National Library of Energy BETA

Sample records for group x-ray science

  1. X-Ray Science Education

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    TV Network external link DNA Interactive external link Reciprocal Net external link X-ray Science Courses and Programs Various educational efforts are closely related to the...

  2. X-ray Science Division (XSD) | Advanced Photon Source

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    XSD Groups XSD Safety and Training XSD Strategic Plan XSD Visitor Program XSD Intranet X-ray Science Division (XSD) XSD enables world-class research using x-rays by developing...

  3. Transient x-ray diffraction and its application to materials science and x-ray optics

    SciTech Connect (OSTI)

    Hauer, A.A.; Kopp, R.; Cobble, J.; Kyrala, G.; Springer, R.

    1997-12-01

    Time resolved x-ray diffraction and scattering have been applied to the measurement of a wide variety of physical phenomena from chemical reactions to shock wave physics. Interest in this method has heightened in recent years with the advent of versatile, high power, pulsed x-ray sources utilizing laser plasmas, electron beams and other methods. In this article, we will describe some of the fundamentals involved in time resolved x-ray diffraction, review some of the history of its development, and describe some recent progress in the field. In this article we will emphasize the use of laser-plasmas as the x-ray source for transient diffraction.

  4. X-ray Science Division: Mission and Goals | Advanced Photon Source

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Science Division (XSD) Search Button About Welcome Overview Visiting the APS Mission & Goals Find People Organization Charts Committees Job Openings User Information...

  5. Science Driver Requirements for Seeded Soft X-ray Free Electron...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Science Driver Requirements for Seeded Soft X-ray Free Electron Lasers Wednesday, December 2, 2015 - 2:00pm SLAC, Redtail Hawk Conference Room 108A Speaker: Fulvio Parmigiani,...

  6. X-Ray Light Sources | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    X-Ray Light Sources Scientific User Facilities (SUF) Division SUF Home About User Facilities X-Ray Light Sources Advanced Light Source (ALS) Advanced Photon Source (APS) Linac Coherent Light Source (LCLS) National Synchrotron Light Source II (NSLS-II) Stanford Synchrotron Radiation Light Source (SSRL) Neutron Scattering Facilities Nanoscale Science Research Centers (NSRCs) Projects Accelerator & Detector Research Science Highlights Principal Investigators' Meetings BES Home User Facilities

  7. X-Ray Microscopy and Imaging: Science and Research

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    fields: Biology and Life Sciences Environmental Sciences Materials Science Nanoscience Optics and Fundamental Physics Our research often employs the following techniques: Coherent...

  8. Workshop: Time Resolved X-Ray Science at High Repetition Rate | Stanford

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Synchrotron Radiation Lightsource Time Resolved X-Ray Science at High Repetition Rate Saturday, October 22, 2011 - 8:30am SSRL Conference Room 137-322 In conjunction with the 2011 LCLS/SSRL User Meeting, SSRL and the APS will jointly host a two-day workshop focused on opportunities with short-pulse, high-repetition rate X-ray Science. The workshop will feature international speakers and panel experts presenting the scientific basis, preliminary results and future potential of high rep-rate

  9. Soft x-ray spectromicroscopy development for materials science at the Advanced Light Source

    SciTech Connect (OSTI)

    Warwick, T.; Padmore, H.; Ade, H.; Hitchcock, A.P.; Rightor, E.G.; Tonner, B.P.

    1996-08-01

    Several third generation synchrotron radiation facilities are now operational and the high brightness of these photon sources offers new opportunities for x-ray microscopy. Well developed synchrotron radiation spectroscopy techniques are being applied in new instruments capable of imaging the surface of a material with a spatial resolution smaller than one micron. There are two aspects to this. One is to further the field of surface science by exploring the effects of spatial variations across a surface on a scale not previously accessible to x-ray measurements. The other is to open up new analytical techniques in materials science using x-rays, on a spatial scale comparable to that of the processes or devices to be studied. The development of the spectromicroscopy program at the Advanced Light Source will employ a variety of instruments, some are already operational. Their development and use will be discussed, and recent results will be presented to illustrate their capabilities.

  10. GALAXIES IN X-RAY GROUPS. II. A WEAK LENSING STUDY OF HALO CENTERING

    SciTech Connect (OSTI)

    George, Matthew R.; Ma, Chung-Pei; Leauthaud, Alexie; Bundy, Kevin; Finoguenov, Alexis; Rykoff, Eli S.; Tinker, Jeremy L.; Wechsler, Risa H.; Massey, Richard; Mei, Simona

    2012-09-20

    Locating the centers of dark matter halos is critical for understanding the mass profiles of halos, as well as the formation and evolution of the massive galaxies that they host. The task is observationally challenging because we cannot observe halos directly, and tracers such as bright galaxies or X-ray emission from hot plasma are imperfect. In this paper, we quantify the consequences of miscentering on the weak lensing signal from a sample of 129 X-ray-selected galaxy groups in the COSMOS field with redshifts 0 < z < 1 and halo masses in the range 10{sup 13}-10{sup 14} M{sub Sun }. By measuring the stacked lensing signal around eight different candidate centers (such as the brightest member galaxy, the mean position of all member galaxies, or the X-ray centroid), we determine which candidates best trace the center of mass in halos. In this sample of groups, we find that massive galaxies near the X-ray centroids trace the center of mass to {approx}< 75 kpc, while the X-ray position and centroids based on the mean position of member galaxies have larger offsets primarily due to the statistical uncertainties in their positions (typically {approx}50-150 kpc). Approximately 30% of groups in our sample have ambiguous centers with multiple bright or massive galaxies, and some of these groups show disturbed mass profiles that are not well fit by standard models, suggesting that they are merging systems. We find that halo mass estimates from stacked weak lensing can be biased low by 5%-30% if inaccurate centers are used and the issue of miscentering is not addressed.

  11. Workshops on Science Enabled by a Coherent, CW, Synchrotron X-ray Source, June 2011

    SciTech Connect (OSTI)

    Brock, Joel

    2012-01-03

    In June of 2011 we held six two-day workshops called "XDL-2011: Science at the Hard X-ray Diffraction Limit". The six workshops covered (1) Diffraction-based imaging techniques, (2) Biomolecular structure from non-crystalline materials, (3) Ultra-fast science, (4) High-pressure science, (5) Materials research with nano-beams and (6) X-ray photon correlation spectroscopy (XPCS), In each workshop, invited speaker from around the world presented examples of novel experiments that require a CW, diffraction-limited source. During the workshop, each invited speaker provided a one-page description of the experiment and an illustrative graphic. The experiments identified by the workshops demonstrate the broad and deep scientific case for a CW coherent synchrotron x-ray source. The next step is to perform detailed simulations of the best of these ideas to test them quantitatively and to guide detailed x-ray beam-line designs. These designs are the first step toward developing detailed facility designs and cost estimates.

  12. X-Ray Microscopy | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Microscopy X-Ray Microscopy This group exploits the unique capabilities of hard X-ray microscopy to visualize and understand the structure and behavior of hybrid, energy-related, and tailored nanomaterials The Hard X-Ray Nanoprobe, located at Sector 26 of the Advanced Photon Source (APS) and operated by our group and APS, is the only dedicated X-ray microscopy beamline within the portfolios of the nation's Nanoscale Science Research Centers. Our scientific program seeks to understand

  13. Sector 3 : High Resolution X-ray Scattering | Advanced Photon...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    & workshops IXN Group Useful Links Current APS status ESAF System GUP System X-Ray Science Division My APS Portal Sector 3 : High Resolution X-ray Scattering Sector 3 is...

  14. The life science X-ray scattering beamline at NSLS-II

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    DiFabio, Jonathan; Yang, Lin; Chodankar, Shirish; Pjerov, Sal; Jakoncic, Jean; Lucas, Michael; Krywka, Christina; Graziano, Vito

    2015-09-30

    We report the current development status of the High Brightness X-ray Scattering for Life Sciences (or Life Science X-ray Scattering, LiX) beamline at the NSLS-II facility of Brookhaven National Laboratory. This instrument will operate in the x-ray energy range of 2.1-18 keV, provide variable beam sizes from 1 micron to ~0.5 mm, and support user experiments in three scientific areas: (1) high-throughput solution scattering, in-line size exclusion chromatography and flow mixers-based time-resolved solution scattering of biological macro-molecules, (2) diffraction from single- and multi-layered lipid membranes, and (3) scattering-based scanning probe imaging of biological tissues. In order to satisfy the beammore » stability required for these experiments and to switch rapidly between different types of experiments, we have adopted a secondary source with refractive lenses for secondary focusing, a detector system consisting of three Pilatus detectors, and specialized experimental modules that can be quickly exchanged and each dedicated to a defined set of experiments. The construction of this beamline is on schedule for completion in September 2015. User experiments are expected to start in Spring 2016.« less

  15. The Soft X-Ray Cosmos: ROSAT Science Symposium and Data Analysis Workshop

    SciTech Connect (OSTI)

    Schlegel, E.M.

    1994-12-31

    These proceedings represent papers presented at the ROSAT Science Symposium and Data Analysis Workshop held in College Park, Maryland. The aim was to showcase the results obtained thus far using ROSAT, the Roentgen Satellite, and to provide a forum for discussion regarding the means for extracting the maximum amount of information from ROSAT data. The cosmic x-ray sources discussed, included the cataclysmic variables, the Algol binary systems, the dark matter, galactic clusters, blazars, and many others. Star formation by galaxy interactions was also discussed. There were ninety one papers presented at the conference and none of these have been abstracted for the Energy Science and Technology database. (AIP)

  16. X-ray-selected galaxy groups in Boötes

    SciTech Connect (OSTI)

    Vajgel, Bruna; Lopes, Paulo A. A.; Jones, Christine; Forman, William R.; Murray, Stephen S.; Goulding, Andrew; Andrade-Santos, Felipe

    2014-10-10

    We present the X-ray and optical properties of the galaxy groups selected in the Chandra X-Boötes survey. We used follow-up Chandra observations to better define the group sample and their X-ray properties. Group redshifts were measured from the AGN and Galaxy Evolution Survey spectroscopic data. We used photometric data from the NOAO Deep Wide Field Survey to estimate the group richness (N {sub gals}) and the optical luminosity (L {sub opt}). Our final sample comprises 32 systems at z < 1.75 with 14 below z = 0.35. For these 14 systems, we estimate velocity dispersions (σ {sub gr}) and perform a virial analysis to obtain the radii (R {sub 200} and R {sub 500}) and total masses (M {sub 200} and M {sub 500}) for groups with at least 5 galaxy members. We use the Chandra X-ray observations to derive the X-ray luminosity (L{sub X} ). We examine the performance of the group properties σ{sub gr}, L {sub opt}, and L{sub X} , as proxies for the group mass. Understanding how well these observables measure the total mass is important to estimate how precisely the cluster/group mass function is determined. Exploring the scaling relations built with the X-Boötes sample and comparing these with samples from the literature, we find a break in the L{sub X} -M {sub 500} relation at approximately M {sub 500} = 5 × 10{sup 13} M {sub ☉} (for M {sub 500} > 5 × 10{sup 13} M {sub ☉}, M{sub 500}∝L{sub X}{sup 0.61±0.02}, while for M {sub 500} ≤ 5 × 10{sup 13} M {sub ☉}, M{sub 500}∝L{sub X}{sup 0.44±0.05}). Thus, the mass-luminosity relation for galaxy groups cannot be described by the same power law as galaxy clusters. A possible explanation for this break is the dynamical friction, tidal interactions, and projection effects that reduce the velocity dispersion values of the galaxy groups. By extending the cluster luminosity function to the group regime, we predict the number of groups that new X-ray surveys, particularly eROSITA, will detect. Based on our cluster/group

  17. The active galactic nucleus population in X-ray-selected galaxy groups at 0.5 < Z < 1.1

    SciTech Connect (OSTI)

    Oh, Semyeong; Woo, Jong-Hak; Matsuoka, Kenta; Mulchaey, John S.; Finoguenov, Alexis; Tanaka, Masayuki; Cooper, Michael C.; Ziparo, Felicia; Bauer, Franz E.

    2014-07-20

    We use Chandra data to study the incidence and properties of active galactic nuclei (AGNs) in 16 intermediate redshift (0.5 < z < 1.1) X-ray-selected galaxy groups in the Chandra Deep Field-South. We measure an AGN fraction of f(L{sub X,H}>10{sup 42};M{sub R}<−20)=8.0{sub −2.3}{sup +3.0}% at z-bar ∼0.74, approximately a factor of two higher than the AGN fraction found for rich clusters at comparable redshift. This extends the trend found at low redshift for groups to have higher AGN fractions than clusters. Our estimate of the AGN fraction is also more than a factor of three higher than that of low redshift X-ray-selected groups. Using optical spectra from various surveys, we also constrain the properties of emission-line selected AGNs in these groups. In contrast to the large population of X-ray AGNs (N(L{sub X,{sub H}} > 10{sup 41} erg s{sup –1}) = 25), we find only four emission-line AGNs, three of which are also X-ray bright. Furthermore, most of the X-ray AGNs in our groups are optically dull (i.e., lack strong emission-lines), similar to those found in low redshift X-ray groups and clusters of galaxies. This contrasts with the AGN population found in low redshift optically selected groups which are dominated by emission-line AGNs. The differences between the optically and X-ray-selected AGNs populations in groups are consistent with a scenario where most AGNs in the densest environments are currently in a low accretion state.

  18. Galaxies in x-ray selected clusters and groups in Dark Energy Survey data. I. Stellar mass growth of bright central galaxies since z ~ 1.2

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Zhang, Y.; Miller, C.; McKay, T.; Rooney, P.; Evrard, A. E.; Romer, A. K.; R. Perfecto; Song, J.; Desai, S.; Mohr, J.; et al

    2016-01-14

    Here, using the science verification data of the Dark Energy Survey for a new sample of 106 X-ray selected clusters and groups, we study the stellar mass growth of bright central galaxies (BCGs) since redshift z ~ 1.2. Compared with the expectation in a semi-analytical model applied to the Millennium Simulation, the observed BCGs become under-massive/under-luminous with decreasing redshift.

  19. X-Ray Light Sources | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    The APS is one of only four third-generation, hard x-ray synchrotron radiation light ... Stanford Synchrotron Radiation Light Source (SSRL) at SLAC National Accelerator Laboratory ...

  20. GALAXIES IN X-RAY GROUPS. III. SATELLITE COLOR AND MORPHOLOGY TRANSFORMATIONS

    SciTech Connect (OSTI)

    George, Matthew R.; Ma, Chung-Pei; Bundy, Kevin; Leauthaud, Alexie; Vulcani, Benedetta; Tinker, Jeremy; Wechsler, Risa H.; Finoguenov, Alexis

    2013-06-20

    While the star formation rates and morphologies of galaxies have long been known to correlate with their local environment, the process by which these correlations are generated is not well understood. Galaxy groups are thought to play an important role in shaping the physical properties of galaxies before entering massive clusters at low redshift, and transformations of satellite galaxies likely dominate the buildup of local environmental correlations. To illuminate the physical processes that shape galaxy evolution in dense environments, we study a sample of 116 X-ray selected galaxy groups at z = 0.2-1 with halo masses of 10{sup 13}-10{sup 14} M{sub Sun} and centroids determined with weak lensing. We analyze morphologies based on Hubble Space Telescope imaging and colors determined from 31 photometric bands for a stellar mass-limited population of 923 satellite galaxies and a comparison sample of 16,644 field galaxies. Controlling for variations in stellar mass across environments, we find significant trends in the colors and morphologies of satellite galaxies with group-centric distance and across cosmic time. Specifically at low stellar mass (log (M{sub *}/M{sub Sun }) = 9.8-10.3), the fraction of disk-dominated star-forming galaxies declines from >50% among field galaxies to <20% among satellites near the centers of groups. This decline is accompanied by a rise in quenched galaxies with intermediate bulge+disk morphologies, and only a weak increase in red bulge-dominated systems. These results show that both color and morphology are influenced by a galaxy's location within a group halo. We suggest that strangulation and disk fading alone are insufficient to explain the observed morphological dependence on environment, and that galaxy mergers or close tidal encounters must play a role in building up the population of quenched galaxies with bulges seen in dense environments at low redshift.

  1. Archimedes' Oldest Writings Under X-ray vision (BNL Women in Science Lecture Series)

    SciTech Connect (OSTI)

    Bergmann, Uwe

    2009-05-20

    Large parts of Archimedes’ writings were recently deciphered at the Stanford Synchrotron Radiation Lightsource at SLAC. A special x-ray technique showed maps of iron in faint traces of partially erased ink. The x-ray images revealed Archimedes’ writings from some of his most important works that were hidden by twelfth-century biblical texts, mold and forged gold paintings.

  2. SSRL School 2007 on Hard X-ray Scattering Techniques in MES

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    May 15-17, 2007 SSRL School on Hard X-ray Scattering Techniques in Materials and Environmental Sciences Group photo taken at the SSRL School on Hard X-ray Scattering Techniques in...

  3. Molecular gas in the x-ray bright group NGC 5044 as revealed by ALMA

    SciTech Connect (OSTI)

    David, Laurence P.; Forman, William; Vrtilek, Jan; Jones, Christine; O'Sullivan, Ewan; Lim, Jeremy; Combes, Francoise; Salome, Philippe; Edge, Alastair; Hamer, Stephen; Sun, Ming; Gastaldello, Fabio; Bardelli, Sandro; Temi, Pasquale; Ohyama, Youichi; Mathews, William; Giacintucci, Simona; Trung, Dinh-V

    2014-09-10

    An ALMA observation of the early-type galaxy NGC 5044, which resides at the center of an X-ray bright group with a moderate cooling flow, detected 24 molecular structures within the central 2.5 kpc. The masses of the molecular structures vary from 3 × 10{sup 5} M {sub ☉} to 10{sup 7} M {sub ☉} and the CO(2-1) linewidths vary from 15 to 65 km s{sup –1}. Given the large CO(2-1) linewidths, the observed structures are likely giant molecular associations (GMAs) and not individual giant molecular clouds (GMCs). Only a few of the GMAs are spatially resolved and the average density of these GMAs yields a GMC volume filling factor of about 15%. The masses of the resolved GMAs are insufficient for them to be gravitationally bound, however, the most massive GMA does contain a less massive component with a linewidth of 5.5 km s{sup –1} (typical of an individual virialized GMC). We also show that the GMAs cannot be pressure confined by the hot gas. Given the CO(2-1) linewidths of the GMAs (i.e., the velocity dispersion of the embedded GMCs) they should disperse on a timescale of about 12 Myr. No disk-like molecular structures are detected and all indications suggest that the molecular gas follows ballistic trajectories after condensing out of the thermally unstable hot gas. The 230 GHz luminosity of the central continuum source is 500 times greater than its low frequency radio luminosity and probably reflects a recent accretion event. The spectrum of the central continuum source also exhibits an absorption feature with a linewidth typical of an individual GMC and an infalling velocity of 250 km s{sup –1}.

  4. X Ray Scattering | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    Research Areas X Ray Scattering Print Text Size: A A A FeedbackShare Page This activity ... matter to achieve an understanding of atomic, electronic, and magnetic structures and ...

  5. GALAXIES IN X-RAY GROUPS. I. ROBUST MEMBERSHIP ASSIGNMENT AND THE IMPACT OF GROUP ENVIRONMENTS ON QUENCHING

    SciTech Connect (OSTI)

    George, Matthew R.; Bundy, Kevin; Leauthaud, Alexie; Finoguenov, Alexis; Tinker, Jeremy; Lin, Yen-Ting; Mei, Simona; Kneib, Jean-Paul; Ilbert, Olivier; Aussel, Herve; Le Floc'h, Emeric; Behroozi, Peter S.; Busha, Michael T.; Capak, Peter; Coccato, Lodovico; Covone, Giovanni; Faure, Cecile; Fiorenza, Stephanie L.; and others

    2011-12-01

    Understanding the mechanisms that lead dense environments to host galaxies with redder colors, more spheroidal morphologies, and lower star formation rates than field populations remains an important problem. As most candidate processes ultimately depend on host halo mass, accurate characterizations of the local environment, ideally tied to halo mass estimates and spanning a range in halo mass and redshift, are needed. In this work, we present and test a rigorous, probabilistic method for assigning galaxies to groups based on precise photometric redshifts and X-ray-selected groups drawn from the COSMOS field. The groups have masses in the range 10{sup 13} {approx}< M{sub 200c}/M{sub Sun} {approx}< 10{sup 14} and span redshifts 0 < z < 1. We characterize our selection algorithm via tests on spectroscopic subsamples, including new data obtained at the Very Large Telescope, and by applying our method to detailed mock catalogs. We find that our group member galaxy sample has a purity of 84% and completeness of 92% within 0.5 R{sub 200c}. We measure the impact of uncertainties in redshifts and group centering on the quality of the member selection with simulations based on current data as well as future imaging and spectroscopic surveys. As a first application of our new group member catalog which will be made publicly available, we show that member galaxies exhibit a higher quenched fraction compared to the field at fixed stellar mass out to z {approx} 1, indicating a significant relationship between star formation and environment at group scales. We also address the suggestion that dusty star-forming galaxies in such groups may impact the high-l power spectrum of the cosmic microwave background and find that such a population cannot explain the low power seen in recent Sunyaev-Zel'dovich measurements.

  6. SSRL School on Synchrotron X-ray Spectroscopy Techniques in Environmen...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Transportation Tourism & Dining SSRL School on Synchrotron X-ray Spectroscopy Techniques in Environmental and Materials Sciences: Theory and Application June 2-5, 2009 Group...

  7. Some like it hot: Linking diffuse X-ray luminosity, baryonic mass, and star formation rate in compact groups of galaxies

    SciTech Connect (OSTI)

    Desjardins, Tyler D.; Gallagher, Sarah C.; Hornschemeier, Ann E.; Tzanavaris, Panayiotis; Walker, Lisa May; Johnson, Kelsey E.; Brandt, William N.; Charlton, Jane C.

    2014-08-01

    We present an analysis of the diffuse X-ray emission in 19 compact groups (CGs) of galaxies observed with Chandra. The hottest, most X-ray luminous CGs agree well with the galaxy cluster X-ray scaling relations in L{sub X} -T and L{sub X} -σ, even in CGs where the hot gas is associated with only the brightest galaxy. Using Spitzer photometry, we compute stellar masses and classify Hickson CGs 19, 22, 40, and 42, and RSCGs 32, 44, and 86 as fossil groups using a new definition for fossil systems that includes a broader range of masses. We find that CGs with total stellar and H I masses ≳ 10{sup 11.3} M{sub ☉} are often X-ray luminous, while lower-mass CGs only sometimes exhibit faint, localized X-ray emission. Additionally, we compare the diffuse X-ray luminosity against both the total UV and 24 μm star formation rates of each CG and optical colors of the most massive galaxy in each of the CGs. The most X-ray luminous CGs have the lowest star formation rates, likely because there is no cold gas available for star formation, either because the majority of the baryons in these CGs are in stars or the X-ray halo, or due to gas stripping from the galaxies in CGs with hot halos. Finally, the optical colors that trace recent star formation histories of the most massive group galaxies do not correlate with the X-ray luminosities of the CGs, indicating that perhaps the current state of the X-ray halos is independent of the recent history of stellar mass assembly in the most massive galaxies.

  8. Toward Control of Matter: Basic Energy Science Needs for a New Class of X-Ray Light Sources

    SciTech Connect (OSTI)

    Arenholz, Elke; Belkacem, Ali; Cocke, Lew; Corlett, John; Falcone, Roger; Fischer, Peter; Fleming, Graham; Gessner, Oliver; Hasan, M. Zahid; Hussain, Zahid; Kevan, Steve; Kirz, Janos; McCurdy, Bill; Nelson, Keith; Neumark, Dan; Nilsson, Anders; Siegmann, Hans; Stocks, Malcolm; Schafer, Ken; Schoenlein, Robert; Spence, John; Weber, Thorsten

    2008-09-24

    Over the past quarter century, light-source user facilities have transformed research in areas ranging from gas-phase chemical dynamics to materials characterization. The ever-improving capabilities of these facilities have revolutionized our ability to study the electronic structure and dynamics of atoms, molecules, and even the most complex new materials, to understand catalytic reactions, to visualize magnetic domains, and to solve protein structures. Yet these outstanding facilities still have limitations well understood by their thousands of users. Accordingly, over the past several years, many proposals and conceptual designs for"next-generation" x-ray light sources have been developed around the world. In order to survey the scientific problems that might be addressed specifically by those new light sources operating below a photon energy of about 3 keV and to identify the scientific requirements that should drive the design of such facilities, a workshop"Science for a New Class of Soft X-Ray Light Sources" was held in Berkeley in October 2007. From an analysisof the most compelling scientific questions that could be identified and the experimental requirements for answering them, we set out to define, without regard to the specific technologies upon which they might be based, the capabilities such light sources would have to deliver in order to dramatically advance the state of research in the areas represented in the programs of the Department of Energy's Office of Basic Energy Sciences (BES). This report is based on the workshop presentations and discussions.

  9. Attosecond Light and Science at the Time-scale of the Electron - Coherent X-Rays from Tabletop Ultrafast Lasers

    ScienceCinema (OSTI)

    Margaret, Murnane [University of Colorado, Boulder and NIST

    2010-09-01

    Ever since the invention of the laser 50 years ago and its application in nonlinear optics, scientists have been striving to extend coherent laser beams into the x-ray region of the spectrum. Very recently however, the prospects for tabletop coherent sources at very short wavelengths, even in the hard x-ray region of the spectrum at wavelengths < 1nm, have brightened considerably. This advance is possible by taking nonlinear optics techniques to an extreme - physics that is the direct result of a new ability to manipulate electrons on the fastest, attosecond, time-scales of our natural world. Several applications have already been demonstrated, including making a movie of how electrons rearrange in a chemical bond changes shape as a molecule breaks apart, following how fast a magnetic material can flip orientation, understanding how fast heat flows in a nanocircuit, or building a microscope without lenses. Nature 460, 1088 (2009); Science 317, 775 (2007); Physical Review Letters 103, 257402 (2009); Nature Materials 9, 26 (2010); Nature 463, 214 (2010); Science 322, 1207 (2008).

  10. Pixel Array Detector for Time-Resolved X-ray Science, September 1, 1997 - September 14, 2000

    SciTech Connect (OSTI)

    Gruner, Sol M.

    2000-11-07

    Progress on the design, fabrication, testing and assembly of two-layer Pixel Array Detectors (PADs) is described. The PADs are developed for challenging time-resolved X-ray imaging applications at synchrotron radiation X-ray sources.

  11. EXPLORING THE DIVERSITY OF GROUPS AT 0.1 < z < 0.8 WITH X-RAY AND OPTICALLY SELECTED SAMPLES

    SciTech Connect (OSTI)

    Connelly, J. L.; Wilman, David J.; Finoguenov, Alexis; Saglia, Roberto; Hou, Annie; Parker, Laura C.; Henderson, Robert D. E.; Mulchaey, John S.; McGee, Sean L.; Balogh, Michael L.; Bower, Richard G.

    2012-09-10

    We present the global group properties of two samples of galaxy groups containing 39 high-quality X-ray-selected systems and 38 optically (spectroscopically) selected systems in coincident spatial regions at 0.12 < z < 0.79. The total mass range of the combined sample is {approx}(10{sup 12}-5) Multiplication-Sign 10{sup 14} M{sub Sun }. Only nine optical systems are associable with X-ray systems. We discuss the confusion inherent in the matching of both galaxies to extended X-ray emission and of X-ray emission to already identified optical systems. Extensive spectroscopy has been obtained and the resultant redshift catalog and group membership are provided here. X-ray, dynamical, and total stellar masses of the groups are also derived and presented. We explore the effects of utilizing different centers and applying three different kinds of radial cut to our systems: a constant cut of 1 Mpc and two r{sub 200} cuts, one based on the velocity dispersion of the system and the other on the X-ray emission. We find that an X-ray-based r{sub 200} results in less scatter in scaling relations and less dynamical complexity as evidenced by results of the Anderson-Darling and Dressler-Schectman tests, indicating that this radius tends to isolate the virialized part of the system. The constant and velocity dispersion based cuts can overestimate membership and can work to inflate velocity dispersion and dynamical and stellar mass. We find L{sub X} -{sigma} and M{sub stellar}-L{sub X} scaling relations for X-ray and optically selected systems are not dissimilar. The mean fraction of mass found in stars, excluding intracluster light, for our systems is {approx}0.014 with a logarithmic standard deviation of 0.398 dex. We also define and investigate a sample of groups which are X-ray underluminous given the total group stellar mass. For these systems the fraction of stellar mass contributed by the most massive galaxy is typically lower than that found for the total population of

  12. A COMBINED LOW-RADIO FREQUENCY/X-RAY STUDY OF GALAXY GROUPS. I. GIANT METREWAVE RADIO TELESCOPE OBSERVATIONS AT 235 MHz AND 610 MHz

    SciTech Connect (OSTI)

    Giacintucci, Simona; O'Sullivan, Ewan; Vrtilek, Jan; David, Laurence P.; Mazzotta, Pasquale; Gitti, Myriam; Jones, Christine; Forman, William R.; Raychaudhury, Somak; Ponman, Trevor; Venturi, Tiziana; Athreya, Ramana M.; Clarke, Tracy E.; Murgia, Matteo; Ishwara-Chandra, C. H.

    2011-05-10

    We present new Giant Metrewave Radio Telescope observations at 235 MHz and 610 MHz of 18 X-ray bright galaxy groups. These observations are part of an extended project, presented here and in future papers, which combines low-frequency radio and X-ray data to investigate the interaction between central active galactic nuclei (AGNs) and the intra-group medium (IGM). The radio images show a very diverse population of group-central radio sources, varying widely in size, power, morphology, and spectral index. Comparison of the radio images with Chandra and XMM-Newton X-ray images shows that groups with significant substructure in the X-ray band and marginal radio emission at {approx}>1 GHz host low-frequency radio structures that correlate with substructures in IGM. Radio-filled X-ray cavities, the most evident form of AGN/IGM interaction in our sample, are found in half of the systems and are typically associated with small, low-, or mid-power double radio sources. Two systems, NGC5044 and NGC4636, possess multiple cavities, which are isotropically distributed around the group center, possibly due to group weather. In other systems the radio/X-ray correlations are less evident. However, the AGN/IGM interaction can manifest itself through the effects of the high-pressure medium on the morphology, spectral properties, and evolution of the radio-emitting plasma. In particular, the IGM can confine fading radio lobes in old/dying radio galaxies and prevent them from dissipating quickly. Evidence for radio emission produced by former outbursts that co-exist with current activity is found in six groups of the sample.

  13. X-ray microtomographic scanners

    SciTech Connect (OSTI)

    Syryamkin, V. I. Klestov, S. A.

    2015-11-17

    The article studies the operating procedures of an X-ray microtomographic scanner and the module of reconstruction and analysis 3D-image of a test sample in particular. An algorithm for 3D-image reconstruction based on image shadow projections and mathematical methods of the processing are described. Chapter 1 describes the basic principles of X-ray tomography and general procedures of the device developed. Chapters 2 and 3 are devoted to the problem of resources saving by the system during the X-ray tomography procedure, which is achieved by preprocessing of the initial shadow projections. Preprocessing includes background noise removing from the images, which reduces the amount of shadow projections in general and increases the efficiency of the group shadow projections compression. In conclusion, the main applications of X-ray tomography are presented.

  14. X-Ray Diagnostics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    including film developing and scanning, and image plate scanning. Related images X-ray framing camera being loaded into the TIM in the Trident North Target Area. X-ray framing...

  15. SSRL School 2008 on Hard X-ray Scattering Techniques in MES

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    May 20-22, 2008 SSRL School on Synchrotron X-ray Absorption Spectroscopy Techniques in Environmental and Materials Sciences: Theory and Application Group photo from the 2008 SSRL...

  16. Controlling X-rays With Light

    SciTech Connect (OSTI)

    Glover, Ernie; Hertlein, Marcus; Southworth, Steve; Allison, Tom; van Tilborg, Jeroen; Kanter, Elliot; Krassig, B.; Varma, H.; Rude, Bruce; Santra, Robin; Belkacem, Ali; Young, Linda

    2010-08-02

    Ultrafast x-ray science is an exciting frontier that promises the visualization of electronic, atomic and molecular dynamics on atomic time and length scales. A largelyunexplored area of ultrafast x-ray science is the use of light to control how x-rays interact with matter. In order to extend control concepts established for long wavelengthprobes to the x-ray regime, the optical control field must drive a coherent electronic response on a timescale comparable to femtosecond core-hole lifetimes. An intense field is required to achieve this rapid response. Here an intense optical control pulse isobserved to efficiently modulate photoelectric absorption for x-rays and to create an ultrafast transparency window. We demonstrate an application of x-ray transparencyrelevant to ultrafast x-ray sources: an all-photonic temporal cross-correlation measurement of a femtosecond x-ray pulse. The ability to control x-ray/matterinteractions with light will create new opportunities at current and next-generation x-ray light sources.

  17. Magnetic imaging with full-field soft x-ray microscopies (Journal...

    Office of Scientific and Technical Information (OSTI)

    Sponsoring Org: USDOE Office of Science (SC) Country of Publication: United States Language: English Subject: 36 MATERIALS SCIENCE X-ray magnetic dichroism; Soft X-ray ...

  18. X-Ray Diagnostics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diagnostics X-Ray Diagnostics Maintenance of existing devices and development of advanced concepts Contact John Oertel (505) 665-3246 Email Hot, dense matter produced by intense laser interaction with a solid target often produces x-rays with energies from 100 eV to those exceeding 100 keV. A suite of diagnostics and methods have been deployed at Trident to diagnose the x-ray emission from laser-matter interaction experiments, or to use the x-rays as a probe of dense matter. These

  19. Development and calibration of mirrors and gratings for the Soft X-ray materials science beamline at the Linac Coherent Light Source free-electron laser

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Soufli, Regina; Fernandez-Perea, Monica; Baker, Sherry L.; Robinson, Jeff C.; Gullikson, Eric M.; Heimann, Philip; Yashchuk, Valerie V.; McKinney, Wayne R.; Schlotter, William F.; Rowen, Michael

    2012-04-18

    This article discusses the development and calibration of the x-ray reflective and diffractive elements for the Soft X-ray Materials Science (SXR) beamline of the Linac Coherent Light Source (LCLS) free-electron laser (FEL), designed for operation in the 500 – 2000 eV region. The surface topography of three Si mirror substrates and two Si diffraction grating substrates was examined by atomic force microscopy (AFM) and optical profilometry. The figure of the mirror substrates was also verified via surface slope measurements with a long trace profiler. A boron carbide (B4C) coating especially optimized for the LCLS FEL conditions was deposited on allmore » SXR mirrors and gratings. Coating thickness uniformity of 0.14 nm root mean square (rms) across clear apertures extending to 205 mm length was demonstrated for all elements, as required to preserve the coherent wavefront of the LCLS source. The reflective performance of the mirrors and the diffraction efficiency of the gratings were calibrated at beamline 6.3.2 at the Advanced Light Source synchrotron. To verify the integrity of the nanometer-scale grating structure, the grating topography was examined by AFM before and after coating. This is to our knowledge the first time B4C-coated diffraction gratings are demonstrated for operation in the soft x-ray region.« less

  20. SMB, X-Ray Spectroscopy & Imaging

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Home » X-Ray Spectroscopy & Imaging X-Ray Spectroscopy & Imaging SSRL has five hard X-ray Spectroscopy beamlines and three Microfocus Imaging beamlines dedicated to Biological and Biomedical research funded by the NIH and DOE-BER. The SMB group supports and develops technical instrumentation and theoretical methods for state-of-the-art tender and hard X-ray spectroscopy and EXAFS studies on metalloproteins, cofactors and metals in medicine. The SMB group has also contributed to the

  1. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in...

  2. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing...

  3. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in ...

  4. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing ...

  5. Neutron and X-ray Detectors

    SciTech Connect (OSTI)

    Carini, Gabriella; Denes, Peter; Gruener, Sol; Lessner, Elianne

    2012-08-01

    The Basic Energy Sciences (BES) X-ray and neutron user facilities attract more than 12,000 researchers each year to perform cutting-edge science at these state-of-the-art sources. While impressive breakthroughs in X-ray and neutron sources give us the powerful illumination needed to peer into the nano- to mesoscale world, a stumbling block continues to be the distinct lag in detector development, which is slowing progress toward data collection and analysis. Urgently needed detector improvements would reveal chemical composition and bonding in 3-D and in real time, allow researchers to watch “movies” of essential life processes as they happen, and make much more efficient use of every X-ray and neutron produced by the source The immense scientific potential that will come from better detectors has triggered worldwide activity in this area. Europe in particular has made impressive strides, outpacing the United States on several fronts. Maintaining a vital U.S. leadership in this key research endeavor will require targeted investments in detector R&D and infrastructure. To clarify the gap between detector development and source advances, and to identify opportunities to maximize the scientific impact of BES user facilities, a workshop on Neutron and X-ray Detectors was held August 1-3, 2012, in Gaithersburg, Maryland. Participants from universities, national laboratories, and commercial organizations from the United States and around the globe participated in plenary sessions, breakout groups, and joint open-discussion summary sessions. Sources have become immensely more powerful and are now brighter (more particles focused onto the sample per second) and more precise (higher spatial, spectral, and temporal resolution). To fully utilize these source advances, detectors must become faster, more efficient, and more discriminating. In supporting the mission of today’s cutting-edge neutron and X-ray sources, the workshop identified six detector research challenges

  6. Chest x-Rays

    Broader source: Energy.gov [DOE]

    The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica.

  7. X-ray beamsplitter

    DOE Patents [OSTI]

    Ceglio, Natale M.; Stearns, Daniel S.; Hawryluk, Andrew M.; Barbee, Jr., Troy W.

    1989-01-01

    An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

  8. X-ray beamsplitter

    DOE Patents [OSTI]

    Ceglio, N.M.; Stearns, D.G.; Hawryluk, A.M.; Barbee, T.W. Jr.

    1987-08-07

    An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5--50 pairs of alternate Mo/Si layers with a period of 20--250 A. The support membrane is 10--200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window. 6 figs.

  9. X-ray generator

    DOE Patents [OSTI]

    Dawson, John M.

    1976-01-01

    Apparatus and method for producing coherent secondary x-rays that are controlled as to direction by illuminating a mixture of high z and low z gases with an intense burst of primary x-rays. The primary x-rays are produced with a laser activated plasma, and these x-rays strip off the electrons of the high z atoms in the lasing medium, while the low z atoms retain their electrons. The neutral atoms transfer electrons to highly excited states of the highly striped high z ions giving an inverted population which produces the desired coherent x-rays. In one embodiment, a laser, light beam provides a laser spark that produces the intense burst of coherent x-rays that illuminates the mixture of high z and low z gases, whereby the high z atoms are stripped while the low z ones are not, giving the desired mixture of highly ionized and neutral atoms. To this end, the laser spark is produced by injecting a laser light beam, or a plurality of beams, into a first gas in a cylindrical container having an adjacent second gas layer co-axial therewith, the laser producing a plasma and the intense primary x-rays in the first gas, and the second gas containing the high and low atomic number elements for receiving the primary x-rays, whereupon the secondary x-rays are produced therein by stripping desired ions in a neutral gas and transfer of electrons to highly excited states of the stripped ions from the unionized atoms. Means for magnetically confining and stabilizing the plasma are disclosed for controlling the direction of the x-rays.

  10. Portable X-Ray Diffraction (XRD) | Open Energy Information

    Open Energy Info (EERE)

    X-ray powder diffraction, which has traditionally been used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline...

  11. X-Ray Diffraction (XRD) | Open Energy Information

    Open Energy Info (EERE)

    under investigation. X-ray powder diffraction is widely used in geology, environmental science, material science, and engineering to rapidly identify unknown crystalline substances...

  12. THE STELLAR MASS–HALO MASS RELATION FOR LOW-MASS X-RAY GROUPS AT 0.5< z< 1 IN THE CDFS WITH CSI

    SciTech Connect (OSTI)

    Patel, Shannon G.; Kelson, Daniel D.; Williams, Rik J.; Mulchaey, John S.; Dressler, Alan; McCarthy, Patrick J.; Shectman, Stephen A.

    2015-01-30

    Since z∼1, the stellar mass density locked in low-mass groups and clusters has grown by a factor of ∼8. Here, we make the first statistical measurements of the stellar mass content of low-mass X-ray groups at 0.5Groups are selected from combined Chandra and XMM-Newton X-ray observations in the Chandra Deep Field South. These ultra-deep observations allow us to identify bona fide low-mass groups at high redshift and enable measurements of their total halo masses. We compute aggregate stellar masses for these halos using galaxies from the Carnegie-Spitzer-IMACS (CSI) spectroscopic redshift survey. Stars comprise ∼3%–4% of the total mass of group halos with masses 10{sup 12.8}group stellar mass can serve as a rough proxy for halo mass. We find no evidence for any significant evolution in the stellar–halo mass relation since z≲1. Quantifying the stellar content in groups since this epoch is critical given that hierarchical assembly leads to such halos growing in number density and hosting increasing shares of quiescent galaxies.

  13. A dedicated superbend x-ray microdiffraction beamline for materials, geo-, and environmental sciences at the advanced light source

    SciTech Connect (OSTI)

    Advanced Light Source; Kunz, Martin; Tamura, Nobumichi; Chen, Kai; MacDowell, Alastair A.; Celestre, Richard S.; Church, Matthew M.; Fakra, Sirine; Domning, Edward E.; Glossinger, James M.; Kirschman, Jonathan L.; Morrison, Gregory Y.; Plate, Dave W.; Smith, Brian V.; Warwick, Tony; Padmore, Howard A.; Ustundag, Ersan; Yashchuk, Valeriy V.

    2009-03-24

    A new facility for microdiffraction strain measurements and microfluorescence mapping has been built on beamline 12.3.2 at the advanced light source of the Lawrence Berkeley National Laboratory. This beamline benefits from the hard x-radiation generated by a 6 T superconducting bending magnet (superbend) This provides a hard x-ray spectrum from 5 to 22 keV and a flux within a 1 mu m spot of ~;;5x109 photons/ s (0.1percent bandwidth at 8 keV). The radiation is relayed from the superbend source to a focus in the experimental hutch by a toroidal mirror. The focus spot is tailored bytwo pairs of adjustable slits, which serve as secondary source point. Inside the lead hutch, a pair of Kirkpatrick-Baez (KB) mirrors placed in a vacuum tank refocuses the secondary slit source onto the sample position. A new KB-bending mechanism with active temperature stabilization allows for more reproducible and stable mirror bending and thus mirror focusing. Focus spots around 1 um are routinely achieved and allow a variety of experiments, which have in common the need of spatial resolution. The effective spatial resolution (~;;0.2 mu m) is limited by a convolution of beam size, scan-stage resolution, and stage stability. A four-bounce monochromator consisting of two channel-cut Si(111) crystals placed between the secondary source and KB-mirrors allows for easy changes between white-beam and monochromatic experiments while maintaining a fixed beam position. High resolution stage scans are performed while recording a fluorescence emission signal or an x-ray diffraction signal coming from either a monochromatic or a white focused beam. The former allows for elemental mapping, whereas the latter is used to produce two-dimensional maps of crystal-phases, -orientation, -texture, and -strain/stress. Typically achieved strain resolution is in the order of 5x10-5 strain units. Accurate sample positioning in the x-ray focus spot is achieved with a commercial laser-triangulation unit. A Si

  14. The Soft X-ray Research instrument at the Linac Coherent Light...

    Office of Scientific and Technical Information (OSTI)

    The Soft X-ray Research instrument at the Linac Coherent Light Source Georgi L. ... Fremont, CA 94539, USA. Keywords: FEL; X-ray; ultrafast; spectroscopy; materials science. ...

  15. X-ray Optics for BES Light Source Facilities

    SciTech Connect (OSTI)

    Mills, Dennis; Padmore, Howard; Lessner, Eliane

    2013-03-27

    potentially revolutionary science involves soft excitations such as magnons and phonons; in general, these are well below the resolution that can be probed by today’s optical systems. The study of these low-energy excitations will only move forward if advances are made in high-resolution gratings for the soft X-ray energy region, and higher-resolution crystal analyzers for the hard X-ray region. In almost all the forefront areas of X-ray science today, the main limitation is our ability to focus, monochromate, and manipulate X-rays at the level required for these advanced measurements. To address these issues, the U.S. Department of Energy (DOE) Office of Basic Energy Sciences (BES) sponsored a workshop, X-ray Optics for BES Light Source Facilities, which was held March 27–29, 2013, near Washington, D.C. The workshop addressed a wide range of technical and organizational issues. Eleven working groups were formed in advance of the meeting and sought over several months to define the most pressing problems and emerging opportunities and to propose the best routes forward for a focused R&D program to solve these problems. The workshop participants identified eight principal research directions (PRDs), as follows: Development of advanced grating lithography and manufacturing for high-energy resolution techniques such as soft X-ray inelastic scattering. Development of higher-precision mirrors for brightness preservation through the use of advanced metrology in manufacturing, improvements in manufacturing techniques, and in mechanical mounting and cooling. Development of higher-accuracy optical metrology that can be used in manufacturing, verification, and testing of optomechanical systems, as well as at wavelength metrology that can be used for quantification of individual optics and alignment and testing of beamlines. Development of an integrated optical modeling and design framework that is designed and maintained specifically for X-ray optics. Development of

  16. X-ray laser

    DOE Patents [OSTI]

    Nilsen, Joseph

    1991-01-01

    An X-ray laser (10) that lases between the K edges of carbon and oxygen, i.e. between 44 and 23 Angstroms, is provided. The laser comprises a silicon (12) and dysprosium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state nickel-like dysprosium ions (34) are resonantly photo-pumped to their upper X-ray laser state by line emission from hydrogen-like silicon ions (32). The novel X-ray laser should prove especially useful for the microscopy of biological specimens.

  17. X-Ray Detection

    Office of Scientific and Technical Information (OSTI)

    ratio, I I on I off , recorded with plus (+, blue) and minus (-, red) x-ray helicities. This measurement was taken at -5 mA, which corresponds to a current...

  18. X-Ray Data from the X-Ray Data Booklet Online

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Thompson, Albert C.; Attwood, David T.; Gullikson, Eric M.; Howells, Malcolm R.; Kortright, Jeffrey B.; Robinson, Arthur L.; Underwood, James H.; Kim, Kwang-Je; Kirz, Janos; Lindau, Ingolf; Pianetta, Piero; Winick, Herman; Williams, Gwyn P.; Scofield, James H.

    The original X-Ray Data Booklet, published in 1985, became a classic reference source. The online version has been significantly revised and updated to reflect today's science. Hundreds of pages of authoritative data provide the x-ray properties of elements, information on synchrotron radiation, scattering processes, optics and detectors, and other related calculations, formulas, and data tables.

  19. X-ray Imaging Workshop

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    microscopy (PEEM), angle resolved photoemission spectroscopy (ARPES), coherent diffraction imaging, x-ray microscopy, micro-tomography, holographic imaging, and x-ray...

  20. X-ray fluorescence mapping

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Microscopy and Imaging: X-ray Fluorescence Mapping Of increasing scientific interest is the detection, quantification and mapping of elemental content of samples, often down...

  1. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the

  2. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the

  3. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the

  4. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  5. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  6. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  7. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  8. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  9. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  10. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  11. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes advantage of the penetrating power of x rays while simultaneously removing the limitations

  12. Inelastic X-ray and Nuclear Resonant Scattering | Advanced Photon...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    XSD-IXN XSD-IXN Home Staff Inelastic X-ray and Nuclear Resonant Scattering The Inelastic X-ray and Nuclear Resonant Scattering group operates beamlines at APS Sectors 3, 9 and 30....

  13. X-ray microtomography

    SciTech Connect (OSTI)

    Landis, Eric N.; Keane, Denis T.

    2010-12-15

    In this tutorial, we describe X-ray microtomography as a technique to nondestructively characterize material microstructure in three dimensions at a micron level spatial resolution. While commercially available laboratory scale instrumentation is available, we focus our attention on synchrotron-based systems, where we can exploit a high flux, monochromatic X-ray beam to produce high fidelity three-dimensional images. A brief description of the physics and the mathematical analysis behind the technique is followed by example applications to specific materials characterization problems, with a particular focus on the utilization of three-dimensional image processing that can be used to extract a wide range of useful information.

  14. X-ray crystallographic analysis of adipocyte fatty acid binding...

    Office of Scientific and Technical Information (OSTI)

    X-ray crystallographic analysis of adipocyte fatty acid binding protein (aP2) modified ... LIFE SCIENCES; ALDEHYDES; CARBOXYLIC ACIDS; CRYSTAL STRUCTURE; IN VIVO; INFLAMMATION; ...

  15. X-ray beam finder

    DOE Patents [OSTI]

    Gilbert, H.W.

    1983-06-16

    An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

  16. Ultra-short wavelength x-ray system

    DOE Patents [OSTI]

    Umstadter, Donald; He, Fei; Lau, Yue-Ying

    2008-01-22

    A method and apparatus to generate a beam of coherent light including x-rays or XUV by colliding a high-intensity laser pulse with an electron beam that is accelerated by a synchronized laser pulse. Applications include x-ray and EUV lithography, protein structural analysis, plasma diagnostics, x-ray diffraction, crack analysis, non-destructive testing, surface science and ultrafast science.

  17. Data System Sciences & Engineering Group

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Architectures for National Security Risk Analysis Streaming Realtime Sensor Networks Visual Analytics Opportunities Contact Us Data System Sciences & Engineering Group DSSE goes...

  18. Soft-x-ray

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Soft-x-ray emission, plasma equilibrium, and fluctuation studies on Madison Symmetric Torus C. Xiao Department of Physics, University of Wisconsin-Madison, Madison, Wisconsin and Department of Physics and Engineering Physics, University of Saskatchewan, Saskatoon, Canada P. Franz Consorzio RFX-Associazione EURATOM ENEA Sulla Fusione, Italy and Istituto Nazionale di Fisica della Materia, Unita' di Ricerca di Padova, Italy B. E. Chapman and D. Craig Department of Physics, University of

  19. Science Education Group | Princeton Plasma Physics Lab

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Science Education Group View larger image Sci Ed Group 15 View larger image Group 21

  20. Fluctuation X-Ray Scattering

    SciTech Connect (OSTI)

    Saldin, PI: D. K.; Co-I's: J. C. H. Spence and P. Fromme

    2013-01-25

    The work supported by the grant was aimed at developing novel methods of finding the structures of biomolecules using x-rays from novel sources such as the x-ray free electron laser and modern synchrotrons

  1. Tunable X-ray source

    DOE Patents [OSTI]

    Boyce, James R.

    2011-02-08

    A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

  2. X-Ray Cross-Complementing Group 1 and Thymidylate Synthase Polymorphisms Might Predict Response to Chemoradiotherapy in Rectal Cancer Patients

    SciTech Connect (OSTI)

    Lamas, Maria J.

    2012-01-01

    Purpose: 5-Fluorouracil-based chemoradiotherapy before total mesorectal excision is currently the standard treatment of Stage II and III rectal cancer patients. We used known predictive pharmacogenetic biomarkers to identify the responders to preoperative chemoradiotherapy in our series. Methods and Materials: A total of 93 Stage II-III rectal cancer patients were genotyped using peripheral blood samples. The genes analyzed were X-ray cross-complementing group 1 (XRCC1), ERCC1, MTHFR, EGFR, DPYD, and TYMS. The patients were treated with 225 mg/m{sup 2}/d continuous infusion of 5-fluorouracil concomitantly with radiotherapy (50.4 Gy) followed by total mesorectal excision. The outcomes were measured by tumor regression grade (TRG) as a major response (TRG 1 and TRG 2) or as a poor response (TRG3, TRG4, and TRG5). Results: The major histopathologic response rate was 47.3%. XRCC1 G/G carriers had a greater probability of response than G/A carriers (odds ratio, 4.18; 95% confidence interval, 1.62-10.74, p = .003) Patients with polymorphisms associated with high expression of thymidylate synthase (2R/3G, 3C/3G, and 3G/3G) showed a greater pathologic response rate compared with carriers of low expression (odds ratio, 2.65; 95% confidence interval, 1.10-6.39, p = .02) No significant differences were seen in the response according to EGFR, ERCC1, MTHFR{sub C}677 and MTHFR{sub A}1298 expression. Conclusions: XRCC1 G/G and thymidylate synthase (2R/3G, 3C/3G, and 3G/3G) are independent factors of a major response. Germline thymidylate synthase and XRCC1 polymorphisms might be useful as predictive markers of rectal tumor response to neoadjuvant chemoradiotherapy with 5-fluorouracil.

  3. SMB, X-ray Emission Spectroscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    include X-ray Emission Spectroscopy (XES), Resonant Inelastic X-ray Scattering (RIXS), High Energy Resolution Fluorescence Detection (HERFD) and X-ray Raman Spectroscopy (XRS). ...

  4. X-ray lithography source

    DOE Patents [OSTI]

    Piestrup, M.A.; Boyers, D.G.; Pincus, C.

    1991-12-31

    A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits is disclosed. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and eliminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an excellent moderate-priced X-ray source for lithography. 26 figures.

  5. X-ray lithography source

    DOE Patents [OSTI]

    Piestrup, Melvin A.; Boyers, David G.; Pincus, Cary

    1991-01-01

    A high-intensity, inexpensive X-ray source for X-ray lithography for the production of integrated circuits. Foil stacks are bombarded with a high-energy electron beam of 25 to 250 MeV to produce a flux of soft X-rays of 500 eV to 3 keV. Methods of increasing the total X-ray power and making the cross section of the X-ray beam uniform are described. Methods of obtaining the desired X-ray-beam field size, optimum frequency spectrum and elminating the neutron flux are all described. A method of obtaining a plurality of station operation is also described which makes the process more efficient and economical. The satisfying of these issues makes transition radiation an exellent moderate-priced X-ray source for lithography.

  6. Radiobiological studies using gamma and x rays.

    SciTech Connect (OSTI)

    Potter, Charles Augustus; Longley, Susan W.; Scott, Bobby R. [Lovelace Respiratory Research Institute, Albuquerque, NM; Lin, Yong [Lovelace Respiratory Research Institute, Albuquerque, NM; Wilder, Julie [Lovelace Respiratory Research Institute, Albuquerque, NM; Hutt, Julie A. [Lovelace Respiratory Research Institute, Albuquerque, NM; Padilla, Mabel T. [Lovelace Respiratory Research Institute, Albuquerque, NM; Gott, Katherine M. [Lovelace Respiratory Research Institute, Albuquerque, NM

    2013-02-01

    There are approximately 500 self-shielded research irradiators used in various facilities throughout the U.S. These facilities use radioactive sources containing either 137Cs or 60Co for a variety of biological investigations. A report from the National Academy of Sciences[1] described the issues with security of particular radiation sources and the desire for their replacement. The participants in this effort prepared two peer-reviewed publications to document the results of radiobiological studies performed using photons from 320-kV x rays and 137Cs on cell cultures and mice. The effectiveness of X rays was shown to vary with cell type.

  7. Ultrafast X-Ray Coherent Control

    SciTech Connect (OSTI)

    Reis, David

    2009-05-01

    This main purpose of this grant was to develop the nascent #12;eld of ultrafast x-ray science using accelerator-based sources, and originally developed from an idea that a laser could modulate the di#11;racting properties of a x-ray di#11;racting crystal on a fast enough time scale to switch out in time a shorter slice from the already short x-ray pulses from a synchrotron. The research was carried out primarily at the Advanced Photon Source (APS) sector 7 at Argonne National Laboratory and the Sub-Picosecond Pulse Source (SPPS) at SLAC; in anticipation of the Linac Coherent Light Source (LCLS) x-ray free electron laser that became operational in 2009 at SLAC (all National User Facilities operated by BES). The research centered on the generation, control and measurement of atomic-scale dynamics in atomic, molecular optical and condensed matter systems with temporal and spatial resolution . It helped develop the ultrafast physics, techniques and scienti#12;c case for using the unprecedented characteristics of the LCLS. The project has been very successful with results have been disseminated widely and in top journals, have been well cited in the #12;eld, and have laid the foundation for many experiments being performed on the LCLS, the world's #12;rst hard x-ray free electron laser.

  8. X-RAY POINT-SOURCE POPULATIONS CONSTITUTING THE GALACTIC RIDGE X-RAY EMISSION

    SciTech Connect (OSTI)

    Morihana, Kumiko [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan)] [Institute of Physical and Chemical Research (RIKEN), 2-1 Hirosawa, Wako, Saitama 351-0198 (Japan); Tsujimoto, Masahiro; Ebisawa, Ken [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan)] [Japan Aerospace Exploration Agency, Institute of Space and Astronautical Science, 3-1-1 Yoshino-dai, Chuo-ku, Sagamihara, Kanagawa 252-5210 (Japan); Yoshida, Tessei, E-mail: morihana@crab.riken.jp [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)] [National Astronomical Observatory of Japan, 2-21-1, Osawa, Mitaka, Tokyo 181-8588 (Japan)

    2013-03-20

    Apparently diffuse X-ray emission has been known to exist along the central quarter of the Galactic Plane since the beginning of X-ray astronomy; this is referred to as the Galactic Ridge X-ray emission (GRXE). Recent deep X-ray observations have shown that numerous X-ray point sources account for a large fraction of the GRXE in the hard band (2-8 keV). However, the nature of these sources is poorly understood. Using the deepest X-ray observations made in the Chandra bulge field, we present the result of a coherent photometric and spectroscopic analysis of individual X-ray point sources for the purpose of constraining their nature and deriving their fractional contributions to the hard-band continuum and Fe K line emission of the GRXE. Based on the X-ray color-color diagram, we divided the point sources into three groups: A (hard), B (soft and broad spectrum), and C (soft and peaked spectrum). The group A sources are further decomposed spectrally into thermal and non-thermal sources with different fractions in different flux ranges. From their X-ray properties, we speculate that the group A non-thermal sources are mostly active galactic nuclei and the thermal sources are mostly white dwarf (WD) binaries such as magnetic and non-magnetic cataclysmic variables (CVs), pre-CVs, and symbiotic stars, whereas the group B and C sources are X-ray active stars in flares and quiescence, respectively. In the log N-log S curve of the 2-8 keV band, the group A non-thermal sources are dominant above Almost-Equal-To 10{sup -14} erg cm{sup -2} s{sup -1}, which is gradually taken over by Galactic sources in the fainter flux ranges. The Fe K{alpha} emission is mostly from the group A thermal (WD binaries) and the group B (X-ray active stars) sources.

  9. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with nanometer-scale resolution in three dimensions nonperiodic objects that are several microns in size. To fill this gap, the technique of coherent x-ray diffraction imaging now under development takes

  10. Fabrication process for a gradient index x-ray lens

    DOE Patents [OSTI]

    Bionta, R.M.; Makowiecki, D.M.; Skulina, K.M.

    1995-01-17

    A process is disclosed for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments in the soft x-ray region. 13 figures.

  11. Fabrication process for a gradient index x-ray lens

    DOE Patents [OSTI]

    Bionta, Richard M.; Makowiecki, Daniel M.; Skulina, Kenneth M.

    1995-01-01

    A process for fabricating high efficiency x-ray lenses that operate in the 0.5-4.0 keV region suitable for use in biological imaging, surface science, and x-ray lithography of integrated circuits. The gradient index x-ray optics fabrication process broadly involves co-sputtering multi-layers of film on a wire, followed by slicing and mounting on block, and then ion beam thinning to a thickness determined by periodic testing for efficiency. The process enables the fabrication of transmissive gradient index x-ray optics for the 0.5-4.0 keV energy range. This process allows the fabrication of optical elements for the next generation of imaging and x-ray lithography instruments m the soft x-ray region.

  12. Solar X-ray physics

    SciTech Connect (OSTI)

    Bornmann, P.L. )

    1991-01-01

    Research on solar X-ray phenomena performed by American scientists during 1987-1990 is reviewed. Major topics discussed include solar images observed during quiescent times, the processes observed during solar flares, and the coronal, interplanetary, and terrestrial phenomena associated with solar X-ray flares. Particular attention is given to the hard X-ray emission observed at the start of the flare, the energy transfer to the soft X-ray emitting plasma, the late resolution of the flare as observed in soft X-ray, and the rate of occurrence of solar flares as a function of time and latitude. Pertinent aspects of nonflaring, coronal X-ray emission and stellar flares are also discussed. 175 refs.

  13. Miniature x-ray source

    DOE Patents [OSTI]

    Trebes, James E.; Stone, Gary F.; Bell, Perry M.; Robinson, Ronald B.; Chornenky, Victor I.

    2002-01-01

    A miniature x-ray source capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature x-ray source comprises a compact vacuum tube assembly containing a cathode, an anode, a high voltage feedthru for delivering high voltage to the anode, a getter for maintaining high vacuum, a connection for an initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is highly x-ray transparent and made, for example, from boron nitride. The compact size and potential for remote operation allows the x-ray source, for example, to be placed adjacent to a material sample undergoing analysis or in proximity to the region to be treated for medical applications.

  14. Lighting Science Group | Open Energy Information

    Open Energy Info (EERE)

    Science Group Jump to: navigation, search Name: Lighting Science Group Place: Dallas, Texas Zip: 75201 Product: LED design company, with multiple patents pending in power...

  15. X-ray shearing interferometer

    DOE Patents [OSTI]

    Koch, Jeffrey A.

    2003-07-08

    An x-ray interferometer for analyzing high density plasmas and optically opaque materials includes a point-like x-ray source for providing a broadband x-ray source. The x-rays are directed through a target material and then are reflected by a high-quality ellipsoidally-bent imaging crystal to a diffraction grating disposed at 1.times. magnification. A spherically-bent imaging crystal is employed when the x-rays that are incident on the crystal surface are normal to that surface. The diffraction grating produces multiple beams which interfere with one another to produce an interference pattern which contains information about the target. A detector is disposed at the position of the image of the target produced by the interfering beams.

  16. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Microscopy Print Electron and x-ray microscopes are a valuable tool for both the life and materials sciences, but they are limited in their ability to image with...

  17. Crystallization and preliminary X-ray diffraction study of phosphopantetheine adenylyltransferase from M. tuberculosis crystallizing in space group P3{sub 2}

    SciTech Connect (OSTI)

    Timofeev, V. I.; Chupova, L. A.; Esipov, R. S.; Kuranova, I. P.

    2015-09-15

    Crystals of M. tuberculosis phosphopantetheine adenylyltransferase were grown in microgravity by the capillary counter-diffusion method through a gel layer. The X-ray diffraction data set suitable for the determination of the three-dimensional structure at atomic resolution was collected from one crystal at the Spring-8 synchrotron facility to 2.00-Å resolution. The crystals belong to sp. gr. P3{sub 2} and have the following unit-cell parameters: a = b = 106.47 Å, c = 71.32 Å, α = γ = 90°, β = 120°. The structure was solved by the molecular-replacement method. There are six subunits of the enzyme comprising a hexamer per asymmetric unit. The hexamer is a biologically active form of phosphopantetheine adenylyltransferase from M. tuberculosis.

  18. Miniature x-ray source

    DOE Patents [OSTI]

    Trebes, James E.; Bell, Perry M.; Robinson, Ronald B.

    2000-01-01

    A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

  19. X-Ray Interactions with Matter from the Center for X-Ray Optics...

    Office of Scientific and Technical Information (OSTI)

    X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO) Title: X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO) The primary interactions of ...

  20. Electromechanical x-ray generator

    DOE Patents [OSTI]

    Watson, Scott A; Platts, David; Sorensen, Eric B

    2016-05-03

    An electro-mechanical x-ray generator configured to obtain high-energy operation with favorable energy-weight scaling. The electro-mechanical x-ray generator may include a pair of capacitor plates. The capacitor plates may be charged to a predefined voltage and may be separated to generate higher voltages on the order of hundreds of kV in the AK gap. The high voltage may be generated in a vacuum tube.

  1. SMB, X-ray Absorption Spectroscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Absorption Spectroscopy X-ray Absorption Spectroscopy X-ray absorption spectroscopy (XAS) is a well-established technique for simultaneous local geometric and electronic structure...

  2. Beyond 3-D X-ray Imaging: Methodology Development and Applications in

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Material Science | Stanford Synchrotron Radiation Lightsource Beyond 3-D X-ray Imaging: Methodology Development and Applications in Material Science Thursday, September 6, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Yijin Liu Seminar There was a revolutionary development of X-ray imaging over the past few decades. The most substantial advancements in this field are closely related to the availability of the new generation of X-ray sources and the advanced X-ray optics. The advanced X-ray Optics

  3. New Directions in X-Ray Light Sources

    ScienceCinema (OSTI)

    Falcone, Roger

    2010-01-08

    July 15, 2008 Berkeley Lab lecture: Molecular movies of chemical reactions and material phase transformations need a strobe of x-rays, the penetrating light that reveals how atoms and molecules assemble in chemical and biological systems and complex materials. Roger Falcone, Director of the Advanced Light Source,will discuss a new generation of x ray sources that will enable a new science of atomic dynamics on ultrafast timescales.

  4. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis Print Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme sensitivity of their surface redox states to temperatures, to gas pressures, and to electrochemical reaction conditions renders them difficult to investigate by conventional surface-science techniques. Recently a team of Stanford and Berkeley Lab researchers used x-rays at the ALS in a novel way to observe the behavior of

  5. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis Print Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme sensitivity of their surface redox states to temperatures, to gas pressures, and to electrochemical reaction conditions renders them difficult to investigate by conventional surface-science techniques. Recently a team of Stanford and Berkeley Lab researchers used x-rays at the ALS in a novel way to observe the behavior of

  6. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis Print Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme sensitivity of their surface redox states to temperatures, to gas pressures, and to electrochemical reaction conditions renders them difficult to investigate by conventional surface-science techniques. Recently a team of Stanford and Berkeley Lab researchers used x-rays at the ALS in a novel way to observe the behavior of

  7. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis Print Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme sensitivity of their surface redox states to temperatures, to gas pressures, and to electrochemical reaction conditions renders them difficult to investigate by conventional surface-science techniques. Recently a team of Stanford and Berkeley Lab researchers used x-rays at the ALS in a novel way to observe the behavior of

  8. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis Print Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme sensitivity of their surface redox states to temperatures, to gas pressures, and to electrochemical reaction conditions renders them difficult to investigate by conventional surface-science techniques. Recently a team of Stanford and Berkeley Lab researchers used x-rays at the ALS in a novel way to observe the behavior of

  9. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis Print Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme sensitivity of their surface redox states to temperatures, to gas pressures, and to electrochemical reaction conditions renders them difficult to investigate by conventional surface-science techniques. Recently a team of Stanford and Berkeley Lab researchers used x-rays at the ALS in a novel way to observe the behavior of

  10. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis ALS X-Rays Shine a New Light on Catalysis Print Thursday, 21 May 2015 11:16 Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme sensitivity of their surface redox states to temperatures, to gas pressures, and to electrochemical reaction conditions renders them difficult to investigate by conventional surface-science techniques. Recently a team of Stanford and Berkeley Lab

  11. X-ray Microscopy and Imaging (XSD-XMI)

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    and (c) technical R&D in collaborations with other groups on nano-focusing x-ray optics, image contrast mechanisms, phase-retrieval methodology, detectors and data...

  12. Ultrashort x-ray backlighters and applications

    SciTech Connect (OSTI)

    Umstadter, D., University of Michigan

    1997-08-01

    Previously, using ultrashort laser pulses focused onto solid targets, we have experimentally studied a controllable ultrafast broadband radiation source in the extreme ultraviolet for time-resolved dynamical studies in ultrafast science [J. Workman, A. Maksimchuk, X. Llu, U. Ellenberger, J. S. Coe, C.-Y. Chien, and D. Umstadter, ``Control of Bright Picosecond X-Ray Emission from Intense Sub- Picosecond Laser-Plasma Interactions,`` Phys. Rev. Lett. 75, 2324 (1995)]. Once armed with a bright ultrafast broadband continuum x-ray source and appropriate detectors, we used the source as a backlighter to study a remotely produced plasma. The application of the source to a problem relevant to high-density matter completes the triad: creating and controlling, efficiently detecting, and applying the source. This work represented the first use of an ultrafast laser- produced x-ray source as a time-resolving probe in an application relevant to atomic, plasma and high-energy-density matter physics. Using the x-ray source as a backlighter, we adopted a pump-probe geometry to investigate the dynamic changes in electronic structure of a thin metallic film as it is perturbed by an ultrashort laser pulse. Because the laser deposits its energy in a skin depth of about 100 {Angstrom} before expansion occurs, up to gigabar pressure shock waves lasting picosecond in duration have been predicted to form in these novel plasmas. This raises the possibility of studying high- energy-density matter relevant to inertial confinement fusion (ICF) and astrophysics in small-scale laboratory experiments. In the past, time-resolved measurements of K-edge shifts in plasmas driven by nanosecond pulses have been used to infer conditions in highly compressed materials. In this study, we used 100-fs laser pulses to impulsively drive shocks into a sample (an untamped 1000 {Angstrom} aluminum film on 2000 {Angstrom} of parylene-n), measuring L-edge shifts.

  13. Scientists tune X-rays with tiny mirrors | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Sciences and Director of the Advanced Photon Source. "This is a premier example of the innovation that results from collaboration between nanoscientists and X-ray scientists."...

  14. 6th Annual SSRL School on Synchrotron X-ray Scattering, May 29...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Transportation About 6th Annual SSRL School on Synchrotron X-ray Scattering Techniques in Materials and Environmental Sciences: Theory and Application May 29-31 2012...

  15. Sure, a textbook can tell you about Bragg's Law and the x-ray...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Report SSRL 6 th Annual School on Synchrotron X-ray Scattering Techniques in Materials and Environmental Sciences: Theory and Application SSRL SR-XRS participants. ...

  16. Compact x-ray source and panel

    DOE Patents [OSTI]

    Sampayon, Stephen E.

    2008-02-12

    A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

  17. Focused X-ray source

    DOE Patents [OSTI]

    Piestrup, M.A.; Boyers, D.G.; Pincus, C.I.; Maccagno, P.

    1990-08-21

    Disclosed is an intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator. 8 figs.

  18. Focused X-ray source

    DOE Patents [OSTI]

    Piestrup, Melvin A.; Boyers, David G.; Pincus, Cary I.; Maccagno, Pierre

    1990-01-01

    An intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator.

  19. Hard x-ray delay line for x-ray photon correlation spectroscopy...

    Office of Scientific and Technical Information (OSTI)

    Hard x-ray delay line for x-ray photon correlation spectroscopy and jitter-free pump-probe experiments at LCLS Citation Details In-Document Search Title: Hard x-ray delay line for...

  20. A computational study of x-ray emission from high-Z x-ray sources...

    Office of Scientific and Technical Information (OSTI)

    A computational study of x-ray emission from high-Z x-ray sources on the National Ignition Facility laser Citation Details In-Document Search Title: A computational study of x-ray ...

  1. Reabsorption of Soft X-Ray Emission at High X-Ray Free-Electron...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Reabsorption of Soft X-Ray Emission at High X-Ray Free-Electron Laser Fluences Citation Details In-Document Search Title: Reabsorption of Soft X-Ray Emission at ...

  2. Femtosecond X-ray Absorption Spectroscopy at a Hard X-ray Free...

    Office of Scientific and Technical Information (OSTI)

    Femtosecond X-ray Absorption Spectroscopy at a Hard X-ray Free Electron Laser: Application to Spin Crossover Dynamics Citation Details In-Document Search Title: Femtosecond X-ray...

  3. A computational study of x-ray emission from high-Z x-ray sources...

    Office of Scientific and Technical Information (OSTI)

    study of x-ray emission from high-Z x-ray sources on the National Ignition Facility laser Citation Details In-Document Search Title: A computational study of x-ray emission...

  4. Microgap x-ray detector

    DOE Patents [OSTI]

    Wuest, Craig R.; Bionta, Richard M.; Ables, Elden

    1994-01-01

    An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

  5. Microgap x-ray detector

    DOE Patents [OSTI]

    Wuest, C.R.; Bionta, R.M.; Ables, E.

    1994-05-03

    An x-ray detector is disclosed which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope. 3 figures.

  6. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Nanoimaging: Instruments and Methods X-Ray Nanoimaging: Instruments and Methods Print To be held as part of SPIE. http://spie.org/OP318 August 28-29, 2013; San Diego, California, USA

  7. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light ... wavelengths relevant to atomic and molecular phenomena) with the advantages of ...

  8. Producing X-rays at the APS

    ScienceCinema (OSTI)

    None

    2013-04-19

    An introduction and overview of the Advanced Photon Source at Argonne National Laboratory, the technology that produces the brightest X-ray beams in the Western Hemisphere, and the research carried out by scientists using those X-rays.

  9. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  10. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  11. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  12. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging

  13. Neutron and X-ray Scattering

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Neutron and X-ray Scattering Neutron and X-ray Scattering When used together, neutrons and high-energy x-rays provide a supremely powerful scientific tool for mining details about the structure of materials. Combining neutrons and high-energy x-rays to explore the frontiers of materials in extreme environments. Illuminating previously inaccessible time and spatial scales. Enabling in situ research to design, discover, and control materials. Get Expertise Donald Brown Email Pushing the limits of

  14. Phase-sensitive X-ray imager

    DOE Patents [OSTI]

    Baker, Kevin Louis

    2013-01-08

    X-ray phase sensitive wave-front sensor techniques are detailed that are capable of measuring the entire two-dimensional x-ray electric field, both the amplitude and phase, with a single measurement. These Hartmann sensing and 2-D Shear interferometry wave-front sensors do not require a temporally coherent source and are therefore compatible with x-ray tubes and also with laser-produced or x-pinch x-ray sources.

  15. Cryotomography x-ray microscopy state

    DOE Patents [OSTI]

    Le Gros, Mark; Larabell, Carolyn A.

    2010-10-26

    An x-ray microscope stage enables alignment of a sample about a rotation axis to enable three dimensional tomographic imaging of the sample using an x-ray microscope. A heat exchanger assembly provides cooled gas to a sample during x-ray microscopic imaging.

  16. LUSI :: LCLS Ultrafast Science Instruments

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    search Go Home Project Pages LUSI Instruments Uniqueness of FEL X-rays X-ray FEL Science About LCLS Science with LCLS Calendar & Meetings Contact Us Office of Science/U.S. DOE Current News: Job Openings Oct. 3, 3:00 PM- SPPS: A window to the world of LCLS Science Meetings: LCLS SAC Meeting October 19-20, 2006 LUSI Lehman Review January 23-24, 2007 LUSI Bi-weekly Team Leader meeting June 23, 2006 LUSI Science Group Leaders Meeting October 18-19 SSRL User Meeting - Soft X-ray Workshop Oct

  17. X-ray transmissive debris shield

    DOE Patents [OSTI]

    Spielman, Rick B.

    1996-01-01

    An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

  18. X-ray transmissive debris shield

    DOE Patents [OSTI]

    Spielman, R.B.

    1996-05-21

    An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

  19. X-ray lithography using holographic images

    DOE Patents [OSTI]

    Howells, Malcolm R.; Jacobsen, Chris

    1995-01-01

    A non-contact X-ray projection lithography method for producing a desired X-ray image on a selected surface of an X-ray-sensitive material, such as photoresist material on a wafer, the desired X-ray image having image minimum linewidths as small as 0.063 .mu.m, or even smaller. A hologram and its position are determined that will produce the desired image on the selected surface when the hologram is irradiated with X-rays from a suitably monochromatic X-ray source of a selected wavelength .lambda.. On-axis X-ray transmission through, or off-axis X-ray reflection from, a hologram may be used here, with very different requirements for monochromaticity, flux and brightness of the X-ray source. For reasonable penetration of photoresist materials by X-rays produced by the X-ray source, the wavelength X, is preferably chosen to be no more than 13.5 nm in one embodiment and more preferably is chosen in the range 1-5 nm in the other embodiment. A lower limit on linewidth is set by the linewidth of available microstructure writing devices, such as an electron beam.

  20. Quantitative Microstructural Imaging by Scanning Laue X-ray Micro- and

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Nanodiffraction Quantitative Microstructural Imaging by Scanning Laue X-ray Micro- and Nanodiffraction Quantitative Microstructural Imaging by Scanning Laue X-ray Micro- and Nanodiffraction Print Monday, 20 June 2016 09:26 Synchrotron Laue x-ray microdiffraction turns 20 this year. The June 2016 issue of MRS Bulletin is dedicated to synchrotron radiation research in materials science and features a review article on the current capabilities, latest technical developments, and emerging

  1. Compact X-ray Light Source Workshop Report

    SciTech Connect (OSTI)

    Thevuthasan, Suntharampillai; Evans, James E.; Terminello, Louis J.; Koppenaal, David W.; Manke, Kristin L.; Plata, Charity

    2012-12-01

    This report, produced jointly by EMSL and FCSD, is the result of a workshop held in September 2011 that examined the utility of a compact x-ray light source (CXLS) in addressing many scientific challenges critical to advancing energy science and technology.

  2. The First Angstrom X-Ray Free-Electron Laser

    SciTech Connect (OSTI)

    Galayda, John; /SLAC

    2012-08-24

    The Linac Coherent Light Source produced its first x-ray laser beam on 10 April 2009. Today it is routinely producing x-ray pulses with energy >2 mJ across the operating range from 820-8,200 eV. The facility has begun operating for atomic/molecular/optical science experiments. Performance of the facility in its first user run (1 October - 21 December) and current machine development activities will be presented. Early results from the preparations for the start of the second user run is also reported.

  3. Spectral brilliance of parametric X-rays at the FAST facility

    SciTech Connect (OSTI)

    Sen, Tanaji; Seiss, Todd

    2015-06-22

    We discuss the generation of parametric X-rays in the new photoinjector at the FAST (Fermilab Accelerator Science and Technology) facility in Fermilab. These experiments will be conducted in addition to channeling X-ray radiation experiments. The low emittance electron beam makes this facility a promising source for creating brilliant X-rays. We discuss the theoretical model and present detailed calculations of the intensity spectrum, energy and angular widths and spectral brilliance under different conditions. Furthermore, we report on expected results with parametric X-rays generated while under channeling conditions.

  4. X-ray transmissive debris shield

    DOE Patents [OSTI]

    Spielman, Rick B.

    1994-01-01

    A composite window structure is described for transmitting x-ray radiation and for shielding radiation generated debris. In particular, separate layers of different x-ray transmissive materials are laminated together to form a high strength, x-ray transmissive debris shield which is particularly suited for use in high energy fluences. In one embodiment, the composite window comprises alternating layers of beryllium and a thermoset polymer.

  5. High speed x-ray beam chopper

    DOE Patents [OSTI]

    McPherson, Armon; Mills, Dennis M.

    2002-01-01

    A fast, economical, and compact x-ray beam chopper with a small mass and a small moment of inertia whose rotation can be synchronized and phase locked to an electronic signal from an x-ray source and be monitored by a light beam is disclosed. X-ray bursts shorter than 2.5 microseconds have been produced with a jitter time of less than 3 ns.

  6. Gamma Radiation & X-Rays

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Gamma Radiation and X-Rays 1. Gamma radiation and X-rays are electromagnetic radiation like visible light, radio waves, and ultraviolet light. These electromagnetic radiations differ only in the amount of energy they have. Gamma rays and X-rays are the most energetic of these. 2. Gamma radiation is able to travel many meters in air and many centimeters in human tissue. It readily penetrates most materials and is sometimes called "penetrating radiation." 3. X-rays are like gamma rays.

  7. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are

  8. X-ray microscopy. Beyond ensemble averages

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Ice, Gene E.; Budai, John D.

    2015-06-23

    This work exemplifies emerging tools to characterize local materials structure and dynamics, made possible by powerful X-ray synchrotron and transmission electron microscopy methods.

  9. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). ...

  10. Compound refractive X-ray lens

    DOE Patents [OSTI]

    Nygren, David R.; Cahn, Robert; Cederstrom, Bjorn; Danielsson, Mats; Vestlund, Jonas

    2000-01-01

    An apparatus and method for focusing X-rays. In one embodiment, his invention is a commercial-grade compound refractive X-ray lens. The commercial-grade compound refractive X-ray lens includes a volume of low-Z material. The volume of low-Z material has a first surface which is adapted to receive X-rays of commercially-applicable power emitted from a commercial-grade X-ray source. The volume of low-Z material also has a second surface from which emerge the X-rays of commercially-applicable power which were received at the first surface. Additionally, the commercial-grade compound refractive X-ray lens includes a plurality of openings which are disposed between the first surface and the second surface. The plurality of openings are oriented such that the X-rays of commercially-applicable power which are received at the first surface, pass through the volume of low-Z material and through the plurality openings. In so doing, the X-rays which emerge from the second surface are refracted to a focal point.

  11. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that

  12. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that

  13. X-ray laser microscope apparatus

    DOE Patents [OSTI]

    Suckewer, Szymon; DiCicco, Darrell S.; Hirschberg, Joseph G.; Meixler, Lewis D.; Sathre, Robert; Skinner, Charles H.

    1990-01-01

    A microscope consisting of an x-ray contact microscope and an optical microscope. The optical, phase contrast, microscope is used to align a target with respect to a source of soft x-rays. The source of soft x-rays preferably comprises an x-ray laser but could comprise a synchrotron or other pulse source of x-rays. Transparent resist material is used to support the target. The optical microscope is located on the opposite side of the transparent resist material from the target and is employed to align the target with respect to the anticipated soft x-ray laser beam. After alignment with the use of the optical microscope, the target is exposed to the soft x-ray laser beam. The x-ray sensitive transparent resist material whose chemical bonds are altered by the x-ray beam passing through the target mater GOVERNMENT LICENSE RIGHTS This invention was made with government support under Contract No. De-FG02-86ER13609 awarded by the Department of Energy. The Government has certain rights in this invention.

  14. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light ...

  15. Gamma and X-ray Dosimetric Method

    DOE Patents [OSTI]

    Taplin, G.V.; Douglas, C.H.

    1954-06-29

    This patent application concerns a highly stable two-phase liquid system for use in a colorimetric dosimeter for measuring X-ray and gamma radiation.

  16. X-ray Attenuation and Absorption Calculations.

    Energy Science and Technology Software Center (OSTI)

    1988-02-25

    This point-source, polychromatic, discrete energy X-ray transport and energy deposition code system calculates first-order spectral estimates of X-ray energy transmission through slab materials and the associated spectrum of energy absorbed by the material.

  17. Phased Contrast X-Ray Imaging

    ScienceCinema (OSTI)

    Erin Miller

    2012-12-31

    The Pacific Northwest National Laboratory is developing a range of technologies to broaden the field of explosives detection. Phased contrast X-ray imaging, which uses silicon gratings to detect distortions in the X-ray wave front, may be applicable to mail or luggage scanning for explosives; it can also be used in detecting other contraband, small-parts inspection, or materials characterization.

  18. Accelerator-driven X-ray Sources

    SciTech Connect (OSTI)

    Nguyen, Dinh Cong

    2015-11-09

    After an introduction which mentions x-ray tubes and storage rings and gives a brief review of special relativity, the subject is treated under the following topics and subtopics: synchrotron radiation (bending magnet radiation, wiggler radiation, undulator radiation, brightness and brilliance definition, synchrotron radiation facilities), x-ray free-electron lasers (linac-driven X-ray FEL, FEL interactions, self-amplified spontaneous emission (SASE), SASE self-seeding, fourth-generation light source facilities), and other X-ray sources (energy recovery linacs, Inverse Compton scattering, laser wakefield accelerator driven X-ray sources. In summary, accelerator-based light sources cover the entire electromagnetic spectrum. Synchrotron radiation (bending magnet, wiggler and undulator radiation) has unique properties that can be tailored to the users’ needs: bending magnet and wiggler radiation is broadband, undulator radiation has narrow spectral lines. X-ray FELs are the brightest coherent X-ray sources with high photon flux, femtosecond pulses, full transverse coherence, partial temporal coherence (SASE), and narrow spectral lines with seeding techniques. New developments in electron accelerators and radiation production can potentially lead to more compact sources of coherent X-rays.

  19. Intranet | APS X-ray Science Division

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    IT Helpdesk Stockroom Catalog | Shopping Cart | Stockroom (Bldg. 401) 2-9082 Key Request Phone Request Argonne Internal Resources: 401 Grill Inside Argonne AMOS, GatePass,...

  20. X-ray Emission from Thunderstorms and Lightning

    ScienceCinema (OSTI)

    Dwyer, Joseph [Florida Institute of Technology, Melbourne, Florida, United States

    2010-01-08

    How lightning is initiated in the relatively low electric fields inside thunderclouds and how it can then propagate for tens of kilometers through virgin air are two of the great unsolved problems in the atmospheric sciences.  Until very recently it was believed that lightning was entirely a conventional discharge, involving only low-energy (a few eV) electrons.  This picture changed completely a few years ago with the discovery of intense x-ray emission from both natural cloud-to-ground lightning and rocket-triggered lightning.  This energetic emission cannot be produced by a conventional discharge, and so the presence of x-rays strongly implies that runaway breakdown plays a role in lightning processes.  During runaway breakdown, electrons are accelerated through air to nearly the speed of light by strong electric fields.  These runaway electrons then emit bremsstrahlung x-rays and gamma-rays during collisions with air.  Indeed, the x-ray and gamma-ray emission produced by runaway breakdown near the tops of thunderstorms is bright enough to be seen from outer space, 600 km away.  As a result, the physics used for decades to describe thunderstorm electrification and lightning discharges is incomplete and needs to be revisited. 

  1. 5th Annual SSRL School on Synchrotron X-ray Scattering Techniques...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Web | People Search SSRL Go 5th Annual SSRL School on Synchrotron X-ray Scattering Techniques in Materials and Environmental Sciences: Theory and Application June 1-3, 2010...

  2. Beyond 3-D X-ray Imaging: Methodology Development and Applications...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Beyond 3-D X-ray Imaging: Methodology Development and Applications in Material Science Thursday, September 6, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Yijin Liu Seminar There was a...

  3. New Directions in X-Ray Light Sources or Fiat Lux: what's under the dome and watching atoms with x-rays (LBNL Summer Lecture Series)

    ScienceCinema (OSTI)

    Falcone, Roger

    2011-04-28

    Summer Lecture Series 2008: Molecular movies of chemical reactions and material phase transformations need a strobe of x-rays, the penetrating light that reveals how atoms and molecules assemble in chemical and biological systems and complex materials. Roger Falcone, Director of the Advanced Light Source,will discuss a new generation of x ray sources that will enable a new science of atomic dynamics on ultrafast timescales.

  4. Probing convex polygons with X-rays

    SciTech Connect (OSTI)

    Edelsbrunner, H.; Skiena, S.S. )

    1988-10-01

    An X-ray probe through a polygon measures the length of intersection between a line and the polygon. This paper considers the properties of various classes of X-ray probes, and shows how they interact to give finite strategies for completely describing convex n-gons. It is shown that (3n/2)+6 probes are sufficient to verify a specified n-gon, while for determining convex polygons (3n-1)/2 X-ray probes are necessary and 5n+O(1) sufficient, with 3n+O(1) sufficient given that a lower bound on the size of the smallest edge of P is known.

  5. Sandia National Laboratories: X-ray vision

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    The Sandia-developed X-Ray Toolkit, or XTK, is a specialized X-ray visualization tool to help bomb disposal squads make fast, accurate, and precise assessments of potentially dangerous devices such as pipe bombs and IEDs. The image here, captured via the XTK software package using its unique image-stitching capability, shows the inner workings of a mock IED. Facebook Twitter YouTube Flickr RSS News X-ray vision By Nancy Salem Photography By Randy Montoya Thursday, September 01, 2016 Sandia, UNM

  6. Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Miaja-Avila, L.; O'Neil, G. C.; Uhlig, J.; Cromer, C. L.; Dowell, M. L.; Jimenez, R.; Hoover, A. S.; Silverman, K. L.; Ullom, J. N.

    2015-03-02

    We describe a laser-driven x-ray plasma source designed for ultrafast x-ray absorption spectroscopy. The source is comprised of a 1 kHz, 20 W, femtosecond pulsed infrared laser and a water target. We present the x-ray spectra as a function of laser energy and pulse duration. Additionally, we investigate the plasma temperature and photon flux as we vary the laser energy. We obtain a 75 μm FWHM x-ray spot size, containing ~106 photons/s, by focusing the produced x-rays with a polycapillary optic. Since the acquisition of x-ray absorption spectra requires the averaging of measurements from >107 laser pulses, we also presentmore » data on the source stability, including single pulse measurements of the x-ray yield and the x-ray spectral shape. In single pulse measurements, the x-ray flux has a measured standard deviation of 8%, where the laser pointing is the main cause of variability. Further, we show that the variability in x-ray spectral shape from single pulses is low, thus justifying the combining of x-rays obtained from different laser pulses into a single spectrum. Finally, we show a static x-ray absorption spectrum of a ferrioxalate solution as detected by a microcalorimeter array. Altogether, our results demonstrate that this water-jet based plasma source is a suitable candidate for laboratory-based time-resolved x-ray absorption spectroscopy experiments.« less

  7. Laser plasma x-ray source for ultrafast time-resolved x-ray absorption spectroscopy

    SciTech Connect (OSTI)

    Miaja-Avila, L.; O'Neil, G. C.; Uhlig, J.; Cromer, C. L.; Dowell, M. L.; Jimenez, R.; Hoover, A. S.; Silverman, K. L.; Ullom, J. N.

    2015-03-02

    We describe a laser-driven x-ray plasma source designed for ultrafast x-ray absorption spectroscopy. The source is comprised of a 1 kHz, 20 W, femtosecond pulsed infrared laser and a water target. We present the x-ray spectra as a function of laser energy and pulse duration. Additionally, we investigate the plasma temperature and photon flux as we vary the laser energy. We obtain a 75 μm FWHM x-ray spot size, containing ~106 photons/s, by focusing the produced x-rays with a polycapillary optic. Since the acquisition of x-ray absorption spectra requires the averaging of measurements from >107 laser pulses, we also present data on the source stability, including single pulse measurements of the x-ray yield and the x-ray spectral shape. In single pulse measurements, the x-ray flux has a measured standard deviation of 8%, where the laser pointing is the main cause of variability. Further, we show that the variability in x-ray spectral shape from single pulses is low, thus justifying the combining of x-rays obtained from different laser pulses into a single spectrum. Finally, we show a static x-ray absorption spectrum of a ferrioxalate solution as detected by a microcalorimeter array. Altogether, our results demonstrate that this water-jet based plasma source is a suitable candidate for laboratory-based time-resolved x-ray absorption spectroscopy experiments.

  8. X-rays Illuminate Ancient Archimedes Text

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ... DailyIndia.com: http:www.dailyindia.comshow48286.phpX-rays-illuminate-Archimedes-writings North Korea Times: http:story.northkoreatimes.comp.xct9ciddd8845aa60952db2id...

  9. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http://spie.org/OP318 August 28-29, 2013; San Diego, California, USA

  10. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light ... wavelengths relevant to atomic and molecular phenomena) with the advantages of ...

  11. X-ray grid-detector apparatus

    DOE Patents [OSTI]

    Boone, John M.; Lane, Stephen M.

    1998-01-27

    A hybrid grid-detector apparatus for x-ray systems wherein a microchannel plate structure has an air-interspaced grid portion and a phosphor/optical fluid-filled grid portion. The grids are defined by multiple adjacent channels separated by lead-glass septa. X-rays entering the air-interspaced grid portion at an angle of impingement upon the septa are attenuated, while non-impinging x-rays pass through to the phosphor/fluid filled portion. X-ray energy is converted to luminescent energy in the phosphor/fluid filled portion and the resultant beams of light are directed out of the phosphor/optical fluid filled portion to an imaging device.

  12. X-ray source for mammography

    DOE Patents [OSTI]

    Logan, C.M.

    1994-12-20

    An x-ray source is described utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms. 6 figures.

  13. X-Ray Nanoimaging: Instruments and Methods

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Nanoimaging: Instruments and Methods To be held as part of SPIE. http:spie.orgOP318 August 28-29, 2013; San Diego, California, USA

  14. Small Angle X-Ray Scattering Detector

    DOE Patents [OSTI]

    Hessler, Jan P.

    2004-06-15

    A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

  15. Femtosecond X-ray protein nanocrystallography

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    pulses from a hard-X-ray free-electron laser, the Linac Coherent Light Source (4). ... We mitigate the problem of radiation damage in crystallography by using pulses briefer ...

  16. Lensless X-Ray Imaging in Reflection

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    be reconstructed by a single Fourier transform; this is known as Fourier transform holography. The problem of getting sufficiently coherent x-rays onto and off of the sample in a...

  17. X-ray source for mammography

    DOE Patents [OSTI]

    Logan, Clinton M.

    1994-01-01

    An x-ray source utilizing anode material which shifts the output spectrum to higher energy and thereby obtains higher penetrating ability for screening mammography application, than the currently utilized anode material. The currently used anode material (molybdenum) produces an energy x-ray spectrum of 17.5/19.6 keV, which using the anode material of this invention (e.g. silver, rhodium, and tungsten) the x-ray spectrum would be in the 20-35 keV region. Thus, the anode material of this invention provides for imaging of breasts with higher than average x-ray opacity without increase of the radiation dose, and thus reduces the risk of induced breast cancer due to the radiation dose administered for mammograms.

  18. X-ray image intensifier phosphor

    DOE Patents [OSTI]

    D'Silva, A.P.; Fassel, V.A.

    1975-12-01

    Y/sub 1-x/Gd/sub x/.PO$sub 4$:Tb$sup 3+$ is an effective phosphor for use in X-ray intensifier screens and in nuclear radiation detection systems.

  19. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biological Imaging by Soft X-Ray Diffraction Microscopy Biological Imaging by Soft X-Ray Diffraction Microscopy Print Wednesday, 30 November 2005 00:00 Electron and x-ray...

  20. Optimization efforts in gated x-ray intensifiers (Conference...

    Office of Scientific and Technical Information (OSTI)

    Optimization efforts in gated x-ray intensifiers Citation Details In-Document Search Title: Optimization efforts in gated x-ray intensifiers Gated x-ray intensifiers are often ...

  1. X-ray laser driven gold targets

    SciTech Connect (OSTI)

    Petrova, Tz. B. Whitney, K. G.; Davis, J.

    2014-03-15

    The femtosecond population dynamics of gold irradiated by a coherent high-intensity (>10{sup 17} W/cm{sup 2}) x-ray laser pulse is investigated theoretically. There are two aspects to the assembled model. One is the construction of a detailed model of platinum-like gold inclusive of all inner-shell states that are created by photoionization of atomic gold and decay either by radiative or Auger processes. Second is the computation of the population dynamics that ensues when an x-ray pulse is absorbed in gold. The hole state generation depends on the intensity and wavelength of the driving x-ray pulse. The excited state populations reached during a few femtosecond timescales are high enough to generate population inversions, whose gain coefficients are calculated. These amplified lines in the emitted x-ray spectrum provide important diagnostics of the radiation dynamics and also suggest a nonlinear way to increase the frequency of the coherent output x-ray pulses relative to the frequency of the driver input x-ray pulse.

  2. Compton backscattered collmated X-ray source

    DOE Patents [OSTI]

    Ruth, Ronald D.; Huang, Zhirong

    2000-01-01

    A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

  3. Compton backscattered collimated x-ray source

    DOE Patents [OSTI]

    Ruth, R.D.; Huang, Z.

    1998-10-20

    A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

  4. Compton backscattered collimated x-ray source

    DOE Patents [OSTI]

    Ruth, Ronald D.; Huang, Zhirong

    1998-01-01

    A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

  5. Laboratory-size three-dimensional x-ray microscope with Wolter type I mirror optics and an electron-impact water window x-ray source

    SciTech Connect (OSTI)

    Ohsuka, Shinji; Ohba, Akira; Onoda, Shinobu; Nakamoto, Katsuhiro; Nakano, Tomoyasu; Miyoshi, Motosuke; Soda, Keita; Hamakubo, Takao

    2014-09-15

    We constructed a laboratory-size three-dimensional water window x-ray microscope that combines wide-field transmission x-ray microscopy with tomographic reconstruction techniques, and observed bio-medical samples to evaluate its applicability to life science research fields. It consists of a condenser and an objective grazing incidence Wolter type I mirror, an electron-impact type oxygen Kα x-ray source, and a back-illuminated CCD for x-ray imaging. A spatial resolution limit of around 1.0 line pairs per micrometer was obtained for two-dimensional transmission images, and 1-μm scale three-dimensional fine structures were resolved.

  6. Category:X-Ray Diffraction (XRD) | Open Energy Information

    Open Energy Info (EERE)

    X-Ray Diffraction (XRD) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Geothermalpower.jpg Looking for the X-Ray Diffraction (XRD) page? For detailed information on...

  7. Direct synchrotron x-ray measurements of local strain fields...

    Office of Scientific and Technical Information (OSTI)

    Accepted Manuscript: Direct synchrotron x-ray measurements of local strain fields in ... September 3, 2016 Title: Direct synchrotron x-ray measurements of local strain fields in ...

  8. Generation of Coherent X-Ray Radiation through Modulation Compression...

    Office of Scientific and Technical Information (OSTI)

    Generation of Coherent X-Ray Radiation through Modulation Compression Citation Details In-Document Search Title: Generation of Coherent X-Ray Radiation through Modulation Compression ...

  9. Experimental X-ray characterization of Gekko XII laser propagation...

    Office of Scientific and Technical Information (OSTI)

    Experimental X-ray characterization of Gekko XII laser propagation through very low ... Citation Details In-Document Search Title: Experimental X-ray characterization of Gekko ...

  10. Integrated X-ray Reflectivity Measurements for Elliptically Curved...

    Office of Scientific and Technical Information (OSTI)

    Title: Integrated X-ray Reflectivity Measurements for Elliptically Curved PET Crystals The elliptically curved pentaerythritol (PET) crystals used in the Supersnout 2 X-ray ...

  11. Simultaneous cryo X-ray ptychographic and fluorescence microscopy...

    Office of Scientific and Technical Information (OSTI)

    Accepted Manuscript: Simultaneous cryo X-ray ptychographic and fluorescence microscopy of green algae Prev Next Title: Simultaneous cryo X-ray ptychographic and fluorescence ...

  12. A Spatially Resolving X-ray Crystal Spectrometer for Measurement...

    Office of Scientific and Technical Information (OSTI)

    394 PPPL- 4394 A Spatially Resolving X-ray Crystal Spectrometer for Measurement of ... Fusion Links A spatially resolving x-ray crystal spectrometer for measurement of ...

  13. Development of a Spatially Resolving X-Ray Crystal Spectrometer...

    Office of Scientific and Technical Information (OSTI)

    Development of a Spatially Resolving X-Ray Crystal Spectrometer For Measurement of ... Links Development of a spatially resolving x-ray crystal spectrometer for measurement of ...

  14. Development Of a Spatially Resolving X-ray Crystal Spectrometer...

    Office of Scientific and Technical Information (OSTI)

    Technical Report: Development Of a Spatially Resolving X-ray Crystal Spectrometer For ... Title: Development Of a Spatially Resolving X-ray Crystal Spectrometer For Measurement Of ...

  15. Integrated X-Ray Reflectivity Measurements for Elliptically Curved...

    Office of Scientific and Technical Information (OSTI)

    Integrated X-Ray Reflectivity Measurements for Elliptically Curved PET Crystals Citation Details In-Document Search Title: Integrated X-Ray Reflectivity Measurements for ...

  16. X-ray transient absorption and picosecond IR spectroscopy of...

    Office of Scientific and Technical Information (OSTI)

    X-ray transient absorption and picosecond IR spectroscopy of fulvalene(tetracarbonyl)diruthenium on photoexcitation Citation Details In-Document Search Title: X-ray transient ...

  17. Experimental X-ray characterization of Gekko XII laser propagation...

    Office of Scientific and Technical Information (OSTI)

    Experimental X-ray characterization of Gekko XII laser propagation through very low ... Title: Experimental X-ray characterization of Gekko XII laser propagation through very low ...

  18. X-Ray Microcomputed Tomography for the Durability Characterization...

    Office of Scientific and Technical Information (OSTI)

    Conference: X-Ray Microcomputed Tomography for the Durability Characterization of Limestone Aggregate Citation Details In-Document Search Title: X-Ray Microcomputed Tomography for...

  19. A paediatric X-ray exposure chart

    SciTech Connect (OSTI)

    Knight, Stephen P

    2014-09-15

    The aim of this review was to develop a radiographic optimisation strategy to make use of digital radiography (DR) and needle phosphor computerised radiography (CR) detectors, in order to lower radiation dose and improve image quality for paediatrics. This review was based on evidence-based practice, of which a component was a review of the relevant literature. The resulting exposure chart was developed with two distinct groups of exposure optimisation strategies – body exposures (for head, trunk, humerus, femur) and distal extremity exposures (elbow to finger, knee to toe). Exposure variables manipulated included kilovoltage peak (kVp), target detector exposure and milli-ampere-seconds (mAs), automatic exposure control (AEC), additional beam filtration, and use of antiscatter grid. Mean dose area product (DAP) reductions of up to 83% for anterior–posterior (AP)/posterior–anterior (PA) abdomen projections were recorded postoptimisation due to manipulation of multiple-exposure variables. For body exposures, the target EI and detector exposure, and thus the required mAs were typically 20% less postoptimisation. Image quality for some distal extremity exposures was improved by lowering kVp and increasing mAs around constant entrance skin dose. It is recommended that purchasing digital X-ray equipment with high detective quantum efficiency detectors, and then optimising the exposure chart for use with these detectors is of high importance for sites performing paediatric imaging. Multiple-exposure variables may need to be manipulated to achieve optimal outcomes.

  20. Research Opportunities in Photochemistry, Solar Energy & Advanced X-ray

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Methods (Stanford, CA) - JCAP Research Opportunities in Photochemistry, Solar Energy & Advanced X-ray Methods (Stanford, CA) Research Opportunities in Photochemistry, Solar Energy & Advanced X-ray Methods (Stanford, CA) Thu, Jun 16, 2016 12:00pm 12:00 Fri, Jun 17, 2016 1:00pm 13:00 "The workshop is aimed at strengthening the connection between mission needs in Basic Energy Sciences and the X-ray facilities and in particular identifying key questions in solar energy conversion

  1. New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Wednesday, 31 August 2005 00:00 Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their

  2. Beyond crystallography: Diffractive imaging using coherent x-ray light sources

    SciTech Connect (OSTI)

    Miao, J.; Ishikawa, T.; Robinson, I. K.; Murnane, M. M.

    2015-04-30

    X-ray crystallography has been central to the development of many fields of science over the past century. It has now matured to a point that as long as good-quality crystals are available, their atomic structure can be routinely determined in three dimensions. However, many samples in physics, chemistry, materials science, nanoscience, geology, and biology are noncrystalline, and thus their three-dimensional structures are not accessible by traditional x-ray crystallography. Overcoming this hurdle has required the development of new coherent imaging methods to harness new coherent x-ray light sources. Here we review the revolutionary advances that are transforming x-ray sources and imaging in the 21st century.

  3. X-ray lithography using holographic images

    DOE Patents [OSTI]

    Howells, M.S.; Jacobsen, C.

    1997-03-18

    Methods for forming X-ray images having 0.25 {micro}m minimum line widths on X-ray sensitive material are presented. A holographic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required. 15 figs.

  4. X-ray lithography using holographic images

    DOE Patents [OSTI]

    Howells, Malcolm S.; Jacobsen, Chris

    1997-01-01

    Methods for forming X-ray images having 0.25 .mu.m minimum line widths on X-ray sensitive material are presented. A holgraphic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required.

  5. New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical

  6. XRS 2016 - 8th SSRL School on Synchrotron X-Ray Scattering Techniques

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    XRS 2016 - 8th SSRL School on Synchrotron X-Ray Scattering Techniques Home Registration Location Visitor Information Transportation About XRS 2016 - 8th SSRL School on Synchrotron X-Ray Scattering Techniques Materials and Environmental Sciences: Theory and Application June 21-23 2016 BL2-1 Feedback Form Agenda 2016 Agenda Maps & Directions Visiting SLAC This school will provide a practical users' guide to planning and conducting scattering measurements at SSRL beam lines, and will cover

  7. The Coherent X-ray Imaging instrument at the Linac Coherent Light Source

    SciTech Connect (OSTI)

    Liang, Mengning; Williams, Garth J.; Messerschmidt, Marc; Seibert, M. Marvin; Montanez, Paul A.; Hayes, Matt; Milathianaki, Despina; Aquila, Andrew; Hunter, Mark S.; Koglin, Jason E.; Schafer, Donald W.; Guillet, Serge; Busse, Armin; Bergan, Robert; Olson, William; Fox, Kay; Stewart, Nathaniel; Curtis, Robin; Miahnahri, Alireza Alan; Boutet, Sbastien

    2015-04-15

    The Coherent X-ray Imaging (CXI) instrument specializes in hard X-ray, in-vacuum, high power density experiments in all areas of science. Two main sample chambers, one containing a 100 nm focus and one a 1 m focus, are available, each with multiple diagnostics, sample injection, pumpprobe and detector capabilities. The flexibility of CXI has enabled it to host a diverse range of experiments, from biological to extreme matter.

  8. New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical

  9. New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    New Zone Plate for Soft X-Ray Microscopy at 15-nm Spatial Resolution Print Analytical tools that combine spatial resolution with elemental and chemical identification at the nanometer scale along with large penetration depth are indispensable for the life and physical sciences. The XM-1 soft x-ray microscope at the ALS produces images that not only reveal structures but can identify their chemical elements and measure magnetic and other properties as well. Now a new method for creating optical

  10. The Soft X-ray research instrument at the Linac Coherent Light Source

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Dakovski, Georgi L.; Heimann, Philip; Holmes, Michael; Krupin, Oleg; European XFEL, Hamburg; Minitti, Michael P.; Mitra, Ankush; Moeller, Stefan; Rowen, Michael; Schlotter, William F.; et al

    2015-04-02

    The Soft X-ray Research instrument provides intense ultrashort X-ray pulses in the energy range 280–2000 eV. A diverse set of experimental stations may be installed to investigate a broad range of scientific topics such as ultrafast chemistry, highly correlated materials, magnetism, surface science, and matter under extreme conditions. A brief description of the main instrument components will be given, followed by some selected scientific highlights.

  11. The Coherent X-ray Imaging instrument at the Linac Coherent Light Source

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Liang, Mengning; Williams, Garth J.; Messerschmidt, Marc; Seibert, M. Marvin; Montanez, Paul A.; Hayes, Matt; Milathianaki, Despina; Aquila, Andrew; Hunter, Mark S.; Koglin, Jason E.; et al

    2015-04-15

    The Coherent X-ray Imaging (CXI) instrument specializes in hard X-ray, in-vacuum, high power density experiments in all areas of science. Two main sample chambers, one containing a 100 nm focus and one a 1 µm focus, are available, each with multiple diagnostics, sample injection, pump–probe and detector capabilities. The flexibility of CXI has enabled it to host a diverse range of experiments, from biological to extreme matter.

  12. PROPX: An X-ray Manipulation Program

    SciTech Connect (OSTI)

    Kyrala, G.A.

    1992-05-01

    An interactive micro-computer program that performs some manipulations on an input x-ray spectrum is introduced and described. The program is used to calculate the effect of absorption of filters, transmission through fibers, responsivity of photocathodes, responsivity of absorptive detectors, folding of responses, plotting of cross sections, and calculation, as a function of electron temperature, of the response due to a bremsstrahlung spectrum. Fluorescence from the targets is not included. Two different x-ray libraries are offered, one covers the x-ray range 30--10,000 eV with 288 energy points, and the other covers the energy range 10 eV to 1 MeV with 250 energy points per decade. 7 refs.

  13. X-ray Thomson Scattering from Dense Plasmas

    SciTech Connect (OSTI)

    Glenzer, S

    2007-05-14

    Advances in the development of laser-produced x-ray sources have enabled a new class of high-energy density physics experiments. Powerful narrow-bandwidth x rays penetrate through short-lived hot dense states of matter and probe the physical properties with spectrally resolved x-ray scattering. Experiments from isochorically-heated plasmas with electron densities in the range of solid density and above have been demonstrated allowing for the first time exploration of the microscopic properties of dense matter regime close to strongly-coupled and Fermi degenerate conditions. Backscatter measurements have accessed the non-collective Compton scattering regime, which provides accurate diagnostic information on the temperature, density and ionization states. The forward scattering spectrum has been shown to measure the collective plasmon oscillations. Besides extracting the standard plasma parameters, density and temperature, forward scattering yields new observables such as a direct measure of collisions, quantum effects and detailed balance. In this talk, we will discuss new results important for applications of this technique for novel experiments in a wide range of research areas such as inertial confinement fusion, radiation-hydrodynamics, material science, and laboratory astrophysics.

  14. Automatic classification of time-variable X-ray sources

    SciTech Connect (OSTI)

    Lo, Kitty K.; Farrell, Sean; Murphy, Tara; Gaensler, B. M.

    2014-05-01

    To maximize the discovery potential of future synoptic surveys, especially in the field of transient science, it will be necessary to use automatic classification to identify some of the astronomical sources. The data mining technique of supervised classification is suitable for this problem. Here, we present a supervised learning method to automatically classify variable X-ray sources in the Second XMM-Newton Serendipitous Source Catalog (2XMMi-DR2). Random Forest is our classifier of choice since it is one of the most accurate learning algorithms available. Our training set consists of 873 variable sources and their features are derived from time series, spectra, and other multi-wavelength contextual information. The 10 fold cross validation accuracy of the training data is ∼97% on a 7 class data set. We applied the trained classification model to 411 unknown variable 2XMM sources to produce a probabilistically classified catalog. Using the classification margin and the Random Forest derived outlier measure, we identified 12 anomalous sources, of which 2XMM J180658.7–500250 appears to be the most unusual source in the sample. Its X-ray spectra is suggestive of a ultraluminous X-ray source but its variability makes it highly unusual. Machine-learned classification and anomaly detection will facilitate scientific discoveries in the era of all-sky surveys.

  15. Differential phase contrast X-ray imaging system and components

    DOE Patents [OSTI]

    Stutman, Daniel; Finkenthal, Michael

    2014-07-01

    A differential phase contrast X-ray imaging system includes an X-ray illumination system, a beam splitter arranged in an optical path of the X-ray illumination system, and a detection system arranged in an optical path to detect X-rays after passing through the beam splitter.

  16. Reflection soft X-ray microscope and method

    DOE Patents [OSTI]

    Suckewer, S.; Skinner, C.H.; Rosser, R.

    1993-01-05

    A reflection soft X-ray microscope is provided by generating soft X-ray beams, condensing the X-ray beams to strike a surface of an object at a predetermined angle, and focusing the X-ray beams reflected from the surface onto a detector, for recording an image of the surface or near surface features of the object under observation.

  17. Reflection soft X-ray microscope and method

    DOE Patents [OSTI]

    Suckewer, Szymon; Skinner, Charles H.; Rosser, Roy

    1993-01-01

    A reflection soft X-ray microscope is provided by generating soft X-ray beams, condensing the X-ray beams to strike a surface of an object at a predetermined angle, and focusing the X-ray beams reflected from the surface onto a detector, for recording an image of the surface or near surface features of the object under observation.

  18. Energy resolved X-ray grating interferometry

    SciTech Connect (OSTI)

    Thuering, T.; Stampanoni, M.; Institute for Biomedical Engineering, Swiss Federal Institute of Technology, Zurich ; Barber, W. C.; Iwanczyk, J. S.; Seo, Y.; Alhassen, F.

    2013-05-13

    Although compatible with polychromatic radiation, the sensitivity in X-ray phase contrast imaging with a grating interferometer is strongly dependent on the X-ray spectrum. We used an energy resolving detector to quantitatively investigate the dependency of the noise from the spectral bandwidth and to consequently optimize the system-by selecting the best energy band matching the experimental conditions-with respect to sensitivity maximization and, eventually, dose. Further, since theoretical calculations of the spectrum are usually limited due to non-ideal conditions, an energy resolving detector accurately quantifies the spectral changes induced by the interferometer including flux reduction and beam hardening.

  19. X-ray focal spot locating apparatus and method

    DOE Patents [OSTI]

    Gilbert, Hubert W.

    1985-07-30

    An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

  20. Multiple wavelength X-ray monochromators

    DOE Patents [OSTI]

    Steinmeyer, P.A.

    1992-11-17

    An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focusing the separate first and second output x-ray radiation wavelengths into separate focal points. 3 figs.

  1. Small Angle X-Ray Scattering Detector

    DOE Patents [OSTI]

    Hessler, Jan P.

    2004-06-15

    A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., q.sub.max /q.sub.min.congruent.100.

  2. Multiple wavelength X-ray monochromators

    DOE Patents [OSTI]

    Steinmeyer, Peter A.

    1992-11-17

    An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focussing the separate first and second output x-ray radiation wavelengths into separate focal points.

  3. SLAC All Access: X-ray Microscope

    ScienceCinema (OSTI)

    Nelson, Johanna; Liu, Yijin

    2014-06-13

    SLAC physicists Johanna Nelson and Yijin Liu give a brief overview of the X-ray microscope at the Stanford Synchrotron Radiation Lightsource (SSRL) that is helping improve rechargeable-battery technology by letting researchers peek into the inner workings of batteries as they operate.

  4. Femtosecond X-ray protein nanocrystallography

    SciTech Connect (OSTI)

    Chapman, Henry N.; Barty, Anton; White, Thomas A.; Aquila, Andrew; Schulz, Joachim; DePonte, Daniel P.; Martin, Andrew V.; Coppola, Nicola; Liang, Mengning; Caleman, Carl; Gumprecht, Lars; Stern, Stephan; Nass, Karol; Fromme, Petra; Hunter, Mark S.; Grotjohann, Ingo; Fromme, Raimund; Kirian, Richard A.; Weierstall, Uwe; Doak, R. Bruce; Schmidt, Kevin E.; Wang, Xiaoyu; Spence, John C. H.; Schlichting, Ilme; Epp, Sascha W.; Rolles, Daniel; Rudenko, Artem; Foucar, Lutz; Rudek, Benedikt; Erk, Benjamin; Schmidt, Carlo; Hömke, André; Strüder, Lothar; Ullrich, Joachim; Krasniqi, Faton; Lomb, Lukas; Shoeman, Robert L.; Bott, Mario; Barends, Thomas R. M.; Kuhnel, Kai-Uwe; Schroter, Claus-Dieter; Hartmann, Robert; Holl, Peter; Reich, Christian; Soltau, Heike; Kimmel, Nils; Weidenspointner, Georg; Pietschner, Daniel; Hauser, Günter; Herrmann, Sven; Schaller, Gerhard; Schopper, Florian; Andritschke, Robert; Boutet, Sébastien; Krzywinski, Jacek; Bostedt, Christoph; Messerschmidt, Marc; Bozek, John D.; Williams, Garth J.; Bogan, Michael J.; Hampton, Christina Y.; Sierra, Raymond G.; Starodub, Dmitri; Gorke, Hubert; Hau-Riege, Stefan P.; Frank, Matthias; Maia, Filipe R. N. C.; Hajdu, Janos; Timneanu, Nicusor; Seibert, M. Marvin; Andreasson, Jakob; Rocker, Andrea; Jönsson, Olof; Svenda, Martin; Holton, James M.; Marchesini, Stefano; Neutze, Richard; Schorb, Sebastian; Rupp, Daniela; Adolph, Marcus; Gorkhover, Tais; Andersson, Inger; Barthelmess, Miriam; Bajt, Saša; Hirsemann, Helmut; Potdevin, Guillaume; Graafsma, Heinz; Nilsson, Björn

    2011-02-03

    X-ray crystallography provides the vast majority of macromolecular structures, but the success of the method relies on growing crystals of sufficient size. In conventional measurements, the necessary increase in X-ray dose to record data from crystals that are too small leads to extensive damage before a diffraction signal can be recorded. It is particularly challenging to obtain large, well-diffracting crystals of membrane proteins, for which fewer than 300 unique structures have been determined despite their importance in all living cells. Here we present a method for structure determination where single-crystal X-ray diffraction ‘snapshots’ are collected from a fully hydrated stream of nanocrystals using femtosecond pulses from a hard-X-ray free-electron laser, the Linac Coherent Light Source. We prove this concept with nanocrystals of photosystem I, one of the largest membrane protein complexes. More than 3,000,000 diffraction patterns were collected in this study, and a three-dimensional data set was assembled from individual photosystem I nanocrystals (~200 nm to 2 μm in size). We mitigate the problem of radiation damage in crystallography by using pulses briefer than the timescale of most damage processes. This offers a new approach to structure determination of macromolecules that do not yield crystals of sufficient size for studies using conventional radiation sources or are particularly sensitive to radiation damage.

  5. X-ray spectroscopy of manganese clusters

    SciTech Connect (OSTI)

    Grush, M.M.

    1996-06-01

    Much of this thesis represents the groundwork necessary in order to probe Mn clusters more productively than with conventional Mn K-edge XAS and is presented in Part 1. Part 2 contains the application of x-ray techniques to Mn metalloproteins and includes a prognosis at the end of each chapter. Individual Mn oxidation states are more readily distinguishable in Mn L-edge spectra. An empirical mixed valence simulation routine for determining the average Mn oxidation state has been developed. The first Mn L-edge spectra of a metalloprotein were measured and interpreted. The energy of Mn K{beta} emission is strongly correlated with average Mn oxidation state. K{beta} results support oxidation states of Mn(III){sub 2}(IV){sub 2} for the S{sub 1} state of Photosystem II chemical chemically reduced preparations contain predominantly Mn(II). A strength and limitation of XAS is that it probes all of the species of a particular element in a sample. It would often be advantageous to selectively probe different forms of the same element. The first demonstration that chemical shifts in x-ray fluorescence energies can be used to obtain oxidation state-selective x-ray absorption spectra is presented. Spin-dependent spectra can also be used to obtain a more simplified picture of local structure. The first spin-polarized extended x-ray absorption fine structure using Mn K{beta} fluorescence detection is shown.

  6. High-resolution ab initio three-dimensional x-ray diffraction microscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Chapman, Henry N.; Barty, Anton; Marchesini, Stefano; Noy, Aleksandr; Hau-Riege, Stefan P.; Cui, Congwu; Howells, Malcolm R.; Rosen, Rachel; He, Haifeng; Spence, John C. H.; et al

    2006-01-01

    Coherent x-ray diffraction microscopy is a method of imaging nonperiodic isolated objects at resolutions limited, in principle, by only the wavelength and largest scattering angles recorded. We demonstrate x-ray diffraction imaging with high resolution in all three dimensions, as determined by a quantitative analysis of the reconstructed volume images. These images are retrieved from the three-dimensional diffraction data using no a priori knowledge about the shape or composition of the object, which has never before been demonstrated on a nonperiodic object. We also construct two-dimensional images of thick objects with greatly increased depth of focus (without loss of transverse spatialmore » resolution). These methods can be used to image biological and materials science samples at high resolution with x-ray undulator radiation and establishes the techniques to be used in atomic-resolution ultrafast imaging at x-ray free-electron laser sources.« less

  7. Comparison of synchrotron x-ray microanalysis with electron and proton microscopy for individual particle analysis

    SciTech Connect (OSTI)

    Janssens, K.H.; van Langevelde, F.; Adams, F.C.; Vis, R.D.; Sutton, S.R.; Rivers, M.L.; Jones, K.W.; Bowen, D.K.

    1991-12-31

    This paper is concerned with the evaluation of the use of synchrotron/radiation induced x-ray fluorescences ({mu}-SRXRF) as implemented at two existing X-ray microprobes for the analysis of individual particles. As representative environmental particulates, National Institutes of Science and Technology (NIST) K227, K309, K441 and K961 glass microspheres were analyzed using two types of X-ray micro probes: the white light microprobe at beamline X26A of the monochromatic (15 keV) X-ray microprobe at station 7.6 of the SRS. For reference, the particles were also analyzed with microanalytical techniques more commonly employed for individual particles analysis such as EPMA and micro-PIXE.

  8. Comparison of synchrotron x-ray microanalysis with electron and proton microscopy for individual particle analysis

    SciTech Connect (OSTI)

    Janssens, K.H.; van Langevelde, F.; Adams, F.C. ); Vis, R.D. ); Sutton, S.R.; Rivers, M.L. ); Jones, K.W. ); Bowen, D.K. )

    1991-01-01

    This paper is concerned with the evaluation of the use of synchrotron/radiation induced x-ray fluorescences ({mu}-SRXRF) as implemented at two existing X-ray microprobes for the analysis of individual particles. As representative environmental particulates, National Institutes of Science and Technology (NIST) K227, K309, K441 and K961 glass microspheres were analyzed using two types of X-ray micro probes: the white light microprobe at beamline X26A of the monochromatic (15 keV) X-ray microprobe at station 7.6 of the SRS. For reference, the particles were also analyzed with microanalytical techniques more commonly employed for individual particles analysis such as EPMA and micro-PIXE.

  9. Bandpass x-ray diode and x-ray multiplier detector

    DOE Patents [OSTI]

    Wang, C.L.

    1982-09-27

    An absorption-edge of an x-ray absorption filter and a quantum jump of a photocathode determine the bandpass characteristics of an x-ray diode detector. An anode, which collects the photoelectrons emitted by the photocathode, has enhanced amplification provided by photoelectron-multiplying means which include dynodes or a microchannel-plate electron-multiplier. Suppression of undesired high frequency response for a bandpass x-ray diode is provided by subtracting a signal representative of energies above the passband from a signal representative of the overall response of the bandpass diode.

  10. Principles of femtosecond X-ray/optical cross-correlation with X-ray induced transient optical reflectivity in solids

    SciTech Connect (OSTI)

    Eckert, S. E-mail: martin.beye@helmholtz-berlin.de; Beye, M. E-mail: martin.beye@helmholtz-berlin.de; Pietzsch, A.; Quevedo, W.; Hantschmann, M.; Ochmann, M.; Huse, N.; Ross, M.; Khalil, M.; Minitti, M. P.; Turner, J. J.; Moeller, S. P.; Schlotter, W. F.; Dakovski, G. L.; Föhlisch, A.

    2015-02-09

    The discovery of ultrafast X-ray induced optical reflectivity changes enabled the development of X-ray/optical cross correlation techniques at X-ray free electron lasers worldwide. We have now linked through experiment and theory the fundamental excitation and relaxation steps with the transient optical properties in finite solid samples. Therefore, we gain a thorough interpretation and an optimized detection scheme of X-ray induced changes to the refractive index and the X-ray/optical cross correlation response.

  11. Making the Old New Again: Measuring Ultrashort X-ray Laser Pulses | U.S.

    Office of Science (SC) Website

    DOE Office of Science (SC) Making the Old New Again: Measuring Ultrashort X-ray Laser Pulses Basic Energy Sciences (BES) BES Home About Research Facilities Science Highlights Benefits of BES Funding Opportunities Basic Energy Sciences Advisory Committee (BESAC) Community Resources Contact Information Basic Energy Sciences U.S. Department of Energy SC-22/Germantown Building 1000 Independence Ave., SW Washington, DC 20585 P: (301) 903-3081 F: (301) 903-6594 E: Email Us More Information »

  12. X-ray imaging crystal spectrometer for extended X-ray sources

    DOE Patents [OSTI]

    Bitter, Manfred L.; Fraenkel, Ben; Gorman, James L.; Hill, Kenneth W.; Roquemore, A. Lane; Stodiek, Wolfgang; von Goeler, Schweickhard E.

    2001-01-01

    Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

  13. Structure and Dynamics of Polymer Nanocomposites by Grazing-Incidence X-Ray

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Techniques (Presentation) | Department of Energy Structure and Dynamics of Polymer Nanocomposites by Grazing-Incidence X-Ray Techniques (Presentation) Structure and Dynamics of Polymer Nanocomposites by Grazing-Incidence X-Ray Techniques (Presentation) Presented at the High Temperature Membrane Working Group (HTMWG) Meeting held on October 10, 2007 in Washington, D.C. htwmg_oct07_wang.pdf (1.78 MB) More Documents & Publications Block Copolymer Separators for Lithium Batteries FY 2004

  14. Rise time measurement for ultrafast X-ray pulses

    DOE Patents [OSTI]

    Celliers, Peter M.; Weber, Franz A.; Moon, Stephen J.

    2005-04-05

    A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

  15. Rise Time Measurement for Ultrafast X-Ray Pulses

    DOE Patents [OSTI]

    Celliers, Peter M.; Weber, Franz A.; Moon, Stephen J.

    2005-04-05

    A pump-probe scheme measures the rise time of ultrafast x-ray pulses. Conventional high speed x-ray diagnostics (x-ray streak cameras, PIN diodes, diamond PCD devices) do not provide sufficient time resolution to resolve rise times of x-ray pulses on the order of 50 fs or less as they are being produced by modern fast x-ray sources. Here, we are describing a pump-probe technique that can be employed to measure events where detector resolution is insufficient to resolve the event. The scheme utilizes a diamond plate as an x-ray transducer and a p-polarized probe beam.

  16. X-ray radiography for container inspection

    DOE Patents [OSTI]

    Katz, Jonathan I.; Morris, Christopher L.

    2011-06-07

    Arrangements of X-ray inspection systems are described for inspecting high-z materials in voluminous objects such as containers. Inspection methods may involve generating a radiographic image based on detected attenuation corresponding to a pulsed beams of radiation transmitted through a voluminous object. The pulsed beams of radiation are generated by a high-energy source and transmitted substantially downward along an incident angle, of approximately 1.degree. to 30.degree., to a vertical axis extending through the voluminous object. The generated radiographic image may be analyzed to detect on localized high attenuation representative of high-z materials and to discriminate high-z materials from lower and intermediate-z materials on the basis of the high density and greater attenuation of high-z material for higher energy (3-10 MeV) X-rays, and the compact nature of threatening masses of fissionable materials.

  17. Sample holder for X-ray diffractometry

    DOE Patents [OSTI]

    Hesch, Victor L.

    1992-01-01

    A sample holder for use with X-ray diffractometers with the capability to rotate the sample, as well as to adjust the position of the sample in the x, y, and z directions. Adjustment in the x direction is accomplished through loosening set screws, moving a platform, and retightening the set screws. Motion translators are used for adjustment in the y and z directions. An electric motor rotates the sample, and receives power from the diffractometer.

  18. High-intensity double-pulse X-ray free-electron laser

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Marinelli, A.; Ratner, D.; Lutman, A. A.; Turner, J.; Welch, J.; Decker, F. J.; Loos, H.; Behrens, C.; Gilevich, S.; Miahnahri, A. A.; et al

    2015-03-06

    The X-ray free-electron laser has opened a new era for photon science, improving the X-ray brightness by ten orders of magnitude over previously available sources. Similar to an optical laser, the spectral and temporal structure of the radiation pulses can be tailored to the specific needs of many experiments by accurately manipulating the lasing medium, that is, the electron beam. Here we report the generation of mJ-level two-colour hard X-ray pulses of few femtoseconds duration with an XFEL driven by twin electron bunches at the Linac Coherent Light Source. This performance represents an improvement of over an order of magnitudemore » in peak power over state-of-the-art two-colour XFELs. The unprecedented intensity and temporal coherence of this new two-colour X-ray free-electron laser enable an entirely new set of scientific applications, ranging from X-ray pump/X-ray probe experiments to the imaging of complex biological samples with multiple wavelength anomalous dispersion.« less

  19. High-intensity double-pulse X-ray free-electron laser

    SciTech Connect (OSTI)

    Marinelli, A.; Ratner, D.; Lutman, A. A.; Turner, J.; Welch, J.; Decker, F. J.; Loos, H.; Behrens, C.; Gilevich, S.; Miahnahri, A. A.; Vetter, S.; Maxwell, T. J.; Ding, Y.; Coffee, R.; Wakatsuki, S.; Huang, Z.

    2015-03-06

    The X-ray free-electron laser has opened a new era for photon science, improving the X-ray brightness by ten orders of magnitude over previously available sources. Similar to an optical laser, the spectral and temporal structure of the radiation pulses can be tailored to the specific needs of many experiments by accurately manipulating the lasing medium, that is, the electron beam. Here we report the generation of mJ-level two-colour hard X-ray pulses of few femtoseconds duration with an XFEL driven by twin electron bunches at the Linac Coherent Light Source. This performance represents an improvement of over an order of magnitude in peak power over state-of-the-art two-colour XFELs. The unprecedented intensity and temporal coherence of this new two-colour X-ray free-electron laser enable an entirely new set of scientific applications, ranging from X-ray pump/X-ray probe experiments to the imaging of complex biological samples with multiple wavelength anomalous dispersion.

  20. TU-A-9A-07: X-Ray Acoustic Computed Tomography (XACT): 100% Sensitivity to X-Ray Absorption

    SciTech Connect (OSTI)

    Xiang, L; Ahmad, M; Nikoozadeh, A; Pratx, G; Khuri-Yakub, B; Xing, L

    2014-06-15

    Purpose: To assess whether X-ray acoustic computed tomography (XACT) is more sensitive to X-ray absorption than that of the conventional X-ray imaging. Methods: First, a theoretical model was built to analyze the X-ray absorption sensitivity of XACT imaging and conventional X-ray imaging. Second, an XACT imaging system was developed to evaluate the X-ray induced acoustic signal generation as well as the sensitivity improvement over transmission x-ray imaging. Ultra-short x-ray pulses (60-nanosecond) were generated from an X-ray source operated at the energy of 150 kVp with a 10-Hz repetition rate. The X-ray pulse was synchronized with the acoustic detection via a x-ray scintillation triggering to acquire the X-ray induced acoustic signal. Results: Theoretical analysis shows that X-ray induced acoustic signal is sensitive only to the X-ray absorption, while completely insensitive to out the X-ray scattering and fluorescence. XACT has reduced background and increased contrast-to-noise ratio, and therefore has increased sensitivity compared to transmission x-ray imaging. For a 50-μm size, gadolinium insertion in tissue exposed to 40 keV X-rays; the sensitivity of XACT imaging is about 28.9 times higher than that of conventional X-ray imaging. Conclusion: X-ray acoustic computer tomography (XACT) as a new imaging modality combines X-ray absorption contrast and high ultrasonic resolution in a single modality. It is feasible to improve the imaging sensitivity with XACT imaging compared with conventional X-ray imaging. Taking advantage of the high ultrasonic resolution, it is possible to perform 3-D imaging with a single x-ray pulse with arrays of transducers without any mechanical motion of the imaging system. This single-shot capability offers the potential of reducing radiation dose by a factor of 1000, and imaging 100 times faster when compared to the conventional X-ray CT, and thus revolutionizing x-ray imaging applications in medicine and biology. The authors

  1. Ambient Pressure Photoelectron Spectroscopy Using Soft X-ray...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Ambient Pressure Photoelectron Spectroscopy Using Soft X-ray and Hard X-ray, and its applications in electrochemistry Friday, December 14, 2012 - 3:30pm SSRL, Bldg. 137, room 322...

  2. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis ALS X-Rays Shine a New Light on Catalysis Print Thursday, 21 May 2015 11:16 Electrocatalysts are responsible for expediting reactions in...

  3. Enabling X-ray free electron laser crystallography for challenging...

    Office of Scientific and Technical Information (OSTI)

    Enabling X-ray free electron laser crystallography for challenging biological systems from a limited number of crystals Citation Details In-Document Search Title: Enabling X-ray ...

  4. NIF and OMEGA X-Ray Environments Summary (Technical Report) ...

    Office of Scientific and Technical Information (OSTI)

    NIF and OMEGA X-Ray Environments Summary Citation Details In-Document Search Title: NIF and OMEGA X-Ray Environments Summary Abstract not provided. Authors: Fournier, K. B. 1 + ...

  5. A Spatially Resolving X-ray Crystal Spectrometer for Measurement...

    Office of Scientific and Technical Information (OSTI)

    A Spatially Resolving X-ray Crystal Spectrometer for Measurement of Ion-temperature and ... Citation Details In-Document Search Title: A Spatially Resolving X-ray Crystal ...

  6. Crystallization and preliminary X-ray crystallographic studies...

    Office of Scientific and Technical Information (OSTI)

    X-ray crystallographic studies of Drep-3, a DFF-related protein from Drosophila melanogaster Citation Details In-Document Search Title: Crystallization and preliminary X-ray ...

  7. Structure and Reactivity of X-ray Amorphous Uranyl Peroxide,...

    Office of Scientific and Technical Information (OSTI)

    Published Article: Structure and Reactivity of X-ray Amorphous Uranyl Peroxide, U 2 O 7 Prev Next Title: Structure and Reactivity of X-ray Amorphous Uranyl Peroxide, U 2 O 7 ...

  8. X-ray imaging of Nonlinear Resonant Gyrotropic Magnetic Vortex...

    Office of Scientific and Technical Information (OSTI)

    X-ray imaging of Nonlinear Resonant Gyrotropic Magnetic Vortex Core Motion in Circular Permalloy Disks Citation Details In-Document Search Title: X-ray imaging of Nonlinear ...

  9. X-ray photonic microsystems for the manipulation of synchrotron...

    Office of Scientific and Technical Information (OSTI)

    (MEMS) when combined with micro-optics have found a wide range of photonics applications. ... for X-rays, a new generation of photonics microsystems for X-ray wavelengths will ...

  10. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    While x-ray transparency will have immediate applications at x-ray light sources, the important result is that the findings lay a foundation for a broader spectrum of applications. ...

  11. NIF and OMEGA X-Ray Environments Summary (Technical Report) ...

    Office of Scientific and Technical Information (OSTI)

    NIF and OMEGA X-Ray Environments Summary Citation Details In-Document Search Title: NIF and OMEGA X-Ray Environments Summary You are accessing a document from the Department of ...

  12. Evaluating the variability of ceramics with x-ray fluorescence

    SciTech Connect (OSTI)

    Crown, P.L.; Schwalbe, L.A.; London, J.R.

    1984-01-01

    Our assessment of prehistoric trade in ceramics depends on our ability to identify and distinguish different sources of manufacture. For the American Southwest, archaeologists have proposed various models of ceramic manufacture and exchange. Until recently, conflicting hypotheses were tested mainly on the basis of petrographic analysis of nonplastic tempering materials. We have extended these analyses to include x-ray fluorescence (XRF). XRF provides a fast and inexpensive means of analyzing large numbers of samples. Since 1982, approximately 500 prehistoric sherds and 40 prepared clay and mineral samples have been examined with XRF. Multivariate statistical techniques have been applied to help identify groupings of samples with possible archaeological significance.

  13. The Science DMZ Eli Dart, Network Engineer ESnet Engineering Group

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Science DMZ Eli Dart, Network Engineer ESnet Engineering Group Winter 2011 Joint Techs Clemson, SC February 1, 2011 Lawrence Berkeley National Laboratory U.S. Department of Energy | Office of Science Overview Science Needs * Data tsunami, new science processes * Current problems * Consequences What is important and how to accomplish it * Important aspects of the network for users * Science DMZ architecture Security Concerns Recap Resources Lawrence Berkeley National Laboratory U.S. Department of

  14. Femtosecond laser-electron x-ray source

    DOE Patents [OSTI]

    Hartemann, Frederic V.; Baldis, Hector A.; Barty, Chris P.; Gibson, David J.; Rupp, Bernhard

    2004-04-20

    A femtosecond laser-electron X-ray source. A high-brightness relativistic electron injector produces an electron beam pulse train. A system accelerates the electron beam pulse train. The femtosecond laser-electron X-ray source includes a high intra-cavity power, mode-locked laser and an x-ray optics system.

  15. X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO)

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Henke, B. L.; Gullikson, E. M.; Davis, J. C.

    The primary interactions of low-energy x-rays within condensed matter, viz. photoabsorption and coherent scattering, are described for photon energies outside the absorption threshold regions by using atomic scattering factors. The atomic scattering factors may be accurately determined from the atomic photoabsorption cross sections using modified Kramers-Kronig dispersion relations. From a synthesis of the currently available experimental data and recent theoretical calculations for photoabsorption, the angle-independent, forward-scattering components of the atomic scattering factors have been thus semiempirically determined and tabulated here for 92 elements and for the region 50-30,000 eV. Atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction. The incoherent scattering contributions that become significant for the light elements at the higher photon energies are similarly determined. The basic x-ray interaction relations that are used in applied x-ray physics are presented here in terms of the atomic scattering factors. The bulk optical constants are also related to the atomic scattering factors. These atomic and optical relations are applied to the detailed calculation of the reflectivity characteristics of a series of practical x-ray mirror, multilayer, and crystal monochromators. Comparisons of the results of this semiempirical,"atom-like", description of x-ray interactions for the low-energy region with those of experiment and ab initio theory are presented.

  16. Different X-ray spectral evolution for black hole X-ray binaries in dual tracks of radio-X-ray correlation

    SciTech Connect (OSTI)

    Cao, Xiao-Feng; Wu, Qingwen; Dong, Ai-Jun

    2014-06-10

    Recently, an 'outlier' track of radio-X-ray correlation was found, which is much steeper than the former universal correlation, where dual tracks were speculated to be triggered by different accretion processes. In this work, we test this issue by exploring hard X-ray spectral evolution in four black-hole X-ray binaries with multiple, quasi-simultaneous radio and X-ray observations. First, we find that hard X-ray photon indices, Γ, are negatively and positively correlated with X-ray fluxes when the X-ray flux, F{sub 3-9} {sub keV}, is below and above a critical flux, F{sub X,} {sub crit}, which are consistent with predictions of the advection-dominated accretion flow and the disk-corona model, respectively. Second, and most importantly, we find that the radio-X-ray correlations are also clearly different when the X-ray fluxes are higher and lower than the critical flux as defined by X-ray spectral evolution. The data points with F{sub 3-9} {sub keV} ≳ F{sub X,} {sub crit} have a steeper radio-X-ray correlation (F{sub X}∝F{sub R}{sup b} and b ∼ 1.1-1.4), which roughly forms the ''outlier'' track. However, the data points with anti-correlation of Γ – F{sub 3-9} {sub keV} either stay in the universal track with b ∼ 0.61 or stay in the transition track (from the universal to 'outlier' tracks or vice versa). Therefore, our results support that the universal and ''outlier'' tracks of radio-X-ray correlations are regulated by radiatively inefficient and radiatively efficient accretion model, respectively.

  17. X-Ray Imaging Crystal Spectrometer for Extended X-Ray Sources

    SciTech Connect (OSTI)

    Bitter, Manfred L.; Fraekel, Benjamin; Gorman, James L.; Hill, Kenneth W.; Roquemore, Lane A.; Stodiek, Wolfgang; Goeler, Schweickhard von

    1999-05-01

    Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokamak fusion experiment to provide spatially and temporally resolved data on plasma parameters such as ion temperature, toroidal and poloidal rotation, electron temperature, impurity ion charge-state distributions, and impurity transport. The imaging properties of these spherically or toroidally curved crystals provide both spectrally and spatially resolved X-ray data from the plasma using only one small spherically or toroidally curved crystal, thus eliminating the requirement for a large array of crystal spectrometers and the need to cross-calibrate the various crystals.

  18. Development of a Novel Tunable X-Ray Source for the RPI-LINAC

    SciTech Connect (OSTI)

    Y. Danon; R.C. Block

    2004-11-30

    This document summarizes the results of a three year effort to develop a parametric x-ray (PXR) source. The emphasis of this research was to demonstrate production of high yield monoenergetic x-rays. Production of PXR is accomplished by placing a crystal in a relativistic electron beam. The process was first demonstrated in 1985 in Russia. Numerous papers were written about the characteristics of PXR from both experimental and theoretical perspectives. The advantage of PXR over other monoenergetic x-ray sources is that it is produced at large angle relative to the electron beam and at high intensity. None of the previous work described in the literature capitalized on this effect to study what is required in order to generate an effective monoenergetic x-ray source that can be used for practical applications. The work summarized here describes the process done in order to optimize the PXR production process by selecting an appropriate crystal and the optimal conditions. The research focused on production of 18 keV x-rays which are suitable for mammography however the results are not limited to this application or energy range. We are the first group to demonstrate x-ray imaging using PXR. Such sources can improve current medical imaging modalities. More research is required in order to design a prototype of a compact source.

  19. Digital X-ray Pipe Inspector Software

    Energy Science and Technology Software Center (OSTI)

    2009-10-29

    The Digital X-ray Pipe Inspector software requires a digital x-ray image of a pipe as input to the program, such as the image in Attachment A Figure 1. The image may be in a variety of software formats such as bitmap, jpeg, tiff, DICOM or DICONDE. The software allows the user to interactively select a region of interest from the image for analysis. This software is used to analyze digital x-ray images of pipes tomore » evaluate loss of wall thickness. The software specifically provides tools to analyze the image in (a) the pipe walls, (b) between the pipe walls. Traditional software uses only the information at the pipe wall while this new software also evaluates the image between the pipewalls. This makes the inspection process faster, more thorough, more efficient, and reduces expensive reshots. Attachment A Figure 2 shows a region of interest (a green box) drawn by the user around an anomaly in the pipe wall. This area is automatically analyzed by the external pipe wall tool with the result shown in Attachment A Figure 3. The edges of the pipe wall are detected and highlighted in yellow and areas where the wall thickness in less the the minimum wall threshold are shown in red. These measurements are typically made manually in other software programs, which lead to errors and inconsistency because the location of the edges are estimated by the user. Attachment A Figure 4 shows a region of interest (a green box) drawn by the user between the pipe walls. As can be seen there are intensity anomalies that correspond to wall defects. However, this information is not used directly by other software programs. In order to fully investigate these anomalies, the pipe would be reinspected in a different orientation to attempt to obtain a view of the anomaly in the pipe wall rather than the interior of the pipe. The pipe may need to be x-rayed a number of times to obtain the correct orientation. This is very costly and time consuming. The new software can perform the

  20. Holographic Methods in X-ray Crystallography

    Energy Science and Technology Software Center (OSTI)

    1995-07-28

    The holographic method makes use of partially modeled electron density and experimentally-measured structure factor amplitudes to recover electron density corresponding to the unmodeled part of a crystal structure. This paper describes a fast algorithm that makes it possible to apply the holographic method to sizable crystallographic problems. The algorithm uses positivity constraints on the electron density, and can incorporate a target electron density, making it similar to solvent flattening. Using both synthetic and experimental data,more » we assess the potential for applying the holographic method to macromolecular x-ray crystallography.« less

  1. Apparatus for monitoring X-ray beam alignment

    DOE Patents [OSTI]

    Steinmeyer, P.A.

    1991-10-08

    A self-contained, hand-held apparatus is provided for monitoring alignment of an X-ray beam in an instrument employing an X-ray source. The apparatus includes a transducer assembly containing a photoresistor for providing a range of electrical signals responsive to a range of X-ray beam intensities from the X-ray beam being aligned. A circuit, powered by a 7.5 VDC power supply and containing an audio frequency pulse generator whose frequency varies with the resistance of the photoresistor, is provided for generating a range of audible sounds. A portion of the audible range corresponds to low X-ray beam intensity. Another portion of the audible range corresponds to high X-ray beam intensity. The transducer assembly may include an a photoresistor, a thin layer of X-ray fluorescent material, and a filter layer transparent to X-rays but opaque to visible light. X-rays from the beam undergoing alignment penetrate the filter layer and excite the layer of fluorescent material. The light emitted from the fluorescent material alters the resistance of the photoresistor which is in the electrical circuit including the audio pulse generator and a speaker. In employing the apparatus, the X-ray beam is aligned to a complete alignment by adjusting the X-ray beam to produce an audible sound of the maximum frequency. 2 figures.

  2. Apparatus for monitoring X-ray beam alignment

    DOE Patents [OSTI]

    Steinmeyer, Peter A.

    1991-10-08

    A self-contained, hand-held apparatus is provided for minitoring alignment of an X-ray beam in an instrument employing an X-ray source. The apparatus includes a transducer assembly containing a photoresistor for providing a range of electrical signals responsive to a range of X-ray beam intensities from the X-ray beam being aligned. A circuit, powered by a 7.5 VDC power supply and containing an audio frequency pulse generator whose frequency varies with the resistance of the photoresistor, is provided for generating a range of audible sounds. A portion of the audible range corresponds to low X-ray beam intensity. Another portion of the audible range corresponds to high X-ray beam intensity. The transducer assembly may include an a photoresistor, a thin layer of X-ray fluorescent material, and a filter layer transparent to X-rays but opaque to visible light. X-rays from the beam undergoing alignment penetrate the filter layer and excite the layer of fluorescent material. The light emitted from the fluorescent material alters the resistance of the photoresistor which is in the electrical circuit including the audio pulse generator and a speaker. In employing the apparatus, the X-ray beam is aligned to a complete alignment by adjusting the X-ray beam to produce an audible sound of the maximum frequency.

  3. RYLLA. [X-ray transport code

    SciTech Connect (OSTI)

    Hyde, R.A.

    1983-06-08

    This paper describes a computer code, RYLLA, which models the deposition of x-rays into thin metal slabs, and transports the resulting photoelectrons, finding the distribution of electrons leaving the slab from both the front and back surfaces. The slab must be homogeneous, but can contain a mixture of up to 5 different elements. Due to the short electron mean free path at low electron energies, RYLLA should be used only for studying thin slabs, roughly < 100 mg/cm/sup 2/ for low Z metals, and < 10 mg/cm/sup 2/ for high Z metals. X-ray energies should be in the range of 1 to 150 keV, as they are deposited only via photoionization and Compton scattering processes. Following photoionization, a hole exists in the electron cloud of the absorbing atom. This fills either by Auger or fluoresence, resulting in lower energy holes which are also filled. Fluoresence photons are transported and absorbed in the same manner as the primary photons, except that they are isotropically produced. Once all photons have been transported and absorbed, and all holes have been filled, a space- and energy-dependent electron source spectrum has been obtained. This is used in a discrete ordinate expansion solution of the 1-D transport equation, which gives the output electron spectra at the two slab surfaces. This paper discusses both the physics and coding of RYLLA. Examples of user input are given, as are some comparisons with other codes.

  4. High-energy and Ultrafast X-Ray Imaging Technologies and Applications

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    August » High-energy and Ultrafast X-Ray Imaging Technologies and Applications High-energy and Ultrafast X-Ray Imaging Technologies and Applications WHEN: Aug 02, 2016 8:00 AM - Aug 03, 2016 5:00 PM WHERE: Hilton Santa Fe at Buffalo Thunder CONTACT: Zhehui (Jeff) Wang (505) 665-5353 CATEGORY: Community Science TYPE: Conference INTERNAL: Calendar Login Event Description The goal of this workshop is to gather leading experts in the fields related to ultrafast high-energy photon imaging and

  5. A laboratory-based hard x-ray monochromator for high-resolution x-ray emission spectroscopy and x-ray absorption near edge structure measurements

    SciTech Connect (OSTI)

    Seidler, G. T. Mortensen, D. R.; Remesnik, A. J.; Pacold, J. I.; Ball, N. A.; Barry, N.; Styczinski, M.; Hoidn, O. R.

    2014-11-15

    We report the development of a laboratory-based Rowland-circle monochromator that incorporates a low power x-ray (bremsstrahlung) tube source, a spherically bent crystal analyzer, and an energy-resolving solid-state detector. This relatively inexpensive, introductory level instrument achieves 1-eV energy resolution for photon energies of ∼5 keV to ∼10 keV while also demonstrating a net efficiency previously seen only in laboratory monochromators having much coarser energy resolution. Despite the use of only a compact, air-cooled 10 W x-ray tube, we find count rates for nonresonant x-ray emission spectroscopy comparable to those achieved at monochromatized spectroscopy beamlines at synchrotron light sources. For x-ray absorption near edge structure, the monochromatized flux is small (due to the use of a low-powered x-ray generator) but still useful for routine transmission-mode studies of concentrated samples. These results indicate that upgrading to a standard commercial high-power line-focused x-ray tube or rotating anode x-ray generator would result in monochromatized fluxes of order 10{sup 6}–10{sup 7} photons/s with no loss in energy resolution. This work establishes core technical capabilities for a rejuvenation of laboratory-based hard x-ray spectroscopies that could have special relevance for contemporary research on catalytic or electrical energy storage systems using transition-metal, lanthanide, or noble-metal active species.

  6. Advances in x-ray computed microtomography at the NSLS

    SciTech Connect (OSTI)

    Dowd, B.A.; Andrews, A.B.; Marr, R.B.; Siddons, D.P.; Jones, K.W.; Peskin, A.M.

    1998-08-01

    The X-Ray Computed Microtomography workstation at beamline X27A at the NSLS has been utilized by scientists from a broad range of disciplines from industrial materials processing to environmental science. The most recent applications are presented here as well as a description of the facility that has evolved to accommodate a wide variety of materials and sample sizes. One of the most exciting new developments reported here resulted from a pursuit of faster reconstruction techniques. A Fast Filtered Back Transform (FFBT) reconstruction program has been developed and implemented, that is based on a refinement of the gridding algorithm first developed for use with radio astronomical data. This program has reduced the reconstruction time to 8.5 sec for a 929 x 929 pixel{sup 2} slice on an R10,000 CPU, more than 8x reduction compared with the Filtered Back-Projection method.

  7. Emerging trends in X-ray spectroscopic studies of plasma produced by intense laser beams

    SciTech Connect (OSTI)

    Arora, V.; Chakera, J. A.; Naik, P. A.; Gupta, P. D.

    2015-07-31

    X-ray line emission from hot dense plasmas, produced by ultra-short high intensity laser systems, has been studied experimentally in recent years for applications in materials science as well as for back-lighter applications. By virtue of the CPA technology, several laser facilities delivering pulses with peak powers in excess of one petawatt (focused intensities > 10{sup 20} W-cm{sup −2}) have either been commissioned across the globe during the last few years or are presently under construction. On the other hand, hard x-ray sources on table top, generating ultra-short duration x-rays at a repetition rate up to 10 kHz, are routinely available for time resolved x-ray diffraction studies. In this paper, the recent experiments on x-ray spectroscopic studies of plasma produced by 45 fs, Ti:sapphire laser pulses (focused iintensity > 10{sup 18} W-cm{sup −2}) at RRCAT Indore will be presented.

  8. Optimization of X-ray tomography through a cooperative computing system in grid

    SciTech Connect (OSTI)

    Hasan, Moin Goraya, Major Singh

    2015-08-28

    Cooperative Computing implemented as Cooperative Computing System (CCS) in grid has been proved a considerably reliable technique to execute the tasks with real time constraints in a grid environment. This technique can be applied in many high performance distributed computing applications. HPC has a large number of applications in various fields of physics. One such application in radiation physics is X-ray tomography. X-Ray tomography contains numerous applications in various fields of science, technology and research. As the technology is changing from analog to digital in almost all the scenarios, this paper presents an idea towards the attachment of X-ray tomography assembly to HPC environment so as to obtain the highly reliable optimization.

  9. Gray scale x-ray mask

    DOE Patents [OSTI]

    Morales, Alfredo M.; Gonzales, Marcela

    2006-03-07

    The present invention describes a method for fabricating an embossing tool or an x-ray mask tool, providing microstructures that smoothly vary in height from point-to-point in etched substrates, i.e., structure which can vary in all three dimensions. The process uses a lithographic technique to transfer an image pattern in the surface of a silicon wafer by exposing and developing the resist and then etching the silicon substrate. Importantly, the photoresist is variably exposed so that when developed some of the resist layer remains. The remaining undeveloped resist acts as an etchant barrier to the reactive plasma used to etch the silicon substrate and therefore provides the ability etch structures of variable depths.

  10. Gated monochromatic x-ray imager

    SciTech Connect (OSTI)

    Oertel, J.A.; Archuleta, T.; Clark, L.

    1995-09-01

    We have recently developed a gated monochromatic x-ray imaging diagnostic for the national Inertial-Confinement Fusion (ICF) program. This new imaging system will be one of the primary diagnostics to be utilized on University of Rochester`s Omega laser fusion facility. The new diagnostic is based upon a Kirkpatrick-Baez (KB) microscope dispersed by diffraction crystals, as first described by Marshall and Su. The dispersed images are gated by four individual proximity focused microchannel plates and recorded on film. Spectral coverage is tunable up to 8 keV, spectral resolution has been measured at 20 eV, temporal resolution is 80 ps, and spatial resolution is better than 10 {mu}m.

  11. Towards simultaneous measurements of electronic and structural properties in ultra-fast x-ray free electron laser absorption spectroscopy experiments

    SciTech Connect (OSTI)

    Gaudin, J.; Fourment, C.; Cho, B. I.; Engelhorn, K.; Galtier, E.; Harmand, M.; Leguay, P. M.; Lee, H. J.; Nagler, B.; Nakatsutsumi, M.; Ozkan, C.; Strmer, M.; Toleikis, S.; Tschentscher, Th.; Heimann, P. A.; Dorchies, F.

    2014-04-17

    The rapidly growing ultrafast science with X-ray lasers unveils atomic scale processes with unprecedented time resolution bringing the so called molecular movie within reach. X-ray absorption spectroscopy is one of the most powerful x-ray techniques providing both local atomic order and electronic structure when coupled with ad-hoc theory. Collecting absorption spectra within few x-ray pulses is possible only in a dispersive setup. We demonstrate ultrafast time-resolved measurements of the LIII-edge x-ray absorption near-edge spectra of irreversibly laser excited Molybdenum using an average of only few x-ray pulses with a signal to noise ratio limited only by the saturation level of the detector. The simplicity of the experimental set-up makes this technique versatile and applicable for a wide range of pump-probe experiments, particularly in the case of non-reversible processes.

  12. Towards simultaneous measurements of electronic and structural properties in ultra-fast x-ray free electron laser absorption spectroscopy experiments

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Gaudin, J.; Fourment, C.; Cho, B. I.; Engelhorn, K.; Galtier, E.; Harmand, M.; Leguay, P. M.; Lee, H. J.; Nagler, B.; Nakatsutsumi, M.; et al

    2014-04-17

    The rapidly growing ultrafast science with X-ray lasers unveils atomic scale processes with unprecedented time resolution bringing the so called “molecular movie” within reach. X-ray absorption spectroscopy is one of the most powerful x-ray techniques providing both local atomic order and electronic structure when coupled with ad-hoc theory. Collecting absorption spectra within few x-ray pulses is possible only in a dispersive setup. We demonstrate ultrafast time-resolved measurements of the LIII-edge x-ray absorption near-edge spectra of irreversibly laser excited Molybdenum using an average of only few x-ray pulses with a signal to noise ratio limited only by the saturation level ofmore » the detector. The simplicity of the experimental set-up makes this technique versatile and applicable for a wide range of pump-probe experiments, particularly in the case of non-reversible processes.« less

  13. Density gradient free electron collisionally excited x-ray laser

    DOE Patents [OSTI]

    Campbell, E.M.; Rosen, M.D.

    1984-11-29

    An operational x-ray laser is provided that amplifies 3p-3s transition x-ray radiation along an approximately linear path. The x-ray laser is driven by a high power optical laser. The driving line focused optical laser beam illuminates a free-standing thin foil that may be associated with a substrate for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the x-ray laser gain medium. The x-ray laser may be driven by more than one optical laser beam. The x-ray laser has been successfully demonstrated to function in a series of experimental tests.

  14. Soft x-ray reduction camera for submicron lithography

    DOE Patents [OSTI]

    Hawryluk, A.M.; Seppala, L.G.

    1991-03-26

    Soft x-ray projection lithography can be performed using x-ray optical components and spherical imaging lenses (mirrors), which form an x-ray reduction camera. The x-ray reduction is capable of projecting a 5x demagnified image of a mask onto a resist coated wafer using 4.5 nm radiation. The diffraction limited resolution of this design is about 135 nm with a depth of field of about 2.8 microns and a field of view of 0.2 cm[sup 2]. X-ray reflecting masks (patterned x-ray multilayer mirrors) which are fabricated on thick substrates and can be made relatively distortion free are used, with a laser produced plasma for the source. Higher resolution and/or larger areas are possible by varying the optic figures of the components and source characteristics. 9 figures.

  15. Soft x-ray reduction camera for submicron lithography

    DOE Patents [OSTI]

    Hawryluk, Andrew M.; Seppala, Lynn G.

    1991-01-01

    Soft x-ray projection lithography can be performed using x-ray optical components and spherical imaging lenses (mirrors), which form an x-ray reduction camera. The x-ray reduction is capable of projecting a 5x demagnified image of a mask onto a resist coated wafer using 4.5 nm radiation. The diffraction limited resolution of this design is about 135 nm with a depth of field of about 2.8 microns and a field of view of 0.2 cm.sup.2. X-ray reflecting masks (patterned x-ray multilayer mirrors) which are fabricated on thick substrates and can be made relatively distortion free are used, with a laser produced plasma for the source. Higher resolution and/or larger areas are possible by varying the optic figures of the components and source characteristics.

  16. Density gradient free electron collisionally excited X-ray laser

    DOE Patents [OSTI]

    Campbell, Edward M.; Rosen, Mordecai D.

    1989-01-01

    An operational X-ray laser (30) is provided that amplifies 3p-3s transition X-ray radiation along an approximately linear path. The X-ray laser (30) is driven by a high power optical laser. The driving line focused optical laser beam (32) illuminates a free-standing thin foil (34) that may be associated with a substrate (36) for improved structural integrity. This illumination produces a generally cylindrically shaped plasma having an essentially uniform electron density and temperature, that exists over a long period of time, and provides the X-ray laser gain medium. The X-ray laser (30) may be driven by more than one optical laser beam (32, 44). The X-ray laser (30) has been successfully demonstrated to function in a series of experimental tests.

  17. Femtosecond nanocrystallography using X-ray lasers for membrane protein

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    structure determination Femtosecond nanocrystallography using X-ray lasers for membrane protein structure determination Authors: Fromme, P., and Spence, J. C. H. Title: Femtosecond nanocrystallography using X-ray lasers for membrane protein structure determination Source: Current Opinion in Structural Biology Year: 2011 Volume: 21 Pages: 509-516 ABSTRACT: The invention of free electron X-ray lasers has opened a new era for membrane protein structure determination with the recent first

  18. ANL CT Reconstruction Algorithm for Utilizing Digital X-ray

    Energy Science and Technology Software Center (OSTI)

    2004-05-01

    Reconstructs X-ray computed tomographic images from large data sets known as 16-bit binary sinograms when using a massively parallelized computer architecture such as a Beowuif cluster by parallelizing the X-ray CT reconstruction routine. The algorithm uses the concept of generation of an image from carefully obtained multiple 1-D or 2-D X-ray projections. The individual projections are filtered using a digital Fast Fourier Transform. The literature refers to this as filtered back projection.

  19. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Wednesday, 29 August 2007 00:00 Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic

  20. Legacy of the X-Ray Laser Program

    SciTech Connect (OSTI)

    Nilsen, J.

    1993-08-06

    The X-Ray Laser Program has evolved from a design effort focusing on developing a Strategic Defense Initiative weapon that protects against Soviet ICBMs to a scientific project that is producing new technologies for industrial and medical research. While the great technical successes and failures of the X-ray laser itself cannot be discussed, this article presents the many significant achievements made as part of the X-ray laser effort that are now being used for other applications at LLNL.

  1. Magnetism studies using resonant, coherent, x-ray scattering | Stanford

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Synchrotron Radiation Lightsource Magnetism studies using resonant, coherent, x-ray scattering Monday, September 10, 2012 - 10:00am SLAC, Bldg. 137, Room 226 Keoki Seu Seminar: With the advent of free electron lasers there has been interest in using coherent x-rays to probe condensed matter systems. Resonant scattering with x-rays allow elemental specificity with magnetic contrast, and coherent light leads to speckle in the scattered pattern due to interference from waves exiting the sample.

  2. 14.05.14 RH Synchrotron X-ray - JCAP

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    High-Throughput Synchrotron X-Ray Experimentation for Combinatorial Phase Matching Gregoire, J. M. et al. High-throughput synchrotron X-ray diffraction for combinatorial phase mapping. Journal of Synchrotron Radiation 21, 1262-1268, DOI: 10.1107/s1600577514016488 (2014). Scientific Achievement Development of new synchrotron X-ray diffraction and fluorescence methods for rapid characterization of material libraries. Significance & impact First demonstration of prototype facility capable of

  3. X-ray interferometry with spherically bent crystals (abstract)

    SciTech Connect (OSTI)

    Koch, Jeffrey A.

    2001-01-01

    Recent progress in manufacturing high-quality spherically bent crystals allows highly monochromatic x-ray beams to be produced, and allows efficient x-ray imaging with {mu}m-scale resolution. This article explores some of the constraints for x-ray interferometry utilizing spherically bent crystals and laser-produced plasma sources, and discusses several shearing interferometer concepts that might be experimentally investigated.

  4. X-ray transmission movies of spontaneous dynamic events

    SciTech Connect (OSTI)

    Smilowitz, L.; Henson, B. F.; Holmes, M.; Novak, A.; Oschwald, D.; Dolgonos, P.; Qualls, B.

    2014-11-15

    We describe a new x-ray radiographic imaging system which allows for continuous x-ray transmission imaging of spontaneous dynamic events. We demonstrate this method on thermal explosions in three plastic bonded formulations of the energetic material octahydro-1,3,5,7-tetranitro-1,3,5,7-tetrazocine. We describe the x-ray imaging system and triggering developed to enable the continuous imaging of a thermal explosion.

  5. Bimolecular Imaging with femtosecond X-ray pulses | Stanford Synchrotron

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Radiation Lightsource Bimolecular Imaging with femtosecond X-ray pulses Wednesday, June 22, 2016 - 3:00pm SLAC, Redtail Hawk Conference Room 108A Speaker: Marvin Seibert, Uppsala University Program Description This talk will be part review, part outlook of the potential for imaging biological structures with fs X-ray pulses, from the first experiments at LCLS to the current single particle imaging initiative. Bimolecular Imaging with femtosecond X-ray pulses

  6. X-Ray Fluorescence (XRF) | Open Energy Information

    Open Energy Info (EERE)

    Dispersive Spectroscopy (WDS) typically performed using a SEM or EPMA, and X-Ray Diffraction (XRD) analyses. Rock Lab Analysis Core Analysis Cuttings Analysis Isotopic...

  7. XRMS: X-Ray Spectroscopy of Magnetic Solids

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    XRMS: X-Ray Spectroscopy of Magnetic Solids October 22-23, 2011 SLAC National Accelerator Laboratory, Menlo Park, CA More information...

  8. High intensity x-ray source using liquid gallium target

    DOE Patents [OSTI]

    Smither, Robert K.; Knapp, Gordon S.; Westbrook, Edwin M.; Forster, George A.

    1990-01-01

    A high intensity x-ray source that uses a flowing stream of liquid gallium as a target with the electron beam impinging directly on the liquid metal.

  9. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ALS X-Rays Shine a New Light on Catalysis Print Electrocatalysts are responsible for expediting reactions in many promising renewable energy technologies. However, the extreme...

  10. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    methods (see previous highlight, "Demonstration of Coherent X-Ray Diffraction Imaging"). Experimental diffraction data used as input to the difference map algorithm....

  11. Subject: Ames Blue Alert - X-ray Shutter Maintenance

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Ames Blue Alert - X-ray Shutter Maintenance Statement: This lesson learned involves an ... 4. Follow the manufacturers suggested maintenance schedule. 5. Follow the standard ...

  12. X-Ray Microscopy Capabilities | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Microscopy Capabilities The Hard X-Ray Nanoprobe (HXN) facility provides scanning fluorescence, scanning diffraction, and full-field transmission and tomographic imaging capabilities with a spatial resolution of 30 nm over a spectral range of 6-12 keV. Modes of Operation Full-Field Transmission Imaging and Nanotomography X-ray transmission imaging uses both the absorption and phase shift of the X-ray beam by the sample as contrast mechanisms. Absorption contrast is used to map the sample

  13. Simulating Wavefront Correction via Deformable Mirrors at X-Ray...

    Office of Scientific and Technical Information (OSTI)

    Conference: Simulating Wavefront Correction via Deformable Mirrors at X-Ray Beamlines Citation Details In-Document Search Title: Simulating Wavefront Correction via Deformable ...

  14. In Situ Ambient Pressure X-ray Photoelectron Spectroscopy Studies...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: In Situ Ambient Pressure X-ray ... Citation Details In-Document Search Title: In Situ Ambient ... Resource Relation: Journal Name: Scientific Reports; Journal ...

  15. Absolute Time-Resolved X-Ray Laser Gain Measurement

    SciTech Connect (OSTI)

    Mocek, T.; Sebban, S.; Zeitoun, Ph.; Faivre, G.; Hallou, A.; Rousseau, J.P.; Maynard, G.; Cros, B.; Fajardo, M.; Kazamias, S.; Dubau, J.; Aubert, D.; Lacheze-Murel, G. de

    2005-10-21

    We present the first direct measurement of the time evolution of the gain of a soft x-ray laser amplifier. The measurement is based on the injection of a seed pulse, obtained by high-order harmonic generation, into an x-ray laser medium. Strong amplification occurs when the seed pulse is synchronized with the gain period. By precisely varying the delay between the x-ray laser plasma creation and the seed pulse injection, the actual temporal evolution of the soft x-ray amplifier gain is obtained with a subpicosecond resolution.

  16. Diagnostics Implemented on NIF - X-ray Diagnostics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-ray Diagnostics Diagnostic acronym Diangostic Port location Built and commisioned by Description of function Published references ARIANE Active Readout in a Neutron Environment (gated x-ray imager) 90-89 (but uses DIM) LLNL ARIANE is a gated x-ray detector measuring x-ray output at yields up to ~1E16 neutrons from TCC. ARIANE uses gated MCP technology adapted to operate in this neutron regime by moving the detector to a position just outside of the target chamber wall. ARIANE is typically used

  17. X-ray image reconstruction from a diffraction pattern alone

    SciTech Connect (OSTI)

    Marchesini, Stefano

    2015-03-16

    X-ray diffraction pattern of a sample of 50 nm colloidal gold particles, recorded at a wavelength of 2.1 nm.

  18. Normal incidence x-ray mirror for chemical microanalysis

    DOE Patents [OSTI]

    Carr, M.J.; Romig, A.D. Jr.

    1987-08-05

    An x-ray mirror for both electron column instruments and micro x-ray fluorescence instruments for making chemical, microanalysis comprises a non-planar mirror having, for example, a spherical reflecting surface for x-rays comprised of a predetermined number of alternating layers of high atomic number material and low atomic number material contiguously formed on a substrate and whose layers have a thickness which is a multiple of the wavelength being reflected. For electron column instruments, the wavelengths of interest lie above 1.5nm, while for x-ray fluorescence instruments, the range of interest is below 0.2nm. 4 figs.

  19. Staff Research Physicist (X-Ray Spectroscopy) | Princeton Plasma...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of X-ray spectrometers for high energy density plasma at the National Ignition Facility (NIF) at the Lawrence Livermore National Laboratory (LLNL, Livermore, California). In...

  20. X-Ray Microscopy Reveals How Crystal Mechanics Drive Battery...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-Ray Microscopy Reveals How Crystal Mechanics Drive Battery Performance Print ... are one of the best performing battery electrode materials, able to repeatedly ...

  1. X-ray compass for determining device orientation

    DOE Patents [OSTI]

    Da Silva, L.B.; Matthews, D.L.; Fitch, J.P.; Everett, M.J.; Colston, B.W.; Stone, G.F.

    1999-06-15

    An apparatus and method for determining the orientation of a device with respect to an x-ray source are disclosed. In one embodiment, the present invention is coupled to a medical device in order to determine the rotational orientation of the medical device with respect to the x-ray source. In such an embodiment, the present invention is comprised of a scintillator portion which is adapted to emit photons upon the absorption of x-rays emitted from the x-ray source. An x-ray blocking portion is coupled to the scintillator portion. The x-ray blocking portion is disposed so as to vary the quantity of x-rays which penetrate the scintillator portion based upon the particular rotational orientation of the medical device with respect to the x-ray source. A photon transport mechanism is also coupled to the scintillator portion. The photon transport mechanism is adapted to pass the photons emitted from the scintillator portion to an electronics portion. By analyzing the quantity of the photons, the electronics portion determines the rotational orientation of the medical device with respect to the x-ray source. 25 figs.

  2. X-ray compass for determining device orientation

    DOE Patents [OSTI]

    Da Silva, Luiz B.; Matthews, Dennis L.; Fitch, Joseph P.; Everett, Matthew J.; Colston, Billy W.; Stone, Gary F.

    1999-01-01

    An apparatus and method for determining the orientation of a device with respect to an x-ray source. In one embodiment, the present invention is coupled to a medical device in order to determine the rotational orientation of the medical device with respect to the x-ray source. In such an embodiment, the present invention is comprised of a scintillator portion which is adapted to emit photons upon the absorption of x-rays emitted from the x-ray source. An x-ray blocking portion is coupled to the scintillator portion. The x-ray blocking portion is disposed so as to vary the quantity of x-rays which penetrate the scintillator portion based upon the particular rotational orientation of the medical device with respect to the x-ray source. A photon transport mechanism is also coupled to the scintillator portion. The photon transport mechanism is adapted to pass the photons emitted from the scintillator portion to an electronics portion. By analyzing the quantity of the photons, the electronics portion determines the rotational orientation of the medical device with respect to the x-ray source.

  3. X-Ray Characterization of Diesel Sprays | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Sprays X-Ray Characterization of Diesel Sprays 2005 Diesel Engine Emissions Reduction (DEER) Conference Presentations and Posters 2005deerpowell.pdf (1.19 MB) More Documents & ...

  4. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic ... The effect is unique in that it allows us to distinguish which atomic species magnetism ...

  5. Advances in X-Ray Diagnostics of Diesel Fuel Sprays

    Broader source: Energy.gov [DOE]

    Recent advances in high-speed X-ray imaging has shown several distinct behaviors of commercial fuel injectors that cannot be seen with more conventional techniques.

  6. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    were able to directly observe redox processes in thin-film iron and cobalt perovskite oxide electrocatalysts using surface-sensitive, x-ray absorption spectroscopy while...

  7. X-Ray Diffraction Microscopy of Magnetic Structures (Journal...

    Office of Scientific and Technical Information (OSTI)

    Prev Next Title: X-Ray Diffraction Microscopy of Magnetic Structures Authors: Turner, Joshua J. ; Huang, Xiaojing ; Krupin, Oleg ; Seu, Keoki A. ; Parks, Daniel ; Kevan,...

  8. Stimulated X-Ray Emission for Spectroscopy | Stanford Synchrotron...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Room 108A Speaker: Clemens Weninger, Max Planck Institute for the Physics of Complex Systems Program Description The recent advance of x-ray free electron lasers (XFELs)...

  9. New X-Ray Matter Interaction Observed at Ultra-High Intensity | U.S. DOE

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Office of Science (SC) New X-Ray Matter Interaction Observed at Ultra-High Intensity Basic Energy Sciences (BES) BES Home About Research Facilities Science Highlights Benefits of BES Funding Opportunities Basic Energy Sciences Advisory Committee (BESAC) Community Resources Contact Information Basic Energy Sciences U.S. Department of Energy SC-22/Germantown Building 1000 Independence Ave., SW Washington, DC 20585 P: (301) 903-3081 F: (301) 903-6594 E: Email Us More Information » 08.05.16 New

  10. X-ray metrology and performance of a 45-cm long x-ray deformable mirror

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Poyneer, Lisa A.; Brejnholt, Nicolai F.; Hill, Randall; Jackson, Jessie; Hagler, Lisle; Celestre, Richard; Feng, Jun

    2016-05-20

    We describe experiments with a 45-cm long x-ray deformable mirror (XDM) that have been conducted in End Station 2, Beamline 5.3.1 at the Advanced Light Source. A detailed description of the hardware implementation is provided. We explain our one-dimensional Fresnel propagation code that correctly handles grazing incidence and includes a model of the XDM. This code is used to simulate and verify experimental results. Initial long trace profiler metrology of the XDM at 7.5 keV is presented. The ability to measure a large (150-nm amplitude) height change on the XDM is demonstrated. The results agree well with the simulated experimentmore » at an error level of 1 μrad RMS. Lastly, direct imaging of the x-ray beam also shows the expected change in intensity profile at the detector.« less

  11. X-ray laser system, x-ray laser and method

    DOE Patents [OSTI]

    London, Richard A.; Rosen, Mordecai D.; Strauss, Moshe

    1992-01-01

    Disclosed is an x-ray laser system comprising a laser containing generating means for emitting short wave length radiation, and means external to said laser for energizing said generating means, wherein when the laser is in an operative mode emitting radiation, the radiation has a transverse coherence length to width ratio of from about 0.05 to 1. Also disclosed is a method of adjusting the parameters of the laser to achieve the desired coherence length to laser width ratio.

  12. Femtosecond x-ray absorption spectroscopy with hard x-ray free electron laser

    SciTech Connect (OSTI)

    Katayama, Tetsuo; Togashi, Tadashi; Tono, Kensuke; Kameshima, Takashi; Inubushi, Yuichi; Sato, Takahiro; Hatsui, Takaki; Yabashi, Makina; Obara, Yuki; Misawa, Kazuhiko; Bhattacharya, Atanu; Kurahashi, Naoya; Ogi, Yoshihiro; Suzuki, Toshinori; Molecular Reaction Dynamics Research Team, RIKEN Center for Advanced Photonics, 2-1 Hirosawa, Wako 351-0198

    2013-09-23

    We have developed a method of dispersive x-ray absorption spectroscopy with a hard x-ray free electron laser (XFEL), generated by a self-amplified spontaneous emission (SASE) mechanism. A transmission grating was utilized for splitting SASE-XFEL light, which has a relatively large bandwidth (ΔE/E ∼ 5 × 10{sup −3}), into several branches. Two primary split beams were introduced into a dispersive spectrometer for measuring signal and reference spectra simultaneously. After normalization, we obtained a Zn K-edge absorption spectrum with a photon-energy range of 210 eV, which is in excellent agreement with that measured by a conventional wavelength-scanning method. From the analysis of the difference spectra, the noise ratio was evaluated to be ∼3 × 10{sup −3}, which is sufficiently small to trace minute changes in transient spectra induced by an ultrafast optical laser. This scheme enables us to perform single-shot, high-accuracy x-ray absorption spectroscopy with femtosecond time resolution.

  13. Polychromatic x-ray micro- and nanodiffraction for spatially-resolved structural studies.

    SciTech Connect (OSTI)

    Budai, J. D.; Liu, W.; Tischler, J. Z.; Pan, Z. W.; Larson, B. C.; Yang, W.; Norton, D. P.; Ice, G. E.; ORNL; Univ. of Georgia; Univ.of Florida; Carnegie Inst. of Washington

    2008-01-01

    The availability of intense, focused synchrotron X-ray microbeams has enabled new techniques for materials investigations with sub-micron spatial resolution. The scanning microbeam setup we have developed at the XOR-UNI beamline at the Advanced Photon Source (APS) is versatile in that it provides 1D, 2D or 3D scans (including depth resolution), and can alternate between polychromatic- and monochromatic-beam modes. Focusing in both modes uses elliptical Kirkpatrick-Baez (K-B) reflecting mirrors. Beam diameters of {approx} 500 nm FWHM are now routine, and 90 nm focus has been demonstrated. In white-beam mode, a CCD detector records a complete Laue diffraction pattern, which is analyzed with an automated indexing program. These X-ray diffraction patterns provide real-space maps of the local lattice structure, crystal orientation, grain morphology, and strain tensor. Spatially-resolved X-ray microdiffraction studies are now providing previously unavailable measurements of local microstructures. These measurements, in turn, yield new insights in several classic fields of materials science. This paper will illustrate the application of polychromatic scanning X-ray microscopy with examples from 1D, 2D and 3D materials systems. In 1D systems, we have mapped the structure and orientation of an individual ZnO nanorod along with the associated Ge catalyst particle used to control the nanocrystal growth. In 2D systems, X-ray microdiffraction studies have revealed the mechanisms for local crystallographic tilting in epitaxial oxide films grown on textured Ni substrates for superconducting applications. In 3D systems, X-ray microscopy investigations have included in-situ studies of microstructural evolution during thermal grain growth in polycrystalline aluminum. In general, these spatially-resolved measurements provide important new insights and are valuable as input for theoretical and computer modeling studies of a wide range of material processes.

  14. Polychromatic X-ray Micro- and Nanodiffraction for Spatially-Resolved Structural Studies

    SciTech Connect (OSTI)

    Budai, John D; Liu, W.; Tischler, Jonathan Zachary; Pan, Zhengwei; Norton, David P.; Larson, Ben C; Yang, Wenge; Ice, Gene E

    2008-01-01

    The availability of intense, focused synchrotron X-ray microbeams has enabled new techniques for materials investigations with sub-micron spatial resolution. The scanning microbeam setup we have developed at the XOR-UNI beamline at the Advanced Photon Source (APS) is versatile in that it provides 1D, 2D or 3D scans (including depth resolution), and can alternate between polychromatic- and monochromatic-beam modes. Focusing in both modes uses elliptical Kirkpatrick-Baez (K-B) reflecting mirrors. Beam diameters of {approx} 500 nm FWHM are now routine, and 90 nm focus has been demonstrated. In white-beam mode, a CCD detector records a complete Laue diffraction pattern, which is analyzed with an automated indexing program. These X-ray diffraction patterns provide real-space maps of the local lattice structure, crystal orientation, grain morphology, and strain tensor. Spatially-resolved X-ray microdiffraction studies are now providing previously unavailable measurements of local microstructures. These measurements, in turn, yield new insights in several classic fields of materials science. This paper will illustrate the application of polychromatic scanning X-ray microscopy with examples from 1D, 2D and 3D materials systems. In 1D systems, we have mapped the structure and orientation of an individual ZnO nanorod along with the associated Ge catalyst particle used to control the nanocrystal growth. In 2D systems, X-ray microdiffraction studies have revealed the mechanisms for local crystallographic tilting in epitaxial oxide films grown on textured Ni substrates for superconducting applications. In 3D systems, X-ray microscopy investigations have included in-situ studies of microstructural evolution during thermal grain growth in polycrystalline aluminum. In general, these spatially-resolved measurements provide important new insights and are valuable as input for theoretical and computer modeling studies of a wide range of material processes.

  15. Qualitative comparison of bremsstrahlung X-rays and 800 MeV protons for tomography of urania fuel pellets

    SciTech Connect (OSTI)

    Morris, C. L.; Bourke, M.; Byler, D. D.; Chen, C. F.; Hogan, G.; Hunter, J. F.; Kwiatkowski, K.; Mariam, F. G.; McClellan, K. J.; Merrill, F.; Morley, D. J.; Saunders, A.

    2013-02-15

    We present an assessment of x-rays and proton tomography as tools for studying the time dependence of the development of damage in fuel rods. We also show data taken with existing facilities at Los Alamos National Laboratory that support this assessment. Data on surrogate fuel rods have been taken using the 800 MeV proton radiography (pRad) facility at the Los Alamos Neutron Science Center (LANSCE), and with a 450 keV bremsstrahlung X-ray tomography facility. The proton radiography pRad facility at LANSCE can provide good position resolution (<70 {mu}m has been demonstrate, 20 {mu}m seems feasible with minor changes) for tomography on activated fuel rods. Bremsstrahlung x-rays may be able to provide better than 100 {mu}m resolution but further development of sources, collimation, and detectors is necessary for x-rays to deal with the background radiation for tomography of activated fuel rods.

  16. Qualitative comparison of bremsstrahlung X-rays and 800 MeV protons for tomography of urania fuel pellets

    SciTech Connect (OSTI)

    Morris, Christopher L.; Bourke, Mark A.; Byler, Darrin D.; Chen, Ching-Fong; Hogan, Gary E.; Hunter, James F.; Kwiatkowski, Kris K.; Mariam, Fesseha G.; McClellan, Kenneth J.; Merrill, Frank E.; Morley, Deborah J.; Saunders, Alexander

    2013-02-11

    We present an assessment of x-rays and proton tomography as tools for studying the time dependence of the development of damage in fuel rods. Also, we show data taken with existing facilities at Los Alamos National Laboratory that support this assessment. Data on surrogate fuel rods has been taken using the 800 MeV proton radiography (pRad) facility at the Los Alamos Neutron Science Center (LANSCE), and with a 450 keV bremsstrahlung X-ray tomography facility. The proton radiography pRad facility at LANSCE can provide good position resolution (<70 μm has been demonstrate, 20 μm seems feasible with minor changes) for tomography on activated fuel rods. Bremsstrahlung x-rays may be able to provide better than 100 μm resolution but further development of sources, collimation and detectors is necessary for x-rays to deal with the background radiation for tomography of activated fuel rods.

  17. Beam Physics in X-Ray Radiography Facilities

    SciTech Connect (OSTI)

    Chen, Y J; Caporaso, G J; Chambers, F W; Falabella, S; Goldin, F J; Guethlein, G; Lauer, E L; McCarrick, J F; Neurath, R; Richardson, R A; Sampayan, S; Weir, J T

    2002-12-02

    Performance of x-ray radiography facilities requires focusing the electron beams to sub-millimeter spots on the x-ray converters. Ions extracted from a converter by impact of a high intensity beam can partially neutralize the beam space charge and change the final focusing system. We will discuss these ion effects and mitigation.

  18. High resolution energy-sensitive digital X-ray

    DOE Patents [OSTI]

    Nygren, David R.

    1995-01-01

    An apparatus and method for detecting an x-ray and for determining the depth of penetration of an x-ray into a semiconductor strip detector. In one embodiment, a semiconductor strip detector formed of semiconductor material is disposed in an edge-on orientation towards an x-ray source such that x-rays From the x-ray source are incident upon and substantially perpendicular to the front edge of the semiconductor strip detector. The semiconductor strip detector is formed of a plurality of segments. The segments are coupled together in a collinear arrangement such that the semiconductor strip detector has a length great enough such that substantially all of the x-rays incident on the front edge of the semiconductor strip detector interact with the semiconductor material which forms the semiconductor strip detector. A plurality of electrodes are connected to the semiconductor strip detect or such that each one of the of semiconductor strip detector segments has at least one of the of electrodes coupled thereto. A signal processor is also coupled to each one of the electrodes. The present detector detects an interaction within the semiconductor strip detector, between an x-ray and the semiconductor material, and also indicates the depth of penetration of the x-ray into the semiconductor strip detector at the time of the interaction.

  19. High resolution energy-sensitive digital X-ray

    DOE Patents [OSTI]

    Nygren, D.R.

    1995-07-18

    An apparatus and method for detecting an x-ray and for determining the depth of penetration of an x-ray into a semiconductor strip detector. In one embodiment, a semiconductor strip detector formed of semiconductor material is disposed in an edge-on orientation towards an x-ray source such that x-rays from the x-ray source are incident upon and substantially perpendicular to the front edge of the semiconductor strip detector. The semiconductor strip detector is formed of a plurality of segments. The segments are coupled together in a collinear arrangement such that the semiconductor strip detector has a length great enough such that substantially all of the x-rays incident on the front edge of the semiconductor strip detector interact with the semiconductor material which forms the semiconductor strip detector. A plurality of electrodes are connected to the semiconductor strip detector such that each one of the semiconductor strip detector segments has at least one of the of electrodes coupled thereto. A signal processor is also coupled to each one of the electrodes. The present detector detects an interaction within the semiconductor strip detector, between an x-ray and the semiconductor material, and also indicates the depth of penetration of the x-ray into the semiconductor strip detector at the time of the interaction. 5 figs.

  20. Broadband high resolution X-ray spectral analyzer

    DOE Patents [OSTI]

    Silver, Eric H.; Legros, Mark; Madden, Norm W.; Goulding, Fred; Landis, Don

    1998-01-01

    A broad bandwidth high resolution x-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces x-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available x-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for x-ray microanalysis or in research applications such as laboratory and astrophysical x-ray and particle spectroscopy.

  1. Broadband high resolution X-ray spectral analyzer

    DOE Patents [OSTI]

    Silver, E.H.; Legros, M.; Madden, N.W.; Goulding, F.; Landis, D.

    1998-07-07

    A broad bandwidth high resolution X-ray fluorescence spectrometer has a performance that is superior in many ways to those currently available. It consists of an array of 4 large area microcalorimeters with 95% quantum efficiency at 6 keV and it produces X-ray spectra between 0.2 keV and 7 keV with an energy resolution of 7 to 10 eV. The resolution is obtained at input count rates per array element of 10 to 50 Hz in real-time, with analog pulse processing and thermal pile-up rejection. This performance cannot be matched by currently available X-ray spectrometers. The detectors are incorporated into a compact and portable cryogenic refrigerator system that is ready for use in many analytical spectroscopy applications as a tool for X-ray microanalysis or in research applications such as laboratory and astrophysical X-ray and particle spectroscopy. 6 figs.

  2. Apparatus for generating x-ray holograms

    DOE Patents [OSTI]

    Rhodes, C.K.; Boyer, K.; Solem, J.C.; Haddad, W.S.

    1990-09-11

    Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced. 7 figs.

  3. Apparatus for generating x-ray holograms

    DOE Patents [OSTI]

    Rhodes, Charles K.; Boyer, Keith; Solem, Johndale C.; Haddad, Waleed S.

    1990-01-01

    Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced.

  4. The X-Ray Microcalorimeter Spectrometer for the International X-Ray Observatory

    SciTech Connect (OSTI)

    Kelley, R. L.; Bandler, S. R.; Kilbourne, C. A.; Porter, F. S.; Shirron, P.; Smith, S. J.; Whitehouse, P.; Ezoe, Y.; Ishisaki, Y.; Ohashi, T.; Fujimoto, R.; Sato, K.; Gottardi, L.; Hartog, R. den; Herder, J.-W. den; Hoevers, H.; Korte, P. de; Kuur, J. van der

    2009-12-16

    The International X-Ray Observatory (IXO) is under formulation by NASA, ESA and JAXA for deployment in 2022. IXO emerged over the last 18 months as the NASA Constellation-X and ESA/JAXA X-Ray Evolving Universe Spectrometer (XEUS) missions were combined. The driving performance requirements for the X-Ray Microcalorimeter Spectrometer (XMS) are a spectral resolution of 2.5 eV over the central 2'x2' in the 0.3-7.0 keV band, and 10 eV to the edge of the 5'x5' field of view (FOV). The XMS is now based on a microcalorimeter array of Transition-Edge Sensor (TES) thermometers with Au/Bi absorbers and a SQUID MUX readout. One of the concepts studied as part of the mission formulation has a core 40x40 array corresponding to a 2'x2' FOV with 3'' pixels surrounded by an outer, annular 52x52 array of 6'' pixels that extends the field of view to 5.4'x5.4' with better than 10 eV resolution. There are several options for implementing the readout and cooling system of the XMS under study in the US, Europe and Japan. The ADR system will have from two to five stages depending on the performance of the cryocooler. Mechanical coolers with sufficient cooling power at 4K are available now, and {approx}2K coolers are under development. In this paper we give an overview of the XMS instrument, and some of the tradeoffs to be addressed for this observatory instrument.

  5. Electron beam-based sources of ultrashort x-ray pulses.

    SciTech Connect (OSTI)

    Zholents, A.; Accelerator Systems Division

    2010-09-30

    A review of various methods for generation of ultrashort x-ray pulses using relativistic electron beam from conventional accelerators is presented. Both spontaneous and coherent emission of electrons is considered. The importance of the time-resolved studies of matter at picosecond (ps), femtosecond (fs), and atttosecond (as) time scales using x-rays has been widely recognized including by award of a Nobel Prize in 1999 [Zewa]. Extensive reviews of scientific drivers can be found in [BES1, BES2, BES3, Lawr, Whit]. Several laser-based techniques have been used to generate ultrashort x-ray pulses including laser-driven plasmas [Murn, Alte, Risc, Rose, Zamp], high-order harmonic generation [Schn, Rund, Wang, Arpi], and laser-driven anode sources [Ande]. In addition, ultrafast streak-camera detectors have been applied at synchrotron sources to achieve temporal resolution on the picosecond time scale [Wulf, Lind1]. In this paper, we focus on a different group of techniques that are based on the use of the relativistic electron beam produced in conventional accelerators. In the first part we review several techniques that utilize spontaneous emission of electrons and show how solitary sub-ps x-ray pulses can be obtained at existing storage ring based synchrotron light sources and linacs. In the second part we consider coherent emission of electrons in the free-electron lasers (FELs) and review several techniques for a generation of solitary sub-fs x-ray pulses. Remarkably, the x-ray pulses that can be obtained with the FELs are not only significantly shorter than the ones considered in Part 1, but also carry more photons per pulse by many orders of magnitude.

  6. Hyperspectral image reconstruction for X-ray fluorescence tomography...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Groups Imaging Data Science Related People Doga Gursoy Tekin Bicer Next article: Iterative reconstruction of magnetic induction using Lorentz transmission electron tomography...

  7. Soft-x-ray spectroscopy study of nanoscale materials

    SciTech Connect (OSTI)

    Guo, J.-H.

    2005-07-30

    The ability to control the particle size and morphology of nanoparticles is of crucial importance nowadays both from a fundamental and industrial point of view considering the tremendous amount of high-tech applications. Controlling the crystallographic structure and the arrangement of atoms along the surface of nanostructured material will determine most of its physical properties. In general, electronic structure ultimately determines the properties of matter. Soft X-ray spectroscopy has some basic features that are important to consider. X-ray is originating from an electronic transition between a localized core state and a valence state. As a core state is involved, elemental selectivity is obtained because the core levels of different elements are well separated in energy, meaning that the involvement of the inner level makes this probe localized to one specific atomic site around which the electronic structure is reflected as a partial density-of-states contribution. The participation of valence electrons gives the method chemical state sensitivity and further, the dipole nature of the transitions gives particular symmetry information. The new generation synchrotron radiation sources producing intensive tunable monochromatized soft X-ray beams have opened up new possibilities for soft X-ray spectroscopy. The introduction of selectively excited soft X-ray emission has opened a new field of study by disclosing many new possibilities of soft X-ray resonant inelastic scattering. In this paper, some recent findings regarding soft X-ray absorption and emission studies of various nanostructured systems are presented.

  8. NEW X-RAY DETECTIONS OF WNL STARS

    SciTech Connect (OSTI)

    Skinner, Stephen L.; Zhekov, Svetozar A.; Guedel, Manuel; Schmutz, Werner; Sokal, Kimberly R.

    2012-05-15

    Previous studies have demonstrated that putatively single nitrogen-type Wolf-Rayet stars (WN stars) without known companions are X-ray sources. However, almost all WN star X-ray detections so far have been of earlier WN2-WN6 spectral subtypes. Later WN7-WN9 subtypes (also known as WNL stars) have proved more difficult to detect, an important exception being WR 79a (WN9ha). We present here new X-ray detections of the WNL stars WR 16 (WN8h) and WR 78 (WN7h). These new results, when combined with previous detections, demonstrate that X-ray emission is present in WN stars across the full range of spectral types, including later WNL stars. The two WN8 stars observed to date (WR 16 and WR 40) show unusually low X-ray luminosities (L{sub x} ) compared to other WN stars, and it is noteworthy that they also have the lowest terminal wind speeds (v{sub {infinity}}). Existing X-ray detections of about a dozen WN stars reveal a trend of increasing L{sub x} with wind luminosity L{sub wind} = (1/2)M-dot v{sup 2}{sub {infinity}}, suggesting that wind kinetic energy may play a key role in establishing X-ray luminosity levels in WN stars.

  9. Soft x-ray capabilities for investigating the strongly correlated electron

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    materials | Stanford Synchrotron Radiation Lightsource Soft x-ray capabilities for investigating the strongly correlated electron materials Friday, September 14, 2012 - 1:00pm SLAC, Bldg. 137, Room 226 Jun-Sik Lee Seminar One of the most challenging extant issues in condensed matter physics and applied materials science is the search for post-silicon based electronics, and multi-functional complex oxides offer hopes that new classes of devices can be developed out of these intriguing

  10. Multilayer structures and laboratory x-ray laser research: SPIE volume 688

    SciTech Connect (OSTI)

    Ceglio, N.M.; Dhez, P.

    1987-01-01

    This book's contents are divided into five sessions. Papers are presented under the following topics: X-ray lasers I; X-ray laser research at the Rutherford Appleton Laboratory; X-ray lasers II. X-ray laser cavity experiments; Multilayer structures I; Multilayer structures II; and X-ray imaging CCD.

  11. Laser-Produced Coherent X-Ray Sources

    SciTech Connect (OSTI)

    Donald Umstadter

    2007-01-31

    We study the generation of x-rays from the interaction of relativistic electrons with ultra-intense laser pulse either directly or via laser generated ion channels. The laser pulse acts as the accelerator and wiggler leading to an all-optical synchrotron-like x-ray source. The mm sized accelerator and micron-sized wiggler leads to a compact source of high brightness, ultrafast x-rays with applications in relativistic nonlinear optics, ultrafast chemistry, biology, inner-shell electronic processes and phase transitions.

  12. Spatiotemporal focusing dynamics in plasmas at X-ray wavelength

    SciTech Connect (OSTI)

    Sharma, A., E-mail: a-physics2001@yahoo.com; Tibai, Z. [Institute of Physics, University of Pecs, Pecs7624 (Hungary)] [Institute of Physics, University of Pecs, Pecs7624 (Hungary); Hebling, J. [Institute of Physics, University of Pecs, Pecs7624 (Hungary) [Institute of Physics, University of Pecs, Pecs7624 (Hungary); Szentagothai Research Centre, University of Pecs, Pecs-7624 (Hungary); Mishra, S. K. [Institute for Plasma Research, Gandhinagar (India)] [Institute for Plasma Research, Gandhinagar (India)

    2014-03-15

    Using a finite curvature beam, we investigate here the spatiotemporal focusing dynamics of a laser pulse in plasmas at X-ray wavelength. We trace the dependence of curvature parameter on the focusing of laser pulse and recognize that the self-focusing in plasma is more intense for the X-ray laser pulse with curved wavefront than with flat wavefront. The simulation results demonstrate that spatiotemporal focusing dynamics in plasmas can be controlled with the appropriate choice of beam-plasma parameters to explore the high intensity effects in X-ray regime.

  13. Characterization of X-ray generator beam profiles.

    SciTech Connect (OSTI)

    Mitchell, Dean J; Harding, Lee T.; Thoreson, Gregory G.; Theisen, Lisa Anne; Parmeter, John Ethan; Thompson, Kyle Richard

    2013-07-01

    T to compute the radiography properties of various materials, the flux profiles of X-ray sources must be characterized. This report describes the characterization of X-ray beam profiles from a Kimtron industrial 450 kVp radiography system with a Comet MXC-45 HP/11 bipolar oil-cooled X-ray tube. The empirical method described here uses a detector response function to derive photon flux profiles based on data collected with a small cadmium telluride detector. The flux profiles are then reduced to a simple parametric form that enables computation of beam profiles for arbitrary accelerator energies.

  14. X-ray backscatter imaging of nuclear materials

    DOE Patents [OSTI]

    Chapman, Jeffrey Allen; Gunning, John E; Hollenbach, Daniel F; Ott, Larry J; Shedlock, Daniel

    2014-09-30

    The energy of an X-ray beam and critical depth are selected to detect structural discontinuities in a material having an atomic number Z of 57 or greater. The critical depth is selected by adjusting the geometry of a collimator that blocks backscattered radiation so that backscattered X-ray originating from a depth less than the critical depth is not detected. Structures of Lanthanides and Actinides, including nuclear fuel rod materials, can be inspected for structural discontinuities such as gaps, cracks, and chipping employing the backscattered X-ray.

  15. Resonant x-ray magnetic scattering in holmium

    SciTech Connect (OSTI)

    Gibbs, D.

    1991-01-01

    We review the results of resonant x-ray magnetic scattering experiments on the rare earth metal holmium. When the incident incident x-ray energy is tuned near the L{sub III} absorption edge, large resonant enhancements of the magnetic scattering and resonant integer harmonics are observed. These results are analyzed within the theory of x-ray resonance exchange scattering assuming electric dipole (2p {yields} 5d) and quadrupole (2p {yields} 4f) transitions among atomic orbitals. 30 refs., 5 figs.

  16. Soft x-ray capabilities for investigating the strongly correlated...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Soft x-ray capabilities for investigating the strongly correlated electron materials Friday, September 14, 2012 - 1:00pm SLAC, Bldg. 137, Room 226 Jun-Sik Lee Seminar One of the...

  17. Vitreous carbon mask substrate for X-ray lithography

    DOE Patents [OSTI]

    Aigeldinger, Georg; Skala, Dawn M.; Griffiths, Stewart K.; Talin, Albert Alec; Losey, Matthew W.; Yang, Chu-Yeu Peter

    2009-10-27

    The present invention is directed to the use of vitreous carbon as a substrate material for providing masks for X-ray lithography. The new substrate also enables a small thickness of the mask absorber used to pattern the resist, and this enables improved mask accuracy. An alternative embodiment comprised the use of vitreous carbon as a LIGA substrate wherein the VC wafer blank is etched in a reactive ion plasma after which an X-ray resist is bonded. This surface treatment provides a surface enabling good adhesion of the X-ray photoresist and subsequent nucleation and adhesion of the electrodeposited metal for LIGA mold-making while the VC substrate practically eliminates secondary radiation effects that lead to delamination of the X-ray resist form the substrate, the loss of isolated resist features, and the formation of a resist layer adjacent to the substrate that is insoluble in the developer.

  18. Characterization of Gas Shales by X-ray Raman Spectroscopy |...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Characterization of Gas Shales by X-ray Raman Spectroscopy Thursday, February 23, 2012 - 10:30am SSRL Third Floor Conference Room 137-322 Drew Pomerantz, Schlumberger ...

  19. Characterization of Gas Shales by X-ray Raman Spectroscopy |...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Characterization of Gas Shales by X-ray Raman Spectroscopy Monday, May 14, 2012 - 3:30pm SSRL Conference Room 137-322 Drew Pomerantz, Schlumberger Unconventional hydrocarbon ...

  20. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Lensless Imaging of Magnetic Nanostructures Work performed on ALS Beamline 12.0.2.2 Citation: J.J. Turner et al., "X-Ray Diffraction Microscopy of Magnetic Structures," Phys....

  1. High order reflectivity of graphite (HOPG) crystals for x ray...

    Office of Scientific and Technical Information (OSTI)

    High order reflectivity of graphite (HOPG) crystals for x ray energies up to 22 keV Citation Details In-Document Search Title: High order reflectivity of graphite (HOPG) crystals ...

  2. Biological Imaging by Soft X-Ray Diffraction Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    and angles of x rays scattered from the sample rather than transmitted through it). Shapiro et al. have now chimed in with the first lensless imaging of a sample as complex as a...

  3. ALS X-Rays Shine a New Light on Catalysis

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    vice versa. At the ALS, researchers were able to directly observe redox processes in thin-film iron and cobalt perovskite oxide electrocatalysts using surface-sensitive, x-ray...

  4. Resonant Soft X-Ray Scattering - Combining Structural with Spectroscop...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray absorption spectroscopy has become an important tool in understanding the electronic structure...

  5. X-Ray Diffraction Microscopy of Magnetic Structures

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    This method can be used at any coherent light source, such as x-ray free-electron lasers, where ultra-short pulses would freeze-frame magnetic changes, offering the potential for ...

  6. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    powerful visible-light lasers to render a nominally opaque material transparent to x rays. ... In a dramatic demonstration, researchers used powerful visible-light lasers to render a ...

  7. Systems and methods for detecting x-rays

    DOE Patents [OSTI]

    Bross, Alan D.; Mellott, Kerry L.; Pla-Dalmau, Anna

    2006-05-02

    Systems and methods for detecting x-rays are disclosed herein. One or more x-ray-sensitive scintillators can be configured from a plurality of heavy element nano-sized particles and a plastic material, such as polystyrene. As will be explained in greater detail herein, the heavy element nano-sized particles (e.g., PbWO4) can be compounded into the plastic material with at least one dopant that permits the plastic material to scintillate. X-rays interact with the heavy element nano-sized particles to produce electrons that can deposit energy in the x-ray sensitive scintillator, which in turn can produce light.

  8. High performance x-ray anti-scatter grid

    DOE Patents [OSTI]

    Logan, Clinton M.

    1995-01-01

    An x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury.

  9. X-ray mask and method for making

    DOE Patents [OSTI]

    Morales, Alfredo M.

    2004-10-26

    The present invention describes a method for fabricating an x-ray mask tool which is a contact lithographic mask which can provide an x-ray exposure dose which is adjustable from point-to-point. The tool is useful in the preparation of LIGA plating molds made from PMMA, or similar materials. In particular the tool is useful for providing an ability to apply a graded, or "stepped" x-ray exposure dose across a photosensitive substrate. By controlling the x-ray radiation dose from point-to-point, it is possible to control the development process for removing exposed portions of the substrate; adjusting it such that each of these portions develops at a more or less uniformly rate regardless of feature size or feature density distribution.

  10. X-ray imaging reveals secrets in battery materials | Argonne...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-ray imaging reveals secrets in battery materials June 22, 2015 Tweet EmailPrint Imaging and data analysis techniques offer new approach to probing material properties In a new...

  11. Intensity Pattern of Diffuse X-Ray Scattering From Thermally...

    Office of Scientific and Technical Information (OSTI)

    Populated Phonons in Fcc d-Pu-Ga Citation Details In-Document Search Title: Intensity Pattern of Diffuse X-Ray Scattering From Thermally Populated Phonons in Fcc d-Pu-Ga ...

  12. Simulation and visualization of attosecond stimulated x-ray Raman...

    Office of Scientific and Technical Information (OSTI)

    Simulation and visualization of attosecond stimulated x-ray Raman spectroscopy signals in trans-N-methylacetamide at the nitrogen and oxygen K-edges Citation Details In-Document ...

  13. Lensless Imaging of Magnetic Nanostructures by X-ray Spectro...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    J. Lning, W. F. Schlotter and J. Sthr (SSRL) The unprecedented properties of X-ray free electron lasers (X-FELs) under development world wide will open the door for entirely...

  14. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Radiation damage due to x-ray absorption is, for instance, an unwanted consequence of ... Laser optics provides a possible path for addressing this issue, as well as for developing ...

  15. Femtosecond Time-Delay X-ray Holography

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    optics to the X-ray regime, such as holography, interferometry, and laser-based imaging. ... Those experiments showed that no damage occurred during the 30 fs duration pulse. However, ...

  16. Self-terminating diffraction gates femtosecond X-ray nanocrystallograp...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    without the requirement for the pulse to terminate before the onset of sample damage. ... indicate that current X-ray free-electron laser technology5 should enable structural ...

  17. High performance x-ray anti-scatter grid

    DOE Patents [OSTI]

    Logan, C.M.

    1995-05-23

    Disclosed are an x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury. 4 Figs.

  18. Simulating Wavefront Correction via Deformable Mirrors at X-Ray...

    Office of Scientific and Technical Information (OSTI)

    DOE Contract Number: W-7405-ENG-48 Resource Type: Conference Resource Relation: Conference: Presented at: X-ray Adaptive Optics, San Diego, CA, United States, Aug 14 - Aug 14, 2012 ...

  19. X-ray photonic microsystems for the manipulation of synchrotron...

    Office of Scientific and Technical Information (OSTI)

    massive size of the silicon single-crystal optics currently used. Here we show that micromechanical systems can be used as X-ray optics to create and preserve the spatial, ...

  20. Probing Spatial, Electronic Structures with X-ray Scattering...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Wednesday, September 5, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Gang Chen Seminar: Structures at atomic scales are traditionally determined through X-ray crystallography that ...

  1. HIgh Rate X-ray Fluorescence Detector

    SciTech Connect (OSTI)

    Grudberg, Peter Matthew

    2013-04-30

    The purpose of this project was to develop a compact, modular multi-channel x-ray detector with integrated electronics. This detector, based upon emerging silicon drift detector (SDD) technology, will be capable of high data rate operation superior to the current state of the art offered by high purity germanium (HPGe) detectors, without the need for liquid nitrogen. In addition, by integrating the processing electronics inside the detector housing, the detector performance will be much less affected by the typically noisy electrical environment of a synchrotron hutch, and will also be much more compact than current systems, which can include a detector involving a large LN2 dewar and multiple racks of electronics. The combined detector/processor system is designed to match or exceed the performance and features of currently available detector systems, at a lower cost and with more ease of use due to the small size of the detector. In addition, the detector system is designed to be modular, so a small system might just have one detector module, while a larger system can have many ?? you can start with one detector module, and add more as needs grow and budget allows. The modular nature also serves to simplify repair. In large part, we were successful in achieving our goals. We did develop a very high performance, large area multi-channel SDD detector, packaged with all associated electronics, which is easy to use and requires minimal external support (a simple power supply module and a closed-loop water cooling system). However, we did fall short of some of our stated goals. We had intended to base the detector on modular, large-area detectors from Ketek GmbH in Munich, Germany; however, these were not available in a suitable time frame for this project, so we worked instead with pnDetector GmbH (also located in Munich). They were able to provide a front-end detector module with six 100 m^2 SDD detectors (two monolithic arrays of three elements each) along with

  2. Research | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    ... Synthesis and Processing Science .pdf file (32KB) Atomic, Molecular, and Optical Science ... Science .pdf file (34KB) Neutron and X-Ray Scattering X-Ray Scattering .pdf file ...

  3. Dose optimization in cardiac x-ray imaging

    SciTech Connect (OSTI)

    Gislason-Lee, Amber J.; McMillan, Catherine; Cowen, Arnold R.; Davies, Andrew G.

    2013-09-15

    Purpose: The aim of this research was to optimize x-ray image quality to dose ratios in the cardiac catheterization laboratory. This study examined independently the effects of peak x-ray tube voltage (kVp), copper (Cu), and gadolinium (Gd) x-ray beam filtration on the image quality to radiation dose balance for adult patient sizes.Methods: Image sequences of polymethyl methacrylate (PMMA) phantoms representing two adult patient sizes were captured using a modern flat panel detector based x-ray imaging system. Tin and copper test details were used to simulate iodine-based contrast medium and stents/guide wires respectively, which are used in clinical procedures. Noise measurement for a flat field image and test detail contrast were used to calculate the contrast to noise ratio (CNR). Entrance surface dose (ESD) and effective dose measurements were obtained to calculate the figure of merit (FOM), CNR{sup 2}/dose. This FOM determined the dose efficiency of x-ray spectra investigated. Images were captured with 0.0, 0.1, 0.25, 0.4, and 0.9 mm Cu filtration and with a range of gadolinium oxysulphide (Gd{sub 2}O{sub 2}S) filtration.Results: Optimum x-ray spectra were the same for the tin and copper test details. Lower peak tube voltages were generally favored. For the 20 cm phantom, using 2 Lanex Fast Back Gd{sub 2}O{sub 2}S screens as x-ray filtration at 65 kVp provided the highest FOM considering ESD and effective dose. Considering ESD, this FOM was only marginally larger than that from using 0.4 mm Cu at 65 kVp. For the 30 cm phantom, using 0.25 mm copper filtration at 80 kVp was most optimal; considering effective dose the FOM was highest with no filtration at 65 kVp.Conclusions: These settings, adjusted for x-ray tube loading limits and clinically acceptable image quality, should provide a useful option for optimizing patient dose to image quality in cardiac x-ray imaging. The same optimal x-ray beam spectra were found for both the tin and copper details, suggesting

  4. Self-cleaning rotating anode X-ray source

    DOE Patents [OSTI]

    Paulikas, Arvydas P.

    1989-01-01

    A self-cleaning rotating anode x-ray source comprising an evacuable housing, a rotatable cylindrical anode within the housing, a source of electrons within the housing which electrons are caused to impinge upon the anode to produce x-rays, and means for ionizing residual particles within the housing and accelerating such ions so as to impinge upon the anode to sputter impurities from the surface thereof.

  5. Frontiers in imaging magnetism with polarized x-rays

    SciTech Connect (OSTI)

    Fischer, Peter

    2015-01-08

    Although magnetic imaging with polarized x-rays is a rather young scientific discipline, the various types of established x-ray microscopes have already taken an important role in state-of-the-art characterization of the properties and behavior of spin textures in advanced materials. The opportunities ahead will be to obtain in a unique way indispensable multidimensional information of the structure, dynamics and composition of scientifically interesting and technologically relevant magnetic materials.

  6. X-ray tube with magnetic electron steering

    DOE Patents [OSTI]

    Reed, Kim W. (Albuquerque, NM); Turman, Bobby N. (Albuquerque, NM); Kaye, Ronald J. (Albuquerque, NM); Schneider, Larry X. (Albuquerque, NM)

    2000-01-01

    An X-ray tube uses a magnetic field to steer electrons. The magnetic field urges electrons toward the anode, increasing the proportion of electrons emitted from the cathode that reach desired portions of the anode and consequently contribute to X-ray production. The magnetic field also urges electrons reflected from the anode back to the anode, further increasing the efficiency of the tube.

  7. Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Techniques | Stanford Synchrotron Radiation Lightsource Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Techniques Wednesday, September 5, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Gang Chen Seminar: Structures at atomic scales are traditionally determined through X-ray crystallography that amplifies scattering intensities by introducing spatial periodicity. For amorphous materials and many macromolecules, such as viruses, proteins and biofilms, it is hard to

  8. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and

  9. Self-cleaning rotating anode x-ray source

    DOE Patents [OSTI]

    Paulikas, A.P.

    1987-06-02

    A self-cleaning rotating anode x-ray source comprising and evacuable housing, a rotatable cylindrical anode within the housing, a source of electrons within the housing which electrons are caused to impinge upon the anode to produce x-rays, and means for ionizing residual particles within the housing and accelerating such ions so as to impinge upon the anode to sputter impurities from the surface thereof. 2 figs.

  10. Apparatus for obtaining an X-ray image

    DOE Patents [OSTI]

    Watanabe, Eiji

    1979-01-01

    A computed tomography apparatus in which a fan-shaped X-ray beam is caused to pass through a section of an object, enabling absorption detection on the opposite side of the object by a detector comprising a plurality of discrete detector elements. An electron beam generating the X-ray beam by impacting upon a target is caused to rotate over the target.

  11. NREL: Measurements and Characterization - X-Ray and UV Photoelectron

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Spectroscopy X-Ray and UV Photoelectron Spectroscopy Example of graph made with cluster tool; plots counts (Y-axis) vs. binding energy (X-axis) for PET Carbon 1S. High-resolution XPS spectra of carbon 1s from polyethylene terephthalate backsheet material, showing excellent quantitative agreement between measured and predicted peak area ratios. Subtle differences in polymer functionality are assessed by deviations from stoichiometry. In photoemission techniques, we use either X-rays or

  12. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and

  13. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and

  14. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and

  15. Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Unexpected Angular Dependence of X-Ray Magnetic Linear Dichroism Print Using spectroscopic information for magnetometry and magnetic microscopy obviously requires detailed theoretical understanding of spectral shape and magnitude of dichroism signals. A research team at ALS Beamline 4.0.2 has now shown unambiguously that, contrary to common belief, spectral shape and magnitude of x-ray magnetic linear dichroism (XMLD) are not only determined by the relative orientation of magnetic moments and

  16. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Using Light to Control How X Rays Interact with Matter Print Wednesday, 27 January 2010 00:00 Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning

  17. 15.05.29 RH Operando X-ray - JCAP

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Direct Observation of a Semiconductor/Liquid Junction by Operando X-Ray Photoelectron Spectroscopy (XPS) Lichterman , M. F. et al. Direct Observation of the Energetics at a Semiconductor/Liquid Junction by Operando X-Ray Photoelectron Spectroscopy. Energy Environ. Sci ., 2015, DOI: 10.1039/C5EE01014D (2015). Scientific Achievement We demonstrated that the operando XPS technique, applied to a semiconductor/liquid junction, can directly measure the positions of the electronic states of the

  18. New focusing multilayer structures for X-ray plasma spectroscopy

    SciTech Connect (OSTI)

    Bibishkin, M S; Luchin, V I; Salashchenko, N N; Chernov, V V; Chkhalo, N I; Kazakov, E D; Shevelko, A P

    2008-02-28

    New focusing short-period multilayer structures are developed which opens up wide possibilities for X-ray and VUV spectroscopy. Multilayer structures are deposited on a flat surface of a mica crystal which is then bent to a small-radius cylinder. The use of this structure in a von Hamos spectrometer for X-ray laser plasma diagnostics is demonstrated. (interaction of laser radiation with matter. laser plasma)

  19. X-ray chemical analyzer for field applications

    DOE Patents [OSTI]

    Gamba, Otto O. M.

    1977-01-01

    A self-supporting portable field multichannel X-ray chemical analyzer system comprising a lightweight, flexibly connected, remotely locatable, radioisotope-excited sensing probe utilizing a cryogenically-cooled solid state semi-conductor crystal detector for fast in situ non-destructive, qualitative and quantitative analysis of elements in solid, powder, liquid or slurried form, utilizing an X-ray energy dispersive spectrometry technique.

  20. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print Wednesday, 31 October 2012 00:00 The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film

  1. Analysis of Off-Nuclear X-Ray Sources in Galaxy NGC 4945 (Technical...

    Office of Scientific and Technical Information (OSTI)

    Analysis of Off-Nuclear X-Ray Sources in Galaxy NGC 4945 Citation Details In-Document Search Title: Analysis of Off-Nuclear X-Ray Sources in Galaxy NGC 4945 Recently, X-ray ...

  2. A New Scheme for Stigmatic X-ray Imaging with Large Magnification...

    Office of Scientific and Technical Information (OSTI)

    F; Beiersdorfer, P; Wang, E; Sanchez del Rio, M; Caughey, T A 70 PLASMA PHYSICS AND FUSION TECHNOLOGY X-ray Imaging X-ray Imaging This paper describes a new x-ray scheme for...

  3. Ultra Fast X-ray Streak Camera for TIM Based Platforms (Conference...

    Office of Scientific and Technical Information (OSTI)

    Ultra Fast X-ray Streak Camera for TIM Based Platforms Citation Details In-Document Search Title: Ultra Fast X-ray Streak Camera for TIM Based Platforms Ultra fast x-ray streak ...

  4. Evaluation of partial coherence correction in X-ray ptychography

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Burdet, Nicolas; Shi, Xiaowen; Parks, Daniel; Clark, Jesse N.; Huang, Xiaojing; Kevan, Stephen D.; Robinson, Ian K.

    2015-02-23

    Coherent X-ray Diffraction Imaging (CDI) and X-ray ptychography both heavily rely on the high degree of spatial coherence of the X-ray illumination for sufficient experimental data quality for reconstruction convergence. Nevertheless, the majority of the available synchrotron undulator sources have a limited degree of partial coherence, leading to reduced data quality and a lower speckle contrast in the coherent diffraction patterns. It is still an open question whether experimentalists should compromise the coherence properties of an X-ray source in exchange for a higher flux density at a sample, especially when some materials of scientific interest are relatively weak scatterers. Amoreprevious study has suggested that in CDI, the best strategy for the study of strong phase objects is to maintain a high degree of coherence of the illuminating X-rays because of the broadening of solution space resulting from the strong phase structures. In this article, we demonstrate the first systematic analysis of the effectiveness of partial coherence correction in ptychography as a function of the coherence properties, degree of complexity of illumination (degree of phase diversity of the probe) and sample phase complexity. We have also performed analysis of how well ptychographic algorithms refine X-ray probe and complex coherence functions when those variables are unknown at the start of reconstructions, for noise-free simulated data, in the case of both real-valued and highly-complex objects.less

  5. X-rays from a microsecond X-pinch

    SciTech Connect (OSTI)

    Appartaim, R. K.

    2013-08-28

    The characteristics of x-rays emitted by X-pinches driven by discharging a current of ∼320 kA with a quarter period of 1 μs in crossed 25 μm wires have been investigated. The x-ray emissions are studied using filtered silicon photodiodes, diamond radiation detectors, and pinhole cameras. The results show that predominantly x-rays from the microsecond X-pinch tend to be emitted in two distinct sets of bursts. The first is predominantly “soft,” i.e., with photon energy hν < 5 keV, followed by a second set of bursts beginning up to 100 ns following the initial bursts, and usually consisting of higher photon energies. Our results show, however, that the x-ray emissions do not contain a significant component with hν > 10 keV as might be expected from electron beam activity within the plasma or from the X-pinch diode. High-resolution images obtained with the observed x-rays suggest a well-defined small source of soft x-rays that demonstrates the potential of the microsecond X-pinch.

  6. Normal incidence X-ray mirror for chemical microanalysis

    DOE Patents [OSTI]

    Carr, Martin J.; Romig, Jr., Alton D.

    1990-01-01

    A non-planar, focusing mirror, to be utilized in both electron column instruments and micro-x-ray fluorescence instruments for performing chemical microanalysis on a sample, comprises a concave, generally spherical base substrate and a predetermined number of alternating layers of high atomic number material and low atomic number material contiguously formed on the base substrate. The thickness of each layer is an integral multiple of the wavelength being reflected and may vary non-uniformly according to a predetermined design. The chemical analytical instruments in which the mirror is used also include a predetermined energy source for directing energy onto the sample and a detector for receiving and detecting the x-rays emitted from the sample; the non-planar mirror is located between the sample and detector and collects the x-rays emitted from the sample at a large solid angle and focuses the collected x-rays to the sample. For electron column instruments, the wavelengths of interest lie above 1.5 nm, while for x-ray fluorescence instruments, the range of interest is below 0.2 nm. Also, x-ray fluorescence instruments include an additional non-planar focusing mirror, formed in the same manner as the previously described m The invention described herein was made in the performance of work under contract with the Department of Energy, Contract No. DE-AC04-76DP00789, and the United States Government has rights in the invention pursuant to this contract.

  7. Lasers, extreme UV and soft X-ray

    SciTech Connect (OSTI)

    Nilsen, Joseph

    2015-09-20

    Three decades ago, large ICF lasers that occupied entire buildings were used as the energy sources to drive the first X-ray lasers. Today X-ray lasers are tabletop, spatially coherent, high-repetition rate lasers that enable many of the standard optical techniques such as interferometry to be extended to the soft X-ray regime between wavelengths of 10 and 50 nm. Over the last decade X-ray laser performance has been improved by the use of the grazing incidence geometry, diode-pumped solid-state lasers, and seeding techniques. The dominant X-ray laser schemes are the monopole collisional excitation lasers either driven by chirped pulse amplification (CPA) laser systems or capillary discharge. The CPA systems drive lasing in neon-like or nickel-like ions, typically in the 10 – 30 nm range, while the capillary system works best for neon-like argon at 46.9 nm. Most researchers use nickel-like ion lasers near 14 nm because they are well matched to the Mo:Si multilayer mirrors that have peak reflectivity near 13 nm and are used in many applications. As a result, the last decade has seen the birth of the X-ray free electron laser (XFEL) that can reach wavelengths down to 0.15 nm and the inner-shell Ne laser at 1.46 nm.

  8. Lasers, extreme UV and soft X-ray

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Nilsen, Joseph

    2015-09-20

    Three decades ago, large ICF lasers that occupied entire buildings were used as the energy sources to drive the first X-ray lasers. Today X-ray lasers are tabletop, spatially coherent, high-repetition rate lasers that enable many of the standard optical techniques such as interferometry to be extended to the soft X-ray regime between wavelengths of 10 and 50 nm. Over the last decade X-ray laser performance has been improved by the use of the grazing incidence geometry, diode-pumped solid-state lasers, and seeding techniques. The dominant X-ray laser schemes are the monopole collisional excitation lasers either driven by chirped pulse amplification (CPA)more » laser systems or capillary discharge. The CPA systems drive lasing in neon-like or nickel-like ions, typically in the 10 – 30 nm range, while the capillary system works best for neon-like argon at 46.9 nm. Most researchers use nickel-like ion lasers near 14 nm because they are well matched to the Mo:Si multilayer mirrors that have peak reflectivity near 13 nm and are used in many applications. As a result, the last decade has seen the birth of the X-ray free electron laser (XFEL) that can reach wavelengths down to 0.15 nm and the inner-shell Ne laser at 1.46 nm.« less

  9. Complete multiwavelength evolution of galactic black hole transients during outburst decay. II. Compact jets and X-ray variability properties

    SciTech Connect (OSTI)

    Diner, T.; Kalemci, E.; Tomsick, J. A.; Buxton, M. M.; Bailyn, C. D.

    2014-11-01

    We investigated the relation between compact jet emission and X-ray variability properties of all black hole transients with multiwavelength coverage during their outburst decays. We studied the evolution of all power spectral components (including low-frequency quasi-periodic oscillations; QPOs), and related this evolution to changes in jet properties tracked by radio and infrared observations. We grouped sources according to their tracks in the radio/X-ray luminosity relation and show that the standards show stronger broadband X-ray variability than outliers at a given X-ray luminosity when the compact jet turns on. This trend is consistent with the internal shock model and can be important for the understanding of the presence of tracks in the radio/X-ray luminosity relation. We also observed that the total and the QPO rms amplitudes increase together during the earlier part of the outburst decay, but after the compact jet turns, either the QPO disappears or its rms amplitude decreases significantly while the total rms amplitudes remain high. We discuss these results with a scenario including a variable corona and a non-variable disk with a mechanism for the QPO separate from the mechanism that creates broad components. Finally, we evaluated the timing predictions of the magnetically dominated accretion flow model that can explain the presence of tracks in the radio/X-ray luminosity relation.

  10. The Coherent X-ray Imaging (CXI) Instrument at the Linac Coherent Light Source (LCLS)

    SciTech Connect (OSTI)

    Boutet, Sebastien; Williams, Garth J.; ,

    2011-08-16

    The Linac Coherent Light Source (LCLS) has become the first ever operational hard X-ray Free Electron Laser in 2009. It will operate as a user facility capable of delivering unique research opportunities in multiple fields of science. The LCLS and the LCLS Ultrafast Science Instruments (LUSI) construction projects are developing instruments designed to make full use of the capabilities afforded by the LCLS beam. One such instrument is being designed to utilize the LCLS coherent beam to image with high resolution any sub-micron object. This instrument is called the Coherent X-ray Imaging (CXI) instrument. This instrument will provide a flexible optical system capable of tailoring key beam parameters for the users. A suite of shot-to-shot diagnostics will also be provided to characterize the beam on every pulse. The provided instrumentation will include multi-purpose sample environments, sample delivery and a custom detector capable of collecting 2D data at 120 Hz. In this article, the LCLS will be briefly introduced along with the technique of Coherent X-ray Diffractive Imaging (CXDI). A few examples of scientific opportunities using the CXI instrument will be described. Finally, the conceptual layout of the instrument will be presented along with a description of the key requirements for the overall system and specific devices required.

  11. Towards three-dimensional and attosecond x-ray imaging at the...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    x-ray wavelength appears desirable to achieve maximal spatial resolution in x-ray diffraction experiments, longer wavelengths turns out to enable the identification of...

  12. X-ray Induced Quasiparticles: New Window on UnconventionalSuperconduc...

    Office of Science (SC) Website

    X-ray Induced Quasiparticles: New Window on Unconventional Superconductivity Basic Energy ... X-ray Induced Quasiparticles: New Window on Unconventional Superconductivity Creation of ...

  13. X-ray micro-diffraction studies of heterogeneous interfaces between...

    Office of Scientific and Technical Information (OSTI)

    Article: X-ray micro-diffraction studies of heterogeneous interfaces between cementitious materials and geological formations Citation Details In-Document Search Title: X-ray ...

  14. X-ray absorption spectroscopy study of Gd[superscript 3+]-loaded...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: X-ray absorption spectroscopy study of Gdsuperscript 3+-loaded ultra-short carbon nanotubes Citation Details In-Document Search Title: X-ray absorption ...

  15. Application of Image And X-Ray Microtomography Technique To Quantify...

    Office of Scientific and Technical Information (OSTI)

    Application of Image And X-Ray Microtomography Technique To Quantify Filler Distribution ... Citation Details In-Document Search Title: Application of Image And X-Ray Microtomography ...

  16. Development of a High Resolution X-Ray Imaging Crystal Spectrometer...

    Office of Scientific and Technical Information (OSTI)

    The affects of x-ray and nuclear-radiation background on the measurement uncertainties are ... Resource Relation: Related Information: Invention Disclosure. Title X-ray Imaging Crystal ...

  17. Development of a High Resolution X-Ray Imaging Crystal Spectrometer

    Office of Scientific and Technical Information (OSTI)

    Development of a High Resolution X-Ray Imaging Crystal Spectrometer for Measurement of ... Development of a High Resolution X-Ray Imaging Crystal Spectrometer for ...

  18. Development of a High Resolution X-Ray Imaging Crystal Spectrometer...

    Office of Scientific and Technical Information (OSTI)

    Development of a High Resolution X-Ray Imaging Crystal Spectrometer for Measurement of ... Development of a High Resolution X-Ray Imaging Crystal Spectrometer for Measurement of ...

  19. Proposed New Accelerator Design for Homeland Security X-Ray Applicatio...

    Office of Scientific and Technical Information (OSTI)

    Design for Homeland Security X-Ray Applications Citation Details In-Document Search Title: Proposed New Accelerator Design for Homeland Security X-Ray Applications In the ...

  20. Achieving hard X-ray nanofocusing using a wedged multilayer Laue...

    Office of Scientific and Technical Information (OSTI)

    anticipate that continuous development on wedged MLLs will advance x-ray nanofocusing optics to new frontiers and enrich capabilities and opportunities for hard X-ray microscopy....

  1. X-Ray Diffraction > Analytical Resources > Research > The Energy Materials

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Center at Cornell Analytical Resources In This Section Differential Electrochemical Mass Spectroscopy (DEMS) Electron Microscopy X-Ray Diffraction X-Ray Diffraction

  2. High brightness--multiple beamlets source for patterned X-ray...

    Office of Scientific and Technical Information (OSTI)

    source for patterned X-ray production Citation Details In-Document Search Title: High brightness--multiple beamlets source for patterned X-ray production Techniques for ...

  3. Synchrotron X-ray Studies of Super-critical Carbon Dioxide /...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Synchrotron X-ray Studies of Super-critical Carbon Dioxide Reservoir Rock Interfaces Project obectives: Utilize synchrotron X-ray measurements, to monitor all aspects of atomic ...

  4. Spherical grating based x-ray Talbot interferometry

    SciTech Connect (OSTI)

    Cong, Wenxiang E-mail: xiy2@rpi.edu Xi, Yan E-mail: xiy2@rpi.edu Wang, Ge E-mail: xiy2@rpi.edu

    2015-11-15

    Purpose: Grating interferometry is a state-of-the-art x-ray imaging approach, which can acquire information on x-ray attenuation, phase shift, and small-angle scattering simultaneously. Phase-contrast imaging and dark-field imaging are very sensitive to microstructural variation and offers superior contrast resolution for biological soft tissues. However, a common x-ray tube is a point-like source. As a result, the popular planar grating imaging configuration seriously restricts the flux of photons and decreases the visibility of signals, yielding a limited field of view. The purpose of this study is to extend the planar x-ray grating imaging theory and methods to a spherical grating scheme for a wider range of preclinical and clinical applications. Methods: A spherical grating matches the wave front of a point x-ray source very well, allowing the perpendicular incidence of x-rays on the grating to achieve a higher visibility over a larger field of view than the planer grating counterpart. A theoretical analysis of the Talbot effect for spherical grating imaging is proposed to establish a basic foundation for x-ray spherical gratings interferometry. An efficient method of spherical grating imaging is also presented to extract attenuation, differential phase, and dark-field images in the x-ray spherical grating interferometer. Results: Talbot self-imaging with spherical gratings is analyzed based on the Rayleigh–Sommerfeld diffraction formula, featuring a periodic angular distribution in a polar coordinate system. The Talbot distance is derived to reveal the Talbot self-imaging pattern. Numerical simulation results show the self-imaging phenomenon of a spherical grating interferometer, which is in agreement with the theoretical prediction. Conclusions: X-ray Talbot interferometry with spherical gratings has a significant practical promise. Relative to planar grating imaging, spherical grating based x-ray Talbot interferometry has a larger field of view and

  5. Transient x-ray diffraction with simultaneous imaging under high strain-rate loading

    SciTech Connect (OSTI)

    Fan, D.; E, J. C.; Zhao, F.; Luo, S. N.; Lu, L.; Li, B.; Qi, M. L.; Sun, T.; Fezzaa, K.; Chen, W.

    2014-11-15

    Real time, in situ, multiframe, diffraction, and imaging measurements on bulk samples under high and ultrahigh strain-rate loading are highly desirable for micro- and mesoscale sciences. We present an experimental demonstration of multiframe transient x-ray diffraction (TXD) along with simultaneous imaging under high strain-rate loading at the Advanced Photon Source beamline 32ID. The feasibility study utilizes high strain-rate Hopkinson bar loading on a Mg alloy. The exposure time in TXD is 2–3 μs, and the frame interval is 26.7–62.5 μs. Various dynamic deformation mechanisms are revealed by TXD, including lattice expansion or compression, crystal plasticity, grain or lattice rotation, and likely grain refinement, as well as considerable anisotropy in deformation. Dynamic strain fields are mapped via x-ray digital image correlation, and are consistent with the diffraction measurements and loading histories.

  6. Claudio Pellegrini and the World’s First Hard X-ray Free-Electron Laser

    SciTech Connect (OSTI)

    Pellegrini, Claudio

    2015-10-20

    President Obama welcomed SLAC's Claudio Pellegrini inside the Oval Office on Tuesday morning as a recipient of the Enrico Fermi Award, one of the highest honors the U.S. government can give to a scientist. Pellegrini, a visiting scientist and consulting professor at SLAC and distinguished professor emeritus at the University of California, Los Angeles, received the award for research that aided in the development of X-ray free-electron lasers (XFELs) including SLAC's Linac Coherent Light Source (LCLS), a DOE Office of Science User Facility that started up in 2009. Here, Pellegrini describes his efforts that contributed to the realization of SLAC’s Linac Coherent Light Source, the world’s first hard X-ray free-electron laser.

  7. Breakthrough: X-ray Laser Captures Atoms and Molecules in Action

    ScienceCinema (OSTI)

    Bergmann, Uwe

    2014-05-21

    The Linac Coherent Light Source at SLAC is the world's most powerful X-ray laser. Just two years after turning on in 2009, breakthrough science is emerging from the LCLS at a rapid pace. A recent experiment used the X-rays to create and probe a 2-million-degree piece of matter in a controlled way for the first time-a significant leap toward understanding the extreme conditions found in the hearts of stars and giant planets, and a finding which could further guide research into nuclear fusion, the mechanism that powers the sun. Upcoming experiments will investigate the fundamental, atomic-scale processes behind such phenomena as superconductivity and magnetism, as well as peering into the molecular workings of photosynthesis in plants.

  8. Apparatus for X-ray diffraction microscopy and tomography of cryo specimens

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Beetz, T.; Howells, M. R.; Jacobsen, C.; Kao, C. -C.; Kirz, J.; Lima, E.; Mentes, T. O.; Miao, H.; Sanchez-Hanke, C.; Sayre, D.; et al

    2005-03-14

    An apparatus for diffraction microscopy of biological and materials science specimens is described. In this system, a coherent soft X-ray beam is selected with a pinhole, and the illuminated specimen is followed by an adjustable beamstop and CCD camera to record diffraction data from non-crystalline specimens. In addition, a Fresnel zone plate can be inserted to allow for direct imaging. The system makes use of a cryogenic specimen holder with cryotransfer capabilities to allow frozen hydrated specimens to be loaded. The specimen can be tilted over a range of ± 80 ° degrees for three-dimensional imaging; this is done bymore » computer-controlled motors, enabling automated alignment of the specimen through a tilt series. The system is now in use for experiments in soft X-ray diffraction microscopy.« less

  9. Gain dynamics in a soft X-ray laser ampli er perturbed by a strong injected X-ray eld

    SciTech Connect (OSTI)

    Wang, Yong; Wang, Shoujun; Oliva, E; Lu, L; Berrill, Mark A; Yin, Liang; Nejdl, J; Luther, Brad; Proux, C; Le, T. T.; Dunn, James; Ros, D; Zeitoun, Philippe; Rocca, Jorge

    2014-01-01

    Seeding soft X-ray plasma ampli ers with high harmonics has been demonstrated to generate high-brightness soft X-ray laser pulses with full spatial and temporal coherence. The interaction between the injected coherent eld and the swept-gain medium has been modelled. However, no exper- iment has been conducted to probe the gain dynamics when perturbed by a strong external seed eld. Here, we report the rst X-ray pump X-ray probe measurement of the nonlinear response of a plasma ampli er perturbed by a strong soft X-ray ultra-short pulse. We injected a sequence of two time-delayed high-harmonic pulses (l518.9 nm) into a collisionally excited nickel-like molybdenum plasma to measure with femto-second resolution the gain depletion induced by the saturated ampli cation of the high-harmonic pump and its subsequent recovery. The measured fast gain recovery in 1.5 1.75 ps con rms the possibility to generate ultra-intense, fully phase-coherent soft X-ray lasers by chirped pulse ampli cation in plasma ampli ers.

  10. X-RAY EMISSION FROM MAGNETIC MASSIVE STARS

    SciTech Connect (OSTI)

    Naz, Yal; Petit, Vronique; Rinbrand, Melanie; Owocki, Stan; Cohen, David; Ud-Doula, Asif; Wade, Gregg A.

    2014-11-01

    Magnetically confined winds of early-type stars are expected to be sources of bright and hard X-rays. To clarify the systematics of the observed X-ray properties, we have analyzed a large series of Chandra and XMM-Newton observations, corresponding to all available exposures of known massive magnetic stars (over 100 exposures covering ?60% of stars compiled in the catalog of Petit et al.). We show that the X-ray luminosity is strongly correlated with the stellar wind mass-loss rate, with a power-law form that is slightly steeper than linear for the majority of the less luminous, lower- M-dot B stars and flattens for the more luminous, higher- M-dot O stars. As the winds are radiatively driven, these scalings can be equivalently written as relations with the bolometric luminosity. The observed X-ray luminosities, and their trend with mass-loss rates, are well reproduced by new MHD models, although a few overluminous stars (mostly rapidly rotating objects) exist. No relation is found between other X-ray properties (plasma temperature, absorption) and stellar or magnetic parameters, contrary to expectations (e.g., higher temperature for stronger mass-loss rate). This suggests that the main driver for the plasma properties is different from the main determinant of the X-ray luminosity. Finally, variations of the X-ray hardnesses and luminosities, in phase with the stellar rotation period, are detected for some objects and they suggest that some temperature stratification exists in massive stars' magnetospheres.

  11. APS Science | Advanced Photon Source

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Science APS Science features articles on Advanced Photon Source research and engineering highlights that are written for the interested public as well as the synchrotron x-ray,...

  12. Method and apparatus for micromachining using hard X-rays

    DOE Patents [OSTI]

    Siddons, David Peter; Johnson, Erik D.; Guckel, Henry; Klein, Jonathan L.

    1997-10-21

    An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures.

  13. Method and apparatus for micromachining using hard X-rays

    DOE Patents [OSTI]

    Siddons, D.P.; Johnson, E.D.; Guckel, H.; Klein, J.L.

    1997-10-21

    An X-ray source such as a synchrotron which provides a significant spectral content of hard X-rays is used to expose relatively thick photoresist such that the portions of the photoresist at an exit surface receive at least a threshold dose sufficient to render the photoresist susceptible to a developer, while the entrance surface of the photoresist receives an exposure which does not exceed a power limit at which destructive disruption of the photoresist would occur. The X-ray beam is spectrally shaped to substantially eliminate lower energy photons while allowing a substantial flux of higher energy photons to pass through to the photoresist target. Filters and the substrate of the X-ray mask may be used to spectrally shape the X-ray beam. Machining of photoresists such as polymethylmethacrylate to micron tolerances may be obtained to depths of several centimeters, and multiple targets may be exposed simultaneously. The photoresist target may be rotated and/or translated in the beam to form solids of rotation and other complex three-dimensional structures. 21 figs.

  14. The History of X-ray Free-Electron Lasers

    SciTech Connect (OSTI)

    Pellegrini, C.; /UCLA /SLAC

    2012-06-28

    The successful lasing at the SLAC National Accelerator Laboratory of the Linear Coherent Light Source (LCLS), the first X-ray free-electron laser (X-ray FEL), in the wavelength range 1.5 to 15 {angstrom}, pulse duration of 60 to few femtoseconds, number of coherent photons per pulse from 10{sup 13} to 10{sup 11}, is a landmark event in the development of coherent electromagnetic radiation sources. Until now electrons traversing an undulator magnet in a synchrotron radiation storage ring provided the best X-ray sources. The LCLS has set a new standard, with a peak X-ray brightness higher by ten orders of magnitudes and pulse duration shorter by three orders of magnitudes. LCLS opens a new window in the exploration of matter at the atomic and molecular scales of length and time. Taking a motion picture of chemical processes in a few femtoseconds or less, unraveling the structure and dynamics of complex molecular systems, like proteins, are some of the exciting experiments made possible by LCLS and the other X-ray FELs now being built in Europe and Asia. In this paper, we describe the history of the many theoretical, experimental and technological discoveries and innovations, starting from the 1960s and 1970s, leading to the development of LCLS.

  15. Nonlinear increase of X-ray intensities from thin foils irradiated with a 200 TW femtosecond laser

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Faenov, A. Ya.; Colgan, J.; Hansen, S. B.; Zhidkov, A.; Pikuz, T. A.; Nishiuchi, M.; Pikuz, S. A.; Skobelev, I. Yu.; Abdallah, J.; Sakaki, H.; et al

    2015-09-02

    We report, for the first time, that the energy of femtosecond optical laser pulses, E, with relativistic intensities I > 1021 W/cm2 is efficiently converted to X-ray radiation, which is emitted by “hot” electron component in collision-less processes and heats the solid density plasma periphery. As shown by direct high-resolution spectroscopic measurements X-ray radiation from plasma periphery exhibits unusual non-linear growth ~E4–5 of its power. The non-linear power growth occurs far earlier than the known regime when the radiation reaction dominates particle motion (RDR). Nevertheless, the radiation is shown to dominate the kinetics of the plasma periphery, changing in thismore » regime (now labeled RDKR) the physical picture of the laser plasma interaction. Although in the experiments reported here we demonstrated by observation of KK hollow ions that X-ray intensities in the keV range exceeds ~1017 W/cm2, there is no theoretical limit of the radiation power. Therefore, such powerful X-ray sources can produce and probe exotic material states with high densities and multiple inner-shell electron excitations even for higher Z elements. As a result, femtosecond laser-produced plasmas may thus provide unique ultra-bright X-ray sources, for future studies of matter in extreme conditions, material science studies, and radiography of biological systems.« less

  16. Nonlinear increase of X-ray intensities from thin foils irradiated with a 200 TW femtosecond laser

    SciTech Connect (OSTI)

    Faenov, A. Ya.; Colgan, J.; Hansen, S. B.; Zhidkov, A.; Pikuz, T. A.; Nishiuchi, M.; Pikuz, S. A.; Skobelev, I. Yu.; Abdallah, J.; Sakaki, H.; Sagisaka, A.; Pirozhkov, A. S.; Ogura, K.; Fukuda, Y.; Kanasaki, M.; Hasegawa, N.; Nishikino, M.; Kando, M.; Watanabe, Y.; Kawachi, T.; Masuda, S.; Hosokai, T.; Kodama, R.; Kondo, K.

    2015-09-02

    We report, for the first time, that the energy of femtosecond optical laser pulses, E, with relativistic intensities I > 1021 W/cm2 is efficiently converted to X-ray radiation, which is emitted by “hot” electron component in collision-less processes and heats the solid density plasma periphery. As shown by direct high-resolution spectroscopic measurements X-ray radiation from plasma periphery exhibits unusual non-linear growth ~E4–5 of its power. The non-linear power growth occurs far earlier than the known regime when the radiation reaction dominates particle motion (RDR). Nevertheless, the radiation is shown to dominate the kinetics of the plasma periphery, changing in this regime (now labeled RDKR) the physical picture of the laser plasma interaction. Although in the experiments reported here we demonstrated by observation of KK hollow ions that X-ray intensities in the keV range exceeds ~1017 W/cm2, there is no theoretical limit of the radiation power. Therefore, such powerful X-ray sources can produce and probe exotic material states with high densities and multiple inner-shell electron excitations even for higher Z elements. As a result, femtosecond laser-produced plasmas may thus provide unique ultra-bright X-ray sources, for future studies of matter in extreme conditions, material science studies, and radiography of biological systems.

  17. Evidence of High Harmonics from Echo-Enabled Harmonic Generation for Seeding X-ray Free Electron Lasers

    SciTech Connect (OSTI)

    Xiang, D.; Colby, E.; Dunning, M.; Gilevich, S.; Hast, C.; Jobe, K.; McCormick, D.; Nelson, J.; Raubenheimer, T.O.; Soong, K.; Stupakov, G.; Szalata, Z.; Walz, D.; Weathersby, S.; Woodle, M.; ,

    2012-02-15

    Echo-enabled harmonic generation free electron lasers hold great promise for the generation of fully coherent radiation in x-ray wavelengths. Here we report the first evidence of high harmonics from the echo-enabled harmonic generation technique in the realistic scenario where the laser energy modulation is comparable to the beam slice energy spread. In this experiment, coherent radiation at the seventh harmonic of the second seed laser is generated when the energy modulation amplitude is about 2-3 times the slice energy spread. The experiment confirms the underlying physics of echo-enabled harmonic generation and may have a strong impact on emerging seeded x-ray free electron lasers that are capable of generating laserlike x rays which will advance many areas of science.

  18. Retrieving spin textures on curved magnetic thin films with full-field soft X-ray microscopies

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Streubel, Robert; Kronast, Florian; Fischer, Peter; Parkinson, Dula; Schmidt, Oliver G.; Makarov, Denys

    2015-07-03

    X-ray tomography is a well-established technique to characterize 3D structures in material sciences and biology; its magnetic analogue—magnetic X-ray tomography—is yet to be developed. We demonstrate the visualization and reconstruction of magnetic domain structures in a 3D curved magnetic thin films with tubular shape by means of full-field soft X-ray microscopies. In the 3D arrangement of the magnetization is retrieved from a set of 2D projections by analysing the evolution of the magnetic contrast with varying projection angle. By using reconstruction algorithms to analyse the angular evolution of 2D projections provides quantitative information about domain patterns and magnetic coupling phenomenamore » between windings of azimuthally and radially magnetized tubular objects. In conclusion, the present approach represents a first milestone towards visualizing magnetization textures of 3D curved thin films with virtually arbitrary shape.« less

  19. Retrieving spin textures on curved magnetic thin films with full-field soft X-ray microscopies

    SciTech Connect (OSTI)

    Streubel, Robert; Kronast, Florian; Fischer, Peter; Parkinson, Dula; Schmidt, Oliver G.; Makarov, Denys

    2015-07-03

    X-ray tomography is a well-established technique to characterize 3D structures in material sciences and biology; its magnetic analogue—magnetic X-ray tomography—is yet to be developed. We demonstrate the visualization and reconstruction of magnetic domain structures in a 3D curved magnetic thin films with tubular shape by means of full-field soft X-ray microscopies. In the 3D arrangement of the magnetization is retrieved from a set of 2D projections by analysing the evolution of the magnetic contrast with varying projection angle. By using reconstruction algorithms to analyse the angular evolution of 2D projections provides quantitative information about domain patterns and magnetic coupling phenomena between windings of azimuthally and radially magnetized tubular objects. In conclusion, the present approach represents a first milestone towards visualizing magnetization textures of 3D curved thin films with virtually arbitrary shape.

  20. Biological imaging by soft x-ray diffraction microscopy

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Shapiro, D.; Thibault, P.; Beetz, T.; Elser, V.; Howells, M.; Jacobsen, C.; Kirz, J.; Lima, E.; Miao, H.; Neiman, A. M.; et al

    2005-10-25

    We have used the method of x-ray diffraction microscopy to image the complex-valued exit wave of an intact and unstained yeast cell. The images of the freeze-dried cell, obtained by using 750-eV x-rays from different angular orientations, portray several of the cell's major internal components to 30-nm resolution. The good agreement among the independently recovered structures demonstrates the accuracy of the imaging technique. To obtain the best possible reconstructions, we have implemented procedures for handling noisy and incomplete diffraction data, and we propose a method for determining the reconstructed resolution. This work represents a previously uncharacterized application of x-ray diffractionmore » microscopy to a specimen of this complexity and provides confidence in the feasibility of the ultimate goal of imaging biological specimens at 10-nm resolution in three dimensions.« less

  1. X-Ray Diffraction Project Final Report, Fiscal Year 2006

    SciTech Connect (OSTI)

    Dane V. Morgan

    2006-10-01

    An x-ray diffraction diagnostic system was developed for determining real-time shock-driven lattice parameter shifts in single crystals at the gas gun at TA-IV at Sandia National Laboratories (SNL). The signal-to-noise ratio and resolution of the system were measured using imaging plates as the detector and by varying the slit width. This report includes tests of the x-ray diffraction system using a phosphor coupled to a charge-coupled device (CCD) camera by a coherent fiber-optic bundle. The system timing delay was measured with a newly installed transistor-transistor logic (TTL) bypass designed to reduce the x-ray delay time. The axial misalignment of the Bragg planes was determined with respect to the optical axis for a set of eight LiF [lithium fluoride] crystals provided by SNL to determine their suitability for gas gun experiments.

  2. X-ray radiography with highly charged ions

    DOE Patents [OSTI]

    Marrs, Roscoe E. (Livermore, CA)

    2000-01-01

    An extremely small (1-250 micron FWHM) beam of slow highly charged ions deexciting on an x-ray production target generates x-ray monochromatic radiation that is passed through a specimen and detected for imaging. The resolution of the x-ray radiograms is improved and such detection is achieved with relatively low dosages of radiation passing through the specimen. An apparatus containing an electron beam ion trap (and modifications thereof) equipped with a focusing column serves as a source of ions that generate radiation projected onto an image detector. Electronic and other detectors are able to detect an increased amount of radiation per pixel than achieved by previous methods and apparati.

  3. Movable anode x-ray source with enhanced anode cooling

    DOE Patents [OSTI]

    Bird, Charles R.; Rockett, Paul D.

    1987-01-01

    An x-ray source having a cathode and a disc-shaped anode with a peripheral surface at constant radius from the anode axis opposed to the cathode. The anode has stub axle sections rotatably carried in heat conducting bearing plates which are mounted by thermoelectric coolers to bellows which normally bias the bearing plates to a retracted position spaced from opposing anode side faces. The bellows cooperate with the x-ray source mounting structure for forming closed passages for heat transport fluid. Flow of such fluid under pressure expands the bellows and brings the bearing plates into heat conducting contact with the anode side faces. A worm gear is mounted on a shaft and engages serrations in the anode periphery for rotating the anode when flow of coolant is terminated between x-ray emission events.

  4. Movable anode x-ray source with enhanced anode cooling

    DOE Patents [OSTI]

    Bird, C.R.; Rockett, P.D.

    1987-08-04

    An x-ray source is disclosed having a cathode and a disc-shaped anode with a peripheral surface at constant radius from the anode axis opposed to the cathode. The anode has stub axle sections rotatably carried in heat conducting bearing plates which are mounted by thermoelectric coolers to bellows which normally bias the bearing plates to a retracted position spaced from opposing anode side faces. The bellows cooperate with the x-ray source mounting structure for forming closed passages for heat transport fluid. Flow of such fluid under pressure expands the bellows and brings the bearing plates into heat conducting contact with the anode side faces. A worm gear is mounted on a shaft and engages serrations in the anode periphery for rotating the anode when flow of coolant is terminated between x-ray emission events. 5 figs.

  5. Progress in Development of Kharkov X-Ray Generator Nestor

    SciTech Connect (OSTI)

    Androsov, V.; Bulyak, V.; Dovbnya, A.; Drebot, I.; Gladkikh, P.; Grevtsev, V.; Grigorev, Yu.; Gvozd, A.; Ivashchenko, V.; Karnaukhov, I.; Kovalyova, N.; Kozin, V.; Lapshin, V.; Lyashchenko, V.; Markov, V.; Mocheshnikov, N.; Mytsykov, A.; Neklyudov, I.; Peev, F.; Rezaev, A.; Shcherbakov, A.; /Kharkov, KIPT /SLAC, SSRL /Eindhoven, Tech. U. /Lebedev Inst. /Kurdyumova Inst. Metalophysics

    2005-09-14

    The sources of the X-rays based on Compton scattering of intense Nd:YAG laser beam on electron beam circulating in a storage ring with beam energy 43-225 MeV is under construction in NSC KIPT. In the paper the progress in development and construction of Kharkov X-ray generator NESTOR is presented. The current status of the main facility system design and development are described. New scheme and main parameters of injection system are presented. The status of power supply system and control system is described. The facility is going to be in operation in the middle of 2007 and generated X-rays flux is expected to be of about 10{sup 13} phot/s.

  6. Data fusion in neutron and X-ray computed tomography

    SciTech Connect (OSTI)

    Schrapp, Michael J.; Goldammer, Matthias; Schulz, Michael; Issani, Siraj; Bhamidipati, Suryanarayana; Böni, Peter

    2014-10-28

    We present a fusion methodology between neutron and X-ray computed tomography (CT). On the one hand, the inspection by X-ray CT of a wide class of multimaterials in non-destructive testing applications suffers from limited information of object features. On the other hand, neutron imaging can provide complementary data in such a way that the combination of both data sets fully characterizes the object. In this contribution, a novel data fusion procedure, called Fusion Regularized Simultaneous Algebraic Reconstruction Technique, is developed where the X-ray reconstruction is modified to fulfill the available data from the imaging with neutrons. The experiments, which were obtained from an aluminum profile containing a steel screw, and attached carbon fiber plates demonstrate that the image quality in CT can be significantly improved when the proposed fusion method is used.

  7. Imaging X-ray Thomson Scattering Spectrometer Design and Demonstration

    SciTech Connect (OSTI)

    Gamboa, E.J.; Huntington, C.M.; Trantham, M.R.; Keiter, P.A; Drake, R.P.; Montgomery, David; Benage, John F.; Letzring, Samuel A.

    2012-05-04

    In many laboratory astrophysics experiments, intense laser irradiation creates novel material conditions with large, one-dimensional gradients in the temperature, density, and ionization state. X-ray Thomson scattering is a powerful technique for measuring these plasma parameters. However, the scattered signal has previously been measured with little or no spatial resolution, which limits the ability to diagnose inhomogeneous plasmas. We report on the development of a new imaging x-ray Thomson spectrometer (IXTS) for the Omega laser facility. The diffraction of x-rays from a toroidally-curved crystal creates high-resolution images that are spatially resolved along a one-dimensional profile while spectrally dispersing the radiation. This focusing geometry allows for high brightness while localizing noise sources and improving the linearity of the dispersion. Preliminary results are presented from a scattering experiment that used the IXTS to measure the temperature profile of a shocked carbon foam.

  8. Ultraviolet germicidal irradiation and its effects on elemental distributions in mouse embryonic fibroblast cells in x-ray fluorescence microanalysis

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Jin, Qiaoling; Vogt, Stefan; Lai, Barry; Chen, Si; Finney, Lydia; Gleber, Sophie-Charlotte; Ward, Jesse; Deng, Junjing; Mak, Rachel; Moonier, Nena; et al

    2015-02-23

    Rapidly-frozen hydrated (cryopreserved) specimens combined with cryo-scanning x-ray fluorescence microscopy provide an ideal approach for investigating elemental distributions in biological cells and tissues. However, because cryopreservation does not deactivate potentially infectious agents associated with Risk Group 2 biological materials, one must be concerned with contamination of expensive and complicated cryogenic x-ray microscopes when working with such materials. We employed ultraviolet germicidal irradiation to decontaminate previously cryopreserved cells under liquid nitrogen, and then investigated its effects on elemental distributions under both frozen hydrated and freeze dried states with x-ray fluorescence microscopy. We show that the contents and distributions of most biologicallymore » important elements remain nearly unchanged when compared with non-ultraviolet-irradiated counterparts, even after multiple cycles of ultraviolet germicidal irradiation and cryogenic x-ray imaging. This provides a potential pathway for rendering Risk Group 2 biological materials safe for handling in multiuser cryogenic x-ray microscopes without affecting the fidelity of the results.« less

  9. Ultraviolet germicidal irradiation and its effects on elemental distributions in mouse embryonic fibroblast cells in x-ray fluorescence microanalysis

    SciTech Connect (OSTI)

    Jin, Qiaoling; Vogt, Stefan; Lai, Barry; Chen, Si; Finney, Lydia; Gleber, Sophie-Charlotte; Ward, Jesse; Deng, Junjing; Mak, Rachel; Moonier, Nena; Jacobsen, Chris; Brody, James P.

    2015-02-23

    Rapidly-frozen hydrated (cryopreserved) specimens combined with cryo-scanning x-ray fluorescence microscopy provide an ideal approach for investigating elemental distributions in biological cells and tissues. However, because cryopreservation does not deactivate potentially infectious agents associated with Risk Group 2 biological materials, one must be concerned with contamination of expensive and complicated cryogenic x-ray microscopes when working with such materials. We employed ultraviolet germicidal irradiation to decontaminate previously cryopreserved cells under liquid nitrogen, and then investigated its effects on elemental distributions under both frozen hydrated and freeze dried states with x-ray fluorescence microscopy. We show that the contents and distributions of most biologically important elements remain nearly unchanged when compared with non-ultraviolet-irradiated counterparts, even after multiple cycles of ultraviolet germicidal irradiation and cryogenic x-ray imaging. This provides a potential pathway for rendering Risk Group 2 biological materials safe for handling in multiuser cryogenic x-ray microscopes without affecting the fidelity of the results.

  10. Absorption and Phase Contrast X-Ray Imaging in Paleontology Using Laboratory and Synchrotron Sources

    SciTech Connect (OSTI)

    Bidola, Pidassa; Stockmar, Marco; Achterhold, Klaus; Pfeiffer, Franz; Pacheco, Mirian L.A.F.; Soriano, Carmen; Beckmann, Felix; Herzen, Julia

    2015-10-01

    X-ray micro-computed tomography (CT) is commonly used for imaging of samples in biomedical or materials science research. Owing to the ability to visualize a sample in a nondestructive way, X-ray CT is perfectly suited to inspect fossilized specimens, which are mostly unique or rare. In certain regions of the world where important sedimentation events occurred in the Precambrian geological time, several fossilized animals are studied to understand questions related to their origin, environment, and life evolution. This article demonstrates the advantages of applying absorption and phase-contrast CT on the enigmatic fossil Corumbella werneri, one of the oldest known animals capable of building hard parts, originally discovered in Corumba (Brazil). Different tomographic setups were tested to visualize the fossilized inner structures: a commercial laboratory-based CT device, two synchrotron-based imaging setups using conventional absorption and propagation-based phase contrast, and a commercial X-ray microscope with a lens-coupled detector system, dedicated for radiography and tomography. Based on our results we discuss the strengths and weaknesses of the different imaging setups for paleontological studies.

  11. Soft X-ray techniques to study mesoscale magnetism

    SciTech Connect (OSTI)

    Kortright, Jeffrey B.

    2003-06-26

    Heterogeneity in magnetization (M) is ubiquitous in modern systems. Even in nominally homogeneous materials, domains or pinning centers typically mediate magnetization reversal. Fundamental lengths determining M structure include the domain wall width and the exchange stiffness length, typically in the 4-400 nm range. Chemical heterogeneity (phase separation, polycrystalline microstructure, lithographic or other patterning, etc.) with length scales from nanometers to microns is often introduced to influence magnetic properties. With 1-2 nm wavelengths {lambda}, soft x-rays in principle can resolve structure down to {lambda}/2, and are well suited to study these mesoscopic length scales [1, 2]. This article highlights recent advances in resonant soft x-ray methods to resolve lateral magnetic structure [3], and discusses some of their relative merits and limitations. Only techniques detecting x-ray photons (rather than photo-electrons) are considered [4], since they are compatible with strong applied fields to probe relatively deeply into samples. The magneto-optical (MO) effects discovered by Faraday and Kerr were observed in the x-ray range over a century later, first at ''hard'' wavelengths in diffraction experiments probing interatomic magnetic structure [5]. In the soft x-ray range, magnetic linear [6] and circular [7] dichroism spectroscopies first developed that average over lateral magnetic structure. These large resonant MO effects enable different approaches to study magnetic structure or heterogeneity that can be categorized as microscopy or scattering [1]. Direct images of magnetic structure result from photo-emission electron microscopes [4, 8] and zone-plate microscopes [9, 10]. Scattering techniques extended into the soft x-ray include familiar specular reflection that laterally averages over structure but can provide depth-resolved information, and diffuse scattering and diffraction that provide direct information about lateral magnetic structure

  12. Bragg x-ray survey spectrometer for ITER

    SciTech Connect (OSTI)

    Varshney, S. K.; Jakhar, S.; Barnsley, R.; O'Mullane, M. G.

    2012-10-15

    Several potential impurity ions in the ITER plasmas will lead to loss of confined energy through line and continuum emission. For real time monitoring of impurities, a seven channel Bragg x-ray spectrometer (XRCS survey) is considered. This paper presents design and analysis of the spectrometer, including x-ray tracing by the Shadow-XOP code, sensitivity calculations for reference H-mode plasma and neutronics assessment. The XRCS survey performance analysis shows that the ITER measurement requirements of impurity monitoring in 10 ms integration time at the minimum levels for low-Z to high-Z impurity ions can largely be met.

  13. Breakthroughs in photonics 2013: X-ray optics

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Soufli, Regina

    2014-04-01

    Here, this review discusses the latest advances in extreme ultraviolet/X-ray optics development, which are motivated by the availability and demands of new X-ray sources and scientific and industrial applications. Among the breakthroughs highlighted are the following: i) fabrication, metrology, and mounting technologies for large-area optical substrates with improved figure, roughness, and focusing properties; ii) multilayer coatings with especially optimized layer properties, achieving improved reflectance, stability, and out-of-band suppression; and iii) nanodiffractive optics with improved efficiency and resolution.

  14. RESONANT INELASTIC X-RAY SCATTERING FROM TRANSITION METAL OXIDES.

    SciTech Connect (OSTI)

    HILL,J.P.

    1999-08-23

    Recent developments in hard x-ray resonant inelastic x-ray scattering as a probe of strongly correlated systems are reviewed. Particular attention is paid to studies of Nd{sub 2}CuO{sub 4}. A charge transfer excitation is observed when the incident photon energy is tuned in the vicinity of the copper K-edge. It is shown that the presence of resonant enhancements is controlled by the polarization dependence of the excitation process and by the overlap between a given intermediate state and the particular excitation being studied. This latter observation has shed light on the non-local effects present in certain intermediate states.

  15. X-ray Diffraction from Membrane Protein Nanocrystals

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    X-ray Diffraction from Membrane Protein Nanocrystals Authors: Hunter, M.S., DePonte, D.P., Shapiro, D.A., Kirian, R.A., Wang, X., Starodub, D., Marchesini, S., Weierstall, U., Doak, R.B., Spence, J.C.H., and Fromme, P. Title: X-ray Diffraction from Membrane Protein Nanocrystals Source: Biophysical Journal Year: 2011 Volume: 100 Pages: 198-206 ABSTRACT: Membrane proteins constitute >30% of the proteins in an average cell, and yet the number of currently known structures of unique membrane

  16. Cooling for a rotating anode X-ray tube

    DOE Patents [OSTI]

    Smither, Robert K. (Hinsdale, IL)

    1998-01-01

    A method and apparatus for cooling a rotating anode X-ray tube. An electromagnetic motor is provided to rotate an X-ray anode with cooling passages in the anode. These cooling passages are coupled to a cooling structure located adjacent the electromagnetic motor. A liquid metal fills the passages of the cooling structure and electrical power is provided to the motor to rotate the anode and generate a rotating magnetic field which moves the liquid metal through the cooling passages and cooling structure.

  17. High resolution collimator system for X-ray detector

    DOE Patents [OSTI]

    Eberhard, Jeffrey W.; Cain, Dallas E.

    1987-01-01

    High resolution in an X-ray computerized tomography (CT) inspection system is achieved by using a collimator/detector combination to limit the beam width of the X-ray beam incident on a detector element to the desired resolution width. In a detector such as a high pressure Xenon detector array, a narrow tapered collimator is provided above a wide detector element. The collimator slits have any desired width, as small as a few mils at the top, the slit width is easily controlled, and they are fabricated on standard machines. The slit length determines the slice thickness of the CT image.

  18. Serial femtosecond X-ray diffraction of enveloped virus microcrystals

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Lawrence, Robert M.; Conrad, Chelsie E.; Zatsepin, Nadia A.; Grant, Thomas D.; Liu, Haiguang; James, Daniel; Nelson, Garrett; Subramanian, Ganesh; Aquila, Andrew; Hunter, Mark S.; et al

    2015-08-20

    Serial femtosecond crystallography (SFX) using X-ray free-electron lasers has produced high-resolution, room temperature, time-resolved protein structures. We report preliminary SFX of Sindbis virus, an enveloped icosahedral RNA virus with ~700 Å diameter. Microcrystals delivered in viscous agarose medium diffracted to ~40 Å resolution. Small-angle diffuse X-ray scattering overlaid Bragg peaks and analysis suggests this results from molecular transforms of individual particles. Viral proteins undergo structural changes during entry and infection, which could, in principle, be studied with SFX. This is a pertinent step toward determining room temperature structures from virus microcrystals that may enable time-resolved studies of enveloped viruses.

  19. Cooled window for X-rays or charged particles

    DOE Patents [OSTI]

    Logan, C.M.

    1996-04-16

    A window is disclosed that provides good structural integrity and a very high capacity for removal of the heat deposited by x-rays, electrons, or ions, with minimum attenuation of the desired beam. The window is cooled by providing microchannels therein through which a coolant is pumped. For example, the window may be made of silicon with etched microchannels therein and covered by a silicon member. A window made of silicon with a total thickness of 520 {micro}m transmits 96% of the x-rays at an energy of 60 keV, and the transmission is higher than 90% for higher energy photons. 1 fig.

  20. Cooled window for X-rays or charged particles

    DOE Patents [OSTI]

    Logan, Clinton M.

    1996-01-01

    A window that provides good structural integrity and a very high capacity for removal of the heat deposited by x-rays, electrons, or ions, with minimum attenuation of the desired beam. The window is cooled by providing microchannels therein through which a coolant is pumped. For example, the window may be made of silicon with etched microchannels therein and covered by a silicon member. A window made of silicon with a total thickness of 520 .mu.m transmits 96% of the x-rays at an energy of 60 keV, and the transmission is higher than 90% for higher energy photons.

  1. Serial femtosecond X-ray diffraction of enveloped virus microcrystals

    SciTech Connect (OSTI)

    Lawrence, Robert M.; Conrad, Chelsie E.; Zatsepin, Nadia A.; Grant, Thomas D.; Liu, Haiguang; James, Daniel; Nelson, Garrett; Subramanian, Ganesh; Aquila, Andrew; Hunter, Mark S.; Liang, Mengning; Boutet, Sbastien; Coe, Jesse; Spence, John C. H.; Weierstall, Uwe; Liu, Wei; Fromme, Petra; Cherezov, Vadim; Hogue, Brenda G.

    2015-08-20

    Serial femtosecond crystallography (SFX) using X-ray free-electron lasers has produced high-resolution, room temperature, time-resolved protein structures. We report preliminary SFX of Sindbis virus, an enveloped icosahedral RNA virus with ~700 diameter. Microcrystals delivered in viscous agarose medium diffracted to ~40 resolution. Small-angle diffuse X-ray scattering overlaid Bragg peaks and analysis suggests this results from molecular transforms of individual particles. Viral proteins undergo structural changes during entry and infection, which could, in principle, be studied with SFX. This is a pertinent step toward determining room temperature structures from virus microcrystals that may enable time-resolved studies of enveloped viruses.

  2. Skyrmion Behavior Revealed by Two X-Ray Studies

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Skyrmion Behavior Revealed by Two X-Ray Studies Skyrmion Behavior Revealed by Two X-Ray Studies Print Thursday, 11 September 2014 15:18 Sometimes, the spins in a magnetic material will form tiny swirls that can move around like particles. The spins themselves stay put-it's the pattern that moves. These quasiparticles have been dubbed "skyrmions," after British physicist Tony Skyrme, who described their mathematics in a series of papers in the early 1960s. Now, over 50 years later,

  3. Predicting X-ray diffuse scattering from translation–libration–screw structural ensembles

    SciTech Connect (OSTI)

    Van Benschoten, Andrew H.; Afonine, Pavel V.; Terwilliger, Thomas C.; Wall, Michael E.; Jackson, Colin J.; Sauter, Nicholas K.; Adams, Paul D.; Urzhumtsev, Alexandre; Fraser, James S.

    2015-07-28

    Identifying the intramolecular motions of proteins and nucleic acids is a major challenge in macromolecular X-ray crystallography. Because Bragg diffraction describes the average positional distribution of crystalline atoms with imperfect precision, the resulting electron density can be compatible with multiple models of motion. Diffuse X-ray scattering can reduce this degeneracy by reporting on correlated atomic displacements. Although recent technological advances are increasing the potential to accurately measure diffuse scattering, computational modeling and validation tools are still needed to quantify the agreement between experimental data and different parameterizations of crystalline disorder. A new tool, phenix.diffuse, addresses this need by employing Guinier's equation to calculate diffuse scattering from Protein Data Bank (PDB)-formatted structural ensembles. As an example case, phenix.diffuse is applied to translation–libration–screw (TLS) refinement, which models rigid-body displacement for segments of the macromolecule. To enable the calculation of diffuse scattering from TLS-refined structures, phenix.tls_as_xyz builds multi-model PDB files that sample the underlying T, L and S tensors. In the glycerophosphodiesterase GpdQ, alternative TLS-group partitioning and different motional correlations between groups yield markedly dissimilar diffuse scattering maps with distinct implications for molecular mechanism and allostery. These methods demonstrate how, in principle, X-ray diffuse scattering could extend macromolecular structural refinement, validation and analysis.

  4. Predicting X-ray diffuse scattering from translation–libration–screw structural ensembles

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Van Benschoten, Andrew H.; Afonine, Pavel V.; Terwilliger, Thomas C.; Wall, Michael E.; Jackson, Colin J.; Sauter, Nicholas K.; Adams, Paul D.; Urzhumtsev, Alexandre; Fraser, James S.

    2015-07-28

    Identifying the intramolecular motions of proteins and nucleic acids is a major challenge in macromolecular X-ray crystallography. Because Bragg diffraction describes the average positional distribution of crystalline atoms with imperfect precision, the resulting electron density can be compatible with multiple models of motion. Diffuse X-ray scattering can reduce this degeneracy by reporting on correlated atomic displacements. Although recent technological advances are increasing the potential to accurately measure diffuse scattering, computational modeling and validation tools are still needed to quantify the agreement between experimental data and different parameterizations of crystalline disorder. A new tool, phenix.diffuse, addresses this need by employing Guinier'smore » equation to calculate diffuse scattering from Protein Data Bank (PDB)-formatted structural ensembles. As an example case, phenix.diffuse is applied to translation–libration–screw (TLS) refinement, which models rigid-body displacement for segments of the macromolecule. To enable the calculation of diffuse scattering from TLS-refined structures, phenix.tls_as_xyz builds multi-model PDB files that sample the underlying T, L and S tensors. In the glycerophosphodiesterase GpdQ, alternative TLS-group partitioning and different motional correlations between groups yield markedly dissimilar diffuse scattering maps with distinct implications for molecular mechanism and allostery. These methods demonstrate how, in principle, X-ray diffuse scattering could extend macromolecular structural refinement, validation and analysis.« less

  5. Soft x-ray diagnostics for pulsed power machines

    SciTech Connect (OSTI)

    Idzorek, G.C.; Coulter, W.L.; Walsh, P.J.; Montoya, R.R.

    1995-08-01

    A variety of soft x-ray diagnostics are being fielded on the Los Alamos National Laboratory Pegasus and Procyon pulsed power systems and also being fielded on joint US/Russian magnetized target fusion experiments known as MAGO (Magnitoye Obzhatiye). The authors have designed a low-cost modular photoemissive detector designated the XRD-96 that uses commercial 1100 series aluminum for the photocathode. In addition to photocathode detectors a number of designs using solid state silicon photodiodes have been designed and fielded. They also present a soft x-ray time-integrated pinhole camera system that uses standard type TMAX-400 photographic film that obviates the need for expensive and no longer produced zero-overcoat soft x-ray emulsion film. In a typical experiment the desired spectral energy cuts, signal intensity levels, and desired field of view will determine diagnostic geometry and x-ray filters selected. The authors have developed several computer codes to assist in the diagnostic design process and data deconvolution. Examples of the diagnostic design process and data analysis for a typical pulsed power experiment are presented.

  6. X-ray divergent-beam (Kossel) technique: A review

    SciTech Connect (OSTI)

    Lider, V. V.

    2011-03-15

    The development of the X-ray divergent-beam (Kossel) technique over the last 50 years is traced. The fundamentals of this technique and ways to implement it experimentally are considered, and its potential for studying the real structure of crystals is analyzed in detail.

  7. Measuring x-ray spectra of flash radiographic sources

    SciTech Connect (OSTI)

    Gehring, Amanda Elizabeth; Espy, Michelle A.; Haines, Todd Joseph; Mendez, Jacob; Moir, David C.; Sedillo, Robert; Shurter, Roger P.; Volegov, Petr Lvovich; Webb, Timothy J

    2015-11-02

    The x-ray spectra of flash radiographic sources is difficult to measure. The sources measured were Radiographic Integrated Test Stand-6 (370 rad at 1 m; 50 ns pulse) and Dual Axis Radiographic Hydrodynamic Test Facility (DARHT) (550 rad at 1 m; 50 ns pulse). Features of the Compton spectrometer are described, and spectra are shown. Additional slides present data on instrumental calibration.

  8. Vanadium-pumped titanium x-ray laser

    DOE Patents [OSTI]

    Nilsen, Joseph

    1992-01-01

    A resonantly photo-pumped x-ray laser (10) is formed of a vanadium (12) and titanium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state neon-like titanium ions (34) are resonantly photo-pumped by line emission from fluorine-like vanadium ions (32).

  9. Vanadium-pumped titanium x-ray laser

    DOE Patents [OSTI]

    Nilsen, J.

    1992-05-26

    A resonantly photo-pumped x-ray laser is formed of a vanadium and titanium foil combination that is driven by two beams of intense line focused optical laser radiation. Ground state neon-like titanium ions are resonantly photo-pumped by line emission from fluorine-like vanadium ions. 4 figs.

  10. Lensless imaging of nanoporous glass with soft X-rays

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Turner, Joshua J.; Nelson, Johanna; Huang, Xiaojing; Steinbrener, Jan; Jacobsen, Chris

    2013-06-01

    Coherent soft X-ray diffraction has been used to image nanoporous glass structure in two dimensions using different methods. The merit of the reconstructions was judged using a new method of Fourier phase correlation with a final, refined image. The porous structure was found to have a much larger average size then previously believed.

  11. Crystal defect studies using x-ray diffuse scattering

    SciTech Connect (OSTI)

    Larson, B.C.

    1980-01-01

    Microscopic lattice defects such as point (single atom) defects, dislocation loops, and solute precipitates are characterized by local electronic density changes at the defect sites and by distortions of the lattice structure surrounding the defects. The effect of these interruptions of the crystal lattice on the scattering of x-rays is considered in this paper, and examples are presented of the use of the diffuse scattering to study the defects. X-ray studies of self-interstitials in electron irradiated aluminum and copper are discussed in terms of the identification of the interstitial configuration. Methods for detecting the onset of point defect aggregation into dislocation loops are considered and new techniques for the determination of separate size distributions for vacancy loops and interstitial loops are presented. Direct comparisons of dislocation loop measurements by x-rays with existing electron microscopy studies of dislocation loops indicate agreement for larger size loops, but x-ray measurements report higher concentrations in the smaller loop range. Methods for distinguishing between loops and three-dimensional precipitates are discussed and possibilities for detailed studies considered. A comparison of dislocation loop size distributions obtained from integral diffuse scattering measurements with those from TEM show a discrepancy in the smaller sizes similar to that described above.

  12. X-rays at Solid-Liquid Surfaces

    SciTech Connect (OSTI)

    Dosch, Helmut (Max Planck Institute for Metals Research) [Max Planck Institute for Metals Research

    2007-05-02

    Solid-liquid interfaces play an important role in many areas of current and future technologies, and in our biosphere. They play a key role in the development of nanofluidics and nanotribology, which sensitively depend on our knowledge of the microscopic structures and phenomena at the solid-liquid interface. The detailed understanding of how a fluid meets a wall is also a theoretical challenge. In particular, the phenomena at repulsive walls are of interest, since they affect many different phenomena, such as water-repellent surfaces or the role of the hydrophobic interaction in protein folding. Recent x-ray reflectivity studies of various solid-liquid interfaces have disclosed rather intriguiing phenomena, which will be discussed in this lecture: premelting of ice in contact with silica; liquid Pb in contact with Si; water in contact with hydrophobic surfaces. These experiments, carried out with high-energy x-ray microbeams, reveal detailed insight into the liquid density profile closest to the wall. A detailed insight into atomistic phenomena at solid-liquid interfaces is also a prerequisite in the microscopic control of electrochemical reactions at interfaces. Recent x-ray studies show the enormous future potential of such non-destructive analytical tools for the in situ observation of (electro-)chemical surface reactions. This lecture will review recent x-ray experiments on solid-liquid interfaces.

  13. Enhanced Electron Efficiency in an X-ray Diode

    SciTech Connect (OSTI)

    K. Sun, L. MacNeil

    2010-05-20

    The goal for this research is to optimize the XRD structure and usage configurations and increase the efficiency of the XRD. This research was successful in optimizing the XRD structure and usage configurations, thus creating a high efficiency XRD. Best efficiency occurs when there is an angle between the photocathode and incident X-rays.

  14. Data needs for X-ray astronomy satellites

    SciTech Connect (OSTI)

    Kallman, T.

    2013-07-11

    I review the current status of atomic data for X-ray astronomy satellites. This includes some of the astrophysical issues which can be addressed, current modeling and analysis techniques, computational tools, the limitations imposed by currently available atomic data, and the validity of standard assumptions. I also discuss the future: challenges associated with future missions and goals for atomic data collection.

  15. Scanning Transmission X-ray Microscope Control Program

    Energy Science and Technology Software Center (OSTI)

    2005-08-05

    User Interface and control software or C++ to run on specifically equipped computer running Windows Operating Systems. Program performs specific control functions required to operate Interferometer controlled scanning transmission X-ray microscopes at ALS beamlines 532 and 11.0.2. Graphical user interface facilitates control, display images and spectra.

  16. Operational properties of fluctuation X-ray scattering data

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Malmerberg, Erik; Kerfeld, Cheryl A.; Zwart, Petrus H.

    2015-03-20

    X-ray scattering images collected on timescales shorter than rotation diffusion times using a (partially) coherent beam result in a significant increase in information content in the scattered data. These measurements, named fluctuation X-ray scattering (FXS), are typically performed on an X-ray free-electron laser (XFEL) and can provide fundamental insights into the structure of biological molecules, engineered nanoparticles or energy-related mesoscopic materials beyond what can be obtained with standard X-ray scattering techniques. In order to understand, use and validate experimental FXS data, the availability of basic data characteristics and operational properties is essential, but has been absent up to this point.more » In this communication, an intuitive view of the nature of FXS data and their properties is provided, the effect of FXS data on the derived structural models is highlighted, and generalizations of the Guinier and Porod laws that can ultimately be used to plan experiments and assess the quality of experimental data are presented.« less

  17. Design aspects of X-ray grating interferometry

    SciTech Connect (OSTI)

    Weitkamp, Timm; Zanette, Irene; Pfeiffer, Franz; David, Christian

    2012-07-31

    Considerations are made for the design of X-ray grating interferometers in general and, in particular, for the case of a parallel beam with a high degree of spatial coherence. We specifically discuss the properties of different types of gratings and the interdependence of instrument parameters and performance characteristics.

  18. X-ray characterization of solid small molecule organic materials

    DOE Patents [OSTI]

    Billinge, Simon; Shankland, Kenneth; Shankland, Norman; Florence, Alastair

    2014-06-10

    The present invention provides, inter alia, methods of characterizing a small molecule organic material, e.g., a drug or a drug product. This method includes subjecting the solid small molecule organic material to x-ray total scattering analysis at a short wavelength, collecting data generated thereby, and mathematically transforming the data to provide a refined set of data.

  19. Convection in X-ray Bursts Michael Zingale Stony Brook University

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Convection in X-ray Bursts Michael Zingale Stony Brook University in collaboration with Ann Almgren, John Bell, Andy Nonaka (LBL); Chris Malone (LANL), Stan Woosley (UCSC) Supported by DOE/Office of Nuclear Physics, DE-FG02-06ER41448 and DE-FG02-87ER40317 to Stony Brook, and NSF award AST-1211563. Computer time: National Energy Research Scientific Computing Center (Office of Science, DOE DE-AC02-05CH11231) Convection in Astrophysics ● Evolution of many stellar systems dominated by convective

  20. X-ray ablation measurements and modeling for ICF applications

    SciTech Connect (OSTI)

    Anderson, A.T.

    1996-09-01

    X-ray ablation of material from the first wall and other components of an ICF (Inertial Confinement Fusion) chamber is a major threat to the laser final optics. Material condensing on these optics after a shot may cause damage with subsequent laser shots. To ensure the successful operation of the ICF facility, removal rates must be predicted accurately. The goal for this dissertation is to develop an experimentally validated x-ray response model, with particular application to the National Ignition Facility (NIF). Accurate knowledge of the x-ray and debris emissions from ICF targets is a critical first step in the process of predicting the performance of the target chamber system. A number of 1-D numerical simulations of NIF targets have been run to characterize target output in terms of energy, angular distribution, spectrum, and pulse shape. Scaling of output characteristics with variations of both target yield and hohlraum wall thickness are also described. Experiments have been conducted at the Nova laser on the effects of relevant x-ray fluences on various materials. The response was diagnosed using post-shot examinations of the surfaces with scanning electron microscope and atomic force microscope instruments. Judgments were made about the dominant removal mechanisms for each material. Measurements of removal depths were made to provide data for the modeling. The finite difference ablation code developed here (ABLATOR) combines the thermomechanical response of materials to x-rays with models of various removal mechanisms. The former aspect refers to energy deposition in such small characteristic depths ({approx} micron) that thermal conduction and hydrodynamic motion are significant effects on the nanosecond time scale. The material removal models use the resulting time histories of temperature and pressure-profiles, along with ancillary local conditions, to predict rates of surface vaporization and the onset of conditions that would lead to spallation.

  1. Optical fiducial timing system for X-ray streak cameras with aluminum coated optical fiber ends

    DOE Patents [OSTI]

    Nilson, David G.; Campbell, E. Michael; MacGowan, Brian J.; Medecki, Hector

    1988-01-01

    An optical fiducial timing system is provided for use with interdependent groups of X-ray streak cameras (18). The aluminum coated (80) ends of optical fibers (78) are positioned with the photocathodes (20, 60, 70) of the X-ray streak cameras (18). The other ends of the optical fibers (78) are placed together in a bundled array (90). A fiducial optical signal (96), that is comprised of 2.omega. or 1.omega. laser light, after introduction to the bundled array (90), travels to the aluminum coated (82) optical fiber ends and ejects quantities of electrons (84) that are recorded on the data recording media (52) of the X-ray streak cameras (18). Since both 2.omega. and 1.omega. laser light can travel long distances in optical fiber with only a slight attenuation, the initial arial power density of the fiducial optical signal (96) is well below the damage threshold of the fused silica or other material that comprises the optical fibers (78, 90). Thus the fiducial timing system can be repeatably used over long durations of time.

  2. Automatic tool alignment in a backscatter X-ray scanning system

    DOE Patents [OSTI]

    Garretson, Justin; Hobart, Clinton G.; Gladwell, Thomas S.; Monda, Mark J.

    2015-11-17

    Technologies pertaining to backscatter x-ray scanning systems are described herein. The backscatter x-ray scanning system includes an x-ray source, which directs collimated x-rays along a plurality of output vectors towards a target. A detector detects diffusely reflected x-rays subsequent to respective collimated x-rays impacting the target, and outputs signals indicative of parameters of the detected x-rays. An image processing system generates an x-ray image based upon parameters of the detected x-rays, wherein each pixel in the image corresponds to a respective output vector. A user selects a particular portion of the image, and a medical device is positioned such that its directional axis is coincident with the output vector corresponding to at least one pixel in the portion of the image.

  3. Automatic tool alignment in a backscatter x-ray scanning system

    DOE Patents [OSTI]

    Garretson, Justin; Hobart, Clinton G.; Gladwell, Thomas S.; Monda, Mark J.

    2015-06-16

    Technologies pertaining to backscatter x-ray scanning systems are described herein. The backscatter x-ray scanning system includes an x-ray source, which directs collimated x-rays along a plurality of output vectors towards a target. A detector detects diffusely reflected x-rays subsequent to respective collimated x-rays impacting the target, and outputs signals indicative of parameters of the detected x-rays. An image processing system generates an x-ray image based upon parameters of the detected x-rays, wherein each pixel in the image corresponds to a respective output vector. A user selects a particular portion of the image, and a tool is positioned such that its directional axis is coincident with the output vector corresponding to at least one pixel in the portion of the image.

  4. A mirror for lab-based quasi-monochromatic parallel x-rays

    SciTech Connect (OSTI)

    Nguyen, Thanhhai; Lu, Xun; Lee, Chang Jun; Jeon, Insu; Jung, Jin-Ho; Jin, Gye-Hwan; Kim, Sung Youb

    2014-09-15

    A multilayered parabolic mirror with six W/Al bilayers was designed and fabricated to generate monochromatic parallel x-rays using a lab-based x-ray source. Using this mirror, curved bright bands were obtained in x-ray images as reflected x-rays. The parallelism of the reflected x-rays was investigated using the shape of the bands. The intensity and monochromatic characteristics of the reflected x-rays were evaluated through measurements of the x-ray spectra in the band. High intensity, nearly monochromatic, and parallel x-rays, which can be used for high resolution x-ray microscopes and local radiation therapy systems, were obtained.

  5. High resolution, multiple-energy linear sweep detector for x-ray imaging

    DOE Patents [OSTI]

    Perez-Mendez, Victor; Goodman, Claude A.

    1996-01-01

    Apparatus for generating plural electrical signals in a single scan in response to incident X-rays received from an object. Each electrical signal represents an image of the object at a different range of energies of the incident X-rays. The apparatus comprises a first X-ray detector, a second X-ray detector stacked upstream of the first X-ray detector, and an X-ray absorber stacked upstream of the first X-ray detector. The X-ray absorber provides an energy-dependent absorption of the incident X-rays before they are incident at the first X-ray detector, but provides no absorption of the incident X-rays before they are incident at the second X-ray detector. The first X-ray detector includes a linear array of first pixels, each of which produces an electrical output in response to the incident X-rays in a first range of energies. The first X-ray detector also includes a circuit that generates a first electrical signal in response to the electrical output of each of the first pixels. The second X-ray detector includes a linear array of second pixels, each of which produces an electrical output in response to the incident X-rays in a second range of energies, broader than the first range of energies. The second X-ray detector also includes a circuit that generates a second electrical signal in response to the electrical output of each of the second pixels.

  6. High resolution, multiple-energy linear sweep detector for x-ray imaging

    DOE Patents [OSTI]

    Perez-Mendez, V.; Goodman, C.A.

    1996-08-20

    Apparatus is disclosed for generating plural electrical signals in a single scan in response to incident X-rays received from an object. Each electrical signal represents an image of the object at a different range of energies of the incident X-rays. The apparatus comprises a first X-ray detector, a second X-ray detector stacked upstream of the first X-ray detector, and an X-ray absorber stacked upstream of the first X-ray detector. The X-ray absorber provides an energy-dependent absorption of the incident X-rays before they are incident at the first X-ray detector, but provides no absorption of the incident X-rays before they are incident at the second X-ray detector. The first X-ray detector includes a linear array of first pixels, each of which produces an electrical output in response to the incident X-rays in a first range of energies. The first X-ray detector also includes a circuit that generates a first electrical signal in response to the electrical output of each of the first pixels. The second X-ray detector includes a linear array of second pixels, each of which produces an electrical output in response to the incident X-rays in a second range of energies, broader than the first range of energies. The second X-ray detector also includes a circuit that generates a second electrical signal in response to the electrical output of each of the second pixels. 12 figs.

  7. Kinematics of Compton backscattering x-ray source for angiography

    SciTech Connect (OSTI)

    Blumberg, L.N.

    1992-05-01

    Calculations of X-Ray production rates, energy spread, and spectrum of Compton-backscattered photons from a Free Electron Laser on an electron beam in a low energy (136-MeV) compact (8.5-m circumference) storage ring indicate that an X-Ray intensity of 34.6 10{sup 7} X-Ray photons per 0.5-mm {times} 0.5-mm pixel for Coronary Angiography near the 33.169-keV iodine K-absorption edge can be achieved in a 4-msec pulse within a scattering cone of 1-mrad half angle. This intensity, at 10-m from the photon-electron interaction point to the patient is about a factor of 10 larger than presently achieved from a 4.5-T superconducting wiggler source in the NSLS 2.5-GeV storage ring and over an area about 5 times larger. The 2.2-keV energy spread of the Compton-backscattered beam is, however, much larger than the 70-eV spread presently attained form the wiggler source and use of a monochromator. The beam spot at the 10-m interaction point-to-patient distance is 20-mm diameter; larger spots are attainable at larger distances but with a corresponding reduction in X-Ray flux. Such a facility could be an inexpensive clinical alternative to present methods of non-invasive Digital Subtraction Angiography (DSA), small enough to be deployed in an urban medical center, and could have other medical, industrial and aerospace applications. Problems with the Compton backscattering source include laser beam heating of the mirror in the FEL oscillator optical cavity, achieving a large enough X-Ray beam spot at the patient, and obtaining radiation damping of the transverse oscillations and longitudinal emittance dilution of the storage ring electron beam resulting from photon-electron collisions without going to higher electron energy where the X-Ray energy spread becomes excessive for DSA. 38 refs.

  8. Proton-induced x-ray fluorescence CT imaging

    SciTech Connect (OSTI)

    Bazalova-Carter, Magdalena Xing, Lei; Ahmad, Moiz; Matsuura, Taeko; Takao, Seishin; Shirato, Hiroki; Umegaki, Kikuo; Matsuo, Yuto; Fahrig, Rebecca

    2015-02-15

    Purpose: To demonstrate the feasibility of proton-induced x-ray fluorescence CT (pXFCT) imaging of gold in a small animal sized object by means of experiments and Monte Carlo (MC) simulations. Methods: First, proton-induced gold x-ray fluorescence (pXRF) was measured as a function of gold concentration. Vials of 2.2 cm in diameter filled with 0%–5% Au solutions were irradiated with a 220 MeV proton beam and x-ray fluorescence induced by the interaction of protons, and Au was detected with a 3 × 3 mm{sup 2} CdTe detector placed at 90° with respect to the incident proton beam at a distance of 45 cm from the vials. Second, a 7-cm diameter water phantom containing three 2.2-diameter vials with 3%–5% Au solutions was imaged with a 7-mm FWHM 220 MeV proton beam in a first generation CT scanning geometry. X-rays scattered perpendicular to the incident proton beam were acquired with the CdTe detector placed at 45 cm from the phantom positioned on a translation/rotation stage. Twenty one translational steps spaced by 3 mm at each of 36 projection angles spaced by 10° were acquired, and pXFCT images of the phantom were reconstructed with filtered back projection. A simplified geometry of the experimental data acquisition setup was modeled with the MC TOPAS code, and simulation results were compared to the experimental data. Results: A linear relationship between gold pXRF and gold concentration was observed in both experimental and MC simulation data (R{sup 2} > 0.99). All Au vials were apparent in the experimental and simulated pXFCT images. Specifically, the 3% Au vial was detectable in the experimental [contrast-to-noise ratio (CNR) = 5.8] and simulated (CNR = 11.5) pXFCT image. Due to fluorescence x-ray attenuation in the higher concentration vials, the 4% and 5% Au contrast were underestimated by 10% and 15%, respectively, in both the experimental and simulated pXFCT images. Conclusions: Proton-induced x-ray fluorescence CT imaging of 3%–5% gold solutions in a

  9. A compact x-ray free electron laser

    SciTech Connect (OSTI)

    Barletta, W.A. . Center for Advanced Accelerators Physics Lawrence Livermore National Lab., CA ); Atac, M.; Cline, D.B.; Kolonko, J. . Center for Advanced Accelerators Physics); Bhowmik, A.; Bobbs, B.; Cover, R.A.; Dixon, F.P.; Rakowsky, G. . Rocketdyne Div.); Gallardo

    1988-01-01

    We present a design concept and simulation of the performance of a compact x-ray, free electron laser driven by ultra-high gradient rf-linacs. The accelerator design is based on recent advances in high gradient technology by a LLNL/SLAC/LBL collaboration and on the development of bright, high current electron sources by BNL and LANL. The GeV electron beams generated with such accelerators can be converted to soft x-rays in the range from 2--10 nm by passage through short period, high field strength wigglers as are being designed at Rocketdyne Linear light sources of this type can produce trains of picosecond (or shorter) pulses of extremely high spectral brilliance suitablee for flash holography of biological specimens in vivo and for studies of fast chemical reactions. 12 refs., 8 figs., 4 tabs.

  10. Towards phasing using high X-ray intensity

    SciTech Connect (OSTI)

    Galli, Lorenzo; Son, Sang-Kil; Barends, Thomas R. M.; White, Thomas A.; Barty, Anton; Botha, Sabine; Boutet, Sébastien; Caleman, Carl; Doak, R. Bruce; Nanao, Max H.; Nass, Karol; Shoeman, Robert L.; Timneanu, Nicusor; Santra, Robin; Schlichting, Ilme; Chapman, Henry N.

    2015-09-30

    X-ray free-electron lasers (XFELs) show great promise for macromolecular structure determination from sub-micrometre-sized crystals, using the emerging method of serial femtosecond crystallography. The extreme brightness of the XFEL radiation can multiply ionize most, if not all, atoms in a protein, causing their scattering factors to change during the pulse, with a preferential `bleaching' of heavy atoms. This paper investigates the effects of electronic damage on experimental data collected from a Gd derivative of lysozyme microcrystals at different X-ray intensities, and the degree of ionization of Gd atoms is quantified from phased difference Fourier maps. A pattern sorting scheme is proposed to maximize the ionization contrast and the way in which the local electronic damage can be used for a new experimental phasing method is discussed.

  11. Inelastic X-ray Scattering from Shocked Liquid Deuterium

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Regan, S. P.; Falk, K.; Gregori, G.; Radha, P. B.; Hu, S. X.; Boehly, T. R.; Crowley, B.; Glenzer, S. H.; Landen, O.; Gericke, D. O.; et al

    2012-12-28

    The Fermi-degenerate plasma conditions created in liquid deuterium by a laser-ablation—driven shock wave were probed with noncollective, spectrally resolved, inelastic x-ray Thomson scattering employing Cl Lyα line emission at 2.96 keV. Thus, these first x-ray Thomson scattering measurements of the microscopic properties of shocked deuterium show an inferred spatially averaged electron temperature of 8±5 eV, an electron density of 2.2(±0.5)×1023 cm-3, and an ionization of 0.8 (-0.25, +0.15). Our two-dimensional hydrodynamic simulations using equation-of-state models suited for the extreme parameters occurring in inertial confinement fusion research and planetary interiors are consistent with the experimental results.

  12. X-ray calibration of Kodak Direct Exposure film

    SciTech Connect (OSTI)

    Brown, D.B.; Burkhalter, P.G.; Rockett, P.D.; Bird, C.R.; Hailey, C.J.; Sullivan, D.

    1985-08-15

    Kodak Direct Exposure film (DEF) has replaced Kodak No-Screen film for use in x-ray diffraction analysis and in autoradiography. DEF is a double-emulsion film which has been found to have improved radio-graphic characteristics over No-Screen. A set of H-D curves has been generated for DEF at five photon energies: 0.930, 1.49, 1.74, 4.51/4.93, and 6.93 keV. The KMSF x-ray calibration facility was utilized to study the absolute sensitivity of this film over its full dynamic range. Physical examination of the film was followed by theoretical modeling, which adequately reproduced the measured curves.

  13. X-ray mask and method for providing same

    DOE Patents [OSTI]

    Morales, Alfredo M. (Pleasanton, CA); Skala, Dawn M. (Fremont, CA)

    2004-09-28

    The present invention describes a method for fabricating an x-ray mask tool which can achieve pattern features having lateral dimension of less than 1 micron. The process uses a thin photoresist and a standard lithographic mask to transfer an trace image pattern in the surface of a silicon wafer by exposing and developing the resist. The exposed portion of the silicon substrate is then anisotropically etched to provide an etched image of the trace image pattern consisting of a series of channels in the silicon having a high depth-to-width aspect ratio. These channels are then filled by depositing a metal such as gold to provide an inverse image of the trace image and thereby providing a robust x-ray mask tool.

  14. X-ray mask and method for providing same

    DOE Patents [OSTI]

    Morales, Alfredo M.; Skala, Dawn M.

    2002-01-01

    The present invention describes a method for fabricating an x-ray mask tool which can achieve pattern features having lateral dimension of less than 1 micron. The process uses a thin photoresist and a standard lithographic mask to transfer an trace image pattern in the surface of a silicon wafer by exposing and developing the resist. The exposed portion of the silicon substrate is then anisotropically etched to provide an etched image of the trace image pattern consisting of a series of channels in the silicon having a high depth-to-width aspect ratio. These channels are then filled by depositing a metal such as gold to provide an inverse image of the trace image and thereby providing a robust x-ray mask tool.

  15. Fiber fed x-ray/gamma ray imaging apparatus

    DOE Patents [OSTI]

    Hailey, C.J.; Ziock, K.P.

    1992-06-02

    X-ray/gamma ray imaging apparatus is disclosed for detecting the position, energy, and intensity of x-ray/gamma ray radiation comprising scintillation means disposed in the path of such radiation and capable of generating photons in response to such radiation; first photodetection means optically bonded to the scintillation means and capable of generating an electrical signal indicative of the intensity, and energy of the radiation detected by the scintillation means; second photodetection means capable of generating an electrical signal indicative of the position of the radiation in the radiation pattern; and means for optically coupling the scintillation means to the second photodetection means. The photodetection means are electrically connected to control and storage means which may also be used to screen out noise by rejecting a signal from one photodetection means not synchronized to a signal from the other photodetection means; and also to screen out signals from scattered radiation. 6 figs.

  16. Phase Effects on Mesoscale Object X-ray Absorption Images

    SciTech Connect (OSTI)

    Martz, Jr., H E; Aufderheide, M B; Barty, A; Lehman, S K; Kozioziemski, B J; Schneberk, D J

    2004-09-24

    At Lawrence Livermore National Laboratory particular emphasis is being placed on the nondestructive characterization (NDC) of 'mesoscale' objects.[Martz and Albrecht 2003] We define mesoscale objects as objects that have mm extent with {micro}m features. Here we confine our discussions to x-ray imaging methods applicable to mesoscale object characterization. The goal is object recovery algorithms including phase to enable emerging high-spatial resolution x-ray imaging methods to ''see'' inside or image mesoscale-size materials and objects. To be successful our imaging characterization effort must be able to recover the object function to one micrometer or better spatial resolution over a few millimeters field-of-view with very high contrast.

  17. Fiber fed x-ray/gamma ray imaging apparatus

    DOE Patents [OSTI]

    Hailey, Charles J.; Ziock, Klaus-Peter

    1992-01-01

    X-ray/gamma ray imaging apparatus is disclosed for detecting the position, energy, and intensity of x-ray/gamma ray radiation comprising scintillation means disposed in the path of such radiation and capable of generating photons in response to such radiation; first photodetection means optically bonded to the scintillation means and capable of generating an electrical signal indicative of the intensity, and energy of the radiation detected by the scintillation means; second photodetection means capable of generating an electrical signal indicative of the position of the radiation in the radiation pattern; and means for optically coupling the scintillation means to the second photodetection means. The photodetection means are electrically connected to control and storage means which may also be used to screen out noise by rejecting a signal from one photodetection means not synchronized to a signal from the other photodetection means; and also to screen out signals from scattered radiation.

  18. Towards phasing using high X-ray intensity

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Galli, Lorenzo; Son, Sang -Kil; Barends, Thomas R. M.; White, Thomas A.; Barty, Anton; Botha, Sabine; Boutet, Sébastien; Caleman, Carl; Doak, R. Bruce; Nanao, Max H.; et al

    2015-09-30

    X-ray free-electron lasers (XFELs) show great promise for macromolecular structure determination from sub-micrometre-sized crystals, using the emerging method of serial femtosecond crystallography. The extreme brightness of the XFEL radiation can multiply ionize most, if not all, atoms in a protein, causing their scattering factors to change during the pulse, with a preferential `bleaching' of heavy atoms. This paper investigates the effects of electronic damage on experimental data collected from a Gd derivative of lysozyme microcrystals at different X-ray intensities, and the degree of ionization of Gd atoms is quantified from phased difference Fourier maps. In conclusion, a pattern sorting schememore » is proposed to maximize the ionization contrast and the way in which the local electronic damage can be used for a new experimental phasing method is discussed.« less

  19. Chandra X-ray Observations of WZ Sge in Superoutburst

    SciTech Connect (OSTI)

    Wheatley, P J; Mauche, C W

    2004-10-13

    We present seven separate Chandra observations of the 2001 superoutburst of WZ Sge. The high-energy outburst was dominated by intense EUV emission lines, which we interpret as boundary layer emission scattered into our line of sight in an accretion disc wind. The direct boundary layer emission was hidden from view, presumably by the accretion disc. The optical outburst orbital hump was detected in the EUV, but the common superhump was not, indicating a geometric mechanism in the former and a dissipative mechanism in the latter. X-rays detected during outburst were not consistent with boundary layer emission and we argue that there must be a second source of X-rays in dwarf novae in outburst.

  20. Inelastic X-ray Scattering from Shocked Liquid Deuterium

    SciTech Connect (OSTI)

    Regan, S. P.; Falk, K.; Gregori, G.; Radha, P. B.; Hu, S. X.; Boehly, T. R.; Crowley, B.; Glenzer, S. H.; Landen, O.; Gericke, D. O.; Doeppner, T.; Meyerhofer, D. D.; Murphy, C. D.; Sangster, T. C.; Vorberger, J.

    2012-12-28

    The Fermi-degenerate plasma conditions created in liquid deuterium by a laser-ablation—driven shock wave were probed with noncollective, spectrally resolved, inelastic x-ray Thomson scattering employing Cl Lyα line emission at 2.96 keV. Thus, these first x-ray Thomson scattering measurements of the microscopic properties of shocked deuterium show an inferred spatially averaged electron temperature of 8±5 eV, an electron density of 2.2(±0.5)×1023 cm-3, and an ionization of 0.8 (-0.25, +0.15). Our two-dimensional hydrodynamic simulations using equation-of-state models suited for the extreme parameters occurring in inertial confinement fusion research and planetary interiors are consistent with the experimental results.

  1. Towards phasing using high X-ray intensity

    SciTech Connect (OSTI)

    Galli, Lorenzo; Son, Sang -Kil; Barends, Thomas R. M.; White, Thomas A.; Barty, Anton; Botha, Sabine; Boutet, Sébastien; Caleman, Carl; Doak, R. Bruce; Nanao, Max H.; Nass, Karol; Shoeman, Robert L.; Timneanu, Nicusor; Santra, Robin; Schlichting, Ilme; Chapman, Henry N.

    2015-09-30

    X-ray free-electron lasers (XFELs) show great promise for macromolecular structure determination from sub-micrometre-sized crystals, using the emerging method of serial femtosecond crystallography. The extreme brightness of the XFEL radiation can multiply ionize most, if not all, atoms in a protein, causing their scattering factors to change during the pulse, with a preferential `bleaching' of heavy atoms. This paper investigates the effects of electronic damage on experimental data collected from a Gd derivative of lysozyme microcrystals at different X-ray intensities, and the degree of ionization of Gd atoms is quantified from phased difference Fourier maps. In conclusion, a pattern sorting scheme is proposed to maximize the ionization contrast and the way in which the local electronic damage can be used for a new experimental phasing method is discussed.

  2. Background-reducing X-ray multilayer mirror

    DOE Patents [OSTI]

    Bloch, Jeffrey J.; Roussel-Dupre', Diane; Smith, Barham W.

    1992-01-01

    Background-reducing x-ray multilayer mirror. A multiple-layer "wavetrap" deposited over the surface of a layered, synthetic-microstructure soft x-ray mirror optimized for reflectivity at chosen wavelengths is disclosed for reducing the reflectivity of undesired, longer wavelength incident radiation incident thereon. In three separate mirror designs employing an alternating molybdenum and silicon layered, mirrored structure overlaid by two layers of a molybdenum/silicon pair anti-reflection coating, reflectivities of near normal incidence 133, 171, and 186 .ANG. wavelengths have been optimized, while that at 304 .ANG. has been minimized. The optimization process involves the choice of materials, the composition of the layer/pairs as well as the number thereof, and the distance therebetween for the mirror, and the simultaneous choice of materials, the composition of the layer/pairs, and their number and distance for the "wavetrap."

  3. Qualitative comparison of bremsstrahlung X-rays and 800 MeV protons for tomography of urania fuel pellets

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Morris, Christopher L.; Bourke, Mark A.; Byler, Darrin D.; Chen, Ching-Fong; Hogan, Gary E.; Hunter, James F.; Kwiatkowski, Kris K.; Mariam, Fesseha G.; McClellan, Kenneth J.; Merrill, Frank E.; et al

    2013-01-01

    We present an assessment of x-rays and proton tomography as tools for studying the time dependence of the development of damage in fuel rods. Also, we show data taken with existing facilities at Los Alamos National Laboratory that support this assessment. Data on surrogate fuel rods has been taken using the 800 MeV proton radiography (pRad) facility at the Los Alamos Neutron Science Center (LANSCE), and with a 450 keV bremsstrahlung X-ray tomography facility. The proton radiography pRad facility at LANSCE can provide good position resolution (<70 μm has been demonstrate, 20 μm seems feasible with minor changes) for tomographymore » on activated fuel rods. Bremsstrahlung x-rays may be able to provide better than 100 μm resolution but further development of sources, collimation and detectors is necessary for x-rays to deal with the background radiation for tomography of activated fuel rods.« less

  4. Type I X-ray burst simulation code

    Energy Science and Technology Software Center (OSTI)

    2007-07-01

    dAGILE is an astrophysical code that simulates accretion of matter onto a neutron star and the subsequent x-ray burst. It is a one-dimensional time-dependent spherically symmetric code with generalized nuclear reaction networks, diffusive radiation/conduction, realistic boundary conditions, and general relativistic hydrodynamics. The code is described in more detail in Astrophysical Journal 650(2006)332 and Astrophysical Journal Supplements 174(2008)261.

  5. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  6. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  7. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  8. Detecting rare, abnormally large grains by x-ray diffraction

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Detecting rare, abnormally large grains by x-ray diffraction - Sandia Energy Energy Search Icon Sandia Home Locations Contact Us Employee Locator Energy & Climate Secure & Sustainable Energy Future Stationary Power Energy Conversion Efficiency Solar Energy Wind Energy Water Power Supercritical CO2 Geothermal Natural Gas Safety, Security & Resilience of the Energy Infrastructure Energy Storage Nuclear Power & Engineering Grid Modernization Battery Testing Nuclear Energy Defense

  9. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow

  10. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow

  11. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow

  12. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow

  13. Using Light to Control How X Rays Interact with Matter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Light to Control How X Rays Interact with Matter Print Schemes that use one light pulse to manipulate interactions of another with matter are well developed in the visible-light regime where an optical control pulse influences how an optical probe pulse interacts with a medium. This approach has opened new research directions in fields like quantum computing and nonlinear optics, while also spawning entirely new research areas, such as electromagnetically induced transparency and slow

  14. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  15. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  16. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  17. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  18. Polarized X-Rays Reveal Molecular Alignment in Printed Electronics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Polarized X-Rays Reveal Molecular Alignment in Printed Electronics Print The printing of electronic devices using giant roll-to-roll presses or inkjet-style printers has recently been made possible by the development of solution-processable organic materials with optoelectronic properties. Organic light-emitting diodes (OLEDs) are already being produced commercially, and sensors, organic thin-film transistors (OTFTs), and organic photovoltaics (OPVs) are also well on their way to commercial

  19. Sensitivity in X-ray grating interferometry on compact systems

    SciTech Connect (OSTI)

    Thuering, Thomas; Modregger, Peter; Haemmerle, Stefan; Weiss, Stephan; Nueesch, Joachim; Stampanoni, Marco

    2012-07-31

    The optimization of compact X-ray grating interferometry systems is crucial for the progress of this technique in industrial devices. Here, an analytical formulation for the sensitivity of the phase contrast image acquisition is derived using previous results from noise analyses. Furthermore, experimental measurements of the sensitivity for different configurations are compared, providing further insight into the dependence on polychromatic radiation. Finally, strategies for the geometrical optimization are given.

  20. Application of x-ray imaging to oil refinery processes

    SciTech Connect (OSTI)

    Gamblin, B.R.; Newton, D.; Smith, G.B.

    1996-12-31

    X-ray imaging is a non-intrusive method of visualizing the flow patterns of rapidly changing multiphase systems and is based on the variation in the absorbance of X-rays by the different phases. BP has applied the X-ray technique to a variety of problems encountered within the oil and petrochemical industries in which two or three phases are present e.g. Fluid Catalytic Cracking (riser, stripper, regenerator) and three phase systems such as slurry bubble column reactors. In general, to obtain the maximum productivity from these units it is essential to optimize the contacting between a catalyst and a process fluid or fluids. This work reports on laboratory experimental work in which full scale refinery components were visualized in order to characterize the existing designs. Modified designs were then tested and evaluated before implementation on the refinery unit. Economic assessments of some of the benefits which can be realized in an oil refinery as a result of such design improvements are also presented. 3 refs., 1 fig.