National Library of Energy BETA

Sample records for hard x-ray telescopes

  1. Application of an EMCCD Camera for Calibration of Hard X-Ray Telescopes

    SciTech Connect (OSTI)

    Vogel, J K; Pivovaroff, M J; Nagarkar, V V; Kudrolli, H; Madsen, K K; Koglin, J E; Christensen, F E; Brejnholt, N F

    2011-11-08

    Recent technological innovations now make it feasible to construct hard x-ray telescopes for space-based astronomical missions. Focusing optics are capable of improving the sensitivity in the energy range above 10 keV by orders of magnitude compared to previously used instruments. The last decade has seen focusing optics developed for balloon experiments and they will soon be implemented in approved space missions such as the Nuclear Spectroscopic Telescope Array (NuSTAR) and ASTRO-H. The full characterization of x-ray optics for astrophysical and solar imaging missions, including measurement of the point spread function (PSF) as well as scattering and reflectivity properties of substrate coatings, requires a very high spatial resolution, high sensitivity, photon counting and energy discriminating, large area detector. Novel back-thinned Electron Multiplying Charge-Coupled Devices (EMCCDs) are highly suitable detectors for ground-based calibrations. Their chip can be optically coupled to a microcolumnar CsI(Tl) scintillator via a fiberoptic taper. Not only does this device exhibit low noise and high spatial resolution inherent to CCDs, but the EMCCD is also able to handle high frame rates due to its controllable internal gain. Additionally, thick CsI(Tl) yields high detection efficiency for x-rays. This type of detector has already proven to be a unique device very suitable for calibrations in astrophysics: such a camera was used to support the characterization of the performance for all NuSTAR optics. Further optimization will enable similar cameras to be improved and used to calibrate x-ray telescopes for future space missions. In this paper, we discuss the advantages of using an EMCCD to calibrate hard x-ray optics. We will illustrate the promising features of this detector solution using examples of data obtained during the ground calibration of the NuSTAR telescopes performed at Columbia University during 2010/2011. Finally, we give an outlook on ongoing

  2. Hard x-ray delay line for x-ray photon correlation spectroscopy...

    Office of Scientific and Technical Information (OSTI)

    Hard x-ray delay line for x-ray photon correlation spectroscopy and jitter-free pump-probe experiments at LCLS Citation Details In-Document Search Title: Hard x-ray delay line for...

  3. Femtosecond X-ray Absorption Spectroscopy at a Hard X-ray Free...

    Office of Scientific and Technical Information (OSTI)

    Femtosecond X-ray Absorption Spectroscopy at a Hard X-ray Free Electron Laser: Application to Spin Crossover Dynamics Citation Details In-Document Search Title: Femtosecond X-ray...

  4. THE LACK OF DIFFUSE, NON-THERMAL HARD X-RAY EMISSION IN THE COMA CLUSTER: THE SWIFT BURST ALERT TELESCOPE'S EYE VIEW

    SciTech Connect (OSTI)

    Wik, Daniel R.; Baumgartner, Wayne H.; Okajima, Takashi; Tueller, Jack; Finoguenov, Alexis; Mushotzky, Richard F.; Clarke, Tracy E.

    2011-02-01

    The Coma Cluster of galaxies hosts the brightest radio halo known and has therefore been the target of numerous searches for associated inverse Compton (IC) emission, particularly at hard X-ray energies where the IC signal must eventually dominate over thermal emission. The most recent search with the Suzaku Hard X-ray Detector failed to confirm previous IC detections with RXTE and BeppoSAX, instead setting an upper limit 2.5 times below their non-thermal flux. However, this discrepancy can be resolved if the IC emission is very extended, beyond the scale of the cluster radio halo. Using reconstructed sky images from the 58-month Swift Burst Alert Telescope (BAT) all-sky survey, the feasibility of such a solution is investigated. Building on Renaud et al., we test and implement a method for extracting the fluxes of extended sources, assuming specified spatial distributions. BAT spectra are jointly fit with an XMM-Newton EPIC-pn spectrum derived from mosaic observations. We find no evidence for large-scale IC emission at the level expected from the previously detected non-thermal fluxes. For all non-thermal spatial distributions considered, which span the gamut of physically reasonable IC models, we determine upper limits for which the largest (most conservative) limit is {approx}<4.2 x 10{sup -12} erg s{sup -1} cm{sup -2} (20-80 keV), which corresponds to a lower limit on the magnetic field B > 0.2 {mu} G. A nominal flux upper limit of <2.7 x 10{sup -12} erg s{sup -1} cm{sup -2}, with corresponding B > 0.25 {mu} G, is derived for the most probable IC distribution given the size of the radio halo and likely magnetic field radial profile.

  5. Achieving hard X-ray nanofocusing using a wedged multilayer Laue...

    Office of Scientific and Technical Information (OSTI)

    anticipate that continuous development on wedged MLLs will advance x-ray nanofocusing optics to new frontiers and enrich capabilities and opportunities for hard X-ray microscopy....

  6. Method and apparatus for micromachining using hard X-rays

    DOE Patents [OSTI]

    Siddons, David Peter; Johnson, Erik D.; Guckel, Henry; Klein, Jonathan L.

    1997-10-21

    An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures.

  7. Method and apparatus for micromachining using hard X-rays

    DOE Patents [OSTI]

    Siddons, D.P.; Johnson, E.D.; Guckel, H.; Klein, J.L.

    1997-10-21

    An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures. 21 figs.

  8. Femtosecond x-ray absorption spectroscopy with hard x-ray free electron laser

    SciTech Connect (OSTI)

    Katayama, Tetsuo; Togashi, Tadashi; Tono, Kensuke; Kameshima, Takashi; Inubushi, Yuichi; Sato, Takahiro; Hatsui, Takaki; Yabashi, Makina; Obara, Yuki; Misawa, Kazuhiko; Bhattacharya, Atanu; Kurahashi, Naoya; Ogi, Yoshihiro; Suzuki, Toshinori; Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198

    2013-09-23

    We have developed a method of dispersive x-ray absorption spectroscopy with a hard x-ray free electron laser (XFEL), generated by a self-amplified spontaneous emission (SASE) mechanism. A transmission grating was utilized for splitting SASE-XFEL light, which has a relatively large bandwidth (ΔE/E ∼ 5 × 10{sup −3}), into several branches. Two primary split beams were introduced into a dispersive spectrometer for measuring signal and reference spectra simultaneously. After normalization, we obtained a Zn K-edge absorption spectrum with a photon-energy range of 210 eV, which is in excellent agreement with that measured by a conventional wavelength-scanning method. From the analysis of the difference spectra, the noise ratio was evaluated to be ∼3 × 10{sup −3}, which is sufficiently small to trace minute changes in transient spectra induced by an ultrafast optical laser. This scheme enables us to perform single-shot, high-accuracy x-ray absorption spectroscopy with femtosecond time resolution.

  9. Application of hard X-ray microprobe methods to clay-rich materials...

    Office of Scientific and Technical Information (OSTI)

    Application of hard X-ray microprobe methods to clay-rich materials Citation Details In-Document Search Title: Application of hard X-ray microprobe methods to clay-rich materials ...

  10. Distributed seeding for narrow-line width hard x-ray free-electron...

    Office of Scientific and Technical Information (OSTI)

    for narrow-line width hard x-ray free-electron lasers Citation Details In-Document Search Title: Distributed seeding for narrow-line width hard x-ray free-electron lasers We ...

  11. Monte-Carlo simulation of noise in hard X-ray Transmission Crystal...

    Office of Scientific and Technical Information (OSTI)

    Monte-Carlo simulation of noise in hard X-ray Transmission Crystal Spectrometers: ... Title: Monte-Carlo simulation of noise in hard X-ray Transmission Crystal Spectrometers: ...

  12. Toward TW-Level, Hard X-Ray Pulses at LCLS (Conference) | SciTech...

    Office of Scientific and Technical Information (OSTI)

    Toward TW-Level, Hard X-Ray Pulses at LCLS Citation Details In-Document Search Title: Toward TW-Level, Hard X-Ray Pulses at LCLS You are accessing a document from the Department ...

  13. A single-shot transmissive spectrometer for hard x-ray free electron...

    Office of Scientific and Technical Information (OSTI)

    Results Journal Article: A single-shot transmissive spectrometer for hard x-ray free electron lasers Citation Details ... We report hard x-ray single-shot spectral measurements of ...

  14. SSRL School 2007 on Hard X-ray Scattering Techniques in MES

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    May 15-17, 2007 SSRL School on Hard X-ray Scattering Techniques in Materials and Environmental Sciences Group photo taken at the SSRL School on Hard X-ray Scattering Techniques in...

  15. The LCLS variable-energy hard X-ray single-shot spectrometer...

    Office of Scientific and Technical Information (OSTI)

    The LCLS variable-energy hard X-ray single-shot spectrometer Citation Details In-Document Search Title: The LCLS variable-energy hard X-ray single-shot spectrometer The engineering ...

  16. A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

    SciTech Connect (OSTI)

    Seidler, G. T. Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R.

    2014-11-15

    We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ∼5 keV to ∼10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}–10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

  17. Expectations for the hard x-ray continuum and gamma-ray line...

    Office of Scientific and Technical Information (OSTI)

    x-ray continuum and gamma-ray line fluxes from the typE IA supernova SN 2014J in M82 Citation Details In-Document Search Title: Expectations for the hard x-ray continuum and ...

  18. Exploring electronic structure through high-resolution hard x-ray

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    spectroscopies | Stanford Synchrotron Radiation Lightsource Exploring electronic structure through high-resolution hard x-ray spectroscopies Tuesday, July 23, 2013 - 11:00am SLAC, Conference Room 137-322 Presented by Dimosthenis Sokaras, Stanford Synchrotron Radiation Lightsource, SLAC National Accelerator Laboratory Modern high brilliance beamlines coupled with recent advances in hard-x-ray optics are establishing high-resolution hard x-ray spectroscopies as a powerful analytical tool for

  19. Investigation of the hard x-ray background in backlit pinhole imagers

    SciTech Connect (OSTI)

    Fein, J. R. Holloway, J. P.; Peebles, J. L.; Keiter, P. A.; Klein, S. R.; Kuranz, C. C.; Manuel, M. J.-E.; Drake, R. P.

    2014-11-15

    Hard x-rays from laser-produced hot electrons (>10 keV) in backlit pinhole imagers can give rise to a background signal that decreases signal dynamic range in radiographs. Consequently, significant uncertainties are introduced to the measured optical depth of imaged plasmas. Past experiments have demonstrated that hard x-rays are produced when hot electrons interact with the high-Z pinhole substrate used to collimate the softer He-? x-ray source. Results are presented from recent experiments performed on the OMEGA-60 laser to further study the production of hard x-rays in the pinhole substrate and how these x-rays contribute to the background signal in radiographs. Radiographic image plates measured hard x-rays from pinhole imagers with Mo, Sn, and Ta pinhole substrates. The variation in background signal between pinhole substrates provides evidence that much of this background comes from x-rays produced in the pinhole substrate itself. A Monte Carlo electron transport code was used to model x-ray production from hot electrons interacting in the pinhole substrate, as well as to model measurements of x-rays from the irradiated side of the targets, recorded by a bremsstrahlung x-ray spectrometer. Inconsistencies in inferred hot electron distributions between the different pinhole substrate materials demonstrate that additional sources of hot electrons beyond those modeled may produce hard x-rays in the pinhole substrate.

  20. Ambient Pressure Photoelectron Spectroscopy Using Soft X-ray and Hard

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-ray, and its applications in electrochemistry | Stanford Synchrotron Radiation Lightsource Ambient Pressure Photoelectron Spectroscopy Using Soft X-ray and Hard X-ray, and its applications in electrochemistry Friday, December 14, 2012 - 3:30pm SSRL, Bldg. 137, room 322 Zhi Liu The synchrotron based ambient pressure x-ray photoelectron spectroscopy (AP-XPS) endstation[1] pioneered at ALS based on differentially pumped electron energy analyzer has been recognized by scientific communities as

  1. The hard X-ray shortages prompted by the clock bursts in GS 1826-238

    SciTech Connect (OSTI)

    Ji, Long; Zhang, Shu; Chen, YuPeng; Zhang, Shuang-Nan; Li, Jian; Torres, Diego F.; Kretschmar, Peter

    2014-02-10

    We report on a study of GS 1826-238 using all available Rossi X-Ray Timing Explorer observations, concentrating on the behavior of the hard X-rays during type-I bursts. We find a hard X-ray shortage at 30-50 keV prompted by the shower of soft X-rays coming from type-I bursts. This shortage happens with a time delay after the peak of the soft flux of 3.6 ± 1.2 s. The behavior of hard X-rays during bursts indicates cooling and reheating of the corona, during which a large amount of energy is required. We speculate that this energy originates from the feedback of the type-I bursts to the accretion process, resulting in a rapid temporary increase of the accretion rate.

  2. Hard disk drive based microsecond x-ray chopper for characterization of ionization chambers and photodiodes

    SciTech Connect (OSTI)

    Müller, O. Lützenkirchen-Hecht, D.; Frahm, R.

    2015-03-15

    A fast X-ray chopper capable of producing ms long X-ray pulses with a typical rise time of few μs was realized. It is ideally suited to investigate the temporal response of X-ray detectors with response times of the order of μs to ms, in particular, any kind of ionization chambers and large area photo diodes. The drive mechanism consists of a brushless DC motor and driver electronics from a common hard disk drive, keeping the cost at an absolute minimum. Due to its simple construction and small dimensions, this chopper operates at home lab based X-ray tubes and synchrotron radiation sources as well. The dynamics of the most important detectors used in time resolved X-ray absorption spectroscopy, namely, ionization chambers and Passivated Implanted Planar Silicon photodiodes, were investigated in detail. The results emphasize the applicability of this X-ray chopper.

  3. IMPULSIVE PHASE CORONAL HARD X-RAY SOURCES IN AN X3.9 CLASS SOLAR...

    Office of Scientific and Technical Information (OSTI)

    We present the analysis of a pair of unusually energetic coronal hard X-ray (HXR) sources detected by the Reuven Ramaty High Energy Solar Spectroscopic Imager during the impulsive ...

  4. Analysis and Interpretation of Hard X-ray Emission fromthe Bullet...

    Office of Scientific and Technical Information (OSTI)

    Analysis and Interpretation of Hard X-ray Emission fromthe Bullet Cluster (1E0657-56), the Most Distant Cluster of Galaxies Observed by the RXTE Citation Details In-Document Search ...

  5. HARD X-RAY OBSERVATIONS OF A JET AND ACCELERATED ELECTRONS IN THE CORONA

    SciTech Connect (OSTI)

    Glesener, Lindsay; Lin, R. P.; Krucker, Saem, E-mail: glesener@ssl.berkeley.edu [Space Science Laboratory, UC Berkeley, 7 Gauss Way, Berkeley, CA 94720 (United States)

    2012-07-20

    We report the first hard X-ray observation of a solar jet on the limb with flare footpoints occulted, so that faint emission from accelerated electrons in the corona can be studied in detail. In this event on 2003 August 21, RHESSI observed a double coronal hard X-ray source in the pre-impulsive phase at both thermal and nonthermal energies. In the impulsive phase, the first of two hard X-ray bursts consists of a single thermal/nonthermal source coinciding with the lower of the two earlier sources, and the second burst shows an additional nonthermal, elongated source, spatially and temporally coincident with the coronal jet. Analysis of the jet hard X-ray source shows that collisional losses by accelerated electrons can deposit enough energy to generate the jet. The hard X-ray time profile above 20 keV matches that of the accompanying Type III and broadband gyrosynchrotron radio emission, indicating both accelerated electrons escaping outward along the jet path and electrons trapped in the flare loop. The double coronal hard X-ray source, the open field lines indicated by Type III bursts, and the presence of a small post-flare loop are consistent with significant electron acceleration in an interchange reconnection geometry.

  6. Optimal focusing for a linac-based hard x-ray source

    SciTech Connect (OSTI)

    Liu, C.; Krafft, G.; Talman, R.

    2011-03-28

    In spite of having a small average beam current limit, a linac can have features that make it attractive as an x-ray source: high energy, ultralow emittance and energy spread, and flexible beamline optics. Unlike a storage ring, in which an (undulator) radiation source is necessarily short and positioned at an electron beam waist, in a linac the undulator can be long and the electron beam can be adjusted to have a (virtual) waist far downstream toward the x-ray target. Using a planned CEBAF beamline as an example, this paper shows that a factor of 2000 in beam current can be overcome to produce a monochromatic hard x-ray source comparable with, or even exceeding, the performance of an x-ray line at a third generation storage ring. Optimal electron beam focusing conditions for x-ray flux density and brilliance are derived, and are verified by simulations using the SRW code.

  7. Metrology for x-ray telescope mirrors in a vertical configuration

    SciTech Connect (OSTI)

    Li, Haizhang; Li, Xiaodan; Grindel, M.W.

    1995-09-01

    Mirrors used in x-ray telescope systems for observations outside of the earth`s atmosphere are usually made of several thin nested shells, each formed by a pair of paraboloidal and hyperboloidal surfaces. The thin shells are very susceptible to self-weight deflection caused by gravity and are nearly impossible to test by conventional interferometric techniques. The metrology requirements for these mirrors are extremely challenging. This paper presents a prototype of a Vertical Scanning Long Trace Profiler (VSLTP) which is optimized to measure the surface figure of x-ray telescope mirrors in a vertical orientation. The optical system of the VSLTP is described. Experimental results from measurements on an x-ray telescope mandrel and tests of the accuracy and repeatability of the prototype VSLTP are presented. The prototype instrument has achieved a height measurement accuracy of about 50 nanometers with a repeatability of better than 20 nanometers, and a slope measurement accuracy of about 1 microradian.

  8. eHXI: A permanently installed, hard x-ray imager for the National Ignition Facility

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Doppner, T.; Bachmann, B.; Albert, F.; Bell, P.; Burns, S.; Celeste, J.; Chow, R.; Divol, L.; Dewald, E. L.; Hohenberger, M.; et al

    2016-06-14

    We have designed and built a multi-pinhole imaging system for high energy x-rays (≥ 50 keV) that is permanently installed in the equatorial plane outside of the target chamber at the National Ignition Facility (NIF). It records absolutely-calibrated, time-integrated x-ray images with the same line-of-sight as the multi-channel, spatially integrating hard x-ray detector FFLEX [McDonald et al., Rev. Sci. Instrum. 75 (2004) 3753], having a side view of indirect-drive inertial confinement fusion (ICF) implosion targets. The equatorial hard x-ray imager (eHXI) has recorded images on the majority of ICF implosion experiments since May 2011. Lastly, eHXI provides valuable information onmore » hot electron distribution in hohlraum experiments, target alignment, potential hohlraum drive asymmetries and serves as a long term reference for the FFLEX diagnostics.« less

  9. Runaway electron energy measurement using hard x-ray spectroscopy in 'Damavand' tokamak

    SciTech Connect (OSTI)

    Rasouli, C.; Farahbod, A. H.; Rasouli, H.; Lamehi, M.; Iraji, D.; Akhtari, K.; Modarresi, H.

    2009-01-15

    Set of experiments has been developed to study existing runaway electrons in ''Damavand'' tokamak plasma upon characteristics of hard x-ray emissions produced by collision of the runaway electrons with the plasma particles and limiters. As a first step, spatial distribution of hard x-ray emissions on the equatorial plane of the torus was considered. Obtained spectra of hard x-ray emissions for different alignments of shielded detector indicate isotropic emissivity in the equatorial plane. This is in agreement with wide angle cone of bremsstrahlung radiations, deduced from the mean value of energy of the runaway electrons. The mean energy was calculated from the slope of the energy spectrum of hard x-ray photons. In the second stage in order to investigate time evolution of energy of the runaway electrons, similar technique were applied to obtain hard x-ray energy in every 3 ms intervals, from the beginning to the end of plasma. The mean energy of the runaway electrons increases during the ramp up phase and reaches its maximum between 3 and 9 ms after plasma formation. Also considering the time dependence of the counted photons in each energy range shows that energetic photons are emitted during the ramp up phase of the plasma current in Damavand tokamak.

  10. Pulse energy measurement at the hard x-ray laser in Japan

    SciTech Connect (OSTI)

    Kato, M.; Tanaka, T.; Saito, N.; Kurosawa, T.; Richter, M.; Sorokin, A. A.; Tiedtke, K.; Kudo, T.; Yabashi, M.; Tono, K.; Ishikawa, T.

    2012-07-09

    The pulse energies of a free electron laser have accurately been measured in the hard x-ray spectral range. In the photon energy regime from 4.4 keV to 16.8 keV, pulse energies up to 100 {mu}J were obtained at the hard x-ray laser facility SACLA (SPring-8 Angstrom Compact free-electron LAser). Two independent methods, using a cryogenic radiometer and a gas monitor detector, were applied and agreement within 3.3% was achieved. Based on our validated pulse energy measurement, a SACLA online monitor detector could be calibrated for all future experiments.

  11. Hard X-ray spatial array diagnostics on Joint Texas Experimental Tokamak

    SciTech Connect (OSTI)

    Huang, D. W.; Chen, Z. Y. Luo, Y. H.; Tong, R. H.; Yan, W.; Jin, W.; Zhuang, G.

    2014-11-15

    A spatially distributed hard X-ray detection array has been developed to diagnose the loss of runaway electron with toroidal and poloidal resolution. The hard X-ray radiation in the energy ranges of 0.31 MeV resulted from runaway electrons can be measured. The detection array consists of 12 CdTe detectors which are arranged surrounding the tokamak. It is found that most runaway electrons which transport to plasma boundary tend to loss on limiters. The application of electrode biasing probe resulted in enhancement of local runaway loss. Resonant magnetic perturbations enhanced the runaway electrons diffusion and showed an asymmetric poloidal loss rate.

  12. Achieving hard X-ray nanofocusing using a wedged multilayer Laue lens

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Huang, Xiaojing; Conley, Raymond; Bouet, Nathalie; Zhou, Juan; Macrander, Albert; Maser, Jorg; Yan, Hanfei; Nazaretski, Evgeny; Lauer, Kenneth; Harder, Ross; et al

    2015-05-04

    We report on the fabrication and the characterization of a wedged multilayer Laue lens for x-ray nanofocusing. The lens was fabricated using a sputtering deposition technique, in which a specially designed mask was employed to introduce a thickness gradient in the lateral direction of the multilayer. X-ray characterization shows an efficiency of 27% and a focus size of 26 nm at 14.6 keV, in a good agreement with theoretical calculations. These results indicate that the desired wedging is achieved in the fabricated structure. We anticipate that continuous development on wedged MLLs will advance x-ray nanofocusing optics to new frontiers andmoreenrich capabilities and opportunities for hard X-ray microscopy.less

  13. Achieving Hard X-ray Nanofocusing Using a Wedged Multilayer Laue Lens

    SciTech Connect (OSTI)

    Huang, Xiaojing; Conley, Raymond; Bouet, Nathalie; Zhou, Juan; Macrander, Albert; Maser, Jorg; Yan, Hanfei; Nazaretski, Evgeny; Lauer, Kenneth; Harder, Ross; Robinson, Ian K.; Kalbfleisch, Sebastian; Chu, Yong S.

    2015-05-04

    Here, we report on the fabrication and the characterization of a wedged multilayer Laue lens for x-ray nanofocusing. The lens was fabricated using a sputtering deposition technique, in which a specially designed mask was employed to introduce a thickness gradient in the lateral direction of the multilayer. X-ray characterization shows an efficiency of 27% and a focus size of 26 nm at 14.6 keV, in a good agreement with theoretical calculations. Our results indicate that the desired wedging is achieved in the fabricated structure. Furthermore, we anticipate that continuous development on wedged MLLs will advance x-ray nanofocusing optics to new frontiers and enrich capabilities and opportunities for hard X-ray microscopy.

  14. Study of runaway electrons using dosimetry of hard x-ray radiations in Damavand tokamak

    SciTech Connect (OSTI)

    Rasouli, C.; Pourshahab, B.; Rasouli, H.; Hosseini Pooya, S. M.; Orouji, T.

    2014-05-15

    In this work several studies have been conducted on hard x-ray emissions of Damavand tokamak based on radiation dosimetry using the Thermoluminescence method. The goal was to understand interactions of runaway electrons with plasma particles, vessel wall, and plasma facing components. Total of 354 GR-200 (LiF:Mg,Cu,P) thermoluminescence dosimeter (TLD) crystals have been placed on 118 points – three TLDs per point – to map hard x-ray radiation doses on the exterior of the vacuum vessel. Results show two distinctive levels of x-ray radiations doses on the exterior of the vessel. The low-dose area on which measured dose is about 0.5 mSv/shot. In the low-dose area there is no particular component inside the vessel. On the contrary, on high-dose area of the vessel, x-ray radiations dose exceeds 30 mSv/shot. The high-dose area coincides with the position of limiters, magnetic probe ducts, and vacuum vessel intersections. Among the high-dose areas, the highest level of dose is measured in the position of the limiter, which could be due to its direct contact with the plasma column and with runaway electrons. Direct collisions of runaway electrons with the vessel wall and plasma facing components make a major contribution for production of hard x-ray photons in Damavand tokamak.

  15. Multimodality hard-x-ray imaging of a chromosome with nanoscale spatial resolution

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Yan, Hanfei; Nazaretski, Evgeny; Lauer, Kenneth R.; Huang, Xiaojing; Wagner, Ulrich; Rau, Christoph; Yusuf, Mohammed; Robinson, Ian K.; Kalbfleisch, Sebastian; Li, Li; et al

    2016-02-05

    Here, we developed a scanning hard x-ray microscope using a new class of x-ray nano-focusing optic called a multilayer Laue lens and imaged a chromosome with nanoscale spatial resolution. The combination of the hard x-ray's superior penetration power, high sensitivity to elemental composition, high spatial-resolution and quantitative analysis creates a unique tool with capabilities that other microscopy techniques cannot provide. Using this microscope, we simultaneously obtained absorption-, phase-, and fluorescence-contrast images of Pt-stained human chromosome samples. The high spatial-resolution of the microscope and its multi-modality imaging capabilities enabled us to observe the internal ultra-structures of a thick chromosome without sectioningmore » it.« less

  16. Study of runaway electrons with Hard X-ray spectrometry of tokamak plasmas

    SciTech Connect (OSTI)

    Shevelev, A.; Chugunov, I.; Khilkevitch, E.; Gin, D.; Doinikov, D.; Naidenov, V.; Kiptily, V.; Collaboration: EFDA-JET Contributors

    2014-08-21

    Hard-X-ray spectrometry is a tool widely used for diagnostic of runaway electrons in existing tokamaks. In future machines, ITER and DEMO, HXR spectrometry will be useful providing information on runaway electron energy, runaway beam current and its profile during disruption.

  17. In-Orbit Performance of the Hard X-Ray Detector on Borad Suzaku

    SciTech Connect (OSTI)

    Kokubun, Motohide; Makishima, Kazuo; Takahashi, Tadayuki; Murakami, Toshio; Tashiro, Makoto; Fukazawa, Yasushi; Kamae, Tuneyoshi; M.Madejski, Greg; Nakazawa, Kazuhiro; Yamaoka, Kazutaka; Terada, Yukikatsu; Yonetoku, Daisuke; Watanabe, Shin; Tamagawa, Toru; Mizuno, Tsunefumi; Kubota, Aya; Isobe, Naoki; Takahashi, Isao; Sato, Goro; Takahashi, Hiromitsu; Hong, Soojing; /Tokyo U. /Wako, RIKEN /JAXA, Sagamihara /Kanazawa U. /Saitama U. /Hiroshima U. /Aoyama Gakuin U. /Nihon U., Narashino /SLAC

    2007-10-26

    The in-orbit performance and calibration of the Hard X-ray Detector (HXD) on board the X-ray astronomy satellite Suzaku are described. Its basic performances, including a wide energy bandpass of 10-600 keV, energy resolutions of {approx}4 keV (FWHM) at 40 keV and {approx}11% at 511 keV, and a high background rejection efficiency, have been confirmed by extensive in-orbit calibrations. The long-term gains of PIN-Si diodes have been stable within 1% for half a year, and those of scintillators have decreased by 5-20%. The residual non-X-ray background of the HXD is the lowest among past non-imaging hard X-ray instruments in energy ranges of 15-70 and 150-500 keV. We provide accurate calibrations of energy responses, angular responses, timing accuracy of the HXD, and relative normalizations to the X-ray CCD cameras using multiple observations of the Crab Nebula.

  18. HARD X-RAY AND MICROWAVE EMISSIONS FROM SOLAR FLARES WITH HARD SPECTRAL INDICES

    SciTech Connect (OSTI)

    Kawate, T.; Nishizuka, N.; Oi, A.; Ohyama, M.; Nakajima, H.

    2012-03-10

    We analyze 10 flare events that radiate intense hard X-ray (HXR) emission with significant photons over 300 keV to verify that the electrons that have a common origin of acceleration mechanism and energy power-law distribution with solar flares emit HXRs and microwaves. Most of these events have the following characteristics. HXRs emanate from the footpoints of flare loops, while microwaves emanate from the tops of flare loops. The time profiles of the microwave emission show delays of peak with respect to those of the corresponding HXR emission. The spectral indices of microwave emissions show gradual hardening in all events, while the spectral indices of the corresponding HXR emissions are roughly constant in most of the events, though rather rapid hardening is simultaneously observed in some for both indices during the onset time and the peak time. These characteristics suggest that the microwave emission emanates from the trapped electrons. Then, taking into account the role of the trapping of electrons for the microwave emission, we compare the observed microwave spectra with the model spectra calculated by a gyrosynchrotron code. As a result, we successfully reproduce the eight microwave spectra. From this result, we conclude that the electrons that have a common acceleration and a common energy distribution with solar flares emit both HXR and microwave emissions in the eight events, though microwave emission is contributed to by electrons with much higher energy than HXR emission.

  19. Extending synchrotron-based atomic physics experiments into the hard X-ray region

    SciTech Connect (OSTI)

    LeBrun, T.

    1996-12-31

    The high-brightness, hard x-ray beams available from third-generation synchrotron sources are opening new opportunities to study the deepest inner shells of atoms, an area where little work has been done and phenomena not observed in less tightly bound inner-shells are manifested. In addition scattering processes which are weak at lower energies become important, providing another tool to investigate atomic structure as well as an opportunity to study photon/atom interactions beyond photoabsorption. In this contribution the authors discuss some of the issues related to extending synchrotron-based atomic physics experiments into the hard x-ray region from the physical and the experimental point of view. They close with a discussion of a technique, resonant Raman scattering, that may prove invaluable in determining the spectra of the very highly-excited states resulting from the excitation of deep inner shells.

  20. Self-standing quasi-mosaic crystals for focusing hard X-rays

    SciTech Connect (OSTI)

    Camattari, Riccardo; Guidi, Vincenzo; Bellucci, Valerio; Neri, Ilaria; Frontera, Filippo; Jentschel, Michael

    2013-05-15

    A quasi mosaic bent crystal for high-resolution diffraction of X and {gamma} rays has been realized. A net curvature was imprinted to the crystal thanks to a series of superficial grooves to keep the curvature without external devices. The crystal highlights very high diffraction efficiency due to quasi mosaic curvature. Quasi mosaic crystals of this kind are proposed for the realization of a high-resolution focusing Laue lens for hard X-rays.

  1. Hard x-ray tomographic studies of the destruction of an energetic electron ring

    SciTech Connect (OSTI)

    Wang, Y.; Gekelman, W.; Pribyl, P.

    2013-05-15

    A tomography system was designed and built at the Large Plasma Device to measure the spatial distribution of hard x-ray (100 KeV-3 MeV) emissivity. The x-rays were generated when a hot electron ring was significantly disrupted by a shear Alfven wave. The plasma is pulsed at 1 Hz (1 shot/s). A lead shielded scintillator detector with an acceptance angle defined by a lead pinhole is mounted on a rotary gimbal and used to detect the x-rays. The system measures one chord per plasma shot using only one detector. A data plane usually consists of several hundred chords. A novel Dot by Dot Reconstruction (DDR) method is introduced to calculate the emissivity profile from the line integrated data. In the experiments, there are often physical obstructions, which make measurements at certain angles impossible. The DDR method works well even in this situation. The method was tested with simulated data, and was found to be more effective than previously published methods for the specific geometry of this experiment. The reconstructed x-ray emissivity from experimental data by this method is shown.

  2. MASS AND ENERGY OF ERUPTING SOLAR PLASMA OBSERVED WITH THE X-RAY TELESCOPE ON HINODE

    SciTech Connect (OSTI)

    Lee, Jin-Yi; Moon, Yong-Jae; Kim, Kap-Sung; Raymond, John C.; Reeves, Katharine K.

    2015-01-10

    We investigate seven eruptive plasma observations by Hinode/XRT. Their corresponding EUV and/or white light coronal mass ejection features are visible in some events. Five events are observed in several passbands in X-rays, which allows for the determination of the eruptive plasma temperature using a filter ratio method. We find that the isothermal temperatures vary from 1.6 to 10 MK. These temperatures are an average weighted toward higher temperature plasma. We determine the mass constraints of eruptive plasmas by assuming simplified geometrical structures of the plasma with isothermal plasma temperatures. This method provides an upper limit to the masses of the observed eruptive plasmas in X-ray passbands since any clumping causes the overestimation of the mass. For the other two events, we assume the temperatures are at the maximum temperature of the X-ray Telescope (XRT) temperature response function, which gives a lower limit of the masses. We find that the masses in XRT, ∼3 × 10{sup 13}-5 × 10{sup 14} g, are smaller in their upper limit than the total masses obtained by LASCO, ∼1 × 10{sup 15} g. In addition, we estimate the radiative loss, thermal conduction, thermal, and kinetic energies of the eruptive plasma in X-rays. For four events, we find that the thermal conduction timescales are much shorter than the duration of eruption. This result implies that additional heating during the eruption may be required to explain the plasma observations in X-rays for the four events.

  3. Hard x-ray transmission crystal spectrometer at the OMEGA-EP laser facility

    SciTech Connect (OSTI)

    Seely, J. F.; Szabo, C. I.; Feldman, U.; Hudson, L. T.; Henins, A.; Audebert, P.; Brambrink, E.

    2010-10-15

    The transmission crystal spectrometer (TCS) is approved for taking data at the OMEGA-EP laser facility since 2009 and will be available for the OMEGA target chamber in 2010. TCS utilizes a Cauchois type cylindrically bent transmission crystal geometry with a source to crystal distance of 600 mm. Spectral images are recorded by image plates in four positions, one IP on the Rowland circle and three others at 200, 400, and 600 mm beyond the Rowland circle. An earlier version of TCS was used at LULI on experiments that determined the x-ray source size from spectral line broadening on one IP positioned behind the Rowland circle. TCS has recorded numerous backlighter spectra at EP for point projection radiography and for source size measurements. Hard x-ray source size can be determined from the source broadening of both K shell emission lines and from K absorption edges in the bremsstrahlung continuum, the latter being a new way to measure the spatial extent of the hard x-ray bremsstrahlung continuum.

  4. Claudio Pellegrini and the World’s First Hard X-ray Free-Electron Laser

    SciTech Connect (OSTI)

    Pellegrini, Claudio

    2015-10-20

    President Obama welcomed SLAC's Claudio Pellegrini inside the Oval Office on Tuesday morning as a recipient of the Enrico Fermi Award, one of the highest honors the U.S. government can give to a scientist. Pellegrini, a visiting scientist and consulting professor at SLAC and distinguished professor emeritus at the University of California, Los Angeles, received the award for research that aided in the development of X-ray free-electron lasers (XFELs) including SLAC's Linac Coherent Light Source (LCLS), a DOE Office of Science User Facility that started up in 2009. Here, Pellegrini describes his efforts that contributed to the realization of SLAC’s Linac Coherent Light Source, the world’s first hard X-ray free-electron laser.

  5. Hard x-ray photoelectron spectroscopy using an environmental cell with silicon nitride membrane windows

    SciTech Connect (OSTI)

    Tsunemi, Eika; Watanabe, Yoshio; Oji, Hiroshi; Cui, Yi-Tao; Son, Jin-Young

    2015-06-21

    We applied hard x-ray photoelectron spectroscopy (HAXPES) to a sample under ambient pressure conditions using an environmental cell with an approximately 24 nm-thick SiN{sub x} membrane window. As a model chemical substance, europium (II) iodide (EuI{sub 2}) sealed in the cell with argon gas was investigated with HAXPES to identify the chemical species present inside the cell. The optical and morphological properties of the sample within the cell were measured with optical and fluorescent microscopy, scanning electron microscopy, cathodoluminescence, and energy dispersive x-ray spectrometry. We confirmed the effectiveness of the gas barrier properties of the cell with the SiN{sub x} window and demonstrated its applicability to various other optical and electron measurements as well as HAXPES.

  6. SWIFT/BAT DETECTION OF HARD X-RAYS FROM TYCHO'S SUPERNOVA REMNANT: EVIDENCE FOR TITANIUM-44

    SciTech Connect (OSTI)

    Troja, E.; Baumgartner, W.; Markwardt, C.; Barthelmy, S.; Gehrels, N.; Segreto, A.; La Parola, V.; Cusumano, G.; Hartmann, D.

    2014-12-10

    We report Swift/Burst Alert Telescope survey observations of the Tycho's supernova remnant, performed over a period of 104 months since the mission's launch. The remnant is detected with high significance (>10σ) below 50 keV. We detect significant hard X-ray emission in the 60-85 keV band, above the continuum level predicted by a simple synchrotron model. The location of the observed excess is consistent with line emission from radioactive titanium-44, so far reported only for Type II supernova explosions. We discuss the implications of these results in the context of the galactic supernova rate, and nucleosynthesis in Type Ia supernova.

  7. Two-Bunch Self-Seeding for Narrow-Bandwidth Hard X-Ray Free-Electron...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Two-Bunch Self-Seeding for Narrow-Bandwidth Hard X-Ray Free-Electron Lasers Citation Details In-Document Search Title: Two-Bunch Self-Seeding for Narrow-Bandwidth...

  8. Two-Bunch Self-Seeding for Narrow-Bandwidth Hard X-Ray Free-Electron...

    Office of Scientific and Technical Information (OSTI)

    one of the most promising methods to accomplish this. In the hard x-ray regime with high- energy electrons, this method requires a large magnetic chicane to match the path length...

  9. Phase-matched generation of coherent soft and hard X-rays using IR lasers

    DOE Patents [OSTI]

    Popmintchev, Tenio V.; Chen, Ming-Chang; Bahabad, Alon; Murnane, Margaret M.; Kapteyn, Henry C.

    2013-06-11

    Phase-matched high-order harmonic generation of soft and hard X-rays is accomplished using infrared driving lasers in a high-pressure non-linear medium. The pressure of the non-linear medium is increased to multi-atmospheres and a mid-IR (or higher) laser device provides the driving pulse. Based on this scaling, also a general method for global optimization of the flux of phase-matched high-order harmonic generation at a desired wavelength is designed.

  10. Nonlinear delayed symmetry breaking in a solid excited by hard x-ray free electron laser pulses

    SciTech Connect (OSTI)

    Ferrer, A.; Johnson, J. A. Mariager, S. O.; Grbel, S.; Staub, U.; Huber, T.; Trant, M.; Johnson, S. L.; Zhu, D.; Chollet, M.; Robinson, J.; Lemke, H. T.; Ingold, G.; Beaud, P.; Milne, C.

    2015-04-13

    We have studied the ultrafast changes of electronic states in bulk ZnO upon intense hard x-ray excitation from a free electron laser. By monitoring the transient anisotropy induced in an optical probe beam, we observe a delayed breaking of the initial c-plane symmetry of the crystal that lasts for several picoseconds. Interaction with the intense x-ray pulses modifies the electronic state filling in a manner inconsistent with a simple increase in electronic temperature. These results may indicate a way to use intense ultrashort x-ray pulses to investigate high-energy carrier dynamics and to control certain properties of solid-state materials.

  11. The LCLS variable-energy hard X-ray single-shot spectrometer

    SciTech Connect (OSTI)

    Rich, David; Zhu, Diling; Turner, James; Zhang, Dehong; Hill, Bruce; Feng, Yiping

    2016-01-01

    The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for the continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10-5or better. Those performance goals have all been achieved during the commissioning of the HXSSS.

  12. The LCLS variable-energy hard X-ray single-shot spectrometer

    SciTech Connect (OSTI)

    Rich, David; Zhu, Diling; Turner, James; Zhang, Dehong; Hill, Bruce; Feng, Yiping

    2016-01-01

    The engineering design, implementation, operation and performance of the new variable-energy hard X-ray single-shot spectrometer (HXSSS) for the LCLS free-electron laser (FEL) are reported. The HXSSS system is based on a cylindrically bent Si thin crystal for dispersing the incident polychromatic FEL beam. A spatially resolved detector system consisting of a Ce:YAG X-ray scintillator screen, an optical imaging system and a low-noise pixelated optical camera is used to record the spectrograph. The HXSSS provides single-shot spectrum measurements for users whose experiments depend critically on the knowledge of the self-amplified spontaneous emission FEL spectrum. It also helps accelerator physicists for the continuing studies and optimization of self-seeding, various improved mechanisms for lasing mechanisms, and FEL performance improvements. The designed operating energy range of the HXSSS is from 4 to 20 keV, with the spectral range of order larger than 2% and a spectral resolution of 2 × 10-5or better. Those performance goals have all been achieved during the commissioning of the HXSSS.

  13. Scattered hard X-ray and γ-ray generation from a chromatic electron beam

    SciTech Connect (OSTI)

    Coleman, J. E.; Welch, D. R.; Miller, C. L.

    2015-11-14

    An array of photon diagnostics has been deployed on a high power relativistic electron beam diode. Electrons are extracted through a 17.8 cm diode from the surface discharge of a carbon fiber velvet cathode with a nominal diode voltage of 3.8 MV. <10% of the 100 ns electron pulse is composed of off energy electrons (1–3 MeV) accelerated during the rise and fall of the pulse that impact the stainless steel beam pipe and generate a Bremsstrahlung spectrum of 0.1–3 MeV photons with a total count of 10{sup 11}. The principal objective of these experiments is to quantify the electron beam dynamics and spatial dynamics of the hard X-ray and γ-ray flux generated in the diode region. A qualitative comparison of experimental and calculated results are presented, including time and energy resolved electron beam propagation and scattered photon measurements with X-ray PIN diodes and a photomultiplier tube indicating a dose dependence on the diode voltage >V{sup 4} and detected photon counts of nearly 10{sup 6} at a radial distance of 1 m which corresponds to dose ∼40 μrad at 1 m.

  14. Achieving Vibration Stability of the NSLS-II Hard X-ray Nanoprobe Beamline

    SciTech Connect (OSTI)

    Simos, N.; Chu, Y. N.; Broadbent, A.; Nazaretski, E.; Margulies, L.; Dyling, O.; Shen, Q.; Fallier, M.

    2010-08-30

    The Hard X-ray Nanoprobe (HXN) Beamline of National Synchrotron Light Source II (NSLS-lI) requires high levels of stability in order to achieve the desired instrument resolution. To ensure that the design of the endstation helps meet the stringent criteria and that natural and cultural vibration is mitigated both passively and actively, a comprehensive study complimentary to the design process has been undertaken. Vibration sources that have the potential to disrupt sensitive experiments such as wind, traffic and NSLS II operating systems have been studied using state of the art simulations and an array of field data. Further, final stage vibration isolation principles have been explored in order to be utilized in supporting endstation instruments. This paper presents results of the various study aspects and their influence on the HXN design optimization.

  15. Suzaku monitoring of hard X-ray emission from ? Carinae over a single binary orbital cycle

    SciTech Connect (OSTI)

    Hamaguchi, Kenji; Corcoran, Michael F.; Yuasa, Takayuki; Ishida, Manabu; Pittard, Julian M.; Russell, Christopher M. P.

    2014-11-10

    The Suzaku X-ray observatory monitored the supermassive binary system ? Carinae 10 times during the whole 5.5 yr orbital cycle between 2005 and 2011. This series of observations presents the first long-term monitoring of this enigmatic system in the extremely hard X-ray band between 15 and 40 keV. During most of the orbit, the 15-25 keV emission varied similarly to the 2-10 keV emission, indicating an origin in the hard energy tail of the kT ? 4 keV wind-wind collision (WWC) plasma. However, the 15-25 keV emission declined only by a factor of three around periastron when the 2-10 keV emission dropped by two orders of magnitude due probably to an eclipse of the WWC plasma. The observed minimum in the 15-25 keV emission occurred after the 2-10 keV flux had already recovered by a factor of ?3. This may mean that the WWC activity was strong, but hidden behind the thick primary stellar wind during the eclipse. The 25-40 keV flux was rather constant through the orbital cycle, at the level measured with INTEGRAL in 2004. This result may suggest a connection of this flux component to the ?-ray source detected in this field. The helium-like Fe K? line complex at ?6.7 keV became strongly distorted toward periastron as seen in the previous cycle. The 5-9 keV spectra can be reproduced well with a two-component spectral model, which includes plasma in collision equilibrium and a plasma in non-equilibrium ionization (NEI) with ? ? 10{sup 11} cm{sup 3} s{sup 1}. The NEI plasma increases in importance toward periastron.

  16. Photon-in photon-out hard X-ray spectroscopy at the Linac Coherent...

    Office of Scientific and Technical Information (OSTI)

    different source characteristics and its resulting impact on sample delivery, X-ray optics, X-ray detection and data acquisition. Here it is described how photon-in photon-out...

  17. MOTIONS OF HARD X-RAY SOURCES DURING AN ASYMMETRIC ERUPTION

    SciTech Connect (OSTI)

    Liu Chang; Jing Ju; Liu Rui; Deng Na; Wang Haimin; Lee, Jeongwoo

    2010-10-01

    Filament eruptions and hard X-ray (HXR) source motions are commonly observed in solar flares, which provide critical information on the coronal magnetic reconnection. This Letter reports an event on 2005 January 15, in which we found an asymmetric filament eruption and a subsequent coronal mass ejection together with complicated motions of HXR sources during the GOES-class X2.6 flare. The HXR sources initially converge to the magnetic polarity inversion line (PIL), and then move in directions either parallel or perpendicular to the PIL depending on the local field configuration. We distinguish the evolution of the HXR source motion in four phases and associate each of them with distinct regions of coronal magnetic fields as reconstructed using a nonlinear force-free field extrapolation. It is found that the magnetic reconnection proceeds along the PIL toward the regions where the overlying field decreases with height more rapidly. It is also found that not only the perpendicular but the parallel motion of the HXR sources correlates well with the HXR light curve. These results are discussed in favor of the torus instability as an important factor in the eruptive process.

  18. KAPPA DISTRIBUTION MODEL FOR HARD X-RAY CORONAL SOURCES OF SOLAR FLARES

    SciTech Connect (OSTI)

    Oka, M.; Ishikawa, S.; Saint-Hilaire, P.; Krucker, S.; Lin, R. P. [Space Sciences Laboratory, University of California Berkeley (United States)] [Space Sciences Laboratory, University of California Berkeley (United States)

    2013-02-10

    Solar flares produce hard X-ray emission, the photon spectrum of which is often represented by a combination of thermal and power-law distributions. However, the estimates of the number and total energy of non-thermal electrons are sensitive to the determination of the power-law cutoff energy. Here, we revisit an 'above-the-loop' coronal source observed by RHESSI on 2007 December 31 and show that a kappa distribution model can also be used to fit its spectrum. Because the kappa distribution has a Maxwellian-like core in addition to a high-energy power-law tail, the emission measure and temperature of the instantaneous electrons can be derived without assuming the cutoff energy. Moreover, the non-thermal fractions of electron number/energy densities can be uniquely estimated because they are functions of only the power-law index. With the kappa distribution model, we estimated that the total electron density of the coronal source region was {approx}2.4 Multiplication-Sign 10{sup 10} cm{sup -3}. We also estimated without assuming the source volume that a moderate fraction ({approx}20%) of electrons in the source region was non-thermal and carried {approx}52% of the total electron energy. The temperature was 28 MK, and the power-law index {delta} of the electron density distribution was -4.3. These results are compared to the conventional power-law models with and without a thermal core component.

  19. Distributed seeding for narrow-line width hard x-ray free-electron lasers

    SciTech Connect (OSTI)

    Nguyen, Dinh Cong; Anisimov, Petr Mikhaylovich; Buechler, Cynthia Eileen; Lewellen, IV, John W.; Marksteiner, Quinn R.

    2015-09-09

    We describe a new FEL line-narrowing technique called distributed seeding (DS), using Si(111) Bragg crystal monochromators to enhance the spectral brightness of the MaRIE hard X-ray freeelectron laser. DS differs from self-seeding in three important aspects. First, DS relies on spectral filtering of the radiation at multiple locations along the undulator, with a monochromator located every few power gain lengths. Second, DS performs filtering early in the exponential gain region before SASE spikes start to appear in the radiation longitudinal profile. Third, DS provides the option to select a wavelength longer than the peak of the SASE gain curve, which leads to improved spectral contrast of the seeded FEL over the SASE background. Timedependent Genesis simulations show the power-vs-z growth curves for DS exhibit behaviors of a seeded FEL amplifier, such as exponential growth region immediately after the filters. Of the seeding approaches considered, the two-stage DS spectra produce the highest contrast of seeded FEL over the SASE background and that the three-stage DS provides the narrowest linewidth with a relative spectral FWHM of 8 X 10-5 .

  20. Hard X-ray emission and {sup 44}Ti line features of the Tycho supernova remnant

    SciTech Connect (OSTI)

    Wang, Wei [National Astronomical Observatories, Chinese Academy of Sciences, 20A Datun Road, Chaoyang District, Beijing 100012 (China); Li, Zhuo, E-mail: wangwei@bao.ac.cn, E-mail: zhuo.li@pku.edu.cn [Department of Astronomy and Kavli Institute for Astronomy and Astrophysics, Peking University, Beijing 100871 (China)

    2014-07-10

    A deep hard X-ray survey of the International Gamma-Ray Astrophysics Laboratory (INTEGRAL) satellite has detected for the first time non-thermal emission up to 90 keV in the Tycho supernova (SN) remnant. Its 3-100 keV spectrum is fitted with a thermal bremsstrahlung of kT ? 0.81 0.45 keV plus a power-law model of ? ? 3.01 0.16. Based on diffusive shock acceleration theory, this non-thermal emission, together with radio measurements, implies that the Tycho remnant may not accelerate protons up to >PeV but to hundreds TeV. Only heavier nuclei may be accelerated to the cosmic ray spectral 'knee'. In addition, using INTEGRAL, we search for soft gamma-ray lines at 67.9 and 78.4 keV that come from the decay of radioactive {sup 44}Ti in the Tycho remnant. A bump feature in the 60-90 keV energy band, potentially associated with the {sup 44}Ti line emission, is found with a marginal significance level of ?2.6?. The corresponding 3? upper limit on the {sup 44}Ti line flux amounts to 1.5 10{sup 5} photon cm{sup 2} s{sup 1}. Implications on the progenitor of the Tycho SN, considered to be a Type Ia SN prototype, are discussed.

  1. Photon-in photon-out hard X-ray spectroscopy at the Linac Coherent Light Source

    SciTech Connect (OSTI)

    Alonso-Mori, Roberto; Sokaras, Dimosthenis; Zhu, Diling; Kroll, Thomas; Chollet, Mathieu; Feng, Yiping; Glownia, James M.; Kern, Jan; Lemke, Henrik T.; Nordlund, Dennis; Robert, Aymeric; Sikorski, Marcin; Song, Sanghoon; Weng, Tsu -Chien; Bergmann, Uwe

    2015-04-15

    X-ray free-electron lasers (FELs) have opened unprecedented possibilities to study the structure and dynamics of matter at an atomic level and ultra-fast timescale. Many of the techniques routinely used at storage ring facilities are being adapted for experiments conducted at FELs. In order to take full advantage of these new sources several challenges have to be overcome. They are related to the very different source characteristics and its resulting impact on sample delivery, X-ray optics, X-ray detection and data acquisition. Here it is described how photon-in photon-out hard X-ray spectroscopy techniques can be applied to study the electronic structure and its dynamics of transition metal systems with ultra-bright and ultra-short FEL X-ray pulses. In particular, some of the experimental details that are different compared with synchrotron-based setups are discussed and illustrated by recent measurements performed at the Linac Coherent Light Source.

  2. Photon-in photon-out hard X-ray spectroscopy at the Linac Coherent Light Source

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Alonso-Mori, Roberto; Sokaras, Dimosthenis; Zhu, Diling; Kroll, Thomas; Chollet, Mathieu; Feng, Yiping; Glownia, James M.; Kern, Jan; Lemke, Henrik T.; Nordlund, Dennis; et al

    2015-04-15

    X-ray free-electron lasers (FELs) have opened unprecedented possibilities to study the structure and dynamics of matter at an atomic level and ultra-fast timescale. Many of the techniques routinely used at storage ring facilities are being adapted for experiments conducted at FELs. In order to take full advantage of these new sources several challenges have to be overcome. They are related to the very different source characteristics and its resulting impact on sample delivery, X-ray optics, X-ray detection and data acquisition. Here it is described how photon-in photon-out hard X-ray spectroscopy techniques can be applied to study the electronic structure andmore » its dynamics of transition metal systems with ultra-bright and ultra-short FEL X-ray pulses. In particular, some of the experimental details that are different compared with synchrotron-based setups are discussed and illustrated by recent measurements performed at the Linac Coherent Light Source.« less

  3. CORONAL THICK TARGET HARD X-RAY EMISSIONS AND RADIO EMISSIONS

    SciTech Connect (OSTI)

    Lee, Jeongwoo; Lim, Daye; Choe, G. S.; Kim, Kap-Sung; Jang, Minhwan

    2013-05-20

    A distinctive class of hard X-ray (HXR) sources located in the corona was recently found, which implies that the collisionally thick target model (CTTM) applies even to the corona. We investigated whether this idea can be independently verified by microwave radiations which have been known as the best companion to HXRs. This study is conducted on the GOES M2.3 class flare which occurred on 2002 September 9 and was observed by the Reuven Ramaty High-Energy Solar Spectroscopic Imager and the Owens Valley Solar Array. Interpreting the observed energy-dependent variation of HXR source size under the CTTM, the coronal density should be as high as 5 Multiplication-Sign 10{sup 11} cm{sup -3} over a distance of up to 12''. To explain the cutoff feature of the microwave spectrum at 3 GHz, however, we require a density no higher than 1 Multiplication-Sign 10{sup 11} cm{sup -3}. Additional constraints must be placed on the temperature and magnetic field of the coronal source in order to reproduce the microwave spectrum as a whole. First, a spectral feature called the Razin suppression requires a magnetic field in a range of 250-350 G along with high viewing angles around 75 Degree-Sign . Second, to avoid excess fluxes at high frequencies due to the free-free emission that was not observed, we need a high temperature {>=}2 Multiplication-Sign 10{sup 7} K. These two microwave spectral features, Razin suppression and free-free emissions, become more significant at regions of high thermal plasma density and are essential for validating and determining additional parameters of the coronal HXR sources.

  4. ELECTRON ENERGY PARTITION IN THE ABOVE-THE-LOOPTOP SOLAR HARD X-RAY SOURCES

    SciTech Connect (OSTI)

    Oka, Mitsuo; Krucker, Säm; Hudson, Hugh S.; Saint-Hilaire, Pascal

    2015-02-01

    Solar flares produce non-thermal electrons with energies up to tens of MeVs. To understand the origin of energetic electrons, coronal hard X-ray (HXR) sources, in particular above-the-looptop sources, have been studied extensively. However, it still remains unclear how energies are partitioned between thermal and non-thermal electrons within the above-the-looptop source. Here we show that the kappa distribution, when compared to conventional spectral models, can better characterize the above-the-looptop HXRs (≳15 keV) observed in four different cases. The widely used conventional model (i.e., the combined thermal plus power-law distribution) can also fit the data, but it returns unreasonable parameter values due to a non-physical sharp lower-energy cutoff E{sub c}. In two cases, extreme-ultraviolet data were available from SDO/AIA and the kappa distribution was still consistent with the analysis of differential emission measure. Based on the kappa distribution model, we found that the 2012 July 19 flare showed the largest non-thermal fraction of electron energies about 50%, suggesting equipartition of energies. Considering the results of particle-in-cell simulations, as well as density estimates of the four cases studied, we propose a scenario in which electron acceleration is achieved primarily by collisionless magnetic reconnection, but the electron energy partition in the above-the-looptop source depends on the source density. In low-density above-the-looptop regions (few times 10{sup 9} cm{sup –3}), the enhanced non-thermal tail can remain and a prominent HXR source is created, whereas in higher-densities (>10{sup 10} cm{sup –3}), the non-thermal tail is suppressed or thermalized by Coulomb collisions.

  5. SSRL School 2008 on Hard X-ray Scattering Techniques in MES

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    May 20-22, 2008 SSRL School on Synchrotron X-ray Absorption Spectroscopy Techniques in Environmental and Materials Sciences: Theory and Application Group photo from the 2008 SSRL...

  6. High-resolution single-shot spectral monitoring of hard x-ray free-electron laser radiation

    SciTech Connect (OSTI)

    Makita, M.; Karvinen, P.; Zhu, D.; Juranic, P. N.; Grünert, J.; Cartier, S.; Jungmann-Smith, J. H.; Lemke, H. T.; Mozzanica, A.; Nelson, S.; Patthey, L.; Sikorski, M.; Song, S.; Feng, Y.; David, C.

    2015-10-16

    We have developed an on-line spectrometer for hard x-ray free-electron laser (XFEL) radiation based on a nanostructured diamond diffraction grating and a bent crystal analyzer. Our method provides high spectral resolution, interferes negligibly with the XFEL beam, and can withstand the intense hard x-ray pulses at high repetition rates of >100 Hz. The spectrometer is capable of providing shot-to-shot spectral information for the normalization of data obtained in scientific experiments and optimization of the accelerator operation parameters. We have demonstrated these capabilities of the setup at the Linac Coherent Light Source, in self-amplified spontaneous emission mode at full energy of >1 mJ with a 120 Hz repetition rate, obtaining a resolving power of Ε/δΕ > 3 × 104. In conclusion, the device was also used to monitor the effects of pulse duration down to 8 fs by analysis of the spectral spike width.

  7. A seven-crystal Johann-type hard x-ray spectrometer at the Stanford Synchrotron Radiation Lightsource

    SciTech Connect (OSTI)

    Sokaras, D.; Weng, T.-C.; Nordlund, D.; Velikov, P.; Wenger, D.; Garachtchenko, A.; George, M.; Borzenets, V.; Johnson, B.; Rabedeau, T.; Alonso-Mori, R.; Bergmann, U.

    2013-05-15

    We present a multicrystal Johann-type hard x-ray spectrometer ({approx}5-18 keV) recently developed, installed, and operated at the Stanford Synchrotron Radiation Lightsource. The instrument is set at the wiggler beamline 6-2 equipped with two liquid nitrogen cooled monochromators - Si(111) and Si(311) - as well as collimating and focusing optics. The spectrometer consists of seven spherically bent crystal analyzers placed on intersecting vertical Rowland circles of 1 m of diameter. The spectrometer is scanned vertically capturing an extended backscattering Bragg angular range (88 Degree-Sign -74 Degree-Sign ) while maintaining all crystals on the Rowland circle trace. The instrument operates in atmospheric pressure by means of a helium bag and when all the seven crystals are used (100 mm of projected diameter each), has a solid angle of about 0.45% of 4{pi} sr. The typical resolving power is in the order of (E/{Delta}E){approx}10 000. The spectrometer's high detection efficiency combined with the beamline 6-2 characteristics permits routine studies of x-ray emission, high energy resolution fluorescence detected x-ray absorption and resonant inelastic x-ray scattering of very diluted samples as well as implementation of demanding in situ environments.

  8. Long-Working-Distance Kirkpatrick-Baez Mirrors for Hard X-ray Beamlines at SPring-8

    SciTech Connect (OSTI)

    Yumoto, H.; Koyama, T.

    2011-09-09

    We designed and installed two types of long-working-distance Kirkpatrick-Baez (KB) mirrors and mirror manipulators, which were customized into each experiment for hard x-ray undulator beamlines at SPring-8. For the BL32XU RIKEN Targeted Proteins beamline, 400-mm-long KB focusing mirrors for a beam size of 1 {mu}m with a 730-mm-long working distance were designed for carrying out the structural analysis of protein microcrystals. We realized a focusing beam size of 0.9x0.9 {mu}m{sup 2}(FWHM) and a focusing intensity of 6x10{sup 10} (photons/s) at an x-ray energy of 12.4 keV. For the BL19LXU RIKEN SR Physics beamline, we developed KB mirrors for 100-nm focusing with a 100-mm-working distance for the purpose of nano-focus x-ray diffraction. A focusing beam size of 100x100 nm{sup 2}(FWHM) and a high focusing intensity of 3.7x10{sup 10} (photons/s) at an x-ray energy of 12.4 keV were realized.

  9. Hard x-ray nanofocusing by refractive lenses of constant thickness

    SciTech Connect (OSTI)

    Seiboth, F. Scholz, M.; Patommel, J.; Hoppe, R.; Wittwer, F.; Reinhardt, J.; Seidel, J.; Knaut, M.; Jahn, A.; Richter, K.; Bartha, J. W.; Falkenberg, G.; Schroer, C. G.

    2014-09-29

    In order to focus light or x rays, the thickness of a refractive lens is typically varied over its aperture. Here, we present a refractive x-ray lens made of lamellae of constant thickness, the refractive lamellar lens. Refractive power is created by a specific bending of the lamellae rather than by a concave lens profile. This very special design has the technological advantage that materials like sapphire or diamond can be used to make lenses by coating techniques. A first lens prototype focused x rays with a photon energy E = 15.25 keV to a lateral beam size of 164 nm × 296 nm full width at half maximum.

  10. Fresnel zone plate stacking in the intermediate field for high efficiency focusing in the hard X-ray regime

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Gleber, Sophie -Charlotte; Wojcik, Michael; Liu, Jie; Roehrig, Chris; Cummings, Marvin; Vila-Comamala, Joan; Li, Kenan; Lai, Barry; Shu, Deming; Vogt, Stefan

    2014-11-05

    Focusing efficiency of Fresnel zone plates (FZPs) for X-rays depends on zone height, while the achievable spatial resolution depends on the width of the finest zones. FZPs with optimal efficiency and sub-100-nm spatial resolution require high aspect ratio structures which are difficult to fabricate with current technology especially for the hard X-ray regime. A possible solution is to stack several zone plates. To increase the number of FZPs within one stack, we first demonstrate intermediate-field stacking and apply this method by stacks of up to five FZPs with adjusted diameters. Approaching the respective optimum zone height, we maximized efficiencies formorehigh resolution focusing at three different energies, 10, 11.8, and 25 keV.less

  11. Microjet formation and hard x-ray production from a liquid metal target irradiated by intense femtosecond laser pulses

    SciTech Connect (OSTI)

    Lar'kin, A. Uryupina, D.; Ivanov, K.; Savel'ev, A.; Bonnet, T.; Gobet, F.; Hannachi, F.; Tarisien, M.; Versteegen, M.; Spohr, K.; Breil, J.; Chimier, B.; Dorchies, F.; Fourment, C.; Leguay, P.-M.; Tikhonchuk, V. T.

    2014-09-15

    By using a liquid metal as a target one may significantly enhance the yield of hard x-rays with a sequence of two intense femtosecond laser pulses. The influence of the time delay between the two pulses is studied experimentally and interpreted with numerical simulations. It was suggested that the first arbitrary weak pulse produces microjets from the target surface, while the second intense pulse provides an efficient electron heating and acceleration along the jet surface. These energetic electrons are the source of x-ray emission while striking the target surface. The microjet formation is explained based on the results given by both optical diagnostics and hydrodynamic modeling by a collision of shocks originated from two distinct zones of laser energy deposition.

  12. Hard X-ray nanofocusing using adaptive focusing optics based on piezoelectric deformable mirrors

    SciTech Connect (OSTI)

    Goto, Takumi; Nakamori, Hiroki; Sano, Yasuhisa; Matsuyama, Satoshi; Kimura, Takashi; Kohmura, Yoshiki; Tamasaku, Kenji; Yabashi, Makina; Ishikawa, Tetsuya

    2015-04-15

    An adaptive Kirkpatrick–Baez mirror focusing optics based on piezoelectric deformable mirrors was constructed at SPring-8 and its focusing performance characteristics were demonstrated. By adjusting the voltages applied to the deformable mirrors, the shape errors (compared to a target elliptical shape) were finely corrected on the basis of the mirror shape determined using the pencil-beam method, which is a type of at-wavelength figure metrology in the X-ray region. The mirror shapes were controlled with a peak-to-valley height accuracy of 2.5 nm. A focused beam with an intensity profile having a full width at half maximum of 110 × 65 nm (V × H) was achieved at an X-ray energy of 10 keV.

  13. Inverse Compton Origin of the Hard X-ray and Soft gamma-ray Emission from the Galactic Ridge

    SciTech Connect (OSTI)

    Porter, Troy A.; Moskalenko, Igor V.; Strong, Andrew W.; Orlando, Elena; Bouchet, Laurent

    2008-09-30

    A recent re-determination of the non-thermal component of the hard X-ray to soft {gamma}-ray emission from the Galactic ridge, using the SPI instrument on the INTErnational Gamma-Ray Astrophysics Laboratory (INTEGRAL) Observatory, is shown to be well reproduced as inverse-Compton emission from the interstellar medium. Both cosmic-ray primary electrons and secondary electrons and positrons contribute to the emission. The prediction uses the GALPROP model and includes a new calculation of the interstellar radiation field. This may solve a long-standing mystery of the origin of this emission, and potentially opens a new window on Galactic cosmic rays.

  14. High-resolution single-shot spectral monitoring of hard x-ray free-electron laser radiation

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Makita, M.; Karvinen, P.; Zhu, D.; Juranic, P. N.; Grünert, J.; Cartier, S.; Jungmann-Smith, J. H.; Lemke, H. T.; Mozzanica, A.; Nelson, S.; et al

    2015-10-16

    We have developed an on-line spectrometer for hard x-ray free-electron laser (XFEL) radiation based on a nanostructured diamond diffraction grating and a bent crystal analyzer. Our method provides high spectral resolution, interferes negligibly with the XFEL beam, and can withstand the intense hard x-ray pulses at high repetition rates of >100 Hz. The spectrometer is capable of providing shot-to-shot spectral information for the normalization of data obtained in scientific experiments and optimization of the accelerator operation parameters. We have demonstrated these capabilities of the setup at the Linac Coherent Light Source, in self-amplified spontaneous emission mode at full energy ofmore » >1 mJ with a 120 Hz repetition rate, obtaining a resolving power of Ε/δΕ > 3 × 104. In conclusion, the device was also used to monitor the effects of pulse duration down to 8 fs by analysis of the spectral spike width.« less

  15. HARD X-RAY LAGS IN ACTIVE GALACTIC NUCLEI: TESTING THE DISTANT REVERBERATION HYPOTHESIS WITH NGC 6814

    SciTech Connect (OSTI)

    Walton, D. J.; Harrison, F. A.; Zoghbi, A.; Reynolds, C. S.; Cackett, E. M.; Uttley, P.; Fabian, A. C.; Kara, E.; Miller, J. M.; Reis, R. C.

    2013-11-10

    We present an X-ray spectral and temporal analysis of the variable active galaxy NGC 6814, observed with Suzaku during 2011 November. Remarkably, the X-ray spectrum shows no evidence for the soft excess commonly observed amongst other active galaxies, despite its relatively low level of obscuration, and is dominated across the whole Suzaku bandpass by the intrinsic powerlaw-like continuum. Despite this, we clearly detect the presence of a low-frequency hard lag of ∼1600 s between the 0.5-2.0 and 2.0-5.0 keV energy bands at greater than 6σ significance, similar to those reported in the literature for a variety of other active galactic nuclei (AGNs). At these energies, any additional emission from, e.g., a very weak, undetected soft excess, or from distant reflection must contribute less than 3% of the observed countrates (at 90% confidence). Given the lack of any significant continuum emission component other than the powerlaw, we can rule out models that invoke distant reprocessing for the observed lag behavior, which must instead be associated with this continuum emission. These results are fully consistent with a propagating fluctuation origin for the low-frequency hard lags, and with the interpretation of the high-frequency soft lags—a common feature seen in the highest quality AGN data with strong soft excesses—as reverberation from the inner accretion disk.

  16. Analysis and Interpretation of Hard X-ray Emission fromthe Bullet...

    Office of Scientific and Technical Information (OSTI)

    Sponsoring Org: USDOE Country of Publication: United States Language: English Subject: 43 PARTICLE ACCELERATORS; DETECTION; ELECTRONS; GALAXIES; KEV RANGE; SYNCHROTRONS; HARD X ...

  17. Ultra-stable sub-meV monochromator for hard X-rays

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Toellner, T. S.; Collins, J.; Goetze, K.; Hu, M. Y.; Preissner, C.; Trakhtenberg, E.; Yan, L.

    2015-07-17

    A high-resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in 151Eu. The first-of-its-kind, fully cryogenic design achieves an energy-alignment stability of 0.017 meV r.m.s. per day, or a 100-fold improvement over other meV-monochromators, and can tolerate higher X-ray power loads than room-temperature designs of comparable resolution. This offers the potential for significantly more accurate measurements of lattice excitation energies using nuclear resonant vibrational spectroscopy if combined with accurate energy calibration using, for example, high-speed Doppler shifting. The design of the monochromator alongmore » with its performance and impact on transmitted beam properties are presented.« less

  18. Ultra-stable sub-meV monochromator for hard X-rays

    SciTech Connect (OSTI)

    Toellner, T. S.; Collins, J.; Goetze, K.; Hu, M. Y.; Preissner, C.; Trakhtenberg, E.; Yan, L.

    2015-07-17

    A high-resolution silicon monochromator suitable for 21.541 keV synchrotron radiation is presented that produces a bandwidth of 0.27 meV. The operating energy corresponds to a nuclear transition in 151Eu. The first-of-its-kind, fully cryogenic design achieves an energy-alignment stability of 0.017 meV r.m.s. per day, or a 100-fold improvement over other meV-monochromators, and can tolerate higher X-ray power loads than room-temperature designs of comparable resolution. This offers the potential for significantly more accurate measurements of lattice excitation energies using nuclear resonant vibrational spectroscopy if combined with accurate energy calibration using, for example, high-speed Doppler shifting. The design of the monochromator along with its performance and impact on transmitted beam properties are presented.

  19. Hard x-ray contact microscopy with 250 nm spatial resolution using a LiF film detector and a tabletop microsource

    SciTech Connect (OSTI)

    Almaviva, S.; Bonfigli, F.; Franzini, I.; Lai, A.; Montereali, R. M.; Pelliccia, D.; Cedola, A.; Lagomarsino, S.

    2006-07-31

    An innovative route for deep-submicrometer spatial resolution hard x-ray microscopy with tabletop x-ray source is proposed. A film of lithium fluoride (LiF) was used as imaging detector in contact mode. We present here the x-ray images recorded on LiF films of a Fresnel zone plate with submicrometer gold structures and of an onion cataphyll. The images were read with an optical confocal microscope in fluorescence mode. The measured spatial resolution was about 250 nm, i.e., close to the resolution limit of the confocal microscope. The advantages and drawbacks, and the possible improvements, of this route are discussed.

  20. Experimental comparison of grating- and propagation-based hard X-ray phase tomography of soft tissue

    SciTech Connect (OSTI)

    Lang, S.; Schulz, G.; Müller, B.; Zanette, I.; Dominietto, M.; Langer, M.; Rack, A.; Le Duc, G.; David, C.; Mohr, J.; Pfeiffer, F.; Weitkamp, T.

    2014-10-21

    When imaging soft tissues with hard X-rays, phase contrast is often preferred over conventional attenuation contrast due its superior sensitivity. However, it is unclear which of the numerous phase tomography methods yields the optimized results at given experimental conditions. Therefore, we quantitatively compared the three phase tomography methods implemented at the beamline ID19 of the European Synchrotron Radiation Facility: X-ray grating interferometry (XGI), and propagation-based phase tomography, i.e., single-distance phase retrieval (SDPR) and holotomography (HT), using cancerous tissue from a mouse model and an entire heart of a rat. We show that for both specimens, the spatial resolution derived from the characteristic morphological features is about a factor of two better for HT and SDPR compared to XGI, whereas the XGI data generally exhibit much better contrast-to-noise ratios for the anatomical features. Moreover, XGI excels in fidelity of the density measurements, and is also more robust against low-frequency artifacts than HT, but it might suffer from phase-wrapping artifacts. Thus, we can regard the three phase tomography methods discussed as complementary. The application will decide which spatial and density resolutions are desired, for the imaging task and dose requirements, and, in addition, the applicant must choose between the complexity of the experimental setup and the one of data processing.

  1. EXTENDED HARD X-RAY EMISSION FROM THE VELA PULSAR WIND NEBULA

    SciTech Connect (OSTI)

    Mattana, F.; Terrier, R.; Zurita Heras, J. A.; Goetz, D.; Caballero, I.; Soldi, S.; Schanne, S.; Ponti, G.; Falanga, M.; Renaud, M.

    2011-12-10

    The nebula powered by the Vela pulsar is one of the best examples of an evolved pulsar wind nebula, allowing access to the particle injection history and the interaction with the supernova ejecta. We report on the INTEGRAL discovery of extended emission above 18 keV from the Vela nebula. The northern side has no known counterparts and it appears larger and more significant than the southern one, which is in turn partially coincident with the cocoon, the soft X-ray, and TeV filament toward the center of the remnant. We also present the spectrum of the Vela nebula in the 18-400 keV energy range as measured by IBIS/ISGRI and SPI on board the INTEGRAL satellite. The apparent discrepancy between IBIS/ISGRI, SPI, and previous measurements is understood in terms of the point-spread function, supporting the hypothesis of a nebula more diffuse than previously thought. A break at {approx}25 keV is found in the spectrum within 6' from the pulsar after including the Suzaku XIS data. Interpreted as a cooling break, this points out that the inner nebula is composed of electrons injected in the last {approx}2000 years. Broadband modeling also implies a magnetic field higher than 10 {mu}G in this region. Finally, we discuss the nature of the northern emission, which might be due to fresh particles injected after the passage of the reverse shock.

  2. Electronic structure of Al- and Ga-doped ZnO films studied by hard X-ray photoelectron spectroscopy

    SciTech Connect (OSTI)

    Gabás, M.; Ramos Barrado, José R.; Torelli, P.; Barrett, N. T.

    2014-01-01

    Al- and Ga-doped sputtered ZnO films (AZO, GZO) are semiconducting and metallic, respectively, despite the same electronic valence structure of the dopants. Using hard X-ray photoelectron spectroscopy we observe that both dopants induce a band in the electronic structure near the Fermi level, accompanied by a narrowing of the Zn 3d/O 2p gap in the valence band and, in the case of GZO, a substantial shift in the Zn 3d. Ga occupies substitutional sites, whereas Al dopants are in both substitutional and interstitial sites. The latter could induce O and Zn defects, which act as acceptors explaining the semiconducting character of AZO and the lack of variation in the optical gap. By contrast, mainly substitutional doping is consistent with the metallic-like behavior of GZO.

  3. Annealing dependence of diamond-metal Schottky barrier heights probed by hard x-ray photoelectron spectroscopy

    SciTech Connect (OSTI)

    Gaowei, M.; Muller, E. M.; Rumaiz, A. K.; Weiland, C.; Cockayne, E.; Woicik, J. C.; Jordan-Sweet, J.; Smedley, J.

    2012-05-14

    Hard x-ray photoelectron spectroscopy was applied to investigate the diamond-metal Schottky barrier heights for several metals and diamond surface terminations. The position of the diamond valence-band maximum was determined by theoretically calculating the diamond density of states and applying cross section corrections. The diamond-platinum Schottky barrier height was lowered by 0.2 eV after thermal annealing, indicating annealing may increase carrier injection in diamond devices leading to photoconductive gain. The platinum contacts on oxygen-terminated diamond was found to provide a higher Schottky barrier and therefore a better blocking contact than that of the silver contact in diamond-based electronic devices.

  4. Visualization of electrochemically driven solid-state phase transformations using operando hard X-ray spectro-imaging

    SciTech Connect (OSTI)

    Li, Linsen; Chen-Wiegart, Yu-chen Karen; Wang, Jiajun; Gao, Peng; Ding, Qi; Yu, Young-Sang; Wang, Feng; Cabana, Jordi; Wang, Jun; Jin, Song

    2015-04-20

    In situ techniques with high temporal, spatial and chemical resolution are key to understand ubiquitous solid-state phase transformations, which are crucial to many technological applications. Hard X-ray spectro-imaging can visualize electrochemically driven phase transformations but demands considerably large samples with strong absorption signal so far. Here we show a conceptually new data analysis method to enable operando visualization of mechanistically relevant weakly absorbing samples at the nanoscale and study electrochemical reaction dynamics of iron fluoride, a promising high-capacity conversion cathode material. In two specially designed samples with distinctive microstructure and porosity, we observe homogeneous phase transformations during both discharge and charge, faster and more complete Li-storage occurring in porous polycrystalline iron fluoride, and further, incomplete charge reaction following a pathway different from conventional belief. In conclusion, these mechanistic insights provide guidelines for designing better conversion cathode materials to realize the promise of high-capacity lithium-ion batteries.

  5. Turbulent pitch-angle scattering and diffusive transport of hard X-ray-producing electrons in flaring coronal loops

    SciTech Connect (OSTI)

    Kontar, Eduard P.; Bian, Nicolas H.; Emslie, A. Gordon; Vilmer, Nicole E-mail: emslieg@wku.edu

    2014-01-10

    Recent observations from RHESSI have revealed that the number of non-thermal electrons in the coronal part of a flaring loop can exceed the number of electrons required to explain the hard X-ray-emitting footpoints of the same flaring loop. Such sources cannot, therefore, be interpreted on the basis of the standard collisional transport model, in which electrons stream along the loop while losing their energy through collisions with the ambient plasma; additional physical processes, to either trap or scatter the energetic electrons, are required. Motivated by this and other observations that suggest that high-energy electrons are confined to the coronal region of the source, we consider turbulent pitch-angle scattering of fast electrons off low-frequency magnetic fluctuations as a confinement mechanism, modeled as a spatial diffusion parallel to the mean magnetic field. In general, turbulent scattering leads to a reduction of the collisional stopping distance of non-thermal electrons along the loop, and hence to an enhancement of the coronal hard X-ray source relative to the footpoints. The variation of source size L with electron energy E becomes weaker than the quadratic behavior pertinent to collisional transport, with the slope of L(E) depending directly on the mean free path ? associated with the non-collisional scattering mechanism. Comparing the predictions of the model with observations, we find that ? ? (10{sup 8}-10{sup 9}) cm for ?30 keV, less than the length of a typical flaring loop and smaller than, or comparable to, the size of the electron acceleration region.

  6. A Low-Charge, Hard X-Ray FEL Driven with an X-band Injector and Accelerator

    SciTech Connect (OSTI)

    Sun, Yipeng; Adolphsen, Chris; Limborg-Deprey, Cecile; Raubenheimer, Tor; Wu, Juhao; /SLAC

    2012-02-17

    After the successful operation of FLASH (Free-Electron Laser in Hamburg) and LCLS (Linac Coherent Light Source), soft and hard X-ray Free Electron Lasers (FELs) are being built, designed or proposed at many accelerator laboratories. Acceleration employing lower frequency RF cavities, ranging from L-band to C-band, is usually adopted in these designs. In the first stage bunch compression, higher-frequency harmonic RF system is employed to linearize the beam's longitudinal phase space, which is nonlinearly chirped during the lower frequency RF acceleration process. In this paper, a hard X-ray FEL design using an all X-band accelerator at 11.424 GHz (from photo-cathode RF gun to linac end) is presented, without the assistance of any harmonic RF linearization. It achieves LCLS-like performance at low charge using X-band linac drivers, which is more versatile, efficient and compact than ones using S-band or C-band rf technology. It employs initially 42 microns long (RMS), low charge (10 pC) electron bunches from an X-band photoinjector. An overall bunch compression ratio of roughly 100 times is proposed in a two stage bunch compressor system. The start-to-end macro-particle 3-D simulation employing several computer codes is presented in this paper, where space charge, wakefields, incoherent and coherent synchrotron radiation (ISR and CSR) effects are included. Employing an undulator with a short period of 1.5 cm, a Genesis FEL simulation shows successful lasing at a wavelength of 0.15 nm with a pulse length of 2 fs and a power saturation length as short as 20 meters, which is equivalent to LCLS low charge mode. Its overall length of both accelerators and undulators is 180 meters (much shorter than the effective LCLS overall length of 1230 meters, including an accelerator length of 1100 meters and an undulator length of 130 meters), which makes it possible to be built in places where only limited space is available.

  7. SPATIALLY RESOLVING A STARBURST GALAXY AT HARD X-RAY ENERGIES: NuSTAR, CHANDRA, AND VLBA OBSERVATIONS OF NGC253

    SciTech Connect (OSTI)

    Wik, D. R.; Lehmer, B. D.; Hornschemeier, A. E.; Yukita, M.; Ptak, A.; Venters, T.; Zhang, W. W.; Zezas, A.; Antoniou, V.; Argo, M. K.; Bechtol, K.; Boggs, S.; Craig, W.; Krivonos, R.; Christensen, F.; Hailey, C.; Harrison, F.; Maccarone, T. J.; Stern, D.

    2014-12-20

    Prior to the launch of NuSTAR, it was not feasible to spatially resolve the hard (E > 10 keV) emission from galaxies beyond the Local Group. The combined NuSTAR data set, comprised of three ?165 ks observations, allows spatial characterization of the hard X-ray emission in the galaxy NGC253 for the first time. As a follow up to our initial study of its nuclear region, we present the first results concerning the full galaxy from simultaneous NuSTAR, Chandra, and Very Long Baseline Array monitoring of the local starburst galaxy NGC253. Above ?10 keV, nearly all the emission is concentrated within 100'' of the galactic center, produced almost exclusively by three nuclear sources, an off-nuclear ultraluminous X-ray source (ULX), and a pulsar candidate that we identify for the first time in these observations. We detect 21 distinct sources in energy bands up to 25 keV, mostly consisting of intermediate state black hole X-ray binaries. The global X-ray emission of the galaxydominated by the off-nuclear ULX and nuclear sources, which are also likely ULXsfalls steeply (photon index ? 3) above 10 keV, consistent with other NuSTAR-observed ULXs, and no significant excess above the background is detected at E > 40 keV. We report upper limits on diffuse inverse Compton emission for a range of spatial models. For the most extended morphologies considered, these hard X-ray constraints disfavor a dominant inverse Compton component to explain the ?-ray emission detected with Fermi and H.E.S.S. If NGC253 is typical of starburst galaxies at higher redshift, their contribution to the E > 10 keV cosmic X-ray background is <1%.

  8. A hard X-ray study of a manganese-terpyridine catalyst in a chromium-based Metal Organic Framework

    SciTech Connect (OSTI)

    Ramsey, Alexandra V.

    2015-08-28

    Hydrogen produced from water splitting is a promising source of clean energy. However, a robust catalyst is necessary to carry out the water oxidation step of water splitting. In this study, the catalyst studied was [(terpy)Mn(μ-O)2Mn(terpy)]3+ (MnTD) synthesized in the Metal Organic Framework (MOF) MIL-101(Cr), and the method used for analysis was hard X-ray powder diffraction. The diffraction data was used to detect the presence of MOF in different catalytic stages, and lattice parameters were assigned to the samples containing MOF. Fourier maps were constructed with GSAS II to determine the contents of the MOF as preliminary studies suggested that MnTD may not be present. Results showed that MOF is present before catalysis occurs but disappears by the time 45 minutes of catalysis has ensued. Changes in the MOF’s lattice parameters and location of electron density in the Fourier maps suggest attractions between the MOF and catalyst that may lead to MOF degradation. Fourier maps also revealed limited, if any, amounts of MnTD, even before catalysis occurred. Molecular manganese oxide may be the source of the high rate of water oxidation catalysis in the studied system.

  9. Visualization of electrochemically driven solid-state phase transformations using operando hard X-ray spectro-imaging

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Li, Linsen; Chen-Wiegart, Yu-chen Karen; Wang, Jiajun; Gao, Peng; Ding, Qi; Yu, Young-Sang; Wang, Feng; Cabana, Jordi; Wang, Jun; Jin, Song

    2015-04-20

    In situ techniques with high temporal, spatial and chemical resolution are key to understand ubiquitous solid-state phase transformations, which are crucial to many technological applications. Hard X-ray spectro-imaging can visualize electrochemically driven phase transformations but demands considerably large samples with strong absorption signal so far. Here we show a conceptually new data analysis method to enable operando visualization of mechanistically relevant weakly absorbing samples at the nanoscale and study electrochemical reaction dynamics of iron fluoride, a promising high-capacity conversion cathode material. In two specially designed samples with distinctive microstructure and porosity, we observe homogeneous phase transformations during both discharge andmore » charge, faster and more complete Li-storage occurring in porous polycrystalline iron fluoride, and further, incomplete charge reaction following a pathway different from conventional belief. In conclusion, these mechanistic insights provide guidelines for designing better conversion cathode materials to realize the promise of high-capacity lithium-ion batteries.« less

  10. A COMBINED LOW-RADIO FREQUENCY/X-RAY STUDY OF GALAXY GROUPS. I. GIANT METREWAVE RADIO TELESCOPE OBSERVATIONS AT 235 MHz AND 610 MHz

    SciTech Connect (OSTI)

    Giacintucci, Simona; O'Sullivan, Ewan; Vrtilek, Jan; David, Laurence P.; Mazzotta, Pasquale; Gitti, Myriam; Jones, Christine; Forman, William R.; Raychaudhury, Somak; Ponman, Trevor; Venturi, Tiziana; Athreya, Ramana M.; Clarke, Tracy E.; Murgia, Matteo; Ishwara-Chandra, C. H.

    2011-05-10

    We present new Giant Metrewave Radio Telescope observations at 235 MHz and 610 MHz of 18 X-ray bright galaxy groups. These observations are part of an extended project, presented here and in future papers, which combines low-frequency radio and X-ray data to investigate the interaction between central active galactic nuclei (AGNs) and the intra-group medium (IGM). The radio images show a very diverse population of group-central radio sources, varying widely in size, power, morphology, and spectral index. Comparison of the radio images with Chandra and XMM-Newton X-ray images shows that groups with significant substructure in the X-ray band and marginal radio emission at {approx}>1 GHz host low-frequency radio structures that correlate with substructures in IGM. Radio-filled X-ray cavities, the most evident form of AGN/IGM interaction in our sample, are found in half of the systems and are typically associated with small, low-, or mid-power double radio sources. Two systems, NGC5044 and NGC4636, possess multiple cavities, which are isotropically distributed around the group center, possibly due to group weather. In other systems the radio/X-ray correlations are less evident. However, the AGN/IGM interaction can manifest itself through the effects of the high-pressure medium on the morphology, spectral properties, and evolution of the radio-emitting plasma. In particular, the IGM can confine fading radio lobes in old/dying radio galaxies and prevent them from dissipating quickly. Evidence for radio emission produced by former outbursts that co-exist with current activity is found in six groups of the sample.

  11. Monte-Carlo simulation of noise in hard X-ray Transmission Crystal Spectrometers: Identification of contributors to the background noise and shielding optimization

    SciTech Connect (OSTI)

    Thfoin, I. Reverdin, C.; Duval, A.; Leboeuf, X.; Lecherbourg, L.; Ross, B.; Hulin, S.; Batani, D.; Santos, J. J.; Vaisseau, X.; Fourment, C.; Giuffrida, L.; Szabo, C. I.; Bastiani-Ceccotti, S.; Brambrink, E.; Koenig, M.; Nakatsutsumi, M.; Morace, A.

    2014-11-15

    Transmission crystal spectrometers (TCS) are used on many laser facilities to record hard X-ray spectra. During experiments, signal recorded on imaging plates is often degraded by a background noise. Monte-Carlo simulations made with the code GEANT4 show that this background noise is mainly generated by diffusion of MeV electrons and very hard X-rays. An experiment, carried out at LULI2000, confirmed that the use of magnets in front of the diagnostic, that bent the electron trajectories, reduces significantly this background. The new spectrometer SPECTIX (Spectromtre PETAL Cristal en TransmIssion X), built for the LMJ/PETAL facility, will include this optimized shielding.

  12. Design and Start-to-End Simulation of an X-Band RF Driven Hard X-Ray FEL with LCLS Injector

    SciTech Connect (OSTI)

    Sun, Yipeng; /SLAC

    2012-08-20

    In this note, it is briefly discussed the accelerator design and start-to-end 3D macro particles simulation (using ELEGANT and GENESIS) of an X-band RF driven hard X-ray FEL with LCLS injector. A preliminary design and LiTrack 1D simulation studies were presented before in an older publication [1]. In numerical simulations this X-band RF driven hard X-ray FEL achieves/exceeds LCLS-like performance in a much shorter overall length of 350 m, compared with 1200 m in the LCLS case. One key feature of this design is that it may achieve a higher final beam current of 5 kA plus a uniform energy profile, mainly due to the employment of stronger longitudinal wake fields in the last X-band RF linac [2].

  13. NuSTAR study of hard X-ray morphology and spectroscopy of PWN G21.50.9

    SciTech Connect (OSTI)

    Nynka, Melania; Hailey, Charles J.; Gotthelf, Eric V.; Mori, Kaya; Perez, Kerstin [Columbia Astrophysics Laboratory, Columbia University, New York, NY 10027 (United States); Reynolds, Stephen P. [Physics Department, NC State University, Raleigh, NC 27695 (United States); An, Hongjun [Department of Physics, McGill University, Rutherford Physics Building, 3600 University Street, Montreal, Quebec H3A 2T8 (Canada); Baganoff, Frederick K. [Center for Space Research, Massachusetts Institute of Technology, Cambridge, MA 02139-4307 (United States); Boggs, Steven E.; Krivonos, Roman; Zoglauer, Andreas [Space Sciences Laboratory, University of California, Berkeley, CA 94720 (United States); Christensen, Finn E. [DTU Space, National Space Institute, Technical University of Denmark, Elektrovej 327, DK-2800 Lyngby (Denmark); Craig, William W. [Lawrence Livermore National Laboratory, Livermore, CA 94550 (United States); Grefenstette, Brian W.; Harrison, Fiona A.; Madsen, Kristin K. [Cahill Center for Astronomy and Astrophysics, California Institute of Technology, Pasadena, CA 91125 (United States); Stern, Daniel [Jet Propulsion Laboratory, California Institute of Technology, Pasadena, CA 91109 (United States); Wik, Daniel R.; Zhang, William W. [NASA Goddard Space Flight Center, Greenbelt, MD 20771 (United States)

    2014-07-01

    We present NuSTAR high-energy X-ray observations of the pulsar wind nebula (PWN)/supernova remnant G21.50.9. We detect integrated emission from the nebula up to ?40 keV, and resolve individual spatial features over a broad X-ray band for the first time. The morphology seen by NuSTAR agrees well with that seen by XMM-Newton and Chandra below 10 keV. At high energies, NuSTAR clearly detects non-thermal emission up to ?20 keV that extends along the eastern and northern rim of the supernova shell. The broadband images clearly demonstrate that X-ray emission from the North Spur and Eastern Limb results predominantly from non-thermal processes. We detect a break in the spatially integrated X-ray spectrum at ?9 keV that cannot be reproduced by current spectral energy distribution models, implying either a more complex electron injection spectrum or an additional process such as diffusion compared to what has been considered in previous work. We use spatially resolved maps to derive an energy-dependent cooling length scale, L(E)?E{sup m} with m = 0.21 0.01. We find this to be inconsistent with the model for the morphological evolution with energy described by Kennel and Coroniti. This value, along with the observed steepening in power-law index between radio and X-ray, can be quantitatively explained as an energy-loss spectral break in the simple scaling model of Reynolds, assuming particle advection dominates over diffusion. This interpretation requires a substantial departure from spherical magnetohydrodynamic, magnetic-flux-conserving outflow, most plausibly in the form of turbulent magnetic-field amplification.

  14. Expectations for the hard x-ray continuum and gamma-ray line fluxes from the typE IA supernova SN 2014J in M82

    SciTech Connect (OSTI)

    The, Lih-Sin [Department of Physics and Astronomy, Clemson University, SC 29634 (United States); Burrows, Adam, E-mail: tlihsin@clemson.edu, E-mail: burrows@astro.princeton.edu [Department of Astrophysical Sciences, Princeton University, Princeton, NJ 08544 (United States)

    2014-05-10

    The hard X-ray continuum and gamma-ray lines from a Type Ia supernova dominate its integrated photon emissions and can provide unique diagnostics of the mass of the ejecta, the {sup 56}Ni yield and spatial distribution, its kinetic energy and expansion speed, and the mechanism of explosion. Such signatures and their time behavior 'X-ray' the bulk debris field in direct fashion, and do not depend on the ofttimes problematic and elaborate UV, optical, and near-infrared spectroscopy and radiative transfer that have informed the study of these events for decades. However, to date no hard photons have ever been detected from a Type Ia supernova in explosion. With the advent of the supernova SN 2014J in M82, at a distance of ?3.5 Mpc, this situation may soon change. Both NuSTAR and INTEGRAL have the potential to detect SN 2014J, and, if spectra and light curves can be measured, would usefully constrain the various explosion models published during the last ?30 yr. In support of these observational campaigns, we provide predictions for the hard X-ray continuum and gamma-line emissions for 15 Type Ia explosion models gleaned from the literature. The model set, containing as it does deflagration, delayed detonation, merger detonation, pulsational delayed detonation, and sub-Chandrasekhar helium detonation models, collectively spans a wide range of properties, and hence signatures. We provide a brief discussion of various diagnostics (with examples), but importantly make the spectral and line results available electronically to aid in the interpretation of the anticipated data.

  15. Electronic structure of β-Ga{sub 2}O{sub 3} single crystals investigated by hard X-ray photoelectron spectroscopy

    SciTech Connect (OSTI)

    Li, Guo-Ling; Zhang, Fabi; Guo, Qixin; Cui, Yi-Tao; Oji, Hiroshi; Son, Jin-Young

    2015-07-13

    By combination of hard X-ray photoelectron spectroscopy (HAXPES) and first-principles band structure calculations, the electronic states of β-Ga{sub 2}O{sub 3} were investigated to deepen the understanding of bulk information for this compound. The valence band spectra of HAXPES presented the main contribution from Ga 4sp, which are well represented by photoionization cross section weighted partial density of states. The experimental data complemented with the theoretical study yield a realistic picture of the electronic structure for β-Ga{sub 2}O{sub 3}.

  16. Simultaneous multiplexed materials characterization using a high-precision hard X-ray micro-slit array

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Zhang, Fan; Allen, Andrew J.; Levine, Lyle E.; Mancini, Derrick C.; Ilavsky, Jan

    2015-01-01

    Here, the needs both for increased experimental throughput and forin operandocharacterization of functional materials under increasingly realistic experimental conditions have emerged as major challenges across the whole of crystallography. A novel measurement scheme that allows multiplexed simultaneous measurements from multiple nearby sample volumes is presented. This new approach enables better measurement statistics or direct probing of heterogeneous structure, dynamics or elemental composition. To illustrate, the submicrometer precision that optical lithography provides has been exploited to create a multiplexed form of ultra-small-angle scattering based X-ray photon correlation spectroscopy (USAXS-XPCS) using micro-slit arrays fabricated by photolithography. Multiplexed USAXS-XPCS is applied to followmore » the equilibrium dynamics of a simple colloidal suspension. While the dependence of the relaxation time on momentum transfer, and its relationship with the diffusion constant and the static structure factor, follow previous findings, this measurements-in-parallel approach reduces the statistical uncertainties of this photon-starved technique to below those associated with the instrument resolution. More importantly, we note the potential of the multiplexed scheme to elucidate the response of different components of a heterogeneous sample underidenticalexperimental conditions in simultaneous measurements. Lastly, in the context of the X-ray synchrotron community, this scheme is, in principle, applicable to all in-line synchrotron techniques. Indeed, it has the potential to open a new paradigm for in operando characterization of heterogeneous functional materials, a situation that will be even further enhanced by the ongoing development of multi-bend achromat storage ring designs as the next evolution of large-scale X-ray synchrotron facilities around the world.« less

  17. Simultaneous multiplexed materials characterization using a high-precision hard X-ray micro-slit array

    SciTech Connect (OSTI)

    Zhang, Fan; Allen, Andrew J.; Levine, Lyle E.; Mancini, Derrick C.; Ilavsky, Jan

    2015-01-01

    Here, the needs both for increased experimental throughput and forin operandocharacterization of functional materials under increasingly realistic experimental conditions have emerged as major challenges across the whole of crystallography. A novel measurement scheme that allows multiplexed simultaneous measurements from multiple nearby sample volumes is presented. This new approach enables better measurement statistics or direct probing of heterogeneous structure, dynamics or elemental composition. To illustrate, the submicrometer precision that optical lithography provides has been exploited to create a multiplexed form of ultra-small-angle scattering based X-ray photon correlation spectroscopy (USAXS-XPCS) using micro-slit arrays fabricated by photolithography. Multiplexed USAXS-XPCS is applied to follow the equilibrium dynamics of a simple colloidal suspension. While the dependence of the relaxation time on momentum transfer, and its relationship with the diffusion constant and the static structure factor, follow previous findings, this measurements-in-parallel approach reduces the statistical uncertainties of this photon-starved technique to below those associated with the instrument resolution. More importantly, we note the potential of the multiplexed scheme to elucidate the response of different components of a heterogeneous sample underidenticalexperimental conditions in simultaneous measurements. Lastly, in the context of the X-ray synchrotron community, this scheme is, in principle, applicable to all in-line synchrotron techniques. Indeed, it has the potential to open a new paradigm for in operando characterization of heterogeneous functional materials, a situation that will be even further enhanced by the ongoing development of multi-bend achromat storage ring designs as the next evolution of large-scale X-ray synchrotron facilities around the world.

  18. Anomalous resistivity effect on multiple ion beam emission and hard x-ray generation in a Mather type plasma focus device

    SciTech Connect (OSTI)

    Behbahani, R. A.; Aghamir, F. M.

    2011-10-15

    Multi ion beam and hard x-ray emissions were detected in a high inductance (more than 100 nH) Mather type plasma focus (PF) device at different filling gas pressures and charging voltages. The signal analysis was performed through the current trace, as it is the fundamental signal from which all of the phenomena in a PF device can be extracted. Two different fitting processes were carried out according to Lee's computational (snow-plow) model. In the first process, only plasma dynamics and classical (Spitzer) resistances were considered as energy consumer parameters for plasma. This led to an unsuccessful fitting and did not answer the energy transfer mechanism into plasma. A second fitting process was considered through the addition of anomalous resistance, which provided the best fit. Anomalous resistance was the source of long decrease in current trace, and multi dips and multi peaks of high voltage probe. Multi-peak features were interpreted considering the second fitting process along with the mechanisms for ion beam production and hard x-ray emission. To show the important role of the anomalous resistance, the duration of the current drop was discussed.

  19. Solar X-ray physics

    SciTech Connect (OSTI)

    Bornmann, P.L. )

    1991-01-01

    Research on solar X-ray phenomena performed by American scientists during 1987-1990 is reviewed. Major topics discussed include solar images observed during quiescent times, the processes observed during solar flares, and the coronal, interplanetary, and terrestrial phenomena associated with solar X-ray flares. Particular attention is given to the hard X-ray emission observed at the start of the flare, the energy transfer to the soft X-ray emitting plasma, the late resolution of the flare as observed in soft X-ray, and the rate of occurrence of solar flares as a function of time and latitude. Pertinent aspects of nonflaring, coronal X-ray emission and stellar flares are also discussed. 175 refs.

  20. Electronic structure of the polymer-cathode interface of an organic electroluminescent device investigated using operando hard x-ray photoelectron spectroscopy

    SciTech Connect (OSTI)

    Ikeuchi, J.; Hamamatsu, H.; Miyamoto, T.; Tanaka, S.; Yamashita, Y.; Yoshikawa, H.; Ueda, S.

    2015-08-28

    The electronic structure of a polymer-cathode interface of an operating organic light-emitting diode (OLED) was directly investigated using hard X-ray photoelectron spectroscopy (HAXPES). The potential distribution profile of the light-emitting copolymer layer as a function of the depth under the Al/Ba cathode layer in the OLED depended on the bias voltage. We found that band bending occurred in the copolymer of 9,9-dioctylfluorene (50%) and N-(4-(2-butyl)-phenyl)diphenylamine (F8-PFB) layer near the cathode at 0 V bias, while a linear potential distribution formed in the F8-PFB when a bias voltage was applied to the OLED. Direct observation of the built-in potential and that band bending formed in the F8-PFB layer in the operating OLED suggested that charges moved in the F8-PFB layer before electron injection from the cathode.

  1. X-Ray Microscopy | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Microscopy X-Ray Microscopy This group exploits the unique capabilities of hard X-ray microscopy to visualize and understand the structure and behavior of hybrid, energy-related, and tailored nanomaterials The Hard X-Ray Nanoprobe, located at Sector 26 of the Advanced Photon Source (APS) and operated by our group and APS, is the only dedicated X-ray microscopy beamline within the portfolios of the nation's Nanoscale Science Research Centers. Our scientific program seeks to understand

  2. INTEGRAL SPI observations of Cygnus X-1 in the soft state: What about the jet contribution in hard X-rays?

    SciTech Connect (OSTI)

    Jourdain, E.; Roques, J. P.; Chauvin, M.

    2014-07-01

    During the first 7 yr of the INTEGRAL mission (2003-2009), Cyg X-1 has essentially been detected in its hard state (HS), with some incursions in intermediate HSs. This long, spectrally stable period allowed in particular the measurement of the polarization of the high-energy component that has long been observed above 200 keV in this peculiar object. This result strongly suggests that here we see the contribution of the jet, known to emit a strong synchrotron radio emission. In 2010 June, Cyg X-1 underwent a completed transition toward a soft state (SS). It gave us the unique opportunity to study in detail the corona emission in this spectral state, and to investigate in particular the behavior of the jet contribution. Indeed, during the SS, the hard X-ray emission decreases drastically, with its maximum energy shifted toward lower energy and its flux divided by a factor of ?5-10. Interestingly, the radio emission follows a similar drop, supporting the correlation between the jet emission and the hard component, even though the flux is too low to quantify the polarization characteristics.

  3. X-ray transmissive debris shield

    DOE Patents [OSTI]

    Spielman, Rick B.

    1996-01-01

    An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

  4. X-ray transmissive debris shield

    DOE Patents [OSTI]

    Spielman, R.B.

    1996-05-21

    An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

  5. SMB, X-Ray Spectroscopy & Imaging

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Home » X-Ray Spectroscopy & Imaging X-Ray Spectroscopy & Imaging SSRL has five hard X-ray Spectroscopy beamlines and three Microfocus Imaging beamlines dedicated to Biological and Biomedical research funded by the NIH and DOE-BER. The SMB group supports and develops technical instrumentation and theoretical methods for state-of-the-art tender and hard X-ray spectroscopy and EXAFS studies on metalloproteins, cofactors and metals in medicine. The SMB group has also contributed to the

  6. SWIFT X-RAY OBSERVATIONS OF CLASSICAL NOVAE. II. THE SUPER SOFT SOURCE SAMPLE

    SciTech Connect (OSTI)

    Schwarz, Greg J.; Ness, Jan-Uwe; Osborne, J. P.; Page, K. L.; Evans, P. A.; Beardmore, A. P.; Walter, Frederick M.; Andrew Helton, L.; Woodward, Charles E.; Bode, Mike; Starrfield, Sumner; Drake, Jeremy J.

    2011-12-01

    The Swift gamma-ray burst satellite is an excellent facility for studying novae. Its rapid response time and sensitive X-ray detector provides an unparalleled opportunity to investigate the previously poorly sampled evolution of novae in the X-ray regime. This paper presents Swift observations of 52 Galactic/Magellanic Cloud novae. We included the X-Ray Telescope (0.3-10 keV) instrument count rates and the UltraViolet and Optical Telescope (1700-8000 A) filter photometry. Also included in the analysis are the publicly available pointed observations of 10 additional novae the X-ray archives. This is the largest X-ray sample of Galactic/Magellanic Cloud novae yet assembled and consists of 26 novae with Super Soft X-ray emission, 19 from Swift observations. The data set shows that the faster novae have an early hard X-ray phase that is usually missing in slower novae. The Super Soft X-ray phase occurs earlier and does not last as long in fast novae compared to slower novae. All the Swift novae with sufficient observations show that novae are highly variable with rapid variability and different periodicities. In the majority of cases, nuclear burning ceases less than three years after the outburst begins. Previous relationships, such as the nuclear burning duration versus t{sub 2} or the expansion velocity of the eject and nuclear burning duration versus the orbital period, are shown to be poorly correlated with the full sample indicating that additional factors beyond the white dwarf mass and binary separation play important roles in the evolution of a nova outburst. Finally, we confirm two optical phenomena that are correlated with strong, soft X-ray emission which can be used to further increase the efficiency of X-ray campaigns.

  7. A Hard X-ray Study of a Manganese-Terpyridine Dimer Catalyst in a Chromium-based Metal Organic Framework - Oral Presentation

    SciTech Connect (OSTI)

    Ramsey, Alexandra

    2015-08-25

    Cleaner forms of energy are needed, and H2 produced from water spliFng is a possible source. However, a robust catalyst is necessary to carry out the water oxidaKon reacKon. Plants uKlize Photosystem II to catalyze water oxidaKon as a part of photosynthesis, and many syntheKc water oxidaKon catalysts use Photosystem II as a model. In this study, the catalyst of interest was [(terpy)Mn(μ-O)2Mn(terpy)]3+ (MnTD), which was synthesized in a chromium-based Metal Organic Framework (MOF) to avoid degradaKon of MnTD molecules. Hard X-ray powder diffracKon was the primary method of analysis. The diffracKon data was used to detect the presence of MOF in samples at different catalyKc stages, and laFce parameters were assigned to the samples containing MOF. Fourier maps were constructed to determine the contents of the MOF as preliminary studies suggested that MnTD may not be present. Results showed that MOF is present before catalysis occurs, but disappears in the iniKal stages of catalysis. Changes in the MOF’s laFce parameters suggest aWracKve interacKons between the MOF and catalyst; these interacKons may lead to the observed MOF degradaKon. Fourier maps also reveal limited, if any, amounts of MnTD in the system. Molecular manganese oxide may be the source of the high rate of water oxidaKon catalysis in the studied system.

  8. CORONAL PROPERTIES OF THE SEYFERT 1.9 GALAXY MCG-05-23-016 DETERMINED FROM HARD X-RAY SPECTROSCOPY WITH NuSTAR

    SciTech Connect (OSTI)

    Balokovi?, M.; Harrison, F. A.; Esmerian, C. J.; Frst, F.; Walton, D. J.; Matt, G.; Marinucci, A.; Zoghbi, A.; Reynolds, C. S.; Ballantyne, D. R.; Boggs, S. E.; Craig, W. W.; Christensen, F. E.; Fabian, A. C.; Parker, M. L.; Hailey, C. J.; Stern, D.; Zhang, W. W.

    2015-02-10

    Measurements of the high-energy cut-off in the coronal continuum of active galactic nuclei have long been elusive for all but a small number of the brightest examples. We present a direct measurement of the cut-off energy in the nuclear continuum of the nearby Seyfert 1.9 galaxy MCG-05-23-016 with unprecedented precision. The high sensitivity of NuSTAR up to 79 keV allows us to clearly disentangle the spectral curvature of the primary continuum from that of its reflection component. Using a simple phenomenological model for the hard X-ray spectrum, we constrain the cut-off energy to 116{sub ?5}{sup +6} keV with 90% confidence. Testing for more complex models and nuisance parameters that could potentially influence the measurement, we find that the cut-off is detected robustly. We further use simple Comptonized plasma models to provide independent constraints for both the kinetic temperature of the electrons in the corona and its optical depth. At the 90% confidence level, we find kT{sub e} = 29 2 keV and ? {sub e} = 1.23 0.08 assuming a slab (disk-like) geometry, and kT{sub e} = 25 2 keV and ? {sub e} = 3.5 0.2 assuming a spherical geometry. Both geometries are found to fit the data equally well and their two principal physical parameters are correlated in both cases. With the optical depth in the ? {sub e} ? 1 regime, the data are pushing the currently available theoretical models of the Comptonized plasma to the limits of their validity. Since the spectral features and variability arising from the inner accretion disk have been observed previously in MCG-05-23-016, the inferred high optical depth implies that a spherical or disk-like corona cannot be homogeneous.

  9. Ambient Pressure Photoelectron Spectroscopy Using Soft X-ray...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Ambient Pressure Photoelectron Spectroscopy Using Soft X-ray and Hard X-ray, and its applications in electrochemistry Friday, December 14, 2012 - 3:30pm SSRL, Bldg. 137, room 322...

  10. X-Ray Diagnostics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    including film developing and scanning, and image plate scanning. Related images X-ray framing camera being loaded into the TIM in the Trident North Target Area. X-ray framing...

  11. Femtosecond X-ray protein nanocrystallography

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    pulses from a hard-X-ray free-electron laser, the Linac Coherent Light Source (4). ... We mitigate the problem of radiation damage in crystallography by using pulses briefer ...

  12. X-Ray Diagnostics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diagnostics X-Ray Diagnostics Maintenance of existing devices and development of advanced concepts Contact John Oertel (505) 665-3246 Email Hot, dense matter produced by intense laser interaction with a solid target often produces x-rays with energies from 100 eV to those exceeding 100 keV. A suite of diagnostics and methods have been deployed at Trident to diagnose the x-ray emission from laser-matter interaction experiments, or to use the x-rays as a probe of dense matter. These

  13. Hard x-ray photoelectron spectroscopy study of Ge{sub 2}Sb{sub 2}Te{sub 5}; as-deposited amorphous, crystalline, and laser-reamorphized

    SciTech Connect (OSTI)

    Richter, Jan H. Tominaga, Junji; Fons, Paul; Kolobov, Alex V.; Ueda, Shigenori; Yoshikawa, Hideki; Yamashita, Yoshiyuki; Ishimaru, Satoshi; Kobayashi, Keisuke

    2014-02-10

    We have investigated the electronic structure of as-deposited, crystalline, and laser-reamorphized Ge{sub 2}Sb{sub 2}Te{sub 5} using high resolution, hard x-ray photoemission spectroscopy. A shift in the Fermi level as well as a broadening of the spectral features in the valence band and the Ge 3d level between the amorphous and crystalline state is observed. Upon amorphization, Ge 3d and Sb 4d spectra show a surprisingly small breaking of resonant bonds and changes in the bonding character as evidenced by the very similar density of states in all cases.

  14. X-ray beamsplitter

    DOE Patents [OSTI]

    Ceglio, Natale M.; Stearns, Daniel S.; Hawryluk, Andrew M.; Barbee, Jr., Troy W.

    1989-01-01

    An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

  15. X-ray beamsplitter

    DOE Patents [OSTI]

    Ceglio, N.M.; Stearns, D.G.; Hawryluk, A.M.; Barbee, T.W. Jr.

    1987-08-07

    An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5--50 pairs of alternate Mo/Si layers with a period of 20--250 A. The support membrane is 10--200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window. 6 figs.

  16. Chest x-Rays

    Broader source: Energy.gov [DOE]

    The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica.

  17. X-ray generator

    DOE Patents [OSTI]

    Dawson, John M.

    1976-01-01

    Apparatus and method for producing coherent secondary x-rays that are controlled as to direction by illuminating a mixture of high z and low z gases with an intense burst of primary x-rays. The primary x-rays are produced with a laser activated plasma, and these x-rays strip off the electrons of the high z atoms in the lasing medium, while the low z atoms retain their electrons. The neutral atoms transfer electrons to highly excited states of the highly striped high z ions giving an inverted population which produces the desired coherent x-rays. In one embodiment, a laser, light beam provides a laser spark that produces the intense burst of coherent x-rays that illuminates the mixture of high z and low z gases, whereby the high z atoms are stripped while the low z ones are not, giving the desired mixture of highly ionized and neutral atoms. To this end, the laser spark is produced by injecting a laser light beam, or a plurality of beams, into a first gas in a cylindrical container having an adjacent second gas layer co-axial therewith, the laser producing a plasma and the intense primary x-rays in the first gas, and the second gas containing the high and low atomic number elements for receiving the primary x-rays, whereupon the secondary x-rays are produced therein by stripping desired ions in a neutral gas and transfer of electrons to highly excited states of the stripped ions from the unionized atoms. Means for magnetically confining and stabilizing the plasma are disclosed for controlling the direction of the x-rays.

  18. Effects of electron recirculation on a hard x-ray source observed during the interaction of a high intensity laser pulse with thin Au targets

    SciTech Connect (OSTI)

    Compant La Fontaine, A.; Courtois, C.; Lefebvre, E.; Bourgade, J. L.; Landoas, O.; Thorp, K.; Stoeckl, C.

    2013-12-15

    The interaction of a high intensity laser pulse on the preplasma of a high-Z solid target produced by the pulse's pedestal generates high-energy electrons. These electrons subsequently penetrate inside the solid target and produce bremsstrahlung photons, generating an x-ray source which can be used for photonuclear studies or to radiograph high area density objects. The source characteristics are compared for targets with thin (20 μm) and thick (100 μm) Au foils on the Omega EP laser at Laboratory for Laser Energetics. Simulations using the particle-in-cell code CALDER show that for a 20 μm thickness Au target, electrons perform multiple round-trips in the target under the effect of the laser ponderomotive potential and the target electrostatic potential. These relativistic electrons have random transverse displacements, with respect to the target normal, attributed to electrostatic fluctuation fields. As a result, the x-ray spot size is increased by a factor 2 for thin target compared to thick targets, in agreement with experimental results. In addition, the computed doses agree with the measured ones provided that electron recirculation in the thin target is taken into account. A dose increase by a factor 1.7 is then computed by allowing for recirculation. In the 100 μm target case, on the other hand, this effect is found to be negligible.

  19. The study of pinch regimes based on radiation-enhanced compression and anomalous resistivity phenomena and their effects on hard x-ray emission in a Mather type dense plasma focus device (SABALAN2)

    SciTech Connect (OSTI)

    Piriaei, D.; Javadi, S.; Ghoranneviss, M.; Mahabadi, T. D.; Saw, S. H.; Lee, S.

    2015-12-15

    In this study, by using argon and nitrogen as the filling gases in a Mather type dense plasma focus device at different values of pressure and charging voltage, two different kinds of pinch regimes were observed for each of the gases. The physics of the pinch regimes could be explained by using the two versions of the Lee's computational model which predicted each of the scenarios and clarified their differences between the two gases according to the radiation-enhanced compression and, additionally, predicted the pinch regimes through the anomalous resistivity effect during the pinch time. This was accomplished through the fitting process (simulation) on the current signal. Moreover, the characteristic amplitude and time scales of the anomalous resistances were obtained. The correlations between the features of the plasma current dip and the emitted hard x-ray pulses were observed. The starting time, intensity, duration, and the multiple or single feature of the emitted hard x-ray strongly correlated to the same respective features of the current dip.

  20. X-ray laser

    DOE Patents [OSTI]

    Nilsen, Joseph

    1991-01-01

    An X-ray laser (10) that lases between the K edges of carbon and oxygen, i.e. between 44 and 23 Angstroms, is provided. The laser comprises a silicon (12) and dysprosium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state nickel-like dysprosium ions (34) are resonantly photo-pumped to their upper X-ray laser state by line emission from hydrogen-like silicon ions (32). The novel X-ray laser should prove especially useful for the microscopy of biological specimens.

  1. X-Ray Detection

    Office of Scientific and Technical Information (OSTI)

    ratio, I I on I off , recorded with plus (+, blue) and minus (-, red) x-ray helicities. This measurement was taken at -5 mA, which corresponds to a current...

  2. X-ray Imaging Workshop

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    microscopy (PEEM), angle resolved photoemission spectroscopy (ARPES), coherent diffraction imaging, x-ray microscopy, micro-tomography, holographic imaging, and x-ray...

  3. X-ray fluorescence mapping

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Microscopy and Imaging: X-ray Fluorescence Mapping Of increasing scientific interest is the detection, quantification and mapping of elemental content of samples, often down...

  4. X-ray microtomography

    SciTech Connect (OSTI)

    Landis, Eric N.; Keane, Denis T.

    2010-12-15

    In this tutorial, we describe X-ray microtomography as a technique to nondestructively characterize material microstructure in three dimensions at a micron level spatial resolution. While commercially available laboratory scale instrumentation is available, we focus our attention on synchrotron-based systems, where we can exploit a high flux, monochromatic X-ray beam to produce high fidelity three-dimensional images. A brief description of the physics and the mathematical analysis behind the technique is followed by example applications to specific materials characterization problems, with a particular focus on the utilization of three-dimensional image processing that can be used to extract a wide range of useful information.

  5. New BNL 3D-Trench Electrode Si Detectors for Radiation Hard Detectors for sLHC and for X-ray Applications

    SciTech Connect (OSTI)

    Li Z.

    2011-05-11

    . Since the large electrode spacing (up to 500 {micro}m) can be realized in the 3D-Trench electrode detector due to their advantage of greatly reduced full depletion voltage, detectors with large pixel cells (therefore small dead volume) can be made for applications in photon science (e.g. X-ray).

  6. X-ray beam finder

    DOE Patents [OSTI]

    Gilbert, H.W.

    1983-06-16

    An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

  7. Different X-ray spectral evolution for black hole X-ray binaries in dual tracks of radio-X-ray correlation

    SciTech Connect (OSTI)

    Cao, Xiao-Feng; Wu, Qingwen; Dong, Ai-Jun

    2014-06-10

    Recently, an 'outlier' track of radio-X-ray correlation was found, which is much steeper than the former universal correlation, where dual tracks were speculated to be triggered by different accretion processes. In this work, we test this issue by exploring hard X-ray spectral evolution in four black-hole X-ray binaries with multiple, quasi-simultaneous radio and X-ray observations. First, we find that hard X-ray photon indices, Γ, are negatively and positively correlated with X-ray fluxes when the X-ray flux, F{sub 3-9} {sub keV}, is below and above a critical flux, F{sub X,} {sub crit}, which are consistent with predictions of the advection-dominated accretion flow and the disk-corona model, respectively. Second, and most importantly, we find that the radio-X-ray correlations are also clearly different when the X-ray fluxes are higher and lower than the critical flux as defined by X-ray spectral evolution. The data points with F{sub 3-9} {sub keV} ≳ F{sub X,} {sub crit} have a steeper radio-X-ray correlation (F{sub X}∝F{sub R}{sup b} and b ∼ 1.1-1.4), which roughly forms the ''outlier'' track. However, the data points with anti-correlation of Γ – F{sub 3-9} {sub keV} either stay in the universal track with b ∼ 0.61 or stay in the transition track (from the universal to 'outlier' tracks or vice versa). Therefore, our results support that the universal and ''outlier'' tracks of radio-X-ray correlations are regulated by radiatively inefficient and radiatively efficient accretion model, respectively.

  8. PROPERTIES OF THE 24 DAY MODULATION IN GX 13+1 FROM NEAR-INFRARED AND X-RAY OBSERVATIONS

    SciTech Connect (OSTI)

    Corbet, Robin H. D.; Pearlman, Aaron B.; Buxton, Michelle; Levine, Alan M. E-mail: aaronp1@umbc.ed

    2010-08-10

    A 24 day period for the low-mass X-ray binary (LMXB) GX 13+1 was previously proposed on the basis of seven years of RXTE All-Sky Monitor (ASM) observations and it was suggested that this was the orbital period of the system. This would make it one of the longest known orbital periods for a Galactic LMXB powered by Roche lobe overflow. We present here the results of (1) K-band photometry obtained with the SMARTS Consortium CTIO 1.3 m telescope on 68 nights over a 10 month interval; (2) continued monitoring with the RXTE ASM, analyzed using a semi-weighted power spectrum instead of the data filtering technique previously used; and (3) Swift Burst Alert Telescope (BAT) hard X-ray observations. Modulation near 24 days is seen in both the K band and additional statistically independent ASM X-ray observations. However, the modulation in the ASM is not strictly periodic. The periodicity is also not detected in the Swift BAT observations, but modulation at the same relative level as seen with the ASM cannot be ruled out. If the 24 day period is the orbital period of system, this implies that the X-ray modulation is caused by structure that is not fixed in location. A possible mechanism for the X-ray modulation is the dipping behavior recently reported from XMM-Newton observations.

  9. X-RAY POINT-SOURCE POPULATIONS CONSTITUTING THE GALACTIC RIDGE X-RAY EMISSION

    SciTech Connect (OSTI)

    Morihana, Kumiko [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan)] [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Tsujimoto, Masahiro; Ebisawa, Ken [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan)] [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan); Yoshida, Tessei, E-mail: morihana@crab.riken.jp [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)] [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)

    2013-03-20

    Apparently diffuse X-ray emission has been known to exist along the central quarter of the Galactic Plane since the beginning of X-ray astronomy; this is referred to as the Galactic Ridge X-ray emission (GRXE). Recent deep X-ray observations have shown that numerous X-ray point sources account for a large fraction of the GRXE in the hard band (2-8 keV). However, the nature of these sources is poorly understood. Using the deepest X-ray observations made in the Chandra bulge field, we present the result of a coherent photometric and spectroscopic analysis of individual X-ray point sources for the purpose of constraining their nature and deriving their fractional contributions to the hard-band continuum and Fe K line emission of the GRXE. Based on the X-ray color-color diagram, we divided the point sources into three groups: A (hard), B (soft and broad spectrum), and C (soft and peaked spectrum). The group A sources are further decomposed spectrally into thermal and non-thermal sources with different fractions in different flux ranges. From their X-ray properties, we speculate that the group A non-thermal sources are mostly active galactic nuclei and the thermal sources are mostly white dwarf (WD) binaries such as magnetic and non-magnetic cataclysmic variables (CVs), pre-CVs, and symbiotic stars, whereas the group B and C sources are X-ray active stars in flares and quiescence, respectively. In the log N-log S curve of the 2-8 keV band, the group A non-thermal sources are dominant above Almost-Equal-To 10{sup -14} erg cm{sup -2} s{sup -1}, which is gradually taken over by Galactic sources in the fainter flux ranges. The Fe K{alpha} emission is mostly from the group A thermal (WD binaries) and the group B (X-ray active stars) sources.

  10. Soft-x-ray

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Soft-x-ray emission, plasma equilibrium, and fluctuation studies on Madison Symmetric Torus C. Xiao Department of Physics, University of Wisconsin-Madison, Madison, Wisconsin and Department of Physics and Engineering Physics, University of Saskatchewan, Saskatoon, Canada P. Franz Consorzio RFX-Associazione EURATOM ENEA Sulla Fusione, Italy and Istituto Nazionale di Fisica della Materia, Unita' di Ricerca di Padova, Italy B. E. Chapman and D. Craig Department of Physics, University of

  11. X-Ray Microscopy Capabilities | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Microscopy Capabilities The Hard X-Ray Nanoprobe (HXN) facility provides scanning fluorescence, scanning diffraction, and full-field transmission and tomographic imaging capabilities with a spatial resolution of 30 nm over a spectral range of 6-12 keV. Modes of Operation Full-Field Transmission Imaging and Nanotomography X-ray transmission imaging uses both the absorption and phase shift of the X-ray beam by the sample as contrast mechanisms. Absorption contrast is used to map the sample

  12. ON THE RECENTLY DISCOVERED CORRELATIONS BETWEEN GAMMA-RAY AND X-RAY PROPERTIES OF GAMMA-RAY BURSTS

    SciTech Connect (OSTI)

    Dado, Shlomo; Dar, Arnon [Physics Department, Technion, Haifa 32000 (Israel)

    2013-09-20

    Recently, many correlations between the prompt {gamma}-ray emission properties and the X-ray afterglow properties of gamma-ray bursts (GRBs) have been inferred from a comprehensive analysis of the X-ray light curves of more than 650 GRBs measured with the Swift X-Ray Telescope (Swift/XRT) during the years 2004-2010. We show that these correlations are predicted by the cannonball (CB) model of GRBs. They result from the dependence of GRB observables on the bulk motion Lorentz factor and viewing angle of the jet of highly relativistic plasmoids (CBs) that produces the observed radiations by interaction with the medium through which it propagates. Moreover, despite their different physical origins, long GRBs (LGRBs) and short-hard bursts (SHBs) in the CB model share similar kinematic correlations, which can be combined into triple correlations satisfied by both LGRBs and SHBs.

  13. Fluctuation X-Ray Scattering

    SciTech Connect (OSTI)

    Saldin, PI: D. K.; Co-I's: J. C. H. Spence and P. Fromme

    2013-01-25

    The work supported by the grant was aimed at developing novel methods of finding the structures of biomolecules using x-rays from novel sources such as the x-ray free electron laser and modern synchrotrons

  14. Ultrafast X-Ray Coherent Control

    SciTech Connect (OSTI)

    Reis, David

    2009-05-01

    This main purpose of this grant was to develop the nascent #12;eld of ultrafast x-ray science using accelerator-based sources, and originally developed from an idea that a laser could modulate the di#11;racting properties of a x-ray di#11;racting crystal on a fast enough time scale to switch out in time a shorter slice from the already short x-ray pulses from a synchrotron. The research was carried out primarily at the Advanced Photon Source (APS) sector 7 at Argonne National Laboratory and the Sub-Picosecond Pulse Source (SPPS) at SLAC; in anticipation of the Linac Coherent Light Source (LCLS) x-ray free electron laser that became operational in 2009 at SLAC (all National User Facilities operated by BES). The research centered on the generation, control and measurement of atomic-scale dynamics in atomic, molecular optical and condensed matter systems with temporal and spatial resolution . It helped develop the ultrafast physics, techniques and scienti#12;c case for using the unprecedented characteristics of the LCLS. The project has been very successful with results have been disseminated widely and in top journals, have been well cited in the #12;eld, and have laid the foundation for many experiments being performed on the LCLS, the world's #12;rst hard x-ray free electron laser.

  15. Tunable X-ray source

    DOE Patents [OSTI]

    Boyce, James R.

    2011-02-08

    A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

  16. In-operando hard X-ray photoelectron spectroscopy study on the impact of current compliance and switching cycles on oxygen and carbon defects in resistive switching Ti/HfO{sub 2}/TiN cells

    SciTech Connect (OSTI)

    Sowinska, Malgorzata Bertaud, Thomas; Walczyk, Damian; Calka, Pauline; Walczyk, Christian; Thiess, Sebastian; Alff, Lambert; Schroeder, Thomas

    2014-05-28

    In this study, direct experimental materials science evidence of the important theoretical prediction for resistive random access memory (RRAM) technologies that a critical amount of oxygen vacancies is needed to establish stable resistive switching in metal-oxide-metal samples is presented. In detail, a novel in-operando hard X-ray photoelectron spectroscopy technique is applied to non-destructively investigates the influence of the current compliance and direct current voltage sweep cycles on the Ti/HfO{sub 2} interface chemistry and physics of resistive switching Ti/HfO{sub 2}/TiN cells. These studies indeed confirm that current compliance is a critical parameter to control the amount of oxygen vacancies in the conducting filaments in the oxide layer during the RRAM cell operation to achieve stable switching. Furthermore, clear carbon segregation towards the Ti/HfO{sub 2} interface under electrical stress is visible. Since carbon impurities impact the oxygen vacancy defect population under resistive switching, this dynamic carbon segregation to the Ti/HfO{sub 2} interface is suspected to negatively influence RRAM device endurance. Therefore, these results indicate that the RRAM materials engineering needs to include all impurities in the dielectric layer in order to achieve reliable device performance.

  17. A combined capacitance-voltage and hard x-ray photoelectron spectroscopy characterisation of metal/Al{sub 2}O{sub 3}/In{sub 0.53}Ga{sub 0.47}As capacitor structures

    SciTech Connect (OSTI)

    Lin, Jun; Povey, Ian M.; Hurley, Paul K.; Walsh, Lee; Hughes, Greg; Woicik, Joseph C.; O'Regan, Terrance P.

    2014-07-14

    Capacitance-Voltage (C-V) characterization and hard x-ray photoelectron spectroscopy (HAXPES) measurements have been used to study metal/Al{sub 2}O{sub 3}/In{sub 0.53}Ga{sub 0.47}As capacitor structures with high (Ni) and low (Al) work function metals. The HAXPES measurements observe a band bending occurring prior to metal deposition, which is attributed to a combination of fixed oxide charges and interface states of donor-type. Following metal deposition, the Fermi level positions at the Al{sub 2}O{sub 3}/In{sub 0.53}Ga{sub 0.47}As interface move towards the expected direction as observed from HAXPES measurements. The In{sub 0.53}Ga{sub 0.47}As surface Fermi level positions determined from both the C-V analysis at zero gate bias and HAXPES measurements are in reasonable agreement. The results are consistent with the presence of electrically active interface states at the Al{sub 2}O{sub 3}/In{sub 0.53}Ga{sub 0.47}As interface and suggest an interface state density increasing towards the In{sub 0.53}Ga{sub 0.47}As valence band edge.

  18. SMB, X-ray Emission Spectroscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    include X-ray Emission Spectroscopy (XES), Resonant Inelastic X-ray Scattering (RIXS), High Energy Resolution Fluorescence Detection (HERFD) and X-ray Raman Spectroscopy (XRS). ...

  19. X-ray lithography source

    DOE Patents [OSTI]

    Piestrup, M.A.; Boyers, D.G.; Pincus, C.

    1991-12-31

    A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits is disclosed. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and eliminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an excellent moderate-priced X-ray source for lithography. 26 figures.

  20. X-ray lithography source

    DOE Patents [OSTI]

    Piestrup, Melvin A.; Boyers, David G.; Pincus, Cary

    1991-01-01

    A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and elminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an exellent moderate-priced X-ray source for lithography.

  1. OPTICAL AND NEAR-INFRARED MONITORING OF THE BLACK HOLE X-RAY BINARY GX 339-4 DURING 2002-2010

    SciTech Connect (OSTI)

    Buxton, Michelle M.; Bailyn, Charles D.; Capelo, Holly L.; Chatterjee, Ritaban; Dincer, Tolga; Kalemci, Emrah; Tomsick, John A.

    2012-06-15

    We present the optical/infrared (O/IR) light curve of the black hole X-ray binary GX 339-4 collected at the SMARTS 1.3 m telescope from 2002 to 2010. During this time the source has undergone numerous state transitions including hard-to-soft state transitions when we see large changes in the near-IR flux accompanied by modest changes in optical flux, and three rebrightening events in 2003, 2005, and 2007 after GX 339-4 transitioned from the soft state to the hard. All but one outburst show similar behavior in the X-ray hardness-intensity diagram. We show that the O/IR colors follow two distinct tracks that reflect either the hard or soft X-ray state of the source. Thus, either of these two X-ray states can be inferred from O/IR observations alone. From these correlations we have constructed spectral energy distributions of the soft and hard states. During the hard state, the near-IR data have the same spectral slope as simultaneous radio data when GX 339-4 was in a bright optical state, implying that the near-IR is dominated by a non-thermal source, most likely originating from jets. Non-thermal emission dominates the near-IR bands during the hard state at all but the faintest optical states, and the fraction of non-thermal emission increases with increasing optical brightness. The spectral slope of the optical bands indicate that a heated thermal source is present during both the soft and hard X-ray states, even when GX 339-4 is at its faintest optical state. We have conducted a timing analysis of the light curve for the hard and soft states and find no evidence of a characteristic timescale within the range of 4-230 days.

  2. X-Ray Light Sources | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    The APS is one of only four third-generation, hard x-ray synchrotron radiation light ... Stanford Synchrotron Radiation Light Source (SSRL) at SLAC National Accelerator Laboratory ...

  3. Miniature x-ray source

    DOE Patents [OSTI]

    Trebes, James E.; Stone, Gary F.; Bell, Perry M.; Robinson, Ronald B.; Chornenky, Victor I.

    2002-01-01

    A miniature x-ray source capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature x-ray source comprises a compact vacuum tube assembly containing a cathode, an anode, a high voltage feedthru for delivering high voltage to the anode, a getter for maintaining high vacuum, a connection for an initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is highly x-ray transparent and made, for example, from boron nitride. The compact size and potential for remote operation allows the x-ray source, for example, to be placed adjacent to a material sample undergoing analysis or in proximity to the region to be treated for medical applications.

  4. Femtosecond X-ray protein nanocrystallography

    SciTech Connect (OSTI)

    Chapman, Henry N.; Barty, Anton; White, Thomas A.; Aquila, Andrew; Schulz, Joachim; DePonte, Daniel P.; Martin, Andrew V.; Coppola, Nicola; Liang, Mengning; Caleman, Carl; Gumprecht, Lars; Stern, Stephan; Nass, Karol; Fromme, Petra; Hunter, Mark S.; Grotjohann, Ingo; Fromme, Raimund; Kirian, Richard A.; Weierstall, Uwe; Doak, R. Bruce; Schmidt, Kevin E.; Wang, Xiaoyu; Spence, John C. H.; Schlichting, Ilme; Epp, Sascha W.; Rolles, Daniel; Rudenko, Artem; Foucar, Lutz; Rudek, Benedikt; Erk, Benjamin; Schmidt, Carlo; Hömke, André; Strüder, Lothar; Ullrich, Joachim; Krasniqi, Faton; Lomb, Lukas; Shoeman, Robert L.; Bott, Mario; Barends, Thomas R. M.; Kuhnel, Kai-Uwe; Schroter, Claus-Dieter; Hartmann, Robert; Holl, Peter; Reich, Christian; Soltau, Heike; Kimmel, Nils; Weidenspointner, Georg; Pietschner, Daniel; Hauser, Günter; Herrmann, Sven; Schaller, Gerhard; Schopper, Florian; Andritschke, Robert; Boutet, Sébastien; Krzywinski, Jacek; Bostedt, Christoph; Messerschmidt, Marc; Bozek, John D.; Williams, Garth J.; Bogan, Michael J.; Hampton, Christina Y.; Sierra, Raymond G.; Starodub, Dmitri; Gorke, Hubert; Hau-Riege, Stefan P.; Frank, Matthias; Maia, Filipe R. N. C.; Hajdu, Janos; Timneanu, Nicusor; Seibert, M. Marvin; Andreasson, Jakob; Rocker, Andrea; Jönsson, Olof; Svenda, Martin; Holton, James M.; Marchesini, Stefano; Neutze, Richard; Schorb, Sebastian; Rupp, Daniela; Adolph, Marcus; Gorkhover, Tais; Andersson, Inger; Barthelmess, Miriam; Bajt, Saša; Hirsemann, Helmut; Potdevin, Guillaume; Graafsma, Heinz; Nilsson, Björn

    2011-02-03

    X-ray crystallography provides the vast majority of macromolecular structures, but the success of the method relies on growing crystals of sufficient size. In conventional measurements, the necessary increase in X-ray dose to record data from crystals that are too small leads to extensive damage before a diffraction signal can be recorded. It is particularly challenging to obtain large, well-diffracting crystals of membrane proteins, for which fewer than 300 unique structures have been determined despite their importance in all living cells. Here we present a method for structure determination where single-crystal X-ray diffraction ‘snapshots’ are collected from a fully hydrated stream of nanocrystals using femtosecond pulses from a hard-X-ray free-electron laser, the Linac Coherent Light Source. We prove this concept with nanocrystals of photosystem I, one of the largest membrane protein complexes. More than 3,000,000 diffraction patterns were collected in this study, and a three-dimensional data set was assembled from individual photosystem I nanocrystals (~200 nm to 2 μm in size). We mitigate the problem of radiation damage in crystallography by using pulses briefer than the timescale of most damage processes. This offers a new approach to structure determination of macromolecules that do not yield crystals of sufficient size for studies using conventional radiation sources or are particularly sensitive to radiation damage.

  5. X-Ray Science Education

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    TV Network external link DNA Interactive external link Reciprocal Net external link X-ray Science Courses and Programs Various educational efforts are closely related to the...

  6. X-ray shearing interferometer

    DOE Patents [OSTI]

    Koch, Jeffrey A.

    2003-07-08

    An x-ray interferometer for analyzing high density plasmas and optically opaque materials includes a point-like x-ray source for providing a broadband x-ray source. The x-rays are directed through a target material and then are reflected by a high-quality ellipsoidally-bent imaging crystal to a diffraction grating disposed at 1.times. magnification. A spherically-bent imaging crystal is employed when the x-rays that are incident on the crystal surface are normal to that surface. The diffraction grating produces multiple beams which interfere with one another to produce an interference pattern which contains information about the target. A detector is disposed at the position of the image of the target produced by the interfering beams.

  7. Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Techniques | Stanford Synchrotron Radiation Lightsource Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Techniques Wednesday, September 5, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Gang Chen Seminar: Structures at atomic scales are traditionally determined through X-ray crystallography that amplifies scattering intensities by introducing spatial periodicity. For amorphous materials and many macromolecules, such as viruses, proteins and biofilms, it is hard to

  8. Miniature x-ray source

    DOE Patents [OSTI]

    Trebes, James E.; Bell, Perry M.; Robinson, Ronald B.

    2000-01-01

    A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

  9. X-ray microtomographic scanners

    SciTech Connect (OSTI)

    Syryamkin, V. I. Klestov, S. A.

    2015-11-17

    The article studies the operating procedures of an X-ray microtomographic scanner and the module of reconstruction and analysis 3D-image of a test sample in particular. An algorithm for 3D-image reconstruction based on image shadow projections and mathematical methods of the processing are described. Chapter 1 describes the basic principles of X-ray tomography and general procedures of the device developed. Chapters 2 and 3 are devoted to the problem of resources saving by the system during the X-ray tomography procedure, which is achieved by preprocessing of the initial shadow projections. Preprocessing includes background noise removing from the images, which reduces the amount of shadow projections in general and increases the efficiency of the group shadow projections compression. In conclusion, the main applications of X-ray tomography are presented.

  10. Neutron and X-ray Detectors

    SciTech Connect (OSTI)

    Carini, Gabriella; Denes, Peter; Gruener, Sol; Lessner, Elianne

    2012-08-01

    (and two computing hurdles that result from the corresponding increase in data volume) for the detector community to overcome in order to realize the full potential of BES neutron and X-ray facilities. Resolving these detector impediments will improve scientific productivity both by enabling new types of experiments, which will expand the scientific breadth at the X-ray and neutron facilities, and by potentially reducing the beam time required for a given experiment. These research priorities are summarized in the table below. Note that multiple, simultaneous detector improvements are often required to take full advantage of brighter sources. High-efficiency hard X-ray sensors: The fraction of incident particles that are actually detected defines detector efficiency. Silicon, the most common direct-detection X-ray sensor material, is (for typical sensor thicknesses) 100% efficient at 8 keV, 25%efficient at 20 keV, and only 3% efficient at 50 keV. Other materials are needed for hard X-rays. Replacement for 3He for neutron detectors: 3He has long been the neutron detection medium of choice because of its high cross section over a wide neutron energy range for the reaction 3He + n —> 3H + 1H + 0.764 MeV. 3He stockpiles are rapidly dwindling, and what is available can be had only at prohibitively high prices. Doped scintillators hold promise as ways to capture neutrons and convert them into light, although work is needed on brighter, more efficient scintillator solutions. Neutron detectors also require advances in speed and resolution. Fast-framing X-ray detectors: Today’s brighter X-ray sources make time-resolved studies possible. For example, hybrid X-ray pixel detectors, initially developed for particle physics, are becoming fairly mature X-ray detectors, with considerable development in Europe. To truly enable time-resolved studies, higher frame rates and dynamic range are required, and smaller pixel sizes are desirable. High-speed spectroscopic X-ray detectors

  11. X-Ray Interactions with Matter from the Center for X-Ray Optics...

    Office of Scientific and Technical Information (OSTI)

    X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO) Title: X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO) The primary interactions of ...

  12. Electromechanical x-ray generator

    DOE Patents [OSTI]

    Watson, Scott A; Platts, David; Sorensen, Eric B

    2016-05-03

    An electro-mechanical x-ray generator configured to obtain high-energy operation with favorable energy-weight scaling. The electro-mechanical x-ray generator may include a pair of capacitor plates. The capacitor plates may be charged to a predefined voltage and may be separated to generate higher voltages on the order of hundreds of kV in the AK gap. The high voltage may be generated in a vacuum tube.

  13. SMB, X-ray Absorption Spectroscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Absorption Spectroscopy X-ray Absorption Spectroscopy X-ray absorption spectroscopy (XAS) is a well-established technique for simultaneous local geometric and electronic structure...

  14. Compact x-ray source and panel

    DOE Patents [OSTI]

    Sampayon, Stephen E.

    2008-02-12

    A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

  15. Focused X-ray source

    DOE Patents [OSTI]

    Piestrup, M.A.; Boyers, D.G.; Pincus, C.I.; Maccagno, P.

    1990-08-21

    Disclosed is an intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator. 8 figs.

  16. Focused X-ray source

    DOE Patents [OSTI]

    Piestrup, Melvin A.; Boyers, David G.; Pincus, Cary I.; Maccagno, Pierre

    1990-01-01

    An intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator.

  17. X-RAY EMISSION FROM MAGNETIC MASSIVE STARS

    SciTech Connect (OSTI)

    Naz, Yal; Petit, Vronique; Rinbrand, Melanie; Owocki, Stan; Cohen, David; Ud-Doula, Asif; Wade, Gregg A.

    2014-11-01

    Magnetically confined winds of early-type stars are expected to be sources of bright and hard X-rays. To clarify the systematics of the observed X-ray properties, we have analyzed a large series of Chandra and XMM-Newton observations, corresponding to all available exposures of known massive magnetic stars (over 100 exposures covering ?60% of stars compiled in the catalog of Petit et al.). We show that the X-ray luminosity is strongly correlated with the stellar wind mass-loss rate, with a power-law form that is slightly steeper than linear for the majority of the less luminous, lower- M-dot B stars and flattens for the more luminous, higher- M-dot O stars. As the winds are radiatively driven, these scalings can be equivalently written as relations with the bolometric luminosity. The observed X-ray luminosities, and their trend with mass-loss rates, are well reproduced by new MHD models, although a few overluminous stars (mostly rapidly rotating objects) exist. No relation is found between other X-ray properties (plasma temperature, absorption) and stellar or magnetic parameters, contrary to expectations (e.g., higher temperature for stronger mass-loss rate). This suggests that the main driver for the plasma properties is different from the main determinant of the X-ray luminosity. Finally, variations of the X-ray hardnesses and luminosities, in phase with the stellar rotation period, are detected for some objects and they suggest that some temperature stratification exists in massive stars' magnetospheres.

  18. RESONANT INELASTIC X-RAY SCATTERING FROM TRANSITION METAL OXIDES.

    SciTech Connect (OSTI)

    HILL,J.P.

    1999-08-23

    Recent developments in hard x-ray resonant inelastic x-ray scattering as a probe of strongly correlated systems are reviewed. Particular attention is paid to studies of Nd{sub 2}CuO{sub 4}. A charge transfer excitation is observed when the incident photon energy is tuned in the vicinity of the copper K-edge. It is shown that the presence of resonant enhancements is controlled by the polarization dependence of the excitation process and by the overlap between a given intermediate state and the particular excitation being studied. This latter observation has shed light on the non-local effects present in certain intermediate states.

  19. Reabsorption of Soft X-Ray Emission at High X-Ray Free-Electron...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Reabsorption of Soft X-Ray Emission at High X-Ray Free-Electron Laser Fluences Citation Details In-Document Search Title: Reabsorption of Soft X-Ray Emission at ...

  20. A computational study of x-ray emission from high-Z x-ray sources...

    Office of Scientific and Technical Information (OSTI)

    A computational study of x-ray emission from high-Z x-ray sources on the National Ignition Facility laser Citation Details In-Document Search Title: A computational study of x-ray ...

  1. A computational study of x-ray emission from high-Z x-ray sources...

    Office of Scientific and Technical Information (OSTI)

    study of x-ray emission from high-Z x-ray sources on the National Ignition Facility laser Citation Details In-Document Search Title: A computational study of x-ray emission...

  2. Microgap x-ray detector

    DOE Patents [OSTI]

    Wuest, Craig R.; Bionta, Richard M.; Ables, Elden

    1994-01-01

    An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

  3. Microgap x-ray detector

    DOE Patents [OSTI]

    Wuest, C.R.; Bionta, R.M.; Ables, E.

    1994-05-03

    An x-ray detector is disclosed which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope. 3 figures.

  4. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light ... wavelengths relevant to atomic and molecular phenomena) with the advantages of ...

  5. Producing X-rays at the APS

    ScienceCinema (OSTI)

    None

    2013-04-19

    An introduction and overview of the Advanced Photon Source at Argonne National Laboratory, the technology that produces the brightest X-ray beams in the Western Hemisphere, and the research carried out by scientists using those X-rays.

  6. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Nanoimaging: Instruments and Methods X-Ray Nanoimaging: Instruments and Methods Print To be held as part of SPIE. http://spie.org/OP318 August 28-29, 2013; San Diego, California, USA

  7. Neutron and X-ray Scattering

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Neutron and X-ray Scattering Neutron and X-ray Scattering When used together, neutrons and high-energy x-rays provide a supremely powerful scientific tool for mining details about the structure of materials. Combining neutrons and high-energy x-rays to explore the frontiers of materials in extreme environments. Illuminating previously inaccessible time and spatial scales. Enabling in situ research to design, discover, and control materials. Get Expertise Donald Brown Email Pushing the limits of

  8. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  9. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  10. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  11. Phase-sensitive X-ray imager

    DOE Patents [OSTI]

    Baker, Kevin Louis

    2013-01-08

    X-ray phase sensitive wave-front sensor techniques are detailed that are capable of measuring the entire two-dimensional x-ray electric field, both the amplitude and phase, with a single measurement. These Hartmann sensing and 2-D Shear interferometry wave-front sensors do not require a temporally coherent source and are therefore compatible with x-ray tubes and also with laser-produced or x-pinch x-ray sources.

  12. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  13. Five Ways SLAC's X-ray Laser Can Change the Way We Live: 'The...

    Office of Environmental Management (EM)

    ... While we know the starting ingredients and outcomes of chemical reactions, the early and middle steps are hard to see in real time at the atomic scale. LCLS X-ray pulses are so ...

  14. Cryotomography x-ray microscopy state

    DOE Patents [OSTI]

    Le Gros, Mark; Larabell, Carolyn A.

    2010-10-26

    An x-ray microscope stage enables alignment of a sample about a rotation axis to enable three dimensional tomographic imaging of the sample using an x-ray microscope. A heat exchanger assembly provides cooled gas to a sample during x-ray microscopic imaging.

  15. ABSOLUTE TIMING OF THE CRAB PULSAR WITH THE INTEGRAL/SPI TELESCOPE

    SciTech Connect (OSTI)

    Molkov, S.; Jourdain, E.; Roques, J. P.

    2010-01-01

    We have investigated the pulse shape evolution of the Crab pulsar emission in the hard X-ray domain of the electromagnetic spectrum. In particular, we have studied the alignment of the Crab pulsar phase profiles measured in the hard X-rays and in other wavebands. To obtain the hard X-ray pulse profiles, we have used six years (2003-2009, with a total exposure of about 4 Ms) of publicly available data of the SPI telescope on-board the International Gamma-Ray Astrophysics Laboratory observatory, folded with the pulsar time solution derived from the Jodrell Bank Crab Pulsar Monthly Ephemeris. We found that the main pulse in the hard X-ray 20-100 keV energy band leads the radio one by 8.18 +- 0.46 milliperiods in phase, or 275 +- 15 mus in time. Quoted errors represent only statistical uncertainties. Our systematic error is estimated to be approx40 mus and is mainly caused by the radio measurement uncertainties. In hard X-rays, the average distance between the main pulse and interpulse on the phase plane is 0.3989 +- 0.0009. To compare our findings in hard X-rays with the soft 2-20 keV X-ray band, we have used data of quasi-simultaneous Crab observations with the proportional counter array monitor on-board the Rossi X-Ray Timing Explorer mission. The time lag and the pulses separation values measured in the 3-20 keV band are 0.00933 +- 0.00016 (corresponding to 310 +- 6 mus) and 0.40016 +- 0.00028 parts of the cycle, respectively. While the pulse separation values measured in soft X-rays and hard X-rays agree, the time lags are statistically different. Additional analysis show that the delay between the radio and X-ray signals varies with energy in the 2-300 keV energy range. We explain such a behavior as due to the superposition of two independent components responsible for the Crab pulsed emission in this energy band.

  16. X-ray Optics for BES Light Source Facilities

    SciTech Connect (OSTI)

    Mills, Dennis; Padmore, Howard; Lessner, Eliane

    2013-03-27

    Each new generation of synchrotron radiation sources has delivered an increase in average brightness 2 to 3 orders of magnitude over the previous generation. The next evolution toward diffraction-limited storage rings will deliver another 3 orders of magnitude increase. For ultrafast experiments, free electron lasers (FELs) deliver 10 orders of magnitude higher peak brightness than storage rings. Our ability to utilize these ultrabright sources, however, is limited by our ability to focus, monochromate, and manipulate these beams with X-ray optics. X-ray optics technology unfortunately lags behind source technology and limits our ability to maximally utilize even today’s X-ray sources. With ever more powerful X-ray sources on the horizon, a new generation of X-ray optics must be developed that will allow us to fully utilize these beams of unprecedented brightness. The increasing brightness of X-ray sources will enable a new generation of measurements that could have revolutionary impact across a broad area of science, if optical systems necessary for transporting and analyzing X-rays can be perfected. The high coherent flux will facilitate new science utilizing techniques in imaging, dynamics, and ultrahigh-resolution spectroscopy. For example, zone-plate-based hard X-ray microscopes are presently used to look deeply into materials, but today’s resolution and contrast are restricted by limitations of the current lithography used to manufacture nanodiffractive optics. The large penetration length, combined in principle with very high spatial resolution, is an ideal probe of hierarchically ordered mesoscale materials, if zone-plate focusing systems can be improved. Resonant inelastic X-ray scattering (RIXS) probes a wide range of excitations in materials, from charge-transfer processes to the very soft excitations that cause the collective phenomena in correlated electronic systems. However, although RIXS can probe high-energy excitations, the most exciting and

  17. EVIDENCE OF NON-THERMAL X-RAY EMISSION FROM HH 80

    SciTech Connect (OSTI)

    Lpez-Santiago, J.; Peri, C. S.; Benaglia, P.; Bonito, R.; Miceli, M.; Albacete-Colombo, J. F.; De Castro, E.

    2013-10-20

    Protostellar jets appear at all stages of star formation when the accretion process is still at work. Jets travel at velocities of hundreds of km s{sup 1}, creating strong shocks when interacting with the interstellar medium. Several cases of jets have been detected in X-rays, typically showing soft emission. For the first time, we report evidence of hard X-ray emission possibly related to non-thermal processes not explained by previous models of the post-shock emission predicted in the jet/ambient interaction scenario. HH 80 is located at the south head of the jet associated with the massive protostar IRAS 18162-2048. It shows soft and hard X-ray emission in regions that are spatially separated, with the soft X-ray emission region situated behind the region of hard X-ray emission. We propose a scenario for HH 80 where soft X-ray emission is associated with thermal processes from the interaction of the jet with denser ambient matter and hard X-ray emission is produced by synchrotron radiation at the front shock.

  18. X-ray lithography using holographic images

    DOE Patents [OSTI]

    Howells, Malcolm R.; Jacobsen, Chris

    1995-01-01

    A non-contact X-ray projection lithography method for producing a desired X-ray image on a selected surface of an X-ray-sensitive material, such as photoresist material on a wafer, the desired X-ray image having image minimum linewidths as small as 0.063 .mu.m, or even smaller. A hologram and its position are determined that will produce the desired image on the selected surface when the hologram is irradiated with X-rays from a suitably monochromatic X-ray source of a selected wavelength .lambda.. On-axis X-ray transmission through, or off-axis X-ray reflection from, a hologram may be used here, with very different requirements for monochromaticity, flux and brightness of the X-ray source. For reasonable penetration of photoresist materials by X-rays produced by the X-ray source, the wavelength X, is preferably chosen to be no more than 13.5 nm in one embodiment and more preferably is chosen in the range 1-5 nm in the other embodiment. A lower limit on linewidth is set by the linewidth of available microstructure writing devices, such as an electron beam.

  19. The cool component and the dichotomy, lateral expansion, and axial rotation of solar X-ray jets

    SciTech Connect (OSTI)

    Moore, Ronald L.; Sterling, Alphonse C.; Falconer, David A.; Robe, Dominic

    2013-06-01

    We present results from a study of 54 polar X-ray jets that were observed in coronal X-ray movies from the X-ray Telescope on Hinode and had simultaneous coverage in movies of the cooler transition region (T ? 10{sup 5} K) taken in the He II 304 band of the Atmospheric Imaging Assembly (AIA) on Solar Dynamics Observatory. These dual observations verify the standard-jet/blowout-jet dichotomy of polar X-ray jets previously found primarily from XRT movies alone. In accord with models of blowout jets and standard jets, the AIA 304 movies show a cool (T ? 10{sup 5} K) component in nearly all blowout X-ray jets and in a small minority of standard X-ray jets, obvious lateral expansion in blowout X-ray jets but none in standard X-ray jets, and obvious axial rotation in both blowout X-ray jets and standard X-ray jets. In our sample, the number of turns of axial rotation in the cool-component standard X-ray jets is typical of that in the blowout X-ray jets, suggesting that the closed bipolar magnetic field in the jet base has substantial twist not only in all blowout X-ray jets but also in many standard X-ray jets. We point out that our results for the dichotomy, lateral expansion, and axial rotation of X-ray jets add credence to published speculation that type-II spicules are miniature analogs of X-ray jets, are generated by granule-size emerging bipoles, and thereby carry enough energy to power the corona and solar wind.

  20. Soft X-ray techniques to study mesoscale magnetism

    SciTech Connect (OSTI)

    Kortright, Jeffrey B.

    2003-06-26

    Heterogeneity in magnetization (M) is ubiquitous in modern systems. Even in nominally homogeneous materials, domains or pinning centers typically mediate magnetization reversal. Fundamental lengths determining M structure include the domain wall width and the exchange stiffness length, typically in the 4-400 nm range. Chemical heterogeneity (phase separation, polycrystalline microstructure, lithographic or other patterning, etc.) with length scales from nanometers to microns is often introduced to influence magnetic properties. With 1-2 nm wavelengths {lambda}, soft x-rays in principle can resolve structure down to {lambda}/2, and are well suited to study these mesoscopic length scales [1, 2]. This article highlights recent advances in resonant soft x-ray methods to resolve lateral magnetic structure [3], and discusses some of their relative merits and limitations. Only techniques detecting x-ray photons (rather than photo-electrons) are considered [4], since they are compatible with strong applied fields to probe relatively deeply into samples. The magneto-optical (MO) effects discovered by Faraday and Kerr were observed in the x-ray range over a century later, first at ''hard'' wavelengths in diffraction experiments probing interatomic magnetic structure [5]. In the soft x-ray range, magnetic linear [6] and circular [7] dichroism spectroscopies first developed that average over lateral magnetic structure. These large resonant MO effects enable different approaches to study magnetic structure or heterogeneity that can be categorized as microscopy or scattering [1]. Direct images of magnetic structure result from photo-emission electron microscopes [4, 8] and zone-plate microscopes [9, 10]. Scattering techniques extended into the soft x-ray include familiar specular reflection that laterally averages over structure but can provide depth-resolved information, and diffuse scattering and diffraction that provide direct information about lateral magnetic structure

  1. Controlling X-rays With Light

    SciTech Connect (OSTI)

    Glover, Ernie; Hertlein, Marcus; Southworth, Steve; Allison, Tom; van Tilborg, Jeroen; Kanter, Elliot; Krassig, B.; Varma, H.; Rude, Bruce; Santra, Robin; Belkacem, Ali; Young, Linda

    2010-08-02

    Ultrafast x-ray science is an exciting frontier that promises the visualization of electronic, atomic and molecular dynamics on atomic time and length scales. A largelyunexplored area of ultrafast x-ray science is the use of light to control how x-rays interact with matter. In order to extend control concepts established for long wavelengthprobes to the x-ray regime, the optical control field must drive a coherent electronic response on a timescale comparable to femtosecond core-hole lifetimes. An intense field is required to achieve this rapid response. Here an intense optical control pulse isobserved to efficiently modulate photoelectric absorption for x-rays and to create an ultrafast transparency window. We demonstrate an application of x-ray transparencyrelevant to ultrafast x-ray sources: an all-photonic temporal cross-correlation measurement of a femtosecond x-ray pulse. The ability to control x-ray/matterinteractions with light will create new opportunities at current and next-generation x-ray light sources.

  2. THE FERMI-GBM X-RAY BURST MONITOR: THERMONUCLEAR BURSTS FROM 4U 0614+09

    SciTech Connect (OSTI)

    Linares, M.; Chakrabarty, D. [Massachusetts Institute of Technology, Kavli Institute for Astrophysics and Space Research, Cambridge, MA 02139 (United States); Connaughton, V.; Bhat, P. N.; Briggs, M. S.; Preece, R. [CSPAR and Physics Department, University of Alabama in Huntsville, Huntsville, AL 35899 (United States); Jenke, P.; Kouveliotou, C.; Wilson-Hodge, C. A. [Space Science Office, VP62, NASA/Marshall Space Flight Center, Huntsville, AL 35812 (United States); Van der Horst, A. J. [Astronomical Institute 'Anton Pannekoek', University of Amsterdam, NL-1090-GE Amsterdam (Netherlands); Camero-Arranz, A.; Finger, M.; Paciesas, W. S. [Universities Space Research Association, Huntsville, AL 35805 (United States); Beklen, E. [Physics Department, Suleyman Demirel University, 32260 Isparta (Turkey); Von Kienlin, A. [Max Planck Institute for Extraterrestrial Physics, Giessenbachstrasse, Postfach 1312, D-85748 Garching (Germany)

    2012-12-01

    Thermonuclear bursts from slowly accreting neutron stars (NSs) have proven difficult to detect, yet they are potential probes of the thermal properties of the NS interior. During the first year of a systematic all-sky search for X-ray bursts using the Gamma-ray Burst Monitor aboard the Fermi Gamma-ray Space Telescope we have detected 15 thermonuclear bursts from the NS low-mass X-ray binary 4U 0614+09 when it was accreting at nearly 1% of the Eddington limit. We measured an average burst recurrence time of 12 {+-} 3 days (68% confidence interval) between 2010 March and 2011 March, classified all bursts as normal duration bursts and placed a lower limit on the recurrence time of long/intermediate bursts of 62 days (95% confidence level). We discuss how observations of thermonuclear bursts in the hard X-ray band compare to pointed soft X-ray observations and quantify such bandpass effects on measurements of burst radiated energy and duration. We put our results for 4U 0614+09 in the context of other bursters and briefly discuss the constraints on ignition models. Interestingly, we find that the burst energies in 4U 0614+09 are on average between those of normal duration bursts and those measured in long/intermediate bursts. Such a continuous distribution in burst energy provides a new observational link between normal and long/intermediate bursts. We suggest that the apparent bimodal distribution that defined normal and long/intermediate duration bursts during the last decade could be due to an observational bias toward detecting only the longest and most energetic bursts from slowly accreting NSs.

  3. Time-resolved Soft X-Ray Imaging (SXRI) diagnostic for use at the NIF and OMEGA lasers (version 2)

    SciTech Connect (OSTI)

    Schneider, M B; Holder, J P; James, D L; Bruns, H C; Celeste, J R; Compton, S; Costa, R L; Ellis, A D; Emig, J A; Hargrove, D; Kalantar, D H; MacGowan, B J; Power, G D; Sorce, C; Rekow, V; Widmann, K; Young, B K; Young, P E; Garcia, O F; McKenney, J; Haugh, M; Goldin, F; MacNeil, L P; Cone, K

    2006-07-21

    The soft x-ray imager (SXRI) built for the first experiments at the National Ignition Facility (NIF) has four soft x-ray channels and one hard x-ray channel. The SXRI is a snout that mounts to a four strip gated imager. This produces four soft x-ray images per strip, which can be separated in time by {approx}60psec. Each soft x-ray channel consists of a mirror plus a filter. The diagnostic was used to study x-ray burnthrough of hot hohlraum targets at the NIF and OMEGA lasers. The SXRI snout design and issues involved in selecting the desired soft x-ray channels are discussed.

  4. Time-resolved Soft X-Ray Imaging (SXRI) diagnostic for use at the NIF and OMEGA lasers

    SciTech Connect (OSTI)

    Schneider, M; Holder, J; James, D; Bruns, H; Celeste, J; Compton, S; Costa, R; Ellis, A; Emig, J; Hargrove, D; Kalantar, D; MacGowan, B; Power, G; Sorce, C; Rekow, V; Widmann, K; Young, B; Young, P; Garcia, O; McKenney, J; Haugh, M; Goldin, F; MacNeil, L; Cone, K

    2006-05-04

    The soft x-ray imager (SXRI) built for the first experiments at the National Ignition Facility (NIF) has four soft x-ray channels and one hard x-ray channel. The SXRI is a snout that mounts to a four strip gated imager. This produces four soft x-ray images per strip, which can be separated in time by {approx}60psec. Each soft x-ray channel consists of a mirror plus a filter. The diagnostic was used to study x-ray burnthrough of hot hohlraum targets at the NIF and OMEGA lasers. The SXRI snout design and issues involved in selecting the desired soft x-ray channels are discussed.

  5. X-ray transmissive debris shield

    DOE Patents [OSTI]

    Spielman, Rick B.

    1994-01-01

    A composite window structure is described for transmitting x-ray radiation and for shielding radiation generated debris. In particular, separate layers of different x-ray transmissive materials are laminated together to form a high strength, x-ray transmissive debris shield which is particularly suited for use in high energy fluences. In one embodiment, the composite window comprises alternating layers of beryllium and a thermoset polymer.

  6. High speed x-ray beam chopper

    DOE Patents [OSTI]

    McPherson, Armon; Mills, Dennis M.

    2002-01-01

    A fast, economical, and compact x-ray beam chopper with a small mass and a small moment of inertia whose rotation can be synchronized and phase locked to an electronic signal from an x-ray source and be monitored by a light beam is disclosed. X-ray bursts shorter than 2.5 microseconds have been produced with a jitter time of less than 3 ns.

  7. A COMPARISON OF X-RAY AND MID-INFRARED SELECTION OF OBSCURED ACTIVE GALACTIC NUCLEI

    SciTech Connect (OSTI)

    Eckart, Megan E.; Harrison, Fiona A.; McGreer, Ian D.; Helfand, David J.; Stern, Daniel

    2010-01-01

    We compare the relative merits of active galactic nuclei (AGNs) selection at X-ray and mid-infrared wavelengths using data from moderately deep fields observed by both Chandra and Spitzer. The X-ray-selected AGN sample and associated photometric and spectroscopic optical follow-up are drawn from a subset of fields studied as part of the Serendipitous Extragalactic X-ray Source Identification (SEXSI) program. Mid-infrared data in these fields are derived from targeted and archival Spitzer imaging, and mid-infrared AGN selection is accomplished primarily through application of the Infrared Array Camera (IRAC) color-color AGN 'wedge' selection technique. Nearly all X-ray sources in these fields which exhibit clear spectroscopic signatures of AGN activity have mid-infrared colors consistent with IRAC AGN selection. These are predominantly the most luminous X-ray sources. X-ray sources that lack high-ionization and/or broad lines in their optical spectra are far less likely to be selected as AGNs by mid-infrared color selection techniques. The fraction of X-ray sources identified as AGNs in the mid-infrared increases monotonically as the X-ray luminosity increases. Conversely, only 22% of mid-infrared-selected AGNs are detected at X-ray energies in the moderately deep ((t{sub exp}) approx 100 ks) SEXSI Chandra data. We hypothesize that IRAC sources with AGN colors that lack X-ray detections are predominantly high-luminosity AGNs that are obscured and/or lie at high redshift. A stacking analysis of X-ray-undetected sources shows that objects in the mid-infrared AGN selection wedge have average X-ray fluxes in the 2-8 keV band 3 times higher than sources that fall outside the wedge. Their X-ray spectra are also harder. The hardness ratio of the wedge-selected stack is consistent with moderate intrinsic obscuration, but is not suggestive of a highly obscured, Compton-thick source population. It is evident from this comparative study that in order to create a complete

  8. X-ray laser microscope apparatus

    DOE Patents [OSTI]

    Suckewer, Szymon; DiCicco, Darrell S.; Hirschberg, Joseph G.; Meixler, Lewis D.; Sathre, Robert; Skinner, Charles H.

    1990-01-01

    A microscope consisting of an x-ray contact microscope and an optical microscope. The optical, phase contrast, microscope is used to align a target with respect to a source of soft x-rays. The source of soft x-rays preferably comprises an x-ray laser but could comprise a synchrotron or other pulse source of x-rays. Transparent resist material is used to support the target. The optical microscope is located on the opposite side of the transparent resist material from the target and is employed to align the target with respect to the anticipated soft x-ray laser beam. After alignment with the use of the optical microscope, the target is exposed to the soft x-ray laser beam. The x-ray sensitive transparent resist material whose chemical bonds are altered by the x-ray beam passing through the target mater GOVERNMENT LICENSE RIGHTS This invention was made with government support under Contract No. De-FG02-86ER13609 awarded by the Department of Energy. The Government has certain rights in this invention.

  9. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). ...

  10. Compound refractive X-ray lens

    DOE Patents [OSTI]

    Nygren, David R.; Cahn, Robert; Cederstrom, Bjorn; Danielsson, Mats; Vestlund, Jonas

    2000-01-01

    An apparatus and method for focusing X-rays. In one embodiment, his invention is a commercial-grade compound refractive X-ray lens. The commercial-grade compound refractive X-ray lens includes a volume of low-Z material. The volume of low-Z material has a first surface which is adapted to receive X-rays of commercially-applicable power emitted from a commercial-grade X-ray source. The volume of low-Z material also has a second surface from which emerge the X-rays of commercially-applicable power which were received at the first surface. Additionally, the commercial-grade compound refractive X-ray lens includes a plurality of openings which are disposed between the first surface and the second surface. The plurality of openings are oriented such that the X-rays of commercially-applicable power which are received at the first surface, pass through the volume of low-Z material and through the plurality openings. In so doing, the X-rays which emerge from the second surface are refracted to a focal point.

  11. Gamma and X-ray Dosimetric Method

    DOE Patents [OSTI]

    Taplin, G.V.; Douglas, C.H.

    1954-06-29

    This patent application concerns a highly stable two-phase liquid system for use in a colorimetric dosimeter for measuring X-ray and gamma radiation.

  12. Gamma Radiation & X-Rays

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Gamma Radiation and X-Rays 1. Gamma radiation and X-rays are electromagnetic radiation like visible light, radio waves, and ultraviolet light. These electromagnetic radiations differ only in the amount of energy they have. Gamma rays and X-rays are the most energetic of these. 2. Gamma radiation is able to travel many meters in air and many centimeters in human tissue. It readily penetrates most materials and is sometimes called "penetrating radiation." 3. X-rays are like gamma rays.

  13. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are

  14. X-ray microscopy. Beyond ensemble averages

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ice, Gene E.; Budai, John D.

    2015-06-23

    This work exemplifies emerging tools to characterize local materials structure and dynamics, made possible by powerful X-ray synchrotron and transmission electron microscopy methods.

  15. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light ...

  16. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that

  17. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that

  18. Some new schemes for producing high-accuracy elliptical X-ray mirrors by elastic bending

    SciTech Connect (OSTI)

    Padmore, H.A.; Howells, M.R.; Irick, S.; Renner, T.; Sandler, R.; Koo, Y.-M.

    1996-08-01

    Although x-ray micro-foci can be produced by a variety of diffractive methods, grazing incidence mirrors are the only route to an achromatic focus. In this paper we describe our efforts to produce elliptically shaped mirrors with the very high figure accuracy necessary for producing a micro-focus. The motivation for this work is provided by the need to produce achromatic foci for a range of applications ranging from tunable micro-focus x-ray photoelectron spectroscopy ({mu}-XPS) at soft x-ray energies to micro-focus white beam x-ray diffraction ({mu}-XRD) at hard x-ray energies. We describe the methodology of beam bending, a practical example of a system we have produced for {mu}-XRD, and results demonstrating the production of a surface with micro-radian figure accuracy.

  19. X-ray and Sunyaev-Zel'Dovich properties of the warm-hot intergalactic medium

    SciTech Connect (OSTI)

    Ursino, E.; Galeazzi, M.; Huffenberger, K.

    2014-07-01

    We use numerical simulations to predict the soft X-ray ([0.4-0.6] keV) and Sunyaev-Zel'dovich (SZ) signal (at 150 GHz) from a large-scale structure in the universe and then compute two-point statistics to study the spatial distribution and time evolution of the signals. The average X-ray signal predicted for the warm-hot intergalactic medium (WHIM) is in good agreement with observational constraints that set it at about 10% of the total diffuse X-ray background. The characteristic angle computed with the autocorrelation function is of the order of some arcminutes and becomes smaller at higher redshift. The power spectrum peak of the SZ due to the WHIM is at l ∼ 10,000 and has an amplitude of ∼0.2 μK{sup 2}, about one order of magnitude below the signal measured with telescopes like Planck, Atacama Cosmology Telescope, and South Pole Telescope. Even if the high-redshift WHIM signal is too weak to be detected using X-rays only, the small-scale correlation between X-ray and SZ maps is dominated by the high-redshift WHIM. This makes the analysis of the SZ signal in support of X-rays a promising tool to study the early time WHIM.

  20. Development of an X-ray pixel detector with multi-port charge-coupled device for X-ray free-electron laser experiments

    SciTech Connect (OSTI)

    Kameshima, Takashi; Ono, Shun; Kudo, Togo; Ozaki, Kyosuke; Kirihara, Yoichi; Kobayashi, Kazuo; Inubushi, Yuichi; Yabashi, Makina; Hatsui, Takaki; Horigome, Toshio; Holland, Andrew; Holland, Karen; Burt, David; Murao, Hajime

    2014-03-15

    This paper presents development of an X-ray pixel detector with a multi-port charge-coupled device (MPCCD) for X-ray Free-Electron laser experiments. The fabrication process of the CCD was selected based on the X-ray radiation hardness against the estimated annual dose of 1.6 × 10{sup 14} photon/mm{sup 2}. The sensor device was optimized by maximizing the full well capacity as high as 5 Me- within 50 μm square pixels while keeping the single photon detection capability for X-ray photons higher than 6 keV and a readout speed of 60 frames/s. The system development also included a detector system for the MPCCD sensor. This paper summarizes the performance, calibration methods, and operation status.

  1. Phased Contrast X-Ray Imaging

    ScienceCinema (OSTI)

    Erin Miller

    2012-12-31

    The Pacific Northwest National Laboratory is developing a range of technologies to broaden the field of explosives detection. Phased contrast X-ray imaging, which uses silicon gratings to detect distortions in the X-ray wave front, may be applicable to mail or luggage scanning for explosives; it can also be used in detecting other contraband, small-parts inspection, or materials characterization.

  2. X-ray Attenuation and Absorption Calculations.

    Energy Science and Technology Software Center (OSTI)

    1988-02-25

    This point-source, polychromatic, discrete energy X-ray transport and energy deposition code system calculates first-order spectral estimates of X-ray energy transmission through slab materials and the associated spectrum of energy absorbed by the material.

  3. Accelerator-driven X-ray Sources

    SciTech Connect (OSTI)

    Nguyen, Dinh Cong

    2015-11-09

    After an introduction which mentions x-ray tubes and storage rings and gives a brief review of special relativity, the subject is treated under the following topics and subtopics: synchrotron radiation (bending magnet radiation, wiggler radiation, undulator radiation, brightness and brilliance definition, synchrotron radiation facilities), x-ray free-electron lasers (linac-driven X-ray FEL, FEL interactions, self-amplified spontaneous emission (SASE), SASE self-seeding, fourth-generation light source facilities), and other X-ray sources (energy recovery linacs, Inverse Compton scattering, laser wakefield accelerator driven X-ray sources. In summary, accelerator-based light sources cover the entire electromagnetic spectrum. Synchrotron radiation (bending magnet, wiggler and undulator radiation) has unique properties that can be tailored to the users’ needs: bending magnet and wiggler radiation is broadband, undulator radiation has narrow spectral lines. X-ray FELs are the brightest coherent X-ray sources with high photon flux, femtosecond pulses, full transverse coherence, partial temporal coherence (SASE), and narrow spectral lines with seeding techniques. New developments in electron accelerators and radiation production can potentially lead to more compact sources of coherent X-rays.

  4. In situ X-ray Characterization of Energy Storage Materials | Stanford

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Synchrotron Radiation Lightsource X-ray Characterization of Energy Storage Materials Tuesday, July 9, 2013 - 11:00am SLAC, Conference Room 137-322 Presented by Johanna Nelson, Stanford Postdoctoral Scholar, SSRL MSD Hard X-ray Department A key factor in the global move towards clean, renewable energy is the electrification of the automobile. Current battery technology limits EV (electric vehicles) to a short travel range, slow recharge, and costly price tag. Li-ion batteries promise the high

  5. The Coherent X-ray Imaging instrument at the Linac Coherent Light Source

    SciTech Connect (OSTI)

    Liang, Mengning; Williams, Garth J.; Messerschmidt, Marc; Seibert, M. Marvin; Montanez, Paul A.; Hayes, Matt; Milathianaki, Despina; Aquila, Andrew; Hunter, Mark S.; Koglin, Jason E.; Schafer, Donald W.; Guillet, Serge; Busse, Armin; Bergan, Robert; Olson, William; Fox, Kay; Stewart, Nathaniel; Curtis, Robin; Miahnahri, Alireza Alan; Boutet, Sbastien

    2015-04-15

    The Coherent X-ray Imaging (CXI) instrument specializes in hard X-ray, in-vacuum, high power density experiments in all areas of science. Two main sample chambers, one containing a 100 nm focus and one a 1 m focus, are available, each with multiple diagnostics, sample injection, pumpprobe and detector capabilities. The flexibility of CXI has enabled it to host a diverse range of experiments, from biological to extreme matter.

  6. Versatile atomic force microscopy setup combined with micro-focused X-ray beam

    SciTech Connect (OSTI)

    Slobodskyy, T. Tholapi, R.; Liefeith, L.; Hansen, W.; Zozulya, A. V. Fester, M.; Sprung, M.

    2015-06-15

    Micro-focused X-ray beams produced by third generation synchrotron sources offer new perspective of studying strains and processes at nanoscale. Atomic force microscope setup combined with a micro-focused synchrotron beam allows precise positioning and nanomanipulation of nanostructures under illumination. In this paper, we report on integration of a portable commercial atomic force microscope setup into a hard X-ray synchrotron beamline. Details of design, sample alignment procedure, and performance of the setup are presented.

  7. The Coherent X-ray Imaging instrument at the Linac Coherent Light Source

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Liang, Mengning; Williams, Garth J.; Messerschmidt, Marc; Seibert, M. Marvin; Montanez, Paul A.; Hayes, Matt; Milathianaki, Despina; Aquila, Andrew; Hunter, Mark S.; Koglin, Jason E.; et al

    2015-04-15

    The Coherent X-ray Imaging (CXI) instrument specializes in hard X-ray, in-vacuum, high power density experiments in all areas of science. Two main sample chambers, one containing a 100 nm focus and one a 1 µm focus, are available, each with multiple diagnostics, sample injection, pump–probe and detector capabilities. The flexibility of CXI has enabled it to host a diverse range of experiments, from biological to extreme matter.

  8. Probing convex polygons with X-rays

    SciTech Connect (OSTI)

    Edelsbrunner, H.; Skiena, S.S. )

    1988-10-01

    An X-ray probe through a polygon measures the length of intersection between a line and the polygon. This paper considers the properties of various classes of X-ray probes, and shows how they interact to give finite strategies for completely describing convex n-gons. It is shown that (3n/2)+6 probes are sufficient to verify a specified n-gon, while for determining convex polygons (3n-1)/2 X-ray probes are necessary and 5n+O(1) sufficient, with 3n+O(1) sufficient given that a lower bound on the size of the smallest edge of P is known.

  9. Sandia National Laboratories: X-ray vision

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    The Sandia-developed X-Ray Toolkit, or XTK, is a specialized X-ray visualization tool to help bomb disposal squads make fast, accurate, and precise assessments of potentially dangerous devices such as pipe bombs and IEDs. The image here, captured via the XTK software package using its unique image-stitching capability, shows the inner workings of a mock IED. Facebook Twitter YouTube Flickr RSS News X-ray vision By Nancy Salem Photography By Randy Montoya Thursday, September 01, 2016 Sandia, UNM

  10. The MPI/AIT X-ray Imager (MAXI): High speed pn-CCD's for x-ray detection

    SciTech Connect (OSTI)

    Strueder, L.; Braeuninger, H.; Meier, M.; Predehl, P.; Reppin, C.; Sterzik, M.; Truemper, J. . Inst. fuer Astrophysik); Cattaneo, P.; Hauff, D.; Lutz, G.; Schuster, K.F.; Schwarz, A. . Werner-Heisenberg-Inst. fuer Physik); Kenziorra, E.; Staubert, A. (Tuebingen

    1989-06-01

    MAXI (MPI/AIT X-RAY Imager) is part of a proposal submitted to the European Space Agency (ESA) as focal plane instrumentation of the X-ray Multi Mission (XMM). Within a collaboration of 13 European institutes we have proposed a fully depleted (sensitive) pn CCD of 280 {mu}m thickness with a homogeneous sensitive area of 36 cm{sup 2} and a pixel size of 150 {times} 150 {mu}m{sup 2} which is well matched with the telescope's angular resolution of 30 arcsec, translating to a position resolution of approximately 1 mm in the focal plane. The X-ray sensitivity is higher than 90% from 250 eV up to 10 keV, the readout time in the full frame mode of the complete focal plane will be 2 ms with a readout noise of better than 5 e{sup {minus}} (rms). Prototypes of all individual components of the camera system have been fabricated and tested. The camera concept will be presented. The measured transfer properties of the CCD and the on-chip electronics will be treated. Taking into account the coupling of the on-chip amplifier to the following front-end electronics the expected performance will be derived.

  11. Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Miaja-Avila, L.; O'Neil, G. C.; Uhlig, J.; Cromer, C. L.; Dowell, M. L.; Jimenez, R.; Hoover, A. S.; Silverman, K. L.; Ullom, J. N.

    2015-03-02

    We describe a laser-driven x-ray plasma source designed for ultrafast x-ray absorption spectroscopy. The source is comprised of a 1 kHz, 20 W, femtosecond pulsed infrared laser and a water target. We present the x-ray spectra as a function of laser energy and pulse duration. Additionally, we investigate the plasma temperature and photon flux as we vary the laser energy. We obtain a 75 μm FWHM x-ray spot size, containing ~106 photons/s, by focusing the produced x-rays with a polycapillary optic. Since the acquisition of x-ray absorption spectra requires the averaging of measurements from >107 laser pulses, we also presentmore » data on the source stability, including single pulse measurements of the x-ray yield and the x-ray spectral shape. In single pulse measurements, the x-ray flux has a measured standard deviation of 8%, where the laser pointing is the main cause of variability. Further, we show that the variability in x-ray spectral shape from single pulses is low, thus justifying the combining of x-rays obtained from different laser pulses into a single spectrum. Finally, we show a static x-ray absorption spectrum of a ferrioxalate solution as detected by a microcalorimeter array. Altogether, our results demonstrate that this water-jet based plasma source is a suitable candidate for laboratory-based time-resolved x-ray absorption spectroscopy experiments.« less

  12. Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy

    SciTech Connect (OSTI)

    Miaja-Avila, L.; O'Neil, G. C.; Uhlig, J.; Cromer, C. L.; Dowell, M. L.; Jimenez, R.; Hoover, A. S.; Silverman, K. L.; Ullom, J. N.

    2015-03-02

    We describe a laser-driven x-ray plasma source designed for ultrafast x-ray absorption spectroscopy. The source is comprised of a 1 kHz, 20 W, femtosecond pulsed infrared laser and a water target. We present the x-ray spectra as a function of laser energy and pulse duration. Additionally, we investigate the plasma temperature and photon flux as we vary the laser energy. We obtain a 75 μm FWHM x-ray spot size, containing ~106 photons/s, by focusing the produced x-rays with a polycapillary optic. Since the acquisition of x-ray absorption spectra requires the averaging of measurements from >107 laser pulses, we also present data on the source stability, including single pulse measurements of the x-ray yield and the x-ray spectral shape. In single pulse measurements, the x-ray flux has a measured standard deviation of 8%, where the laser pointing is the main cause of variability. Further, we show that the variability in x-ray spectral shape from single pulses is low, thus justifying the combining of x-rays obtained from different laser pulses into a single spectrum. Finally, we show a static x-ray absorption spectrum of a ferrioxalate solution as detected by a microcalorimeter array. Altogether, our results demonstrate that this water-jet based plasma source is a suitable candidate for laboratory-based time-resolved x-ray absorption spectroscopy experiments.

  13. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light ... wavelengths relevant to atomic and molecular phenomena) with the advantages of ...

  14. X-ray grid-detector apparatus

    DOE Patents [OSTI]

    Boone, John M.; Lane, Stephen M.

    1998-01-27

    A hybrid grid-detector apparatus for x-ray systems wherein a microchannel plate structure has an air-interspaced grid portion and a phosphor/optical fluid-filled grid portion. The grids are defined by multiple adjacent channels separated by lead-glass septa. X-rays entering the air-interspaced grid portion at an angle of impingement upon the septa are attenuated, while non-impinging x-rays pass through to the phosphor/fluid filled portion. X-ray energy is converted to luminescent energy in the phosphor/fluid filled portion and the resultant beams of light are directed out of the phosphor/optical fluid filled portion to an imaging device.

  15. X-ray source for mammography

    DOE Patents [OSTI]

    Logan, C.M.

    1994-12-20

    An x-ray source is described utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms. 6 figures.

  16. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http:spie.orgOP318 August 28-29, 2013; San Diego, California, USA

  17. Small Angle X-Ray Scattering Detector

    DOE Patents [OSTI]

    Hessler, Jan P.

    2004-06-15

    A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

  18. X-rays Illuminate Ancient Archimedes Text

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ... DailyIndia.com: http:www.dailyindia.comshow48286.phpX-rays-illuminate-Archimedes-writings North Korea Times: http:story.northkoreatimes.comp.xct9ciddd8845aa60952db2id...

  19. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http://spie.org/OP318 August 28-29, 2013; San Diego, California, USA

  20. X-ray source for mammography

    DOE Patents [OSTI]

    Logan, Clinton M.

    1994-01-01

    An x-ray source utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms.

  1. X-ray image intensifier phosphor

    DOE Patents [OSTI]

    D'Silva, A.P.; Fassel, V.A.

    1975-12-01

    Y/sub 1-x/Gd/sub x/.PO$sub 4$:Tb$sup 3+$ is an effective phosphor for use in X-ray intensifier screens and in nuclear radiation detection systems.

  2. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    be reconstructed by a single Fourier transform; this is known as Fourier transform holography. The problem of getting sufficiently coherent x-rays onto and off of the sample in a...

  3. Optimization efforts in gated x-ray intensifiers (Conference...

    Office of Scientific and Technical Information (OSTI)

    Optimization efforts in gated x-ray intensifiers Citation Details In-Document Search Title: Optimization efforts in gated x-ray intensifiers Gated x-ray intensifiers are often ...

  4. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray...

  5. X-ray laser driven gold targets

    SciTech Connect (OSTI)

    Petrova, Tz. B. Whitney, K. G.; Davis, J.

    2014-03-15

    The femtosecond population dynamics of gold irradiated by a coherent high-intensity (>10{sup 17} W/cm{sup 2}) x-ray laser pulse is investigated theoretically. There are two aspects to the assembled model. One is the construction of a detailed model of platinum-like gold inclusive of all inner-shell states that are created by photoionization of atomic gold and decay either by radiative or Auger processes. Second is the computation of the population dynamics that ensues when an x-ray pulse is absorbed in gold. The hole state generation depends on the intensity and wavelength of the driving x-ray pulse. The excited state populations reached during a few femtosecond timescales are high enough to generate population inversions, whose gain coefficients are calculated. These amplified lines in the emitted x-ray spectrum provide important diagnostics of the radiation dynamics and also suggest a nonlinear way to increase the frequency of the coherent output x-ray pulses relative to the frequency of the driver input x-ray pulse.

  6. Compton backscattered collmated X-ray source

    DOE Patents [OSTI]

    Ruth, Ronald D.; Huang, Zhirong

    2000-01-01

    A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

  7. Compton backscattered collimated x-ray source

    DOE Patents [OSTI]

    Ruth, R.D.; Huang, Z.

    1998-10-20

    A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

  8. Compton backscattered collimated x-ray source

    DOE Patents [OSTI]

    Ruth, Ronald D.; Huang, Zhirong

    1998-01-01

    A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

  9. X-RAYS FROM THE POWER SOURCES OF THE CEPHEUS A STAR-FORMING REGION

    SciTech Connect (OSTI)

    Pravdo, Steven H.; Tsuboi, Yohko; Uzawa, Akiko; Ezoe, Yuichiro E-mail: tsuboi@phys.chuo-u.ac.j E-mail: ezoe@phys.metro-u.ac.j

    2009-10-20

    We report an observation of X-ray emission from the exciting region of Cepheus A with the Chandra/ACIS instrument. What had been an unresolved X-ray source comprising the putative power sources is now resolved into at least three point-like sources, each with similar X-ray properties and differing radio and submillimeter properties. The sources are HW9, HW3c, and a new source that is undetected at other wavelengths 'h10'. They each have inferred X-ray luminosities >= 10{sup 31} erg s{sup -1} with hard spectra, T >= 10{sup 7} K, and high low-energy absorption equivalent to tens to as much as a hundred magnitudes of visual absorption. The star usually assumed to be the most massive and energetic, HW2, is not detected with an upper limit about seven times lower than the detections. The X-rays may arise via thermal bremsstrahlung in diffuse emission regions associated with a gyrosynchrotron source for the radio emission, or they could arise from powerful stellar winds. We also analyzed the Spitzer/IRAC mid-IR observation from this star formation region and present the X-ray results and mid-IR classifications of the nearby stars. HH 168 is not as underluminous in X-rays as previously reported.

  10. SIMULTANEOUS X-RAY AND ULTRAVIOLET OBSERVATIONS OF THE SW SEXTANTIS STAR DW URSAE MAJORIS

    SciTech Connect (OSTI)

    Hoard, D. W.; Wachter, S.; Lu, Ting-Ni; Knigge, Christian; Homer, Lee; Szkody, Paula; Still, M.; Long, Knox S.; Dhillon, V. S.

    2010-11-15

    We present the first pointed X-ray observation of DW Ursae Majoris, a novalike cataclysmic variable (CV) and one of the archetype members of the SW Sextantis class, obtained with the XMM-Newton satellite. These data provide the first detailed look at an SW Sex star in the X-ray regime (with previous X-ray knowledge of the SW Sex stars limited primarily to weak or non-detections in the ROSAT All Sky Survey). It is also one of only a few XMM-Newton observations (to date) of any high mass transfer rate novalike CV, and the only one in the evolutionarily important 3-4 hr orbital period range. The observed X-ray spectrum of DW UMa is very soft, with {approx}95% of the detected X-ray photons at energies <2 keV. The spectrum can be fit equally well by a one-component cooling flow model, with a temperature range of 0.2-3.5 keV, or a two-component, two-temperature thermal plasma model, containing hard ({approx}5-6 keV) and soft ({approx}0.8 keV) components. The X-ray light curve of DW UMa shows a likely partial eclipse, implying X-ray reprocessing in a vertically extended region, and an orbital modulation, implying a structural asymmetry in the X-ray reprocessing site (e.g., it cannot be a uniform corona). We also obtained a simultaneous near-ultraviolet light curve of DW UMa using the Optical Monitor on XMM-Newton. This light curve is similar in appearance to published optical-UV light curves of DW UMa and shows a prominent deep eclipse. Regardless of the exact nature of the X-ray reprocessing site in DW UMa, the lack of a prominent hard X-ray total eclipse and very low fraction of high energy X-rays point to the presence of an optically and geometrically thick accretion disk that obscures the boundary layer and modifies the X-ray spectrum emitted near the white dwarf.

  11. A broadband X-ray study of the Geminga pulsar with NuSTAR And XMM-Newton

    SciTech Connect (OSTI)

    Mori, Kaya; Gotthelf, Eric V.; Halpern, Jules P.; Beloborodov, Andrei M.; Hailey, Charles J.; Dufour, Francois; Kaspi, Victoria M.; An, Hongjun; Bachetti, Matteo; Boggs, Steven E.; Craig, William W.; Christensen, Finn E.; Harrison, Fiona A.; Kouveliotou, Chryssa; Pivovaroff, Michael J.; Stern, Daniel; Zhang, William W.

    2014-10-01

    We report on the first hard X-ray detection of the Geminga pulsar above 10 keV using a 150 ks observation with the Nuclear Spectroscopic Telescope Array (NuSTAR) observatory. The double-peaked pulse profile of non-thermal emission seen in the soft X-ray band persists at higher energies. Broadband phase-integrated spectra over the 0.2-20 keV band with NuSTAR and archival XMM-Newton data do not fit to a conventional two-component model of a blackbody plus power law, but instead exhibit spectral hardening above ∼5 keV. We find that two spectral models fit the data well: (1) a blackbody (kT {sub 1} ∼ 42 eV) with a broken power law (Γ{sub 1} ∼ 2.0, Γ{sub 2} ∼ 1.4 and E {sub break} ∼ 3.4 keV) and (2) two blackbody components (kT {sub 1} ∼ 44 eV and kT {sub 2} ∼ 195 eV) with a power-law component (Γ ∼ 1.7). In both cases, the extrapolation of the Rayleigh-Jeans tail of the thermal component is consistent with the UV data, while the non-thermal component overpredicts the near-infrared data, requiring a spectral flattening at E ∼ 0.05-0.5 keV. While strong phase variation of the power-law index is present below ∼5 keV, our phase-resolved spectroscopy with NuSTAR indicates that another hard non-thermal component with Γ ∼ 1.3 emerges above ∼5 keV. The spectral hardening in non-thermal X-ray emission as well as spectral flattening between the optical and X-ray bands argue against the conjecture that a single power law may account for multi-wavelength non-thermal spectra of middle-aged pulsars.

  12. In situ laser heating and radial synchrotron x-ray diffraction in a diamond anvil cell

    SciTech Connect (OSTI)

    Kunz, Martin; Caldwell, Wendel A.; Miyagi, Lowell; Wenk, Hans-Rudolf

    2007-06-15

    We report a first combination of diamond anvil cell radial x-ray diffraction with in situ laser heating. The laser-heating setup of ALS beamline 12.2.2 was modified to allow one-sided heating of a sample in a diamond anvil cell with an 80 W yttrium lithium fluoride laser while probing the sample with radial x-ray diffraction. The diamond anvil cell is placed with its compressional axis vertical, and perpendicular to the beam. The laser beam is focused onto the sample from the top while the sample is probed with hard x-rays through an x-ray transparent boron-epoxy gasket. The temperature response of preferred orientation of (Fe,Mg)O is probed as a test experiment. Recrystallization was observed above 1500 K, accompanied by a decrease in stress.

  13. X-Ray Microcomputed Tomography for the Durability Characterization...

    Office of Scientific and Technical Information (OSTI)

    Conference: X-Ray Microcomputed Tomography for the Durability Characterization of Limestone Aggregate Citation Details In-Document Search Title: X-Ray Microcomputed Tomography for...

  14. Integrated X-ray Reflectivity Measurements for Elliptically Curved...

    Office of Scientific and Technical Information (OSTI)

    Title: Integrated X-ray Reflectivity Measurements for Elliptically Curved PET Crystals The elliptically curved pentaerythritol (PET) crystals used in the Supersnout 2 X-ray ...

  15. Simultaneous cryo X-ray ptychographic and fluorescence microscopy...

    Office of Scientific and Technical Information (OSTI)

    Accepted Manuscript: Simultaneous cryo X-ray ptychographic and fluorescence microscopy of green algae Prev Next Title: Simultaneous cryo X-ray ptychographic and fluorescence ...

  16. A Spatially Resolving X-ray Crystal Spectrometer for Measurement...

    Office of Scientific and Technical Information (OSTI)

    394 PPPL- 4394 A Spatially Resolving X-ray Crystal Spectrometer for Measurement of ... Fusion Links A spatially resolving x-ray crystal spectrometer for measurement of ...

  17. Development of a Spatially Resolving X-Ray Crystal Spectrometer...

    Office of Scientific and Technical Information (OSTI)

    Development of a Spatially Resolving X-Ray Crystal Spectrometer For Measurement of ... Links Development of a spatially resolving x-ray crystal spectrometer for measurement of ...

  18. Development Of a Spatially Resolving X-ray Crystal Spectrometer...

    Office of Scientific and Technical Information (OSTI)

    Technical Report: Development Of a Spatially Resolving X-ray Crystal Spectrometer For ... Title: Development Of a Spatially Resolving X-ray Crystal Spectrometer For Measurement Of ...

  19. Integrated X-Ray Reflectivity Measurements for Elliptically Curved...

    Office of Scientific and Technical Information (OSTI)

    Integrated X-Ray Reflectivity Measurements for Elliptically Curved PET Crystals Citation Details In-Document Search Title: Integrated X-Ray Reflectivity Measurements for ...

  20. X-ray transient absorption and picosecond IR spectroscopy of...

    Office of Scientific and Technical Information (OSTI)

    X-ray transient absorption and picosecond IR spectroscopy of fulvalene(tetracarbonyl)diruthenium on photoexcitation Citation Details In-Document Search Title: X-ray transient ...

  1. Category:X-Ray Diffraction (XRD) | Open Energy Information

    Open Energy Info (EERE)

    X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Geothermalpower.jpg Looking for the X-Ray Diffraction (XRD) page? For detailed information on...

  2. Direct synchrotron x-ray measurements of local strain fields...

    Office of Scientific and Technical Information (OSTI)

    Accepted Manuscript: Direct synchrotron x-ray measurements of local strain fields in ... September 3, 2016 Title: Direct synchrotron x-ray measurements of local strain fields in ...

  3. Generation of Coherent X-Ray Radiation through Modulation Compression...

    Office of Scientific and Technical Information (OSTI)

    Generation of Coherent X-Ray Radiation through Modulation Compression Citation Details In-Document Search Title: Generation of Coherent X-Ray Radiation through Modulation Compression ...

  4. Experimental X-ray characterization of Gekko XII laser propagation...

    Office of Scientific and Technical Information (OSTI)

    Experimental X-ray characterization of Gekko XII laser propagation through very low ... Citation Details In-Document Search Title: Experimental X-ray characterization of Gekko ...

  5. Experimental X-ray characterization of Gekko XII laser propagation...

    Office of Scientific and Technical Information (OSTI)

    Experimental X-ray characterization of Gekko XII laser propagation through very low ... Title: Experimental X-ray characterization of Gekko XII laser propagation through very low ...

  6. Transient x-ray diffraction and its application to materials science and x-ray optics

    SciTech Connect (OSTI)

    Hauer, A.A.; Kopp, R.; Cobble, J.; Kyrala, G.; Springer, R.

    1997-12-01

    Time resolved x-ray diffraction and scattering have been applied to the measurement of a wide variety of physical phenomena from chemical reactions to shock wave physics. Interest in this method has heightened in recent years with the advent of versatile, high power, pulsed x-ray sources utilizing laser plasmas, electron beams and other methods. In this article, we will describe some of the fundamentals involved in time resolved x-ray diffraction, review some of the history of its development, and describe some recent progress in the field. In this article we will emphasize the use of laser-plasmas as the x-ray source for transient diffraction.

  7. Hard x-ray nanotomography of amorphous aluminosilicate cements.

    SciTech Connect (OSTI)

    Provis, J. L.; Rose, V.; Winarski, R. P.; van Deventer, J. S. J.

    2011-08-01

    Nanotomographic reconstruction of a sample of low-CO{sub 2} 'geopolymer' cement provides the first three-dimensional view of the pore structure of the aluminosilicate geopolymer gel, as well as evidence for direct binding of geopolymer gel onto unreacted fly ash precursor particles. This is central to understanding and optimizing the durability of concretes made using this new class of binder, and demonstrates the value of nanotomography in providing a three-dimensional view of nanoporous inorganic materials.

  8. X-ray technology behind NASA's black-hole hunter (NuSTAR)

    ScienceCinema (OSTI)

    Craig, Bill

    2014-05-22

    Livermore Lab astrophysicist Bill Craig describes his team's role in developing X-ray imaging technology for the NASA Nuclear Spectroscopic Telescope Array (NuSTAR) mission. The black-hole-hunting spacecraft bagged its first 10 supermassive black holes this week

  9. X-ray technology behind NASA's black-hole hunter (NuSTAR)

    SciTech Connect (OSTI)

    Craig, Bill

    2013-09-10

    Livermore Lab astrophysicist Bill Craig describes his team's role in developing X-ray imaging technology for the NASA Nuclear Spectroscopic Telescope Array (NuSTAR) mission. The black-hole-hunting spacecraft bagged its first 10 supermassive black holes this week

  10. X-ray lithography using holographic images

    DOE Patents [OSTI]

    Howells, M.S.; Jacobsen, C.

    1997-03-18

    Methods for forming X-ray images having 0.25 {micro}m minimum line widths on X-ray sensitive material are presented. A holographic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required. 15 figs.