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Sample records for high purity germanium

  1. High Purity Germanium Detectors at LBNL | U.S. DOE Office of...

    Office of Science (SC) Website

    Purity Germanium Detectors at LBNL Nuclear Physics (NP) NP Home About Research Facilities Science Highlights Benefits of NP Applications of Nuclear Science Applications of Nuclear ...

  2. High Purity Germanium Detectors at LBNL | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    Purity Germanium Detectors at LBNL Nuclear Physics (NP) NP Home About Research Facilities Science Highlights Benefits of NP Applications of Nuclear Science Applications of Nuclear Science Archives Small Business Innovation / Technology Transfer Funding Opportunities Nuclear Science Advisory Committee (NSAC) Community Resources Contact Information Nuclear Physics U.S. Department of Energy SC-26/Germantown Building 1000 Independence Ave., SW Washington, DC 20585 P: (301) 903-3613 F: (301) 903-3833

  3. High-Purity Germanium Spectroscopy at Rates in Excess of 10^{6} Events/s

    SciTech Connect (OSTI)

    VanDevender, Brent A.; Dion, Michael P.; Fast, James E.; Rodriguez, Douglas C.; Taubman, Matthew S.; Wilen, Christopher D.; Wood, Lynn S.; Wright, Michael E.

    2014-10-01

    AbstractIn gamma spectroscopy, a compromise must be made between energy resolution and event-rate capability. Some foreseen nuclear material safeguards applications require a spectrometer with energy resolution typical of high purity germanium (HPGe) detectors, operated at rates up to and exceeding 106 events per second. We report the performance of an HPGe spectrometer adapted to run at such rates. Our system consists of a commercial semi-coaxial HPGe detector, a modified high-voltagerail, resistive-feedback, charge-sensitive preamplifier and a continuous waveform digitizer. Digitized waveforms are analyzed offline with a novel time-variant trapezoidal filter algorithm. Several time-invariant trapezoidal filters are run in parallel and the slowest one not rejected by instantaneous pileup conditions is used to measure each pulse height. We have attained full-widthat- half-maximum energy resolution of less than 8 keV measured at 662 keV with 1:08*106 per second incoming event rate and 38% throughput. An additional constraint on the width of the fast trigger filter removes a significant amount of edge pileup that passes the first pileup cut, reducing throughput to 26%. While better resolution has been reported by other authors, our throughput is over an order of magnitude higher than any other reported HPGe system operated at such an event rate.

  4. Performance of A Compact Multi-crystal High-purity Germanium Detector Array for Measuring Coincident Gamma-ray Emissions

    SciTech Connect (OSTI)

    Howard, Chris; Daigle, Stephen; Buckner, Matt; Erikson, Luke E.; Runkle, Robert C.; Stave, Sean C.; Champagne, Art; Cooper, Andrew; Downen, Lori; Glasgow, Brian D.; Kelly, Keegan; Sallaska, Anne

    2015-05-21

    The Multi-sensor Airborne Radiation Survey (MARS) detector is a 14-crystal array of high-purity germanium (HPGe) detectors housed in a single cryostat. The array was used to measure the astrophysical S-factor for the 14N(p,?)15O* reaction for several transition energies at an effective center of mass energy of 163 keV. Owing to the segmented nature of the MARS detector, the effect of gamma-ray summing was greatly reduced in comparison to past experiments which utilized large, single-crystal detectors. The new S-factor values agree within the uncertainties with the past measurements. Details of the analysis and detector performance will be presented.

  5. High purity polonium recovery

    DOE Patents [OSTI]

    Chong, Clyde H. H.; Love, Calvin M.; Prisc, Martin D.; Russo, Alexander J.

    1976-01-01

    Apparatus and method for providing larger quantities of higher purity polonium suitable, as vapor distilled, for heat source elements for radioisotopic generators or the like.

  6. Method of high purity silane preparation

    DOE Patents [OSTI]

    Tsuo, Y. Simon (Golden, CO); Belov, Eugene P. (Moscow, RU); Gerlivanov, Vadim G. (Moscow, RU); Zadde, Vitali V. (Moscow, RU); Kleschevnikova, Solomonida I. (Moscow, RU); Korneev, Nikolai N. (Moscow, RU); Lebedev, Eugene N. (Moscow, RU); Pinov, Akhsarbek B. (Moscow, RU); Ryabenko, Eugene A. (Moscow, RU); Strebkov, Dmitry S. (Moscow, RU); Chernyshev, Eugene A. (Moscow, RU)

    2000-01-01

    A process for the preparation of high purity silane, suitable for forming thin layer silicon structures in various semiconductor devices and high purity poly- and single crystal silicon for a variety of applications, is provided. Synthesis of high-purity silane starts with a temperature assisted reaction of metallurgical silicon with alcohol in the presence of a catalyst. Alcoxysilanes formed in the silicon-alcohol reaction are separated from other products and purified. Simultaneous reduction and oxidation of alcoxysilanes produces gaseous silane and liquid secondary products, including, active part of a catalyst, tetra-alcoxysilanes, and impurity compounds having silicon-hydrogen bonds. Silane is purified by an impurity adsorption technique. Unreacted alcohol is extracted and returned to the reaction with silicon. Concentrated mixture of alcoxysilanes undergoes simultaneous oxidation and reduction in the presence of a catalyst at the temperature -20.degree. C. to +40.degree. C. during 1 to 50 hours. Tetra-alcoxysilane extracted from liquid products of simultaneous oxidation and reduction reaction is directed to a complete hydrolysis. Complete hydrolysis of tetra-alcoxysilane results in formation of industrial silica sol and alcohol. Alcohol is dehydrated by tetra-alcoxysilane and returned to the reaction with silicon.

  7. Low cost routes to high purity silicon and derivatives thereof

    DOE Patents [OSTI]

    Laine, Richard M; Krug, David James; Marchal, Julien Claudius; Mccolm, Andrew Stewart

    2013-07-02

    The present invention is directed to a method for providing an agricultural waste product having amorphous silica, carbon, and impurities; extracting from the agricultural waste product an amount of the impurities; changing the ratio of carbon to silica; and reducing the silica to a high purity silicon (e.g., to photovoltaic silicon).

  8. Germanium-76 Sample Analysis

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Engelhard, Mark H.; Zhu, Zihua

    2011-04-01

    The MAJORANA DEMONSTRATOR is a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0???). The DEMONSTRATOR will utilize 76Ge from Russia, and the first one gram sample was received from the supplier for analysis on April 24, 2011. The Environmental Molecular Sciences facility, a DOE user facility at PNNL, was used to make the required isotopic and chemical purity measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR. The results of this first analysis are reported here.

  9. Method and apparatus for producing high purity silicon

    DOE Patents [OSTI]

    Olson, Jerry M. (Lakewood, CO)

    1984-01-01

    A method for producing high purity silicon includes forming a copper silie alloy and positioning the alloy within an enclosure. A filament member is also placed within the enclosure opposite the alloy. The enclosure is then filled with a chemical vapor transport gas adapted for transporting silicon. Finally, both the filament member and the alloy are heated to temperatures sufficient to cause the gas to react with silicon at the alloy surface and deposit the reacted silicon on the filament member. In addition, an apparatus for carrying out this method is also disclosed.

  10. Method and apparatus for producing high purity silicon

    DOE Patents [OSTI]

    Olson, J.M.

    1983-05-27

    A method for producing high purity silicon includes forming a copper silicide alloy and positioning the alloy within an enclosure. A filament member is also placed within the enclosure opposite the alloy. The enclosure is then filled with a chemical vapor transport gas adapted for transporting silicon. Finally, both the filament member and the alloy are heated to temperatures sufficient to cause the gas to react with silicon at the alloy surface and deposit the reacted silicon on the filament member. In addition, an apparatus for carrying out this method is also disclosed.

  11. MAJORANA Collaboration's experience with germanium detectors

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Mertens, S.; Abgrall, N.; Avignone, F. T.; Barabash, A. S.; Bertrand, F. E.; Brudanin, V.; Busch, M.; Buuck, M.; Byram, D.; Caldwell, A. S.; et al

    2015-05-01

    The goal of the Majorana Demonstrator project is to search for 0νββ decay in 76Ge. Of all candidate isotopes for 0νββ, 76Ge has some of the most favorable characteristics. Germanium detectors are a well established technology, and in searches for 0νββ, the high purity germanium crystal acts simultaneously as source and detector. Furthermore, p-type germanium detectors provide excellent energy resolution and a specially designed point contact geometry allows for sensitive pulse shape discrimination. This paper will summarize the experiences the MAJORANA collaboration made with enriched germanium detectors manufactured by ORTEC®®. The process from production, to characterization and integration in MAJORANAmore » mounting structure will be described. A summary of the performance of all enriched germanium detectors will be given.« less

  12. MAJORANA Collaboration's experience with germanium detectors

    SciTech Connect (OSTI)

    Mertens, S.; Abgrall, N.; Avignone, F. T.; Barabash, A. S.; Bertrand, F. E.; Brudanin, V.; Busch, M.; Buuck, M.; Byram, D.; Caldwell, A. S.; Chan, Y. -D.; Christofferson, C. D.; Cuesta, C.; Detwiler, J. A.; Efremenko, Yu; Ejiri, H.; Elliott, S. R.; Galindo-Uribarri, A.; Giovanetti, G. K.; Goett, J.; Green, M. P.; Gruszko, J.; Guinn, I.; Guiseppe, V. E.; Henning, R.; Hoppe, E. W.; Howard, S.; Howe, M. A.; Jasinski, B. R.; Keeter, K. J.; Kidd, M. F.; Konovalov, S. I.; Kouzes, R. T.; LaFerriere, B. D.; Leon, J.; MacMullin, J.; Martin, R. D.; Meijer, S. J.; Orrell, J. L.; O'Shaughnessy, C.; Overman, N. R.; Poon, A. W. P.; Radford, D. C.; Rager, J.; Rielage, K.; Robertson, R. G. H.; Romero-Romero, E.; Ronquest, M. C.; Shanks, B.; Shirchenko, M.; Snyder, N.; Tedeschi, D.; Trimble, J. E.; Varner, R. L.; Vasilyev, S.; Vetter, K.; Vorren, K.; White, B. R.; Wilkerson, J. F.; Wiseman, C.; Xu, W.; Yakushev, E.; Yu, C. -H.; Yumatov, V.

    2015-05-01

    The goal of the Majorana Demonstrator project is to search for 0??? decay in 76Ge. Of all candidate isotopes for 0???, 76Ge has some of the most favorable characteristics. Germanium detectors are a well established technology, and in searches for 0???, the high purity germanium crystal acts simultaneously as source and detector. Furthermore, p-type germanium detectors provide excellent energy resolution and a specially designed point contact geometry allows for sensitive pulse shape discrimination. This paper will summarize the experiences the MAJORANA collaboration made with enriched germanium detectors manufactured by ORTEC. The process from production, to characterization and integration in MAJORANA mounting structure will be described. A summary of the performance of all enriched germanium detectors will be given.

  13. The Importance of Domain Size and Purity in High-Efficiency Organic...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymerorganic photovoltaic cells hinges on excitons-electronhole pairs energized by...

  14. Electrolytic production of high purity aluminum using inert anodes

    DOE Patents [OSTI]

    Ray, Siba P. (Murrysville, PA); Liu, Xinghua (Monroeville, PA); Weirauch, Jr., Douglas A. (Murrysville, PA)

    2001-01-01

    A method of producing commercial purity aluminum in an electrolytic reduction cell comprising inert anodes is disclosed. The method produces aluminum having acceptable levels of Fe, Cu and Ni impurities. The inert anodes used in the process preferably comprise a cermet material comprising ceramic oxide phase portions and metal phase portions.

  15. Electrolytic production of high purity aluminum using ceramic inert anodes

    DOE Patents [OSTI]

    Ray, Siba P. (Murrysville, PA); Liu, Xinghua (Monroeville, PA); Weirauch, Douglas A. (Murrysville, PA); DiMilia, Robert A. (Baton Rouge, LA); Dynys, Joseph M. (New Kensington, PA); Phelps, Frankie E. (Apollo, PA); LaCamera, Alfred F. (Trafford, PA)

    2002-01-01

    A method of producing commercial purity aluminum in an electrolytic reduction cell comprising ceramic inert anodes is disclosed. The method produces aluminum having acceptable levels of Fe, Cu and Ni impurities. The ceramic inert anodes used in the process may comprise oxides containing Fe and Ni, as well as other oxides, metals and/or dopants.

  16. Electric characteristics of germanium Vertical Multijunction (VMJ) photovoltaic cells under high intensity illumination

    SciTech Connect (OSTI)

    Unishkov, V.A.

    1997-03-01

    This paper presents the results of the performance evaluation of Vertical Multijunction (VMJ) germanium (Ge) photovoltaic (PV) cells. Vertical Multijunction Germanium Photovoltaic cells offer several advantages for Thermophotovoltaic (TPV) applications such as high intensity light conversion, low series resistance, more efficient coupling to lower temperature sources, high output voltage, simplified heat rejection system as well as potentially simple fabrication technology and low cost photovoltaic converter device. {copyright} {ital 1997 American Institute of Physics.}

  17. High-efficiency spectral purity filter for EUV lithography

    DOE Patents [OSTI]

    Chapman, Henry N.

    2006-05-23

    An asymmetric-cut multilayer diffracts EUV light. A multilayer cut at an angle has the same properties as a blazed grating, and has been demonstrated to have near-perfect performance. Instead of having to nano-fabricate a grating structure with imperfections no greater than several tens of nanometers, a thick multilayer is grown on a substrate and then cut at an inclined angle using coarse and inexpensive methods. Effective grating periods can be produced this way that are 10 to 100 times smaller than those produced today, and the diffraction efficiency of these asymmetric multilayers is higher than conventional gratings. Besides their ease of manufacture, the use of an asymmetric multilayer as a spectral purity filter does not require that the design of an EUV optical system be modified in any way, unlike the proposed use of blazed gratings for such systems.

  18. Active noise canceling system for mechanically cooled germanium radiation detectors

    DOE Patents [OSTI]

    Nelson, Karl Einar; Burks, Morgan T

    2014-04-22

    A microphonics noise cancellation system and method for improving the energy resolution for mechanically cooled high-purity Germanium (HPGe) detector systems. A classical adaptive noise canceling digital processing system using an adaptive predictor is used in an MCA to attenuate the microphonics noise source making the system more deployable.

  19. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print Wednesday, 27 March 2013 00:00 The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the

  20. PREPARATION OF HIGH PURITY UF$sub 4$

    DOE Patents [OSTI]

    Magner, J.E.; Long, R.S.; Ellis, D.A.; Grinstead, R.R.

    1962-04-17

    S>A process for preparing very highly pure uranous tetrafluoride from impure uranium laden solvent extraction strip solutions, ion exchange process and resin-inpulp process eluate solutions which are at least 8M in hydrochloric acid is described. The process first comprises treating any of the above-mentioned solutions with a reducing agent to reduce the uranium to the + 4 oxidation state, and then contacting the reduced solution with an extractant phase comprising about 10 to 70% of tri-butyl phosphate in an organic solvent-diluent selected from benzene, ethyl-benzene, chlorobenzene, xylene, kerosene, or the like. The uranium is extracted into the extractant phase and is subsequently precipitated by treating the extractant with an aqueous fluoride solution. The highly pure uranous tetrafluoride precipitate is separated from the phases and recovered for subsequent utilization. (AEC)

  1. Fused salt processing of impure plutonium dioxide to high-purity plutonium metal

    SciTech Connect (OSTI)

    Mullins, L.J.; Christensen, D.C.; Babcock, B.R.

    1982-01-01

    A process for converting impure plutonium dioxide (approx. 96% pure) to high-purity plutonium metal (>99.9%) was developed. The process consists of reducing the oxide to an impure plutonium metal intermediate with calcium metal in molten calcium chloride. The impure intermediate metal is cast into an anode and electrorefined to produce high-purity plutonium metal. The oxide reduction step is being done now on a 0.6-kg scale with the resulting yield being >99.5%. The electrorefining is being done on a 4.0-kg scale with the resulting yield being 80 to 85%. The purity of the product, which averages 99.98%, is essentially insensitive to the purity of the feed metal. The yield, however, is directly dependent on the chemical composition of the feed. To date, approximately 250 kg of impure oxide has been converted to pure metal by this processing sequence. The availability of impure plutonium dioxide, together with the need for pure plutonium metal, makes this sequence a valuable plutonium processing tool.

  2. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the discovery of mixed domains of donor and acceptor molecules, many have pictured the excitons' journey as easy

  3. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the discovery of mixed domains of donor and acceptor molecules, many have pictured the excitons' journey as easy

  4. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the discovery of mixed domains of donor and acceptor molecules, many have pictured the excitons' journey as easy

  5. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the discovery of mixed domains of donor and acceptor molecules, many have pictured the excitons' journey as easy

  6. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the discovery of mixed domains of donor and acceptor molecules, many have pictured the excitons' journey as easy

  7. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the discovery of mixed domains of donor and acceptor molecules, many have pictured the excitons' journey as easy

  8. The Importance of Domain Size and Purity in High-Efficiency Organic Solar

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cells The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Print The efficiency of polymer/organic photovoltaic cells hinges on excitons-electron/hole pairs energized by sunlight-getting to the interfaces of donor and acceptor domains quickly, before recombining. At the interfaces, they become free charges that must then reach device electrodes. With the discovery of mixed domains of donor and acceptor molecules, many have pictured the excitons' journey as easy

  9. Germanium-76 Sample Analysis: Revision 3

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Zhu, Zihua; Engelhard, Mark H.

    2011-09-19

    The MAJORANA DEMONSTRATOR is a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0{nu}{beta}{beta}). The DEMONSTRATOR will utilize 76Ge from Russia. The first one-gram sample was received from the supplier for analysis on April 24, 2011. The second one-gram sample was received from the supplier for analysis on July 12, 2011. The third sample, which came from the first large shipment of germanium from the vendor, was received from Oak Ridge National Laboratory (ORNL) on September 13, 2011. The Environmental Molecular Sciences facility, a DOE user facility at PNNL, was used to make the required isotopic and chemical purity measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR. The results of these analyses are reported here. The isotopic composition of a sample of natural germanium was also measured twice. Differences in the result between these two measurements led to a re-measurement of the second 76Ge sample.

  10. Simulations for Tracking Cosmogenic Activation in Germanium and Copper

    SciTech Connect (OSTI)

    Aguayo, Estanislao; Kouzes, Richard T.; Orrell, John L.

    2011-11-01

    High-purity germanium (HPGe) detectors housed in copper cryostats and shielding materials are used in measurements of the extraordinarily rare nuclear decay process, neutrinoless double-beta decay (0???), and for dark matter searches. Cosmogenic production of 68Ge and 60Co in the germanium and copper represent an irreducible background to these experiments as the subsequent decays of these isotopes can mimic the signals of interest. These radioactive isotopes can be removed by chemical and/or isotopic separation, but begin to grow-in to the material after separation until the material is moved deep underground. This work is motivated by the need to have a reliable, experimentally benchmarked simulation tool for evaluating shielding materials used during transportation and near-surface manufacturing of experiment components. The resulting simulations tool has been used to enhance the effectiveness of an existing transport shield used to ship enriched germanium from the separations facility to the detector manufacturing facility.

  11. New red phosphor for near-ultraviolet light-emitting diodes with high color-purity

    SciTech Connect (OSTI)

    Wang, Zhengliang; He, Pei; Wang, Rui; Zhao, Jishou; Gong, Menglian

    2010-02-15

    New red phosphors, Na{sub 5}Eu(MoO{sub 4}){sub 4} doped with boron oxide were prepared by the solid-state reaction. Their structure and photo-luminescent properties were investigated. With the introduction of boron oxide, the red emission intensity of the phosphors under 395 nm excitation is strengthened, with high color-purity (x = 0.673, y = 0.327). The single red light-emitting diode was obtained by combining InGaN chip with the red phosphor, bright red light can be observed by naked eyes from the red light-emitting diodes under a forward bias of 20 mA.

  12. SIMULTANEOUS PRODUCTION OF HIGH-PURITY HYDROGEN AND SEQUESTRATION-READY CO2 FROM SYNGAS

    SciTech Connect (OSTI)

    Linda Denton; Hana Lorethova; Tomasz Wiltowski; Court Moorefield; Parag Kulkarni; Vladimir Zamansky; Ravi Kumar

    2003-12-01

    This final report summarizes the progress made on the program ''Simultaneous Production of High-Purity Hydrogen and Sequestration-Ready CO{sub 2} from Syngas (contract number DE-FG26-99FT40682)'', during October 2000 through September of 2003. GE Energy and Environmental Research (GE-EER) and Southern Illinois University (SIU) at Carbondale conducted the research work for this program. This program addresses improved methods to efficiently produce simultaneous streams of high-purity hydrogen and separated carbon dioxide from synthesis gas (syngas). The syngas may be produced through either gasification of coal or reforming of natural gas. The process of production of H{sub 2} and separated CO{sub 2} utilizes a dual-bed reactor and regenerator system. The reactor produces hydrogen and the regenerator produces separated CO{sub 2}. The dual-bed system can be operated under either a circulating fluidized-bed configuration or a cyclic fixed-bed configuration. Both configurations were evaluated in this project. The experimental effort was divided into lab-scale work at SIU and bench-scale work at GE-EER. Tests in a lab-scale fluidized bed system demonstrated the process for the conversion of syngas to high purity H{sub 2} and separated CO{sub 2}. The lab-scale system generated up to 95% H{sub 2} (on a dry basis). Extensive thermodynamic analysis of chemical reactions between the syngas and the fluidized solids determined an optimum range of temperature and pressure operation, where the extent of the undesirable reactions is minimum. The cycling of the process between hydrogen generation and oxygen regeneration has been demonstrated. The fluidized solids did not regenerate completely and the hydrogen purity in the reuse cycle dropped to 70% from 95% (on a dry basis). Changes in morphology and particle size may be the most dominant factor affecting the efficiency of the repeated cycling between hydrogen production and oxygen regeneration. The concept of simultaneous production of hydrogen and separated stream of CO{sub 2} was proved using a fixed bed 2 reactor system at GE-EER. This bench-scale cyclic fixed-bed reactor system designed to reform natural gas to syngas has been fabricated in another coordinated DOE project. This system was modified to reform natural gas to syngas and then convert syngas to H{sub 2} and separated CO{sub 2}. The system produced 85% hydrogen (dry basis).

  13. Process for producing high purity isoolefins and dimers thereof by dissociation of ethers

    DOE Patents [OSTI]

    Smith, L.A. Jr.; Jones, E.M. Jr.; Hearn, D.

    1984-05-08

    Alkyl tertiary butyl ether or alkyl tertiary amyl ether is dissociated by vapor phase contact with a cation acidic exchange resin at temperatures in the range of 150 to 250 F at LHSV of 0.1 to 20 to produce a stream consisting of unreacted ether, isobutene or isoamylene and an alcohol corresponding to the alkyl radical. After the alcohol is removed, the ether/isoolefin stream may be fractionated to obtain a high purity isoolefin (99+%) or the ether/isoolefin stream can be contacted in liquid phase with a cation acidic exchange resin to selectively dimerize the isoolefin in a highly exothermic reaction, followed by fractionation of the dimerization product to produce high purity diisoolefin (97+%). In the case where the alkyl is C[sub 3] to C[sub 6] and the corresponding alcohol is produced on dissociation of the ether, combined dissociation-distillation may be carried out such that isoolefin is the overhead product and alcohol the bottom. 2 figs.

  14. Process for producing high purity isoolefins and dimers thereof by dissociation of ethers

    DOE Patents [OSTI]

    Smith, Jr., Lawrence A. (Bellaire, TX); Jones, Jr., Edward M. (Friendswood, TX); Hearn, Dennis (Houston, TX)

    1984-01-01

    Alkyl tertiary butyl ether or alkyl tertiary amyl ether is dissociated by vapor phase contact with a cation acidic exchange resin at temperatures in the range of 150.degree. to 250.degree. F. at LHSV of 0.1 to 20 to produce a stream consisting of unreacted ether, isobutene or isoamylene and an alcohol corresponding to the alkyl radical. After the alcohol is removed, the ether/isoolefin stream may be fractionated to obtain a high purity isoolefin (99+%) or the ether/isoolefin stream can be contacted in liquid phase with a cation acidic exchange resin to selectively dimerize the isoolefin in a highly exothermic reaction, followed by fractionation of the dimerization product to produce high purity diisoolefin (97+%). In the case where the alkyl is C.sub.3 to C.sub.6 and the corresponding alcohol is produced on dissociation of the ether, combined dissociation-distillation may be carried out such that isoolefin is the overhead product and alcohol the bottom.

  15. Process for producing high purity silicon nitride by the direct reaction between elemental silicon and nitrogen-hydrogen liquid reactants

    DOE Patents [OSTI]

    Pugar, E.A.; Morgan, P.E.D.

    1987-09-15

    A process is disclosed for producing, at a low temperature, a high purity reaction product consisting essentially of silicon, nitrogen, and hydrogen which can then be heated to produce a high purity alpha silicon nitride. The process comprises: reacting together a particulate elemental high purity silicon with a high purity nitrogen-hydrogen reactant in its liquid state (such as ammonia or hydrazine) having the formula: N/sub n/H/sub (n+m)/ wherein: n = 1--4 and m = 2 when the nitrogen-hydrogen reactant is straight chain, and 0 when the nitrogen-hydrogen reactant is cyclic. High purity silicon nitride can be formed from this intermediate product by heating the intermediate product at a temperature of from about 1200--1700/degree/C for a period from about 15 minutes up to about 2 hours to form a high purity alpha silicon nitride product. The discovery of the existence of a soluble Si/endash/N/endash/H intermediate enables chemical pathways to be explored previously unavailable in conventional solid-state approaches to silicon-nitrogen ceramics

  16. Process for producing high purity silicon nitride by the direct reaction between elemental silicon and nitrogen-hydrogen liquid reactants

    DOE Patents [OSTI]

    Pugar, Eloise A.; Morgan, Peter E. D.

    1990-01-01

    A process is disclosed for producing, at a low temperature, a high purity reaction product consisting essentially of silicon, nitrogen, and hydrogen which can then be heated to produce a high purity alpha silicon nitride. The process comprises: reacting together a particulate elemental high purity silicon with a high purity nitrogen-hydrogen reactant in its liquid state (such as ammonia or hydrazine) having the formula: N.sub.n H.sub.(n+m) wherein: n=1-4 and m=2 when the nitrogen-hydrogen reactant is straight chain, and 0 when the nitrogen-hydrogen reactant is cyclic. High purity silicon nitride can be formed from this intermediate product by heating the intermediate product at a temperature of from about 1200.degree.-1700.degree. C. for a period from about 15 minutes up to about 2 hours to form a high purity alpha silicon nitride product. The discovery of the existence of a soluble Si-N-H intermediate enables chemical pathways to be explored previously unavailable in conventional solid state approaches to silicon-nitrogen ceramics.

  17. Surface preparation for high purity alumina ceramics enabling direct brazing in hydrogen atmospheres

    DOE Patents [OSTI]

    Cadden, Charles H. (Danville, CA); Yang, Nancy Yuan Chi (Lafayette, CA); Hosking, Floyd M. (Albuquerque, NM)

    2001-01-01

    The present invention relates to a method for preparing the surface of a high purity alumina ceramic or sapphire specimen that enables direct brazing in a hydrogen atmosphere using an active braze alloy. The present invention also relates to a method for directly brazing a high purity alumina ceramic or sapphire specimen to a ceramic or metal member using this method of surface preparation, and to articles produced by this brazing method. The presence of silicon, in the form of a SiO.sub.2 -containing surface layer, can more than double the tensile bond strength in alumina ceramic joints brazed in a hydrogen atmosphere using an active Au-16Ni-0.75 Mo-1.75V filler metal. A thin silicon coating applied by PVD processing can, after air firing, produce a semi-continuous coverage of the alumina surface with a SiO.sub.2 film. Room temperature tensile strength was found to be proportional to the fraction of air fired surface covered by silicon-containing films. Similarly, the ratio of substrate fracture versus interface separation was also related to the amount of surface silicon present prior to brazing. This process can replace the need to perform a "moly-manganese" metallization step.

  18. Production of carbon monoxide-free hydrogen and helium from a high-purity source

    DOE Patents [OSTI]

    Golden, Timothy Christopher (Allentown, PA); Farris, Thomas Stephen (Bethlehem, PA)

    2008-11-18

    The invention provides vacuum swing adsorption processes that produce an essentially carbon monoxide-free hydrogen or helium gas stream from, respectively, a high-purity (e.g., pipeline grade) hydrogen or helium gas stream using one or two adsorber beds. By using physical adsorbents with high heats of nitrogen adsorption, intermediate heats of carbon monoxide adsorption, and low heats of hydrogen and helium adsorption, and by using vacuum purging and high feed stream pressures (e.g., pressures of as high as around 1,000 bar), pipeline grade hydrogen or helium can purified to produce essentially carbon monoxide -free hydrogen and helium, or carbon monoxide, nitrogen, and methane-free hydrogen and helium.

  19. Formation of nanotwin networks during high-temperature crystallization of amorphous germanium

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Sandoval, Luis; Reina, Celia; Marian, Jaime

    2015-11-26

    Germanium is an extremely important material used for numerous functional applications in many fields of nanotechnology. In this paper, we study the crystallization of amorphous Ge using atomistic simulations of critical nano-metric nuclei at high temperatures. We find that crystallization occurs by the recurrent transfer of atoms via a diffusive process from the amorphous phase into suitably-oriented crystalline layers. We accompany our simulations with a comprehensive thermodynamic and kinetic analysis of the growth process, which explains the energy balance and the interfacial growth velocities governing grain growth. For the <111> crystallographic orientation, we find a degenerate atomic rearrangement process, withmore » two zero-energy modes corresponding to a perfect crystalline structure and the formation of a Σ3 twin boundary. Continued growth in this direction results in the development a twin network, in contrast with all other growth orientations, where the crystal grows defect-free. This particular mechanism of crystallization from amorphous phases is also observed during solid-phase epitaxial growth of <111> semiconductor crystals, where growth is restrained to one dimension. Lastly, we calculate the equivalent X-ray diffraction pattern of the obtained nanotwin networks, providing grounds for experimental validation.« less

  20. Formation of nanotwin networks during high-temperature crystallization of amorphous germanium

    SciTech Connect (OSTI)

    Sandoval, Luis; Reina, Celia; Marian, Jaime

    2015-11-26

    Germanium is an extremely important material used for numerous functional applications in many fields of nanotechnology. In this paper, we study the crystallization of amorphous Ge using atomistic simulations of critical nano-metric nuclei at high temperatures. We find that crystallization occurs by the recurrent transfer of atoms via a diffusive process from the amorphous phase into suitably-oriented crystalline layers. We accompany our simulations with a comprehensive thermodynamic and kinetic analysis of the growth process, which explains the energy balance and the interfacial growth velocities governing grain growth. For the <111> crystallographic orientation, we find a degenerate atomic rearrangement process, with two zero-energy modes corresponding to a perfect crystalline structure and the formation of a Σ3 twin boundary. Continued growth in this direction results in the development a twin network, in contrast with all other growth orientations, where the crystal grows defect-free. This particular mechanism of crystallization from amorphous phases is also observed during solid-phase epitaxial growth of <111> semiconductor crystals, where growth is restrained to one dimension. Lastly, we calculate the equivalent X-ray diffraction pattern of the obtained nanotwin networks, providing grounds for experimental validation.

  1. Local deposition of high-purity Pt nanostructures by combining electron beam induced deposition and atomic layer deposition

    SciTech Connect (OSTI)

    Mackus, A. J. M.; Sanden, M. C. M. van de; Kessels, W. M. M.; Mulders, J. J. L.

    2010-06-15

    An approach for direct-write fabrication of high-purity platinum nanostructures has been developed by combining nanoscale lateral patterning by electron beam induced deposition (EBID) with area-selective deposition of high quality material by atomic layer deposition (ALD). Because virtually pure, polycrystalline Pt nanostructures are obtained, the method extends the application possibilities of EBID, whereas compared to other area-selective ALD approaches, a much higher resolution is attainable; potentially down to sub-10 nm lateral dimensions.

  2. Germanium detectors in homeland security at PNNL

    SciTech Connect (OSTI)

    Stave, S.

    2015-05-01

    Neutron and gamma-ray detection is used for non-proliferation and national security applications. While lower energy resolution detectors such as NaI(Tl) have their place, high purity germanium (HPGe) also has a role to play. A detection with HPGe is often a characterization due to the very high energy resolution. However, HPGe crystals remain small and expensive leaving arrays of smaller crystals as an excellent solution. PNNL has developed two similar HPGe arrays for two very different applications. One array, the Multisensor Aerial Radiation Survey (MARS) detector is a fieldable array that has been tested on trucks, boats, and helicopters. The CASCADES HPGe array is an array designed to assay samples in a low background environment. The history of HPGe arrays at PNNL and the development of MARS and CASCADES will be detailed in this paper along with some of the other applications of HPGe at PNNL.

  3. Germanium detectors in homeland security at PNNL

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Stave, S.

    2015-05-01

    Neutron and gamma-ray detection is used for non-proliferation and national security applications. While lower energy resolution detectors such as NaI(Tl) have their place, high purity germanium (HPGe) also has a role to play. A detection with HPGe is often a characterization due to the very high energy resolution. However, HPGe crystals remain small and expensive leaving arrays of smaller crystals as an excellent solution. PNNL has developed two similar HPGe arrays for two very different applications. One array, the Multisensor Aerial Radiation Survey (MARS) detector is a fieldable array that has been tested on trucks, boats, and helicopters. The CASCADESmore » HPGe array is an array designed to assay samples in a low background environment. The history of HPGe arrays at PNNL and the development of MARS and CASCADES will be detailed in this paper along with some of the other applications of HPGe at PNNL.« less

  4. Phonon Quasidiffusion in Cryogenic Dark Matter Search Large Germanium Detectors

    SciTech Connect (OSTI)

    Leman, S.W.; /MIT, MKI; Cabrera, B.; /Stanford U., Phys. Dept.; McCarthy, K.A.; /MIT, MKI; Pyle, M.; /Stanford U., Phys. Dept.; Resch, R.; /SLAC; Sadoulet, B.; Sundqvist, K.M.; /LBL, Berkeley; Brink, P.L.; Cherry, M.; /Stanford U., Phys. Dept.; Do Couto E Silva, E.; /SLAC; Figueroa-Feliciano, E.; /MIT, MKI; Mirabolfathi, N.; Serfass, B.; /UC, Berkeley; Tomada, A.; /Stanford U., Phys. Dept.

    2012-06-04

    We present results on quasidiffusion studies in large, 3 inch diameter, 1 inch thick [100] high purity germanium crystals, cooled to 50 mK in the vacuum of a dilution refrigerator, and exposed with 59.5 keV gamma-rays from an Am-241 calibration source. We compare data obtained in two different detector types, with different phonon sensor area coverage, with results from a Monte Carlo. The Monte Carlo includes phonon quasidiffusion and the generation of phonons created by charge carriers as they are drifted across the detector by ionization readout channels.

  5. Qualification and initial characterization of a high-purity 233U spike for use in uranium analyses

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Mathew, K. J.; Canaan, R. D.; Hexel, C.; Giaquinto, J.; Krichinsky, A. M.

    2015-08-20

    Several high-purity 233U items potentially useful as isotope dilution mass spectrometry standards for safeguards, non-proliferation, and nuclear forensics measurements are identified and rescued from downblending. By preserving the supply of 233U materials of different pedigree for use as source materials for certified reference materials (CRMs), it is ensured that the safeguards community has high quality uranium isotopic standards required for calibration of the analytical instruments. One of the items identified as a source material for a high-purity CRM is characterized for the uranium isotope-amount ratios using thermal ionization mass spectrometry (TIMS). Additional verification measurements on this material using quadrupole inductivelymore » coupled plasma mass spectrometry (ICPMS) are also performed. As a result, the comparison of the ICPMS uranium isotope-amount ratios with the TIMS data, with much smaller uncertainties, validated the ICPMS measurement practices. ICPMS is proposed for the initial screening of the purity of items in the rescue campaign.« less

  6. Qualification and initial characterization of a high-purity 233U spike for use in uranium analyses

    SciTech Connect (OSTI)

    Mathew, K. J.; Canaan, R. D.; Hexel, C.; Giaquinto, J.; Krichinsky, A. M.

    2015-08-20

    Several high-purity 233U items potentially useful as isotope dilution mass spectrometry standards for safeguards, non-proliferation, and nuclear forensics measurements are identified and rescued from downblending. By preserving the supply of 233U materials of different pedigree for use as source materials for certified reference materials (CRMs), it is ensured that the safeguards community has high quality uranium isotopic standards required for calibration of the analytical instruments. One of the items identified as a source material for a high-purity CRM is characterized for the uranium isotope-amount ratios using thermal ionization mass spectrometry (TIMS). Additional verification measurements on this material using quadrupole inductively coupled plasma mass spectrometry (ICPMS) are also performed. As a result, the comparison of the ICPMS uranium isotope-amount ratios with the TIMS data, with much smaller uncertainties, validated the ICPMS measurement practices. ICPMS is proposed for the initial screening of the purity of items in the rescue campaign.

  7. High-capacity nanostructured germanium-containing materials and lithium alloys thereof

    DOE Patents [OSTI]

    Graetz, Jason A. (Upton, NY); Fultz, Brent T. (Pasadena, CA); Ahn, Channing (Pasadena, CA); Yazami, Rachid (Los Angeles, CA)

    2010-08-24

    Electrodes comprising an alkali metal, for example, lithium, alloyed with nanostructured materials of formula Si.sub.zGe.sub.(z-1), where 0germanium exhibit a combination of improved capacities, cycle lives, and/or cycling rates compared with similar electrodes made from graphite. These electrodes are useful as anodes for secondary electrochemical cells, for example, batteries and electrochemical supercapacitors.

  8. High Purity Hydrogen Production with In-Situ Carbon Dioxide and Sulfur Capture in a Single Stage Reactor

    SciTech Connect (OSTI)

    Nihar Phalak; Shwetha Ramkumar; Daniel Connell; Zhenchao Sun; Fu-Chen Yu; Niranjani Deshpande; Robert Statnick; Liang-Shih Fan

    2011-07-31

    Enhancement in the production of high purity hydrogen (H{sub 2}) from fuel gas, obtained from coal gasification, is limited by thermodynamics of the water gas shift (WGS) reaction. However, this constraint can be overcome by conducting the WGS in the presence of a CO{sub 2}-acceptor. The continuous removal of CO{sub 2} from the reaction mixture helps to drive the equilibrium-limited WGS reaction forward. Since calcium oxide (CaO) exhibits high CO{sub 2} capture capacity as compared to other sorbents, it is an ideal candidate for such a technique. The Calcium Looping Process (CLP) developed at The Ohio State University (OSU) utilizes the above concept to enable high purity H{sub 2} production from synthesis gas (syngas) derived from coal gasification. The CLP integrates the WGS reaction with insitu CO{sub 2}, sulfur and halide removal at high temperatures while eliminating the need for a WGS catalyst, thus reducing the overall footprint of the hydrogen production process. The CLP comprises three reactors - the carbonator, where the thermodynamic constraint of the WGS reaction is overcome by the constant removal of CO{sub 2} product and high purity H{sub 2} is produced with contaminant removal; the calciner, where the calcium sorbent is regenerated and a sequestration-ready CO{sub 2} stream is produced; and the hydrator, where the calcined sorbent is reactivated to improve its recyclability. As a part of this project, the CLP was extensively investigated by performing experiments at lab-, bench- and subpilot-scale setups. A comprehensive techno-economic analysis was also conducted to determine the feasibility of the CLP at commercial scale. This report provides a detailed account of all the results obtained during the project period.

  9. Preparation of uniform nanoparticles of ultra-high purity metal oxides, mixed metal oxides, metals, and metal alloys

    DOE Patents [OSTI]

    Woodfield, Brian F.; Liu, Shengfeng; Boerio-Goates, Juliana; Liu, Qingyuan; Smith, Stacey Janel

    2012-07-03

    In preferred embodiments, metal nanoparticles, mixed-metal (alloy) nanoparticles, metal oxide nanoparticles and mixed-metal oxide nanoparticles are provided. According to embodiments, the nanoparticles may possess narrow size distributions and high purities. In certain preferred embodiments, methods of preparing metal nanoparticles, mixed-metal nanoparticles, metal oxide nanoparticles and mixed-metal nanoparticles are provided. These methods may provide tight control of particle size, size distribution, and oxidation state. Other preferred embodiments relate to a precursor material that may be used to form nanoparticles. In addition, products prepared from such nanoparticles are disclosed.

  10. Preparation of high purity plutonium oxide for radiochemistry instrument calibration standards and working standards

    SciTech Connect (OSTI)

    Wong, A.S.; Stalnaker, N.D.

    1997-04-01

    Due to the lack of suitable high level National Institute of Standards and Technology (NIST) traceable plutonium solution standards from the NIST or commercial vendors, the CST-8 Radiochemistry team at Los Alamos National Laboratory (LANL) has prepared instrument calibration standards and working standards from a well-characterized plutonium oxide. All the aliquoting steps were performed gravimetrically. When a {sup 241}Am standardized solution obtained from a commercial vendor was compared to these calibration solutions, the results agreed to within 0.04% for the total alpha activity. The aliquots of the plutonium standard solutions and dilutions were sealed in glass ampules for long term storage.

  11. A simplified method for obtaining high-purity perchlorate from groundwater for isotope analyses.

    SciTech Connect (OSTI)

    vonKiparski, G; Hillegonds, D

    2011-04-04

    Investigations into the occurrence and origin of perchlorate (ClO{sub 4}{sup -}) found in groundwater from across North America have been sparse until recent years, and there is mounting evidence that natural formation mechanisms are important. New opportunities for identifying groundwater perchlorate and its origin have arisen with the utilization of improved detection methods and sampling techniques. Additionally, application of the forensic potential of isotopic measurements has begun to elucidate sources, potential formation mechanisms and natural attenuation processes. Procedures developed appear to be amenable to enable high precision stable isotopic analyses, as well as lower precision AMS analyses of {sup 36}Cl. Immediate work is in analyzing perchlorate isotope standards and developing full analytical accuracy and uncertainty expectations. Field samples have also been collected, and will be analyzed when final qa/qc samples are deemed acceptable.

  12. Experimental Demonstration of Advanced Palladium Membrane Separators for Central High Purity Hydrogen Production

    SciTech Connect (OSTI)

    Sean Emerson; Neal Magdefrau; Susanne Opalka; Ying She; Catherine Thibaud-Erkey; Thoman Vanderspurt; Rhonda Willigan

    2010-06-30

    The overall objectives for this project were to: (1) confirm the high stability and resistance of a PdCu trimetallic alloy to carbon and carbide formation and, in addition, resistance to sulfur, halides, and ammonia; (2) develop a sulfur, halide, and ammonia resistant alloy membrane with a projected hydrogen permeance of 25 m{sup 3}m{sup -2}atm{sup -0.5}h{sup -1} at 400 C and capable of operating at pressures of 12.1 MPa ({approx}120 atm, 1750 psia); and (3) construct and experimentally validate the performance of 0.1 kg/day H{sup 2} PdCu trimetallic alloy membrane separators at feed pressures of 2 MPa (290 psia) in the presence of H{sub 2}S, NH{sub 3}, and HCl. This project successfully increased the technology readiness level of palladium-based metallic membranes for hydrogen separation from coal-biomass gasifier exhaust or similar hydrogen-containing gas streams. The reversible tolerance of palladium-copper (PdCu) alloys was demonstrated for H{sub 2}S concentrations varying from 20 ppmv up to 487 ppmv and NH{sub 3} concentrations up to 9 ppmv. In addition, atomistic modeling validated the resistance of PdCu alloys to carbon formation, irreversible sulfur corrosion, and chlorine attack. The experimental program highlighted two key issues which must be addressed as part of future experimental programs: (1) tube defects and (2) non-membrane materials of construction. Four out of five FCC PdCu separators developed leaks during the course of the experimental program because {approx}10% of the alloy tubes contained a single defect that resulted in a thin, weak point in the tube walls. These defects limited operation of the existing tubes to less than 220 psig. For commercial applications of a PdCu alloy hydrogen separator under high sulfur concentrations, it was determined that stainless steel 316 is not suitable for housing or supporting the device. Testing with sulfur concentrations of 487 {+-} 4 ppmv resulted in severe corrosion of the stainless steel components of the separators. The project identified an experimental methodology for quantifying the impact of gas contaminants on PdCu alloy membrane performance as well as an atomistic modeling approach to screen metal alloys for their resistance to irreversible sulfur corrosion. Initial mathematical descriptions of the effect of species such as CO and H{sub 2}S were developed, but require further experimental work to refine. At the end of the project, an improvement to the experimental approach for acquiring the necessary data for the permeability model was demonstrated in preliminary tests on an enhanced PdCu separator. All of the key DOE 2010 technical targets were met or exceeded except for the hydrogen flux. The highest flux observed for the project, 125 ft{sup 3}ft{sup -2}h{sup -1}, was obtained on a single tube separator with the aforementioned enhanced PdCu separator with a hydrogen feed pressure of 185 psig at 500 C.

  13. Germanium detector passivated with hydrogenated amorphous germanium

    DOE Patents [OSTI]

    Hansen, William L. (Walnut Creek, CA); Haller, Eugene E. (Berkeley, CA)

    1986-01-01

    Passivation of predominantly crystalline semiconductor devices (12) is provided for by a surface coating (21) of sputtered hydrogenated amorphous semiconductor material. Passivation of a radiation detector germanium diode, for example, is realized by sputtering a coating (21) of amorphous germanium onto the etched and quenched diode surface (11) in a low pressure atmosphere of hydrogen and argon. Unlike prior germanium diode semiconductor devices (12), which must be maintained in vacuum at cryogenic temperatures to avoid deterioration, a diode processed in the described manner may be stored in air at room temperature or otherwise exposed to a variety of environmental conditions. The coating (21) compensates for pre-existing undesirable surface states as well as protecting the semiconductor device (12) against future impregnation with impurities.

  14. Couples Magnetic and Structural Transitions in High-Purity Dy and Gd5SbxGe4-x

    SciTech Connect (OSTI)

    Alexander S. Chernyshov

    2006-08-09

    Magnetic materials exhibiting magnetic phase transitions simultaneously with structural rearrangements of their crystal lattices hold a promise for numerous applications including magnetic refrigeration, magnetomechanical devices and sensors. We undertook a detailed study of a single crystal of dysprosium metal, which is a classical example of a system where magnetic and crystallographic sublattices can be either coupled or decoupled from one another. Magnetocaloric effect, magnetization, ac magnetic susceptibility, and heat capacity of high purity single crystals of dysprosium have been investigated over broad temperature and magnetic field intervals with the magnetic field vector parallel to either the a- or c-axes of the crystal. Notable differences in the behavior of the physical properties when compared to Dy samples studied in the past have been observed between 110 K and 125 K, and between 178 K and {approx}210 K. A plausible mechanism based on the formation of antiferromagnetic clusters in the impure Dy has been suggested in order to explain the reduction of the magnetocaloric effect in the vicinity of the Neel point. Experimental and theoretical investigations of the influence of commensurability effects on the magnetic phase diagram and the value of the magnetocaloric effect have been conducted. The presence of newly found anomalies in the physical properties has been considered as evidence of previously unreported states of Dy. The refined magnetic phase diagram of dysprosium with the magnetic field vector parallel to the a-axis of a crystal has been constructed and discussed. The magnetic and crystallographic properties of Gd{sub 5}Sb{sub x}Ge{sub 4-x} pseudo-binary system were studied by x-ray diffraction (at room temperature), heat capacity, ac-magnetic susceptibility, and magnetization in the temperature interval 5-320 K in magnetic fields up to 100 kOe. The magnetic properties of three composition (x = 0.5, 1,2) were examined in detail. The Gd{sub 5}Sb{sub 2}Ge{sub 2} compound that adopts Tm{sub 5}Sb{sub 2}Si{sub 2}-type of structure (space group is Cmca), shows a second order FM-PM transition at 200 K, whereas Gd{sub 5}Sb{sub x}Ge{sub 4-x} compounds for x = 0.5 and x = 1 (Sm{sub 5}Ge{sub 4}-type of structure, space group is Pnma) exhibit first order phase transformations at 45 K and 37 K, respectively.

  15. Measurement of the dielectric properties of high-purity sapphire at 1.865 GHZ from 2-10 Kelvin

    SciTech Connect (OSTI)

    N. Pogue, P. McIntyre, Akhdiyor Sattarov, Charles Reece

    2012-06-01

    A dielectric test cavity was designed and tested to measure the microwave dielectric properties of ultrapure sapphire at cryogenic temperatures. Measurements were performed by placing a large cylindrical crystal of sapphire in a Nb superconducting cavity operating in the TE01 mode at 1.865 GHz. The dielectric constant, heat capacity, and loss tangent were all calculated using experimental data and RF modeling software. The motivation for these measurements was to determine if such a sapphire could be used as a dielectric lens to focus the magnetic field onto a sample wafer in a high field wafer test cavity. The measured properties have been used to finalize the design of the wafer test cavity.

  16. Astroparticle physics with a customized low-background broad energy Germanium detector

    SciTech Connect (OSTI)

    Aalseth, Craig E.; Amman, M.; Avignone, Frank T.; Back, Henning O.; Barabash, Alexander S.; Barbeau, P. S.; Bergevin, M.; Bertrand, F.; Boswell, M.; Brudanin, V.; Bugg, William; Burritt, Tom H.; Busch, Matthew; Capps, Greg L.; Chan, Yuen-Dat; Collar, J. I.; Cooper, R. J.; Creswick, R.; Detwiler, Jason A.; Diaz, J.; Doe, Peter J.; Efremenko, Yuri; Egorov, Viatcheslav; Ejiri, H.; Elliott, Steven R.; Ely, James H.; Esterline, James H.; Farach, H. A.; Fast, James E.; Fields, N.; Finnerty, P.; Fujikawa, Brian; Fuller, Erin S.; Gehman, Victor M.; Giovanetti, G. K.; Guiseppe, Vincente; Gusey, K.; Hallin, A. L.; Harper, Gregory; Hazama, R.; Henning, Reyco; Hime, Andrew; Hoppe, Eric W.; Hossbach, Todd W.; Howe, M. A.; Johnson, R. A.; Keeter, K.; Keillor, Martin E.; Keller, C.; Kephart, Jeremy D.; Kidd, Mary; Knecht, A.; Kochetov, Oleg; Konovalov, S.; Kouzes, Richard T.; Leviner, L.; Loach, J. C.; Luke, P.; MacMullin, S.; Marino, Michael G.; Martin, R. D.; Mei, Dong-Ming; Miley, Harry S.; Miller, M. L.; Mizouni, Leila; Myers, Allan W.; Nomachi, Masaharu; Orrell, John L.; Peterson, David; Phillips, D.; Poon, Alan; Prior, Gersende; Qian, J.; Radford, D. C.; Rielage, Keith; Robertson, R. G. H.; Rodriguez, Larry; Rykaczewski, Krzysztof P.; Salazar, Harold; Schubert, Alexis G.; Shima, T.; Shirchenko, M.; Steele, David; Strain, J.; Swift, Gary; Thomas, K.; Timkin, V.; Tornow, W.; Van Wechel, T. D.; Vanyushin, I.; Varner, R. L.; Vetter, Kai; Wilkerson, J. F.; Wolfe, B. A.; Xiang, W.; Yakushev, E.; Yaver, Harold; Young, A.; Yu, Chang-Hong; Yumatov, Vladimir; Zhang, C.; Zimmerman, S.

    2011-10-01

    The Majorana Collaboration is building the Majorana Demonstrator, a 60 kg array of high purity germanium detectors housed in an ultra-low background shield at the Sanford Underground Laboratory in Lead, SD. The Majorana Demonstrator will search for neutrinoless double-beta decay of 76Ge while demonstrating the feasibility of a tonne-scale experiment. It may also carry out a dark matter search in the 1-10 GeV/c mass range. We have found that customized Broad Energy Germanium (BEGe) detectors produced by Canberra have several desirable features for a neutrinoless double-beta decay experiment, including low electronic noise, excellent pulse shape analysis capabilities, and simple fabrication. We have deployed a customized BEGe, the Majorana Low-Background BEGe at Kimballton (MALBEK), in a low-background cryostat and shield at the Kimballton Underground Research Facility in Virginia. This paper will focus on the detector characteristics and measurements that can be performed with such a radiation detector in a low-background environment.

  17. Robust Low-Cost Water-Gas Shift Membrane Reactor for High-Purity Hydrogen Production form Coal-Derived Syngas

    SciTech Connect (OSTI)

    James Torkelson; Neng Ye; Zhijiang Li; Decio Coutinho; Mark Fokema

    2008-05-31

    This report details work performed in an effort to develop a low-cost, robust water gas shift membrane reactor to convert coal-derived syngas into high purity hydrogen. A sulfur- and halide-tolerant water gas shift catalyst and a sulfur-tolerant dense metallic hydrogen-permeable membrane were developed. The materials were integrated into a water gas shift membrane reactor in order to demonstrate the production of >99.97% pure hydrogen from a simulated coal-derived syngas stream containing 2000 ppm hydrogen sulfide. The objectives of the program were to (1) develop a contaminant-tolerant water gas shift catalyst that is able to achieve equilibrium carbon monoxide conversion at high space velocity and low steam to carbon monoxide ratio, (2) develop a contaminant-tolerant hydrogen-permeable membrane with a higher permeability than palladium, (3) demonstrate 1 L/h purified hydrogen production from coal-derived syngas in an integrated catalytic membrane reactor, and (4) conduct a cost analysis of the developed technology.

  18. Germanium films by polymer-assisted deposition (Patent) | SciTech...

    Office of Scientific and Technical Information (OSTI)

    Title: Germanium films by polymer-assisted deposition Highly ordered Ge films are prepared directly on single crystal Si substrates by applying an aqueous coating solution having ...

  19. Germanium films by polymer-assisted deposition

    DOE Patents [OSTI]

    Jia, Quanxi; Burrell, Anthony K.; Bauer, Eve; Ronning, Filip; McCleskey, Thomas Mark; Zou, Guifu

    2013-01-15

    Highly ordered Ge films are prepared directly on single crystal Si substrates by applying an aqueous coating solution having Ge-bound polymer onto the substrate and then heating in a hydrogen-containing atmosphere. A coating solution was prepared by mixing water, a germanium compound, ethylenediaminetetraacetic acid, and polyethyleneimine to form a first aqueous solution and then subjecting the first aqueous solution to ultrafiltration.

  20. Surface Passivation of Germanium Nanowires

    SciTech Connect (OSTI)

    Adhikari, Hemant; Sun, Shiyu; Pianetta, Piero; Chidsey, Chirstopher E.D.; McIntyre, Paul C.; /SLAC, SSRL

    2005-05-13

    The surface of single crystal, cold-wall CVD-grown germanium nanowires was studied by synchrotron radiation photoemission spectroscopy (SR-PES) and also by conventional XPS. The as-grown germanium nanowires seem to be hydrogen terminated. Exposure to laboratory atmosphere leads to germanium oxide growth with oxidation states of Ge{sup 1+}, Ge{sup 2+}, Ge{sup 3+}, while exposure to UV light leads to a predominance of the Ge{sup 4+} oxidation state. Most of the surface oxide could be removed readily by aqueous HF treatment which putatively leaves the nanowire surface hydrogen terminated with limited stability in air. Alternatively, chlorine termination could be achieved by aq. HCl treatment of the native oxide-coated nanowires. Chlorine termination was found to be relatively more stable than the HF-last hydrogen termination.

  1. Preparation of High Purity, High Molecular-Weight Chitin from Ionic Liquids for Use as an Adsorbate for the Extraction of Uranium from Seawater (Workscope MS-FC: Fuel Cycle R&D)

    SciTech Connect (OSTI)

    Rogers, Robin

    2013-12-21

    Ensuring a domestic supply of uranium is a key issue facing the wider implementation of nuclear power. Uranium is mostly mined in Kazakhstan, Australia, and Canada, and there are few high-grade uranium reserves left worldwide. Therefore, one of the most appealing potential sources of uranium is the vast quantity dissolved in the oceans (estimated to be 4.4 billion tons worldwide). There have been research efforts centered on finding a means to extract uranium from seawater for decades, but so far none have resulted in an economically viable product, due in part to the fact that the materials that have been successfully demonstrated to date are too costly (in terms of money and energy) to produce on the necessary scale. Ionic Liquids (salts which melt below 100{degrees}C) can completely dissolve raw crustacean shells, leading to recovery of a high purity, high molecular weight chitin powder and to fibers and films which can be spun directly from the extract solution suggesting that continuous processing might be feasible. The work proposed here will utilize the unprecedented control this makes possible over the chitin fiber a) to prepare electrospun nanofibers of very high surface area and in specific architectures, b) to modify the fiber surfaces chemically with selective extractant capacity, and c) to demonstrate their utility in the direct extraction and recovery of uranium from seawater. This approach will 1) provide direct extraction of chitin from shellfish waste thus saving energy over the current industrial process for obtaining chitin; 2) allow continuous processing of nanofibers for very high surface area fibers in an economical operation; 3) provide a unique high molecular weight chitin not available from the current industrial process leading to stronger, more durable fibers; and 4) allow easy chemical modification of the large surface areas of the fibers for appending uranyl selective functionality providing selectivity and ease of stripping. The resulting sorbent should prove economically feasible, as well as providing an overall net energy gain.

  2. Germanium Oxide Nanoparticlesfor Superior Battery Electrodes - Energy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Innovation Portal Advanced Materials Advanced Materials Find More Like This Return to Search Germanium Oxide Nanoparticlesfor Superior Battery Electrodes Brookhaven National Laboratory Contact BNL About This Technology Technology Marketing Summary Compared to the graphite found in some batteries, similar elements such as tin, silicon, and germanium have much higher theoretical capacities for lithium ions, making them strong candidates for electrode materials. These new amorphous germanium

  3. Electromechanically-cooled germanium radiation detector system...

    Office of Scientific and Technical Information (OSTI)

    Electromechanically-cooled germanium radiation detector system Citation Details ... Save Share this Record Citation Formats MLA APA Chicago Bibtex Export Metadata Endnote ...

  4. The Majorana Demonstrator: A search for neutrinoless double-beta decay of germanium-76

    SciTech Connect (OSTI)

    Elliott, S. R.; Boswell, M.; Goett, J.; Rielage, K.; Ronquest, M. C.; Xu, W. [Los Alamos National Laboratory, Los Alamos, NM (United States); Abgrall, N.; Chan, Y-D.; Hegai, A.; Martin, R. D.; Mertens, S.; Poon, A. W. P. [Nuclear Science Division, Lawrence Berkeley National Laboratory, Berkeley, CA (United States); Aguayo, E.; Fast, J. E.; Hoppe, E. W.; Kouzes, R. T.; LaFerriere, B. D.; Orrell, J. L.; Overman, N. R.; Soin, A. [Pacific Northwest National Laboratory, Richland, WA (United States); and others

    2013-12-30

    The MAJORANA collaboration is searching for neutrinoless double beta decay using {sup 76}Ge, which has been shown to have a number of advantages in terms of sensitivities and backgrounds. The observation of neutrinoless double-beta decay would show that lepton number is violated and that neutrinos are Majorana particles and would simultaneously provide information on neutrino mass. Attaining sensitivities for neutrino masses in the inverted hierarchy region, 15 - 50 meV, will require large, tonne-scale detectors with extremely low backgrounds, at the level of ?1 count/t-y or lower in the region of the signal. The MAJORANA collaboration, with funding support from DOE Office of Nuclear Physics and NSF Particle Astrophysics, is constructing the DEMONSTRATOR, an array consisting of 40 kg of p-type point-contact high-purity germanium (HPGe) detectors, of which ?30 kg will be enriched to 87% in {sup 76}Ge. The DEMONSTRATOR is being constructed in a clean room laboratory facility at the 4850' level (4300 m.w.e.) of the Sanford Underground Research Facility (SURF) in Lead, SD. It utilizes a compact graded shield approach with the inner portion consisting of ultra-clean Cu that is being electroformed and machined underground. The primary aim of the DEMONSTRATOR is to show the feasibility of a future tonne-scale measurement in terms of backgrounds and scalability.

  5. Imaging the oblique propagation of electrons in germanium crystals...

    Office of Scientific and Technical Information (OSTI)

    electrons in germanium crystals at low temperature and low electric field This content ... electrons in germanium crystals at low temperature and low electric field Authors: ...

  6. ?-tin?Imma?sh Phase Transitions of Germanium (Journal Article...

    Office of Scientific and Technical Information (OSTI)

    DOE PAGES Search Results Publisher's Accepted Manuscript: -tinImmash Phase Transitions of Germanium Prev Next Title: -tinImmash Phase Transitions of Germanium...

  7. Germanium multiphase equation of state

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Crockett, Scott D.; Lorenzi-Venneri, Giulia De; Kress, Joel D.; Rudin, Sven P.

    2014-05-07

    A new SESAME multiphase germanium equation of state (EOS) has been developed using the best available experimental data and density functional theory (DFT) calculations. The equilibrium EOS includes the Ge I (diamond), the Ge II (β-Sn) and the liquid phases. The foundation of the EOS is based on density functional theory calculations which are used to determine the cold curve and the Debye temperature. Results are compared to Hugoniot data through the solid-solid and solid-liquid transitions. We propose some experiments to better understand the dynamics of this element

  8. Mechanically Cooled Large-Volume Germanium Detector Systems for Neclear Explosion Monitoring DOENA27323-2

    SciTech Connect (OSTI)

    Hull, E.L.

    2006-10-30

    Compact maintenance free mechanical cooling systems are being developed to operate large volume high-resolution gamma-ray detectors for field applications. To accomplish this we are utilizing a newly available generation of Stirling-cycle mechanical coolers to operate the very largest volume germanium detectors with no maintenance. The user will be able to leave these systems unplugged on the shelf until needed. The maintenance-free operating lifetime of these detector systems will exceed 5 years. Three important factors affect the operation of mechanically cooled germanium detectors: temperature, vacuum, and vibration. These factors will be studied in the laboratory at the most fundamental levels to insure a solid understanding of the physical limitations each factor places on a practical mechanically cooled germanium detector system. Using this knowledge, mechanically cooled germanium detector prototype systems will be designed and fabricated.

  9. Solution synthesis of germanium nanocrystals

    DOE Patents [OSTI]

    Gerung, Henry (Albuquerque, NM); Boyle, Timothy J. (Kensington, MD); Bunge, Scott D. (Cuyahoga Falls, OH)

    2009-09-22

    A method for providing a route for the synthesis of a Ge(0) nanometer-sized material from. A Ge(II) precursor is dissolved in a ligand heated to a temperature, generally between approximately 100.degree. C. and 400.degree. C., sufficient to thermally reduce the Ge(II) to Ge(0), where the ligand is a compound that can bond to the surface of the germanium nanomaterials to subsequently prevent agglomeration of the nanomaterials. The ligand encapsulates the surface of the Ge(0) material to prevent agglomeration. The resulting solution is cooled for handling, with the cooling characteristics useful in controlling the size and size distribution of the Ge(0) materials. The characteristics of the Ge(II) precursor determine whether the Ge(0) materials that result will be nanocrystals or nanowires.

  10. Optical properties of colloidal germanium nanocrystals

    SciTech Connect (OSTI)

    WILCOXON,JESS P.; PROVENCIO,PAULA P.; SAMARA,GEORGE A.

    2000-05-01

    Highly crystalline germanium (Ge) nanocrystals in the size range 2--10 nm were grown in inverse micelles and purified and size-separated by high pressure liquid chromatography with on-line optical and electrical diagnostics. The nanocrystals retain the diamond structure of bulk Ge down to at least 2.0 nm (containing about 150 Ge atoms). The background- and impurity-free extinction and photoluminescence (PL) spectra of these nanocrystals revealed rich structure which was interpreted in terms of the bandstructure of Ge shifted to higher energies by quantum confinement. The shifts ranged from {minus}0.1 eV to over 1 eV for the various transitions. PL in the range 350--700 nm was observed from nanocrystals 2--5 nm in size. The 2.0 nm nanocrystals yielded the most intense PL (at 420 nm) which is believed to be intrinsic and attributed to direct recombination at {Gamma}. Excitation at high energy (250 nm) populates most of the conduction bands resulting in competing recombination channels and the observed broad PL spectra.

  11. MaGe - a GEANT4-based Monte Carlo Application Framework for Low-background Germanium Experiments

    SciTech Connect (OSTI)

    Boswell, M.; Chan, Yuen-Dat; Detwiler, Jason A.; Finnerty, P.; Henning, R.; Gehman, Victor; Johnson, Robert A.; Jordan, David V.; Kazkaz, Kareem; Knapp, Markus; Kroninger, Kevin; Lenz, Daniel; Leviner, L.; Liu, Jing; Liu, Xiang; MacMullin, S.; Marino, Michael G.; Mokhtarani, A.; Pandola, Luciano; Schubert, Alexis G.; Schubert, J.; Tomei, Claudia; Volynets, Oleksandr

    2011-06-13

    We describe a physics simulation software framework, MAGE, that is based on the GEANT4 simulation toolkit. MAGE is used to simulate the response of ultra-low radioactive background radiation detectors to ionizing radiation, speci?cally the MAJ ORANA and GE RDA neutrinoless double-beta decay experiments. MAJ ORANA and GERDA use high-purity germanium technology to search for the neutrinoless double-beta decay of the 76 Ge isotope, and MAGE is jointly developed between these two collaborations. The MAGE framework contains simulated geometries of common objects, prototypes, test stands, and the actual experiments. It also implements customized event generators, GE ANT 4 physics lists, and output formats. All of these features are available as class libraries that are typically compiled into a single executable. The user selects the particular experimental setup implementation at run-time via macros. The combination of all these common classes into one framework reduces duplication of efforts, eases comparison between simulated data and experiment, and simpli?es the addition of new detectors to be simulated. This paper focuses on the software framework, custom event generators, and physics list.

  12. Titanium and germanium lined hohlraums and halfraums as multi...

    Office of Scientific and Technical Information (OSTI)

    Titanium and germanium lined hohlraums and halfraums as multi-keV X-ray radiators Citation Details In-Document Search Title: Titanium and germanium lined hohlraums and halfraums as...

  13. Recovery of germanium-68 from irradiated targets

    DOE Patents [OSTI]

    Phillips, Dennis R.; Jamriska, Sr., David J.; Hamilton, Virginia T.

    1993-01-01

    A process for selective separation of germanium-68 from proton irradiated molybdenum targets is provided and includes dissolving the molybdenum target in a hydrogen peroxide solution to form a first ion-containing solution, contacting the first ion-containing solution with a cationic resin whereby ions selected from the group consisting of molybdenum, niobium, technetium, selenium, vanadium, arsenic, germanium, zirconium and rubidium remain in a second ion-containing solution while ions selected from the group consisting of rubidium, zinc, beryllium, cobalt, iron, manganese, chromium, strontium, yttrium and zirconium are selectively adsorbed by the first resin, adjusting the pH of the second ion-containing solution to within a range of from about 0.7 to about 3.0, adjusting the soluble metal halide concentration in the second ion-containing solution to a level adapted for subsequent separation of germanium, contacting the pH-adjusted, soluble metal halide-containing second ion-containing solution with a dextran-based material whereby germanium ions are separated by the dextran-based material, and recovering the germanium from the dextran-based material, preferably by distillation.

  14. Method for producing evaporation inhibiting coating for protection of silicon--germanium and silicon--molybdenum alloys at high temperatures in vacuum

    DOE Patents [OSTI]

    Chao, P.J.

    1974-01-01

    A method is given for protecting Si--Ge and Si-- Mo alloys for use in thermocouples. The alloys are coated with silicon to inhibit the evaporation of the alloys at high tempenatures in a vacuum. Specific means and methods are provided. (5 fig) (Official Gazette)

  15. Germanium-induced stabilization of a very high-k zirconia phase in ZrO{sub 2}/GeO{sub 2} gate stacks

    SciTech Connect (OSTI)

    Tsipas, P.; Volkos, S. N.; Sotiropoulos, A.; Galata, S. F.; Mavrou, G.; Tsoutsou, D.; Panayiotatos, Y.; Dimoulas, A.; Marchiori, C.; Fompeyrine, J.

    2008-08-25

    Electrical data on ZrO{sub 2}/GeO{sub 2} stacks prepared by atomic oxygen beam deposition on Ge at 225 deg. C reveal a relatively weak dependence of the stack equivalent oxide thickness upon the ZrO{sub 2} thickness. This trend points to a very high zirconia dielectric permittivity (k) value which is estimated to be around 44. This is indicative of zirconia crystallization into a tetragonal phase which is also supported by x-ray diffraction data. X-ray photoelectron spectroscopy analysis is in line with the assumption that due to a finite GeO{sub 2} decomposition, Ge is incorporated into the growing ZrO{sub 2}, thus, stabilizing the high-k tetragonal phase.

  16. Erratum: ''Titanium and germanium lined hohlraums and halfraums...

    Office of Scientific and Technical Information (OSTI)

    Country of Publication: United States Language: English Subject: 70 PLASMA PHYSICS AND FUSION TECHNOLOGY; GERMANIUM; ICF DEVICES; INERTIAL CONFINEMENT; KEV RANGE; LASER TARGETS; ...

  17. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of removing-silicon (and germanium) nanostructures at precise wafer locations. This strategy holds the potential for fabricating transistors in fewer steps with less material...

  18. Young’s modulus of [111] germanium nanowires

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Maksud, M.; Yoo, J.; Harris, C. T.; Palapati, N. K. R.; Subramanian, A.

    2015-11-02

    Our paper reports a diameter-independent Young’s modulus of 91.9 ± 8.2 GPa for [111] Germanium nanowires (Ge NWs). When the surface oxide layer is accounted for using a core-shell NW approximation, the YM of the Ge core approaches a near theoretical value of 147.6 ± 23.4 GPa. The ultimate strength of a NW device was measured at 10.9 GPa, which represents a very high experimental-to-theoretical strength ratio of ~75%. Furthermore, with increasing interest in this material system as a high-capacity lithium-ion battery anode, the presented data provide inputs that are essential in predicting its lithiation-induced stress fields and fracture behavior.

  19. Youngs modulus of [111] germanium nanowires

    SciTech Connect (OSTI)

    Maksud, M.; Yoo, J.; Harris, C. T.; Palapati, N. K. R.; Subramanian, A.

    2015-11-02

    Our paper reports a diameter-independent Youngs modulus of 91.9 8.2 GPa for [111] Germanium nanowires (Ge NWs). When the surface oxide layer is accounted for using a core-shell NW approximation, the YM of the Ge core approaches a near theoretical value of 147.6 23.4 GPa. The ultimate strength of a NW device was measured at 10.9 GPa, which represents a very high experimental-to-theoretical strength ratio of ~75%. Furthermore, with increasing interest in this material system as a high-capacity lithium-ion battery anode, the presented data provide inputs that are essential in predicting its lithiation-induced stress fields and fracture behavior.

  20. Screening of the quantum-confined Stark effect in AlN/GaN nanowire superlattices by germanium doping

    SciTech Connect (OSTI)

    Hille, P. Mener, J.; Becker, P.; Teubert, J.; Schrmann, J.; Eickhoff, M.; Mata, M. de la; Rosemann, N.; Chatterjee, S.; Magn, C.; Arbiol, J.; Institucio Catalana de Recerca i Estudis Avanats , 08010 Barcelona, CAT

    2014-03-10

    We report on electrostatic screening of polarization-induced internal electric fields in AlN/GaN nanowire heterostructures with germanium-doped GaN nanodiscs embedded between AlN barriers. The incorporation of germanium at concentrations above 10{sup 20}?cm{sup 3} shifts the photoluminescence emission energy of GaN nanodiscs to higher energies accompanied by a decrease of the photoluminescence decay time. At the same time, the thickness-dependent shift in emission energy is significantly reduced. In spite of the high donor concentration, a degradation of the photoluminescence properties is not observed.

  1. Actinium radioisotope products of enhanced purity

    DOE Patents [OSTI]

    Meikrantz, David Herbert; Todd, Terry Allen; Tranter, Troy Joseph; Horwitz, E. Philip

    2010-06-15

    A product includes actinium-225 (.sup.225Ac) and less than about 1 microgram (.mu.g) of iron (Fe) per millicurie (mCi) of actinium-225. The product may have a radioisotopic purity of greater than about 99.99 atomic percent (at %) actinium-225 and daughter isotopes of actinium-225, and may be formed by a method that includes providing a radioisotope mixture solution comprising at least one of uranium-233 (.sup.233U) and thorium-229 (.sup.229Th), extracting the at least one of uranium-233 and thorium-229 into an organic phase, substantially continuously contacting the organic phase with an aqueous phase, substantially continuously extracting actinium-225 into the aqueous phase, and purifying the actinium-225 from the aqueous phase. In some embodiments, the product may include less than about 1 nanogram (ng) of iron per millicurie (mCi) of actinium-225, and may include less than about 1 microgram (.mu.g) each of magnesium (Mg), Chromium (Cr), and manganese (Mn) per millicurie (mCi) of actinium-225.

  2. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Direct-Write of Silicon and Germanium Nanostructures Direct-Write of Silicon and Germanium Nanostructures Print Wednesday, 29 June 2011 00:00 Nanostructured materials (nanowires, nanotubes, nanoclusters, graphene) are attractive possible alternatives to traditionally microfabricated silicon in continuing the miniaturization trend in the electronics industry. To go from nanomaterials to electronics, however, the precise one-by-one assembly of billions of nanoelements into a functioning circuit is

  3. Geometrical and band-structure effects on phonon-limited hole mobility in rectangular cross-sectional germanium nanowires

    SciTech Connect (OSTI)

    Tanaka, H. Mori, S.; Morioka, N.; Suda, J.; Kimoto, T.

    2014-12-21

    We calculated the phonon-limited hole mobility in rectangular cross-sectional [001], [110], [111], and [112]-oriented germanium nanowires, and the hole transport characteristics were investigated. A tight-binding approximation was used for holes, and phonons were described by a valence force field model. Then, scattering probability of holes by phonons was calculated taking account of hole-phonon interaction atomistically, and the linearized Boltzmann's transport equation was solved to calculate the hole mobility at low longitudinal field. The dependence of the hole mobility on nanowire geometry was analyzed in terms of the valence band structure of germanium nanowires, and it was found that the dependence was qualitatively reproduced by considering an average effective mass and the density of states of holes. The calculation revealed that [110] germanium nanowires with large height along the [001] direction show high hole mobility. Germanium nanowires with this geometry are also expected to exhibit high electron mobility in our previous work, and thus they are promising for complementary metal-oxide-semiconductor (CMOS) applications.

  4. Germanium blocked impurity band infrared detectors

    SciTech Connect (OSTI)

    Rossington, C.S.; Haller, E.E.

    1988-08-01

    Germanium blocked impurity band (BIB) photoconductors have been fabricated and characterized for responsivity, dark current, and noise equivalent power. BIB photoconductors theoretically provide an extension of the spectral response, a reduction in sensitivity to cosmic radiation and a reduction in noise characteristics compared with conventional photoconductors. Silicon BIB detectors have been successfully developed by researchers at Rockwell International, which do indeed meet their theoretical potential. In the proper configuration, these same Si BIB detectors are capable of continuous detection of individual photons in the wavelength range from 0.4 to 28 ..mu..m. Until the BIB concept was developed, detection of individual photons was only possible with photomultiplier tubes which detected visible light. Due to the successes of the Si BIB detectors, it seemed natural to extend this concept to Ge detectors, which would then allow an extension of the spectral response over conventional Ge detectors from /approximately/100 ..mu..m to /approximately/200 ..mu..m. 8 refs., 2 figs.

  5. Germanium FCC structure from a colloidal crystal template

    SciTech Connect (OSTI)

    Miguez, H.; Meseguer, F.; Lopez, C.; Holgado, M.; Andreasen, G.; Mifsud, A.; Fornes, V.

    2000-05-16

    Here, the authors show a method to fabricate a macroporous structure in which the pores, essentially identical, arrange regularly in a face-centered cubic (FCC) lattice. The result is a network of air spheres in a germanium medium. This structure presents the highest dielectric contrast ({epsilon}{sub Ge}/{epsilon}{sub air} = 16) ever achieved in the optical regime in such periodic structures, which could result in important applications in photonics. The authors employ solid silica colloidal crystals (opals) as templates within which a cyclic germanium growth process is carried out. Thus, the three-dimensional periodicity of the host is inherited by the guest. Afterward, the silica is removed and a germanium opal replica is obtained.

  6. Erratum: ''Titanium and germanium lined hohlraums and halfraums as

    Office of Scientific and Technical Information (OSTI)

    multi-keV x-ray radiators'' [Phys. Plasmas 16, 052704 (2009)] (Journal Article) | SciTech Connect Erratum: ''Titanium and germanium lined hohlraums and halfraums as multi-keV x-ray radiators'' [Phys. Plasmas 16, 052704 (2009)] Citation Details In-Document Search Title: Erratum: ''Titanium and germanium lined hohlraums and halfraums as multi-keV x-ray radiators'' [Phys. Plasmas 16, 052704 (2009)] No abstract prepared. Authors: Girard, F. ; Primout, M. ; Villette, B. ; Stemmler, Ph. ; Jacquet,

  7. Global High-purity Pentoxide Industry 2015 Market Research Report...

    Open Energy Info (EERE)

    on. Then it analyzed the world's main region market conditions, including the product price, profit, capacity, production, capacity utilization, supply, demand and industry...

  8. Self-assembly of tin wires via phase transformation of heteroepitaxial germanium-tin on germanium substrate

    SciTech Connect (OSTI)

    Wang, Wei; Li, Lingzi; Yeo, Yee-Chia; Tok, Eng Soon

    2015-06-14

    This work demonstrates and describes for the first time an unusual strain-relaxation mechanism by the formation and self-assembly of well-ordered tin wires during the thermal annealing of epitaxial Ge{sub 0.83}Sn{sub 0.17}-on-Ge(001) substrate. Fully strained germanium-tin alloys (Ge{sub 0.83}Sn{sub 0.17}) were epitaxially grown on Ge(001) substrate by molecular beam epitaxy. The morphological and compositional evolution of Ge{sub 0.83}Sn{sub 0.17} during thermal annealing is studied by atomic force microscopy, X-ray diffraction, transmission electron microscopy. Under certain annealing conditions, the Ge{sub 0.83}Sn{sub 0.17} layer decomposes into two stable phases, and well-defined Sn wires that are preferentially oriented along two orthogonal ?100? azimuths are formed. The formation of the Sn wires is related to the annealing temperature and the Ge{sub 0.83}Sn{sub 0.17} thickness, and can be explained by the nucleation of a grain with Sn islands on the outer front, followed by grain boundary migration. The Sn wire formation process is found to be thermally activated, and an activation enthalpy (E{sub c}) of 0.41?eV is extracted. This thermally activated phase transformation, i.e., 2D epitaxial layer to 3D wires, occurs via a mechanism akin to cellular precipitation. This synthesis route of Sn wires opens new possibilities for creation of nanoscale patterns at high-throughput without the need for lithography.

  9. Diffusion of n-type dopants in germanium

    SciTech Connect (OSTI)

    Chroneos, A.; Bracht, H.

    2014-03-15

    Germanium is being actively considered by the semiconductor community as a mainstream material for nanoelectronic applications. Germanium has advantageous materials properties; however, its dopant-defect interactions are less understood as compared to the mainstream material, silicon. The understanding of self- and dopant diffusion is essential to form well defined doped regions. Although p-type dopants such as boron exhibit limited diffusion, n-type dopants such as phosphorous, arsenic, and antimony diffuse quickly via vacancy-mediated diffusion mechanisms. In the present review, we mainly focus on the impact of intrinsic defects on the diffusion mechanisms of donor atoms and point defect engineering strategies to restrain donor atom diffusion and to enhance their electrical activation.

  10. GeMini: The Next Generation Mechanically-Cooled Germanium Spectrometer

    SciTech Connect (OSTI)

    Burks, M

    2008-06-13

    The next-generation mechanically-cooled germanium spectrometer has been developed. GeMini (GErmanium MINIature spectrometer) has been designed to bring high-resolution gamma-ray spectroscopy to a range of demanding field environments. Intended applications include short-notice and surprise inspections where positive nuclide identification of radioactive materials is required. GeMini weighs 2.75 kg (6 lbs) total including the detector, cryostat, cryocooler, batteries, electronics and readout. It is very low power allowing it to operate for 10 hours on a single set of rechargeable batteries. This instrument employs technology adapted from the gamma-ray spectrometer currently flying on NASA's Mercury MESSENGER spacecraft. Specifically, infrared shielding techniques allow for a vast reduction of thermal load. This in turn allows for a smaller, lighter-weight design, well-suited for a hand-held instrument. Two working prototypes have been built and tested in the lab. The target energy resolution is 3 keV fwhm or better for 1332 keV gamma-rays. The detectors currently achieve around 4.5 keV resolution, which is slightly higher than our goal due to microphonic noise. Our present work focuses on improving the resolution through mechanical and electronic means of reducing the microphonic noise. This paper will focus on the performance of the instrument and its applicability for inspectors in the field.

  11. Titanium and germanium lined hohlraums and halfraums as multi-keV x-ray radiators

    SciTech Connect (OSTI)

    Girard, F.; Primout, M.; Villette, B.; Stemmler, Ph.; Jacquet, L.; Babonneau, D. [CEA, DAM, DIF, F-91297 Arpajon (France); Fournier, K. B. [Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94550 (United States)

    2009-05-15

    As multi-keV x-ray radiators, hohlraums and halfraums with inner walls coated with metallic materials (called liner) have been tested for the first time with laser as the energy drive. For titanium, conversion efficiencies (CEs) are up to {approx}14% for emission into 4{pi}, integrating between 4.6 and 6.5 keV when a large diameter hohlraum is used. Germanium CE is {approx}0.8% into 4{pi} between 9 and 13 keV. The highest CEs have been obtained with a 1 ns squared pulse and phase plates giving laser absorption near 99%. These high CEs are due to long-lasting, good plasma conditions for multi-keV x-ray production maintained by plasma confinement inside the plastic cylinder and plasma collision leading to a burst of x rays at a time that depends on target size. As photon emitters at 4.7 keV, titanium-lined hohlraums are the most efficient solid targets and data are close to CEs for gas targets, which are considered as the upper limit for x-ray yields since their low density allows good laser absorption and low kinetics losses. As 10.3 keV x-ray emitters, exploded germanium foils give best results one order of magnitude more efficient than thick targets; doped aerogels and lined hohlraums give similar yields, about three times lower than those from exploded foils.

  12. Holey Germanium - New Routes to Ordered Nanoporous Semiconductors

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Holey Germanium - New Routes to Ordered Nanoporous Semiconductors Nanoporous or mesoporous inorganic materials with homogeneous pore sizes have found broad applications in separations, as supports for size selective catalysis, and as low dielectric materials. For all of these applications, it is the pore space that is important, and so the inorganic framework is generally formed from a simple material like silica or another oxide. In an effort to extend the range of potential applications for

  13. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Direct-Write of Silicon and Germanium Nanostructures Print Nanostructured materials (nanowires, nanotubes, nanoclusters, graphene) are attractive possible alternatives to traditionally microfabricated silicon in continuing the miniaturization trend in the electronics industry. To go from nanomaterials to electronics, however, the precise one-by-one assembly of billions of nanoelements into a functioning circuit is required-clearly not a simple task. An interdisciplinary team from the University

  14. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Direct-Write of Silicon and Germanium Nanostructures Print Nanostructured materials (nanowires, nanotubes, nanoclusters, graphene) are attractive possible alternatives to traditionally microfabricated silicon in continuing the miniaturization trend in the electronics industry. To go from nanomaterials to electronics, however, the precise one-by-one assembly of billions of nanoelements into a functioning circuit is required-clearly not a simple task. An interdisciplinary team from the University

  15. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Direct-Write of Silicon and Germanium Nanostructures Print Nanostructured materials (nanowires, nanotubes, nanoclusters, graphene) are attractive possible alternatives to traditionally microfabricated silicon in continuing the miniaturization trend in the electronics industry. To go from nanomaterials to electronics, however, the precise one-by-one assembly of billions of nanoelements into a functioning circuit is required-clearly not a simple task. An interdisciplinary team from the University

  16. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Direct-Write of Silicon and Germanium Nanostructures Print Nanostructured materials (nanowires, nanotubes, nanoclusters, graphene) are attractive possible alternatives to traditionally microfabricated silicon in continuing the miniaturization trend in the electronics industry. To go from nanomaterials to electronics, however, the precise one-by-one assembly of billions of nanoelements into a functioning circuit is required-clearly not a simple task. An interdisciplinary team from the University

  17. The Majorana Demonstrator: First Module of Germanium Detectors Comes Online

    Office of Science (SC) Website

    | U.S. DOE Office of Science (SC) The Majorana Demonstrator: First Module of Germanium Detectors Comes Online Nuclear Physics (NP) NP Home About Research Facilities Science Highlights Benefits of NP Funding Opportunities Nuclear Science Advisory Committee (NSAC) Community Resources Contact Information Nuclear Physics U.S. Department of Energy SC-26/Germantown Building 1000 Independence Ave., SW Washington, DC 20585 P: (301) 903-3613 F: (301) 903-3833 E: Email Us More Information » 09.01.15

  18. Metastable phases in mechanically alloyed aluminum germanium powders

    SciTech Connect (OSTI)

    Yvon, P.J.; Schwarz, R.B.

    1993-03-01

    Aluminum and germanium form a simple eutectic system with no stable intermetallic phase, and limited mutual solubility. We report the formation of a metastable rhombohedral,{gamma}{sub 1} phase by mechanically alloying aluminum and germanium powders. This phase, which appears for compositions between 20 and 50 at. % germanium, has also been observed in rapidly quenched alloys, but there is disagreement as to its composition. By measuring the heat of crystallization as a function of composition, we determined the composition of the {gamma}{sub 1} phase to be Al{sub 70}Ge{sub 30}. We also produced Al{sub 70}Ge{sub 30} by arc melting the pure elements, followed by splat-quenching at a cooling rate in the range of 10{sup 8} K s{sup {minus}1}. This method produced two metastable phases, one of which was found to be the {gamma}{sub 1} phase obtained by mechanical alloying. The other was a monoclinic phase reported earlier in the literature as {gamma}{sub 2}.

  19. Extreme argon purity in a large, non-evacuated cryostat

    SciTech Connect (OSTI)

    Tope, Terry; Adamowski, Mark; Carls, B.; Hahn, A.; Jaskierny, W.; Jostlein, H.; Kendziora, C.; Lockwitz, S.; Pahlka, B.; Plunkett, R.; Pordes, S.; Rebel, B.; Schmitt, R.; Skup, E.; Stancari, M.; Yang, T.

    2014-01-29

    Liquid Argon Time Projection Chambers (LArTPCs) show promise as scalable devices for the large detectors needed for long-baseline neutrino oscillation physics. Over the last several years at Fermilab a staged approach to developing the technology for large detectors has been developed. The TPC detectors require ultra-pure liquid argon with respect to electronegative contaminants such as oxygen and water. The tolerable electronegative contamination level may be as pure as 60 parts per trillion of oxygen. Three liquid argon cryostats operated at Fermilab have achieved the extreme purity required by TPCs. These three cryostats used evacuation to remove atmospheric contaminants as the first purification step prior to filling with liquid argon. Future physics experiments may require very large detectors with tens of kilotonnes of liquid argon mass. The capability to evacuate such large cryostats adds significant cost to the cryostat itself in addition to the cost of a large scale vacuum pumping system. This paper describes a 30 ton liquid argon cryostat at Fermilab which uses purging to remove atmospheric contaminants instead of evacuation as the first purification step. This cryostat has achieved electronegative contamination levels better than 60 parts per trillion of oxygen equivalent. The results of this liquid argon purity demonstration will strongly influence the design of future TPC cryostats.

  20. Biogenic opal germanium/silicon ratios used to monitor upwelling intensity in Newport Lagoon section, Monterey Formation, California

    SciTech Connect (OSTI)

    Murnane, R.J.

    1986-04-01

    Empirical evidence and modeling of geochemical cycles of silicon (Si) and germanium (Ge) suggest that opal Ge/Si ratios record water Ge/Si ratios although some fractionation of germanium from silicon occurs during biogenic opal formation. Modeling results also suggest that opal Ge/Si ratios could record changes in upwelling intensity. In today's oceans, areas of high productivity associated with upwelling show relatively elevated surface-water nutrient concentrations, whereas areas of low productivity with restricted upwelling exhibit low surface-water nutrient concentrations. Fractionation of germanium from silicon during biogenic opal formation would cause the surface ocean's Ge/Si ratio to increase as surface-water nutrient concentrations are lowered. Diatomites from the Newport Lagoon section of the Monterey Formation were analyzed to test the hypothesis that biogenic opal Ge/Si ratios could be used to trace upwelling intensity. Diatom assemblages of the Monterey Formation vary with upwelling intensity over a time scale of millions of years. Samples collected from the middle and late Miocene have high ratios (up to 8 x 10/sup -7/) when diatom assemblages indicate relatively weak upwelling, and low ratios (less than 6 x 10/sup -7/) when diatom assemblages indicate relatively strong upwelling. These ratios agree with modeling predictions. Opal Ge/Si ratios may also record upwelling fluctuations on much shorter times scales. Adjacent, centimeter-scale, lighter and darker layers record past variations in biogenic and terrigenous inputs to ocean-bottom sediments. Opal Ge/Si ratios may indicate whether the darker layers result from a relative decrease in surface-water productivity in response to a reduction in upwelling intensity, or only from a relative increase in terrigenous detrital inputs.

  1. Mechanically Cooled Large-Volume Germanium Detector Systems for Nuclear Explosion Monitoring

    SciTech Connect (OSTI)

    Hull, Ethan L.; Pehl, Richard H.; Lathrop, James R.; Martin, Gregory N.; Mashburn, R. B.; Miley, Harry S.; Aalseth, Craig E.; Hossbach, Todd W.; Bowyer, Ted W.

    2006-09-21

    Compact maintenance free mechanical cooling systems are being developed to operate large volume (~570 cm3, ~3 kg, 140% or larger) germanium detectors for field applications. We are using a new generation of Stirling-cycle mechanical coolers for operating the very largest volume germanium detectors with absolutely no maintenance or liquid nitrogen requirements. The user will be able to leave these systems unplugged on the shelf until needed. The flip of a switch will bring a system to life in ~1 hour for measurements. The maintenance-free operating lifetime of these detector systems will exceed five years. These features are necessary for remote long-duration liquid-nitrogen free deployment of large-volume germanium gamma-ray detector systems for Nuclear Explosion Monitoring (NEM). The Radionuclide Aerosol Sampler/Analyzer (RASA) will greatly benefit from the availability of such detectors by eliminating the need for liquid nitrogen at RASA sites while still allowing the very largest available germanium detectors to be utilized. These mechanically cooled germanium detector systems being developed here will provide the largest, most sensitive detectors possible for use with the RASA. To provide such systems, the appropriate technical fundamentals are being researched. Mechanical cooling of germanium detectors has historically been a difficult endeavor. The success or failure of mechanically cooled germanium detectors stems from three main technical issues: temperature, vacuum, and vibration. These factors affect one another. There is a particularly crucial relationship between vacuum and temperature. These factors will be experimentally studied both separately and together to insure a solid understanding of the physical limitations each factor places on a practical mechanically cooled germanium detector system for field use. Using this knowledge, a series of mechanically cooled germanium detector prototype systems are being designed and fabricated. Our collaborators at Pacific Northwest National Laboratory (PNNL) will evaluate these detector systems on the bench top and eventually in RASA systems to insure reliable and practical operation.

  2. A Multi-Contact, Low Capacitance HPGe Detector for High Rate Gamma Spectroscopy

    SciTech Connect (OSTI)

    Cox, Christopher

    2014-12-04

    The detection, identification and non-destructive assay of special nuclear materials and nuclear fission by-products are critically important activities in support of nuclear non-proliferation programs. Both national and international nuclear safeguard agencies recognize that current accounting methods for spent nuclear fuel are inadequate from a safeguards perspective. Radiation detection and analysis by gamma-ray spectroscopy is a key tool in this field, but no instrument exists that can deliver the required performance (energy resolution and detection sensitivity) in the presence of very high background count rates encountered in the nuclear safeguards arena. The work of this project addresses this critical need by developing a unique gamma-ray detector based on high purity germanium that has the previously unachievable property of operating in the 1 million counts-per-second range while achieving state-of-the-art energy resolution necessary to identify and analyze the isotopes of interest. The technical approach was to design and fabricate a germanium detector with multiple segmented electrodes coupled to multi-channel high rate spectroscopy electronics. Dividing the germanium detector’s signal electrode into smaller sections offers two advantages; firstly, the energy resolution of the detector is potentially improved, and secondly, the detector is able to operate at higher count rates. The design challenges included the following; determining the optimum electrode configuration to meet the stringent energy resolution and count rate requirements; determining the electronic noise (and therefore energy resolution) of the completed system after multiple signals are recombined; designing the germanium crystal housing and vacuum cryostat; and customizing electronics to perform the signal recombination function in real time. In this phase I work, commercial off-the-shelf electrostatic modeling software was used to develop the segmented germanium crystal geometry, which underwent several iterations before an optimal electrode configuration was found. The model was tested and validated against real-world measurements with existing germanium detectors. Extensive modeling of electronic noise was conducted using established formulae, and real-world measurements were performed on candidate front-end electronic components. This initial work proved the feasibility of the design with respect to expected high count rate and energy resolution performance. Phase I also delivered the mechanical design of the detector housing and vacuum cryostat to be built in Phase II. Finally, a Monte Carlo simulation was created to show the response of the complete design to a Cs-137 source. This development presents a significant advance for nuclear safeguards instrumentation with increased speed and accuracy of detection and identification of special nuclear materials. Other significant applications are foreseen for a gamma-ray detector that delivers high energy resolution (1keV FWHM noise) at high count rate (1 Mcps), especially in the areas of physics research and materials analysis.

  3. Method of manufacturing a niobium-aluminum-germanium superconductive material

    DOE Patents [OSTI]

    Wang, John L. (San Francisco, CA); Pickus, Milton R. (Oakland, CA); Douglas, Kent E. (Redondo Beach, CA)

    1980-01-01

    A method for manufacturing flexible Nb.sub.3 (Al,Ge) multifilamentary superconductive material in which a sintered porous niobium compact is infiltrated with an aluminum-germanium alloy and thereafter deformed and heat treated in a series of steps at different successively higher temperatures preferably below 1000.degree. C. to produce filaments composed of Nb.sub.3 (Al,G3) within the compact. By avoiding temperatures in excess of 1000.degree. C. during the heat treatment, cladding material such as copper can be applied to facilitate a deformation step preceding the heat treatment and can remain in place through the heat treatment to also serve as a temperature stabilizer for supeconductive material produced. Further, these lower heat treatment temperatures favor formation of filaments with reduced grain size and, hence with more grain boundaries which in turn increase the current-carrying capacity of the superconductive material.

  4. Corrosion in Supercritical carbon Dioxide: Materials, Environmental Purity, Surface Treatments, and Flow Issues

    SciTech Connect (OSTI)

    Sridharan, Kumar; Anderson, Mark

    2013-12-10

    The supercritical CO{sub 2} Brayton cycle is gaining importance for power conversion in the Generation IV fast reactor system because of its high conversion efficiencies. When used in conjunction with a sodium fast reactor, the supercritical CO{sub 2} cycle offers additional safety advantages by eliminating potential sodium-water interactions that may occur in a steam cycle. In power conversion systems for Generation IV fast reactors, supercritical CO{sub 2} temperatures could be in the range of 30C to 650C, depending on the specific component in the system. Materials corrosion primarily at high temperatures will be an important issue. Therefore, the corrosion performance limits for materials at various temperatures must be established. The proposed research will have four objectives centered on addressing corrosion issues in a high-temperature supercritical CO{sub 2} environment: Task 1: Evaluation of corrosion performance of candidate alloys in high-purity supercritical CO{sub 2}: The following alloys will be tested: Ferritic-martensitic Steels NF616 and HCM12A, austenitic alloys Incoloy 800H and 347 stainless steel, and two advanced concept alloys, AFA (alumina forming austenitic) steel and MA754. Supercritical CO{sub 2} testing will be performed at 450C, 550C, and 650C at a pressure of 20 MPa, in a test facility that is already in place at the proposing university. High purity CO{sub 2} (99.9998%) will be used for these tests. Task 2: Investigation of the effects of CO, H{sub 2}O, and O{sub 2} impurities in supercritical CO{sub 2} on corrosion: Impurities that will inevitably present in the CO{sub 2} will play a critical role in dictating the extent of corrosion and corrosion mechanisms. These effects must be understood to identify the level of CO{sub 2} chemistry control needed to maintain sufficient levels of purity to manage corrosion. The individual effects of important impurities CO, H{sub 2}O, and O{sub 2} will be investigated by adding them separately to high purity CO{sub 2}. Task 3: Evaluation of surface treatments on the corrosion performance of alloys in supercritical CO{sub 2}: Surface treatments can be very beneficial in improving corrosion resistance. Shot peening and yttrium and aluminum surface treatments will be investigated. Shot peening refines the surface grain sizes and promotes protective Cr-oxide layer formation. Both yttrium and aluminum form highly stable oxide layers (Y{sub 2}O{sub 3} and Al{sub 2}O{sub 3}), which can get incorporated in the growing Fe-oxide layer to form an impervious complex oxide to enhance corrosion resistance. Task 4: Study of flow-assisted corrosion of select alloys in supercritical CO{sub 2} under a selected set of test conditions: To study the effects of flow-assisted corrosion, tests will be conducted in a supercritical CO{sub 2} flow loop. An existing facility used for supercritical water flow studies at the proposing university will be modified for use in this task. The system is capable of flow velocities up to 10 m/s and can operate at temperatures and pressures of up to 650C and 20 MPa, respectively. All above tasks will be performed in conjunction with detailed materials characterization and analysis using scanning electron microscopy/energy dispersive spectroscopy (SEM-EDS), x-ray diffraction (XRD), Auger electron spectroscopy (AES) techniques, and weight change measurements. Inlet and outlet gas compositions will be monitored using gas chromatography-mass spectrometry (GCMS).

  5. Mechanically Cooled Large-Volume Germanium Detector Systems for Nuclear Explosion Monitoring DOENA27323-1

    SciTech Connect (OSTI)

    Hull, E.L.

    2006-07-28

    Compact maintenance free mechanical cooling systems are being developed to operate large volume germanium detectors for field applications. To accomplish this we are utilizing a newly available generation of Stirling-cycle mechanical coolers to operate the very largest volume germanium detectors with no maintenance. The user will be able to leave these systems unplugged on the shelf until needed. The flip of a switch will bring a system to life in ~ 1 hour for measurements. The maintenance-free operating lifetime of these detector systems will exceed 5 years. These features are necessary for remote long-duration liquid-nitrogen free deployment of large-volume germanium gamma-ray detector systems for Nuclear Explosion Monitoring. The Radionuclide Aerosol Sampler/Analyzer (RASA) will greatly benefit from the availability of such detectors by eliminating the need for liquid nitrogen at RASA sites while still allowing the very largest available germanium detectors to be reliably utilized.

  6. Electronic and magnetic properties of Fe and Mn doped two dimensional hexagonal germanium sheets

    SciTech Connect (OSTI)

    Soni, Himadri R. Jha, Prafulla K.

    2014-04-24

    Using first principles density functional theory calculations, the present paper reports systematic total energy calculations of the electronic properties such as density of states and magnetic moment of pristine and iron and manganese doped two dimensional hexagonal germanium sheets.

  7. Germanium films by polymer-assisted deposition (Patent) | SciTech...

    Office of Scientific and Technical Information (OSTI)

    deposition Citation Details In-Document Search Title: Germanium films by polymer-assisted deposition You are accessing a document from the Department of Energy's (DOE) SciTech...

  8. Withdrawal from Production and Distribution of the Radioisotope Germanium-68 Used for Calibration Sources

    Broader source: Energy.gov [DOE]

    Questions Regarding Federal Register “Notice of Intent to Withdraw from Production and Distribution of the Radioisotope Germanium-68 Used for Calibration Sources” (79 FR 19610, April 9, 2014)

  9. Imaging the oblique propagation of electrons in germanium crystals at low

    Office of Scientific and Technical Information (OSTI)

    temperature and low electric field (Journal Article) | DOE PAGES Imaging the oblique propagation of electrons in germanium crystals at low temperature and low electric field This content will become publicly available on January 11, 2017 « Prev Next » Title: Imaging the oblique propagation of electrons in germanium crystals at low temperature and low electric field Authors: Moffatt, R. A. [1] ; Cabrera, B. [1] ; Corcoran, B. M. [1] ; Kreikebaum, J. M. [1] ; Redl, P. [1] ; Shank, B. [1] ;

  10. Improving the Cycling Life of Aluminum and Germanium Thin Films for use as

    Office of Scientific and Technical Information (OSTI)

    Anodic Materials in Li-Ion Batteries. (Technical Report) | SciTech Connect Technical Report: Improving the Cycling Life of Aluminum and Germanium Thin Films for use as Anodic Materials in Li-Ion Batteries. Citation Details In-Document Search Title: Improving the Cycling Life of Aluminum and Germanium Thin Films for use as Anodic Materials in Li-Ion Batteries. Abstract not provided. Authors: Hudak, Nicholas ; Huber, Dale L. ; Gulley, Gerald Publication Date: 2014-09-01 OSTI Identifier:

  11. Influence of Electronic Type Purity on the Lithiation of Single-Walled Carbon Nanotubes

    SciTech Connect (OSTI)

    Jaber-Ansari, Laila; Iddir, Hakim; Curtiss, Larry A.; Hersam, Mark C.

    2014-03-25

    Single-walled carbon nanotubes (SWCNTs) have emerged as one of the leading additives for high-capacity nanocomposite lithium ion battery electrodes due to their ability to improve electrode conductivity, current collection efficiency, and charge/discharge rate for high power applications. However, since as-grown SWCNTs possess a distribution of physical and electronic structures, it is of high interest to determine which subpopulations of SWCNTs possess the highest lithiation capacity and to develop processing methods that can enhance the lithiation capacity of underperforming SWCNT species. Toward this end, SWCNT electronic type purity is controlled via density gradient ultracentrifugation, enabling a systematic study of the lithiation of SWCNTs as a function of metal versus semiconducting content. Experimentally, vacuum-filtered freestanding films of metallic SWCNTs are found to accommodate lithium with an order of magnitude higher capacity than their semiconducting counterparts, which is consistent with ab initio molecular dynamics and density functional theory calculations in the limit of isolated SWCNTs. In contrast, SWCNT film densification leads to the enhancement of the lithiation capacity of semiconducting SWCNTs to levels comparable to metallic SWCNTs, which is corroborated by theoretical calculations that show increased lithiation of semiconducting SWCNTs in the limit of small SWCNT*SWCNT spacing. Overall, these results will inform ongoing efforts to utilize SWCNTs as conductive additives in nanocomposite lithium ion battery electrodes.

  12. The MAJORANA DEMONSTRATOR: A Search for Neutrinoless Double-beta Decay of Germanium-76

    SciTech Connect (OSTI)

    Schubert, Alexis G.; Aguayo, Estanislao; Avignone, F. T.; Zhang, C.; Back, Henning O.; Barabash, Alexander S.; Bergevin, M.; Bertrand, F.; Boswell, M.; Brudanin, V.; Busch, Matthew; Chan, Yuen-Dat; Christofferson, Cabot-Ann; Collar, J. I.; Combs, Dustin C.; Cooper, R. J.; Detwiler, Jason A.; Leon, Jonathan D.; Doe, Peter J.; Efremenko, Yuri; Egorov, Viatcheslav; Ejiri, H.; Elliott, S. R.; Esterline, James H.; Fast, James E.; Fields, N.; Finnerty, P.; Fraenkle, Florian; Gehman, Victor M.; Giovanetti, G. K.; Green, M.; Guiseppe, Vincente; Gusey, K.; Hallin, A. L.; Hazama, R.; Henning, Reyco; Hime, Andrew; Hoppe, Eric W.; Horton, Mark; Howard, Stanley; Howe, Mark; Johnson, R. A.; Keeter, K.; Keillor, Martin E.; Keller, C.; Kephart, Jeremy D.; Kidd, M. F.; Knecht, A.; Kochetov, Oleg; Konovalov, S.; Kouzes, Richard T.; LaFerriere, Brian D.; LaRoque, B. H.; Leviner, L.; Loach, J. C.; MacMullin, S.; Marino, Michael G.; Martin, R. D.; Mei, Dong-Ming; Merriman, Jason H.; Miller, M. L.; Mizouni, Leila; Nomachi, Masaharu; Orrell, John L.; Overman, Nicole R.; Phillips, D.; Poon, Alan; Perumpilly, Gopakumar; Prior, Gersende; Radford, D. C.; Rielage, Keith; Robertson, R. G. H.; Ronquest, M. C.; Shima, T.; Shirchenko, M.; Snavely, Kyle J.; Sobolev, V.; Steele, David; Strain, J.; Thomas, K.; Timkin, V.; Tornow, Werner; Vanyushin, I.; Varner, R. L.; Vetter, Kai; Vorren, Kris R.; Wilkerson, J. F.; Wolfe, B. A.; Yakushev, E.; Young, A.; Yu, Chang-Hong; Yumatov, Vladimir

    2012-09-28

    The observation of neutrinoless double-beta decay would determine whether the neutrino is a Majorana particle and provide information on the absolute scale of neutrino mass. The MAJORANA Collaboration is constructing the DEMONSTRATOR, an array of germanium detectors, to search for neutrinoless double-beta decay of 76Ge. The DEMONSTRATOR will contain 40 kg of germanium; up to 30 kg will be enriched to 86% in 76Ge. The DEMONSTRATOR will be deployed deep underground in an ultra-low-background shielded environment. Operation of the DEMONSTRATOR aims to determine whether a future tonne-scale germanium experiment can achieve a background goal of one count per tonne-year in a 4-keV region of interest around the 76Ge neutrinoless double-beta decay Q-value of 2039 keV.

  13. High density-high purity graphite prepared by hot isostatic pressing in refractory metal containers

    DOE Patents [OSTI]

    Hoenig, C.L.

    1994-08-09

    Porous graphite in solid form is hot isostatically pressed in a refractory metal container to produce a solid graphite monolith with a bulk density greater than or equal to 2.10 g/cc. The refractory metal container is formed of tantalum, niobium, tungsten, molybdenum or alloys thereof in the form of a canister or alternatively plasma sprayed, chemically vapor deposited, or coated by some other suitable means onto graphite. Hot isostatic pressing at 2,200 C and 30 KSI (206.8 MPa) argon pressure for two hours produces a bulk density of 2.10 g/cc. Complex shapes can be made. 1 fig.

  14. High density-high purity graphite prepared by hot isostatic pressing in refractory metal containers

    DOE Patents [OSTI]

    Hoenig, Clarence L. (Livermore, CA)

    1994-01-01

    Porous graphite in solid form is hot isostatically pressed in a refractory metal container to produce a solid graphite monolith with a bulk density greater than or equal to 2.10 g/cc. The refractory metal container is formed of tantalum, niobium, tungsten, molybdenum or alloys thereof in the form of a canister or alternatively plasma sprayed, chemically vapor deposited, or coated by some other suitable means onto graphite. Hot isostatic pressing at 2200.degree. C. and 30 KSI (206.8 MPa) argon pressure for two hours produces a bulk density of 2.10 g/cc. Complex shapes can be made.

  15. GERDA, a GERmanium Detector Array for the search for neutrinoless {beta}{beta} decay in 76Ge

    SciTech Connect (OSTI)

    Pandola, L.; Tomei, C. [INFN, Laboratori Nazionali del Gran Sasso, S.S. 17 bis km 18.910, 67010 Assergi (AQ) (Italy)

    2006-07-11

    The GERDA project, searching for neutrinoless double beta-decay of 76Ge with enriched germanium detectors submerged in a cryogenic bath, has been approved for installation at the Gran Sasso National Laboratory (LNGS), Italy. The GERDA technique is aiming at a dramatic reduction of the background due to radioactive contaminations of the materials surrounding the detectors. This will lead to a sensitivity of about 1026 years on the half-life of neutrinoless double beta decay. Already in the first phase of the experiment, GERDA will be able to investigate with high statistical significance the claimed evidence for neutrinoless double beta decay of 76Ge based on the data of the Heidelberg-Moscow experiment.

  16. Optimization of the Transport Shield for Neutrinoless Double Beta-decay Enriched Germanium

    SciTech Connect (OSTI)

    Aguayo Navarrete, Estanislao; Kouzes, Richard T.; Orrell, John L.; Reid, Douglas J.; Fast, James E.

    2012-04-15

    This document presents results of an investigation of the material and geometry choice for the transport shield of germanium, the active detector material used in 76Ge neutrinoless double beta decay searches. The objective of this work is to select the optimal material and geometry to minimize cosmogenic production of radioactive isotopes in the germanium material. The design of such a shield is based on the calculation of the cosmogenic production rate of isotopes that are known to cause interfering backgrounds in 76Ge neutrinoless double beta decay searches.

  17. Doping of germanium and silicon crystals with non-hydrogenic acceptors for far infrared lasers

    DOE Patents [OSTI]

    Haller, Eugene E. (Berkeley, CA); Brundermann, Erik (Berlin, DE)

    2000-01-01

    A method for doping semiconductors used for far infrared lasers with non-hydrogenic acceptors having binding energies larger than the energy of the laser photons. Doping of germanium or silicon crystals with beryllium, zinc or copper. A far infrared laser comprising germanium crystals doped with double or triple acceptor dopants permitting the doped laser to be tuned continuously from 1 to 4 terahertz and to operate in continuous mode. A method for operating semiconductor hole population inversion lasers with a closed cycle refrigerator.

  18. Titanium and germanium lined hohlraums and halfraums as multi-keV X-ray

    Office of Scientific and Technical Information (OSTI)

    radiators (Journal Article) | SciTech Connect Titanium and germanium lined hohlraums and halfraums as multi-keV X-ray radiators Citation Details In-Document Search Title: Titanium and germanium lined hohlraums and halfraums as multi-keV X-ray radiators Authors: Girard, F ; Primout, M ; Fournier, K B ; Villette, B ; Stemmler, P ; Jacquet, L ; Babonneau, D Publication Date: 2009-05-06 OSTI Identifier: 956852 Report Number(s): LLNL-JRNL-413391 DOE Contract Number: W-7405-ENG-48 Resource Type:

  19. Low energy consumption method for separating gaseous mixtures and in particular for medium purity oxygen production

    DOE Patents [OSTI]

    Jujasz, Albert J. (North Olmsted, OH); Burkhart, James A. (Olmsted Falls, OH); Greenberg, Ralph (New York, NY)

    1988-01-01

    A method for the separation of gaseous mixtures such as air and for producing medium purity oxygen, comprising compressing the gaseous mixture in a first compressor to about 3.9-4.1 atmospheres pressure, passing said compressed gaseous mixture in heat exchange relationship with sub-ambient temperature gaseous nitrogen, dividing the cooled, pressurized gaseous mixture into first and second streams, introducing the first stream into the high pressure chamber of a double rectification column, separating the gaseous mixture in the rectification column into a liquid oxygen-enriched stream and a gaseous nitrogen stream and supplying the gaseous nitrogen stream for cooling the compressed gaseous mixture, removing the liquid oxygen-enriched stream from the low pressure chamber of the rectification column and pumping the liquid, oxygen-enriched steam to a predetermined pressure, cooling the second stream, condensing the cooled second stream and evaporating the oxygen-enriched stream in an evaporator-condenser, delivering the condensed second stream to the high pressure chamber of the rectification column, and heating the oxygen-enriched stream and blending the oxygen-enriched stream with a compressed blend-air stream to the desired oxygen concentration.

  20. Characteristics of Signals Originating Near the Lithium-Diffused N+ Contact

    Office of Scientific and Technical Information (OSTI)

    of High Purity Germanium P-Type Point Contact Detectors (Journal Article) | SciTech Connect Characteristics of Signals Originating Near the Lithium-Diffused N+ Contact of High Purity Germanium P-Type Point Contact Detectors Citation Details In-Document Search Title: Characteristics of Signals Originating Near the Lithium-Diffused N+ Contact of High Purity Germanium P-Type Point Contact Detectors A study of signals originating near the lithium-diffused n+ contact of p-type point contact (PPC)

  1. The Fuel Accident Condition Simulator (FACS) furnace system for high temperature performance testing of VHTR fuel

    SciTech Connect (OSTI)

    Paul A. Demkowicz; David V. Laug; Dawn M. Scates; Edward L. Reber; Lyle G. Roybal; John B. Walter; Jason M. Harp; Robert N. Morris

    2012-10-01

    The AGR-1 irradiation of TRISO-coated particle fuel specimens was recently completed and represents the most successful such irradiation in US history, reaching peak burnups of greater than 19% FIMA with zero failures out of 300,000 particles. An extensive post-irradiation examination (PIE) campaign will be conducted on the AGR-1 fuel in order to characterize the irradiated fuel properties, assess the in-pile fuel performance in terms of coating integrity and fission metals release, and determine the fission product retention behavior during high temperature safety testing. A new furnace system has been designed, built, and tested to perform high temperature accident tests. The Fuel Accident Condition Simulator furnace system is designed to heat fuel specimens at temperatures up to 2000 degrees C in helium while monitoring the release of volatile fission metals (e.g. Cs, Ag, Sr, and Eu), iodine, and fission gases (Kr, Xe). Fission gases released from the fuel to the sweep gas are monitored in real time using dual cryogenic traps fitted with high purity germanium detectors. Condensable fission products are collected on a plate attached to a water-cooled cold finger that can be exchanged periodically without interrupting the test. Analysis of fission products on the condensation plates involves dry gamma counting followed by chemical analysis of selected isotopes. This paper will describe design and operational details of the Fuel Accident Condition Simulator furnace system and the associated fission gas monitoring system, as well as preliminary system calibration results.

  2. Method and apparatus for measuring purity of noble gases

    DOE Patents [OSTI]

    Austin, Robert (Largo, FL)

    2008-04-01

    A device for detecting impurities in a noble gas includes a detection chamber and a source of pulsed ultraviolet light. The pulse of the ultraviolet light is transferred into the detection chamber and onto a photocathode, thereby emitting a cloud of free electrons into the noble gas within the detection chamber. The cloud of electrons is attracted to the opposite end of the detection chamber by a high positive voltage potential at that end and focused onto a sensing anode. If there are impurities in the noble gas, some or all of the electrons within the cloud will bond with the impurity molecules and not reach the sensing anode. Therefore, measuring a lower signal at the sensing anode indicates a higher level of impurities while sensing a higher signal indicates fewer impurities. Impurities in the range of one part per billion can be measured by this device.

  3. Search for: All records | SciTech Connect

    Office of Scientific and Technical Information (OSTI)

    (1) germanium 76 (1) grand unified theory (1) high-purity ge detectors (1) ... in the 4 keV region of interest (ROI) around the 2039 keV Q-value of the decay. ...

  4. Recommendations for a Static Cosmic Ray Shield for Enriched Germanium Detectors

    SciTech Connect (OSTI)

    Aguayo Navarrete, Estanislao; Orrell, John L.; Ankney, Austin S.; Berguson, Timothy J.

    2011-09-21

    This document provides a detailed study of cost and materials that could be used to shield the detector material of the international Tonne-scale germanium neutrinoless double-beta decay experiment from hadronic particles from cosmic ray showers at the Earth's surface. This work was motivated by the need for a shield that minimizes activation of the enriched germanium during storage; in particular, when the detector material is being worked on at the detector manufacturer's facility. This work considers two options for shielding the detector material from cosmic ray particles. One option is to use a pre-existing structure already located near the detector manufacturer, such as Canberra Industries in Meriden, Connecticut. The other option is to build a shield onsite at a detector manufacturer's site. This paper presents a cost and efficiency analysis of such construction.

  5. Density functional calculation of the structural and electronic properties of germanium quantum dots

    SciTech Connect (OSTI)

    Anas, M. M.; Gopir, G.

    2015-04-24

    We apply first principles density functional computational methods to study the structures, densities of states (DOS), and higher occupied molecular orbital (HOMO) lowest unoccupied molecular orbital (LUMO) gaps of selected free-standing Ge semiconductor quantum dots up to 1.8nm. Our calculations are performed using numerical atomic orbital approach where linear combination of atomic orbital was applied. The surfaces of the quantum dots was passivized by hydrogen atoms. We find that surface passivation does affect the electronic properties associated with the changes of surface state, electron localization, and the energy gaps of germanium nanocrystals as well as the confinement of electrons inside the quantum dots (QDs). Our study shows that the energy gaps of germanium quantum dots decreases with the increasing dot diameter. The size-dependent variations of the computed HOMO-LUMO gaps in our quantum dots model were found to be consistent with the effects of quantum confinement reported in others theoretical and experimental calculation.

  6. Nanorods of Silicon and Germanium with Well-Defined Shapes and Sizes

    SciTech Connect (OSTI)

    Slavi C. Sevov

    2012-05-03

    We have made number of important discoveries along the major goals of the project, namely i) electrodeposition of germanium thin films from clusters, ii) synthesis of cluster-based surfactants with long hydrocarbon chains and micelles made of them, iii) grafting of Ge{sub 9}-clusters onto self assembled films of siloxanes attached to glass substrates, iv) doping of Ge{sub 9}-clusters, and v) expanding the clusters to ten-atom cages of Ge{sub 10}{sup 2-}.

  7. Magnetic Microcalorimeter Gamma Detectors for High-Precision Non-Destructive Analysis, FY14 Extended Annual Report

    SciTech Connect (OSTI)

    Friedrich, S.

    2015-02-06

    Cryogenic gamma (?) detectors with operating temperatures of ~0.1 K or below offer 10 better energy resolution than conventional high-purity germanium detectors that are currently used for non-destructive analysis (NDA) of nuclear materials. This can greatly increase the accuracy of NDA, especially at low-energies where gamma rays often have similar energies and cannot be resolved by Ge detectors. We are developing cryogenic ?detectors based on metallic magnetic calorimeters (MMCs), which have the potential of higher resolution, faster count rates and better linearity than other cryogenic detector technologies. High linearity is essential to add spectra from different pixels in detector arrays that are needed for high sensitivity. Here we discuss the fabrication of a new generation of MMC ?detectors in FY2014, and the resulting improvements in energy resolution and linearity of the new design. As an example of the type of NDA that cryogenic detectors enable, we demonstrate the direct detection of Pu-242 emissions with our MMC ?detectors in the presence of Pu-240, and show that a quantitative NDA analysis agrees with the mass spectrometry

  8. Asymptotic geometric phase and purity for phase qubit dispersively coupled to lossy LC circuit

    SciTech Connect (OSTI)

    Mohamed, A.-B.A.; Obada, A.-S.F.

    2011-09-15

    Analytical descriptions of the geometric phases (GPs) for the total system and subsystems are studied for a current biased Josephson phase qubit strongly coupled to a lossy LC circuit in the dispersive limit. It is found that, the GP and purity depend on the damping parameter which leads to the phenomenon of GP death. Coherence parameter delays the phenomenon of a regular sequence of deaths and births of the GP. The asymptotic behavior of the GP and the purity for the qubit-LC resonator state closely follow that for the qubit state, but however, for the LC circuit these asymptotic values are equal to zero. - Highlights: > The model of a current biased Josephson phase qubit, strongly coupled to loss LC circuit, is considered. > Analytical descriptions of the geometric phase (GP) of this model, in the dispersive limit, are studied. > The GP and purity depend on the dissipation which leads to the GP death phenomenon. > Coherence parameter delays the phenomenon of a regular sequence of deaths and births of the GP.

  9. Summary Report of Summer Work: High Purity Single Crystal Growth & Microstructure of Ferritic-Martensitic Steels

    SciTech Connect (OSTI)

    Pestovich, Kimberly Shay

    2015-08-18

    Harnessing the power of the nuclear sciences for national security and to benefit others is one of Los Alamos National Laboratory’s missions. MST-8 focuses on manipulating and studying how the structure, processing, properties, and performance of materials interact at the atomic level under nuclear conditions. Within this group, single crystal scintillators contribute to the safety and reliability of weapons, provide global security safeguards, and build on scientific principles that carry over to medical fields for cancer detection. Improved cladding materials made of ferritic-martensitic alloys support the mission of DOE-NE’s Fuel Cycle Research and Development program to close the nuclear fuel cycle, aiming to solve nuclear waste management challenges and thereby increase the performance and safety of current and future reactors.

  10. Design of an Online Fission Gas Monitoring System for Post-irradiation Examination Heating Tests of Coated Fuel Particles for High-Temperature Gas-Cooled Reactors

    SciTech Connect (OSTI)

    Dawn Scates

    2010-10-01

    A new Fission Gas Monitoring System (FGMS) has been designed at the Idaho National Laboratory (INL) for use of monitoring online fission gas-released during fuel heating tests. The FGMS will be used with the Fuel Accident Condition Simulator (FACS) at the Hot Fuels Examination Facility (HFEF) located at the Materials and Fuels Complex (MFC) within the INL campus. Preselected Advanced Gas Reactor (AGR) TRISO (Tri-isotropic) fuel compacts will undergo testing to assess the fission product retention characteristics under high temperature accident conditions. The FACS furnace will heat the fuel to temperatures up to 2,000C in a helium atmosphere. Released fission products such as Kr and Xe isotopes will be transported downstream to the FGMS where they will accumulate in cryogenically cooledcollection traps and monitored with High Purity Germanium (HPGe) detectors during the heating process. Special INL developed software will be used to monitor the accumulated fission products and will report data in near real-time. These data will then be reported in a form that can be readily available to the INL reporting database. This paper describes the details of the FGMS design, the control and acqusition software, system calibration, and the expected performance of the FGMS. Preliminary online data may be available for presentation at the High Temperature Reactor (HTR) conference.

  11. Metastable phases in the aluminum-germanium alloy system: Synthesis by mechanical alloying and pressure induced transformations

    SciTech Connect (OSTI)

    Yvon, P.

    1994-01-01

    Al and Ge form a simple equilibrium eutectic with limited mutual solubility and no intermetallic intermediate phases. We used a regular solution approach to model effects of pressure on Al-Ge. Effects of pressure are to extend solubility of Ge in Al, to displace the eutectic composition towards the Ge rich side, and to slightly decrease the eutectic temperature. We designed thermobaric treatments to induce crystal-to-glass transformations in fine grain mixtures of Al and Ge. We used Merrill-Bassett diamond anvil cells to perform experiments at high pressures. We built an x-ray apparatus to determine the structure of alloys at pressure and from cryogenic temperatures to 400C. Two-phase Al-Ge samples with fine microstructures were prepared by splat-quenching and mechanical alloying. We observed a crystal-to-glass transformation at about 80 kbar. The amorphous phase formed was metastable at ambient temperature after pressure release. This was confirmed by TEM. The amorphous phase obtained by pressurization was found to have a liquid-like structure and was metallic. In the TEM samples we also observed the presence of a second amorphous phase formed upon release of the pressure. This second phase had a tetrahedrally-bonded continuous random network structure, similar to that of semi-conducting amorphous germanium.

  12. The MAJORANA DEMONSTRATOR: An R and D project towards a tonne-scale germanium neutrinoless double-beta decay search

    SciTech Connect (OSTI)

    Aalseth, C. E.; Ely, J.; Fast, J. E.; Fuller, E.; Hoppe, E. W.; Keillor, M.; Kouzes, R. T.; Miley, H. S.; Orrell, J. L.; Thompson, R.; Warner, R. [Pacific Northwest National Laboratory, Richland, WA (United States); Amman, M.; Bergevin, M.; Chan, Y.-D.; Detwiler, J. A.; Fujikawa, B.; Loach, J. C.; Luke, P. N.; Poon, A. W. P; Prior, G. [Lawrence Berkeley National Laboratory, Berkeley, CA (United States)] (and others)

    2009-12-17

    The MAJORANA collaboration is pursuing the development of the so-called MAJORANA DEMONSTRATOR. The DEMONSTRATOR is intended to perform research and development towards a tonne-scale germanium-based experiment to search for the neutrinoless double-beta decay of {sup 76}Ge. The DEMONSTRATOR can also perform a competitive direct dark matter search for light WIMPs in the 1-10 GeV/c{sup 2} mass range. It will consist of approximately 60 kg of germanium detectors in an ultra-low background shield located deep underground at the Sanford Underground Laboratory in Lead, SD. The DEMONSTRATOR will also perform background and technology studies, and half of the detector mass will be enriched germanium. This talk will review the motivation, design, technology and status of the Demonstrator.

  13. The MAJORANA DEMONSTRATOR: An R&D project towards a tonne-scale germanium neutrinoless double-beta decay search

    SciTech Connect (OSTI)

    Aalseth, Craig E.; Amman, M.; Amsbaugh, John F.; Avignone, F. T.; Back, Henning O.; Barabash, A.; Barbeau, Phil; Beene, Jim; Bergevin, M.; Bertrand, F.; Boswell, M.; Brudanin, V.; Bugg, William; Burritt, Tom H.; Chan, Yuen-Dat; Collar, J. I.; Cooper, R. J.; Creswick, R.; Detwiler, Jason A.; Doe, P. J.; Efremenko, Yuri; Egorov, Viatcheslav; Ejiri, H.; Elliott, Steven R.; Ely, James H.; Esterline, James H.; Farach, H. A.; Fast, James E.; Fields, N.; Finnerty, P.; Fujikawa, Brian; Fuller, Erin S.; Gehman, Victor; Giovanetti, G. K.; Guiseppe, Vincente; Gusey, K.; Hallin, A. L.; Hazama, R.; Henning, Reyco; Hime, Andrew; Hoppe, Eric W.; Hossbach, Todd W.; Howe, M. A.; Johnson, R. A.; Keeter, K.; Keillor, Martin E.; Keller, C.; Kephart, Jeremy D.; Kidd, Mary; Kochetov, Oleg; Konovalov, S.; Kouzes, Richard T.; Lesko, Kevin; Leviner, L.; Loach, J. C.; Luke, P.; MacMullin, S.; Marino, Michael G.; Mei, Dong-Ming; Miley, Harry S.; Miller, M.; Mizouni, Leila K.; Montoya, A.; Myers, A. W.; Nomachi, Masaharu; Odom, Brian; Orrell, John L.; Phillips, D.; Poon, Alan; Prior, Gersende; Qian, J.; Radford, D. C.; Rielage, Keith; Robertson, R. G. H.; Rodriguez, Larry; Rykaczewski, Krzysztof P.; Schubert, Alexis G.; Shima, T.; Shirchenko, M.; Strain, J.; Thomas, K.; Thompson, Robert C.; Timkin, V.; Tornow, W.; Van Wechel, T. D.; Vanyushin, I.; Vetter, Kai; Warner, Ray A.; Wilkerson, J.; Wouters, Jan; Yakushev, E.; Young, A.; Yu, Chang-Hong; Yumatov, Vladimir; Zhang, C. L.; Zimmerman, S.

    2009-12-17

    The MAJORANA collaboration is pursuing the development of the so-called MAJORANA DEMONSTRATOR. The DEMONSTRATOR is intended to perform research and development towards a tonne-scale germanium-based experiment to search for the neutrinoless double-beta decay of 76Ge. The DEMONSTRATOR can also perform a competitive direct dark matter search for light WIMPs in the 1?10GeV/c2 mass range. It will consist of approximately 60 kg. of germanium detectors in an ultra-low background shield located deep underground at the Sanford Underground Laboratory in Lead, SD. The DEMONSTRATOR will also perform background and technology studies, and half of the detector mass will be enriched germanium. This talk will review the motivation, design, technology and status of the Demonstrator.

  14. Next-Generation Germanium Spectrometer Background Reduction Techniques at 2 MeV

    SciTech Connect (OSTI)

    Brodzinski, Ronald L.

    2005-04-01

    The Majorana project, a next-generation 76Ge neutrinoless double-beta decay experiment being undertaken by a large international collaboration, has the goal of measuring the neutrinoless double-beta decay rate by observing monochromatic events at 2039 keV in 500 kg of isotopically enriched 76Ge gamma-ray spectrometers. In order to achieve the desired sensitivity limit, the background in the 2037-2041 keV region must be reduced to <1 event per year in the entire germanium array. The effects of various background reduction techniques, and the combination thereof, to produce a huge 76Ge spectrometer array with virtually zero background are discussed.

  15. In operandi observation of dynamic annealing: A case study of boron in germanium nanowire devices

    SciTech Connect (OSTI)

    Kole?nik-Gray, Maria M.; Krsti?, Vojislav; Sorger, Christian; Weber, Heiko B.; Biswas, Subhajit; Holmes, Justin D.

    2015-06-08

    We report on the implantation of boron in individual, electrically contacted germanium nanowires with varying diameter and present a technique that monitors the electrical properties of a single device during implantation of ions. This method gives improved access to study the dynamic annealing ability of the nanowire at room temperature promoted by its quasi-one-dimensional confinement. Based on electrical data, we find that the dopant activation efficiency is nontrivially diameter dependent. As the diameter decreases, a transition from a pronounced dynamic-annealing to a radiation-damage dominated regime is observed.

  16. Simulation of the deflection of 200- and 450-GeV protons by a bent germanium crystal

    SciTech Connect (OSTI)

    Koshcheev, V. P. Kholodov, A. K.; Morgun, D. A.

    2009-04-15

    It is shown that the result obtained by numerically solving the kinetic Fokker-Planck equation in the transverse-energy space on the basis of computer simulations of channeled-particle trajectories describes well the results of an experiment that studied the deflection of 200- and 450-GeV protons by a bent germanium crystal.

  17. Method using laser irradiation for the production of atomically clean crystalline silicon and germanium surfaces

    DOE Patents [OSTI]

    Ownby, Gary W. (Knoxville, TN); White, Clark W. (Oak Ridge, TN); Zehner, David M. (Lenoir City, TN)

    1981-01-01

    This invention relates to a new method for removing surface impurities from crystalline silicon or germanium articles, such as off-the-shelf p- or n-type wafers to be doped for use as junction devices. The principal contaminants on such wafers are oxygen and carbon. The new method comprises laser-irradiating the contaminated surface in a non-reactive atmosphere, using one or more of Q-switched laser pulses whose parameters are selected to effect melting of the surface without substantial vaporization thereof. In a typical application, a plurality of pulses is used to convert a surface region of an off-the-shelf silicon wafer to an automatically clean region. This can be accomplished in a system at a pressure below 10.sup.-8 Torr, using Q-switched ruby-laser pulses having an energy density in the range of from about 60 to 190 MW/cm.sup.2.

  18. A Segmented, Enriched N-type Germanium Detector for Neutrinoless Double Beta-Decay Experiments

    SciTech Connect (OSTI)

    Leviner, L.; Aalseth, Craig E.; Ahmed, M. W.; Avignone, F. T.; Back, Henning O.; Barabash, Alexander S.; Boswell, M.; De Braeckeleer, L.; Brudanin, V.; Chan, Yuen-Dat; Egorov, Viatcheslav; Elliott, Steven R.; Gehman, Victor M.; Hossbach, Todd W.; Kephart, Jeremy; Kidd, M. F.; Konovalov, S.; Lesko, Kevin; Li, Jingyi; Mei, Dongming; Mikhailov, S.; Miley, Harry S.; Radford, D. C.; Reeves, James H.; Sandukovsky, Viatcheslav; Umatov, Valdimir; Underwood, T. A.; Tornow, W.; Wu, Y. K.; Young, A.

    2014-01-21

    We present data characterizing the performance of the _rst segmented, N- type Ge detector, isotopically enriched to 85% 76Ge. This detector, based on the Ortec PT6x2 design and referred to as SEGA (Segmented, Enriched Germanium Assembly), was developed as a possible prototype for neutrinoless double beta-decay measurements by the Majorana collaboration. We present some of the general characteristics (including bias potential, efficiency, leakage current, and integral cross-talk) for this detector in its temporary cryostat. We also present an analysis of the resolution of the detector, and demonstrate that for all but two segments there is at least one channel that reaches the Majorana resolution goal below 4 keV FWHM at 2039 keV, and all channels are below 4.5 keV FWHM.

  19. Electronic states of lithium passivated germanium nanowires: An ab-initio study

    SciTech Connect (OSTI)

    Trejo, A.; Carvajal, E.; Vzquez-Medina, R.; Cruz-Irisson, M.

    2014-05-15

    A study of the electronic and structural properties of germanium nanowires (GeNWs) was performed using the ab-initio Density Functional Theory within the generalized gradient approximation where electron-ion interactions are described by ultrasoft pseudopotentials. To study the effects of the lithium in the surface of the GeNWs we compare the electronic band structures of Hydrogen passivated GeNWs with those of partial and totally Li passivated GeNWs. The nanowires were constructed in the [001], [111] and [110] directions, using the supercell model to create different wire diameters. The results show that in the case of partial Li passivation there are localized orbitals near the valence band maximum, which would create a p-doped-kind of state. The total Li passivation created metallic states for all the wires.

  20. Lattice dynamics and thermoelectric properties of nanocrystalline silicon-germanium alloys

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Claudio, Tania; Stein, Niklas; Peterman, Nils; Stroppa, Daniel; Koza, Michael M.; Wiggers, Hartmut; Klobes, B.; Schierning, Gabi; Hermann, Raphael P.

    2015-10-26

    The lattice dynamics and thermoelectric properties of sintered phosphorus-doped nanostructured silicon- germanium alloys obtained by gas-phase synthesis were studied. Measurements of the density of phonon states by inelastic neutron scattering were combined with measurements of the elastic constants and the low- temperature heat capacity. A strong influence of nanostructuring and alloying on the lattice dynamics was observed. The thermoelectric transport properties of samples with different doping as well as samples sintered at different temperature were characterized between room temperature and 1000C. A peak figure of merit zT = 0:88 at 900C is observed and comparatively insensitive to the aforementioned param-moreeter variations.less

  1. Argon–germane in situ plasma clean for reduced temperature Ge on Si epitaxy by high density plasma chemical vapor deposition

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Douglas, Erica A.; Sheng, Josephine J.; Verley, Jason C.; Carroll, Malcolm S.

    2015-06-04

    We found that the demand for integration of near infrared optoelectronic functionality with silicon complementary metal oxide semiconductor (CMOS) technology has for many years motivated the investigation of low temperature germanium on silicon deposition processes. Our work describes the development of a high density plasma chemical vapor deposition process that uses a low temperature (<460 °C) in situ germane/argon plasma surface preparation step for epitaxial growth of germanium on silicon. It is shown that the germane/argon plasma treatment sufficiently removes SiOx and carbon at the surface to enable germanium epitaxy. Finally, the use of this surface preparation step demonstrates anmore » alternative way to produce germanium epitaxy at reduced temperatures, a key enabler for increased flexibility of integration with CMOS back-end-of-line fabrication.« less

  2. Argon–germane in situ plasma clean for reduced temperature Ge on Si epitaxy by high density plasma chemical vapor deposition

    SciTech Connect (OSTI)

    Douglas, Erica A.; Sheng, Josephine J.; Verley, Jason C.; Carroll, Malcolm S.

    2015-06-04

    We found that the demand for integration of near infrared optoelectronic functionality with silicon complementary metal oxide semiconductor (CMOS) technology has for many years motivated the investigation of low temperature germanium on silicon deposition processes. Our work describes the development of a high density plasma chemical vapor deposition process that uses a low temperature (<460 °C) in situ germane/argon plasma surface preparation step for epitaxial growth of germanium on silicon. It is shown that the germane/argon plasma treatment sufficiently removes SiOx and carbon at the surface to enable germanium epitaxy. Finally, the use of this surface preparation step demonstrates an alternative way to produce germanium epitaxy at reduced temperatures, a key enabler for increased flexibility of integration with CMOS back-end-of-line fabrication.

  3. Improved WIMP-search reach of the CDMS II germanium data

    SciTech Connect (OSTI)

    Agnese, R.

    2015-10-12

    CDMS II data from the five-tower runs at the Soudan Underground Laboratory were reprocessed with an improved charge-pulse fitting algorithm. Two new analysis techniques to reject surface-event backgrounds were applied to the 612 kg days germanium-detector weakly interacting massive particle (WIMP)-search exposure. An extended analysis was also completed by decreasing the 10 keV analysis threshold to ~5 keV, to increase sensitivity near a WIMP mass of 8 GeV/c2. After unblinding, there were zero candidate events above a deposited energy of 10 keV and six events in the lower-threshold analysis. This yielded minimum WIMP-nucleon spin-independent scattering cross-section limits of 1.8×10–44 and 1.18×10–41 at 90% confidence for 60 and 8.6 GeV/c2 WIMPs, respectively. This improves the previous CDMS II result by a factor of 2.4 (2.7) for 60 (8.6) GeV/c2 WIMPs.

  4. Improved WIMP-search reach of the CDMS II germanium data

    SciTech Connect (OSTI)

    Agnese, R.; Anderson, A. J.; Asai, M.; Balakishiyeva, D.; Barker, D.; Basu Thakur, R.; Bauer, D. A.; Billard, J.; Borgland, A.; Bowles, M. A.; Brandt, D.; Brink, P. L.; Bunker, R.; Cabrera, B.; Caldwell, D. O.; Calkins, R.; Cerdeno, D. G.; Chagani, H.; Chen, Y.; Cooley, J.; Cornell, B.; Crewdson, C. H.; Cushman, Priscilla B.; Daal, M.; Di Stefano, P. C.; Doughty, T.; Esteban, L.; Fallows, S.; Figueroa-Feliciano, E.; Godfrey, G. L.; Golwala, S. R.; Hall, Jeter C.; Harris, H. R.; Hertel, S. A.; Hofer, T.; Holmgren, D.; Hsu, L.; Huber, M. E.; Jardin, D. M.; Jastram, A.; Kamaev, O.; Kara, B.; Kelsey, M. H.; Kennedy, A.; Kiveni, M.; Koch, K.; Leder, A.; Loer, B.; Lopez Asamar, E.; Lukens, P.; Mahapatra, R.; Mandic, V.; McCarthy, K. A.; Mirabolfathi, N.; Moffatt, R. A.; Oser, S. M.; Page, K.; Page, W. A.; Partridge, R.; Pepin, M.; Phipps, A.; Prasad, K.; Pyle, M.; Qiu, H.; Rau, W.; Redl, P.; Reisetter, A.; Ricci, Y.; Rogers, H. E.; Saab, T.; Sadoulet, B.; Sander, J.; Schneck, K.; Schnee, R. W.; Scorza, S.; Serfass, B.; Shank, B.; Speller, D.; Toback, D.; Upadhyayula, S.; Villano, A. N.; Welliver, B.; Wilson, J. S.; Wright, D. H.; Yang, X.; Yellin, S.; Yen, J. J.; Young, B. A.; Zhang, J.

    2015-10-31

    CDMS II data from the five-tower runs at the Soudan Underground Laboratory were reprocessed with an improved charge-pulse fitting algorithm. Two new analysis techniques to reject surface-event backgrounds were applied to the 612 kg days germanium-detector weakly interacting massive particle (WIMP)-search exposure. An extended analysis was also completed by decreasing the 10 keV analysis threshold to ~5 keV, to increase sensitivity near a WIMP mass of 8 GeV/c2. After unblinding, there were zero candidate events above a deposited energy of 10 keV and six events in the lower-threshold analysis. This yielded minimum WIMP-nucleon spin-independent scattering cross-section limits of 1.810-44 and 1.1810-41 at 90% confidence for 60 and 8.6 GeV/c2 WIMPs, respectively. This improves the previous CDMS II result by a factor of 2.4 (2.7) for 60 (8.6) GeV/c2 WIMPs.

  5. Improved WIMP-search reach of the CDMS II germanium data

    SciTech Connect (OSTI)

    Agnese, R.

    2015-10-12

    CDMS II data from the five-tower runs at the Soudan Underground Laboratory were reprocessed with an improved charge-pulse fitting algorithm. Two new analysis techniques to reject surface-event backgrounds were applied to the 612 kg days germanium-detector weakly interacting massive particle (WIMP)-search exposure. An extended analysis was also completed by decreasing the 10 keV analysis threshold to ~5 keV, to increase sensitivity near a WIMP mass of 8 GeV/c2. After unblinding, there were zero candidate events above a deposited energy of 10 keV and six events in the lower-threshold analysis. This yielded minimum WIMP-nucleon spin-independent scattering cross-section limits of 1.81044 and 1.181041 at 90% confidence for 60 and 8.6 GeV/c2 WIMPs, respectively. This improves the previous CDMS II result by a factor of 2.4 (2.7) for 60 (8.6) GeV/c2 WIMPs.

  6. Improved WIMP-search reach of the CDMS II germanium data

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Agnese, R.

    2015-10-12

    CDMS II data from the five-tower runs at the Soudan Underground Laboratory were reprocessed with an improved charge-pulse fitting algorithm. Two new analysis techniques to reject surface-event backgrounds were applied to the 612 kg days germanium-detector weakly interacting massive particle (WIMP)-search exposure. An extended analysis was also completed by decreasing the 10 keV analysis threshold to ~5 keV, to increase sensitivity near a WIMP mass of 8 GeV/c2. After unblinding, there were zero candidate events above a deposited energy of 10 keV and six events in the lower-threshold analysis. This yielded minimum WIMP-nucleon spin-independent scattering cross-section limits of 1.8×10–44 andmore » 1.18×10–41 at 90% confidence for 60 and 8.6 GeV/c2 WIMPs, respectively. This improves the previous CDMS II result by a factor of 2.4 (2.7) for 60 (8.6) GeV/c2 WIMPs.« less

  7. Absolute x-ray yields from laser-irradiated germanium-doped low-density aerogels

    SciTech Connect (OSTI)

    Fournier, K. B.; Satcher, J. H.; May, M. J.; Poco, J. F.; Sorce, C. M.; Colvin, J. D.; Hansen, S. B.; MacLaren, S. A.; Moon, S. J.; Davis, J. F. [Lawrence Livermore National Laboratory, Livermore, California 94551 (United States); Girard, F.; Villette, B.; Primout, M.; Babonneau, D. [Commissariat a l'Energie Atomique-Direction des Application Militaires (CEA/DAM), Ile-de-France, F91297 Arpajon (France); Coverdale, C. A.; Beutler, D. E. [Sandia National Laboratory, Albuquerque, New Mexico 87185 (United States)

    2009-05-15

    The x-ray yields from laser-irradiated germanium-doped ultra-low-density aerogel plasmas have been measured in the energy range from sub-keV to {approx_equal}15 keV at the OMEGA laser facility at the Laboratory for Laser Energetics, University of Rochester. The targets' x-ray yields have been studied for variation in target size, aerogel density, laser pulse length, and laser intensity. For targets that result in plasmas with electron densities in the range of {approx_equal}10% of the critical density for 3{omega} light, one can expect 10-11 J/sr of x rays with energies above 9 keV, and 600-800 J/sr for energies below 3.5 keV. In addition to the x-ray spectral yields, the x-ray temporal waveforms have been measured and it is observed that the emitted x rays generally follow the delivered laser power, with late-time enhancements of emitted x-ray power correlated with hydrodynamic compression of the hot plasma. Further, the laser energy reflected from the target by plasma instabilities is found to be 2%-7% of the incident energy for individual beam intensities {approx_equal}10{sup 14}-10{sup 15} W/cm{sup 2}. The propagation of the laser heating in the target volume has been characterized with two-dimensional imaging. Source-region heating is seen to be correlated with the temporal profile of the emitted x-ray power.

  8. Characterization of hydrogenated amorphous germanium compounds obtained by x-ray chemical vapor deposition of germane: Effect of the irradiation dose on optical parameters and structural order

    SciTech Connect (OSTI)

    Arrais, Aldo; Benzi, Paola; Bottizzo, Elena; Demaria, Chiara

    2007-11-15

    Hydrogenated nonstoichiometric germanium materials have been produced by x-ray activated-chemical vapor deposition from germane. The reactions pattern leading to the solid products has been investigated. The dose effect on the composition, the local bonding configuration, and structural characteristics of the deposited solids has been studied using infrared absorption and Raman spectroscopy and has been discussed. Optical parameters have been also determined from ultraviolet-visible spectrophotometry data. The results show that the solids are formed by a random bound network of germanium and hydrogen atoms with a-Ge zones dispersed in the matrix. The Raman results and optical parameters indicate that the structural order, both short-range and intermediate-range, decreases with increasing irradiation time. This behavior suggests that the solid is involved in the reactions leading to the final product and indicates that the formation of amorphous germanium zones is stimulated by postdeposition irradiation, which induces compositional and structural modifications.

  9. Direct Evidence for Abrupt Postcrystallization Germanium Precipitation in Thin Phase-Change Films of Sb-15 at. % Ge

    SciTech Connect (OSTI)

    Cabral,C.; Krusin-Elbaum, L.; Bruley, J.; Raoux, S.; Deline, V.; Madan, A.; Pinto, T.

    2008-01-01

    We present evidence for the instability in the crystalline (metallic) state of binary Te-free phase-change Ge-Sb thin films considered for integration into nonvolatile nanosized memory cells. We find that while the amorphous (semiconducting) phase of eutectic Sb-15 at. % Ge is very robust until Sb crystallization at 240 C, at about 350 C, germanium rapidly precipitates out. Ge precipitation, visualized directly with transmission electron microscopy, is exothermic and is found to affect the films' reflectivity, resistance, and stress. It converts melting into a two-step process, which may seriously impact the switching reliability of a device.

  10. Foundations for quantitative microstructural models to track evolution of the metallurgical state during high purity Nb cavity fabrication

    SciTech Connect (OSTI)

    Bieler, Thomas R; Wright, Neil T; Compton, Chris C

    2014-03-15

    The goal of the Materials Science SRF Cavity Group of Michigan State University and the National Superconducting Cyclotron has been (and continues to be) to understand quantitatively the effects of process history on functional properties. These relationships were assessed via studies on Nb samples and cavity parts, which had various combinations of forming processes, welding, heat treatments, and surface preparation. A primary focus was on large-grain cavity building strategies. Effects of processing operations and exposure to hydrogen on the thermal conductivity has been identified in single and bi-crystal samples, showing that the thermal conductivity can be altered by a factor of 5 depending on process history. Characterization of single crystal tensile samples show a strong effect of crystal orientation on deformation resistance and shape changes. Large grain half cells were examined to characterize defect content and surface damage effects, which provided quantitative information about the depth damage layers from forming.

  11. Calcium looping process for high purity hydrogen production integrated with capture of carbon dioxide, sulfur and halides

    DOE Patents [OSTI]

    Ramkumar, Shwetha; Fan, Liang-Shih

    2013-07-30

    A process for producing hydrogen comprising the steps of: (i) gasifying a fuel into a raw synthesis gas comprising CO, hydrogen, steam, sulfur and halide contaminants in the form of H.sub.2S, COS, and HX, wherein X is a halide; (ii) passing the raw synthesis gas through a water gas shift reactor (WGSR) into which CaO and steam are injected, the CaO reacting with the shifted gas to remove CO.sub.2, sulfur and halides in a solid-phase calcium-containing product comprising CaCO.sub.3, CaS and CaX.sub.2; (iii) separating the solid-phase calcium-containing product from an enriched gaseous hydrogen product; and (iv) regenerating the CaO by calcining the solid-phase calcium-containing product at a condition selected from the group consisting of: in the presence of steam, in the presence of CO.sub.2, in the presence of synthesis gas, in the presence of H.sub.2 and O.sub.2, under partial vacuum, and combinations thereof.

  12. Calcium looping process for high purity hydrogen production integrated with capture of carbon dioxide, sulfur and halides

    DOE Patents [OSTI]

    Ramkumar, Shwetha; Fan, Liang-Shih

    2015-11-04

    A process for producing hydrogen comprising the steps of: (i) gasifying a fuel into a raw synthesis gas comprising CO, hydrogen, steam, sulfur and halide contaminants in the form of H.sub.2S, COS, and HX, wherein X is a halide; (ii) passing the raw synthesis gas through a water gas shift reactor (WGSR) into which CaO and steam are injected, the CaO reacting with the shifted gas to remove CO.sub.2, sulfur and halides in a solid-phase calcium-containing product comprising CaCO.sub.3, CaS and CaX.sub.2; (iii) separating the solid-phase calcium-containing product from an enriched gaseous hydrogen product; and (iv) regenerating the CaO by calcining the solid-phase calcium-containing product at a condition selected from the group consisting of: in the presence of steam, in the presence of CO.sub.2, in the presence of synthesis gas, in the presence of H.sub.2 and O.sub.2, under partial vacuum, and combinations thereof.

  13. Alleviation of fermi-level pinning effect at metal/germanium interface by the insertion of graphene layers

    SciTech Connect (OSTI)

    Baek, Seung-heon Chris; Seo, Yu-Jin; Oh, Joong Gun; Albert Park, Min Gyu; Bong, Jae Hoon; Yoon, Seong Jun; Lee, Seok-Hee, E-mail: seokheelee@ee.kaist.ac.kr [Department of Electrical Engineering, Korea Advanced Institute of Science and Technology (KAIST), 291 Daehak-ro, Yuseong-gu, Daejeon 305-701 (Korea, Republic of); Seo, Minsu; Park, Seung-young [Division of Materials Science, Korea Basic Science Institute (KBSI), 169-148 Daehak-ro, Yuseong-gu, Daejeon 305-333 (Korea, Republic of); Park, Byong-Guk [Department of Materials Science and Engineering, Korea Advanced Institute of Science and Technology (KAIST), 291 Daehak-ro, Yuseong-gu, Daejeon 305-701 (Korea, Republic of)

    2014-08-18

    In this paper, we report the alleviation of the Fermi-level pinning on metal/n-germanium (Ge) contact by the insertion of multiple layers of single-layer graphene (SLG) at the metal/n-Ge interface. A decrease in the Schottky barrier height with an increase in the number of inserted SLG layers was observed, which supports the contention that Fermi-level pinning at metal/n-Ge contact originates from the metal-induced gap states at the metal/n-Ge interface. The modulation of Schottky barrier height by varying the number of inserted SLG layers (m) can bring about the use of Ge as the next-generation complementary metal-oxide-semiconductor material. Furthermore, the inserted SLG layers can be used as the tunnel barrier for spin injection into Ge substrate for spin-based transistors.

  14. High Accuracy U-235 Enrichment Verification Station for Low Enriched Uranium Alloys

    SciTech Connect (OSTI)

    Lillard, C. R.; Hayward, J. P.; Williamson, M. R.

    2012-06-07

    The Y-12 National Security Complex is playing a role in the U.S. High Performance Research Reactor (USHPRR) Conversion program sponsored by the U.S. National Nuclear Security Administration's Office of Global Threat Reduction. The USHPRR program has a goal of converting remaining U.S. reactors that continue to use highly enriched uranium (HEU) fuel to low enriched uranium (LEU) fuel. The USHPRR program is currently developing a LEU Uranium-Molybdenum (U-Mo) monolithic fuel for use in the U.S. high performance research reactors.Y-12 is supporting both the fuel development and fuel fabrication efforts by fabricating low enriched U-Mo foils from its own source material for irradiation experiments and for optimizing the fabrication process in support of scaling up the process to a commercial production scale. Once the new fuel is qualified, Y-12 will produce and ship U-Mo coupons with verified 19.75% +0.2% - 0.3% U-235 enrichment to be fabricated into fuel elements for the USHPRRs. Considering this small enrichment tolerance and the transition into HEU being set strictly at 20% U-235, a characterization system with a measurement uncertainty of less than or equal to 0.1% in enrichment is desired to support customer requirements and minimize production costs. Typical uncertainty for most available characterization systems today is approximately 1-5%; therefore, a specialized system must be developed which results in a reduced measurement uncertainty. A potential system using a High-Purity Germanium (HPGe) detector has been procured, and tests have been conducted to verify its capabilities with regards to the requirements. Using four U-Mo enrichment standards fabricated with complete isotopic and chemical characterization, infinite thickness and peak-ratio enrichment measurement methods have been considered for use. As a result of inhomogeneity within the U-Mo samples, FRAM, an isotopic analysis software, has been selected for initial testing. A systematic approach towards observing effects on FRAM's enrichment analysis has been conducted with regards to count and dead time.

  15. HIgh Rate X-ray Fluorescence Detector

    SciTech Connect (OSTI)

    Grudberg, Peter Matthew

    2013-04-30

    The purpose of this project was to develop a compact, modular multi-channel x-ray detector with integrated electronics. This detector, based upon emerging silicon drift detector (SDD) technology, will be capable of high data rate operation superior to the current state of the art offered by high purity germanium (HPGe) detectors, without the need for liquid nitrogen. In addition, by integrating the processing electronics inside the detector housing, the detector performance will be much less affected by the typically noisy electrical environment of a synchrotron hutch, and will also be much more compact than current systems, which can include a detector involving a large LN2 dewar and multiple racks of electronics. The combined detector/processor system is designed to match or exceed the performance and features of currently available detector systems, at a lower cost and with more ease of use due to the small size of the detector. In addition, the detector system is designed to be modular, so a small system might just have one detector module, while a larger system can have many ?? you can start with one detector module, and add more as needs grow and budget allows. The modular nature also serves to simplify repair. In large part, we were successful in achieving our goals. We did develop a very high performance, large area multi-channel SDD detector, packaged with all associated electronics, which is easy to use and requires minimal external support (a simple power supply module and a closed-loop water cooling system). However, we did fall short of some of our stated goals. We had intended to base the detector on modular, large-area detectors from Ketek GmbH in Munich, Germany; however, these were not available in a suitable time frame for this project, so we worked instead with pnDetector GmbH (also located in Munich). They were able to provide a front-end detector module with six 100 m^2 SDD detectors (two monolithic arrays of three elements each) along with associated preamplifiers; these detectors surpassed the performance we expected to get from the Ketek detectors, however they are housed in a sealed module, which does not offer the ease of repair and expandability we??d hoped to achieve with the Ketek SDD??s. Our packaging efforts were quite successful, as we came up with a very compact way to mount the detector and to house the associated electronics, as well as a very effective way to reliably take out the heat (from the electronics as well as the detector??s Peltier coolers) without risk of condensation and without external airflow or vibration, which could create problems for the target applications. While we were able to design compact processing electronics that fit into the detector assembly, they are still at the prototype stage, and would require a significant redesign to achieve product status. We have not yet tested this detector at a synchrotron facility; we do still plan on working with some close contacts at the nearby Stanford Synchrotron Radiation Laboratory (SSRL) to get some testing with the beam (using existing commercial electronics for readout, as the integrated processor is not ready for use).

  16. Cryogenic Preamplification of a Single-Electron-Transistor using a Silicon-Germanium Heterojunction-Bipolar-Transistor

    SciTech Connect (OSTI)

    Curry, Matthew J.; England, Troy Daniel; Bishop, Nathaniel; Ten Eyck, Gregory A.; Wendt, Joel R.; Pluym, Tammy; Lilly, Michael; Carr, Stephen M; Carroll, Malcolm S.

    2015-05-21

    We examine a silicon-germanium heterojunction bipolar transistor (HBT) for cryogenic pre-amplification of a single electron transistor (SET). The SET current modulates the base current of the HBT directly. The HBT-SET circuit is immersed in liquid helium, and its frequency response from low frequency to several MHz is measured. The current gain and the noise spectrum with the HBT result in a signal-to-noise-ratio (SNR) that is a factor of 10100 larger than without the HBT at lower frequencies. Furthermore, the transition frequency defined by SNR = 1 has been extended by as much as a factor of 10 compared to without the HBT amplification. The power dissipated by the HBT cryogenic pre-amplifier is approximately 5 nW to 5 ?W for the investigated range of operation. We found that the circuit is also operated in a single electron charge read-out configuration in the time-domain as a proof-of-principle demonstration of the amplification approach for single spin read-out.

  17. Cryogenic Preamplification of a Single-Electron-Transistor using a Silicon-Germanium Heterojunction-Bipolar-Transistor

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Curry, Matthew J.; Sandia National Lab.; England, Troy Daniel; Bishop, Nathaniel; Ten Eyck, Gregory A.; Wendt, Joel R.; Pluym, Tammy; Lilly, Michael; Carr, Stephen M; Sandia National Lab.; et al

    2015-05-21

    We examine a silicon-germanium heterojunction bipolar transistor (HBT) for cryogenic pre-amplification of a single electron transistor (SET). The SET current modulates the base current of the HBT directly. The HBT-SET circuit is immersed in liquid helium, and its frequency response from low frequency to several MHz is measured. The current gain and the noise spectrum with the HBT result in a signal-to-noise-ratio (SNR) that is a factor of 10–100 larger than without the HBT at lower frequencies. Furthermore, the transition frequency defined by SNR = 1 has been extended by as much as a factor of 10 compared to withoutmore » the HBT amplification. The power dissipated by the HBT cryogenic pre-amplifier is approximately 5 nW to 5 μW for the investigated range of operation. We found that the circuit is also operated in a single electron charge read-out configuration in the time-domain as a proof-of-principle demonstration of the amplification approach for single spin read-out.« less

  18. High speed flow cytometric separation of viable cells

    DOE Patents [OSTI]

    Sasaki, Dennis T. (Mountain View, CA); Van den Engh, Gerrit J. (Seattle, WA); Buckie, Anne-Marie (Margate, GB)

    1995-01-01

    Hematopoietic cell populations are separated to provide cell sets and subsets as viable cells with high purity and high yields, based on the number of original cells present in the mixture. High-speed flow cytometry is employed using light characteristics of the cells to separate the cells, where high flow speeds are used to reduce the sorting time.

  19. High speed flow cytometric separation of viable cells

    DOE Patents [OSTI]

    Sasaki, D.T.; Van den Engh, G.J.; Buckie, A.M.

    1995-11-14

    Hematopoietic cell populations are separated to provide cell sets and subsets as viable cells with high purity and high yields, based on the number of original cells present in the mixture. High-speed flow cytometry is employed using light characteristics of the cells to separate the cells, where high flow speeds are used to reduce the sorting time.

  20. Steering of an ultrarelativistic proton beam by a bent germanium crystal

    SciTech Connect (OSTI)

    De Salvador, D.; Carturan, S.; Bazzan, M.; Argiolas, N.; Carnera, A.; Bagli, E.; Mazzolari, A.; Lytovchenko, O.; Della Mea, G.; Guidi, V.; Bolognini, D.; Hasan, S.; Prest, M.; Vallazza, E.

    2011-06-06

    Curved crystals, thanks to the electrostatic potential generated by the coherent atomic structure, may deflect ultrarelativistic charged particles by means of channeling and volume reflection effects. Most of the experimental knowledge about these phenomena was gathered with Si crystals, though the performance could be improved by using materials with a larger atomic number. In this letter, we investigate planar and axial channeling and volume reflection in a high quality Ge short strip crystal. All the effects are demonstrated to occur in agreement with theoretical expectations, which take into account the stronger confinement potential for an ideal Ge crystal.

  1. Ballistic electron transport calculation of strained germanium-tin fin field-effect transistors

    SciTech Connect (OSTI)

    Lan, H.-S.; Liu, C. W.

    2014-05-12

    The dependence of ballistic electron current on Sn content, sidewall orientations, fin width, and uniaxial stress is theoretically studied for the GeSn fin field-effect transistors. Alloying Sn increases the direct ? valley occupancy and enhances the injection velocity at virtual source node. (112{sup }) sidewall gives the highest current enhancement due to the rapidly increasing ? valley occupancy. The non-parabolicity of the ? valley affects the occupancy significantly. However, uniaxial tensile stress and the shrinkage of fin width reduce the ? valley occupancy, and the currents are enhanced by increasing occupancy of specific indirect L valleys with high injection velocity.

  2. Evolution of microstructural defects with strain effects in germanium nanocrystals synthesized at different annealing temperatures

    SciTech Connect (OSTI)

    Zhang, Minghuan; Cai, Rongsheng; Zhang, Yujuan; Wang, Chao; Wang, Yiqian; Ross, Guy G.; Barba, David

    2014-07-01

    Ge nanocrystals (Ge-ncs) were produced by implantation of {sup 74}Ge{sup +} into a SiO{sub 2} film on (100) Si, followed by high-temperature annealing from 700 °C to 1100 °C. Transmission electron microscopy (TEM) studies show that the average size of Ge-ncs increases with the annealing temperature. High-resolution TEM (HRTEM) investigations reveal the presence of planar and linear defects in the formed Ge-ncs, whose relative concentrations are determined at each annealing temperature. The relative concentration of planar defects is almost independent of the annealing temperature up to 1000 °C. However, from 1000 °C to 1100 °C, its concentration decreases dramatically. For the linear defects, their concentration varies considerably with the annealing temperatures. In addition, by measuring the interplanar spacing of Ge-ncs from the HRTEM images, a strong correlation is found between the dislocation percentage and the stress field intensity. Our results provide fundamental insights regarding both the presence of microstructural defects and the origin of the residual stress field within Ge-ncs, which can shed light on the fabrication of Ge-ncs with quantified crystallinity and appropriate size for the advanced Ge-nc devices. - Highlights: • Growth of Ge nanocrystals at different annealing temperatures was investigated. • Strain field has great effects on the formation of dislocations. • Different mechanisms are proposed to explain growth regimes of Ge nanocrystals.

  3. Frustrated incomplete donor ionization in ultra-low resistivity germanium films

    SciTech Connect (OSTI)

    Xu, Chi; Menndez, J.; Senaratne, C. L.; Kouvetakis, J.

    2014-12-08

    The relationship between carrier concentration and donor atomic concentration has been determined in n-type Ge films doped with P. The samples were carefully engineered to minimize non-active dopant incorporation by using specially designed P(SiH{sub 3}){sub 3} and P(GeH{sub 3}){sub 3} hydride precursors. The in situ nature of the doping and the growth at low temperatures, facilitated by the Ge{sub 3}H{sub 8} and Ge{sub 4}H{sub 10} Ge sources, promote the creation of ultra-low resistivity films with flat doping profiles that help reduce the errors in the concentration measurements. The results show that Ge deviates strongly from the incomplete ionization expected when the donor atomic concentration exceeds N{sub d}?=?10{sup 17}?cm{sup ?3}, at which the energy separation between the donor and Fermi levels ceases to be much larger than the thermal energy. Instead, essentially full ionization is seen even at the highest doping levels beyond the solubility limit of P in Ge. The results can be explained using a model developed for silicon by Altermatt and coworkers, provided the relevant model parameter is properly scaled. The findings confirm that donor solubility and/or defect formation, not incomplete ionization, are the major factors limiting the achievement of very high carrier concentrations in n-type Ge. The commercially viable chemistry approach applied here enables fabrication of supersaturated and fully ionized prototypes with potential for broad applications in group-IV semiconductor technologies.

  4. High volume production of nanostructured materials

    DOE Patents [OSTI]

    Ripley, Edward B. (Knoxville, TN); Morrell, Jonathan S. (Knoxville, TN); Seals, Roland D. (Oak Ridge, TN); Ludtka, Gerard M. (Oak Ridge, TN)

    2009-10-13

    A system and method for high volume production of nanoparticles, nanotubes, and items incorporating nanoparticles and nanotubes. Microwave, radio frequency, or infrared energy vaporizes a metal catalyst which, as it condenses, is contacted by carbon or other elements such as silicon, germanium, or boron to form agglomerates. The agglomerates may be annealed to accelerate the production of nanotubes. Magnetic or electric fields may be used to align the nanotubes during their production. The nanotubes may be separated from the production byproducts in aligned or non-aligned configurations. The agglomerates may be formed directly into tools, optionally in compositions that incorporate other materials such as abrasives, binders, carbon-carbon composites, and cermets.

  5. Workshop on nuclear structure at moderate and high spin: Slide report

    SciTech Connect (OSTI)

    Not Available

    1986-10-01

    The workshop was scheduled to coincide with the beginning of operation of a number of large arrays of Compton-suppressed germanium detectors. The workshop was divided into 14 sessions containing 3 presentations each. The topics of these sessions were superdeformation, heavy rare earths, single-particle configurations, band termination, continuum properties, light rare-earths, new techniques, high temperatures, transfer reactions, transition region, shapes, lifetimes, and moments. This publication consists of the slides used in all of the presentations at the workshop.

  6. Advancing the Technology Base for High Temperature Hydrogen Membranes

    SciTech Connect (OSTI)

    Dye, Robert C.; Moss, Thomas S.

    1997-12-31

    High purity hydrogen is a critical component for at least two major industrial processes: 1) the refining of conventional steels and raw pig iron into low carbon steels and high purity iron used for high performance magnets in motors, generators, alternators, transformers, and etc.; and 2) refining metallurgical grade silicon to the high- purity, polycrystalline silicon used in fabricating single crystal silicon wafers for semiconductor manufacturing. In the process of producing low carbon iron products, CO and CO2 impurities prevent efficient removal of the carbon already in the raw iron. In the refining of metallurgical grade silicon, the presence of any impurity above the part-per- million level prevents the ultimate fabrication of the large scale single crystals that are essential to the semiconductor device. In a lesser magnitude role, high quality hydrogen is used in a variety of other processes, including specialty metals refining (e.g., iridium, osmium, palladium, platinum, and ruthenium) and R{ampersand}D in areas such as organic synthesis and development of certain types of fuel cells. In all of these applications, a high-temperature hydrogen membrane can provide a method for achieving a very high purity level of hydrogen in a manner that is more economical and/or more rugged than existing techniques.

  7. Production of aluminum-silicon alloy and ferrosilicon and commercial purity aluminum by the direct reduction process. Second annual technical report for the period 1978 September 1-1979 December 31

    SciTech Connect (OSTI)

    Bruno, M.J.

    1980-10-01

    A new computer program was developed for simultaneously solving heat and mass balance at steady state for a flowing one-dimensional chemical reactor. Bench scale reactor results confirmed that minimum final stage reaction temperature is 1950 to 2000/sup 0/C, depending on the Fe/sub 2/O/sub 3/ concentration in the burden. Additions of Fe/sub 2/O/sub 3/ to the charge produced significant increase in metallic yield. A new bench reactor was designed, built, and operated to facilitate semi-continuous operation, using O/sub 2/ injection to burn coke supporting the burden, resulting in burden movement. Validity of the equipment and test procedures was demonstrated by successfully operating the reactor as an iron blast furnace at 1500/sup 0/C. Bench scale fractional crystallizer runs were continued to determine the impurity effects of Fe up to 6.9% and Ti up to 1.25% on alloy product purity and yield. High initial impurity concentrations resulted in less pure Al-Si product and product yield below 50% due to Al and Si losses as Fe-Si-Al and Ti-Si-Al intermetallics. Long term testing was continued in the large bench scale membrane cell to evaluate woven cloth membrane and other construction materials, operating procedures, and effects of operating parameters on cell performance. Included in the latter were starting alloy composition, current density, anode-cathode spacing, and electrolyte composition.

  8. Method and apparatus for measuring lung density by Compton backscattering

    DOE Patents [OSTI]

    Loo, B.W.; Goulding, F.S.

    1988-03-11

    The density of the lung of a patient suffering from pulmonary edema is monitored by irradiating the lung by a single collimated beam of monochromatic photons and measuring the energies of photons compton back-scattered from the lung by a single high-resolution, high-purity germanium detector. A compact system geometry and a unique data extraction scheme are utilized to minimize systematic errors due to the presence of the chestwall and multiple scattering. 11 figs., 1 tab.

  9. Method and apparatus for measuring lung density by Compton backscattering

    DOE Patents [OSTI]

    Loo, Billy W. (Oakland, CA); Goulding, Frederick S. (Lafayette, CA)

    1991-01-01

    The density of the lung of a patient suffering from pulmonary edema is monitored by irradiating the lung by a single collimated beam of monochromatic photons and measuring the energies of photons Compton backscattered from the lung by a single high-resolution, high-purity germanium detector. A compact system geometry and a unique data extraction scheme are utilized to monimize systematic errors due to the presence of the chestwall and multiple scattering.

  10. Methods for high volume production of nanostructured materials

    DOE Patents [OSTI]

    Ripley, Edward B. (Knoxville, TN); Morrell, Jonathan S. (Knoxville, TN); Seals, Roland D. (Oak Ridge, TN); Ludtka, Gerald M. (Oak Ridge, TN)

    2011-03-22

    A system and method for high volume production of nanoparticles, nanotubes, and items incorporating nanoparticles and nanotubes. Microwave, radio frequency, or infrared energy vaporizes a metal catalyst which, as it condenses, is contacted by carbon or other elements such as silicon, germanium, or boron to form agglomerates. The agglomerates may be annealed to accelerate the production of nanotubes. Magnetic or electric fields may be used to align the nanotubes during their production. The nanotubes may be separated from the production byproducts in aligned or non-aligned configurations. The agglomerates may be formed directly into tools, optionally in compositions that incorporate other materials such as abrasives, binders, carbon-carbon composites, and cermets.

  11. Handheld isotope identification system

    DOE Patents [OSTI]

    Frankle, Christen M. (Los Alamos, NM); Becker, John A. (Alameda, CA); Cork,; Christopher P. (Pleasant Hill, CA); Madden, Norman W. (Livermore, CA)

    2007-01-09

    A portable radiation detector using a high-purity germanium crystal as the sensing device. The crystal is fabricated such that it exhibits a length to width ratio greater than 1:1 and is oriented within the detector to receive radiation along the width of said crystal. The crystal is located within a container pressurized with ultra-pure nitrogen, and the container is located within a cryostat under vacuum.

  12. Microsoft Word - DOE-ID-12-005 New Mexico.doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    5 SECTION A. Project Title: Equipment Upgrade for the UNM AGN-201M Reactor - University of New Mexico SECTION B. Project Description The University of New Mexico will acquire a computer and associated hardware to measure control rod scram times, a laptop computer and associated electronics such as MCS and MCA systems for operating a High Purity Germanium detector, a Frisker and micro R meter for personnel protection and radiation surveys, a new interface for the data channel, NCRP reports, and

  13. Low Background Signal Readout Electronics for the Majorana Demonstrator

    Office of Scientific and Technical Information (OSTI)

    (Conference) | SciTech Connect Low Background Signal Readout Electronics for the Majorana Demonstrator Citation Details In-Document Search Title: Low Background Signal Readout Electronics for the Majorana Demonstrator The MAJORANA Collaboration will seek neutrinoless double beta decay (0νββ) in 76Ge using isotopically enriched p-type point contact (PPC) high purity Germanium (HPGe) detectors. A tonne-scale array of HPGe detectors would require background levels below 1

  14. Investigation of Naturally Occurring Radio Nuclides in Shir-kuh Granites

    SciTech Connect (OSTI)

    Mazarei, Mohammad Mehdi; Zarei, Mojtaba

    2011-12-26

    One of the principle natural radiation resources is Granite which can be dangerous for human because of its radiations. Based on this fact, in this research we attempt to specify the activity amount of these natural radio nuclides, existing in Shir-kuh Granite of Yazd state. To specify the activity amount of this natural radio nuclides, it has been applied the measurement method of Gamma spectroscopy using high purity Germanium (HPGe) detector.

  15. Women @ Energy: Astrid Tomada | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    Astrid Tomada, Staff Engineer at SLAC National Accelerator Laboratory. Astrid Tomada, Staff Engineer at SLAC National Accelerator Laboratory. Astrid Tomada is a Staff Engineer at SLAC National Accelerator Laboratory, a position she has held since 2011. She is an expert in high-purity germanium and silicon detectors for dark matter particle and X-ray experiments, encompassing fabrication, inspection, and packaging of detectors. She has deep experience in the area of equipment quality assurance

  16. High Specific Activity Sn-117m by Post Irradiation Isotope Separation

    SciTech Connect (OSTI)

    DAuria, John

    2015-04-16

    ElectroMagnetic Isotope Separation (EMIS) is used in the production of enriched stable isotopes. We demonstrated the feasibility of using EMIS to produce medium Specific Activity 117mSm using high purity 116Sn target material irradiated in a high flux reactor.

  17. Early diagenesis of germanium in sediments of the Antarctic South Atlantic: In search of the missing Ge sink

    SciTech Connect (OSTI)

    King, S.L.; Froelich, P.N.; Jahnke, R.A.

    2000-04-01

    Pore water and solid-phase geochemistry profiles were obtained from several cores between 41{degree}S and 53{degree}S in the Atlantic sector of the Southern Ocean. Pore water nitrate, manganese, and iron profiles delineate standard redox zones in these sediments, and help characterize those with classic vs. burn-down behaviors. Pore water Si and Ge profiles demonstrate that Ge released during opal dissolution is removed pervasively throughout the uppermost interval of silicate release, and also downwards into the suboxic zone by as yet unidentified precipitation mechanisms. These results indicate that early diagenesis of Ge is uncoupled from that of opal. Solid-phase extractions (Fe, Mn, U, Mo, Ge, Cu, Ni, Co, V, and Cd) in a few cores suggest that anthigenic Ge removal in the suboxic zone is not associated with peaks in authigenic Mn cycling (MnO{sub 2} and related metals) but rather with processes deeper in the sediments, perhaps Fe or U diagenesis. Below the interval of Ge removal, pre water Ge increases linearly with depth by over two orders of magnitude, indicating a deep (below recovery) source of large magnitude. The fraction of opal-derived Ge precipitated authigenically in these sediments ranges from {approximately}1 to 96% and correlates strongly with the detrital fraction as well as the detrital to opal ratio, both of which generally decrease from north to south. The Ge sink observed in these sediments would need to be globally representative to account for the entire missing Ge sink in today's oceanic Ge balance, which seems unlikely. Benthic fluxes of Ge and Si estimated from these pore water profiles and from measurements in three benthic flux chamber experiments at high carbon-rain continental margin sites demonstrate that the Ge/Si rate released from the seafloor in locations with high benthic silicate and carbon fluxes is congruent with Holocene opal dissolution (Ge/Si {approximately} 0.7 x 10{sup {minus}6}). In contrast, Ge/Si flux ratios in areas with low silicate fluxes are Ge-depleted (Ge/Si < 0.5 x 10{sup {minus}6}). The authors speculate that glacial-interglacial changes in oceanic Ge/Si as recorded in diatoms may be due in part to variations in this authigenic Ge sink, perhaps related to shifts in siliceous productivity from open ocean (Antarctic) siliceous oozes during interglacials to areas of higher detrital input (Sub Antarctic, continental margins) and possibly also to generally more reducing conditions in sediments during glacials.

  18. GERDA phase II detectors: Behind the production and characterisation at low background conditions

    SciTech Connect (OSTI)

    Maneschg, Werner [Max-Planck-Institut fr Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany)] [Max-Planck-Institut fr Kernphysik, Saupfercheckweg 1, 69117 Heidelberg (Germany); Collaboration: GERDA Collaboration; and others

    2013-08-08

    The low background GERmanium Detector Array (GERDA) at Laboratori Nazionali del Gran Sasso (LNGS) is designed to search for the rare neutrinoless double beta decay (0???) in {sup 76}Ge. Bare germanium diodes are operated in liquid argon which is used as coolant, as passive and soon active as well shield against external radiation. Currently, Phase I of the experiment is running using ?15 kg of co-axial High Purity Germanium diodes. In order to increase the sensitivity of the experiment 30 Broad Energy Germanium (BEGe) diodes will be added within 2013. This presentation reviews the production chain of the new BEGe detectors from isotopic enrichment to diode production and testing. As demonstrated all steps were carefully planned in order to minimize the exposure of the enriched germanium to cosmic radiation. Following this premise, acceptance and characterisation measurement of the newly produced diodes have been performed within the HEROICA project in the Belgian underground laboratory HADES close to the diode manufacturer. The test program and the results from a subset of the recently terminated GERDA Phase II BEGe survey will be presented.

  19. High Efficiency Triple-Junction Amorphous Silicon Alloy Photovoltaic Technology, Final Technical Report, 6 March 1998 - 15 October 2001

    SciTech Connect (OSTI)

    Guha, S.

    2001-11-08

    This report describes the research program intended to expand, enhance, and accelerate knowledge and capabilities for developing high-performance, two-terminal multijunction amorphous silicon (a-Si) alloy cells, and modules with low manufacturing cost and high reliability. United Solar uses a spectrum-splitting, triple-junction cell structure. The top cell uses an amorphous silicon alloy of {approx}1.8-eV bandgap to absorb blue photons. The middle cell uses an amorphous silicon germanium alloy ({approx}20% germanium) of {approx}1.6-eV bandgap to capture green photons. The bottom cell has {approx}40% germanium to reduce the bandgap to {approx}1.4-eV to capture red photons. The cells are deposited on a stainless-steel substrate with a predeposited silver/zinc oxide back reflector to facilitate light-trapping. A thin layer of antireflection coating is applied to the top of the cell to reduce reflection loss. The major research activities conducted under this program were: (1) Fundamental studies to improve our understanding of materials and devices; the work included developing and analyzing a-Si alloy and a-SiGe alloy materials prepared near the threshold of amorphous-to-microcrystalline transition and studying solar cells fabricated using these materials. (2) Deposition of small-area cells using a radio-frequency technique to obtain higher deposition rates. (3) Deposition of small-area cells using a modified very high frequency technique to obtain higher deposition rates. (4) Large-area cell research to obtain the highest module efficiency. (5) Optimization of solar cells and modules fabricated using production parameters in a large-area reactor.

  20. The Majorana low-noise low-background front-end electronics

    SciTech Connect (OSTI)

    Abgrall, N.; Aguayo, E.; Avignone, III, F. T.; Barabash, A. S.; Bertrand, F. E.; Boswell, M.; Brudanin, V.; Busch, M.; Byram, D.; Caldwell, A. S.; Chan, Y. -D.; Christofferson, C. D.; Combs, D. C.; Cuesta, C.; Detwiler, J. A.; Doe, P. J.; Efremenko, Yu.; Egorov, V.; Ejiri, H.; Elliott, S. R.; Fast, J. E.; Finnerty, P.; Fraenkle, F. M.; Galindo-Uribarri, A.; Giovanetti, G. K.; Goett, J.; Green, M. P.; Gruszko, J.; Guiseppe, V. E.; Gusev, K.; Hallin, A. L.; Hazama, R.; Hegai, A.; Henning, R.; Hoppe, E. W.; Howard, S.; Howe, M. A.; Keeter, K. J.; Kidd, M. F.; Kochetov, O.; Konovalov, S. I.; Kouzes, R. T.; LaFerriere, B. D.; Leon, J.; Leviner, L. E.; Loach, J. C.; MacMullin, J.; MacMullin, S.; Martin, R. D.; Meijer, S.; Mertens, S.; Nomachi, M.; Orrell, J. L.; O'Shaughnessy, C.; Overman, N. R.; Phillips, II, D. G.; Poon, A. W.P.; Pushkin, K.; Radford, D. C.; Rager, J.; Rielage, K.; Robertson, R. G.H.; Romero-Romero, E.; Ronquest, M. C.; Schubert, A. G.; Shanks, B.; Shima, T.; Shirchenko, M.; Snavely, K. J.; Snyder, N.; Suriano, A. M.; Thompson, J.; Timkin, V.; Tornow, W.; Trimble, J. E.; Varner, R. L.; Vasilyev, S.; Vetter, K.; Vorren, K.; White, B. R.; Wilkerson, J. F.; Wiseman, C.; Xu, W.; Yakushev, E.; Young, A. R.; Yu, C. -H.; Yumatov, V.

    2015-03-24

    The Majorana Demonstrator will search for the neutrinoless double beta decay (??(0?)) of the isotope ??Ge with a mixed array of enriched and natural germanium detectors. In view of the next generation of tonne-scale germanium-based ??(0?)-decay searches, a major goal of the Majorana Demonstrator is to demonstrate a path forward to achieving a background rate at or below 1 cnt/(ROI-t-y) in the 4 keV region of interest (ROI) around the 2039-keV Q-value of the ??Ge ??(0?)-decay. Such a requirement on the background level significantly constrains the design of the readout electronics, which is further driven by noise and energy resolution performances. We present here the low-noise low-background front-end electronics developed for the low-capacitance p-type point contact (P-PC) germanium detectors of the Majorana Demonstrator. This resistive-feedback front-end, specifically designed to have low mass, is fabricated on a radioassayed fused-silica substrate where the feedback resistor consists of a sputtered thin film of high purity amorphous germanium and the feedback capacitor is based on the capacitance between gold conductive traces.

  1. The Majorana low-noise low-background front-end electronics

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Abgrall, N.; Aguayo, E.; Avignone, III, F. T.; Barabash, A. S.; Bertrand, F. E.; Boswell, M.; Brudanin, V.; Busch, M.; Byram, D.; Caldwell, A. S.; et al

    2015-03-24

    The Majorana Demonstrator will search for the neutrinoless double beta decay (ββ(0ν)) of the isotope ⁷⁶Ge with a mixed array of enriched and natural germanium detectors. In view of the next generation of tonne-scale germanium-based ββ(0ν)-decay searches, a major goal of the Majorana Demonstrator is to demonstrate a path forward to achieving a background rate at or below 1 cnt/(ROI-t-y) in the 4 keV region of interest (ROI) around the 2039-keV Q-value of the ⁷⁶Ge ββ(0ν)-decay. Such a requirement on the background level significantly constrains the design of the readout electronics, which is further driven by noise and energy resolutionmore » performances. We present here the low-noise low-background front-end electronics developed for the low-capacitance p-type point contact (P-PC) germanium detectors of the Majorana Demonstrator. This resistive-feedback front-end, specifically designed to have low mass, is fabricated on a radioassayed fused-silica substrate where the feedback resistor consists of a sputtered thin film of high purity amorphous germanium and the feedback capacitor is based on the capacitance between gold conductive traces.« less

  2. Enhancing the detector for advanced neutron capture experiments

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Couture, A.; Mosby, S.; Baramsai, B.; Bredeweg, T. A.; Jandel, M.; Macon, K.; O’Donnell, J. M.; Rusev, G.; Taddeucci, T. N; Ullmann, J. L.; et al

    2015-05-28

    The Detector for Advanced Neutron Capture Experiments (DANCE) has been used for extensive studies of neutron capture, gamma decay, photon strength functions, and prompt and delayed fission-gamma emission. Despite these successes, the potential measurements have been limited by the data acquisition hardware. We report on a major upgrade of the DANCE data acquisition that simultaneously enables strait-forward coupling to auxiliary detectors, including high-resolution high-purity germanium detectors and neutron tagging array. The upgrade will enhance the time domain accessible for time-of-flight neutron measurements as well as improve the resolution in the DANCE barium fluoride crystals for photons.

  3. Reducing 68Ge Background in Dark Matter Experiments

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Orrell, John L.

    2011-03-01

    Experimental searches for dark matter include experiments with sub-0.5 keV-energy threshold high purity germanium detectors. Experimental efforts, in partnership with the CoGeNT Collaboration operating at the Soudan Underground Laboratory, are focusing on energy threshold reduction via noise abatement, reduction of backgrounds from cosmic ray generated isotopes, and ubiquitous environmental radioactive sources. The most significant cosmic ray produced radionuclide is 68Ge. This paper evaluates reducing this background by freshly mining and processing germanium ore. The most probable outcome is a reduction of the background by a factor of two, and at most a factor of four. A very cost effective alternative is to obtain processed Ge as soon as possible and store it underground for 18 months.

  4. A dark matter search with MALBEK

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Giovanetti, G. K.; Abgrall, N.; Aguayo, E.; Avignone, III, F. T.; Barabash, A. S.; Bertrand, F. E.; Boswell, M.; Brudanin, V.; Busch, M.; Byram, D.; et al

    2015-01-01

    The Majorana Demonstrator is an array of natural and enriched high purity germanium detectors that will search for the neutrinoless double-beta decay of ⁷⁶Ge and perform a search for weakly interacting massive particles (WIMPs) with masses below 10 GeV. As part of the Majorana research and development efforts, we have deployed a modified, low-background broad energy germanium detector at the Kimballton Underground Research Facility. With its sub-keV energy threshold, this detector is sensitive to potential non-Standard Model physics, including interactions with WIMPs. We discuss the backgrounds present in the WIMP region of interest and explore the impact of slow surfacemore »event contamination when searching for a WIMP signal.« less

  5. Low background counting techniques at SNOLAB

    SciTech Connect (OSTI)

    Lawson, Ian; Cleveland, Bruce [SNOLAB, 1039 Regional Rd 24, Lively, ON P3Y 1N2 (Canada)] [SNOLAB, 1039 Regional Rd 24, Lively, ON P3Y 1N2 (Canada)

    2013-08-08

    Many of the experiments currently searching for dark matter, studying properties of neutrinos or searching for neutrinoless double beta decay require very low levels of radioactive backgrounds both in their own construction materials and in the surrounding environment. These low background levels are required so that the experiments can achieve the required sensitivities for their searches. SNOLAB has several facilities which are used to directly measure these radioactive backgrounds. This proceedings will describe SNOLAB's High Purity Germanium Detectors, one of which has been in continuous use for the past seven years measuring materials for many experiments in operation or under construction at SNOLAB. A description of the characterisation of SNOLAB's new germanium well detector will be presented. In addition, brief descriptions of SNOLAB's alpha-beta and electrostatic counters will be presented and a description of SNOLAB's future low background counting laboratory will be given.

  6. The MAJORANA DEMONSTRATOR for 0???: Current status and future plans

    SciTech Connect (OSTI)

    Green, M. P. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Abgrall, N. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Aguayo, E. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Avignone, III, F. T. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Univ. of South Carolina, Columbia, SC (United States); Barabash, A. S. [Institute for Theoretical and Experimental Physics, Moscow (Russia); Bertrand, F. E. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Boswell, M. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Brudanin, V. [Joint Institute for Nuclear Research, Dubna (Russia); Busch, M. [Duke Univ., Durham, NC (United States); Triange Univ. Nuclear Lab., Durham, NC (United States); Byram, D. [Univ. of South Dakota, Vermillion, SD (United States); Caldwell, A. S. [South Dakota School of Mines and Technology, Rapid CIty, SD (United States); Chan, Y. -D. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Christofferson, C. D. [South Dakota School of Mines and Technology, Rapid CIty, SD (United States); Combs, D. C. [North Carolina State Univ., Raleigh, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Cuesta, C. [Univ. of Washington, Seattle, WA (United States); Detwiler, J. A. [Univ. of Washington, Seattle, WA (United States); Doe, P. J. [Univ. of Washington, Seattle, WA (United States); Efremenko, Yu. [Univ. of Tennessee, Knoxville, TN (United States); Egorov, V. [Joint Institute for Nuclear Research, Dubna (Russia); Ejiri, H. [Osaka Univ., Osaka (Japan); Elliott, S. R. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Fast, J. E. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Finnerty, P. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Fraenkle, F. M. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Galindo-Uribarri, A. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Giovanetti, G. K. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Goett, J. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Gruszko, J. [Univ. of Washington, Seattle, WA (United States); Guiseppe, V. E. [Univ. of South Carolina, Columbia, SC (United States); Gusev, K. [Joint Institute for Nuclear Research, Dubna (Russia); Hallin, A. L. [Univ. of Alberta, Edmonton, AB (Canada); Hazama, R. [Osaka Univ., Osaka (Japan); Hegai, A. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); North Carolina State Univ., Raleigh, NC (United States); Henning, R. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Hoppe, E. W. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Howard, S. [South Dakota School of Mines and Technology, Rapid CIty, SD (United States); Howe, M. A. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Keeter, K. J. [Black Hills State Univ., Spearfish, SD (United States); Kidd, M. F. [Tennessee Tech Univ., Cookeville, TN (United States); Kochetov, O. [Joint Institute for Nuclear Research, Dubna (Russia); Konovalov, S. I. [Institute for Theoretical and Experimental Physics, Moscow (Russia); Kouzes, R. T. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); LaFerriere, B. D. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Leon, J. [Univ. of Washington, Seattle, WA (United States); Leviner, L. E. [North Carolina State Univ., Raleigh, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Loach, J. C. [Shanghai Jiao Tong Univ., Shanghai (China); MacMullin, J. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); MacMullin, S. [Univ. of North Carolina, Chapel Hill, NC (United States)

    2015-01-01

    The Majorana Demonstrator will search for neutrinoless-double-beta decay (0???) in 76Ge, while establishing the feasibility of a future tonne-scale germanium-based 0??? experiment, and performing searches for new physics beyond the Standard Model. The experiment, currently under construction at the Sanford Underground Research Facility in Lead, SD, will consist of a pair of modular high-purity germanium detector arrays housed inside of a compact copper, lead, and polyethylene shield. Through a combination of strict materials qualifications and assay, low-background design, and powerful background rejection techniques, the Demonstrator aims to achieve a background rate in the 0??? region of interest (ROI) of no more than 3 counts in the 0???-decay ROI per tonne of target isotope per year (cnts/(ROI-t-y)). The current status of the Demonstrator is discussed, as are plans for its completion.

  7. A dark matter search with MALBEK

    SciTech Connect (OSTI)

    Giovanetti, G. K. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Abgrall, N. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Aguayo, E. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Avignone, III, F. T. [Univ. of South Carolina, Columbia, SC (United States); Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Barabash, A. S. [Institute for Theoretical and Experimental Physics, Moscow (Russia); Bertrand, F. E. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Boswell, M. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Brudanin, V. [Joint Institute for Nuclear Research, Dubna (Russia); Busch, M. [Duke Univ., Durham, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Byram, D. [Univ. of South Dakota, Vermillion, SD (United States); Caldwell, A. S. [South Dakota School of Mines and Technology, Rapid City, SD (United States); Chan, Y. -D. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Christofferson, C. D. [South Dakota School of Mines and Technology, Rapid City, SD (United States); Combs, D. C. [North Carolina State Univ., Raleigh, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Cuesta, C. [Univ. of Washington, Seattle, WA (United States); Detwiler, J. A. [Univ. of Washington, Seattle, WA (United States); Doe, P. J. [Univ. of Washington, Seattle, WA (United States); Efremenko, Yu. [Univ. of Tennessee, Knoxville, TN (United States); Egorov, V. [Joint Institute for Nuclear Research, Dubna (Russia); Ejiri, H. [Osaka Univ., Osaka (Japan); Elliott, S. R. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Fast, J. E. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Finnerty, P. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Fraenkle, F. M. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Galindo-Uribarri, A. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Goett, J. [Los Alamos National Lab. (LANL), Los Alamos, NM (United States); Green, M. P. [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Gruszko, J. [Univ. of Washington, Seattle, WA (United States); Guiseppe, V. E. [Univ. of South Carolina, Columbia, SC (United States); Gusev, K. [Joint Institute for Nuclear Research, Dubna (Russia); Hallin, A. L. [Univ. of Alberta, Edmonton, AB (Canada); Hazama, R. [Osaka Univ., Osaka (Japan); Hegai, A. [Lawrence Berkeley National Lab. (LBNL), Berkeley, CA (United States); Tuebingen Univ., Tuebingen (Germany); Henning, R. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Hoppe, E. W. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Howard, S. [South Dakota School of Mines and Technology, Rapid City, SD (United States); Howe, M. A. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Keeter, K. J. [Black Hills State Univ., Spearfish, SD (United States); Kidd, M. F. [Tennessee Tech Univ., Cookeville, TN (United States); Kochetov, O. [Joint Institute for Nuclear Research, Dubna (Russia); Konovalov, S. I. [Institute for Theoretical and Experimental Physics, Moscow (Russia); Kouzes, R. T. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); LaFerriere, B. D. [Pacific Northwest National Lab. (PNNL), Richland, WA (United States); Leon, J. [Univ. of Washington, Seattle, WA (United States); Leviner, L. E. [North Carolina State Univ., Raleigh, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); Loach, J. C. [Shanghai Jiao Tong Univ., Shanghai (China); MacMullin, J. [Univ. of North Carolina, Chapel Hill, NC (United States); Triangle Univ. Nuclear Lab., Durham, NC (United States); MacMullin, S. [Univ. of North Carolina, Chapel Hill, NC (United States)

    2015-01-01

    The Majorana Demonstrator is an array of natural and enriched high purity germanium detectors that will search for the neutrinoless double-beta decay of ??Ge and perform a search for weakly interacting massive particles (WIMPs) with masses below 10 GeV. As part of the Majorana research and development efforts, we have deployed a modified, low-background broad energy germanium detector at the Kimballton Underground Research Facility. With its sub-keV energy threshold, this detector is sensitive to potential non-Standard Model physics, including interactions with WIMPs. We discuss the backgrounds present in the WIMP region of interest and explore the impact of slow surface event contamination when searching for a WIMP signal.

  8. The Majorana Demonstrator for 0vBB: Current Status and Future Plans

    SciTech Connect (OSTI)

    Green, Matthew P; Avignone, F. T.; Galindo-Uribarri, Alfredo {nmn}; Radford, David C; Romero-Romero, Elisa; Varner Jr, Robert L; White, Brandon R; Wilkerson, J. F.; Majorana,

    2015-01-01

    The Majorana Demonstrator will search for neutrinoless-double-beta decay (0 ) in 76Ge, while establishing the feasibility of a future tonne-scale germanium-based 0 experiment, and performing searches for new physics beyond the Standard Model. The experiment, currently under construction at the Sanford Underground Research Facility in Lead, SD, will consist of a pair of modular high-purity germanium detector arrays housed inside of a compact copper, lead, and polyethylene shield. Through a combination of strict materials qualifications and assay, low-background design, and powerful background rejection techniques, the Demonstrator aims to achieve a background rate in the 0 region of interest (ROI) of no more than 3cnts/(ROI-t-y). The current status of the Demonstrator is discussed, as are plans for its completion.

  9. Activation Layer Stabilization of High Polarization Photocathodes in Sub-Optimal RF Gun Environments

    SciTech Connect (OSTI)

    Gregory A. Mulhollan

    2010-11-16

    Specific activation recipes for bulk, 100 nm thick MBE grown and high polarization III-V photocathode material have been developed which mitigate the effects of exposure to background gasses. Lifetime data using four representative gasses were acquired for bulk GaAs, 100 nm unstrained GaAs and strained superlattice GaAs/GaAsP, all activated both with Cs and then Cs and Li (bi-alkali). Each photoemitter showed marked resilience improvement when activated using the bi-alkali recipe compared to the standard single alkali recipe. A dual alkali activation system at SLAC was constructed, baked and commissioned with the purpose of performing spin-polarization measurements on electrons emitted from the bi-alkali activated surfaces. An end station at SSRL was configured with the required sources for energy resolved photoemission measurements on the bi-alkali activated and CO2 dosed surfaces. The bi-alkali recipes were successfully implemented at SLAC/SSRL. Measurements at SLAC of the photoelectron spin-polarization from the modified activation surface showed no sign of a change in value compared to the standard activated material, i.e., no ill effects. Analysis of photoemission data indicates that the addition of Li to the activation layer results in a multi-layer structure. The presence of Li in the activation layer also acts as an inhibitor to CO2 absorption, hence better lifetimes in worse vacuum were achieved. The bi-alkali activation has been tested on O2 activated GaAs for comparison with NF3 activated surfaces. Comparable resilience to CO2 exposure was achieved for the O2 activated surface. An RF PECVD amorphous silicon growth system was modified to allow high temperature heat cleaning of GaAs substrates prior to film deposition. Growth versus thickness data were collected. Very thin amorphous silicon germanium layers were optimized to exhibit good behavior as an electron emitter. Growth of the amorphous silicon germanium films on the above substrates was fine tuned with respect to time and power to moderate plasma damage to the photo-generating layer. Auger electron spectroscopy was used to analyze the composition and thickness of the emitter layers. AFM studies showed conformal growth on the GaAs substrates. Measurements at SLAC on the photoemitted electrons from high polarization substrates coated with amorphous silicon germanium indicated an ~10% relative drop in spin-polarization at the wavelength corresponding to the maximum spin-polarization when compared to the uncoated material,

  10. Majorana Electroformed Copper Mechanical Analysis

    SciTech Connect (OSTI)

    Overman, Nicole R.; Overman, Cory T.; Kafentzis, Tyler A.; Edwards, Danny J.; Hoppe, Eric W.

    2012-04-30

    The MAJORANA DEMONSTRATOR is a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay. The DEMONSTRATOR will utilize ultra high purity electroformed copper for a variety of detector components and shielding. A preliminary mechanical evaluation was performed on the Majorana prototype electroformed copper material. Several samples were removed from a variety of positions on the mandrel. Tensile testing, optical metallography, scanning electron microscopy, and hardness testing were conducted to evaluate mechanical response. Analyses carried out on the Majorana prototype copper to this point show consistent mechanical response from a variety of test locations. Evaluation shows the copper meets or exceeds the design specifications.

  11. Reproducibility of High-Q SRF Cavities by High Temperature Heat Treatment

    SciTech Connect (OSTI)

    Dhakal, Pashupati; Ciovati, Gianluigi; Kneisel, Peter; Myneni, Ganapati Rao

    2014-07-01

    Recent work on high-temperature (> 600 °C) heat treatment of ingot Nb cavities in a customized vacuum furnace for several hours showed the possibility of achieving Q0-values of up to ~5×1010 at 2.0 K, 1.5 GHz and accelerating gradients of ~20 MV/m. This contribution presents results on further studies of the heat treatment process to produce cavities with high Q0 values for continuous-wave accelerator application. Single-cell cavities of different Nb purity have been processed through few cycles of heat-treatments and chemical etching. Measurements of Q0 as a function of temperature at low RF field and of Q0 as a function of the RF field at or below 2.0 K have been made after each treatment. Measurements by TOF-SIMS of the impurities’ depth profiles were made on samples heat treated with the cavities.

  12. High specific activity silicon-32

    DOE Patents [OSTI]

    Phillips, D.R.; Brzezinski, M.A.

    1996-06-11

    A process for preparation of silicon-32 is provided and includes contacting an irradiated potassium chloride target, including spallation products from a prior irradiation, with sufficient water, hydrochloric acid or potassium hydroxide to form a solution, filtering the solution, adjusting pH of the solution from about 5.5 to about 7.5, admixing sufficient molybdate-reagent to the solution to adjust the pH of the solution to about 1.5 and to form a silicon-molybdate complex, contacting the solution including the silicon-molybdate complex with a dextran-based material, washing the dextran-based material to remove residual contaminants such as sodium-22, separating the silicon-molybdate complex from the dextran-based material as another solution, adding sufficient hydrochloric acid and hydrogen peroxide to the solution to prevent reformation of the silicon-molybdate complex and to yield an oxidation state of the molybdate adapted for subsequent separation by an anion exchange material, contacting the solution with an anion exchange material whereby the molybdate is retained by the anion exchange material and the silicon remains in solution, and optionally adding sufficient alkali metal hydroxide to adjust the pH of the solution to about 12 to 13. Additionally, a high specific activity silicon-32 product having a high purity is provided.

  13. High specific activity silicon-32

    DOE Patents [OSTI]

    Phillips, Dennis R. (Los Alamos, NM); Brzezinski, Mark A. (Santa Barbara, CA)

    1996-01-01

    A process for preparation of silicon-32 is provided and includes contacting an irradiated potassium chloride target, including spallation products from a prior irradiation, with sufficient water, hydrochloric acid or potassium hydroxide to form a solution, filtering the solution, adjusting pH of the solution to from about 5.5 to about 7.5, admixing sufficient molybdate-reagent to the solution to adjust the pH of the solution to about 1.5 and to form a silicon-molybdate complex, contacting the solution including the silicon-molybdate complex with a dextran-based material, washing the dextran-based material to remove residual contaminants such as sodium-22, separating the silicon-molybdate complex from the dextran-based material as another solution, adding sufficient hydrochloric acid and hydrogen peroxide to the solution to prevent reformation of the silicon-molybdate complex and to yield an oxidization state of the molybdate adapted for subsequent separation by an anion exchange material, contacting the solution with an anion exchange material whereby the molybdate is retained by the anion exchange material and the silicon remains in solution, and optionally adding sufficient alkali metal hydroxide to adjust the pH of the solution to about 12 to 13. Additionally, a high specific activity silicon-32 product having a high purity is provided.

  14. Conceptual design of a high throughput electrorefining of a uranium by using graphite cathode

    SciTech Connect (OSTI)

    Lee, J.H.; Kang, Y.H.; Hwang, S.C.; Park, S.B.; Shim, J.B.; Lee, H.S.; Kim, E.H.; Park, S.W.

    2007-07-01

    Conceptual designing of a high throughput electro-refiner was performed by using basic experimental data and a commercial computational fluid dynamic code, CFX. An electro-refiner concept equipped with a graphite cathode bundle was designed to recover a high purity uranium product continuously without a noble metal contamination. The performance of the process for a decontamination of a noble metal in a uranium product was evaluated as a function of the process parameters such as the rotation speeds of the stirrer and the anode basket. (authors)

  15. High temperature support apparatus and method of use for casting materials

    DOE Patents [OSTI]

    Clark, Roger F; Cliber, James A; Stoddard, Nathan G; Gerber, Jesse I; Roberts, Raymond J; Wilmerton, Mark A

    2015-02-10

    This invention relates to a system and a method of use for large ceramic member support and manipulation at elevated temperatures in non-oxidizing atmospheres, such as using carbon-carbon composite materials for producing high purity silicon in the manufacture of solar modules. The high temperature apparatus of this invention includes one or more support ribs, one or more cross braces in combination with the one or more support ribs, and a shaped support liner positionable upon the one or more support ribs and the one or more cross braces.

  16. High-efficiency solar cell and method for fabrication

    DOE Patents [OSTI]

    Hou, H.Q.; Reinhardt, K.C.

    1999-08-31

    A high-efficiency 3- or 4-junction solar cell is disclosed with a theoretical AM0 energy conversion efficiency of about 40%. The solar cell includes p-n junctions formed from indium gallium arsenide nitride (InGaAsN), gallium arsenide (GaAs) and indium gallium aluminum phosphide (InGaAlP) separated by n-p tunnel junctions. An optional germanium (Ge) p-n junction can be formed in the substrate upon which the other p-n junctions are grown. The bandgap energies for each p-n junction are tailored to provide substantially equal short-circuit currents for each p-n junction, thereby eliminating current bottlenecks and improving the overall energy conversion efficiency of the solar cell. Additionally, the use of an InGaAsN p-n junction overcomes super-bandgap energy losses that are present in conventional multi-junction solar cells. A method is also disclosed for fabricating the high-efficiency 3- or 4-junction solar cell by metal-organic chemical vapor deposition (MOCVD). 4 figs.

  17. High-efficiency solar cell and method for fabrication

    DOE Patents [OSTI]

    Hou, Hong Q.; Reinhardt, Kitt C.

    1999-01-01

    A high-efficiency 3- or 4-junction solar cell is disclosed with a theoretical AM0 energy conversion efficiency of about 40%. The solar cell includes p-n junctions formed from indium gallium arsenide nitride (InGaAsN), gallium arsenide (GaAs) and indium gallium aluminum phosphide (InGaAlP) separated by n-p tunnel junctions. An optional germanium (Ge) p-n junction can be formed in the substrate upon which the other p-n junctions are grown. The bandgap energies for each p-n junction are tailored to provide substantially equal short-circuit currents for each p-n junction, thereby eliminating current bottlenecks and improving the overall energy conversion efficiency of the solar cell. Additionally, the use of an InGaAsN p-n junction overcomes super-bandgap energy losses that are present in conventional multi-junction solar cells. A method is also disclosed for fabricating the high-efficiency 3- or 4-junction solar cell by metal-organic chemical vapor deposition (MOCVD).

  18. Complex crystallization dynamics in amorphous germanium observed...

    Office of Scientific and Technical Information (OSTI)

    Date: 2013-02-01 OSTI Identifier: 1102279 Type: Publisher's Accepted Manuscript Journal Name: Physical Review B Additional Journal Information: Journal Volume: 87; Journal...

  19. Assessing the benefits of OHER (Office of Health and Environmental Research) research: Three case studies

    SciTech Connect (OSTI)

    Nesse, R.J.; Callaway, J.M.; Englin, J.E.; Klan, M.S.; Nicholls, A.K.; Serot, D.E.

    1987-09-01

    This research was undertaken to estimate the societal benefits and costs of selected past research performed for the Office of Health and Environmental Research (OHER) of the US Department of Energy (DOE). Three case studies of representative OHER and DOE research were performed. One of these, the acid rain case study, includes research conducted elsewhere in DOE. The other two cases were the OHER marine research program and the development of high-purity germanium that is used in radiation detectors. The acid rain case study looked at the research benefits and costs of furnace sorbent injection and duct injection, technologies that might reduce acid deposition precursors. Both appear to show benefits in excess of costs. We examined in detail one of the OHER marine research program's accomplishments - the increase in environmental information used by the Outer Continental Shelf leasing program to manage bidding for off-shore oil drilling. The results of an econometric model show that environmental information of the type supported by OHER is unequivocally linked to government and industry leasing decisions. The germanium case study indicated that the benefits of germanium radiation detectors were significant.

  20. Mechanisms of stress corrosion cracking for iron-based alloys in high-temperature water

    SciTech Connect (OSTI)

    Zhou, X.Y.; Congleton, J.; Bahraloloom, A.

    1998-11-01

    Stress corrosion cracking (SCC) susceptibilities of a series of iron-based alloys (IBA), including some high-purity irons, were evaluated in lithiated water at temperatures up to 300 C. Inclusion distributions in each material were established using quantitative metallography and energy dispersive x-ray analysis (EDX). Electrochemical measurements were performed to investigate film formation kinetics. Results showed the minimum potential for SCC was a function of the inclusion content. Reducing the inclusion content in IBA moved the minimum potential for SCC in the anodic direction and/or increased the temperature for the onset of cracking but did not eliminate SCC.

  1. Production of high specific activity silicon-32

    DOE Patents [OSTI]

    Phillips, Dennis R. (Los Alamos, NM); Brzezinski, Mark A. (Santa Barbara, CA)

    1994-01-01

    A process for preparation of silicon-32 is provide and includes contacting an irradiated potassium chloride target, including spallation products from a prior irradiation, with sufficient water, hydrochloric acid or potassium hydroxide to form a solution, filtering the solution, adjusting pH of the solution to from about 5.5 to about 7.5, admixing sufficient molybdate-reagent to the solution to adjust the pH of the solution to about 1.5 and to form a silicon-molybdate complex, contacting the solution including the silicon-molybdate complex with a dextran-based material, washing the dextran-based material to remove residual contaminants such as sodium-22, separating the silicon-molybdate complex from the dextran-based material as another solution, adding sufficient hydrochloric acid and hydrogen peroxide to the solution to prevent reformation of the silicon-molybdate complex and to yield an oxidization state of the molybdate adapted for subsequent separation by an anion exchange material, contacting the solution with an anion exchange material whereby the molybdate is retained by the anion exchange material and the silicon remains in solution, and optionally adding sufficient alkali metal hydroxide to adjust the pH of the solution to about 12 to 13. Additionally, a high specific activity silicon-32 product having a high purity is provided.

  2. Grain boundary depletion and migration during selective oxidation of Cr in a Ni-5Cr binary alloy exposed to high-temperature hydrogenated water

    SciTech Connect (OSTI)

    Schreiber, Daniel K.; Olszta, Matthew J.; Bruemmer, Stephen M.

    2014-10-01

    High-resolution microscopy of a high-purity Ni-5Cr alloy exposed to 360C hydrogenated water reveals intergranular selective oxidation of Cr accompanied by local Cr depletion and diffusion-induced grain boundary migration (DIGM). The corrosion-product oxide consists of a porous, interconnected network of Cr2O3 platelets with no further O ingress into the metal ahead. Extensive grain boundary depletion of Cr (to <0.05at.%) is observed typically 20100 nm wide as a result of DIGM and reaching depths of many micrometers beyond the oxidation front.

  3. Recent Observation of Hydrogen-Induced Cracking of High-Strength Steels

    SciTech Connect (OSTI)

    McMahon, Jr, C J; Liu, Xinyu; Kameda, Jun; Morgan, Michael J

    2008-09-14

    The present progress report shows that the ultra-high-strength 4340-type steel, even if ideally pure, cannot safely be used for service in a hydrogen environment. Some of the strength must be given up in favor of more toughness, which can be achieved by reducing the carbon content and increasing the nickel content. The 5%NiCrMoV steel with about 0.1% carbon shows promise in this regard, especially in an aqueous environment and in hydrogen at around atmospheric pressure. However, we have not yet achieved a purity level high enough to establish the baseline behavior of an ideally pure version of this steel in high-pressure hydrogen.

  4. High speed, multi-channel, user programmable digital data acquisition system.

    SciTech Connect (OSTI)

    Sabourov, Konstantin; Hennig, Wolfgang; Walby, Mark

    2013-11-18

    As applications for radiation detection become more demanding, and in turn improvements are made in the technology of radiation detection, there is a need for high speed digital detector readout electronics matching these improvements. Specifically, full control over the on-line processing resources of modern digital electronics is desirable so that researchers can develop custom algorithms for special applications.In the proposed effort, the 500 MHz digital readout electronics previously developed by our company will be redesigned to allow user access to the on-line processing resources. In Phase I, the division of online processing into vendor and user firmware sections has been studied on existing hardware. In Phase II, the hardware will be upgraded to better facilitate the division, and the firmware will be restructured into a robust vendor logic block (providing standard functions such as host I/O, on-board memory I/O, energy computation, MCA spectra, timestamps, waveform capture, run statistics, and triggering and timing) and a user logic block for custom algorithms (with templates and examples for frequently used functions). Investigating several options to divide online processing, it was determined that the most promising approach is to partition a single FPGA integrated circuit into a vendor and user section, which is supported in newer devices. The analog front end of the existing electronics proved suitable for most applications, in particular high rate measurements with germanium detectors. The design architecture for new electronics was developed, combining one of the new FPGA device with the analog front end.

  5. Guiding of low-energy electrons by highly ordered Al{sub 2}O{sub 3} nanocapillaries

    SciTech Connect (OSTI)

    Milosavljevic, A. R.; Vikor, Gy.; Pesic, Z. D.; Kolarz, P.; Sevic, D.; Marinkovic, B. P.; Matefi-Tempfli, S.; Matefi-Tempfli, M.; Piraux, L.

    2007-03-15

    We report an experimental study of guided transmission of low-energy (200-350 eV) electrons through highly ordered Al{sub 2}O{sub 3} nanocapillaries with large aspect ratio (140 nm diameter and 15 {mu}m length). The nanochannel array was prepared using self-ordering phenomena during a two-step anodization process of a high-purity aluminum foil. The experimental results clearly show the existence of the guiding effect, as found for highly charged ions. The guiding of the electron beam was observed for tilt angles up to 12 degree sign . As seen for highly charged ions, the guiding efficiency increases with decreasing electron incident energy. The transmission efficiency appeared to be significantly lower than observed for highly charged ions and, moreover, the intensity of transmitted electrons significantly decreases with decreasing impact energy.

  6. High PRF high current switch

    DOE Patents [OSTI]

    Moran, Stuart L. (Fredericksburg, VA); Hutcherson, R. Kenneth (College Park, MD)

    1990-03-27

    A triggerable, high voltage, high current, spark gap switch for use in pu power systems. The device comprises a pair of electrodes in a high pressure hydrogen environment that is triggered by introducing an arc between one electrode and a trigger pin. Unusually high repetition rates may be obtained by undervolting the switch, i.e., operating the trigger at voltages much below the self-breakdown voltage of the device.

  7. Testing the Ge detectors for the MAJORANA DEMONSTRATOR

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Xu, W.; Abgrall, N.; Aguayo, E.; Avignone, F. T.; Barabash, A. S.; Bertrand, F. E.; Boswell, M.; Brudanin, V.; Busch, M.; Byram, D.; et al

    2015-03-24

    High purity germanium (HPGe) crystals will be used for the MAJORANA DEMONSTRATOR, where they serve as both the source and the detector for neutrinoless double beta decay. It is crucial for the experiment to understand the performance of the HPGe crystals. A variety of crystal properties are being investigated, including basic properties such as energy resolution, efficiency, uniformity, capacitance, leakage current and crystal axis orientation, as well as more sophisticated properties, e.g. pulse shapes and dead layer and transition layer distributions. In this talk, we will present our measurements that characterize the HPGe crystals. We will also discuss the ourmore » simulation package for the detector characterization setup, and show that additional information can be extracted from data-simulation comparisons.« less

  8. Low Background Counting At SNOLAB

    SciTech Connect (OSTI)

    Lawson, Ian; Cleveland, Bruce [SNOLAB, 1039 Regional Rd 24, Lively, ON P3Y 1N2 (Canada)

    2011-04-27

    It is a continuous and ongoing effort to maintain radioactivity in materials and in the environment surrounding most underground experiments at very low levels. These low levels are required so that experiments can achieve the required detection sensitivities for the detection of low-energy neutrinos, searches for dark matter and neutrinoless double-beta decay. SNOLAB has several facilities which are used to determine these low background levels in the materials and the underground environment. This proceedings will describe the SNOLAB High Purity Germanium Detector which has been in continuous use for the past five years and give results of many of the items that have been counted over that period. Brief descriptions of SNOLAB's alpha-beta and electrostatic counters will be given, and the radon levels at SNOLAB will be discussed.

  9. Testing the Ge detectors for the MAJORANA DEMONSTRATOR

    SciTech Connect (OSTI)

    Xu, W.; Abgrall, N.; Aguayo, E.; Avignone, F. T.; Barabash, A. S.; Bertrand, F. E.; Boswell, M.; Brudanin, V.; Busch, M.; Byram, D.; Caldwell, A. S.; Chan, Y. -D.; Christofferson, C. D.; Combs, D. C.; Cuesta, C.; Detwiler, J. A.; Doe, P. J.; Efremenko, Yu.; Egorov, V.; Ejiri, H.; Elliott, S. R.; Fast, J. E.; Finnerty, P.; Fraenkle, F. M.; Galindo-Uribarri, A.; Giovanetti, G. K.; Goett, J.; Green, M. P.; Gruszko, J.; Guiseppe, V. E.; Gusev, K.; Hallin, A. L.; Hazama, R.; Hegai, A.; Henning, R.; Hoppe, E. W.; Howard, S.; Howe, M. A.; Keeter, K. J.; Kidd, M. F.; Kochetov, O.; Konovalov, S. I.; Kouzes, R. T.; LaFerriere, B. D.; Leon, J.; Leviner, L. E.; Loach, J. C.; MacMullin, J.; MacMullin, S.; Martin, R. D.; Meijer, S.; Mertens, S.; Nomachi, M.; Orrell, J. L.; O'Shaughnessy, C.; Overman, N. R.; Phillips, D. G.; Poon, A. W.P.; Pushkin, K.; Radford, D. C.; Rager, J.; Rielage, K.; Robertson, R. G.H.; Romero-Romero, E.; Ronquest, M. C.; Schubert, A. G.; Shanks, B.; Shima, T.; Shirchenko, M.; Snavely, K. J.; Snyder, N.; Suriano, A. M.; Thompson, J.; Timkin, V.; Tornow, W.; Trimble, J. E.; Varner, R. L.; Vasilyev, S.; Vetter, K.; Vorren, K.; White, B. R.; Wilkerson, J. F.; Wiseman, C.; Yakushev, E.; Young, A. R.; Yu, C. -H.; Yumatov, V.

    2015-03-24

    High purity germanium (HPGe) crystals will be used for the MAJORANA DEMONSTRATOR, where they serve as both the source and the detector for neutrinoless double beta decay. It is crucial for the experiment to understand the performance of the HPGe crystals. A variety of crystal properties are being investigated, including basic properties such as energy resolution, efficiency, uniformity, capacitance, leakage current and crystal axis orientation, as well as more sophisticated properties, e.g. pulse shapes and dead layer and transition layer distributions. In this talk, we will present our measurements that characterize the HPGe crystals. We will also discuss the our simulation package for the detector characterization setup, and show that additional information can be extracted from data-simulation comparisons.

  10. Construction and Testing of a Low-power Cryostat for MARS

    SciTech Connect (OSTI)

    Aalseth, Craig E.; Caggiano, Joseph A.; Day, Anthony R.; Fast, James E.; Fuller, Erin S.

    2007-10-01

    A low-power cryostat was designed and built for the Multi-sensor Airborne Radiation Survey (MARS) project for the purpose of housing a close-packed high-purity germanium (HPGe) detector array of 14 HPGe detectors. The power consumption of the cold mass in the cryostat was measured to be 4.07(11) watts, sufficient for 5.5 days of continuous operation using only 8 liters of liquid nitrogen. Temperatures throughout the cryostat were measured by platinum resistance temperature detectors. These measurements were used to determine the emissivity of the copper used in the floating radiation shield and outer cryostat wall, which was constructed using chemically cleaned and passivated copper metal. Using a PNNL-developed passivation process, an emissivity of 2.5(3)% was achieved for copper.

  11. Ion-induced gamma-ray detection of fast ions escaping from fusion plasmas

    SciTech Connect (OSTI)

    Nishiura, M. Mushiake, T.; Doi, K.; Wada, M.; Taniike, A.; Matsuki, T.; Shimazoe, K.; Yoshino, M.; Nagasaka, T.; Tanaka, T.; Kisaki, M.; Fujimoto, Y.; Fujioka, K.; Yamaoka, H.; Matsumoto, Y.

    2014-11-15

    A 12 12 pixel detector has been developed and used in a laboratory experiment for lost fast-ion diagnostics. With gamma rays in the MeV range originating from nuclear reactions {sup 9}Be(?, n?){sup 12}C, {sup 9}Be(d, n?){sup 12}C, and {sup 12}C(d, p?){sup 13}C, a high purity germanium (HPGe) detector measured a fine-energy-resolved spectrum of gamma rays. The HPGe detector enables the survey of background-gamma rays and Doppler-shifted photo peak shapes. In the experiments, the pixel detector produces a gamma-ray image reconstructed from the energy spectrum obtained from total photon counts of irradiation passing through the detector's lead collimator. From gamma-ray image, diagnostics are able to produce an analysis of the fast ion loss onto the first wall in principle.

  12. In situ determination of /sup 241/Am on Enewetak Atoll. Date of survey: July 1977-December 1979

    SciTech Connect (OSTI)

    Tipton, W.J.; Fritzsche, A.E.; Jaffe, R.J.; Villaire, A.E.

    1981-11-01

    An in situ gamma ray spectrometer system was operated at Enewetak Atoll from July 1977 to December 1979 in support of the Enewetak Cleanup Project. The system employed a high purity germanium planar detector suspended at a height of 7.4 m above ground. Conversion factors were established to relate measured photopeak count rate data to source concentration in the soil. Data obtained for /sup 241/Am, together with plutonium-to-americium ratios obtained from soil sample analyses, were used to establish area-averaged surface (0 to 3 cm) transuranic concentration values. In areas which exceeded cleanup criteria, measurements were made in an iterative fashion to guide soil removal until levels were reduced below the cleanup criteria. Final measurements made after soil removal had been completed were used to document remaining surface transuranic concentration values and to establish external exposure rate levels due to /sup 137/Cs and /sup 60/Co.

  13. Diamond detector for high rate monitors of fast neutrons beams

    SciTech Connect (OSTI)

    Giacomelli, L.; Rebai, M.; Cippo, E. Perelli; Tardocchi, M.; Fazzi, A.; Andreani, C.; Pietropaolo, A.; Frost, C. D.; Rhodes, N.; Schooneveld, E.; Gorini, G.

    2012-06-19

    A fast neutron detection system suitable for high rate measurements is presented. The detector is based on a commercial high purity single crystal diamond (SDD) coupled to a fast digital data acquisition system. The detector was tested at the ISIS pulsed spallation neutron source. The SDD event signal was digitized at 1 GHz to reconstruct the deposited energy (pulse amplitude) and neutron arrival time; the event time of flight (ToF) was obtained relative to the recorded proton beam signal t{sub 0}. Fast acquisition is needed since the peak count rate is very high ({approx}800 kHz) due to the pulsed structure of the neutron beam. Measurements at ISIS indicate that three characteristics regions exist in the biparametric spectrum: i) background gamma events of low pulse amplitudes; ii) low pulse amplitude neutron events in the energy range E{sub dep}= 1.5-7 MeV ascribed to neutron elastic scattering on {sup 12}C; iii) large pulse amplitude neutron events with E{sub n} < 7 MeV ascribed to {sup 12}C(n,{alpha}){sup 9}Be and 12C(n,n')3{alpha}.

  14. Determination of TCAP (Thermal Cycling Absorption Process) Raffinate Purity

    Broader source: Energy.gov [DOE]

    Presentation from the 36th Tritium Focus Group Meeting held in Los Alamos, New Mexico, November 3-5, 2015.

  15. Carbohydrate markers of organism purity and growth environment

    SciTech Connect (OSTI)

    Wunschel, David S.; Fox, Alvin

    2012-01-01

    Recent experience with Bacillus spore characterization has demonstrated that carbohydrate content can provide potentially vital bioforensic information. Like other metabolites, the carbohydrate profiles of samples reflect variations in cellular structures as well as presence of residual carbohydrates from the medium found as trace components. The presence and characteristics of residual carbohydrates, such as agar, represent strong indicators of culturing method. The methods to detect residual carbohydrates can be extended to other compounds used in processing and preservation of microbes in a dry form.

  16. Determination of uranium and thorium in semiconductor memory materials by high fluence neutron activation analysis

    SciTech Connect (OSTI)

    Dyer, F.F.; Emery, J.F.; Northcutt, K.J.; Scott, R.M.

    1981-01-01

    Uranium and thorium were measured by absolute neutron activation analysis in high-purity materials used to manufacture semiconductor memories. The main thrust of the study concerned aluminum and aluminum alloys used as sources for thin film preparation, evaporated metal films, and samples from the Czochralski silicon crystal process. Average levels of U and Th were found for the source alloys to be approx. 65 and approx. 45 ppB, respectively. Levels of U and Th in silicon samples fell in the range of a few parts per trillion. Evaporated metal films contained about 1 ppB U and Th, but there is some question about these results due to the possibility of contamination.

  17. Percolating porosity in ultrafine grained copper processed by High Pressure Torsion

    SciTech Connect (OSTI)

    Wegner, Matthias Leuthold, Jrn; Peterlechner, Martin; Divinski, Sergiy V. Wilde, Gerhard; Setman, Daria; Zehetbauer, Michael; Pippan, Reinhard

    2013-11-14

    Defect structures in copper of different purity (nominally 99.99 and 99.999?wt.?%) deformed via High Pressure Torsion (HPT) with varying processing parameters are investigated utilizing the radiotracer diffusion technique. While the degree of deformation is kept constant, the effects of applied quasi-hydrostatic pressure, processing temperature, post-deformation annealing treatments, and of the impurity concentration on the deformed samples are analyzed in terms of the formation of interconnected internal porosity. Furthermore, the anisotropy of the developing porosity network is examined. The porosity channels occurred to be interconnected along the direction parallel to the surface normal with a volume fraction of the order of a few ppm while no long-range penetration along the internal porosity could be detected when measured along the azimuthal or radial directions of a HPT processed sample.

  18. Hydrogen, lithium, and lithium hydride production

    DOE Patents [OSTI]

    Brown, Sam W; Spencer, Larry S; Phillips, Michael R; Powell, G. Louis; Campbell, Peggy J

    2014-03-25

    A method of producing high purity lithium metal is provided, where gaseous-phase lithium metal is extracted from lithium hydride and condensed to form solid high purity lithium metal. The high purity lithium metal may be hydrided to provide high purity lithium hydride.

  19. Lignol Innovations, Inc. Demonstration-Scale Biorefinery

    Broader source: Energy.gov [DOE]

    The Lignol Innovations, Inc., biorefinery will produce cellulosic ethanol, high purity lignin, and furfural from hardwoods.

  20. The MAJORANA DEMONSTRATOR for 0νββ: Current status and future plans

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Green, M. P.; Abgrall, N.; Aguayo, E.; Avignone, III, F. T.; Barabash, A. S.; Bertrand, F. E.; Boswell, M.; Brudanin, V.; Busch, M.; Byram, D.; et al

    2015-01-01

    The Majorana Demonstrator will search for neutrinoless-double-beta decay (0νββ) in 76Ge, while establishing the feasibility of a future tonne-scale germanium-based 0νββ experiment, and performing searches for new physics beyond the Standard Model. The experiment, currently under construction at the Sanford Underground Research Facility in Lead, SD, will consist of a pair of modular high-purity germanium detector arrays housed inside of a compact copper, lead, and polyethylene shield. Through a combination of strict materials qualifications and assay, low-background design, and powerful background rejection techniques, the Demonstrator aims to achieve a background rate in the 0νββ region of interest (ROI) of nomore » more than 3 counts in the 0νββ-decay ROI per tonne of target isotope per year (cnts/(ROI-t-y)). The current status of the Demonstrator is discussed, as are plans for its completion.« less

  1. NID Copper Sample Analysis

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Zhu, Zihua

    2011-02-01

    The current focal point of the nuclear physics program at PNNL is the MAJORANA DEMONSTRATOR, and the follow-on Tonne-Scale experiment, a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0???). This experiment requires the use of germanium isotopically enriched in 76Ge. The DEMONSTRATOR will utilize 76Ge from Russia, but for the Tonne-Scale experiment it is hoped that an alternate technology under development at Nonlinear Ion Dynamics (NID) will be a viable, US-based, lower-cost source of separated material. Samples of separated material from NID require analysis to determine the isotopic distribution and impurities. The MAJORANA DEMONSTRATOR is a DOE and NSF funded project with a major science impact. DOE is funding NID through an SBIR grant for development of their separation technology for application to the Tonne-Scale experiment. The Environmental Molecular Sciences facility (EMSL), a DOE user facility at PNNL, has the required mass spectroscopy instruments for making these isotopic measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR and for the development of the future separation technology required for the Tonne-Scale experiment. A sample of isotopically separated copper was provided by NID to PNNL for isotopic analysis as a test of the NID technology. The results of that analysis are reported here.

  2. Majorana Demonstrator Bolted Joint Mechanical and Thermal Analysis

    SciTech Connect (OSTI)

    Aguayo Navarrete, Estanislao; Reid, Douglas J.; Fast, James E.

    2012-06-01

    The MAJORANA DEMONSTRATOR is designed to probe for neutrinoless double-beta decay, an extremely rare process with a half-life in the order of 1026 years. The experiment uses an ultra-low background, high-purity germanium detector array. The germanium crystals are both the source and the detector in this experiment. Operating these crystals as ionizing radiation detectors requires having them under cryogenic conditions (below 90 K). A liquid nitrogen thermosyphon is used to extract the heat from the detectors. The detector channels are arranged in strings and thermally coupled to the thermosyphon through a cold plate. The cold plate is joined to the thermosyphon by a bolted joint. This circular plate is housed inside the cryostat can. This document provides a detailed study of the bolted joint that connects the cold plate and the thermosyphon. An analysis of the mechanical and thermal properties of this bolted joint is presented. The force applied to the joint is derived from the torque applied to each one of the six bolts that form the joint. The thermal conductivity of the joint is measured as a function of applied force. The required heat conductivity for a successful experiment is the combination of the thermal conductivity of the detector string and this joint. The thermal behavior of the joint is experimentally implemented and analyzed in this study.

  3. High-Efficiency Amorphous Silicon Alloy Based Solar Cells and Modules; Final Technical Progress Report, 30 May 2002--31 May 2005

    SciTech Connect (OSTI)

    Guha, S.; Yang, J.

    2005-10-01

    The principal objective of this R&D program is to expand, enhance, and accelerate knowledge and capabilities for development of high-efficiency hydrogenated amorphous silicon (a-Si:H) and amorphous silicon-germanium alloy (a-SiGe:H) related thin-film multijunction solar cells and modules with low manufacturing cost and high reliability. Our strategy has been to use the spectrum-splitting triple-junction structure, a-Si:H/a-SiGe:H/a-SiGe:H, to improve solar cell and module efficiency, stability, and throughput of production. The methodology used to achieve the objectives included: (1) explore the highest stable efficiency using the triple-junction structure deposited using RF glow discharge at a low rate, (2) fabricate the devices at a high deposition rate for high throughput and low cost, and (3) develop an optimized recipe using the R&D batch large-area reactor to help the design and optimization of the roll-to-roll production machines. For short-term goals, we have worked on the improvement of a-Si:H and a-SiGe:H alloy solar cells. a-Si:H and a-SiGe:H are the foundation of current a-Si:H based thin-film photovoltaic technology. Any improvement in cell efficiency, throughput, and cost reduction will immediately improve operation efficiency of our manufacturing plant, allowing us to further expand our production capacity.

  4. High e

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    e ne rgy data s am ple ● NuMI beam events provide an useful calibration sample ● Collected over 70K candidates before shutdown The highest energy events are prim arily from kaon decays. Two sam ples at high energy provide normalization and shape inform ation for kaon backgrounds to oscillation analysis: ● ν e events passing oscillation event selection cuts ● ν µ induced CCQE, CCπ+events Reconstructed neutrino energy EνQE(GeV) ν from other particles ν from pions ν from Kaons -

  5. Particle Release Experiment (PRex) Final Report

    SciTech Connect (OSTI)

    Keillor, Martin E.; Arrigo, Leah M.; Detwiler, Rebecca S.; Kernan, Warnick J.; Kirkham, Randy R.; MacDougall, Matthew R.; Chipman, Veraun D.; Milbrath, Brian D.; Rishel, Jeremy P.; Seifert, Allen; Seifert, Carolyn E.; Smart, John E.; Emer, Dudley

    2014-09-30

    An experiment to release radioactive particles representative of small-scale venting from an underground nuclear test was conducted to gather data in support of treaty verification and monitoring activities. For this experiment, a CO2-driven air cannon was used to release La-140 at ambient temperatures. Lanthanum-140 was chosen to represent the fission fragments because of its short half-life and prominent gamma-ray emissions; the choice was also influenced by the successful production and use of La-140 with low levels of radioactive contaminants in a Defence Research and Development Canada Field Trial. The source was created through activation of high-purity natural lanthanum oxide at the reactor of Washington State University, Pullman, Washington. Multiple varieties of witness plates and air samplers were laid in an irregular grid covering the area over which the plume was modeled to deposit. Aerial survey, a NaI(Tl) mobile spectrometer, and handheld and backpack instruments ranging from polyvinyl toluene to high-purity germanium were used to survey the plume. Additionally, three varieties of soil sampling were investigated. The relative sensitivity and utility of sampling and survey methods are discussed in the context of On-Site Inspection. The measurements and samples show a high degree of correlation and form a valuable set of test data.

  6. High-Performance Sorbents for Carbon Dioxide Capture from Air

    SciTech Connect (OSTI)

    Sholl, David; Jones, Christopher

    2013-03-13

    This project has focused on capture of CO{sub 2} from ambient air (air capture). If this process is technically and economically feasible, it could potentially contribute to net reduction of CO{sub 2} emissions in ways that are complementary to better developed techniques for CO{sub 2} from concentrated point sources. We focused on cyclic adsorption processes for CO{sub 2} capture from air in which the entire cycle is performed at moderate temperatures. The project involved both experimental studies of sorbent materials and process level modeling of cyclic air capture processes. In our experimental work, a series of amine-functionalized silica adsorbents were prepared and characterized to determine the impact of molecular architecture on CO{sub 2} capture. Some key findings were: Amine functionalized silicas can be prepared with high enough CO{sub 2} capacities under ambient conditions to merit consideration for use in air capture processes. Primary amines are better candidates for CO{sub 2} capture than secondary or tertiary amines, both in terms of amine efficiency for CO{sub 2} adsorption and enhanced water affinity. Mechanistic understanding of degradation of these materials can enable control of molecular architecture to significantly improve material stability. Our process modeling work provided the first publically available cost and energy estimates for cyclic adsorption processes for air capture of CO{sub 2}. Some key findings were: Cycles based on diurnal ambient heating and cooling cannot yield useful purities or amounts of captured CO{sub 2}. Cycles based on steam desorption at 110 oC can yield CO{sub 2} purities of ~88%. The energy requirements for cycles using steam desorption are dominated by needs for thermal input, which results in lower costs than energy input in the form of electricity. Cyclic processes with operational costs of less than $100 tCO{sub 2}-net were described, and these results point to process and material improvements that could substantially reduce these costs. The most critical conclusions from our work are that (i) CO{sub 2} capture from ambient air using moderate temperature cyclic adsorption processes is technically feasible and (ii) the operational costs of realistic versions of these processes are moderate enough to encourage future development of this technology. Because of the very modest net investment that has been made in R&D associated with this approach from all sources worldwide (relative to the massive public and private investment that has been made in technologies for CO{sub 2} from concentrated point sources), our results strongly suggest that continued development of air capture is justified.

  7. A High-Performance Rechargeable Iron Electrode for Large-Scale Battery-Based Energy Storage

    SciTech Connect (OSTI)

    Manohar, AK; Malkhandi, S; Yang, B; Yang, C; Prakash, GKS; Narayanan, SR

    2012-01-01

    Inexpensive, robust and efficient large-scale electrical energy storage systems are vital to the utilization of electricity generated from solar and wind resources. In this regard, the low cost, robustness, and eco-friendliness of aqueous iron-based rechargeable batteries are particularly attractive and compelling. However, wasteful evolution of hydrogen during charging and the inability to discharge at high rates have limited the deployment of iron-based aqueous batteries. We report here new chemical formulations of the rechargeable iron battery electrode to achieve a ten-fold reduction in the hydrogen evolution rate, an unprecedented charging efficiency of 96%, a high specific capacity of 0.3 Ah/g, and a twenty-fold increase in discharge rate capability. We show that modifying high-purity carbonyl iron by in situ electro-deposition of bismuth leads to substantial inhibition of the kinetics of the hydrogen evolution reaction. The in situ formation of conductive iron sulfides mitigates the passivation by iron hydroxide thereby allowing high discharge rates and high specific capacity to be simultaneously achieved. These major performance improvements are crucial to advancing the prospect of a sustainable large-scale energy storage solution based on aqueous iron-based rechargeable batteries. (C) 2012 The Electrochemical Society. [DOI: 10.1149/2.034208jes] All rights reserved.

  8. Twinned silicon and germanium nanocrystals: Formation, stability and quantum confinement

    SciTech Connect (OSTI)

    Yu, Ting; Pi, Xiaodong Ni, Zhenyi; Zhang, Hui; Yang, Deren

    2015-03-15

    Although twins are often observed in Si/Ge nanocrystals (NCs), little theoretical investigation has been carried out to understand this type of important planar defects in Si/Ge NCs. We now study the twinning of Si/Ge NCs in the frame work of density functional theory by representatively considering single-twinned and fivefold-twinned Si/Ge NCs. It is found that the formation of twinned Si/Ge NCs is thermodynamically possible. The effect of twinning on the formation of Si NCs is different from that of Ge NCs. For both Si and Ge NCs twinning enhances their stability. The quantum confinement effect is weakened by twinning for Si NCs. Twinning actually enhances the quantum confinement of Ge NCs when they are small (<136 atoms), while weakening the quantum confinement of Ge NCs as their size is large (>136 atoms). The current results help to better understand the experimental work on twinned Si/Ge NCs and guide the tuning of Si/Ge-NC structures for desired properties.

  9. Titanium and germanium lined hohlraums and halfraums as multi...

    Office of Scientific and Technical Information (OSTI)

    the National Technical Information Service, Springfield, VA at www.ntis.gov. Authors: Girard, F ; Primout, M ; Fournier, K B ; Villette, B ; Stemmler, P ; Jacquet, L ; Babonneau,...

  10. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    electron microscopes at ALS Beamlines 7.3.1 and 11.0.1. From Sand to Processor Modern electronic integrated circuits are made of silicon. Silicon is the most abundant element...

  11. Improving the Cycling Life of Aluminum and Germanium Thin Films...

    Office of Scientific and Technical Information (OSTI)

    Close Cite: Bibtex Format Close 0 pages in this document matching the terms "" Search For Terms: Enter terms in the toolbar above to search the full text of this document for ...

  12. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Z. Zhu, A. Scholl, J.D. Torrey, and M. Rolandi, "Serial and parallel Si, Ge, and SiGe direct-write with scanning probes and conductive stamps," Nano Lett. 11, 2386 (2011). ALS...

  13. Thermoelectric Properties of Rare-Earth-Ruthenium-Germanium Compounds...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cobalt substitution for ruthenium enhances the semiconductor character but does not improve the thermoelectric properties. URL: Link to article - Journal of Applied Physics...

  14. Maximum Likelihood Analysis of Low Energy CDMS II Germanium Data

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Agnese, R.

    2015-03-30

    We report on the results of a search for a Weakly Interacting Massive Particle (WIMP) signal in low-energy data of the Cryogenic Dark Matter Search experiment using a maximum likelihood analysis. A background model is constructed using GEANT4 to simulate the surface-event background from Pb210decay-chain events, while using independent calibration data to model the gamma background. Fitting this background model to the data results in no statistically significant WIMP component. In addition, we also perform fits using an analytic ad hoc background model proposed by Collar and Fields, who claimed to find a large excess of signal-like events in ourmore » data. Finally, we confirm the strong preference for a signal hypothesis in their analysis under these assumptions, but excesses are observed in both single- and multiple-scatter events, which implies the signal is not caused by WIMPs, but rather reflects the inadequacy of their background model.« less

  15. Direct band gap electroluminescence from bulk germanium at room...

    Office of Scientific and Technical Information (OSTI)

    Sciences, Kyushu University, 6-1 Kasuga-koen, Kasuga, Fukuoka 816-8580 (Japan) Art, Science and Technology Center for Cooperative Research, Kyushu University, 6-1...

  16. Improving the Cycling Life of Aluminum and Germanium Thin Films...

    Office of Scientific and Technical Information (OSTI)

    Bibtex Format Close 0 pages in this document matching the terms "" Search For Terms: Enter terms in the toolbar above to search the full text of this document for pages...

  17. Direct-Write of Silicon and Germanium Nanostructures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    deliver desired stimuli or chemicals to a small area of a sample surface. Specifically, atomic force microscopy (AFM) has been employed in several nanofabrication schemes....

  18. Road Map for Studies to Produce Consistent and High Performance SRF Accelerator Structures

    SciTech Connect (OSTI)

    Ganapati Rao Myneni; John F. OHanlon

    2007-06-20

    Superconducting Radio Frequency (SRF) accelerator structures made from high purity niobium are becoming the technological choice for a large number of future accelerators and energy recovery LINACs (ERL). Most of the presently planned accelerators and ERL requirements will be met with some effort by the current SRF technology where accelerating gradients of about 20 MV/m can be produced on a routine basis with an acceptable yield. However, the XFEL at DESY and the planned ILC require acceleration gradients more than 28 MV/m and 35 MV/m respectively. At the recent ILC meeting at Snowmass (2005) concern was expressed regarding the wide spread in the achieved accelerator gradients and the relatively low yields. For obtaining accelerating gradients of 35 MV/m in SRF accelerator structures consistently, a deeper understanding of the causes for the spread has to be gained and advances have to be made in many scientific and high technology fields, including materials, surface and vacuum sciences, application of reliable processes and procedures, which provide contamination free surfaces and avoid recontamination and cryogenics related technologies. In this contribution a road map for studies needed to produce consistent and high performance SRF accelerator structures from the needed materials development to clean and non-recontaminating processes and procedures will be presented.

  19. Nanoporous, Metal Carbide, Surface Diffusion Membranes for High Temperature Hydrogen Separations

    SciTech Connect (OSTI)

    Way, J.; Wolden, Colin

    2013-09-30

    Colorado School of Mines (CSM) developed high temperature, hydrogen permeable membranes that contain no platinum group metals with the goal of separating hydrogen from gas mixtures representative of gasification of carbon feedstocks such as coal or biomass in order to meet DOE NETL 2015 hydrogen membrane performance targets. We employed a dual synthesis strategy centered on transition metal carbides. In the first approach, novel, high temperature, surface diffusion membranes based on nanoporous Mo{sub 2}C were fabricated on ceramic supports. These were produced in a two step process that consisted of molybdenum oxide deposition followed by thermal carburization. Our best Mo{sub 2}C surface diffusion membrane achieved a pure hydrogen flux of 367 SCFH/ft{sup 2} at a feed pressure of only 20 psig. The highest H{sub 2}/N{sub 2} selectivity obtained with this approach was 4.9. A transport model using dusty gas theory was derived to describe the hydrogen transport in the Mo{sub 2}C coated, surface diffusion membranes. The second class of membranes developed were dense metal foils of BCC metals such as vanadium coated with thin (< 60 nm) Mo{sub 2}C catalyst layers. We have fabricated a Mo{sub 2}C/V composite membrane that in pure gas testing delivered a H{sub 2} flux of 238 SCFH/ft{sup 2} at 600 C and 100 psig, with no detectable He permeance. This exceeds the 2010 DOE Target flux. This flux is 2.8 times that of pure Pd at the same membrane thickness and test conditions and over 79% of the 2015 flux target. In mixed gas testing we achieved a permeate purity of ?99.99%, satisfying the permeate purity milestone, but the hydrogen permeance was low, ~0.2 SCFH/ft{sup 2}.psi. However, during testing of a Mo{sub 2}C coated Pd alloy membrane with DOE 1 feed gas mixture a hydrogen permeance of >2 SCFH/ft{sup 2}.psi was obtained which was stable during the entire test, meeting the permeance associated with the 2010 DOE target flux. Lastly, the Mo{sub 2}C/V composite membranes were shown to be stable for at least 168 hours = one week, including cycling at high temperature and alternating He/H{sub 2} exposure.

  20. High Energy Physics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High Energy Physics science-innovationassetsimagesicon-science.jpg High Energy Physics Investigating the field of high energy physics through experiments that strengthen our ...

  1. High-Temperature-High-Volume Lifting for Enhanced Geothermal...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    High-Temperature-High-Volume Lifting for Enhanced Geothermal Systems High-Temperature-High-Volume Lifting for Enhanced Geothermal Systems High-Temperature-High-Volume Lifting for ...

  2. High efficiency and high concentration in photovoltaics

    SciTech Connect (OSTI)

    Yamaguchi, Masafumi; Luque, A.

    1999-10-01

    In this paper, the authors present the state-of-the-art of multijunction solar cells and the future prospects of this technology. Their use in terrestrial applications will likely be for concentrators operating at very high concentrations. Some trends are also discussed and the authors present a cost calculation showing that highly efficient cells under very high concentration would be able to produce electricity at costs competitive with electricity generation costs for some utilities.

  3. High Performance Computing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    HPC INL Logo Home High-Performance Computing INL's high-performance computing center provides general use scientific computing capabilities to support the lab's efforts in advanced...

  4. High pressure, high current, low inductance, high reliability sealed terminals

    DOE Patents [OSTI]

    Hsu, John S. (Oak Ridge, TN) [Oak Ridge, TN; McKeever, John W. (Oak Ridge, TN) [Oak Ridge, TN

    2010-03-23

    The invention is a terminal assembly having a casing with at least one delivery tapered-cone conductor and at least one return tapered-cone conductor routed there-through. The delivery and return tapered-cone conductors are electrically isolated from each other and positioned in the annuluses of ordered concentric cones at an off-normal angle. The tapered cone conductor service can be AC phase conductors and DC link conductors. The center core has at least one service conduit of gate signal leads, diagnostic signal wires, and refrigerant tubing routed there-through. A seal material is in direct contact with the casing inner surface, the tapered-cone conductors, and the service conduits thereby hermetically filling the interstitial space in the casing interior core and center core. The assembly provides simultaneous high-current, high-pressure, low-inductance, and high-reliability service.

  5. High Temperature, High Pressure Devices for Zonal Isolation in...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    High Temperature, High Pressure Devices for Zonal Isolation in Geothermal Wells High Temperature, High Pressure Devices for Zonal Isolation in Geothermal Wells High Temperature, ...

  6. High strength, high ductility low carbon steel

    DOE Patents [OSTI]

    Koo, Jayoung (Berkeley, CA); Thomas, Gareth (Berkeley, CA)

    1978-01-01

    A high strength, high ductility low carbon steel consisting essentially of iron, 0.05-0.15 wt% carbon, and 1-3 wt% silicon. Minor amounts of other constituents may be present. The steel is characterized by a duplex ferrite-martensite microstructure in a fibrous morphology. The microstructure is developed by heat treatment consisting of initial austenitizing treatment followed by annealing in the (.alpha. + .gamma.) range with intermediate quenching.

  7. HIGHLY ENRICHED URANIUM BLEND DOWN PROGRAM AT THE SAVANNAH RIVER SITE PRESENT AND FUTURE

    SciTech Connect (OSTI)

    Magoulas, V; Charles Goergen, C; Ronald Oprea, R

    2008-06-05

    The Department of Energy (DOE) and Tennessee Valley Authority (TVA) entered into an Interagency Agreement to transfer approximately 40 metric tons of highly enriched uranium (HEU) to TVA for conversion to fuel for the Browns Ferry Nuclear Power Plant. Savannah River Site (SRS) inventories included a significant amount of this material, which resulted from processing spent fuel and surplus materials. The HEU is blended with natural uranium (NU) to low enriched uranium (LEU) with a 4.95% 235U isotopic content and shipped as solution to the TVA vendor. The HEU Blend Down Project provided the upgrades needed to achieve the product throughput and purity required and provided loading facilities. The first blending to low enriched uranium (LEU) took place in March 2003 with the initial shipment to the TVA vendor in July 2003. The SRS Shipments have continued on a regular schedule without any major issues for the past 5 years and are due to complete in September 2008. The HEU Blend program is now looking to continue its success by dispositioning an additional approximately 21 MTU of HEU material as part of the SRS Enriched Uranium Disposition Project.

  8. Reactor Physics Measurements and Benchmark Specifications for Oak Ridge Highly Enriched Uranium Sphere (ORSphere)

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Marshall, Margaret A.

    2014-11-04

    In the early 1970s Dr. John T. Mihalczo (team leader), J.J. Lynn, and J.R. Taylor performed experiments at the Oak Ridge Critical Experiments Facility (ORCEF) with highly enriched uranium (HEU) metal (called Oak Ridge Alloy or ORALLOY) in an effort to recreate GODIVA I results with greater accuracy than those performed at Los Alamos National Laboratory in the 1950s. The purpose of the Oak Ridge ORALLOY Sphere (ORSphere) experiments was to estimate the unreflected and unmoderated critical mass of an idealized sphere of uranium metal corrected to a density, purity, and enrichment such that it could be compared with themore » GODIVA I experiments. Additionally, various material reactivity worths, the surface material worth coefficient, the delayed neutron fraction, the prompt neutron decay constant, relative fission density, and relative neutron importance were all measured. The critical assembly, material reactivity worths, the surface material worth coefficient, and the delayed neutron fraction were all evaluated as benchmark experiment measurements. The reactor physics measurements are the focus of this paper; although for clarity the critical assembly benchmark specifications are briefly discussed.« less

  9. Reactor Physics Measurements and Benchmark Specifications for Oak Ridge Highly Enriched Uranium Sphere (ORSphere)

    SciTech Connect (OSTI)

    Marshall, Margaret A.

    2014-11-04

    In the early 1970s Dr. John T. Mihalczo (team leader), J.J. Lynn, and J.R. Taylor performed experiments at the Oak Ridge Critical Experiments Facility (ORCEF) with highly enriched uranium (HEU) metal (called Oak Ridge Alloy or ORALLOY) in an effort to recreate GODIVA I results with greater accuracy than those performed at Los Alamos National Laboratory in the 1950s. The purpose of the Oak Ridge ORALLOY Sphere (ORSphere) experiments was to estimate the unreflected and unmoderated critical mass of an idealized sphere of uranium metal corrected to a density, purity, and enrichment such that it could be compared with the GODIVA I experiments. Additionally, various material reactivity worths, the surface material worth coefficient, the delayed neutron fraction, the prompt neutron decay constant, relative fission density, and relative neutron importance were all measured. The critical assembly, material reactivity worths, the surface material worth coefficient, and the delayed neutron fraction were all evaluated as benchmark experiment measurements. The reactor physics measurements are the focus of this paper; although for clarity the critical assembly benchmark specifications are briefly discussed.

  10. NID Copper Sample Analysis

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Zhu, Zihua

    2011-09-12

    The current focal point of the nuclear physics program at PNNL is the MAJORANA DEMONSTRATOR, and the follow-on Tonne-Scale experiment, a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0???). This experiment requires the use of germanium isotopically enriched in 76Ge. The MAJORANA DEMONSTRATOR is a DOE and NSF funded project with a major science impact. The DEMONSTRATOR will utilize 76Ge from Russia, but for the Tonne-Scale experiment it is hoped that an alternate technology, possibly one under development at Nonlinear Ion Dynamics (NID), will be a viable, US-based, lower-cost source of separated material. Samples of separated material from NID require analysis to determine the isotopic distribution and impurities. DOE is funding NID through an SBIR grant for development of their separation technology for application to the Tonne-Scale experiment. The Environmental Molecular Sciences facility (EMSL), a DOE user facility at PNNL, has the required mass spectroscopy instruments for making isotopic measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR and for the development of the future separation technology required for the Tonne-Scale experiment. A sample of isotopically separated copper was provided by NID to PNNL in January 2011 for isotopic analysis as a test of the NID technology. The results of that analysis are reported here. A second sample of isotopically separated copper was provided by NID to PNNL in August 2011 for isotopic analysis as a test of the NID technology. The results of that analysis are also reported here.

  11. The Design of an Ultra-Low Background Thermosyphon for the Majorana Demonstrator

    SciTech Connect (OSTI)

    Aguayo Navarrete, Estanislao; Busch, Matthew; Daniels, Randy; Fast, James E.; Green, Matthew P.; Reid, Douglas J.

    2013-05-01

    The MAJORANA DEMONSTRATOR (MJD) is an ultra-low background neutrinoless double-beta decay (0???) experiment that will deploy up to 40 kg of high purity germanium detectors (HPGe). The goal of this experiment is to demonstrate the feasibility of building a detector array with less than 1 event/ton-year in a 4 keV region of interest around the 0??? signal. HPGe diodes, when used as ionizing radiation detectors, need to be maintained at a temperature close to that of liquid nitrogen (77 K). This work describes the R&D results of a cryogenic system capable of meeting the requirements of low background and the cooling capacity required to successfully operate such a detector system. The MJD germanium detector modules will operate at liquid nitrogen temperature to provide adequate cooling for a full range of HPGe impurity concentrations. This paper shows the experimental results obtained using a two-phase horizontal thermosyphon using liquid nitrogen as the MJDs cooling system. The cold test shows that the proposed thermosyphon has sufficient cooling power to handle the heat load of an MJD module. Results for the temperature gradient across the thermosyphon, cooling capacity, and design considerations demonstrate that the thermosyphon can effectively remove the calculated heat load of each module of the experiment. The thermosyphon will be bolted to a cold plate from which detector strings will hang. The thermal conductivity of a mockup of the MJD bolted thermal joint is experimentally determined to be below 0.1 K/W.

  12. HerMES: Candidate high-redshift galaxies discovered with Herschel/Spire

    SciTech Connect (OSTI)

    Dowell, C. Darren; Bock, J.; Bridge, C.; Cooray, A.; Conley, A.; Glenn, J.; Arumugam, V.; Asboth, V.; Aussel, H.; Bthermin, M.; Boselli, A.; Buat, V.; Burgarella, D.; Cabrera-Lavers, A.; Casey, C. M.; Chapman, S. C.; Clements, D. L.; Conversi, L.; Dannerbauer, H.; and others

    2014-01-01

    We present a method for selecting z > 4 dusty, star-forming galaxies (DSFGs) using Herschel/Spectral and Photometric Imaging Receiver 250/350/500 ?m flux densities to search for red sources. We apply this method to 21 deg{sup 2} of data from the HerMES survey to produce a catalog of 38 high-z candidates. Follow-up of the first five of these sources confirms that this method is efficient at selecting high-z DSFGs, with 4/5 at z = 4.3-6.3 (and the remaining source at z = 3.4), and that they are some of the most luminous dusty sources known. Comparison with previous DSFG samples, mostly selected at longer wavelengths (e.g., 850 ?m) and in single-band surveys, shows that our method is much more efficient at selecting high-z DSFGs, in the sense that a much larger fraction are at z > 3. Correcting for the selection completeness and purity, we find that the number of bright (S {sub 500} {sub ?m} ? 30 mJy), red Herschel sources is 3.3 0.8 deg{sup 2}. This is much higher than the number predicted by current models, suggesting that the DSFG population extends to higher redshifts than previously believed. If the shape of the luminosity function for high-z DSFGs is similar to that at z ? 2, rest-frame UV based studies may be missing a significant component of the star formation density at z = 4-6, even after correction for extinction.

  13. High Energy Physics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High Energy Physics /science-innovation/_assets/images/icon-science.jpg High Energy Physics Investigating the field of high energy physics through experiments that strengthen our fundamental understanding of matter, energy, space, and time. Advanced Scientific Computing Research Basic Energy Sciences Biological and Environmental Research Fusion Energy Sciences High Energy Physics Nuclear Physics Advanced Scientific Computing Research Pioneering accelerator technology to improve the intensity of

  14. High power microwave generator

    DOE Patents [OSTI]

    Ekdahl, Carl A. (Albuquerque, NM)

    1986-01-01

    A microwave generator efficiently converts the energy of an intense relativistic electron beam (REB) into a high-power microwave emission using the Smith-Purcell effect which is related to Cerenkov radiation. Feedback for efficient beam bunching and high gain is obtained by placing a cylindrical Smith-Purcell transmission grating on the axis of a toroidal resonator. High efficiency results from the use of a thin cold annular highly-magnetized REB that is closely coupled to the resonant structure.

  15. High power microwave generator

    DOE Patents [OSTI]

    Ekdahl, C.A.

    1983-12-29

    A microwave generator efficiently converts the energy of an intense relativistic electron beam (REB) into a high-power microwave emission using the Smith-Purcell effect which is related to Cerenkov radiation. Feedback for efficient beam bunching and high gain is obtained by placing a cylindrical Smith-Purcell transmission grating on the axis of a toroidal resonator. High efficiency results from the use of a thin cold annular highly-magnetized REB that is closely coupled to the resonant structure.

  16. Fuel Accident Condition Simulator (FACS) Furnace for Post-Irradiation Heating Tests of VHTR Fuel Compacts

    SciTech Connect (OSTI)

    Paul A Demkowicz; Paul Demkowicz; David V Laug

    2010-10-01

    Abstract Fuel irradiation testing and post-irradiation examination are currently in progress as part of the Next Generation Nuclear Plant Fuels Development and Qualification Program. The PIE campaign will include extensive accident testing of irradiated very high temperature reactor fuel compacts to verify fission product retention characteristics at high temperatures. This work will be carried out at both the Idaho National Laboratory (INL) and the Oak Ridge National Laboratory, beginning with accident tests on irradiated fuel from the AGR-1 experiment in 2010. A new furnace system has been designed, built, and tested at INL to perform high temperature accident tests. The Fuel Accident Condition Simulator furnace system is designed to heat fuel specimens at temperatures up to 2000C in helium while monitoring the release of volatile fission metals (e.g. Cs, Ag, Sr, Eu, and I) and fission gases (Kr, Xe). Fission gases released from the fuel to the sweep gas are monitored in real time using dual cryogenic traps fitted with high purity germanium detectors. Condensable fission products are collected on a plate attached to a water-cooled cold finger that can be exchanged periodically without interrupting the test. Analysis of fission products on the condensation plates involves dry gamma counting followed by chemical analysis of selected isotopes. This paper will describe design and operational details of the Fuel Accident Condition Simulator (FACS) furnace system, as well as preliminary system calibration results.

  17. High performance systems

    SciTech Connect (OSTI)

    Vigil, M.B.

    1995-03-01

    This document provides a written compilation of the presentations and viewgraphs from the 1994 Conference on High Speed Computing given at the High Speed Computing Conference, {open_quotes}High Performance Systems,{close_quotes} held at Gleneden Beach, Oregon, on April 18 through 21, 1994.

  18. High power, high beam quality regenerative amplifier

    DOE Patents [OSTI]

    Hackel, L.A.; Dane, C.B.

    1993-08-24

    A regenerative laser amplifier system generates high peak power and high energy per pulse output beams enabling generation of X-rays used in X-ray lithography for manufacturing integrated circuits. The laser amplifier includes a ring shaped optical path with a limited number of components including a polarizer, a passive 90 degree phase rotator, a plurality of mirrors, a relay telescope, and a gain medium, the components being placed close to the image plane of the relay telescope to reduce diffraction or phase perturbations in order to limit high peak intensity spiking. In the ring, the beam makes two passes through the gain medium for each transit of the optical path to increase the amplifier gain to loss ratio. A beam input into the ring makes two passes around the ring, is diverted into an SBS phase conjugator and proceeds out of the SBS phase conjugator back through the ring in an equal but opposite direction for two passes, further reducing phase perturbations. A master oscillator inputs the beam through an isolation cell (Faraday or Pockels) which transmits the beam into the ring without polarization rotation. The isolation cell rotates polarization only in beams proceeding out of the ring to direct the beams out of the amplifier. The diffraction limited quality of the input beam is preserved in the amplifier so that a high power output beam having nearly the same diffraction limited quality is produced.

  19. High power, high beam quality regenerative amplifier

    DOE Patents [OSTI]

    Hackel, Lloyd A. (Livermore, CA); Dane, Clifford B. (Livermore, CA)

    1993-01-01

    A regenerative laser amplifier system generates high peak power and high energy per pulse output beams enabling generation of X-rays used in X-ray lithography for manufacturing integrated circuits. The laser amplifier includes a ring shaped optical path with a limited number of components including a polarizer, a passive 90 degree phase rotator, a plurality of mirrors, a relay telescope, and a gain medium, the components being placed close to the image plane of the relay telescope to reduce diffraction or phase perturbations in order to limit high peak intensity spiking. In the ring, the beam makes two passes through the gain medium for each transit of the optical path to increase the amplifier gain to loss ratio. A beam input into the ring makes two passes around the ring, is diverted into an SBS phase conjugator and proceeds out of the SBS phase conjugator back through the ring in an equal but opposite direction for two passes, further reducing phase perturbations. A master oscillator inputs the beam through an isolation cell (Faraday or Pockels) which transmits the beam into the ring without polarization rotation. The isolation cell rotates polarization only in beams proceeding out of the ring to direct the beams out of the amplifier. The diffraction limited quality of the input beam is preserved in the amplifier so that a high power output beam having nearly the same diffraction limited quality is produced.

  20. High Tech Halloween

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High Tech Halloween High Tech Halloween WHEN: Oct 30, 2015 4:00 PM - 6:30 PM WHERE: Bradbury Science Museum 1350 Central Avenue, Los Alamos, New Mexico, 87544 USA CONTACT: Linda Anderman (505) 665-9196 CATEGORY: Bradbury INTERNAL: Calendar Login High Tech Halloween Event Description High-Tech Halloween is the Bradbury Science Museum's contribution to Downtown Los Alamos' annual Trick-or-Treat on MainStreet event taking place the Friday before Halloween. At this year's High-Tech Halloween, you

  1. Low Cost, High Temperature, High Ripple Current DC Bus Capacitors...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Low Cost, High Temperature, High Ripple Current DC Bus Capacitors Low Cost, High Temperature, High Ripple Current DC Bus Capacitors 2010 DOE Vehicle Technologies and Hydrogen...

  2. High-pressure, high-temperature plastic deformation of sintered...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: High-pressure, high-temperature plastic deformation of sintered diamonds Citation Details In-Document Search Title: High-pressure, high-temperature plastic ...

  3. The high-pressure-high-temperature behavior of bassanite (Journal...

    Office of Scientific and Technical Information (OSTI)

    The high-pressure-high-temperature behavior of bassanite Citation Details In-Document Search Title: The high-pressure-high-temperature behavior of bassanite The pressure evolution ...

  4. Energy Storage Testing and Analysis High Power and High Energy...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Testing and Analysis High Power and High Energy Development Energy Storage Testing and Analysis High Power and High Energy Development 2009 DOE Hydrogen Program and Vehicle ...

  5. High pressure and high temperature apparatus

    DOE Patents [OSTI]

    Voronov, Oleg A.

    2005-09-13

    A design for high pressure/high temperature apparatus and reaction cell to achieve .about.30 GPa pressure in .about.1 cm volume and .about.100 GPa pressure in .about.1 mm volumes and 20-5000.degree. C. temperatures in a static regime. The device includes profiled anvils (28) action on a reaction cell (14, 16) containing the material (26) to be processed. The reaction cell includes a heater (18) surrounded by insulating layers and screens. Surrounding the anvils are cylindrical inserts and supporting rings (30-48) whose hardness increases towards the reaction cell. These volumes may be increased considerably if applications require it, making use of presses that have larger loading force capability, larger frames and using larger anvils.

  6. High output lamp with high brightness

    DOE Patents [OSTI]

    Kirkpatrick, Douglas A.; Bass, Gary K.; Copsey, Jesse F.; Garber, Jr., William E.; Kwong, Vincent H.; Levin, Izrail; MacLennan, Donald A.; Roy, Robert J.; Steiner, Paul E.; Tsai, Peter; Turner, Brian P.

    2002-01-01

    An ultra bright, low wattage inductively coupled electrodeless aperture lamp is powered by a solid state RF source in the range of several tens to several hundreds of watts at various frequencies in the range of 400 to 900 MHz. Numerous novel lamp circuits and components are disclosed including a wedding ring shaped coil having one axial and one radial lead, a high accuracy capacitor stack, a high thermal conductivity aperture cup and various other aperture bulb configurations, a coaxial capacitor arrangement, and an integrated coil and capacitor assembly. Numerous novel RF circuits are also disclosed including a high power oscillator circuit with reduced complexity resonant pole configuration, parallel RF power FET transistors with soft gate switching, a continuously variable frequency tuning circuit, a six port directional coupler, an impedance switching RF source, and an RF source with controlled frequency-load characteristics. Numerous novel RF control methods are disclosed including controlled adjustment of the operating frequency to find a resonant frequency and reduce reflected RF power, controlled switching of an impedance switched lamp system, active power control and active gate bias control.

  7. Time-resolved measurements of the hot-electron population in ignition-scale experiments on the National Ignition Facility (invited)

    SciTech Connect (OSTI)

    Hohenberger, M. Stoeckl, C.; Albert, F.; Palmer, N. E.; Dppner, T.; Divol, L.; Dewald, E. L.; Bachmann, B.; MacPhee, A. G.; LaCaille, G.; Bradley, D. K.; Lee, J. J.

    2014-11-15

    In laser-driven inertial confinement fusion, hot electrons can preheat the fuel and prevent fusion-pellet compression to ignition conditions. Measuring the hot-electron population is key to designing an optimized ignition platform. The hot electrons in these high-intensity, laser-driven experiments, created via laser-plasma interactions, can be inferred from the bremsstrahlung generated by hot electrons interacting with the target. At the National Ignition Facility (NIF) [G. H. Miller, E. I. Moses, and C. R. Wuest, Opt. Eng. 43, 2841 (2004)], the filter-fluorescer x-ray (FFLEX) diagnostica multichannel, hard x-ray spectrometer operating in the 20500 keV rangehas been upgraded to provide fully time-resolved, absolute measurements of the bremsstrahlung spectrum with ?300 ps resolution. Initial time-resolved data exhibited significant background and low signal-to-noise ratio, leading to a redesign of the FFLEX housing and enhanced shielding around the detector. The FFLEX x-ray sensitivity was characterized with an absolutely calibrated, energy-dispersive high-purity germanium detector using the high-energy x-ray source at NSTec Livermore Operations over a range of K-shell fluorescence energies up to 111 keV (U K{sub ?}). The detectors impulse response function was measured in situ on NIF short-pulse (?90 ps) experiments, and in off-line tests.

  8. Highly directional thermal emitter

    DOE Patents [OSTI]

    Ribaudo, Troy; Shaner, Eric A; Davids, Paul; Peters, David W

    2015-03-24

    A highly directional thermal emitter device comprises a two-dimensional periodic array of heavily doped semiconductor structures on a surface of a substrate. The array provides a highly directional thermal emission at a peak wavelength between 3 and 15 microns when the array is heated. For example, highly doped silicon (HDSi) with a plasma frequency in the mid-wave infrared was used to fabricate nearly perfect absorbing two-dimensional gratings structures that function as highly directional thermal radiators. The absorption and emission characteristics of the HDSi devices possessed a high degree of angular dependence for infrared absorption in the 10-12 micron range, while maintaining high reflectivity of solar radiation (.about.64%) at large incidence angles.

  9. High voltage coaxial switch

    DOE Patents [OSTI]

    Rink, J.P.

    1983-07-19

    A coaxial high voltage, high current switch having a solid cylindrical cold cathode coaxially surrounded by a thin hollow cylindrical inner electrode and a larger hollow cylindrical outer electrode. A high voltage trigger between the cathode and the inner electrode causes electrons to be emitted from the cathode and flow to the inner electrode preferably through a vacuum. Some of the electrons penetrate the inner electrode and cause a volumetric discharge in the gas (which may be merely air) between the inner and outer electrodes. The discharge provides a low impedance path between a high voltage charge placed on the outer electrode and a load (which may be a high power laser) coupled to the inner electrode. For high repetition rate the gas between the inner and outer electrodes may be continuously exchanged or refreshed under pressure. 3 figs.

  10. High voltage coaxial switch

    DOE Patents [OSTI]

    Rink, John P. (Los Alamos, NM)

    1983-07-19

    A coaxial high voltage, high current switch having a solid cylindrical cold cathode coaxially surrounded by a thin hollow cylindrical inner electrode and a larger hollow cylindrical outer electrode. A high voltage trigger between the cathode and the inner electrode causes electrons to be emitted from the cathode and flow to the inner electrode preferably through a vacuum. Some of the electrons penetrate the inner electrode and cause a volumetric discharge in the gas (which may be merely air) between the inner and outer electrodes. The discharge provides a low impedance path between a high voltage charge placed on the outer electrode and a load (which may be a high power laser) coupled to the inner electrode. For high repetition rate the gas between the inner and outer electrodes may be continuously exchanged or refreshed under pressure.

  11. High temperature furnace

    DOE Patents [OSTI]

    Borkowski, Casimer J.

    1976-08-03

    A high temperature furnace for use above 2000.degree.C is provided that features fast initial heating and low power consumption at the operating temperature. The cathode is initially heated by joule heating followed by electron emission heating at the operating temperature. The cathode is designed for routine large temperature excursions without being subjected to high thermal stresses. A further characteristic of the device is the elimination of any ceramic components from the high temperature zone of the furnace.

  12. High temperature refrigerator

    DOE Patents [OSTI]

    Steyert, Jr., William A.

    1978-01-01

    A high temperature magnetic refrigerator which uses a Stirling-like cycle in which rotating magnetic working material is heated in zero field and adiabatically magnetized, cooled in high field, then adiabatically demagnetized. During this cycle said working material is in heat exchange with a pumped fluid which absorbs heat from a low temperature heat source and deposits heat in a high temperature reservoir. The magnetic refrigeration cycle operates at an efficiency 70% of Carnot.

  13. High School Science Bowl

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High School Science Bowl High School Science Bowl WHEN: Feb 07, 2015 8:00 AM - 4:00 PM WHERE: Highland High School 4700 Coal Ave SE, Albuquerque, USA CATEGORY: Community INTERNAL: Calendar Login Event Description The Science Bowl is a Jeopardy-like event for high school and middle school students who have a strong interest in mathematics and science. The competition is in the form of a round robin in the morning and double elimination after lunch. Teams consist of four students and one optional

  14. High Energy Cost Grants

    Broader source: Energy.gov [DOE]

    The High Energy Cost Grant Program provides financial assistance for the improvement of energy generation, transmission, and distribution facilities servicing eligible rural communities with home...

  15. High Performance Sustainable Buildings

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    science and bioscience capabiities. Occupational Medicine will become a High Performance Sustainable Building in 2013. On the former County landfill, a photovoltaic array field...

  16. High power, high frequency, vacuum flange

    DOE Patents [OSTI]

    Felker, Brian (Livermore, CA); McDaniel, Michael R. (Manteca, CA)

    1993-01-01

    An improved waveguide flange is disclosed for high power operation that helps prevent arcs from being initiated at the junctions between waveguide sections. The flanges at the end of the waveguide sections have counterbores surrounding the waveguide tubes. When the sections are bolted together the counterbores form a groove that holds a fully annealed copper gasket. Each counterbore has a beveled step that is specially configured to insure the gasket forms a metal-to-metal vacuum seal without gaps or sharp edges. The resultant inner surface of the waveguide is smooth across the junctions between waveguide sections, and arcing is prevented.

  17. High power, high frequency, vacuum flange

    DOE Patents [OSTI]

    Felker, B.; McDaniel, M.R.

    1993-03-23

    An improved waveguide flange is disclosed for high power operation that helps prevent arcs from being initiated at the junctions between waveguide sections. The flanges at the end of the waveguide sections have counter bores surrounding the waveguide tubes. When the sections are bolted together the counter bores form a groove that holds a fully annealed copper gasket. Each counterbore has a beveled step that is specially configured to insure the gasket forms a metal-to-metal vacuum seal without gaps or sharp edges. The resultant inner surface of the waveguide is smooth across the junctions between waveguide sections, and arcing is prevented.

  18. High coking value pitch

    SciTech Connect (OSTI)

    Miller, Douglas J.; Chang, Ching-Feng; Lewis, Irwin C.; Lewis, Richard T.

    2014-06-10

    A high coking value pitch prepared from coal tar distillate and has a low softening point and a high carbon value while containing substantially no quinoline insolubles is disclosed. The pitch can be used as an impregnant or binder for producing carbon and graphite articles.

  19. High density photovoltaic

    SciTech Connect (OSTI)

    Haigh, R.E.; Jacobson, G.F.; Wojtczuk, S.

    1997-10-14

    Photovoltaic technology can directly generate high voltages in a solid state material through the series interconnect of many photovoltaic diodes. We are investigating the feasibility of developing an electrically isolated, high-voltage power supply using miniature photovoltaic devices that convert optical energy to electrical energy.

  20. High temperature sensor

    DOE Patents [OSTI]

    Tokarz, Richard D.

    1982-01-01

    A high temperature sensor includes a pair of electrical conductors separated by a mass of electrical insulating material. The insulating material has a measurable resistivity within the sensor that changes in relation to the temperature of the insulating material within a high temperature range (1,000 to 2,000 K.). When required, the sensor can be encased within a ceramic protective coating.

  1. High Efficiency, Illumination Quality OLEDs for Lighting

    SciTech Connect (OSTI)

    Joseph Shiang; James Cella; Kelly Chichak; Anil Duggal; Kevin Janora; Chris Heller; Gautam Parthasarathy; Jeffery Youmans; Joseph Shiang

    2008-03-31

    The goal of the program was to demonstrate a 45 lumen per watt white light device based upon the use of multiple emission colors through the use of solution processing. This performance level is a dramatic extension of the team's previous 15 LPW large area illumination device. The fundamental material system was based upon commercial polymer materials. The team was largely able to achieve these goals, and was able to deliver to DOE a 90 lumen illumination source that had an average performance of 34 LPW a 1000 cd/m{sup 2} with peak performances near 40LPW. The average color temperature is 3200K and the calculated CRI 85. The device operated at a brightness of approximately 1000cd/m{sup 2}. The use of multiple emission colors particularly red and blue, provided additional degrees of design flexibility in achieving white light, but also required the use of a multilayered structure to separate the different recombination zones and prevent interconversion of blue emission to red emission. The use of commercial materials had the advantage that improvements by the chemical manufacturers in charge transport efficiency, operating life and material purity could be rapidly incorporated without the expenditure of additional effort. The program was designed to take maximum advantage of the known characteristics of these material and proceeded in seven steps. (1) Identify the most promising materials, (2) assemble them into multi-layer structures to control excitation and transport within the OLED, (3) identify materials development needs that would optimize performance within multilayer structures, (4) build a prototype that demonstrates the potential entitlement of the novel multilayer OLED architecture (5) integrate all of the developments to find the single best materials set to implement the novel multilayer architecture, (6) further optimize the best materials set, (7) make a large area high illumination quality white OLED. A photo of the final deliverable is shown. In 2003, a large area, OLED based illumination source was demonstrated that could provide light with a quality, quantity, and efficiency on par with what can be achieved with traditional light sources. The demonstration source was made by tiling together 16 separate 6-inch x 6-inch blue-emitting OLEDs. The efficiency, total lumen output, and lifetime of the OLED based illumination source were the same as what would be achieved with an 80 watt incandescent bulb. The devices had an average efficacy of 15 LPW and used solution-processed OLEDs. The individual 6-inch x 6-inch devices incorporated three technology strategies developed specifically for OLED lighting -- downconversion for white light generation, scattering for outcoupling efficiency enhancement, and a scalable monolithic series architecture to enable large area devices. The downconversion approach consists of optically coupling a blue-emitting OLED to a set of luminescent layers. The layers are chosen to absorb the blue OLED emission and then luminescence with high efficiency at longer wavelengths. The composition and number of layers are chosen so that the unabsorbed blue emission and the longer wavelength re-emission combine to make white light. A downconversion approach has the advantage of allowing a wide variety of colors to be made from a limited set of blue emitters. In addition, one does not have to carefully tune the emission wavelength of the individual electro-luminescent species within the OLED device in order to achieve white light. The downconversion architecture used to develop the 15LPW large area light source consisted of a polymer-based blue-emitting OLED and three downconversion layers. Two of the layers utilized perylene based dyes from BASF AG of Germany with high quantum efficiency (>98%) and one of the layers consisted of inorganic phosphor particles (Y(Gd)AG:Ce) with a quantum efficiency of {approx}85%. By independently varying the optical density of the downconversion layers, the overall emission spectrum could be adjusted to maximize performance for lighting (e.g. blackbody temperature, color rendering and luminous efficacy) while keeping the properties of the underlying blue OLED constant. The success of the downconversion approach is ultimately based upon the ability to produce efficient emission in the blue. Table 1 presents a comparison of the current performance of the conjugated polymer, dye-doped polymer, and dendrimer approaches to making a solution-processed blue OLED as 2006. Also given is the published state of the art performance of a vapor-deposited blue OLED. One can see that all the approaches to a blue OLED give approximately the same external quantum efficiency at 500 cd/m{sup 2}. However, due to its low operating voltage, the fluorescent conjugated polymer approach yields a superior power efficiency at the same brightness.

  2. HIGH-FIDELITY RADIO ASTRONOMICAL POLARIMETRY USING A MILLISECOND PULSAR AS A POLARIZED REFERENCE SOURCE

    SciTech Connect (OSTI)

    Van Straten, W.

    2013-01-15

    A new method of polarimetric calibration is presented in which the instrumental response is derived from regular observations of PSR J0437-4715 based on the assumption that the mean polarized emission from this millisecond pulsar remains constant over time. The technique is applicable to any experiment in which high-fidelity polarimetry is required over long timescales; it is demonstrated by calibrating 7.2 years of high-precision timing observations of PSR J1022+1001 made at the Parkes Observatory. Application of the new technique followed by arrival time estimation using matrix template matching yields post-fit residuals with an uncertainty-weighted standard deviation of 880 ns, two times smaller than that of arrival time residuals obtained via conventional methods of calibration and arrival time estimation. The precision achieved by this experiment yields the first significant measurements of the secular variation of the projected semimajor axis, the precession of periastron, and the Shapiro delay; it also places PSR J1022+1001 among the 10 best pulsars regularly observed as part of the Parkes Pulsar Timing Array (PPTA) project. It is shown that the timing accuracy of a large fraction of the pulsars in the PPTA is currently limited by the systematic timing error due to instrumental polarization artifacts. More importantly, long-term variations of systematic error are correlated between different pulsars, which adversely affects the primary objectives of any pulsar timing array experiment. These limitations may be overcome by adopting the techniques presented in this work, which relax the demand for instrumental polarization purity and thereby have the potential to reduce the development cost of next-generation telescopes such as the Square Kilometre Array.

  3. Instrument for stable high temperature Seebeck coefficient and resistivity measurements under controlled oxygen partial pressure

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ihlefeld, Jon F.; Brown-Shaklee, Harlan James; Sharma, Peter Anand

    2015-04-28

    The transport properties of ceramic materials strongly depend on oxygen activity, which is tuned by changing the partial oxygen pressure (pO2) prior to and during measurement. Within, we describe an instrument for highly stable measurements of Seebeck coefficient and electrical resistivity at temperatures up to 1300 K with controlled oxygen partial pressure. An all platinum construction is used to avoid potential materials instabilities that can cause measurement drift. Two independent heaters are employed to establish a small temperature gradient for Seebeck measurements, while keeping the average temperature constant and avoiding errors associated with pO2-induced drifts in thermocouple readings. Oxygen equilibriummore » is monitored using both an O2 sensor and the transient behavior of the resistance as a proxy. A pO2 range of 10-25–100 atm can be established with appropriate gas mixtures. Seebeck measurements were calibrated against a high purity platinum wire, Pt/Pt–Rh thermocouple wire, and a Bi2Te3 Seebeck coefficient Standard Reference Material. To demonstrate the utility of this instrument for oxide materials we present measurements as a function of pO2 on a 1 % Nb-doped SrTiO3 single crystal, and show systematic changes in properties consistent with oxygen vacancy defect chemistry. Thus, an approximately 11% increase in power factor over a pO2 range of 10-19–10-8 atm at 973 K for the donor-doped single crystals is observed.« less

  4. Application of cadmium-zinc-telluride detectors in U-235 enrichment measurements

    SciTech Connect (OSTI)

    Ruhter, W.D.; Gunnink, R.

    1994-04-01

    High-resolution, gamma- and x-ray spectrometry are used routinely in nuclear safeguards verification measurements of plutonium and uranium in the field. These measurements are mostly performed with high-purity germanium (HPGe) detectors, that require cooling to liquid-nitrogen temperatures, thus limiting their utility in field and unattended safeguards measurement applications. NaI scintillation detectors do not require cooling, but their moderate energy resolution (10% at 122 keV) is insufficient in most cases for reliable verification measurements. Semiconductor detectors that operate at room temperature, such as cadmium-zinc-telluride (CdZnTe) detectors, with energy resolution performance reaching 2.0% at 122 keV may complement HPGe detectors for certain safeguards verification applications. The authors used a 5x5x5 mm CdZnTe detector to measure U-235 enrichments ranging from 3% to 75%. They use a spectrum analysis technique that fits U-235, U-238, and U K x-ray response profiles to data in the 89- to 100-keV region of gamma-ray spectrum. From the relative magnitudes of the U-235 and U-238 profiles they determine the U-235 enrichment with an accuracy of about 10% with CdZnTe detectors.

  5. Deconvolution of mixed gamma emitters using peak parameters

    SciTech Connect (OSTI)

    Gadd, Milan S; Garcia, Francisco; Magadalena, Vigil M

    2011-01-14

    When evaluating samples containing mixtures of nuclides using gamma spectroscopy the situation sometimes arises where the nuclides present have photon emissions that cannot be resolved by the detector. An example of this is mixtures of {sup 241}Am and plutonium that have L x-ray emissions with slightly different energies which cannot be resolved using a high-purity germanium detector. It is possible to deconvolute the americium L x-rays from those plutonium based on the {sup 241}Am 59.54 keV photon. However, this requires accurate knowledge of the relative emission yields. Also, it often results in high uncertainties in the plutonium activity estimate due to the americium yields being approximately an order of magnitude greater than those for plutonium. In this work, an alternative method of determining the relative fraction of plutonium in mixtures of {sup 241}Am and {sup 239}Pu based on L x-ray peak location and shape parameters is investigated. The sensitivity and accuracy of the peak parameter method is compared to that for conventional peak decovolution.

  6. High Explosives Testing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High Explosives Testing High Explosives Testing In the 1940s, high explosives were tested at Los Alamos. August 1, 2013 The design and testing for "Little Boy" took place at Gun Site The design and testing for "Little Boy" took place at Gun Site. RELATED IMAGES http://farm8.staticflickr.com/7390/9778165821_9976c43bda_t.jpg Enlarge http://farm4.staticflickr.com/3817/9631800990_1c130beec7

  7. High Performance Sustainable Building

    Broader source: Directives, Delegations, and Requirements [Office of Management (MA)]

    2011-11-09

    This Guide highlights the DOE O 413.3B drivers for incorporating high performance sustainable building (HPSB) principles into Critical Decisions 1 through 4 and provides guidance for implementing the Order's HPSB requirements.

  8. High Performance Sustainable Building

    Broader source: Directives, Delegations, and Requirements [Office of Management (MA)]

    2011-11-09

    This Guide provides approaches for implementing the High Performance Sustainable Building (HPSB) requirements of DOE Order 413.3B, Program and Project Management for the Acquisition of Capital Assets. Supersedes DOE G 413.3-6.

  9. High pressure furnace

    DOE Patents [OSTI]

    Morris, D.E.

    1993-09-14

    A high temperature high pressure furnace has a hybrid partially externally heated construction. A metallic vessel fabricated from an alloy having a composition of at least 45% nickel, 15% chrome, and 10% tungsten is utilized (the preferred alloy including 55% nickel, 22% chrome, 14% tungsten, 2% molybdenum, 3% iron (maximum) and 5% cobalt (maximum)). The disclosed alloy is fabricated into 11/4 or 2 inch, 32 mm or 50 mm bar stock and has a length of about 22 inches, 56 cm. This bar stock has an aperture formed therein to define a closed high temperature, high pressure oxygen chamber. The opposite and closed end of the vessel is provided with a small blind aperture into which a thermocouple can be inserted. The closed end of the vessel is inserted into an oven, preferably heated by standard nickel chrome electrical elements and having a heavily insulated exterior. 19 figures.

  10. High pressure furnace

    DOE Patents [OSTI]

    Morris, Donald E. (Kensington, CA)

    1993-01-01

    A high temperature high pressure furnace has a hybrid partially externally heated construction. A metallic vessel fabricated from an alloy having a composition of at least 45% nickel, 15% chrome, and 10% tungsten is utilized (the preferred alloy including 55% nickel, 22% chrome, 14% tungsten, 2% molybdenum, 3% iron (maximum) and 5% cobalt (maximum). The disclosed alloy is fabricated into 11/4 or 2 inch, 32 mm or 50 mm bar stock and has a length of about 22 inches, 56 cm. This bar stock has an aperture formed therein to define a closed high temperature, high pressure oxygen chamber. The opposite and closed end of the vessel is provided with a small blind aperture into which a thermocouple can be inserted. The closed end of the vessel is inserted into an oven, preferably heated by standard nickel chrome electrical elements and having a heavily insulated exterior.

  11. High pressure oxygen furnace

    DOE Patents [OSTI]

    Morris, Donald E. (Kensington, CA)

    1992-01-01

    A high temperature high pressure oxygen furnace having a hybrid partially externally heated construction is disclosed. A metallic bar fabricated from an alloy having a composition of at least 45% nickel, 15% chrome, and 10% tungsten is utilized (the preferred alloy including 55% nickel, 22% chrome, 14% tungsten, 2% molybdenum, 3% iron (maximum) and 5% cobalt (maximum). The disclosed alloy is fabricated into 11/4 inch bar stock and has a length of about 17 inches. This bar stock is gun drilled for over 16 inches of its length with 0.400 inch aperture to define a closed high temperature, high pressure oxygen chamber. The opposite and closed end of the bar is provided with a small support aperture into which both a support and a thermocouple can be inserted. The closed end of the gun drilled bar is inserted into an oven, preferably heated by standard nickel chrome electrical elements and having a heavily insulated exterior.

  12. High pressure oxygen furnace

    DOE Patents [OSTI]

    Morris, D.E.

    1992-07-14

    A high temperature high pressure oxygen furnace having a hybrid partially externally heated construction is disclosed. A metallic bar fabricated from an alloy having a composition of at least 45% nickel, 15% chrome, and 10% tungsten is utilized, the preferred alloy including 55% nickel, 22% chrome, 14% tungsten, 2% molybdenum, 3% iron (maximum) and 5% cobalt (maximum). The disclosed alloy is fabricated into 11/4 inch bar stock and has a length of about 17 inches. This bar stock is gun drilled for over 16 inches of its length with 0.400 inch aperture to define a closed high temperature, high pressure oxygen chamber. The opposite and closed end of the bar is provided with a small support aperture into which both a support and a thermocouple can be inserted. The closed end of the gun drilled bar is inserted into an oven, preferably heated by standard nickel chrome electrical elements and having a heavily insulated exterior. 5 figs.

  13. High-Temperature Superconductivity

    ScienceCinema (OSTI)

    Peter Johnson

    2010-01-08

    Like astronomers tweaking images to gain a more detailed glimpse of distant stars, physicists at Brookhaven National Laboratory have found ways to sharpen images of the energy spectra in high-temperature superconductors ? materials that carry electrical c

  14. High-Speed Photography

    SciTech Connect (OSTI)

    Paisley, D.L.; Schelev, M.Y.

    1998-08-01

    The applications of high-speed photography to a diverse set of subjects including inertial confinement fusion, laser surgical procedures, communications, automotive airbags, lightning etc. are briefly discussed. (AIP) {copyright} {ital 1998 Society of Photo-Optical Instrumentation Engineers.}

  15. High temperature pressure gauge

    DOE Patents [OSTI]

    Echtler, J. Paul (Pittsburgh, PA); Scandrol, Roy O. (Library, PA)

    1981-01-01

    A high temperature pressure gauge comprising a pressure gauge positioned in fluid communication with one end of a conduit which has a diaphragm mounted in its other end. The conduit is filled with a low melting metal alloy above the diaphragm for a portion of its length with a high temperature fluid being positioned in the remaining length of the conduit and in the pressure gauge.

  16. High efficiency incandescent lighting

    DOE Patents [OSTI]

    Bermel, Peter; Ilic, Ognjen; Chan, Walker R.; Musabeyoglu, Ahmet; Cukierman, Aviv Ruben; Harradon, Michael Robert; Celanovic, Ivan; Soljacic, Marin

    2014-09-02

    Incandescent lighting structure. The structure includes a thermal emitter that can, but does not have to, include a first photonic crystal on its surface to tailor thermal emission coupled to, in a high-view-factor geometry, a second photonic filter selected to reflect infrared radiation back to the emitter while passing visible light. This structure is highly efficient as compared to standard incandescent light bulbs.

  17. High Performance Sustainable Buildings

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Buildings Goal 3: High Performance Sustainable Buildings Maintaining the conditions of a building improves the health of not only the surrounding ecosystems, but also the well-being of its occupants. Energy Conservation» Efficient Water Use & Management» High Performance Sustainable Buildings» Greening Transportation» Green Purchasing & Green Technology» Pollution Prevention» Science Serving Sustainability» ENVIRONMENTAL SUSTAINABILITY GOALS at LANL The Radiological Laboratory

  18. High Temperature Aqueous Chemistry

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Accurate knowledge of aqueous chemistry at high temperatures and pressures is important in many applications including nuclear waste disposal and energy extraction. Sandia's Defense Waste Management Programs is equipped with a state-of-the-art hydrothermal experimental system that allows us to obtain high quality kinetic and equilibrium data at temperatures and pressures of interest up to 600 o C and 1,000 bars (100 MPa). This state-of-the-art hydrothermal experimental system includes the

  19. High-temperature sensor

    DOE Patents [OSTI]

    Not Available

    1981-01-29

    A high temperature sensor is described which includes a pair of electrical conductors separated by a mass of electrical insulating material. The insulating material has a measurable resistivity within the sensor that changes in relation to the temperature of the insulating material within a high temperature range (1000 to 2000/sup 0/K). When required, the sensor can be encased within a ceramic protective coating.

  20. High conductivity composite metal

    DOE Patents [OSTI]

    Zhou, R.; Smith, J.L.; Embury, J.D.

    1998-01-06

    Electrical conductors and methods of producing them are disclosed, where the conductors possess both high strength and high conductivity. Conductors are comprised of carbon steel and a material chosen from a group consisting of copper, nickel, silver, and gold. Diffusion barriers are placed between these two materials. The components of a conductor are assembled and then the assembly is subjected to heat treating and mechanical deformation steps. 10 figs.

  1. High conductivity composite metal

    DOE Patents [OSTI]

    Zhou, Ruoyi; Smith, James L.; Embury, John David

    1998-01-01

    Electrical conductors and methods of producing them, where the conductors possess both high strength and high conductivity. Conductors are comprised of carbon steel and a material chosen from a group consisting of copper, nickel, silver, and gold. Diffusion barriers are placed between these two materials. The components of a conductor are assembled and then the assembly is subjected to heat treating and mechanical deformation steps.

  2. High Burnup Effects Program

    SciTech Connect (OSTI)

    Barner, J.O.; Cunningham, M.E.; Freshley, M.D.; Lanning, D.D.

    1990-04-01

    This is the final report of the High Burnup Effects Program (HBEP). It has been prepared to present a summary, with conclusions, of the HBEP. The HBEP was an international, group-sponsored research program managed by Battelle, Pacific Northwest Laboratories (BNW). The principal objective of the HBEP was to obtain well-characterized data related to fission gas release (FGR) for light water reactor (LWR) fuel irradiated to high burnup levels. The HBEP was organized into three tasks as follows: Task 1 -- high burnup effects evaluations; Task 2 -- fission gas sampling; and Task 3 -- parameter effects study. During the course of the HBEP, a program that extended over 10 years, 82 fuel rods from a variety of sources were characterized, irradiated, and then examined in detail after irradiation. The study of fission gas release at high burnup levels was the principal objective of the program and it may be concluded that no significant enhancement of fission gas release at high burnup levels was observed for the examined rods. The rim effect, an as yet unquantified contributor to athermal fission gas release, was concluded to be the one truly high-burnup effect. Though burnup enhancement of fission gas release was observed to be low, a full understanding of the rim region and rim effect has not yet emerged and this may be a potential area of further research. 25 refs., 23 figs., 4 tabs.

  3. High Reliability, High TemperatureThermoelectric Power Generation...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Reliability, High TemperatureThermoelectric Power Generation Materials and Technologies High Reliability, High TemperatureThermoelectric Power Generation Materials and Technologies...

  4. High surface area, high permeability carbon monoliths

    SciTech Connect (OSTI)

    Lagasse, R.R.; Schroeder, J.L. [Sandia National Labs., Albuquerque, NM (United States). Organic Materials Processing Dept.

    1994-12-31

    The goal of this work is to prepare carbon monoliths having precisely tailored pore size distribution. Prior studies have demonstrated that poly(acrylonitrile) can be processed into a precursor having tailored macropore structure. Since the macropores were preserved during pyrolysis, this synthetic process provided a route to porous carbon having macropores with size =0.1 to 10{mu}m. No micropores of size <2 nm could be detected in the carbon, however, by nitrogen adsorption. In the present work, the authors have processed a different polymer, poly(vinylidene chloride) into a macroporous precursor, Pyrolysis produced carbon monoliths having macropores derived from the polymer precursor as well as extensive microporosity produced during the pyrolysis of the polymer. One of these carbons had BET surface area of 1,050 m{sup 2}/g and about 1.2 cc/g total pore volume, with about 1/3 of the total pore volume in micropores and the remainder in 1{mu}m macropores. No mesopores in the intermediate size range could be detected by nitrogen adsorption. Carbon materials having high surface area as well as micron size pores have potential applications as electrodes for double layer supercapacitors containing liquid electrolyte, or as efficient media for performing chemical separations.

  5. Experimental investigation of factors limiting slow axis beam quality in 9xx nm high power broad area diode lasers

    SciTech Connect (OSTI)

    Winterfeldt, M. Crump, P.; Wenzel, H.; Erbert, G.; Trnkle, G.

    2014-08-14

    GaAs-based broad-area diode lasers are needed with improved lateral beam parameter product (BPP{sub lat}) at high power. An experimental study of the factors limiting BPP{sub lat} is therefore presented, using extreme double-asymmetric (EDAS) vertical structures emitting at 910?nm. Continuous wave, pulsed and polarization-resolved measurements are presented and compared to thermal simulation. The importance of thermal and packaging-induced effects is determined by comparing junction -up and -down devices. Process factors are clarified by comparing diodes with and without index-guiding trenches. We show that in all cases studied, BPP{sub lat} is limited by a non-thermal BPP ground-level and a thermal BPP, which depends linearly on self-heating. Measurements as a function of pulse width confirm that self-heating rather than bias-level dominates. Diodes without trenches show low BPP ground-level, and a thermal BPP which depends strongly on mounting, due to changes in the temperature profile. The additional lateral guiding in diodes with trenches strongly increases the BPP ground-level, but optically isolates the stripe from the device edges, suppressing the influence of the thermal profile, leading to a BPP-slope that is low and independent of mounting. Trenches are also shown to initiate strain fields that cause parasitic TM-polarized emission with large BPP{sub lat}, whose influence on total BPP{sub lat} remains small, provided the overall polarization purity is >95%.

  6. The high-pressure-high-temperature behavior of bassanite (Journal...

    Office of Scientific and Technical Information (OSTI)

    The high-pressure-high-temperature behavior of bassanite Citation Details In-Document Search Title: The high-pressure-high-temperature behavior of bassanite The pressure evolution of ...

  7. High-Pressure and High-Temperature Powder Diffraction (Journal...

    Office of Scientific and Technical Information (OSTI)

    High-Pressure and High-Temperature Powder Diffraction Citation Details In-Document Search Title: High-Pressure and High-Temperature Powder Diffraction Authors: Fei, Yingwei ; Wang, ...

  8. Sandia Energy - High Performance Computing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High Performance Computing Home Energy Research Advanced Scientific Computing Research (ASCR) High Performance Computing High Performance Computingcwdd2015-03-18T21:41:24+00:00...

  9. Sandia Energy - High Pressure Chemistry

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High Pressure Chemistry Home Transportation Energy Predictive Simulation of Engines Combustion Chemistry Combustion Kinetics High Pressure Chemistry High Pressure ChemistryAshley...

  10. High Temperature, High Pressure Devices for Zonal Isolation in Geothermal

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Wells | Department of Energy High Temperature, High Pressure Devices for Zonal Isolation in Geothermal Wells High Temperature, High Pressure Devices for Zonal Isolation in Geothermal Wells High Temperature, High Pressure Devices for Zonal Isolation in Geothermal Wells PDF icon fabian_ctd_ zonal_isolation_peer2013.pdf More Documents & Publications High Temperature, High Pressure Devices for Zonal Isolation in Geothermal Wells track 3: enhanced geothermal systems (EGS) | geothermal 2015

  11. High-Temperature-High-Volume Lifting for Enhanced Geothermal Systems |

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Department of Energy High-Temperature-High-Volume Lifting for Enhanced Geothermal Systems High-Temperature-High-Volume Lifting for Enhanced Geothermal Systems High-Temperature-High-Volume Lifting for Enhanced Geothermal Systems presentation at the April 2013 peer review meeting held in Denver, Colorado. PDF icon turnquist_high_temp_tools_peer2013.pdf More Documents & Publications High-Temperature Motor Windings for Downhole Pumps Used in Geothermal Energy Production

  12. High-energy detector

    DOE Patents [OSTI]

    Bolotnikov, Aleksey E.; Camarda, Giuseppe; Cui, Yonggang; James, Ralph B.

    2011-11-22

    The preferred embodiments are directed to a high-energy detector that is electrically shielded using an anode, a cathode, and a conducting shield to substantially reduce or eliminate electrically unshielded area. The anode and the cathode are disposed at opposite ends of the detector and the conducting shield substantially surrounds at least a portion of the longitudinal surface of the detector. The conducting shield extends longitudinally to the anode end of the detector and substantially surrounds at least a portion of the detector. Signals read from one or more of the anode, cathode, and conducting shield can be used to determine the number of electrons that are liberated as a result of high-energy particles impinge on the detector. A correction technique can be implemented to correct for liberated electron that become trapped to improve the energy resolution of the high-energy detectors disclosed herein.

  13. High brightness electron accelerator

    DOE Patents [OSTI]

    Sheffield, Richard L. (Los Alamos, NM); Carlsten, Bruce E. (Los Alamos, NM); Young, Lloyd M. (Los Alamos, NM)

    1994-01-01

    A compact high brightness linear accelerator is provided for use, e.g., in a free electron laser. The accelerator has a first plurality of acclerating cavities having end walls with four coupling slots for accelerating electrons to high velocities in the absence of quadrupole fields. A second plurality of cavities receives the high velocity electrons for further acceleration, where each of the second cavities has end walls with two coupling slots for acceleration in the absence of dipole fields. The accelerator also includes a first cavity with an extended length to provide for phase matching the electron beam along the accelerating cavities. A solenoid is provided about the photocathode that emits the electons, where the solenoid is configured to provide a substantially uniform magnetic field over the photocathode surface to minimize emittance of the electons as the electrons enter the first cavity.

  14. High resolution data acquisition

    DOE Patents [OSTI]

    Thornton, Glenn W.; Fuller, Kenneth R.

    1993-01-01

    A high resolution event interval timing system measures short time intervals such as occur in high energy physics or laser ranging. Timing is provided from a clock (38) pulse train (37) and analog circuitry (44) for generating a triangular wave (46) synchronously with the pulse train (37). The triangular wave (46) has an amplitude and slope functionally related to the time elapsed during each clock pulse in the train. A converter (18, 32) forms a first digital value of the amplitude and slope of the triangle wave at the start of the event interval and a second digital value of the amplitude and slope of the triangle wave at the end of the event interval. A counter (26) counts the clock pulse train (37) during the interval to form a gross event interval time. A computer (52) then combines the gross event interval time and the first and second digital values to output a high resolution value for the event interval.

  15. High resolution data acquisition

    DOE Patents [OSTI]

    Thornton, G.W.; Fuller, K.R.

    1993-04-06

    A high resolution event interval timing system measures short time intervals such as occur in high energy physics or laser ranging. Timing is provided from a clock, pulse train, and analog circuitry for generating a triangular wave synchronously with the pulse train (as seen in diagram on patent). The triangular wave has an amplitude and slope functionally related to the time elapsed during each clock pulse in the train. A converter forms a first digital value of the amplitude and slope of the triangle wave at the start of the event interval and a second digital value of the amplitude and slope of the triangle wave at the end of the event interval. A counter counts the clock pulse train during the interval to form a gross event interval time. A computer then combines the gross event interval time and the first and second digital values to output a high resolution value for the event interval.

  16. High strength alloys

    DOE Patents [OSTI]

    Maziasz, Phillip James [Oak Ridge, TN; Shingledecker, John Paul [Knoxville, TN; Santella, Michael Leonard [Knoxville, TN; Schneibel, Joachim Hugo [Knoxville, TN; Sikka, Vinod Kumar [Oak Ridge, TN; Vinegar, Harold J [Bellaire, TX; John, Randy Carl [Houston, TX; Kim, Dong Sub [Sugar Land, TX

    2010-08-31

    High strength metal alloys are described herein. At least one composition of a metal alloy includes chromium, nickel, copper, manganese, silicon, niobium, tungsten and iron. System, methods, and heaters that include the high strength metal alloys are described herein. At least one heater system may include a canister at least partially made from material containing at least one of the metal alloys. At least one system for heating a subterranean formation may include a tubular that is at least partially made from a material containing at least one of the metal alloys.

  17. High strength alloys

    DOE Patents [OSTI]

    Maziasz, Phillip James; Shingledecker, John Paul; Santella, Michael Leonard; Schneibel, Joachim Hugo; Sikka, Vinod Kumar; Vinegar, Harold J.; John, Randy Carl; Kim, Dong Sub

    2012-06-05

    High strength metal alloys are described herein. At least one composition of a metal alloy includes chromium, nickel, copper, manganese, silicon, niobium, tungsten and iron. System, methods, and heaters that include the high strength metal alloys are described herein. At least one heater system may include a canister at least partially made from material containing at least one of the metal alloys. At least one system for heating a subterranean formation may include a tublar that is at least partially made from a material containing at least one of the metal alloys.

  18. High Availability Electronics Standards

    SciTech Connect (OSTI)

    Larsen, R.S.; /SLAC

    2006-12-13

    Availability modeling of the proposed International Linear Collider (ILC) predicts unacceptably low uptime with current electronics systems designs. High Availability (HA) analysis is being used as a guideline for all major machine systems including sources, utilities, cryogenics, magnets, power supplies, instrumentation and controls. R&D teams are seeking to achieve total machine high availability with nominal impact on system cost. The focus of this paper is the investigation of commercial standard HA architectures and packaging for Accelerator Controls and Instrumentation. Application of HA design principles to power systems and detector instrumentation are also discussed.

  19. Frequently Asked Questions | The Ames Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Frequently Asked Questions For more information about working with the MPC please visit our Terms & Conditions page. Purity FAQ Why do we need high purity metals? How pure are Ames Laboratory's rare earth metals? When discussing purity, what do you mean by 5N or 3N? What is the basis for purity? What is the difference between atomic and weight based reporting? What is the measurement error? Stoichiometry FAQ How do you achieve precise stoichiometry in alloying? Will the true stoichiometry

  20. High Performance Sustainable Building

    Broader source: Directives, Delegations, and Requirements [Office of Management (MA)]

    2008-06-20

    The guide supports DOE O 413.3A and provides useful information on the incorporation of high performance sustainable building principles into building-related General Plant Projects and Institutional General Plant Projects at DOE sites. Canceled by DOE G 413.3-6A. Does not cancel other directives.

  1. High speed door assembly

    DOE Patents [OSTI]

    Shapiro, C.

    1993-04-27

    A high speed door assembly is described, comprising an actuator cylinder and piston rods, a pressure supply cylinder and fittings, an electrically detonated explosive bolt, a honeycomb structured door, a honeycomb structured decelerator, and a structural steel frame encasing the assembly to close over a 3 foot diameter opening within 50 milliseconds of actuation, to contain hazardous materials and vapors within a test fixture.

  2. High Impact Technology Hub

    Broader source: Energy.gov [DOE]

    The High Impact Technology Hub is a one stop shop for information associated with technology demonstrations in occupied, operational buildings. Resources posted to Hub should accelerate the selection and evaluation of technology demonstration projects and enable transparency into DOEs market stimulation and tech to market activities.

  3. High Power Cryogenic Targets

    SciTech Connect (OSTI)

    Gregory Smith

    2011-08-01

    The development of high power cryogenic targets for use in parity violating electron scattering has been a crucial ingredient in the success of those experiments. As we chase the precision frontier, the demands and requirements for these targets have grown accordingly. We discuss the state of the art, and describe recent developments and strategies in the design of the next generation of these targets.

  4. CSTI high capacity power

    SciTech Connect (OSTI)

    Winter, J.M.

    1994-09-01

    The SP-100 program was established in 1983 by DOD, DOE, and NASA as a joint program to develop the technology necessary for space nuclear power systems for military and civil application. During FY86 and 87, the NASA SP-100 Advanced Technology Program was devised to maintain the momentum of promising technology advancement efforts started during Phase I of SP-100 and to strengthen, in key areas, the chances for successful development and growth capability of space nuclear reactor power systems for future space applications. In FY88, the Advanced Technology Program was incorporated into NASA`s new Civil Space Technology Initiative (CSTI). The CSTI Program was established to provide the foundation for technology development in automation and robotics, information, propulsion, and power. The CSTI High Capacity Power Program builds on the technology efforts of the SP-100 program, incorporates the previous NASA SP-100 Advanced Technology project, and provides a bridge to NASA Project Pathfinder. The elements of CSTI High Capacity Power development include Conversion Systems, Thermal Management, Power Management, System Diagnostics, and Environmental Interactions. Technology advancement in all areas, including materials, is required to assure the high reliability and 7 to 10 year lifetime demanded for future space nuclear power systems. The overall program will develop and demonstrate the technology base required to provide a wide range of modular power systems as well as allowing mission independence from solar and orbital attitude requirements. Several recent advancements in CSTI High Capacity power development will be discussed.

  5. High Temperature ESP Monitoring

    Broader source: Energy.gov [DOE]

    The purpose of the High Temperature ESP Monitoring project is to develop a down-hole monitoring system to be used in wells with bottom hole temperature up to 300 °C for measuring motor temperature; pump discharge pressure; and formation temperature and pressure.

  6. Highly oxidized superconductors

    DOE Patents [OSTI]

    Morris, Donald E. (Kensington, CA)

    1994-01-01

    Novel superconducting materials in the form of compounds, structures or phases are formed by performing otherwise known syntheses in a highly oxidizing atmosphere rather than that created by molecular oxygen at atmospheric pressure or below. This leads to the successful synthesis of novel superconducting compounds which are thermodynamically stable at the conditions under which they are formed.

  7. Highly oxidized superconductors

    DOE Patents [OSTI]

    Morris, D.E.

    1994-09-20

    Novel superconducting materials in the form of compounds, structures or phases are formed by performing otherwise known synthesis in a highly oxidizing atmosphere rather than that created by molecular oxygen at atmospheric pressure or below. This leads to the successful synthesis of novel superconducting compounds which are thermodynamically stable at the conditions under which they are formed. 16 figs.

  8. High expression Zymomonas promoters

    DOE Patents [OSTI]

    Viitanen, Paul V.; Tao, Luan; Zhang, Yuying; Caimi, Perry G.; McCole, Laura : Zhang, Min; Chou, Yat-Chen; McCutchen, Carol M.; Franden, Mary Ann

    2011-08-02

    Identified are mutants of the promoter of the Z. mobilis glyceraldehyde-3-phosphate dehydrogenase gene, which direct improved expression levels of operably linked heterologous nucleic acids. These are high expression promoters useful for expression of chimeric genes in Zymomonas, Zymobacter, and other related bacteria.

  9. WDR-PK-AK-018

    SciTech Connect (OSTI)

    Hollister, R

    2009-08-26

    Method - CES SOP-HW-P556 'Field and Bulk Gamma Analysis'. Detector - High-purity germanium, 40% relative efficiency. Calibration - The detector was calibrated on February 8, 2006 using a NIST-traceable sealed source, and the calibration was verified using an independent sealed source. Count Time and Geometry - The sample was counted for 20 minutes at 72 inches from the detector. A lead collimator was used to limit the field-of-view to the region of the sample. The drum was rotated 180 degrees halfway through the count time. Date and Location of Scans - June 1,2006 in Building 235 Room 1136. Spectral Analysis Spectra were analyzed with ORTEC GammaVision software. Matrix and geometry corrections were calculated using OR TEC Isotopic software. A background spectrum was measured at the counting location. No man-made radioactivity was observed in the background. Results were determined from the sample spectra without background subtraction. Minimum detectable activities were calculated by the Nureg 4.16 method. Results - Detected Pu-238, Pu-239, Am-241 and Am-243.

  10. Rain-Induced Increase in Background Radiation Detected by Radiation Portal Monitors

    SciTech Connect (OSTI)

    Hausladen, Paul; Blessinger, Christopher S; Guzzardo, Tyler; Livesay, Jake

    2012-07-01

    A complete understanding of both the steady state and transient background measured by Radiation Portal Monitors (RPMs) is essential to predictable system performance, as well as maximization of detection sensitivity. To facilitate this understanding, a test bed for the study of natural background in RPMs has been established at the Oak Ridge National Laboratory. This work was performed in support of the Second Line of Defense Program's mission to detect the illicit movement of nuclear material. In the present work, transient increases in gamma ray counting rates in RPMs due to rain are investigated. The increase in background activity associated with rain, which has been well documented in the field of environmental radioactivity, originates from the atmospheric deposition of two radioactive daughters of radon-222, namely lead-214 and bismuth-214 (henceforth {sup 222}Rn, {sup 214}Pb and {sup 214}Bi). In this study, rainfall rates recorded by a co-located weather station are compared with RPM count rates and High Purity Germanium spectra. The data verifies these radionuclides are responsible for the dominant transient natural background fluctuations in RPMs. Effects on system performance and potential mitigation strategies are discussed.

  11. Majorana Thermosyphon Prototype Experimental Results

    SciTech Connect (OSTI)

    Fast, James E.; Reid, Douglas J.; Aguayo Navarrete, Estanislao

    2010-12-17

    Objective The Majorana demonstrator will operate at liquid Nitrogen temperatures to ensure optimal spectrometric performance of its High Purity Germanium (HPGe) detector modules. In order to transfer the heat load of the detector module, the Majorana demonstrator requires a cooling system that will maintain a stable liquid nitrogen temperature. This cooling system is required to transport the heat from the detector chamber outside the shield. One approach is to use the two phase liquid-gas equilibrium to ensure constant temperature. This cooling technique is used in a thermosyphon. The thermosyphon can be designed so the vaporization/condensing process transfers heat through the shield while maintaining a stable operating temperature. A prototype of such system has been built at PNNL. This document presents the experimental results of the prototype and evaluates the heat transfer performance of the system. The cool down time, temperature gradient in the thermosyphon, and heat transfer analysis are studied in this document with different heat load applied to the prototype.

  12. Splitting of the pygmy dipole resonance in {sup 138}Ba and {sup 140}Ce observed in the ({alpha},{alpha}{sup '}{gamma}) reaction

    SciTech Connect (OSTI)

    Endres, J.; Hasper, J.; Zilges, A.; Savran, D.; Berg, A. M. van den; Dendooven, P.; Woertche, H. J.; Fritzsche, M.; Harakeh, M. N.

    2009-09-15

    The N=82 nuclei {sup 140}Ce and {sup 138}Ba have been investigated by means of the ({alpha},{alpha}{sup '}{gamma}) coincidence method to study the pygmy dipole resonance (PDR). The experiments have been performed at the AGOR cyclotron at KVI, Groningen, at a primary beam energy of E{sub {alpha}}=136 MeV. The Big-Bite Spectrometer and seven large-volume high-purity germanium detectors were used in coincidence to perform a simultaneous spectroscopy of the scattered {alpha} particles and the {gamma} decay. The comparison with results of nuclear resonance fluorescence experiments reveals a splitting of the PDR into two components. Up to about 6 MeV the same states that could be observed in ({gamma},{gamma}{sup '}) are also excited in {alpha}-scattering experiments, whereas the higher-lying states are missing in the ({alpha},{alpha}{sup '}{gamma}) reaction. This indicates a structural splitting of the PDR into two modes with different underlying structure.

  13. Assessing Lanthanum-Bromide Detectors for Safeguards Applications

    SciTech Connect (OSTI)

    Gariazzo, Claudio Andres; Saavedra, Steven F; Smith, Steven E; Solodov, Alexander A

    2008-01-01

    Major detector technologies currently being used for gamma-ray spectroscopy in safeguards applications include systems based on sodium iodide (NaI), cadmium-zinc-telluride (CZT), cadmium-telluride (CdTe), and high-purity germanium (HPGe) crystals. Recently, a new scintillation detector based on a lanthanum bromide (LaBr3) crystal has become commercially available. The declared benefits of this new detector technology include higher resolution and improved efficiency compared with similarly configured NaI-based systems. Both detector systems offer the advantage of room-temperature operation. This paper describes the results of a study assessing the safeguards applicability and advantages for isotopic and quantitative analyses of uranium using the LaBr3-based detector, as well as an investigation into the general operating characteristics of the LaBr3-based detector. The results are compared with those from a widely used NaI-based detector system (Canberra's Inspector-1000 multichannel analyzer) operated under similar environmental conditions and hardware configuration, using commercially available software packages (NaIGEM and Genie-2000).

  14. Thermoelectrics Partnership: High Performance Thermoelectric...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    High Performance Thermoelectric Waste Heat Recovery System Based on Zintl Phase Materials with Embedded Nanoparticles Thermoelectrics Partnership: High Performance Thermoelectric...

  15. High Selectivity Oxygen Delignification

    SciTech Connect (OSTI)

    Arthur J. Ragauskas Lucian A. Lucia Hasan Jameel

    2005-09-30

    The overall objective of this program was to develop improved extended oxygen delignification (EOD) technologies for current U.S. pulp mill operations. This was accomplished by: (1) Identifying pulping conditions that optimize O and OO performance; (2) Identifying structural features of lignin that enhance reactivity towards EOD of high kappa pulps; (3) Identifying factors minimizing carbohydrate degradation and improve pulp strength of EOD high kappa pulps; (4) Developing a simple, reproducible method of quantifying yield gains from EOD; and (5) Developing process conditions that significantly reduce the capital requirements of EOD while optimizing the yield benefits. Key research outcomes included, demonstrating the use of a mini-O sequence such as (E+O)Dkf:0.05(E+O) or Dkf:0.05(E+O)(E+O) without interstage washing could capture approximately 60% of the delignification efficiency of a conventional O-stage without the major capital requirements associated with an O-stage for conventional SW kraft pulps. The rate of formation and loss of fiber charge during an O-stage stage can be employed to maximize net fiber charge. Optimal fiber charge development and delignification are two independent parameters and do not parallel each other. It is possible to utilize an O-stage to enhance overall cellulosic fiber charge of low and high kappa SW kraft pulps which is beneficial for physical strength properties. The application of NIR and multi-variant analysis was developed into a rapid and simple method of determining the yield of pulp from an oxygen delignification stage that has real-world mill applications. A focus point of this program was the demonstration that Kraft pulping conditions and oxygen delignification of high and low-kappa SW and HW pulps are intimately related. Improved physical pulp properties and yield can be delivered by controlling the H-factor and active alkali charge. Low AA softwood kraft pulp with a kappa number 30 has an average improvement of 2% in yield and 4 cP in viscosity in comparison to high AA pulp for the oxygen delignification. This difference is also seen for high-kappa SW kraft pulps with an average improvement of {approx}3% in yield and 3 cP in viscosity for low AA high kappa number 50 pulp. Low AA hardwood kappa number 20 pulp had an average improvement of {approx}4% in yield and 6-12 cP in viscosity as compared to high AA pulp. Lower kraft cooking temperature (160 vs. 170 C) in combination with the medium AA provides a practical approach for integrating high kappa pulping of hardwoods (i.e., low rejects) with an advanced extended oxygen delignification stage. ECF pulp bleaching of low and high kappa kraft SW and HW pulps exhibit comparable optical and physical strength properties when bleached D(EPO)D.

  16. Aluminum for bonding Si-Ge alloys to graphite

    DOE Patents [OSTI]

    Eggemann, Robert V.

    1976-01-13

    Improved thermoelectric device and process, comprising the high-temperature, vacuum bonding of a graphite contact and silicon-germanium thermoelectric element by the use of a low void, aluminum, metallurgical shim with low electrical resistance sandwiched therebetween.

  17. Systems Analyses of Advanced Brayton Cycles For High Efficiency Zero Emission Plants

    SciTech Connect (OSTI)

    A. D. Rao; J. Francuz; H. Liao; A. Verma; G. S. Samuelsen

    2006-11-01

    Table 1 shows that the systems efficiency, coal (HHV) to power, is 35%. Table 2 summarizes the auxiliary power consumption within the plant. Thermoflex was used to simulate the power block and Aspen Plus the balance of plant. The overall block flow diagram is presented in Figure A1.3-1 and the key unit process flow diagrams are shown in subsequent figures. Stream data are given in Table A1.3-1. Equipment function specifications are provided in Tables A1.3-2 through 17. The overall plant scheme consists of a cryogenic air separation unit supplying 95% purity O{sub 2} to GE type high pressure (HP) total quench gasifiers. The raw gas after scrubbing is treated in a sour shift unit to react the CO with H{sub 2}O to form H{sub 2} and CO{sub 2}. The gas is further treated to remove Hg in a sulfided activated carbon bed. The syngas is desulfurized and decarbonized in a Selexol acid gas removal unit and the decarbonized syngas after humidification and preheat is fired in GE 7H type steam cooled gas turbines. Intermediate pressure (IP) N{sub 2} from the ASU is also supplied to the combustors of the gas turbines as additional diluent for NOx control. A portion of the air required by the ASU is extracted from the gas turbines. The plant consists of the following major process units: (1) Air Separation Unit (ASU); (2) Gasification Unit; (3) CO Shift/Low Temperature Gas Cooling (LTGC) Unit; (4) Acid Gas Removal Unit (AGR) Unit; (5) Fuel Gas Humidification Unit; (6) Carbon Dioxide Compression/Dehydration Unit; (7) Claus Sulfur Recovery/Tail Gas Treating Unit (SRU/TGTU); and (8) Power Block.

  18. Fast high-temperature superconductor switch for high current applications

    Office of Scientific and Technical Information (OSTI)

    (Journal Article) | SciTech Connect Fast high-temperature superconductor switch for high current applications Citation Details In-Document Search Title: Fast high-temperature superconductor switch for high current applications Reversible operation of a high current superconductor switch based on the quench of high-resistance second generation high temperature superconducting wire is demonstrated. The quench is induced by a burst of an ac field generated by an inductively coupled

  19. Gamma-Ray Library and Uncertainty Analysis: Passively Emitted Gamma Rays Used in Safeguards Technology

    SciTech Connect (OSTI)

    Parker, W

    2009-09-18

    Non-destructive gamma-ray analysis is a fundamental part of nuclear safeguards, including nuclear energy safeguards technology. Developing safeguards capabilities for nuclear energy will certainly benefit from the advanced use of gamma-ray spectroscopy as well as the ability to model various reactor scenarios. There is currently a wide variety of nuclear data that could be used in computer modeling and gamma-ray spectroscopy analysis. The data can be discrepant (with varying uncertainties), and it may difficult for a modeler or software developer to determine the best nuclear data set for a particular situation. To use gamma-ray spectroscopy to determine the relative isotopic composition of nuclear materials, the gamma-ray energies and the branching ratios or intensities of the gamma-rays emitted from the nuclides in the material must be well known. A variety of computer simulation codes will be used during the development of the nuclear energy safeguards, and, to compare the results of various codes, it will be essential to have all the {gamma}-ray libraries agree. Assessing our nuclear data needs allows us to create a prioritized list of desired measurements, and provides uncertainties for energies and especially for branching intensities. Of interest are actinides, fission products, and activation products, and most particularly mixtures of all of these radioactive isotopes, including mixtures of actinides and other products. Recent work includes the development of new detectors with increased energy resolution, and studies of gamma-rays and their lines used in simulation codes. Because new detectors are being developed, there is an increased need for well known nuclear data for radioactive isotopes of some elements. Safeguards technology should take advantage of all types of gamma-ray detectors, including new super cooled detectors, germanium detectors and cadmium zinc telluride detectors. Mixed isotopes, particularly mixed actinides found in nuclear reactor streams can be especially challenging to identify. The super cooled detectors have a marked improvement in energy resolution, allowing the possibility of deconvolution of mixtures of gamma rays that was unavailable with high purity germanium detectors. Isotopic analysis codes require libraries of gamma rays. In certain situations, isotope identification can be made in the field, sometimes with a short turnaround time, depending on the choice of detector and software analysis package. Sodium iodide and high purity germanium detectors have been successfully used in field scenarios. The newer super cooled detectors offer dramatically increased resolution, but they have lower efficiency and so can require longer collection times. The different peak shapes require software development for the specific detector type and field application. Libraries can be tailored to specific scenarios; by eliminating isotopes that are certainly not present, the analysis time may be shortened and the accuracy may be increased. The intent of this project was to create one accurate library of gamma rays emitted from isotopes of interest to be used as a reliable reference in safeguards work. All simulation and spectroscopy analysis codes can draw upon this best library to improve accuracy and cross-code consistency. Modeling codes may include MCNP and COG. Gamma-ray spectroscopy analysis codes may include MGA, MGAU, U235 and FRAM. The intent is to give developers and users the tools to use in nuclear energy safeguards work. In this project, the library created was limited to a selection of actinide isotopes of immediate interest to reactor technology. These isotopes included {sup 234-238}U, {sup 237}Np, {sup 238-242}Pu, {sup 241,243}Am and {sup 244}Cm. These isotopes were examined, and the best of gamma-ray data, including line energies and relative strengths were selected.

  20. High-performance steels

    SciTech Connect (OSTI)

    Barsom, J.M.

    1996-03-01

    Steel is the material of choice in structures such as storage tanks, gas and oil distribution pipelines, high-rise buildings, and bridges because of its strength, ductility, and fracture toughness, as well as its repairability and recyclability. Furthermore, these properties are continually being improved via advances in steelmaking, casting, rolling, and chemistry. Developments in steelmaking have led to alloys having low sulfur, sulfide shape control, and low hydrogen. They provide reduced chemical segregation, higher fracture toughness, better through-thickness and weld heat-affected zone properties, and lower susceptibility to hydrogen cracking. Processing has moved beyond traditional practices to designed combinations of controlled rolling and cooling known as thermomechanical control processes (TMCP). In fact, chemical composition control and TMCP now enable such precise adjustment of final properties that these alloys are now known as high-performance steels (HPS), engineered materials having properties tailored for specific applications.

  1. High frequency reference electrode

    DOE Patents [OSTI]

    Kronberg, J.W.

    1994-05-31

    A high frequency reference electrode for electrochemical experiments comprises a mercury-calomel or silver-silver chloride reference electrode with a layer of platinum around it and a layer of a chemically and electrically resistant material such as TEFLON around the platinum covering all but a small ring or halo' at the tip of the reference electrode, adjacent to the active portion of the reference electrode. The voltage output of the platinum layer, which serves as a redox electrode, and that of the reference electrode are coupled by a capacitor or a set of capacitors and the coupled output transmitted to a standard laboratory potentiostat. The platinum may be applied by thermal decomposition to the surface of the reference electrode. The electrode provides superior high-frequency response over conventional electrodes. 4 figs.

  2. High frequency reference electrode

    DOE Patents [OSTI]

    Kronberg, James W.

    1994-01-01

    A high frequency reference electrode for electrochemical experiments comprises a mercury-calomel or silver-silver chloride reference electrode with a layer of platinum around it and a layer of a chemically and electrically resistant material such as TEFLON around the platinum covering all but a small ring or "halo" at the tip of the reference electrode, adjacent to the active portion of the reference electrode. The voltage output of the platinum layer, which serves as a redox electrode, and that of the reference electrode are coupled by a capacitor or a set of capacitors and the coupled output transmitted to a standard laboratory potentiostat. The platinum may be applied by thermal decomposition to the surface of the reference electrode. The electrode provides superior high-frequency response over conventional electrodes.

  3. High Temperature ESP Monitoring

    SciTech Connect (OSTI)

    Jack Booker; Brindesh Dhruva

    2011-06-20

    The objective of the High Temperature ESP Monitoring project was to develop a downhole monitoring system to be used in wells with bottom hole well temperatures up to 300C for measuring motor temperature, formation pressure, and formation temperature. These measurements are used to monitor the health of the ESP motor, to track the downhole operating conditions, and to optimize the pump operation. A 220 C based High Temperature ESP Monitoring system was commercially released for sale with Schlumberger ESP motors April of 2011 and a 250 C system with will be commercially released at the end of Q2 2011. The measurement system is now fully qualified, except for the sensor, at 300 C.

  4. High temperature probe

    DOE Patents [OSTI]

    Swan, Raymond A.

    1994-01-01

    A high temperature probe for sampling, for example, smokestack fumes, and is able to withstand temperatures of 3000.degree. F. The probe is constructed so as to prevent leakage via the seal by placing the seal inside the water jacket whereby the seal is not exposed to high temperature, which destroys the seal. The sample inlet of the probe is also provided with cooling fins about the area of the seal to provide additional cooling to prevent the seal from being destroyed. Also, a heated jacket is provided for maintaining the temperature of the gas being tested as it passes through the probe. The probe includes pressure sensing means for determining the flow velocity of an efficient being sampled. In addition, thermocouples are located in various places on the probe to monitor the temperature of the gas passing there through.

  5. High temperature measuring device

    DOE Patents [OSTI]

    Tokarz, Richard D.

    1983-01-01

    A temperature measuring device for very high design temperatures (to 2,000.degree. C.). The device comprises a homogenous base structure preferably in the form of a sphere or cylinder. The base structure contains a large number of individual walled cells. The base structure has a decreasing coefficient of elasticity within the temperature range being monitored. A predetermined quantity of inert gas is confined within each cell. The cells are dimensionally stable at the normal working temperature of the device. Increases in gaseous pressure within the cells will permanently deform the cell walls at temperatures within the high temperature range to be measured. Such deformation can be correlated to temperature by calibrating similarly constructed devices under known time and temperature conditions.

  6. High efficiency gas burner

    DOE Patents [OSTI]

    Schuetz, Mark A. (Belmont, MA)

    1983-01-01

    A burner assembly provides for 100% premixing of fuel and air by drawing the air into at least one high velocity stream of fuel without power assist. Specifically, the nozzle assembly for injecting the fuel into a throat comprises a plurality of nozzles in a generally circular array. Preferably, swirl is imparted to the air/fuel mixture by angling the nozzles. The diffuser comprises a conical primary diffuser followed by a cusp diffuser.

  7. High-speed

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    speed three-wave polarimeter-interferometer diagnostic for Madison symmetric torus B. H. Deng, D. L. Brower, and W. X. Ding Electrical Engineering Department, University of California, Los Angeles, California 90095 M. D. Wyman, B. E. Chapman, and J. S. Sarff Department of Physics, University of Wisconsin, Madison, Wisconsin 53706 ͑Received 5 May 2006; presented on 10 May 2006; accepted 11 June 2006; published online 27 September 2006͒ A high-speed three-wave polarimeter-interferometer

  8. High current ion source

    DOE Patents [OSTI]

    Brown, Ian G. (1088 Woodside Rd., Berkeley, CA 94708); MacGill, Robert A. (645 Kern St., Richmond, CA 94805); Galvin, James E. (2 Commodore Dr. #276, Emeryville, CA 94608)

    1990-01-01

    An ion source utilizing a cathode and anode for producing an electric arc therebetween. The arc is sufficient to vaporize a portion of the cathode to form a plasma. The plasma leaves the generation region and expands through another regon. The density profile of the plasma may be flattened using a magnetic field formed within a vacuum chamber. Ions are extracted from the plasma to produce a high current broad on beam.

  9. high renewable energy penetration

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    high renewable energy penetration - Sandia Energy Energy Search Icon Sandia Home Locations Contact Us Employee Locator Energy & Climate Secure & Sustainable Energy Future Stationary Power Energy Conversion Efficiency Solar Energy Wind Energy Water Power Supercritical CO2 Geothermal Natural Gas Safety, Security & Resilience of the Energy Infrastructure Energy Storage Nuclear Power & Engineering Grid Modernization Battery Testing Nuclear Fuel Cycle Defense Waste Management Programs

  10. high-power LEDs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    high-power LEDs - Sandia Energy Energy Search Icon Sandia Home Locations Contact Us Employee Locator Energy & Climate Secure & Sustainable Energy Future Stationary Power Energy Conversion Efficiency Solar Energy Wind Energy Water Power Supercritical CO2 Geothermal Natural Gas Safety, Security & Resilience of the Energy Infrastructure Energy Storage Nuclear Power & Engineering Grid Modernization Battery Testing Nuclear Fuel Cycle Defense Waste Management Programs Advanced Nuclear

  11. High Performance Window Attachments

    Energy Savers [EERE]

    High Performance Window Attachments D. Charlie Curcija Lawrence Berkeley National Laboratory dccurcija@lbl.gov 510-495-2602 April 4, 2013 2 | Building Technologies Office eere.energy.gov Purpose & Objectives Impact of Project: * Motivate manufacturers to make improvements in Window systems U-Factors, SHGC and daylighting utilization * Increase awareness of benefits from energy efficient window attachments Problem Statement: * A wide range of residential window attachments are available, but

  12. High voltage pulse conditioning

    DOE Patents [OSTI]

    Springfield, Ray M. (Sante Fe, NM); Wheat, Jr., Robert M. (Los Alamos, NM)

    1990-01-01

    Apparatus for conditioning high voltage pulses from particle accelerators in order to shorten the rise times of the pulses. Flashover switches in the cathode stalk of the transmission line hold off conduction for a determinable period of time, reflecting the early portion of the pulses. Diodes upstream of the switches divert energy into the magnetic and electrostatic storage of the capacitance and inductance inherent to the transmission line until the switches close.

  13. High Energy Density Microwaves

    SciTech Connect (OSTI)

    Phillips, R.M. [Stanford Linear Accelerator Center, Stanford, CA 94309 (United States)

    1999-04-01

    These proceedings represent papers presented at the RF98 Workshop entitled `High Energy Density Microwaves` held in California in October, 1998. The topics discussed were predominantly accelerator{minus}related. The Workshop dealt, for the most part, with the generation and control of electron beams, the amplification of RF signals, the design of mode converters, and the effect of very high RF field gradients. This Workshop was designed to address the concerns of the microwave tube industry worldwide, the plasma physicists who deal with very high beam currents and gigawatts of RF power, and researchers in accelerator centers around the world. Papers were presented on multibeam klystrons, gyrotron development, plasmas in microwave tubes, RF breakdown, and alternatives to conventional linear coliders at 1 TeV and above. The Workshop was partially sponsored by the US Department of Energy. There were 46 papers presented at the conference,out of which 19 have been abstracted for the Energy,Science and Technology database.(AIP)

  14. High pressure ceramic joint

    DOE Patents [OSTI]

    Ward, Michael E. (Poway, CA); Harkins, Bruce D. (San Diego, CA)

    1993-01-01

    Many recuperators have components which react to corrosive gases and are used in applications where the donor fluid includes highly corrosive gases. These recuperators have suffered reduced life, increased service or maintenance, and resulted in increased cost. The present joint when used with recuperators increases the use of ceramic components which do not react to highly corrosive gases. Thus, the present joint used with the present recuperator increases the life, reduces the service and maintenance, and reduces the increased cost associated with corrosive action of components used to manufacture recuperators. The present joint is comprised of a first ceramic member, a second ceramic member, a mechanical locking device having a groove defined in one of the first ceramic member and the second ceramic member. The joint and the mechanical locking device is further comprised of a refractory material disposed in the groove and contacting the first ceramic member and the second ceramic member. The present joint mechanically provides a high strength load bearing joint having good thermal cycling characteristics, good resistance to a corrosive environment and good steady state strength at elevated temperatures.

  15. High pressure ceramic joint

    DOE Patents [OSTI]

    Ward, M.E.; Harkins, B.D.

    1993-11-30

    Many recuperators have components which react to corrosive gases and are used in applications where the donor fluid includes highly corrosive gases. These recuperators have suffered reduced life, increased service or maintenance, and resulted in increased cost. The present joint when used with recuperators increases the use of ceramic components which do not react to highly corrosive gases. Thus, the present joint used with the present recuperator increases the life, reduces the service and maintenance, and reduces the increased cost associated with corrosive action of components used to manufacture recuperators. The present joint is comprised of a first ceramic member, a second ceramic member, a mechanical locking device having a groove defined in one of the first ceramic member and the second ceramic member. The joint and the mechanical locking device is further comprised of a refractory material disposed in the groove and contacting the first ceramic member and the second ceramic member. The present joint mechanically provides a high strength load bearing joint having good thermal cycling characteristics, good resistance to a corrosive environment and good steady state strength at elevated temperatures. 4 figures.

  16. High energy physics

    SciTech Connect (OSTI)

    Kernan, A.; Shen, B.C.; Ma, E.

    1997-07-01

    This proposal is for the continuation of the High Energy Physics program at the University of California at Riverside. In hadron collider physics the authors will complete their transition from experiment UA1 at CERN to the DZERO experiment at Fermilab. On experiment UA1 their effort will concentrate on data analysis at Riverside. At Fermilab they will coordinate the high voltage system for all detector elements. They will also carry out hardware/software development for the D0 muon detector. The TPC/Two-Gamma experiment has completed its present phase of data-taking after accumulating 160 pb{sup {minus}}1 of luminosity. The UC Riverside group will continue data and physics analysis and make minor hardware improvement for the high luminosity run. The UC Riverside group is participating in design and implementation of the data acquisition system for the OPAL experiment at LEP. Mechanical and electronics construction of the OPAL hadron calorimeter strip readout system is proceeding on schedule. Data analysis and Monte Carlo detector simulation efforts are proceeding in preparation for the first physics run when IEP operation comenses in fall 1989.

  17. High temperature interfacial superconductivity

    DOE Patents [OSTI]

    Bozovic, Ivan (Mount Sinai, NY); Logvenov, Gennady (Port Jefferson Station, NY); Gozar, Adrian Mihai (Port Jefferson, NY)

    2012-06-19

    High-temperature superconductivity confined to nanometer-scale interfaces has been a long standing goal because of potential applications in electronic devices. The spontaneous formation of a superconducting interface in bilayers consisting of an insulator (La.sub.2CuO.sub.4) and a metal (La.sub.1-xSr.sub.xCuO.sub.4), neither of which is superconducting per se, is described. Depending upon the layering sequence of the bilayers, T.sub.c may be either .about.15 K or .about.30 K. This highly robust phenomenon is confined to within 2-3 nm around the interface. After exposing the bilayer to ozone, T.sub.c exceeds 50 K and this enhanced superconductivity is also shown to originate from a 1 to 2 unit cell thick interfacial layer. The results demonstrate that engineering artificial heterostructures provides a novel, unconventional way to fabricate stable, quasi two-dimensional high T.sub.c phases and to significantly enhance superconducting properties in other superconductors. The superconducting interface may be implemented, for example, in SIS tunnel junctions or a SuFET.

  18. Apparatus and process for the refrigeration, liquefaction and separation of gases with varying levels of purity

    DOE Patents [OSTI]

    Bingham, Dennis N. (Idaho Falls, ID); Wilding, Bruce M. (Idaho Falls, ID); McKellar, Michael G. (Idaho Falls, ID)

    2002-01-01

    A process for the separation and liquefaction of component gasses from a pressurized mix gas stream is disclosed. The process involves cooling the pressurized mixed gas stream in a heat exchanger so as to condensing one or more of the gas components having the highest condensation point; separating the condensed components from the remaining mixed gas stream in a gas-liquid separator; cooling the separated condensed component stream by passing it through an expander; and passing the cooled component stream back through the heat exchanger such that the cooled component stream functions as the refrigerant for the heat exchanger. The cycle is then repeated for the remaining mixed gas stream so as to draw off the next component gas and further cool the remaining mixed gas stream. The process continues until all of the component gases are separated from the desired gas stream. The final gas stream is then passed through a final heat exchanger and expander. The expander decreases the pressure on the gas stream, thereby cooling the stream and causing a portion of the gas stream to liquify within a tank. The portion of the gas which is hot liquefied is passed back through each of the heat exchanges where it functions as a refrigerant.

  19. Apparatus and process for the refrigeration, liquefaction and separation of gases with varying levels of purity

    DOE Patents [OSTI]

    Bingham, Dennis N. (Idaho Falls, ID); Wilding, Bruce M. (Idaho Falls, ID); McKellar, Michael G. (Idaho Falls, ID)

    2000-01-01

    A process for the separation and liquefaction of component gasses from a pressurized mix gas stream is disclosed. The process involves cooling the pressurized mixed gas stream in a heat exchanger so as to condense one or more of the gas components having the highest condensation point; separating the condensed components from the remaining mixed gas stream in a gas-liquid separator; cooling the separated condensed component stream by passing it through an expander; and passing the cooled component stream back through the heat exchanger such that the cooled component stream functions as the refrigerant for the heat exchanger. The cycle is then repeated for the remaining mixed gas stream so as to draw off the next component gas and further cool the remaining mixed gas stream. The process continues until all of the component gases are separated from the desired gas stream. The final gas stream is then passed through a final heat exchanger and expander. The expander decreases the pressure on the gas stream, thereby cooling the stream and causing a portion of the gas stream to liquify within a tank. The portion of the gas which is not liquefied is passed back through each of the heat exchanges where it functions as a refrigerant.

  20. High mobility high efficiency organic films based on pure organic materials

    DOE Patents [OSTI]

    Salzman, Rhonda F. (Ann Arbor, MI); Forrest, Stephen R. (Ann Arbor, MI)

    2009-01-27

    A method of purifying small molecule organic material, performed as a series of operations beginning with a first sample of the organic small molecule material. The first step is to purify the organic small molecule material by thermal gradient sublimation. The second step is to test the purity of at least one sample from the purified organic small molecule material by spectroscopy. The third step is to repeat the first through third steps on the purified small molecule material if the spectroscopic testing reveals any peaks exceeding a threshold percentage of a magnitude of a characteristic peak of a target organic small molecule. The steps are performed at least twice. The threshold percentage is at most 10%. Preferably the threshold percentage is 5% and more preferably 2%. The threshold percentage may be selected based on the spectra of past samples that achieved target performance characteristics in finished devices.

  1. HIGH EFFICIENCY SYNGAS GENERATION

    SciTech Connect (OSTI)

    Robert J. Copeland; Yevgenia Gershanovich; Brian Windecker

    2005-02-01

    This project investigated an efficient and low cost method of auto-thermally reforming natural gas to hydrogen and carbon monoxide. Reforming is the highest cost step in producing products such as methanol and Fisher Tropsch liquids (i.e., gas to liquids); and reducing the cost of reforming is the key to reducing the cost of these products. Steam reforming is expensive because of the high cost of the high nickel alloy reforming tubes (i.e., indirectly fired reforming tubes). Conventional auto-thermal or Partial Oxidation (POX) reforming minimizes the size and cost of the reformers and provides a near optimum mixture of CO and hydrogen. However POX requires pure oxygen, which consumes power and significantly increases the cost to reforming. Our high efficiency process extracts oxygen from low-pressure air with novel oxygen sorbent and transfers the oxygen to a nickel-catalyzed reformer. The syngas is generated at process pressure (typically 20 to 40 bar) without nitrogen dilution and has a 1CO to 2H{sub 2} ratio that is near optimum for the subsequent production of Fisher-Tropsch liquid to liquids and other chemicals (i.e., Gas to Liquids, GTL). Our high process efficiency comes from the way we transfer the oxygen into the reformer. All of the components of the process, except for the oxygen sorbent, are commonly used in commercial practice. A process based on a longlived, regenerable, oxygen transfer sorbent could substantially reduce the cost of natural gas reforming to syngas. Lower cost syngas (CO + 2H{sub 2}) that is the feedstock for GTL would reduce the cost of GTL and for other commercial applications (e.g., methanol, other organic chemicals). The vast gas resources of Alaska's North Slope (ANS) offer more than 22 Tcf of gas and GTL production in this application alone, and could account for as much as 300,000 to 700,000 bpd for 20 to 30+ years. We developed a new sorbent, which is an essential part of the High Efficiency Oxygen Process (HOP). We tested the sorbent and observed that it has both a good oxygen capacity and operates as a highly effective reforming catalyst. We conducted a long duration tests of the sorbent (1,500 hours of continuous operation in the HOP cycle). Although the sorbent lost some oxygen capacity with cycling, the sorbent oxygen capacity stabilized after 1,000 hours and remained constant to the end of the test, 1,500 hour. The activity of the catalyst to reform methane to a hydrogen and carbon monoxide mixture was unchanged through the oxidation/reduction cycling. Our cost and performance analyses indicated a significant reduction in the cost of GTL production when using the HOP process integrated into a GTL plant.

  2. High efficiency photoionization detector

    DOE Patents [OSTI]

    Anderson, D.F.

    1984-01-31

    A high efficiency photoionization detector is described using tetraaminoethylenes in a gaseous state having a low ionization potential and a relative photoionization cross section which closely matches the emission spectrum of xenon gas. Imaging proportional counters are also disclosed using the novel photoionization detector of the invention. The compound of greatest interest is TMAE which comprises tetrakis(dimethylamino)ethylene which has a measured ionization potential of 5.36 [+-] 0.02 eV, and a vapor pressure of 0.35 torr at 20 C. 6 figs.

  3. High temperature detonator

    DOE Patents [OSTI]

    Johnson, James O. (Los Alamos, NM); Dinegar, Robert H. (Los Alamos, NM)

    1988-01-01

    A detonator assembly is provided which is usable at high temperatures about 300.degree. C. A detonator body is provided with an internal volume defining an anvil surface. A first acceptor explosive is disposed on the anvil surface. A donor assembly having an ignition element, an explosive material, and a flying plate, are placed in the body effective to accelerate the flying plate to impact the first acceptor explosive on the anvil for detonating the first acceptor explosive. A second acceptor explosive is eccentrically located in detonation relationship with the first acceptor explosive to thereafter effect detonation of a main charge.

  4. High Tc Superconductivity

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    by C. Kim (SSRL), D. H. Lu (Stanford), K. M. Shen (Stanford) and Z.-X. Shen (Stanford/SSRL) Extensive research efforts to study the novel electronic properties of high-Tc superconductors and their related materials by angle-resolved photoemission spectroscopy at a recently commissioned Beam Line 5-4 (led by Z.-X. Shen) continue to be successful, producing many important results. These results, which are highlighted by five articles recently published in Physical Review Letters and one in

  5. Manufacturing High Temperature Systems

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Manufacturing and Scale Up Challenges Joseph Hartvigsen Ceramatec, Inc. National Renewable Energy Laboratory Golden, CO February 28, 2014 Antipode Assertions * Electric power generation is not the limitation - To misquote Jay Leno "Use all you want, we'll make more" - http://atomicinsights.com/2013/02/use-all-the-electricity-you-want-well-make-more.html * High electric costs come from working the demand curve from below rather than above * "Grid Storage" is a misleading

  6. Theoretical High Energy Physics

    SciTech Connect (OSTI)

    Christ, Norman H.; Weinberg, Erick J.

    2014-07-14

    we provide reports from each of the six faculty supported by the Department of Energy High Energy Physics Theory grant at Columbia University. Each is followed by a bibliography of the references cited. A complete list of all of the publications in the 12/1/2010-04/30/2014 period resulting from research supported by this grant is provided in the following section. The final section lists the Ph.D. dissertations based on research supported by the grant that were submitted during this period.

  7. High Energy QCD

    SciTech Connect (OSTI)

    Yuri Kovchegov

    2012-05-31

    The project significantly advanced our understanding of the theory of strong interactions known as quantum chromodynamics (QCD) in high energy collisions of elementary particles and nuclei. QCD is one of the four fundamental forces of nature, but is understood quite poorly due to the complexity of strong interactions. This project advanced our understanding of QCD in the very high energy collisions of protons and nuclei, where densities of quarks and gluons inside the colliding particles are so high (due to high energy) that complicated nonlinear interactions between quarks and gluons become important. This regime is known as gluon (or parton) saturation. The result of the project is a significant improvement of our understanding of the physics of gluon saturation: important (running coupling) corrections to the existing description of the process (the so-called Balitsky-Kovchegov equation) have been calculated, placing the BK equation in good agreement with the experimental data on deep inelastic scattering (DIS), a process where an electron is collided with the proton to probe the proton's internal structure. Corresponding cross section for quark and gluon production in DIS and nuclear collisions have been calculated and corrected correspondingly, resulting in new and interesting predictions for the physics to be probed in heavy ion collisions at the Large Hadron Collider (LHC). The dense gluon systems play an important role in collisions of ultrarelativistic large nuclei, which are performed in order to create a plasma of quarks and gluons (QGP). An important question in the field is how exactly this QGP is produced in a collision of two heavy ions. The conclusion of this project is that QGP production happens due to strong coupling effects between quarks and gluons. This made theoretical description of QGP production only possible using the methods emerging from string theory. Using these methods QGP production was well understood as a result of this project. The project was mainly accomplished by analytic calculations, with occasional use of personal computers and a supercomputer to perform numerical calculations. As such it is very economic and technically effective. The benefit to public is by broadening our understanding of fundamental physics. Strong interactions are responsible for about 98$\\%$ of the visible mass in the Universe, and their understanding is vital both for understanding how the Universe works and for which physics lies beyond the known interactions of Standard Model of particle physics.

  8. High flux reactor

    DOE Patents [OSTI]

    Lake, James A.; Heath, Russell L.; Liebenthal, John L.; DeBoisblanc, Deslonde R.; Leyse, Carl F.; Parsons, Kent; Ryskamp, John M.; Wadkins, Robert P.; Harker, Yale D.; Fillmore, Gary N.; Oh, Chang H.

    1988-01-01

    A high flux reactor is comprised of a core which is divided into two symetric segments housed in a pressure vessel. The core segments include at least one radial fuel plate. The spacing between the plates functions as a coolant flow channel. The core segments are spaced axially apart such that a coolant mixing plenum is formed between them. A channel is provided such that a portion of the coolant bypasses the first core section and goes directly into the mixing plenum. The outlet coolant from the first core segment is mixed with the bypass coolant resulting in a lower inlet temperature to the lower core segment.

  9. High speed flywheel

    DOE Patents [OSTI]

    McGrath, Stephen V. (Knoxville, TN)

    1991-01-01

    A flywheel for operation at high speeds utilizes two or more ringlike coments arranged in a spaced concentric relationship for rotation about an axis and an expansion device interposed between the components for accommodating radial growth of the components resulting from flywheel operation. The expansion device engages both of the ringlike components, and the structure of the expansion device ensures that it maintains its engagement with the components. In addition to its expansion-accommodating capacity, the expansion device also maintains flywheel stiffness during flywheel operation.

  10. High power microwave generator

    DOE Patents [OSTI]

    Minich, Roger W. (Patterson, CA)

    1988-01-01

    A device (10) for producing high-powered and coherent microwaves is described. The device comprises an evacuated, cylindrical, and hollow real cathode (20) that is driven to inwardly field emit relativistic electrons. The electrons pass through an internally disposed cylindrical and substantially electron-transparent cylindrical anode (24), proceed toward a cylindrical electron collector electrode (26), and form a cylindrical virtual cathode (32). Microwaves are produced by spatial and temporal oscillations of the cylindrical virtual cathode (32), and by electrons that reflex back and forth between the cylindrical virtual cathode (32) and the cylindrical real cathode (20).

  11. High efficiency photoionization detector

    DOE Patents [OSTI]

    Anderson, David F.

    1984-01-01

    A high efficiency photoionization detector using tetraaminoethylenes in a gaseous state having a low ionization potential and a relative photoionization cross section which closely matches the emission spectrum of xenon gas. Imaging proportional counters are also disclosed using the novel photoionization detector of the invention. The compound of greatest interest is TMAE which comprises tetrakis(dimethylamino)ethylene which has a measured ionization potential of 5.36.+-.0.02 eV, and a vapor pressure of 0.35 torr at 20.degree. C.

  12. High-nitrogen explosives

    SciTech Connect (OSTI)

    Naud, D.; Hiskey, M. A.; Kramer, J. F.; Bishop, R. L.; Harry, H. H.; Son, S. F.; Sullivan, G. K.

    2002-01-01

    The syntheses and characterization of various tetrazine and furazan compounds offer a different approach to explosives development. Traditional explosives - such as TNT or RDX - rely on the oxidation of the carbon and hydrogen atoms by the oxygen carrying nitro group to produce the explosive energy. High-nitrogen compounds rely instead on large positive heats of formation for that energy. Some of these high-nitrogen compounds have been shown to be less sensitive to initiation (e.g. by impact) when compared to traditional nitro-containing explosives of similar performances. Using the precursor, 3,6-bis-(3,5-dimethylpyrazol-1-yl)-s-tetrazine (BDT), several useful energetic compounds based on the s-tetrazine system have been synthesized and studied. The compound, 3,3{prime}-azobis(6-amino-s-tetrazine) or DAAT, detonates as a half inch rate stick despite having no oxygen in the molecule. Using perfluoroacetic acid, DAAT can be oxidized to give mixtures of N-oxide isomers (DAAT03.5) with an average oxygen content of about 3.5. This energetic mixture burns at extremely high rates and with low dependency on pressure. Another tetrazine compound of interest is 3,6-diguanidino-s-tetrazine(DGT) and its dinitrate and diperchlorate salts. DGT is easily synthesized by reacting BDT with guanidine in methanol. Using Caro's acid, DGT can be further oxidized to give 3,6-diguanidino-s-tetrazine-1,4-di-N-oxide (DGT-DO). Like DGT, the di-N-oxide can react with nitric acid or perchloric acid to give the dinitrate and the diperchlorate salts. The compounds, 4,4{prime}-diamino-3,3{prime}-azoxyfurazan (DAAF) and 4,4{prime}-diamino-3,3{prime}-azofurazan (DAAzF), may have important future roles in insensitive explosive applications. Neither DAAF nor DAAzF can be initiated by laboratory impact drop tests, yet both have in some aspects better explosive performances than 1,3,5-triamino-2,4,6-trinitrobenzene TATB - the standard of insensitive high explosives. The thermal stability of DAAzF is equal to that of hexanitrostilbene (HNS), yet it has a greater CJ pressure and detonation velocity. In an effort to reduce the critical diameter of TATB without sacrificing its insensitivity, we have studied the explosive performances of TATB mixed with DAAzlF (X-0561) and TATB mixed with DAAF (X-0563).

  13. High Risk Plan

    Office of Environmental Management (EM)

    Risk Plan John Bashista Melissa Rider Jeff Davis Timeline to date * OMB memo on Improving Government Acquisition issued July 29, 2009 - Review existing contracts and acquisition practices to save 7% of baseline contract spending (3.5% in FY 2010 and 3.5% in FY 2011) - Reduce high risk contracts by 10% the share of dollars obligated in FY2010 - Final plan was due and submitted on November 2, 2009 - OMB reviewed and requested revision Dec 23, 2009 - Revision submitted April 21, 2010 M&Os are

  14. High Temperature, High Voltage Fully Integrated Gate Driver Circuit...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    -- Washington D.C. PDF icon ape03marlino.pdf More Documents & Publications High Temperature, High Voltage Fully Integrated Gate Driver Circuit Smart Integrated Power Module ...

  15. High Temperature, High Voltage Fully Integrated Gate Driver Circuit...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    D.C. PDF icon ape003tolbert2010p.pdf More Documents & Publications High Temperature, High Voltage Fully Integrated Gate Driver Circuit Wide Bandgap Materials Smart ...

  16. High speed transient sampler

    DOE Patents [OSTI]

    McEwan, Thomas E. (Livermore, CA)

    1995-01-01

    A high speed sampler comprises a meandered sample transmission line for transmitting an input signal, a straight strobe transmission line for transmitting a strobe signal, and a plurality of sampling gates along the transmission lines. The sampling gates comprise a four terminal diode bridge having a first strobe resistor connected from a first terminal of the bridge to the positive strobe line, a second strobe resistor coupled from the third terminal of the bridge to the negative strobe line, a tap connected to the second terminal of the bridge and to the sample transmission line, and a sample holding capacitor connected to the fourth terminal of the bridge. The resistance of the first and second strobe resistors is much higher than the signal transmission line impedance in the preferred system. This results in a sampling gate which applies a very small load on the sample transmission line and on the strobe generator. The sample holding capacitor is implemented using a smaller capacitor and a larger capacitor isolated from the smaller capacitor by resistance. The high speed sampler of the present invention is also characterized by other optimizations, including transmission line tap compensation, stepped impedance strobe line, a multi-layer physical layout, and unique strobe generator design. A plurality of banks of such samplers are controlled for concatenated or interleaved sample intervals to achieve long sample lengths or short sample spacing.

  17. High speed transient sampler

    DOE Patents [OSTI]

    McEwan, T.E.

    1995-11-28

    A high speed sampler comprises a meandered sample transmission line for transmitting an input signal, a straight strobe transmission line for transmitting a strobe signal, and a plurality of sampling gates along the transmission lines. The sampling gates comprise a four terminal diode bridge having a first strobe resistor connected from a first terminal of the bridge to the positive strobe line, a second strobe resistor coupled from the third terminal of the bridge to the negative strobe line, a tap connected to the second terminal of the bridge and to the sample transmission line, and a sample holding capacitor connected to the fourth terminal of the bridge. The resistance of the first and second strobe resistors is much higher than the signal transmission line impedance in the preferred system. This results in a sampling gate which applies a very small load on the sample transmission line and on the strobe generator. The sample holding capacitor is implemented using a smaller capacitor and a larger capacitor isolated from the smaller capacitor by resistance. The high speed sampler of the present invention is also characterized by other optimizations, including transmission line tap compensation, stepped impedance strobe line, a multi-layer physical layout, and unique strobe generator design. A plurality of banks of such samplers are controlled for concatenated or interleaved sample intervals to achieve long sample lengths or short sample spacing. 17 figs.

  18. High temperature thermometric phosphors

    DOE Patents [OSTI]

    Allison, S.W.; Cates, M.R.; Boatner, L.A.; Gillies, G.T.

    1999-03-23

    A high temperature phosphor consists essentially of a material having the general formula LuPO{sub 4}:Dy{sub x},Eu{sub y} wherein: 0.1 wt % {<=} x {<=} 20 wt % and 0.1 wt % {<=} y {<=} 20 wt %. The high temperature phosphor is in contact with an article whose temperature is to be determined. The article having the phosphor in contact with it is placed in the environment for which the temperature of the article is to be determined. The phosphor is excited by a laser causing the phosphor to fluoresce. The emission from the phosphor is optically focused into a beam-splitting mirror which separates the emission into two separate emissions, the emission caused by the dysprosium dopant and the emission caused by the europium dopant. The separated emissions are optically filtered and the intensities of the emission are detected and measured. The ratio of the intensity of each emission is determined and the temperature of the article is calculated from the ratio of the intensities of the separate emissions. 2 figs.

  19. High temperature thermometric phosphors

    DOE Patents [OSTI]

    Allison, Stephen W.; Cates, Michael R.; Boatner, Lynn A.; Gillies, George T.

    1999-03-23

    A high temperature phosphor consists essentially of a material having the general formula LuPO.sub.4 :Dy.sub.(x),Eu.sub.y) wherein: 0.1 wt %.ltoreq.x.ltoreq.20 wt % and 0.1 wt %.ltoreq.y.ltoreq.20 wt %. The high temperature phosphor is in contact with an article whose temperature is to be determined. The article having the phosphor in contact with it is placed in the environment for which the temperature of the article is to be determined. The phosphor is excited by a laser causing the phosphor to fluoresce. The emission from the phosphor is optically focused into a beam-splitting mirror which separates the emission into two separate emissions, the emission caused by the dysprosium dopant and the emission caused by the europium dopent. The separated emissions are optically filtered and the intensities of the emission are detected and measured. The ratio of the intensity of each emission is determined and the temperature of the article is calculated from the ratio of the intensities of the separate emissions.

  20. High throughput optical scanner

    DOE Patents [OSTI]

    Basiji, David A. (Seattle, WA); van den Engh, Gerrit J. (Seattle, WA)

    2001-01-01

    A scanning apparatus is provided to obtain automated, rapid and sensitive scanning of substrate fluorescence, optical density or phosphorescence. The scanner uses a constant path length optical train, which enables the combination of a moving beam for high speed scanning with phase-sensitive detection for noise reduction, comprising a light source, a scanning mirror to receive light from the light source and sweep it across a steering mirror, a steering mirror to receive light from the scanning mirror and reflect it to the substrate, whereby it is swept across the substrate along a scan arc, and a photodetector to receive emitted or scattered light from the substrate, wherein the optical path length from the light source to the photodetector is substantially constant throughout the sweep across the substrate. The optical train can further include a waveguide or mirror to collect emitted or scattered light from the substrate and direct it to the photodetector. For phase-sensitive detection the light source is intensity modulated and the detector is connected to phase-sensitive detection electronics. A scanner using a substrate translator is also provided. For two dimensional imaging the substrate is translated in one dimension while the scanning mirror scans the beam in a second dimension. For a high throughput scanner, stacks of substrates are loaded onto a conveyor belt from a tray feeder.

  1. High Performance Buildings Database

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    The High Performance Buildings Database is a shared resource for the building industry, a unique central repository of in-depth information and data on high-performance, green building projects across the United States and abroad. The database includes information on the energy use, environmental performance, design process, finances, and other aspects of each project. Members of the design and construction teams are listed, as are sources for additional information. In total, up to twelve screens of detailed information are provided for each project profile. Projects range in size from small single-family homes or tenant fit-outs within buildings to large commercial and institutional buildings and even entire campuses. The database is a data repository as well. A series of Web-based data-entry templates allows anyone to enter information about a building project into the database. Once a project has been submitted, each of the partner organizations can review the entry and choose whether or not to publish that particular project on its own Web site.

  2. High Temperature Membrane Working Group

    Broader source: Energy.gov [DOE]

    The High Temperature Membrane Working Group consists of government, industry, and university researchers interested in developing high temperature membranes for fuel cells.

  3. High-␤,

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ␤, improved confinement reversed-field pinch plasmas at high density M. D. Wyman, 1,a͒ B. E. Chapman, 1 J. W. Ahn, 1 A. F. Almagri, 1 J. K. Anderson, 1 F. Bonomo, 2 D. L. Brower, 3 S. K. Combs, 4 D. Craig, 1,5 D. J. Den Hartog, 1 B. H. Deng, 3 W. X. Ding, 3 F. Ebrahimi, 1 D. A. Ennis, 1 G. Fiksel, 1 C. R. Foust, 4 P. Franz, 2 S. Gangadhara, 1 J. A. Goetz, 1 R. O'Connell, 1 S. P. Oliva, 1 S. C. Prager, 1 J. A. Reusch, 1 J. S. Sarff, 1 H. D. Stephens, 1 and T. Yates 3 1 Department of Physics,

  4. High voltage feedthrough bushing

    DOE Patents [OSTI]

    Brucker, John P. (Espanola, NM)

    1993-01-01

    A feedthrough bushing for a high voltage diode provides for using compression sealing for all sealing surfaces. A diode assembly includes a central conductor extending through the bushing and a grading ring assembly circumferentially surrounding and coaxial with the central conductor. A flexible conductive plate extends between and compressively seals against the central conductor and the grading ring assembly, wherein the flexibility of the plate allows inner and outer portions of the plate to axially translate for compression sealing against the central conductor and the grading ring assembly, respectively. The inner portion of the plate is bolted to the central conductor for affecting sealing. A compression beam is also bolted to the central conductor and engages the outer portion of the plate to urge the outer portion toward the grading ring assembly to obtain compression sealing therebetween.

  5. High Efficiency, Clean Combustion

    SciTech Connect (OSTI)

    Donald Stanton

    2010-03-31

    Energy use in trucks has been increasing at a faster rate than that of automobiles within the U.S. transportation sector. According to the Energy Information Administration (EIA) Annual Energy Outlook (AEO), a 23% increase in fuel consumption for the U.S. heavy duty truck segment is expected between 2009 to 2020. The heavy duty vehicle oil consumption is projected to grow between 2009 and 2050 while light duty vehicle (LDV) fuel consumption will eventually experience a decrease. By 2050, the oil consumption rate by LDVs is anticipated to decrease below 2009 levels due to CAFE standards and biofuel use. In contrast, the heavy duty oil consumption rate is anticipated to double. The increasing trend in oil consumption for heavy trucks is linked to the vitality, security, and growth of the U.S. economy. An essential part of a stable and vibrant U.S. economy is a productive U.S. trucking industry. Studies have shown that the U.S. gross domestic product (GDP) is strongly correlated to freight transport. Over 90% of all U.S. freight tonnage is transported by diesel power and over 75% is transported by trucks. Given the vital role that the trucking industry plays in the economy, improving the efficiency of the transportation of goods was a central focus of the Cummins High Efficient Clean Combustion (HECC) program. In a commercial vehicle, the diesel engine remains the largest source of fuel efficiency loss, but remains the greatest opportunity for fuel efficiency improvements. In addition to reducing oil consumption and the dependency on foreign oil, this project will mitigate the impact on the environment by meeting US EPA 2010 emissions regulations. Innovation is a key element in sustaining a U.S. trucking industry that is competitive in global markets. Unlike passenger vehicles, the trucking industry cannot simply downsize the vehicle and still transport the freight with improved efficiency. The truck manufacturing and supporting industries are faced with numerous challenges to reduce oil consumption and greenhouse gases, meet stringent emissions regulations, provide customer value, and improve safety. The HECC program successfully reduced engine fuel consumption and greenhouse gases while providing greater customer valve. The US EPA 2010 emissions standard poses a significant challenge for developing clean diesel powertrains that meet the DoE Vehicle Technologies Multi-Year Program Plan (MYPP) for fuel efficiency improvement while remaining affordable. Along with exhaust emissions, an emphasis on heavy duty vehicle fuel efficiency is being driven by increased energy costs as well as the potential regulation of greenhouse gases. An important element of the success of meeting emissions while significantly improving efficiency is leveraging Cummins component technologies such as fuel injection equipment, aftertreatment, turbomahcinery, electronic controls, and combustion systems. Innovation in component technology coupled with system integration is enabling Cummins to move forward with the development of high efficiency clean diesel products with a long term goal of reaching a 55% peak brake thermal efficiency for the engine plus aftertreatment system. The first step in developing high efficiency clean products has been supported by the DoE co-sponsored HECC program. The objectives of the HECC program are: (1) To design and develop advanced diesel engine architectures capable of achieving US EPA 2010 emission regulations while improving the brake thermal efficiency by 10% compared to the baseline (a state of the art 2007 production diesel engine). (2) To design and develop components and subsystems (fuel systems, air handling, controls, etc) to enable construction and development of multi-cylinder engines. (3) To perform an assessment of the commercial viability of the newly developed engine technology. (4) To specify fuel properties conducive to improvements in emissions, reliability, and fuel efficiency for engines using high-efficiency clean combustion (HECC) technologies. To demonstrate the technology is compatible with B2

  6. Vehicle Technologies Office Merit Review 2015: High Energy High Power

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Battery Exceeding PHEV-40 Requirements | Department of Energy Energy High Power Battery Exceeding PHEV-40 Requirements Vehicle Technologies Office Merit Review 2015: High Energy High Power Battery Exceeding PHEV-40 Requirements Presentation given by TIAX LLC at 2015 DOE Hydrogen and Fuel Cells Program and Vehicle Technologies Office Annual Merit Review and Peer Evaluation Meeting about high energy high power battery exceeding PHEV-40 requirements. PDF icon es209_rempel_2015_p.pdf More

  7. Neil Dasgupta 2012 Poster

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    proposes to study nanowire (NW) architectures based on abundant materials with reduced material thickness and purity requirements, without the need for high temperature or high ...

  8. Infrared spectroscopic and modeling studies of H{sub 2}/CH{sub 4} microwave plasma gas phase from low to high pressure and power

    SciTech Connect (OSTI)

    Rond, C. Lombardi, G.; Gicquel, A.; Hamann, S.; Rpcke, J.; Wartel, M.

    2014-09-07

    InfraRed Tunable Diode Laser Absorption Spectroscopy technique has been implemented in a H{sub 2}/CH{sub 4} Micro-Wave (MW frequency f?=?2.45 GHz) plasma reactor dedicated to diamond deposition under high pressure and high power conditions. Parametric studies such as a function of MW power, pressure, and admixtures of methane have been carried out on a wide range of experimental conditions: the pressure up to 270 mbar and the MW power up to 4?kW. These conditions allow high purity Chemical Vapor Deposition diamond deposition at high growth rates. Line integrated absorption measurements have been performed in order to monitor hydrocarbon species, i.e., CH{sub 3}, CH{sub 4}, C{sub 2}H{sub 2}, C{sub 2}H{sub 4}, and C{sub 2}H{sub 6}. The densities of the stable detected species were found to vary in the range of 10{sup 12}10{sup 17} molecules cm{sup ?3}, while the methyl radical CH{sub 3} (precursor of diamond growth under these conditions) measured into the plasma bulk was found up to 10{sup 14} molecules cm{sup ?3}. The experimental densities have been compared to those provided by 1D-radial thermochemical model for low power and low pressure conditions (up to 100 mbar/2?kW). These densities have been axially integrated. Experimental measurements under high pressure and power conditions confirm a strong increase of the degree of dissociation of the precursor, CH{sub 4}, associated to an increase of the C{sub 2}H{sub 2} density, the most abundant reaction product in the plasma.

  9. FSU High Energy Physics

    SciTech Connect (OSTI)

    Prosper, Harrison B.; Adams, Todd; Askew, Andrew; Berg, Bernd; Blessing, Susan K.; Okui, Takemichi; Owens, Joseph F.; Reina, Laura; Wahl, Horst D.

    2014-12-01

    The High Energy Physics group at Florida State University (FSU), which was established in 1958, is engaged in the study of the fundamental constituents of matter and the laws by which they interact. The group comprises theoretical and experimental physicists, who sometimes collaborate on projects of mutual interest. The report highlights the main recent achievements of the group. Significant, recent, achievements of the group’s theoretical physicists include progress in making precise predictions in the theory of the Higgs boson and its associated processes, and in the theoretical understanding of mathematical quantities called parton distribution functions that are related to the structure of composite particles such as the proton. These functions are needed to compare data from particle collisions, such as the proton-proton collisions at the CERN Large Hadron Collider (LHC), with theoretical predictions. The report also describes the progress in providing analogous functions for heavy nuclei, which find application in neutrino physics. The report highlights progress in understanding quantum field theory on a lattice of points in space and time (an area of study called lattice field theory), the progress in constructing several theories of potential new physics that can be tested at the LHC, and interesting new ideas in the theory of the inflationary expansion of the very early universe. The focus of the experimental physicists is the Compact Muon Solenoid (CMS) experiment at CERN. The report, however, also includes results from the D0 experiment at Fermilab to which the group made numerous contributions over a period of many years. The experimental group is particularly interested in looking for new physics at the LHC that may provide the necessary insight to extend the standard model (SM) of particle physics. Indeed, the search for new physics is the primary task of contemporary particle physics, one motivated by the need to explain certain facts, such as the non-zero neutrino masses or the overwhelming astrophysical evidence for an invisible form of matter, called dark matter, that has had a marked effect on the evolution of structure in the universe. The report highlights the main, recent, experimental achievements of the experimental group, which include the investigation of properties of the W and Z bosons; the search for new heavy stable charged particles and the search for a proposed property of nature called supersymmetry in proton-proton collisions that yield high energy photons. In addition, we report a few results from a more general search for supersymmetry at the LHC, initiated by the group. The report also highlights the group's significant contributions, both theoretical and experimental, to the 2012 discovery of the Higgs boson and the measurement of its properties.

  10. High Temperature Membrane Working Group

    Broader source: Energy.gov [DOE]

    This presentation provides an overview of the High Temperature Membrane Working Group Meeting in May 2007.

  11. High Performance Network Monitoring

    SciTech Connect (OSTI)

    Martinez, Jesse E

    2012-08-10

    Network Monitoring requires a substantial use of data and error analysis to overcome issues with clusters. Zenoss and Splunk help to monitor system log messages that are reporting issues about the clusters to monitoring services. Infiniband infrastructure on a number of clusters upgraded to ibmon2. ibmon2 requires different filters to report errors to system administrators. Focus for this summer is to: (1) Implement ibmon2 filters on monitoring boxes to report system errors to system administrators using Zenoss and Splunk; (2) Modify and improve scripts for monitoring and administrative usage; (3) Learn more about networks including services and maintenance for high performance computing systems; and (4) Gain a life experience working with professionals under real world situations. Filters were created to account for clusters running ibmon2 v1.0.0-1 10 Filters currently implemented for ibmon2 using Python. Filters look for threshold of port counters. Over certain counts, filters report errors to on-call system administrators and modifies grid to show local host with issue.

  12. High pressure capillary connector

    SciTech Connect (OSTI)

    Renzi, Ronald F.

    2005-08-09

    A high pressure connector capable of operating at pressures of 40,000 psi or higher is provided. This connector can be employed to position a first fluid-bearing conduit that has a proximal end and a distal end to a second fluid-bearing conduit thereby providing fluid communication between the first and second fluid-bearing conduits. The connector includes (a) an internal fitting assembly having a body cavity with (i) a lower segment that defines a lower segment aperture and (ii) an interiorly threaded upper segment, (b) a first member having a first member aperture that traverses its length wherein the first member aperture is configured to accommodate the first fluid-bearing conduit and wherein the first member is positioned in the lower segment of the internal fitting assembly, and (c) a second member having a second member aperture that traverses its length wherein the second member is positioned in the upper segment of the fitting assembly and wherein a lower surface of the second member is in contact with an upper surface of the first member to assert a compressive force onto the first member and wherein the first member aperture and the second member aperture are coaxial.

  13. High power connection system

    DOE Patents [OSTI]

    Schaefer, Christopher E. (Warren, OH); Beer, Robert C. (Noblesville, IN); McCall, Mark D. (Youngstown, OH)

    2000-01-01

    A high power connection system adapted for automotive environments which provides environmental and EMI shielding includes a female connector, a male connector, and a panel mount. The female connector includes a female connector base and a snap fitted female connector cover. The male connector includes a male connector base and a snap fitted male connector cover. The female connector base has at least one female power terminal cavity for seatably receiving a respective female power terminal. The male connector base has at least one male power terminal cavity for seatably receiving a respective male power terminal. The female connector is covered by a cover seal and a conductive shroud. A pair of lock arms protrude outward from the front end of the male connector base, pass through the panel mount and interface with a lever of a lever rotatably connected to the shroud to thereby mechanically assist mating of the male and female connectors. Safety terminals in the male and female connectors provide a last-to-connect-first-to-break connection with an HVIL circuit.

  14. High capacity oil burner

    SciTech Connect (OSTI)

    Pedrosa, O.A. Jr.; Couto, N.C.; Fanqueiro, R.C.C.

    1983-11-01

    The present invention relates to a high capacity oil burner comprising a cylindrical atomizer completely surrounded by a protective cylindrical housing having a diameter from 2 to 3 times greater than the diameter of said atomizer; liquid fuels being injected under pressure into said atomizer and accumulating within said atomizer in a chamber for the accumulation of liquid fuels, and compressed air being injected into a chamber for the accumulation of air; cylindrical holes communicating said chamber for the accumulation of liquid fuels with the outside and cylindrical holes communicating said chamber for the accumulation of air with said cylindrical holes communicating the chamber for the accumulation of liquids with the outside so that the injection of compressed air into said liquid fuel discharge holes atomizes said fuel which is expelled to the outside through the end portions of said discharge holes which are circumferentially positioned to be burnt by a pilot flame; said protecting cylindrical housing having at its ends perforated circular rings into which water is injected under pressure to form a protecting fan-like water curtain at the rear end of the housing and a fan-like water curtain at the flame to reduce the formation of soot; the burning efficiency of said burner being superior to 30 barrels of liquid fuel per day/kg of the apparatus.

  15. High-Rate, High-Capacity Binder-Free Electrode

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Office of Energy Efficiency and Renewable Energy operated by the Alliance for Sustainable Energy, LLC High-Rate, High-Capacity Binder-Free Electrode Patent: PCT-09-41 Chunmei Ban ...

  16. High Efficiency Integrated Package

    SciTech Connect (OSTI)

    Ibbetson, James

    2013-09-15

    Solid-state lighting based on LEDs has emerged as a superior alternative to inefficient conventional lighting, particularly incandescent. LED lighting can lead to 80 percent energy savings; can last 50,000 hours 2-50 times longer than most bulbs; and contains no toxic lead or mercury. However, to enable mass adoption, particularly at the consumer level, the cost of LED luminaires must be reduced by an order of magnitude while achieving superior efficiency, light quality and lifetime. To become viable, energy-efficient replacement solutions must deliver system efficacies of ? 100 lumens per watt (LPW) with excellent color rendering (CRI > 85) at a cost that enables payback cycles of two years or less for commercial applications. This development will enable significant site energy savings as it targets commercial and retail lighting applications that are most sensitive to the lifetime operating costs with their extended operating hours per day. If costs are reduced substantially, dramatic energy savings can be realized by replacing incandescent lighting in the residential market as well. In light of these challenges, Cree proposed to develop a multi-chip integrated LED package with an output of > 1000 lumens of warm white light operating at an efficacy of at least 128 LPW with a CRI > 85. This product will serve as the light engine for replacement lamps and luminaires. At the end of the proposed program, this integrated package was to be used in a proof-of-concept lamp prototype to demonstrate the components viability in a common form factor. During this project Cree SBTC developed an efficient, compact warm-white LED package with an integrated remote color down-converter. Via a combination of intensive optical, electrical, and thermal optimization, a package design was obtained that met nearly all project goals. This package emitted 1295 lm under instant-on, room-temperature testing conditions, with an efficacy of 128.4 lm/W at a color temperature of ~2873K and 83 CRI. As such, the packages performance exceeds DOEs warm-white phosphor LED efficacy target for 2013. At the end of the program, we assembled an A19 sized demonstration bulb housing the integrated package which met Energy Star intensity variation requirements. With further development to reduce overall component cost, we anticipate that an integrated remote converter package such as developed during this program will find application in compact, high-efficacy LED-based lamps, particularly those requiring omnidirectional emission.

  17. High density, high-aspect-ratio precision polyimide nanofilters | Argonne

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    National Laboratory High density, high-aspect-ratio precision polyimide nanofilters December 1, 2009 Tweet EmailPrint Collaborative users from Creatv MicroTech, Inc. and Los Alamos National Laboratory, working with CNM's Nanofabrication & Devices Group, have demonstrated a novel fabrication process that produces high-porosity polymer nanofilters with smooth, uniform. and straight pores and high aspect ratios. Nanofilters have a wide range of applications for various size-exclusion-based

  18. Toward comprehensive studies of liquids at high pressures and high

    Office of Scientific and Technical Information (OSTI)

    temperatures: Combined structure, elastic wave velocity, and viscosity measurements in the Paris–Edinburgh cell (Journal Article) | SciTech Connect SciTech Connect Search Results Journal Article: Toward comprehensive studies of liquids at high pressures and high temperatures: Combined structure, elastic wave velocity, and viscosity measurements in the Paris–Edinburgh cell Citation Details In-Document Search Title: Toward comprehensive studies of liquids at high pressures and high

  19. PALLADIUM/COPPER ALLOY COMPOSITE MEMBRANES FOR HIGH TEMPERATURE HYDROGEN SEPARATION FROM COAL-DERIVED GAS STREAMS

    SciTech Connect (OSTI)

    J. Douglas Way

    2003-01-01

    For hydrogen from coal gasification to be used economically, processing approaches that produce a high purity gas must be developed. Palladium and its alloys, nickel, platinum and the metals in Groups 3 to 5 of the Periodic Table are all permeable to hydrogen. Hydrogen permeable metal membranes made of palladium and its alloys are the most widely studied due to their high hydrogen permeability, chemical compatibility with many hydrocarbon containing gas streams, and infinite hydrogen selectivity. Our Pd composite membranes have demonstrated stable operation at 450 C for over 70 days. Coal derived synthesis gas will contain up to 15000 ppm H{sub 2}S as well as CO, CO{sub 2}, N{sub 2} and other gases. Highly selectivity membranes are necessary to reduce the H{sub 2}S concentration to acceptable levels for solid oxide and other fuel cell systems. Pure Pd-membranes are poisoned by sulfur, and suffer from mechanical problems caused by thermal cycling and hydrogen embrittlement. Recent advances have shown that Pd-Cu composite membranes are not susceptible to the mechanical, embrittlement, and poisoning problems that have prevented widespread industrial use of Pd for high temperature H{sub 2} separation. These membranes consist of a thin ({le} 5 {micro}m) film of metal deposited on the inner surface of a porous metal or ceramic tube. With support from this DOE Grant, we have fabricated thin, high flux Pd-Cu alloy composite membranes using a sequential electroless plating approach. Thin, Pd{sub 60}Cu{sub 40} films exhibit a hydrogen flux more than ten times larger than commercial polymer membranes for H{sub 2} separation, resist poisoning by H{sub 2}S and other sulfur compounds typical of coal gas, and exceed the DOE Fossil Energy target hydrogen flux of 80 ml/cm{sup 2} {center_dot} min = 0.6 mol/m{sup 2} {center_dot} s for a feed pressure of 40 psig. Similar Pd-membranes have been operated at temperatures as high as 750 C. We have developed practical electroless plating procedures for fabrication of thin Pd-Cu composite membranes at any scale.

  20. Ultra high vacuum broad band high power microwave window

    DOE Patents [OSTI]

    Nguyen-Tuong, Viet (Seaford, VA); Dylla, III, Henry Frederick (Yorktown, VA)

    1997-01-01

    An improved high vacuum microwave window has been developed that utilizes high density polyethylene coated on two sides with SiOx, SiNx, or a combination of the two. The resultant low dielectric and low loss tangent window creates a low outgassing, low permeation seal through which broad band, high power microwave energy may be passed. No matching device is necessary and the sealing technique is simple. The features of the window are broad band transmission, ultra-high vacuum compatibility with a simple sealing technique, low voltage standing wave ratio, high power transmission and low cost.

  1. Ultra high vacuum broad band high power microwave window

    DOE Patents [OSTI]

    Nguyen-Tuong, V.; Dylla, H.F. III

    1997-11-04

    An improved high vacuum microwave window has been developed that utilizes high density polyethylene coated on two sides with SiOx, SiNx, or a combination of the two. The resultant low dielectric and low loss tangent window creates a low outgassing, low permeation seal through which broad band, high power microwave energy may be passed. No matching device is necessary and the sealing technique is simple. The features of the window are broad band transmission, ultra-high vacuum compatibility with a simple sealing technique, low voltage standing wave ratio, high power transmission and low cost. 5 figs.

  2. APPARATUS FOR REGULATING HIGH VOLTAGE

    DOE Patents [OSTI]

    Morrison, K.G.

    1951-03-20

    This patent describes a high-voltage regulator of the r-f type wherein the modulation of the r-f voltage is accomplished at a high level, resulting in good stabilization over a large range of load conditions.

  3. Introduction to High Performance Computing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Introduction to High Performance Computing Introduction to High Performance Computing June 10, 2013 Photo on 7 30 12 at 7.10 AM Downloads Download File Gerber-HPC-2.pdf...

  4. High-Pressure Hydrogen Tanks

    Broader source: Energy.gov [DOE]

    Presentation on High-Pressure Hydrogen Tanks for the DOE Hydrogen Delivery High-Pressure Tanks and Analysis Project Review Meeting held February 8-9, 2005 at Argonne National Laboratory

  5. High voltage variable diameter insulator

    DOE Patents [OSTI]

    Vanacek, D.L.; Pike, C.D.

    1982-07-13

    A high voltage feedthrough assembly having a tubular insulator extending between the ground plane ring and the high voltage ring. The insulator is made of Pyrex and decreases in diameter from the ground plane ring to the high voltage ring, producing equipotential lines almost perpendicular to the wall of the insulator to optimize the voltage-holding capability of the feedthrough assembly.

  6. Determination of the Quantity of I-135 Released from the AGR Experiment Series

    SciTech Connect (OSTI)

    Scates, Dawn Marie; Walter, John Bradley; Reber, Edward Lawrence; Sterbentz, James William; Petti, David Andrew

    2014-10-01

    A series of three Advanced Gas Reactor (AGR) experiments have been conducted in the Advanced Test Reactor (ATR) at Idaho National Laboratory (INL). From 2006 through 2014, these experiments supported the development and qualification of the new U.S. tri structural isotropic (TRISO) particle fuel for Very High Temperature Reactors (VHTR). Each AGR experiment consisted of multiple fueled capsules, each plumbed for independent temperature control using a mix of helium and neon gases. The gas leaving a capsule was routed to individual Fission Product Monitor (FPM) detectors. For intact fuel particles, the TRISO particle coatings provide a substantial barrier to fission product release. However, particles with failed coatings, whether because of a minute percentage of initially defective particles, those which fail during irradiation, or those designed to fail (DTF) particles, can release fission products to the flowing gas stream. Because reactive fission product elements like iodine and cesium quickly deposit on cooler capsule components and piping structures as the effluent gas leaves the reactor core, only the noble fission gas isotopes of Kr and Xe tend to reach FPM detectors. The FPM system utilizes High Purity Germanium (HPGe) detectors coupled with a thallium activated sodium iodide NaI(Tl) scintillator. The germanium detector provides individual isotopic information, while the NaI(Tl) scintillator is used as a gross count rate meter. During irradiation, the 135mXe concentration reaching the FPM detectors is from both direct fission and by decay of the accumulated 135I. About ~2.5 hours after irradiation (ten 15.3 minute 135mXe half lives) the directly produced 135mXe has decayed and only the longer lived 135I remains as a source. Decay systematics dictate that 135mXe will be in secular equilibrium with its 135I parent, such that its production rate very nearly equals the decay rate of the parent, and its concentration in the flowing gas stream will appear to decay with the parent half life. This equilibrium condition enables the determination of the amount of 135I released from the fuel particles by measurement of the 135mXe at the FPM following reactor shutdown. In this paper, the 135I released will be reported and compared to similar releases for noble gases as well as the unexpected finding of 131I deposition from intentional impure gas injection into capsule 11 of experiment AGR 3/4.

  7. HIGH-INTENSITY, HIGH CHARGE-STATE HEAVY ION SOURCES

    SciTech Connect (OSTI)

    ALESSI,J.G.

    2004-08-16

    There are many accelerator applications for high intensity heavy ion sources, with recent needs including dc beams for RIA, and pulsed beams for injection into synchrotrons such as RHIC and LHC. The present status of sources producing high currents of high charge state heavy ions is reviewed. These sources include ECR, EBIS, and Laser ion sources. Benefits and limitations for these type sources are described. Possible future improvements in these sources are also mentioned.

  8. Interplay of Metalloligand and Organic Ligand to Tune Micropores within Isostructural Mixed-Metal Organic Frameworks (M MOFs) for Their Highly Selective Separation of Chiral and Achiral Small Molecules

    SciTech Connect (OSTI)

    Madhab, Das; He, Yabing; Kim, Jaheon; Guo, Qunsheng; Zhao, Cong-Gui; Hong, Kunlun; Xiang, Sheng-Chang; Zhang, Zhangjing; Thomas, K Mark; Krishna, Rajamani; Chen, Banglin

    2012-01-01

    Four porous isostructural mixed-metal-organic frameworks (M'MOFs) have been synthesized and structurally characterized. The pores within these M'MOFs are systematically tuned by the interplay of both the metalloligands and organic ligands which have enabled us not only to direct their highly selective separation of chiral alcohols 1-phenylethanol (PEA), 2-butanol (BUT), and 2-pentanol (2-PEN) with the highest ee up to 82.4% but also to lead highly selective separation of achiral C{sub 2}H{sub 2}/C{sub 2}H{sub 4} separation. The potential application of these M'MOFs for the fixed bed pressure swing adsorption (PSA) separation of C{sub 2}H{sub 2}/C{sub 2}H{sub 4} has been further examined and compared by the transient breakthrough simulations in which the purity requirement of 40 ppm in the outlet gas can be readily fulfilled by the fixed bed M'MOF-4a adsorber at ambient conditions.

  9. High-Temperature-High-Volume Lifting For Enhanced Geothermal...

    Open Energy Info (EERE)

    include high-temperature drive system materials, journal and thrust bearings, and corrosion and erosion-resistant lifting pump components. Finally, in Phase 3, the overall...

  10. Method of using a germanium layer transfer to Si for photovoltaic applications and heterostructure made thereby

    DOE Patents [OSTI]

    Atwater, Jr., Harry A.; Zahler, James M.

    2006-11-28

    Ge/Si and other nonsilicon film heterostructures are formed by hydrogen-induced exfoliation of the Ge film which is wafer bonded to a cheaper substrate, such as Si. A thin, single-crystal layer of Ge is transferred to Si substrate. The bond at the interface of the Ge/Si heterostructures is covalent to ensure good thermal contact, mechanical strength, and to enable the formation of an ohmic contact between the Si substrate and Ge layers. To accomplish this type of bond, hydrophobic wafer bonding is used, because as the invention demonstrates the hydrogen-surface-terminating species that facilitate van der Waals bonding evolves at temperatures above 600.degree. C. into covalent bonding in hydrophobically bound Ge/Si layer transferred systems.

  11. Valley-dependent spin polarization and long-lived electron spins in germanium

    SciTech Connect (OSTI)

    Giorgioni, Anna Vitiello, Elisa; Grilli, Emanuele; Guzzi, Mario; Pezzoli, Fabio

    2014-10-13

    Spin orientation and relaxation of conduction band electrons in bulk Ge are addressed by studying the steady-state circular polarization of the indirect gap photoluminescence (PL) at low temperatures. This provides a direct experimental proof of recently predicted spin-dependent selection rules for phonon-mediated optical transitions in Ge. In addition, we observe valley-dependent circularly polarized emission, and map the concomitant redistribution of electron spins within the multi-valley conduction band of Ge by gaining simultaneous access to the circular dichroism of light emitted across the direct and the indirect gap transitions. Finally, the lifetime of L-valley electrons is measured by means of decay curves of the indirect gap PL emission, yielding spin relaxation times in the order of hundreds of ns.

  12. Germanium subcells for multijunction GaInP/GaInAs/Ge solar cells

    SciTech Connect (OSTI)

    Kalyuzhnyy, N. A.; Gudovskikh, A. S.; Evstropov, V. V.; Lantratov, V. M.; Mintairov, S. A.; Timoshina, N. Kh.; Shvarts, M. Z.; Andreev, V. M.

    2010-11-15

    Photovoltaic converters based on n-GaInP/n-p-Ge heterostructures grown by the OMVPE under different conditions of formation of the p-n junction are studied. The heterostructures are intended for use as narrow-gap subcells of the GaInP/GaInAs/Ge three-junction solar cells. It is shown that, in Ge p-tn junctions, along with the diffusion mechanism, the tunneling mechanism of the current flow exists; therefore, the two-diode electrical equivalent circuit of the Ge p-n junction is used. The diode parameters are determined for both mechanisms from the analysis of both dark and 'light' current-voltage dependences. It is shown that the elimination of the component of the tunneling current allows one to increase the efficiency of the Ge subcell by {approx}1% with conversion of nonconcentrated solar radiation. The influence of the tunneling current on the efficiency of the Ge-based devices can be in practice reduced to zero at photogenerated current density of {approx}1.5 A/cm{sup 2} due to the use of the concentrated solar radiation.

  13. High-Throughput, High-Precision Hot Testing Tool for High-Brightness

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Light-Emitting Diode Testing | Department of Energy Throughput, High-Precision Hot Testing Tool for High-Brightness Light-Emitting Diode Testing High-Throughput, High-Precision Hot Testing Tool for High-Brightness Light-Emitting Diode Testing Lead Performer: KLA-Tencor Corporation - Milpitas, CA Partners: Ocean Optics - Dunedin, FL DOE Total Funding: $3,994,729 Cost Share: $4,626,422 Project Term: 8/15/2012 - 9/30/2015 Funding Opportunity: SSL Manufacturing R&D Funding Opportunity

  14. High resolution time interval meter

    DOE Patents [OSTI]

    Martin, A.D.

    1986-05-09

    Method and apparatus are provided for measuring the time interval between two events to a higher resolution than reliability available from conventional circuits and component. An internal clock pulse is provided at a frequency compatible with conventional component operating frequencies for reliable operation. Lumped constant delay circuits are provided for generating outputs at delay intervals corresponding to the desired high resolution. An initiation START pulse is input to generate first high resolution data. A termination STOP pulse is input to generate second high resolution data. Internal counters count at the low frequency internal clock pulse rate between the START and STOP pulses. The first and second high resolution data are logically combined to directly provide high resolution data to one counter and correct the count in the low resolution counter to obtain a high resolution time interval measurement.

  15. Summary of Field Measurement on UF6 Cylinders Using Electro-Mechanically Cooled Systems

    SciTech Connect (OSTI)

    McGinnis, Brent R; Smith, Steven E; Solodov, Alexander A; Whitaker, J Michael; Morgan, James B; MayerII, Richard L.; Montgomery, J. Brent

    2009-01-01

    Measurement of the enrichment of solid state UF6 stored within large metal cylinders is a task commonly performed by plant operators and inspectors. The measurement technologies typically used range from low-resolution, high-efficiency sodium iodide detectors to high-resolution, moderate-efficiency high-purity germanium (HPGe) detectors. The technology used and methods deployed are dependent upon the material being measured, environmental conditions, time constraints, and measurement-precision requirements. Operators and inspectors typically use specially designed, HPGe detectors that are cooled with liquid nitrogen in situations where high-resolution measurements are required. However, the requirement for periodically refilling the system with liquid nitrogen makes remote usage cumbersome and slow. The task of cooling the detector reduces the available time for the inspector to perform other safeguards activities while on site. If the inspector has to reduce the count time for each selected cylinder to ensure that all preselected cylinders are measured during the inspection, the resulting measurement uncertainties may be increased, making it more difficult to detect and verify potential discrepancies in the operator's declarations. However, recent advances in electromechanically cooled HPGe detectors may provide the inspector with an improved verification tool by eliminating the need for liquid nitrogen. This report provides a summary of test results for field measurements performed using electromechanically cooled HPGe detectors on depleted, natural, and low-enriched uranium cylinders. The results of the study provide valuable information to inspectors and operators regarding the capabilities and limitations of electromechanically cooled systems based on true field-measurement conditions.

  16. High Temperature, High Voltage Fully Integrated Gate Driver Circuit |

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Department of Energy 10 DOE Vehicle Technologies and Hydrogen Programs Annual Merit Review and Peer Evaluation Meeting, June 7-11, 2010 -- Washington D.C. PDF icon ape003_tolbert_2010_p.pdf More Documents & Publications High Temperature, High Voltage Fully Integrated Gate Driver Circuit Wide Bandgap Materials Smart Integrated Power Module

  17. High Temperature, High Voltage Fully Integrated Gate Driver Circuit |

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Department of Energy 09 DOE Hydrogen Program and Vehicle Technologies Program Annual Merit Review and Peer Evaluation Meeting, May 18-22, 2009 -- Washington D.C. PDF icon ape_03_marlino.pdf More Documents & Publications High Temperature, High Voltage Fully Integrated Gate Driver Circuit Smart Integrated Power Module Wide Bandgap Materials

  18. High voltage variable diameter insulator

    DOE Patents [OSTI]

    Vanecek, David L. (Martinez, CA); Pike, Chester D. (Pinole, CA)

    1984-01-01

    A high voltage feedthrough assembly (10) having a tubular insulator (15) extending between the ground plane ring (16) and the high voltage ring (30). The insulator (15) is made of Pyrex and decreases in diameter from the ground plane ring (16) to the high voltage ring (30), producing equipotential lines almost perpendicular to the wall (27) of the insulator (15) to optimize the voltage-holding capability of the feedthrough assembly (10).

  19. Software and High Performance Computing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Software and High Performance Computing Software and High Performance Computing Providing world-class high performance computing capability that enables unsurpassed solutions to complex problems of strategic national interest Contact thumbnail of Kathleen McDonald Head of Intellectual Property, Business Development Executive Kathleen McDonald Richard P. Feynman Center for Innovation (505) 667-5844 Email Software Computational physics, computer science, applied mathematics, statistics and the

  20. High Impact Technology Hub- Results

    Broader source: Energy.gov [DOE]

    Highlights, outcomes and activities to support the adoption of High Impact Technologies. Technology Highlights preview early results from current technology demonstrations. Case Studies overview...

  1. High Mesa | Open Energy Information

    Open Energy Info (EERE)

    High Mesa Sector Wind energy Facility Type Commercial Scale Wind Facility Status In Service Owner Exelon Wind Developer Exelon Wind Energy Purchaser Idaho Power Location...

  2. High Impact Technology HQ- Results

    Broader source: Energy.gov [DOE]

    Highlights, outcomes and activities to support the adoption of High Impact Technologies.  Technology Highlights preview early results from current technology demonstrations.  Case Studies overview...

  3. High field gradient particle accelerator

    DOE Patents [OSTI]

    Nation, John A.; Greenwald, Shlomo

    1989-01-01

    A high electric field gradient electron accelerator utilizing short duration, microwave radiation, and capable of operating at high field gradients for high energy physics applications or at reduced electric field gradients for high average current intermediate energy accelerator applications. Particles are accelerated in a smooth bore, periodic undulating waveguide, wherein the period is so selected that the particles slip an integral number of cycles of the r.f. wave every period of the structure. This phase step of the particles produces substantially continuous acceleration in a traveling wave without transverse magnetic or other guide means for the particle.

  4. High field gradient particle accelerator

    DOE Patents [OSTI]

    Nation, J.A.; Greenwald, S.

    1989-05-30

    A high electric field gradient electron accelerator utilizing short duration, microwave radiation, and capable of operating at high field gradients for high energy physics applications or at reduced electric field gradients for high average current intermediate energy accelerator applications is disclosed. Particles are accelerated in a smooth bore, periodic undulating waveguide, wherein the period is so selected that the particles slip an integral number of cycles of the r.f. wave every period of the structure. This phase step of the particles produces substantially continuous acceleration in a traveling wave without transverse magnetic or other guide means for the particle. 10 figs.

  5. Highly Enriched Uranium Materials Facility

    National Nuclear Security Administration (NNSA)

    Appropriations Subcommittee, is shown some of the technology in the Highly Enriched Uranium Materials Facility by Warehousing and Transportation Operations Manager Byron...

  6. HIGH

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Highlights International Oil Markets Prices. We have found little need to adjust our oil price forecast from last month's report, since no evidence of significantly more bullish (or bearish) sentiment on the world oil market has arisen since last month. Our estimate from the December Outlook for the November imported oil cost still looks good at $23.50 and our current estimate for December's price at $24.75 is only slightly above last month's expected December level ($24.50). Thus, annual

  7. High

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    confinement plasmas in the Madison Symmetric Torus reversed-field pinch a... B. E. Chapman, b) A. F. Almagri, J. K. Anderson, T. M. Biewer, P. K. Chattopadhyay, C.-S. Chiang, D. Craig, D. J. Den Hartog, G. Fiksel, C. B. Forest, A. K. Hansen, D. Holly, N. E. Lanier, R. O'Connell, S. C. Prager, J. C. Reardon, J. S. Sarff, and M. D. Wyman Department of Physics, University of Wisconsin-Madison, Madison, Wisconsin 53706 D. L. Brower, W. X. Ding, Y. Jiang, and S. D. Terry Department of Electrical

  8. High

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    throughput spectrometer for fast localized Doppler measurements D. Craig, a͒ D. J. Den Hartog, D. A. Ennis, S. Gangadhara, and D. Holly The Center for Magnetic Self-Organization in Laboratory and Astrophysical Plasmas, 1150 University Avenue, University of Wisconsin-Madison, Madison, Wisconsin 53706 ͑Received 26 June 2006; accepted 27 November 2006; published online 4 January 2007͒ A new custom-built duo spectrometer has been commissioned for fast localized Doppler measurements of plasma ions

  9. High

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    resolution soft x-ray tomography in the Madison Symmetric Torus P. Franz a) Consorzio RFX-Associazione EURATOM ENEA sulla fusione, Padova, Italy and Istituto Nazionale di Fisica della Materia, Unità di Ricerca di Padova, Italy F. Bonomo, G. Gadani, and L. Marrelli Consorzio RFX-Associazione EURATOM ENEA sulla fusione, Padova, Italy P. Martin and P. Piovesan Consorzio RFX-Associazione EURATOM ENEA sulla fusione, Padova, Italy and Istituto Nazionale di Fisica della Materia, Unità di Ricerca di

  10. high

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    1999 Highlights International Oil Markets Prices. World oil prices for the remainder of 1999 and all of 2000 are expected to remain above $20 per barrel. EIA believes that prices will rise from average November levels (an estimated $23.50 per barrel for the price paid by U.S. refiners for imported crude) by about $1 per barrel by December, due to increased demand in the winter and Y2K precautionary building of end-user inventories (see a brief discussion on Y2K impacts below). The world oil

  11. high

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    0 Highlights International Oil Markets Prices. We have raised our world oil price projection by about $2 per barrel for this month because of assumed greater compliance by OPEC to targeted cuts, especially for the second quarter of 2000 (Figure 1). The expected decline in world petroleum inventories continues (Figure 2), and, given the generally stiff resolve of OPEC members to maintain production cuts, any sign of a turnaround in stocks may be postponed until later this year than previously

  12. high

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Summary Our short-term outlook for a wide array of energy prices has been adjusted upward as international and domestic energy supply conditions have tightened. We think that crude oil prices are as likely as not to end the year $2 to $3 per barrel higher than our previous projections. Thus, we think that the probability of West Texas Intermediate costing an average of $30 per barrel or more at midwinter is about 50 percent. On their current track, heating oil prices are likely to be about 30

  13. Lloyd Energy Systems | Open Energy Information

    Open Energy Info (EERE)

    Sydney, New South Wales, Australia Zip: 200 Sector: Solar Product: Makes high-purity graphite blocks to store energy (particularly solar energy) as heat, with steam turbines to...

  14. Fuel Cell Technologies Office Multi-Year Research, Development...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    ... Finally, the high purity of hydrogen required for fuel cells ... efficiently utilize the solar spectrum but are often less ... dark and light-induced degradation due to corrosion ...

  15. ALSNews Vol. 340

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    information, read the shutdown update page. In This Issue Studying the Solar System's Chemical Recipe The Importance of Domain Size and Purity in High-Efficiency Organic Solar...

  16. Search for: All records | SciTech Connect

    Office of Scientific and Technical Information (OSTI)

    teosub 2 (1) background radiation (1) cables (1) electric potential (1) gamma spectroscopy (1) high-purity ge detectors (1) icp mass spectroscopy (1) inorganic, organic,...

  17. Hydrophen | Open Energy Information

    Open Energy Info (EERE)

    to: navigation, search Name: Hydrophen Place: Cambridge, Massachusetts Sector: Hydro, Hydrogen Product: Start-up planning to produce high-purity hydrogen from water. Coordinates:...

  18. Preparations of rare earth-iron alloys by thermite reduction

    DOE Patents [OSTI]

    Schmidt, Frederick A. (Ames, IA); Peterson, David T. (Ames, IA); Wheelock, John T. (Nevada, IA)

    1986-09-16

    An improved method for the preparation of high-purity rare earth-iron alloys by the aluminothermic reduction of a mixture of rare earth and iron fluorides.

  19. ALSNews Vol. 340

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Chemical Recipe The Importance of Domain Size and Purity in High-Efficiency Organic Solar Cells Ring Leader: Eli Rotenberg Industry @ ALS: Moving Memristor and Neuristor Research...

  20. Clean Fractionation - Energy Innovation Portal

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    separation, Clean Fractionation segregates cellulose, hemicellulose, and lignin into three high-purity streams for conversion into value-added products, including ethanol biofuel. ...

  1. The Ames Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    and single crystals. We provide research and developmental quantities of high-purity materials and unique characterization services to scientists at university, industry, and...

  2. Micro Materials Japan Inc | Open Energy Information

    Open Energy Info (EERE)

    Materials Japan Inc Jump to: navigation, search Name: Micro Materials Japan Inc Place: Omura, Nagasaki, Japan Zip: 856-0806 Product: Japanese manufacturer of high purity wafers and...

  3. PPP Equipment Corporation | Open Energy Information

    Open Energy Info (EERE)

    PPP Equipment Corporation Sector: Solar Product: PPP-E designs, produces and markets Chemical Vapor Deposition (CVD) reactors and converter systems producing high-purity...

  4. High temperature lightweight foamed cements

    DOE Patents [OSTI]

    Sugama, Toshifumi (Mastic Beach, NY)

    1989-01-01

    Cement slurries are disclosed which are suitable for use in geothermal wells since they can withstand high temperatures and high pressures. The formulation consists of cement, silica flour, water, a retarder, a foaming agent, a foam stabilizer, and a reinforcing agent. A process for producing these cements is also disclosed.

  5. High temperature lightweight foamed cements

    DOE Patents [OSTI]

    Sugama, Toshifumi.

    1989-10-03

    Cement slurries are disclosed which are suitable for use in geothermal wells since they can withstand high temperatures and high pressures. The formulation consists of cement, silica flour, water, a retarder, a foaming agent, a foam stabilizer, and a reinforcing agent. A process for producing these cements is also disclosed. 3 figs.

  6. Temperature controlled high voltage regulator

    DOE Patents [OSTI]

    Chiaro, Jr., Peter J. (Clinton, TN); Schulze, Gerald K. (Knoxville, TN)

    2004-04-20

    A temperature controlled high voltage regulator for automatically adjusting the high voltage applied to a radiation detector is described. The regulator is a solid state device that is independent of the attached radiation detector, enabling the regulator to be used by various models of radiation detectors, such as gas flow proportional radiation detectors.

  7. Electrokinetically pumped high pressure sprays

    DOE Patents [OSTI]

    Schoeniger, Joseph S. (Oakland, CA); Paul, Phillip H. (Livermore, CA); Schoeniger, Luke (Pittsford, NY)

    2005-11-01

    An electrokinetic pump capable of producing high pressure is combined with a nozzle having a submicron orifice to provide a high pressure spray device. Because of its small size, the device can be contained within medical devices such as an endoscope for delivering biological materials such as DNA, chemo therapeutic agents, or vaccines to tissues and cells.

  8. Electrokinetically pumped high pressure sprays

    DOE Patents [OSTI]

    Schoeniger, Joseph S. (Oakland, CA); Paul, Phillip H. (Livermore, CA); Schoeniger, Luke (Pittsford, NY)

    2002-01-01

    An electrokinetic pump capable of producing high pressure is combined with a nozzle having a submicron orifice to provide a high pressure spray device. Because of its small size, the device can be contained within medical devices such as an endoscope for delivering biological materials such as DNA, chemo therapeutic agents, or vaccines to tissues and cells.

  9. Multidisciplinary University Research Initiative: High Operating...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Research Initiative: High Operating Temperature Fluids Multidisciplinary University Research Initiative: High Operating Temperature Fluids Multidisciplinary University ...

  10. High-Performance Nanostructured Coating

    Broader source: Energy.gov [DOE]

    The High-Performance Nanostructured Coating fact sheet details a SunShot project led by a University of California, San Diego research team working to develop a new high-temperature spectrally selective coating for receiver surfaces. These receiver surfaces, used in concentrating solar power systems, rely on high-temperature SSCs to effectively absorb solar energy without emitting much blackbody radiation.The optical properties of the SSC directly determine the efficiency and maximum attainable temperature of solar receivers, which in turn influence the power-conversion efficiency and overall system cost.

  11. JC3 High Impact Assessment Bulletins | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    High Impact Assessment Bulletins JC3 High

  12. UESC and High Tech Facilities

    Broader source: Energy.gov [DOE]

    Presentation—given at the April 2012 Federal Utility Partnership Working Group (FUPWG) meeting—about the Federal Energy Management Program's (FEMP's) High-Tech Building Utility Energy Service Contract (UESC) Partnership led by the Lawrence Berkeley National Laboratory (LBNL).

  13. High temperature structural insulating material

    DOE Patents [OSTI]

    Chen, W.Y.

    1984-07-27

    A high temperature structural insulating material useful as a liner for cylinders of high temperature engines through the favorable combination of high service temperature (above about 800/sup 0/C), low thermal conductivity (below about 0.2 W/m/sup 0/C), and high compressive strength (above about 250 psi). The insulating material is produced by selecting hollow ceramic beads with a softening temperature above about 800/sup 0/C, a diameter within the range of 20-200 ..mu..m, and a wall thickness in the range of about 2 to 4 ..mu..m; compacting the beads and a compatible silicate binder composition under pressure and sintering conditions to provide the desired structural form with the structure having a closed-cell, compact array of bonded beads.

  14. High temperature structural insulating material

    DOE Patents [OSTI]

    Chen, Wayne Y.

    1987-01-01

    A high temperature structural insulating material useful as a liner for cylinders of high temperature engines through the favorable combination of high service temperature (above about 800.degree. C.), low thermal conductivity (below about 0.2 W/m.degree. C.), and high compressive strength (above about 250 psi). The insulating material is produced by selecting hollow ceramic beads with a softening temperature above about 800.degree. C., a diameter within the range of 20-200 .mu.m, and a wall thickness in the range of about 2-4 .mu.m; compacting the beads and a compatible silicate binder composition under pressure and sintering conditions to provide the desired structural form with the structure having a closed-cell, compact array of bonded beads.

  15. High-Level Waste Requirements

    Broader source: Directives, Delegations, and Requirements [Office of Management (MA)]

    1999-07-09

    The guide provides the criteria for determining which DOE radioactive wastes are to be managed as high-level waste in accordance with DOE M 435.1-1.

  16. High temperature current mirror amplifier

    DOE Patents [OSTI]

    Patterson, III, Raymond B. (Melbourne, FL)

    1984-05-22

    A high temperature current mirror amplifier having biasing means in the transdiode connection of the input transistor for producing a voltage to maintain the base-collector junction reversed-biased and a current means for maintaining a current through the biasing means at high temperatures so that the base-collector junction of the input transistor remained reversed-biased. For accuracy, a second current mirror is provided with a biasing means and current means on the input leg.

  17. High average power pockels cell

    DOE Patents [OSTI]

    Daly, Thomas P. (Pleasanton, CA)

    1991-01-01

    A high average power pockels cell is disclosed which reduces the effect of thermally induced strains in high average power laser technology. The pockels cell includes an elongated, substantially rectangular crystalline structure formed from a KDP-type material to eliminate shear strains. The X- and Y-axes are oriented substantially perpendicular to the edges of the crystal cross-section and to the C-axis direction of propagation to eliminate shear strains.

  18. High resolution, high rate x-ray spectrometer

    DOE Patents [OSTI]

    Goulding, F.S.; Landis, D.A.

    1983-07-14

    It is an object of the invention to provide a pulse processing system for use with detected signals of a wide dynamic range which is capable of very high counting rates, with high throughput, with excellent energy resolution and a high signal-to-noise ratio. It is a further object to provide a pulse processing system wherein the fast channel resolving time is quite short and substantially independent of the energy of the detected signals. Another object is to provide a pulse processing system having a pile-up rejector circuit which will allow the maximum number of non-interfering pulses to be passed to the output. It is also an object of the invention to provide new methods for generating substantially symmetrically triangular pulses for use in both the main and fast channels of a pulse processing system.

  19. Extended length microchannels for high density high throughput electrophoresis systems

    DOE Patents [OSTI]

    Davidson, James C. (Livermore, CA); Balch, Joseph W. (Livermore, CA)

    2000-01-01

    High throughput electrophoresis systems which provide extended well-to-read distances on smaller substrates, thus compacting the overall systems. The electrophoresis systems utilize a high density array of microchannels for electrophoresis analysis with extended read lengths. The microchannel geometry can be used individually or in conjunction to increase the effective length of a separation channel while minimally impacting the packing density of channels. One embodiment uses sinusoidal microchannels, while another embodiment uses plural microchannels interconnected by a via. The extended channel systems can be applied to virtually any type of channel confined chromatography.

  20. High-Rate, High-Capacity Binder-Free Electrode

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Office of Energy Efficiency and Renewable Energy operated by the Alliance for Sustainable Energy, LLC High-Rate, High-Capacity Binder-Free Electrode Patent: PCT-09-41 Chunmei Ban Zhuangchun Wu Anne Dillon National Renewable Energy Laboratory PCT: 09-41 Binderfree electrode 2 Outline  What is the technology  Why it is better than other technologies  How far away from market  Technical details  Market analysis National Renewable Energy Laboratory PCT: 09-41 Binderfree electrode 3

  1. Fission Product Monitoring of TRISO Coated Fuel For The Advanced Gas Reactor -1 Experiment

    SciTech Connect (OSTI)

    Dawn M. Scates; John K. Hartwell; John b. Walter

    2010-10-01

    The US Department of Energy has embarked on a series of tests of TRISO-coated particle reactor fuel intended for use in the Very High Temperature Reactor (VHTR) as part of the Advanced Gas Reactor (AGR) program. The AGR-1 TRISO fuel experiment, currently underway, is the first in a series of eight fuel tests planned for irradiation in the Advanced Test Reactor (ATR) located at the Idaho National Laboratory (INL). The AGR-1 experiment reached a peak compact averaged burn up of 9% FIMA with no known TRISO fuel particle failures in March 2008. The burnup goal for the majority of the fuel compacts is to have a compact averaged burnup greater than 18% FIMA and a minimum compact averaged burnup of 14% FIMA. At the INL the TRISO fuel in the AGR-1 experiment is closely monitored while it is being irradiated in the ATR. The effluent monitoring system used for the AGR-1 fuel is the Fission Product Monitoring System (FPMS). The FPMS is a valuable tool that provides near real-time data indicative of the AGR-1 test fuel performance and incorporates both high-purity germanium (HPGe) gamma-ray spectrometers and sodium iodide [NaI(Tl)] scintillation detector-based gross radiation monitors. To quantify the fuel performance, release-to-birth ratios (R/Bs) of radioactive fission gases are computed. The gamma-ray spectra acquired by the AGR-1 FPMS are analyzed and used to determine the released activities of specific fission gases, while a dedicated detector provides near-real time count rate information. Isotopic build up and depletion calculations provide the associated isotopic birth rates. This paper highlights the features of the FPMS, encompassing the equipment, methods and measures that enable the calculation of the release-to-birth ratios. Some preliminary results from the AGR-1 experiment are also presented.

  2. High resolution digital delay timer

    DOE Patents [OSTI]

    Martin, Albert D. (Los Alamos, NM)

    1988-01-01

    Method and apparatus are provided for generating an output pulse following a trigger pulse at a time delay interval preset with a resolution which is high relative to a low resolution available from supplied clock pulses. A first lumped constant delay (20) provides a first output signal (24) at predetermined interpolation intervals corresponding to the desired high resolution time interval. Latching circuits (26, 28) latch the high resolution data (24) to form a first synchronizing data set (60). A selected time interval has been preset to internal counters (142, 146, 154) and corrected for circuit propagation delay times having the same order of magnitude as the desired high resolution. Internal system clock pulses (32, 34) count down the counters to generate an internal pulse delayed by an interval which is functionally related to the preset time interval. A second LCD (184) corrects the internal signal with the high resolution time delay. A second internal pulse is then applied to a third LCD (74) to generate a second set of synchronizing data (76) which is complementary with the first set of synchronizing data (60) for presentation to logic circuits (64). The logic circuits (64) further delay the internal output signal (72) to obtain a proper phase relationship of an output signal (80) with the internal pulses (32, 34). The final delayed output signal (80) thereafter enables the output pulse generator (82) to produce the desired output pulse (84) at the preset time delay interval following input of the trigger pulse (10, 12).

  3. High Burnup Fuel Behavior Modeling

    SciTech Connect (OSTI)

    Jahingir, M.; Rand, R.; Stachowski, R.; Miles, B.; Kusagaya, K.

    2007-07-01

    This paper discusses the development and qualification of the PRIME03 code to address high burnup mechanisms and to improve uranium utilization in current and new reactor designs. Materials properties and behavioral models have been updated from previous thermal-mechanical codes to reflect the effects of burnup on fuel pellet thermal conductivity, Zircaloy creep, fuel pellet relocation, and fission gas release. These new models are based on results of in-pool and post irradiation examination (PIE) of commercial boiling water reactor (BWR) fuel rods at high burnup and results from international experimental programs. The new models incorporated into PRIME03 also address specific high burnup effects associated with formation of pellet rim porosity at high exposure. The PRIME03 code is qualified by comparison of predicted and measured fuel performance parameters for a large number of high, low, and moderate burnup test and commercial reactor rod. The extensive experimental qualification of the PRIME03 prediction capabilities confirms that it is a reliable best-estimate predictor of fuel rod thermal-mechanical performance over a wide range of design and operating conditions. (authors)

  4. Ultra High Temperature | Open Energy Information

    Open Energy Info (EERE)

    Ultra High Temperature Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Print PDF Sanyal Temperature Classification: Ultra High Temperature Dictionary.png Ultra High...

  5. Gasification of high ash, high ash fusion temperature bituminous coals

    DOE Patents [OSTI]

    Liu, Guohai; Vimalchand, Pannalal; Peng, WanWang

    2015-11-13

    This invention relates to gasification of high ash bituminous coals that have high ash fusion temperatures. The ash content can be in 15 to 45 weight percent range and ash fusion temperatures can be in 1150.degree. C. to 1500.degree. C. range as well as in excess of 1500.degree. C. In a preferred embodiment, such coals are dealt with a two stage gasification process--a relatively low temperature primary gasification step in a circulating fluidized bed transport gasifier followed by a high temperature partial oxidation step of residual char carbon and small quantities of tar. The system to process such coals further includes an internally circulating fluidized bed to effectively cool the high temperature syngas with the aid of an inert media and without the syngas contacting the heat transfer surfaces. A cyclone downstream of the syngas cooler, operating at relatively low temperatures, effectively reduces loading to a dust filtration unit. Nearly dust- and tar-free syngas for chemicals production or power generation and with over 90%, and preferably over about 98%, overall carbon conversion can be achieved with the preferred process, apparatus and methods outlined in this invention.

  6. High thermal conductivity connector having high electrical isolation

    DOE Patents [OSTI]

    Nieman, Ralph C. (Downers Grove, IL); Gonczy, John D. (Oak Lawn, IL); Nicol, Thomas H. (St. Charles, IL)

    1995-01-01

    A method and article for providing a low-thermal-resistance, high-electrical-isolation heat intercept connection. The connection method involves clamping, by thermal interference fit, an electrically isolating cylinder between an outer metallic ring and an inner metallic disk. The connection provides durable coupling of a heat sink and a heat source.

  7. Hydrogen Selective Inorganic membranes for Gas Separations under High Pressure Intermediate Temperature Hydrocarbonic Envrionment

    SciTech Connect (OSTI)

    Rich Ciora; Paul KT Liu

    2012-06-27

    In this project, we have successfully developed a full scale commercially ready carbon molecular sieve (CMS) based membrane for applications in H{sub 2} recovery from refinery waste and other aggressive gas streams. Field tests at a refinery pilot plant and a coal gasification facility have successfully demonstrated its ability to recovery hydrogen from hydrotreating and raw syngas respectively. High purity H{sub 2} and excellent stability of the membrane permeance and selectivity were obtained in testing conducted over >500 hours at each site. The results from these field tests as well as laboratory testing conclude that the membranes can be operated at high pressures (up to 1,000 psig) and temperatures (up to 300 C) in presence of aggressive contaminants, such as sulfur and nitrogen containing species (H{sub 2}S, CO{sub 2}, NH{sub 3}, etc), condensable hydrocarbons, tar-like species, heavy metals, etc. with no observable effect on membrane performance. By comparison, similar operating conditions and/or environments would rapidly destroy competing membranes, such as polymeric, palladium, zeolitic, etc. Significant cost savings can be achieved through recovering H{sub 2} from refinery waste gas using this newly developed CMS membrane. Annual savings of $2 to 4MM/year (per 20,000 scfd of waste gas) can be realized by recovering the H{sub 2} for reuse (versus fuel). Projecting these values over the entire US market, potential H{sub 2} savings from refinery waste gases on the order of 750 to 1,000MM scfd and $750 to $1,000MM per year are possible. In addition to the cost savings, potential energy savings are projected to be ca. 150 to 220 tBTU/yr and CO{sub 2} gas emission reductions are projected to be ca. 5,000 to 6,500MMtons/year. The full scale membrane bundle developed as part of this project, i.e., 85 x 30 inch ceramic membrane tubes packaged into a full ceramic potting, is an important accomplishment. No comparable commercial scale product exists in the inorganic membrane field. Further, this newly developed full scale bundle concept can be extended to other thin film inorganic membrane technology (Pd, zeolite, etc), providing a potential commercialization pathway for these membrane materials that demonstrate high potential in a variety of separation applications yet remain a laboratory 'novelty' for lack of a full scale support. Overall, the project has been highly successful and all of the project objectives have been met. We have developed the first of its kind commercial scale carbon molecular sieve membrane and demonstrated its performance in field testing under aggressive operating conditions and in the presence of chemical contaminants that would rapidly destroy alternative organic and inorganic membranes. This innovative membrane permits H{sub 2} recovery from gas streams that up until now have not been successfully treated with membrane or conventional technology. Our end user participant is currently pursuing the field demonstration of this membrane for hydrogen recovery at its refinery site.

  8. Electrokinetic high pressure hydraulic system

    DOE Patents [OSTI]

    Paul, Phillip H.; Rakestraw, David J.; Arnold, Don W.; Hencken, Kenneth R.; Schoeniger, Joseph S.; Neyer, David W.

    2001-01-01

    An electrokinetic high pressure hydraulic pump for manipulating fluids in capillary-based systems. The pump uses electro-osmotic flow to provide a high pressure hydraulic system, having no moving mechanical parts, for pumping and/or compressing fluids, for providing valve means and means for opening and closing valves, for controlling fluid flow rate, and manipulating fluid flow generally and in capillary-based systems (Microsystems), in particular. The compact nature of the inventive high pressure hydraulic pump provides the ability to construct a micro-scale or capillary-based HPLC system that fulfills the desire for small sample quantity, low solvent consumption, improved efficiency, the ability to run samples in parallel, and field portability. Control of pressure and solvent flow rate is achieved by controlling the voltage applied to an electrokinetic pump.

  9. Electrokinetic high pressure hydraulic system

    DOE Patents [OSTI]

    Paul, Phillip H.; Rakestraw, David J.; Arnold, Don W.; Hencken, Kenneth R.; Schoeniger, Joseph S.; Neyer, David W.

    2003-06-03

    An electrokinetic high pressure hydraulic pump for manipulating fluids in capillary-based system. The pump uses electro-osmotic flow to provide a high pressure hydraulic system, having no moving mechanical parts, for pumping and/or compressing fluids, for providing valve means and means for opening and closing valves, for controlling fluid flow rate, and manipulating fluid flow generally and in capillary-based systems (microsystems), in particular. The compact nature of the inventive high pressure hydraulic pump provides the ability to construct a micro-scale or capillary-based HPLC system that fulfills the desire for small sample quantity, low solvent consumption, improved efficiency, the ability to run samples in parallel, and field portability. Control of pressure and solvent flow rate is achieved by controlling the voltage applied to an electrokinetic pump.

  10. High Exposure Facility Technical Description

    SciTech Connect (OSTI)

    Carter, Gregory L.; Stithem, Arthur R.; Murphy, Mark K.; Smith, Alex K.

    2008-02-12

    The High Exposure Facility is a collimated high-level gamma irradiator that is located in the basement of the 318 building. It was custom developed by PNNL back in 1982 to meet the needs for high range radiological instrument calibrations and dosimeter irradiations. At the time no commercially available product existed that could create exposure rates up to 20,000 R/h. This document is intended to pass on the design criteria that was employed to create this unique facility, while maintaining compliance with ANSI N543-1974, "General Safety Standard for Installations Using Non-Medical X-Ray and Sealed Gamma-Ray Sources, Energies up to 10 MeV."

  11. High elastic modulus polymer electrolytes

    DOE Patents [OSTI]

    Balsara, Nitash Pervez; Singh, Mohit; Eitouni, Hany Basam; Gomez, Enrique Daniel

    2013-10-22

    A polymer that combines high ionic conductivity with the structural properties required for Li electrode stability is useful as a solid phase electrolyte for high energy density, high cycle life batteries that do not suffer from failures due to side reactions and dendrite growth on the Li electrodes, and other potential applications. The polymer electrolyte includes a linear block copolymer having a conductive linear polymer block with a molecular weight of at least 5000 Daltons, a structural linear polymer block with an elastic modulus in excess of 1.times.10.sup.7 Pa and an ionic conductivity of at least 1.times.10.sup.-5 Scm.sup.-1. The electrolyte is made under dry conditions to achieve the noted characteristics.

  12. High pressure liquid level monitor

    DOE Patents [OSTI]

    Bean, Vern E. (Frederick, MD); Long, Frederick G. (Ijamsville, MD)

    1984-01-01

    A liquid level monitor for tracking the level of a coal slurry in a high-pressure vessel including a toroidal-shaped float with magnetically permeable bands thereon disposed within the vessel, two pairs of magnetic field generators and detectors disposed outside the vessel adjacent the top and bottom thereof and magnetically coupled to the magnetically permeable bands on the float, and signal processing circuitry for combining signals from the top and bottom detectors for generating a monotonically increasing analog control signal which is a function of liquid level. The control signal may be utilized to operate high-pressure control valves associated with processes in which the high-pressure vessel is used.

  13. INL High Performance Building Strategy

    SciTech Connect (OSTI)

    Jennifer D. Morton

    2010-02-01

    High performance buildings, also known as sustainable buildings and green buildings, are resource efficient structures that minimize the impact on the environment by using less energy and water, reduce solid waste and pollutants, and limit the depletion of natural resources while also providing a thermally and visually comfortable working environment that increases productivity for building occupants. As Idaho National Laboratory (INL) becomes the nations premier nuclear energy research laboratory, the physical infrastructure will be established to help accomplish this mission. This infrastructure, particularly the buildings, should incorporate high performance sustainable design features in order to be environmentally responsible and reflect an image of progressiveness and innovation to the public and prospective employees. Additionally, INL is a large consumer of energy that contributes to both carbon emissions and resource inefficiency. In the current climate of rising energy prices and political pressure for carbon reduction, this guide will help new construction project teams to design facilities that are sustainable and reduce energy costs, thereby reducing carbon emissions. With these concerns in mind, the recommendations described in the INL High Performance Building Strategy (previously called the INL Green Building Strategy) are intended to form the INL foundation for high performance building standards. This revised strategy incorporates the latest federal and DOE orders (Executive Order [EO] 13514, Federal Leadership in Environmental, Energy, and Economic Performance [2009], EO 13423, Strengthening Federal Environmental, Energy, and Transportation Management [2007], and DOE Order 430.2B, Departmental Energy, Renewable Energy, and Transportation Management [2008]), the latest guidelines, trends, and observations in high performance building construction, and the latest changes to the Leadership in Energy and Environmental Design (LEED) Green Building Rating System (LEED 2009). The document employs a two-level approach for high performance building at INL. The first level identifies the requirements of the Guiding Principles for Sustainable New Construction and Major Renovations, and the second level recommends which credits should be met when LEED Gold certification is required.

  14. High Performance Photovoltaic Project Overview

    SciTech Connect (OSTI)

    Symko-Davies, M.; McConnell, R.

    2005-01-01

    The High-Performance Photovoltaic (HiPerf PV) Project was initiated by the U.S. Department of Energy to substantially increase the viability of photovoltaics (PV) for cost-competitive applications so that PV can contribute significantly to our energy supply and environment in the 21st century. To accomplish this, the National Center for Photovoltaics (NCPV) directs in-house and subcontracted research in high-performance polycrystalline thin-film and multijunction concentrator devices. In this paper, we describe the recent research accomplishments in the in-house directed efforts and the research efforts under way in the subcontracted area.

  15. High energy overcurrent protective device

    DOE Patents [OSTI]

    Praeg, Walter F. (Palos Park, IL)

    1982-01-01

    Electrical loads connected to capacitance elements in high voltage direct current systems are protected from damage by capacitance discharge overcurrents by connecting between the capacitance element and the load, a longitudinal inductor comprising a bifilar winding wound about a magnetic core, which forms an incomplete magnetic circuit. A diode is connected across a portion of the bifilar winding which conducts a unidirectional current only. Energy discharged from the capacitance element is stored in the inductor and then dissipated in an L-R circuit including the diode and the coil winding. Multiple high voltage circuits having capacitance elements may be connected to loads through bifilar windings all wound about the aforementioned magnetic core.

  16. High temperature superconductor current leads

    DOE Patents [OSTI]

    Hull, John R. (Hinsdale, IL); Poeppel, Roger B. (Glen Ellyn, IL)

    1995-01-01

    An electrical lead having one end for connection to an apparatus in a cryogenic environment and the other end for connection to an apparatus outside the cryogenic environment. The electrical lead includes a high temperature superconductor wire and an electrically conductive material distributed therein, where the conductive material is present at the one end of the lead at a concentration in the range of from 0 to about 3% by volume, and at the other end of the lead at a concentration of less than about 20% by volume. Various embodiments are shown for groups of high temperature superconductor wires and sheaths.

  17. High ratio recirculating gas compressor

    DOE Patents [OSTI]

    Weinbrecht, J.F.

    1989-08-22

    A high ratio positive displacement recirculating rotary compressor is disclosed. The compressor includes an integral heat exchanger and recirculation conduits for returning cooled, high pressure discharge gas to the compressor housing to reducing heating of the compressor and enable higher pressure ratios to be sustained. The compressor features a recirculation system which results in continuous and uninterrupted flow of recirculation gas to the compressor with no direct leakage to either the discharge port or the intake port of the compressor, resulting in a capability of higher sustained pressure ratios without overheating of the compressor. 10 figs.

  18. Electrokinetic high pressure hydraulic system

    DOE Patents [OSTI]

    Paul, Phillip H. (Livermore, CA); Rakestraw, David J. (Fremont, CA)

    2000-01-01

    A compact high pressure hydraulic pump having no moving mechanical parts for converting electric potential to hydraulic force. The electrokinetic pump, which can generate hydraulic pressures greater than 2500 psi, can be employed to compress a fluid, either liquid or gas, and manipulate fluid flow. The pump is particularly useful for capillary-base systems. By combining the electrokinetic pump with a housing having chambers separated by a flexible member, fluid flow, including high pressure fluids, is controlled by the application of an electric potential, that can vary with time.

  19. High temperature superconductor current leads

    DOE Patents [OSTI]

    Hull, J.R.; Poeppel, R.B.

    1995-06-20

    An electrical lead is disclosed having one end for connection to an apparatus in a cryogenic environment and the other end for connection to an apparatus outside the cryogenic environment. The electrical lead includes a high temperature superconductor wire and an electrically conductive material distributed therein, where the conductive material is present at the one end of the lead at a concentration in the range of from 0 to about 3% by volume, and at the other end of the lead at a concentration of less than about 20% by volume. Various embodiments are shown for groups of high temperature superconductor wires and sheaths. 9 figs.

  20. High-Average Power Facilities

    SciTech Connect (OSTI)

    Dowell, David H.; Power, John G.; /Argonne

    2012-09-05

    There has been significant progress in the development of high-power facilities in recent years yet major challenges remain. The task of WG4 was to identify which facilities were capable of addressing the outstanding R&D issues presently preventing high-power operation. To this end, information from each of the facilities represented at the workshop was tabulated and the results are presented herein. A brief description of the major challenges is given, but the detailed elaboration can be found in the other three working group summaries.

  1. High temperature current mirror amplifier

    DOE Patents [OSTI]

    Patterson, R.B. III.

    1984-05-22

    Disclosed is a high temperature current mirror amplifier having biasing means in the transdiode connection of the input transistor for producing a voltage to maintain the base-collector junction reversed-biased and a current means for maintaining a current through the biasing means at high temperatures so that the base-collector junction of the input transistor remained reversed-biased. For accuracy, a second current mirror is provided with a biasing means and current means on the input leg. 2 figs.

  2. High ratio recirculating gas compressor

    DOE Patents [OSTI]

    Weinbrecht, John F. (601 Oakwood Pl., NE., Albuquerque, NM 87123)

    1989-01-01

    A high ratio positive displacement recirculating rotary compressor is disclosed. The compressor includes an integral heat exchanger and recirculation conduits for returning cooled, high pressure discharge gas to the compressor housing to reducing heating of the compressor and enable higher pressure ratios to be sustained. The compressor features a recirculation system which results in continuous and uninterrupted flow of recirculation gas to the compressor with no direct leakage to either the discharge port or the intake port of the compressor, resulting in a capability of higher sustained pressure ratios without overheating of the compressor.

  3. High loading uranium fuel plate

    DOE Patents [OSTI]

    Wiencek, Thomas C.; Domagala, Robert F.; Thresh, Henry R.

    1990-01-01

    Two embodiments of a high uranium fuel plate are disclosed which contain a meat comprising structured uranium compound confined between a pair of diffusion bonded ductile metal cladding plates uniformly covering the meat, the meat having a uniform high fuel loading comprising a content of uranium compound greater than about 45 Vol. % at a porosity not greater than about 10 Vol. %. In a first embodiment, the meat is a plurality of parallel wires of uranium compound. In a second embodiment, the meat is a dispersion compact containing uranium compound. The fuel plates are fabricated by a hot isostatic pressing process.

  4. Removing High Explosives from Groundwater

    Broader source: Energy.gov [DOE]

    LOS ALAMOS, N.M. – In an initiative supported by EM, Los Alamos National Laboratory’s Corrective Actions Program is addressing high explosive contamination in surface water and groundwater at a location this summer in the forests surrounding the laboratory.

  5. High-efficiency photovoltaic cells

    DOE Patents [OSTI]

    Yang, H.T.; Zehr, S.W.

    1982-06-21

    High efficiency solar converters comprised of a two cell, non-lattice matched, monolithic stacked semiconductor configuration using optimum pairs of cells having bandgaps in the range 1.6 to 1.7 eV and 0.95 to 1.1 eV, and a method of fabrication thereof, are disclosed. The high band gap subcells are fabricated using metal organic chemical vapor deposition (MOCVD), liquid phase epitaxy (LPE) or molecular beam epitaxy (MBE) to produce the required AlGaAs layers of optimized composition, thickness and doping to produce high performance, heteroface homojunction devices. The low bandgap subcells are similarly fabricated from AlGa(As)Sb compositions by LPE, MBE or MOCVD. These subcells are then coupled to form a monolithic structure by an appropriate bonding technique which also forms the required transparent intercell ohmic contact (IOC) between the two subcells. Improved ohmic contacts to the high bandgap semiconductor structure can be formed by vacuum evaporating to suitable metal or semiconductor materials which react during laser annealing to form a low bandgap semiconductor which provides a low contact resistance structure.

  6. High Impact Technology (HIT) Catalyst

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Impact Technology (HIT) Catalyst Images courtesy CREE, True Manufacturing, A.O. Smith, Bernstein Associates, Cambridge Engineering, Alliance Laundry Systems, NREL Commercial Buildings Integration Building Technologies Office 2 How can we catalyze the adoption of high impact commercial building technologies? Occupants Financial Institutions Government Utilities Scientists Manufacturers Dealers Suppliers Owners Stakeholder Engagement & Partnerships Managers Designers Engineers 3 Building

  7. High temperature turbine engine structure

    DOE Patents [OSTI]

    Boyd, Gary L. (Tempe, AZ)

    1990-01-01

    A high temperature turbine engine includes a hybrid ceramic/metallic rotor member having ceramic/metal joint structure. The disclosed joint is able to endure higher temperatures than previously possible, and aids in controlling heat transfer in the rotor member.

  8. High pressure neon arc lamp

    DOE Patents [OSTI]

    Sze, Robert C.; Bigio, Irving J.

    2003-07-15

    A high pressure neon arc lamp and method of using the same for photodynamic therapies is provided. The high pressure neon arc lamp includes a housing that encloses a quantity of neon gas pressurized to about 500 Torr to about 22,000 Torr. At each end of the housing the lamp is connected by electrodes and wires to a pulse generator. The pulse generator generates an initial pulse voltage to breakdown the impedance of the neon gas. Then the pulse generator delivers a current through the neon gas to create an electrical arc that emits light having wavelengths from about 620 nanometers to about 645 nanometers. A method for activating a photosensitizer is provided. Initially, a photosensitizer is administered to a patient and allowed time to be absorbed into target cells. Then the high pressure neon arc lamp is used to illuminate the target cells with red light having wavelengths from about 620 nanometers to about 645 nanometers. The red light activates the photosensitizers to start a chain reaction that may involve oxygen free radicals to destroy the target cells. In this manner, a high pressure neon arc lamp that is inexpensive and efficiently generates red light useful in photodynamic therapy is provided.

  9. High Performance Outdoor Lighting Accelerator

    Broader source: Energy.gov [DOE]

    Hosted by the U.S. Department of Energy (DOE)s Weatherization and Intergovernmental Programs Office (WIPO), this webinar covered the expansion of the Better Buildings platform to include the newest initiative for the public sector: the High Performance Outdoor Lighting Accelerator (HPOLA).

  10. High Performance Bulk Thermoelectric Materials

    SciTech Connect (OSTI)

    Ren, Zhifeng

    2013-03-31

    Over 13 plus years, we have carried out research on electron pairing symmetry of superconductors, growth and their field emission property studies on carbon nanotubes and semiconducting nanowires, high performance thermoelectric materials and other interesting materials. As a result of the research, we have published 104 papers, have educated six undergraduate students, twenty graduate students, nine postdocs, nine visitors, and one technician.

  11. High temperature turbine engine structure

    DOE Patents [OSTI]

    Boyd, Gary L. (Tempe, AZ)

    1991-01-01

    A high temperature turbine engine includes a rotor portion having axially stacked adjacent ceramic rotor parts. A ceramic/ceramic joint structure transmits torque between the rotor parts while maintaining coaxial alignment and axially spaced mutually parallel relation thereof despite thermal and centrifugal cycling.

  12. High precision redundant robotic manipulator

    DOE Patents [OSTI]

    Young, K.K.D.

    1998-09-22

    A high precision redundant robotic manipulator for overcoming contents imposed by obstacles or imposed by a highly congested work space is disclosed. One embodiment of the manipulator has four degrees of freedom and another embodiment has seven degrees of freedom. Each of the embodiments utilize a first selective compliant assembly robot arm (SCARA) configuration to provide high stiffness in the vertical plane, a second SCARA configuration to provide high stiffness in the horizontal plane. The seven degree of freedom embodiment also utilizes kinematic redundancy to provide the capability of avoiding obstacles that lie between the base of the manipulator and the end effector or link of the manipulator. These additional three degrees of freedom are added at the wrist link of the manipulator to provide pitch, yaw and roll. The seven degrees of freedom embodiment uses one revolute point per degree of freedom. For each of the revolute joints, a harmonic gear coupled to an electric motor is introduced, and together with properly designed based servo controllers provide an end point repeatability of less than 10 microns. 3 figs.

  13. High precision redundant robotic manipulator

    DOE Patents [OSTI]

    Young, Kar-Keung David (Mountain View, CA)

    1998-01-01

    A high precision redundant robotic manipulator for overcoming contents imposed by obstacles or imposed by a highly congested work space. One embodiment of the manipulator has four degrees of freedom and another embodiment has seven degreed of freedom. Each of the embodiments utilize a first selective compliant assembly robot arm (SCARA) configuration to provide high stiffness in the vertical plane, a second SCARA configuration to provide high stiffness in the horizontal plane. The seven degree of freedom embodiment also utilizes kinematic redundancy to provide the capability of avoiding obstacles that lie between the base of the manipulator and the end effector or link of the manipulator. These additional three degrees of freedom are added at the wrist link of the manipulator to provide pitch, yaw and roll. The seven degrees of freedom embodiment uses one revolute point per degree of freedom. For each of the revolute joints, a harmonic gear coupled to an electric motor is introduced, and together with properly designed based servo controllers provide an end point repeatability of less than 10 microns.

  14. Sandia National Laboratories: Research: High Consequence, Automation...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High-Consequence Automation Robotics Homepage About Robotics Research & Development Advanced Controls Advanced Manipulation Cybernetics High-Consequence Automation Demilitarization...

  15. Materials Characterization Capabilities at the High Temperature...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Materials Characterization Capabilities at the High Temperature Materials Laboratory: ... Success Stories from the High Temperature Materials Laboratory (HTML) User ...

  16. Materials Characterization Capabilities at the High Temperature...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Materials Characterization Capabilities at the High Temperature Materials Laboratory and ... Materials Characterization Capabilities at the High Temperature Materials Laboratory and ...

  17. High Impact Technology Catalyst: Technology Deployment Strategies...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Catalyst: Technology Deployment Strategies High Impact Technology Catalyst: Technology Deployment Strategies The Energy Department released the High Impact Technology Catalyst: ...

  18. High performance internal reforming unit for high temperature fuel cells

    DOE Patents [OSTI]

    Ma, Zhiwen (Sandy Hook, CT); Venkataraman, Ramakrishnan (New Milford, CT); Novacco, Lawrence J. (Brookfield, CT)

    2008-10-07

    A fuel reformer having an enclosure with first and second opposing surfaces, a sidewall connecting the first and second opposing surfaces and an inlet port and an outlet port in the sidewall. A plate assembly supporting a catalyst and baffles are also disposed in the enclosure. A main baffle extends into the enclosure from a point of the sidewall between the inlet and outlet ports. The main baffle cooperates with the enclosure and the plate assembly to establish a path for the flow of fuel gas through the reformer from the inlet port to the outlet port. At least a first directing baffle extends in the enclosure from one of the sidewall and the main baffle and cooperates with the plate assembly and the enclosure to alter the gas flow path. Desired graded catalyst loading pattern has been defined for optimized thermal management for the internal reforming high temperature fuel cells so as to achieve high cell performance.

  19. High energy resolution, high angular acceptance crystal monochromator

    DOE Patents [OSTI]

    Alp, Ercan E. (Bolingbrook, IL); Mooney, Timothy M. (Westmont, IL); Toellner, Thomas (Green Bay, WI)

    1996-06-04

    A 4-bounce dispersive crystal monochromator reduces the bandpass of synchrotron radiation to a 10-50 meV range without sacrificing angular acceptance. The monochromator includes the combination of an asymmetrical channel-cut single crystal of lower order reflection and a symmetrical channel-cut single crystal of higher order reflection in a nested geometric configuration. In the disclosed embodiment, a highly asymmetrically cut (.alpha.=20) outer silicon crystal (4 2 2) with low order reflection is combined with a symmetrically cut inner silicon crystal (10 6 4) with high order reflection to condition a hard x-ray component (5-30 keV) of synchrotron radiation down to the .mu.eV-neV level. Each of the crystals is coupled to the combination of a positioning inchworm and angle encoder via a respective rotation stage for accurate relative positioning of the crystals and precise energy tuning of the monochromator.

  20. High energy resolution, high angular acceptance crystal monochromator

    DOE Patents [OSTI]

    Alp, E.E.; Mooney, T.M.; Toellner, T.

    1996-06-04

    A 4-bounce dispersive crystal monochromator reduces the bandpass of synchrotron radiation to a 10-50 meV range without sacrificing angular acceptance. The monochromator includes the combination of an asymmetrical channel-cut single crystal of lower order reflection and a symmetrical channel-cut single crystal of higher order reflection in a nested geometric configuration. In the disclosed embodiment, a highly asymmetrically cut ({alpha}=20) outer silicon crystal (4 2 2) with low order reflection is combined with a symmetrically cut inner silicon crystal (10 6 4) with high order reflection to condition a hard x-ray component (5--30 keV) of synchrotron radiation down to the {micro}eV-neV level. Each of the crystals is coupled to the combination of a positioning inchworm and angle encoder via a respective rotation stage for accurate relative positioning of the crystals and precise energy tuning of the monochromator. 7 figs.