rest-frame optical morphological properties of the background galaxies from 12 new systems. Sources with the largest near-IR magnification factors also tend to be the most compact, consistent with the size bias predicted from simulations and previous lensing models for submillimeter galaxies (SMGs). For four new sources that also have high-resolution submillimeter maps, we test for differential lensing between the stellar and dust components and find that the 880 ?m magnification factor (?{sub 880}) is ?1.5 times higher than the near-IR magnification factor (?{sub NIR}), on average. We also find that the stellar emission is ?2 times more extended in size than dust. The rest-frame optical properties of our sample of Herschel-selected lensed SMGs are consistent with those of unlensed SMGs, which suggests that the two populations are similar.

  13. Turbulence patterns and neutrino flavor transitions in high-resolution supernova models

    SciTech Connect (OSTI)

    Borriello, Enrico; Mirizzi, Alessandro [II. Institut fr Theoretische Physik, Universitt Hamburg, Luruper Chaussee 149, D-22761 Hamburg (Germany); Chakraborty, Sovan [Max-Planck-Institut fr Physik (Werner-Heisenberg-Institut), Fhringer Ring 6, D-80805 Mnchen (Germany); Janka, Hans-Thomas [Max-Planck-Institut fr Astrophysik, Karl-Schwarzschild-Str. 1, 85748 Garching (Germany); Lisi, Eligio, E-mail: enrico.borriello@desy.de, E-mail: sovan@mppmu.mpg.de, E-mail: thj@mpa-garching.mpg.de, E-mail: eligio.lisi@ba.infn.it, E-mail: alessandro.mirizzi@desy.de [INFNSezione di Bari, Via Orabona 4, 70126 Bari (Italy)

    2014-11-01

    During the shock-wave propagation in a core-collapse supernova (SN), matter turbulence may affect neutrino flavor conversion probabilities. Such effects have been usually studied by adding parametrized small-scale random fluctuations (with arbitrary amplitude) on top of coarse, spherically symmetric matter density profiles. Recently, however, two-dimensional (2D) SN models have reached a space resolution high enough to directly trace anisotropic density profiles, down to scales smaller than the typical neutrino oscillation length. In this context, we analyze the statistical properties of a large set of SN matter density profiles obtained in a high-resolution 2D simulation, focusing on a post-bounce time (2 s) suited to study shock-wave effects on neutrino propagation on scales as small as O(100) km and possibly below. We clearly find the imprint of a broken (Kolmogorov-Kraichnan) power-law structure, as generically expected in 2D turbulence spectra. We then compute the flavor evolution of SN neutrinos along representative realizations of the turbulent matter density profiles, and observe no or modest damping of the neutrino crossing probabilities on their way through the shock wave. In order to check the effect of possibly unresolved fluctuations at scales below O(100) km, we also apply a randomization procedure anchored to the power spectrum calculated from the simulation, and find consistent results within 1? fluctuations. These results show the importance of anchoring turbulence effects on SN neutrinos to realistic, fine-grained SN models.

  14. Indexing Permafrost Soil Organic Matter Degradation Using High-Resolution Mass Spectrometry

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Mann, Benjamin F.; Chen, Hongmei; Herndon, Elizabeth M.; Chu, Rosalie K.; Tolic, Nikola; Portier, Evan F.; Roy Chowdhury, Taniya; Robinson, Errol W.; Callister, Stephen J.; Wullschleger, Stan D.; et al

    2015-06-12

    Microbial degradation of soil organic matter (SOM) is a key process for terrestrial carbon cycling, although the molecular details of these transformations remain unclear. This study reports the application of ultrahigh resolution mass spectrometry to profile the molecular composition of SOM and its degradation during a simulated warming experiment. A soil sample, collected near Barrow, Alaska, USA, was subjected to a 40-day incubation under anoxic conditions and analyzed before and after the incubation to determine changes of SOM composition. A CHO index based on molecular C, H, and O data was utilized to codify SOM components according to their observedmore » degradation potentials. Compounds with a CHO index score between –1 and 0 in a water-soluble fraction (WSF) demonstrated high degradation potential, with a highest shift of CHO index occurred in the N-containing group of compounds, while similar stoichiometries in a base-soluble fraction (BSF) did not. Additionally, compared with the classical H:C vs O:C van Krevelen diagram, CHO index allowed for direct visualization of the distribution of heteroatoms such as N in the identified SOM compounds. We demonstrate that CHO index is useful not only in characterizing arctic SOM at the molecular level but also enabling quantitative description of SOM degradation, thereby facilitating incorporation of the high resolution MS datasets to future mechanistic models of SOM degradation and prediction of greenhouse gas emissions.« less

  15. Variability of Photovoltaic Power in the State of Gujarat Using High Resolution Solar Data

    SciTech Connect (OSTI)

    Hummon, M.; Cochran, J.; Weekley, A.; Lopez, A.; Zhang, J.; Stoltenberg, B.; Parsons, B.; Batra, P.; Mehta, B.; Patel, D.

    2014-03-01

    India has ambitious goals for high utilization of variable renewable power from wind and solar, and deployment has been proceeding at a rapid pace. The western state of Gujarat currently has the largest amount of solar generation of any Indian state, with over 855 Megawatts direct current (MWDC). Combined with over 3,240 MW of wind, variable generation renewables comprise nearly 18% of the electric-generating capacity in the state. A new historic 10-kilometer (km) gridded solar radiation data set capturing hourly insolation values for 2002-2011 is available for India. We apply an established method for downscaling hourly irradiance data to one-minute irradiance data at potential PV power production locations for one year, 2006. The objective of this report is to characterize the intra-hour variability of existing and planned photovoltaic solar power generation in the state of Gujarat (a total of 1.9 gigawatts direct current (GWDC)), and of five possible expansion scenarios of solar generation that reflect a range of geographic diversity (each scenario totals 500-1,000 MW of additional solar capacity). The report statistically analyzes one year's worth of power variability data, applied to both the baseline and expansion scenarios, to evaluate diurnal and seasonal power fluctuations, different timescales of variability (e.g., from one to 15 minutes), the magnitude of variability (both total megawatts and relative to installed solar capacity), and the extent to which the variability can be anticipated in advance. The paper also examines how Gujarat Energy Transmission Corporation (GETCO) and the Gujarat State Load Dispatch Centre (SLDC) could make use of the solar variability profiles in grid operations and planning.

  16. High-resolution spectroscopy used to measure inertial confinement fusion neutron spectra on Omega (invited)

    SciTech Connect (OSTI)

    Forrest, C. J.; Radha, P. B.; Glebov, V. Yu.; Goncharov, V. N.; Knauer, J. P.; Pruyne, A.; Romanofsky, M.; Sangster, T. C.; Shoup, M. J. III; Stoeckl, C.; Casey, D. T.; Gatu-Johnson, M.; Gardner, S.

    2012-10-15

    The areal density ({rho}R) of cryogenic DT implosions on Omega is inferred by measuring the spectrum of neutrons that elastically scatter off the dense deuterium (D) and tritium (T) fuel. Neutron time-of-flight (nTOF) techniques are used to measure the energy spectrum with high resolution. High signal-to-background data has been recorded on cryogenic DT implosions using a well-collimated 13.4-m line of sight and an nTOF detector with an advanced liquid scintillator compound. An innovative method to analyze the elastically scattered neutron spectra was developed using well-known cross sections of the DT nuclear reactions. The estimated areal densities are consistent with alternative {rho}R measurements and 1-D simulations.

  17. High-resolution metagenomics targets major functional types in complex microbial communities

    SciTech Connect (OSTI)

    Kalyuzhnaya, Marina G.; Lapidus, Alla; Ivanova, Natalia; Copeland, Alex C.; McHardy, Alice C.; Szeto, Ernest; Salamov, Asaf; Grigoriev, Igor V.; Suciu, Dominic; Levine, Samuel R.; Markowitz, Victor M.; Rigoutsos, Isidore; Tringe, Susannah G.; Bruce, David C.; Richardson, Paul M.; Lidstrom, Mary E.; Chistoserdova, Ludmila

    2009-08-01

    Most microbes in the biosphere remain uncultured and unknown. Whole genome shotgun (WGS) sequencing of environmental DNA (metagenomics) allows glimpses into genetic and metabolic potentials of natural microbial communities. However, in communities of high complexity metagenomics fail to link specific microbes to specific ecological functions. To overcome this limitation, we selectively targeted populations involved in oxidizing single-carbon (C{sub 1}) compounds in Lake Washington (Seattle, USA) by labeling their DNA via stable isotope probing (SIP), followed by WGS sequencing. Metagenome analysis demonstrated specific sequence enrichments in response to different C{sub 1} substrates, highlighting ecological roles of individual phylotypes. We further demonstrated the utility of our approach by extracting a nearly complete genome of a novel methylotroph Methylotenera mobilis, reconstructing its metabolism and conducting genome-wide analyses. This approach allowing high-resolution genomic analysis of ecologically relevant species has the potential to be applied to a wide variety of ecosystems.

  18. High resolution interface nanochemistry and structure: Final project report, December 1, 1993--February 28, 1997

    SciTech Connect (OSTI)

    Carpenter, R.W.; Lin, S.H.

    1997-02-27

    Work includes studies of interface and grain boundary chemistry and structure in silicon nitride matrix/silicon carbide whisker composites, and in monolithic silicon nitride and silicon carbide synthesized by several different methods. Off-stoichiometric, impurity, and sintering aid elemental distributions in these materials (and other ceramics) have been of great interest because of expected effects on properties but these distributions have proven very difficult to measure because the spatial resolution required is high. The authors made a number of these measurements for the first time, using techniques and instrumentation developed here. Interfaces between metals and SiC are the basis for important metal matrix composites and contacts for high temperature SiC-based solid state electronic devices. The authors have investigated ultrapure interfaces between Ti, Hf, Ti-Hf alloys, Pt, and Co and Si-terminated (0001) 6H SiC single crystals for the first time.

  19. TH-A-BRF-09: Integration of High-Resolution MRSI Into Glioblastoma Treatment Planning

    SciTech Connect (OSTI)

    Schreibmann, E; Cordova, J; Shu, H; Crocker, I; Curran, W; Holder, C; Shim, H

    2014-06-15

    Purpose: Identification of a metabolite signature that shows significant tumor cell infiltration into normal brain in regions that do not appear abnormal on standard MRI scans would be extremely useful for radiation oncologists to choose optimal regions of brain to treat, and to quantify response beyond the MacDonald criteria. We report on integration of high-resolution magnetic resonance spectroscopic imaging (HR-MRSI) with radiation dose escalation treatment planning to define and target regions at high risk for recurrence. Methods: We propose to supplement standard MRI with a special technique performed on an MRI scanner to measure the metabolite levels within defined volumes. Metabolite imaging was acquired using an advanced MRSI technique combining 3D echo-planar spectroscopic imaging (EPSI) with parallel acquisition (GRAPPA) using a multichannel head coil that allows acquisition of whole brain metabolite maps with 108 μl resolution in 12 minutes implemented on a 3T MR scanner. Elevation in the ratio of two metabolites, choline (Cho, elevated in proliferating high-grade gliomas) and N-acetyl aspartate (NAA, a normal neuronal metabolite), was used to image infiltrating high-grade glioma cells in vivo. Results: The metabolite images were co-registered with standard contrast-enhanced T1-weighted MR images using in-house registration software and imported into the treatment-planning system. Regions with tumor infiltration are identified on the metabolic images and used to create adaptive IMRT plans that deliver a standard dose of 60 Gy to the standard target volume and an escalated dose of 75 Gy (or higher) to the most suspicious regions, identified as areas with elevated Cho/NAA ratio. Conclusion: We have implemented a state-of-the-art HR-MRSI technology that can generate metabolite maps of the entire brain in a clinically acceptable scan time, coupled with introduction of an imaging co-registration/ analysis program that combines MRSI data with standard imaging studies in a clinically useful fashion.

  20. SIEMENS ADVANCED QUANTRA FTICR MASS SPECTROMETER FOR ULTRA HIGH RESOLUTION AT LOW MASS

    SciTech Connect (OSTI)

    Spencer, W; Laura Tovo, L

    2008-07-08

    The Siemens Advanced Quantra Fourier Transform Ion Cyclotron Resonance (FTICR) mass spectrometer was evaluated as an alternative instrument to large double focusing mass spectrometers for gas analysis. High resolution mass spectrometers capable of resolving the common mass isomers of the hydrogen isotopes are used to provide data for accurate loading of reservoirs and to monitor separation of tritium, deuterium, and helium. Conventional double focusing magnetic sector instruments have a resolution that is limited to about 5000. The Siemens FTICR instrument achieves resolution beyond 400,000 and could possibly resolve the tritium ion from the helium-3 ion, which differ by the weight of an electron, 0.00549 amu. Working with Y-12 and LANL, SRNL requested Siemens to modify their commercial Quantra system for low mass analysis. To achieve the required performance, Siemens had to increase the available waveform operating frequency from 5 MHz to 40 MHz and completely redesign the control electronics and software. However, they were able to use the previous ion trap, magnet, passive pump, and piezo-electric pulsed inlet valve design. NNSA invested $1M in this project and acquired four systems, two for Y-12 and one each for SRNL and LANL. Siemens claimed a $10M investment in the Quantra systems. The new Siemens Advanced Quantra demonstrated phenomenal resolution in the low mass range. Resolution greater than 400,000 was achieved for mass 2. The new spectrometer had a useful working mass range to 500 Daltons. However, experiments found that a continuous single scan from low mass to high was not possible. Two useful working ranges were established covering masses 1 to 6 and masses 12 to 500 for our studies. A compromise performance condition enabled masses 1 to 45 to be surveyed. The instrument was found to have a dynamic range of about three orders of magnitude and quantitative analysis is expected to be limited to around 5 percent without using complex fitting algorithms. Analysis of low concentration ions, at the ppm level, required a separate analysis using ion ejection techniques. Chemical ionization due to the formation of the MH{sup +} ion or MD{sup +} increased the complexity of the spectra compared to magnetic sector mass spectra and formation of the protonated or deuterated complex was a dynamic function of the trap ion concentration. This made quantitative measurement more of a challenge. However, the resolution of the instrument was far superior to any other mass spectrometry technique that has been applied to the analysis of the hydrogen isotopes. The piezo-electric picoliter injection device offers a new way of submitting small quantities of atmospheric pressure sample gas for analysis. The new software had many improvements over the previous version but significant flaws in the beta codes remain that make the prototype units less than ideal. The instrument is a promising new technology that experience will likely improve. Unfortunately, Siemens has concluded that the technology will not be a commercial success and has decided to stop producing this product.

  1. High resolution monochromator for inelastic scattering studies of high energy phonons using undulator radiation at the advanced photon source

    SciTech Connect (OSTI)

    Macrander, A.T.; Schwoerer-Boehning, M.; Abbamonte, P.M.; Hu, M.

    1997-08-01

    A monochromator for use at 13.84 keV with a calculated bandpass of 5.2 meV was designed built, and tested. Tuning was performed by rotating the inner crystal of a pair of nested silicon channel-cut crystals. The inner crystal employs the (884) reflection, and the outer crystal employs a collimating asymmetric (422) reflection (dynamical asymmetry factor, b, equal to {minus}17.5). Tests were done with a double-crystal Si(111) pre-monochromator situated upstream of the high resolution monochromator and a Si(777) backscattering crystal situated downstream. For this optical arrangement an ideal value of 6.3 meV as calculated by x-ray dynamical diffraction theory applies for the FWHM of the convolution of the net monochromator reflectivity function with that of the Si(777) reflection. This calculated value is to be compared to the value of 7.1 meV measured by tuning the high resolution monochromator. Measured efficiencies were less than ideal by a factor of 3.2 to 4.9, where the larger flux reduction factors were found with higher positron storage ring currents.

  2. Heavy resid asphaltene characterization using high resolution and laser desorption mass spectrometry

    SciTech Connect (OSTI)

    Hunt, J.E.; Kim, Y.; Winans, R.E.

    1995-12-31

    Resid is the nondistillable portion of crude oil, generally thought to consist largely of unsaturated molecules of considerable size and ring number. Such molecules must be upgraded to more saturated compounds if they are to be used as fuel sources. Current processing of resid is performed though coking, thermal and catalytic cracking, deasphalting and hydroprocessing. Thermal treatments, however, produce large quantities of low-value coke and hydroprocessing is expensive. Asphaltenes comprise the most process resistant portion of the resid. They contain high concentrations of heteroatoms and a high degree of unsaturation. Because these undesirable characteristics are concentrated in asphaltenes, finding an improved method of upgrading asphaltenes is a prerequisite to improving the upgrading of whole resid to viable fuel. Asphaltenes have, at present, only an operational definition. They are insoluble in straight chain saturated hydrocarbons. Very little is known about the structure of compounds in asphaltenes. They are a highly diverse group of compounds that are resistant to analysis by conventional methods. Conclusions about the structures of asphaltenes tends to be speculative. In this study desorption electron impact (HREIMS), chemical ionization high resolution mass spectrometry (HRCIMS), and laser desorption mass spectrometry (LD) have been applied to deasphalted oils (DAO) and asphaltenes derived from heavy Maya resid. LD data should yield information on the high molecular weight aromatic compounds, while HRMS can provide molecular characterization.

  3. FIRST HIGH-RESOLUTION IMAGES OF THE SUN IN THE 2796 Mg II k LINE

    SciTech Connect (OSTI)

    Riethmller, T. L.; Solanki, S. K.; Hirzberger, J.; Danilovic, S.; Barthol, P.; Gandorfer, A.; Gizon, L.; Berkefeld, T.; Schmidt, W.; Knlker, M.; Del Toro Iniesta, J. C.

    2013-10-10

    We present the first high-resolution solar images in the Mg II k 2796 line. The images, taken through a 4.8 broad interference filter, were obtained during the second science flight of Sunrise in 2013 June by the Sunrise Filter Imager (SuFI) instrument. The Mg II k images display structures that look qualitatively very similar to images taken in the core of Ca II H. The Mg II images exhibit reversed granulation (or shock waves) in the internetwork regions of the quiet Sun, at intensity contrasts that are similar to those found in Ca II H. Very prominent in Mg II are bright points, both in the quiet Sun and in plage regions, particularly near the disk center. These are much brighter than at other wavelengths sampled at similar resolution. Furthermore, Mg II k images also show fibril structures associated with plage regions. Again, the fibrils are similar to those seen in Ca II H images, but tend to be more pronounced, particularly in weak plage.

  4. Unsupervised individual tree crown detection in high-resolution satellite imagery

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Skurikhin, Alexei N.; McDowell, Nate G.; Middleton, Richard S.

    2016-01-26

    Rapidly and accurately detecting individual tree crowns in satellite imagery is a critical need for monitoring and characterizing forest resources. We present a two-stage semiautomated approach for detecting individual tree crowns using high spatial resolution (0.6 m) satellite imagery. First, active contours are used to recognize tree canopy areas in a normalized difference vegetation index image. Given the image areas corresponding to tree canopies, we then identify individual tree crowns as local extrema points in the Laplacian of Gaussian scale-space pyramid. The approach simultaneously detects tree crown centers and estimates tree crown sizes, parameters critical to multiple ecosystem models. Asmore » a demonstration, we used a ground validated, 0.6 m resolution QuickBird image of a sparse forest site. The two-stage approach produced a tree count estimate with an accuracy of 78% for a naturally regenerating forest with irregularly spaced trees, a success rate equivalent to or better than existing approaches. In addition, our approach detects tree canopy areas and individual tree crowns in an unsupervised manner and helps identify overlapping crowns. Furthermore, the method also demonstrates significant potential for further improvement.« less

  5. High resolution transmission electron microscopy of melamine-formaldehyde aerogels and silica aerogels

    SciTech Connect (OSTI)

    Ruben, G.C. (Dartmouth Coll., Hanover, NH (United States). Dept. of Biological Sciences)

    1991-09-01

    The goal of the high resolution transmission electron microscopy (HRTEM) was to image the structure of two tetramethyl orthosilicate (TMOS) and two melamine-formaldehyde (MF) aerogels at the single polymer chain level{sup 1,2}. With this level of structural resolution we hoped to interrelate each aerogel's structure with its physical properties and its method of synthesis. Conventional single-step base catalysed TMOS aerogels show strings of spheroidal particles linked together with minimal necking. The spheroidal particles range from 86--132 {Angstrom} and average 113{plus minus}10 {Angstrom} in diameter{sup 2}. In contrast the TMOS aerogels reported on here were made by a two step method. After extended silica chains are grown in solution under acidic conditions with a substoichiometric amount of water, the reaction is stopped and the methanol hydrolysed from TMOS is removed. Then base catalysis and additional water are added to cause gel formation is a nonalcoholic solvent. The MF aerogels were prepared for HRTEM by fracturing them on a stereo microscope stage with razor knife so that fractured pieces with smooth flat surfaces could be selected for platinum-carbon replication. The two silica (TMOS) aerogels were both transparent and difficult to see. These aerogels were fractured on a stereo microscope stage with tweezers. 6 refs., 4 figs.

  6. A compact and miniaturized high resolution capacitance dilatometer for measuring thermal expansion and magnetostriction

    SciTech Connect (OSTI)

    Kuechler, R.; Bauer, T.; Brando, M.; Steglich, F.

    2012-09-15

    We describe the design, construction, calibration, and two different applications of a miniature capacitance dilatometer. The device is suitable for thermal expansion and magnetostriction measurements from 300 K down to about 25 mK, with a resolution of 0.02 A at low temperatures. The main body of the dilatometer is fabricated from a single block of a Be-Cu alloy by electrical discharge milling. This creates an extremely compact high-resolution measuring cell. We have successfully tested and operated dilatometers of this new type with the commonly used physical property measurement system by quantum design, as well as with several other cryogenic refrigeration systems down to 25 mK and in magnetic fields up to 20 T. Here, the capacitance is measured with a commercially available capacitance bridge. Using a piezoelectric rotator from Attocube Systems, the cell can be rotated at T= 25 mK inside of an inner vacuum chamber of 40 mm diameter. The miniaturized design for the one-axis rotation setup allows a rotation of 360 Degree-Sign .

  7. LANAI HIGH-DENSITY IRRADIANCE SENSOR NETWORK FOR CHARACTERIZING SOLAR RESOURCE VARIABILITY OF MW-SCALE PV SYSTEM

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    LANAI HIGH-DENSITY IRRADIANCE SENSOR NETWORK FOR CHARACTERIZING SOLAR RESOURCE VARIABILITY OF MW-SCALE PV SYSTEM Scott Kuszamaul 1 , Abraham Ellis 1 , Joshua Stein 1 , and Lars Johnson 2 1 Sandia National Laboratories, Albuquerque, NM, USA 2 SunPower Corporation, Richmond, CA, USA ABSTRACT Sandia National Laboratories (Sandia) and SunPower Corporation (SunPower) have completed design and deployment of an autonomous irradiance monitoring system based on wireless mesh communications and a battery

  8. High-Resolution Characterization of Intergranular Attack and Stress Corrosion Cracking of Alloy 600 in High-Temperature Primary Water

    SciTech Connect (OSTI)

    Thomas, Larry E.; Bruemmer, Stephen M.

    2000-06-01

    Intergranular (IG) attack regions and stress-corrosion cracks in alloy 600 U-bend samples tested in 330C, pressurized-water-reactor water have been characterized by analytical transmission electron microscopy (ATEM). Observations of cross-sectional samples revealed short oxidized zones preceding crack tips and narrow (10-nm wide), deeply penetrated, oxidized zones along grain boundaries exposed along open cracks. High-resolution TEM imaging and fine-probe analysis were used to determine the local chemistries and structures in these corrosion-affected zones. Matrix areas surrounding the crack tips appeared highly strained, whereas the IG penetrations generally did not. The predominant oxide structure found along crack walls and just ahead of crack tips was NiO with metal-atom ratios similar to the alloy. The attacked grain boundaries off open cracks contained similar fine-grained NiO-structure oxide together with local areas of Cr-rich oxide and Ni-rich metal. In contrast, Cr-rich oxide identified as Cr2O3 predominated at the leading edges of the IG attack. Stereoscopic imaging of these tip structures revealed nm-scale porosity and tunnels within the oxide and pores along the grain-boundary plane ahead of the oxide. The general interpretation of these results is that IG attack and cracking follows local dissolution or oxidation and the formation of pores at grain boundaries. This degradation occurs at the nanometer scale and therefore requires high-resolution ATEM methods to reveal detailed characteristics. Experimental support for several possible IG degradation mechanisms is considered.

  9. Ultraviolet high-spectral-resolution Doppler lidar for measuring wind field and aerosol optical properties

    SciTech Connect (OSTI)

    Imaki, Masaharu; Kobayashi, Takao

    2005-10-01

    An ultraviolet incoherent Doppler lidar that incorporates the high-spectral-resolution (HSR) technique has been developed for measuring the wind field and aerosol optical properties in the troposphere. An injection seeded and tripled Nd:YAG laser at an ultraviolet wavelength of 355 nm was used in the lidar system. The HRS technique can resolve the aerosol Mie backscatter and the molecular Rayleigh backscatter to derive the signal components. By detecting the Mie backscatter, a great increase in the Doppler filter sensitivity was realized compared to the conventional incoherent Doppler lidars that detected the Rayleigh backscatter. The wind velocity distribution in a two-dimensional cross section was measured. By using the HSR technique, multifunction and absolute value measurements were realized for aerosol extinction, and volume backscatter coefficients; the laser beam transmittance, the lidar ratio, and the backscatter ratio are derived from these measurements.

  10. A tunable low-energy photon source for high-resolution angle-resolved photoemission spectroscopy

    SciTech Connect (OSTI)

    Harter, John W.; Monkman, Eric J.; Shai, Daniel E.; Nie Yuefeng; Uchida, Masaki; Burganov, Bulat; Chatterjee, Shouvik; King, Philip D. C.; Shen, Kyle M.

    2012-11-15

    We describe a tunable low-energy photon source consisting of a laser-driven xenon plasma lamp coupled to a Czerny-Turner monochromator. The combined tunability, brightness, and narrow spectral bandwidth make this light source useful in laboratory-based high-resolution photoemission spectroscopy experiments. The source supplies photons with energies up to {approx}7 eV, delivering under typical conditions >10{sup 12} ph/s within a 10 meV spectral bandwidth, which is comparable to helium plasma lamps and many synchrotron beamlines. We first describe the lamp and monochromator system and then characterize its output, with attention to those parameters which are of interest for photoemission experiments. Finally, we present angle-resolved photoemission spectroscopy data using the light source and compare its performance to a conventional helium plasma lamp.

  11. Energy optimization of a regular macromolecular crystallography beamline for ultra-high-resolution crystallography

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Rosenbaum, Gerd; Ginell, Stephan L.; Chen, Julian C.-H.

    2015-01-01

    In this study, a practical method for operating existing undulator synchrotron beamlines at photon energies considerably higher than their standard operating range is described and applied at beamline 19-ID of the Structural Biology Center at the Advanced Photon Source enabling operation at 30 keV. Adjustments to the undulator spectrum were critical to enhance the 30 keV flux while reducing the lower- and higher-energy harmonic contamination. A Pd-coated mirror and Al attenuators acted as effective low- and high-bandpass filters. The resulting flux at 30 keV, although significantly lower than with X-ray optics designed and optimized for this energy, allowed for accuratemore » data collection on crystals of the small protein crambin to 0.38 Å resolution.« less

  12. High resolution, shallow seismic reflection survey of the Pen Branch fault

    SciTech Connect (OSTI)

    Stieve, A.

    1991-05-15

    The purpose of this project, at the Savannah River River Site (SRS) was to acquire, process, and interpret 28 km (17.4 miles) of high resolution seismic reflection data taken across the trace of the Pen Branch fault and other suspected, intersecting north-south trending faults. The survey was optimized for the upper 300 ft of geologic strata in order to demonstrate the existence of very shallow, flat lying horizons, and to determine the depth of the fault or to sediments deformed by the fault. Field acquisition and processing parameters were selected to define small scale spatial variability and structural features in the vicinity of the Pen Branch fault leading to the definition and the location of the Pen Branch fault, the shallowest extent of the fault, and the quantification of the sense and magnitude of motion. Associated geophysical, borehole, and geologic data were incorporated into the investigation to assist in the determination of optimal parameters and aid in the interpretation.

  13. Compact, high-resolution, gamma ray imaging for scintimammography and other medical diagostic applications

    DOE Patents [OSTI]

    Majewski, Stanislaw; Weisenberger, Andrew G.; Wojcik, Randolph F.; Steinbach, Daniela

    1999-01-01

    A high resolution gamma ray imaging device includes an aluminum housing, a lead screen collimator at an opened end of the housing, a crystal scintillator array mounted behind the lead screen collimator, a foam layer between the lead screen collimator and the crystal scintillator array, a photomultiplier window coupled to the crystal with optical coupling grease, a photomultiplier having a dynode chain body and a base voltage divider with anodes, anode wire amplifiers each connected to four anodes and a multi pin connector having pin connections to each anode wire amplifier. In one embodiment the crystal scintillator array includes a yttrium aluminum perovskite (YAP) crystal array. In an alternate embodiment, the crystal scintillator array includes a gadolinium oxyorthosilicate (GSO) crystal array.

  14. Tip radius preservation for high resolution imaging in amplitude modulation atomic force microscopy

    SciTech Connect (OSTI)

    Ramos, Jorge R.

    2014-07-28

    The acquisition of high resolution images in atomic force microscopy (AFM) is correlated to the cantilever's tip shape, size, and imaging conditions. In this work, relative tip wear is quantified based on the evolution of a direct experimental observable in amplitude modulation atomic force microscopy, i.e., the critical amplitude. We further show that the scanning parameters required to guarantee a maximum compressive stress that is lower than the yield/fracture stress of the tip can be estimated via experimental observables. In both counts, the optimized parameters to acquire AFM images while preserving the tip are discussed. The results are validated experimentally by employing IgG antibodies as a model system.

  15. High-resolution NMR spectroscopy of biological tissues usingprojected Magic Angle Spinning

    SciTech Connect (OSTI)

    Martin, Rachel W.; Jachmann, Rebecca C.; Sakellariou, Dimitris; Nielsen, Ulla Gro; Pines, Alexander

    2005-01-27

    High-resolution NMR spectra of materials subject toanisotropic broadening are usually obtained by rotating the sample aboutthe magic angle, which is 54.7 degrees to the static magnetic field. Inprojected Magic Angle Spinning (p-MAS), the sample is spun about twoangles, neither of which is the magic angle. This provides a method ofobtaining isotropic spectra while spinning at shallow angles. The p-MASexperiment may be used in situations where spinning the sample at themagic angle is not possible due to geometric or other constraints,allowing the choice of spinning angle to be determined by factors such asthe shape of the sample, rather than by the spin physics. The applicationof this technique to bovine tissue samples is demonstrated as a proof ofprinciple for future biological or medical applications.

  16. High resolution electron microscopy study of as-prepared and annealed tungsten-carbon multilayers

    SciTech Connect (OSTI)

    Nguyen, T.D.; Gronsky, R.; Kortright, J.B.

    1988-12-01

    A series of sputtered tungsten-carbon multilayer structures with periods ranging from 2 to 12 nm in the as-prepared state and after annealing at 500/degree/C for 4 hours has been studied with high resolution transmission electron microscopy. The evolution with annealing of the microstructure of these multilayers depends on their period. As-prepared structures appear predominantly amorphous from TEM imaging and diffraction. Annealing results in crystallization of the W-rich layers into WC in the larger period samples, and less complete or no crystallization in the smaller period samples. X-ray scattering reveals that annealing expands the period in a systematic way. The layers remain remarkably well-defined after annealing under these conditions. 12 refs., 4 figs., 1 tab.

  17. Applying high resolution SyXRD analysis on sulfate attacked concrete field samples

    SciTech Connect (OSTI)

    Stroh, J.; Schlegel, M.-C.; Irassar, E.F.; Meng, B.; Emmerling, F.

    2014-12-15

    High resolution synchrotron X-ray diffraction (SyXRD) was applied for a microstructural profile analysis of concrete deterioration after sulfate attack. The cement matrices consist of ordinary Portland cement and different amounts of supplementary cementitious materials, such as fly ash, natural pozzolana and granulated blast furnace slag. The changes of the phase composition were determined along the direction of sulfate ingress. This approach allows the identification of reaction fronts and zones of different phase compositions and conclusions about the mechanisms of sulfate attack. Two reaction fronts were localized in the initial 4 mm from the sample surface. The mechanism of deterioration caused by the exposition in the sulfate-bearing soil is discussed. SyXRD is shown to be a reliable method for investigation of cementitious materials with aggregates embedded in natural environments.

  18. Surface composition, microstructure and corrosion resistance of AZ31 magnesium alloy irradiated by high-intensity pulsed ion beam

    SciTech Connect (OSTI)

    Li, P., E-mail: pli@sqnc.edu.cn [Department of Physics and Information Engineering, Shangqiu Normal University, Shangqiu 476000 (China); Surface Engineering Laboratory, School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Lei, M.K., E-mail: surfeng@dlut.edu.cn [Surface Engineering Laboratory, School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China); Zhu, X.P. [Surface Engineering Laboratory, School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024 (China)

    2011-06-15

    High-intensity pulsed ion beam (HIPIB) irradiation of AZ31 magnesium alloy is performed and electrochemical corrosion experiment of irradiated samples is carried out by using potentiodynamic polarization technology in order to explore the effect of HIPIB irradiation on corrosion resistance of magnesium alloy. The surface composition, cross-sectional morphology and microstructure are characterized by using electron probe microanalyzer, optical microscope and transmission electron microscope, respectively. The results indicated that HIPIB irradiation leads to a significant improvement in corrosion resistance of magnesium alloy, in terms of the considerable increase in both corrosion potential and pitting breakdown potential. The microstructural refinement and surface purification induced by HIPIB irradiation are responsible for the improved corrosion resistance. - Research Highlights: {yields} A modified layer about 30 {mu}m thick is obtained by HIPIB irradiation. {yields} Selective ablation of element/impurity phase having lower melting point is observed. {yields} More importantly, microstructural refinement occurred on the irradiated surface. {yields} The modified layer exhibited a significantly improved corrosion resistance. {yields} Improved corrosion resistance is ascribed to the combined effect induced by HIPIB.

  19. High-resolution structure of a retroviral protease folded as a monomer

    SciTech Connect (OSTI)

    Gilski, Miroslaw [A. Mickiewicz University, 60-780 Poznan (Poland); Polish Academy of Sciences, 61-704 Poznan (Poland); Kazmierczyk, Maciej; Krzywda, Szymon [A. Mickiewicz University, 60-780 Poznan (Poland); Zbransk, Helena [Academy of Sciences of the Czech Republic, 166 10 Prague (Czech Republic); Cooper, Seth; Popovi?, Zoran [University of Washington, Box 352350, Seattle, WA 98195 (United States); Khatib, Firas; DiMaio, Frank; Thompson, James; Baker, David [University of Washington, Box 357350, Seattle, WA 98195 (United States); Pichov, Iva [Academy of Sciences of the Czech Republic, 166 10 Prague (Czech Republic); Jaskolski, Mariusz, E-mail: mariuszj@amu.edu.pl [A. Mickiewicz University, 60-780 Poznan (Poland); Polish Academy of Sciences, 61-704 Poznan (Poland)

    2011-11-01

    The crystal structure of MasonPfizer monkey virus protease folded as a monomer has been solved by molecular replacement using a model generated by players of the online game Foldit. The structure shows at high resolution the details of a retroviral protease folded as a monomer which can guide rational design of protease dimerization inhibitors as retroviral drugs. MasonPfizer monkey virus (M-PMV), a D-type retrovirus assembling in the cytoplasm, causes simian acquired immunodeficiency syndrome (SAIDS) in rhesus monkeys. Its pepsin-like aspartic protease (retropepsin) is an integral part of the expressed retroviral polyproteins. As in all retroviral life cycles, release and dimerization of the protease (PR) is strictly required for polyprotein processing and virion maturation. Biophysical and NMR studies have indicated that in the absence of substrates or inhibitors M-PMV PR should fold into a stable monomer, but the crystal structure of this protein could not be solved by molecular replacement despite countless attempts. Ultimately, a solution was obtained in mr-rosetta using a model constructed by players of the online protein-folding game Foldit. The structure indeed shows a monomeric protein, with the N- and C-termini completely disordered. On the other hand, the flap loop, which normally gates access to the active site of homodimeric retropepsins, is clearly traceable in the electron density. The flap has an unusual curled shape and a different orientation from both the open and closed states known from dimeric retropepsins. The overall fold of the protein follows the retropepsin canon, but the C{sup ?} deviations are large and the active-site DTG loop (here NTG) deviates up to 2.7 from the standard conformation. This structure of a monomeric retropepsin determined at high resolution (1.6 ) provides important extra information for the design of dimerization inhibitors that might be developed as drugs for the treatment of retroviral infections, including AIDS.

  20. COMPLEX ORGANIC MOLECULES AT HIGH SPATIAL RESOLUTION TOWARD ORION-KL. I. SPATIAL SCALES

    SciTech Connect (OSTI)

    Widicus Weaver, Susanna L.; Friedel, Douglas N. E-mail: friedel@astro.illinois.edu

    2012-08-01

    Here we present high spatial resolution (<1'') observations of molecular emission in Orion-KL conducted using the Combined Array for Research in Millimeter-wave Astronomy. This work was motivated by recent millimeter continuum imaging studies of this region conducted at a similarly high spatial resolution, which revealed that the bulk of the emission arises from numerous compact sources, rather than the larger-scale extended structures typically associated with the Orion Hot Core and Compact Ridge. Given that the spatial extent of molecular emission greatly affects the determination of molecular abundances, it is important to determine the true spatial scale for complex molecules in this region. Additionally, it has recently been suggested that the relative spatial distributions of complex molecules in a source might give insight into the chemical mechanisms that drive complex chemistry in star-forming regions. In order to begin to address these issues, this study seeks to determine the spatial distributions of ethyl cyanide [C{sub 2}H{sub 5}CN], dimethyl ether [(CH{sub 3}){sub 2}O], methyl formate [HCOOCH{sub 3}], formic acid [HCOOH], acetone [(CH{sub 3}){sub 2}CO], SiO, methanol [CH{sub 3}OH], and methyl cyanide [CH{sub 3}CN] in Orion-KL at {lambda} = 3 mm. We find that for all observed molecules, the molecular emission arises from multiple components of the cloud that include a range of spatial scales and physical conditions. Here, we present the results of these observations and discuss the implications for studies of complex molecules in star-forming regions.

  1. A HIGH-RESOLUTION ATLAS OF URANIUM-NEON IN THE H BAND

    SciTech Connect (OSTI)

    Redman, Stephen L.; Terrien, Ryan; Mahadevan, Suvrath; Ramsey, Lawrence W.; Bender, Chad F. [Department of Astronomy and Astrophysics, Pennsylvania State University, University Park, PA 16802 (United States); Ycas, Gabriel G. [Department of Physics, University of Colorado, Boulder, CO 80309 (United States); Osterman, Steven N. [Center for Astrophysics and Space Astronomy, University of Colorado, Boulder, CO 80309 (United States); Diddams, Scott A.; Quinlan, Franklyn [Time and Frequency Division, National Institute of Standards and Technology, Boulder, CO 80305 (United States); Lawler, James E. [Department of Physics, University of Wisconsin, 1150 University Avenue, Madison, WI 53706 (United States); Nave, Gillian [Atomic Physics Division, National Institute of Standards and Technology, Gaithersburg, MD 20899 (United States)

    2012-03-01

    We present a high-resolution (R Almost-Equal-To 50,000) atlas of a uranium-neon (U/Ne) hollow-cathode spectrum in the H band (1454-1638 nm) for the calibration of near-infrared spectrographs. We obtained this U/Ne spectrum simultaneously with a laser-frequency comb spectrum, which we used to provide a first-order calibration to the U/Ne spectrum. We then calibrated the U/Ne spectrum using the recently published uranium line list of Redman et al., which is derived from high-resolution Fourier transform spectrometer measurements. These two independent calibrations allowed us to easily identify emission lines in the hollow-cathode lamp that do not correspond to known (classified) lines of either uranium or neon, and to compare the achievable precision of each source. Our frequency comb precision was limited by modal noise and detector effects, while the U/Ne precision was limited primarily by the signal-to-noise ratio (S/N) of the observed emission lines and our ability to model blended lines. The standard deviation in the dispersion solution residuals from the S/N-limited U/Ne hollow-cathode lamp was 50% larger than the standard deviation of the dispersion solution residuals from the modal-noise-limited laser-frequency comb. We advocate the use of U/Ne lamps for precision calibration of near-infrared spectrographs, and this H-band atlas makes these lamps significantly easier to use for wavelength calibration.

  2. Using Measurements of Fill Factor at High Irradiance to Deduce Heterobarrier Band Offsets: Preprint

    SciTech Connect (OSTI)

    Olson, J. M.; Steiner, M. A.; Kanevce, A.

    2011-07-01

    Using a 2D device simulation tool, we examine the high irradiance behavior of a single junction, GaAs concentrator cell as a function of the doping in the back surface confinement layer. The confinement layer is designed to be a barrier for both holes and electrons in the base of the solar cell. For a p-type base we show that the FF of the cell at high concentrations is a strong function of both the magnitude of the valence band offset and the doping level in the barrier. In short, for a given valence band offset (VBO), there is a critical barrier doping, below which the FF drops rapidly with lower doping. This behavior is confirmed experimentally for a GaInP/GaAs double heterostructure solar cell where the critical doping concentration (at 500 suns) in the back surface confinement layer is ~1e18 cm-3 for a VBO of 300 meV.

  3. High-resolution Tangential AXUV Arrays for Radiated Power Density Measurements on NSTX-U

    SciTech Connect (OSTI)

    Delgado-Aparicio, L; Bell, R E; Faust, I; Tritz, K; Diallo, A; Gerhardt, S P; Kozub, T A; LeBlanc, B P; Stratton, B C

    2014-07-01

    Precise measurements of the local radiated power density and total radiated power are a matter of the uttermost importance for understanding the onset of impurity-induced instabilities and the study of particle and heat transport. Accounting of power balance is also needed for the understanding the physics of various divertor con#12;gurations for present and future high-power fusion devices. Poloidal asymmetries in the impurity density can result from high Mach numbers and can impact the assessment of their flux-surface-average and hence vary the estimates of P[sub]rad (r, t) and (Z[sub]eff); the latter is used in the calculation of the neoclassical conductivity and the interpretation of non-inductive and inductive current fractions. To this end, the bolometric diagnostic in NSTX-U will be upgraded, enhancing the midplane coverage and radial resolution with two tangential views, and adding a new set of poloidally-viewing arrays to measure the 2D radiation distribution. These systems are designed to contribute to the near- and long-term highest priority research goals for NSTX-U which will integrate non-inductive operation at reduced collisionality, with high-pressure, long energy-confinement-times and a divertor solution with metal walls.

  4. Practical high resolution detection method for laser-induced breakdown spectroscopy

    SciTech Connect (OSTI)

    Andrew J. Effenberger Jr; Jill R. Scott

    2012-02-01

    A Fabry-Perot etalon was coupled to a Czerny-Turner spectrometer to acquire high-resolution measurements in laser-induced breakdown spectroscopy (LIBS). The spectrometer was built using an inexpensive etalon coupled to a standard 0.5-m imaging spectrometer. The Hg emission doublet at 313.2 nm was used to evaluate instrument performance because it has a splitting of 29 pm. The 313.2 nm doublet was chosen due to the similar splitting seen in isotope splitting from uranium at 424.437 nm, which is 25 pm. The Hg doublet was easily resolved from a continuous source Hg-lamp with a 2 s acquisition. The doublet was also resolved in LIBS spectra of cinnabar (HgS) from the accumulation of 600 laser shots at rate of 10 Hz, or 1 min, under a helium atmosphere. In addition to observed spitting of the 313.2 nm Hg doublet, the FWHM of the 313.1844 nm line from the doublet is reported at varying He atmospheric pressures. The high performance, low cost, and compact footprint makes this system highly competitive with 2-m double pass Czerny-Turner spectrometers.

  5. Appending High-Resolution Elevation Data to GPS Speed Traces for Vehicle Energy Modeling and Simulation

    SciTech Connect (OSTI)

    Wood, E.; Burton, E.; Duran, A.; Gonder, J.

    2014-06-01

    Accurate and reliable global positioning system (GPS)-based vehicle use data are highly valuable for many transportation, analysis, and automotive considerations. Model-based design, real-world fuel economy analysis, and the growing field of autonomous and connected technologies (including predictive powertrain control and self-driving cars) all have a vested interest in high-fidelity estimation of powertrain loads and vehicle usage profiles. Unfortunately, road grade can be a difficult property to extract from GPS data with consistency. In this report, we present a methodology for appending high-resolution elevation data to GPS speed traces via a static digital elevation model. Anomalous data points in the digital elevation model are addressed during a filtration/smoothing routine, resulting in an elevation profile that can be used to calculate road grade. This process is evaluated against a large, commercially available height/slope dataset from the Navteq/Nokia/HERE Advanced Driver Assistance Systems product. Results will show good agreement with the Advanced Driver Assistance Systems data in the ability to estimate road grade between any two consecutive points in the contiguous United States.

  6. High dose Xe ion irradiation of yttria stabilized zirconia : influence of sputtering on implanted ion profile and retained damage /.

    SciTech Connect (OSTI)

    Afanasyev, I. V.; Sickafus, K.

    2001-01-01

    Fully-stabilized zirconia is known as a radiation resistant material. The objective of many experinients on zirconia has been to test the susceptibility of this material to amorphization. Because zirconia exhibits high radiation tolerance, this has made very high fluence ion irradiation experiments a necessity and so, additional iiradiation-inducetl effects such as surface sputtering become important. In this paper, we present results from 340 keV Xe' irradiations of yttria-stabilized zirconia (YSZ) to fluences ranging froiri 1.10' to 1.5.1OZ1 ions/m2. No iunorphization of YSZ was observed after irradiation to even the highest ion fluences. To assess sputtering effects at high fluence, an analytical model was developed, using ion range and damage distribulions calculated using Monte Carlo simulations for ion-solid interactions. Analysis results and experimental data revealed that at high fluences, the implanted ion and damago distribution profiles are significantly modified by sputtering.

  7. High Dose Neutron Irradiation of Hi-Nicalon Type S Silicon Carbide Composites, Part 2. Mechanical and Physical Properties

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Katoh, Yutai; Nozawa, Takashi; Shih, Chunghao Phillip; Ozawa, Kazumi; Koyanagi, Takaaki; Porter, Wallace D; Snead, Lance Lewis

    2015-01-07

    Nuclear-grade silicon carbide (SiC) composite material was examined for mechanical and thermophysical properties following high-dose neutron irradiation in the High Flux Isotope Reactor at a temperature range of 573–1073 K. Likewise, the material was chemical vapor-infiltrated SiC-matrix composite with a two-dimensional satin weave Hi-Nicalon Type S SiC fiber reinforcement and a multilayered pyrocarbon/SiC interphase. Moderate (1073 K) to very severe (573 K) degradation in mechanical properties was found after irradiation to >70 dpa, whereas no evidence was found for progressive evolution in swelling and thermal conductivity. The swelling was found to recover upon annealing beyond the irradiation temperature, indicating themore » irradiation temperature, but only to a limited extent. Moreover, the observed strength degradation is attributed primarily to fiber damage for all irradiation temperatures, particularly a combination of severe fiber degradation and likely interphase damage at relatively low irradiation temperatures.« less

  8. Detailed Hydrographic Feature Extraction from High-Resolution LiDAR Data

    SciTech Connect (OSTI)

    Danny L. Anderson

    2012-05-01

    Detailed hydrographic feature extraction from high-resolution light detection and ranging (LiDAR) data is investigated. Methods for quantitatively evaluating and comparing such extractions are presented, including the use of sinuosity and longitudinal root-mean-square-error (LRMSE). These metrics are then used to quantitatively compare stream networks in two studies. The first study examines the effect of raster cell size on watershed boundaries and stream networks delineated from LiDAR-derived digital elevation models (DEMs). The study confirmed that, with the greatly increased resolution of LiDAR data, smaller cell sizes generally yielded better stream network delineations, based on sinuosity and LRMSE. The second study demonstrates a new method of delineating a stream directly from LiDAR point clouds, without the intermediate step of deriving a DEM. Direct use of LiDAR point clouds could improve efficiency and accuracy of hydrographic feature extractions. The direct delineation method developed herein and termed “mDn”, is an extension of the D8 method that has been used for several decades with gridded raster data. The method divides the region around a starting point into sectors, using the LiDAR data points within each sector to determine an average slope, and selecting the sector with the greatest downward slope to determine the direction of flow. An mDn delineation was compared with a traditional grid-based delineation, using TauDEM, and other readily available, common stream data sets. Although, the TauDEM delineation yielded a sinuosity that more closely matches the reference, the mDn delineation yielded a sinuosity that was higher than either the TauDEM method or the existing published stream delineations. Furthermore, stream delineation using the mDn method yielded the smallest LRMSE.

  9. MAINTAINING HIGH RESOLUTION MASS SPECTROMETRY CAPABILITIES FOR NATIONAL NUCLEAR SECURITY ADMINISTRATION APPLICATIONS

    SciTech Connect (OSTI)

    Wyrick, S.; Cordaro, J.; Reeves, G.; Mcintosh, J.; Mauldin, C.; Tietze, K.; Varble, D.

    2011-06-06

    The Department of Energy (DOE) National Nuclear Security Administration (NNSA) has a specialized need for analyzing low mass gas species at very high resolutions. The currently preferred analytical method is electromagnetic sector mass spectrometry. This method allows the NNSA Nuclear Security Enterprise (NSE) to resolve species of similar masses down to acceptable minimum detection limits (MDLs). Some examples of these similar masses are helium-4/deuterium and carbon monoxide/nitrogen. Through the 1980s and 1990s, there were two vendors who supplied and supported these instruments. However, with declining procurements and down turns in the economy, the supply of instruments, service and spare parts from these vendors has become less available, and in some cases, nonexistent. The largest NSE user of this capability is the Savannah River Site (SRS), located near Aiken, South Carolina. The Research and Development Engineering (R&DE) Group in the Savannah River National Laboratory (SRNL) investigated the areas of instrument support that were needed to extend the life cycle of these aging instruments. Their conclusions, as to the focus areas of electromagnetic sector mass spectrometers to address, in order of priority, were electronics, software and hardware. Over the past 3-5 years, the R&DE Group has designed state of the art electronics and software that will allow high resolution legacy mass spectrometers, critical to the NNSA mission, to be operated for the foreseeable future. The funding support for this effort has been from several sources, including the SRS Defense Programs, NNSA Readiness Campaign, Pantex Plant and Sandia National Laboratory. To date, electronics systems have been upgraded on one development system at SRNL, two production systems at Pantex and one production system at Sandia National Laboratory. An NSE working group meets periodically to review strategies going forward. The R&DE Group has also applied their work to the electronics for a Thermal Ionization Mass Spectrometer (TIMS) instrument, which applies a similar mass spectrometric technology for resolving high mass isotopes, such as plutonium and uranium. Due to non-compete clauses for DOE, all work has been performed and applied to instruments which are obsolete and are no longer supported by the original vendor.

  10. Radiation tolerance survey of selected silicon photomultipliers to high energy neutron irradiation

    SciTech Connect (OSTI)

    Barbosa, Fernando J.; McKisson, John E.; Qiang, Yi; Steinberger, William; Xi, Wenze; Zorn, Carl J.

    2012-11-01

    A key feature of silicon photomultipliers (SiPMs) that can hinder their wider use in medium and high energy physics applications is their relatively high sensitivity to high energy background radiation, with particular regard to high energy neutrons. Dosages of 1010 neq/cm2 can damage them severely. In this study, some standard versions along with some new formulations are irradiated with a high intensity 241AmBe source up to a total dose of 5 109 neq/cm2. Key parameters monitored include dark noise, photon detection efficiency (PDE), gain, and voltage breakdown. Only dark noise was found to change significantly for this range of dosage. Analysis of the data indicates that within each vendor's product line, the change in dark noise is very similar as a function of increasing dose. At present, the best strategy for alleviating the effects of radiation damage is to cool the devices to minimize the effects of increased dark noise with accumulated dose.

  11. Back-scattering channel-cut high-resolution monochromator for inelastic x-ray scattering

    SciTech Connect (OSTI)

    Kushnir, V.I.; Abbamonte, P.M.; Macrander, A.T.; Schwoerer-Boehning, M.

    1997-08-01

    We report on a design and on some experimental results for the performance of a new high energy resolution monochromator. It is a large channel-cut Si crystal with a 197 mm separation between the two faces designed to operate in a near-backscattering regime. The device was tested as a second monochromator on Sector 3 of the Synchrotron Radiation Instrumentation Collaborative Access Team (SRI-CAT) at the Advanced Photon Source using the Si(777) reflection at a photon energy of 13.84 keV. The same monochromator can be used for other energies with reflections of the type (hhh). Special care has been taken to equalize the temperature of the two faces by employing a Peltier heat pump. A Si(111) double-crystal pre-monochromator designed to withstand the high heat load of the undulator radiation was used upstream on the beamline. The measured throughput efficiency of the Si(777) channel-cut monochromator was less ideal by a factor of 1.9. Dynamical diffraction theory was used to calculate the throughput of an ideally perfect crystal.

  12. Experimental Investigation and High Resolution Simulation of In-Situ Combustion Processes

    SciTech Connect (OSTI)

    Margot Gerritsen; Tony Kovscek

    2008-04-30

    This final technical report describes work performed for the project 'Experimental Investigation and High Resolution Numerical Simulator of In-Situ Combustion Processes', DE-FC26-03NT15405. In summary, this work improved our understanding of in-situ combustion (ISC) process physics and oil recovery. This understanding was translated into improved conceptual models and a suite of software algorithms that extended predictive capabilities. We pursued experimental, theoretical, and numerical tasks during the performance period. The specific project objectives were (i) identification, experimentally, of chemical additives/injectants that improve combustion performance and delineation of the physics of improved performance, (ii) establishment of a benchmark one-dimensional, experimental data set for verification of in-situ combustion dynamics computed by simulators, (iii) develop improved numerical methods that can be used to describe in-situ combustion more accurately, and (iv) to lay the underpinnings of a highly efficient, 3D, in-situ combustion simulator using adaptive mesh refinement techniques and parallelization. We believe that project goals were met and exceeded as discussed.

  13. Estimating global and North American methane emissions with high spatial resolution using GOSAT satellite data

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Turner, A. J.; Jacob, D. J.; Wecht, K. J.; Maasakkers, J. D.; Lundgren, E.; Andrews, A. E.; Biraud, S. C.; Boesch, H.; Bowman, K. W.; Deutscher, N. M.; et al

    2015-06-30

    We use 2009–2011 space-borne methane observations from the Greenhouse Gases Observing SATellite (GOSAT) to estimate global and North American methane emissions with 4° × 5° and up to 50 km × 50 km spatial resolution, respectively. GEOS-Chem and GOSAT data are first evaluated with atmospheric methane observations from surface and tower networks (NOAA/ESRL, TCCON) and aircraft (NOAA/ESRL, HIPPO), using the GEOS-Chem chemical transport model as a platform to facilitate comparison of GOSAT with in situ data. This identifies a high-latitude bias between the GOSAT data and GEOS-Chem that we correct via quadratic regression. Our global adjoint-based inversion yields a totalmore » methane source of 539 Tg a−1 with some important regional corrections to the EDGARv4.2 inventory used as a prior. Results serve as dynamic boundary conditions for an analytical inversion of North American methane emissions using radial basis functions to achieve high resolution of large sources and provide error characterization. We infer a US anthropogenic methane source of 40.2–42.7 Tg a−1, as compared to 24.9–27.0 Tg a−1 in the EDGAR and EPA bottom-up inventories, and 30.0–44.5 Tg a−1 in recent inverse studies. Our estimate is supported by independent surface and aircraft data and by previous inverse studies for California. We find that the emissions are highest in the southern–central US, the Central Valley of California, and Florida wetlands; large isolated point sources such as the US Four Corners also contribute. Using prior information on source locations, we attribute 29–44 % of US anthropogenic methane emissions to livestock, 22–31 % to oil/gas, 20 % to landfills/wastewater, and 11–15 % to coal. Wetlands contribute an additional 9.0–10.1 Tg a−1.« less

  14. Estimating global and North American methane emissions with high spatial resolution using GOSAT satellite data

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Turner, A. J.; Jacob, D. J.; Wecht, K. J.; Maasakkers, J. D.; Biraud, S. C.; Boesch, H.; Bowman, K. W.; Deutscher, N. M.; Dubey, M. K.; Griffith, D. W. T.; et al

    2015-02-18

    We use 2009–2011 space-borne methane observations from the Greenhouse Gases Observing SATellite (GOSAT) to constrain global and North American inversions of methane emissions with 4° × 5° and up to 50 km × 50 km spatial resolution, respectively. The GOSAT data are first evaluated with atmospheric methane observations from surface networks (NOAA, TCCON) and aircraft (NOAA/DOE, HIPPO), using the GEOS-Chem chemical transport model as a platform to facilitate comparison of GOSAT with in situ data. This identifies a high-latitude bias between the GOSAT data and GEOS-Chem that we correct via quadratic regression. The surface and aircraft data are subsequently usedmore » for independent evaluation of the methane source inversions. Our global adjoint-based inversion yields a total methane source of 539 Tg a−1 and points to a large East Asian overestimate in the EDGARv4.2 inventory used as a prior. Results serve as dynamic boundary conditions for an analytical inversion of North American methane emissions using radial basis functions to achieve high resolution of large sources and provide full error characterization. We infer a US anthropogenic methane source of 40.2–42.7 Tg a−1, as compared to 24.9–27.0 Tg a−1 in the EDGAR and EPA bottom-up inventories, and 30.0–44.5 Tg a−1 in recent inverse studies. Our estimate is supported by independent surface and aircraft data and by previous inverse studies for California. We find that the emissions are highest in the South-Central US, the Central Valley of California, and Florida wetlands, large isolated point sources such as the US Four Corners also contribute. We attribute 29–44% of US anthropogenic methane emissions to livestock, 22–31% to oil/gas, 20% to landfills/waste water, and 11–15% to coal with an additional 9.0–10.1 Tg a−1 source from wetlands.« less

  15. Novel Large Area High Resolution Neutron Detector for the Spallation Neutron Source

    SciTech Connect (OSTI)

    Lacy, Jeffrey L

    2009-05-22

    Neutron scattering is a powerful technique that is critically important for materials science and structural biology applications. The knowledge gained from past developments has resulted in far-reaching advances in engineering, pharmaceutical and biotechnology industries, to name a few. New facilities for neutron generation at much higher flux, such as the SNS at Oak Ridge, TN, will greatly enhance the capabilities of neutron scattering, with benefits that extend to many fields and include, for example, development of improved drug therapies and materials that are stronger, longer-lasting, and more impact-resistant. In order to fully realize this enhanced potential, however, higher neutron rates must be met with improved detection capabilities, particularly higher count rate capability in large size detectors, while maintaining practicality. We have developed a neutron detector with the technical and economic advantages to accomplish this goal. This new detector has a large sensitive area, offers 3D spatial resolution, high sensitivity and high count rate capability, and it is economical and practical to produce. The proposed detector technology is based on B-10 thin film conversion of neutrons in long straw-like gas detectors. A stack of many such detectors, each 1 meter in length, and 4 mm in diameter, has a stopping power that exceeds that of He-3 gas, contained at practical pressures within an area detector. With simple electronic readout methods, straw detector arrays can provide spatial resolution of 4 mm FWHM or better, and since an array detector of such form consists of several thousand individual elements per square meter, count rates in a 1 m^2 detector can reach 2?10^7 cps. Moreover, each individual event can be timetagged with a time resolution of less than 0.1 ?sec, allowing accurate identification of neutron energy by time of flight. Considering basic elemental cost, this novel neutron imaging detector can be commercially produced economically, probably at a small fraction of the cost of He-3 detectors. In addition to neutron scattering science, the fully developed base technology can be used as a rugged, low-cost neutron detector in area monitoring and surveying. Radiation monitors are used in a number of other settings for occupational and environmental radiation safety. Such a detector can also be used in environmental monitoring and remote nuclear power plant monitoring. For example, the Department of Energy could use it to characterize nuclear waste dumps, coordinate clean-up efforts, and assess the radioactive contaminants in the air and water. Radiation monitors can be used to monitor the age and component breakdown of nuclear warheads and to distinguish between weapons and reactor grade plutonium. The UN's International Atomic Energy Agency (IAEA) uses radiation monitors for treaty verification, remote monitoring, and enforcing the non-proliferation of nuclear weapons. As part of treaty verification, monitors can be used to certify the contents of containers during inspections. They could be used for portal monitoring to secure border checkpoints, sea ports, air cargo centers, public parks, sporting venues, and key government buildings. Currently, only 2% of all sea cargo shipped is inspected for radiation sources. In addition, merely the presence of radiation is detected and nothing is known about the radioactive source until further testing. The utilization of radiation monitors with neutron sensitivity and capability of operation in hostile port environments would increase the capacity and effectiveness of the radioactive scanning processes.

  16. Changes in Moisture Flux over the Tibetan Plateau during 1979-2011: Insights from a High Resolution Simulation

    SciTech Connect (OSTI)

    Gao, Yanhong; Leung, Lai-Yung R.; Zhang, Yongxin; Cuo, Lan

    2015-05-15

    Net precipitation (precipitation minus evapotranspiration, P-E) changes between 1979 and 2011 from a high resolution regional climate simulation and its reanalysis forcing are analyzed over the Tibet Plateau (TP) and compared to the global land data assimilation system (GLDAS) product. The high resolution simulation better resolves precipitation changes than its coarse resolution forcing, which contributes dominantly to the improved P-E change in the regional simulation compared to the global reanalysis. Hence, the former may provide better insights about the drivers of P-E changes. The mechanism behind the P-E changes is explored by decomposing the column integrated moisture flux convergence into thermodynamic, dynamic, and transient eddy components. High-resolution climate simulation improves the spatial pattern of P-E changes over the best available global reanalysis. High-resolution climate simulation also facilitates new and substantial findings regarding the role of thermodynamics and transient eddies in P-E changes reflected in observed changes in major river basins fed by runoff from the TP. The analysis revealed the contrasting convergence/divergence changes between the northwestern and southeastern TP and feedback through latent heat release as an important mechanism leading to the mean P-E changes in the TP.

  17. Hubble space telescope high-resolution imaging of Kepler small and cool exoplanet host stars

    SciTech Connect (OSTI)

    Gilliland, Ronald L.; Cartier, Kimberly M. S.; Wright, Jason T.; Adams, Elisabeth R.; Ciardi, David R.

    2015-01-01

    High-resolution imaging is an important tool for follow-up study of exoplanet candidates found via transit detection with the Kepler mission. We discuss here Hubble Space Telescope imaging with the WFC3 of 23 stars that host particularly interesting Kepler planet candidates based on their small size and cool equilibrium temperature estimates. Results include detections, exclusion of background stars that could be a source of false positives for the transits, and detection of physically associated companions in a number of cases providing dilution measures necessary for planet parameter refinement. For six Kepler objects of interest, we find that there is ambiguity regarding which star hosts the transiting planet(s), with potentially strong implications for planetary characteristics. Our sample is evenly distributed in G, K, and M spectral types. Albeit with a small sample size, we find that physically associated binaries are more common than expected at each spectral type, reaching a factor of 10 frequency excess in M. We document the program detection sensitivities, detections, and deliverables to the Kepler follow-up program archive.

  18. Upgrades of the high resolution imaging x-ray crystal spectrometers on experimental advanced superconducting tokamak

    SciTech Connect (OSTI)

    Lu, B.; Wang, F.; Fu, J.; Li, Y.; Wan, B.; Shi, Y.; Bitter, M.; Hill, K. W.; Lee, S. G.

    2012-10-15

    Two imaging x-ray crystal spectrometers, the so-called 'poloidal' and 'tangential' spectrometers, were recently implemented on experimental advanced superconducting tokamak (EAST) to provide spatially and temporally resolved impurity ion temperature (T{sub i}), electron temperature (T{sub e}) and rotation velocity profiles. They are derived from Doppler width of W line for Ti, the intensity ratio of Li-like satellites to W line for Te, and Doppler shift of W line for rotation. Each spectrometer originally consisted of a spherically curved crystal and a two-dimensional multi-wire proportional counter (MWPC) detector. Both spectrometers have now been upgraded. The layout of the tangential spectrometer was modified, since it had to be moved to a different port, and the spectrometer was equipped with two high count rate Pilatus detectors (Model 100 K) to overcome the count rate limitation of the MWPC and to improve its time resolution. The poloidal spectrometer was equipped with two spherically bent crystals to record the spectra of He-like and H-like argon simultaneously and side by side on the original MWPC. These upgrades are described, and new results from the latest EAST experimental campaign are presented.

  19. High-resolution thermal expansion measurements under helium-gas pressure

    SciTech Connect (OSTI)

    Manna, Rudra Sekhar; Wolf, Bernd; Souza, Mariano de; Lang, Michael

    2012-08-15

    We report on the realization of a capacitive dilatometer, designed for high-resolution measurements of length changes of a material for temperatures 1.4 K Less-Than-Or-Slanted-Equal-To T Less-Than-Or-Slanted-Equal-To 300 K and hydrostatic pressure P Less-Than-Or-Slanted-Equal-To 250 MPa. Helium ({sup 4}He) is used as a pressure-transmitting medium, ensuring hydrostatic-pressure conditions. Special emphasis has been given to guarantee, to a good approximation, constant-pressure conditions during temperature sweeps. The performance of the dilatometer is demonstrated by measurements of the coefficient of thermal expansion at pressures P Asymptotically-Equal-To 0.1 MPa (ambient pressure) and 104 MPa on a single crystal of azurite, Cu{sub 3}(CO{sub 3}){sub 2}(OH){sub 2}, a quasi-one-dimensional spin S = 1/2 Heisenberg antiferromagnet. The results indicate a strong effect of pressure on the magnetic interactions in this system.

  20. High resolution capillary column development for selective separations in gas chromatography

    SciTech Connect (OSTI)

    Przybyciel, M.

    1985-01-01

    A review of techniques for the preparation of high resolution capillary columns for gas chromatography is presented. Surface roughing, surface deactivation, stationary phase coating, and stationary phase crosslinking are discussed. Criteria for the selection of GC stationary phases and procedures for column evaluation are presented. A method is proposed for the isolation and determination of crude oil contamination in tropical plants and sediments. The method uses Florisil (TM) chromatography for the simultaneous clean-up and fractionation of aliphatic and aromatic hydrocarbons. Crosslinked SE-54 fused silica capillary columns prepared in our laboratory were employed for all GC separations. Mass spectrometry was used to help locate and identify specific oil components despite the intense background of the chromatogram. Crude oil components were identified in extracts of mangrove plant samples collected from the Peck Slip oil spill site at Media Munda, Puerto Rico. Crude oil components were also identified in sediment samples from controlled oil spill of Prudhoe Bay oil at Laguna de Chiriqui, Panama.

  1. A 5.5-Mb high-resolution integrated map of distal 11q13

    SciTech Connect (OSTI)

    Merscher, S.; Bekri, S.; De Leeuw, B.

    1997-02-01

    The distal part of 11q13, which contains several genes relevant to human diseases, has been poorly mapped as part of genome-wide mapping efforts. In the prospect of drawing a fine-scale integrated map of the area containing KRN1 and OMP, we have established a framework of markers by hybridization to DNA of somatic cell hybrids and by fluorescence in situ hybridization (FISH) on metaphase chromosomes. The probes studied were used to isolate 27 YACs and 16 cosmids that could be organized in three contigs covering approximately 6 Mb. These contigs were separated by two gaps that are likely to contain sequences underrepresented in YAC libraries. They were then integrated based on long-range restriction mapping and DNA-fiber FISH into a high-resolution physical map, which covers a 5.5-Mb region and includes 36 anonymous markers and 10 genes. This map will be used to search for genes within the 2/3 of this region where none have been localized as yet. It will also lay the ground for the characterization of an amplicon surrounding GARP in breast cancer and for the search of disease genes within this region. 42 refs., 2 figs., 2 tabs.

  2. Magnetic lens apparatus for use in high-resolution scanning electron microscopes and lithographic processes

    DOE Patents [OSTI]

    Crewe, Albert V. (Dune Acres, IN)

    2000-01-01

    Disclosed are lens apparatus in which a beam of charged particlesis brought to a focus by means of a magnetic field, the lens being situated behind the target position. In illustrative embodiments, a lens apparatus is employed in a scanning electron microscopeas the sole lens for high-resolution focusing of an electron beam, and in particular, an electron beam having an accelerating voltage of from about 10 to about 30,000 V. In one embodiment, the lens apparatus comprises an electrically-conducting coil arranged around the axis of the beam and a magnetic pole piece extending along the axis of the beam at least within the space surrounded by the coil. In other embodiments, the lens apparatus comprises a magnetic dipole or virtual magnetic monopole fabricated from a variety of materials, including permanent magnets, superconducting coils, and magnetizable spheres and needles contained within an energy-conducting coil. Multiple-array lens apparatus are also disclosed for simultaneous and/or consecutive imaging of multiple images on single or multiple specimens. The invention further provides apparatus, methods, and devices useful in focusing charged particle beams for lithographic processes.

  3. High-Resolution Modeling to Assess Tropical Cyclone Activity in Future Climate Regimes

    SciTech Connect (OSTI)

    Lackmann, Gary

    2013-06-10

    Applied research is proposed with the following objectives: (i) to determine the most likely level of tropical cyclone intensity and frequency in future climate regimes, (ii) to provide a quantitative measure of uncertainty in these predictions, and (iii) to improve understanding of the linkage between tropical cyclones and the planetary-scale circulation. Current mesoscale weather forecasting models, such as the Weather Research and Forecasting (WRF) model, are capable of simulating the full intensity of tropical cyclones (TC) with realistic structures. However, in order to accurately represent both the primary and secondary circulations in these systems, model simulations must be configured with sufficient resolution to explicitly represent convection (omitting the convective parameterization scheme). Most previous numerical studies of TC activity at seasonal and longer time scales have not utilized such explicit convection (EC) model runs. Here, we propose to employ the moving nest capability of WRF to optimally represent TC activity on a seasonal scale using a downscaling approach. The statistical results of a suite of these high-resolution TC simulations will yield a realistic representation of TC intensity on a seasonal basis, while at the same time allowing analysis of the feedback that TCs exert on the larger-scale climate system. Experiments will be driven with analyzed lateral boundary conditions for several recent Atlantic seasons, spanning a range of activity levels and TC track patterns. Results of the ensemble of WRF simulations will then be compared to analyzed TC data in order to determine the extent to which this modeling setup can reproduce recent levels of TC activity. Next, the boundary conditions (sea-surface temperature, tropopause height, and thermal/moisture profiles) from the recent seasons will be altered in a manner consistent with various future GCM/RCM scenarios, but that preserves the large-scale shear and incipient disturbance activity. This will allow (i) a direct comparison of future TC activity that could be expected for an active or inactive season in an altered climate regime, and (ii) a measure of the level of uncertainty and variability in TC activity resulting from different carbon emission scenarios.

  4. THE HIGH-RESOLUTION EXTREME-ULTRAVIOLET SPECTRUM OF N{sub 2} BY ELECTRON IMPACT

    SciTech Connect (OSTI)

    Heays, A. N.; Ajello, J. M.; Aguilar, A.; Lewis, B. R.; Gibson, S. T.

    2014-04-01

    We have analyzed high-resolution (FWHM = 0.2 ) extreme-ultraviolet (EUV, 800-1350 ) laboratory emission spectra of molecular nitrogen excited by an electron impact at 20 and 100 eV under (mostly) optically thin, single-scattering experimental conditions. A total of 491 emission features were observed from N{sub 2} electronic-vibrational transitions and atomic N I and N II multiplets and their emission cross sections were measured. Molecular emission was observed at vibrationally excited ground-state levels as high as v'' = 17, from the a {sup 1}? {sub g} , b {sup 1}? {sub u} , and b'{sup 1}? {sub u} {sup +} excited valence states and the Rydberg series c'{sub n} {sub +1} {sup 1}? {sub u} {sup +}, c{sub n} {sup 1}? {sub u} , and o{sub n} {sup 1}? {sub u} for n between 3 and 9. The frequently blended molecular emission bands were disentangled with the aid of a sophisticated and predictive quantum-mechanical model of excited states that includes the strong coupling between valence and Rydberg electronic states and the effects of predissociation. Improved model parameters describing electronic transition moments were obtained from the experiment and allowed for a reliable prediction of the vibrationally summed electronic emission cross section, including an extrapolation to unobserved emission bands and those that are optically thick in the experimental spectra. Vibrationally dependent electronic excitation functions were inferred from a comparison of emission features following 20 and 100 eV electron-impact collisional excitation. The electron-impact-induced fluorescence measurements are compared with Cassini Ultraviolet Imaging Spectrograph observations of emissions from Titan's upper atmosphere.

  5. Merging high resolution geophysical and geochemical surveys to reduce exploration risk at glass buttes, Oregon

    SciTech Connect (OSTI)

    Walsh, Patrick; Fercho, Steven; Perkin, Doug; Martini, Brigette; Boshmann, Darrick

    2015-06-01

    The engineering and studies phase of the Glass Buttes project was aimed at reducing risk during the early stages of geothermal project development. The project’s inclusion of high resolution geophysical and geochemical surveys allowed Ormat to evaluate the value of these surveys both independently and in combination to quantify the most valuable course of action for exploration in an area where structure, permeability, and temperature are the most pressing questions. The sizes of the thermal anomalies at Glass Buttes are unusually large. Over the course of Phase I Ormat acquired high resolution LIDAR data to accurately map fault manifestations at the surface and collected detailed gravity and aeromagnetic surveys to map subsurface structural features. In addition, Ormat collected airborne hyperspectral data to assist with mapping the rock petrology and mineral alteration assemblages along Glass Buttes faults and magnetotelluric (MT) survey to try to better constrain the structures at depth. Direct and indirect identification of alteration assemblages reveal not only the geochemical character and temperature of the causative hydrothermal fluids but can also constrain areas of upflow along specific fault segments. All five datasets were merged along with subsurface lithologies and temperatures to predict the most likely locations for high permeability and hot fluids. The Glass Buttes temperature anomalies include 2 areas, totaling 60 km2 (23 mi2) of measured temperature gradients over 165° C/km (10° F/100ft). The Midnight Point temperature anomaly includes the Strat-1 well with 90°C (194 °F) at 603 m (1981 ft) with a 164 °C/km (10°F/100ft) temperature gradient at bottom hole and the GB-18 well with 71°C (160 °F) at 396 m (1300 ft) with a 182°C/km (11°F/100ft) gradient. The primary area of alteration and elevated temperature occurs near major fault intersections associated with Brothers Fault Zone and Basin and Range systems. Evidence for faulting is observed in each data set as follows. Field observations include fault plane orientations, complicated fault intersections, and hydrothermal alteration apparently pre-dating basalt flows. Geophysical anomalies include large, linear gradients in gravity and aeromagnetic data with magnetic lows possibly associated with alteration. Resistivity low anomalies also appear to have offsets associated with faulting. Hyperspectral and XRF identified alteration and individual volcanic flow units, respectively. When incorporated into a 3D geologic model, the fault intersections near the highest proven temperature and geophysical anomalies provide the first priority targets at Midnight Point. Ormat geologists selected the Midnight Point 52-33 drilling target based on a combination of pre-existing drilling data, geologic field work, geophysical interpretation, and geochemical analysis. Deep temperatures of well 52-33 was lower than anticipated. Temperature gradients in the well mirrored those found in historical drilling, but they decreased below 1500 ft and were isothermal below 2000 ft.

  6. Response of nanostructured ferritic alloys to high-dose heavy ion irradiation

    SciTech Connect (OSTI)

    Parish, Chad M.; White, Ryan M.; LeBeau, James M.; Miller, Michael K.

    2014-02-01

    A latest-generation aberration-corrected scanning/transmission electron microscope (STEM) is used to study heavy-ion-irradiated nanostructured ferritic alloys (NFAs). Results are presented for STEM X-ray mapping of NFA 14YWT irradiated with 10 MeV Pt to 16 or 160 dpa at -100°C and 750°C, as well as pre-irradiation reference material. Irradiation at -100°C results in ballistic destruction of the beneficial microstructural features present in the pre-irradiated reference material, such as Ti-Y-O nanoclusters (NCs) and grain boundary (GB) segregation. Irradiation at 750°C retains these beneficial features, but indicates some coarsening of the NCs, diffusion of Al to the NCs, and a reduction of the Cr-W GB segregation (or solute excess) content. Ion irradiation combined with the latest-generation STEM hardware allows for rapid screening of fusion candidate materials and improved understanding of irradiation-induced microstructural changes in NFAs.

  7. Calibration grooming and alignment for LDUA High Resolution Stereoscopic Video Camera System (HRSVS)

    SciTech Connect (OSTI)

    Pardini, A.F.

    1998-01-27

    The High Resolution Stereoscopic Video Camera System (HRSVS) was designed by the Savannah River Technology Center (SRTC) to provide routine and troubleshooting views of tank interiors during characterization and remediation phases of underground storage tank (UST) processing. The HRSVS is a dual color camera system designed to provide stereo viewing of the interior of the tanks including the tank wall in a Class 1, Division 1, flammable atmosphere. The HRSVS was designed with a modular philosophy for easy maintenance and configuration modifications. During operation of the system with the LDUA, the control of the camera system will be performed by the LDUA supervisory data acquisition system (SDAS). Video and control status 1458 will be displayed on monitors within the LDUA control center. All control functions are accessible from the front panel of the control box located within the Operations Control Trailer (OCT). The LDUA will provide all positioning functions within the waste tank for the end effector. Various electronic measurement instruments will be used to perform CG and A activities. The instruments may include a digital volt meter, oscilloscope, signal generator, and other electronic repair equipment. None of these instruments will need to be calibrated beyond what comes from the manufacturer. During CG and A a temperature indicating device will be used to measure the temperature of the outside of the HRSVS from initial startup until the temperature has stabilized. This device will not need to be in calibration during CG and A but will have to have a current calibration sticker from the Standards Laboratory during any acceptance testing. This sensor will not need to be in calibration during CG and A but will have to have a current calibration sticker from the Standards Laboratory during any acceptance testing.

  8. Analysis of several high-resolution infrared bands of spiropentane, C5H8

    SciTech Connect (OSTI)

    Maki, Arthur G.; Price, Joseph E.; Harzan, J.; Nibler, Joseph W.; Weber, Alfons; Masiello, Tony; Blake, Thomas A.

    2015-06-01

    he high-resolution infrared absorption spectrum of spiropentane (C5H8) has been measured from 200 to 4000 cm 1, and a detailed analysis is presented for eight bands in the region from 700 to 2200 cm 1. Two fundamental perpendicular bands were analyzed, m22 and m24 near 1050 and 780 cm 1, respectively, along with two fundamental parallel bands, m14 and m16 near 1540 and 990 cm1, respectively. Two other fundamentals, m17 and m23, are seen as intense overlapping bands near 880 cm*1 and are Coriolis-coupled, producing a complex mixture in which only P-branch transitions could be tentatively assigned for m17. In addition, three binary combination bands were fit at about 1570, 2082, and 2098 cm*1 which are assigned as either 2m24 or m5 + m16 in the first case, m4 + m22 in the second case, and 2m22 in the latter case. The two l-type resonance constants, q+ and q*, were determined for each of the two perpendicular fundamentals m22 and m24. Those two constants were also responsible for splittings observed in the K = 3 levels of m24. For the ground state the order of the split K = 2 B1/B2 levels has been reversed from that reported previously, based on the measurements and assignments for the m24 band. Rovibrational parameters deduced from the analyses are compared with those obtained from density functional Gaussian calculations at the anharmonic level.

  9. CHANDRA HIGH-RESOLUTION OBSERVATIONS OF CID-42, A CANDIDATE RECOILING SUPERMASSIVE BLACK HOLE

    SciTech Connect (OSTI)

    Civano, F.; Elvis, M.; Lanzuisi, G.; Aldcroft, T.; Trichas, M.; Fruscione, A.; Bongiorno, A.; Brusa, M.; Blecha, L.; Loeb, A.; Comastri, A.; Gilli, R.; Salvato, M.; Komossa, S.; Koekemoer, A.; Mainieri, V.; Piconcelli, E.; Vignali, C.

    2012-06-10

    We present Chandra High Resolution Camera observations of CID-42, a candidate recoiling supermassive black hole (SMBH) at z = 0.359 in the COSMOS survey. CID-42 shows two optical compact sources resolved in the HST/ACS image embedded in the same galaxy structure and a velocity offset of {approx}1300 km s{sup -1} between the H{beta} broad and narrow emission line, as presented by Civano et al. Two scenarios have been proposed to explain the properties of CID-42: a gravitational wave (GW) recoiling SMBH and a double Type 1/Type 2 active galactic nucleus (AGN) system, where one of the two is recoiling because of slingshot effect. In both scenarios, one of the optical nuclei hosts an unobscured AGN, while the other one, either an obscured AGN or a star-forming compact region. The X-ray Chandra data allow us to unambiguously resolve the X-ray emission and unveil the nature of the two optical sources in CID-42. We find that only one of the optical nuclei is responsible for the whole X-ray unobscured emission observed and a 3{sigma} upper limit on the flux of the second optical nucleus is measured. The upper limit on the X-ray luminosity plus the analysis of the multiwavelength spectral energy distribution indicate the presence of a star-forming region in the second source rather than an obscured SMBH, thus favoring the GW recoil scenario. However, the presence of a very obscured SMBH cannot be fully ruled out. A new X-ray feature, in a SW direction with respect to the main source, is discovered and discussed.

  10. Thermal, tensile and rheological properties of high density polyethylene (HDPE) processed and irradiated by gamma-ray in different atmospheres

    SciTech Connect (OSTI)

    Ferreto, H. F. R. E-mail: ana-feitoza@yahoo.com.br; Oliveira, A. C. F. E-mail: ana-feitoza@yahoo.com.br; Parra, D. F. E-mail: ablugao@ipen.br; Lugo, A. B. E-mail: ablugao@ipen.br; Gaia, R.

    2014-05-15

    The aim of this paper is to investigate structural changes of high density polyethylene (HDPE) modified by ionizing radiation (gamma rays) in different atmospheres. The gamma radiation process for modification of commercial polymers is a widely applied technique to promote new physical-chemical and mechanical properties. Gamma irradiation originates free radicals which can induce chain scission or recombination, providing its annihilation, branching or crosslinking. This polymer was irradiated with gamma source of {sup 60}Co at doses of 5, 10, 20, 50 or 100 kGy at a dose rate of 5 kGy/h. The changes in molecular structure of HDPE, after gamma irradiations were evaluated using thermogravimetric analysis (TGA) and tensile machine and oscillatory rheology. The results showed the variations of the properties depending on the dose at each atmosphere.

  11. Complete dipole response in {sup 208}Pb from high-resolution polarized proton scattering at 0 deg

    SciTech Connect (OSTI)

    Neumann-Cosel, P. von; Kalmykov, Y.; Poltoratska, I.; Ponomarev, V. Yu.; Richter, A.; Wambach, J.; Adachi, T.; Fujita, Y.; Matsubara, H.; Sakemi, Y.; Shimizu, Y.; Tameshige, Y.; Yosoi, M.; Bertulani, C. A.; Carter, J.; Fujita, H.; Dozono, M.; Fujita, K.; Hashimoto, H.; Hatanaka, K.

    2009-01-28

    The structure of electric and magnetic dipole modes in {sup 208}Pb is investigated in a high-resolution measurement of the (p-vector,p-vector') reaction under 0 deg. First results on the E1 strength in the region of the pygmy dipole resonance are reported.

  12. High-resolution mineralogical characterization and biogeochemical modeling of uranium reaction pathways at the FRC

    SciTech Connect (OSTI)

    Chen Zhu

    2006-06-15

    High-Resolution Mineralogical Characterization and Biogeochemical Modeling of Uranium Reduction Pathways at the Oak Ridge Field-Research Center (FRC) Chen Zhu, Indiana University, David R. Veblen, Johns Hopkins University We have successfully completed a proof-of-concept, one-year grant on a three-year proposal from the former NABIR program, and here we seek additional two-year funding to complete and publish the research. Using a state-of-the-art 300-kV, atomic resolution, Field Emission Gun Transmission Electron Microscope (TEM), we have successfully identified three categories of mineral hosts for uranium in contaminated soils: (1) iron oxides; (2) mixed manganese-iron oxides; and (3) uranium phosphates. Method development using parallel electron energy loss spectroscopy (EELS) associated with the TEM shows great promise for characterizing the valence states of immobilized U during bioremediation. We have also collected 27 groundwater samples from two push-pull field biostimulation tests, which form two time series from zero to approximately 600 hours. The temporal evolution in major cations, anions, trace elements, and the stable isotopes 34S, 18O in sulfate, 15N in nitrate, and 13C in dissolved inorganic carbon (DIC) clearly show that biostimulation resulted in reduction of nitrate, Mn(IV), Fe(III), U(VI), sulfate, and Tc(VII), and these reduction reactions were intimately coupled with a complex network of inorganic reactions evident from alkalinity, pH, Na, K, Mg, and Ca concentrations. From these temporal trends, apparent zero order rates were regressed. However, our extensive suite of chemical and isotopic data sets, perhaps the first and only comprehensive data set available at the FRC, show that the derived rates from these field biostimulation experiments are composite and lump-sum rates. There were several reactions that were occurring at the same time but were masked by these pseudo-zero order rates. A reaction-path model comprising a total of nine redox couples (NO3–/NH4+, MnO2(s)/Mn2+, Fe(OH)3(s) /Fe2+, TcO4–/TcO2(s), UO22+/UO2(s), SO42–/HS–, CO2/CH4, ethanol/acetate, and H+/H2.) is used to simulate the temporal biogeochemical evolution observed in the field tests. Preliminary results show that the models based on thermodynamics and more complex rate laws can generate the apparent zero order rates when several concurrent or competing reactions occur. Professor Alex Halliday of Oxford University, UK, and his postdoctoral associates are measuring the uranium isotopes in our groundwater samples. Newly developed state-of-the-art analytical techniques in measuring variability in 235U/238U offer the potential to distinguish biotic and abiotic uranium reductive mechanisms.

  13. Ionized gas kinematics at high resolution. IV. Star formation and a rotating core in the Medusa (NGC 4194)

    SciTech Connect (OSTI)

    Beck, Sara C.; Lacy, John; Turner, Jean; Greathouse, Thomas; Neff, Susan

    2014-05-20

    NGC 4194 is a post-merger starburst known as The Medusa for its striking tidal features. We present here a detailed study of the structure and kinematics of ionized gas in the central 0.65 kpc of the Medusa. The data include radio continuum maps with resolution up to 0.''18 (35 pc) and a 12.8 ?m [Ne II] data cube with spectral resolution ?4 km s{sup 1}: the first high-resolution, extinction-free observations of this remarkable object. The ionized gas has the kinematic signature of a core in solid-body rotation. The starburst has formed a complex of bright compact H II regions, probably excited by deeply embedded super star clusters, but none of these sources is a convincing candidate for a Galactic nucleus. The nuclei of the merger partners that created the Medusa have not yet been identified.

  14. Ultra high vacuum fracture and transfer device for AES analysis of irradiated austenitic stainless steel

    SciTech Connect (OSTI)

    Urie, M.W.; Panayotou, N.F.; Robinson, J.E.

    1980-01-01

    An ultrahigh vacuum fracture and transfer device for analysis of irradiated and non-irradiated SS 316 fuel cladding is described. Mechanical property tests used to study the behavior of cladding during reactor transient over-power conditions are reported. The stress vs temperature curves show minimal differences between unirradiated cladding and unfueled cladding. The fueled cladding fails at a lower temperature. All fueled specimens failed in an intergranular mode. (FS)

  15. SOUTHERN MASSIVE STARS AT HIGH ANGULAR RESOLUTION: OBSERVATIONAL CAMPAIGN AND COMPANION DETECTION

    SciTech Connect (OSTI)

    Sana, H.; Lacour, S.; Gauchet, L.; Pickel, D.; Berger, J.-P.; Norris, B.; Olofsson, J.; Absil, O.; De Koter, A.; Kratter, K.; Schnurr, O.; Zinnecker, H.

    2014-11-01

    Multiplicity is one of the most fundamental observable properties of massive O-type stars and offers a promising way to discriminate between massive star formation theories. Nevertheless, companions at separations between 1 and 100 milliarcsec (mas) remain mostly unknown due to intrinsic observational limitations. At a typical distance of 2 kpc, this corresponds to projected physical separations of 2-200 AU. The Southern MAssive Stars at High angular resolution survey (SMaSH+) was designed to fill this gap by providing the first systematic interferometric survey of Galactic massive stars. We observed 117 O-type stars with VLTI/PIONIER and 162 O-type stars with NACO/Sparse Aperture Masking (SAM), probing the separation ranges 1-45 and 30-250 mas and brightness contrasts of ΔH < 4 and ΔH < 5, respectively. Taking advantage of NACO's field of view, we further uniformly searched for visual companions in an 8'' radius down to ΔH = 8. This paper describes observations and data analysis, reports the discovery of almost 200 new companions in the separation range from 1 mas to 8'' and presents a catalog of detections, including the first resolved measurements of over a dozen known long-period spectroscopic binaries. Excluding known runaway stars for which no companions are detected, 96 objects in our main sample (δ < 0°; H < 7.5) were observed both with PIONIER and NACO/SAM. The fraction of these stars with at least one resolved companion within 200 mas is 0.53. Accounting for known but unresolved spectroscopic or eclipsing companions, the multiplicity fraction at separation ρ < 8'' increases to f {sub m} = 0.91 ± 0.03. The fraction of luminosity class V stars that have a bound companion reaches 100% at 30 mas while their average number of physically connected companions within 8'' is f {sub c} = 2.2 ± 0.3. This demonstrates that massive stars form nearly exclusively in multiple systems. The nine non-thermal radio emitters observed by SMaSH+ are all resolved, including the newly discovered pairs HD 168112 and CPD–47°2963. This lends strong support to the universality of the wind-wind collision scenario to explain the non-thermal emission from O-type stars.

  16. Characterizing Aerosol Distributions and Optical Properties Using the NASA Langley High Spectral Resolution Lidar

    SciTech Connect (OSTI)

    Hostetler, Chris; Ferrare, Richard

    2013-02-14

    The objective of this project was to provide vertically and horizontally resolved data on aerosol optical properties to assess and ultimately improve how models represent these aerosol properties and their impacts on atmospheric radiation. The approach was to deploy the NASA Langley Airborne High Spectral Resolution Lidar (HSRL) and other synergistic remote sensors on DOE Atmospheric Science Research (ASR) sponsored airborne field campaigns and synergistic field campaigns sponsored by other agencies to remotely measure aerosol backscattering, extinction, and optical thickness profiles. Synergistic sensors included a nadir-viewing digital camera for context imagery, and, later in the project, the NASA Goddard Institute for Space Studies (GISS) Research Scanning Polarimeter (RSP). The information from the remote sensing instruments was used to map the horizontal and vertical distribution of aerosol properties and type. The retrieved lidar parameters include profiles of aerosol extinction, backscatter, depolarization, and optical depth. Products produced in subsequent analyses included aerosol mixed layer height, aerosol type, and the partition of aerosol optical depth by type. The lidar products provided vertical context for in situ and remote sensing measurements from other airborne and ground-based platforms employed in the field campaigns and was used to assess the predictions of transport models. Also, the measurements provide a data base for future evaluation of techniques to combine active (lidar) and passive (polarimeter) measurements in advanced retrieval schemes to remotely characterize aerosol microphysical properties. The project was initiated as a 3-year project starting 1 January 2005. It was later awarded continuation funding for another 3 years (i.e., through 31 December 2010) followed by a 1-year no-cost extension (through 31 December 2011). This project supported logistical and flight costs of the NASA sensors on a dedicated aircraft, the subsequent analysis and archival of the data, and the presentation of results in conferences, workshops, and publications. DOE ASR field campaigns supported under this project included - MAX-Mex /MILAGRO (2006) - TexAQS 2006/GoMACCS (2006) - CHAPS (2007) - RACORO (2009) - CARE/CalNex (2010) In addition, data acquired on HSRL airborne field campaigns sponsored by other agencies were used extensively to fulfill the science objectives of this project and the data acquired have been made available to other DOE ASR investigators upon request.

  17. Identifying high energy density stream-reaches through refined geospatial resolution in hydropower resource assessment

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Pasha, M. Fayzul K.; Yang, Majntxov; Yeasmin, Dilruba; Saetern, Sen; Kao, Shih -Chieh; Smith, Brennan T.

    2016-01-07

    Benefited from the rapid development of multiple geospatial data sets on topography, hydrology, and existing energy-water infrastructures, the reconnaissance level hydropower resource assessment can now be conducted using geospatial models in all regions of the US. Furthermore, the updated techniques can be used to estimate the total undeveloped hydropower potential across all regions, and may eventually help identify further hydropower opportunities that were previously overlooked. To enhance the characterization of higher energy density stream-reaches, this paper explored the sensitivity of geospatial resolution on the identification of hydropower stream-reaches using the geospatial merit matrix based hydropower resource assessment (GMM-HRA) model. GMM-HRAmore » model simulation was conducted with eight different spatial resolutions on six U.S. Geological Survey (USGS) 8-digit hydrologic units (HUC8) located at three different terrains; Flat, Mild, and Steep. The results showed that more hydropower potential from higher energy density stream-reaches can be identified with increasing spatial resolution. Both Flat and Mild terrains exhibited lower impacts compared to the Steep terrain. Consequently, greater attention should be applied when selecting the discretization resolution for hydropower resource assessments in the future study.« less

  18. High-resolution x-ray spectrometer based on spherically bent crystals for investigations of femtosecond laser plasmas

    SciTech Connect (OSTI)

    Young, B.K.; Osterheld, A.L.; Price, D.F.; Shepherd, R.; Stewart, R.E.; Faenov, A.Y.; Magunov, A.I.; Pikuz, T.A.; Skobelev, I.Y.; Flora, F.; Bollanti, S.; Di Lazzaro, P.; Letardi, T.; Grilli, A.; Palladino, L.; Reale, A.; Scafati, A.; Reale, L.

    1998-12-01

    Ultrashort-pulse, laser-produced plasmas have become very interesting laboratory sources to study spectroscopically due to their very high densities and temperatures, and the high laser-induced electromagnetic fields present. Typically, these plasmas are of very small volume and very low emissivity. Thus, studying these near point source plasmas requires advanced experimental techniques. We present a new spectrometer design called the focusing spectrometer with spatial resolution (FSSR-2D) based on a spherically bent crystal which provides simultaneous high spectral ({lambda}/{Delta}{lambda}{approx}10{sup 4}) and spatial resolution ({approx}10thinsp{mu}m) as well as high luminosity (high collection efficiency). We described in detail the FSSR-2D case in which a small, near point source plasma is investigated. An estimate for the spectral and spatial resolution for the spectrometer is outlined based on geometric considerations. Using the FSSR-2D instrument, experimental data measured from both a 100 fs and a nanosecond pulse laser-produced plasma are presented. {copyright} {ital 1998 American Institute of Physics.}

  19. Focusing, in-chamber spectrometer triplet for high resolution measurements on the Sandia Z facility

    SciTech Connect (OSTI)

    Wenger, D. F.; Sinars, D. B.; Rochau, G. A.; Bailey, J. E.; Porter, J. L.; Faenov, A. Ya.; Pikuz, T. A.; Pikuz, S. A.

    2006-10-15

    An early prototype of a focusing spectrometer with one-dimensional (1D) spatial resolution (FSSR) instrument was previously developed for use in the vacuum chamber of the Sandia Z facility [Sinars et al., J. Quant. Spectrosc. Radiat. Transf. 99, 595 (2006)]. This instrument used a single, spherically bent crystal to measure time-integrated Ar spectra from 0.295-0.378 nm with {lambda}/{delta}{lambda}>2000 and a 1D axial spatial resolution of {approx}50 {mu}m. We present the design of a final version of this instrument that improves the shielding, can be aligned more accurately, and uses three crystals instead of one. The last change enables coverage of multiple spectral ranges if different crystals are used, or multiple times if identical crystals and time-gated detectors are used. We also present results from initial prototyping tests on the Z facility using two crystals in a time-integrated mode.

  20. High-resolution monochromatic x-ray imaging system based on spherically bent crystals

    SciTech Connect (OSTI)

    Aglitskiy, Y.; Lehecka, T.; Obenschain, S.; Bodner, S.; Pawley, C.; Gerber, K.; Sethian, J.; Brown, C.M.; Seely, J.; Feldman, U.; Holland, G.

    1998-08-01

    We have developed an improved x-ray imaging system based on spherically curve crystals. It is designed and used for diagnostics of targets ablatively accelerated by the Nike KrF laser. A spherically curved quartz crystal (2d=6.687 {Angstrom}, R=200 mm) has been used to produce monochromatic backlit images with the He-like Si resonance line (1865 eV) as the source of radiation. The spatial resolution of the x-ray optical system is 1.7 {mu}m in selected places and 2{endash}3 {mu}m over a larger area. Time-resolved backlit monochromatic images of polystyrene planar targets driven by the Nike facility have been obtained with a spatial resolution of 2.5 {mu}m in selected places and 5 {mu}m over the focal spot of the Nike laser. {copyright} 1998 Optical Society of America

  1. High resolution monochromatic X-ray imaging system based on spherically bent crystals

    SciTech Connect (OSTI)

    Aglitskiy, Y.; Lehecka, T.; Obenschain, S.; Bodner, S.; Pawley, C.; Gerber, K.; Sethian, J.; Brown, C. M.; Seely, J.; Feldman, U.; Holland, G.

    1997-05-05

    We have developed a new X-ray imaging system based on spherically curved crystals. It is designed and used for diagnostics of targets ablatively accelerated by the Nike KrF laser. The imaging system is used for plasma diagnostics of the main target and for characterization of potential backlighters. A spherically curved quartz crystal (2d=6.687 A, R=200 mm) is used to produce monochromatic backlit images with the He-like Si resonance line (1865 eV) as the source of radiation. The spatial resolution of the X-ray optical system is 3-4 {mu}m. Time resolved backlit monochromatic images of CH planar targets driven by the Nike facility have been obtained with 6-7 {mu}m spatial resolution.

  2. High resolution monochromatic X-ray imaging system based on spherically bent crystals

    SciTech Connect (OSTI)

    Aglitskiy, Y.; Lehecka, T.; Obenschain, S.; Bodner, S.; Pawley, C.; Gerber, K.; Sethian, J.; Brown, C.M.; Seely, J.; Feldman, U.; Holland, G.

    1997-05-01

    We have developed a new X-ray imaging system based on spherically curved crystals. It is designed and used for diagnostics of targets ablatively accelerated by the Nike KrF laser [1,2]. The imaging system is used for plasma diagnostics of the main target and for characterization of potential backlighters. A spherically curved quartz crystal (2d=6.687{Angstrom}, R=200mm) is used to produce monochromatic backlit images with the He-like Si resonance line (1865 eV) as the source of radiation. The spatial resolution of the X-ray optical system is 3{endash}4 {mu}m. Time resolved backlit monochromatic images of CH planar targets driven by the Nike facility have been obtained with 6{endash}7 {mu}m spatial resolution. {copyright} {ital 1997 American Institute of Physics.}

  3. Changes in Moisture Flux Over the Tibetan Plateau During 1979-2011: Insights from a High Resolution Simulation

    SciTech Connect (OSTI)

    Gao, Yanhong; Leung, Lai-Yung R.; Zhang, Yongxin; Cuo, Lan

    2015-05-01

    Net precipitation (precipitation minus evapotranspiration, P-E) changes from a high resolution regional climate simulation and its reanalysis forcing are analyzed over the Tibet Plateau (TP) and compared to the global land data assimilation system (GLDAS) product. The mechanism behind the P-E changes is explored by decomposing the column integrated moisture flux convergence into thermodynamic, dynamic, and transient eddy components. High-resolution climate simulation improves the spatial pattern of P-E changes over the best available global reanalysis. Improvement in simulating precipitation changes at high elevations contributes dominantly to the improved P-E changes. High-resolution climate simulation also facilitates new and substantial findings regarding the role of thermodynamics and transient eddies in P-E changes reflected in observed changes in major river basins fed by runoff from the TP. The analysis revealed the contrasting convergence/divergence changes between the northwestern and southeastern TP and feedback through latent heat release as an important mechanism leading to the mean P-E changes in the TP.

  4. Microstructural Characterization of Irradiated U-7Mo/Al-5Si Dispersion to High Fission Density

    SciTech Connect (OSTI)

    J. Gan; B. D. Miller; D. D. Keiser, Jr.; A. B. Robinson; J. W. Madden; P. G. Medvedev; D. M. Wachs

    2014-11-01

    The fuel development program for research and test reactors calls for improved knowledge on the effect of microstructure on fuel performance in reactors. This work summarizes the recent TEM microstructural characterization of an irradiated U-7Mo/Al-5Si dispersion fuel plate (R3R050) irradiated in the Advanced Test Reactor (ATR) at Idaho National Laboratory to 5.21021 fissions/cm3. While a large fraction of the fuel grains is decorated with large bubbles, there is no evidence showing interlinking of these large bubbles at the specified fission density. The attachment of solid fission product precipitates to the bubbles is likely the result of fission product diffusion into these bubbles. The process of fission gas bubble superlattice collapse appears through bubble coalescence. The results are compared with the previous TEM work of the dispersion fuels irradiated to lower fission density from the same fuel plate.

  5. Deployment of High Resolution Real-Time Distribution Level Metering on Maui: Preprint

    SciTech Connect (OSTI)

    Bank, J.

    2013-01-01

    In order to support the ongoing Maui Smart Grid demonstration project advanced metering has been deployed at the distribution transformer level in Maui Electric Company's Kihei Circuit on the Island of Maui. This equipment has been custom designed to provide accurately time-stamped Phasor and Power Quality data in real time. Additionally, irradiance sensors have been deployed at a few selected locations in proximity to photovoltaic (PV) installations. The received data is being used for validation of existing system models and for impact studies of future system hardware. Descriptions of the hardware and its installation, and some preliminary metering results are presented. Real-time circuit visualization applications for the data are also under development.

  6. Proposed Mission Concept for the Astrophysical Plasma-dynamic Explorer (APEX): An EUV High-Resolution Spectroscopic SMEX

    SciTech Connect (OSTI)

    Kowalski, M P

    2004-07-02

    EUVE and the ROSAT WFC have left a tremendous legacy in astrophysics at EUV wavelengths. More recently, Chandra and XMM-Newton have demonstrated at X-ray wavelengths the power of high-resolution astronomical spectroscopy, which allows the identification of weak emission lines, the measurement of Doppler shifts and line profiles, and the detection of narrow absorption features. This leads to a complete understanding of the density, temperature, abundance, magnetic, and dynamic structure of astrophysical plasmas. However, the termination of the EUVE mission has left a gaping hole in spectral coverage at crucial EUV wavelengths ({approx}100-300 Angstroms), where hot (10{sup 5}-10{sup 8} K) plasmas radiate most strongly and produce critical spectral diagnostics. CHIPS will fill this hole only partially as it is optimized for diffuse emission and has only moderate resolution (R{approx}150). For discrete sources, we have successfully flown a follow-on instrument to the EUVE spectrometer (A{sub eff} {approx}1 cm{sup 2}, R {approx}400), the high-resolution spectrometer J-PEX (A{sub eff} {approx}3 cm{sup 2}, R {approx}3000). Here we build on the J-PEX prototype and present a strawman design for an orbiting spectroscopic observatory, APEX, a SMEX-class instrument containing a suite of 8 spectrometers that together achieve both high effective area (A{sub eff}>20 cm{sup 2}) and high spectral resolution (R{approx}10,000) over the range 100-300 Angstroms. We also discuss alternate configurations for shorter and longer wavelengths.

  7. Virtually distortion-free imaging system for large field, high resolution lithography using electrons, ions or other particle beams

    DOE Patents [OSTI]

    Hawryluk, A.M.; Ceglio, N.M.

    1993-01-12

    Virtually distortion free large field high resolution imaging is performed using an imaging system which contains large field distortion or field curvature. A reticle is imaged in one direction through the optical system to form an encoded mask. The encoded mask is then imaged back through the imaging system onto a wafer positioned at the reticle position. Particle beams, including electrons, ions and neutral particles, may be used as well as electromagnetic radiation.

  8. High-Resolution PFPE-based Molding Techniques for Nanofabrication of High-Pattern Density, Sub-20 nm Features: A Fundamental Materials Approach

    SciTech Connect (OSTI)

    Williams, Stuart S.; Retterer, Scott; Lopez, Rene; Ruiz, Ricardo; Samulski, Edward T.; DeSimone, Joseph M.

    2010-04-14

    Several perfluoropolyether (PFPE)-based elastomers for high-resolution replica molding applications are explored. The modulus of the elastomeric materials was increased through synthetic and additive approaches while maintaining relatively low surface tension values (<25 mN/m). Using large area (>4 in.{sup 2}) master templates, we experimentally show the relationship between mold resolution and material properties such as modulus and surface tension for materials used in this study. A composite mold approach was used to form flexible molds out of stiff, high modulus materials that allow for replication of sub-20 nm post structures. Sub-100 nm line grating master templates, formed using e-beam lithography, were used to determine the experimental stability of the molding materials. It was observed that as the feature spacing decreased, high modulus PFPE tetramethacrylate (TMA) composite molds were able to effectively replicate the nanograting structures without cracking or tear-out defects that typically occur with high modulus elastomers.

  9. 4-D High-Resolution Seismic Reflection Monitoring of Miscible CO2 Injected into a Carbonate Reservoir

    SciTech Connect (OSTI)

    Richard D. Miller; Abdelmoneam E. Raef; Alan P. Byrnes; William E. Harrison

    2007-06-30

    The objective of this research project was to acquire, process, and interpret multiple high-resolution 3-D compressional wave and 2-D, 2-C shear wave seismic data in the hopes of observing changes in fluid characteristics in an oil field before, during, and after the miscible carbon dioxide (CO{sub 2}) flood that began around December 1, 2003, as part of the DOE-sponsored Class Revisit Project (DOE No.DE-AC26-00BC15124). Unique and key to this imaging activity is the high-resolution nature of the seismic data, minimal deployment design, and the temporal sampling throughout the flood. The 900-m-deep test reservoir is located in central Kansas oomoldic limestones of the Lansing-Kansas City Group, deposited on a shallow marine shelf in Pennsylvanian time. After 30 months of seismic monitoring, one baseline and eight monitor surveys clearly detected changes that appear consistent with movement of CO{sub 2} as modeled with fluid simulators and observed in production data. Attribute analysis was a very useful tool in enhancing changes in seismic character present, but difficult to interpret on time amplitude slices. Lessons learned from and tools/techniques developed during this project will allow high-resolution seismic imaging to be routinely applied to many CO{sub 2} injection programs in a large percentage of shallow carbonate oil fields in the midcontinent.

  10. Lanai high-density irradiance sensor network for characterizing solar resource variability of MW-scale PV system.

    SciTech Connect (OSTI)

    Stein, Joshua S.; Johnson, Lars; Ellis, Abraham; Kuszmaul, Scott S.

    2012-01-01

    Sandia National Laboratories (Sandia) and SunPower Corporation (SunPower) have completed design and deployment of an autonomous irradiance monitoring system based on wireless mesh communications and a battery operated data acquisition system. The Lanai High-Density Irradiance Sensor Network is comprised of 24 LI-COR{reg_sign} irradiance sensors (silicon pyranometers) polled by 19 RF Radios. The system was implemented with commercially available hardware and custom developed LabVIEW applications. The network of solar irradiance sensors was installed in January 2010 around the periphery and within the 1.2 MW ac La Ola PV plant on the island of Lanai, Hawaii. Data acquired at 1 second intervals is transmitted over wireless links to be time-stamped and recorded on SunPower data servers at the site for later analysis. The intent is to study power and solar resource data sets to correlate the movement of cloud shadows across the PV array and its effect on power output of the PV plant. The irradiance data sets recorded will be used to study the shape, size and velocity of cloud shadows. This data, along with time-correlated PV array output data, will support the development and validation of a PV performance model that can predict the short-term output characteristics (ramp rates) of PV systems of different sizes and designs. This analysis could also be used by the La Ola system operator to predict power ramp events and support the function of the future battery system. This experience could be used to validate short-term output forecasting methodologies.

  11. Development of a high-resolution bathymetry dataset for the Columbia River through the Hanford Reach

    SciTech Connect (OSTI)

    Coleman, Andre M.; Ward, Duane L.; Larson, Kyle B.; Lettrick, Joseph W.

    2010-10-08

    A bathymetric and topographic data collection and processing effort involving existing and newly collected data has been performed for the Columbia River through the Hanford Reach in central Washington State, extending 60-miles from the tailrace of Priest Rapids Dam (river mile 397) to near the vicinity of the Interstate 182 bridge just upstream of the Yakima River confluence (river mile 337). The contents of this report provide a description of the data collections, data inputs, processing methodology, and final data quality assessment used to develop a comprehensive and continuous merged 1m resolution bathymetric and topographic surface dataset for the Columbia River through the Hanford Reach.

  12. New Strategies for 0.5 mm Resolution, High Sensitivity, Multi- Radionuclide Imaging

    SciTech Connect (OSTI)

    Levin, Craig S; Levin, Craig

    2015-02-28

    This project constitutes a 0.5-millimeter resolution radionuclide detector system built from CZT. (1) A novel dual-crystal photon detector module design with cross-strip electrode patterns was developed; (2) The module mechanical assembly was built; (3) A data acquisition (DAQ) chain for the module was produced; (4) A software tool was developed to incorporate novel time and energy measurement calibration techniques. (5) A small multi-detector prototype of the radionuclide imaging system was built from this module for system-level characterizations.

  13. Concurrent in situ ion irradiation transmission electron microscope

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Hattar, K.; Bufford, D. C.; Buller, D. L.

    2014-08-29

    An in situ ion irradiation transmission electron microscope has been developed and is operational at Sandia National Laboratories. This facility permits high spatial resolution, real time observation of electron transparent samples under ion irradiation, implantation, mechanical loading, corrosive environments, and combinations thereof. This includes the simultaneous implantation of low-energy gas ions (0.8–30 keV) during high-energy heavy ion irradiation (0.8–48 MeV). In addition, initial results in polycrystalline gold foils are provided to demonstrate the range of capabilities.

  14. High post-irradiation ductility thermomechanical treatment for precipitation strengthened austenitic alloys

    DOE Patents [OSTI]

    Laidler, James J. (Richland, WA); Borisch, Ronald R. (Kennewick, WA); Korenko, Michael K. (Rockville, MD)

    1982-01-01

    A method for improving the post-irradiation ductility is described which prises a solution heat treatment following which the materials are cold worked. They are included to demonstrate the beneficial effect of this treatment on the swelling resistance and the ductility of these austenitic precipitation hardenable alloys.

  15. High-resolution radio observations of W50, the remnant associated with SS 433

    SciTech Connect (OSTI)

    Elston, R.; Baum, S.

    1987-12-01

    The NRAO VLA has been used to observe the radio source W50 with 30 arcsec and 1 arcmin resolutions at 20 cm. It is found that the overall structure of W50 is well delineated by filamentary structure. W50 possesses a nearly circular shell reminiscent of an evolved supernova remnant such as CTB1 and the Cygnus Loop. The most unusual features of W50 are the edge-brightened radio ears which extend beyond the shell. These ears appear morphologically distinct from the shell and have minimum energy pressures three times greater than are present in the shell. Thus, while no direct connection is observed between SS433 and the ears, it is suggested that the ears are the result of the interaction of the ram pressure of the collimated jets of SS433 with a supernova remnant shell. At 30 arcsec resolution the western ear of W50 is depolarized, suggesting that W50 and S74 are at a common distance of about 3 kpc. 27 references.

  16. Unambiguous determination of H-atom positions: comparing results from neutron and high-resolution X-ray crystallography

    SciTech Connect (OSTI)

    Gardberg, Anna S.; Del Castillo, Alexis R.; Weiss, Kevin L.; Meilleur, Flora; Blakeley, Matthew P.; Myles, Dean A.A.

    2010-11-19

    The locations of H atoms in biological structures can be difficult to determine using X-ray diffraction methods. Neutron diffraction offers a relatively greater scattering magnitude from H and D atoms. Here, 1.65 {angstrom} resolution neutron diffraction studies of fully perdeuterated and selectively CH{sub 3}-protonated perdeuterated crystals of Pyrococcus furiosus rubredoxin (D-rubredoxin and HD-rubredoxin, respectively) at room temperature (RT) are described, as well as 1.1 {angstrom} resolution X-ray diffraction studies of the same protein at both RT and 100 K. The two techniques are quantitatively compared in terms of their power to directly provide atomic positions for D atoms and analyze the role played by atomic thermal motion by computing the {sigma} level at the D-atom coordinate in simulated-annealing composite D-OMIT maps. It is shown that 1.65 {angstrom} resolution RT neutron data for perdeuterated rubredoxin are {approx}8 times more likely overall to provide high-confidence positions for D atoms than 1.1 {angstrom} resolution X-ray data at 100 K or RT. At or above the 1.0{sigma} level, the joint X-ray/neutron (XN) structures define 342/378 (90%) and 291/365 (80%) of the D-atom positions for D-rubredoxin and HD-rubredoxin, respectively. The X-ray-only 1.1 {angstrom} resolution 100 K structures determine only 19/388 (5%) and 8/388 (2%) of the D-atom positions above the 1.0{sigma} level for D-rubredoxin and HD-rubredoxin, respectively. Furthermore, the improved model obtained from joint XN refinement yielded improved electron-density maps, permitting the location of more D atoms than electron-density maps from models refined against X-ray data only.

  17. High resolution short focal distance Bent Crystal Laue Analyzer for copper K edge x-ray absorption spectroscopy

    SciTech Connect (OSTI)

    Kujala, N. G.; Barrea, R. A.; Karanfil, C.

    2011-06-15

    We have developed a compact short focal distance Bent Crystal Laue Analyzer (BCLA) for Cu speciation studies of biological systems with specific applications to cancer biology. The system provides high energy resolution and high background rejection. The system is composed of an aluminum block serving as a log spiral bender for a 15 micron thick Silicon 111 crystal and a set of soller slits. The energy resolution of the BCLA--about 14 eV at the Cu K{alpha} line-- allows resolution of the Cu K{alpha}{sub 1} and CuK{alpha}{sub 2} lines. The system is easily aligned by using a set of motorized XYZ linear stages. Two operation modes are available: incident energy scans (IES) and emission energy scans (EES). IES allows scanning of the incident energy while the BCLA system is maintained at a preselected fixed position - typically CuK{alpha}{sub 1} line. EES is used when the incident energy is fixed and the analyzer is scanned to provide the peak profile of the emission lines of Cu.

  18. Experimentally characterizing the electronic structures of f-electron systems using advanced high resolution Fourier transform microwave spectroscopies

    SciTech Connect (OSTI)

    Cooke, Stephen, A

    2013-02-03

    We aim to (i) provide data that directly addresses the fundamental roles of actinide valence electrons in chemical bonding, and (ii) serve to provide prototypical data for the heavy element computational chemistry community. These goals will be achieved through the first pure rotational spectroscopic measurements on prototypical systems at ultra-high resolution. These systems encompass low oxidation state uranium and thorium compounds including, but not limited to, UX and ThX, X = F, Cl, Br, I, and UY and ThY, Y = O, S, and other simple U and Th-containing compounds. Our primary experimental tools involve time-domain rotational spectroscopy achieving line widths and resolutions of a few kHz.

  19. A High Resolution, Multi-stop, Time-to-Digital Converter for Nuclear Time-of-Flight Measurements

    SciTech Connect (OSTI)

    D. F. Spencer; J. Cole; M. Drigert; R. Aryaeinejad

    2006-01-01

    A high-resolution, multi-stop, time-to-digital converter (TDC) was designed and developed to precisely measure the times-of-flight (TOF) of incident neutrons responsible for induced fission and capture reactions on actinide targets. The minimum time resolution is 1 ns. The TDC design was implemented into a single, dual-wide CAMAC module. The CAMAC bus is used for command and control as well as an alternative data output. A high-speed ECL interface, compatible with LeCroy FERA modules, was also provided for the principle data output path. An Actel high-speed field programmable gate array (FPGA) chip was incorporated with an external oscillator and an internal multiple clock phasing system. This device implemented the majority of the high-speed register functions, the state machine for the FERA interface, and the high-speed counting circuit used for the TDC conversion. An external microcontroller was used to monitor and control system-level changes. In this work we discuss the performance of this TDC module as well as its application.

  20. Apparatus and method to achieve high-resolution microscopy with non-diffracting or refracting radiation

    DOE Patents [OSTI]

    Tobin, Jr., Kenneth W.; Bingham, Philip R.; Hawari, Ayman I.

    2012-11-06

    An imaging system employing a coded aperture mask having multiple pinholes is provided. The coded aperture mask is placed at a radiation source to pass the radiation through. The radiation impinges on, and passes through an object, which alters the radiation by absorption and/or scattering. Upon passing through the object, the radiation is detected at a detector plane to form an encoded image, which includes information on the absorption and/or scattering caused by the material and structural attributes of the object. The encoded image is decoded to provide a reconstructed image of the object. Because the coded aperture mask includes multiple pinholes, the radiation intensity is greater than a comparable system employing a single pinhole, thereby enabling a higher resolution. Further, the decoding of the encoded image can be performed to generate multiple images of the object at different distances from the detector plane. Methods and programs for operating the imaging system are also disclosed.

  1. High Resolution RANS NLH Study of Stage 67 Tip Injection Physics

    SciTech Connect (OSTI)

    Matheson, Michael A

    2014-01-01

    Numerical prediction of the Stage 67 transonic fan stage employing wall jet tip injection flow control and study of the physical mechanisms leading to stall suppression and stability enhancement afforded by endwall recirculation/injection is the focus of this paper. Reynolds averaged Navier-Stokes computations were used to perform detailed analysis of the Stage 67 configuration experimentally tested at NASA s Glenn Research Center in 2004. Time varying prediction of the stage plus recirculation and injection flowpath were performed utilizing the Nonlinear Harmonic approach. Significantly higher grid resolution per passage was achieved than what has been generally employed in prior reported numerical studies of spike stall phenomena in transonic compressors. This paper focuses on characterizing the physics of spike stall embryonic stage phenomena and the impact of tip injection, resulting in experimentally and numerically demonstrated stall suppression

  2. High-resolution emissions of CO{sub 2} from power generation in the USA - article no. G04008

    SciTech Connect (OSTI)

    Petron, G.; Tans, P.; Frost, G.; Chao, D.L.; Trainer, M. [NOAA, Boulder, CO (United States). Earth Systems Research Laboratory

    2008-10-15

    Electricity generation accounts for close to 40% of the U.S. CO{sub 2} emissions from fossil fuel burning, making it the economic sector with the largest source of CO{sub 2}. Since the late 1990s, the Environmental Protection Agency Clean Air Markets Division (EPA CAMD) has kept a repository of hourly CO{sub 2} emission data for most power plants in the conterminous United States. In this study, the CAMD CO{sub 2} data are used to derive a high spatiotemporal resolution CO{sub 2} emissions inventory for the electricity generation sector (inventory available on request). Data from 1998 to 2006 have been processed. This unique inventory can be used to improve the understanding of the carbon cycle at fine temporal and spatial scales. The CAMD data set provides the first quantitative estimates of the diurnal and seasonal cycles of the emissions as well as the year to year variability. Emissions peak in the summertime owing to the widespread use of air conditioning. Summertime emissions are in fact highly correlated with the daily average temperature. In conjunction with the EPA Emissions and Generation Resource Integrated Database (eGRID), we have derived high-resolution maps of CO{sub 2} emissions by fossil fuel burned (coal, gas, oil) for the year 2004. The CAMD data set also reflects regional anomalies in power generation such as the August 2003 blackout in the northeastern United States and the 2000-2001 increase in production in California. We recommend that all sectors of the economy report similar high-resolution CO{sub 2} emissions because of their great usefulness both for carbon cycle science and for greenhouse gases emissions mitigation and regulation.

  3. Facility for high heat flux testing of irradiated fusion materials and components using infrared plasma arc lamps

    SciTech Connect (OSTI)

    Sabau, Adrian S; Ohriner, Evan Keith; Kiggans, Jim; Harper, David C; Snead, Lance Lewis; Schaich, Charles Ross

    2014-01-01

    A new high-heat flux testing facility using water-wall stabilized high-power high-pressure argon Plasma Arc Lamps (PALs) has been developed for fusion applications. It can handle irradiated plasma facing component materials and mock-up divertor components. Two PALs currently available at ORNL can provide maximum incident heat fluxes of 4.2 and 27 MW/m2 over a heated area of 9x12 and 1x10 cm2, respectively, which are fusion-prototypical steady state heat flux conditions. The facility will be described and the main differences between the photon-based high-heat flux testing facilities, such as PALs, and the e-beam and particle beam facilities more commonly used for fusion HHF testing are discussed. The components of the test chamber were designed to accommodate radiation safety and materials compatibility requirements posed by high-temperature exposure of low levels irradiated tungsten articles. Issues related to the operation and temperature measurements during testing are presented and discussed.

  4. High resolution mass spectrometry method and system for analysis of whole proteins and other large molecules

    DOE Patents [OSTI]

    Reilly, Peter T. A. [Knoxville, TN; Harris, William A. [Naperville, IL

    2010-03-02

    A matrix assisted laser desorption/ionization (MALDI) method and related system for analyzing high molecular weight analytes includes the steps of providing at least one matrix-containing particle inside an ion trap, wherein at least one high molecular weight analyte molecule is provided within the matrix-containing particle, and MALDI on the high molecular weight particle while within the ion trap. A laser power used for ionization is sufficient to completely vaporize the particle and form at least one high molecular weight analyte ion, but is low enough to avoid fragmenting the high molecular weight analyte ion. The high molecular weight analyte ion is extracted out from the ion trap, and is then analyzed using a detector. The detector is preferably a pyrolyzing and ionizing detector.

  5. Testing of Performance of Optical Fibers Under Irradiation in Intense Radiation Fields, When Subjected to Very High Temperatures

    SciTech Connect (OSTI)

    Blue, Thomas; Windl, Wolfgang; Dickerson, Bryan

    2013-01-03

    The primary objective of this project is to measure and model the performance of optical fibers in intense radiation fields when subjected to very high temperatures. This research will pave the way for fiber optic and optically based sensors under conditions expected in future high-temperature gas-cooled reactors. Sensor life and signal-to-noise ratios are susceptible to attenuation of the light signal due to scattering and absorbance in the fibers. This project will provide an experimental and theoretical study of the darkening of optical fibers in high-radiation and high-temperature environments. Although optical fibers have been studied for moderate radiation fluence and flux levels, the results of irradiation at very high temperatures have not been published for extended in-core exposures. Several previous multi-scale modeling efforts have studied irradiation effects on the mechanical properties of materials. However, model-based prediction of irradiation-induced changes in silicaâ??s optical transport properties has only recently started to receive attention due to possible applications as optical transmission components in fusion reactors. Nearly all damage-modeling studies have been performed in the molecular-dynamics domain, limited to very short times and small systems. Extended-time modeling, however, is crucial to predicting the long-term effects of irradiation at high temperatures, since the experimental testing may not encompass the displacement rate that the fibers will encounter if they are deployed in the VHTR. The project team will pursue such extended-time modeling, including the effects of the ambient and recrystallization. The process will be based on kinetic MC modeling using the concept of amorphous material consisting of building blocks of defect-pairs or clusters, which has been successfully applied to kinetic modeling in amorphized and recrystallized silicon. Using this procedure, the team will model compensation for rate effects, and the interplay of rate effects with the effects of annealing, to accurately predict the fibersâ?? reliability and expected lifetime

  6. Time-resolved photoemission apparatus achieving sub-20-meV energy resolution and high stability

    SciTech Connect (OSTI)

    Ishida, Y.; Togashi, T.; Yamamoto, K.; Tanaka, M.; Kiss, T.; Otsu, T.; Kobayashi, Y.; Shin, S.

    2014-12-15

    The paper describes a time- and angle-resolved photoemission apparatus consisting of a hemispherical analyzer and a pulsed laser source. We demonstrate 1.48-eV pump and 5.92-eV probe measurements at the ?10.5-meV and ?240-fs resolutions by use of fairly monochromatic 170-fs pulses delivered from a regeneratively amplified Ti:sapphire laser system operating typically at 250 kHz. The apparatus is capable to resolve the optically filled superconducting peak in the unoccupied states of a cuprate superconductor, Bi{sub 2}Sr{sub 2}CaCu{sub 2}O{sub 8+?}. A dataset recorded on Bi(111) surface is also presented. Technical descriptions include the followings: A simple procedure to fine-tune the spatio-temporal overlap of the pump-and-probe beams and their diameters; achieving a long-term stability of the system that enables a normalization-free dataset acquisition; changing the repetition rate by utilizing acoustic optical modulator and frequency-division circuit.

  7. NGC 4102: HIGH-RESOLUTION INFRARED OBSERVATIONS OF A NUCLEAR STARBURST RING

    SciTech Connect (OSTI)

    Beck, Sara C.; Lacy, John H.; Turner, Jean L.

    2010-10-20

    The composite galaxy NGC 4102 hosts a LINER nucleus and a starburst. We mapped NGC 4102 in the 12.8 {mu}m line of [Ne II], using the echelon spectrometer TEXES on the NASA IRTF, to obtain a data cube with 1.''5 spatial, and 25 km s{sup -1} spectral, resolution. Combining near-infrared, radio, and the [Ne II] data shows that the extinction to the starburst is substantial, more than 2 mag at the K band, and that the neon abundance is less than half solar. We find that the star formation in the nuclear region is confined to a rotating ring or disk of 4.''3 ({approx}300 pc) diameter, inside the inner Lindblad resonance. This region is an intense concentration of mass, with a dynamical mass {approx}3 x 10{sup 9} M{sub sun}, and of star formation. The young stars in the ring produce the [Ne II] flux reported by Spitzer for the entire galaxy. The mysterious blue component of line emission detected in the near-infrared is also seen in [Ne II]; it is not a normal active galactic nucleus outflow.

  8. Development of high-spatial and high-mass resolution mass spectrometric imaging (MSI) and its application to the study of small metabolites and endogenous molecules of plants

    SciTech Connect (OSTI)

    Jun, Ji Hyun

    2011-11-30

    High-spatial and high-mass resolution laser desorption ionization (LDI) mass spectrometric (MS) imaging technology was developed for the attainment of MS images of higher quality containing more information on the relevant cellular and molecular biology in unprecedented depth. The distribution of plant metabolites is asymmetric throughout the cells and tissues, and therefore the increase in the spatial resolution was pursued to reveal the localization of plant metabolites at the cellular level by MS imaging. For achieving high-spatial resolution, the laser beam size was reduced by utilizing an optical fiber with small core diameter (25 μm) in a vacuum matrix-assisted laser desorption ionization-linear ion trap (vMALDI-LTQ) mass spectrometer. Matrix application was greatly improved using oscillating capillary nebulizer. As a result, single cell level spatial resolution of ~ 12 μm was achieved. MS imaging at this high spatial resolution was directly applied to a whole Arabidopsis flower and the substructures of an anther and single pollen grains at the stigma and anther were successfully visualized. MS imaging of high spatial resolution was also demonstrated to the secondary roots of Arabidopsis thaliana and a high degree of localization of detected metabolites was successfully unveiled. This was the first MS imaging on the root for molecular species. MS imaging with high mass resolution was also achieved by utilizing the LTQ-Orbitrap mass spectrometer for the direct identification of the surface metabolites on the Arabidopsis stem and root and differentiation of isobaric ions having the same nominal mass with no need of tandem mass spectrometry (MS/MS). MS imaging at high-spatial and high-mass resolution was also applied to cer1 mutant of the model system Arabidopsis thaliana to demonstrate its usefulness in biological studies and reveal associated metabolite changes in terms of spatial distribution and/or abundances compared to those of wild-type. The spatial distribution of targeted metabolites, mainly waxes and flavonoids, was systematically explored on various organs, including flowers, leaves, stems, and roots at high spatial resolution of ~ 12-50 μm and the changes in the abundance level of these metabolites were monitored on the cer1 mutant with respect to the wild-type. This study revealed the metabolic biology of CER1 gene on each individual organ level with very detailed high spatial resolution. The separate MS images of isobaric metabolites, i.e. C29 alkane vs. C28 aldehyde could be constructed on both genotypes from MS imaging at high mass resolution. This allows tracking of abundance changes for those compounds along with the genetic mutation, which is not achievable with low mass resolution mass spectrometry. This study supported previous hypothesis of molecular function of CER1 gene as aldehyde decarbonylase, especially by displaying hyper accumulation of aldehydes and C30 fatty acid and decrease in abundance of alkanes and ketones in several plant organs of cer1 mutant. The scope of analytes was further directed toward internal cell metabolites from the surface metabolites of the plant. MS profiling and imaging of internal cell metabolites were performed on the vibratome section of Arabidopsis leaf. Vibratome sectioning of the leaf was first conducted to remove the surface cuticle layer and it was followed by enzymatic treatment of the section to induce the digestion of primary cell walls, middle lamella, and expose the internal cells underneath to the surface for detection with the laser by LDI-MS. The subsequent MS imaging onto the enzymatically treated vibratome section allowed us to map the distribution of the metabolites in the internal cell layers, linolenic acid (C18:3 FA) and linoleic acid (C18:2 FA). The development of an assay for relative quantification of analytes at the single subcellular/organelle level by LDI-MS imaging was attempted and both plausibility and significant obstacles were seen. As a test system, native plant organelle, chloroplasts isolated from the spinach leaves were used and the localization of isolated chloroplasts dispersed on the target plate in low density was monitored by detecting the ion signal of chlorophyll a (Chl a) degradation products such as pheophytin a and pheophobide a by LDI-MS imaging in combination with fluorescence microscopy. The number of chloroplasts and their localization visualized in the MS image exactly matched those in the fluorescence image especially at low density, which first shows the plausibility of single-organelle level quantification of analytes by LDI-MS. The accumulation level of Chl a within a single chloroplast detected by LDI-MS was compared to the fluorescence signal on a pixel-to-pixel basis to further confirm the correlations of the accumulation levels measured by two methods. The proportional correlation was observed only for the chloroplasts which do not show the significant leakage of chlorophyll indicated by MS ion signal of Chl a degradation products and fluorescence signal, which was presumably caused by the prior fluorescence measurement before MS imaging. Further investigation is necessary to make this method more complete and develop LDI-MS imaging as an effective analytical tool to evaluate a relative accumulation of analytes of interest at the single subcellular/organelle level.

  9. Simulation of High-Resolution Magnetic Resonance Images on the IBM Blue Gene/L Supercomputer Using SIMRI

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Baum, K. G.; Menezes, G.; Helguera, M.

    2011-01-01

    Medical imaging system simulators are tools that provide a means to evaluate system architecture and create artificial image sets that are appropriate for specific applications. We have modified SIMRI, a Bloch equation-based magnetic resonance image simulator, in order to successfully generate high-resolution 3D MR images of the Montreal brain phantom using Blue Gene/L systems. Results show that redistribution of the workload allows an anatomically accurate 256 3 voxel spin-echo simulation in less than 5 hours when executed on an 8192-node partition of a Blue Gene/L system.

  10. High-resolution imaging of selenium in kidneys: a localized selenium pool associated with glutathione peroxidase 3

    SciTech Connect (OSTI)

    Malinouski, M.; Kehr, S.; Finney, L.; Vogt, S.; Carlson, B.A.; Seravalli, J.; Jin, R.; Handy, D.E.; Park, T.J.; Loscalzo, J.; Hatfield, D.L.; Gladyshev, V.N.

    2012-04-17

    Recent advances in quantitative methods and sensitive imaging techniques of trace elements provide opportunities to uncover and explain their biological roles. In particular, the distribution of selenium in tissues and cells under both physiological and pathological conditions remains unknown. In this work, we applied high-resolution synchrotron X-ray fluorescence microscopy (XFM) to map selenium distribution in mouse liver and kidney. Liver showed a uniform selenium distribution that was dependent on selenocysteine tRNA{sup [Ser]Sec} and dietary selenium. In contrast, kidney selenium had both uniformly distributed and highly localized components, the latter visualized as thin circular structures surrounding proximal tubules. Other parts of the kidney, such as glomeruli and distal tubules, only manifested the uniformly distributed selenium pattern that co-localized with sulfur. We found that proximal tubule selenium localized to the basement membrane. It was preserved in Selenoprotein P knockout mice, but was completely eliminated in glutathione peroxidase 3 (GPx3) knockout mice, indicating that this selenium represented GPx3. We further imaged kidneys of another model organism, the naked mole rat, which showed a diminished uniformly distributed selenium pool, but preserved the circular proximal tubule signal. We applied XFM to image selenium in mammalian tissues and identified a highly localized pool of this trace element at the basement membrane of kidneys that was associated with GPx3. XFM allowed us to define and explain the tissue topography of selenium in mammalian kidneys at submicron resolution.

  11. Analog morphocorrelation: new technique with implications for high-resolution absolute age dating

    SciTech Connect (OSTI)

    Arnold, A.J.; Parker, W.C.; Berggren, W.A.

    1986-05-01

    The conventional approach to increased biostratigraphic resolution involves identifying additional datum planes defined by discrete events. Multivariate techniques used to refine a conventional taxonomic zonal scheme offer no improvement in precision; however, since the characters on which the zonal boundaries are based often show continuous stratigraphic variation, they offer an opportunity for continuous stratigraphic correlation based on the stage of evolution. Morphometric analysis was conducted on two lineages: (1) the Globorotalia cibaoensis-G. crassaformis linage, using a reference section from the early Pliocene of the Rio Grande rise, spanning approximately 2.6 m.y.; and (2) the G. conoidea-G.inflata lineage, using a reference section from the late Miocene to the Holocene from the southwest Pacific, spanning approximately 8 m.y. Stepwise multiple regression of morphologic variates generated an equation with an age-prediction precision (95% confidence) of +/- 122 k.y. in the G. crassaformis lineage and +/- 463 k.y. in the G conoidea lineage (accuracy depends on calibration of absolute dates in the reference section and our knowledge of sedimentation rates over the measured interval). Using single-equation analog morphocorrelation, any sample overlapped by the reference lineage can be correlated, which reduce the need for repeated sampling in a search for discrete events. The authors demonstrate that analysis of continuous morphologic variation can increase stratigraphic precision with a few carefully chosen variables, and that analog morpho-correlation can yield absolute dates, rather than relative dates with quantified error. Any disadvantages inherent in analog morphocorrelation are also found in conventional biostratigraphic techniques, but are usually unquantified and unrecognized.

  12. Performance of AGR-1 High-Temperature Reactor Fuel During Post-Irradiation Heating Tests

    SciTech Connect (OSTI)

    Morris, Robert Noel; Baldwin, Charles A; Hunn, John D; Demkowicz, Paul; Reber, Edward

    2014-01-01

    The fission product retention of irradiated low-enriched uranium oxide/uranium carbide TRISO fuel compacts from the AGR-1 experiment has been evaluated at temperatures of 1600 1800 C during post-irradiation safety tests. Fourteen compacts (a total of ~58,000 particles) with a burnup ranging from 13.4 to 19.1% FIMA have been tested using dedicated furnace systems at Idaho National Laboratory and Oak Ridge National Laboratory. The release of fission products 110mAg, 134Cs, 137Cs, 154Eu, 155Eu, 90Sr, and 85Kr was monitored while heating the fuel specimens in flowing helium. The behavior of silver, europium, and strontium appears to be dominated by inventory that was originally released through intact SiC coating layers during irradiation, but was retained in the compact at the end of irradiation and subsequently released during the safety tests. However, at a test temperature of 1800 C, the data suggest that release of these elements through intact coatings may become significant after ~100 h. Cesium was very well retained by intact SiC layers, with a fractional release <5 10-6 after 300 h at 1600 C or 100 h at 1800 C. However, it was rapidly released from individual particles if the SiC layer failed, and therefore the overall cesium release fraction was dominated by the SiC defect and failure fractions in the fuel compacts. No complete TRISO coating layer failures were observed after 300 h at 1600 or 1700 C, and 85Kr release was very low during the tests (particles with breached SiC, but intact outer pyrocarbon, retained most of their krypton). Krypton release from TRISO failures was only observed after ~210 h at 1800 C in one compact. Post-safety-test examination of fuel compacts and particles has focused on identifying specific particles from each compact with notable fission product release and detailed analysis of the coating layers to understand particle behavior.

  13. Swelling in several commercial alloys irradiated to very high neutron fluence

    SciTech Connect (OSTI)

    Gelles, D.S.; Pintler, J.S.

    1983-01-01

    Swelling values have been obtained from a set of commercial alloys irradiated in EBR-II to a peak fluence of 2.5 x 10/sup 23/ n/cm/sup 2/ (E > 0.1 MeV) or approx. 125 dpa covering the range 400 to 650/sup 0/C. The alloys can be ranked for swelling resistance from highest to lowest as follows: the martensitic and ferritic alloys, the niobium based alloys, the precipitation strengthened iron and nickel based alloys, the molybdenum alloys and the austenitic alloys.

  14. High-Heat Flux Testing of Irradiated Tungsten based Materials for Fusion Applications using Infrared Plasma Arc Lamps

    SciTech Connect (OSTI)

    Sabau, Adrian S; Ohriner, Evan Keith; Kiggans Jr, James O; Schaich, Charles Ross; Ueda, Yoshio; Harper, David C; Katoh, Yutai; Snead, Lance Lewis; Byun, Thak Sang

    2014-01-01

    Testing of advanced materials and component mock-ups under prototypical fusion high-heat flux conditions, while historically a mainstay of fusion research has proved challenging, especially for irradiated materials. A new high-heat flux testing facility based on water-wall Plasma Arc Lamps (PALs) is now being used for materials and small component testing. Two PAL systems, utilizing a 12,000 C plasma arc contained in a quartz tube cooled by a spiral water flow over the inside tube surface, are currently in use. The first PAL system provides a maximum incident heat flux of 4.2 MW/m2 over an area of 9x12 cm2. The second PAL available at ORNL provides a maximum incident heat flux of 27 MW/m2 over an area of 1x10 cm2. The absorbed heat fluxes into a tungsten target for the two PALs are approximately 1.97 and 12.7 MW/m2, respectively. This paper will present the overall design of the new PAL facilities as well as the design and implementation of the Irradiated Material Target Station (IMTS). The IMTS is primarily designed for testing the effects of heat flux or thermal cycling on material coupons of interested, such as those for plasma facing components. Moreover, IMTS designs are underway to extend the testing of small mock-ups for assessing the combined heating and thermomechanical effects of cooled, irradiated components. For the testing of material coupons , the specimens are placed in a shallow recess within the molybdenum holder that is attached to a water-cooled copper alloy rod. As the measurement of the specimen temperature for PAL is historically challenging since traditional approaches of temperature measurement cannot be employed due to the infrared heating and proximity of the PAL reflector to the specimen that does not allow a direct line of site, experiments for temperature calibration are presented. Finally, results for the high-heat flux testing of tungsten-based materials using the PAL are presented. As a demonstration of the system, results will be shown of thermal fatigue and high-heat flux testing of tungsten coupon specimens that were neutron irradiated in the HFIR reactor to neutron dose consistent to ITER lifetime.

  15. High-Heat Flux Testing of Irradiated Tungsten based Materials for Fusion Applications using Infrared Plasma Arc Lamps

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Sabau, Adrian S; Ohriner, Evan Keith; Kiggans, Jr, James O; Schaich, Charles Ross; Ueda, Yoshio; Harper, David C; Katoh, Yutai; Snead, Lance Lewis; Byun, Thak Sang

    2014-01-01

    Testing of advanced materials and component mock-ups under prototypical fusion high-heat flux conditions, while historically a mainstay of fusion research has proved challenging, especially for irradiated materials. A new high-heat flux testing facility based on water-wall Plasma Arc Lamps (PALs) is now being used for materials and small component testing. Two PAL systems, utilizing a 12,000 C plasma arc contained in a quartz tube cooled by a spiral water flow over the inside tube surface, are currently in use. The first PAL system provides a maximum incident heat flux of 4.2 MW/m2 over an area of 9x12 cm2. The secondmore » PAL available at ORNL provides a maximum incident heat flux of 27 MW/m2 over an area of 1x10 cm2. The absorbed heat fluxes into a tungsten target for the two PALs are approximately 1.97 and 12.7 MW/m2, respectively. This paper will present the overall design of the new PAL facilities as well as the design and implementation of the Irradiated Material Target Station (IMTS). The IMTS is primarily designed for testing the effects of heat flux or thermal cycling on material coupons of interested, such as those for plasma facing components. Moreover, IMTS designs are underway to extend the testing of small mock-ups for assessing the combined heating and thermomechanical effects of cooled, irradiated components. For the testing of material coupons , the specimens are placed in a shallow recess within the molybdenum holder that is attached to a water-cooled copper alloy rod. As the measurement of the specimen temperature for PAL is historically challenging since traditional approaches of temperature measurement cannot be employed due to the infrared heating and proximity of the PAL reflector to the specimen that does not allow a direct line of site, experiments for temperature calibration are presented. Finally, results for the high-heat flux testing of tungsten-based materials using the PAL are presented. As a demonstration of the system, results will be shown of thermal fatigue and high-heat flux testing of tungsten coupon specimens that were neutron irradiated in the HFIR reactor to neutron dose consistent to ITER lifetime.« less

  16. A novel apparatus for in situ compression of submicron structures and particles in a high resolution SEM

    SciTech Connect (OSTI)

    Romeis, S.; Paul, J.; Ziener, M.; Peukert, W.

    2012-09-15

    We report on the development and characterization of a novel in situ manipulation device to perform stressing experiments on the submicron scale inside a high resolution field emission scanning electron microscope. The instrument comprises two main assembly groups: an upper part for positioning and moving a mounted probe and a force sensor as well as a specimen support as lower part. The upper part consists of a closed loop tripod piezoelectric scanner mounted on a self-locking coarse positioning stage. Two interlocked steel springs and a linear variable differential transformer measuring the springs' deflections compose the lower part of the instrument. This arrangement acts as force-sensor and sample support. In comparison to already well-established concepts a wide measuring range is covered by adjusting the spring constant between 30 N/m and 50000 N/m. Moreover, the new device offers striking advantages with respect to force calibration and sample deformation measurements. Force calibration is performed using the eigenfrequency of the force detection system directly inside the SEM. Deformation data are obtained with high accuracy by simultaneously recording displacements above and below the specimen. The detrimental apparatus compliance is determined, and the influence on measured data subsequently minimized: an easy to validate two-springs-in-series model is used for data correction. A force resolution in normal direction of 100 nN accompanied by a sample deformation resolution of 5 nm can be achieved with the instrument using an appropriate load cell stiffness. The capabilities and versatility of this instrument are exemplified by compression experiments performed on submicron amorphous silica particles.

  17. HIGH-TIME-RESOLUTION MEASUREMENTS OF THE POLARIZATION OF THE CRAB PULSAR AT 1.38 GHz

    SciTech Connect (OSTI)

    Słowikowska, Agnieszka; Stappers, Benjamin W.; Harding, Alice K.; O'Dell, Stephen L.; Elsner, Ronald F.; Weisskopf, Martin C.; Van der Horst, Alexander J.

    2015-01-20

    Using the Westerbork Synthesis Radio Telescope, we obtained high-time-resolution measurements of the full polarization of the Crab pulsar. At a resolution of 1/8192 of the 34 ms pulse period (i.e., 4.1 μs), the 1.38 GHz linear-polarization measurements are in general agreement with previous lower-time-resolution 1.4 GHz measurements of linear polarization in the main pulse (MP), in the interpulse (IP), and in the low-frequency component (LFC). We find the MP and IP to be linearly polarized at about 24% and 21% with no discernible difference in polarization position angle. However, contrary to theoretical expectations and measurements in the visible, we find no evidence for significant variation (sweep) in the polarization position angle over the MP, the IP, or the LFC. We discuss the implications, which appear to be in contradiction to theoretical expectations. We also detect weak circular polarization in the MP and IP, and strong (≈20%) circular polarization in the LFC, which also exhibits very strong (≈98%) linear polarization at a position angle of 40° from that of the MP or IP. The properties are consistent with the LFC, which is a low-altitude component, and the MP and IP, which are high-altitude caustic components. Current models for the MP and IP emission do not readily account for the absence of pronounced polarization changes across the pulse. We measure IP and LFC pulse phases relative to the MP consistent with recent measurements, which have shown that the phases of these pulse components are evolving with time.

  18. A digital map of the high center (HC) and low center (LC) polygon boundaries delineated from high resolution LiDAR data for Barrow, Alaska

    SciTech Connect (OSTI)

    Gangodagamage, Chandana; Wullschleger, Stan

    2014-07-03

    This dataset represent a map of the high center (HC) and low center (LC) polygon boundaries delineated from high resolution LiDAR data for the arctic coastal plain at Barrow, Alaska. The polygon troughs are considered as the surface expression of the ice-wedges. The troughs are in lower elevations than the interior polygon. The trough widths were initially identified from LiDAR data, and the boundary between two polygons assumed to be located along the lowest elevations on trough widths between them.

  19. Study of hydrogen in coals, polymers, oxides, and muscle water by nuclear magnetic resonance; extension of solid-state high-resolution techniques. [Hydrogen molybdenum bronze

    SciTech Connect (OSTI)

    Ryan, L.M.

    1981-10-01

    Nuclear magnetic resonance (NMR) spectroscopy has been an important analytical and physical research tool for several decades. One area of NMR which has undergone considerable development in recent years is high resolution NMR of solids. In particular, high resolution solid state /sup 13/C NMR spectra exhibiting features similar to those observed in liquids are currently achievable using sophisticated pulse techniques. The work described in this thesis develops analogous methods for high resolution /sup 1/H NMR of rigid solids. Applications include characterization of hydrogen aromaticities in fossil fuels, and studies of hydrogen in oxides and bound water in muscle.

  20. High resolution InSb quantum well ballistic nanosensors for room temperature applications

    SciTech Connect (OSTI)

    Gilbertson, Adam; Cohen, L. F.; Lambert, C. J.; Solin, S. A.

    2013-12-04

    We report the room temperature operation of a quasi-ballistic InSb quantum well Hall sensor that exhibits a high frequency sensitivity of 560nT/?Hz at 20uA bias current. The device utilizes a partitioned buffer layer design that suppresses leakage currents through the mesa floor and can sustain large current densities.

  1. High-resolution x-ray diffraction study of the heavy-fermion compound YbBiPt

    SciTech Connect (OSTI)

    Ueland, B. G.; Saunders, S. M.; Bud'ko, S. L.; Schmiedeshoff, G. M.; Canfield, P. C.; Kreyssig, A.; Goldman, A. I.

    2015-11-30

    In this study, YbBiPt is a heavy-fermion compound possessing significant short-range antiferromagnetic correlations below a temperature of T*=0.7K, fragile antiferromagnetic order below TN = 0.4K, a Kondo temperature of TK ? 1K, and crystalline-electric-field splitting on the order of E/kB = 1 10K. Whereas the compound has a face-centered-cubic lattice at ambient temperature, certain experimental data, particularly those from studies aimed at determining its crystalline-electric-field scheme, suggest that the lattice distorts at lower temperature. Here, we present results from high-resolution, high-energy x-ray diffraction experiments which show that, within our experimental resolution of ? 6 10 105 , no structural phase transition occurs between T = 1.5 and 50 K. In combination with results from dilatometry measurements, we further show that the compound's thermal expansion has a minimum at ? 18 K and a region of negative thermal expansion for 9 ? T ? 18 K. Despite diffraction patterns taken at 1.6 K which indicate that the lattice is face-centered cubic and that the Yb resides on a crystallographic site with cubic point symmetry, we demonstrate that the linear thermal expansion may be modeled using crystalline-electric-field level schemes appropriate for Yb3+ residing on a site with either cubic or less than cubic point symmetry.

  2. High-resolution single-shot spectral monitoring of hard x-ray free-electron laser radiation

    SciTech Connect (OSTI)

    Makita, M.; Karvinen, P.; Zhu, D.; Juranic, P. N.; Grünert, J.; Cartier, S.; Jungmann-Smith, J. H.; Lemke, H. T.; Mozzanica, A.; Nelson, S.; Patthey, L.; Sikorski, M.; Song, S.; Feng, Y.; David, C.

    2015-10-16

    We have developed an on-line spectrometer for hard x-ray free-electron laser (XFEL) radiation based on a nanostructured diamond diffraction grating and a bent crystal analyzer. Our method provides high spectral resolution, interferes negligibly with the XFEL beam, and can withstand the intense hard x-ray pulses at high repetition rates of >100 Hz. The spectrometer is capable of providing shot-to-shot spectral information for the normalization of data obtained in scientific experiments and optimization of the accelerator operation parameters. We have demonstrated these capabilities of the setup at the Linac Coherent Light Source, in self-amplified spontaneous emission mode at full energy of >1 mJ with a 120 Hz repetition rate, obtaining a resolving power of Ε/δΕ > 3 × 104. In conclusion, the device was also used to monitor the effects of pulse duration down to 8 fs by analysis of the spectral spike width.

  3. High-resolution neutron diffraction study of CuNCN: New evidence of structure anomalies at low temperature

    SciTech Connect (OSTI)

    Jacobs, Philipp; Houben, Andreas; Dronskowski, Richard; Tchougreff, Andrei L.; Lomonosov Moscow State University, Department of Chemistry and Poncelet Laboratory of Mathematics in Interaction with Physics and Informatics, Independent University of Moscow, Moscow Center for Continuous Mathematical Education, Bolshoi Vlasevsky Per. 11, 119002 Moscow

    2013-12-14

    Copper carbodiimide (CuNCN) is the nitrogen-containing analogue of cupric oxide. Based on high-resolution neutron-diffraction data, CuNCN's lattice parameters are derived as a function of the temperature. In accordance with a recent synchrotron study, a clear trend in the cell parameter a is observed accompanying the changing magnetic behavior. With decreasing temperature, a slowly decreases to a minimum at ?100 K after which it rises again. The same trendalbeit more pronouncedis observed for the c lattice parameter at ?35 K. The herein presented neutron powder-diffraction data also support the conjectured sequence of transitions from the high-temperature one-dimensional resonating valence-bond (RVB) state to a transient two-dimensional RVB state and eventually, at lowest temperatures, into another two-dimensional RVB state, presumably the ground state.

  4. Design and Nuclear-Safety Related Simulations of Bare-Pellet Test Irradiations for the Production of Pu-238 in the High Flux Isotope Reactor using COMSOL

    SciTech Connect (OSTI)

    Freels, James D; Jain, Prashant K; Hobbs, Randy W

    2012-01-01

    The Oak Ridge National Laboratory (ORNL)is developing technology to produce plutonium-238 for the National Aeronautics and Space Administration (NASA) as a power source material for powering vehicles while in deep-space[1]. The High Flux Isotope Reactor (HFIR) of ORNL has been utilized to perform test irradiations of incapsulated neptunium oxide (NpO2) and aluminum powder bare pellets for purposes of understanding the performance of the pellets during irradiation[2]. Post irradiation examinations (PIE) are currently underway to assess the effect of temperature, thermal expansion, swelling due to gas production, fission products, and other phenomena

  5. Spatially resolved high-resolution x-ray spectroscopy of high-current plasma-focus discharges

    SciTech Connect (OSTI)

    ZajaPc, S.; Rzadkiewicz, J.; Scholz, M.; Paduch, M.; Zielinska, E.; Rosmej, O.; Yongtao, Zhao; Gojska, A.

    2010-10-15

    Soft x-ray emission from a Mather-type plasma-focus device (PF-1000) operated at {approx}400 kJ was measured. The high density and temperature plasma were generated by the discharge in the deuterium-argon gas mixture in the modified (high-current) plasma-focus configuration. A spherically bent mica crystal spectrograph viewing the axial output of the pinch region was used to measure the x-ray spectra. Spatially resolved spectra including the characteristic x-ray lines of highly ionized Ar and continua were recorded by means of an x-ray film. The x-ray emission of PF-1000 device was studied at different areas of the pinch.

  6. Combinatorial Screening of Advanced Scintillators for High Resolution X-ray Detectors

    SciTech Connect (OSTI)

    Cheng, Shifan; Tao, Dejie; Lynch, Michael; Yuan, Xianglong; Li, Yiqun

    2008-05-12

    The lack of efficient scintillators is a major problem for developing powerful x-ray detectors that are widely used in homeland security, industrial and scientific research. Intematix has developed and applied a high throughput screening process and corresponding crystal growth technology to significantly speed up the discovery process for new efficient scintillators. As a result, Intematix has invented and fabricated three new scintillators both in powder and bulk forms, which possess promising properties such as better radiation hardness and better matching for silicon diode.

  7. Reconstruction of a high-resolution late holocene arctic paleoclimate record from Colville River delta sediments.

    SciTech Connect (OSTI)

    Schreiner, Kathryn Melissa; Lowry, Thomas Stephen

    2013-10-01

    This work was partially supported by the Sandia National Laboratories,Laboratory Directed Research and Development' (LDRD) fellowship program in conjunction with Texas A&M University (TAMU). The research described herein is the work of Kathryn M. Schreiner (Katie') and her advisor, Thomas S. Bianchi and represents a concise description of Katie's dissertation that was submitted to the TAMU Office of Graduate Studies in May 2013 in partial fulfillment of her doctorate of philosophy degree. High Arctic permafrost soils contain a massive amount of organic carbon, accounting for twice as much carbon as what is currently stored as carbon dioxide in the atmosphere. However, with current warming trends this sink is in danger of thawing and potentially releasing large amounts of carbon as both carbon dioxide and methane into the atmosphere. It is difficult to make predictions about the future of this sink without knowing how it has reacted to past temperature and climate changes. This project investigated long term, fine scale particulate organic carbon (POC) delivery by the high-Arctic Colville River into Simpson's Lagoon in the near-shore Beaufort Sea. Modern POC was determined to be a mixture of three sources (riverine soils, coastal erosion, and marine). Downcore POC measurements were performed in a core close to the Colville River output and a core close to intense coastal erosion. Inputs of the three major sources were found to vary throughout the last two millennia, and in the Colville River core covary significantly with Alaskan temperature reconstructions.

  8. Learning Scene Categories from High Resolution Satellite Image for Aerial Video Analysis

    SciTech Connect (OSTI)

    Cheriyadat, Anil M

    2011-01-01

    Automatic scene categorization can benefit various aerial video processing applications. This paper addresses the problem of predicting the scene category from aerial video frames using a prior model learned from satellite imagery. We show that local and global features in the form of line statistics and 2-D power spectrum parameters respectively can characterize the aerial scene well. The line feature statistics and spatial frequency parameters are useful cues to distinguish between different urban scene categories. We learn the scene prediction model from highresolution satellite imagery to test the model on the Columbus Surrogate Unmanned Aerial Vehicle (CSUAV) dataset ollected by high-altitude wide area UAV sensor platform. e compare the proposed features with the popular Scale nvariant Feature Transform (SIFT) features. Our experimental results show that proposed approach outperforms te SIFT model when the training and testing are conducted n disparate data sources.

  9. A HIGH-RESOLUTION SPECTROSCOPIC SEARCH FOR THE REMAINING DONOR FOR TYCHO'S SUPERNOVA

    SciTech Connect (OSTI)

    Kerzendorf, Wolfgang E.; Yong, David; Schmidt, Brian P.; Murphy, Simon J.; Bessell, Michael S.; Simon, Joshua D.; Jeffery, C. Simon; Anderson, Jay; Podsiadlowski, Philipp; Gal-Yam, Avishay; Silverman, Jeffrey M.; Filippenko, Alexei V.; Nomoto, Ken'ichi; Venn, Kim A.; Foley, Ryan J.

    2013-09-10

    In this paper, we report on our analysis using Hubble Space Telescope astrometry and Keck-I HIRES spectroscopy of the central six stars of Tycho's supernova remnant (SN 1572). With these data, we measured the proper motions, radial velocities, rotational velocities, and chemical abundances of these objects. Regarding the chemical abundances, we do not confirm the unusually high [Ni/Fe] ratio previously reported for Tycho-G. Rather, we find that for all metrics in all stars, none exhibit the characteristics expected from traditional Type Ia supernova single-degenerate-scenario calculations. The only possible exception is Tycho-B, a rare, metal-poor A-type star; however, we are unable to find a suitable scenario for it. Thus, we suggest that SN 1572 cannot be explained by the standard single-degenerate model.

  10. Applications of high resolution NMR to geochemistry: crystalline, glass, and molten silicates

    SciTech Connect (OSTI)

    Schneider, E.

    1985-11-01

    The nuclear spin interactions and the associated quantum mechanical dynamics which are present in solid state NMR are introduced. A brief overview of aluminosilicate structure is presented and crystalline structure is then reviewed, with emphasis on the contributions made by /sup 29/Si NMR spectroscopy. The local structure of glass aluminosilicates as observed by NMR, is presented with analysis of the information content of /sup 29/Si spectra. A high-temperature (to 1300/sup 0/C) NMR spectroscopic investigation of the local environment and dynamics of molecular motion in molten aluminosilicates is described. A comparison is made of silicate liquid, glass, and crystalline local structure. The atomic and molecular motions present in a melt are investigated through relaxation time (T/sub 1/ and T/sub 2/) measurements as a function of composition and temperature for /sup 23/Na and /sup 29/Si.

  11. TU-F-BRE-04: Development of a High-Resolution EPID Based Dosimetry Strategy for Radiosurgery QA

    SciTech Connect (OSTI)

    Han, B; Ding, A; Xing, L; Wang, L

    2014-06-15

    Purpose: To systematically investigate a high spatial-resolution (0.2mm) electronic portal imaging device (EPID) for CyberKnife (CK) based radiosurgery system quality assurance (QA). Methods: An EPID-based dosimetric measurement technique is applied to CK output measurement and field size verification. A Monte Carlo (MC) simulated pixel-to-pixel EPID response specific to CK is used to convert a raw EPID-measured image of a radiosurgery field into water-based dose distribution. The output factors are measured using EPID for radiosurgery fields formed by fixed and variable aperture (Iris) cones. Circular fields of 5, 7.5, 10, 15, 30 and 60mm diameters are measured and compared with diode measurements. The equivalent diameters are determined by analyzing the area received dose greater than half maximum. Results: For both fixed and Iris cones, the EPID measured output factors of circular fields of 5mm to 60mm diameters are in good agreement with the radiosurgery diode measurements. The mean output differences are 1.0% and 1.5% for fixed and Iris cone respectively. The max differences are 2.2% for the 15mm fixed cone, and 1.8% for the 10mm Iris field. The equivalent diameters derived from the EPID measurements are in good agreement comparing to the water scan result with mean differences of 0.210.09mm and 0.020.22mm for fixed and Iris cone, respectively. The high detector density EPID is able to measure the whole radiation field and identify the field edge and center. Therefore, there is no need to align the detector center perfectly at field center and the setup time is greatly reduced for QA. Conclusion: The high spatial-resolution EPID is proved to be an accurate and efficient dosimetric tool for radiosurgery QA and especially useful in Cyberknife QA for variable aperture collimators.

  12. Short range micro-power impulse radar with high resolution swept range gate with damped transmit and receive cavities

    DOE Patents [OSTI]

    McEwan, T.E.

    1998-06-30

    A radar range finder and hidden object locator is based on ultra-wide band radar with a high resolution swept range gate. The device generates an equivalent time amplitude scan with atypical range of 4 inches to 20 feet, and an analog range resolution as limited by a jitter of on the order of 0.01 inches. A differential sampling receiver is employed to effectively eliminate ringing and other aberrations induced in the receiver by the near proximity of the transmit antenna, so a background subtraction is not needed, simplifying the circuitry while improving performance. Uses of the invention include a replacement of ultrasound devices for fluid level sensing, automotive radar, such as cruise control and parking assistance, hidden object location, such as stud and rebar finding. Also, this technology can be used when positioned over a highway lane to collect vehicle count and speed data for traffic control. Techniques are used to reduce clutter in the receive signal, such as decoupling the receive and transmit cavities by placing a space between them, using conductive or radiative damping elements on the cavities, and using terminating plates on the sides of the openings. 20 figs.

  13. Short range micro-power impulse radar with high resolution swept range gate with damped transmit and receive cavities

    DOE Patents [OSTI]

    McEwan, Thomas E.

    1998-01-01

    A radar range finder and hidden object locator is based on ultra-wide band radar with a high resolution swept range gate. The device generates an equivalent time amplitude scan with atypical range of 4 inches to 20 feet, and an analog range resolution as limited by a jitter of on the order of 0.01 inches. A differential sampling receiver is employed to effectively eliminate ringing and other aberrations induced in the receiver by the near proximity of the transmit antenna, so a background subtraction is not needed, simplifying the circuitry while improving performance. Uses of the invention include a replacement of ultrasound devices for fluid level sensing, automotive radar, such as cruise control and parking assistance, hidden object location, such as stud and rebar finding. Also, this technology can be used when positioned over a highway lane to collect vehicle count and speed data for traffic control. Techniques are used to reduce clutter in the receive signal, such as decoupling the receive and transmit cavities by placing a space between them, using conductive or radiative damping elements on the cavities, and using terminating plates on the sides of the openings.

  14. Experiments with the High Resolution Kaon Spectrometer at Jlab Hall C and the New Spectroscopy of ^12_Lambda B Hypernuclei

    SciTech Connect (OSTI)

    Tang, Liguang; Chen, Chunhua; Gogami, Toshiyuki; Kawama, Daisuke; Han, Yuncheng; Yuan, Lulin; Matsumura, Akihiko; Okayasu, Yuichi; Seva, Tomislav; Rodriguez, Victor; Baturin, Pavlo; Acha Quimper, Armando; Achenbach, Carsten; Ahmidouch, Abdellah; Albayrak, Ibrahim; Androic, Darko; Asaturyan, Arshak; Asaturyan, Razmik; Ates, Ozgur; Badui, Rafael; Baker, Oliver; Benmokhtar, Fatiha; Boeglin, Werner; Bono, Jason; Bosted, Peter; Brash, Edward; Carter, Philip; Carlini, Roger; Chiba, Atsushi; Christy, Michael; Cole, Leon; Dalton, Mark; Danagoulian, Samuel; Daniel, Aji; De Leo, Raffaele; Dharmawardane, Kahanawita; Doi, Daisuke; Egiyan, Kim; Elaasar, Mostafa; Ent, Rolf; Fenker, Howard; Fujii, Yu; Furic, Miroslav; Gabrielyan, Marianna; Gan, Liping; Garibaldi, Franco; Gaskell, David; Gasparian, Ashot; Gibson, Edward; Gueye, Paul; Hashimoto, Osamu; Honda, D.; Horn, Tanja; Hu, Bitao; Hungerford, Ed; Jayalath, Chandana; Jones, Mark; Johnston, Kathleen; Kalantarians, Narbe; Kanda, Hiroki; Kaneta, M.; Kato, F.; Kato, Seigo; Kawai, Masaharu; Keppel, Cynthia; Khanal, Hari; Kohl, M.; Kramer, Laird; Lan, Kejian; Li, Ya; Habarakada Liyanage, Anusha; Luo, Wei; Mack, David; Maeda, Kazushige; Malace, Simona; Margaryan, Amur; Marikyan, Gagik; Markowitz, Pete; Maruta, Tomofumi; Maruyama, Nayuta; Maxwell, Victor; Millener, David; Miyoshi, Toshinobu; Mkrtchyan, Arthur; Mkrtchyan, Hamlet; Motoba, Toshio; Nagao, Sho; Nakamura, Satoshi; Narayan, Amrendra; Neville, Casey; Niculescu, Gabriel; Niculescu, Maria; Nunez, Angel; Nuruzzaman, nfn; Nomura, Hiroshi; Nonaka, Kenichi; Ohtani, Atsushi; Oyamada, Masamichi; Perez, Naipy; Petkovic, Tomislav; Pochodzalla, J.; Qiu, Xiyu; Randeniya, Kapugodage; Raue, Brian; Reinhold, Joerg; Rivera, R.; Roche, Julie; Samanta, Chhanda; Sato, Yoshinori; Sawatzky, Bradley; Segbefia, Edwin; Schott, Diane; Shichijo, Ayako; Simicevic, Neven; Smith, Gregory; Song, Yushou; Sumihama, Mizuki; Tadevosyan, Vardan; Takahashi, Toshiyuki; Taniya, Naotaka; Tsukada, Kyo; Tvaskis, Vladas; Veilleux, Micah; Vulcan, William; Wells, Steven; Wesselmann, Frank; Wood, Stephen; Yamamoto, Taku; Yan, Chen; Ye, Z.; Yokota, Kosuke; Zhamkochyan, Simon; Zhu, Lingyan

    2014-09-01

    Since the pioneering experiment, E89-009 studying hypernuclear spectroscopy using the $(e,e^{\\prime}K^+)$ reaction was completed, two additional experiments, E01-011 and E05-115, were performed at Jefferson Lab. These later experiments used a modified experimental design, the "Tilt Method", to dramatically suppress the large electromagnetic background, and allowed for a substantial increase in luminosity. Additionally, a new kaon spectrometer, HKS (E01-011), a new electron spectrometer, HES, and a new splitting magnet were added to produce precision, high-resolution hypernuclear spectroscopy. These two experiments, E01-011 and E05-115, resulted in two new data sets, producing sub-MeV energy resolution in the spectra of ${}^{7}_{\\Lambda}\\text{He}$, ${}^{12}_{\\Lambda}\\text{B}$ and ${}^{28}_{\\Lambda} \\text{Al}$ and ${}^{7}_{\\Lambda}\\text{He}$, ${}^{10}_{\\Lambda}\\text{Be}$, ${}^{12}_{\\Lambda}\\text{B}$ and ${}^{52}_{\\Lambda}\\text{V}$. All three experiments obtained a ${}^{12}_{\\Lambda}\\text{B}$, spectrum, which is the most characteristic $p$-shell hypernucleus and is commonly used for calibration. Independent analyses of these different experiments demonstrate excellent consistency and provide the clearest level structure to date of this hypernucleus as produced by the $(e,e^{\\prime}K^+)$ reaction. This paper presents details of these experiments, and the extraction and analysis of the observed ${}^{12}_{\\Lambda}\\text{B}$ spectrum.

  15. High-resolution line-shape spectroscopy during a laser pulse based on Dual-Broad-Band-CARS interferometry

    SciTech Connect (OSTI)

    Vereschagin, Konstantin A; Vereschagin, Alexey K; Smirnov, Valery V; Stelmakh, O M; Fabelinskii, V I; Clauss, W; Klimenko, D N; Oschwald, M E-mail: Al_Vereshchagin@mail.r E-mail: stelmakh@kapella.gpi.r

    2006-07-31

    A high-resolution spectroscopic method is developed for recording Raman spectra of molecular transitions in transient objects during a laser pulse with a resolution of {approx}0.1 cm{sup -1}. The method is based on CARS spectroscopy using a Fabry-Perot interferometer for spectral analysis of the CARS signal and detecting a circular interferometric pattern on a two-dimensional multichannel photodetector. It is shown that the use of the Dual-Broad-Band-CARS configuration to obtain the CARS process provides the efficient averaging of the spectral-amplitude noise of the CARS signal generated by a laser pulse and, in combination with the angular integration of the two-dimensional interference pattern, considerably improves the quality of interferograms. The method was tested upon diagnostics of the transient oxygen-hydrogen flame where information on the shapes of spectral lines of the Q-branch of hydrogen molecules required for measuring temperature was simultaneously obtained and used. (special issue devoted to the 90th anniversary of a.m. prokhorov)

  16. Formation of voids and secondary-phase precipitates in the Fe-16Cr-15Ni-2Mo-1Mn-Ti-Si steel under high-doze neutron irradiation and during post-irradiation annealing

    SciTech Connect (OSTI)

    Portnykh, I. A. Kozlov, A. V.; Shcherbakov, E. N.; Asiptsov, O. I.

    2009-12-15

    The effect of high-dose neutron irradiation on the structural changes in Fe-16Cr-15Ni-2Mo-1Mn-Ti-Si austenitic steel have been investigated. Samples irradiated at temperatures of 390, 500, and 600{sup o} to damage doses of 46, 86, and 46 dpa, respectively, were analyzed by electron microscopy and dilatometry. The quantitative characteristics of radiation voids and secondary-phase precipitates formed under neutron irradiation are obtained. Their behavior upon heating to 700{sup o}C and annealing at this temperature for 2 h is studied. It is shown that annealing leads to the dissociation of small voids, which is accompanied by the growth of large ones. The secondary-phase precipitates are partially dissolved upon annealing, and their volume fraction decreases.

  17. Final Technical Report for DE-FG02-06ER15835: Chemical Imaging with 100nm Spatial Resolution: Combining High Resolution Flurosecence Microscopy and Ion Mobility Mass Spectrometry

    SciTech Connect (OSTI)

    Buratto, Steven K.

    2013-09-03

    We have combined, in a single instrument, high spatial resolution optical microscopy with the chemical specificity and conformational selectivity of ion mobility mass spectrometry. We discuss the design and construction of this apparatus as well as our efforts in applying this technique to thin films of molecular semiconductor materials.

  18. Single-shot high-resolution characterization of optical pulses by temporal phase diversity

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Dorrer, C.; Waxer, L. J.; Kalb, A.; Hill, E. M.; Bromage, J.

    2015-01-01

    The concept of temporal phase diversity is proposed and applied to the temporal characterization of optical pulses. The experimental trace is composed of the measured power of a plurality of ancillary optical pulses derived from the pulse under test by adding known amounts of chromatic dispersion. The spectral phase of the pulse under test is retrieved by minimizing the error between the experimental trace and a trace calculated from the optical spectrum using the known diagnostic parameters. An assembly composed of splitters and dispersive delay fibers has been used to generate 64 ancillary pulses whose instantaneous power can be detectedmorein a single shot with a high-bandwidth photodiode and oscilloscope. Pulse-shape reconstruction for pulses shorter than the photodetection impulse response has been demonstrated.The diagnostic is experimentally shown to accurately characterize pulses from a chirped-pulseamplification system when its stretcher is detuned from the position for optimal recompression. Various investigations of the performance with respect to the number of ancillary pulses and the range of chromatic dispersion generated in the diagnostic are presented.less

  19. The multiplicity of massive stars: A high angular resolution survey with the HST fine guidance sensor

    SciTech Connect (OSTI)

    Aldoretta, E. J.; Gies, D. R.; Henry, T. J.; Jao, W.-C.; Norris, R. P. E-mail: gies@chara.gsu.edu E-mail: jao@chara.gsu.edu; and others

    2015-01-01

    We present the results of an all-sky survey made with the Fine Guidance Sensor on the Hubble Space Telescope to search for angularly resolved binary systems among massive stars. The sample of 224 stars is comprised mainly of Galactic O- and B-type stars and luminous blue variables, plus a few luminous stars in the Large Magellanic Cloud. The FGS TRANS mode observations are sensitive to the detection of companions with an angular separation between 0.″01 and 1.″0 and brighter than △m=5. The FGS observations resolved 52 binary and 6 triple star systems and detected partially resolved binaries in 7 additional targets (43 of these are new detections). These numbers yield a companion detection frequency of 29% for the FGS survey. We also gathered literature results on the numbers of close spectroscopic binaries and wider astrometric binaries among the sample, and we present estimates of the frequency of multiple systems and the companion frequency for subsets of stars residing in clusters and associations, field stars, and runaway stars. These results confirm the high multiplicity fraction, especially among massive stars in clusters and associations. We show that the period distribution is approximately flat in increments of logP. We identify a number of systems of potential interest for long-term orbital determinations, and we note the importance of some of these companions for the interpretation of the radial velocities and light curves of close binaries that have third companions.

  20. A semiparametric spatio-temporal model for solar irradiance data

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Patrick, Joshua D.; Harvill, Jane L.; Hansen, Clifford W.

    2016-03-01

    Here, we evaluate semiparametric spatio-temporal models for global horizontal irradiance at high spatial and temporal resolution. These models represent the spatial domain as a lattice and are capable of predicting irradiance at lattice points, given data measured at other lattice points. Using data from a 1.2 MW PV plant located in Lanai, Hawaii, we show that a semiparametric model can be more accurate than simple interpolation between sensor locations. We investigate spatio-temporal models with separable and nonseparable covariance structures and find no evidence to support assuming a separable covariance structure. These results indicate a promising approach for modeling irradiance atmore » high spatial resolution consistent with available ground-based measurements. Moreover, this kind of modeling may find application in design, valuation, and operation of fleets of utility-scale photovoltaic power systems.« less

  1. High-resolution transmission electron microscopy study of carbon deposited on the NiO/MgO solid solution catalysts

    SciTech Connect (OSTI)

    Hu, Y.H.; Ruckenstein, E.

    1999-05-15

    The carbon deposition due to the CH{sub 4} decomposition at 790 C over NiO/MgO catalysts was investigated by high-resolution transmission electron microscopy. While no deposits could be detected over the catalysts with a NiO content smaller than 9.1 wt%, they were detected over the catalysts with NiO contents of 23 and 50 wt%. The carbon deposits are composed of platelets located at distances of about 0.34 nm, corresponding to the graphitic carbon. Various structures of the deposited carbon were observed: (a) carbon consisting of platelets parallel to the surface of the particle, which covers a catalyst particle, (b) nanotubes composed of platelets parallel to their axis, and (c) carbon vortexes consisting of platelets parallel to their axis.

  2. Two-beam ultrabroadband coherent anti-Stokes Raman spectroscopy for high resolution gas-phase multiplex imaging

    SciTech Connect (OSTI)

    Bohlin, Alexis; Kliewer, Christopher J.

    2014-01-20

    We propose and develop a method for wideband coherent anti-Stokes Raman spectroscopy (CARS) in the gas phase and demonstrate the single-shot measurement of N{sub 2}, H{sub 2}, CO{sub 2}, O{sub 2}, and CH{sub 4}. Pure-rotational and vibrational O-, Q-, and S- branch spectra are collected simultaneously, with high spectral and spatial resolution, and within a single-laser-shot. The relative intensity of the rotational and vibrational signals can be tuned arbitrarily using polarization techniques. The ultrashort 7 fs pump and Stokes pulses are automatically overlapped temporally and spatially using a two-beam CARS technique, and the crossed probe beam allows for excellent spatial sectioning of the probed location.

  3. Vibronic fine structure in high-resolution x-ray absorption spectra from ion-bombarded boron nitride nanotubes

    SciTech Connect (OSTI)

    Petravic, Mladen; Peter, Robert; Varasanec, Marijana; Li Luhua; Chen Ying; Cowie, Bruce C. C.

    2013-05-15

    The authors have applied high-resolution near-edge x-ray absorption fine structure measurements around the nitrogen K-edge to study the effects of ion-bombardment on near-surface properties of boron nitride nanotubes. A notable difference has been observed between surface sensitive partial electron yield (PEY) and bulk sensitive total electron yield (TEY) fine-structure measurements. The authors assign the PEY fine structure to the coupling of excited molecular vibrational modes to electronic transitions in NO molecules trapped just below the surface. Oxidation resistance of the boron nitride nanotubes is significantly reduced by low energy ion bombardment, as broken B-N bonds are replaced by N-O bonds involving oxygen present in the surface region. In contrast to the PEY spectra, the bulk sensitive TEY measurements on as-grown samples do not exhibit any fine structure while the ion-bombarded samples show a clear vibronic signature of molecular nitrogen.

  4. DENSITY WAVES EXCITED BY LOW-MASS PLANETS IN PROTOPLANETARY DISKS. II. HIGH-RESOLUTION SIMULATIONS OF THE NONLINEAR REGIME

    SciTech Connect (OSTI)

    Dong Ruobing; Stone, James M.; Rafikov, Roman R. E-mail: rrr@astro.princeton.edu

    2011-11-01

    We investigate numerically the propagation of density waves excited by a low-mass planet in a protoplanetary disk in the nonlinear regime, using two-dimensional local shearing box simulations with the grid-based code Athena at high spatial resolution (256 grid points per scale height h). The nonlinear evolution results in the wave steepening into a shock, causing damping and angular momentum transfer to the disk. On long timescales this leads to spatial redistribution of the disk density, causing migration feedback and potentially resulting in gap opening. Previous numerical studies concentrated on exploring these secondary phenomena as probes of the nonlinear wave evolution. Here we focus on exploring the evolution of the basic wave properties, such as its density profile evolution, shock formation, and post-shock wave behavior, and provide comparison with analytical theory. The generation of potential vorticity at the shock is computed analytically and is subsequently verified by simulations and used to pinpoint the shock location. We confirm the theoretical relation between the shocking length and the planet mass (including the effect of the equation of state), and the post-shock decay of the angular momentum flux carried by the wave. The post-shock evolution of the wave profile is explored, and we quantitatively confirm its convergence to the theoretically expected N-wave shape. The accuracy of various numerical algorithms used to compute the nonlinear wave evolution is also investigated: we find that higher order spatial reconstruction and high resolution are crucial for capturing the shock formation correctly.

  5. SU-E-I-40: New Method for Measurement of Task-Specific, High-Resolution Detector System Performance

    SciTech Connect (OSTI)

    Loughran, B; Singh, V; Jain, A; Bednarek, D; Rudin, S

    2014-06-01

    Purpose: Although generalized linear system analytic metrics such as GMTF and GDQE can evaluate performance of the whole imaging system including detector, scatter and focal-spot, a simplified task-specific measured metric may help to better compare detector systems. Methods: Low quantum-noise images of a neuro-vascular stent with a modified ANSI head phantom were obtained from the average of many exposures taken with the high-resolution Micro-Angiographic Fluoroscope (MAF) and with a Flat Panel Detector (FPD). The square of the Fourier Transform of each averaged image, equivalent to the measured product of the system GMTF and the object function in spatial-frequency space, was then divided by the normalized noise power spectra (NNPS) for each respective system to obtain a task-specific generalized signal-to-noise ratio. A generalized measured relative object detectability (GM-ROD) was obtained by taking the ratio of the integral of the resulting expressions for each detector system to give an overall metric that enables a realistic systems comparison for the given detection task. Results: The GM-ROD provides comparison of relative performance of detector systems from actual measurements of the object function as imaged by those detector systems. This metric includes noise correlations and spatial frequencies relevant to the specific object. Additionally, the integration bounds for the GM-ROD can be selected to emphasis the higher frequency band of each detector if high-resolution image details are to be evaluated. Examples of this new metric are discussed with a comparison of the MAF to the FPD for neuro-vascular interventional imaging. Conclusion: The GM-ROD is a new direct-measured task-specific metric that can provide clinically relevant comparison of the relative performance of imaging systems. Supported by NIH Grant: 2R01EB002873 and an equipment grant from Toshiba Medical Systems Corporation.

  6. High-resolution x-ray diffraction study of the heavy-fermion compound YbBiPt

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ueland, B. G.; Iowa State Univ., Ames, IA; Saunders, S. M.; Iowa State Univ., Ames, IA; Bud'ko, S. L.; Iowa State Univ., Ames, IA; Schmiedeshoff, G. M.; Canfield, P. C.; Iowa State Univ., Ames, IA; Kreyssig, A.; et al

    2015-11-30

    In this study, YbBiPt is a heavy-fermion compound possessing significant short-range antiferromagnetic correlations below a temperature of T*=0.7K, fragile antiferromagnetic order below TN = 0.4K, a Kondo temperature of TK ≈ 1K, and crystalline-electric-field splitting on the order of E/kB = 1 – 10K. Whereas the compound has a face-centered-cubic lattice at ambient temperature, certain experimental data, particularly those from studies aimed at determining its crystalline-electric-field scheme, suggest that the lattice distorts at lower temperature. Here, we present results from high-resolution, high-energy x-ray diffraction experiments which show that, within our experimental resolution of ≈ 6 – 10 × 10–5 Å,more » no structural phase transition occurs between T = 1.5 and 50 K. In combination with results from dilatometry measurements, we further show that the compound's thermal expansion has a minimum at ≈ 18 K and a region of negative thermal expansion for 9 ≲ T ≲ 18 K. Despite diffraction patterns taken at 1.6 K which indicate that the lattice is face-centered cubic and that the Yb resides on a crystallographic site with cubic point symmetry, we demonstrate that the linear thermal expansion may be modeled using crystalline-electric-field level schemes appropriate for Yb3+ residing on a site with either cubic or less than cubic point symmetry.« less

  7. High resolution soft x-ray spectroscopy of low Z K-shell emission from laser-produced plasmas

    SciTech Connect (OSTI)

    Dunn, J; Magee, E W; Shepherd, R; Chen, H; Hansen, S B; Moon, S J; Brown, G V; Gu, M; Beiersdorfer, P; Purvis, M A

    2008-05-21

    A large radius, R = 44.3 m, High Resolution Grating Spectrometer (HRGS) with 2400 line/mm variable line spacing has been designed for laser-produced plasma experiments conducted at the Lawrence Livermore National Laboratory Jupiter Laser Facility. The instrument has been run with a low-noise, charge-coupled device detector to record high signal-to-noise spectra in the 10-50 {angstrom} wavelength range. The instrument can be run with a 10-20 {micro}m wide slit to achieve the best spectral resolving power, approaching 1000 and similar to crystal spectrometers at 12-20 {angstrom}, or in slitless operation with a small symmetrical emission source. We describe preliminary spectra emitted from various H-like and He-like low Z ion plasmas heated by 100-500 ps (FWHM), 527 nm wavelength laser pulses. This instrument can be developed as a useful spectroscopy platform relevant to laboratory-based astrophysics as well as high energy density plasma studies.

  8. Solids irradiator

    DOE Patents [OSTI]

    Morris, Marvin E.; Pierce, Jim D.; Whitfield, Willis J.

    1979-01-01

    A novel facility for irradiation of solids embodying pathogens wherein solids are conveyed through an irradiation chamber in individual containers of an endless conveyor.

  9. Catalytic Mechanism of Perosamine N-Acetyltransferase Revealed by High-Resolution X-ray Crystallographic Studies and Kinetic Analyses

    SciTech Connect (OSTI)

    Thoden, James B.; Reinhardt, Laurie A.; Cook, Paul D.; Menden, Patrick; Cleland, W.W.; Holden, Hazel M.

    2012-09-17

    N-Acetylperosamine is an unusual dideoxysugar found in the O-antigens of some Gram-negative bacteria, including the pathogenic Escherichia coli strain O157:H7. The last step in its biosynthesis is catalyzed by PerB, an N-acetyltransferase belonging to the left-handed {beta}-helix superfamily of proteins. Here we describe a combined structural and functional investigation of PerB from Caulobacter crescentus. For this study, three structures were determined to 1.0 {angstrom} resolution or better: the enzyme in complex with CoA and GDP-perosamine, the protein with bound CoA and GDP-N-acetylperosamine, and the enzyme containing a tetrahedral transition state mimic bound in the active site. Each subunit of the trimeric enzyme folds into two distinct regions. The N-terminal domain is globular and dominated by a six-stranded mainly parallel {beta}-sheet. It provides most of the interactions between the protein and GDP-perosamine. The C-terminal domain consists of a left-handed {beta}-helix, which has nearly seven turns. This region provides the scaffold for CoA binding. On the basis of these high-resolution structures, site-directed mutant proteins were constructed to test the roles of His 141 and Asp 142 in the catalytic mechanism. Kinetic data and pH-rate profiles are indicative of His 141 serving as a general base. In addition, the backbone amide group of Gly 159 provides an oxyanion hole for stabilization of the tetrahedral transition state. The pH-rate profiles are also consistent with the GDP-linked amino sugar substrate entering the active site in its unprotonated form. Finally, for this investigation, we show that PerB can accept GDP-3-deoxyperosamine as an alternative substrate, thus representing the production of a novel trideoxysugar.

  10. OZSPEC-2: An improved broadband high-resolution elliptical crystal x-ray spectrometer for high-energy density physics experiments (invited)

    SciTech Connect (OSTI)

    Heeter, R. F.; Anderson, S. G.; Booth, R.; Brown, G. V.; Emig, J.; Fulkerson, S.; McCarville, T.; Norman, D.; Schneider, M. B.; Young, B. K. F.

    2008-10-15

    A novel time, space, and energy-resolved x-ray spectrometer has been developed which produces, in a single snapshot, a broadband and relatively calibrated spectrum of the x-ray emission from a high-energy density laboratory plasma. The opacity zipper spectrometer (OZSPEC-1) records a nearly continuous spectrum for x-ray energies from 240 to 5800 eV in a single shot. The second-generation OZSPEC-2, detailed in this work, records fully continuous spectra on a single shot from any two of these three bands: 270-650, 660-1580, and 1960-4720 eV. These instruments thus record thermal and line radiation from a wide range of plasmas. These instruments' single-shot bandwidth is unmatched in a time-gated spectrometer; conversely, other broadband instruments are either time-integrated (using crystals or gratings), lack spectral resolution (diode arrays), or cover a lower energy band (gratings). The OZSPECs are based on the zipper detector, a large-format (100x35 mm) gated microchannel plate detector, with spectra dispersed along the 100 mm dimension. OZSPEC-1 and -2 both use elliptically bent crystals of OHM, RAP, and/or PET. Individual spectra are gated in 100 ps. OZSPEC-2 provides one-dimensional spatial imaging with 30-50 {mu}m resolution over a 1500 {mu}m field of view at the source. The elliptical crystal design yields broad spectral coverage with resolution E/{delta}E>500, strong rejection of hard x-ray backgrounds, and negligible source broadening for extended sources. Near-term applications include plasma opacity measurements, detailed spectra of inertial fusion Hohlraums, and laboratory astrophysics experiments.

  11. Insights into Stress Corrosion Cracking Mechanisms from High-Resolution Measurements of Crack-Tip Structures and Compositions

    SciTech Connect (OSTI)

    Bruemmer, Stephen M.; Thomas, Larry E.

    2004-11-25

    Recent results are presented demonstrating the application of cross-sectional analytical transmission electron microscopy (ATEM) to corrosion and cracking in high-temperature, light-water-reactor (LWR) environments. Structural, compositional and crystallographic characterizations of crack-tip oxide films and interfaces at near-atomic resolutions reveal evidence for unexpected local environments, corrosion reactions and local changes in the alloy metallurgy. Information obtained by high-resolution imaging and analysis indicates the corrosion processes that occur during crack advance, and provides insights into the mechanisms controlling environmental degradation. Examples of intergranular stress-corrosion cracking (IGSCC) in Ni- and Fe-base stainless alloys are reviewed to illustrate the value of this approach. Comparisons are made between crack characteristics found in components removed from long-term LWR service and those in materials tested under well-controlled laboratory conditions. Key insights into crack corrosion environments and advance mechanisms are established for Ni-base alloy 600 in steam-generator, secondary-water environments. Solution impurities such as Pb are often found in high concentrations at leading-edge reaction zones within porous, corrosion-product films. The presence of nanometer-wide, deeply attacked grain boundaries off the main SCC cracks (without evidence for plastic deformation) is believed to indicate a major role of active-path IG corrosion in the SCC process. Similar characteristics are identified for alloy 600 cracking in primary water. This suggests that Pb may only accelerate the IG corrosion process and not alter the basic degradation mechanism. Quite different IGSCC crack and crack-tip characteristics have been discovered for Fe-base stainless steels in LWR environments. More classic SCC crack and crack-tip structures have been seen in non-sensitized materials with wall oxide films extending to the tips. Cracked components after long-term service exposure show distinct differences in the crack-tip region microchemistry versus shorter-term laboratory SCC samples. Compositional changes in the metal ahead of many crack tips suggest that selective dissolution/oxidation occurs at the leading edge of degradation. Results for specific samples are used to demonstrate the ability of cross-sectional ATEM to reveal new details of crack-tip structures that cannot be detected by other methods.

  12. High-resolution single-shot spectral monitoring of hard x-ray free-electron laser radiation

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Makita, M.; Karvinen, P.; Zhu, D.; Juranic, P. N.; Grünert, J.; Cartier, S.; Jungmann-Smith, J. H.; Lemke, H. T.; Mozzanica, A.; Nelson, S.; et al

    2015-10-16

    We have developed an on-line spectrometer for hard x-ray free-electron laser (XFEL) radiation based on a nanostructured diamond diffraction grating and a bent crystal analyzer. Our method provides high spectral resolution, interferes negligibly with the XFEL beam, and can withstand the intense hard x-ray pulses at high repetition rates of >100 Hz. The spectrometer is capable of providing shot-to-shot spectral information for the normalization of data obtained in scientific experiments and optimization of the accelerator operation parameters. We have demonstrated these capabilities of the setup at the Linac Coherent Light Source, in self-amplified spontaneous emission mode at full energy ofmore » >1 mJ with a 120 Hz repetition rate, obtaining a resolving power of Ε/δΕ > 3 × 104. In conclusion, the device was also used to monitor the effects of pulse duration down to 8 fs by analysis of the spectral spike width.« less

  13. Ultrasonic Transducer Irradiation Test Results

    SciTech Connect (OSTI)

    Daw, Joshua; Palmer, Joe; Ramuhalli, Pradeep; Keller, Paul; Montgomery, Robert; Chien, Hual-Te; Kohse, Gordon; Tittmann, Bernhard; Reinhardt, Brian; Rempe, Joy

    2015-02-01

    Ultrasonic technologies offer the potential for high-accuracy and -resolution in-pile measurement of a range of parameters, including geometry changes, temperature, crack initiation and growth, gas pressure and composition, and microstructural changes. Many Department of Energy-Office of Nuclear Energy (DOE-NE) programs are exploring the use of ultrasonic technologies to provide enhanced sensors for in-pile instrumentation during irradiation testing. For example, the ability of small diameter ultrasonic thermometers (UTs) to provide a temperature profile in candidate metallic and oxide fuel would provide much needed data for validating new fuel performance models. Other ongoing efforts include an ultrasonic technique to detect morphology changes (such as crack initiation and growth) and acoustic techniques to evaluate fission gas composition and pressure. These efforts are limited by the lack of identified ultrasonic transducer materials capable of long term performance under irradiation test conditions. For this reason, the Pennsylvania State University (PSU) was awarded an ATR NSUF project to evaluate the performance of promising magnetostrictive and piezoelectric transducers in the Massachusetts Institute of Technology Research Reactor (MITR) up to a fast fluence of at least 1021 n/cm2. The goal of this research is to characterize and demonstrate magnetostrictive and piezoelectric transducer operation during irradiation, enabling the development of novel radiation-tolerant ultrasonic sensors for use in Material Testing Reactors (MTRs). As such, this test is an instrumented lead test and real-time transducer performance data is collected along with temperature and neutron and gamma flux data. The current work bridges the gap between proven out-of-pile ultrasonic techniques and in-pile deployment of ultrasonic sensors by acquiring the data necessary to demonstrate the performance of ultrasonic transducers. To date, one piezoelectric transducer and two magnetostrictive transducers have demonstrated reliable operation under irradiation. The irradiation is ongoing.

  14. Insights into Stress Corrosion Cracking Mechanisms from High-Resolution Measurements of Crack-Tip Structures and Compositions

    SciTech Connect (OSTI)

    Bruemmer, Stephen M.; Thomas, Larry E.

    2010-04-05

    The fundamental basis for mechanistic understanding and modeling of SCC remains in question for many systems. Specific mechanisms controlling SCC can vary with changes in alloy characteristics, applied/residual stress or environmental conditions. The local crack electrochemistry, crack-tip mechanics and material metallurgy are the main factors controlling crack growth. These localized properties are difficult or impossible to measure in active cracks. Nevertheless, it is essential to quantitatively interrogate these crack-tip conditions if mechanistic understanding is to be obtained. A major recent advance has been the ability to investigate SCC cracks and crack tips using high-resolution ATEM techniques. ATEM enables the characterization of SCC cracks including trapped tip solution chemistries, corrosion product/film compositions and structures, and elemental composition gradients and defect microstructures along the crack walls and at the crack tip. A wide variety of methods for imaging and analyses at resolutions down to the atomic level can be used to examine the crack and corrosion film characteristics. Surface films and reaction layers have been examined by cross-sectional TEM techniques, but little work had been conducted on environmentally induced internal cracks until that of Lewis and co-workers [1-3] and the current authors [4-17]. This capability combined with modern ATEM techniques has enabled exciting new insights into corrosion processes occurring at buried interfaces and is being used to identify mechanisms controlling IGSCC in boiling water reactor (BWR) and pressurized water reactor (PWR) components. The objective of this paper is to summarize certain results focused on IGSCC of Fe- base and Ni-base stainless alloys in high-temperature water environments. Representative crack-tip examples will be shown to illustrate specific aspects that are characteristic of SCC in the material/environment combinations. Differences and similarities in crack-tip structures- chemistries will be highlighted comparing Fe-base 316/304SS to Ni-base alloy 600/182 and for tests in oxidizing versus hydrogenated water environments.

  15. Local electronic effects and irradiation resistance in high-entropy alloys

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Egami, Takeshi; Stocks, George Malcolm; Nicholson, Don; Khorgolkhuu, Od; Ojha, Madhusudan

    2015-01-01

    High-entropy alloys are multicomponent solid solutions in which various elements with different chemistries and sizes occupy the same crystallographic lattice sites. Thus, none of the atoms perfectly fit the lattice site, giving rise to considerable local lattice distortions and atomic-level stresses. These characteristics can be beneficial for performance under both radiation and in a high-temperature environment, making them attractive candidates as nuclear materials. We discuss electronic origin of the atomic-level stresses based upon first-principles calculations using a density functional theory approach.

  16. Applications of high-resolution spatial discretization scheme and Jacobian-free NewtonKrylov method in two-phase flow problems

    SciTech Connect (OSTI)

    Zou, Ling; Zhao, Haihua; Zhang, Hongbin

    2015-09-01

    The majority of the existing reactor system analysis codes were developed using low-order numerical schemes in both space and time. In many nuclear thermalhydraulics applications, it is desirable to use higher-order numerical schemes to reduce numerical errors. High-resolution spatial discretization schemes provide high order spatial accuracy in smooth regions and capture sharp spatial discontinuity without nonphysical spatial oscillations. In this work, we adapted an existing high-resolution spatial discretization scheme on staggered grids in two-phase flow applications. Fully implicit time integration schemes were also implemented to reduce numerical errors from operator-splitting types of time integration schemes. The resulting nonlinear system has been successfully solved using the Jacobian-free NewtonKrylov (JFNK) method. The high-resolution spatial discretization and high-order fully implicit time integration numerical schemes were tested and numerically verified for several two-phase test problems, including a two-phase advection problem, a two-phase advection with phase appearance/disappearance problem, and the water faucet problem. Numerical results clearly demonstrated the advantages of using such high-resolution spatial and high-order temporal numerical schemes to significantly reduce numerical diffusion and therefore improve accuracy. Our study also demonstrated that the JFNK method is stable and robust in solving two-phase flow problems, even when phase appearance/disappearance exists.

  17. Chemical Characterization of Crude Petroleum Using Nanospray Desorption Electrospray Ionization Coupled with High-Resolution Mass Spectrometry

    SciTech Connect (OSTI)

    Eckert, Peter A.; Roach, Patrick J.; Laskin, Alexander; Laskin, Julia

    2012-02-07

    Nanospray desorption electrospray ionization (nano-DESI) combined with high-resolution mass spectrometry was used for the first time for the analysis of liquid petroleum crude oil samples. The analysis was performed in both positive and negative ionization modes using three solvents one of which (acetonitrile/toluene mixture) is commonly used in petroleomics studies while two other polar solvents (acetonitrile/water and methanol/water mixtures) are generally not compatible with petroleum characterization using mass spectrometry. The results demonstrate that nano-DESI analysis efficiently ionizes petroleum constituents soluble in a particular solvent. When acetonitrile/toluene is used as a solvent, nano-DESI generates electrospray-like spectra. In contrast, strikingly different spectra were obtained using acetonitrile/water and methanol/water. Comparison with the literature data indicates that these solvents selectively extract water-soluble constituents of the crude oil. Water-soluble compounds are predominantly observed as sodium adducts in nano-DESI spectra indicating that addition of sodium to the solvent may be a viable approach for efficient ionization of water-soluble crude oil constituents. Nano-DESI enables rapid screening of different classes of compounds in crude oil samples using solvents that are rarely used for petroleum characterization.

  18. Concurrent in situ ion irradiation transmission electron microscope

    SciTech Connect (OSTI)

    Hattar, K.; Bufford, D. C.; Buller, D. L.

    2014-08-29

    An in situ ion irradiation transmission electron microscope has been developed and is operational at Sandia National Laboratories. This facility permits high spatial resolution, real time observation of electron transparent samples under ion irradiation, implantation, mechanical loading, corrosive environments, and combinations thereof. This includes the simultaneous implantation of low-energy gas ions (0.830 keV) during high-energy heavy ion irradiation (0.848 MeV). In addition, initial results in polycrystalline gold foils are provided to demonstrate the range of capabilities.

  19. High Spectral Resolution Infrared and Raman Lidar Observations for the ARM Program: Clear and Cloudy Sky Applications

    SciTech Connect (OSTI)

    Henry Revercomb, David Tobin, Robert Knuteson, Lori Borg, Leslie Moy

    2009-06-17

    This grant began with the development of the Atmospheric Emitted Radiance Interferometer (AERI) for ARM. The AERI has provided highly accurate and reliable observations of downwelling spectral radiance (Knuteson et al. 2004a, 2004b) for application to radiative transfer, remote sensing of boundary layer temperature and water vapor, and cloud characterization. One of the major contributions of the ARM program has been its success in improving radiation calculation capabilities for models and remote sensing that evolved from the multi-year, clear-sky spectral radiance comparisons between AERI radiances and line-by-line calculations (Turner et al. 2004). This effort also spurred us to play a central role in improving the accuracy of water vapor measurements, again helping ARM lead the way in the community (Turner et al. 2003a, Revercomb et al. 2003). In order to add high-altitude downlooking AERI-like observations over the ARM sites, we began the development of an airborne AERI instrument that has become known as the Scanning High-resolution Interferometer Sounder (Scanning-HIS). This instrument has become an integral part of the ARM Unmanned Aerospace Vehicle (ARM-UAV) program. It provides both a cross-track mapping view of the earth and an uplooking view from the 12-15 km altitude of the Scaled Composites Proteus aircraft when flown over the ARM sites for IOPs. It has successfully participated in the first two legs of the grand tour of the ARM sites (SGP and NSA), resulting in a very good comparison with AIRS observations in 2002 and in an especially interesting data set from the arctic during the Mixed-Phase Cloud Experiment (M-PACE) in 2004. More specifically, our major achievements for ARM include 1. Development of the Atmospheric Emitted Radiance Interferometer (AERI) to function like a satellite on the ground for ARM, providing a steady stream of accurately calibrated spectral radiances for Science Team clear sky and cloud applications (Knuteson et al. 2004a), 2. Detailed radiometric calibration and characterization of AERI radiances, with uncertainty estimates established from complete error analyses and proven by inter-comparison tests (Knuteson et al. 2004b), 3. AERI data quality assessment and maintenance over the extended time frames needed to support ARM (Dedecker et al., 2005) 4. Key role in the radiative transfer model improvements from the AERI/LBLRTM QME (Turner et al. 2004) and AERI-ER especially from the SHEBA experiment (Tobin et al. 1999), 5. Contributed scientific and programmatic leadership leading to significant water vapor accuracy improvements and uncertainty assessments for the low to mid troposphere (Turner et al. 2003a, Revercomb et al. 2003), 6. Leadership of the ARM assessment of the accuracy of water vapor observations from radiosondes, Raman Lidar and in situ aircraft observations in the upper troposphere and lower stratosphere (Tobin et al. 2002, Ferrare et al. 2004), 7. New techniques for characterizing clouds from AERI (DeSlover et al. 1999, Turner 2003b, Turner et al. 2003b), 8. Initial design and development of the Scanning-HIS aircraft instrument and application to ARM UAV Program missions (Revercomb et al. 2005), and 9. Coordinated efforts leading to the use of ARM observations as a key validation tool for the high resolution Atmospheric IR Sounder on the NASA Aqua platform (Tobin et al. 2005a) 10. Performed ARM site and global clear sky radiative closure studies that shows closure of top-of-atmosphere flux at the level of ~1 W/m2 (Moy et al 2008 and Section 3 of this appendix) 11. Performed studies to characterize SGP site cirrus cloud property retrievals and assess impacts on computed fluxes and heating rate profiles (Borg et al. 2008 and Section 2 of this appendix).

  20. Radiation bronchitis and stenosis secondary to high dose rate endobronchial irradiation

    SciTech Connect (OSTI)

    Speiser, B.L. ); Spratling, L.

    1993-03-15

    The purpose of the study was to describe a new clinical entity observed in follow-up bronchoscopies in patients who were treated with high dose rate and medium dose rate remote afterloading brachytherapy of the tracheobronchial tree. Patients were treated by protocol with medium dose rate, 47 patients receiving 1000 cGy at a 5 mm depth times three fractions, high dose rate 144 patients receiving 1000 cGy at a 10 mm depth for three fractions and high dose rate 151 patients receiving cGy at a 10 mm depth for three fractions followed by bronchoscopy. Incidence of this entity was 9% for the first group, 12% for the second, and 13% for the third group. Reactions were grade 1 consisting of mild inflammatory response with a partial whitish circumferential membrane in an asymptomatic patient; grade 2, thicker complete white circumferential membrane with cough and/or obstructive problems requiring intervention; grade 3, severe inflammatory response with marked membranous exudate and mild fibrotic reaction; and grade 4 a predominant fibrotic reaction with progressive stenosis. Variables associated with a slightly increased incidence of radiation bronchitis and stenosis included: large cell carcinoma histology, curative intent, prior laser photoresection, and/or concurrent external radiation. Survival was the strongest predictor of the reaction. Radiation bronchitis and stenosis is a new clinical entity that must be identified in bronchial brachytherapy patients and treated appropriately. 23 refs., 3 figs., 7 tabs.

  1. Nonlinear photoresponse of field effect transistors terahertz detectors at high irradiation intensities

    SciTech Connect (OSTI)

    But, D. B.; Drexler, C.; Ganichev, S. D.; Sakhno, M. V.; Sizov, F. F.; Dyakonova, N.; Drachenko, O.; Gutin, A.; Knap, W.

    2014-04-28

    Terahertz power dependence of the photoresponse of field effect transistors, operating at frequencies from 0.1 to 3 THz for incident radiation power density up to 100?kW/cm{sup 2} was studied for Si metaloxidesemiconductor field-effect transistors and InGaAs high electron mobility transistors. The photoresponse increased linearly with increasing radiation intensity up to the kW/cm{sup 2} range. Nonlinearity followed by saturation of the photoresponse was observed for all investigated field effect transistors for intensities above several kW/cm{sup 2}. The observed photoresponse nonlinearity is explained by nonlinearity and saturation of the transistor channel current. A theoretical model of terahertz field effect transistor photoresponse at high intensity was developed. The model explains quantitative experimental data both in linear and nonlinear regions. Our results show that dynamic range of field effect transistors is very high and can extend over more than six orders of magnitudes of power densities (from ?0.5 mW/cm{sup 2} to ?5?kW/cm{sup 2})

  2. Two- and three-dimensional ultrananocrystalline diamond (UNCD) structures for a high resolution diamond-based MEMS technology.

    SciTech Connect (OSTI)

    Auciello, O.; Krauss, A. R.; Gruen, D. M.; Busmann, H. G.; Meyer, E. M.; Tucek, J.; Sumant, A.; Jayatissa, A.; Moldovan, N.; Mancini, D. C.; Gardos, M. N.

    2000-01-17

    Silicon is currently the most commonly used material for the fabrication of microelectromechanical systems (MEMS). However, silicon-based MEMS will not be suitable for long-endurance devices involving components rotating at high speed, where friction and wear need to be minimized, components such as 2-D cantilevers that may be subjected to very large flexural displacements, where stiction is a problem, or components that will be exposed to corrosive environments. The mechanical, thermal, chemical, and tribological properties of diamond make it an ideal material for the fabrication of long-endurance MEMS components. Cost-effective fabrication of these components could in principle be achieved by coating Si with diamond films and using conventional lithographic patterning methods in conjunction with e. g. sacrificial Ti or SiO{sub 2} layers. However, diamond coatings grown by conventional chemical vapor deposition (CVD) methods exhibit a coarse-grained structure that prevents high-resolution patterning, or a fine-grained microstructure with a significant amount of intergranular non-diamond carbon. The authors demonstrate here the fabrication of 2-D and 3-D phase-pure ultrananocrystalline diamond (UNCD) MEMS components by coating Si with UNCD films, coupled with lithographic patterning methods involving sacrificial release layers. UNCD films are grown by microwave plasma CVD using C{sub 60}-Ar or CH{sub 4}-Ar gas mixtures, which result in films that have 3--5 nm grain size, are 10--20 times smoother than conventionally grown diamond films, are extremely resistant to corrosive environments, and are predicted to have a brittle fracture strength similar to that of single crystal diamond.

  3. New generation NMR bioreactor coupled with high-resolution NMR spectroscopy leads to novel discoveries in Moorella thermoaceticum metabolic profiles

    SciTech Connect (OSTI)

    Xue, Junfeng; Isern, Nancy G.; Ewing, R James; Liyu, Andrey V.; Sears, Jesse A.; Knapp, Harlan; Iversen, Jens; Sisk, Daniel R.; Ahring, Birgitte K.; Majors, Paul D.

    2014-06-20

    An in-situ nuclear magnetic resonance (NMR) bioreactor was developed and employed to monitor microbial metabolism under batch-growth conditions in real time. We selected Moorella thermoacetica ATCC 49707 as a test case. M. thermoacetica (formerly Clostridium thermoaceticum) is a strictly anaerobic, thermophilic, acetogenic, gram-positive bacterium with potential for industrial production of chemicals. The metabolic profiles of M. thermoacetica were characterized during growth in batch mode on xylose (a component of lignocellulosic biomass) using the new generation NMR bioreactor in combination with high-resolution, high sensitivity NMR (HR-NMR) spectroscopy. In-situ NMR measurements were performed using water-suppressed H-1 NMR spectroscopy at an NMR frequency of 500 MHz, and aliquots of the bioreactor contents were taken for 600 MHz HR-NMR spectroscopy at specific intervals to confirm metabolite identifications and expand metabolite coverage. M. thermoacetica demonstrated the metabolic potential to produce formate, ethanol and methanol from xylose, in addition to its known capability of producing acetic acid. Real-time monitoring of bioreactor conditions showed a temporary pH decrease, with a concomitant increase in formic acid during exponential growth. Fermentation experiments performed outside of the magnet showed that the strong magnetic field employed for NMR detection did not significantly affect cell metabolism. Use of the in-situ NMR bioreactor facilitated monitoring of the fermentation process in real time, enabling identification of intermediate and end-point metabolites and their correlation with pH and biomass produced during culture growth. Real-time monitoring of culture metabolism using the NMR bioreactor in combination with the HR-NMR spectroscopy will allow optimization of the metabolism of microorganisms producing valuable bioproducts.

  4. High-resolution study of photoinduced modification in fused silica produced by a tightly focused femtosecond laser beam in the presence of aberrations

    SciTech Connect (OSTI)

    Hnatovsky, C.; Taylor, R.S.; Simova, E.; Bhardwaj, V.R.; Rayner, D.M.; Corkum, P.B.

    2005-07-01

    An ultrahigh-resolution (20 nm) technique of selective chemical etching and atomic force microscopy has been used to study the photoinduced modification in fused silica produced at various depths by tightly focused femtosecond laser radiation affected by spherical aberration. We demonstrate that shapes of the irradiated zones near the threshold for modification can be predicted by taking proper account of spherical aberration caused by the refractive index mismatched air-silica interface. We establish a depth dependence of the pulse energy required to initiate modification and characterize the relationship between numerical aperture of the writing lens and practically achievable writing depth. We also show that spatial characteristics of the laser-modified zones can be controlled by a specially designed focusing system which allows correction for a variable amount of spherical aberration.

  5. Selectable resistance-area product by dilute highly charged ion irradiation

    SciTech Connect (OSTI)

    Pomeroy, J. M.; Grube, H.; Perrella, A. C.; Gillaspy, J. D. [National Institute of Standards and Technology, Gaithersburg, Maryland 20899 (United States)

    2007-08-13

    Considerable effort worldwide has been invested in producing low resistance-area (RA) product magnetic tunnel junction sensors for future hard drive read heads. Here the authors present a method of producing tunnel barriers with a selectable RA value spanning orders of magnitude. A single process recipe is used with only the dose of highly charged ions (HCIs) varied. The HCIs reduce the tunnel barrier integrity, providing enhanced conduction that reduces the overall RA product. The final RA product is selected by appropriate choice of the HCI density; e.g., 100 HCIs/{mu}m{sup 2} typically results in the RA product being reduced by a factor of 100.

  6. High-resolution dynamically downscaled projections of precipitation in the mid and late 21st century over North America

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    none,

    2015-07-29

    This study performs high-spatial-resolution (12 km) Weather Research and Forecasting (WRF) simulations over a very large domain (7200 km × 6180 km, covering much of North America) to explore changes in mean and extreme precipitation in the mid and late 21st century under Representative Concentration Pathways 4.5 (RCP 4.5) and 8.5 (RCP 8.5). We evaluate WRF model performance for a historical simulation and future projections, applying the Community Climate System Model version 4 (CCSM4) as initial and boundary conditions with and without a bias correction. WRF simulations using boundary and initial conditions from both versions of CCSM4 show smaller biasesmore » versus evaluation data sets than does CCSM4 over western North America. WRF simulations also improve spatial details of precipitation over much of North America. However, driving the WRF with the bias-corrected CCSM4 does not always reduce the bias. WRF-projected changes in precipitation include decreasing intensity over the southwestern United States, increasing intensity over the eastern United States and most of Canada, and an increase in the number of days with heavy precipitation over much of North America. Projected precipitation changes are more evident in the late 21st century than the mid 21st century, and they are more evident under RCP 8.5 than under RCP 4.5 in the late 21st century. Uncertainties in the projected changes in precipitation due to different warming scenarios are non-negligible. Differences in summer precipitation changes between WRF and CCSM4 are significant over most of the United States.« less

  7. High-resolution dynamically downscaled projections of precipitation in the mid and late 21st century over North America

    SciTech Connect (OSTI)

    none,

    2015-07-29

    This study performs high-spatial-resolution (12 km) Weather Research and Forecasting (WRF) simulations over a very large domain (7200 km × 6180 km, covering much of North America) to explore changes in mean and extreme precipitation in the mid and late 21st century under Representative Concentration Pathways 4.5 (RCP 4.5) and 8.5 (RCP 8.5). We evaluate WRF model performance for a historical simulation and future projections, applying the Community Climate System Model version 4 (CCSM4) as initial and boundary conditions with and without a bias correction. WRF simulations using boundary and initial conditions from both versions of CCSM4 show smaller biases versus evaluation data sets than does CCSM4 over western North America. WRF simulations also improve spatial details of precipitation over much of North America. However, driving the WRF with the bias-corrected CCSM4 does not always reduce the bias. WRF-projected changes in precipitation include decreasing intensity over the southwestern United States, increasing intensity over the eastern United States and most of Canada, and an increase in the number of days with heavy precipitation over much of North America. Projected precipitation changes are more evident in the late 21st century than the mid 21st century, and they are more evident under RCP 8.5 than under RCP 4.5 in the late 21st century. Uncertainties in the projected changes in precipitation due to different warming scenarios are non-negligible. Differences in summer precipitation changes between WRF and CCSM4 are significant over most of the United States.

  8. Non-intrusive, high-resolution, real-time, two-dimensional imaging of multiphase materials using acoustic array sensors

    SciTech Connect (OSTI)

    Cassiède, M.; Shaw, J. M.

    2015-04-15

    Two parallel multi-element ultrasonic acoustic arrays combined with sets of focal laws for acoustic signal generation and a classical tomographic inversion algorithm are used to generate real-time two-dimensional micro seismic acoustic images of multiphase materials. Proof of concept and calibration measurements were performed for single phase and two phase liquids, uniform polyvinyl chloride (PVC) plates, and aluminum cylinders imbedded in PVC plates. Measurement artefacts, arising from the limited range of viewing angles, and the compromise between data acquisition rate and image quality are discussed. The angle range of scanning and the image resolution were varied, and the effects on the quality of the reproduction of the speed of sound profiles of model solids and liquids with known geometries and compositions were analysed in detail. The best image quality results were obtained for a scanning angle range of [−35°, 35°] at a step size of 2.5° post processed to generate images on a 40 μm square grid. The data acquisition time for high quality images with a 30 mm × 40 mm view field is 10 min. Representation of two-phase solids with large differences in speed of sound between phases and where one phase is dispersed in the form of macroscopic objects (greater than 1 mm in diameter) proved to be the most difficult to image accurately. Liquid-liquid and liquid-vapor phase boundaries, in micro porous solids by contrast, were more readily defined. Displacement of air by water and water by heptane in natural porous limestone provides illustrative kinetic examples. Measurement results with these realistic cases demonstrate the feasibility of the technique to monitor in real time and on the micrometer length scale local composition and flow of organic liquids in inorganic porous media, one of many envisioned engineering applications. Improvement of data acquisition rate is an area for future collaborative study.

  9. High-resolution grazing-incidence grating spectrometer for temperature measurements of low-Z ions emitting in the 100300 spectral band

    SciTech Connect (OSTI)

    Widmann, K., E-mail: widmann1@llnl.gov; Beiersdorfer, P.; Magee, E. W. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Boyle, D. P.; Kaita, R.; Majeski, R. [Princeton Plasma Physics Laboratory, Princeton, New Jersey 08543 (United States)

    2014-11-15

    We have constructed a high-resolution grazing-incidence spectrometer designed for measuring the ion temperature of low-Z elements, such as Li{sup +} or Li{sup 2+}, which radiate near 199 and 135 , respectively. Based on measurements at the Livermore Electron Beam Ion Trap we have shown that the instrumental resolution is better than 48 m at the 200 setting and better than 40 m for the 135- range. Such a high spectral resolution corresponds to an instrumental limit for line-width based temperature measurements of about 45 eV for the 199 Li{sup +} and 65 eV for the 135 Li{sup 2+} lines. Recently obtained survey spectra from the Lithium Tokamak Experiment at the Princeton Plasma Physics Laboratory show the presence of these lithium emission lines and the expected core ion temperature of approximately 70 eV is sufficiently high to demonstrate the feasibility of utilizing our high-resolution spectrometer as an ion-temperature diagnostic.

  10. High resolution biomedical imaging system with direct detection of x-rays via a charge coupled device

    DOE Patents [OSTI]

    Atac, M.; McKay, T.A.

    1998-04-21

    An imaging system is provided for direct detection of x-rays from an irradiated biological tissue. The imaging system includes an energy source for emitting x-rays toward the biological tissue and a charge coupled device (CCD) located immediately adjacent the biological tissue and arranged transverse to the direction of irradiation along which the x-rays travel. The CCD directly receives and detects the x-rays after passing through the biological tissue. The CCD is divided into a matrix of cells, each of which individually stores a count of x-rays directly detected by the cell. The imaging system further includes a pattern generator electrically coupled to the CCD for reading a count from each cell. A display device is provided for displaying an image representative of the count read by the pattern generator from the cells of the CCD. 13 figs.

  11. High resolution biomedical imaging system with direct detection of x-rays via a charge coupled device

    DOE Patents [OSTI]

    Atac, Muzaffer; McKay, Timothy A.

    1998-01-01

    An imaging system is provided for direct detection of x-rays from an irradiated biological tissue. The imaging system includes an energy source for emitting x-rays toward the biological tissue and a charge coupled device (CCD) located immediately adjacent the biological tissue and arranged transverse to the direction of irradiation along which the x-rays travel. The CCD directly receives and detects the x-rays after passing through the biological tissue. The CCD is divided into a matrix of cells, each of which individually stores a count of x-rays directly detected by the cell. The imaging system further includes a pattern generator electrically coupled to the CCD for reading a count from each cell. A display device is provided for displaying an image representative of the count read by the pattern generator from the cells of the CCD.

  12. TU-F-BRE-01: A High Resolution Micro Fiber Scintillator Detector Optimized for SRS and SBRT in Vivo Real Time Treatment Verification

    SciTech Connect (OSTI)

    Izaguirre, E; Rangaraj, D; Price, S; Knewtson, T; Loyalka, S

    2014-06-15

    Purpose: We have built a high resolution real time scintillating fiber detector prototype to determine in real time the accuracy of stereotactic radiosurgery (SRS) and stereotactic body radiotherapy (SBRT) treatments when only a fraction of the planned dose was delivered. The motivation of this work is to enhance dose delivery accuracy and to achieve error free radiosurgery. Methods: A high density array of scintillating fibers and a high speed photo detectors array were integrated to implement a high resolution real time dosimeter that can sample with high resolution pulsed SRS and SBRT beams cross sections. The high efficiency of the developed system allows to read each linac pulse in real time and to compute the accumulated dose and dose errors when only a fraction of the beam was delivered. The fibers are highly packed in a substrate that is directly coupled to two 128 pixel arrays with a pitch matching the fiber spacing to achieve accurate spatial localization. The small cross section of the fiber array allows stacking multiple fiber arrays to measure independent angular profiles that are digitally processed in parallel for real time dosimetry. Results: We implemented a high density array detector prototype with a pitch of 0.5 mm, readout speed of 1.2 msec, and a response time of 0.5 usec. The fast reading speed has the capability to determining the dose in flattening free filter beams. The detector can be installed in transmission mode at the output port of a micro-MLC. Treatment deviations smaller than 3% are detected when less than 1/100 of the planned dose was delivered. Conclusions: We built a prototype of a high resolution fiber scintillator array detector for SRS and SBRT in vivo dosimetry. Results show that the developed detector has the potential to assure error free SRS and SBRT treatments.

  13. Heavy-ion irradiation induced diamond formation in carbonaceous materials.

    SciTech Connect (OSTI)

    Daulton, T. L.

    1999-01-08

    The basic mechanisms of metastable phase formation produced under highly non-equilibrium thermodynamic conditions within high-energy particle tracks are investigated. In particular, the possible formation of diamond by heavy-ion irradiation of graphite at ambient temperature is examined. This work was motivated, in part, by earlier studies which discovered nanometer-grain polycrystalline diamond aggregates of submicron-size in uranium-rich carbonaceous mineral assemblages of Precambrian age. It was proposed that the radioactive decay of uranium formed diamond in the fission particle tracks produced in the carbonaceous minerals. To test the hypothesis that nanodiamonds can form by ion irradiation, fine-grain polycrystalline graphite sheets were irradiated with 400 MeV Kr ions. The ion irradiated graphite (and unirradiated graphite control) were then subjected to acid dissolution treatments to remove the graphite and isolate any diamonds that were produced. The acid residues were then characterized by analytical and high-resolution transmission electron microscopy. The acid residues of the ion-irradiated graphite were found to contain ppm concentrations of nanodiamonds, suggesting that ion irradiation of bulk graphite at ambient temperature can produce diamond.

  14. Stepped-anneal and total helium/hydrogen measurements in high-energy proton-irradiated tungsten

    SciTech Connect (OSTI)

    Oliver, B.M.; Hamilton, M.L.; Garner, F.A.; Sommer, W.F.; Maloy, S.A.; Ferguson, P.D.

    1998-12-31

    To provide structural material design data for the Accelerator Production of Tritium (APT) project, a 1 mA, 800 MeV proton beam at the Los Alamos Neutron Science Center (LANSCE) was used to irradiate a large number of metal samples, including a tungsten target similar to that being considered as the neutron source for the tritium production. The maximum proton fluence to the tungsten target was {approximately} 10{sup 21} protons/cm{sup 2}. An unavoidable byproduct of spallation reactions is the formation of large amounts of hydrogen and helium. Postulated accident scenarios for APT involving the use of tungsten rods clad with Alloy 718, raise concerns as to the amount and rate of release of these gases due to temperatures increases from afterheat accumulation, with the major concern being pressurizing and possibly failure of the cladding. To address these issues, portions of the LANSCE tungsten rods were subjected to temperature histories calculated as likely to occur, and the time-dependent evolution of helium and hydrogen gases was measured. Stepped-anneal and total helium/hydrogen measurements were conducted on multiple samples of the tungsten material. Helium measurements were conducted at Pacific Northwest National Laboratory (PNNL) using a high-sensitivity magnetic-sector isotope-dilution helium analysis system. Stepped-anneal measurements were conducted at temperatures from {approximately} 25 C to {approximately} 1,600 C in {approximately} 100 C steps. Total helium measurements were conducted by rapid vaporization after completion of the stepped-anneal process, and are compared with Monte Carlo calculations performed at Los Alamos National Laboratory (LANL) using the LAHET code system. Hydrogen measurements were conducted between {approximately} 750 C and {approximately} 1,200 C using a high-temperature furnace that had been extensively modified for the application. Hydrogen detection was accomplished by periodic sampling of the furnace gas using a separate quadrupole analyzer. Hydrogen measurements are also compared with LANL calculations.

  15. High resolution NMR study of T{sub 1} magnetic relaxation dispersion. IV. Proton relaxation in amino acids and Met-enkephalin pentapeptide

    SciTech Connect (OSTI)

    Pravdivtsev, Andrey N.; Yurkovskaya, Alexandra V.; Ivanov, Konstantin L.; Vieth, Hans-Martin

    2014-10-21

    Nuclear Magnetic Relaxation Dispersion (NMRD) of protons was studied in the pentapeptide Met-enkephalin and the amino acids, which constitute it. Experiments were run by using high-resolution Nuclear Magnetic Resonance (NMR) in combination with fast field-cycling, thus enabling measuring NMRD curves for all individual protons. As in earlier works, Papers I–III, pronounced effects of intramolecular scalar spin-spin interactions, J-couplings, on spin relaxation were found. Notably, at low fields J-couplings tend to equalize the apparent relaxation rates within networks of coupled protons. In Met-enkephalin, in contrast to the free amino acids, there is a sharp increase in the proton T{sub 1}-relaxation times at high fields due to the changes in the regime of molecular motion. The experimental data are in good agreement with theory. From modelling the relaxation experiments we were able to determine motional correlation times of different residues in Met-enkephalin with atomic resolution. This allows us to draw conclusions about preferential conformation of the pentapeptide in solution, which is also in agreement with data from two-dimensional NMR experiments (rotating frame Overhauser effect spectroscopy). Altogether, our study demonstrates that high-resolution NMR studies of magnetic field-dependent relaxation allow one to probe molecular mobility in biomolecules with atomic resolution.

  16. Improved Ga grading of sequentially produced Cu(In,Ga)Se{sub 2} solar cells studied by high resolution X-ray fluorescence

    SciTech Connect (OSTI)

    Schöppe, Philipp; Schnohr, Claudia S.; Oertel, Michael; Kusch, Alexander; Johannes, Andreas; Eckner, Stefanie; Reislöhner, Udo; Ronning, Carsten; Burghammer, Manfred; Martínez-Criado, Gema

    2015-01-05

    There is particular interest to investigate compositional inhomogeneity of Cu(In,Ga)Se{sub 2} solar cell absorbers. We introduce an approach in which focused ion beam prepared thin lamellas of complete solar cell devices are scanned with a highly focused synchrotron X-ray beam. Analyzing the resulting fluorescence radiation ensures high resolution compositional analysis combined with high spatial resolution. Thus, we are able to detect subtle variations of the Ga/(Ga + In) ratio down to 0.01 on a submicrometer scale. We observed that for sequentially processed solar cells a higher selenization temperature leads to absorbers with almost homogenous Ga/(Ga + In) ratio, which significantly improved the conversion efficiency.

  17. High dose neutron irradiation of Hi-Nicalon Type S silicon carbide composites, Part 1: Microstructural evaluations

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Perez-Bergquist, Alex G; Nozawa, Takashi; Shih, Chunghao Phillip; Leonard, Keith J; Snead, Lance Lewis; Katoh, Yutai

    2015-01-01

    Over the past decade, significant progress has been made in the development of silicon carbide (SiC) composites, composed of near-stoichiometric SiC fibers embedded in a crystalline SiC matrix, to the point that such materials can now be considered nuclear grade. Recent neutron irradiation studies of Hi-Nicalon Type S SiC composites showed excellent radiation response at damage levels of 30 40 dpa at temperatures of 300 800 C. However, more recent studies of these same fiber composites irradiated to damage levels of >70 dpa at similar temperatures showed a marked decrease in ultimate flexural strength, particularly at 300 C. Here, electronmore » microscopy is used to analyze the microstructural evolution of these irradiated composites in order to investigate the cause of the degradation. While minimal changes were observed in Hi-Nicalon Type S SiC composites irradiated at 800 C, substantial microstructural evolution is observed in those irradiated at 300 C. Specifically, carbonaceous particles in the fibers grew by 25% compared to the virgin case, and severe cracking occurred at interphase layers.« less

  18. High dose neutron irradiation of Hi-Nicalon Type S silicon carbide composites, Part 1: Microstructural evaluations

    SciTech Connect (OSTI)

    Perez-Bergquist, Alex G; Nozawa, Takashi; Shih, Chunghao Phillip; Leonard, Keith J; Snead, Lance Lewis; Katoh, Yutai

    2015-01-01

    Over the past decade, significant progress has been made in the development of silicon carbide (SiC) composites, composed of near-stoichiometric SiC fibers embedded in a crystalline SiC matrix, to the point that such materials can now be considered nuclear grade. Recent neutron irradiation studies of Hi-Nicalon Type S SiC composites showed excellent radiation response at damage levels of 30 40 dpa at temperatures of 300 800 C. However, more recent studies of these same fiber composites irradiated to damage levels of >70 dpa at similar temperatures showed a marked decrease in ultimate flexural strength, particularly at 300 C. Here, electron microscopy is used to analyze the microstructural evolution of these irradiated composites in order to investigate the cause of the degradation. While minimal changes were observed in Hi-Nicalon Type S SiC composites irradiated at 800 C, substantial microstructural evolution is observed in those irradiated at 300 C. Specifically, carbonaceous particles in the fibers grew by 25% compared to the virgin case, and severe cracking occurred at interphase layers.

  19. High dose neutron irradiations of Hi-Nicalon Type S silicon carbide composites, Part 1: Microstructural evaluations

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Perez-Bergquist, Alex G.; Nozawa, Takashi; Shih, Chunghao Phillip; Leonard, Keith J.; Snead, Lance Lewis; Katoh, Yutai

    2014-07-01

    Over the past decade, significant progress has been made in the development of silicon carbide (SiC) composites, composed of near-stoichiometric SiC fibers embedded in a crystalline SiC matrix, to the point that such materials can now be considered nuclear grade. Recent neutron irradiation studies of Hi-Nicalon Type S SiC composites showed excellent radiation response at damage levels of 30-40 dpa at temperatures of 300-800 °C. However, more recent studies of these same fiber composites irradiated to damage levels of >70 dpa at similar temperatures showed a marked decrease in ultimate flexural strength, particularly at 300 °C. Here, electron microscopy ismore » used to analyze the microstructural evolution of these irradiated composites in order to investigate the cause of the degradation. While minimal changes were observed in Hi-Nicalon Type S SiC composites irradiated at 800 °C, substantial microstructural evolution is observed in those irradiated at 300° C. Furthermore, carbonaceous particles in the fibers grew by 25% compared to the virgin case, and severe cracking occurred at interphase layers.« less

  20. HIGH-RESOLUTION EXPANDED VERY LARGE ARRAY IMAGE OF DIMETHYL ETHER (CH{sub 3}){sub 2}O IN ORION-KL

    SciTech Connect (OSTI)

    Favre, C.; Wootten, H. A.; Remijan, A. J.; Brouillet, N.; Despois, D.; Baudry, A.; Wilson, T. L. E-mail: brouillet@obs.u-bordeaux1.fr E-mail: baudry@obs.u-bordeaux1.fr E-mail: aremijan@nrao.edu

    2011-09-20

    We report the first subarcsecond (0.''65 x 0.''51) image of the dimethyl ether molecule, (CH{sub 3}){sub 2}O, toward the Orion Kleinmann-Low nebula. The observations were carried at 43.4 GHz with the Expanded Very Large Array (EVLA). The distribution of the lower energy transition 6{sub 1,5}-6{sub 0,6}, EE (E {sub u} = 21 K) mapped in this study is in excellent agreement with the published dimethyl ether emission maps imaged with a lower resolution. The main emission peaks are observed toward the Compact Ridge and Hot Core southwest components, at the northern parts of the Compact Ridge and in an intermediate position between the Compact Ridge and the Hot Core. A notable result is that the distribution of dimethyl ether is very similar to that of another important larger O-bearing species, the methyl formate (HCOOCH{sub 3}), imaged at a lower resolution. Our study shows that higher spectral resolution (WIDAR correlator) and increased spectral coverage provided by the EVLA offer new possibilities for imaging complex molecular species. The sensitivity improvement and the other EVLA improvements make this instrument well suited for high sensitivity, high angular resolution, and molecular line imaging.

  1. Neutron radiography of irradiated nuclear fuel at Idaho National Laboratory

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Craft, Aaron E.; Wachs, Daniel M.; Okuniewski, Maria A.; Chichester, David L.; Williams, Walter J.; Papaioannou, Glen C.; Smolinski, Andrew T.

    2015-09-10

    Neutron radiography of irradiated nuclear fuel provides more comprehensive information about the internal condition of irradiated nuclear fuel than any other non-destructive technique to date. Idaho National Laboratory (INL) has multiple nuclear fuels research and development programs that routinely evaluate irradiated fuels using neutron radiography. The Neutron Radiography reactor (NRAD) sits beneath a shielded hot cell facility where neutron radiography and other evaluation techniques are performed on these highly radioactive objects. The NRAD currently uses the foil-film transfer technique for imaging fuel that is time consuming but provides high spatial resolution. This study describes the NRAD and hot cell facilities,more » the current neutron radiography capabilities available at INL, planned upgrades to the neutron imaging systems, and new facilities being brought online at INL related to neutron imaging.« less

  2. Neutron radiography of irradiated nuclear fuel at Idaho National Laboratory

    SciTech Connect (OSTI)

    Craft, Aaron E.; Wachs, Daniel M.; Okuniewski, Maria A.; Chichester, David L.; Williams, Walter J.; Papaioannou, Glen C.; Smolinski, Andrew T.

    2015-09-10

    Neutron radiography of irradiated nuclear fuel provides more comprehensive information about the internal condition of irradiated nuclear fuel than any other non-destructive technique to date. Idaho National Laboratory (INL) has multiple nuclear fuels research and development programs that routinely evaluate irradiated fuels using neutron radiography. The Neutron Radiography reactor (NRAD) sits beneath a shielded hot cell facility where neutron radiography and other evaluation techniques are performed on these highly radioactive objects. The NRAD currently uses the foil-film transfer technique for imaging fuel that is time consuming but provides high spatial resolution. This study describes the NRAD and hot cell facilities, the current neutron radiography capabilities available at INL, planned upgrades to the neutron imaging systems, and new facilities being brought online at INL related to neutron imaging.

  3. Low-energy inverse photoemission spectroscopy using a high-resolution grating spectrometer in the near ultraviolet range

    SciTech Connect (OSTI)

    Yoshida, Hiroyuki

    2013-10-15

    An inverse photoemission spectroscopy (IPES) apparatus using a Czerny-Turner grating spectrometer is demonstrated. Previous IPES instruments based on grating spectrometers used a concave grating and operated in the vacuum ultraviolet range. The reflectance of such gratings is lower than 20% and the aberration cannot be finely corrected leading to an energy resolution of up to 0.1 eV. In the present study, employing the low energy IPES regime [H. Yoshida, Chem. Phys. Lett. 539–540, 180 (2012)], incident electrons with a kinetic energy below 5 eV are used, while photon emission in the range of between 250 and 370 nm is analyzed with a 10-cm Czerny-Turner grating spectrometer. The signal intensity is at least 30 times higher than the previous apparatus. The resolution of photon detection is set at 0.07 eV though the ultimate resolution is one order of magnitude higher. The experiment is performed both by sweeping the electron energy (isochromat mode) and by simultaneously analyzing the photon of whole wavelength range (tunable photon energy mode)

  4. Quantification of dislocation nucleation stress in TiN through high-resolution in situ indentation experiments and first principles calculations

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Li, N.; Yadav, S. K.; Liu, X. -Y.; Wang, J.; Hoagland, R. G.; Mara, N.; Misra, A.

    2015-11-05

    Using the in situ indentation of TiN in a high-resolution transmission electron microscope, the nucleation of full as well as partial dislocations has been observed from {001} and {111} surfaces, respectively. The critical elastic strains associated with the nucleation of the dislocations were analyzed from the recorded atomic displacements, and the nucleation stresses corresponding to the measured critical strains were computed using density functional theory. The resolved shear stress was estimated to be 13.8 GPa for the partial dislocation 1/6 <110> {111} and 6.7 GPa for the full dislocation ½ <110> {110}. Moreover, such an approach of quantifying nucleation stressesmore » for defects via in situ high-resolution experiment coupled with density functional theory calculation may be applied to other unit processes.« less

  5. Laser hazard analysis for LASIRIS Model MAG-501L-670M-1000-45[degree]-K diode laser associated with high resolution pulsed scanner.

    SciTech Connect (OSTI)

    Augustoni, Arnold L.

    2004-11-01

    A laser hazard analysis and safety assessment was performed for the LASIRISTM Model MAG-501L-670M-1000-45o-K diode laser associated with the High Resolution Pulse Scanner based on the ANSI Standard Z136.1-2000, American National Standard for the Safe Use of Lasers and the ANSI Standard Z136.6-2000, American National Standard for the Safe Use of Lasers Outdoors. The laser was evaluated for both indoor and outdoor use.

  6. HIGH-RESOLUTION LABORATORY SPECTRA ON THE λ131 CHANNEL OF THE AIA INSTRUMENT ON BOARD THE SOLAR DYNAMICS OBSERVATORY

    SciTech Connect (OSTI)

    Träbert, Elmar; Beiersdorfer, Peter; Brickhouse, Nancy S.; Golub, Leon

    2014-03-01

    Extreme ultraviolet spectra of C, O, F, Ne, Si, S, Ar, Ca, Fe, and Ni have been excited in an electron beam ion trap and studied with much higher resolution than available on Solar Dynamics Observatory (SDO) in order to ascertain the spectral composition of the SDO observations. We presently show our findings in the wavelength range 124-134 Å, which encompasses the λ131 observation channel of the Atmospheric Imaging Assembly (AIA). While the general interpretation of the spectral composition of the λ131 Fe channel is being corroborated, a number of new lines have been observed that might help to improve the diagnostic value of the SDO/AIA data.

  7. Development of vertically aligned ZnO-nanowires scintillators for high spatial resolution x-ray imaging

    SciTech Connect (OSTI)

    Kobayashi, Masakazu Komori, Jun; Shimidzu, Kaiji; Izaki, Masanobu; Uesugi, Kentaro; Takeuchi, Akihisa; Suzuki, Yoshio

    2015-02-23

    Newly designed scintillator of (0001)-oriented ZnO vertical nanowires (vnws) for X-ray imaging was prepared on a Ga-doped ZnO/soda-lime glass by electrodeposition, and the light emission feature was estimated in a synchrotron radiation facility. The ZnO-vnws scintillator revealed a strong light emission and improved resolution on CMOS image compared with that for the ZnO-layer scintillator, although the light emission performance was deteriorated in comparison to the Lu{sub 3}Al{sub 5}O{sub 12:}Ce{sup 3+}. The light emission property closely related to the nanostructure and the resultant photoluminescence characteristic.

  8. Development of a lab-scale, high-resolution, tube-generated X-ray computed-tomography system for three-dimensional (3D) materials characterization

    SciTech Connect (OSTI)

    Mertens, J.C.E. Williams, J.J. Chawla, Nikhilesh

    2014-06-01

    The design and construction of a modular high resolution X-ray computed tomography (XCT) system is highlighted in this paper. The design approach is detailed for meeting a specified set of instrument performance goals tailored towards experimental versatility and high resolution imaging. The XCT tool is unique in the detector and X-ray source design configuration, enabling control in the balance between detection efficiency and spatial resolution. The system package is also unique: The sample manipulation approach implemented enables a wide gamut of in situ experimentation to analyze structure evolution under applied stimulus, by optimizing scan conditions through a high degree of controllability. The component selection and design process is detailed: Incorporated components are specified, custom designs are shared, and the approach for their integration into a fully functional XCT scanner is provided. Custom designs discussed include the dual-target X-ray source cradle which maintains position and trajectory of the beam between the two X-ray target configurations with respect to a scintillator mounting and positioning assembly and the imaging sensor, as well as a novel large-format X-ray detector with enhanced adaptability. The instrument is discussed from an operational point of view, including the details of data acquisition and processing implemented for 3D imaging via micro-CT. The performance of the instrument is demonstrated on a silica-glass particle/hydroxyl-terminated-polybutadiene (HTPB) matrix binder PBX simulant. Post-scan data processing, specifically segmentation of the sample's relevant microstructure from the 3D reconstruction, is provided to demonstrate the utility of the instrument. - Highlights: Custom built X-ray tomography system for microstructural characterization Detector design for maximizing polychromatic X-ray detection efficiency X-ray design offered for maximizing X-ray flux with respect to imaging resolution Novel lab-scale XCT data acquisition and data processing methods 3D characterization of glass-bead mock plastic-bonded-explosive stimulant.

  9. IONIZED GAS KINEMATICS AT HIGH RESOLUTION. II. DISCOVERY OF A DOUBLE INFRARED CLUSTER IN II Zw 40

    SciTech Connect (OSTI)

    Beck, Sara; Lahad, Ohr; Turner, Jean; Lacy, John; Greathouse, Thomas

    2013-04-10

    The nearby dwarf galaxy II Zw 40 hosts an intense starburst. At the center of the starburst is a bright compact radio and infrared source, thought to be a giant dense H II region containing Almost-Equal-To 14, 000 O stars. Radio continuum images suggest that the compact source is actually a collection of several smaller emission regions. We accordingly use the kinematics of the ionized gas to probe the structure of the radio-infrared emission region. With TEXES on the NASA-IRTF we measured the 10.5 {mu}m [S IV] emission line with effective spectral resolutions, including thermal broadening, of {approx}25 and {approx}3 km s{sup -1} and spatial resolution {approx}1''. The line profile shows two distinct, spatially coextensive, emission features. The stronger feature is at galactic velocity and has FWHM 47 km s{sup -1}. The second feature is {approx}44 km s{sup -1} redward of the first and has FWHM 32 km s{sup -1}. We argue that these are two giant embedded clusters, and estimate their masses to be Almost-Equal-To 3 Multiplication-Sign 10{sup 5} M{sub Sun} and Almost-Equal-To 1.5 Multiplication-Sign 10{sup 5} M{sub Sun }. The velocity shift is unexpectedly large for such a small spatial offset. We suggest that it may arise in a previously undetected kinematic feature remaining from the violent merger that formed the galaxy.

  10. High-resolution (e, 2e + ion) study of electron-impact ionization and fragmentation of methane

    SciTech Connect (OSTI)

    Ren, Xueguang Pflger, Thomas; Weyland, Marvin; Baek, Woon Yong; Rabus, Hans; Ullrich, Joachim; Dorn, Alexander

    2015-05-07

    The ionization and fragmentation of methane induced by low-energy (E{sub 0} = 66 eV) electron-impact is investigated using a reaction microscope. The momentum vectors of all three charged final state particles, two outgoing electrons, and one fragment ion, are detected in coincidence. Compared to the earlier study [Xu et al., J. Chem. Phys. 138, 134307 (2013)], considerable improvements to the instrumental mass and energy resolutions have been achieved. The fragment products CH{sub 4}{sup +}, CH{sub 3}{sup +}, CH{sub 2}{sup +}, CH{sup +}, and C{sup +} are clearly resolved. The binding energy resolution of ?E = 2.0 eV is a factor of three better than in the earlier measurements. The fragmentation channels are investigated by measuring the ion kinetic energy distributions and the binding energy spectra. While being mostly in consistence with existing photoionization studies the results show differences including missing fragmentation channels and previously unseen channels.

  11. IN-SITU ASSAY OF TRANSURANIC RADIONUCLIDES IN THE VADOSE ZONE USING HIGH-RESOLUTION SPECTRAL GAMMA LOGGING - A HANFORD CASE STUDY

    SciTech Connect (OSTI)

    ROHAY VJ; HENWOOD P; MCCAIN R

    2009-11-30

    High-resolution spectral gamma logging in steel-cased boreholes is used to detect and quantify transuranic radionuclides in the subsurface. Pu-239, Pu-241, Am-241, and Np-237 are identified based on characteristic decay gammas. Typical minimum detectable levels are on the order of 20 to 40 nCi/g. In intervals of high transuranic concentrations, gamma rays from other sources may complicate analysis and interpretation. Gamma rays detected in the borehole may originate from three sources: decay of the parent transuranic radionuclide or a daughter; alpha interactions; and interactions with neutrons resulting from either spontaneous fission or alpha particle interactions.

  12. High-resolution diffraction microscopy using the plane-wave field of a nearly diffraction limited focused x-ray beam

    SciTech Connect (OSTI)

    Takahashi, Yukio; Nishino, Yoshinori; Ishikawa, Tetsuya; Tsutsumi, Ryosuke; Kubo, Hideto; Furukawa, Hayato; Mimura, Hidekazu; Matsuyama, Satoshi; Zettsu, Nobuyuki; Matsubara, Eiichiro; Yamauchi, Kazuto

    2009-08-01

    X-ray waves in the center of the beam waist of nearly diffraction limited focused x-ray beams can be considered to have amplitude and phase that are both almost uniform, i.e., they are x-ray plane waves. Here we report the results of an experimental demonstration of high-resolution diffraction microscopy using the x-ray plane wave of the synchrotron x-ray beam focused using Kirkpatrik-Baez mirrors. A silver nanocube with an edge length of {approx}100 nm is illuminated with the x-ray beam focused to a {approx}1 {mu}m spot at 12 keV. A high-contrast symmetric diffraction pattern of the nanocube is observed in the forward far field. An image of the nanocube is successfully reconstructed by an iterative phasing method and its half-period resolution is 3.0 nm. This method does not only dramatically improve the spatial resolution of x-ray microscopy but also is a key technology for realizing single-pulse diffractive imaging using x-ray free-electron lasers.

  13. A Large-Scale, High-Resolution Hydrological Model Parameter Data Set for Climate Change Impact Assessment for the Conterminous US

    SciTech Connect (OSTI)

    Oubeidillah, Abdoul A; Kao, Shih-Chieh; Ashfaq, Moetasim; Naz, Bibi S; Tootle, Glenn

    2014-01-01

    To extend geographical coverage, refine spatial resolution, and improve modeling efficiency, a computation- and data-intensive effort was conducted to organize a comprehensive hydrologic dataset with post-calibrated model parameters for hydro-climate impact assessment. Several key inputs for hydrologic simulation including meteorologic forcings, soil, land class, vegetation, and elevation were collected from multiple best-available data sources and organized for 2107 hydrologic subbasins (8-digit hydrologic units, HUC8s) in the conterminous United States at refined 1/24 (~4 km) spatial resolution. Using high-performance computing for intensive model calibration, a high-resolution parameter dataset was prepared for the macro-scale Variable Infiltration Capacity (VIC) hydrologic model. The VIC simulation was driven by DAYMET daily meteorological forcing and was calibrated against USGS WaterWatch monthly runoff observations for each HUC8. The results showed that this new parameter dataset may help reasonably simulate runoff at most US HUC8 subbasins. Based on this exhaustive calibration effort, it is now possible to accurately estimate the resources required for further model improvement across the entire conterminous United States. We anticipate that through this hydrologic parameter dataset, the repeated effort of fundamental data processing can be lessened, so that research efforts can emphasize the more challenging task of assessing climate change impacts. The pre-organized model parameter dataset will be provided to interested parties to support further hydro-climate impact assessment.

  14. TESTING THE HYPOTHESIS THAT METHANOL MASER RINGS TRACE CIRCUMSTELLAR DISKS: HIGH-RESOLUTION NEAR-INFRARED AND MID-INFRARED IMAGING

    SciTech Connect (OSTI)

    De Buizer, James M.; Bartkiewicz, Anna; Szymczak, Marian

    2012-08-01

    Milliarcsecond very long baseline interferometry maps of regions containing 6.7 GHz methanol maser emission have lead to the recent discovery of ring-like distributions of maser spots and the plausible hypothesis that they may be tracing circumstellar disks around forming high-mass stars. We aimed to test this hypothesis by imaging these regions in the near- and mid-infrared at high spatial resolution and compare the observed emission to the expected infrared morphologies as inferred from the geometries of the maser rings. In the near-infrared we used the Gemini North adaptive optics system of ALTAIR/NIRI, while in the mid-infrared we used the combination of the Gemini South instrument T-ReCS and super-resolution techniques. Resultant images had a resolution of {approx}150 mas in both the near-infrared and mid-infrared. We discuss the expected distribution of circumstellar material around young and massive accreting (proto)stars and what infrared emission geometries would be expected for the different maser ring orientations under the assumption that the masers are coming from within circumstellar disks. Based upon the observed infrared emission geometries for the four targets in our sample and the results of spectral energy distribution modeling of the massive young stellar objects associated with the maser rings, we do not find compelling evidence in support of the hypothesis that methanol masers rings reside in circumstellar disks.

  15. Magnetoacoustic tomography with magnetic induction for high-resolution bioimepedance imaging through vector source reconstruction under the static field of MRI magnet

    SciTech Connect (OSTI)

    Mariappan, Leo; Hu, Gang; He, Bin

    2014-02-15

    Purpose: Magnetoacoustic tomography with magnetic induction (MAT-MI) is an imaging modality to reconstruct the electrical conductivity of biological tissue based on the acoustic measurements of Lorentz force induced tissue vibration. This study presents the feasibility of the authors' new MAT-MI system and vector source imaging algorithm to perform a complete reconstruction of the conductivity distribution of real biological tissues with ultrasound spatial resolution. Methods: In the present study, using ultrasound beamformation, imaging point spread functions are designed to reconstruct the induced vector source in the object which is used to estimate the object conductivity distribution. Both numerical studies and phantom experiments are performed to demonstrate the merits of the proposed method. Also, through the numerical simulations, the full width half maximum of the imaging point spread function is calculated to estimate of the spatial resolution. The tissue phantom experiments are performed with a MAT-MI imaging system in the static field of a 9.4 T magnetic resonance imaging magnet. Results: The image reconstruction through vector beamformation in the numerical and experimental studies gives a reliable estimate of the conductivity distribution in the object with a ∼1.5 mm spatial resolution corresponding to the imaging system frequency of 500 kHz ultrasound. In addition, the experiment results suggest that MAT-MI under high static magnetic field environment is able to reconstruct images of tissue-mimicking gel phantoms and real tissue samples with reliable conductivity contrast. Conclusions: The results demonstrate that MAT-MI is able to image the electrical conductivity properties of biological tissues with better than 2 mm spatial resolution at 500 kHz, and the imaging with MAT-MI under a high static magnetic field environment is able to provide improved imaging contrast for biological tissue conductivity reconstruction.

  16. Scanning Electron Microscopy Analysis of Fuel/Matrix Interaction Layers in Highly-Irradiated UMo Dispersion Fuel Plates with Al and AlSi Alloy Matrices

    SciTech Connect (OSTI)

    Dennis D. Keiser, Jr.; Jan-Fong Jue; Brandon D. Miller; Jian Gan; Adam B. Robinson; Pavel Medvedev; James Madden; Dan Wachs; Mitch Meyer

    2014-04-01

    In order to investigate how the microstructure of fuel/matrix-interaction (FMI) layers change during irradiation, different U7Mo dispersion fuel plates have been irradiated to high fission density and then characterized using scanning electron microscopy (SEM). Specifially, samples from irradiated U7Mo dispersion fuel elements with pure Al, Al2Si and AA4043 (~4.5 wt.%Si) matrices were SEM characterized using polished samples and samples that were prepared with a focused ion beam (FIB). Features not observable for the polished samples could be captured in SEM images taken of the FIB samples. For the Al matrix sample, a relatively large FMI layer develops, with enrichment of Xe at the FMI layer/Al matrix interface and evidence of debonding. Overall, a significant penetration of Si from the FMI layer into the U7Mo fuel was observed for samples with Si in the Al matrix, which resulted in a change of the size (larger) and shape (round) of the fission-gas bubbles. Additionally, solid-fission-product phases were observed to nucleate and grow within these bubbles. These changes in the localized regions of the microstructure of the U7Mo may contribute to changes observed in the macroscopic swelling of fuel plates with AlSi matrices.

  17. Local Optical Spectroscopies for Subnanometer Spatial Resolution Chemical Imaging

    SciTech Connect (OSTI)

    Weiss, Paul

    2014-01-20

    The evanescently coupled photon scanning tunneling microscopes (STMs) have special requirements in terms of stability and optical access. We have made substantial improvements to the stability, resolution, and noise floor of our custom-built visible-photon STM, and will translate these advances to our infrared instrument. Double vibration isolation of the STM base with a damping system achieved increased rigidity, giving high tunneling junction stability for long-duration and high-power illumination. Light frequency modulation with an optical chopper and phase-sensitive detection now enhance the signal-to-noise ratio of the tunneling junction during irradiation.

  18. A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

    SciTech Connect (OSTI)

    Seidler, G. T. Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R.

    2014-11-15

    We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ?5 keV to ?10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

  19. Demonstration of a Novel, Integrated, Multi-Scale Procedure for High-Resolution 3D Reservoir Characterization and Improved CO2-EOR/Sequestration Management, SACROC Unit

    SciTech Connect (OSTI)

    Scott R. Reeves

    2007-09-30

    The primary goal of this project was to demonstrate a new and novel approach for high resolution, 3D reservoir characterization that can enable better management of CO{sub 2} enhanced oil recovery (EOR) projects and, looking to the future, carbon sequestration projects. The approach adopted has been the subject of previous research by the DOE and others, and relies primarily upon data-mining and advanced pattern recognition approaches. This approach honors all reservoir characterization data collected, but accepts that our understanding of how these measurements relate to the information of most interest, such as how porosity and permeability vary over a reservoir volume, is imperfect. Ideally the data needed for such an approach includes surface seismic to provide the greatest amount of data over the entire reservoir volume of interest, crosswell seismic to fill the resolution gap between surface seismic and wellbore-scale measurements, geophysical well logs to provide the vertical resolution sought, and core data to provide the tie to the information of most interest. These data are combined via a series of one or more relational models to enable, in its most successful application, the prediction of porosity and permeability on a vertical resolution similar to logs at each surface seismic trace location. In this project, the procedure was applied to the giant (and highly complex) SACROC unit of the Permian basin in West Texas, one of the world's largest CO{sub 2}-EOR projects and a potentially world-class geologic sequestration site. Due to operational scheduling considerations on the part of the operator of the field, the crosswell data was not obtained during the period of project performance (it is currently being collected however as part of another DOE project). This compromised the utility of the surface seismic data for the project due to the resolution gap between it and the geophysical well logs. An alternative approach was adopted that utilized a relational model to predict porosity and permeability profiles from well logs at each well location, and a 3D geostatistical variogram to generate the reservoir characterization over the reservoir volume of interest. A reservoir simulation model was built based upon this characterization and history-matched without making significant changes to it, thus validating the procedure. While not the same procedure as originally planned, the procedure ultimately employed proved successful and demonstrated that the general concepts proposed (i.e., data mining and advanced pattern recognition methods) have the flexibility to achieve the reservoir characterization objectives sought even with imperfect or incomplete data.

  20. A method to determine fault vectors in 4H-SiC from stacking sequences observed on high resolution transmission electron microscopy images

    SciTech Connect (OSTI)

    Wu, Fangzhen; Wang, Huanhuan; Raghothamachar, Balaji; Dudley, Michael; Mueller, Stephan G.; Chung, Gil; Sanchez, Edward K.; Hansen, Darren; Loboda, Mark J.; Zhang, Lihua; Su, Dong; Kisslinger, Kim; Stach, Eric

    2014-09-14

    A new method has been developed to determine the fault vectors associated with stacking faults in 4H-SiC from their stacking sequences observed on high resolution TEM images. This method, analogous to the Burgers circuit technique for determination of dislocation Burgers vector, involves determination of the vectors required in the projection of the perfect lattice to correct the deviated path constructed in the faulted material. Results for several different stacking faults were compared with fault vectors determined from X-ray topographic contrast analysis and were found to be consistent. This technique is expected to applicable to all structures comprising corner shared tetrahedra.

  1. Development of a High Resolution X-Ray Imaging Crystal Spectrometer for Measurement of Ion-Temperature and Rotation-Velocity Profiles in Fusion Energy Research Plasmas

    Office of Scientific and Technical Information (OSTI)

    96 PPPL- 4296 Development of a High Resolution X-Ray Imaging Crystal Spectrometer for Measurement of Ion-Temperature and Rotation-Velocity Profiles in Fusion Energy Research Plasmas February 2008 K.W. HILL, M.L. BITTER, Ch. BROENNIMANN, E.F. EIKENBERRY, A. Ince-CUSHMAN, S.G. LEE, J.E. RICE, S. SCOTT and R. BARNSLEY Princeton Plasma Physics Laboratory Report Disclaimers Full Legal Disclaimer This report was prepared as an account of work sponsored by an agency of the United States Government.

  2. Tissue irradiator

    DOE Patents [OSTI]

    Hungate, F.P.; Riemath, W.F.; Bunnell, L.R.

    1975-12-16

    A tissue irradiator is provided for the in-vivo irradiation of body tissue. The irradiator comprises a radiation source material contained and completely encapsulated within vitreous carbon. An embodiment for use as an in- vivo blood irradiator comprises a cylindrical body having an axial bore therethrough. A radioisotope is contained within a first portion of vitreous carbon cylindrically surrounding the axial bore, and a containment portion of vitreous carbon surrounds the radioisotope containing portion, the two portions of vitreous carbon being integrally formed as a single unit. Connecting means are provided at each end of the cylindrical body to permit connections to blood- carrying vessels and to provide for passage of blood through the bore. In a preferred embodiment, the radioisotope is thulium-170 which is present in the irradiator in the form of thulium oxide. A method of producing the preferred blood irradiator is also provided, whereby nonradioactive thulium-169 is dispersed within a polyfurfuryl alcohol resin which is carbonized and fired to form the integral vitreous carbon body and the device is activated by neutron bombardment of the thulium-169 to produce the beta-emitting thulium-170.

  3. Kalman-filtered compressive sensing for high resolution estimation of anthropogenic greenhouse gas emissions from sparse measurements.

    SciTech Connect (OSTI)

    Ray, Jaideep; Lee, Jina; Lefantzi, Sophia; Yadav, Vineet; Michalak, Anna M.; van Bloemen Waanders, Bart Gustaaf; McKenna, Sean Andrew

    2013-09-01

    The estimation of fossil-fuel CO2 emissions (ffCO2) from limited ground-based and satellite measurements of CO2 concentrations will form a key component of the monitoring of treaties aimed at the abatement of greenhouse gas emissions. The limited nature of the measured data leads to a severely-underdetermined estimation problem. If the estimation is performed at fine spatial resolutions, it can also be computationally expensive. In order to enable such estimations, advances are needed in the spatial representation of ffCO2 emissions, scalable inversion algorithms and the identification of observables to measure. To that end, we investigate parsimonious spatial parameterizations of ffCO2 emissions which can be used in atmospheric inversions. We devise and test three random field models, based on wavelets, Gaussian kernels and covariance structures derived from easily-observed proxies of human activity. In doing so, we constructed a novel inversion algorithm, based on compressive sensing and sparse reconstruction, to perform the estimation. We also address scalable ensemble Kalman filters as an inversion mechanism and quantify the impact of Gaussian assumptions inherent in them. We find that the assumption does not impact the estimates of mean ffCO2 source strengths appreciably, but a comparison with Markov chain Monte Carlo estimates show significant differences in the variance of the source strengths. Finally, we study if the very different spatial natures of biogenic and ffCO2 emissions can be used to estimate them, in a disaggregated fashion, solely from CO2 concentration measurements, without extra information from products of incomplete combustion e.g., CO. We find that this is possible during the winter months, though the errors can be as large as 50%.

  4. HIGH-RESOLUTION MID-INFRARED IMAGING OF THE CIRCUMSTELLAR DISKS OF HERBIG Ae/Be STARS

    SciTech Connect (OSTI)

    Marinas, N.; Telesco, C. M.; Packham, C.; Fisher, R. S.

    2011-08-20

    We have imaged the circumstellar environments of 17 Herbig Ae/Be stars at 12 and 18 {mu}m using MICHELLE on Gemini North and T-ReCS on Gemini South. Our sample contained eight Group I sources, those having large rising near- to far-infrared (IR) fluxes, and nine Group II sources, those having more modest mid-IR fluxes relative to their near-IR flux (in the classification of Meeus et al.). We have resolved extended emission from all Group I sources in our target list. The majority of these sources have radially symmetric mid-IR emission extending from a radius of 10 AU to hundreds of AU. Only one of the nine Group II sources is resolved at the FWHM level, with another two Group II sources resolved at fainter levels. Models by Dullemond et al. explain the observed spectral energy distribution of Group II sources using self-shadowed cold disks. If this is the case for all the Group II sources, we do not expect to detect extended emission with this study, since the IR emission measured should arise from a region only a few AU in size, which is smaller than our resolution. The fact that we do resolve some of the Group II sources implies that their disks are not completely flat, and might represent an intermediate stage. We also find that none of the more massive (>3 M{sub sun}) Herbig Ae/Be stars in our sample belongs to Group I, which may point to a relationship between stellar mass and circumstellar dust evolution. Disks around more massive stars might evolve faster so that stars are surrounded by a more evolved flat disk by the time they become optically visible, or they might follow a different evolutionary path altogether.

  5. High energy resolution five-crystal spectrometer for high quality fluorescence and absorption measurements on an x-ray absorption spectroscopy beamline

    SciTech Connect (OSTI)

    Llorens, Isabelle; Lahera, Eric; Delnet, William; Proux, Olivier; Dermigny, Quentin; Gelebart, Frederic; Morand, Marc; Shukla, Abhay; Bardou, Nathalie; Ulrich, Olivier; and others

    2012-06-15

    Fluorescence detection is classically achieved with a solid state detector (SSD) on x-ray absorption spectroscopy (XAS) beamlines. This kind of detection however presents some limitations related to the limited energy resolution and saturation. Crystal analyzer spectrometers (CAS) based on a Johann-type geometry have been developed to overcome these limitations. We have tested and installed such a system on the BM30B/CRG-FAME XAS beamline at the ESRF dedicated to the structural investigation of very dilute systems in environmental, material and biological sciences. The spectrometer has been designed to be a mobile device for easy integration in multi-purpose hard x-ray synchrotron beamlines or even with a laboratory x-ray source. The CAS allows to collect x-ray photons from a large solid angle with five spherically bent crystals. It will cover a large energy range allowing to probe fluorescence lines characteristic of all the elements from Ca (Z = 20) to U (Z = 92). It provides an energy resolution of 1-2 eV. XAS spectroscopy is the main application of this device even if other spectroscopic techniques (RIXS, XES, XRS, etc.) can be also achieved with it. The performances of the CAS are illustrated by two experiments that are difficult or impossible to perform with SSD and the complementarity of the CAS vs SSD detectors is discussed.

  6. Development of a High Resolution, Real Time, Distribution-Level Metering System and Associated Visualization, Modeling, and Data Analysis Functions

    SciTech Connect (OSTI)

    Bank, J.; Hambrick, J.

    2013-05-01

    NREL is developing measurement devices and a supporting data collection network specifically targeted at electrical distribution systems to support research in this area. This paper describes the measurement network which is designed to apply real-time and high speed (sub-second) measurement principles to distribution systems that are already common for the transmission level in the form of phasor measurement units and related technologies.

  7. COLLABORATIVE RESEARCH: TOWARDS ADVANCED UNDERSTANDING AND PREDICTIVE CAPABILITY OF CLIMATE CHANGE IN THE ARCTIC USING A HIGH-RESOLUTION REGIONAL ARCTIC CLIMATE SYSTEM MODEL

    SciTech Connect (OSTI)

    Gutowski, William J.

    2013-02-07

    The motivation for this project was to advance the science of climate change and prediction in the Arctic region. Its primary goals were to (i) develop a state-of-the-art Regional Arctic Climate system Model (RACM) including high-resolution atmosphere, land, ocean, sea ice and land hydrology components and (ii) to perform extended numerical experiments using high performance computers to minimize uncertainties and fundamentally improve current predictions of climate change in the northern polar regions. These goals were realized first through evaluation studies of climate system components via one-way coupling experiments. Simulations were then used to examine the effects of advancements in climate component systems on their representation of main physics, time-mean fields and to understand variability signals at scales over many years. As such this research directly addressed some of the major science objectives of the BER Climate Change Research Division (CCRD) regarding the advancement of long-term climate prediction.

  8. Oxidized crystalline (3 1)-O surface phases of InAs and InSb studied by high-resolution photoelectron spectroscopy

    SciTech Connect (OSTI)

    Tuominen, M. E-mail: pekka.laukkanen@utu.fi; Lng, J.; Dahl, J.; Yasir, M.; Mkel, J.; Punkkinen, M. P. J.; Laukkanen, P. E-mail: pekka.laukkanen@utu.fi; Kokko, K.; Kuzmin, M.; Osiecki, J. R.; Schulte, K.

    2015-01-05

    The pre-oxidized crystalline (31)-O structure of InAs(100) has been recently found to significantly improve insulator/InAs junctions for devices, but the atomic structure and formation of this useful oxide layer are not well understood. We report high-resolution photoelectron spectroscopy analysis of (31)-O on InAs(100) and InSb(100). The findings reveal that the atomic structure of (31)-O consists of In atoms with unexpected negative (between ?0.64 and ?0.47?eV) and only moderate positive (In{sub 2}O type) core-level shifts; highly oxidized group-V sites; and four different oxygen sites. These fingerprint shifts are compared to those of previously studied oxides of III-V to elucidate oxidation processes.

  9. Application of high-resolution time-of-flight chemical ionization mass spectrometry measurements to estimate volatility distributions of α-pinene and naphthalene oxidation products

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Chhabra, P. S.; Lambe, A. T.; Canagaratna, M. R.; Stark, H.; Jayne, J. T.; Onasch, T. B.; Davidovits, P.; Kimmel, J. R.; Worsnop, D. R.

    2015-01-05

    Recent developments in high-resolution time-of-flight chemical ionization mass spectrometry (HR-ToF-CIMS) have made it possible to directly detect atmospheric organic compounds in real time with high sensitivity and with little or no fragmentation, including low-volatility, highly oxygenated organic vapors that are precursors to secondary organic aerosol formation. Here, using ions identified by high-resolution spectra from an HR-ToF-CIMS with acetate reagent ion chemistry, we develop an algorithm to estimate the vapor pressures of measured organic acids. The algorithm uses identified ion formulas and calculated double bond equivalencies, information unavailable in quadrupole CIMS technology, as constraints for the number of possible oxygen-containing functionalmore » groups. The algorithm is tested with acetate chemical ionization mass spectrometry (acetate-CIMS) spectra of O3 and OH oxidation products of α-pinene and naphthalene formed in a flow reactor with integrated OH exposures ranged from 1.2 × 1011 to 9.7 × 1011 molec s cm−3, corresponding to approximately 1.0 to 7.5 days of equivalent atmospheric oxidation. Measured gas-phase organic acids are similar to those previously observed in environmental chamber studies. For both precursors, we find that acetate-CIMS spectra capture both functionalization (oxygen addition) and fragmentation (carbon loss) as a function of OH exposure. The level of fragmentation is observed to increase with increased oxidation. The predicted condensed-phase secondary organic aerosol (SOA) average acid yields and O/C and H/C ratios agree within uncertainties with previous chamber and flow reactor measurements and ambient CIMS results. While acetate reagent ion chemistry is used to selectively measure organic acids, in principle this method can be applied to additional reagent ion chemistries depending on the application.« less

  10. Irradiation subassembly

    DOE Patents [OSTI]

    Seim, O.S.; Filewicz, E.C.; Hutter, E.

    1973-10-23

    An irradiation subassembly for use in a nuclear reactor is described which includes a bundle of slender elongated irradiation -capsules or fuel elements enclosed by a coolant tube and having yieldable retaining liner between the irradiation capsules and the coolant tube. For a hexagonal bundle surrounded by a hexagonal tube the yieldable retaining liner may consist either of six segments corresponding to the six sides of the tube or three angular segments each corresponding in two adjacent sides of the tube. The sides of adjacent segments abut and are so cut that metal-tometal contact is retained when the volume enclosed by the retaining liner is varied and Springs are provided for urging the segments toward the center of the tube to hold the capsules in a closely packed configuration. (Official Gazette)

  11. PROJECT PROFILE: Rapid QSTS Simulations for High-Resolution Comprehensive Assessment of Distributed PV Impacts (SuNLaMP)

    Broader source: Energy.gov [DOE]

    This project, led by Sandia National Laboratory and supported by the National Renewable Energy Laboratory, will accelerate Quasi Static Time Series (QSTS) simulation capabilities through the use of new and innovative methods for advanced time-series analysis. Currently, QSTS analysis is not commonly performed in photovoltaic (PV) interconnection studies because of the data requirements and computational burden. This project will address both of these issues by developing advanced QSTS methods that greatly reduce the required computational time and by developing high-proxy data sets.

  12. Visual Comfort Analysis of Innovative Interior and Exterior Shading Systems for Commercial Buildings using High Resolution Luminance Images

    SciTech Connect (OSTI)

    Konis, Kyle; Lee, Eleanor; Clear, Robert

    2011-01-11

    The objective of this study was to explore how calibrated high dynamic range (HDR) images (luminance maps) acquired in real world daylit environments can be used to characterize, evaluate, and compare visual comfort conditions of innovative facade shading and light-redirecting systems. Detailed (1536 x 1536 pixel) luminance maps were time-lapse acquired from two view positions in an unoccupied full scale testbed facility. These maps were analyzed using existing visual comfort metrics to quantify how innovative interior and exterior shading systems compare to conventional systems under real sun and sky conditions over a solstice-to-solstice test interval. The results provide a case study in the challenges and potential of methods of visualizing, evaluating and summarizing daily and seasonal variation of visual comfort conditions computed from large sets of image data.

  13. Mapping pan-Arctic methane emissions at high spatial resolution using an adjoint atmospheric transport and inversion method and process-based wetland and lake biogeochemical models

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Tan, Z.; Zhuang, Q.; Henze, D. K.; Frankenberg, C.; Dlugokencky, E.; Sweeney, C.; Turner, A. J.

    2015-11-18

    Understanding methane emissions from the Arctic, a fast warming carbon reservoir, is important for projecting changes in the global methane cycle under future climate scenarios. Here we optimize Arctic methane emissions with a nested-grid high-resolution inverse model by assimilating both high-precision surface measurements and column-average SCIAMACHY satellite retrievals of methane mole fraction. For the first time, methane emissions from lakes are integrated into an atmospheric transport and inversion estimate, together with prior wetland emissions estimated by six different biogeochemical models. We find that, the global methane emissions during July 2004June 2005 ranged from 496.4 to 511.5 Tg yr?1, with wetlandmoremethane emissions ranging from 130.0 to 203.3 Tg yr?1. The Arctic methane emissions during July 2004June 2005 were in the range of 14.630.4 Tg yr?1, with wetland and lake emissions ranging from 8.8 to 20.4 Tg yr?1 and from 5.4 to 7.9 Tg yr?1 respectively. Canadian and Siberian lakes contributed most of the estimated lake emissions. Due to insufficient measurements in the region, Arctic methane emissions are less constrained in northern Russia than in Alaska, northern Canada and Scandinavia. Comparison of different inversions indicates that the distribution of global and Arctic methane emissions is sensitive to prior wetland emissions. Evaluation with independent datasets shows that the global and Arctic inversions improve estimates of methane mixing ratios in boundary layer and free troposphere. The high-resolution inversions provide more details about the spatial distribution of methane emissions in the Arctic.less

  14. Time-Resolved Quantitative Measurement of OH HO2 and CH2O in Fuel Oxidation Reactions by High Resolution IR Absorption Spectroscopy.

    SciTech Connect (OSTI)

    Huang, Haifeng; Rotavera, Brandon; Taatjes, Craig A.

    2014-08-01

    Combined with a Herriott-type multi-pass slow flow reactor, high-resolution differential direct absorption spectroscopy has been used to probe, in situ and quantitatively, hydroxyl (OH), hydroperoxy (HO 2 ) and formaldehyde (CH 2 O) molecules in fuel oxidation reactions in the reactor, with a time resolution of about 1 micro-second. While OH and CH 2 O are probed in the mid-infrared (MIR) region near 2870nm and 3574nm respectively, HO 2 can be probed in both regions: near-infrared (NIR) at 1509nm and MIR at 2870nm. Typical sensitivities are on the order of 10 10 - 10 11 molecule cm -3 for OH at 2870nm, 10 11 molecule cm -3 for HO 2 at 1509nm, and 10 11 molecule cm -3 for CH 2 O at 3574nm. Measurements of multiple important intermediates (OH and HO 2 ) and product (CH 2 O) facilitate to understand and further validate chemical mechanisms of fuel oxidation chemistry.

  15. A high resolution and large solid angle x-ray Raman spectroscopy end-station at the Stanford Synchrotron Radiation Lightsource

    SciTech Connect (OSTI)

    Sokaras, D.; Nordlund, D.; Weng, T.-C.; Velikov, P.; Wenger, D.; Garachtchenko, A.; George, M.; Borzenets, V.; Johnson, B.; Rabedeau, T.; Mori, R. Alonso; Bergmann, U.; Qian, Q.

    2012-04-15

    We present a new x-ray Raman spectroscopy end-station recently developed, installed, and operated at the Stanford Synchrotron Radiation Lightsource. The end-station is located at wiggler beamline 6-2 equipped with two monochromators-Si(111) and Si(311) as well as collimating and focusing optics. It consists of two multi-crystal Johann type spectrometers arranged on intersecting Rowland circles of 1 m diameter. The first one, positioned at the forward scattering angles (low-q), consists of 40 spherically bent and diced Si(110) crystals with 100 mm diameters providing about 1.9% of 4{pi} sr solid angle of detection. When operated in the (440) order in combination with the Si (311) monochromator, an overall energy resolution of 270 meV is obtained at 6462.20 eV. The second spectrometer, consisting of 14 spherically bent Si(110) crystal analyzers (not diced), is positioned at the backward scattering angles (high-q) enabling the study of non-dipole transitions. The solid angle of this spectrometer is about 0.9% of 4{pi} sr, with a combined energy resolution of 600 meV using the Si (311) monochromator. These features exceed the specifications of currently existing relevant instrumentation, opening new opportunities for the routine application of this photon-in/photon-out hard x-ray technique to emerging research in multidisciplinary scientific fields, such as energy-related sciences, material sciences, physical chemistry, etc.

  16. Design, Construction, and Initial Test of High Spatial Resolution Thermometry Arrays for Detection of Surface Temperature Profiles on SRF Cavities in Super Fluid Helium

    SciTech Connect (OSTI)

    Ari Palczewski, Rongli Geng, Grigory Eremeev

    2011-07-01

    We designed and built two high resolution (0.6-0.55mm special resolution [1.1-1.2mm separation]) thermometry arrays prototypes out of the Allen Bradley 90-120 ohm 1/8 watt resistor to measure surface temperature profiles on SRF cavities. One array was designed to be physically flexible and conform to any location on a SRF cavity; the other was modeled after the common G-10/stycast 2850 thermometer and designed to fit on the equator of an ILC (Tesla 1.3GHz) SRF cavity. We will discuss the advantages and disadvantages of each array and their construction. In addition we will present a case study of the arrays performance on a real SRF cavity TB9NR001. TB9NR001 presented a unique opportunity to test the performance of each array as it contained a dual (4mm separation) cat eye defect which conventional methods such as OST (Oscillating Superleak second-sound Transducers) and full coverage thermometry mapping were unable to distinguish between. We will discuss the new arrays ability to distinguish between the two defects and their preheating performance.

  17. High-resolution Elemental Mapping of Human Placental Chorionic Villi Using Synchrotron X-ray Fluorescence Spectroscopy

    SciTech Connect (OSTI)

    Punshon, Tracy; Chen, Si; Finney, Lydia; Howard, Louisa; Jackson, Brian P.; Karagas, Margaret R.; Ornvold, Kim

    2015-09-01

    The placenta is the organ that mediates transport of nutrients and waste materials between mother and fetus. Synchrotron X-ray fluorescence (SXRF) microanalysis is a tool for imaging the distribution and quantity of elements in biological tissue, which can be used to study metal transport across biological membranes. Our aims were to pilot placental biopsy specimen preparation techniques that could be integrated into an ongoing epidemiology birth cohort study without harming rates of sample acquisition. We studied the effects of fixative (formalin or glutaraldehyde) and storage duration (30 days or immediate processing) on metal distribution and abundance and investigated a thaw-fixation protocol for archived specimens stored at -80 A degrees C. We measured fixative elemental composition with and without a placental biopsy via inductively coupled plasma mass spectrometry (ICP-MS) to quantify fixative-induced elemental changes. Formalin-fixed specimens showed hemolysis of erythrocytes. The glutaraldehyde-paraformaldehyde solution in HEPES buffer (GTA-HEPES) had superior anatomical preservation, avoided hemolysis, and minimized elemental loss, although some cross-linking of exogenous Zn was evident. Elemental loss from tissue stored in fixative for 1 month showed variable losses (a parts per thousand 40 % with GTA-HEPES), suggesting storage duration be controlled for. Thawing of tissue held at -80 A degrees C in a GTA-HEPES solution provided high-quality visual images and elemental images

  18. Surface water processes in the Indonesian Throughflow as documented by a high-resolution coral (Delta)14C record

    SciTech Connect (OSTI)

    Fallon, S J; Guilderson, T P

    2008-04-23

    To explore the seasonal to decadal variability in surface water masses that contribute to the Indonesian Throughflow we have generated a 115-year bi-monthly coral-based radiocarbon time-series from a coral in the Makassar Straits. In the pre-bomb (pre-1955) era from 1890 to 1954, the radiocarbon time series occasionally displays a small seasonal signal (10-15{per_thousand}). After 1954 the radiocarbon record increases rapidly, in response to the increased atmospheric {sup 14}C content caused by nuclear weapons testing. From 1957 to 1986 the record displays clear seasonal variability from 15 to 60{per_thousand} and the post-bomb peak (163 per mil) occurred in 1974. The seasonal cycle of radiocarbon can be attributed to variations of surface waters passing through South Makassar Strait. Southern Makassar is under the influence of the Northwest Monsoon, which is responsible for the high Austral summer radiocarbon (North Pacific waters) and the Southeast Monsoon that flushes back a mixture of low (South Pacific and upwelling altered) radiocarbon water from the Banda Sea. The coral record also shows a significant {sup 14}C peak in 1955 due to bomb {sup 14}C water advected into this region in the form of CaCO{sub 3} particles (this implies that the particles were advected intact and then become entrapped in the coral skeleton--is this what we really mean? Wouldn't even fine particles settle out over the inferred transit time from Bikini to MAK?) or water particles with dissolved labeled CO{sub 2} produced during fallout from the Castle tests in 1954.

  19. Atomic arrangement at ZnTe/CdSe interfaces determined by high resolution scanning transmission electron microscopy and atom probe tomography

    SciTech Connect (OSTI)

    Bonef, Bastien; Rouvire, Jean-Luc; Jouneau, Pierre-Henri; Bellet-Amalric, Edith; Grard, Lionel; Mariette, Henri; Andr, Rgis; Bougerol, Catherine; Grenier, Adeline

    2015-02-02

    High resolution scanning transmission electron microscopy and atom probe tomography experiments reveal the presence of an intermediate layer at the interface between two binary compounds with no common atom, namely, ZnTe and CdSe for samples grown by Molecular Beam Epitaxy under standard conditions. This thin transition layer, of the order of 1 to 3 atomic planes, contains typically one monolayer of ZnSe. Even if it occurs at each interface, the direct interface, i.e., ZnTe on CdSe, is sharper than the reverse one, where the ZnSe layer is likely surrounded by alloyed layers. On the other hand, a CdTe-like interface was never observed. This interface knowledge is crucial to properly design superlattices for optoelectronic applications and to master band-gap engineering.

  20. Advanced Reservoir Characterization and Development through High-Resolution 3C3D Seismic and Horizontal Drilling: Eva South Marrow Sand Unit, Texas County, Oklahoma

    SciTech Connect (OSTI)

    Wheeler,David M.; Miller, William A.; Wilson, Travis C.

    2002-03-11

    The Eva South Morrow Sand Unit is located in western Texas County, Oklahoma. The field produces from an upper Morrow sandstone, termed the Eva sandstone, deposited in a transgressive valley-fill sequence. The field is defined as a combination structural stratigraphic trap; the reservoir lies in a convex up -dip bend in the valley and is truncated on the west side by the Teepee Creek fault. Although the field has been a successful waterflood since 1993, reservoir heterogeneity and compartmentalization has impeded overall sweep efficiency. A 4.25 square mile high-resolution, three component three-dimensional (3C3D) seismic survey was acquired in order to improve reservoir characterization and pinpoint the optimal location of a new horizontal producing well, the ESU 13-H.

  1. Application of PILATUS II Detector Modules for High Resolution X-Ray Imaging Crystal Spectrometers on the Alcator C-Mod Tokamak

    SciTech Connect (OSTI)

    M.L. Bitter, Ch. Borennimann, E.F. Eikenberry, K.W. Hill, A. Ince-Chushman, S.G. Lee, J.E. Rice, and S. Scott.

    2007-07-23

    A new type of X-ray imaging crystal spectrometer for Doppler measurements of the radial profiles of the ion temperature and plasma rotation velocity in tokamak plasmas is presently being developed in a collaboration between various laboratories. The spectrometer will consist of a spherically bent crystal and a two-dimensional position sensitive detector; and it will record temporally and spatially resolved X-ray line spectra from highly-charged ions. The detector must satisfy challenging requirements with respect to count rate and spatial resolution. The paper presents the results from a recent test of a PILATUS II detector module on Alcator C-Mod, which demonstrate that the PILATUS II detector modules will satisfy these requirements.

  2. Study of Chelyabinsk LL5 meteorite fragment with a light lithology and its fusion crust using Mssbauer spectroscopy with a high velocity resolution

    SciTech Connect (OSTI)

    Maksimova, Alevtina A.; Petrova, Evgeniya V.; Grokhovsky, Victor I.; Oshtrakh, Michael I. Semionkin, Vladimir A.

    2014-10-27

    Study of Chelyabinsk LL5 ordinary chondrite fragment with a light lithology and its fusion crust, fallen on February 15, 2013, in Russian Federation, was carried out using Mssbauer spectroscopy with a high velocity resolution. The Mssbauer spectra of the internal matter and fusion crust were fitted and all components were related to iron-bearing phases such as olivine, pyroxene, troilite, Fe-Ni-Co alloy, and chromite in the internal matter and olivine, pyroxene, troilite, Fe-Ni-Co alloy, and magnesioferrite in the fusion crust. A comparison of the content of different phases in the internal matter and in the fusion crust of this fragment showed that ferric compounds resulted from olivine, pyroxene, and troilite combustion in the atmosphere.

  3. High-resolution study of 0{sup +} and 2{sup +} excitations in {sup 168}Er with the (p,t) reaction

    SciTech Connect (OSTI)

    Bucurescu, D. [Horia Hulubei National Institute of Physics and Nuclear Engineering, P.O. Box MG-6, R-76900 Bucharest (Romania); Graw, G.; Hertenberger, R. [Sektion Physik, Ludwig Maximilians Universitaet Muenchen, Am Coulombwall 1, D-85748 Garching (Germany); Wirth, H.-F.; Faestermann, T.; Kruecken, R.; Mahgoub, M. [Physik Department, Technische Universitaet Muenchen, D-85748 Garching (Germany); Lo Iudice, N. [Dipartimento di Scienze Fisiche, Universita di Napoli 'Federico II' and Istituto Nazionale di Fisica Nucleare, Monte S Angelo, Via Cintia I-80126 Naples (Italy); Sushkov, A.V.; Shirikova, N.Yu. [Bogoliubov Laboratory of Theoretical Physics, Joint Institute for Nuclear Research, RU-141980 Dubna (Russian Federation); Sun, Y. [Department of Physics and Joint Institute for Nuclear Astrophysics, University of Notre Dame, Notre Dame, Indiana 46556 (United States); Department of Physics, Tsinghua University, Beijing 100084 (China); Department of Physics, Xuzhou Normal University, Xuzhou, Jiangsu 221009 (China); Jolie, J.; Brentano, P. von; Braun, N.; Heinze, S.; Moeller, O.; Muecher, D.; Scholl, C. [Institut fuer Kernphysik, Universitaet zu Koeln, D-50937 Cologne (Germany); Casten, R.F.; Meyer, D.A. [Wright Nuclear Structure Laboratory, Yale University, New Haven, Connecticut 06520-8124 (United States)

    2006-06-15

    Excited states in the deformed nucleus {sup 168}Er have been studied with high-energy resolution, in the (p,t) reaction, with the Munich Q3D spectrograph. A number of 25 excited 0{sup +} states (four tentative) and 63 2{sup +} states have been assigned up to 4.0 MeV excitation energy. This unusually rich characterization of the 0{sup +} and 2{sup +} states in a deformed nucleus, close to a complete level scheme, offers a unique opportunity to check, in detail, models of nuclear structure that incorporate many excitation modes. A comparison of the experimental data is made with two such models: the quasiparticle-phonon model (QPM), and the projected shell model (PSM). The PSM wave functions appear to contain fewer correlations than those of the QPM and than required by the data.

  4. Multi-wavelength high-resolution observations of a small-scale emerging magnetic flux event and the chromospheric and coronal response

    SciTech Connect (OSTI)

    Vargas Domínguez, Santiago; Kosovichev, Alexander; Yurchyshyn, Vasyl

    2014-10-20

    State-of-the-art solar instrumentation is now revealing magnetic activity of the Sun with unprecedented temporal and spatial resolutions. Observations with the 1.6 m aperture New Solar Telescope (NST) of the Big Bear Solar Observatory are making next steps in our understanding of the solar surface structure. Granular-scale magnetic flux emergence and the response of the solar atmosphere are among the key research topics of high-resolution solar physics. As part of a joint observing program with NASA's Interface Region Imaging Spectrograph (IRIS) mission on 2013 August 7, the NST observed active region NOAA 11,810 in the photospheric TiO 7057 Å band with a resolution of pixel size of 0.''034 and chromospheric He I 10830 Å and Hα 6563 Å wavelengths. Complementary data are provided by the Solar Dynamics Observatory (SDO) and Hinode space-based telescopes. The region displayed a group of solar pores, in the vicinity of which we detect a small-scale buoyant horizontal magnetic flux tube causing granular alignments and interacting with the preexisting ambient field in the upper atmospheric layers. Following the expansion of distorted granules at the emergence site, we observed a sudden appearance of an extended surge in the He I 10830 Å data (bandpass of 0.05 Å). The IRIS transition region imaging caught ejection of a hot plasma jet associated with the He I surge. The SDO/HMI data used to study the evolution of the magnetic and Doppler velocity fields reveal emerging magnetic loop-like structures. Hinode/Ca II H and IRIS filtergrams detail the connectivities of the newly emerged magnetic field in the lower solar chromosphere. From these data, we find that the orientation of the emerging magnetic field lines from a twisted flux tube formed an angle of ∼45° with the overlying ambient field. Nevertheless, the interaction of emerging magnetic field lines with the pre-existing overlying field generates high-temperature emission regions and boosts the surge/jet production. The localized heating is detected before and after the first signs of the surge/jet ejection. We compare the results with previous observations and theoretical models and propose a scenario for the activation of plasma jet/surges and confined heating triggered by buoyant magnetic flux tubes rising up into a magnetized upper environment. Such process may play a significant role in the mass and energy flow from the interior to the corona.

  5. WE-G-BRE-01: A High Power Nanotube X-Ray Microbeam Irradiator for Preclinical Brain Tumor Treatment

    SciTech Connect (OSTI)

    Chtcheprov, P; Inscoe, C; Zhang, L; Lu, J; Zhou, O; Chang, S; Sprenger, F; Laganis, P

    2014-06-15

    Purpose: Microbeam radiation therapy (MRT) is a new type of cancer treatment undergoing studies at various synchrotron facilities. The principle of MRT is using arrays of microscopically small, low-energy X-radiation for the treatment of various radio-resistant, deep-seated tumors. Our motivation is to develop a compact and inexpensive image guided MRT irradiator to use in the research lab setting. After a successful initial demonstration, here we report a second generation carbon nanotube (CNT) cathode based MRT tube, capable of producing multiple microbeam lines with an anticipated dose rate of 11 Gy/min per line. Methods: The system uses multiple line CNT source arrays to generate multiple focal lines on the anode. The increase in dose-rate, compared to our first generation system, is achieved by increasing the operating voltage from 160 kVp to 225kVp, adding multiple simultaneous focal lines on the anode, and a more efficient cooling mechanism using a 6kW oil-cooled anode. Results: This work will present the design and development process, challenges and solutions to meeting operating specifications, and the final design of the tube and collimator, along with optimization and stabilization of its use. A detailed characterization of its capabilities will be included with a comprehensive measurement of its X-ray focal line dimensions, an evaluation of its collimator alignment and microbeam dimensions, and phantom-based quantification of its dosimetric output. Conclusion: The development of a second generation, compact, multiple line MRT device using carbon nanotube (CNT) cathode based X-ray technology and a novel oil cooled anode design is presented here. With this new source, we are capable of delivering a total microbeam radiation dose comparable to the low end of the synchrotron based MRT systems for small animal brain tumor models.

  6. A high-resolution whole genome radiation hybrid map of human chromosome 17q22-q25.3 across the genes for GH and TK

    SciTech Connect (OSTI)

    Foster, J.W.; Schafer, A.J.; Critcher, R.

    1996-04-15

    We have constructed a whole genome radiation hybrid (WG-RH) map across a region of human chromosome 17q, from growth hormone (GH) to thymidine kinase (TK). A panel of 128 WG-RH hybrid cell lines generated by X-irradiation and fusion has been tested for the retention of 39 sequence-tagged site (STS) markers by the polymerase chain reaction. This genome mapping technique has allowed the integration of existing VNTR and microsatellite markers with additional new markers and existing STS markers previously mapped to this region by other means. The WG-RH map includes eight expressed sequence tag (EST) and three anonymous markers developed for this study, together with 23 anonymous microsatellites and five existing ESTs. Analysis of these data resulted in a high-density comprehensive map across this region of the genome. A subset of these markers has been used to produce a framework map consisting of 20 loci ordered with odds greater than 1000:1. The markers are of sufficient density to build a YAC contig across this region based on marker content. We have developed sequence tags for both ends of a 2.1-Mb YAC and mapped these using the WG-RH panel, allowing a direct comparison of cRay{sub 6000} to physical distance. 31 refs., 3 figs., 2 tabs.

  7. Time-resolved x-ray imaging of high-power laser-irradiated under-dense silica aerogels and agar foams

    SciTech Connect (OSTI)

    Koch, J.A.; Estabrook, K.G.; Bauer, J.D. [and others

    1995-08-01

    This paper presents the results of experiments in which a high-power laser was used to irradiate low density (4 - 9 mg/cm{sup 3}) silica aerogel and agar foam targets. The laser-solid interaction and energy transport through the material were monitored with time-resolved imaging diagnostics, and the data show the production and propagation of an x-ray emission front in the plasma. The emission-front trajectory data are found to be in significant disagreement with detailed simulations, which predict a much more rapid heating of the cold material, and the data suggest that this discrepancy is not explainable by target inhomogeneities. Evidence suggests that energy transport into the cold material may be dominated by thermal conduction; however, no completely satisfactory explanation for the discrepancies is identified, and further experimental and theoretical research is necessary in order to resolve this important problem in laser-plasma interaction physics.

  8. BIOLOGICAL IRRADIATION FACILITY

    DOE Patents [OSTI]

    McCorkle, W.H.; Cern, H.S.

    1962-04-24

    A facility for irradiating biological specimens with neutrons is described. It includes a reactor wherein the core is off center in a reflector. A high-exposure room is located outside the reactor on the side nearest the core while a low-exposure room is located on the opposite side. Means for converting thermal neutrons to fast neutrons are movably disposed between the reactor core and the high and low-exposure rooms. (AEC)

  9. High spatial resolution particle detectors

    DOE Patents [OSTI]

    Boatner, Lynn A.; Mihalczo, John T.

    2012-09-04

    Disclosed below are representative embodiments of methods, apparatus, and systems for detecting particles, such as radiation or charged particles. One exemplary embodiment disclosed herein is particle detector comprising an optical fiber with a first end and second end opposite the first end. The optical fiber of this embodiment further comprises a doped region at the first end and a non-doped region adjacent to the doped region. The doped region of the optical fiber is configured to scintillate upon interaction with a target particle, thereby generating one or more photons that propagate through the optical fiber and to the second end. Embodiments of the disclosed technology can be used in a variety of applications, including associated particle imaging and cold neutron scattering.

  10. High spatial resolution particle detectors

    DOE Patents [OSTI]

    Boatner, Lynn A.; Mihalczo, John T.

    2015-10-13

    Disclosed below are representative embodiments of methods, apparatus, and systems for detecting particles, such as radiation or charged particles. One exemplary embodiment disclosed herein is particle detector comprising an optical fiber with a first end and second end opposite the first end. The optical fiber of this embodiment further comprises a doped region at the first end and a non-doped region adjacent to the doped region. The doped region of the optical fiber is configured to scintillate upon interaction with a target particle, thereby generating one or more photons that propagate through the optical fiber and to the second end. Embodiments of the disclosed technology can be used in a variety of applications, including associated particle imaging and cold neutron scattering.

  11. High resolution printing of charge

    DOE Patents [OSTI]

    Rogers, John; Park, Jang-Ung

    2015-06-16

    Provided are methods of printing a pattern of charge on a substrate surface, such as by electrohydrodynamic (e-jet) printing. The methods relate to providing a nozzle containing a printable fluid, providing a substrate having a substrate surface and generating from the nozzle an ejected printable fluid containing net charge. The ejected printable fluid containing net charge is directed to the substrate surface, wherein the net charge does not substantially degrade and the net charge retained on the substrate surface. Also provided are functional devices made by any of the disclosed methods.

  12. High resolution track etch autoradiography

    DOE Patents [OSTI]

    Solares, G.; Zamenhof, R.G.

    1994-12-27

    A detector assembly is disclosed for use in obtaining alpha-track autoradiographs, the detector assembly including a substantially boron-free substrate; a detector layer deposited on the substantially boron-free substrate, the detector layer being capable of recording alpha particle tracks and exhibiting evidence of the alpha tracks in response to being exposed to an etchant, the detector layer being less than about 2 microns thick; and a protective layer deposited on the detector layer, the protective layer being resistant to the etchant and having a thickness of about 0.5 to 1 microns. 13 figures.

  13. High resolution track etch autoradiography

    DOE Patents [OSTI]

    Solares, Guido (Arlington, MA); Zamenhof, Robert G. (Brookline, MA)

    1994-01-01

    A detector assembly for use in obtaining alpha-track autoradiographs, the detector assembly including a substantially boron-free substrate; a detector layer deposited on the substantially boron-free substrate, the detector layer being capable of recording alpha particle tracks and exhibiting evidence of the alpha tracks in response to being exposed to an etchant, the detector layer being less than about 2 microns thick; and a protective layer deposited on the detector layer, the protective layer being resistant to the etchant and having a thickness of about 0.5 to 1 microns.

  14. STELLAR CORONAE, SOLAR FLARES: A DETAILED COMPARISON OF {sigma} GEM, HR 1099, AND THE SUN IN HIGH-RESOLUTION X-RAYS

    SciTech Connect (OSTI)

    Huenemoerder, David P.; Phillips, Kenneth J. H.; Sylwester, Janusz; Sylwester, Barbara E-mail: kennethjhphillips@yahoo.com E-mail: bs@cbk.pan.wroc.pl

    2013-05-10

    The Chandra High Energy Transmission Grating Spectrometer (HETG) spectra of the coronally active binary stars {sigma} Gem and HR 1099 are among the highest fluence observations for such systems taken at high spectral resolution in X-rays with this instrument. This allows us to compare their properties in detail to solar flare spectra obtained with the Russian CORONAS-F spacecraft's RESIK instrument at similar resolution in an overlapping bandpass. Here we emphasize the detailed comparisons of the 3.3-6.1 A region (including emission from highly ionized S, Si, Ar, and K) from solar flare spectra to the corresponding {sigma} Gem and HR 1099 spectra. We also model the larger wavelength range of the HETG, from 1.7 to 25 A - having emission lines from Fe, Ca, Ar, Si, Al, Mg, Ne, O, and N-to determine coronal temperatures and abundances. {sigma} Gem is a single-lined coronally active long-period binary which has a very hot corona. HR 1099 is a similar, but shorter period, double-lined system. With very deep HETG exposures we can even study emission from some of the weaker species, such as K, Na, and Al, which are important since they have the lowest first ionization potentials, a parameter well known to be correlated with elemental fractionation in the solar corona. The solar flare temperatures reach Almost-Equal-To 20 MK, comparable to the {sigma} Gem and HR 1099 coronae. During the Chandra exposures, {sigma} Gem was slowly decaying from a flare and its spectrum is well characterized by a collisional ionization equilibrium plasma with a broad temperature distribution ranging from 2 to 60 MK, peaking near 25 MK, but with substantial emission from 50 MK plasma. We have detected K XVIII and Na XI emission which allow us to set limits on their abundances. HR 1099 was also quite variable in X-rays, also in a flare state, but had no detectable K XVIII. These measurements provide new comparisons of solar and stellar coronal abundances, especially at the lowest first ionization potential (FIP) values. The low FIP elements do not show enhancement in the stellar coronae as they do in the Sun, except perhaps for K in {sigma} Gem. While {sigma} Gem and HR 1099 differ in their emission measure distributions, they have very similar elemental abundances.

  15. A HIGH SPATIAL RESOLUTION MID-INFRARED SPECTROSCOPIC STUDY OF THE NUCLEI AND STAR-FORMING REGIONS IN LUMINOUS INFRARED GALAXIES

    SciTech Connect (OSTI)

    Diaz-Santos, Tanio; Alonso-Herrero, Almudena; Colina, Luis; Pereira-Santaella, Miguel; Packham, Christopher; Telesco, Charles M.; Levenson, N. A.; Roche, Patrick F.

    2010-03-01

    We present a high spatial (diffraction-limited) resolution ({approx}0.''3) mid-infrared (MIR) spectroscopic study of the nuclei and star-forming regions of four local luminous infrared galaxies (LIRGs) using T-ReCS on the Gemini South telescope. We investigate the spatial variations of the features seen in the N-band spectra of LIRGs on scales of {approx}100 pc, which allow us to resolve their nuclear regions and separate the active galactic nucleus (AGN) emission from that of the star formation (SF). We compare (qualitatively and quantitatively) our Gemini T-ReCS nuclear and integrated spectra of LIRGs with those obtained with Spitzer IRS. Star-forming regions and AGNs show distinct features in the MIR spectra, and we spatially separate these, which is not possible using the Spitzer data. The 9.7 {mu}m silicate absorption feature is weaker in the nuclei of the LIRGs than in the surrounding regions. This is probably due to the either clumpy or compact environment of the central AGN or young, nuclear starburst. We find that the [Ne II]12.81 {mu}m luminosity surface density is tightly and directly correlated with that of Paalpha for the LIRG star-forming regions (slope of 1.00 +- 0.02). Although the 11.3 {mu}m PAH feature shows also a trend with Paalpha, this is not common for all the regions and the slope is significantly lower. We also find that the [Ne II]12.81 {mu}m/Paalpha ratio does not depend on the Paalpha equivalent width (EW), i.e., on the age of the ionizing stellar populations, suggesting that, on the scales probed here, the [Ne II]12.81 {mu}m emission line is a good tracer of the SF activity in LIRGs. On the other hand, the 11.3 {mu}m PAH/Paalpha ratio increases for smaller values of the Paalpha EW (increasing ages), indicating that the 11.3 {mu}m PAH feature can also be excited by older stars than those responsible for the Paalpha emission. Finally, more data are needed in order to address the different physical processes (age of the stellar populations, hardness and intensity of the radiation field, mass of the star-forming regions) affecting the energetics of the polycyclic aromatic hydrocarbon features in a statistical way. Additional high spatial resolution observations are essential to investigating the SF in local LIRGs at the smallest scales and determining ultimately whether they share the same physical properties as high-z LIRGs, ULIRGs, and submillimiter galaxies and therefore belong to the same galaxy population.

  16. Molecular Characterization of Organosulfates in Organic Aerosols from Shanghai and Los Angeles Urban Areas by Nanospray-Desorption Electrospray Ionization High-Resolution Mass Spectrometry

    SciTech Connect (OSTI)

    Tao, Shikang; Lu, Xiaohui; Levac, Nicole A.; Bateman, Adam P.; Nguyen, Tran B.; Bones, David L.; Nizkorodov, Sergey; Laskin, Julia; Laskin, Alexander; Yang, Xin

    2014-08-21

    Aerosol samples collected in the urban areas of Shanghai and Los Angeles were analyzed by nanospray-desorption electrospray ionization mass spectrometry (nano-DESI MS) with high mass resolution (m/?m=100,000). Solvent mixtures of acetonitrile/water and acetonitrile/toluene were used to extract and ionize polar and non-polar compounds, respectively. A diverse mixture of oxygenated hydrocarbons, organosulfates, organonitrates, and organics with reduced nitrogen were detected in the Los Angeles sample. Majority of the organics in the Shanghai sample were detected as organosulfates. The dominant organosulfates in the two samples have distinctly different molecular characteristics. Specifically, organosulfates in the Los Angeles sample were dominated by isoprene- or monoterpene-derived products, while organosulfates of yet unknown origin in the Shanghai sample had distinctive characteristics of long aliphatic carbon chains and low degree of oxidation and unsaturation. The use of acetonitrile/toluene solvent facilitated identification of this type of organosulfates, suggesting they could be missed in previous studies relying on sample extraction using common polar solvents. The high molecular weight and low degree of unsaturation and oxidization of the organosulfates detected in the Shanghai sample suggest that they may act as surfactants, and plausibly affect the surface tension and hygroscopicity of the atmospheric particulate matter. We propose that direct esterification of carbonyl or hydroxyl compounds by sulfates or sulfuric acid in liquid phase could be the formation pathway of these special organosulfates. Long-chain alkanes from vehicle emissions might be their precursors.

  17. HIGH-RESOLUTION CALCULATION OF THE SOLAR GLOBAL CONVECTION WITH THE REDUCED SPEED OF SOUND TECHNIQUE. II. NEAR SURFACE SHEAR LAYER WITH THE ROTATION

    SciTech Connect (OSTI)

    Hotta, H.; Rempel, M.; Yokoyama, T.

    2015-01-01

    We present a high-resolution, highly stratified numerical simulation of rotating thermal convection in a spherical shell. Our aim is to study in detail the processes that can maintain a near surface shear layer (NSSL) as inferred from helioseismology. Using the reduced speed of sound technique, we can extend our global convection simulation to 0.99 R {sub ?} and include, near the top of our domain, small-scale convection with short timescales that is only weakly influenced by rotation. We find the formation of an NSSL preferentially in high latitudes in the depth range of r = 0.95-0.975 R {sub ?}. The maintenance mechanisms are summarized as follows. Convection under the weak influence of rotation leads to Reynolds stresses that transport angular momentum radially inward in all latitudes. This leads to the formation of a strong poleward-directed meridional flow and an NSSL, which is balanced in the meridional plane by forces resulting from the ?v{sub r}{sup ?}v{sub ?}{sup ?}? correlation of turbulent velocities. The origin of the required correlations depends to some degree on latitude. In high latitudes, a positive correlation ?v{sub r}{sup ?}v{sub ?}{sup ?}? is induced in the NSSL by the poleward meridional flow whose amplitude increases with the radius, while a negative correlation is generated by the Coriolis force in bulk of the convection zone. In low latitudes, a positive correlation ?v{sub r}{sup ?}v{sub ?}{sup ?}? results from rotationally aligned convection cells ({sup b}anana cells{sup )}. The force caused by these Reynolds stresses is in balance with the Coriolis force in the NSSL.

  18. SU-E-CAMPUS-I-04: Automatic Skin-Dose Mapping for An Angiographic System with a Region-Of-Interest, High-Resolution Detector

    SciTech Connect (OSTI)

    Vijayan, S; Rana, V; Setlur Nagesh, S; Ionita, C; Rudin, S; Bednarek, D

    2014-06-15

    Purpose: Our real-time skin dose tracking system (DTS) has been upgraded to monitor dose for the micro-angiographic fluoroscope (MAF), a high-resolution, small field-of-view x-ray detector. Methods: The MAF has been mounted on a changer on a clinical C-Arm gantry so it can be used interchangeably with the standard flat-panel detector (FPD) during neuro-interventional procedures when high resolution is needed in a region-of-interest. To monitor patient skin dose when using the MAF, our DTS has been modified to automatically account for the change in scatter for the very small MAF FOV and to provide separated dose distributions for each detector. The DTS is able to provide a color-coded mapping of the cumulative skin dose on a 3D graphic model of the patient. To determine the correct entrance skin exposure to be applied by the DTS, a correction factor was determined by measuring the exposure at the entrance surface of a skull phantom with an ionization chamber as a function of entrance beam size for various beam filters and kVps. Entrance exposure measurements included primary radiation, patient backscatter and table forward scatter. To allow separation of the dose from each detector, a parameter log is kept that allows a replay of the procedure exposure events and recalculation of the dose components.The graphic display can then be constructed showing the dose distribution from the MAF and FPD separately or together. Results: The DTS is able to provide separate displays of dose for the MAF and FPD with field-size specific scatter corrections. These measured corrections change from about 49% down to 10% when changing from the FPD to the MAF. Conclusion: The upgraded DTS allows identification of the patient skin dose delivered when using each detector in order to achieve improved dose management as well as to facilitate peak skin-dose reduction through dose spreading. Research supported in part by Toshiba Medical Systems Corporation and NIH Grants R43FD0158401, R44FD0158402 and R01EB002873.

  19. A report on high-level nuclear waste transportation: Prepared pursuant to assembly concurrent resolution No. 8 of the 1987 Nevada Legislature

    SciTech Connect (OSTI)

    1988-12-01

    This report has been prepared by the staff of the State of Nevada Agency for Nuclear Projects/Nuclear Waste Project Office (NWPO) in response to Assembly Concurrent Resolution No. 8 (ACR 8), passed by the Nevada State Legislature in 1987. ACR 8 directed the NWPO, in cooperation with affected local governments and the Legislative committee on High-Level Radioactive Waste, to prepare this report which scrutinizes the US Department of Energy`s (DOE) plans for transportation of high-level radioactive waste to the proposed yucca Mountain repository, which reviews the regulatory structure under which shipments to a repository would be made and which presents NWPO`s plans for addressing high-level radioactive waste transportation issues. The report is divided into three major sections. Section 1.0 provides a review of DOE`s statutory requirements, its repository transportation program and plans, the major policy, programmatic, technical and institutional issues and specific areas of concern for the State of Nevada. Section 2.0 contains a description of the current federal, state and tribal transportation regulatory environment within which nuclear waste is shipped and a discussion of regulatory issues which must be resolved in order for the State to minimize risks and adverse impacts to its citizens. Section 3.0 contains the NWPO plan for the study and management of repository-related transportation. The plan addresses four areas, including policy and program management, regulatory studies, technical reviews and studies and institutional relationships. A fourth section provides recommendations for consideration by State and local officials which would assist the State in meeting the objectives of the plan.

  20. NSUF Irradiated Materials Library

    SciTech Connect (OSTI)

    Cole, James Irvin

    2015-09-01

    The Nuclear Science User Facilities has been in the process of establishing an innovative Irradiated Materials Library concept for maximizing the value of previous and on-going materials and nuclear fuels irradiation test campaigns, including utilization of real-world components retrieved from current and decommissioned reactors. When the ATR national scientific user facility was established in 2007 one of the goals of the program was to establish a library of irradiated samples for users to access and conduct research through competitively reviewed proposal process. As part of the initial effort, staff at the user facility identified legacy materials from previous programs that are still being stored in laboratories and hot-cell facilities at the INL. In addition other materials of interest were identified that are being stored outside the INL that the current owners have volunteered to enter into the library. Finally, over the course of the last several years, the ATR NSUF has irradiated more than 3500 specimens as part of NSUF competitively awarded research projects. The Logistics of managing this large inventory of highly radioactive poses unique challenges. This document will describe materials in the library, outline the policy for accessing these materials and put forth a strategy for making new additions to the library as well as establishing guidelines for minimum pedigree needed to be included in the library to limit the amount of material stored indefinitely without identified value.

  1. Indirect Tumor Cell Death After High-Dose Hypofractionated Irradiation: Implications for Stereotactic Body Radiation Therapy and Stereotactic Radiation Surgery

    SciTech Connect (OSTI)

    Song, Chang W.; Lee, Yoon-Jin; Griffin, Robert J.; Park, Inhwan; Koonce, Nathan A.; Hui, Susanta; Kim, Mi-Sook; Dusenbery, Kathryn E.; Sperduto, Paul W.; Cho, L. Chinsoo

    2015-09-01

    Purpose: The purpose of this study was to reveal the biological mechanisms underlying stereotactic body radiation therapy (SBRT) and stereotactic radiation surgery (SRS). Methods and Materials: FSaII fibrosarcomas grown subcutaneously in the hind limbs of C3H mice were irradiated with 10 to 30 Gy of X rays in a single fraction, and the clonogenic cell survival was determined with in vivo–in vitro excision assay immediately or 2 to 5 days after irradiation. The effects of radiation on the intratumor microenvironment were studied using immunohistochemical methods. Results: After cells were irradiated with 15 or 20 Gy, cell survival in FSaII tumors declined for 2 to 3 days and began to recover thereafter in some but not all tumors. After irradiation with 30 Gy, cell survival declined continuously for 5 days. Cell survival in some tumors 5 days after 20 to 30 Gy irradiation was 2 to 3 logs less than that immediately after irradiation. Irradiation with 20 Gy markedly reduced blood perfusion, upregulated HIF-1α, and increased carbonic anhydrase-9 expression, indicating that irradiation increased tumor hypoxia. In addition, expression of VEGF also increased in the tumor tissue after 20 Gy irradiation, probably due to the increase in HIF-1α activity. Conclusions: Irradiation of FSaII tumors with 15 to 30 Gy in a single dose caused dose-dependent secondary cell death, most likely by causing vascular damage accompanied by deterioration of intratumor microenvironment. Such indirect tumor cell death may play a crucial role in the control of human tumors with SBRT and SRS.

  2. Evaluation of stacking faults and associated partial dislocations in AlSb/GaAs (001) interface by aberration-corrected high-resolution transmission electron microscopy

    SciTech Connect (OSTI)

    Wen, C.; Ge, B. H.; Cui, Y. X.; Li, F. H.; Zhu, J.; Yu, R.; Cheng, Z. Y.

    2014-11-15

    The stacking faults (SFs) in an AlSb/GaAs (001) interface were investigated using a 300 kV spherical aberration-corrected high-resolution transmission electron microscope (HRTEM). The structure and strain distribution of the single and intersecting (V-shaped) SFs associated with partial dislocations (PDs) were characterized by the [110] HRTEM images and geometric phase analysis, respectively. In the biaxial strain maps ?{sub xx} and ?{sub yy}, a SF can be divided into several sections under different strain states (positive or negative strain values). Furthermore, the strain state for the same section of a SF is in contrast to each other in ?{sub xx} and ?{sub yy} strain maps. The modification in the strain states was attributed to the variation in the local atomic displacements for the SF in the AlSb film on the GaAs substrate recorded in the lattice image. Finally, the single SF was found to be bounded by two 30 PDs. A pair of 30 PDs near the heteroepitaxial interface reacted to form a Lomer-Cottrell sessile dislocation located at the vertices of V-shaped SFs with opposite screw components. The roles of misfit dislocations, such as the PDs, in strain relaxation were also discussed.

  3. In-situ high resolution transmission electron microscopy observation of silicon nanocrystal nucleation in a SiO{sub 2} bilayered matrix

    SciTech Connect (OSTI)

    Yang, T. C.-J. Wu, L.; Lin, Z.; Jia, X.; Puthen-Veettil, B.; Zhang, T.; Conibeer, G.; Perez-Wurfl, I.; Kauffmann, Y.; Rothschild, A.

    2014-08-04

    Solid-state nucleation of Si nanocrystals in a SiO{sub 2} bilayered matrix was observed at temperatures as low as 450?C. This was achieved by aberration corrected high-resolution transmission electron microscopy (HRTEM) with real-time in-situ heating up to 600?C. This technique is a valuable characterization tool especially with the recent interest in Si nanostructures for light emitting devices, non-volatile memories, and third-generation photovoltaics which all typically require a heating step in their fabrication. The control of size, shape, and distribution of the Si nanocrystals are critical for these applications. This experimental study involves in-situ observation of the nucleation of Si nanocrystals in a SiO{sub 2} bilayered matrix fabricated through radio frequency co-sputtering. The results show that the shapes of Si nanocrystals in amorphous SiO{sub 2} bilayered matrices are irregular and not spherical, in contrast to many claims in the literature. Furthermore, the Si nanocrystals are well confined within their layers by the amorphous SiO{sub 2}. This study demonstrates the potential of in-situ HRTEM as a tool to observe the real time nucleation of Si nanocrystals in a SiO{sub 2} bilayered matrix. Furthermore, ideas for improvements on this in-situ heating HRTEM technique are discussed.

  4. High spatial resolution mapping of deposition layers on plasma facing materials by laser ablation microprobe time-of-flight mass spectroscopy

    SciTech Connect (OSTI)

    Xiao, Qingmei; Li, Cong; Hai, Ran; Zhang, Lei; Feng, Chunlei; Ding, Hongbin, E-mail: hding@dlut.edu.cn [School of Physics and Optical Electronic Technology, Key Laboratory of Materials Modification by Laser, Ion and Electron Beams, Chinese Ministry of Education, Dalian University of Technology, Dalian 116024 (China); Zhou, Yan; Yan, Longwen; Duan, Xuru [Southwestern Institute of Physics, P.O. Box 432, No. 3 South Section 3, Circle Road 2, Chengdu 610041, Sichuan (China)

    2014-05-15

    A laser ablation microprobe time-of-flight mass spectroscopy (LAM-TOF-MS) system with high spatial resolution, ?20 nm in depth and ?500 ?m or better on the surface, is developed to analyze the composition distributions of deposition layers on the first wall materials or first mirrors in tokamak. The LAM-TOF-MS system consists of a laser ablation microprobe combined with a TOF-MS and a data acquisition system based on a LabVIEW program software package. Laser induced ablation combined with TOF-MS is an attractive method to analyze the depth profile of deposited layer with successive laser shots, therefore, it can provide information for composition reconstruction of the plasma wall interaction process. In this work, we demonstrate that the LAM-TOF-MS system is capable of characterizing the depth profile as well as mapping 2D composition of deposited film on the molybdenum first mirror retrieved from HL-2A tokamak, with particular emphasis on some of the species produced during the ablation process. The presented LAM-TOF-MS system provides not only the 3D characterization of deposition but also the removal efficiency of species of concern.

  5. Analysis of the rotational structure in the high-resolution infrared spectra of trans-hexatriene-2-d1 and -3-d1

    SciTech Connect (OSTI)

    Craig, Norman C.; Chen, Yihui; van Besien, Herman; Blake, Thomas A.

    2014-09-01

    The 2-d1 and 3-d1 isotopologues of trans-hexatriene have been synthesized, and their high-resolution (0.0015 cm-1) IR spectra have been recorded. For each of the isotopologues the rotational structure in four C-type bands for out-of-plane vibrational modes has been analyzed, and the ground state combination differences (GSCDs) have been pooled. Ground state rotational constants have been fitted to the GSCDs. For the 2-d species, A0, B0, and C0 values of 0.7837254(5), 0.0442806(3), and 0.0419299(2) cm-1 were fitted to 2450 GSCDs. For the 3-d species, A0, B0, and C0 values of 0.7952226(8), 0.0446149(7), and 0.0422661(4) cm-1 were fitted to 2234 GSCDs. For the eleven out-of-plane modes of the two isotopologues, predictions of anharmonic wavenumbers and harmonic intensities have been computed and compared with experiment where possible.

  6. A new spectrometer design for the x-ray spectroscopy of laser-produced plasmas with high (sub-ns) time resolution

    SciTech Connect (OSTI)

    Bitter, M. Hill, K. W.; Efthimion, P. C.; Delgado-Aparicio, L.; Pablant, N.; Lu, Jian; Beiersdorfer, P.; Chen, Hui

    2014-11-15

    This paper describes a new type of x-ray crystal spectrometer, which can be used in combination with gated x-ray detectors to obtain spectra from laser-produced plasmas with a high (sub-ns) time resolution. The spectrometer consists of a convex, spherically bent crystal, which images individual spectral lines as perfectly straight lines across multiple, sequentially gated, strip detectors. Since the Bragg-reflected rays are divergent, the distance between detector and crystal is arbitrary, so that this distance can be appropriately chosen to optimize the experimental arrangement with respect to the detector parameters. The spectrometer concept was verified in proof-of-principle experiments by imaging the L?{sub 1}- and L?{sub 2}-lines of tungsten, at 9.6735 and 9.96150 keV, from a micro-focus x-ray tube with a tungsten target onto a two-dimensional pixilated Pilatus detector, using a convex, spherically bent Si-422 crystal with a radius of curvature of 500 mm.

  7. THE 300 km s{sup -1} STELLAR STREAM NEAR SEGUE 1: INSIGHTS FROM HIGH-RESOLUTION SPECTROSCOPY OF ITS BRIGHTEST STAR

    SciTech Connect (OSTI)

    Frebel, Anna; Casey, Andrew R.; Lunnan, Ragnhild; Norris, John E.; Wyse, Rosemary F. G.; Gilmore, Gerard

    2013-07-01

    We present a chemical abundance analysis of 300S-1, the brightest likely member star of the 300 km s{sup -1} stream near the faint satellite galaxy Segue 1. From a high-resolution Magellan/MIKE spectrum, we determine a metallicity of [Fe/H] = -1.46 {+-} 0.05 {+-} 0.23 (random and systematic uncertainties) for star 300S-1, and find an abundance pattern similar to typical halo stars at this metallicity. Comparing our stellar parameters to theoretical isochrones, we estimate a distance of 18 {+-} 7 kpc. Both the metallicity and distance estimates are in good agreement with what can be inferred from comparing the Sloan Digital Sky Survey photometric data of the stream stars to globular cluster sequences. While several other structures overlap with the stream in this part of the sky, the combination of kinematic, chemical, and distance information makes it unlikely that these stars are associated with either the Segue 1 galaxy, the Sagittarius Stream, or the Orphan Stream. Streams with halo-like abundance signatures, such as the 300 km s{sup -1} stream, present another observational piece for understanding the accretion history of the Galactic halo.

  8. Particle detector spatial resolution

    DOE Patents [OSTI]

    Perez-Mendez, Victor

    1992-01-01

    Method and apparatus for producing separated columns of scintillation layer material, for use in detection of X-rays and high energy charged particles with improved spatial resolution. A pattern of ridges or projections is formed on one surface of a substrate layer or in a thin polyimide layer, and the scintillation layer is grown at controlled temperature and growth rate on the ridge-containing material. The scintillation material preferentially forms cylinders or columns, separated by gaps conforming to the pattern of ridges, and these columns direct most of the light produced in the scintillation layer along individual columns for subsequent detection in a photodiode layer. The gaps may be filled with a light-absorbing material to further enhance the spatial resolution of the particle detector.

  9. Particle detector spatial resolution

    DOE Patents [OSTI]

    Perez-Mendez, V.

    1992-12-15

    Method and apparatus for producing separated columns of scintillation layer material, for use in detection of X-rays and high energy charged particles with improved spatial resolution is disclosed. A pattern of ridges or projections is formed on one surface of a substrate layer or in a thin polyimide layer, and the scintillation layer is grown at controlled temperature and growth rate on the ridge-containing material. The scintillation material preferentially forms cylinders or columns, separated by gaps conforming to the pattern of ridges, and these columns direct most of the light produced in the scintillation layer along individual columns for subsequent detection in a photodiode layer. The gaps may be filled with a light-absorbing material to further enhance the spatial resolution of the particle detector. 12 figs.

  10. STARTUP REACTIVITY ACCOUNTABILITY ATTRIBUTED TO ISOTOPIC TRANSMUTATIONS IN THE IRRADIATED BERYLLIUM REFLECTOR OF THE HIGH FLUX ISTOTOPE REACTOR

    SciTech Connect (OSTI)

    Chandler, David [ORNL] [ORNL; Maldonado, G Ivan [ORNL] [ORNL; Primm, Trent [ORNL] [ORNL

    2010-01-01

    The objective of this study is to develop a methodology to predict the reactivity impact as a function of outage time between cycles of 3He, 6Li, and other poisons in the High Flux Isotope Reactor s (HFIR) beryllium reflector. The reactivity worth at startup of the HFIR has been incorrectly predicted in the past after the reactor has been shut-down for long periods of time. The incorrect prediction was postulated to be due to the erroneous calculation of 3He buildup in the beryllium reflector. It is necessary to develop a better estimate of the start-of-cycle symmetric critical control element positions since if the estimated and actual symmetrical critical control element positions differ by more than $1.55 in reactivity (approximately one-half inch in control element startup position), HFIR is to be shutdown and a technical evaluation is performed to resolve the discrepancy prior to restart. 3He is generated and depleted during operation, but during an outage, the depletion of 3He ceases because it is a stable isotope. 3He is born from the radioactive decay of tritium, and thus the concentration of 3He increases during shutdown. The computer program SCALE, specifically the TRITON and CSAS5 control modules including the KENO V.A, COUPLE, and ORIGEN functional modules were utilized in this study. An equation relating the down time (td) to the change in symmetric control element position was generated and validated against measurements for approximately 40 HFIR operating cycles. The newly-derived correlation was shown to improve accuracy of predictions for long periods of down time.

  11. Mapping intra-field yield variation using high resolution satellite imagery to integrate bioenergy and environmental stewardship in an agricultural watershed

    SciTech Connect (OSTI)

    Hamada, Yuki; Ssegane, Herbert; Negri, Maria Cristina

    2015-07-31

    Biofuels are important alternatives for meeting our future energy needs. Successful bioenergy crop production requires maintaining environmental sustainability and minimum impacts on current net annual food, feed, and fiber production. The objectives of this study were to: (1) determine under-productive areas within an agricultural field in a watershed using a single date; high resolution remote sensing and (2) examine impacts of growing bioenergy crops in the under-productive areas using hydrologic modeling in order to facilitate sustainable landscape design. Normalized difference indices (NDIs) were computed based on the ratio of all possible two-band combinations using the RapidEye and the National Agricultural Imagery Program images collected in summer 2011. A multiple regression analysis was performed using 10 NDIs and five RapidEye spectral bands. The regression analysis suggested that the red and near infrared bands and NDI using red-edge and near infrared that is known as the red-edge normalized difference vegetation index (RENDVI) had the highest correlation (R2 = 0.524) with the reference yield. Although predictive yield map showed striking similarity to the reference yield map, the model had modest correlation; thus, further research is needed to improve predictive capability for absolute yields. Forecasted impact using the Soil and Water Assessment Tool model of growing switchgrass (Panicum virgatum) on under-productive areas based on corn yield thresholds of 3.1, 4.7, and 6.3 Mg·ha-1 showed reduction of tile NO3-N and sediment exports by 15.9%–25.9% and 25%–39%, respectively. Corresponding reductions in water yields ranged from 0.9% to 2.5%. While further research is warranted, the study demonstrated the integration of remote sensing and hydrologic modeling to quantify the multifunctional value of projected future landscape patterns in a context of sustainable bioenergy crop production.

  12. Mapping intra-field yield variation using high resolution satellite imagery to integrate bioenergy and environmental stewardship in an agricultural watershed

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Hamada, Yuki; Ssegane, Herbert; Negri, Maria Cristina

    2015-07-31

    Biofuels are important alternatives for meeting our future energy needs. Successful bioenergy crop production requires maintaining environmental sustainability and minimum impacts on current net annual food, feed, and fiber production. The objectives of this study were to: (1) determine under-productive areas within an agricultural field in a watershed using a single date; high resolution remote sensing and (2) examine impacts of growing bioenergy crops in the under-productive areas using hydrologic modeling in order to facilitate sustainable landscape design. Normalized difference indices (NDIs) were computed based on the ratio of all possible two-band combinations using the RapidEye and the National Agriculturalmore » Imagery Program images collected in summer 2011. A multiple regression analysis was performed using 10 NDIs and five RapidEye spectral bands. The regression analysis suggested that the red and near infrared bands and NDI using red-edge and near infrared that is known as the red-edge normalized difference vegetation index (RENDVI) had the highest correlation (R2 = 0.524) with the reference yield. Although predictive yield map showed striking similarity to the reference yield map, the model had modest correlation; thus, further research is needed to improve predictive capability for absolute yields. Forecasted impact using the Soil and Water Assessment Tool model of growing switchgrass (Panicum virgatum) on under-productive areas based on corn yield thresholds of 3.1, 4.7, and 6.3 Mg·ha-1 showed reduction of tile NO3-N and sediment exports by 15.9%–25.9% and 25%–39%, respectively. Corresponding reductions in water yields ranged from 0.9% to 2.5%. While further research is warranted, the study demonstrated the integration of remote sensing and hydrologic modeling to quantify the multifunctional value of projected future landscape patterns in a context of sustainable bioenergy crop production.« less

  13. Effects of irradiation temperature on Charpy and tensile properties of high-copper, low upper-shelf, submerged-arc welds

    SciTech Connect (OSTI)

    Nanstad, R.K.; Berggren, R.G.

    1992-12-31

    This paper presents analyses of the Charpy impact and tensile test data, including adjustments for irradiation temperature and fluence normalization which make possible comparison of the irradiation sensitivity of the different welds. Analyses revealed dependence of yield and ultimate strength on irradiation temperature {minus}0.8 MPA/{degrees}C, respectively. Similarly, the Charpy impact energy changes due to irradiation temperature were {minus}0.5{degrees}C/{degrees}C for transition shift and {minus}0.05 J/{degrees}C for upper-shelf energy decrease. After adjustment to an irradiation temperature of 288{degrees}C and normalization to a fluence of 8 {times} 10{sup 18} neutrons/cm{sup 2} percentage increases in yield strength due to irradiation ranged from about 21 to 35% while those for ultimate strength ranged from about 13 to 20%. The Charpy transition temperature shifts ranged from 59 to 123{degrees}C while the postirradiation upper-shelf energies ranged from 58 to 79 J.

  14. Evolution of titania nanotubes-supported WO{sub x} species by in situ thermo-Raman spectroscopy, X-ray diffraction and high resolution transmission electron microscopy

    SciTech Connect (OSTI)

    Cortes-Jacome, M.A.; Angeles-Chavez, C.; Morales, M.; Lopez-Salinas, E.; Toledo-Antonio, J.A.

    2007-10-15

    Structural evolution of WO{sub x} species on the surface of titania nanotubes was followed by in situ thermo-Raman spectroscopy. A total of 15 wt% of W atoms were loaded on the surface of a hydroxylated titania nanotubes by impregnation with ammonium metatungstate solution and then, the sample was thermally treated in a Linkam cell at different temperatures in nitrogen flow. The band characteristic of the W=O bond was observed at 962 cm{sup -1} in the dried sample, which vanished between 300 and 700 deg. C, and reappear again after annealing at 800 deg. C, along with a broad band centered at 935 cm{sup -1}, attributed to the v{sub 1} vibration of W=O in tetrahedral coordination. At 900 and 1000 deg. C, the broad band decomposed into four bands at 923, 934, 940 and 950 cm{sup -1}, corresponding to the symmetric and asymmetric vibration of W=O bonds in Na{sub 2}WO{sub 4} and Na{sub 2}W{sub 2}O{sub 7} phases as determined by X-ray diffraction and High resolution transmission electron microscopy (HRTEM). The structure of the nanotubular support was kept at temperatures below 450 deg. C, thereafter, it transformed into anatase being stabilized at temperatures as high as 900 deg. C. At 1000 deg. C, anatase phase partially converted into rutile. After annealing at 1000 deg. C, a core-shell model material was obtained, with a shell of ca. 5 nm thickness, composed of sodium tungstate nanoclusters, and a core composed mainly of rutile TiO{sub 2} phase. - Graphical abstract: Titania nanotubes loaded with 15 wt% W atoms were characterized from room temperature (rt) to 1000 deg. C by thermo-Raman spectroscopy in N{sub 2}. At 1000 deg. C, a core-shell model material was obtained, with a shell thickness of ca. 5 nm composed by nanoclusters of sodium tungstate, and a core composed mainly of rutile TiO{sub 2} phase.

  15. High-resolution rovibrational study of the Coriolis-coupled nu(12) and nu(15) modes of [1.1.1]propellane

    SciTech Connect (OSTI)

    Kirkpatrick, Robynne W.; Masiello, Tony; Jariyasopit, Narumol; Nibler, Joseph W.; Maki, Arthur G.; Blake, Thomas A.; Weber, Alfons

    2009-01-02

    Infrared spectra of the small strained cage molecule [1.1.1]propellane have been obtained at high resolution (0.0015 cm-1) and the J and K, l rovibrational structure has been resolved for the first time. We recently used combination-differences to obtain ground state parameters for propellane; over 4,100 differences from five fundamental and four combination bands were used in this process. The combination-difference approach eliminated errors due to localized perturbations in the upper state levels of the transitions and gave well-determined ground state parameters. In the current work, these ground state parameters were used in a determination of the upper state parameters for the v12(e?) perpendicular and v15(a2?) parallel bands. Over 4000 infrared transitions were fitted for each band, with J, K values ranging up to 71, 51 and 92, 90 respectively. While the transition frequencies for both bands can be fit nicely using separate analyses for each band, the strong intensity perturbations observed in the weaker v12 band indicated that Coriolis coupling between the two modes was significant and should be included. Due to correlations with other parameters, the Coriolis coupling parameter Zy15z,12x for the v15 and v12 interaction is poorly determined by a transition frequency fit alone. However, by combining the frequency fit with a fit of experimental intensities, a value of -0.42 was obtained, quite close to that predicted from the ab initio calculation (-0.44). This intensity fit also yielded a (dz/dQ15z)/(dx/dQ12x) dipole derivative ratio of 36.5, in reasonable agreement with a value of 29.2 predicted by Gaussian ab initio density functional calculations using a cc-pVTZ basis. This ratio is unusually high due to large charge movement as the novel central Caxial-Caxial bond is displaced along the symmetry axis of the molecule for the v15 mode.

  16. Spectral restoration in high resolution electron energy loss spectroscopy based on iterative semi-blind Lucy-Richardson algorithm applied to rutile surfaces

    SciTech Connect (OSTI)

    Lazzari, Rmi Li, Jingfeng Jupille, Jacques

    2015-01-15

    A new spectral restoration algorithm of reflection electron energy loss spectra is proposed. It is based on the maximum likelihood principle as implemented in the iterative Lucy-Richardson approach. Resolution is enhanced and point spread function recovered in a semi-blind way by forcing cyclically the zero loss to converge towards a Dirac peak. Synthetic phonon spectra of TiO{sub 2} are used as a test bed to discuss resolution enhancement, convergence benefit, stability towards noise, and apparatus function recovery. Attention is focused on the interplay between spectral restoration and quasi-elastic broadening due to free carriers. A resolution enhancement by a factor up to 6 on the elastic peak width can be obtained on experimental spectra of TiO{sub 2}(110) and helps revealing mixed phonon/plasmon excitations.

  17. Note: Design and construction of a multi-scale, high-resolution, tube-generated X-Ray computed-tomography system for three-dimensional (3D) imaging

    SciTech Connect (OSTI)

    Mertens, J. C. E.; Williams, J. J.; Chawla, Nikhilesh

    2014-01-15

    The design and construction of a high resolution modular x-ray computed tomography (XCT) system is described. The approach for meeting a specified set of performance goals tailored toward experimental versatility is highlighted. The instrument is unique in its detector and x-ray source configuration, both of which enable elevated optimization of spatial and temporal resolution. The process for component selection is provided. The selected components are specified, the custom component design discussed, and the integration of both into a fully functional XCT instrument is outlined. The novelty of this design is a new lab-scale detector and imaging optimization through x-ray source and detector modularity.

  18. Validation of the Physics Analysis used to Characterize the AGR-1 TRISO Fuel Irradiation Test

    SciTech Connect (OSTI)

    Sterbentz, James W.; Harp, Jason M.; Demkowicz, Paul A.; Hawkes, Grant L.; Chang, Gray S.

    2015-05-01

    The results of a detailed physics depletion calculation used to characterize the AGR-1 TRISO-coated particle fuel test irradiated in the Advanced Test Reactor (ATR) at the Idaho National Laboratory are compared to measured data for the purpose of validation. The particle fuel was irradiated for 13 ATR power cycles over three calendar years. The physics analysis predicts compact burnups ranging from 11.30-19.56% FIMA and cumulative neutron fast fluence from 2.21?4.39E+25 n/m2 under simulated high-temperature gas-cooled reactor conditions in the ATR. The physics depletion calculation can provide a full characterization of all 72 irradiated TRISO-coated particle compacts during and post-irradiation, so validation of this physics calculation was a top priority. The validation of the physics analysis was done through comparisons with available measured experimental data which included: 1) high-resolution gamma scans for compact activity and burnup, 2) mass spectrometry for compact burnup, 3) flux wires for cumulative fast fluence, and 4) mass spectrometry for individual actinide and fission product concentrations. The measured data are generally in very good agreement with the calculated results, and therefore provide an adequate validation of the physics analysis and the results used to characterize the irradiated AGR-1 TRISO fuel.

  19. Taheri-Saramad x-ray detector (TSXD): A novel high spatial resolution x-ray imager based on ZnO nano scintillator wires in polycarbonate membrane

    SciTech Connect (OSTI)

    Taheri, A. Saramad, S.; Ghalenoei, S.; Setayeshi, S.

    2014-01-15

    A novel x-ray imager based on ZnO nanowires is designed and fabricated. The proposed architecture is based on scintillation properties of ZnO nanostructures in a polycarbonate track-etched membrane. Because of higher refractive index of ZnO nanowire compared to the membrane, the nanowire acts as an optical fiber that prevents the generated optical photons to spread inside the detector. This effect improves the spatial resolution of the imager. The detection quantum efficiency and spatial resolution of the fabricated imager are 11% and <6.8 μm, respectively.

  20. SU-E-CAMPUS-T-05: Validation of High-Resolution 3D Patient QA for Proton Pencil Beam Scanning and IMPT by Polymer Gel Dosimetry

    SciTech Connect (OSTI)

    Cardin, A; Avery, S; Ding, X; Kassaee, A; Lin, L; Maryanski, M

    2014-06-15

    Purpose: Validation of high-resolution 3D patient QA for proton pencil beam scanning and IMPT by polymer gel dosimetry. Methods: Four BANG3Pro polymer gel dosimeters (manufactured by MGS Research Inc, Madison, CT) were used for patient QA at the Robert's Proton Therapy Center (RPTC, Philadelphia, PA). All dosimeters were sealed in identical thin-wall Pyrex glass spheres. Each dosimeter contained a set of markers for 3D registration purposes. The dosimeters were mounted in a consistent and reproducible manner using a custom build holder. Two proton pencil beam scanning plans were designed using Varian Eclipse treatment planning system: 1) A two-field intensity modulated proton therapy (IMPT) plan and 2) one single field uniform dose (SFUD) plan. The IMPT fields were evaluated as a composite plan and individual fields, the SFUD plan was delivered as a single field plan.Laser CT scanning was performed using the manufacturer's OCTOPUS-IQ axial transmission laser CT scanner using a 1 mm slice thickness. 3D registration, analysis, and OD/cm to absorbed dose calibrations were perfomed using DICOM RT-Dose and CT files, and software developed by the manufacturer. 3D delta index, a metric equivalent to the gamma tool, was used for dose comparison. Results: Very good agreement with single IMPT fields and with SFUD was obtained. Composite IMPT fields had a less satisfactory agreement. The single fields had 3D delta index passing rates (3% dose difference, 3 mm DTA) of 98.98% and 94.91%. The composite 3D delta index passing rate was 80.80%. The SFUD passing rate was 93.77%. Required shifts of the dose distributions were less than 4 mm. Conclusion: A formulation of the BANG3Pro polymer gel dosimeter, suitable for 3D QA of proton patient plans is established and validated. Likewise, the mailed QA analysis service provided by the manufacturer is a practical option when required resources are unavailable. We fully disclose that the subject of this research regards a production of MGS Research, Inc.