Sample records for gaslab flask sampling

  1. Glass flask air sample analysis through Gas Chromatography in India: Implications for constraining CO2 surface fluxes

    E-Print Network [OSTI]

    for an air inlet (equipped with a 7µm filter), a pump and a battery placed below the ON/OFF button, a flow to the site measurements, they are prepared and evacuated. We pump and heat the flasks. During pumping the temperature is +60 dc. Flasks are pumped for 72 hours. Outlook Air sampling started at two new stations, Cape

  2. ARM-LBNL-NOAA Flask Sampler for Carbon Cycle Gases

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Torn, Margaret

    Data from ccg-flasks are sampled at the ARM SGP site and analyzed by the NOAA Earth System Research Laboratory (ESRL) as part of the NOAA Cooperative Global Air Sampling Network. Surface samples are collected from a 60m tower at the SGP Central Facility, usually once per week on one afternoon. The aircraft samples are collected approximately weekly from a chartered aircraft, and the collection flight path is centered over the tower where the surface samples are collected. Samples are collected by the ARM/LBNL Carbon Project. CO2 flask data contains measurements of CO2 concentration and CO2 stable isotope ratios (13CO2 and C18OO) from flasks collected at the SGP site. The flask samples are collected at 2m, 4m, 25m, and 60m along the 60m tower.

  3. ARM Carbon Cycle Gases Flasks at SGP Site

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Biraud, Sebastien

    Data from flasks are sampled at the Atmospheric Radiation Measurement Program ARM, Southern Great Plains Site and analyzed by the National Oceanic and Atmospheric Administration NOAA, Earth System Research Laboratory ESRL. The SGP site is included in the NOAA Cooperative Global Air Sampling Network. The surface samples are collected from a 60 m tower at the ARM SGP Central Facility, usually once per week in the afternoon. The aircraft samples are collected approximately weekly from a chartered aircraft, and the collection flight path is centered over the tower where the surface samples are collected. The samples are collected by the ARM and LBNL Carbon Project.

  4. CIS 192: Lecture 10 Web Development with Flask

    E-Print Network [OSTI]

    Plotkin, Joshua B.

    CIS 192: Lecture 10 Web Development with Flask Lili Dworkin University of Pennsylvania #12;Last at successively higher integers When we refer to i, we get what it currently points to #12;Web Frameworks We

  5. Development and application of the scintillation flask technique for the measurement of indoor radon-222 concentrations

    E-Print Network [OSTI]

    Vasquez, Gerard Michael

    1986-01-01T23:59:59.000Z

    half-life. Exposure to alpha emitting radon progeny is the major source of natural radiation doses to the lung (NCRP84b). Almost all of this is received indoors, where radon levels are elevated due to a trapping effect 1n the enclosed areas. Since... measure indoor radon and radon progeny levels, a suitable detection method must be developed. Charles (Ch84) designed and constructed an air grab sampling system using "scintillation flasks". There were, however, some minor problems with the system...

  6. The application of a scintillation flask technique for the measurement of radon emanation

    E-Print Network [OSTI]

    Charles, Martha

    1984-01-01T23:59:59.000Z

    that these flasks are reliable in a wide spectrum of situations, including the severe conditions of uranium mines, because of their mechanical durability. Phosphors Scintillation cells are internally coated with a silver activated zinc sulfide phospor (Zn... Technique in Coating the Flask MATERIALS AND METHODS Procedures for Flask Construction Bonding Solution and Storage Construction of a Light Tight Box Electronics and Photomultiplier Tube Calibration of the Flask Accumulator Method 2 4 8 9 ll 12...

  7. Flask: A Language for Data-driven Sensor Network Geoffrey Mainland, Matt Welsh, and Greg Morrisett

    E-Print Network [OSTI]

    processing to reduce energy and radio bandwidth usage. As a result, application developers typically invest chains of operators into a dataflow graph that may reside on individual nodes or span multiple nodes in the network. To compose dataflow graphs across sensor nodes, Flask supports a lean, general

  8. Inverse modeling of CO2 sources and sinks using satellite observations of CO2 from TES and surface flask measurements

    SciTech Connect (OSTI)

    Nassar, Ray [University of Toronto; Jones, DBA [University of Toronto; Kulawik, SS [Jet Propulsion Laboratory, Pasadena, CA; Worden, JR [Jet Propulsion Laboratory, Pasadena, CA; Bowman, K [Jet Propulsion Laboratory, Pasadena, CA; Andres, Robert Joseph [ORNL; Suntharalingam, P [University of East Anglia, Norwich, United Kingdom; Chen, j. [University of Toronto; Brenninkmeijer, CAM [Max Planck Institut fur Chemie, Mainz; Schuck, TJ [Max Planck Institut fur Chemie, Mainz; Conway, T.J. [NOAA, Boulder, CO; Worthy, DE [Environment Canada

    2011-01-01T23:59:59.000Z

    We infer CO2 surface fluxes using satellite observations of mid-tropospheric CO2 from the Tropospheric Emission Spectrometer (TES) and measurements of CO2 from surface flasks in a time-independent inversion analysis based on the GEOS-Chem model. Using TES CO2 observations over oceans, spanning 40 S 40 N, we find that the horizontal and vertical coverage of the TES and flask data are complementary. This complementarity is demonstrated by combining the datasets in a joint inversion, which provides better constraints than from either dataset alone, when a posteriori CO2 distributions are evaluated against independent ship and aircraft CO2 data. In particular, the joint inversion offers improved constraints in the tropics where surface measurements are sparse, such as the tropical forests of South America. Aggregating the annual surface-to-atmosphere fluxes from the joint inversion for the year 2006 yields 1.13 0.21 PgC for the global ocean, 2.77 0.20 PgC for the global land biosphere and 3.90 0.29 PgC for the total global natural flux (defined as the sum of all biospheric, oceanic, and biomass burning contributions but excluding CO2 emissions from fossil fuel combustion). These global ocean and global land fluxes are shown to be near the median of the broad range of values from other inversion results for 2006. To achieve these results, a bias in TES CO2 in the Southern Hemisphere was assessed and corrected using aircraft flask data, and we demonstrate that our results have low sensitivity to variations in the bias correction approach. Overall, this analysis suggests that future carbon data assimilation systems can benefit by integrating in situ and satellite observations of CO2 and that the vertical information provided by satellite observations of mid-tropospheric CO2 combined with measurements of surface CO2, provides an important additional constraint for flux inversions.

  9. ARM - Instrument - flask

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcal Documentation(AVIRIS) ProductsAirborneOctobergovInstrumentsecmwfdiag Documentation

  10. ARM - Campaign Instrument - flask

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary)morphinanInformation DesertgovInstrumentsap-surf Comments? We would loveair Comments?govInstrumentsflask Comments?

  11. Sampling box

    DOE Patents [OSTI]

    Phillips, Terrance D. (617 Chestnut Ct., Aiken, SC 29803); Johnson, Craig (100 Midland Rd., Oak Ridge, TN 37831-0895)

    2000-01-01T23:59:59.000Z

    An air sampling box that uses a slidable filter tray and a removable filter cartridge to allow for the easy replacement of a filter which catches radioactive particles is disclosed.

  12. E-Print Network 3.0 - acid fermentative production Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    SUPPLY Summary: , (12) PC for process monitoring. 2.4 Shake flask fermentations acid Biogas Step 1 Wet oxidation Step 2... ETHANOL PRODUCTION FROM DIFFERENT CARBON SOURCES USING...

  13. VAPOR PRESSURE ISOTOPE EFFECTS IN THE MEASUREMENT OF ENVIRONMENTAL TRITIUM SAMPLES.

    SciTech Connect (OSTI)

    Kuhne, W.

    2012-12-03T23:59:59.000Z

    Standard procedures for the measurement of tritium in water samples often require distillation of an appropriate sample aliquot. This distillation process may result in a fractionation of tritiated water and regular light water due to the vapor pressure isotope effect, introducing either a bias or an additional contribution to the total tritium measurement uncertainty. The magnitude of the vapor pressure isotope effect is characterized as functions of the amount of water distilled from the sample aliquot and the heat settings for the distillation process. The tritium concentration in the distillate is higher than the tritium concentration in the sample early in the distillation process, it then sharply decreases due to the vapor pressure isotope effect and becomes lower than the tritium concentration in the sample, until the high tritium concentration retained in the boiling flask is evaporated at the end of the process. At that time, the tritium concentration in the distillate again overestimates the sample tritium concentration. The vapor pressure isotope effect is more pronounced the slower the evaporation and distillation process is conducted; a lower heat setting during the evaporation of the sample results in a larger bias in the tritium measurement. The experimental setup used and the fact that the current study allowed for an investigation of the relative change in vapor pressure isotope effect in the course of the distillation process distinguish it from and extend previously published measurements. The separation factor as a quantitative measure of the vapor pressure isotope effect is found to assume values of 1.034 {+-} 0.033, 1.052 {+-} 0.025, and 1.066 {+-} 0.037, depending on the vigor of the boiling process during distillation of the sample. A lower heat setting in the experimental setup, and therefore a less vigorous boiling process, results in a larger value for the separation factor. For a tritium measurement in water samples, this implies that the tritium concentration could be underestimated by 3 - 6%.

  14. E-Print Network 3.0 - adapted seawater microbiota Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    sydowii, a Summary: seawater and inoculated on KMV ((glucose (1 g l1 ), gelatin hydro- lysate (1 g l1 ), yeast extract (0.1 g... in fifteen 250 ml flasks containing...

  15. ESPC IDIQ Contract Sample

    Broader source: Energy.gov [DOE]

    Document displays a sample indefinite delivery, indefinite quantity (IDIQ) energy savings performance contract (ESPC).

  16. Rain sampling device

    DOE Patents [OSTI]

    Nelson, D.A.; Tomich, S.D.; Glover, D.W.; Allen, E.V.; Hales, J.M.; Dana, M.T.

    1991-05-14T23:59:59.000Z

    The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of the precipitation from the chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device. 11 figures.

  17. Rain sampling device

    DOE Patents [OSTI]

    Nelson, Danny A. (Richland, WA); Tomich, Stanley D. (Richland, WA); Glover, Donald W. (Prosser, WA); Allen, Errol V. (Benton City, WA); Hales, Jeremy M. (Kennewick, WA); Dana, Marshall T. (Richland, WA)

    1991-01-01T23:59:59.000Z

    The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of said precipitation from said chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device.

  18. COMPUTER SCIENCE SAMPLE PROGRAM

    E-Print Network [OSTI]

    Gering, Jon C.

    COMPUTER SCIENCE SAMPLE PROGRAM (First Math Course MATH 198) This sample program suggests one way CS 181: Foundations of Computer Science II CS 180: Foundations of Computer Science I CS 191

  19. Sampled data lattice filters

    E-Print Network [OSTI]

    Thrift, William Terry

    1980-01-01T23:59:59.000Z

    SAMPLED DATA LATTICE FILTERS A Thesis by WILLIAM TERRY THRIFT III Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE December 1979 Major Subfect...: Electrical Engineering SAMPLED DATA LATTICE FILTERS A Thesis by WILLIAM TERRY THRIFT III Approved as to style and content by: (Chair an of Committee) (Hea f Department) (Member) (Member) (Member) (Member) December 1979 ABSTRACT Sampled Data...

  20. Rehabilitation Services Sample Occupations

    E-Print Network [OSTI]

    Ronquist, Fredrik

    /Industries Correction Agencies Drug Treatment Centers Addiction Counselor Advocacy Occupations Art Therapist BehavioralRehabilitation Services Sample Occupations Sample Work Settings Child & Day Care Centers Clinics................................ IIB 29-1000 E4 Careers in Counseling and Human Services .........IIB 21-1010 C7 Careers in Health Care

  1. Sampling system and method

    DOE Patents [OSTI]

    Decker, David L.; Lyles, Brad F.; Purcell, Richard G.; Hershey, Ronald Lee

    2013-04-16T23:59:59.000Z

    The present disclosure provides an apparatus and method for coupling conduit segments together. A first pump obtains a sample and transmits it through a first conduit to a reservoir accessible by a second pump. The second pump further conducts the sample from the reservoir through a second conduit.

  2. Biological sample collector

    DOE Patents [OSTI]

    Murphy, Gloria A. (French Camp, CA)

    2010-09-07T23:59:59.000Z

    A biological sample collector is adapted to a collect several biological samples in a plurality of filter wells. A biological sample collector may comprise a manifold plate for mounting a filter plate thereon, the filter plate having a plurality of filter wells therein; a hollow slider for engaging and positioning a tube that slides therethrough; and a slide case within which the hollow slider travels to allow the tube to be aligned with a selected filter well of the plurality of filter wells, wherein when the tube is aligned with the selected filter well, the tube is pushed through the hollow slider and into the selected filter well to sealingly engage the selected filter well and to allow the tube to deposit a biological sample onto a filter in the bottom of the selected filter well. The biological sample collector may be portable.

  3. Waste classification sampling plan

    SciTech Connect (OSTI)

    Landsman, S.D.

    1998-05-27T23:59:59.000Z

    The purpose of this sampling is to explain the method used to collect and analyze data necessary to verify and/or determine the radionuclide content of the B-Cell decontamination and decommissioning waste stream so that the correct waste classification for the waste stream can be made, and to collect samples for studies of decontamination methods that could be used to remove fixed contamination present on the waste. The scope of this plan is to establish the technical basis for collecting samples and compiling quantitative data on the radioactive constituents present in waste generated during deactivation activities in B-Cell. Sampling and radioisotopic analysis will be performed on the fixed layers of contamination present on structural material and internal surfaces of process piping and tanks. In addition, dose rate measurements on existing waste material will be performed to determine the fraction of dose rate attributable to both removable and fixed contamination. Samples will also be collected to support studies of decontamination methods that are effective in removing the fixed contamination present on the waste. Sampling performed under this plan will meet criteria established in BNF-2596, Data Quality Objectives for the B-Cell Waste Stream Classification Sampling, J. M. Barnett, May 1998.

  4. Water Sample Concentrator

    ScienceCinema (OSTI)

    Idaho National Laboratory

    2010-01-08T23:59:59.000Z

    Automated portable device that concentrates and packages a sample of suspected contaminated water for safe, efficient transport to a qualified analytical laboratory. This technology will help safeguard against pathogen contamination or chemical and biolog

  5. Dissolution actuated sample container

    DOE Patents [OSTI]

    Nance, Thomas A.; McCoy, Frank T.

    2013-03-26T23:59:59.000Z

    A sample collection vial and process of using a vial is provided. The sample collection vial has an opening secured by a dissolvable plug. When dissolved, liquids may enter into the interior of the collection vial passing along one or more edges of a dissolvable blocking member. As the blocking member is dissolved, a spring actuated closure is directed towards the opening of the vial which, when engaged, secures the vial contents against loss or contamination.

  6. SAMPLING AND ANALYSIS PROTOCOLS

    SciTech Connect (OSTI)

    Jannik, T; P Fledderman, P

    2007-02-09T23:59:59.000Z

    Radiological sampling and analyses are performed to collect data for a variety of specific reasons covering a wide range of projects. These activities include: Effluent monitoring; Environmental surveillance; Emergency response; Routine ambient monitoring; Background assessments; Nuclear license termination; Remediation; Deactivation and decommissioning (D&D); and Waste management. In this chapter, effluent monitoring and environmental surveillance programs at nuclear operating facilities and radiological sampling and analysis plans for remediation and D&D activities will be discussed.

  7. Liquid sampling system

    DOE Patents [OSTI]

    Larson, L.L.

    1984-09-17T23:59:59.000Z

    A conduit extends from a reservoir through a sampling station and back to the reservoir in a closed loop. A jet ejector in the conduit establishes suction for withdrawing liquid from the reservoir. The conduit has a self-healing septum therein upstream of the jet ejector for receiving one end of a double-ended cannula, the other end of which is received in a serum bottle for sample collection. Gas is introduced into the conduit at a gas bleed between the sample collection bottle and the reservoir. The jet ejector evacuates gas from the conduit and the bottle and aspirates a column of liquid from the reservoir at a high rate. When the withdrawn liquid reaches the jet ejector the rate of flow therethrough reduces substantially and the gas bleed increases the pressure in the conduit for driving liquid into the sample bottle, the gas bleed forming a column of gas behind the withdrawn liquid column and interrupting the withdrawal of liquid from the reservoir. In the case of hazardous and toxic liquids, the sample bottle and the jet ejector may be isolated from the reservoir and may be further isolated from a control station containing remote manipulation means for the sample bottle and control valves for the jet ejector and gas bleed. 5 figs.

  8. Fluid sampling system

    DOE Patents [OSTI]

    Houck, E.D.

    1994-10-11T23:59:59.000Z

    An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to be decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank. 4 figs.

  9. Fluid sampling system

    DOE Patents [OSTI]

    Houck, Edward D. (Idaho Falls, ID)

    1994-01-01T23:59:59.000Z

    An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank.

  10. Viscous sludge sample collector

    DOE Patents [OSTI]

    Beitel, George A [Richland, WA

    1983-01-01T23:59:59.000Z

    A vertical core sample collection system for viscous sludge. A sample tube's upper end has a flange and is attached to a piston. The tube and piston are located in the upper end of a bore in a housing. The bore's lower end leads outside the housing and has an inwardly extending rim. Compressed gas, from a storage cylinder, is quickly introduced into the bore's upper end to rapidly accelerate the piston and tube down the bore. The lower end of the tube has a high sludge entering velocity to obtain a full-length sludge sample without disturbing strata detail. The tube's downward motion is stopped when its upper end flange impacts against the bore's lower end inwardly extending rim.

  11. Environmental Science: Sample Pathway

    E-Print Network [OSTI]

    Goldberg, Bennett

    Environmental Science: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Core GE 100 Intro to Env Science ES 105 Env Earth Science Sophomore Year CGS Core (CGS NS201 will fulfill CAS BI107 & 124) MA 115 Statistics Summer Environmental Internship Junior Year CH 171 Chem for Health Sciences CH

  12. Decoupled Sampling for Graphics Pipelines

    E-Print Network [OSTI]

    Ragan-Kelley, Jonathan Millar

    We propose a generalized approach to decoupling shading from visibility sampling in graphics pipelines, which we call decoupled sampling. Decoupled sampling enables stochastic supersampling of motion and defocus blur at ...

  13. Fluid sampling apparatus and method

    DOE Patents [OSTI]

    Yeamans, D.R.

    1998-02-03T23:59:59.000Z

    Incorporation of a bellows in a sampling syringe eliminates ingress of contaminants, permits replication of amounts and compression of multiple sample injections, and enables remote sampling for off-site analysis. 3 figs.

  14. Sample introducing apparatus and sample modules for mass spectrometer

    DOE Patents [OSTI]

    Thompson, Cyril V. (Knoxville, TN); Wise, Marcus B. (Kingston, TN)

    1993-01-01T23:59:59.000Z

    An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus.

  15. Sample introducing apparatus and sample modules for mass spectrometer

    DOE Patents [OSTI]

    Thompson, C.V.; Wise, M.B.

    1993-12-21T23:59:59.000Z

    An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus. 5 figures.

  16. Soil sampling kit and a method of sampling therewith

    DOE Patents [OSTI]

    Thompson, Cyril V. (Knoxville, TN)

    1991-01-01T23:59:59.000Z

    A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allow an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds.

  17. Soil sampling kit and a method of sampling therewith

    DOE Patents [OSTI]

    Thompson, C.V.

    1991-02-05T23:59:59.000Z

    A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allows an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds. 11 figures.

  18. Sample holder with optical features

    DOE Patents [OSTI]

    Milas, Mirko; Zhu, Yimei; Rameau, Jonathan David

    2013-07-30T23:59:59.000Z

    A sample holder for holding a sample to be observed for research purposes, particularly in a transmission electron microscope (TEM), generally includes an external alignment part for directing a light beam in a predetermined beam direction, a sample holder body in optical communication with the external alignment part and a sample support member disposed at a distal end of the sample holder body opposite the external alignment part for holding a sample to be analyzed. The sample holder body defines an internal conduit for the light beam and the sample support member includes a light beam positioner for directing the light beam between the sample holder body and the sample held by the sample support member.

  19. Sample Environment Plans and Progress

    E-Print Network [OSTI]

    Pennycook, Steve

    Sample Environment Plans and Progress at the SNS & HFIR SNS HFIR User Group Meeting American Conference on Neutron Scattering Ottawa, Canada June 26 ­ 30, 2010 Lou Santodonato Sample Environment Group our sample environment capabilities Feedback SHUG meetings User surveys Sample Environment Steering

  20. Stack sampling apparatus

    SciTech Connect (OSTI)

    Lind, Randall F; Lloyd, Peter D; Love, Lonnie J; Noakes, Mark W; Pin, Francois G; Richardson, Bradley S; Rowe, John C

    2014-09-16T23:59:59.000Z

    An apparatus for obtaining samples from a structure includes a support member, at least one stabilizing member, and at least one moveable member. The stabilizing member has a first portion coupled to the support member and a second portion configured to engage with the structure to restrict relative movement between the support member and the structure. The stabilizing member is radially expandable from a first configuration where the second portion does not engage with a surface of the structure to a second configuration where the second portion engages with the surface of the structure.

  1. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado, Disposal

  2. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,

  3. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,and

  4. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOld

  5. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOld

  6. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOldOld

  7. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction,

  8. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction,Groundwater and

  9. Sample Changes and Issues

    Annual Energy Outlook 2013 [U.S. Energy Information Administration (EIA)]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) " ,"ClickPipelines AboutDecemberSteamYear Jan FebThousand Cubic Feet)Year JanC.9.3. Receipts8.160Sample

  10. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling at

  11. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling at4

  12. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling

  13. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C. 20545 OCT 28Sacandaga SiteSep NovWater Sampling

  14. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C. 20545 OCT 28Sacandaga SiteSep NovWaterSampling

  15. Fluid sampling tool

    DOE Patents [OSTI]

    Garcia, A.R.; Johnston, R.G.; Martinez, R.K.

    1999-05-25T23:59:59.000Z

    A fluid sampling tool is described for sampling fluid from a container. The tool has a fluid collecting portion which is drilled into the container wall, thereby affixing it to the wall. The tool may have a fluid extracting section which withdraws fluid collected by the fluid collecting section. The fluid collecting section has a fluted shank with an end configured to drill a hole into a container wall. The shank has a threaded portion for tapping the borehole. The shank is threadably engaged to a cylindrical housing having an inner axial passageway sealed at one end by a septum. A flexible member having a cylindrical portion and a bulbous portion is provided. The housing can be slid into an inner axial passageway in the cylindrical portion and sealed to the flexible member. The bulbous portion has an outer lip defining an opening. The housing is clamped into the chuck of a drill, the lip of the bulbous section is pressed against a container wall until the shank touches the wall, and the user operates the drill. Wall shavings (kerf) are confined in a chamber formed in the bulbous section as it folds when the shank advances inside the container. After sufficient advancement of the shank, an o-ring makes a seal with the container wall. 6 figs.

  16. Fluid sampling tool

    DOE Patents [OSTI]

    Johnston, Roger G. (Los Alamos, NM); Garcia, Anthony R. E. (Espanola, NM); Martinez, Ronald K. (Santa Cruz, NM)

    2001-09-25T23:59:59.000Z

    The invention includes a rotatable tool for collecting fluid through the wall of a container. The tool includes a fluid collection section with a cylindrical shank having an end portion for drilling a hole in the container wall when the tool is rotated, and a threaded portion for tapping the hole in the container wall. A passageway in the shank in communication with at least one radial inlet hole in the drilling end and an opening at the end of the shank is adapted to receive fluid from the container. The tool also includes a cylindrical chamber affixed to the end of the shank opposite to the drilling portion thereof for receiving and storing fluid passing through the passageway. The tool also includes a flexible, deformable gasket that provides a fluid-tight chamber to confine kerf generated during the drilling and tapping of the hole. The invention also includes a fluid extractor section for extracting fluid samples from the fluid collecting section.

  17. Specified assurance level sampling procedure

    SciTech Connect (OSTI)

    Willner, O.

    1980-11-01T23:59:59.000Z

    In the nuclear industry design specifications for certain quality characteristics require that the final product be inspected by a sampling plan which can demonstrate product conformance to stated assurance levels. The Specified Assurance Level (SAL) Sampling Procedure has been developed to permit the direct selection of attribute sampling plans which can meet commonly used assurance levels. The SAL procedure contains sampling plans which yield the minimum sample size at stated assurance levels. The SAL procedure also provides sampling plans with acceptance numbers ranging from 0 to 10, thus, making available to the user a wide choice of plans all designed to comply with a stated assurance level.

  18. Sampling for Bacteria in Wells

    E-Print Network [OSTI]

    Lesikar, Bruce J.

    2001-11-15T23:59:59.000Z

    This publication will instruct you on the proper procedures for collecting a sample from a water well for bacteriological analysis....

  19. Sample Residential Program Term Sheet

    Broader source: Energy.gov (indexed) [DOE]

    Goal DRAFT U.S. DOE Sample Residential Program Term Sheet - DRAFT Introduction is seeking to develop an energy...

  20. Post-Award Deliverables Sample (Second Part of Sample Deliverables...

    Broader source: Energy.gov (indexed) [DOE]

    Task Orders (IDIQ Attachment. J-4) Sample Statement of Work - Standard Service Offerings for Contractor-Identified Project ESPC TASK ORDER REQUEST FOR PROPOSAL (TO RFP) TEMPLATE...

  1. Acceptance sampling using judgmental and randomly selected samples

    SciTech Connect (OSTI)

    Sego, Landon H.; Shulman, Stanley A.; Anderson, Kevin K.; Wilson, John E.; Pulsipher, Brent A.; Sieber, W. Karl

    2010-09-01T23:59:59.000Z

    We present a Bayesian model for acceptance sampling where the population consists of two groups, each with different levels of risk of containing unacceptable items. Expert opinion, or judgment, may be required to distinguish between the high and low-risk groups. Hence, high-risk items are likely to be identifed (and sampled) using expert judgment, while the remaining low-risk items are sampled randomly. We focus on the situation where all observed samples must be acceptable. Consequently, the objective of the statistical inference is to quantify the probability that a large percentage of the unsampled items in the population are also acceptable. We demonstrate that traditional (frequentist) acceptance sampling and simpler Bayesian formulations of the problem are essentially special cases of the proposed model. We explore the properties of the model in detail, and discuss the conditions necessary to ensure that required samples sizes are non-decreasing function of the population size. The method is applicable to a variety of acceptance sampling problems, and, in particular, to environmental sampling where the objective is to demonstrate the safety of reoccupying a remediated facility that has been contaminated with a lethal agent.

  2. Adaptive Sampling for Environmental Robotics

    E-Print Network [OSTI]

    Mohammad Rahimi; Richard Pon; Deborah Estrin; William J. Kaiser; Mani Srivastava; Gaurav S. Sukhatme

    2003-01-01T23:59:59.000Z

    186, 2003. S. Thrun, “Robotics Mapping: A survey”, Exploringtechnique to environmental robotics applications includingSampling for Environmental Robotics Mohammad Rahimi †,‡‡ ,

  3. Sample Residential Program Term Sheet

    Broader source: Energy.gov [DOE]

    A sample for defining and elaborating on the specifics of a clean energy loan program. Author: U.S. Department of Energy

  4. Homeowner Soil Sample Information Form

    E-Print Network [OSTI]

    Provin, Tony

    2007-04-11T23:59:59.000Z

    Homeowners should submit this form with their soil samples when requesting a soil test from the Texas A&M Soil Testing Laboratory....

  5. Defining And Characterizing Sample Representativeness For DWPF Melter Feed Samples

    SciTech Connect (OSTI)

    Shine, E. P.; Poirier, M. R.

    2013-10-29T23:59:59.000Z

    Representative sampling is important throughout the Defense Waste Processing Facility (DWPF) process, and the demonstrated success of the DWPF process to achieve glass product quality over the past two decades is a direct result of the quality of information obtained from the process. The objective of this report was to present sampling methods that the Savannah River Site (SRS) used to qualify waste being dispositioned at the DWPF. The goal was to emphasize the methodology, not a list of outcomes from those studies. This methodology includes proven methods for taking representative samples, the use of controlled analytical methods, and data interpretation and reporting that considers the uncertainty of all error sources. Numerous sampling studies were conducted during the development of the DWPF process and still continue to be performed in order to evaluate options for process improvement. Study designs were based on use of statistical tools applicable to the determination of uncertainties associated with the data needs. Successful designs are apt to be repeated, so this report chose only to include prototypic case studies that typify the characteristics of frequently used designs. Case studies have been presented for studying in-tank homogeneity, evaluating the suitability of sampler systems, determining factors that affect mixing and sampling, comparing the final waste glass product chemical composition and durability to that of the glass pour stream sample and other samples from process vessels, and assessing the uniformity of the chemical composition in the waste glass product. Many of these studies efficiently addressed more than one of these areas of concern associated with demonstrating sample representativeness and provide examples of statistical tools in use for DWPF. The time when many of these designs were implemented was in an age when the sampling ideas of Pierre Gy were not as widespread as they are today. Nonetheless, the engineers and statisticians used carefully thought out designs that systematically and economically provided plans for data collection from the DWPF process. Key shared features of the sampling designs used at DWPF and the Gy sampling methodology were the specification of a standard for sample representativeness, an investigation that produced data from the process to study the sampling function, and a decision framework used to assess whether the specification was met based on the data. Without going into detail with regard to the seven errors identified by Pierre Gy, as excellent summaries are readily available such as Pitard [1989] and Smith [2001], SRS engineers understood, for example, that samplers can be biased (Gy?s extraction error), and developed plans to mitigate those biases. Experiments that compared installed samplers with more representative samples obtained directly from the tank may not have resulted in systematically partitioning sampling errors into the now well-known error categories of Gy, but did provide overall information on the suitability of sampling systems. Most of the designs in this report are related to the DWPF vessels, not the large SRS Tank Farm tanks. Samples from the DWPF Slurry Mix Evaporator (SME), which contains the feed to the DWPF melter, are characterized using standardized analytical methods with known uncertainty. The analytical error is combined with the established error from sampling and processing in DWPF to determine the melter feed composition. This composition is used with the known uncertainty of the models in the Product Composition Control System (PCCS) to ensure that the wasteform that is produced is comfortably within the acceptable processing and product performance region. Having the advantage of many years of processing that meets the waste glass product acceptance criteria, the DWPF process has provided a considerable amount of data about itself in addition to the data from many special studies. Demonstrating representative sampling directly from the large Tank Farm tanks is a difficult, if not unsolvable enterprise due to li

  6. Database Sampling with Functional Dependencies

    E-Print Network [OSTI]

    Riera, Jesús Bisbal

    Database Sampling with Functional Dependencies Jes´us Bisbal, Jane Grimson Department of Computer there is a need to prototype the database which the applications will use when in operation. A prototype database can be built by sampling data from an existing database. Including relevant semantic information when

  7. Sample push-out fixture

    DOE Patents [OSTI]

    Biernat, John L. (Scotia, NY)

    2002-11-05T23:59:59.000Z

    This invention generally relates to the remote removal of pelletized samples from cylindrical containment capsules. V-blocks are used to receive the samples and provide guidance to push out rods. Stainless steel liners fit into the v-channels on the v-blocks which permits them to be remotely removed and replaced or cleaned to prevent cross contamination between capsules and samples. A capsule holder securely holds the capsule while allowing manual up/down and in/out movement to align each sample hole with the v-blocks. Both end sections contain identical v-blocks; one that guides the drive out screw and rods or manual push out rods and the other to receive the samples as they are driven out of the capsule.

  8. Sample rotating turntable kit for infrared spectrometers

    DOE Patents [OSTI]

    Eckels, Joel Del (Livermore, CA); Klunder, Gregory L. (Oakland, CA)

    2008-03-04T23:59:59.000Z

    An infrared spectrometer sample rotating turntable kit has a rotatable sample cup containing the sample. The infrared spectrometer has an infrared spectrometer probe for analyzing the sample and the rotatable sample cup is adapted to receive the infrared spectrometer probe. A reflectance standard is located in the rotatable sample cup. A sleeve is positioned proximate the sample cup and adapted to receive the probe. A rotator rotates the rotatable sample cup. A battery is connected to the rotator.

  9. Sample Business Plan Framework 3

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  10. Sample Business Plan Framework 2

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  11. Sample Business Plan Framework 4

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  12. Sample Business Plan Framework 1

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  13. Sampling based on local bandwidth

    E-Print Network [OSTI]

    Wei, Dennis

    2007-01-01T23:59:59.000Z

    The sampling of continuous-time signals based on local bandwidth is considered in this thesis. In an intuitive sense, local bandwidth refers to the rate at which a signal varies locally. One would expect that signals should ...

  14. Depth-discrete sampling port

    DOE Patents [OSTI]

    Pemberton, Bradley E. (Aiken, SC); May, Christopher P. (Columbia, MD); Rossabi, Joseph (Aiken, SC); Riha, Brian D. (Augusta, GA); Nichols, Ralph L. (North Augusta, SC)

    1999-01-01T23:59:59.000Z

    A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

  15. Depth-discrete sampling port

    DOE Patents [OSTI]

    Pemberton, Bradley E. (Aiken, SC); May, Christopher P. (Columbia, MD); Rossabi, Joseph (Aiken, SC); Riha, Brian D. (Augusta, GA); Nichols, Ralph L. (North Augusta, SC)

    1998-07-07T23:59:59.000Z

    A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

  16. Reference Potential source Data type Sampling site Type of samples Number of samples Method of source

    E-Print Network [OSTI]

    Meskhidze, Nicholas

    samples for Saharan dust from Libya back trajectory analysis Kandler et al. 2009 PSA NAF-2 Illite NAF-4 Illite/kaolinite ratio Chlorite/kaolinite ratio Carbonate content Libya (here: central

  17. Inertial impaction air sampling device

    DOE Patents [OSTI]

    Dewhurst, K.H.

    1987-12-10T23:59:59.000Z

    An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

  18. Spent nuclear fuel sampling strategy

    SciTech Connect (OSTI)

    Bergmann, D.W.

    1995-02-08T23:59:59.000Z

    This report proposes a strategy for sampling the spent nuclear fuel (SNF) stored in the 105-K Basins (105-K East and 105-K West). This strategy will support decisions concerning the path forward SNF disposition efforts in the following areas: (1) SNF isolation activities such as repackaging/overpacking to a newly constructed staging facility; (2) conditioning processes for fuel stabilization; and (3) interim storage options. This strategy was developed without following the Data Quality Objective (DQO) methodology. It is, however, intended to augment the SNF project DQOS. The SNF sampling is derived by evaluating the current storage condition of the SNF and the factors that effected SNF corrosion/degradation.

  19. Inertial impaction air sampling device

    DOE Patents [OSTI]

    Dewhurst, Katharine H. (13150 Wenonah SE. Apt. 727, Albuquerque, NM 87123)

    1990-01-01T23:59:59.000Z

    An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry.

  20. Inertial impaction air sampling device

    DOE Patents [OSTI]

    Dewhurst, K.H.

    1990-05-22T23:59:59.000Z

    An inertial impactor is designed which is to be used in an air sampling device for collection of respirable size particles in ambient air. The device may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

  1. Sample Licensing Agreements | Partnerships | ORNL

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 -the Mid-Infrared0 ResourceAwardsSafeguards and SecuritySafety Salt LakeSampleSample

  2. Offline solid phase microextraction sampling system

    DOE Patents [OSTI]

    Harvey, Chris A. (French Camp, CA)

    2008-12-16T23:59:59.000Z

    An offline solid phase microextraction (SPME) sampling apparatus for enabling SPME samples to be taken a number of times from a previously collected fluid sample (e.g. sample atmosphere) stored in a fused silica lined bottle which keeps volatile organics in the fluid sample stable for weeks at a time. The offline SPME sampling apparatus has a hollow body surrounding a sampling chamber, with multiple ports through which a portion of a previously collected fluid sample may be (a) released into the sampling chamber, (b) SPME sampled to collect analytes for subsequent GC analysis, and (c) flushed/purged using a fluidically connected vacuum source and purging fluid source to prepare the sampling chamber for additional SPME samplings of the same original fluid sample, such as may have been collected in situ from a headspace.

  3. Waste tank characterization sampling limits

    SciTech Connect (OSTI)

    Tusler, L.A.

    1994-09-02T23:59:59.000Z

    This document is a result of the Plant Implementation Team Investigation into delayed reporting of the exotherm in Tank 241-T-111 waste samples. The corrective actions identified are to have immediate notification of appropriate Tank Farm Operations Shift Management if analyses with potential safety impact exceed established levels. A procedure, WHC-IP-0842 Section 12.18, ``TWRS Approved Sampling and Data Analysis by Designated Laboratories`` (WHC 1994), has been established to require all tank waste sampling (including core, auger and supernate) and tank vapor samples be performed using this document. This document establishes levels for specified analysis that require notification of the appropriate shift manager. The following categories provide numerical values for analysis that may indicate that a tank is either outside the operating specification or should be evaluated for inclusion on a Watch List. The information given is intended to translate an operating limit such as heat load, expressed in Btu/hour, to an analysis related limit, in this case cesium-137 and strontium-90 concentrations. By using the values provided as safety flags, the analytical laboratory personnel can notify a shift manager that a tank is in potential violation of an operating limit or that a tank should be considered for inclusion on a Watch List. The shift manager can then take appropriate interim measures until a final determination is made by engineering personnel.

  4. Sample Internship Posting Department Name

    E-Print Network [OSTI]

    Bordenstein, Seth

    Sample Internship Posting Department Name: Internship Title: Location: Description of Organization are examples from other internship postings Interns will: · Analyze potential investments · Shadow team members(s) in ________ is desirable For a list of majors see http://admissions.vanderbilt.edu/major Internship Period: The following

  5. Environmental surveillance master sampling schedule

    SciTech Connect (OSTI)

    Bisping, L.E.

    1994-02-01T23:59:59.000Z

    This document contains the planned 1994 schedules for routine collection of samples for the Surface Environmental Surveillance Project (SESP), Drinking Water Project, and Ground-Water Surveillance Project. Samples are routinely collected for the SESP and analyzed to determine the quality of air, surface water, soil, sediment, wildlife, vegetation, foodstuffs, and farm products at Hanford Site and surrounding communities. The responsibility for monitoring the onsite drinking water falls outside the scope of the SESP. The Hanford Environmental Health Foundation is responsible for monitoring the nonradiological parameters as defined in the National Drinking Water Standards while PNL conducts the radiological monitoring of the onsite drinking water. PNL conducts the drinking water monitoring project concurrent with the SESP to promote efficiency and consistency, utilize the expertise developed over the years, and reduce costs associated with management, procedure development, data management, quality control and reporting. The ground-water sampling schedule identifies ground-water sampling events used by PNL for environmental surveillance of the Hanford Site.

  6. Environmental Analysis & Policy: Sample Pathway

    E-Print Network [OSTI]

    Goldberg, Bennett

    Environmental Analysis & Policy: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Sustainable Development OR Spring GE 425 U.S. Environmental Policy (Senior) GE 309 Intermediate Env Analysis (Fall) EAP Elective Summer Environmental Internship Senior Year GE 420 Env Policy Analysis 4 th Semester

  7. AUTOMATING GROUNDWATER SAMPLING AT HANFORD

    SciTech Connect (OSTI)

    CONNELL CW; HILDEBRAND RD; CONLEY SF; CUNNINGHAM DE

    2009-01-16T23:59:59.000Z

    Until this past October, Fluor Hanford managed Hanford's integrated groundwater program for the U.S. Department of Energy (DOE). With the new contract awards at the Site, however, the CH2M HILL Plateau Remediation Company (CHPRC) has assumed responsibility for the groundwater-monitoring programs at the 586-square-mile reservation in southeastern Washington State. These programs are regulated by the Resource Conservation and Recovery Act (RCRA) and the Comprehensive Environmental Response Compensation and Liability Act (CERCLA). The purpose of monitoring is to track existing groundwater contamination from past practices, as well as other potential contamination that might originate from RCRA treatment, storage, and disposal (TSD) facilities. An integral part of the groundwater-monitoring program involves taking samples of the groundwater and measuring the water levels in wells scattered across the site. More than 1,200 wells are sampled each year. Historically, field personnel or 'samplers' have been issued pre-printed forms that have information about the well(s) for a particular sampling evolution. This information is taken from the Hanford Well Information System (HWIS) and the Hanford Environmental Information System (HEIS)--official electronic databases. The samplers used these hardcopy forms to document the groundwater samples and well water-levels. After recording the entries in the field, the samplers turned the forms in at the end of the day and the collected information was posted onto a spreadsheet that was then printed and included in a log book. The log book was then used to make manual entries of the new information into the software application(s) for the HEIS and HWIS databases. This is a pilot project for automating this tedious process by providing an electronic tool for automating water-level measurements and groundwater field-sampling activities. The automation will eliminate the manual forms and associated data entry, improve the accuracy of the information recorded, and enhance the efficiency and sampling capacity of field personnel. The goal of the effort is to eliminate 100 percent of the manual input to the database(s) and replace the management of paperwork by the field and clerical personnel with an almost entirely electronic process. These activities will include the following: scheduling the activities of the field teams, electronically recording water-level measurements, electronically logging and filing Groundwater Sampling Reports (GSR), and transferring field forms into the site-wide Integrated Document Management System (IDMS).

  8. HIPPO_NOAA_Flask_Data_Users_Guide_20121130 1 Revision Date: November 30, 2012

    E-Print Network [OSTI]

    atmospheric concentrations of CO2, CH4, CO, H2, N2O, halocarbon, hydrocarbon, and sulfur-containing trace, K. H. Rosenlof, E. A. Ray, B. Hall, M. A. Zondlo, M. Diao, R. Keeling, J. Bent, E. L. Atlas, R. Lueb

  9. ARM - PI Product - ARM-LBNL-NOAA Flask Sampler for Carbon Cycle Gases

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc Documentation RUC : XDCResearchWarmingMethane BackgroundFacilityOtherCF during

  10. Hanford Site Environmental Surveillance Master Sampling Schedule

    SciTech Connect (OSTI)

    Bisping, Lynn E.

    2000-01-27T23:59:59.000Z

    This document contains the CY2000 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes sampling locations, sample types, and analyses to be performed.

  11. Summary IsotoperatioanalysesofatmosphericCO2 atnatu-ral abundance have significant potential for contributing to our

    E-Print Network [OSTI]

    Ehleringer, Jim

    --300 µl is accomplished by linking a commercially available, trace gas condenser and gas chromatograph are stored in either gas- tight syringes or 100-ml flasks. The small sample volume required makes it possible measurements. When linked with an infrared gas analyzer, pump and flask sampling system, it is feasible

  12. Tank farm backlog soil sample analysis plan

    SciTech Connect (OSTI)

    Ahlers, J.D., Westinghouse Hanford

    1996-07-17T23:59:59.000Z

    This document describes the measures to collect samples, perform testing on samples, and make decisions to obtain a Contained- in Determination for tank farms backlog soil.

  13. Adaptive Sampling in Hierarchical Simulation

    SciTech Connect (OSTI)

    Knap, J; Barton, N R; Hornung, R D; Arsenlis, A; Becker, R; Jefferson, D R

    2007-07-09T23:59:59.000Z

    We propose an adaptive sampling methodology for hierarchical multi-scale simulation. The method utilizes a moving kriging interpolation to significantly reduce the number of evaluations of finer-scale response functions to provide essential constitutive information to a coarser-scale simulation model. The underlying interpolation scheme is unstructured and adaptive to handle the transient nature of a simulation. To handle the dynamic construction and searching of a potentially large set of finer-scale response data, we employ a dynamic metric tree database. We study the performance of our adaptive sampling methodology for a two-level multi-scale model involving a coarse-scale finite element simulation and a finer-scale crystal plasticity based constitutive law.

  14. Environmental surveillance master sampling schedule

    SciTech Connect (OSTI)

    Bisping, L E

    1992-01-01T23:59:59.000Z

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the US Department of Energy (DOE). This document contains the planned schedule for routine sample collection for the Surface Environmental Surveillance Project (SESP) and Ground-Water Monitoring Project. Samples for radiological analyses include Air-Particulate Filter, gases and vapor; Water/Columbia River, Onsite Pond, Spring, Irrigation, and Drinking; Foodstuffs/Animal Products including Whole Milk, Poultry and Eggs, and Beef; Foodstuffs/Produce including Leafy Vegetables, Vegetables, and Fruit; Foodstuffs/Farm Products including Wine, Wheat and Alfalfa; Wildlife; Soil; Vegetation; and Sediment. Direct Radiation Measurements include Terrestrial Locations, Columbia River Shoreline Locations, and Onsite Roadway, Railway and Aerial, Radiation Surveys.

  15. Rock Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data CenterFranconia, Virginia:FAQ < RAPID Jump to: navigation, searchVirginia BlueRiverwoods,Rock Sampling Details Activities (18) Areas

  16. INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING DISTRIBUTION, AND POPULATION

    E-Print Network [OSTI]

    Yu, Alex

    INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING Keywords: Parametric test, sample, population, sampling distributions Parametric tests are frequently parametric tests, nor hold beliefs that are consistent with that framework. The parametric test framework

  17. Sample introduction apparatus for a flow cytometer

    DOE Patents [OSTI]

    Van den Engh, Ger (Seattle, WA)

    1998-01-01T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

  18. Sample introduction system for a flow cytometer

    DOE Patents [OSTI]

    Engh, G. van den

    1997-02-11T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

  19. Sample introduction system for a flow cytometer

    DOE Patents [OSTI]

    Van den Engh, Ger (Seattle, WA)

    1997-01-01T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

  20. Sample introduction apparatus for a flow cytometer

    DOE Patents [OSTI]

    Van den Engh, G.

    1998-03-10T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

  1. Synchronized sampling improves fault location

    SciTech Connect (OSTI)

    Kezunovic, M. [Texas A and M Univ., College Station, TX (United States)] [Texas A and M Univ., College Station, TX (United States); Perunicic, B. [Lamar Univ., Beaumont, TX (United States)] [Lamar Univ., Beaumont, TX (United States)

    1995-04-01T23:59:59.000Z

    Transmission line faults must be located accurately to allow maintenance crews to arrive at the scene and repair the faulted section as soon as possible. Rugged terrain and geographical layout cause some sections of power transmission lines to be difficult to reach. In the past, a variety of fault location algorithms were introduced as either an add-on feature in protective relays or stand-alone implementation in fault locators. In both cases, the measurements of current and voltages were taken at one terminal of a transmission line only. Under such conditions, it may become difficult to determine the fault location accurately, since data from other transmission line ends are required for more precise computations. In the absence of data from the other end, existing algorithms have accuracy problems under several circumstances, such as varying switching and loading conditions, fault infeed from the other end, and random value of fault resistance. Most of the one-end algorithms were based on estimation of voltage and current phasors. The need to estimate phasors introduces additional difficulty in high-speed tripping situations where the algorithms may not be fast enough in determining fault location accurately before the current signals disappear due to the relay operation and breaker opening. This article introduces a unique concept of high-speed fault location that can be implemented either as a simple add-on to the digital fault recorders (DFRs) or as a stand-alone new relaying function. This advanced concept is based on the use of voltage and current samples that are synchronously taken at both ends of a transmission line. This sampling technique can be made readily available in some new DFR designs incorporating receivers for accurate sampling clock synchronization using the satellite Global Positioning System (GPS).

  2. Licensing Guide and Sample License

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample6, 2011 LawrenceE CAnalytical InstrumentationEnergy

  3. Sample Environments at Sector 30

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 -the Mid-Infrared0 ResourceAwardsSafeguards and SecuritySafety Salt LakeSample

  4. TRU waste-sampling program

    SciTech Connect (OSTI)

    Warren, J.L.; Zerwekh, A.

    1985-08-01T23:59:59.000Z

    As part of a TRU waste-sampling program, Los Alamos National Laboratory retrieved and examined 44 drums of /sup 238/Pu- and /sup 239/Pu-contaminated waste. The drums ranged in age from 8 months to 9 years. The majority of drums were tested for pressure, and gas samples withdrawn from the drums were analyzed by a mass spectrometer. Real-time radiography and visual examination were used to determine both void volumes and waste content. Drum walls were measured for deterioration, and selected drum contents were reassayed for comparison with original assays and WIPP criteria. Each drum tested at atmospheric pressure. Mass spectrometry revealed no problem with /sup 239/Pu-contaminated waste, but three 8-month-old drums of /sup 238/Pu-contaminated waste contained a potentially hazardous gas mixture. Void volumes fell within the 81 to 97% range. Measurements of drum walls showed no significant corrosion or deterioration. All reassayed contents were within WIPP waste acceptance criteria. Five of the drums opened and examined (15%) could not be certified as packaged. Three contained free liquids, one had corrosive materials, and one had too much unstabilized particulate. Eleven drums had the wrong (or not the most appropriate) waste code. In many cases, disposal volumes had been inefficiently used. 2 refs., 23 figs., 7 tabs.

  5. Method and apparatus for data sampling

    DOE Patents [OSTI]

    Odell, Daniel M. C. (Aiken, SC)

    1994-01-01T23:59:59.000Z

    A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium.

  6. Method and apparatus for data sampling

    DOE Patents [OSTI]

    Odell, D.M.C.

    1994-04-19T23:59:59.000Z

    A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples is described. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium. 6 figures.

  7. Fluid sampling system for a nuclear reactor

    DOE Patents [OSTI]

    Lau, L.K.; Alper, N.I.

    1994-11-22T23:59:59.000Z

    A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump. 1 fig.

  8. Fluid sampling system for a nuclear reactor

    DOE Patents [OSTI]

    Lau, Louis K. (Monroeville, PA); Alper, Naum I. (Monroeville, PA)

    1994-01-01T23:59:59.000Z

    A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump.

  9. ALARA ASSESSMENT OF SETTLER SLUDGE SAMPLING METHODS

    SciTech Connect (OSTI)

    NELSEN LA

    2009-01-30T23:59:59.000Z

    The purpose of this assessment is to compare underwater and above water settler sludge sampling methods to determine if the added cost for underwater sampling for the sole purpose of worker dose reductions is justified. Initial planning for sludge sampling included container, settler and knock-out-pot (KOP) sampling. Due to the significantly higher dose consequence of KOP sludge, a decision was made to sample KOP underwater to achieve worker dose reductions. Additionally, initial plans were to utilize the underwater sampling apparatus for settler sludge. Since there are no longer plans to sample KOP sludge, the decision for underwater sampling for settler sludge needs to be revisited. The present sampling plan calls for spending an estimated $2,500,000 to design and construct a new underwater sampling system (per A21 C-PL-001 RevOE). This evaluation will compare and contrast the present method of above water sampling to the underwater method that is planned by the Sludge Treatment Project (STP) and determine if settler samples can be taken using the existing sampling cart (with potentially minor modifications) while maintaining doses to workers As Low As Reasonably Achievable (ALARA) and eliminate the need for costly redesigns, testing and personnel retraining.

  10. Sample Residential Program Term Sheet | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    Sample Residential Program Term Sheet Sample Residential Program Term Sheet A sample for defining and elaborating on the specifics of a clean energy loan program. Sample...

  11. An introduction to boson-sampling

    E-Print Network [OSTI]

    Bryan T. Gard; Keith R. Motes; Jonathan P. Olson; Peter P. Rohde; Jonathan P. Dowling

    2014-06-26T23:59:59.000Z

    Boson-sampling is a simplified model for quantum computing that may hold the key to implementing the first ever post-classical quantum computer. Boson-sampling is a non-universal quantum computer that is significantly more straightforward to build than any universal quantum computer proposed so far. We begin this chapter by motivating boson-sampling and discussing the history of linear optics quantum computing. We then summarize the boson-sampling formalism, discuss what a sampling problem is, explain why boson-sampling is easier than linear optics quantum computing, and discuss the Extended Church-Turing thesis. Next, sampling with other classes of quantum optical states is analyzed. Finally, we discuss the feasibility of building a boson-sampling device using existing technology.

  12. Principles for Sampling Airborne Radioactivity from Stacks

    SciTech Connect (OSTI)

    Glissmeyer, John A.

    2010-10-18T23:59:59.000Z

    This book chapter describes the special processes involved in sampling the airborne effluents from nuclear faciities. The title of the book is Radioactive Air Sampling Methods. The abstract for this chapter was cleared as PNNL-SA-45941.

  13. General Sample Submission Form University of Utah

    E-Print Network [OSTI]

    Hill, Chris

    in all applicable information as completely as possible Sample Information Sample ID / Description/MS/MS (FTMS) ______ Maldi/FTMS ______ Maldi/ToF ______ ESI/MS ______ ESI/FTMS _____ Location and Staff MS file

  14. Sample holder for X-ray diffractometry

    DOE Patents [OSTI]

    Hesch, Victor L. (Los Alamos, NM)

    1992-01-01T23:59:59.000Z

    A sample holder for use with X-ray diffractometers with the capability to rotate the sample, as well as to adjust the position of the sample in the x, y, and z directions. Adjustment in the x direction is accomplished through loosening set screws, moving a platform, and retightening the set screws. Motion translators are used for adjustment in the y and z directions. An electric motor rotates the sample, and receives power from the diffractometer.

  15. E-Print Network 3.0 - air pollution sampling Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    sampling Search Powered by Explorit Topic List Advanced Search Sample search results for: air pollution sampling Page: << < 1 2 3 4 5 > >> 1 griculture is in the spotlight as a...

  16. Sample storage/disposal study

    SciTech Connect (OSTI)

    Valenzuela, B.D.

    1994-09-29T23:59:59.000Z

    Radioactive waste from defense operations has accumulated at the Hanford Site`s underground waste tanks since the late 1940`s. Each tank must be analyzed to determine whether it presents any harm to the workers at the Hanford Site, the public or the environment. Analyses of the waste aids in the decision making process in preparation of future tank waste stabilization procedures. Characterization of the 177 waste tanks on the Hanford Site will produce a large amount of archived material. This also brings up concerns as to how the excess waste tank sample material from 325 and 222-S Analytical Laboratories will be handled. Methods to archive and/or dispose of the waste have been implemented into the 222-S and 325 Laboratory procedures. As the amount of waste characterized from laboratory analysis grows, an examination of whether the waste disposal system will be able to compensate for this increase in the amount of waste needs to be examined. Therefore, the need to find the safest, most economically sound method of waste storage/disposal is important.

  17. E-Print Network 3.0 - air samples collected Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Collection NASA's Stardust sample return capsule successfully landed at the Summary: Aerogel: Stardust Collection Material 12;NASA's Stardust sample return capsule...

  18. E-Print Network 3.0 - adaptive sampling strategy Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ray tracing, Whitted Whi80 proposed an adaptive sampling strategy which first... (Eds.) Adaptive Sampling for Geometry-aware Reconstruction Filters Pablo Bauszat1 and Martin...

  19. E-Print Network 3.0 - assurance sampling method Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    for NRDA followed standard operating procedure (SOP), water sampling plans, Summary: procedures, and NOAA's Analytical Quality Assurance Project Plan (QAPP). Samples were sent to...

  20. Rotary Mode Core Sample System availability improvement

    SciTech Connect (OSTI)

    Jenkins, W.W.; Bennett, K.L.; Potter, J.D. [Westinghouse Hanford Co., Richland, WA (United States); Cross, B.T.; Burkes, J.M.; Rogers, A.C. [Southwest Research Institute (United States)

    1995-02-28T23:59:59.000Z

    The Rotary Mode Core Sample System (RMCSS) is used to obtain stratified samples of the waste deposits in single-shell and double-shell waste tanks at the Hanford Site. The samples are used to characterize the waste in support of ongoing and future waste remediation efforts. Four sampling trucks have been developed to obtain these samples. Truck I was the first in operation and is currently being used to obtain samples where the push mode is appropriate (i.e., no rotation of drill). Truck 2 is similar to truck 1, except for added safety features, and is in operation to obtain samples using either a push mode or rotary drill mode. Trucks 3 and 4 are now being fabricated to be essentially identical to truck 2.

  1. Sample sizes for confidence limits for reliability.

    SciTech Connect (OSTI)

    Darby, John L.

    2010-02-01T23:59:59.000Z

    We recently performed an evaluation of the implications of a reduced stockpile of nuclear weapons for surveillance to support estimates of reliability. We found that one technique developed at Sandia National Laboratories (SNL) under-estimates the required sample size for systems-level testing. For a large population the discrepancy is not important, but for a small population it is important. We found that another technique used by SNL provides the correct required sample size. For systems-level testing of nuclear weapons, samples are selected without replacement, and the hypergeometric probability distribution applies. Both of the SNL techniques focus on samples without defects from sampling without replacement. We generalized the second SNL technique to cases with defects in the sample. We created a computer program in Mathematica to automate the calculation of confidence for reliability. We also evaluated sampling with replacement where the binomial probability distribution applies.

  2. Proper Oil Sampling Intervals and Sample Collection Techniques Gasoline/Diesel/Natural Gas Engines

    E-Print Network [OSTI]

    Proper Oil Sampling Intervals and Sample Collection Techniques Gasoline/Diesel/Natural Gas Engines: · Oil samples can be collected during oil changes. Follow manufacturers recommendations on frequency (hours, mileage, etc) of oil changes. · Capture a sample from the draining oil while the oil is still hot

  3. Combustion characteristics of 24 lignite samples

    SciTech Connect (OSTI)

    Sensogut, C.; Ozsen, H.; Demirbas, A. [Selcuk University, Konya (Turkey)

    2008-07-01T23:59:59.000Z

    In this study, the combustion characteristics such as thermogravimetric analysis (TGA) and differential thermogravimetric analysis (DTGA), burning profile, ignition temperature, and peak temperature were analyzed for 24 lignite samples from different areas of Turkey. The samples were heated up to 900{sup o}C at a constant rate of 10{sup o} C/min in a 5 mL/min flow of dry air. The burning profiles of the samples studied, combined with proximate, sulfur analysis and calorimetry results, contribute to a clearer identification of lignite samples' structure and a better understanding of the coalification process. The lignite samples have been tested with particle size of 0-0.05 mm. Ignition temperatures of the samples have been determined from their burning profiles.

  4. 100 Area Columbia River sediment sampling

    SciTech Connect (OSTI)

    Weiss, S.G. [Westinghouse Hanford Co., Richland, WA (United States)

    1993-09-08T23:59:59.000Z

    Forty-four sediment samples were collected from 28 locations in the Hanford Reach of the Columbia River to assess the presence of metals and man-made radionuclides in the near shore and shoreline settings of the Hanford Site. Three locations were sampled upriver of the Hanford Site plutonium production reactors. Twenty-two locations were sampled near the reactors. Three locations were sampled downstream of the reactors near the Hanford Townsite. Sediment was collected from depths of 0 to 6 in. and between 12 to 24 in. below the surface. Samples containing concentrations of metals exceeding the 95 % upper threshold limit values (DOE-RL 1993b) are considered contaminated. Contamination by arsenic, chromium, copper, lead, and zinc was found. Man-made radionuclides occur in all samples except four collected opposite the Hanford Townsite. Man-made radionuclide concentrations were generally less than 1 pCi/g.

  5. APPROPRIATE ZOOPLANKTON SAMPLING METHODOLOGY FOR OTEC SITES

    E-Print Network [OSTI]

    Commins, M.L.

    2014-01-01T23:59:59.000Z

    Thermal Energy Conversion (OTEC) sites. Participants J.Zooplankton Sampling for OTEC Sites t~thodology Edited bywho gave an overview of the OTEC program, and the policies

  6. PolyChord: nested sampling for cosmology

    E-Print Network [OSTI]

    Handley, W J; Lasenby, A N

    2015-01-01T23:59:59.000Z

    PolyChord is a novel nested sampling algorithm tailored for high dimensional parameter spaces. In addition, it can fully exploit a hierarchy of parameter speeds such as is found in CosmoMC and CAMB. It utilises slice sampling at each iteration to sample within the hard likelihood constraint of nested sampling. It can identify and evolve separate modes of a posterior semi-independently and is parallelised using openMPI. PolyChord is available for download at: http://ccpforge.cse.rl.ac.uk/gf/project/polychord/

  7. Procedures for sampling radium-contaminated soils

    SciTech Connect (OSTI)

    Fleischhauer, H.L.

    1985-10-01T23:59:59.000Z

    Two procedures for sampling the surface layer (0 to 15 centimeters) of radium-contaminated soil are recommended for use in remedial action projects. Both procedures adhere to the philosophy that soil samples should have constant geometry and constant volume in order to ensure uniformity. In the first procedure, a ''cookie cutter'' fashioned from pipe or steel plate, is driven to the desired depth by means of a slide hammer, and the sample extracted as a core or plug. The second procedure requires use of a template to outline the sampling area, from which the sample is obtained using a trowel or spoon. Sampling to the desired depth must then be performed incrementally. Selection of one procedure over the other is governed primarily by soil conditions, the cookie cutter being effective in nongravelly soils, and the template procedure appropriate for use in both gravelly and nongravelly soils. In any event, a minimum sample volume of 1000 cubic centimeters is recommended. The step-by-step procedures are accompanied by a description of the minimum requirements for sample documentation. Transport of the soil samples from the field is then addressed in a discussion of the federal regulations for shipping radioactive materials. Interpretation of those regulations, particularly in light of their application to remedial action soil-sampling programs, is provided in the form of guidance and suggested procedures. Due to the complex nature of the regulations, however, there is no guarantee that our interpretations of them are complete or entirely accurate. Preparation of soil samples for radium-226 analysis by means of gamma-ray spectroscopy is described.

  8. SAMPLE: software for VAX FORTRAN execution timing

    SciTech Connect (OSTI)

    Lowe, L.H.

    1983-01-01T23:59:59.000Z

    SAMPLE is a set of subroutines in use at the Los Alamos National Laboratory for collecting CPU timings of various FORTRAN program sections - usually individual subroutines. These measurements have been useful in making programs run faster. The presentation includes a description of the software and examples of its use. The software is available on the directory (SAMPLE) of the VAX SIG tape.

  9. Disc valve for sampling erosive process streams

    DOE Patents [OSTI]

    Mrochek, J.E.; Dinsmore, S.R.; Chandler, E.W.

    1984-08-16T23:59:59.000Z

    This is a patent for a disc-type, four-port sampling valve for service with erosive high temperature process streams. Inserts and liners of ..cap alpha..-silicon carbide respectively, in the faceplates and in the sampling cavities, limit erosion while providing lubricity for a smooth and precise operation. 1 fig.

  10. Hanford Site Environmental Surveillance Master Sampling Schedule

    SciTech Connect (OSTI)

    LE Bisping

    1999-02-12T23:59:59.000Z

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest National Laboratory (PNNL) for the U.S. Department of Energy (DOE). Sampling is conducted to evaluate levels of radioactive and nonradioactive pollutants in the Hanford environs, as required in DOE Order 5400.1, ''General Environmental protection Program,'' and DOE Order 5400.5, ''Radiation Protection of the Public and the Environment.'' The sampling methods are described in the Environmental Monitoring Plan, United States Department of Energy, Richland Operations Office, DOE/RL-91-50, Rev.2, U.S. Department of Energy, Richland, Washington. This document contains the CY1999 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes the sampling location, sample type, and analyses to be performed on the sample. In some cases, samples are scheduled on a rotating basis and may not be collected in 1999 in which case the anticipated year for collection is provided. In addition, a map is included for each media showing approximate sampling locations.

  11. Atmospheric sampling glow discharge ionization source

    DOE Patents [OSTI]

    McLuckey, S.A.; Glish, G.L.

    1989-07-18T23:59:59.000Z

    An atmospheric sampling glow discharge ionization source that can be used in combination with an analytical instrument which operates at high vacuum, such as a mass spectrometer. The atmospheric sampling glow discharge ionization source comprises a chamber with at least one pair of electrodes disposed therein, an inlet for a gaseous sample to be analyzed and an outlet communicating with an analyzer which operates at subatmospheric pressure. The ionization chamber is maintained at a pressure below atmospheric pressure, and a voltage difference is applied across the electrodes to induce a glow discharge between the electrodes, so that molecules passing through the inlet are ionized by the glow discharge and directed into the analyzer. The ionization source accepts the sample under atmospheric pressure conditions and processes it directly into the high vacuum instrument, bridging the pressure gap and drawing off unwanted atmospheric gases. The invention also includes a method for analyzing a gaseous sample using the glow discharge ionization source described above. 3 figs.

  12. E-Print Network 3.0 - attachment iii sample Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Search Sample search results for: attachment iii sample Page: << < 1 2 3 4 5 > >> 1 NIH Electronic Applications: Annotated SF 424 (R&R) Form Set Summary: Attach Biographical...

  13. E-Print Network 3.0 - attachment ii sample Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Search Sample search results for: attachment ii sample Page: << < 1 2 3 4 5 > >> 1 NIH Electronic Applications: Annotated SF 424 (R&R) Form Set Summary: Attach Biographical...

  14. E-Print Network 3.0 - adaptive importance sampling Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Liu, Fan Wang, Gagan Agrawal Summary: Adaptive Stratified Sampling for Data Mining on the Deep Web Tantan Liu, Fan Wang, Gagan Agrawal... a->Y - Adaptive sampling: more data are...

  15. E-Print Network 3.0 - actinide sample exposures Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1-1 1.2.1 Task 1: Review of radionuclide sampling data at the Radioactive Waste Management Complex... . . . . . . . ....

  16. Automated collection and processing of environmental samples

    DOE Patents [OSTI]

    Troyer, Gary L. (Richland, WA); McNeece, Susan G. (Richland, WA); Brayton, Darryl D. (Richland, WA); Panesar, Amardip K. (Kennewick, WA)

    1997-01-01T23:59:59.000Z

    For monitoring an environmental parameter such as the level of nuclear radiation, at distributed sites, bar coded sample collectors are deployed and their codes are read using a portable data entry unit that also records the time of deployment. The time and collector identity are cross referenced in memory in the portable unit. Similarly, when later recovering the collector for testing, the code is again read and the time of collection is stored as indexed to the sample collector, or to a further bar code, for example as provided on a container for the sample. The identity of the operator can also be encoded and stored. After deploying and/or recovering the sample collectors, the data is transmitted to a base processor. The samples are tested, preferably using a test unit coupled to the base processor, and again the time is recorded. The base processor computes the level of radiation at the site during exposure of the sample collector, using the detected radiation level of the sample, the delay between recovery and testing, the duration of exposure and the half life of the isotopes collected. In one embodiment, an identity code and a site code are optically read by an image grabber coupled to the portable data entry unit.

  17. Hanford Site Environmental Surveillance Master Sampling Schedule

    SciTech Connect (OSTI)

    LE Bisping

    2000-01-27T23:59:59.000Z

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest National Laboratory (PNNL) for the U.S. Department of Energy (DOE). Sampling is conducted to evaluate levels of radioactive and nonradioactive pollutants in the Hanford environs, as required in DOE Order 5400.1, General Environmental Protection Program: and DOE Order 5400.5, Radiation Protection of the Public and the Environment. The sampling design is described in the Operations Office, Environmental Monitoring Plan, United States Department of Energy, Richland DOE/RL-91-50, Rev.2, U.S. Department of Energy, Richland, Washington. This document contains the CY 2000 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes sampling locations, sample types, and analyses to be performed. In some cases, samples are scheduled on a rotating basis and may not be collected in 2000 in which case the anticipated year for collection is provided. In addition, a map showing approximate sampling locations is included for each media scheduled for collection.

  18. Vapor and gas sampling of Single-Shell Tank 241-T-111 using the vapor sampling system

    SciTech Connect (OSTI)

    Caprio, G.S.

    1995-09-01T23:59:59.000Z

    This document presents sampling data resulting from the January 20, 1995, sampling of SST 241-T-111 using the vapor sampling system.

  19. Vapor and gas sampling of single-shell tank 241-BY-112 using the vapor sampling system

    SciTech Connect (OSTI)

    Caprio, G.S.

    1995-09-20T23:59:59.000Z

    This document presents sampling data from the November 18, 1994, sampling of SST 241-BY-112 using the vapor sampling system.

  20. Vapor and gas sampling of Single-Shell Tank 241-A-101 using the Vapor Sampling System

    SciTech Connect (OSTI)

    Caprio, G.S.

    1995-11-01T23:59:59.000Z

    This document presents sampling data resulting from the June 8, 1995, sampling of SST 241-A-101 using the Vapor Sampling System.

  1. Multibore sample cell increases EPR sensitivity for aqueous samples Yuri E. Nesmelov *, David D. Thomas

    E-Print Network [OSTI]

    Thomas, David D.

    Multibore sample cell increases EPR sensitivity for aqueous samples Yuri E. Nesmelov *, David D calculations, verified by experiment, to explain why the sensitivity of biological EPR can be dramatically increased by dividing the aqueous sample into separate compartments. In biological EPR, the major factor

  2. Vapor port and groundwater sampling well

    DOE Patents [OSTI]

    Hubbell, Joel M. (Idaho Falls, ID); Wylie, Allan H. (Idaho Falls, ID)

    1996-01-01T23:59:59.000Z

    A method and apparatus has been developed for combining groundwater monitoring wells with unsaturated-zone vapor sampling ports. The apparatus allows concurrent monitoring of both the unsaturated and the saturated zone from the same well at contaminated areas. The innovative well design allows for concurrent sampling of groundwater and volatile organic compounds (VOCs) in the vadose (unsaturated) zone from a single well, saving considerable time and money. The sample tubes are banded to the outer well casing during installation of the well casing.

  3. Gas sampling system for a mass spectrometer

    DOE Patents [OSTI]

    2003-12-30T23:59:59.000Z

    The present invention relates generally to a gas sampling system, and specifically to a gas sampling system for transporting a hazardous process gas to a remotely located mass spectrometer. The gas sampling system includes a capillary tube having a predetermined capillary length and capillary diameter in communication with the supply of process gas and the mass spectrometer, a flexible tube surrounding and coaxial with the capillary tube intermediate the supply of process gas and the mass spectrometer, a heat transfer tube surrounding and coaxial with the capillary tube, and a heating device in communication the heat transfer tube for substantially preventing condensation of the process gas within the capillary tube.

  4. Vapor port and groundwater sampling well

    DOE Patents [OSTI]

    Hubbell, J.M.; Wylie, A.H.

    1996-01-09T23:59:59.000Z

    A method and apparatus have been developed for combining groundwater monitoring wells with unsaturated-zone vapor sampling ports. The apparatus allows concurrent monitoring of both the unsaturated and the saturated zone from the same well at contaminated areas. The innovative well design allows for concurrent sampling of groundwater and volatile organic compounds (VOCs) in the vadose (unsaturated) zone from a single well, saving considerable time and money. The sample tubes are banded to the outer well casing during installation of the well casing. 10 figs.

  5. Sampling device for withdrawing a representative sample from single and multi-phase flows

    DOE Patents [OSTI]

    Apley, Walter J. (Pasco, WA); Cliff, William C. (Richland, WA); Creer, James M. (Richland, WA)

    1984-01-01T23:59:59.000Z

    A fluid stream sampling device has been developed for the purpose of obtaining a representative sample from a single or multi-phase fluid flow. This objective is carried out by means of a probe which may be inserted into the fluid stream. Individual samples are withdrawn from the fluid flow by sampling ports with particular spacings, and the sampling parts are coupled to various analytical systems for characterization of the physical, thermal, and chemical properties of the fluid flow as a whole and also individually.

  6. Surface sampling concentration and reaction probe

    DOE Patents [OSTI]

    Van Berkel, Gary J; Elnaggar, Mariam S

    2013-07-16T23:59:59.000Z

    A method of analyzing a chemical composition of a specimen is described. The method can include providing a probe comprising an outer capillary tube and an inner capillary tube disposed co-axially within the outer capillary tube, where the inner and outer capillary tubes define a solvent capillary and a sampling capillary in fluid communication with one another at a distal end of the probe; contacting a target site on a surface of a specimen with a solvent in fluid communication with the probe; maintaining a plug volume proximate a solvent-specimen interface, wherein the plug volume is in fluid communication with the probe; draining plug sampling fluid from the plug volume through the sampling capillary; and analyzing a chemical composition of the plug sampling fluid with an analytical instrument. A system for performing the method is also described.

  7. WRAP Module 1 sampling and analysis plan

    SciTech Connect (OSTI)

    Mayancsik, B.A.

    1995-03-24T23:59:59.000Z

    This document provides the methodology to sample, screen, and analyze waste generated, processed, or otherwise the responsibility of the Waste Receiving and Processing Module 1 facility. This includes Low-Level Waste, Transuranic Waste, Mixed Waste, and Dangerous Waste.

  8. Adaptive Importance Sampling via Stochastic Convex Programming

    E-Print Network [OSTI]

    Adaptive Importance Sampling via Stochastic Convex Programming Ernest K. Ryu1 and Stephen P. Boyd1 Abstract We show that the variance of the Monte Carlo estimator that is importance sam- pled from

  9. Generalized Sampling-Based Feedback Motion Planners

    E-Print Network [OSTI]

    Kumar, Sandip

    2012-02-14T23:59:59.000Z

    states. In the deterministic robotics motion planning community, sampling based algorithms like probabilistic roadmaps (PRM) and rapidly exploring random trees (RRTs) have been successful in solving very high dimensional deterministic problem. However...

  10. Date: July 2 E Sample Handli

    E-Print Network [OSTI]

    Fischer, Emily V.

    25, 2013 Page 3 of 11 1. PURPOSE AND APPLICABILITY This standard operating procedure .........................................................................................................7 9. PROCEDURAL STEPS .........................................................................9 11.1 Cleaning and Maintenance of the Sample Handling Laboratory

  11. SAMPLING AND ANALYSIS PLAN CSMRI SITE REMEDIATION

    E-Print Network [OSTI]

    Littleton, CO 80127 #12;CSMRI Site Remediation Quality Assurance Project Plan March 30, 2004 SAMPLING Environmental Consultants, Inc. Approved By: Date: Sally Cuffin Project Quality Assurance Manager New Horizons...................................................................................................................................3 2.5 Decision Rules

  12. Experimental analysis of municipal solid waste samples

    E-Print Network [OSTI]

    Mendoza Sanchez, Itza

    2002-01-01T23:59:59.000Z

    EXPERIMENTAL ANALYSIS OF MUNICIPAL SOLID WASTE SAMPLES A Thesis by ITZA MENDOZA SANCHEZ Submitted to the Office of Graduate Studies of Texas ASM University tn partial fulfillment of the requirements for the degree of MASTER OF SCIENCE May... 2002 Major Subject: Civil Engmeering EXPERIMENTAL ANALYSIS OF MUNICIPAL SOLID WASTE SAMPLES A Thesis by ITZA MENDOZA SANCHEZ Submitted to the Office of Graduate Studies of Texas A&M Umversity in partial fulfillment of the requirements...

  13. A study of bioaerosol sampling cyclones

    E-Print Network [OSTI]

    Moncla, Brandon Wayne

    2005-02-17T23:59:59.000Z

    A STUDY OF BIOAEROSOL SAMPLING CYCLONES A Thesis by BRANDON WAYNE MONCLA Submitted to the Office of Graduate Studies of Texas A&M University in partial fulfillment of the requirements for the degree of MASTER... OF SCIENCE December 2004 Major Subject: Mechanical Engineering A STUDY OF BIOAEROSOL SAMPLING CYCLONES A Thesis by BRANDON WAYNE MONCLA Submitted to Texas A&M University in partial fulfillment...

  14. Hanford Site Environmental Surveillance Master Sampling Schedule

    SciTech Connect (OSTI)

    Bisping, Lynn E.

    2002-01-16T23:59:59.000Z

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by Pacific Northwest National Laboratory (PNNL) for the U.S. Department of Energy (DOE). Sampling is conducted to evaluate levels of radioactive and nonradioactive pollutants in the Hanford environs. The document contains the CY 2002 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project.

  15. Improved DESI-MS Performance using Edge Sampling and aRotational Sample Stage

    SciTech Connect (OSTI)

    Kertesz, Vilmos [ORNL; Van Berkel, Gary J [ORNL

    2008-01-01T23:59:59.000Z

    The position of the surface to be analyzed relative to the sampling orifice or capillary into the mass spectrometer has been known to dramatically affect the observed signal levels in desorption electrospray ionization mass spectrometry (DESIMS). In analyses of sample spots on planar surfaces, DESI-MS signal intensities as much as five times greater were routinely observed when the bottom of the sampling capillary was appropriately positioned beneath the surface plane ( edge sampling") compared to when the capillary just touched the surface. To take advantage of the optimum "edge sampling" geometry and to maximize the number of samples that could be analyzed in this configuration, a rotational sample stage was integrated into a typical DESI-MS setup. The rapid quantitative determination of caffeine in two diet sport drinks (Diet Turbo Tea, Speed Stack Grape) spiked with an isotopically labeled internal standard demonstrated the utility of this approach.

  16. Rapid determination of actinides in asphalt samples

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Maxwell, Sherrod L.; Culligan, Brian K.; Hutchison, Jay B.

    2014-01-12T23:59:59.000Z

    A new rapid method for the determination of actinides in asphalt samples has been developed that can be used in emergency response situations or for routine analysis If a radiological dispersive device (RDD), Improvised Nuclear Device (IND) or a nuclear accident such as the accident at the Fukushima Nuclear Power Plant in March, 2011 occurs, there will be an urgent need for rapid analyses of many different environmental matrices, including asphalt materials, to support dose mitigation and environmental clean up. The new method for the determination of actinides in asphalt utilizes a rapid furnace step to destroy bitumen and organics present in the asphalt and sodium hydroxide fusion to digest the remaining sample. Sample preconcentration steps are used to collect the actinides and a new stacked TRU Resin + DGA Resin column method is employed to separate the actinide isotopes in the asphalt samples. The TRU Resin plus DGA Resin separation approach, which allows sequential separation of plutonium, uranium, americium and curium isotopes in asphalt samples, can be applied to soil samples as well.

  17. On sampling fractions and electron shower shapes

    SciTech Connect (OSTI)

    Peryshkin, Alexander; Raja, Rajendran; /Fermilab

    2011-12-01T23:59:59.000Z

    We study the usage of various definitions of sampling fractions in understanding electron shower shapes in a sampling multilayer electromagnetic calorimeter. We show that the sampling fractions obtained by the conventional definition (I) of (average observed energy in layer)/(average deposited energy in layer) will not give the best energy resolution for the calorimeter. The reason for this is shown to be the presence of layer by layer correlations in an electromagnetic shower. The best resolution is obtained by minimizing the deviation from the total input energy using a least squares algorithm. The 'sampling fractions' obtained by this method (II) are shown to give the best resolution for overall energy. We further show that the method (II) sampling fractions are obtained by summing the columns of a non-local {lambda} tensor that incorporates the correlations. We establish that the sampling fractions (II) cannot be used to predict the layer by layer energies and that one needs to employ the full {lambda} tensor for this purpose. This effect is again a result of the correlations.

  18. Analytical instrument with apparatus for sample concentrating

    DOE Patents [OSTI]

    Zaromb, Solomon (Hinsdale, IL)

    1989-01-01T23:59:59.000Z

    A system for analysis of trace concentrations of contaminants in air includes a portable liquid chromatograph and a preconcentrator for the contaminants to be analyzed. The preconcentrator includes a sample bag having an inlet valve and an outlet valve for collecting an air sample. When the sample is collected the sample bag is connected in series with a sorbing apparatus in a recirculation loop. The sorbing apparatus has an inner gas-permeable container containing a sorbent material and an outer gas-impermeable container. The sample is circulated through the outer container and around the inner container for trapping and preconcentrating the contaminants in the sorbent material. The sorbent material may be a liquid having the same composition as the mobile phase of the chromatograph for direct injection thereinto. Alternatively, the sorbent material may be a porous, solid body, to which mobile phase liquid is added after preconcentration of the contaminants for dissolving the contaminants, the liquid solution then being withdrawn for injection into the chromatograph.

  19. Standard guide for sampling radioactive tank waste

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2011-01-01T23:59:59.000Z

    1.1 This guide addresses techniques used to obtain grab samples from tanks containing high-level radioactive waste created during the reprocessing of spent nuclear fuels. Guidance on selecting appropriate sampling devices for waste covered by the Resource Conservation and Recovery Act (RCRA) is also provided by the United States Environmental Protection Agency (EPA) (1). Vapor sampling of the head-space is not included in this guide because it does not significantly affect slurry retrieval, pipeline transport, plugging, or mixing. 1.2 The values stated in inch-pound units are to be regarded as standard. No other units of measurement are included in this standard. 1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

  20. Radioactive sample effects on EDXRF spectra

    SciTech Connect (OSTI)

    Worley, Christopher G [Los Alamos National Laboratory

    2008-01-01T23:59:59.000Z

    Energy dispersive X-ray fluorescence (EDXRF) is a rapid, straightforward method to determine sample elemental composition. A spectrum can be collected in a few minutes or less, and elemental content can be determined easily if there is adequate energy resolution. Radioactive alpha emitters, however, emit X-rays during the alpha decay process that complicate spectral interpretation. This is particularly noticeable when using a portable instrument where the detector is located in close proximity to the instrument analysis window held against the sample. A portable EDXRF instrument was used to collect spectra from specimens containing plutonium-239 (a moderate alpha emitter) and americium-241 (a heavy alpha emitter). These specimens were then analyzed with a wavelength dispersive XRF (WDXRF) instrument to demonstrate the differences to which sample radiation-induced X-ray emission affects the detectors on these two types of XRF instruments.

  1. Sample Desorption/Onization From Mesoporous Silica

    DOE Patents [OSTI]

    Iyer, Srinivas (Los Alamos, NM); Dattelbaum, Andrew M. (Los Alamos, NM)

    2005-10-25T23:59:59.000Z

    Mesoporous silica is shown to be a sample holder for laser desorption/ionization of mass spectrometry. Supported mesoporous silica was prepared by coating an ethanolic silicate solution having a removable surfactant onto a substrate to produce a self-assembled, ordered, nanocomposite silica thin film. The surfactant was chosen to provide a desired pore size between about 1 nanometer diameter and 50 nanometers diameter. Removal of the surfactant resulted in a mesoporous silica thin film on the substrate. Samples having a molecular weight below 1000, such as C.sub.60 and tryptophan, were adsorbed onto and into the mesoporous silica thin film sample holder and analyzed using laser desorption/ionization mass spectrometry.

  2. DWPF SMECT PVV SAMPLE CHARACTERIZATION AND REMEDIATION

    SciTech Connect (OSTI)

    Bannochie, C.; Crawford, C.

    2013-06-18T23:59:59.000Z

    On April 2, 2013, a solid sample of material collected from the Defense Waste Processing Facility’s Process Vessel Vent (PVV) jumper for the Slurry Mix Evaporator Condensate Tank (SMECT) was received at the Savannah River National Laboratory (SRNL). DWPF has experienced pressure spikes within the SMECT and other process vessels which have resulted in processing delays while a vacuum was re-established. Work on this sample was requested in a Technical Assistance Request (TAR). This document reports the results of chemical and physical property measurements made on the sample, as well as insights into the possible impact to the material using DWPF’s proposed remediation methods. DWPF was interested in what the facility could expect when the material was exposed to either 8M nitric acid or 90% formic acid, the two materials they have the ability to flush through the PVV line in addition to process water once the line is capped off during a facility outage.

  3. E-Print Network 3.0 - atmospheric sampling program Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    12 days... samples, a study was conducted as part of the NAWQA ... Source: Fleskes, Joe - Dixon Field Station, Western Ecological Research Center, USGS Collection:...

  4. E-Print Network 3.0 - animal fat samples Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    in liver and fat tissue... , and epididymal fat) and blood samples as ... Source: Bass, Joe - Departments of Biochemistry, Molecular Biology, and Cell Biology & Neurobiology and...

  5. E-Print Network 3.0 - air sample extract Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    -linked immunosorbent as- say (ELISA) to measure paraquat in human-exposure samples (air filters, personal air monitors... analysis, paraquat collected in ... Source: Hammock,...

  6. E-Print Network 3.0 - air sampling requirements Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Center Collection: Energy Storage, Conversion and Utilization 98 Evaluation of HVAC filters as a sampling mechanism for indoor microbial communities Summary: in HVAC filter...

  7. E-Print Network 3.0 - adequate sample sizes Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    SYSTEMS WITH REPLICA... , thus preventing adequate system sampling and appropriate comparison of simulation results... . o Latour "A Parallel Tempering Algorithm for...

  8. E-Print Network 3.0 - automated sample transfer Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    code) - Prepare sample dilution: o Use stock ... Source: Kaber, David B. - Department of Industrial and Systems Engineering, North Carolina State University Collection:...

  9. E-Print Network 3.0 - automating groundwater sampling Sample...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    GROUNDWATER MANAGEMENT... summary of selected case studies is presented below. BACKGROUND A typical groundwater sampling event... . Automation through the use of sensors...

  10. E-Print Network 3.0 - automated blood sampling Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Summary: screening for lead poisoning: capillary blood sampling and automated Delves-cup atomic- absorption analysis... ... Source: National Center for Environmental Health-...

  11. E-Print Network 3.0 - animal tissue samples Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Summary: infectious agents and contaminated samples between the laboratory and animal facility in a sealed, secondary... tissue harvest in the animal room or arrange with animal...

  12. E-Print Network 3.0 - arterio-venous blood sampling Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    was sampled from... nutritional sources. By measuring arterio-venous transit times of a fluorescent dye, Rovainen et al (1993... Active dilation of penetrating arterioles...

  13. E-Print Network 3.0 - aqueous bulk sample Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    that aqueous processing has shifted some samples to heavier compositions. A lower bulk solar... processes involving aqueous fluids, given the potential solubility of lithium...

  14. E-Print Network 3.0 - archival tumor samples Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    results for: archival tumor samples Page: << < 1 2 3 4 5 > >> 1 Robust Estimation for Brain Tumor Segmentation Summary: Robust Estimation for Brain Tumor Segmentation 1 Marcel...

  15. E-Print Network 3.0 - air particulate samples Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    search results for: air particulate samples Page: << < 1 2 3 4 5 > >> 1 Prevention of Air Pollution from Ships: Diesel Engine Particulate Emission Reduction via...

  16. E-Print Network 3.0 - andalusian population sample Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    worldwide population, pro- viding a well-established structure for Y... - tance to the Middle East. Unfortunately, samples from the appropriate ... Source: Cavalli-Sforza, Luigi...

  17. E-Print Network 3.0 - attachment iv sample Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Sciences, University of Michigan Collection: Geosciences 4 BLOOD SAMPLING SYSTEM TROUBLESHOOTING TIPS Summary: to cleanse the latex-free SAFESETTM port from which the...

  18. Statistical sampling method for releasing decontaminated vehicles

    SciTech Connect (OSTI)

    Lively, J.W.; Ware, J.A. [Rust Geotech, Grand Junction, CO (United States)

    1996-06-01T23:59:59.000Z

    Earth moving vehicles (e.g., dump trucks, belly dumps) commonly haul radiologically contaminated materials from a site being remediated to a disposal site. Traditionally, each vehicle must be surveyed before being released. The logistical difficulties of implementing the traditional approach on a large scale demand that an alternative be devised. A statistical method (MIL-STD-105E, {open_quotes}Sampling Procedures and Tables for Inspection by Attributes{close_quotes}) for assessing product quality from a continuous process was adapted to the vehicle decontamination process. This method produced a sampling scheme that automatically compensates and accommodates fluctuating batch sizes and changing conditions without the need to modify or rectify the sampling scheme in the field. Vehicles are randomly selected (sampled) upon completion of the decontamination process to be surveyed for residual radioactive surface contamination. The frequency of sampling is based on the expected number of vehicles passing through the decontamination process in a given period and the confidence level desired. This process has been successfully used for 1 year at the former uranium mill site in Monticello, Utah (a CERCLA regulated clean-up site). The method forces improvement in the quality of the decontamination process and results in a lower likelihood that vehicles exceeding the surface contamination standards are offered for survey. Implementation of this statistical sampling method on Monticello Projects has resulted in more efficient processing of vehicles through decontamination and radiological release, saved hundreds of hours of processing time, provided a high level of confidence that release limits are met, and improved the radiological cleanliness of vehicles leaving the controlled site.

  19. Performance evaluation soil samples utilizing encapsulation technology

    DOE Patents [OSTI]

    Dahlgran, J.R.

    1999-08-17T23:59:59.000Z

    Performance evaluation soil samples and method of their preparation uses encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration. 1 fig.

  20. Performance evaluation soil samples utilizing encapsulation technology

    DOE Patents [OSTI]

    Dahlgran, James R. (Idaho Falls, ID)

    1999-01-01T23:59:59.000Z

    Performance evaluation soil samples and method of their preparation using encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration.

  1. An economic approach to acceptance sampling

    E-Print Network [OSTI]

    Ruth, Robert Justin

    1973-01-01T23:59:59.000Z

    AN ECONOMIC APPROACH TO ACCEPTANCE SAMPLING A Thesis by ROBERT JUSTIN RUTH Subm1tted to the Graduate College of Texas AkM University in Partial fulfillment of the requirement for the degree of MASTER OP SCIENCE May 1973 Ma)or Sub... JUSTIN RUTH I Approved as to style and content by& , J ~ W P. H. Newell Head Departmen J McNicho e Mem er 8w~ D. R. Shreve Member May 1973 ABSTRACT An Economic Approach to Acceptance Sampling (&m 1973) Robert Justin Ruth, S. S ~ , Virgin1a...

  2. RAPID DETERMINATION OF RADIOSTRONTIUM IN SEAWATER SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.

    2013-01-16T23:59:59.000Z

    A new method for the determination of radiostrontium in seawater samples has been developed at the Savannah River National Laboratory (SRNL) that allows rapid preconcentration and separation of strontium and yttrium isotopes in seawater samples for measurement. The new SRNL method employs a novel and effective pre-concentration step that utilizes a blend of calcium phosphate with iron hydroxide to collect both strontium and yttrium rapidly from the seawater matrix with enhanced chemical yields. The pre-concentration steps, in combination with rapid Sr Resin and DGA Resin cartridge separation options using vacuum box technology, allow seawater samples up to 10 liters to be analyzed. The total {sup 89}Sr + {sup 90}Sr activity may be determined by gas flow proportional counting and recounted after ingrowth of {sup 90}Y to differentiate {sup 89}Sr from {sup 90}Sr. Gas flow proportional counting provides a lower method detection limit than liquid scintillation or Cerenkov counting and allows simultaneous counting of samples. Simultaneous counting allows for longer count times and lower method detection limits without handling very large aliquots of seawater. Seawater samples up to 6 liters may be analyzed using Sr Resin for {sup 89}Sr and {sup 90}Sr with a Minimum Detectable Activity (MDA) of 1-10 mBq/L, depending on count times. Seawater samples up to 10 liters may be analyzed for {sup 90}Sr using a DGA Resin method via collection and purification of {sup 90}Y only. If {sup 89}Sr and other fission products are present, then {sup 91}Y (beta energy 1.55 MeV, 58.5 day half-life) is also likely to be present. {sup 91}Y interferes with attempts to collect {sup 90}Y directly from the seawater sample without initial purification of Sr isotopes first and {sup 90}Y ingrowth. The DGA Resin option can be used to determine {sup 90}Sr, and if {sup 91}Y is also present, an ingrowth option with using DGA Resin again to collect {sup 90}Y can be performed. An MDA for {sup 90}Sr of <1 mBq/L for an 8 hour count may be obtained using 10 liter seawater sample aliquots.

  3. Surface Water Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home5b9fcbce19 No revisionEnvReviewNonInvasiveExplorationUT-g GrantAtlas (PACAOpenSummerside WindSolarSampling Jump to:Sampling Jump

  4. Supplemental Text Analysis of the ice core samples

    E-Print Network [OSTI]

    Massachusetts at Amherst, University of

    into a continuous sequence of samples (NIF2, 2197 samples; NIF3, 1980 samples; SIF1, 706 samples; SIF2, 834 samples and the sixth core, NIF1 (drilled one meter from NIF2) has been reserved for other measurements such as AMS 14 C. These comments follow the dating discussion in chronological order. The net down wasting of the NIF (as discussed

  5. A BASIS FOR MODIFYING THE TANK 12 COMPOSITE SAMPLING DESIGN

    SciTech Connect (OSTI)

    Shine, G.

    2014-11-25T23:59:59.000Z

    The SRR sampling campaign to obtain residual solids material from the Savannah River Site (SRS) Tank Farm Tank 12 primary vessel resulted in obtaining appreciable material in all 6 planned source samples from the mound strata but only in 5 of the 6 planned source samples from the floor stratum. Consequently, the design of the compositing scheme presented in the Tank 12 Sampling and Analysis Plan, Pavletich (2014a), must be revised. Analytical Development of SRNL statistically evaluated the sampling uncertainty associated with using various compositing arrays and splitting one or more samples for compositing. The variance of the simple mean of composite sample concentrations is a reasonable standard to investigate the impact of the following sampling options. Composite Sample Design Option (a). Assign only 1 source sample from the floor stratum and 1 source sample from each of the mound strata to each of the composite samples. Each source sample contributes material to only 1 composite sample. Two source samples from the floor stratum would not be used. Composite Sample Design Option (b). Assign 2 source samples from the floor stratum and 1 source sample from each of the mound strata to each composite sample. This infers that one source sample from the floor must be used twice, with 2 composite samples sharing material from this particular source sample. All five source samples from the floor would be used. Composite Sample Design Option (c). Assign 3 source samples from the floor stratum and 1 source sample from each of the mound strata to each composite sample. This infers that several of the source samples from the floor stratum must be assigned to more than one composite sample. All 5 source samples from the floor would be used. Using fewer than 12 source samples will increase the sampling variability over that of the Basic Composite Sample Design, Pavletich (2013). Considering the impact to the variance of the simple mean of the composite sample concentrations, the recommendation is to construct each sample composite using four or five source samples. Although the variance using 5 source samples per composite sample (Composite Sample Design Option (c)) was slightly less than the variance using 4 source samples per composite sample (Composite Sample Design Option (b)), there is no practical difference between those variances. This does not consider that the measurement error variance, which is the same for all composite sample design options considered in this report, will further dilute any differences. Composite Sample Design Option (a) had the largest variance for the mean concentration in the three composite samples and should be avoided. These results are consistent with Pavletich (2014b) which utilizes a low elevation and a high elevation mound source sample and two floor source samples for each composite sample. Utilizing the four source samples per composite design, Pavletich (2014b) utilizes aliquots of Floor Sample 4 for two composite samples.

  6. Reliability Assessment Using Discriminative Sampling and Metamodeling

    E-Print Network [OSTI]

    Wang, Gaofeng Gary

    1 05M-400 Reliability Assessment Using Discriminative Sampling and Metamodeling G. Gary Wang Dept ABSTRACT Reliability assessment is the foundation for reliability engineering and reliability-based design optimization. It has been a difficult task, however, to perform both accurate and efficient reliability

  7. Biology: Sample Pathway Semester I Semester II

    E-Print Network [OSTI]

    Goldberg, Bennett

    Biology: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Core CAS CH101 CAS CH102 and NS202. Major Requirements: The major in Biology is 16 courses. Courses taken to satisfy CAS major. The biology concentration also offers specializations in Ecology and Conservation Biology, Neurobiology, Cell

  8. Updated June 2013 Biomedical Engineering Sample Curriculum

    E-Print Network [OSTI]

    Subramanian, Venkat

    Updated June 2013 Biomedical Engineering Sample Curriculum WU Course Fall Spring Home Institution at WU Introduction to Biomedical Engineering BME 140 3 Biomechanics BME 240 3 Physiological Control Quantitative Physiology I & II BME 301A, 301B 4 4 Biomedical Engineering Design BME 401 3 Transport Phenomena I

  9. Updated May 2014 Biomedical Engineering Sample Curriculum

    E-Print Network [OSTI]

    Subramanian, Venkat

    Updated May 2014 Biomedical Engineering Sample Curriculum WU Course Fall Spring Home Institution (3 at WU Introduction to Biomedical Engineering BME 140 3 Biomechanics BME 240 3 Physiological Control Quantitative Physiology I & II BME 301A, 301B 4 4 Biomedical Engineering Design BME 401 3 Transport Phenomena

  10. Statistical Complexity of Sampled Chaotic Attractors

    E-Print Network [OSTI]

    Luciana De Micco; Juana Graciela Fernández; Hilda Angela Larrondo; Angelo Plastino; Osvaldo Anibal Rosso

    2011-05-19T23:59:59.000Z

    We analyze the statistical complexity vs. entropy plane-representation of sampled chaotic attractors as a function of the sampling period {\\tau}. It is shown that if the Bandt and Pompe procedure is used to assign a probability distribution function (PDF) to the pertinent time series, the statistical complexity measure (SCM) attains a definite maximum for a specific sampling period tM. If the usual histogram approach is used instead in order to assign the PDF to the time series, the SCM remains almost constant at any sampling period {\\tau}. The significance of tM is further investigated by comparing it with typical times given in the literature for the two main reconstruction processes: the Takens' one in a delay-time embedding, and the exact Nyquist-Shannon reconstruction. It is shown that tM is compatible with those times recommended as adequate delay ones in Takens' reconstruction. The reported results correspond to three representative chaotic systems having correlation dimension 2 < D2 < 3. One recent experiment confirms the analysis presented here.

  11. Analytical Chemistry Division's sample transaction system

    SciTech Connect (OSTI)

    Stanton, J.S.; Tilson, P.A.

    1980-10-01T23:59:59.000Z

    The Analytical Chemistry Division uses the DECsystem-10 computer for a wide range of tasks: sample management, timekeeping, quality assurance, and data calculation. This document describes the features and operating characteristics of many of the computer programs used by the Division. The descriptions are divided into chapters which cover all of the information about one aspect of the Analytical Chemistry Division's computer processing.

  12. Physics 321 Exam 1 Sample Questions

    E-Print Network [OSTI]

    Hart, Gus

    of motion. Briefly explain the meaning of each law. 4. Describe one case where Newton's third law does .T At what frequency is the response a maximum? What does FWHM mean? What is the expression we usePhysics 321 Exam 1 Sample Questions 1. Write the second order differential equation as two first

  13. Analysis of large soil samples for actinides

    SciTech Connect (OSTI)

    Maxwell, III; Sherrod L. (Aiken, SC)

    2009-03-24T23:59:59.000Z

    A method of analyzing relatively large soil samples for actinides by employing a separation process that includes cerium fluoride precipitation for removing the soil matrix and precipitates plutonium, americium, and curium with cerium and hydrofluoric acid followed by separating these actinides using chromatography cartridges.

  14. Particle Size Distribution of Gypseous Samples

    E-Print Network [OSTI]

    Arnett, Morgan P.

    2010-01-16T23:59:59.000Z

    to conditions in the field. In order to understand the true characterization of the soil and the gypsum particles, the entire soil sample should be analyzed. Four different approaches to the BaCl2 method presented in the literature (Hesse, 1976, Matar...

  15. Updated May 2014 Computer Engineering Sample Curriculum

    E-Print Network [OSTI]

    Subramanian, Venkat

    if student did not complete a social science course at the 300-400 or junior/senior level at their homeUpdated May 2014 Computer Engineering Sample Curriculum *Engineering Professional Practice required Differential Equations Math 217 3 General Physics I, II Physics 117A, 118A 4 4 General Chemistry I Chem 111A 3

  16. Updated June 2013 Computer Engineering Sample Curriculum

    E-Print Network [OSTI]

    Subramanian, Venkat

    required if student did not complete 300-400 social science course at their home institution WU Course FallUpdated June 2013 Computer Engineering Sample Curriculum *Engineering Professional Practice General Physics I, II Physics 117A, 118A 4 4 General Chemistry I Chem 111A 3 General Chemistry Laboratory

  17. Hanford site transuranic waste sampling plan

    SciTech Connect (OSTI)

    GREAGER, T.M.

    1999-05-13T23:59:59.000Z

    This sampling plan (SP) describes the selection of containers for sampling of homogeneous solids and soil/gravel and for visual examination of transuranic and mixed transuranic (collectively referred to as TRU) waste generated at the U.S. Department of Energy (DOE) Hanford Site. The activities described in this SP will be conducted under the Hanford Site TRU Waste Certification Program. This SP is designed to meet the requirements of the Transuranic Waste Characterization Quality Assurance Program Plan (CAO-94-1010) (DOE 1996a) (QAPP), site-specific implementation of which is described in the Hanford Site Transuranic Waste Characterization Program Quality Assurance Project Plan (HNF-2599) (Hanford 1998b) (QAPP). The QAPP defines the quality assurance (QA) requirements and protocols for TRU waste characterization activities at the Hanford Site. In addition, the QAPP identifies responsible organizations, describes required program activities, outlines sampling and analysis strategies, and identifies procedures for characterization activities. The QAPP identifies specific requirements for TRU waste sampling plans. Table 1-1 presents these requirements and indicates sections in this SP where these requirements are addressed.

  18. Sampling the National Deep Web Denis Shestakov

    E-Print Network [OSTI]

    Hammerton, James

    Sampling the National Deep Web Denis Shestakov Department of Media Technology, Aalto University pages filled with information from myriads of online databases. This part of the Web, known as the deep a problem of deep Web characterization: how to estimate the total number of online databases on the Web? We

  19. Argonne Premium Coal Sample Bank The Argonne Premium Coal (APC) Sample Bank can supply

    E-Print Network [OSTI]

    Maranas, Costas

    Argonne Premium Coal Sample Bank Background Overview T The Argonne Premium Coal (APC) Sample Bank, there are well over 600 peer-reviewed journals articles addressing the structure and behavior of the Argonne of the Office of Basic Energy Sciences of the U. S. Department of Energy. From 1983­1985 Argonne National

  20. Sample Results From The Interim Salt Disposition Program Macrobatch 6 Tank 21H Qualification Samples

    SciTech Connect (OSTI)

    Peters, T. B.; Fink, S. D.

    2012-12-20T23:59:59.000Z

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H in support of qualification of Macrobatch (Salt Batch) 6 for the Interim Salt Disposition Project (ISDP). This document reports partial results of the analyses of samples of Tank 21H. No issues with the projected Salt Batch 6 strategy are identified.

  1. Sample Results from the Interim Salt Disposition Program Macrobatch 6 Tank 21H Qualification Samples

    SciTech Connect (OSTI)

    Peters, T. B.; Fink, S. D.

    2012-12-11T23:59:59.000Z

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H in support of qualification of Macrobatch (Salt Batch) 6 for the Interim Salt Disposition Project (ISDP). This document reports partial results of the analyses of samples of Tank 21H. No issues with the projected Salt Batch 6 strategy are identified.

  2. Method of isolating an oilfield flowline sample for analysis without shearing the sample

    SciTech Connect (OSTI)

    Brickhouse, P.E.

    1990-03-06T23:59:59.000Z

    This patent describes a method for isolating an oil field production flowline sample for analysis without shearing the sample. It comprises: placing an isolation chamber in fluid communication with a sampling port of an oilfield production flowline. The isolation chamber comprising a closed vessel, a first entry port into the vessel, and a first exit port out of the vessel controlled by a first valve. The sampling port is controlled by a valve; opening a sampling port valve while the first valve is closed to permit pressure within the isolation chamber to equalize the pressure within the first entry port and the flowline; opening the first valve to permit oilfield production to pass from the flowline through the sampling port and the first entry port into the isolation chamber and out of the first valve; closing the first valve; closing the sampling port valve; allowing the oilfield production fluid contained within the isolation chamber to separate for a period of time, and removing a sample of fluid from the isolation chamber for examination.

  3. Fast and Easy Sample Dialysis When downstream quality matters,

    E-Print Network [OSTI]

    Lebendiker, Mario

    samples with convenience · No need to use a syringe to load or remove samples. Simply load your sampleL Milli-Q® water Conductivity standard curve using NaCl Protein recovery after 5 hours: 89% Volume

  4. Mass spectrometer having a derivatized sample presentation apparatus

    DOE Patents [OSTI]

    Nelson, Randall W. (Phoenix, AZ)

    2000-07-25T23:59:59.000Z

    A mass spectrometer having a derivatized sample presentation apparatus is provided. The sample presentation apparatus has a complex bound to the surface of the sample presentation apparatus. This complex includes a molecule which may chemically modify a biomolecule.

  5. Hanford analytical sample projections FY 1998--FY 2002

    SciTech Connect (OSTI)

    Joyce, S.M.

    1997-12-10T23:59:59.000Z

    Sample projections are compiled for the Hanford site based on inputs from the major programs for the years 1998 through 2002. Sample projections are categorized by radiation level, protocol, sample matrix and Program. Analyses requirements are also presented.

  6. Hanford Site Environmental Surveillance Master Sampling Schedule, January 2001

    SciTech Connect (OSTI)

    Bisping, Lynn E.

    2001-01-08T23:59:59.000Z

    This document contains the CY 2001 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes sampling locations, sample types, and analyses to be performed.

  7. Sample size in factor analysis: The role of model error

    E-Print Network [OSTI]

    MacCallum, R. C.; Widaman, K. F.; Preacher, K. J.; Hong, Sehee

    2001-01-01T23:59:59.000Z

    This article examines effects of sample size and other design features on correspondence between factors obtained from analysis of sample data and those present in the population from which the samples were drawn. We extend ...

  8. Combining Functional and Structural Genomics to Sample the Essential...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Functional and Structural Genomics to Sample the Essential Burkholderia Structome. Combining Functional and Structural Genomics to Sample the Essential Burkholderia Structome....

  9. Preliminary/Sample Residential EE Loan Term Sheet and Underwriting...

    Broader source: Energy.gov (indexed) [DOE]

    sample or preliminary term sheet for single family residential energy efficiency loans. Author: Energy Efficiency Finance Corp. PreliminarySample Residential Energy Efficiency...

  10. Rb-Sr Geochronologic Investigation Of Precambrian Samples From...

    Open Energy Info (EERE)

    by eight samples. Because these samples are more representative of mineral systems or granite gneiss -amphibolite mixtures, the age is interpreted as being anomalously old....

  11. Transition Path Sampling of Water Exchange Rates and Mechanisms...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Path Sampling of Water Exchange Rates and Mechanisms around Aqueous Ions . Transition Path Sampling of Water Exchange Rates and Mechanisms around Aqueous Ions . Abstract: The rates...

  12. Commercial Building Energy Asset Score Sample Report | Department...

    Broader source: Energy.gov (indexed) [DOE]

    Sample Report Commercial Building Energy Asset Score Sample Report Example report showing the results of an energy asset score rating on a building Commercial Building Energy Asset...

  13. Commercial Building Energy Asset Score Sample Report | Department...

    Broader source: Energy.gov (indexed) [DOE]

    Score Sample Report Commercial Building Energy Asset Score Sample Report Example report showing the results of an energy asset score rating on a building energyassetscoresample...

  14. Sample Contract Language for Information Technology Using Energy...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Sample Contract Language for Information Technology Using Energy-Efficient Products Sample Contract Language for Information Technology Using Energy-Efficient Products Document...

  15. Microfluidic-Based Robotic Sampling System for Radioactive Solutions

    SciTech Connect (OSTI)

    Jack D. Law; Julia L. Tripp; Tara E. Smith; Veronica J. Rutledge; Troy G. Garn; John Svoboda; Larry Macaluso

    2014-02-01T23:59:59.000Z

    A novel microfluidic based robotic sampling system has been developed for sampling and analysis of liquid solutions in nuclear processes. This system couples the use of a microfluidic sample chip with a robotic system designed to allow remote, automated sampling of process solutions in-cell and facilitates direct coupling of the microfluidic sample chip with analytical instrumentation. This system provides the capability for near real time analysis, reduces analytical waste, and minimizes the potential for personnel exposure associated with traditional sampling methods. A prototype sampling system was designed, built and tested. System testing demonstrated operability of the microfluidic based sample system and identified system modifications to optimize performance.

  16. asthmatic population sample: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    sample allocation and effort in detecting population differentiation Dordrecht 2014 Abstract One of the most pressing issues in spatial genetics concerns sampling....

  17. Apparatus and method for maintaining multi-component sample gas constituents in vapor phase during sample extraction and cooling

    DOE Patents [OSTI]

    Felix, Larry Gordon; Farthing, William Earl; Irvin, James Hodges; Snyder, Todd Robert

    2010-05-11T23:59:59.000Z

    A dilution apparatus for diluting a gas sample. The apparatus includes a sample gas conduit having a sample gas inlet end and a diluted sample gas outlet end, and a sample gas flow restricting orifice disposed proximate the sample gas inlet end connected with the sample gas conduit and providing fluid communication between the exterior and the interior of the sample gas conduit. A diluted sample gas conduit is provided within the sample gas conduit having a mixing end with a mixing space inlet opening disposed proximate the sample gas inlet end, thereby forming an annular space between the sample gas conduit and the diluted sample gas conduit. The mixing end of the diluted sample gas conduit is disposed at a distance from the sample gas flow restricting orifice. A dilution gas source connected with the sample gas inlet end of the sample gas conduit is provided for introducing a dilution gas into the annular space, and a filter is provided for filtering the sample gas. The apparatus is particularly suited for diluting heated sample gases containing one or more condensable components.

  18. Site monitoring from soil sample analysis

    SciTech Connect (OSTI)

    Illsley, C.T.

    1982-01-01T23:59:59.000Z

    Soil samples have been collected for the past three years as part of a long range monitoring program. The program was designed to provide information on possible migration of plutonium in soil and to provide data for comparison with the EPA proposed guidance on transuranium elements in the environment. Samples have been collected at six locations west of Indiana Street within the eastern boundaries of the Rocky Flats Plant site. The EPA comparison study has been performed at five sites and the plutonium migration study is underway at the sixth site. The data on plutonium analyses will be compared to the EPA screening level of 0.20 ..mu..Ci/m/sup 2/ (74 x 10/sup 8/ Bq/km/sup 2/) in the five boundary sites. Possible migration trends will be examined for the plutonium data on soils from the other site.

  19. Natural Radioactivity of Boron Added Clay Samples

    SciTech Connect (OSTI)

    Akkurt, I.; Guenoglu, K. [Sueleyman Demirel University, Faculty of Arts and Sciences, Dept. of Physics, Isparta (Turkey); Canakcii, H. [Gaziantep University, Engineering Faculty, Civil Engineering Dept., Gaziantep (Turkey); Mavi, B. [Amasya University, Faculty of Arts and Sciences, Dept. of Physics, Amasya (Turkey)

    2011-12-26T23:59:59.000Z

    Clay, consisting fine-grained minerals, is an interesting materials and can be used in a variety of different fields especially in dermatology application. Using clay such a field it is important to measure its natural radioactivity. Thus the purpose of this study is to measure {sup 226}Ra, {sup 232}Th and {sup 40}K concentration in clay samples enriched with boron. Three different types of clay samples were prepared where boron is used in different rate. The measurements have been determined using a gamma-ray spectrometry consists of a 3''x3'' NaI(Tl) detector. From the measured activity the radium equivalent activities (Ra{sub eq}), external hazard index (H{sub ex}), absorbed dose rate in air (D) and annual effective dose (AED) have also been obtained.

  20. SEARCH, blackbox optimization, and sample complexity

    SciTech Connect (OSTI)

    Kargupta, H. [Los Alamos National Lab., NM (United States). Computational Science Methods Div.; Goldberg, D.E. [Univ. of Illinois, Urbana, IL (United States). Dept. of General Engineering

    1996-05-01T23:59:59.000Z

    The SEARCH (Search Envisioned As Relation and Class Hierarchizing) framework developed elsewhere (Kargupta, 1995; Kargupta and Goldberg, 1995) offered an alternate perspective toward blackbox optimization -- optimization in presence of little domain knowledge. The SEARCH framework investigates the conditions essential for transcending the limits of random enumerative search using a framework developed in terms of relations, classes and partial ordering. This paper presents a summary of some of the main results of that work. A closed form bound on the sample complexity in terms of the cardinality of the relation space, class space, desired quality of the solution and the reliability is presented. This also leads to the identification of the class of order-k delineable problems that can be solved in polynomial sample complexity. These results are applicable to any blackbox search algorithms, including evolutionary optimization techniques.

  1. Transuranic waste characterization sampling and analysis plan

    SciTech Connect (OSTI)

    NONE

    1994-12-31T23:59:59.000Z

    Los Alamos National Laboratory (the Laboratory) is located approximately 25 miles northwest of Santa Fe, New Mexico, situated on the Pajarito Plateau. Technical Area 54 (TA-54), one of the Laboratory`s many technical areas, is a radioactive and hazardous waste management and disposal area located within the Laboratory`s boundaries. The purpose of this transuranic waste characterization, sampling, and analysis plan (CSAP) is to provide a methodology for identifying, characterizing, and sampling approximately 25,000 containers of transuranic waste stored at Pads 1, 2, and 4, Dome 48, and the Fiberglass Reinforced Plywood Box Dome at TA-54, Area G, of the Laboratory. Transuranic waste currently stored at Area G was generated primarily from research and development activities, processing and recovery operations, and decontamination and decommissioning projects. This document was created to facilitate compliance with several regulatory requirements and program drivers that are relevant to waste management at the Laboratory, including concerns of the New Mexico Environment Department.

  2. Well purge and sample apparatus and method

    DOE Patents [OSTI]

    Schalla, R.; Smith, R.M.; Hall, S.H.; Smart, J.E.; Gustafson, G.S.

    1995-10-24T23:59:59.000Z

    The present invention specifically permits purging and/or sampling of a well but only removing, at most, about 25% of the fluid volume compared to conventional methods and, at a minimum, removing none of the fluid volume from the well. The invention is an isolation assembly with a packer, pump and exhaust, that is inserted into the well. The isolation assembly is designed so that only a volume of fluid between the outside diameter of the isolation assembly and the inside diameter of the well over a fluid column height from the bottom of the well to the top of the active portion (lower annulus) is removed. The packer is positioned above the active portion thereby sealing the well and preventing any mixing or contamination of inlet fluid with fluid above the packer. Ports in the wall of the isolation assembly permit purging and sampling of the lower annulus along the height of the active portion. 8 figs.

  3. Well purge and sample apparatus and method

    DOE Patents [OSTI]

    Schalla, Ronald (Kennewick, WA); Smith, Ronald M. (Richland, WA); Hall, Stephen H. (Kennewick, WA); Smart, John E. (Richland, WA); Gustafson, Gregg S. (Redmond, WA)

    1995-01-01T23:59:59.000Z

    The present invention specifically permits purging and/or sampling of a well but only removing, at most, about 25% of the fluid volume compared to conventional methods and, at a minimum, removing none of the fluid volume from the well. The invention is an isolation assembly with a packer, pump and exhaust, that is inserted into the well. The isolation assembly is designed so that only a volume of fluid between the outside diameter of the isolation assembly and the inside diameter of the well over a fluid column height from the bottom of the well to the top of the active portion (lower annulus) is removed. The packer is positioned above the active portion thereby sealing the well and preventing any mixing or contamination of inlet fluid with fluid above the packer. Ports in the wall of the isolation assembly permit purging and sampling of the lower annulus along the height of the active portion.

  4. Snake and Columbia Rivers Sediment Sampling Project

    SciTech Connect (OSTI)

    Pinza, M.R.; Word, J.Q; Barrows, E.S.; Mayhew, H.L.; Clark, D.R. (Battelle/Marine Sciences Lab., Sequim, WA (United States))

    1992-12-01T23:59:59.000Z

    The disposal of dredged material in water is defined as a discharge under Section 404 of the Clean Water Act and must be evaluated in accordance with US Environmental Protection Agency regulation 40 CFR 230. Because contaminant loads in the dredged sediment or resuspended sediment may affect water quality or contaminant loading, the US Army Corps of Engineers (USACE), Walla Walla District, has requested Battelle/Marine Sciences Laboratory to collect and chemically analyze sediment samples from areas that may be dredged near the Port Authority piers on the Snake and Columbia rivers. Sediment samples were also collected at River Mile (RM) stations along the Snake River that may undergo resuspension of sediment as a result of the drawdown. Chemical analysis included grain size, total organic carbon, total volatile solids, ammonia, phosphorus, sulfides, oil and grease, total petroleum hydrocarbons, metals, polynuclear aromatic hydrocarbons, pesticides, polychlorinated biphenyls, and 21 congeners of polychlorinated dibenzodioxins and dibenzofurans.

  5. SAMPLE RESULTS FROM THE INTEGRATED SALT DISPOSITION PROGRAM MACROBATCH 5 TANK 21H QUALIFICATION SAMPLES

    SciTech Connect (OSTI)

    Peters, T.; Fink, S.

    2012-03-26T23:59:59.000Z

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H in support of qualification of Macrobatch (Salt Batch) 5 for the Integrated Salt Disposition Project (ISDP). This document reports partial results of the analyses of samples of Tank 21H. No issues with the projected Salt Batch 5 strategy are identified. Results of the analyses of the Tank 21H samples from this report in conjunction with the findings of the previous report, indicates that the material does not display any unusual characteristics.

  6. Sample and Implied Volatility in GARCH Models

    E-Print Network [OSTI]

    Kokoszka, Piotr

    Sample and Implied Volatility in GARCH Models Lajos Horva´th University of Utah Piotr Kokoszka Utah of various GARCH-type models is a function hðq� of the parameter vector q which is estimated by bq. For most distributions of the differences ^2 � hðq� and ^2 � hðbq� for broad classes of GARCH-type models. Even though

  7. Radiation absorption properties of different plaster samples

    SciTech Connect (OSTI)

    Akkurt, Iskender; Guenoglu, Kadir; Mavi, Betuel; K Latin-Small-Letter-Dotless-I l Latin-Small-Letter-Dotless-I ncarslan, Semsettin; Seven, Aysun [Suleyman Demirel University, Faculty of Arts and Sciences, Department of Physics, Isparta (Turkey); Amasya University, Faculty of Arts and Sciences, Department of Physics, Amasya (Turkey); Suleyman Demirel University, Faculty of Technical Education, Department of Construction Education, Isparta (Turkey)

    2012-09-06T23:59:59.000Z

    Although the plaster is one of the oldest known synthetic building materials, nowadays, it is used as interior coating of walls and ceilings of buildings. Thus measuring its radiation shielding properties is vital. For this purpose, radiation absorption properties of different plaster samples in this study. The measurements have been performed using gamma spectrometer system which connected to 3'' Multiplication-Sign 3''NaI (TI) detector.

  8. The IRAS Revised Bright Galaxy Sample (RBGS)

    E-Print Network [OSTI]

    Sanders, D B; Kim, D C; Surace, J A; Soifer, B T

    2003-01-01T23:59:59.000Z

    IRAS flux densities, redshifts, and infrared luminosities are reported for all sources identified in the IRAS Revised Bright Galaxy Sample (RBGS), a complete flux-limited survey of all extragalactic objects with total 60 micron flux density greater than 5.24 Jy, covering the entire sky surveyed by IRAS at Galactic latitude |b| > 5 degrees. The RBGS includes 629 objects, with a median (mean) sample redshift of 0.0082 (0.0126) and a maximum redshift of 0.0876. The RBGS supersedes the previous two-part IRAS Bright Galaxy Samples, which were compiled before the final ("Pass 3") calibration of the IRAS Level 1 Archive in May 1990. The RBGS also makes use of more accurate and consistent automated methods to measure the flux of objects with extended emission. Basic properties of the RBGS sources are summarized, including estimated total infrared luminosities, as well as updates to cross-identifications with sources from optical galaxy catalogs established using the NASA/IPAC Extragalactic Database (NED). In addition...

  9. Small Waste Tank Sampling and Retrieval System

    SciTech Connect (OSTI)

    Magleby, Mary Theresa

    2002-08-01T23:59:59.000Z

    At the Test Reactor Area of the Idaho National Engineering and Environmental Laboratory (INEEL), four 1500-gal catch tanks were found to contain RCRAhazardous waste. A system was needed to obtain a representative sample of the liquid, as well as the hardpacked heels, and to ultimately homogenize and remove the tank contents for disposal. After surveying the available technologies, the AEA Fluidic Pulse Mixing and Retrieval System was chosen for a technology demonstration. A demonstration, conducted with nonhazardous surrogate material, proved that the system was capable of loosening the hard-packed heel, homogenizing the entire tank contents, and collecting a representative sample. Based on the success of the demonstration, a detailed evaluation was done to determine the applicability of the system to other tanks. The evaluation included the sorting of data on more than 700 tanks to select candidates for further deployment of the system. A detailed study was also done to determine if the purchase of a second system would be cost effective. The results of the evaluation indicated that a total of thirteen tanks at the INEEL are amenable to sampling and/or remediation using the AEA Fluidic Pulse Mixing and Retrieval System. Although the currently-owned system appears sufficient for the needs of one INEEL program, it is insufficient to meet the combined needs at the INEEL. The INEEL will commence operation of the system on the TRA-730 Catch Tank System in June 2002.

  10. Gage for measuring displacements in rock samples

    DOE Patents [OSTI]

    Holcomb, David J. (Albuquerque, NM); McNamee, Michael J. (Albuquerque, NM)

    1986-01-01T23:59:59.000Z

    A gage for measuring diametral displacement within a rock sample for use in a rock mechanics laboratory and in the field, comprises a support ring housing a linear variable differential transformer, a mounting screw, and a leaf spring. The mounting screw is adjustable and defines a first point of contact with the rock sample. The leaf spring has opposite ends fixed to the inner periphery of the mounting ring. An intermediate portion of the leaf spring projecting radially inward from the ring is formed with a dimple defining a second point of contact with the sample. The first and second points of contact are diametrically opposed to each other. The LVDT is mounted in the ring with its axis parallel to the line of measurement and its core rod received in the dimple of the leaf spring. Any change in the length of the line between the first and second support points is directly communicated to the LVDT. The leaf spring is rigid to completely support lateral forces so that the LVDT is free of all load for improved precision.

  11. E-Print Network 3.0 - amniotic fluid samples Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    CLINICALCHEMISTRY,Vol. 24, No. 7, 1978 1131 Summary: ;N. normal amniotic fluid; 1'S, Tay-Sachs amniotic fluid. Four serial fourfold dilutions of each sample were... and the...

  12. E-Print Network 3.0 - air sampling system Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    system... in correlation to the air exchange rate and the sampling duration time for an ice rink arena. The theoretical ACH... higher values ( i.e. areas very close to the main...

  13. E-Print Network 3.0 - ash samples pressurized Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    group of seven fly ash samples, and have... of coal in conventional and or advanced clean coal technology combustors. These include fly ash, bottom... ash, boiler slag, and flue...

  14. E-Print Network 3.0 - acceptance sampling Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Liu, Fan Wang, Gagan Agrawal Summary: Adaptive Stratified Sampling for Data Mining on the Deep Web Tantan Liu, Fan Wang, Gagan Agrawal... - Acquiring data from the deep web is time...

  15. SAMPLE RESULTS FROM MCU SOLIDS OUTAGE

    SciTech Connect (OSTI)

    Peters, T.; Washington, A.; Oji, L.; Coleman, C.; Poirier, M.

    2014-09-22T23:59:59.000Z

    Savannah River National Laboratory (SRNL) has received several solid and liquid samples from MCU in an effort to understand and recover from the system outage starting on April 6, 2014. SRNL concludes that the presence of solids in the Salt Solution Feed Tank (SSFT) is the likely root cause for the outage, based upon the following discoveries ? A solids sample from the extraction contactor #1 proved to be mostly sodium oxalate ? A solids sample from the scrub contactor#1 proved to be mostly sodium oxalate ? A solids sample from the Salt Solution Feed Tank (SSFT) proved to be mostly sodium oxalate ? An archived sample from Tank 49H taken last year was shown to contain a fine precipitate of sodium oxalate ? A solids sample from the extraction contactor #1 drain pipe from extraction contactor#1 proved to be mostly sodium aluminosilicate ? A liquid sample from the SSFT was shown to have elevated levels of oxalate anion compared to the expected concentration in the feed Visual inspection of the SSFT indicated the presence of precipitated or transferred solids, which were likely also in the Salt Solution Receipt Tank (SSRT). The presence of the solids coupled with agitation performed to maintain feed temperature resulted in oxalate solids migration through the MCU system and caused hydraulic issues that resulted in unplanned phase carryover from the extraction into the scrub, and ultimately the strip contactors. Not only did this carryover result in the Strip Effluent (SE) being pushed out of waste acceptance specification, but it resulted in the deposition of solids into several of the contactors. At the same time, extensive deposits of aluminosilicates were found in the drain tube in the extraction contactor #1. However it is not known at this time how the aluminosilicate solids are related to the oxalate solids. The solids were successfully cleaned out of the MCU system. However, future consideration must be given to the exclusion of oxalate solids into the MCU system. There were 53 recommendations for improving operations recently identified. Some additional considerations or additional details are provided below as recommendations. ? From this point on, IC-Anions analyses of the DSSHT should be part of the monthly routine analysis in order to spot negative trends in the oxalate leaving the MCU system. Care must be taken to monitor the oxalate content to watch for sudden precipitation of oxalate salts in the system. ? Conduct a study to optimize the cleaning strategy at ARP-MCU through decreasing the concentration or entirely eliminating the oxalic acid. ? The contents of the SSFT should remain unagitated. Routine visual observation should be maintained to ensure there is not a large buildup of solids. As water with agitation provided sufficient removal of the solids in the feed tank, it should be considered as a good means for dissolving oxalate solids if they are found in the future. ? Conduct a study to improve prediction of oxalate solubility in salt batch feed materials. As titanium and mercury have been found in various solids in this report, evaluate if either element plays a role in oxalate solubility during processing. ? Salt batch characterization focuses primarily on characterization and testing of unaltered Tank 21H material; however, non-typical feeds are developed through cleaning, washing, and/or sump transfers. As these solutions are processed through MCU, they may precipitate solids or reduce performance. Salt batch characterization and testing should be expanded to encompass a broader range of feeds that may be processed through ARPMCU.

  16. Tank 241-C-111 headspace gas and vapor sample results - August 1993 samples

    SciTech Connect (OSTI)

    Huckaby, J.L.

    1994-11-14T23:59:59.000Z

    Tank 241-C-111 is on the ferrocyanide Watch List. Gas and vapor samples were collected to assure safe conditions before planned intrusive work was performed. Sample analyses showed that hydrogen is about ten times higher in the tank headspace than in ambient air. Nitrous oxide is about sixty times higher than ambient levels. The hydrogen cyanide concentration was below 0.04 ppbv, and the average NO{sub x} concentration was 8.6 ppmv.

  17. Can We Improve Over Weber Sampling of Haptic Amit Bhardwaj

    E-Print Network [OSTI]

    Dabeer, Onkar

    Can We Improve Over Weber Sampling of Haptic Signals? Amit Bhardwaj Dept. of Electrical Engineering an adaptive sampling scheme based on Weber's law of perception. In this paper, we explore other possible sampling schemes that improve over Weber sampling. I. INTRODUCTION As devices for sensing and rendering

  18. Aqueous samples from B-Plant, Tank 9-1

    SciTech Connect (OSTI)

    Bell, K.E.

    1995-01-13T23:59:59.000Z

    This document is the final report for the B-Plant Tank 9-1 sampling and analysis program. This report is divided into three parts: first, a narrative about the history, sampling effort, quality control, sample tracking/laboratory identification, and a summary of the analysis; second, sampling and custody data; and lastly, a set of compiled data from the laboratory analysis.

  19. Nebular mixing constrained by the Stardust samples

    SciTech Connect (OSTI)

    OGLIORE, R. C.; WESTPHAL, A. J.; GAINSFORTH, Z.; BUTTERWORTH, A. L.; FAKRA, S. C.; Marcus, Matthew A.

    2010-03-22T23:59:59.000Z

    Using X-ray microprobe analysis of samples from comet Wild 2 returned by the Stardust mission, we determine that the crystalline Fe-bearing silicate fraction in this Jupiter-family comet is greater than 0.5. Assuming this mixture is a composite of crystalline inner solar system material and amorphous cold molecular cloud material, we deduce that more than half of Wild 2 has been processed in the inner solar system. Several models exist that explain the presence of crystalline materials in comets. We explore some of these models in light of our results.

  20. Draft Sample Collection Instrument | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on Delicious Rank EERE:Year in Review: TopEnergy DOEDealingVehicle1 Closing the Circle: TheDraft Sample Collection

  1. Template:SampleTemplate | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on Office of InspectorConcentrating SolarElectric Coop, Inc Place:Innovation & Solutions HomeTeksunSampleTemplate Jump

  2. Radioactive Samples / Materials at the APS

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsrucLas ConchasPassive Solar HomePromising Science for1 20115,PerformanceUsing Radioactive Samples /

  3. LCLS Equipment Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample Environment: Magnet and6 th7525T HE F IRSTA3LCLS

  4. LCLS Prep Lab Images | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample Environment: Magnet and6 th7525T HE FLCLSLCLS Prep Lab

  5. Sample Projects - Combustion Energy Frontier Research Center

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsrucLas ConchasPassive Solar HomePromisingStoriesSANDIA1 0-SA-02and Technical InformationSample

  6. Category:Field Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on Office of InspectorConcentrating SolarElectricEnergyCTBarreis aCallahanWind FarmAdd a new Federal Oil and GasSampling

  7. Waste Sampling and Characterization Facility - Hanford Site

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsrucLasDelivered energy consumption byAbout Printable VersionProtective ActionsWasteSampling and

  8. Surface Gas Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home5b9fcbce19 No revisionEnvReviewNonInvasiveExplorationUT-g GrantAtlas (PACAOpenSummerside WindSolarSampling Jump to: navigation,

  9. Form:SampleForm | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home5b9fcbce19 NoPublicIDAPowerPlantSitingConstruction.pdfNotify98.pdf JumpFlixMapFile Jump to: navigation,SampleForm Jump to:

  10. Category:Gas Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home5b9fcbce19 NoPublic Utilities Address: 160Benin: EnergyBostonFacilityCascade SierraStatusGeothermalpower.jpgGas FluxGas Sampling

  11. Category:SamplePages | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on Office of Inspector GeneralDepartmentAUDIT REPORTOpenWendeGuoCatalyst Renewables Jump to:EnOpenEIThisSamplePages Jump

  12. Hoe Creek 1990 quarterly sampling cumulative report

    SciTech Connect (OSTI)

    Crader, S.E.; Huntington, G.S.

    1991-03-01T23:59:59.000Z

    Groundwater samples were collected and analyzed for benzene and for total phenols three times during 1990. This report summarizes the results of these sampling events and compares the results with those obtained in previous years. Possible further options for remediation of the Hoe Creek site was addressed. Three underground coal gasification (UCG) burns were performed by Lawrence Livermore National Laboratory for the US Department of Energy in 1976, 1977, and 1979 at the Hoe Creek site, which is about 20 miles south of Gillette, Wyoming. As a result of these burns, there has been considerable contamination of groundwater by various organic compounds. There have been three efforts at remediating this situation. In 1986 and again in 1987, contaminated water was pumped out, treated, and reinjected. In 1989, the water was pumped, treated, and sprayed into the atmosphere. Benzene and total phenols have been monitored at various monitoring wells as the site during 1990. The highest detected benzene concentration in 1990 was 220 {mu}g/L, and the highest total phenols concentration was 430 {mu}g/L. It is apparent that contamination is still above baseline levels, although the concentration of total phenols is far less than immediately after the burns. The burned coal seams are still releasing organic compounds into the groundwater that passes through them.

  13. On-line microdialysis sample cleanup for electrospray ionization mass spectrometry of nucleic acid samples

    SciTech Connect (OSTI)

    Liu, C.; Wu, Q.; Harms, A.C.; Smith, R.D. [Pacific Northwest National Lab., Richland, WA (United States)] [Pacific Northwest National Lab., Richland, WA (United States)

    1996-09-15T23:59:59.000Z

    A major limitation of electrospray ionization mass spectrometry (ESI-MS) for oligonucleotide analysis arises due to sodium adduction, a problem that increases with molecular weight. Sodium adduction can preclude useful measurements when limited sample sizes prevent off-line cleanup. A novel and generally useful on-line microdialysis technique is described for the rapid (nearly 1-5 min) DNA sample cleanup for ESI-MS. Mass spectra of oligonucleotides of different size and sequence showing no significant sodium adduct peaks were obtained using the on-line microdialysis system with sodium chloride concentrations as high as 250 mM. Signal-to-noise ratios were also greatly enhanced compared to direct infusion of the original samples. By using ammonium acetate as the dialysis buffer, it was also found that the noncovalent association of double-stranded oligonucleotides could be preserved during the microdialysis process, allowing analysis by ESI-MS. 33 refs., 6 figs.

  14. Time-domain sampling of x-ray pulses using an ultrafast sample response

    SciTech Connect (OSTI)

    Gaal, P.; Shayduk, R. [Helmholtz-Zentrum Berlin fuer Materialien und Energie GmbH, Wilhelm-Conrad-Roentgen Campus, BESSY II, Albert-Einstein-Str. 15, 12489 Berlin (Germany); Schick, D.; Herzog, M.; Bojahr, A.; Goldshteyn, J.; Navirian, H. A.; Leitenberger, W. [Institut fuer Physik und Astronomie, Universitaet Potsdam, Karl-Liebknecht-Str. 24-25, 14476 Potsdam (Germany); Vrejoiu, I. [Max-Planck-Institut fuer Mikrostrukturphysik, Weinberg 2, 06120 Halle (Germany); Khakhulin, D.; Wulff, M. [European Synchrotron Radiation Facility (ESRF), 6 rue Jules Horowitz, 38000 Grenoble (France); Bargheer, M. [Helmholtz-Zentrum Berlin fuer Materialien und Energie GmbH, Wilhelm-Conrad-Roentgen Campus, BESSY II, Albert-Einstein-Str. 15, 12489 Berlin (Germany); Institut fuer Physik und Astronomie, Universitaet Potsdam, Karl-Liebknecht-Str. 24-25, 14476 Potsdam (Germany)

    2012-12-10T23:59:59.000Z

    We employ the ultrafast response of a 15.4 nm thin SrRuO{sub 3} layer grown epitaxially on a SrTiO{sub 3} substrate to perform time-domain sampling of an x-ray pulse emitted from a synchrotron storage ring. Excitation of the sample with an ultrashort laser pulse triggers coherent expansion and compression waves in the thin layer, which turn the diffraction efficiency on and off at a fixed Bragg angle during 5 ps. This is significantly shorter than the duration of the synchrotron x-ray pulse of 100 ps. Cross-correlation measurements of the ultrafast sample response and the synchrotron x-ray pulse allow to reconstruct the x-ray pulse shape.

  15. GASOLINE VEHICLE EXHAUST PARTICLE SAMPLING STUDY

    SciTech Connect (OSTI)

    Kittelson, D; Watts, W; Johnson, J; Zarling, D Schauer,J Kasper, K; Baltensperger, U; Burtscher, H

    2003-08-24T23:59:59.000Z

    The University of Minnesota collaborated with the Paul Scherrer Institute, the University of Wisconsin (UWI) and Ricardo, Inc to physically and chemically characterize the exhaust plume from recruited gasoline spark ignition (SI) vehicles. The project objectives were: (1) Measure representative particle size distributions from a set of on-road SI vehicles and compare these data to similar data collected on a small subset of light-duty gasoline vehicles tested on a chassis dynamometer with a dilution tunnel using the Unified Drive Cycle, at both room temperature (cold start) and 0 C (cold-cold start). (2) Compare data collected from SI vehicles to similar data collected from Diesel engines during the Coordinating Research Council E-43 project. (3) Characterize on-road aerosol during mixed midweek traffic and Sunday midday periods and determine fleet-specific emission rates. (4) Characterize bulk- and size-segregated chemical composition of the particulate matter (PM) emitted in the exhaust from the gasoline vehicles. Particle number concentrations and size distributions are strongly influenced by dilution and sampling conditions. Laboratory methods were evaluated to dilute SI exhaust in a way that would produce size distributions that were similar to those measured during laboratory experiments. Size fractionated samples were collected for chemical analysis using a nano-microorifice uniform deposit impactor (nano-MOUDI). In addition, bulk samples were collected and analyzed. A mixture of low, mid and high mileage vehicles were recruited for testing during the study. Under steady highway cruise conditions a significant particle signature above background was not measured, but during hard accelerations number size distributions for the test fleet were similar to modern heavy-duty Diesel vehicles. Number emissions were much higher at high speed and during cold-cold starts. Fuel specific number emissions range from 1012 to 3 x 1016 particles/kg fuel. A simple relationship between number and mass emissions was not observed. Data were collected on-road to compare weekday with weekend air quality around the Twin Cities area. This portion of the study resulted in the development of a method to apportion the Diesel and SI contribution to on-road aerosol.

  16. Minutes of the 28th Annual Plutonium Sample Exchange Meeting. Part II: metal sample exchange

    SciTech Connect (OSTI)

    Not Available

    1984-01-01T23:59:59.000Z

    Contents of this publication include the following list of participating laboratories; agenda; attendees; minutes of October 25 and 26 meeting; and handout materials supplied by speakers. The handout materials cover the following: statistics and reporting; plutonium - chemical assay 100% minus impurities; americium neptunium, uranium, carbon and iron data; emission spectroscopy data; plutonium metal sample exchange; the calorimetry sample exchange; chlorine determination in plutonium metal using phyrohydrolysis; spectrophotometric determination of 238-plutonium in oxide; plutonium measurement capabilities at the Savannah River Plant; and robotics in radiochemical laboratory.

  17. Monte Carlo stratified source-sampling

    SciTech Connect (OSTI)

    Blomquist, R.N.; Gelbard, E.M.

    1997-09-01T23:59:59.000Z

    In 1995, at a conference on criticality safety, a special session was devoted to the Monte Carlo {open_quotes}eigenvalue of the world{close_quotes} problem. Argonne presented a paper, at that session, in which the anomalies originally observed in that problem were reproduced in a much simplified model-problem configuration, and removed by a version of stratified source-sampling. The original test-problem was treated by a special code designed specifically for that purpose. Recently ANL started work on a method for dealing with more realistic eigenvalue of the world configurations, and has been incorporating this method into VIM. The original method has been modified to take into account real-world statistical noise sources not included in the model problem. This paper constitutes a status report on work still in progress.

  18. Flow cytometric detection method for DNA samples

    DOE Patents [OSTI]

    Nasarabadi,Shanavaz (Livermore, CA); Langlois, Richard G. (Livermore, CA); Venkateswaran, Kodumudi S. (Round Rock, TX)

    2011-07-05T23:59:59.000Z

    Disclosed herein are two methods for rapid multiplex analysis to determine the presence and identity of target DNA sequences within a DNA sample. Both methods use reporting DNA sequences, e.g., modified conventional Taqman.RTM. probes, to combine multiplex PCR amplification with microsphere-based hybridization using flow cytometry means of detection. Real-time PCR detection can also be incorporated. The first method uses a cyanine dye, such as, Cy3.TM., as the reporter linked to the 5' end of a reporting DNA sequence. The second method positions a reporter dye, e.g., FAM.TM. on the 3' end of the reporting DNA sequence and a quencher dye, e.g., TAMRA.TM., on the 5' end.

  19. High throughput liquid absorption preconcentrator sampling instrument

    DOE Patents [OSTI]

    Zaromb, S.; Bozen, R.M.

    1992-12-22T23:59:59.000Z

    A system for detecting trace concentrations of an analyte in air includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container comprising a wettable material. The wettable material is continuously wetted with an analyte-sorbing liquid which flows from one part of the container to a lower end. Sampled air flows through the container in contact with the wetted material with a swirling motion which results in efficient transfer of analyte vapors or aerosol particles to the sorbing liquid and preconcentration of traces of analyte in the liquid. The preconcentrated traces of analyte may be either detected within the container or removed therefrom for injection into a separate detection means or for subsequent analysis. 12 figs.

  20. Extreme pressure fluid sample transfer pump

    DOE Patents [OSTI]

    Halverson, Justin E. (Grovertown, GA); Bowman, Wilfred W. (North Augusta, SC)

    1990-01-01T23:59:59.000Z

    A transfer pump for samples of fluids at very low or very high pressures comprising a cylinder having a piston sealed with an O-ring, the piston defining forward and back chambers, an inlet and exit port and valve arrangement for the fluid to enter and leave the forward chamber, and a port and valve arrangement in the back chamber for adjusting the pressure across the piston so that the pressure differential across the piston is essentially zero and approximately equal to the pressure of the fluid so that the O-ring seals against leakage of the fluid and the piston can be easily moved, regardless of the pressure of the fluid. The piston may be actuated by a means external to the cylinder with a piston rod extending through a hole in the cylinder sealed with a bellows attached to the piston head and the interior of the back chamber.

  1. Flow cytometric detection method for DNA samples

    DOE Patents [OSTI]

    Nasarabadi, Shanavaz (Livermore, CA); Langlois, Richard G. (Livermore, CA); Venkateswaran, Kodumudi S. (Livermore, CA)

    2006-08-01T23:59:59.000Z

    Disclosed herein are two methods for rapid multiplex analysis to determine the presence and identity of target DNA sequences within a DNA sample. Both methods use reporting DNA sequences, e.g., modified conventional Taqman.RTM. probes, to combine multiplex PCR amplification with microsphere-based hybridization using flow cytometry means of detection. Real-time PCR detection can also be incorporated. The first method uses a cyanine dye, such as, Cy3.TM., as the reporter linked to the 5' end of a reporting DNA sequence. The second method positions a reporter dye, e.g., FAM, on the 3' end of the reporting DNA sequence and a quencher dye, e.g., TAMRA, on the 5' end.

  2. Amphiphilic mediated sample preparation for micro-flow cytometry

    DOE Patents [OSTI]

    Clague, David S. (Livermore, CA); Wheeler, Elizabeth K. (Livermore, CA); Lee, Abraham P. (Irvine, CA)

    2006-07-25T23:59:59.000Z

    A flow cytometer includes a flow cell for detecting the sample, an oil phase in the flow cell, a water phase in the flow cell, an oil-water interface between the oil phase and the water phase, a detector for detecting the sample at the oil-water interface, and a hydrophobic unit operatively connected to the sample. The hydrophobic unit is attached to the sample. The sample and the hydrophobic unit are placed in an oil and water combination. The sample is detected at the interface between the oil phase and the water phase.

  3. Amphiphilic mediated sample preparation for micro-flow cytometry

    DOE Patents [OSTI]

    Clague, David S. (Livermore, CA); Wheeler, Elizabeth K. (Livermore, CA); Lee, Abraham P. (Irvine, CA)

    2009-03-17T23:59:59.000Z

    A flow cytometer includes a flow cell for detecting the sample, an oil phase in the flow cell, a water phase in the flow cell, an oil-water interface between the oil phase and the water phase, a detector for detecting the sample at the oil-water interface, and a hydrophobic unit operatively connected to the sample. The hydrophobic unit is attached to the sample. The sample and the hydrophobic unit are placed in an oil and water combination. The sample is detected at the interface between the oil phase and the water phase.

  4. Method and apparatus for imaging a sample on a device

    DOE Patents [OSTI]

    Trulson, Mark (Santa Clara, CA); Stern, David (Mountain View, CA); Fiekowsky, Peter (Los Altos, CA); Rava, Richard (Palo Alto, CA); Walton, Ian (Menlo Park, CA); Fodor, Stephen P. A. (Palo Alto, CA)

    2001-01-01T23:59:59.000Z

    A method and apparatus for imaging a sample are provided. An electromagnetic radiation source generates excitation radiation which is sized by excitation optics to a line. The line is directed at a sample resting on a support and excites a plurality of regions on the sample. Collection optics collect response radiation reflected from the sample I and image the reflected radiation. A detector senses the reflected radiation and is positioned to permit discrimination between radiation reflected from a certain focal plane in the sample and certain other planes within the sample.

  5. Apparatus for testing skin samples or the like

    DOE Patents [OSTI]

    Holland, J.M.

    1982-08-31T23:59:59.000Z

    An apparatus for testing the permeability of living skin samples has a flat base with a plurality of sample-holding cavities formed in its upper surface, the samples being placed in counterbores in the cavities with the epidermis uppermost. O-rings of Teflon washers are respectively placed on the samples and a flat cover is connected to the base to press the rings against the upper surfaces of the samples. Media to maintain tissue viability and recovery of metabolites is introduced into the lower portion of the sample-holding cavities through passages in the base. Test materials are introduced through holes in the cover plate after assembly of the chamber.

  6. On two-sample data analysis by exponential model

    E-Print Network [OSTI]

    Choi, Sujung

    2005-11-01T23:59:59.000Z

    of score functions, components, comparison distribution, comparison density and exponential model. Assume that we have a random sample X 1 ,???,X m from a continuous distribution F(y)=P(X i ? y),i =1,???,mand a random sample Y 1 ,???,Y n from a continuous... distribution G(y)=P(Y i ? y),i=1,???,n. Also as- sume independence of the two samples. The two-sample problem tests homogeneity of two samples and formally can be stated asH 0 : F = G. To solve the two-sample prob- lem, a number of tests have been proposed...

  7. Method and apparatus for processing a test sample to concentrate an analyte in the sample from a solvent in the sample

    DOE Patents [OSTI]

    Turner, T.D.; Beller, L.S.; Clark, M.L.; Klingler, K.M.

    1997-10-14T23:59:59.000Z

    A method of processing a test sample to concentrate an analyte in the sample from a solvent in the sample includes: (a) boiling the test sample containing the analyte and solvent in a boiling chamber to a temperature greater than or equal to the solvent boiling temperature and less than the analyte boiling temperature to form a rising sample vapor mixture; (b) passing the sample vapor mixture from the boiling chamber to an elongated primary separation tube, the separation tube having internal sidewalls and a longitudinal axis, the longitudinal axis being angled between vertical and horizontal and thus having an upper region and a lower region; (c) collecting the physically transported liquid analyte on the internal sidewalls of the separation tube; and (d) flowing the collected analyte along the angled internal sidewalls of the separation tube to and pass the separation tube lower region. The invention also includes passing a turbulence inducing wave through a vapor mixture to separate physically transported liquid second material from vaporized first material. Apparatus is also disclosed for effecting separations. Further disclosed is a fluidically powered liquid test sample withdrawal apparatus for withdrawing a liquid test sample from a test sample container and for cleaning the test sample container. 8 figs.

  8. Verification of the Accuracy of Sample-Size Equation Calculations for Visual Sample Plan Version 0.9C

    SciTech Connect (OSTI)

    Davidson, James R.

    2001-01-29T23:59:59.000Z

    Visual Sample Plan (VSP) is a software tool being developed to facilitate the design of environmental sampling plans using a site-map visual interface, standard sample-size equations, a variety of sampling grids and random sampling plans, and graphs to visually depict the results to the user. This document provides comparisons between sample sizes calculated by VSP Version 0.9C, and sample sizes calculated by test code written in the S-Plus language. All sample sizes calculated by VSP matched the independently calculated sample sizes. Also the VSP implementation of the ELIGPRID-PC algorithm for hot spot probabilities is shown to match previous results for 100 standard test cases. The Conclusions and Limitations section of this document lists some aspects of VSP that were not tested by this suite of tests and recommends simulation-based enhancements for future versions of VSP.

  9. SAMPLE RESULTS FROM THE INTEGRATED SALT DISPOSITION PROGRAM MACROBATCH 4 TANK 21H QUALIFICATION SAMPLES

    SciTech Connect (OSTI)

    Peters, T.; Fink, S.

    2011-06-22T23:59:59.000Z

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H to qualify them for use in the Integrated Salt Disposition Program (ISDP) Batch 4 processing. All sample results agree with expectations based on prior analyses where available. No issues with the projected Salt Batch 4 strategy are identified. This revision includes additional data points that were not available in the original issue of the document, such as additional plutonium results, the results of the monosodium titanate (MST) sorption test and the extraction, scrub strip (ESS) test. This report covers the revision to the Tank 21H qualification sample results for Macrobatch (Salt Batch) 4 of the Integrated Salt Disposition Program (ISDP). A previous document covers initial characterization which includes results for a number of non-radiological analytes. These results were used to perform aluminum solubility modeling to determine the hydroxide needs for Salt Batch 4 to prevent the precipitation of solids. Sodium hydroxide was then added to Tank 21 and additional samples were pulled for the analyses discussed in this report. This work was specified by Task Technical Request and by Task Technical and Quality Assurance Plan (TTQAP).

  10. Sampling for Beryllium Surface Contamination using Wet, Dry and Alcohol Wipe Sampling

    SciTech Connect (OSTI)

    Kerr, Kent

    2004-12-17T23:59:59.000Z

    This research project was conducted at the National Nuclear Security Administration's Kansas City Plant, operated by Honeywell Federal Manufacturing and Technologies, in conjunction with the Safety Sciences Department of Central Missouri State University, to compare relative removal efficiencies of three wipe sampling techniques currently used at Department of Energy facilities. Efficiencies of removal of beryllium contamination from typical painted surfaces were tested by wipe sampling with dry Whatman 42 filter paper, with water-moistened (Ghost Wipe) materials, and by methanol-moistened wipes. Test plates were prepared using 100 mm X 15 mm Pyrex Petri dishes with interior surfaces spray painted with a bond coat primer. To achieve uniform deposition over the test plate surface, 10 ml aliquots of solution containing 1 beryllium and 0.1 ml of metal working fluid were transferred to the test plates and subsequently evaporated. Metal working fluid was added to simulate the slight oiliness common on surfaces in metal working shops where fugitive oil mist accumulates over time. Sixteen test plates for each wipe method (dry, water, and methanol) were processed and sampled using a modification of wiping patterns recommended by OSHA Method 125G. Laboratory and statistical analysis showed that methanol-moistened wipe sampling removed significantly more (about twice as much) beryllium/oil-film surface contamination as water-moistened wipes (p< 0.001), which removed significantly more (about twice as much) residue as dry wipes (p <0.001). Evidence for beryllium sensitization via skin exposure argues in favor of wipe sampling with wetting agents that provide enhanced residue removal efficiency.

  11. Characterizing tensile loading responses of 3D printed samples

    E-Print Network [OSTI]

    Haid, Christopher M

    2014-01-01T23:59:59.000Z

    An experimental study was performed to characterize the loading response of samples manufactured through 3D printing. Tensile testing was performed on a number of 3D printed samples created through Fused Filament Fabrication ...

  12. Gas Sampling At Valles Caldera - Sulphur Springs Geothermal Area...

    Open Energy Info (EERE)

    and Janik, 1992). Hot spring gas samples were collected by submerging a 20-cm-diameter plastic funnel into the pool over the bubble stream. Fumarole gas samples were collected by...

  13. A rugged continuous air monitor for sampling radionuclides

    E-Print Network [OSTI]

    Martinez, Joseph Thaddeus

    2002-01-01T23:59:59.000Z

    A new rugged continuous air monitor (CAM) for sampling radionuclide has been developed. The sampler was designed for analyzing aerosols from occupied environments of laboratories and samples extracted from stacks and ducts. Experiments were...

  14. UMTRA project water sampling and analysis plan, Maybell, Colorado

    SciTech Connect (OSTI)

    Not Available

    1994-06-01T23:59:59.000Z

    This water sampling and analysis plan (WSAP) describes planned water sampling activities and provides the regulatory and technical basis for ground water sampling in 1994 at the US Department of Energy`s (DOE) Uranium Mill Tailings Remedial Action (UMTRA) Project site in Maybell, Colorado. The WSAP identifies and justifies sampling locations, analytical parameters, and sampling frequencies at the site. The ground water data will be used for site characterization and risk assessment. The regulatory basis for the ground water and surface water monitoring activities is derived from the EPA regulations in 40 CFR Part 192 (1993) and the proposed EPA standards of 1987 (52 FR 36000). Sampling procedures are guided by the UMTRA Project standard operating procedures (SOP) (JEG, n.d.), the Technical Approach Document (TAD) (DOE, 1989), and the most effective technical approach for the site. This WSAP also includes a summary and the results of water sampling activities from 1989 through 1992 (no sampling was performed in 1993).

  15. aggregate soil samples: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    and questionnaires for your own identification. Directions for obtaining soil samples Norton, Jay B. 35 Testing Your Soil: How to Collect and Send Samples Texas A&M University...

  16. Field Sampling Report -Water 2005 SFEI PRISM-Methods Development

    E-Print Network [OSTI]

    of aquatic toxicity by Pacific Eco-Risk (PER) (2 twenty-liter carboys). 2.2 Personnel The personnel and work transferred remaining samples to AMS in Livermore April 18, 2005 0800-1200 Mr. Salop shipped remaining samples

  17. Sampling Efficiency and Biodiversity Peter Neal & John Moriary

    E-Print Network [OSTI]

    Sidorov, Nikita

    Sampling Efficiency and Biodiversity Peter Neal & John Moriary First version: 9 June 2009 Research #12;Sampling efficiency and biodiversity Peter Neal and John Moriary June 9, 2009 1 Introduction Given

  18. Ris-R-620(M? An Intercomparison ofSampling

    E-Print Network [OSTI]

    5 1 Risø National Laboratory, Roskilde, Denmark 2 Radiation Protection Institute, Dublin, Ireland 3. The number of samples taken by each laboratory var- ied from one to five. The multiple sampling has given

  19. forEnvironmentalManagementofMilitaryLands Guide to Sampling Soil

    E-Print Network [OSTI]

    ....................................................................................................................................4 COMPACTION SAMPLING GUIDELINES resistance, which can be measured using a penetrometer much more rapidly that bulk density samples can to measure soil compaction because of their easy, rapid, and economical operation (Perumpral, 1987

  20. AN ADAPTIVE SAMPLING APPROACH TO INCOMPRESSIBLE PARTICLE-BASED FLUID

    E-Print Network [OSTI]

    Hong, Woo-Suck

    2010-01-16T23:59:59.000Z

    I propose a particle-based technique for simulating incompressible uid that includes adaptive re nement of particle sampling. Each particle represents a mass of uid in its local region. Particles are split into several particles for ner sampling...

  1. Water Sampling At Valles Caldera - Sulphur Springs Geothermal...

    Open Energy Info (EERE)

    Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Water Sampling At Valles Caldera - Sulphur Springs Geothermal Area (Trainer, 1974)...

  2. Volume 2 Appendices: Sample Solicitation and Contracting Document

    SciTech Connect (OSTI)

    Baechler, Michael C.

    2011-09-01T23:59:59.000Z

    Appendices for the report A Guide to Performance Contracting with ESCOs. The appendices include a sample solicitation and contracting document

  3. Manipulator for rotating and translating a sample holder

    DOE Patents [OSTI]

    van de Water, Jeroen (Breugel, NL); van den Oetelaar, Johannes (Eindhoven, NL); Wagner, Raymond (Gorinchem, NL); Slingerland, Hendrik Nicolaas (Venlo, NL); Bruggers, Jan Willem (Eindhoven, NL); Ottevanger, Adriaan Huibert Dirk (Malden, NL); Schmid, Andreas (Berkeley, CA); Olson, Eric A. (Champaign, IL); Petrov, Ivan G. (Champaign, IL); Donchev, Todor I. (Urbana, IL); Duden, Thomas (Kensington, CA)

    2011-02-08T23:59:59.000Z

    A manipulator for use in e.g. a Transmission Electron Microscope (TEM) is described, said manipulator capable of rotating and translating a sample holder (4). The manipulator clasps the round sample holder between two members (3A, 3B), said members mounted on actuators (2A, 2B). Moving the actuators in the same direction results in a translation of the sample holder, while moving the actuators in opposite directions results in a rotation of the sample holder.

  4. Optimization Online - Convergence analysis of sampling-based ...

    E-Print Network [OSTI]

    Vincent Guigues

    2014-08-19T23:59:59.000Z

    Aug 19, 2014 ... Convergence analysis of sampling-based decomposition methods for risk-averse multistage stochastic convex programs.

  5. Methods for characterizing, classifying, and identifying unknowns in samples

    DOE Patents [OSTI]

    Grate, Jay W [West Richland, WA; Wise, Barry M [Manson, WA

    2002-01-01T23:59:59.000Z

    Disclosed is a method for taking the data generated from an array of responses from a multichannel instrument, and determining the characteristics of a chemical in the sample without the necessity of calibrating or training the instrument with known samples containing the same chemical. The characteristics determined by the method are then used to classify and identify the chemical in the sample. The method can also be used to quantify the concentration of the chemical in the sample.

  6. Biomolecular Path Sampling Enabled by Processing in Network Storage

    E-Print Network [OSTI]

    Thain, Douglas

    parallel biomolec- ular sampling methods such as Folding@home [8] have been successfully mapped to grid

  7. arbitrarily distributed samples: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Distributed Transaction Management Parallel Database Systems Distributed Object DBMS Chen, Yangjun 405 Quantum Metropolis Sampling CERN Preprints Summary: Quantum...

  8. CHARACTERIZATION OF CORE SAMPLE COLLECTED FROM THE SALTSTONE DISPOSAL FACILITY

    SciTech Connect (OSTI)

    Cozzi, A.; Duncan, A.

    2010-01-28T23:59:59.000Z

    During the month of September 2008, grout core samples were collected from the Saltstone Disposal Facility, Vault 4, cell E. This grout was placed during processing campaigns in December 2007 from Deliquification, Dissolution and Adjustment Batch 2 salt solution. The 4QCY07 Waste Acceptance Criteria sample collected on 11/16/07 represents the salt solution in the core samples. Core samples were retrieved to initiate the historical database of properties of emplaced Saltstone and to demonstrate the correlation between field collected and laboratory prepared samples. Three samples were collected from three different locations. Samples were collected using a two-inch diameter concrete coring bit. In April 2009, the core samples were removed from the evacuated sample container, inspected, transferred to PVC containers, and backfilled with nitrogen. Samples furthest from the wall were the most intact cylindrically shaped cored samples. The shade of the core samples darkened as the depth of coring increased. Based on the visual inspection, sample 3-3 was selected for all subsequent analysis. The density and porosity of the Vault 4 core sample, 1.90 g/cm{sup 3} and 59.90% respectively, were comparable to values achieved for laboratory prepared samples. X-ray diffraction analysis identified phases consistent with the expectations for hydrated Saltstone. Microscopic analysis revealed morphology features characteristic of cementitious materials with fly ash and calcium silicate hydrate gel. When taken together, the results of the density, porosity, x-ray diffraction analysis and microscopic analysis support the conclusion that the Vault 4, Cell E core sample is representative of the expected waste form.

  9. Optimization of proteomic sample preparation procedures for comprehens...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    procedures for comprehensive protein characterization of pathogenic systems. Optimization of proteomic sample preparation procedures for comprehensive protein...

  10. DESIGN OF THE TRANSCONDUCTANCE AMPLIFIER FOR FREQUENCY DOMAIN SAMPLING RECEIVER

    E-Print Network [OSTI]

    Chen, XI

    2010-01-16T23:59:59.000Z

    degeneration circuit ...................... 31 3-5 (a) Simulated noise performance before source degeneration, (b) Simulated noise performance after source degeneration ...................... 32 3-6 Schematic of the high linear Gm... in Fig.2-6. The circuit is differential. ? ? ? Gm?? ? ? ? ? ? Sample Sample Sample Sample 1Out ? 1Out ? 2Out ? 2Out ? Interleaved output LNA ? ? ? ? Fig.2-6 The schematic of a single path 9 2-3. Noise and distortions...

  11. Free Energy Guided Sampling Ting Zhou and Amedeo Caflisch*

    E-Print Network [OSTI]

    Caflisch, Amedeo

    Free Energy Guided Sampling Ting Zhou and Amedeo Caflisch* Department of Biochemistry, University of Zurich, CH-8057 Zurich, Switzerland *S Supporting Information ABSTRACT: A free energy-guided sampling dynamics. Using the cut-based free energy profile and Markov state models, FEGS speeds up sampling

  12. physics/0512181 Modelling dynamics of samples exposed to

    E-Print Network [OSTI]

    not only the sample but also the optical elements of the FEL beamline. Radiation damage by photons from December 2005 Abstract: We apply Boltzmann equations for modelling the radiation damage in samples. Rapid progress of radiation damage in these samples prevents an accurate determination

  13. Blue Moon sampling, vectorial reaction coordinates, and unbiased constrained dynamics

    E-Print Network [OSTI]

    Van Den Eijnden, Eric

    Blue Moon sampling, vectorial reaction coordinates, and unbiased constrained dynamics Giovanni force in terms of a conditional expectation which can be computed by Blue Moon sampling Introduction Fifteen years ago the Blue Moon ensemble method was introduced to sample rare events that occur

  14. Training Samples in Objective Bayesian Model Selection 1

    E-Print Network [OSTI]

    West, Mike

    Training Samples in Objective Bayesian Model Selection 1 by James O. Berger Duke University North Central to several objective approaches to Bayesian model selection is the use of training samples prescription for choosing training samples is to choose them to be as small as possible, subject to yielding

  15. Sampling and Analysis Plan for PUREX canyon vessel flushing

    SciTech Connect (OSTI)

    Villalobos, C.N.

    1995-03-01T23:59:59.000Z

    A sampling and analysis plan is necessary to provide direction for the sampling and analytical activities determined by the data quality objectives. This document defines the sampling and analysis necessary to support the deactivation of the Plutonium-Uranium Extraction (PUREX) facility vessels that are regulated pursuant to Washington Administrative Code 173-303.

  16. Water Evaporation: A Transition Path Sampling Study

    E-Print Network [OSTI]

    Patrick Varilly; David Chandler

    2012-10-11T23:59:59.000Z

    We use transition path sampling to study evaporation in the SPC/E model of liquid water. Based on thousands of evaporation trajectories, we characterize the members of the transition state ensemble (TSE), which exhibit a liquid-vapor interface with predominantly negative mean curvature at the site of evaporation. We also find that after evaporation is complete, the distributions of translational and angular momenta of the evaporated water are Maxwellian with a temperature equal to that of the liquid. To characterize the evaporation trajectories in their entirety, we find that it suffices to project them onto just two coordinates: the distance of the evaporating molecule to the instantaneous liquid-vapor interface, and the velocity of the water along the average interface normal. In this projected space, we find that the TSE is well-captured by a simple model of ballistic escape from a deep potential well, with no additional barrier to evaporation beyond the cohesive strength of the liquid. Equivalently, they are consistent with a near-unity probability for a water molecule impinging upon a liquid droplet to condense. These results agree with previous simulations and with some, but not all, recent experiments.

  17. Brine Sampling and Evaluation Program, 1990 report

    SciTech Connect (OSTI)

    Deal, D.E.; Abitz, R.J.; Myers, J.; Case, J.B.; Martin, M.L.; Roggenthen, W.M. [International Technology Corp., Albuquerque, NM (United States)] [International Technology Corp., Albuquerque, NM (United States); Belski, D.S. [Westinghouse Electric Corp., Carlsbad, NM (United States). Waste Isolation Div.] [Westinghouse Electric Corp., Carlsbad, NM (United States). Waste Isolation Div.

    1991-08-01T23:59:59.000Z

    The data presented in this report are the result of Brine Sampling and Evaluation Program (BSEP) activities at the Waste Isolation Pilot Plant (WIPP) during 1990. When excavations began in 1982, small brine seepages (weeps) were observed on the walls. These brine occurrences were initially described as part of the Site Validation Program. Brine studies were formalized in 1985. The BSEP activities document and investigate the origins, hydraulic characteristics, extent, and composition of brine occurrences in the Permian Salado Formation and seepage of that brine into the excavations at the WIPP. The brine chemistry is important because it assists in understanding the origin of the brine and because it may affect possible chemical reactions in the buried waste after sealing the repository. The volume of brine and the hydrologic system that drives the brine seepage also need to be understood to assess the long-term performance of the repository. After more than eight years of observations (1982--1990), no credible evidence exists to indicate that enough naturally occurring brine will seep into the WIPP excavations to be of practical concern. The detailed observations and analyses summarized herein and in previous BSEP reports confirm the evidence apparent during casual visits to the underground workings -- that the excavations are remarkably dry.

  18. Brine Sampling and Evaluation Program, 1991 report

    SciTech Connect (OSTI)

    Deal, D.E.; Abitz, R.J.; Myers, J.; Martin, M.L.; Milligan, D.J.; Sobocinski, R.W.; Lipponer, P.P.J. [International Technology Corp., Albuquerque, NM (United States)] [International Technology Corp., Albuquerque, NM (United States); Belski, D.S. [Westinghouse Electric Corp., Carlsbad, NM (United States). Waste Isolation Div.] [Westinghouse Electric Corp., Carlsbad, NM (United States). Waste Isolation Div.

    1993-09-01T23:59:59.000Z

    The data presented in this report are the result of Brine Sampling and Evaluation Program (BSEP) activities at the Waste Isolation Pilot Plan (WIPP) during 1991. These BSEP activities document and investigate the origins, hydraulic characteristics, extent, and composition of brine occurrences in the Permian Salado Formation and seepage of that brine into the excavations at the WIPP. When excavations began at the WIPP in 1982, small brine seepages (weeps) were observed on the walls. Brine studies began as part of the Site Validation Program and were formalized as a program in its own right in 1985. During nine years of observations (1982--1991), evidence has mounted that the amount of brine seeping into the WIPP excavations is limited, local, and only a small fraction of that required to produce hydrogen gas by corroding the metal in the waste drums and waste inventory. The data through 1990 is discussed in detail and summarized by Deal and others (1991). The data presented in this report describes progress made during the calendar year 1991 and focuses on four major areas: (1) quantification of the amount of brine seeping across vertical surfaces in the WIPP excavations (brine ``weeps); (2) monitoring of brine inflow, e.g., measuring brines recovered from holes drilled downward from the underground drifts (downholes), upward from the underground drifts (upholes), and from subhorizontal holes; (3) further characterization of brine geochemistry; and (4) preliminary quantification of the amount of brine that might be released by squeezing the underconsolidated clays present in the Salado Formation.

  19. Liquid-absorption preconcentrator sampling instrument

    DOE Patents [OSTI]

    Zaromb, Solomon (Hinsdale, IL)

    1990-01-01T23:59:59.000Z

    A system for detecting trace concentrations of an analyte in air and includes a preconcentrator for the analyte and an analyte detector. The preconcentrator includes an elongated tubular container in which is disposed a wettable material extending substantially the entire length of the container. One end of the wettable material is continuously wetted with an analyte-sorbing liquid, which flows to the other end of the container. Sample air is flowed through the container in contact with the wetted material for trapping and preconcentrating the traces of analyte in the sorbing liquid, which is then collected at the other end of the container and discharged to the detector. The wetted material may be a wick comprising a bundle of fibers, one end of which is immersed in a reservoir of the analyte-sorbing liquid, or may be a liner disposed on the inner surface of the container, with the sorbing liquid being centrifugally dispersed onto the liner at one end thereof. The container is preferably vertically oriented so that gravity effects the liquid flow.

  20. Minfer: Inferring Motif Statistics From Sampled Edges

    E-Print Network [OSTI]

    Wang, Pinghui; Towsley, Don

    2015-01-01T23:59:59.000Z

    Characterizing motif (i.e., locally connected subgraph patterns) statistics is important for understanding complex networks such as online social networks and communication networks. Previous work made the strong assumption that the graph topology of interest is known, and that the dataset either fits into main memory or stored on disks such that it is not expensive to obtain all neighbors of any given node. In practice, researchers have to deal with the situation where the graph topology is unknown, either because the graph is dynamic, or because it is expensive to collect and store all topological and meta information on disk. Hence, what is available to researchers is only a snapshot of the graph generated by sampling edges from the graph at random, which we called a "RESampled graph". Clearly, a RESampled graph's motif statistics may be quite different from the underlying original graph. To solve this challenge, we propose a framework and implement a system called Minfer, which can take the given RESample...

  1. Sampling Artifacts from Conductive Silicone Tubing

    SciTech Connect (OSTI)

    Timko, Michael T.; Yu, Zhenhong; Kroll, Jesse; Jayne, John T.; Worsnop, Douglas R.; Miake-Lye, Richard C.; Onasch, Timothy B.; Liscinsky, David; Kirchstetter, Thomas W.; Destaillats, Hugo; Holder, Amara L.; Smith, Jared D.; Wilson, Kevin R.

    2009-05-15T23:59:59.000Z

    We report evidence that carbon impregnated conductive silicone tubing used in aerosol sampling systems can introduce two types of experimental artifacts: 1) silicon tubing dynamically absorbs carbon dioxide gas, requiring greater than 5 minutes to reach equilibrium and 2) silicone tubing emits organic contaminants containing siloxane that adsorb onto particles traveling through it and onto downstream quartz fiber filters. The consequence can be substantial for engine exhaust measurements as both artifacts directly impact calculations of particulate mass-based emission indices. The emission of contaminants from the silicone tubing can result in overestimation of organic particle mass concentrations based on real-time aerosol mass spectrometry and the off-line thermal analysis of quartz filters. The adsorption of siloxane contaminants can affect the surface properties of aerosol particles; we observed a marked reduction in the water-affinity of soot particles passed through conductive silicone tubing. These combined observations suggest that the silicone tubing artifacts may have wide consequence for the aerosol community and should, therefore, be used with caution. Gentle heating, physical and chemical properties of the particle carriers, exposure to solvents, and tubing age may influence siloxane uptake. The amount of contamination is expected to increase as the tubing surface area increases and as the particle surface area increases. The effect is observed at ambient temperature and enhanced by mild heating (<100 oC). Further evaluation is warranted.

  2. Microfluidic DNA sample preparation method and device

    DOE Patents [OSTI]

    Krulevitch, Peter A. (Pleasanton, CA); Miles, Robin R. (Danville, CA); Wang, Xiao-Bo (San Diego, CA); Mariella, Raymond P. (Danville, CA); Gascoyne, Peter R. C. (Bellaire, TX); Balch, Joseph W. (Livermore, CA)

    2002-01-01T23:59:59.000Z

    Manipulation of DNA molecules in solution has become an essential aspect of genetic analyses used for biomedical assays, the identification of hazardous bacterial agents, and in decoding the human genome. Currently, most of the steps involved in preparing a DNA sample for analysis are performed manually and are time, labor, and equipment intensive. These steps include extraction of the DNA from spores or cells, separation of the DNA from other particles and molecules in the solution (e.g. dust, smoke, cell/spore debris, and proteins), and separation of the DNA itself into strands of specific lengths. Dielectrophoresis (DEP), a phenomenon whereby polarizable particles move in response to a gradient in electric field, can be used to manipulate and separate DNA in an automated fashion, considerably reducing the time and expense involved in DNA analyses, as well as allowing for the miniaturization of DNA analysis instruments. These applications include direct transport of DNA, trapping of DNA to allow for its separation from other particles or molecules in the solution, and the separation of DNA into strands of varying lengths.

  3. Prospecting by sampling and analysis of airborne particulates and gases

    DOE Patents [OSTI]

    Sehmel, G.A.

    1984-05-01T23:59:59.000Z

    A method is claimed for prospecting by sampling airborne particulates or gases at a ground position and recording wind direction values at the time of sampling. The samples are subsequently analyzed to determine the concentrations of a desired material or the ratios of the desired material to other identifiable materials in the collected samples. By comparing the measured concentrations or ratios to expected background data in the vicinity sampled, one can select recorded wind directions indicative of the upwind position of the land-based source of the desired material.

  4. Multi-well sample plate cover penetration system

    DOE Patents [OSTI]

    Beer, Neil Reginald (Pleasanton, CA)

    2011-12-27T23:59:59.000Z

    An apparatus for penetrating a cover over a multi-well sample plate containing at least one individual sample well includes a cutting head, a cutter extending from the cutting head, and a robot. The cutting head is connected to the robot wherein the robot moves the cutting head and cutter so that the cutter penetrates the cover over the multi-well sample plate providing access to the individual sample well. When the cutting head is moved downward the foil is pierced by the cutter that splits, opens, and folds the foil inward toward the well. The well is then open for sample aspiration but has been protected from cross contamination.

  5. SAMPLING-BASED ROADMAP OF TREES FOR PARALLEL MOTION PLANNING 1 Sampling-Based Roadmap of Trees for Parallel

    E-Print Network [OSTI]

    Chen, Brian Y.

    SAMPLING-BASED ROADMAP OF TREES FOR PARALLEL MOTION PLANNING 1 Sampling-Based Roadmap of Trees for multiple query motion planning (Probabilistic Roadmap Method - PRM) with sampling-based tree methods algorithms, roadmap, tree, PRM, EST, RRT, SRT. I. INTRODUCTION HIGH-DIMENSIONAL problems such as those

  6. Optimal sampling efficiency in Monte Carlo sampling with an approximate potential

    SciTech Connect (OSTI)

    Coe, Joshua D [Los Alamos National Laboratory; Shaw, M Sam [Los Alamos National Laboratory; Sewell, Thomas D [U MISSOURI

    2009-01-01T23:59:59.000Z

    Building on the work of Iftimie et al., Boltzmann sampling of an approximate potential (the 'reference' system) is used to build a Markov chain in the isothermal-isobaric ensemble. At the endpoints of the chain, the energy is evaluated at a higher level of approximation (the 'full' system) and a composite move encompassing all of the intervening steps is accepted on the basis of a modified Metropolis criterion. For reference system chains of sufficient length, consecutive full energies are statistically decorrelated and thus far fewer are required to build ensemble averages with a given variance. Without modifying the original algorithm, however, the maximum reference chain length is too short to decorrelate full configurations without dramatically lowering the acceptance probability of the composite move. This difficulty stems from the fact that the reference and full potentials sample different statistical distributions. By manipulating the thermodynamic variables characterizing the reference system (pressure and temperature, in this case), we maximize the average acceptance probability of composite moves, lengthening significantly the random walk between consecutive full energy evaluations. In this manner, the number of full energy evaluations needed to precisely characterize equilibrium properties is dramatically reduced. The method is applied to a model fluid, but implications for sampling high-dimensional systems with ab initio or density functional theory (DFT) potentials are discussed.

  7. ENVIRONMENTAL SAMPLING AND ANALYSIS - GETTING IT RIGHT

    SciTech Connect (OSTI)

    CONNELL CW

    2008-01-22T23:59:59.000Z

    The Department of Energy's Hanford Site in southeastern Washington State was established in the 1940s as part of the Manhattan Project. Hanford's role was to produce weapons-grade nuclear material for defense, and by 1989, when the Site's mission changed from operations to cleanup, Hanford had produced more than 60 percent of the nation's plutonium. The legacy of Hanford's production years is enormous in terms of nuclear and hazardous waste, especially the 270 billion gallons of contaminated groundwater and the 5 million cubic yards of contaminated soil. Managing the contaminated soil and groundwater are particularly important because the Columbia River, the lifeblood of the northwest and the nation's eighth largest river, bounds the Site. Fluor Hanford's Soil & Groundwater Remediation Project (S&GRP) integrates all of the activities that deal with remediating and monitoring the groundwater across the Site. The S&GRP uses a detailed series of steps to record, track, and verify information. The Sample and Data Management (SDM) Process consists of 10 integrated steps that start with the data quality objectives process that establishes the mechanism for collecting the right information with the right people. The process ends with data quality assessment, which is used to ensure that all quantitative data (e.g., field screening, fixed laboratory) are the right type, and of adequate quality to support the decision-making process. Steps 3 through 10 of the process are production steps and are integrated electronically. The detailed plans, procedures, and systems used day-to-day by the SDM process require a high degree of accuracy and reliability. Tools must be incorporated into the processes that minimize errors. This paper discusses all of the elements of the SDM process in detail.

  8. Sample Self-Heating in the Portable Dilution Refrigerator Figure 1. Self-heating of a model sample in a dilution refrigerator. Sample temperature is

    E-Print Network [OSTI]

    Weston, Ken

    1 Sample Self-Heating in the Portable Dilution Refrigerator Figure 1. Self-heating of a model were curious as to what the internal temperature of the sample may have been as it was heating ~ 6 pW, self heating begins to occur. The most dramatic result of this test was that a temperature

  9. Robotic Deployment for Environmental Sampling Applications Dan O. Popa, Koushil Sreenath and Frank L. Lewis

    E-Print Network [OSTI]

    Sreenath, Koushil

    in oceanography and meteorology [Bennet2002]. The term adaptive sampling has been used to denote sampling

  10. Enhanced AFCI Sampling, Analysis, and Safeguards Technology Review

    SciTech Connect (OSTI)

    John Svoboda

    2009-09-01T23:59:59.000Z

    The focus of this study includes the investigation of sampling technologies used in industry and their potential application to nuclear fuel processing. The goal is to identify innovative sampling methods using state of the art techniques that could evolve into the next generation sampling and analysis system for metallic elements. Sampling and analysis of nuclear fuel recycling plant processes is required both to monitor the operations and ensure Safeguards and Security goals are met. In addition, environmental regulations lead to additional samples and analysis to meet licensing requirements. The volume of samples taken by conventional means, can restrain productivity while results samples are analyzed, require process holding tanks that are sized to meet analytical issues rather than process issues (and that create a larger facility footprint), or, in some cases, simply overwhelm analytical laboratory capabilities. These issues only grow when process flowsheets propose new separations systems and new byproduct material for transmutation purposes. Novel means of streamlining both sampling and analysis are being evaluated to increase the efficiency while meeting all requirements for information. This report addresses just a part of the effort to develop and study novel methods by focusing on the sampling and analysis of aqueous samples for metallic elements. It presents an overview of the sampling requirements, including frequency, sensitivity, accuracy, and programmatic drivers, to demonstrate the magnitude of the task. The sampling and analysis system needed for metallic element measurements is then discussed, and novel options being applied to other industrial analytical needs are presented. Inductively coupled mass spectrometry instruments are the most versatile for metallic element analyses and are thus chosen as the focus for the study. Candidate novel means of process sampling, as well as modifications that are necessary to couple such instruments to introduce these samples, are discussed. A suggested path forward based on an automated microchip capillary based sampling system interfaced to the analysis spectrometer is presented. The ability to obtain micro liter volume samples coupled with remote automated means of sample tracking and transport to the instrument would greatly improve analytical efficiency while reducing both personnel exposure and radioactive waste. Application of this sampling technique to new types of mass spectrometers for selective elemental isotopic analysis could also provide significant improvements in safeguards and security analyses.

  11. Sample handling for kinetics and molecular assembly in flow cytometry

    SciTech Connect (OSTI)

    Sklar, L.A. [Los Alamos National Lab., NM (United States). National Flow Cytometry Resource]|[Univ. of New Mexico, Albuquerque, NM (United States). School of Medicine; Seamer, L.C.; Kuckuck, F.; Prossnitz, E.; Edwards, B. [Univ. of New Mexico, Albuquerque, NM (United States). School of Medicine; Posner, G. [Northern Arizona Univ., Flagstaff, AZ (United States). Dept. of Chemistry

    1998-07-01T23:59:59.000Z

    Flow cytometry discriminates particle associated fluorescence from the fluorescence of the surrounding medium. It permits assemblies of macromolecular complexes on beads or cells to be detected in real-time with precision and specificity. The authors have investigated two types of robust sample handling systems which provide sub-second resolution and high throughput: (1) mixers which use stepper-motor driven syringes to initiate chemical reactions in msec time frames; and (2) flow injection controllers with valves and automated syringes used in chemical process control. In the former system, the authors used fast valves to overcome the disparity between mixing 100 {micro}ls of sample in 100 msecs and delivering sample to a flow cytometer at 1 {micro}l/sec. Particles were detected within 100 msec after mixing, but turbulence was created which lasted for 1 sec after injection of the sample into the flow cytometer. They used optical criteria to discriminate particles which were out of alignment due to the turbulent flow. Complex sample handling protocols involving multiple mixing steps and sample dilution have also been achieved. With the latter system they were able to automate sample handling and delivery with intervals of a few seconds. The authors used a fluidic approach to defeat turbulence caused by sample introduction. By controlling both sheath and sample with individual syringes, the period of turbulence was reduced to {approximately} 200 msecs. Automated sample handling and sub-second resolution should permit broad analytical and diagnostic applications of flow cytometry.

  12. Sample Results From The Interim Salt Disposition Program Macrobatch 7 Tank 21H Qualification Samples

    SciTech Connect (OSTI)

    Peters, T. B.; Washington, A. L. II

    2013-08-08T23:59:59.000Z

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H in support of qualification of Macrobatch (Salt Batch) 7 for the Interim Salt Disposition Program (ISDP). An ARP and several ESS tests were also performed. This document reports characterization data on the samples of Tank 21H as well as simulated performance of ARP/MCU. No issues with the projected Salt Batch 7 strategy are identified, other than the presence of visible quantities of dark colored solids. A demonstration of the monosodium titanate (0.2 g/L) removal of strontium and actinides provided acceptable 4 hour average decontamination factors for Pu and Sr of 3.22 and 18.4, respectively. The Four ESS tests also showed acceptable behavior with distribution ratios (D(Cs)) values of 15.96, 57.1, 58.6, and 65.6 for the MCU, cold blend, hot blend, and Next Generation Solvent (NGS), respectively. The predicted value for the MCU solvent was 13.2. Currently, there are no models that would allow a prediction of extraction behavior for the other three solvents. SRNL recommends that a model for predicting extraction behavior for cesium removal for the blended solvent and NGS be developed. While no outstanding issues were noted, the presence of solids in the samples should be investigated in future work. It is possible that the solids may represent a potential reservoir of material (such as potassium) that could have an impact on MCU performance if they were to dissolve back into the feed solution. This salt batch is intended to be the first batch to be processed through MCU entirely using the new NGS-MCU solvent.

  13. Calculating Confidence, Uncertainty, and Numbers of Samples When Using Statistical Sampling Approaches to Characterize and Clear Contaminated Areas

    SciTech Connect (OSTI)

    Piepel, Gregory F.; Matzke, Brett D.; Sego, Landon H.; Amidan, Brett G.

    2013-04-27T23:59:59.000Z

    This report discusses the methodology, formulas, and inputs needed to make characterization and clearance decisions for Bacillus anthracis-contaminated and uncontaminated (or decontaminated) areas using a statistical sampling approach. Specifically, the report includes the methods and formulas for calculating the • number of samples required to achieve a specified confidence in characterization and clearance decisions • confidence in making characterization and clearance decisions for a specified number of samples for two common statistically based environmental sampling approaches. In particular, the report addresses an issue raised by the Government Accountability Office by providing methods and formulas to calculate the confidence that a decision area is uncontaminated (or successfully decontaminated) if all samples collected according to a statistical sampling approach have negative results. Key to addressing this topic is the probability that an individual sample result is a false negative, which is commonly referred to as the false negative rate (FNR). The two statistical sampling approaches currently discussed in this report are 1) hotspot sampling to detect small isolated contaminated locations during the characterization phase, and 2) combined judgment and random (CJR) sampling during the clearance phase. Typically if contamination is widely distributed in a decision area, it will be detectable via judgment sampling during the characterization phrase. Hotspot sampling is appropriate for characterization situations where contamination is not widely distributed and may not be detected by judgment sampling. CJR sampling is appropriate during the clearance phase when it is desired to augment judgment samples with statistical (random) samples. The hotspot and CJR statistical sampling approaches are discussed in the report for four situations: 1. qualitative data (detect and non-detect) when the FNR = 0 or when using statistical sampling methods that account for FNR > 0 2. qualitative data when the FNR > 0 but statistical sampling methods are used that assume the FNR = 0 3. quantitative data (e.g., contaminant concentrations expressed as CFU/cm2) when the FNR = 0 or when using statistical sampling methods that account for FNR > 0 4. quantitative data when the FNR > 0 but statistical sampling methods are used that assume the FNR = 0. For Situation 2, the hotspot sampling approach provides for stating with Z% confidence that a hotspot of specified shape and size with detectable contamination will be found. Also for Situation 2, the CJR approach provides for stating with X% confidence that at least Y% of the decision area does not contain detectable contamination. Forms of these statements for the other three situations are discussed in Section 2.2. Statistical methods that account for FNR > 0 currently only exist for the hotspot sampling approach with qualitative data (or quantitative data converted to qualitative data). This report documents the current status of methods and formulas for the hotspot and CJR sampling approaches. Limitations of these methods are identified. Extensions of the methods that are applicable when FNR = 0 to account for FNR > 0, or to address other limitations, will be documented in future revisions of this report if future funding supports the development of such extensions. For quantitative data, this report also presents statistical methods and formulas for 1. quantifying the uncertainty in measured sample results 2. estimating the true surface concentration corresponding to a surface sample 3. quantifying the uncertainty of the estimate of the true surface concentration. All of the methods and formulas discussed in the report were applied to example situations to illustrate application of the methods and interpretation of the results.

  14. ARTIFACT FORMATION DURING NEUTRALIZATION OF TANK 50 SAMPLES

    SciTech Connect (OSTI)

    Crump, S.; Young, J.

    2014-08-01T23:59:59.000Z

    Degradation products have been identified in the extracts of Tank 50 samples analyzed by semivolatile organic compound analysis (SVOA) using gas chromatography/mass spectrometry (GC/MS). These materials, identified as short chain alkyl alcohols, were formed by acidification during sample preparation. A number of questions were raised about the formation of these and other materials reported in Tank 50 surface samples, and this report serves to address these questions.

  15. Zinc sorption by iron oxides and soil samples

    E-Print Network [OSTI]

    Yli-Halla, Markku Juhani

    1989-01-01T23:59:59.000Z

    (Head of Department) May 1989 ABSTRACT Zinc Sorption by Iron Oxides and Soil Samples. (May 1989) Markku Juhani Yli-Halla, M. S. University of Helsinki, Finland Chair of Advisory Committee: Dr. Richard H. Loeppert Zn sorption by synthetic Fe oxide... and soil samples was studied. The purpose was to examine the effect of crystallinity and adsorbed silica on Zn adsorption by synthetic Fe oxide using goethite and ferrihydrite as test materials. Zn sorption by acid soil samples from Finland and a...

  16. Characterization of Vadose Zone Sediment: Uncontaminated RCRA Borehole Core Samples and Composite Samples

    SciTech Connect (OSTI)

    Serne, R. Jeffrey; Bjornstad, Bruce N.; Schaef, Herbert T.; Williams, Bruce A.; Lanigan, David C.; Horton, Duane G.; Clayton, Ray E.; Mitroshkov, Alexandre V.; Legore, Virginia L.; O'Hara, Matthew J.; Brown, Christopher F.; Parker, Kent E.; Kutnyakov, Igor V.; Serne, Jennifer N.; Last, George V.; Smith, Steven C.; Lindenmeier, Clark W.; Zachara, John M.; Burke, Deborah S.

    2008-09-11T23:59:59.000Z

    This report was revised in September 2008 to remove acid-extractable sodium data from Tables 4.14, 4.16, 5.20, 5.22, 5.43, and 5.45. The sodium data was removed due to potential contamination introduced during the acid extraction process. The rest of the text remains unchanged from the original report issued in February 2002. The overall goal of the of the Tank Farm Vadose Zone Project, led by CH2M HILL Hanford Group, Inc., is to define risks from past and future single-shell tank farm activities. To meet this goal, CH2M HILL Hanford Group, Inc. asked scientists from Pacific Northwest National Laboratory to perform detailed analyses on vadose zone sediment from within the S-SX Waste Management Area. This report is one in a series of four reports to present the results of these analyses. Specifically, this report contains all the geologic, geochemical, and selected physical characterization data collected on vadose zone sediment recovered from Resource Conservation and Recovery Act (RCRA) borehole bore samples and composite samples.

  17. UNIVERSITY OF CALIFORNIA SAN DIEGO Sampled Simulation for Multithreaded Processors

    E-Print Network [OSTI]

    Sair, Suleyman

    . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 A. Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 18 1. Sample Starting; they made me possible. iv #12;EPIGRAPH Measure with a micrometer. Mark with a chalk. Cut with an axe. Ray

  18. NNSA implements nondestructive gas sampling technique for nuclear...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    implements ... NNSA implements nondestructive gas sampling technique for nuclear weapon components Posted: June 12, 2012 - 1:34pm The National Nuclear Security Administration...

  19. Soil separator and sampler and method of sampling

    DOE Patents [OSTI]

    O'Brien, Barry H. (Idaho Falls, ID) [Idaho Falls, ID; Ritter, Paul D. (Idaho Falls, ID) [Idaho Falls, ID

    2010-02-16T23:59:59.000Z

    A soil sampler includes a fluidized bed for receiving a soil sample. The fluidized bed may be in communication with a vacuum for drawing air through the fluidized bed and suspending particulate matter of the soil sample in the air. In a method of sampling, the air may be drawn across a filter, separating the particulate matter. Optionally, a baffle or a cyclone may be included within the fluidized bed for disentrainment, or dedusting, so only the finest particulate matter, including asbestos, will be trapped on the filter. The filter may be removable, and may be tested to determine the content of asbestos and other hazardous particulate matter in the soil sample.

  20. Soil Sampling At Waunita Hot Springs Geothermal Area (Ringrose...

    Open Energy Info (EERE)

    Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Soil Sampling At Waunita Hot Springs Geothermal Area (Ringrose & Pearl, 1981) Exploration...

  1. EFFECT OF TRANSPORTING SALTSTONE SAMPLES PRIOR TO SET

    SciTech Connect (OSTI)

    Reigel, M.

    2013-05-21T23:59:59.000Z

    The Saltstone Sampling and Analyses Plan provides a basis for the quantity (and configuration) of saltstone grout samples required for conducting a study directed towards correlation of the Performance Assessment (PA) related properties of field-emplaced samples and samples processed and cured in the laboratory. The testing described in the saltstone sampling and analyses plan will be addressed in phases. The initial testing (Phase I) includes collecting samples from the process room in the Saltstone Production Facility (SPF) and transporting them to Savannah River National Laboratory (SRNL) where they will cure under a temperature profile that mimics the temperature in the Saltstone Disposal Unit (SDU) and then be analyzed. SRNL has previously recommended that after the samples of fresh (uncured) saltstone are obtained from the SPF process room, they are allowed to set prior to transporting them to SRNL for curing. The concern was that if the samples are transported before they are set, the vibrations during transport may cause artificial delay of structure development which could result in preferential settling or segregation of the saltstone slurry. However, the results of this testing showed there was no clear distinction between the densities of the cylinder sections for any of the transportation scenarios tested (1 day, 1 hour, and 0 minutes set time prefer to transportation) . The bottom section of each cylinder was the densest for each transportation scenario, which indicates some settling in all the samples. Triplicate hydraulic conductivity measurements on samples from each set of time and transportation scenarios indicated that those samples transported immediately after pouring had the highest hydraulic conductivity. Conversely, samples that were allowed to sit for an hour before being transported had the lowest hydraulic conductivity. However, the hydraulic conductivities of all three samples fell within an acceptable range. Based on the cured property analysis of the three samples, there is no clear conclusion about transporting the samples before they are set; however, experience with saltstone grout indicates the samples should sit and develop some structure before being transported to SRNL for curing.

  2. Water Sampling At Valles Caldera - Sulphur Springs Geothermal...

    Open Energy Info (EERE)

    2) Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Water Sampling At Valles Caldera - Sulphur Springs Geothermal Area (Goff, Et Al., 1982)...

  3. Water Sampling At Valley Of Ten Thousand Smokes Region Area ...

    Open Energy Info (EERE)

    Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Water Sampling At Valley Of Ten Thousand Smokes Region Area (Keith, Et Al., 1992)...

  4. Water-Gas Samples At Valles Caldera - Redondo Geothermal Area...

    Open Energy Info (EERE)

    Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Water-Gas Samples At Valles Caldera - Redondo Geothermal Area (Janik & Goff, 2002)...

  5. Water Sampling At Valles Caldera - Redondo Geothermal Area (Goff...

    Open Energy Info (EERE)

    Water Sampling At Valles Caldera - Redondo Geothermal Area (Goff, Et Al., 1982) Exploration Activity Details Location Valles Caldera - Redondo Geothermal Area Exploration Technique...

  6. Water Sampling At Mt Princeton Hot Springs Geothermal Area (Olson...

    Open Energy Info (EERE)

    Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Water Sampling At Mt Princeton Hot Springs Geothermal Area (Olson & Dellechaie, 1976)...

  7. Water Sampling At Valles Caldera - Sulphur Springs Area (Rao...

    Open Energy Info (EERE)

    Jump to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Water Sampling At Valles Caldera - Sulphur Springs Area (Rao, Et Al., 1996) Exploration...

  8. Sample Questions | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    Regionals Middle School Rules, Forms, and Resources Sample Questions National Science Bowl (NSB) NSB Home About High School Middle School Middle School Students Middle...

  9. Sample Questions | U.S. DOE Office of Science (SC)

    Office of Science (SC) Website

    Regionals High School Rules, Forms, and Resources Sample Questions National Science Bowl (NSB) NSB Home About High School High School Students High School Coaches High...

  10. Nevada Sample Application for Permit Under Utility Environmental...

    Open Energy Info (EERE)

    Sample Application for Permit Under Utility Environmental Protection Act Jump to: navigation, search OpenEI Reference LibraryAdd to library PermittingRegulatory Guidance -...

  11. Rank test for multivariate two sample data using projection pursuit.

    E-Print Network [OSTI]

    Gunathilaka, Unawatuna Gamage

    2007-01-01T23:59:59.000Z

    ??Construction of an asymptotically distribution free test for the hypothesis that two multivariate random samples are identically distributed has been a topic among many statisticians… (more)

  12. ambient air sampling: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    of California eScholarship Repository Summary: chamber, passive sampling, passive solar house, measurementhouse, we planed the distribution of fresh air, passivepassive...

  13. Method and apparatus for imaging a sample on a device

    DOE Patents [OSTI]

    Trulson, Mark (Santa Clara, CA); Stern, David (Mountain View, CA); Fiekowsky, Peter (Los Altos, CA); Rava, Richard (Palo Alto, CA); Walton, Ian (Menlo Park, CA); Fodor, Stephen P. A. (Palo Alto, CA)

    1996-01-01T23:59:59.000Z

    The present invention provides methods and systems for detecting a labeled marker on a sample located on a support. The imaging system comprises a body for immobilizing the support, an excitation radiation source and excitation optics to generate and direct the excitation radiation at the sample. In response, labeled material on the sample emits radiation which has a wavelength that is different from the excitation wavelength, which radiation is collected by collection optics and imaged onto a detector which generates an image of the sample.

  14. Virtual experiments: Combining realistic neutron scattering instrument and sample simulations

    SciTech Connect (OSTI)

    Farhi, E. [Institut Laue Langevin, BP 156, 38042 Grenoble Cedex 9 (France)], E-mail: farhi@ill.fr; Hugouvieux, V. [INRA, UR1268 Biopolymeres Interactions Assemblages, F-44300 Nantes (France); Johnson, M.R. [Institut Laue Langevin, BP 156, 38042 Grenoble Cedex 9 (France); Kob, W. [Laboratoire des Colloides, Verres et Nanomateriaux, Universite Montpellier II, place E. Bataillon, 34095 Montpellier Cedex 5 (France)

    2009-08-01T23:59:59.000Z

    A new sample component is presented for the Monte Carlo, ray-tracing program, McStas, which is widely used to simulate neutron scattering instruments. The new component allows the sample to be described by its material dynamic structure factor, which is separated into coherent and incoherent contributions. The effects of absorption and multiple scattering are treated and results from simulations and previous experiments are compared. The sample component can also be used to treat any scattering material which may be close to the sample and therefore contaminates the total, measured signal.

  15. Geothermal: Sponsored by OSTI -- Testing and sampling procedures...

    Office of Scientific and Technical Information (OSTI)

    Testing and sampling procedures for geothermal-compressured wells. Final report Geothermal Technologies Legacy Collection HelpFAQ | Site Map | Contact Us HomeBasic Search About...

  16. Chapter 11, Sample Design Cross-Cutting Protocols: The Uniform...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Sample Mean to Estimate a Population Mean Evaluations often need to estimate the average energy consumption for particular equipment types, such as residential refrigeration. When...

  17. Surface Gas Sampling At Valles Caldera - Redondo Area (Goff ...

    Open Energy Info (EERE)

    to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Surface Gas Sampling At Valles Caldera - Redondo Area (Goff & Janik, 2002) Exploration Activity...

  18. Surface Gas Sampling At International Geothermal Area Mexico...

    Open Energy Info (EERE)

    to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Surface Gas Sampling At International Geothermal Area Mexico (Norman, Et Al., 2002) Exploration...

  19. Surface Gas Sampling At Valles Caldera - Sulphur Springs Area...

    Open Energy Info (EERE)

    Surface Gas Sampling At Valles Caldera - Sulphur Springs Area (Goff & Janik, 2002) Exploration Activity Details Location Valles Caldera - Sulphur Springs Area Exploration Technique...

  20. Surface Gas Sampling At Fenton Hill HDR Geothermal Area (Grigsby...

    Open Energy Info (EERE)

    to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Surface Gas Sampling At Fenton Hill HDR Geothermal Area (Grigsby, Et Al., 1983) Exploration...

  1. Surface Gas Sampling At Fenton Hill HDR Geothermal Area (Goff...

    Open Energy Info (EERE)

    to: navigation, search GEOTHERMAL ENERGYGeothermal Home Exploration Activity: Surface Gas Sampling At Fenton Hill HDR Geothermal Area (Goff & Janik, 2002) Exploration Activity...

  2. Rock Sampling At San Francisco Volcanic Field Area (Warpinski...

    Open Energy Info (EERE)

    geologically mapped the target area, obtained rock samples for age dating and mineral chemistry, performed gravity and magnetic surveys, and integrated these results to identify...

  3. Interpretation of Water Sample Analysis, Waunita Hot Spring Project...

    Open Energy Info (EERE)

    R. H. Carpenter (Colorado Geological Survey in Cooperation with the U.S. Department of Energy). 1981. Interpretation of Water Sample Analysis, Waunita Hot Spring Project,...

  4. aerosol samples collected: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    elements analysis of aerosol samples from some CiteSeer Summary: Aerosols deposits on filters from ten Romanian towns with different kinds and levels of industrial development...

  5. ancient geologic samples: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    superconducting quantum interference device SQUID-temperature RT sample scanning superconduct- ing quantum interference device SQUID microscopy SSM is a very Weiss, Benjamin P....

  6. Particulate Matter Sampling and Volatile Organic Compound Removal...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Organic Compound Removal for Characterization of Spark Ignited Direct Injection Engine Particulate Matter Sampling and Volatile Organic Compound Removal for Characterization...

  7. analyzing tissue samples: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    into an organization's structure and dynamics. The creation and analysis of sample social media network datasets is described to illustrate types of enterprise networks and...

  8. Solving Maximum-Entropy Sampling Problems Using Factored Masks

    E-Print Network [OSTI]

    Samuel Burer

    2005-03-02T23:59:59.000Z

    Mar 2, 2005 ... Abstract: We present a practical approach to Anstreicher and Lee's masked spectral bound for maximum-entropy sampling, and we describe ...

  9. A masked spectral bound for maximum-entropy sampling

    E-Print Network [OSTI]

    Kurt Anstreicher

    2003-09-16T23:59:59.000Z

    Sep 16, 2003 ... Abstract: We introduce a new masked spectral bound for the maximum-entropy sampling problem. This bound is a continuous generalization of ...

  10. anisotropic nmr samples: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    artifacts. Abbreviations: FFT fast Fourier transform; LP linear prediction; MEM maximum entropy method; SN signal-to-noise ratio unknown authors 24 Cryogenic sample...

  11. IBM Research Report Solving Maximum-Entropy Sampling ...

    E-Print Network [OSTI]

    2005-02-28T23:59:59.000Z

    Feb 28, 2005 ... Solving Maximum-Entropy Sampling Problems Using. Factored Masks. Samuel Burer. Department of Management Sciences. University of Iowa.

  12. Northern Marshall Islands radiological survey: sampling and analysis summary

    SciTech Connect (OSTI)

    Robison, W.L.; Conrado, C.L.; Eagle, R.J.; Stuart, M.L.

    1981-07-23T23:59:59.000Z

    A radiological survey was conducted in the Northern Marshall Islands to document reamining external gamma exposures from nuclear tests conducted at Enewetak and Bikini Atolls. An additional program was later included to obtain terrestrial and marine samples for radiological dose assessment for current or potential atoll inhabitants. This report is the first of a series summarizing the results from the terrestrial and marine surveys. The sample collection and processing procedures and the general survey methodology are discussed; a summary of the collected samples and radionuclide analyses is presented. Over 5400 samples were collected from the 12 atolls and 2 islands and prepared for analysis including 3093 soil, 961 vegetation, 153 animal, 965 fish composite samples (average of 30 fish per sample), 101 clam, 50 lagoon water, 15 cistern water, 17 groundwater, and 85 lagoon sediment samples. A complete breakdown by sample type, atoll, and island is given here. The total number of analyses by radionuclide are 8840 for /sup 241/Am, 6569 for /sup 137/Cs, 4535 for /sup 239 +240/Pu, 4431 for /sup 90/Sr, 1146 for /sup 238/Pu, 269 for /sup 241/Pu, and 114 each for /sup 239/Pu and /sup 240/Pu. A complete breakdown by sample category, atoll or island, and radionuclide is also included.

  13. C-104 Solid Phase Characterization of Sample 4C-13-1 From Tank 241-C-104 Closure Sampling Event

    SciTech Connect (OSTI)

    Cooke, Gary A.; Pestovich, John A.

    2013-06-12T23:59:59.000Z

    One solid grab sample from closure sampling in Riser 7 of tank 214-C-I04 (C-I04) was examined to determine the solid phases that were present. The sample was analyzed using X-ray diffraction (XRD) and scanning electron microscopy (SEM). The purpose of this analysis was to see if the presence of hydrated phases could provide a possible explanation for the high moisture content obtained from thermogravimetric analysis (TGA).

  14. 1. Introduction Obtaining valid reservoir fluid samples is

    E-Print Network [OSTI]

    Williams, John M.

    sampling in gas condensate wells, but this approach requires special small scale separation systems and possible financial penalties. For example, an oil sample which has lost some of its dissolved gas would have increased viscosity, and could lead to a reservoir appearing to be uneconomic to produce. A gas-condensate

  15. The Chemical Analysis of Argonne Premium Coal Samples

    E-Print Network [OSTI]

    Laughlin, Robert B.

    The Chemical Analysis of Argonne Premium Coal Samples U.S. GEOLOGICAL SURVEY BULLETIN 2144 #12 from the offices listed below. Detailed ordering instructions, along with prices of the last offerings OFFICE, WASHINGTON : 1997 The Chemical Analysis of Argonne Premium Coal Samples Edited by Curtis A

  16. Sample-Specific Cancer Pathway Analysis Using PARADIGM

    E-Print Network [OSTI]

    Benz, Stephen Charles

    2012-01-01T23:59:59.000Z

    across the OV sam- ples using IPA cuto? 3.3. Only HSP90AA1His- tograms of each sample’s IPA in FOXM1 or in any othersubnets found for a variety of IPA cuto?s. The red line rep-

  17. Standard Cross-Cultural Sample1 (updated September 2008)

    E-Print Network [OSTI]

    White, Douglas R.

    Standard Cross-Cultural Sample1 : on-line (updated September 2008) George P. Murdock and Douglas R. White University of Pittsburgh ABSTRACT: The Standard Cross-Cultural Sample contains the best also provides standard Galton's problem controls for historical nonindependence of cases

  18. Design unbiased estimation in line intersect sampling using segmented

    E-Print Network [OSTI]

    Design unbiased estimation in line intersect sampling using segmented transects D A V I D L . R applications of line intersect sampling, transects consist of multiple, connected segments in a prescribed, suitably generalized to segmented transect designs. The relative efficiency and utility of segmented

  19. Statistics and samples 1.1 What is statistics?

    E-Print Network [OSTI]

    Irwin, Darren

    1 1 Statistics and samples 1.1 What is statistics? Biologists study the properties of living things to get sam- pled and who did not. Statistics is a technology that describes and measures aspects of nature from samples. Most importantly, statistics lets us quantify the uncertainty of these meas- ures

  20. Statistical Model Criticism using Kernel Two Sample Tests

    E-Print Network [OSTI]

    Ghahramani, Zoubin

    Statistical Model Criticism using Kernel Two Sample Tests James Robert Lloyd Department Abstract We propose an exploratory approach to statistical model criticism using maximum mean discrepancy a statistic by which to measure discrepancies between data and a statistical model. MMD two sample tests

  1. Real-Time Texture Synthesis by Patch-Based Sampling

    E-Print Network [OSTI]

    Oliva, Aude

    well for a wide variety of textures ranging from regular to stochastic. By sampling patches according. Given an input sam- ple texture Iin, synthesize a texture Iout that is sufficiently different from the given sample texture, yet appears perceptually to be generated by the same underlying stochastic process

  2. Exact and Approximate Sampling by Systematic Stochastic Search

    E-Print Network [OSTI]

    Tenenbaum, Josh

    Exact and Approximate Sampling by Systematic Stochastic Search Vikash Mansinghka MIT BCS & CSAIL exact samples over high-dimensional spaces from exact sam- ples over lower-dimensional subspaces. Our do this by generalizing ideas from classic AI search to the stochastic setting. Just as systematic

  3. Inference in Successive Sampling Discovery Models Duke University

    E-Print Network [OSTI]

    West, Mike

    sample selection mechanisms, and other practical issues. Several analyses of published oil reserve data being sampled. Discovery of oil reserves is their central, very interesting example. The current paper of the other remaining units. In the oil discovery application of Nair and Wang (1989), for example, the four

  4. Cold Vacuum Drying Facility Stack Air Sampling System Qualification Tests

    SciTech Connect (OSTI)

    Glissmeyer, John A.

    2001-01-24T23:59:59.000Z

    This report documents tests that were conducted to verify that the air monitoring system for the Cold Vacuum Drying Facility ventilation exhaust stack meets the applicable regulatory criteria regarding the placement of the air sampling probe, sample transport, and stack flow measurement accuracy.

  5. RELATIONSHIP BETWEEN COMPOSITION AND TOXICITY OF ENGINE EMISSION SAMPLES

    SciTech Connect (OSTI)

    (1)Mauderly, J; Seagrave, J; McDonald; J (2)Eide,I (3)Zielinska, B (4)Lawson, D

    2003-08-24T23:59:59.000Z

    Differences in the lung toxicity and bacterial mutagenicity of seven samples from gasoline and diesel vehicle emissions were reported previously [1]. Filter and vapor-phase semivolatile organic samples were collected from normal and high-emitter gasoline and diesel vehicles operated on chassis dynamometers on the Unified Driving Cycle, and the compositions of the samples were measured in detail. The two fractions of each sample were combined in their original mass collection ratios, and the toxicity of the seven samples was compared by measuring inflammation and tissue damage in rat lungs and mutagenicity in bacteria. There was good agreement among the toxicity response variables in ranking the samples and demonstrating a five-fold range of toxicity. The relationship between chemical composition and toxicity was analyzed by a combination of principal component analysis (PCA) and partial least squares regression (PLS, also known as projection to latent surfaces). The PCA /PLS analysis revealed the chemical constituents co-varying most strongly with toxicity and produced models predicting the relative toxicity of the samples with good accuracy. The results demonstrated the utility of the PCA/PLS approach, which is now being applied to additional samples, and it also provided a starting point for confirming the compounds that actually cause the effects.

  6. Multivariate classification of infrared spectra of cell and tissue samples

    DOE Patents [OSTI]

    Haaland, David M. (Albuquerque, NM); Jones, Howland D. T. (Albuquerque, NM); Thomas, Edward V. (Albuquerque, NM)

    1997-01-01T23:59:59.000Z

    Multivariate classification techniques are applied to spectra from cell and tissue samples irradiated with infrared radiation to determine if the samples are normal or abnormal (cancerous). Mid and near infrared radiation can be used for in vivo and in vitro classifications using at least different wavelengths.

  7. Sampling Hay Bales and Pastures for Forage Analysis

    E-Print Network [OSTI]

    Provin, Tony; Pitt, John L.

    2002-05-03T23:59:59.000Z

    Forage analysis helps you know the nutritive value of forage and plan for any supplements that might be needed. To get an accurate analysis, hay and pastures must be sampled properly. In this publication you will learn how to sample both round...

  8. Probe for high resolution NMR with sample reorientation

    DOE Patents [OSTI]

    Pines, Alexander (Berkeley, CA); Samoson, Ago (Tallinn, SU)

    1990-01-01T23:59:59.000Z

    An improved NMR probe and method are described which substantially improve the resolution of NMR measurements made on powdered or amorphous or otherwise orientationally disordered samples. The apparatus mechanically varies the orientation of the sample such that the time average of two or more sets of spherical harmonic functions are zero.

  9. Probe for high resolution NMR with sample reorientation

    DOE Patents [OSTI]

    Pines, A.; Samoson, A.

    1990-02-06T23:59:59.000Z

    An improved NMR probe and method are described which substantially improve the resolution of NMR measurements made on powdered or amorphous or otherwise orientationally disordered samples. The apparatus mechanically varies the orientation of the sample such that the time average of two or more sets of spherical harmonic functions are zero. 8 figs.

  10. Asymmetric Nested Lattice Samples Peter Z. G. Qian1

    E-Print Network [OSTI]

    Qian, Peter Z. G.

    Asymmetric Nested Lattice Samples Peter Z. G. Qian1 , Mingyao Ai2,3 , Youngdeok Hwang1 and Heng Su4-filling designs, called asymmetric nested lattice samples. As a stepping-stone to the proposed approach, we introduce two methods for generating asymmetric nested orthogonal arrays. We then present two elaborate

  11. 384 Power plant waste water sampling and analysis plan

    SciTech Connect (OSTI)

    Hagerty, K.J.; Knotek, H.M.

    1995-01-01T23:59:59.000Z

    This document presents the 384 Power House Sampling and Analysis Plan. The Plan describes sampling methods, locations, frequency, analytes, and stream descriptions. The effluent streams from 384, were characterized in 1989, in support of the Stream Specific Report (WHC-EP-0342, Addendum 1).

  12. Application of Sampling Based Model Predictive Control to an Autonomous

    E-Print Network [OSTI]

    Collins, Emmanuel

    Unmanned Underwater Vehicles (UUVs) can be utilized to perform difficult tasks in cluttered environments55 Application of Sampling Based Model Predictive Control to an Autonomous Underwater Vehicle for an autonomous underwater vehicle (AUV). The algorithm combines the benefits of sampling-based motion planning

  13. RELIABILITY OF SAMPLING INSPECTION SCHEMES APPLIED TO REPLACEMENT STEAM GENERATORS

    E-Print Network [OSTI]

    Cizelj, Leon

    RELIABILITY OF SAMPLING INSPECTION SCHEMES APPLIED TO REPLACEMENT STEAM GENERATORS Guy Roussel the size of the random sample of tubes to be inspected in replacement steam generators is revisited in this paper. A procedure to estimate the maximum number of defective tubes left in the steam generator after

  14. Nevada National Security Site Integrated Groundwater Sampling Plan, Revision 0

    SciTech Connect (OSTI)

    Marutzky, Sam; Farnham, Irene

    2014-10-01T23:59:59.000Z

    The purpose of the Nevada National Security Site (NNSS) Integrated Sampling Plan (referred to herein as the Plan) is to provide a comprehensive, integrated approach for collecting and analyzing groundwater samples to meet the needs and objectives of the U.S. Department of Energy (DOE), National Nuclear Security Administration Nevada Field Office (NNSA/NFO) Underground Test Area (UGTA) Activity. Implementation of this Plan will provide high-quality data required by the UGTA Activity for ensuring public protection in an efficient and cost-effective manner. The Plan is designed to ensure compliance with the UGTA Quality Assurance Plan (QAP). The Plan’s scope comprises sample collection and analysis requirements relevant to assessing the extent of groundwater contamination from underground nuclear testing. This Plan identifies locations to be sampled by corrective action unit (CAU) and location type, sampling frequencies, sample collection methodologies, and the constituents to be analyzed. In addition, the Plan defines data collection criteria such as well-purging requirements, detection levels, and accuracy requirements; identifies reporting and data management requirements; and provides a process to ensure coordination between NNSS groundwater sampling programs for sampling of interest to UGTA. This Plan does not address compliance with requirements for wells that supply the NNSS public water system or wells involved in a permitted activity.

  15. Analysis Of The Tank 6F Final Characterization Samples-2012

    SciTech Connect (OSTI)

    Oji, L. N.; Diprete, D. P.; Coleman, C. J.; Hay, M. S.; Shine, E. P.

    2012-09-27T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm-243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

  16. ANALYSIS OF THE TANK 6F FINAL CHARACTERIZATION SAMPLES-2012

    SciTech Connect (OSTI)

    Oji, L.; Diprete, D.; Coleman, C.; Hay, M.; Shine, G.

    2012-06-28T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm-243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

  17. Analysis of the Tank 6F Final Characterization Samples-2012

    SciTech Connect (OSTI)

    Oji, L. N.; Diprete, D. P.; Coleman, C. J.; Hay, M. S.; Shine, E. P.

    2013-01-31T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm- 243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

  18. UMTRA project water sampling and analysis plan, Tuba City, Arizona

    SciTech Connect (OSTI)

    NONE

    1996-02-01T23:59:59.000Z

    Planned, routine ground water sampling activities at the U.S. Department of Energy (DOE) Uranium Mill Tailings Remedial Action (UMTRA) Project site in Tuba City, Arizona, are described in the following sections of this water sampling and analysis plan (WSAP). This plan identifies and justifies the sampling locations, analytical parameters, detection limits, and sampling frequency for the stations routinely monitored at the site. The ground water data are used for site characterization and risk assessment. The regulatory basis for routine ground water monitoring at UMTRA Project sites is derived from the U.S. Environmental Protection Agency (EPA) regulations in 40 CFR Part 192 (1994) and the final EPA standards of 1995 (60 FR 2854). Sampling procedures are guided by the UMTRA Project standard operating procedures (SOP) (JEG, n.d.), and the most effective technical approach for the site.

  19. UMTRA project water sampling and analysis plan -- Shiprock, New Mexico

    SciTech Connect (OSTI)

    Not Available

    1994-02-01T23:59:59.000Z

    Water sampling and analysis plan (WSAP) is required for each U.S. Department of Energy (DOE) Uranium Mill Tailings Remedial Action (UMTRA) Project site to provide a basis for ground water and surface water sampling at disposal and former processing sites. This WSAP identifies and justifies the sampling locations, analytical parameters, detection limits, and sampling frequency for the monitoring stations at the Navaho Reservation in Shiprock, New Mexico, UMTRA Project site. The purposes of the water sampling at Shiprock for fiscal year (FY) 1994 are to (1) collect water quality data at new monitoring locations in order to build a defensible statistical data base, (2) monitor plume movement on the terrace and floodplain, and (3) monitor the impact of alluvial ground water discharge into the San Juan River. The third activity is important because the community of Shiprock withdraws water from the San Juan River directly across from the contaminated alluvial floodplain below the abandoned uranium mill tailings processing site.

  20. Fluidics platform and method for sample preparation and analysis

    DOE Patents [OSTI]

    Benner, W. Henry; Dzenitis, John M.; Bennet, William J.; Baker, Brian R.

    2014-08-19T23:59:59.000Z

    Herein provided are fluidics platform and method for sample preparation and analysis. The fluidics platform is capable of analyzing DNA from blood samples using amplification assays such as polymerase-chain-reaction assays and loop-mediated-isothermal-amplification assays. The fluidics platform can also be used for other types of assays and analyzes. In some embodiments, a sample in a sealed tube can be inserted directly. The following isolation, detection, and analyzes can be performed without a user's intervention. The disclosed platform may also comprises a sample preparation system with a magnetic actuator, a heater, and an air-drying mechanism, and fluid manipulation processes for extraction, washing, elution, assay assembly, assay detection, and cleaning after reactions and between samples.

  1. Characterization of various bitumen samples from tar sands

    SciTech Connect (OSTI)

    Majid, A.; Bornais, J.; Hutchison, R.A. (National Research Council of Canada, Ottawa, ON (Canada). Div. of Chemistry)

    1989-01-01T23:59:59.000Z

    The authors have investigated twenty three bitumen samples obtained using different separation methods such as: ultracentrifugation, Dean-Stark extraction, solvent extraction employing vigorous agitation, hot water separation and the Solvent Extraction Spherical Agglomeration technique. These samples were extracted from oil sand feedstocks of different grades, Suncor sludge pond tailings and mineral agglomerates obtained form the Solvent Extraction Spherical Agglomeration process. All of the bitumen samples were examined on a comparative basis using various analytical techniques. These included: fractionation into asphaltenes and maltenes: elemental analyses; molecular weight determination using vapour pressure osmometry and gel permeation chromatography, infrared, proton and /sup 13/C nuclear magnetic resonance spectroscopy. Proton /sup 13/C n.m.r. spectroscopic data were used to determine the distribution of various types of hydrogens and carbons in the samples. These data were also used to derive various molecular parameters in order to investigate average molecular structures of different bitumen samples and some of their asphaltene fractions.

  2. Concepts for Environmental Radioactive Air Sampling and Monitoring

    SciTech Connect (OSTI)

    Barnett, J. M.

    2011-11-04T23:59:59.000Z

    Environmental radioactive air sampling and monitoring is becoming increasingly important as regulatory agencies promulgate requirements for the measurement and quantification of radioactive contaminants. While researchers add to the growing body of knowledge in this area, events such as earthquakes and tsunamis demonstrate how nuclear systems can be compromised. The result is the need for adequate environmental monitoring to assure the public of their safety and to assist emergency workers in their response. Two forms of radioactive air monitoring include direct effluent measurements and environmental surveillance. This chapter presents basic concepts for direct effluent sampling and environmental surveillance of radioactive air emissions, including information on establishing the basis for sampling and/or monitoring, criteria for sampling media and sample analysis, reporting and compliance, and continual improvement.

  3. Integrated fiducial sample mount and software for correlated microscopy

    SciTech Connect (OSTI)

    Timothy R McJunkin; Jill R. Scott; Tammy L. Trowbridge; Karen E. Wright

    2014-02-01T23:59:59.000Z

    A novel design sample mount with integrated fiducials and software for assisting operators in easily and efficiently locating points of interest established in previous analytical sessions is described. The sample holder and software were evaluated with experiments to demonstrate the utility and ease of finding the same points of interest in two different microscopy instruments. Also, numerical analysis of expected errors in determining the same position with errors unbiased by a human operator was performed. Based on the results, issues related to acquiring reproducibility and best practices for using the sample mount and software were identified. Overall, the sample mount methodology allows data to be efficiently and easily collected on different instruments for the same sample location.

  4. DOE methods for evaluating environmental and waste management samples.

    SciTech Connect (OSTI)

    Goheen, S C; McCulloch, M; Thomas, B L; Riley, R G; Sklarew, D S; Mong, G M; Fadeff, S K [eds.; Pacific Northwest Lab., Richland, WA (United States)

    1994-04-01T23:59:59.000Z

    DOE Methods for Evaluating Environmental and Waste Management Samples (DOE Methods) provides applicable methods in use by. the US Department of Energy (DOE) laboratories for sampling and analyzing constituents of waste and environmental samples. The development of DOE Methods is supported by the Laboratory Management Division (LMD) of the DOE. This document contains chapters and methods that are proposed for use in evaluating components of DOE environmental and waste management samples. DOE Methods is a resource intended to support sampling and analytical activities that will aid in defining the type and breadth of contamination and thus determine the extent of environmental restoration or waste management actions needed, as defined by the DOE, the US Environmental Protection Agency (EPA), or others.

  5. Self-contained cryogenic gas sampling apparatus and method

    DOE Patents [OSTI]

    McManus, G.J.; Motes, B.G.; Bird, S.K.; Kotter, D.K.

    1996-03-26T23:59:59.000Z

    Apparatus for obtaining a whole gas sample, is composed of: a sample vessel having an inlet for receiving a gas sample; a controllable valve mounted for controllably opening and closing the inlet; a valve control coupled to the valve for opening and closing the valve at selected times; a portable power source connected for supplying operating power to the valve control; and a cryogenic coolant in thermal communication with the vessel for cooling the interior of the vessel to cryogenic temperatures. A method is described for obtaining an air sample using the apparatus described above, by: placing the apparatus at a location at which the sample is to be obtained; operating the valve control to open the valve at a selected time and close the valve at a selected subsequent time; and between the selected times maintaining the vessel at a cryogenic temperature by heat exchange with the coolant. 3 figs.

  6. High-Throughput Mode Liquid Microjunction Surface Sampling Probe

    SciTech Connect (OSTI)

    Van Berkel, Gary J [ORNL; Kertesz, Vilmos [ORNL; King, Richard C. [PharmaCadence

    2009-01-01T23:59:59.000Z

    A simple and automated spot sampling operation mode for a liquid microjunction surface sampling probe/electrospray ionization mass spectrometry (LMJ-SSP/ESI-MS) system is reported. Prior manual and automated spot sampling methods with this probe relied on a careful, relatively slow alignment of the probe and surface distance (<20 m spacing) to form the probe-to-surface liquid microjunction critical to successful surface sampling. Moreover, sampling multiple spots required retraction of the surface from the probe and a repeat of this careful probe-to-surface distance alignment at the next sampling position. With the method described here, the probe was not positioned as close to the surface, the exact probeto-surface positioning was found to be less critical (spanning distances from about 100-300 m), and this distance was not altered during the sampling of an entire array of sample spots. With the probe positioned within the appropriate distance from the surface, the liquid microjunction was formed by letting the liquid from the sampling end of the probe extend out from the probe to the surface. This was accomplished by reducing the selfaspiration liquid flow rate of the probe to a value less than the volume flow rate pumped into the probe. When the self-aspiration rate of the probe was subsequently increased, analytes on the surface that dissolved at the liquid microjunction were aspirated back into the probe with the liquid that created the liquid microjunction and electrosprayed. Presented here are the basics of this new sampling mode, as well as data that illustrate the potential analytical capabilities of the device to conduct highthroughput quantitative analysis.

  7. Improved mesh based photon sampling techniques for neutron activation analysis

    SciTech Connect (OSTI)

    Relson, E.; Wilson, P. P. H.; Biondo, E. D. [University of Wisconsin-Madison, 1500 Engineering Drive, Madison, WI 53706 (United States)

    2013-07-01T23:59:59.000Z

    The design of fusion power systems requires analysis of neutron activation of large, complex volumes, and the resulting particles emitted from these volumes. Structured mesh-based discretization of these problems allows for improved modeling in these activation analysis problems. Finer discretization of these problems results in large computational costs, which drives the investigation of more efficient methods. Within an ad hoc subroutine of the Monte Carlo transport code MCNP, we implement sampling of voxels and photon energies for volumetric sources using the alias method. The alias method enables efficient sampling of a discrete probability distribution, and operates in 0(1) time, whereas the simpler direct discrete method requires 0(log(n)) time. By using the alias method, voxel sampling becomes a viable alternative to sampling space with the 0(1) approach of uniformly sampling the problem volume. Additionally, with voxel sampling it is straightforward to introduce biasing of volumetric sources, and we implement this biasing of voxels as an additional variance reduction technique that can be applied. We verify our implementation and compare the alias method, with and without biasing, to direct discrete sampling of voxels, and to uniform sampling. We study the behavior of source biasing in a second set of tests and find trends between improvements and source shape, material, and material density. Overall, however, the magnitude of improvements from source biasing appears to be limited. Future work will benefit from the implementation of efficient voxel sampling - particularly with conformal unstructured meshes where the uniform sampling approach cannot be applied. (authors)

  8. E-Print Network 3.0 - assessment databases measurements Sample...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Database... and Sampling Guide http:usda-ars.nmsu.edumonitassessmonitoring.php Limited version in Manual Volume II Yes... Sampling Guide Determine how many samples or...

  9. June 2010 Visual Sample Plan Version 6.03.1 3.0 Sampling Plan Development Within VSP

    E-Print Network [OSTI]

    a confidence interval on a mean and places them on the map. Locate Hot Spots Use systematic grid sampling a predetermined threshold and places them on the map. This is called a one-sample problem. Compare Average mean or median and places them on the map. This is typically used when a reference area has been

  10. Lavender Foal Syndrome Hair Sample Sheet Please tape hair samples within boxed area as illustrated and place in individual envelope.

    E-Print Network [OSTI]

    Keinan, Alon

    Lavender Foal Syndrome Hair Sample Sheet Please tape hair samples within boxed area as illustrated and place in individual envelope. *Pull 50 hairs from the tail or mane (do not use hairs shed on brush) #Hairs must be pulled, not cut #Hairs must contain hair root *Align the "roots" of the hairs and trim

  11. ANALYSIS OF THE TANK 5F FINAL CHARATERIZATION SAMPLES-2011

    SciTech Connect (OSTI)

    Oji, L.; Diprete, D.; Coleman, C.; Hay, M.

    2012-01-20T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by SRR to provide sample preparation and analysis of the Tank 5F final characterization samples to determine the residual tank inventory prior to grouting. Two types of samples were collected and delivered to SRNL: floor samples across the tank and subsurface samples from mounds near risers 1 and 5 of Tank 5F. These samples were taken from Tank 5F between January and March 2011. These samples from individual locations in the tank (nine floor samples and six mound Tank 5F samples) were each homogenized and combined in a given proportion into 3 distinct composite samples to mimic the average composition in the entire tank. These Tank 5F composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 5F composite samples include bulk density and water leaching of the solids to account for water soluble species. With analyses for certain challenging radionuclides as the exception, all composite Tank 5F samples were analyzed and reported in triplicate. The target detection limits for isotopes analyzed were based on customer desired detection limits as specified in the technical task request documents. SRNL developed new methodologies to meet these target detection limits and provide data for the extensive suite of components. While many of the target detection limits were met for the species characterized for Tank 5F, as specified in the technical task request, some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The Technical Task Request allows that while the analyses of these isotopes is needed, meeting the detection limits for these isotopes is a lower priority than meeting detection limits for the other specified isotopes. The isotopes whose detection limits were not met in all cases included the following: Al-26, Sn-126, Sb-126, Sb-126m, Eu-152 and Cf-249. SRNL, in conjunction with the plant customer, reviewed all these cases and determined that the impacts were negligible.

  12. SAMPLE RESULTS FROM THE INTEGRATED SALT DISPOSITION PROGRAM MACROBATCH 5 TANK 21H QUALIFICATION MST, ESS AND PODD SAMPLES

    SciTech Connect (OSTI)

    Peters, T.; Fink, S.

    2012-04-24T23:59:59.000Z

    Savannah River National Laboratory (SRNL) performed experiments on qualification material for use in the Integrated Salt Disposition Program (ISDP) Batch 5 processing. This qualification material was a composite created from recent samples from Tank 21H and archived samples from Tank 49H to match the projected blend from these two tanks. Additionally, samples of the composite were used in the Actinide Removal Process (ARP) and extraction-scrub-strip (ESS) tests. ARP and ESS test results met expectations. A sample from Tank 21H was also analyzed for the Performance Objectives Demonstration Document (PODD) requirements. SRNL was able to meet all of the requirements, including the desired detection limits for all the PODD analytes. This report details the results of the Actinide Removal Process (ARP), Extraction-Scrub-Strip (ESS) and Performance Objectives Demonstration Document (PODD) samples of Macrobatch (Salt Batch) 5 of the Integrated Salt Disposition Program (ISDP).

  13. MERCURY AND LEAD SAMPLING AT MINNESOTA POWER'S BOSWELL ENERGY CENTER

    SciTech Connect (OSTI)

    Dennis L. Laudal

    2000-08-01T23:59:59.000Z

    At the request of the Minnesota Power, Inc., the Energy & Environmental Research Center (EERC) sampled for lead at the stack (or duct directly leading to the stack) for three units at the Boswell Energy Center. All sampling was done in triplicate using U.S. Environmental Protection Agency (EPA) Method 12, with sampling procedures following EPA Methods 1 through 4. During the test program, lead sampling was done using EPA Method 12 in the duct at the outlet of the baghouse serving Unit 2 and the duct at the outlet of the wet particulate scrubber serving Unit 3. For Unit 4, lead sampling was done at the stack. The specific objective for the project was to determine the concentration of lead in the flue gas being emitted into the atmosphere from the Boswell Energy Center. The test program was performed during the period of May 8 through 11, 2000. This report presents the test data, sample calculations, and results, and a discussion of the lead sampling performed at the Boswell Energy Center. The detailed test data and test results, raw test data, process data, laboratory reports, and equipment calibration records are provided in Appendices A, B, and C.

  14. Standard practice for bulk sampling of liquid uranium hexafluoride

    E-Print Network [OSTI]

    American Society for Testing and Materials. Philadelphia

    2001-01-01T23:59:59.000Z

    1.1 This practice covers methods for withdrawing representative samples of liquid uranium hexafluoride (UF6) from bulk quantities of the material. Such samples are used for determining compliance with the applicable commercial specification, for example Specification C787 and Specification C996. 1.2 It is assumed that the bulk liquid UF6 being sampled comprises a single quality and quantity of material. This practice does not address any special additional arrangements that might be required for taking proportional or composite samples, or when the sampled bulk material is being added to UF6 residues already in a container (“heels recycle”). 1.3 The number of samples to be taken, their nominal sample weight, and their disposition shall be agreed upon between the parties. 1.4 The scope of this practice does not include provisions for preventing criticality incidents. 1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of th...

  15. Characterization Of Sample HTF-13-13-128

    SciTech Connect (OSTI)

    Pareizs, J. M.

    2013-09-25T23:59:59.000Z

    Savannah River Remediation (SRR) has requested that Savannah River National Laboratory (SRNL) characterize a sample of Tank 13 in preparation for Sludge Batch 9 (SB9). A 200 mL sample of Tank 13 was received by SRNL on July 22, 2013 (Tank Farm sample ID HTF-13-13-128). Characterization of the sample to meet the requirements of the request is complete. Results include: visual observations; slurry and supernatant density; weight percent total and insoluble solids; supernatant characterization; total alpha, total beta, and several radionuclide analyses; and elemental analyses of the dried solids. The sample was very fluid. After settling overnight, there was a small layer of solids on the bottom of the sample container (a 250 mL HDPE bottle) with the remainder being clear supernatant. To better show the sludge solids relative to the overall sample, 25 mL of slurry was placed in a graduated cylinder and allowed to settle over a weekend (approximately 90 hours). The sludge layer was at the approximately 4 mL. The small visually observed quantity of insoluble solids was confirmed with a low weight percent insoluble solids of 0.94%.

  16. Automatic sample Dewar for MX beam-line

    SciTech Connect (OSTI)

    Charignon, T.; Tanchon, J.; Trollier, T.; Ravex, A. [Absolut-System, Meylan, 38240 (France); Theveneau, P. [European Synchrotron Radiation Facility, Grenoble, 38000 (France)

    2014-01-29T23:59:59.000Z

    It is very common for crystals of large biological macromolecules to show considerable variation in quality of their diffraction. In order to increase the number of samples that are tested for diffraction quality before any full data collections at the ESRF*, an automatic sample Dewar has been implemented. Conception and performances of the Dewar are reported in this paper. The automatic sample Dewar has 240 samples capability with automatic loading/unloading ports. The storing Dewar is capable to work with robots and it can be integrated in a full automatic MX** beam-line. The samples are positioned in the front of the loading/unloading ports with and automatic rotating plate. A view port has been implemented for data matrix camera reading on each sample loaded in the Dewar. At last, the Dewar is insulated with polyurethane foam that keeps the liquid nitrogen consumption below 1.6 L/h. At last, the static insulation also makes vacuum equipment and maintenance unnecessary. This Dewar will be useful for increasing the number of samples tested in synchrotrons.

  17. Enhanced Sampling and Analysis, Selection of Technology for Testing

    SciTech Connect (OSTI)

    Svoboda, John; Meikrantz, David

    2010-02-01T23:59:59.000Z

    The focus of this study includes the investigation of sampling technologies used in industry and their potential application to nuclear fuel processing. The goal is to identify innovative sampling methods using state of the art techniques that could evolve into the next generation sampling and analysis system for metallic elements. This report details the progress made in the first half of FY 2010 and includes a further consideration of the research focus and goals for this year. Our sampling options and focus for the next generation sampling method are presented along with the criteria used for choosing our path forward. We have decided to pursue the option of evaluating the feasibility of microcapillary based chips to remotely collect, transfer, track and supply microliters of sample solutions to analytical equipment in support of aqueous processes for used nuclear fuel cycles. Microchip vendors have been screened and a choice made for the development of a suitable microchip design followed by production of samples for evaluation by ANL, LANL, and INL on an independent basis.

  18. Ad Hoc Sample Policy Accepting Samples from Private Citizens or NGOs. Our lab works with over 50 different partners across the political spectrum. One reason

    E-Print Network [OSTI]

    Ad Hoc Sample Policy ­ Accepting Samples from Private Citizens or NGOs. Our lab works with over 50 have enacted the following laboratory policy: All ad hoc samples (i.e., samples not part of an ongoing ask that if anyone is submitting an ad hoc sample to the lab they use the chain of custody form found

  19. EML Surface Air Sampling Program, 1990--1993 data

    SciTech Connect (OSTI)

    Larsen, R.J.; Sanderson, C.G.; Kada, J.

    1995-11-01T23:59:59.000Z

    Measurements of the concentrations of specific atmospheric radionuclides in air filter samples collected for the Environmental Measurements Laboratory`s Surface Air Sampling Program (SASP) during 1990--1993, with the exception of April 1993, indicate that anthropogenic radionuclides, in both hemispheres, were at or below the lower limits of detection for the sampling and analytical techniques that were used to collect and measure them. The occasional detection of {sup 137}Cs in some air filter samples may have resulted from resuspension of previously deposited debris. Following the April 6, 1993 accident and release of radionuclides into the atmosphere at a reprocessing plant in the Tomsk-7 military nuclear complex located 16 km north of the Siberian city of Tomsk, Russia, weekly air filter samples from Barrow, Alaska; Thule, Greenland and Moosonee, Canada were selected for special analyses. The naturally occurring radioisotopes that the authors measure, {sup 7}Be and {sup 210}Pb, continue to be detected in most air filter samples. Variations in the annual mean concentrations of {sup 7}Be at many of the sites appear to result primarily from changes in the atmospheric production rate of this cosmogenic radionuclide. Short-term variations in the concentrations of {sup 7}Be and {sup 210}Pb continued to be observed at many sites at which weekly air filter samples were analyzed. The monthly gross gamma-ray activity and the monthly mean surface air concentrations of {sup 7}Be, {sup 95}Zr, {sup 137}Cs, {sup 144}Ce, and {sup 210}Pb measured at sampling sites in SASP during 1990--1993 are presented. The weekly mean surface air concentrations of {sup 7}Be, {sup 95}Zr, {sup 137}Cs, {sup 144}Ce, and {sup 210}Pb for samples collected during 1990--1993 are given for 17 sites.

  20. Thermal modeling of core sampling in flammable gas waste tanks. Part 2: Rotary-mode sampling

    SciTech Connect (OSTI)

    Unal, C.; Poston, D.; Pasamehmetoglu, K.O. [Los Alamos National Lab., NM (United States). Nuclear Systems Design and Analysis Group; Witwer, K.S. [Westinghouse Hanford Co., Richland, WA (United States). Engineering Testing Lab.

    1997-08-01T23:59:59.000Z

    The radioactive waste stored in underground storage tanks at Hanford site includes mixtures of sodium nitrate and sodium nitrite with organic compounds. The waste can produce undesired violent exothermic reactions when heated locally during the rotary-mode sampling. Experiments are performed varying the downward force at a maximum rotational speed of 55 rpm and minimum nitrogen purge flow of 30 scfm. The rotary drill bit teeth-face temperatures are measured. The waste is simulated with a low thermal conductivity hard material, pumice blocks. A torque meter is used to determine the energy provided to the drill string. The exhaust air-chip temperature as well as drill string and drill bit temperatures and other key operating parameters were recorded. A two-dimensional thermal model is developed. The safe operating conditions were determined for normal operating conditions. A downward force of 750 at 55 rpm and 30 scfm nitrogen purge flow was found to yield acceptable substrate temperatures. The model predicted experimental results reasonably well. Therefore, it could be used to simulate abnormal conditions to develop procedures for safe operations.

  1. Stringent and efficient assessment of Boson-Sampling devices

    E-Print Network [OSTI]

    Malte C. Tichy; Klaus Mayer; Andreas Buchleitner; Klaus Mřlmer

    2014-07-11T23:59:59.000Z

    Boson-Sampling holds the potential to experimentally falsify the Extended Church Turing thesis. The computational hardness of Boson-Sampling, however, complicates the certification that an experimental device yields correct results in the regime in which it outmatches classical computers. To certify a boson-sampler, one needs to verify quantum predictions and rule out models that yield these predictions without true many-boson interference. We show that a semiclassical model for many-boson propagation reproduces coarse-grained observables that were proposed as witnesses of Boson-Sampling. A test based on Fourier matrices is demonstrated to falsify physically plausible alternatives to coherent many-boson propagation.

  2. Transuranic waste characterization sampling and analysis methods manual

    SciTech Connect (OSTI)

    NONE

    1995-05-01T23:59:59.000Z

    The Transuranic Waste Characterization Sampling and Analysis Methods Manual (Methods Manual) provides a unified source of information on the sampling and analytical techniques that enable Department of Energy (DOE) facilities to comply with the requirements established in the current revision of the Transuranic Waste Characterization Quality Assurance Program Plan (QAPP) for the Waste Isolation Pilot Plant (WIPP) Transuranic (TRU) Waste Characterization Program (the Program). This Methods Manual includes all of the testing, sampling, and analytical methodologies accepted by DOE for use in implementing the Program requirements specified in the QAPP.

  3. TRU Waste Sampling Program: Volume I. Waste characterization

    SciTech Connect (OSTI)

    Clements, T.L. Jr.; Kudera, D.E.

    1985-09-01T23:59:59.000Z

    Volume I of the TRU Waste Sampling Program report presents the waste characterization information obtained from sampling and characterizing various aged transuranic waste retrieved from storage at the Idaho National Engineering Laboratory and the Los Alamos National Laboratory. The data contained in this report include the results of gas sampling and gas generation, radiographic examinations, waste visual examination results, and waste compliance with the Waste Isolation Pilot Plant-Waste Acceptance Criteria (WIPP-WAC). A separate report, Volume II, contains data from the gas generation studies.

  4. Analysis report for 241-BY-104 auger samples

    SciTech Connect (OSTI)

    Beck, M.A.; Bechtold, D.B.; Hey, B.E.

    1992-10-26T23:59:59.000Z

    This document details the analytical sample results for two auger samples of the tip 15 cm (6 in.) of tank 241-BY-104 salt cake. The thermal response of tank 241-BY-104 auger samples is generally mild. The level of cyanide and iron, and therefore of ferrocyanide is very low. Evidence of inhomogeneity is present for tank 241-By-104 salt cake. Mass and charge balances were less than ideal. The concentrations found for the major constituents, except chromium, are in line with the expectations.

  5. High throughput analysis of samples in flowing liquid

    DOE Patents [OSTI]

    Ambrose, W. Patrick (Los Alamos, NM); Grace, W. Kevin (Los Alamos, NM); Goodwin, Peter M. (Los Alamos, NM); Jett, James H. (Los Alamos, NM); Orden, Alan Van (Fort Collins, CO); Keller, Richard A. (White Rock, NM)

    2001-01-01T23:59:59.000Z

    Apparatus and method enable imaging multiple fluorescent sample particles in a single flow channel. A flow channel defines a flow direction for samples in a flow stream and has a viewing plane perpendicular to the flow direction. A laser beam is formed as a ribbon having a width effective to cover the viewing plane. Imaging optics are arranged to view the viewing plane to form an image of the fluorescent sample particles in the flow stream, and a camera records the image formed by the imaging optics.

  6. Sample design for the residential energy consumption survey

    SciTech Connect (OSTI)

    Not Available

    1994-08-01T23:59:59.000Z

    The purpose of this report is to provide detailed information about the multistage area-probability sample design used for the Residential Energy Consumption Survey (RECS). It is intended as a technical report, for use by statisticians, to better understand the theory and procedures followed in the creation of the RECS sample frame. For a more cursory overview of the RECS sample design, refer to the appendix entitled ``How the Survey was Conducted,`` which is included in the statistical reports produced for each RECS survey year.

  7. Analytical Services Mass Spec. Analysis LC/MS and LC/MS/MS Sample Submission Form

    E-Print Network [OSTI]

    Crawford, T. Daniel

    the analysis. · Label all samples clearly with your name, date and the sample's ID. · You are responsible to this form! Desired Priority: [ ] Standard [ ] Rush Priority Ionization type: [ ] ESI (+) [ ] ESI only #Samples: ____ Priority: ____ #MSn : ____ Sample ID: ____ #Prep: ____ Receive date

  8. Groundwater Sampling and THOMAS HARTER is UC Cooperative Extension Hydrogeology Specialist, University of

    E-Print Network [OSTI]

    Pasternack, Gregory B.

    or for physical and chemical alteration of a sample due to inappropriate sample collection, transport, or storage Department of Health Services, which specifies minimum guidelines for sampling frequency and sampling

  9. E-Print Network 3.0 - adenocarcinomes du pancreas Sample Search...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    uniform sampling against adaptive sampling on the pancreas... to Figure 5, we see a comparison of uniform sampling against grid sampling on the pancreas case of Section 3 Source:...

  10. E-Print Network 3.0 - applications Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Engineering, University of Cambridge Collection: Engineering 5 SAMPLE TELEPHONE REFERENCE QUESTIONS Applicant's Name Summary: SAMPLE TELEPHONE REFERENCE QUESTIONS Applicant's Name:...

  11. E-Print Network 3.0 - application mnogofaznye anodnye Sample...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Collection: Engineering 5 SAMPLE TELEPHONE REFERENCE QUESTIONS Applicant's Name Summary: SAMPLE TELEPHONE REFERENCE QUESTIONS Applicant's Name: Position Applied For: Company...

  12. E-Print Network 3.0 - applications rozrobka tekhnologyiyi Sample...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Collection: Engineering 5 SAMPLE TELEPHONE REFERENCE QUESTIONS Applicant's Name Summary: SAMPLE TELEPHONE REFERENCE QUESTIONS Applicant's Name: Position Applied For: Company...

  13. Double Shell Tank (DST) Process Waste Sampling Subsystem Specification

    SciTech Connect (OSTI)

    RASMUSSEN, J.H.

    2000-05-03T23:59:59.000Z

    This specification establishes the performance requirements and provides references to the requisite codes and standards to be applied to the Double-Shell Tank (DST) Process Waste Sampling Subsystem which supports the first phase of Waste Feed Delivery.

  14. Soil Sampling At Long Valley Caldera Geothermal Area (Klusman...

    Open Energy Info (EERE)

    Activity Date - 1979 Usefulness useful DOE-funding Unknown Exploration Basis A1-horizon soil samples collected in the vicinity of the resurgent dome and a known geothermal source...

  15. Status of Baseline Sampling for Elements in Soil and Vegetation...

    Open Energy Info (EERE)

    Sampling for Elements in Soil and Vegetation at Four Kgra's in the Imperial Valley, California Jump to: navigation, search OpenEI Reference LibraryAdd to library Journal Article:...

  16. Testing Your Soil: How to Collect and Send Samples

    E-Print Network [OSTI]

    Provin, Tony; Pitt, John L.

    2002-06-26T23:59:59.000Z

    Soil tests can be used to estimate the kinds and amounts of soil nutrients available to plants and as aids in determining fertilizer needs. This publication covers the three-step procedure for obtaining sample bags and instructions, collecting...

  17. Department of Chemistry Mass Spectrometry Sample Submission Form

    E-Print Network [OSTI]

    Simons, Jack

    's ID. · You are responsible to pick up your samples within 7 days after the analysis. · Please call 801: [ ] Standard (LRMS) [ ] Exact Mass (HRMS) Ionization type: [ ] ESI [ ] MALDI [ ] EI (GC/MS only) Scans required

  18. Effect of sample disturbance in opalinus clay shales

    E-Print Network [OSTI]

    Pei, Jianyong, 1975-

    2004-01-01T23:59:59.000Z

    The sample disturbance problem for different geomaterials is reviewed in this thesis. A general discussion on the disturbance sources and complexities of the disturbance problem is followed by detailed reviews on disturbance ...

  19. B-Cell waste classification sampling and analysis plan

    SciTech Connect (OSTI)

    HOBART, R.L.

    1999-09-22T23:59:59.000Z

    This report documents the methods used to collect and analyze samples to obtain data necessary to verify and/or determine the radionuclide content of the 324 Facility B-Cell decontamination and decommissioning waste stream.

  20. ISOLOK VALVE ACCEPTANCE TESTING FOR DWPF SME SAMPLING PROCESS

    SciTech Connect (OSTI)

    Edwards, T.; Hera, K.; Coleman, C.; Jones, M.; Wiedenman, B.

    2011-12-05T23:59:59.000Z

    Evaluation of the Defense Waste Processing Facility (DWPF) Chemical Process Cell (CPC) cycle time identified several opportunities to improve the CPC processing time. Of the opportunities, a focus area related to optimizing the equipment and efficiency of the sample turnaround time for DWPF Analytical Laboratory was identified. The Mechanical Systems & Custom Equipment Development (MS&CED) Section of the Savannah River National Laboratory (SRNL) evaluated the possibility of using an Isolok{reg_sign} sampling valve as an alternative to the Hydragard{reg_sign} valve for taking process samples. Previous viability testing was conducted with favorable results using the Isolok sampler and reported in SRNL-STI-2010-00749 (1). This task has the potential to improve operability, reduce maintenance time and decrease CPC cycle time. This report summarizes the results from acceptance testing which was requested in Task Technical Request (TTR) HLW-DWPF-TTR-2010-0036 (2) and which was conducted as outlined in Task Technical and Quality Assurance Plan (TTQAP) SRNL-RP-2011-00145 (3). The Isolok to be tested is the same model which was tested, qualified, and installed in the Sludge Receipt Adjustment Tank (SRAT) sample system. RW-0333P QA requirements apply to this task. This task was to qualify the Isolok sampler for use in the DWPF Slurry Mix Evaporator (SME) sampling process. The Hydragard, which is the current baseline sampling method, was used for comparison to the Isolok sampling data. The Isolok sampler is an air powered grab sampler used to 'pull' a sample volume from a process line. The operation of the sampler is shown in Figure 1. The image on the left shows the Isolok's spool extended into the process line and the image on the right shows the sampler retracted and then dispensing the liquid into the sampling container. To determine tank homogeneity, a Coliwasa sampler was used to grab samples at a high and low location within the mixing tank. Data from the two locations were compared to determine if the contents of the tank were well mixed. The Coliwasa sampler is a tube with a stopper at the bottom and is designed to obtain grab samples from specific locations within the drum contents. A position paper (4) was issued to address the prototypic flow loop issues and simulant selections. A statistically designed plan (5) was issued to address the total number of samples each sampler needed to pull, to provide the random order in which samples were pulled and to group samples for elemental analysis. The TTR required that the Isolok sampler perform as well as the Hydragard sampler during these tests to ensure the acceptability of the Isolok sampler for use in the DWPF sampling cells. Procedure No.L9.4-5015 was used to document the sample parameters and process steps. Completed procedures are located in R&D Engineering job folder 23269.

  1. More Than 14 Million Environmental Sampling Records from National...

    Broader source: Energy.gov (indexed) [DOE]

    and about 300,000 samples. The data span a wide range of media including air, soil, sediment, biota, and water, and it includes various analytes and time periods. "The system was...

  2. Method and apparatus for sampling low-yield wells

    DOE Patents [OSTI]

    Last, George V. (Richland, WA); Lanigan, David C. (Kennewick, WA)

    2003-04-15T23:59:59.000Z

    An apparatus and method for collecting a sample from a low-yield well or perched aquifer includes a pump and a controller responsive to water level sensors for filling a sample reservoir. The controller activates the pump to fill the reservoir when the water level in the well reaches a high level as indicated by the sensor. The controller deactivates the pump when the water level reaches a lower level as indicated by the sensors. The pump continuously activates and deactivates the pump until the sample reservoir is filled with a desired volume, as indicated by a reservoir sensor. At the beginning of each activation cycle, the controller optionally can select to purge an initial quantity of water prior to filling the sample reservoir. The reservoir can be substantially devoid of air and the pump is a low volumetric flow rate pump. Both the pump and the reservoir can be located either inside or outside the well.

  3. Dose Rate Calculations for Rotary Mode Core Sampling Exhauster

    E-Print Network [OSTI]

    Foust, D J

    2000-01-01T23:59:59.000Z

    This document provides the calculated estimated dose rates for three external locations on the Rotary Mode Core Sampling (RMCS) exhauster HEPA filter housing, per the request of Characterization Field Engineering.

  4. Apparatus for preparing a sample for mass spectrometry

    DOE Patents [OSTI]

    Villa-Aleman, E.

    1994-05-10T23:59:59.000Z

    An apparatus is described for preparing a sample for analysis by a mass spectrometer system. The apparatus has an entry chamber and an ionization chamber separated by a skimmer. A capacitor having two space-apart electrodes followed by one or more ion-imaging lenses is disposed in the ionization chamber. The chamber is evacuated and the capacitor is charged. A valve injects a sample gas in the form of sample pulses into the entry chamber. The pulse is collimated by the skimmer and enters the ionization chamber. When the sample pulse passes through the gap between the electrodes, it discharges the capacitor and is thereby ionized. The ions are focused by the imaging lenses and enter the mass analyzer, where their mass and charge are analyzed. 1 figures.

  5. New approach to the fault location problem using synchronized sampling

    E-Print Network [OSTI]

    Mrkic, Jasna

    2012-06-07T23:59:59.000Z

    This thesis presents a new approach to solving the problem of fault location on a transmission line using synchronized data from both ends of the line. The synchronized phase voltage and current samples taken during the fault transient are used...

  6. Line search methods with variable sample size for unconstrained ...

    E-Print Network [OSTI]

    2011-06-27T23:59:59.000Z

    Jun 27, 2011 ... Key words: stochastic optimization, line search, simulations, sample average ...... Utility of agent i for alternative j is given by. Ui,j = Vi,j + ?i,j,.

  7. Embed and Project: Discrete Sampling with Universal Hashing

    E-Print Network [OSTI]

    Bejerano, Gill

    Embed and Project: Discrete Sampling with Universal Hashing Stefano Ermon, Carla P. Gomes Dept Markov Chain Monte Carlo (MCMC) methods. MCMC techniques are a specialized form of local search that only

  8. REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 1

    E-Print Network [OSTI]

    Minnesota, University of

    REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 1 DIESEL EXHAUST.D. and Megan Arnold University of Minnesota Department of Mechanical Engineering Center for Diesel Research....................................................................................... 3 Diesel aerosol size instrumentation............................................................ 4

  9. REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 2

    E-Print Network [OSTI]

    Minnesota, University of

    REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS Supplemental Report # 2 AEROSOL DYMAMICS Arnold University of Minnesota Department of Mechanical Engineering Center for Diesel Research................................................................................................. 3 Diesel aerosol composition and structure................................................... 3

  10. Instant Profiling: Instrumentation Sampling for Profiling Datacenter Applications

    E-Print Network [OSTI]

    Tomkins, Andrew

    Instant Profiling: Instrumentation Sampling for Profiling Datacenter Applications Hyoun Kyu Cho Profile-guided optimization possesses huge potential to save costs for datacenters. Hardware performance programmers find code regions to optimize by monitoring datacenter applications continuously on live traffic

  11. Micropyrolyzer for chemical analysis of liquid and solid samples

    DOE Patents [OSTI]

    Mowry, Curtis D. (Albuquerque, NM); Morgan, Catherine H. (Ann Arbor, MI); Manginell, Ronald P. (Albuquerque, NM); Frye-Mason, Gregory C. (Cedar Crest, NM)

    2006-07-18T23:59:59.000Z

    A micropyrolyzer has applications to pyrolysis, heated chemistry, and thermal desorption from liquid or solid samples. The micropyrolyzer can be fabricated from semiconductor materials and metals using standard integrated circuit technologies. The micropyrolyzer enables very small volume samples of less than 3 microliters and high sample heating rates of greater than 20.degree. C. per millisecond. A portable analyzer for the field analysis of liquid and solid samples can be realized when the micropyrolyzer is combined with a chemical preconcentrator, chemical separator, and chemical detector. Such a portable analyzer can be used in a variety of government and industrial applications, such as non-proliferation monitoring, chemical and biological warfare detection, industrial process control, water and air quality monitoring, and industrial hygiene.

  12. Sample Documents for On-Site Renewable Power Purchase Agreements

    Broader source: Energy.gov [DOE]

    The Federal Energy Management Program (FEMP) works with Federal agencies and partners to assemble sample documents from past on-site renewable power purchase agreement (PPA) projects to help streamline the PPA process.

  13. A Multi-Sample Cs-Sputter Negative Ion Source

    SciTech Connect (OSTI)

    Alton, G.D.; Ball, J.A.; Bao, Y.; Cui, B.; Reed, C.A.; Williams, C.

    1998-10-05T23:59:59.000Z

    A multi-sample Cs sputter negative-ion source, equipped with a conical-geometry, W-surface-ionizer has been designed and fabricated that permits sample changes without disruption of on-line accelerator operation. Sample changing is effected by actuating an electro-pneumatic control system located at ground potential that drives an air-motor-driven sample-indexing-system mounted at high voltage; this arrangement avoids complications associated with indexing mechanisms that rely on electronic power-supplies located at high potential. In-beam targets are identified by LED indicator lights derived from a fiber-optic, Gray-code target-position sensor. Aspects of the overall source design and details of the indexing mechanism along with operational parameters, ion optics. intensities, and typical emittances for a variety of negative-ion species will be presented in this report.

  14. Geometry-Based Sampling of Conformational Transitions in Proteins

    E-Print Network [OSTI]

    de Groot, Bert

    Structure Article Geometry-Based Sampling of Conformational Transitions in Proteins Daniel Seeliger of the binding site when using a holo structure, or by not identifying the correct binding pose when using an apo

  15. A Mineralogical Petrographic And Geochemical Study Of Samples...

    Open Energy Info (EERE)

    The composition of the hydrothermal fluid was determined and correlated with the mineralogy. Isotopic ratios of C and O for one calcite sample taken from 341 m depth were...

  16. Relationship between classifier performance and distributional complexity for small samples

    E-Print Network [OSTI]

    Attoor, Sanju Nair

    2004-11-15T23:59:59.000Z

    Given a limited number of samples for classification, several issues arise with respect to design, performance and analysis of classifiers. This is especially so in the case of microarray-based classification. In this paper, we use a complexity...

  17. Long-Term Ecological Monitoring Field Sampling Plan for 2007

    SciTech Connect (OSTI)

    T. Haney

    2007-07-31T23:59:59.000Z

    This field sampling plan describes the field investigations planned for the Long-Term Ecological Monitoring Project at the Idaho National Laboratory Site in 2007. This plan and the Quality Assurance Project Plan for Waste Area Groups 1, 2, 3, 4, 5, 6, 7, 10, and Removal Actions constitute the sampling and analysis plan supporting long-term ecological monitoring sampling in 2007. The data collected under this plan will become part of the long-term ecological monitoring data set that is being collected annually. The data will be used t determine the requirements for the subsequent long-term ecological monitoring. This plan guides the 2007 investigations, including sampling, quality assurance, quality control, analytical procedures, and data management. As such, this plan will help to ensure that the resulting monitoring data will be scientifically valid, defensible, and of known and acceptable quality.

  18. RAPID DETERMINATION OF RA-226 IN ENVIRONMENTAL SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.

    2012-01-03T23:59:59.000Z

    A new rapid method for the determination of {sup 226}Ra in environmental samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used for emergency response or routine sample analyses. The need for rapid analyses in the event of a Radiological Dispersive Device or Improvised Nuclear Device event is well-known. In addition, the recent accident at Fukushima Nuclear Power Plant in March, 2011 reinforces the need to have rapid analyses for radionuclides in environmental samples in the event of a nuclear accident. {sup 226}Ra (T1/2 = 1,620 years) is one of the most toxic of the long-lived alpha-emitters present in the environment due to its long life and its tendency to concentrate in bones, which increases the internal radiation dose of individuals. The new method to determine {sup 226}Ra in environmental samples utilizes a rapid sodium hydroxide fusion method for solid samples, calcium carbonate precipitation to preconcentrate Ra, and rapid column separation steps to remove interferences. The column separation process uses cation exchange resin to remove large amounts of calcium, Sr Resin to remove barium and Ln Resin as a final purification step to remove {sup 225}Ac and potential interferences. The purified {sup 226}Ra sample test sources are prepared using barium sulfate microprecipitation in the presence of isopropanol for counting by alpha spectrometry. The method showed good chemical recoveries and effective removal of interferences. The determination of {sup 226}Ra in environmental samples can be performed in less than 16 h for vegetation, concrete, brick, soil, and air filter samples with excellent quality for emergency or routine analyses. The sample preparation work takes less than 6 h. {sup 225}Ra (T1/2 = 14.9 day) tracer is used and the {sup 225}Ra progeny {sup 217}At is used to determine chemical yield via alpha spectrometry. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory radium particles are effectively digested. The preconcentration and column separation steps can also be applied to aqueous samples with good results.

  19. Statistical Analysis of Tank 5 Floor Sample Results

    SciTech Connect (OSTI)

    Shine, E. P.

    2013-01-31T23:59:59.000Z

    Sampling has been completed for the characterization of the residual material on the floor of Tank 5 in the F-Area Tank Farm at the Savannah River Site (SRS), near Aiken, SC. The sampling was performed by Savannah River Remediation (SRR) LLC using a stratified random sampling plan with volume-proportional compositing. The plan consisted of partitioning the residual material on the floor of Tank 5 into three non-overlapping strata: two strata enclosed accumulations, and a third stratum consisted of a thin layer of material outside the regions of the two accumulations. Each of three composite samples was constructed from five primary sample locations of residual material on the floor of Tank 5. Three of the primary samples were obtained from the stratum containing the thin layer of material, and one primary sample was obtained from each of the two strata containing an accumulation. This report documents the statistical analyses of the analytical results for the composite samples. The objective of the analysis is to determine the mean concentrations and upper 95% confidence (UCL95) bounds for the mean concentrations for a set of analytes in the tank residuals. The statistical procedures employed in the analyses were consistent with the Environmental Protection Agency (EPA) technical guidance by Singh and others [2010]. Savannah River National Laboratory (SRNL) measured the sample bulk density, nonvolatile beta, gross alpha, and the radionuclide1, elemental, and chemical concentrations three times for each of the composite samples. The analyte concentration data were partitioned into three separate groups for further analysis: analytes with every measurement above their minimum detectable concentrations (MDCs), analytes with no measurements above their MDCs, and analytes with a mixture of some measurement results above and below their MDCs. The means, standard deviations, and UCL95s were computed for the analytes in the two groups that had at least some measurements above their MDCs. The identification of distributions and the selection of UCL95 procedures generally followed the protocol in Singh, Armbya, and Singh [2010]. When all of an analyte's measurements lie below their MDCs, only a summary of the MDCs can be provided. The measurement results reported by SRNL are listed, and the results of this analysis are reported. The data were generally found to follow a normal distribution, and to be homogenous across composite samples.

  20. Recent results of the investigation of a micro-fluidic sampling chip and sampling system for hot cell aqueous processing streams

    SciTech Connect (OSTI)

    Tripp, J.; Smith, T.; Law, J. [Idaho National Laboratory: P.O. Box 1625, Idaho Falls, ID 83415 (United States)

    2013-07-01T23:59:59.000Z

    A Fuel Cycle Research and Development project has investigated an innovative sampling method that could evolve into the next generation sampling and analysis system for metallic elements present in aqueous processing streams. Initially sampling technologies were evaluated and micro-fluidic sampling chip technology was selected and tested. A conceptual design for a fully automated microcapillary-based system was completed and a robotic automated sampling system was fabricated. The mechanical and sampling operation of the completed sampling system was investigated. Different sampling volumes have been tested. It appears that the 10 ?l volume has produced data that had much smaller relative standard deviations than the 2 ?l volume. In addition, the production of a less expensive, mass produced sampling chip was investigated to avoid chip reuse thus increasing sampling reproducibility/accuracy. The micro-fluidic-based robotic sampling system's mechanical elements were tested to ensure analytical reproducibility and the optimum robotic handling of micro-fluidic sampling chips. (authors)

  1. Retained Gas Sampling Results for the Flammable Gas Program

    SciTech Connect (OSTI)

    J.M. Bates; L.A. Mahoney; M.E. Dahl; Z.I. Antoniak

    1999-11-18T23:59:59.000Z

    The key phenomena of the Flammable Gas Safety Issue are generation of the gas mixture, the modes of gas retention, and the mechanisms causing release of the gas. An understanding of the mechanisms of these processes is required for final resolution of the safety issue. Central to understanding is gathering information from such sources as historical records, tank sampling data, tank process data (temperatures, ventilation rates, etc.), and laboratory evaluations conducted on tank waste samples.

  2. Double Shell Tank (DST) Process Waste Sampling Subsystem Definition Report

    SciTech Connect (OSTI)

    RASMUSSEN, J.H.

    2000-04-25T23:59:59.000Z

    This report defines the Double-Shell Tank (DST) Process Waste Sampling Subsystem (PWSS). This subsystem definition report fully describes and identifies the system boundaries of the PWSS. This definition provides a basis for developing functional, performance, and test requirements (i.e., subsystem specification), as necessary, for the PWSS. The resultant PWSS specification will include the sampling requirements to support the transfer of waste from the DSTs to the Privatization Contractor during Phase 1 of Waste Feed Delivery.

  3. Microscopic Lensing by a Dense, Cold Atomic Sample

    E-Print Network [OSTI]

    Stetson Roof; Kasie Kemp; Mark Havey; I. M. Sokolov; D. V. Kupriyanov

    2014-12-01T23:59:59.000Z

    We demonstrate that a cold, dense sample of 87Rb atoms can exhibit a micron-scale lensing effect, much like that associated with a macroscopically-sized lens. The experiment is carried out in the fashion of traditional z-scan measurements but in much weaker fields and where close attention is paid to the detuning dependence of the transmitted light. The results are interpreted using numerical simulations and by modeling the sample as a thin lens with a spherical focal length.

  4. Case depth verification of hardened samples with Barkhausen noise sweeps

    SciTech Connect (OSTI)

    Santa-aho, Suvi; Vippola, Minnamari; Lepistö, Toivo [Tampere University of Technology, Department of Materials Science, P.O. Box 589, 33101 Tampere (Finland); Hakanen, Merja [Stresstech Oy, Tikkutehtaantie 1, 40800 Vaajakoski (Finland); Sorsa, Aki; Leiviskä, Kauko [University of Oulu, Control Engineering Laboratory, P.O. Box 4300, FIN-90014 University of Oulu (Finland)

    2014-02-18T23:59:59.000Z

    An interesting topic of recent Barkhausen noise (BN) method studies is the application of the method to case depth evaluation of hardened components. The utilization of BN method for this purpose is based on the difference in the magnetic properties between the hardened case and the soft core. Thus, the detection of case depth with BN can be achieved. The measurements typically have been carried out by using low magnetizing frequencies which have deeper penetration to the ferromagnetic samples than the conventional BN measurement. However, the penetration depth is limited due to eddy current damping of the signal. We introduce here a newly found sweep measurement concept for the case depth evaluation. In this study sweep measurements were carried out with various magnetizing frequencies and magnetizing voltages to detect the effect of different frequency and voltage and their correspondence to the actual case depth values verified from destructive characterization. Also a BN measurement device that has an implemented sweep analysis option was utilised. The samples were either induction or case-hardened samples and sample geometry contained both rod samples and gear axle samples with different case depth values. Samples were also further characterized with Xray diffraction to study the residual stress state of the surface. The detailed data processing revealed that also other calculated features than the maximum slope division of the 1st derivative of the BN signal could hold the information about the case depth value of the samples. The sweep method was able to arrange the axles into correct order according to the case depth value even though the axles were used.

  5. Analysis of HEU samples from the ULBA Metallurgical Plant

    SciTech Connect (OSTI)

    Gift, E.H.

    1995-05-01T23:59:59.000Z

    In early March 1994, eight highly enriched uranium (HEU) samples were collected from materials stored at the Ulba Metallurgical Plant in Oskamen (Ust Kamenogorsk), Kazakhstan. While at the plant site, portions of four samples were dissolved and analyzed by mass spectrograph at the Ulba analytical laboratory by Ulba analysts. Three of these mass spectrograph solutions and the eight HEU samples were subsequently delivered to the Y-12 Plant for complete chemical and isotopic analyses. Chemical forms of the eight samples were uranium metal chips, U0{sub 2} powder, uranium/beryllium oxide powder, and uranium/beryllium alloy rods. All were declared by the Ulba plant to have a uranium assay of {approximately}90 wt % {sup 235}U. The uranium/beryllium powder and alloy samples were also declared to range from about 8 to 28 wt % uranium. The chemical and uranium isotopic analyses done at the Y-12 Plant confirm the Ulba plant declarations. All samples appear to have been enriched using some reprocessed uranium, probably from recovery of uranium from plutonium production reactors. As a result, all samples contain some {sup 236}U and {sup 232}U and have small but measurable quantities of plutonium. This plutonium could be the result of either contamination carried over from the enrichment process or cross-contamination from weapons material. It is not the result of direct reactor exposure. Neither the {sup 232}U nor the plutonium concentrations are sufficiently high to provide a significant industrial health hazard. Both are well within established or proposed acceptance criteria for storage at Y-12. The trace metal analyses showed that, with the exception of beryllium, there are no trace metals in any of these HEU samples that pose a significant health hazard.

  6. Determination of actinides in urine and fecal samples

    DOE Patents [OSTI]

    McKibbin, Terry T. (Larimer County, CO)

    1993-01-01T23:59:59.000Z

    A method of determining the radioactivity of specific actinides that are carried in urine or fecal sample material is disclosed. The samples are ashed in a muffle furnace, dissolved in an acid, and then treated in a series of steps of reduction, oxidation, dissolution, and precipitation, including a unique step of passing a solution through a chloride form anion exchange resin for separation of uranium and plutonium from americium.

  7. Determination of actinides in urine and fecal samples

    DOE Patents [OSTI]

    McKibbin, T.T.

    1993-03-02T23:59:59.000Z

    A method of determining the radioactivity of specific actinides that are carried in urine or fecal sample material is disclosed. The samples are ashed in a muffle furnace, dissolved in an acid, and then treated in a series of steps of reduction, oxidation, dissolution, and precipitation, including a unique step of passing a solution through a chloride form anion exchange resin for separation of uranium and plutonium from americium.

  8. Differences in radar derived rainfall amounts due to sampling intervals

    E-Print Network [OSTI]

    Zdenek, David James

    1986-01-01T23:59:59.000Z

    DIFFERENCES IN RADAR DERIVED RAINFALL AMOUNTS DUE TO SAMPLING INTERVALS A Thesis by DAVID JAMES ZDENEK Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE... December 1986 Major Subject: Meteorology DIFFERENCES IN RADAR DERIVED RAINFALL AMOUNTS DUE TO SAMPLING INTERVALS A Thesis by DAVID JAMES ZDENEK Approved as to style and content by: eorge L. Huebner (Chairman of Committee) CP~ CG~& Robert C...

  9. Comparison of sampling techniques for Heliothis species in cotton

    E-Print Network [OSTI]

    Walters, Michelle Lynn

    1986-01-01T23:59:59.000Z

    December 19g& Najor Subject: Entomology COMPARISON OF SAMPLING TECHNIQUES FOR HELIOTHIS SPECIES IN COTTON A Thesis by MICHELLE LYNN WALTERS Approved as to style and content by: J. K. Walker, Jr. (Chairman of Committee) J. K. Olson (Member) A. E.... Percival (Member) 2 & F/yg. (Member) F, G. Maxwell (Head of Department) December 1986 ABSTRACT Comparison of Sampling Techniques for Heliothis Species in Cotton. (December 1986) Nichelle Lynn Walters, B. S. , Arizona State University; Chairman...

  10. ( Sample of Shipment Notice) Federal Records Center | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on Delicious Rank EERE:YearRound-Up from theDepartment( Sample of Shipment Notice) Federal Records Center ( Sample of

  11. UMTRA project water sampling and analysis plan, Monument Valley, Arizona

    SciTech Connect (OSTI)

    Not Available

    1994-04-01T23:59:59.000Z

    The Monument Valley Uranium Mill Tailings Remedial Action (UMTRA) Project site in Cane Valley is a former uranium mill that has undergone surface remediation in the form of tailings and contaminated materials removal. Contaminated materials from the Monument Valley (Arizona) UMTRA Project site have been transported to the Mexican Hat (Utah) UMTRA Project site for consolidation with the Mexican Hat tailings. Tailings removal was completed in February 1994. Three geologic units at the site contain water: the unconsolidated eolian and alluvial deposits (alluvial aquifer), the Shinarump Conglomerate (Shinarump Member), and the De Chelly Sandstone. Water quality analyses indicate the contaminant plume has migrated north of the site and is mainly in the alluvial aquifer. An upward hydraulic gradient in the De Chelly Sandstone provides some protection to that aquifer. This water sampling and analysis plan recommends sampling domestic wells, monitor wells, and surface water in April and September 1994. The purpose of sampling is to continue periodic monitoring for the surface program, evaluate changes to water quality for site characterization, and provide data for the baseline risk assessment. Samples taken in April will be representative of high ground water levels and samples taken in September will be representative of low ground water levels. Filtered and nonfiltered samples will be analyzed for plume indicator parameters and baseline risk assessment parameters.

  12. Visual Sample Plan Version 7.0 User's Guide

    SciTech Connect (OSTI)

    Matzke, Brett D.; Newburn, Lisa LN; Hathaway, John E.; Bramer, Lisa M.; Wilson, John E.; Dowson, Scott T.; Sego, Landon H.; Pulsipher, Brent A.

    2014-03-01T23:59:59.000Z

    User's guide for VSP 7.0 This user's guide describes Visual Sample Plan (VSP) Version 7.0 and provides instructions for using the software. VSP selects the appropriate number and location of environmental samples to ensure that the results of statistical tests performed to provide input to risk decisions have the required confidence and performance. VSP Version 7.0 provides sample-size equations or algorithms needed by specific statistical tests appropriate for specific environmental sampling objectives. It also provides data quality assessment and statistical analysis functions to support evaluation of the data and determine whether the data support decisions regarding sites suspected of contamination. The easy-to-use program is highly visual and graphic. VSP runs on personal computers with Microsoft Windows operating systems (XP, Vista, Windows 7, and Windows 8). Designed primarily for project managers and users without expertise in statistics, VSP is applicable to two- and three-dimensional populations to be sampled (e.g., rooms and buildings, surface soil, a defined layer of subsurface soil, water bodies, and other similar applications) for studies of environmental quality. VSP is also applicable for designing sampling plans for assessing chem/rad/bio threat and hazard identification within rooms and buildings, and for designing geophysical surveys for unexploded ordnance (UXO) identification.

  13. Assessment of the 296-S-21 Stack Sampling Probe Location

    SciTech Connect (OSTI)

    Glissmeyer, John A.

    2006-09-08T23:59:59.000Z

    Tests were performed to assess the suitability of the location of the air sampling probe on the 296-S-21 stack according to the criteria of ANSI N13.1-1999, Sampling and Monitoring Releases of Airborne Radioactive Substances from the Stacks and Ducts of Nuclear Facilities. Pacific Northwest National Laboratory conducted most tests on a 3.67:1 scale model of the stack. CH2MHill also performed some limited confirmatory tests on the actual stack. The tests assessed the capability of the air-monitoring probe to extract a sample representative of the effluent stream. The tests were conducted for the practical combinations of operating fans and addressed: (1) Angular Flow--The purpose is to determine whether the velocity vector is aligned with the sampling nozzle. The average yaw angle relative to the nozzle axis should not be more than 20. The measured values ranged from 5 to 11 degrees on the scale model and 10 to 12 degrees on the actual stack. (2) Uniform Air Velocity--The gas momentum across the stack cross section where the sample is extracted should be well mixed or uniform. The uniformity is expressed as the variability of the measurements about the mean, the coefficient of variance (COV). The lower the COV value, the more uniform the velocity. The acceptance criterion is that the COV of the air velocity must be ?20% across the center two-thirds of the area of the stack. At the location simulating the sampling probe, the measured values ranged form 4 to 11%, which are within the criterion. To confirm the validity of the scale model results, air velocity uniformity measurements were made both on the actual stack and on the scale model at the test ports 1.5 stack diameters upstream of the sampling probe. The results ranged from 6 to 8% COV on the actual stack and 10 to 13% COV on the scale model. The average difference for the eight runs was 4.8% COV, which is within the validation criterion. The fact that the scale model results were slightly higher than the actual stack suggests that the other test results on the scale model are conservative relative to the actual stack. (3) Uniform Concentration of Tracer Gases--A uniform contaminant concentration in the sampling plane enables the extraction of samples that represent the true concentration. This was first tested using a tracer gas to represent gaseous effluents. The fan is a good mixer, so injecting the tracer downstream of the fans provides worst-case results. The acceptance criteria are that (1) the COV of the measured tracer gas concentration is ?20% across the center two-thirds of the sampling plane and (2) at no point in the sampling plane does the concentration vary from the mean by >30%. The results on the scale model at the point simulating the sampling probe ranged from 0.3 to 6 %COV, and the maximum single point deviation from the mean was -10%. (4) Uniform Concentration of Tracer Particles--Uniformity in contaminant concentration at the sampling probe was further demonstrated using tracer particles large enough to exhibit inertial effects. Particles of 10-?m aerodynamic diameter were used. The acceptance criterion is that the COV of particle concentration is ?20% across the center two-thirds of the sampling plane. The scale model results ranged form 2 to 9%. Based on these tests, the location of the air sampling probe on the 296-S-21 stack meets the requirements of the ANSI/HPS N13.1-1999 standard.

  14. Atmospheric deposition: sample handling, storage, and analytical procedures for chemical characterization of event-based samples in North Dakota

    SciTech Connect (OSTI)

    Houghton, R.L.; Berger, M.; Zander, N.; Dutchek, S.K.

    1983-01-01T23:59:59.000Z

    The North Dakota atmospheric-deposition network uses HASL-type collectors to sample wet and dry deposition on an event basis for analysis of 8 principal mineral, 3 nutrient, and 15 trace constituents. Comparison of the compositions of wet deposition collected in adjacent collectors sampled on weekly and event bases indicates that nonevent sampling leads to significant contamination of wet-deposition samples with dry deposition. Elevation of the collectors 10 feet above ground surface may decrease wind-blown soil contamination significantly. This manual presents a summary of the research procedures adopted by the North Dakota District of the US Geological Survey to investigate the consequences of increased fossil-fuel combustion on the quality of atmospheric deposition. The manual has been tested by field operatives for 3 years and shown to be an effective field guide and management tool. 44 references, 3 figures, 13 tables.

  15. Waste minimization in analytical chemistry through innovative sample preparation techniques.

    SciTech Connect (OSTI)

    Smith, L. L.

    1998-05-28T23:59:59.000Z

    Because toxic solvents and other hazardous materials are commonly used in analytical methods, characterization procedures result in significant and costly amount of waste. We are developing alternative analytical methods in the radiological and organic areas to reduce the volume or form of the hazardous waste produced during sample analysis. For the radiological area, we have examined high-pressure, closed-vessel microwave digestion as a way to minimize waste from sample preparation operations. Heated solutions of strong mineral acids can be avoided for sample digestion by using the microwave approach. Because reactivity increases with pressure, we examined the use of less hazardous solvents to leach selected contaminants from soil for subsequent analysis. We demonstrated the feasibility of this approach by extracting plutonium from a NET reference material using citric and tartaric acids with microwave digestion. Analytical results were comparable to traditional digestion methods, while hazardous waste was reduced by a factor often. We also evaluated the suitability of other natural acids, determined the extraction performance on a wider variety of soil types, and examined the extraction efficiency of other contaminants. For the organic area, we examined ways to minimize the wastes associated with the determination of polychlorinated biphenyls (PCBs) in environmental samples. Conventional methods for analyzing semivolatile organic compounds are labor intensive and require copious amounts of hazardous solvents. For soil and sediment samples, we have a method to analyze PCBs that is based on microscale extraction using benign solvents (e.g., water or hexane). The extraction is performed at elevated temperatures in stainless steel cells containing the sample and solvent. Gas chromatography-mass spectrometry (GC/MS) was used to quantitate the analytes in the isolated extract. More recently, we developed a method utilizing solid-phase microextraction (SPME) for natural water samples. In this SPME technique, a fused-silica fiber coated with a polymeric film is exposed to the sample, extraction is allowed to take place, and then the analytes are thermally desorbed for GC analysis. Unlike liquid-liquid extraction or solid-phase extraction, SPME consumes all of the extracted sample in the analysis, significantly reducing the required sample volume.

  16. Trench sampling report Salmon Site Lamar County, Mississippi

    SciTech Connect (OSTI)

    Not Available

    1994-07-01T23:59:59.000Z

    This report describes trench excavation and sample-collection activities conducted by IT Corporation (IT) as part of the ongoing Remedial Investigation and Feasibility Study at the Salmon Site, Lamar County, Mississippi (DOE, 1992). During construction, operation, and closure of the site wastes of unknown composition were buried in pits on site. Surface-geophysical field investigations were conducted intermittently between November 1992 and October 1993 to identify potential waste-burial sites and buried metallic materials. The geophysical investigations included vertical magnetic gradient, electromagnetic conductivity, electromagnetic in-phase component, and ground-penetrating radar surveys. A number of anomalies identified by the magnetic gradiometer survey in the Reynolds Electrical & Engineering Co., Inc., (REECo) pits area indicated buried metallic objects. All of the anomalies were field checked to determine if any were caused by surface features or debris. After field checking, 17 anomalies were still unexplained; trenching was planned to attempt to identify their sources. Between December 8, 1993, and December 17, 1993, 15 trenches were excavated and soil samples were collected at the anomalies. Samples were collected, placed in 250- and 500-milliliter (m{ell}) amber glass containers, and shipped on ice to IT Analytical Services (ITAS) in St. Louis, Missouri, using standard IT chain-of-custody procedures. The samples were analyzed for various chemical and radiological parameters. Data validation has not been conducted on any of the samples. During excavation and sampling, soil samples were also collected by IT for the MSDEQ and the Mississippi Department of Radiological Health, in accordance with their instructions, and delivered into their custody.

  17. WRAP Module 1 sampling strategy and waste characterization alternatives study

    SciTech Connect (OSTI)

    Bergeson, C.L.

    1994-09-30T23:59:59.000Z

    The Waste Receiving and Processing Module 1 Facility is designed to examine, process, certify, and ship drums and boxes of solid wastes that have a surface dose equivalent of less than 200 mrem/h. These wastes will include low-level and transuranic wastes that are retrievably stored in the 200 Area burial grounds and facilities in addition to newly generated wastes. Certification of retrievably stored wastes processing in WRAP 1 is required to meet the waste acceptance criteria for onsite treatment and disposal of low-level waste and mixed low-level waste and the Waste Isolation Pilot Plant Waste Acceptance Criteria for the disposal of TRU waste. In addition, these wastes will need to be certified for packaging in TRUPACT-II shipping containers. Characterization of the retrievably stored waste is needed to support the certification process. Characterization data will be obtained from historical records, process knowledge, nondestructive examination nondestructive assay, visual inspection of the waste, head-gas sampling, and analysis of samples taken from the waste containers. Sample characterization refers to the method or methods that are used to test waste samples for specific analytes. The focus of this study is the sample characterization needed to accurately identify the hazardous and radioactive constituents present in the retrieved wastes that will be processed in WRAP 1. In addition, some sampling and characterization will be required to support NDA calculations and to provide an over-check for the characterization of newly generated wastes. This study results in the baseline definition of WRAP 1 sampling and analysis requirements and identifies alternative methods to meet these requirements in an efficient and economical manner.

  18. Radioisotope Electric Propulsion for Deep Space Sample Return

    SciTech Connect (OSTI)

    Noble, Robert J.; /SLAC

    2009-07-14T23:59:59.000Z

    The need to answer basic questions regarding the origin of the Solar System will motivate robotic sample return missions to destinations like Pluto, its satellite Charon, and objects in the Kuiper belt. To keep the mission duration short enough to be of interest, sample return from objects farther out in the Solar System requires increasingly higher return velocities. A sample return mission involves several complicated steps to reach an object and obtain a sample, but only the interplanetary return phase of the mission is addressed in this paper. Radioisotope electric propulsion is explored in this parametric study as a means to propel small, dedicated return vehicles for transferring kilogram-size samples from deep space to Earth. Return times for both Earth orbital rendezvous and faster, direct atmospheric re-entry trajectories are calculated for objects as far away as 100 AU. Chemical retro-rocket braking at Earth is compared to radioisotope electric propulsion but the limited deceleration capability of chemical rockets forces the return trajectories to be much slower.

  19. Rapid Determination Of Radiostrontium In Large Soil Samples

    SciTech Connect (OSTI)

    Maxwell, Sherrod L.; Culligan, Brian K.; Shaw, Patrick J.

    2012-05-24T23:59:59.000Z

    A new method for the determination of radiostrontium in large soil samples has been developed at the Savannah River Environmental Laboratory (Aiken, SC, USA) that allows rapid preconcentration and separation of strontium in large soil samples for the measurement of strontium isotopes by gas flow proportional counting. The need for rapid analyses in the event of a Radiological Dispersive Device (RDD) or Improvised Nuclear Device (IND) event is well-known. In addition, the recent accident at Fukushima Nuclear Power Plant in March, 2011 reinforces the need to have rapid analyses for radionuclides in environmental samples in the event of a nuclear accident. The method employs a novel pre-concentration step that utilizes an iron hydroxide precipitation (enhanced with calcium phosphate) followed by a final calcium fluoride precipitation to remove silicates and other matrix components. The pre-concentration steps, in combination with a rapid Sr Resin separation using vacuum box technology, allow very large soil samples to be analyzed for {sup 89,90}Sr using gas flow proportional counting with a lower method detection limit. The calcium fluoride precipitation eliminates column flow problems typically associated with large amounts of silicates in large soil samples.

  20. Use of passive sampling devices to determine soil contaminant concentrations

    SciTech Connect (OSTI)

    Johnson, K.A. [Clemson Univ., Pendleton, SC (United States); [Washington State Univ., Richland, WA (United States); Hooper, M.J. [Clemson Univ., Pendleton, SC (United States); Weisskopf, C.P. [Washington State Univ., Richland, WA (United States)

    1996-12-31T23:59:59.000Z

    The effective remediation of contaminated sites requires accurate identification of chemical distributions. A rapid sampling method using passive sampling devices (PSDs) can provide a thorough site assessment. We have been pursuing their application in terrestrial systems and have found that they increase the ease and speed of analysis, decrease solvent usage and overall cost, and minimize the transport of contaminated soils. Time and cost savings allow a higher sampling frequency than is generally the case using traditional methods. PSDs have been used in the field in soils of varying physical properties and have been successful in estimating soil concentrations ranging from 1 {mu}g/kg (parts per billion) to greater than 200 mg/kg (parts per million). They were also helpful in identifying hot spots within the sites. Passive sampling devices show extreme promise as an analytical tool to rapidly characterize contaminant distributions in soil. There are substantial time and cost savings in laboratory personnel and supplies. By selectively excluding common interferences that require sample cleanup, PSDs can be retrieved from the field and processed rapidly (one technician can process approximately 90 PSDs in an 8-h work day). The results of our studies indicate that PSDs can be used to accurately estimate soil contaminant concentrations and provide lower detection limits. Further, time and cost savings will allow a more thorough and detailed characterization of contaminant distributions. 13 refs., 4 figs., 2 tabs.

  1. Method for preconcentrating a sample for subsequent analysis

    DOE Patents [OSTI]

    Zaromb, Solomon (Hinsdale, IL)

    1990-01-01T23:59:59.000Z

    A system for analysis of trace concentration of contaminants in air includes a portable liquid chromatograph and a preconcentrator for the contaminants to be analyzed. The preconcentrator includes a sample bag having an inlet valve and an outlet valve for collecting an air sample. When the sample is collected the sample bag is connected in series with a sorbing apparatus in a recirculation loop. The sorbing apparatus has an inner gas-permeable container containing a sorbent material and an outer gas-impermeable container. The sample is circulated through the outer container and around the inner container for trapping and preconcentrating the contaminants in the sorbent material. The sorbent material may be a liquid having the same composition as the mobile phase of the chromatograph for direct injection thereinto. Alternatively, the sorbent material may be a porous, solid body, to which mobile phase liquid is added after preconcentration of the contaminants for dissolving the contaminants, the liquid solution then being withdrawn for injection into the chromatograph.

  2. Analytical instrument with apparatus and method for sample concentrating

    DOE Patents [OSTI]

    Zaromb, S.

    1986-08-04T23:59:59.000Z

    A system for analysis of trace concentrations of contaminants in air includes a portable liquid chromatograph and a preconcentrator for the contaminants to be analyzed. The preconcentrator includes a sample bag having an inlet valve and an outlet valve for collecting an air sample. When the sample is collected the sample bag is connected in series with a sorbing apparatus in a recirculation loop. The sorbing apparatus has an inner gas-permeable container containing a sorbent material and an outer gas-impermeable container. The sample is circulated through the outer container and around the inner container for trapping and preconcentrating the contaminants in the sorbent material. The sorbent material may be a liquid having the same composition as the mobile phase of the chromatograph for direct injection thereinto. Alternatively, the sorbent material may be a porous, solid body, to which mobile phase liquid is added after preconcentration of the contaminants for dissolving the contaminants, the liquid solution then being withdrawn for injection into the chromatograph.

  3. Hanford Site Environmental Surveillance Master Sampling Schedule for Calendar Year 2011

    SciTech Connect (OSTI)

    Bisping, Lynn E.

    2011-01-21T23:59:59.000Z

    This document contains the calendar year 2011 schedule for the routine collection of samples for the Surface Environmental Surveillance Project and the Drinking Water Monitoring Project. Each section includes sampling locations, sampling frequencies, sample types, and analyses to be performed. In some cases, samples are scheduled on a rotating basis. If a sample will not be collected in 2011, the anticipated year for collection is provided. Maps showing approximate sampling locations are included for media scheduled for collection in 2011.

  4. Trends and Future Challenges in Sampling the Deep Terrestrial Biosphere

    SciTech Connect (OSTI)

    Wilkins, Michael J.; Daly, Rebecca; Mouser, Paula J.; Trexler, Ryan; Sharma, Shihka; Cole, David R.; Wrighton, Kelly C.; Biddle , Jennifer F.; Denis, Elizabeth; Fredrickson, Jim K.; Kieft, Thomas L.; Onstott, T. C.; Peterson, Lee; Pfiffner, Susan M.; Phelps, Tommy J.; Schrenk, Matthew O.

    2014-09-12T23:59:59.000Z

    Research in the deep terrestrial biosphere is driven by interest in novel biodiversity and metabolisms, biogeochemical cycling, and the impact of human activities on this ecosystem. As this interest continues to grow, it is important to ensure that when subsurface investigations are proposed, materials recovered from the subsurface are sampled and preserved in an appropriate manner to limit contamination and ensure preservation of accurate microbial, geochemical, and mineralogical signatures. On February 20th, 2014, a workshop on “Trends and Future Challenges in Sampling The Deep Subsurface” was coordinated in Columbus, Ohio by The Ohio State University and West Virginia University faculty, and sponsored by The Ohio State University and the Sloan Foundation’s Deep Carbon Observatory. The workshop aims were to identify and develop best practices for the collection, preservation, and analysis of terrestrial deep rock samples. This document summarizes the information shared during this workshop.

  5. Retrospective dosimetry analyses of reactor vessel cladding samples

    SciTech Connect (OSTI)

    Greenwood, L. R.; Soderquist, C. Z. [Battelle Pacific Northwest National Laboratory, Richland, WA 99352 (United States); Fero, A. H. [Westinghouse Electric Company, Cranberry Twp., PA 16066 (United States)

    2011-07-01T23:59:59.000Z

    Reactor pressure vessel cladding samples for Ringhals Units 3 and 4 in Sweden were analyzed using retrospective reactor dosimetry techniques. The objective was to provide the best estimates of the neutron fluence for comparison with neutron transport calculations. A total of 51 stainless steel samples consisting of chips weighing approximately 100 to 200 mg were removed from selected locations around the pressure vessel and were sent to Pacific Northwest National Laboratory for analysis. The samples were fully characterized and analyzed for radioactive isotopes, with special interest in the presence of Nb-93m. The RPV cladding retrospective dosimetry results will be combined with a re-evaluation of the surveillance capsule dosimetry and with ex-vessel neutron dosimetry results to form a comprehensive 3D comparison of measurements to calculations performed with 3D deterministic transport code. (authors)

  6. GICHD Mine Dog Testing Project - Soil Sample Results No.3

    SciTech Connect (OSTI)

    PHELAN, JAMES M.; BARNETT, JAMES L.; BENDER, SUSAN FAE ANN; ARCHULETA, LUISA M.

    2003-03-01T23:59:59.000Z

    A mine dog evaluation project initiated by the Geneva International Center for Humanitarian Demining is evaluating the capability and reliability of mine detection dogs. The performance of field-operational mine detection dogs will be measured in test minefields in Afghanistan and Bosnia containing actual, but unfused landmines. Repeated performance testing over two years through various seasonal weather conditions will provide data simulating near real world conditions. Soil samples will be obtained adjacent to the buried targets repeatedly over the course of the test. Chemical analysis results from these soil samples will be used to evaluate correlations between mine dog detection performance and seasonal weather conditions. This report documents the analytical chemical methods and results from the third batch of soils received. This batch contained samples from Kharga, Afghanistan collected in October 2002.

  7. GICHD mine dog testing project - soil sample results #4.

    SciTech Connect (OSTI)

    Barnett, James L.; Phelan, James M.; Archuleta, Luisa M.; Wood, Tyson B.; Donovan, Kelly L.; Bender, Susan Fae Ann

    2003-08-01T23:59:59.000Z

    A mine dog evaluation project initiated by the Geneva International Center for Humanitarian Demining is evaluating the capability and reliability of mine detection dogs. The performance of field-operational mine detection dogs will be measured in test minefields in Afghanistan and Bosnia containing actual, but unfused landmines. Repeated performance testing over two years through various seasonal weather conditions will provide data simulating near real world conditions. Soil samples will be obtained adjacent to the buried targets repeatedly over the course of the test. Chemical analysis results from these soil samples will be used to evaluate correlations between mine dog detection performance and seasonal weather conditions. This report documents the analytical chemical methods and results from the fourth batch of soils received. This batch contained samples from Kharga, Afghanistan collected in April 2003 and Sarajevo, Bosnia collected in May 2003.

  8. Sampling probe for microarray read out using electrospray mass spectrometry

    DOE Patents [OSTI]

    Van Berkel, Gary J.

    2004-10-12T23:59:59.000Z

    An automated electrospray based sampling system and method for analysis obtains samples from surface array spots having analytes. The system includes at least one probe, the probe including an inlet for flowing at least one eluting solvent to respective ones of a plurality of spots and an outlet for directing the analyte away from the spots. An automatic positioning system is provided for translating the probe relative to the spots to permit sampling of any spot. An electrospray ion source having an input fluidicly connected to the probe receives the analyte and generates ions from the analyte. The ion source provides the generated ions to a structure for analysis to identify the analyte, preferably being a mass spectrometer. The probe can be a surface contact probe, where the probe forms an enclosing seal along the periphery of the array spot surface.

  9. Concentric micro-nebulizer for direct sample insertion

    DOE Patents [OSTI]

    Fassel, V.A.; Rice, G.W.; Lawrence, K.E.

    1984-03-06T23:59:59.000Z

    A concentric micro-nebulizer and method for introducing liquid samples into a plasma established in a plasma torch including a first tube connected to a source of plasma gas. The concentric micro-nebulizer has inner and outer concentric tubes extending upwardly within the torch for connection to a source of nebulizer gas and to a source of liquid solvent and to a source of sample liquid. The inner tube is connected to the source of liquid solvent and to the source of sample liquid and the outer tube is connected to the source of nebulizer gas. The outer tube has an orifice positioned slightly below the plasma when it is established, with the inner and outer tubes forming an annulus therebetween with the annular spacing between the tubes at said orifice being less than about 0.05mm. The dead volume of the inner tube is less than about 5 microliters.

  10. Broadband sample holder for microwave spectroscopy of superconducting qubits

    SciTech Connect (OSTI)

    Averkin, A. S.; Karpov, A.; Glushkov, E.; Abramov, N. [National University of Science and Technology (MISIS), Leninskiy prosp. 4, Moscow, 119049 (Russian Federation); Shulga, K. [National University of Science and Technology (MISIS), Leninskiy prosp. 4, Moscow, 119049 (Russian Federation); Russian Quantum Center (RQC), 100 Novaya St., Skolkovo, Moscow region, 143025 (Russian Federation); Huebner, U. [Leibniz Institute of Photonic Technology (IPHT), PO Box 100239, D-07702 Jena (Germany); Il'ichev, E. [Russian Quantum Center (RQC), 100 Novaya St., Skolkovo, Moscow region, 143025 (Russian Federation); Leibniz Institute of Photonic Technology (IPHT), PO Box 100239, D-07702 Jena (Germany); Ustinov, A. V. [National University of Science and Technology (MISIS), Leninskiy prosp. 4, Moscow, 119049 (Russian Federation); Russian Quantum Center (RQC), 100 Novaya St., Skolkovo, Moscow region, 143025 (Russian Federation); Physikalisches Institut, Karlsruhe Institute of Technology (KIT), D-76131 Karlsruhe (Germany)

    2014-10-15T23:59:59.000Z

    We present a practical design and implementation of a broadband sample holder suitable for microwave experiments with superconducting integrated circuits at millikelvin temperatures. Proposed design can be easily integrated in standard dilution cryostats, has flat pass band response in a frequency range from 0 to 32 GHz, allowing the RF testing of the samples with substrate size up to 4 × 4 mm{sup 2}. The parasitic higher modes interference in the holder structure is analyzed and prevented via design considerations. The developed setup can be used for characterization of superconducting parametric amplifiers, bolometers, and qubits. We tested the designed sample holder by characterizing of a superconducting flux qubit at 20 mK temperature.

  11. Statistical Methods and Tools for Hanford Staged Feed Tank Sampling

    SciTech Connect (OSTI)

    Fountain, Matthew S.; Brigantic, Robert T.; Peterson, Reid A.

    2013-10-01T23:59:59.000Z

    This report summarizes work conducted by Pacific Northwest National Laboratory to technically evaluate the current approach to staged feed sampling of high-level waste (HLW) sludge to meet waste acceptance criteria (WAC) for transfer from tank farms to the Hanford Waste Treatment and Immobilization Plant (WTP). The current sampling and analysis approach is detailed in the document titled Initial Data Quality Objectives for WTP Feed Acceptance Criteria, 24590-WTP-RPT-MGT-11-014, Revision 0 (Arakali et al. 2011). The goal of this current work is to evaluate and provide recommendations to support a defensible, technical and statistical basis for the staged feed sampling approach that meets WAC data quality objectives (DQOs).

  12. A General Investigation of Optimized Atmospheric Sample Duration

    SciTech Connect (OSTI)

    Eslinger, Paul W.; Miley, Harry S.

    2012-11-28T23:59:59.000Z

    ABSTRACT The International Monitoring System (IMS) consists of up to 80 aerosol and xenon monitoring systems spaced around the world that have collection systems sensitive enough to detect nuclear releases from underground nuclear tests at great distances (CTBT 1996; CTBTO 2011). Although a few of the IMS radionuclide stations are closer together than 1,000 km (such as the stations in Kuwait and Iran), many of them are 2,000 km or more apart. In the absence of a scientific basis for optimizing the duration of atmospheric sampling, historically scientists used a integration times from 24 hours to 14 days for radionuclides (Thomas et al. 1977). This was entirely adequate in the past because the sources of signals were far away and large, meaning that they were smeared over many days by the time they had travelled 10,000 km. The Fukushima event pointed out the unacceptable delay time (72 hours) between the start of sample acquisition and final data being shipped. A scientific basis for selecting a sample duration time is needed. This report considers plume migration of a nondecaying tracer using archived atmospheric data for 2011 in the HYSPLIT (Draxler and Hess 1998; HYSPLIT 2011) transport model. We present two related results: the temporal duration of the majority of the plume as a function of distance and the behavior of the maximum plume concentration as a function of sample collection duration and distance. The modeled plume behavior can then be combined with external information about sampler design to optimize sample durations in a sampling network.

  13. RAPID DETERMINATION OF {sup 210} PO IN WATER SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.

    2013-05-22T23:59:59.000Z

    A new rapid method for the determination of {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that can be used for emergency response or routine water analyses. If a radiological dispersive device (RDD) event or a radiological attack associated with drinking water supplies occurs, there will be an urgent need for rapid analyses of water samples, including drinking water, ground water and other water effluents. Current analytical methods for the assay of {sup 210}Po in water samples have typically involved spontaneous auto-deposition of {sup 210}Po onto silver or other metal disks followed by counting by alpha spectrometry. The auto-deposition times range from 90 minutes to 24 hours or more, at times with yields that may be less than desirable. If sample interferences are present, decreased yields and degraded alpha spectrums can occur due to unpredictable thickening in the deposited layer. Separation methods have focused on the use of Sr Resin?, often in combination with 210Pb analysis. A new rapid method for {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that utilizes a rapid calcium phosphate co-precipitation method, separation using DGA Resin? (N,N,N?,N? tetraoctyldiglycolamide extractant-coated resin, Eichrom Technologies or Triskem-International), followed by rapid microprecipitation of {sup 210}Po using bismuth phosphate for counting by alpha spectrometry. This new method can be performed quickly with excellent removal of interferences, high chemical yields and very good alpha peak resolution, eliminating any potential problems with the alpha source preparation for emergency or routine samples. A rapid sequential separation method to separate {sup 210} Po and actinide isotopes was also developed. This new approach, rapid separation with DGA Resin plus microprecipitation for alpha source preparation, is a significant advance in radiochemistry for the rapid determination of {sup 210}Po.

  14. Characteristics of electromagnetic interference generated during discharge of Mylar samples

    SciTech Connect (OSTI)

    Leung, P.L.

    1984-12-01T23:59:59.000Z

    This paper discusses the measurements of the electromagnetic interference (EMI) generated during discharges of Mylar samples. The two components of EMI, the conducted emission and the radiated emission, are characterized by the replacement current and the radiated RF spectrum respectively. The measured radiated RF spectra reveal important information on the source of the electromagnetic radiation. The possible sources are the replacement current pulse and the discharged generated plasma. The scaling of the amplitudes of the EMI, as a function of the area of the test sample, is also discussed.

  15. The Group Evolution Multiwavelength Study (GEMS): the Sample and Datasets

    E-Print Network [OSTI]

    Duncan A. Forbes; Trevor Ponman; Frazer Pearce; John Osmond; Virginia Kilborn; Sarah Brough; Somak Raychaudhury; Carole Mundell; Trevor Miles; Katie Kern

    2006-02-09T23:59:59.000Z

    Galaxy groups have been under-studied relative to their richer counterparts -- clusters. The Group Evolution Multiwavelength Study (GEMS) aims to redress some the balance. Here we describe the GEMS sample selection and resulting sample of 60 nearby (distance dataset of X-ray, optical and HI imaging. ROSAT X-ray images of each group are presented. GEMS also utilizes near-infrared imaging from the 2MASS survey and optical spectra from the 6dFGS. These observational data are complemented by mock group catalogues generated from the latest LCDM simulations with gas physics included. Existing GEMS publications are briefly highlighted as are future publication plans.

  16. Sampling and Analysis Plan - Waste Treatment Plant Seismic Boreholes Project

    SciTech Connect (OSTI)

    Reidel, Steve P.

    2006-05-26T23:59:59.000Z

    This sampling and analysis plan (SAP) describes planned data collection activities for four entry boreholes through the sediment overlying the basalt, up to three new deep rotary boreholes through the basalt and sedimentary interbeds, and one corehole through the basalt and sedimentary interbeds at the Waste Treatment Plant (WTP) site. The SAP will be used in concert with the quality assurance plan for the project to guide the procedure development and data collection activities needed to support borehole drilling, geophysical measurements, and sampling. This SAP identifies the American Society of Testing Materials standards, Hanford Site procedures, and other guidance to be followed for data collection activities.

  17. Adaptive Sampling Algorithms for Probabilistic Risk Assessment of Nuclear Simulations

    SciTech Connect (OSTI)

    Diego Mandelli; Dan Maljovec; Bei Wang; Valerio Pascucci; Peer-Timo Bremer

    2013-09-01T23:59:59.000Z

    Nuclear simulations are often computationally expensive, time-consuming, and high-dimensional with respect to the number of input parameters. Thus exploring the space of all possible simulation outcomes is infeasible using finite computing resources. During simulation-based probabilistic risk analysis, it is important to discover the relationship between a potentially large number of input parameters and the output of a simulation using as few simulation trials as possible. This is a typical context for performing adaptive sampling where a few observations are obtained from the simulation, a surrogate model is built to represent the simulation space, and new samples are selected based on the model constructed. The surrogate model is then updated based on the simulation results of the sampled points. In this way, we attempt to gain the most information possible with a small number of carefully selected sampled points, limiting the number of expensive trials needed to understand features of the simulation space. We analyze the specific use case of identifying the limit surface, i.e., the boundaries in the simulation space between system failure and system success. In this study, we explore several techniques for adaptively sampling the parameter space in order to reconstruct the limit surface. We focus on several adaptive sampling schemes. First, we seek to learn a global model of the entire simulation space using prediction models or neighborhood graphs and extract the limit surface as an iso-surface of the global model. Second, we estimate the limit surface by sampling in the neighborhood of the current estimate based on topological segmentations obtained locally. Our techniques draw inspirations from topological structure known as the Morse-Smale complex. We highlight the advantages and disadvantages of using a global prediction model versus local topological view of the simulation space, comparing several different strategies for adaptive sampling in both contexts. One of the most interesting models we propose attempt to marry the two by obtaining a coarse global representation using prediction models, and a detailed local representation based on topology. Our methods are validated on several analytical test functions as well as a small nuclear simulation dataset modeled after a simplified Pressurized Water Reactor.

  18. SAMPLE: Parity Violating Electron Scattering from Hydrogen and Deuterium

    E-Print Network [OSTI]

    E. J. Beise; J. Arrington; D. H. Beck; E. Candell; R. Carr; G. Dodson; K. Dow; F. Duncan; M. Farkhondeh; B. W. Filippone; T. FOrest; H. Gao; W. Korsch; S. Kowalski; A. Lung; R. D. McKeown; R. Mohring; B. A. Mueller; J. Napolitano; M. Pitt; N. Simicevic; E. Tsentalovich; S. Wells

    1996-02-06T23:59:59.000Z

    Recently, there has been considerable theoretical interest in determining strange quark contributions to hadronic matrix elements. Such matrix elements can be accessed through the nucleon's neutral weak form factors as determined in parity violating electron scattering. The SAMPLE experiment will measure the strange magnetic form factor $G_M^s$ at low momentum transfer. By combining measurements from hydrogen and deuterium the theoretical uncertainties in the measurement can be greatly reduced and the result will be limited by experimental errors only. A summary of recent progress on the SAMPLE experiment is presented.

  19. Sample preparation and detection device for infectious agents

    DOE Patents [OSTI]

    Miles, Robin R.; Wang, Amy W.; Fuller, Christopher K.; Lemoff, Asuncion V.; Bettencourt, Kerry A.; Yu, June

    2003-06-10T23:59:59.000Z

    A sample preparation and analysis device which incorporates both immunoassays and PCR assays in one compact, field-portable microchip. The device provides new capabilities in fluid and particle control which allows the building of a fluidic chip with no moving parts, thus decreasing fabrication cost and increasing the robustness of the device. The device can operate in a true continuous (not batch) mode. The device incorporates magnetohydrodynamic (MHD) pumps to move the fluid through the system, acoustic mixing and fractionation, dielectropheretic (DEP) sample concentration and purification, and on-chip optical detection capabilities.

  20. LANSCE | Lujan Center | Sample and Equipment Shipping Instructions

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample Environment: Magnet and cryostat systemSample Shipping

  1. Multi-Boson Correlation Interferometry and Boson Sampling in Time

    E-Print Network [OSTI]

    Vincenzo Tamma; Simon Laibacher

    2014-10-29T23:59:59.000Z

    We develop a general description of multi-boson interference based on correlated measurements in arbitrary passive linear interferometers for single input bosons with arbitrary temporal distributions. Our results allow us to fully describe boson sampling in time at the output of a random interferometer, in which the sampling takes place not only over the interferometer output ports but also over the joint-detection times. For any joint detection, both the time-dependent probability density and the time-averaged probability can be expressed by the permanents of matrices depending on the interferometer evolution and on the boson temporal distributions.

  2. Thermophoretic separation of aerosol particles from a sampled gas stream

    DOE Patents [OSTI]

    Postma, A.K.

    1984-09-07T23:59:59.000Z

    This disclosure relates to separation of aerosol particles from gas samples withdrawn from within a contained atmosphere, such as containment vessels for nuclear reactors or other process equipment where remote gaseous sampling is required. It is specifically directed to separation of dense aerosols including particles of any size and at high mass loadings and high corrosivity. The United States Government has rights in this invention pursuant to Contract DE-AC06-76FF02170 between the US Department of Energy and Westinghouse Electric Corporation.

  3. DOE-2 sample run book: Version 2.1E

    SciTech Connect (OSTI)

    Winkelmann, F.C.; Birdsall, B.E.; Buhl, W.F.; Ellington, K.L.; Erdem, A.E. [Lawrence Berkeley Lab., CA (United States); Hirsch, J.J.; Gates, S. [Hirsch (James J.) and Associates, Camarillo, CA (United States)

    1993-11-01T23:59:59.000Z

    The DOE-2 Sample Run Book shows inputs and outputs for a variety of building and system types. The samples start with a simple structure and continue to a high-rise office building, a medical building, three small office buildings, a bar/lounge, a single-family residence, a small office building with daylighting, a single family residence with an attached sunspace, a ``parameterized`` building using input macros, and a metric input/output example. All of the samples use Chicago TRY weather. The main purpose of the Sample Run Book is instructional. It shows the relationship of LOADS-SYSTEMS-PLANT-ECONOMICS inputs, displays various input styles, and illustrates many of the basic and advanced features of the program. Many of the sample runs are preceded by a sketch of the building showing its general appearance and the zoning used in the input. In some cases we also show a 3-D rendering of the building as produced by the program DrawBDL. Descriptive material has been added as comments in the input itself. We find that a number of users have loaded these samples onto their editing systems and use them as ``templates`` for creating new inputs. Another way of using them would be to store various portions as files that can be read into the input using the {number_sign}{number_sign} include command, which is part of the Input Macro feature introduced in version DOE-2.lD. Note that the energy rate structures here are the same as in the DOE-2.lD samples, but have been rewritten using the new DOE-2.lE commands and keywords for ECONOMICS. The samples contained in this report are the same as those found on the DOE-2 release files. However, the output numbers that appear here may differ slightly from those obtained from the release files. The output on the release files can be used as a check set to compare results on your computer.

  4. SOLVENT HOLD TANK SAMPLE RESULTS FOR MCU-13-1403/1404/1405/1406/1407/1408: QUARTERLY SAMPLE FROM SEPTEMBER 2013

    SciTech Connect (OSTI)

    Fondeur, F.; Taylor-Pashow, K.

    2013-11-20T23:59:59.000Z

    Savannah River National Laboratory (SRNL) analyzed solvent samples from the Modular Caustic-Side Solvent Extraction Unit (MCU) in support of continuing operations. A quarterly analysis of the solvent is required to maintain solvent composition within specifications. Analytical results of the analyses of Solvent Hold Tank (SHT) samples MCU-13-1403, MCU-13-1404, MCU-13-1405, MCU-13-1406, MCU-13-1407, and MCU-13-1408 received on September 17, 2013 are reported. This sample was taken after the addition of the Next Generation Solvent (NGS) cocktail to produce a NGS-MCU blended solvent. The results show that the solvent contains a slight excess of Isopar? L and a deficit concentration of modifier and TiDG when compared to the target composition. Addition of TiDG trim is recommended. SRNL also analyzed the SHT sample for {sup 137}Cs content and determined the measured value is within tolerance and that the value has returned to levels observed in 2011. In contrast to what was observed in the heel prior to adding the NGS cocktail, no organic impurities were detected in these solvent samples.

  5. Report on Electrochemcial Corrosion Testing of 241-SY-102 Grab Samples from the 2012 Grab Sampling Campaign

    SciTech Connect (OSTI)

    Wyrwas, Richard B.; Lamothe, Margaret E.

    2013-05-30T23:59:59.000Z

    This report describes the results of the electrochemical testing performed on tank 241-SY-102 (SY-102) grab samples that were collected in support of corrosion mitigation. The objective of the work presented here was to determine corrosion resistance of tank SY-102 to the grab samples collected using electrochemical methods up to 50°C as well as to satisfy data quality objectives. Grab samples were collected at multiple elevations from Riser 003. The electrochemical corrosion testing was planned to consist of linear polarization resistance testing (LPR) and cyclic potentiodynamic polarization (CPP) testing at 50°C. The temperature would be lowered to 40 °C and the test repeated if the CPP curve indicated pitting corrosion at 50°C. Ifno pitting was indicated by the CPP curve, then a duplicate scan would be repeated at 50°C to confirm the first result. The testing would be complete if the duplicate CPP scan was consistent with the first. This report contains the CPP results of the testing of grab sample 2SY-12-03 and 2SY-12-03DUP composite sample tested under these conditions. There was no indication of pitting at 50°C, and the duplicate scan was in agreement with the first scan. Since no further testing was required, a third scan with a shorter rest time was performed and is present in this report.

  6. A COMPLETE SAMPLE OF BRIGHT SWIFT LONG GAMMA-RAY BURSTS. I. SAMPLE PRESENTATION, LUMINOSITY FUNCTION AND EVOLUTION

    SciTech Connect (OSTI)

    Salvaterra, R. [INAF, IASF Milano, via E. Bassini 15, I-20133 Milano (Italy); Campana, S.; Vergani, S. D.; Covino, S.; D'Avanzo, P.; Fugazza, D.; Ghirlanda, G.; Ghisellini, G.; Melandri, A.; Sbarufatti, B.; Tagliaferri, G. [INAF, Osservatorio Astronomico di Brera, via E. Bianchi 46, I-23807 Merate (Saint Lucia) (Italy); Nava, L. [SISSA, via Bonomea 265, I-34136 Trieste (Italy); Flores, H. [Laboratoire GEPI, Observatoire de Paris, CNRS-UMR8111, Univ. Paris-Diderot 5 place Jules Janssen, 92195 Meudon (France); Piranomonte, S., E-mail: ruben@lambrate.inaf.it [INAF, Osservatorio Astronomico di Roma, via Frascati 33, 00040 Monte Porzio Catone, Rome (Italy)

    2012-04-10T23:59:59.000Z

    We present a carefully selected sub-sample of Swift long gamma-ray bursts (GRBs) that is complete in redshift. The sample is constructed by considering only bursts with favorable observing conditions for ground-based follow-up searches, which are bright in the 15-150 keV Swift/BAT band, i.e., with 1-s peak photon fluxes in excess to 2.6 photons s{sup -1} cm{sup -2}. The sample is composed of 58 bursts, 52 of them with redshift for a completeness level of 90%, while another two have a redshift constraint, reaching a completeness level of 95%. For only three bursts we have no constraint on the redshift. The high level of redshift completeness allows us for the first time to constrain the GRB luminosity function and its evolution with cosmic times in an unbiased way. We find that strong evolution in luminosity ({delta}{sub l} = 2.3 {+-} 0.6) or in density ({delta}{sub d} = 1.7 {+-} 0.5) is required in order to account for the observations. The derived redshift distributions in the two scenarios are consistent with each other, in spite of their different intrinsic redshift distributions. This calls for other indicators to distinguish among different evolution models. Complete samples are at the base of any population studies. In future works we will use this unique sample of Swift bright GRBs to study the properties of the population of long GRBs.

  7. Getting the Best Out of Fluid Samples John M. Williams, SPE, Science Support Services

    E-Print Network [OSTI]

    Williams, John M.

    and temperatures may be unstable. In bottomhole samples of a highly volatile oil or a gas condensate, no "break essentially involves collecting surface samples of the oil and gas from the production test separator, bottomhole samples from the wellbore, or both types of samples. For separator gas samples, the quality checks

  8. RAPID SEPARATION OF ACTINIDES AND RADIOSTRONTIUM IN VEGETATION SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.

    2010-06-01T23:59:59.000Z

    A new rapid method for the determination of actinides and radiostrontium in vegetation samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used in emergency response situations or for routine analysis. The actinides in vegetation method utilizes a rapid sodium hydroxide fusion method, a lanthanum fluoride matrix removal step, and a streamlined column separation process with stacked TEVA, TRU and DGA Resin cartridges. Lanthanum was separated rapidly and effectively from Am and Cm on DGA Resin. Alpha emitters are prepared using rare earth microprecipitation for counting by alpha spectrometry. The purified {sup 90}Sr fractions are mounted directly on planchets and counted by gas flow proportional counting. The method showed high chemical recoveries and effective removal of interferences. The actinide and {sup 90}Sr in vegetation sample analysis can be performed in less than 8 h with excellent quality for emergency samples. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory actinide particles or vegetation residue after furnace heating is effectively digested.

  9. November 21, 2000 PV Lesson Plan 2 Sample Questions & Answers

    E-Print Network [OSTI]

    Oregon, University of

    November 21, 2000 PV Lesson Plan 2 ­ Sample Questions & Answers Prepared for the Oregon Million Solar Roofs Coalition By Frank Vignola ­ University of Oregon Solar Radiation Monitoring Lab John Hocken your understanding: 1. The typical voltage of a silicon solar cell is about 0.5 volts; where does

  10. Nonparametric and semiparametric regression analysis of group testing samples

    E-Print Network [OSTI]

    Xie, Minge

    the assumption that the group testing result is positive if at least one individual sample in the corresponding designs in attempt to find optimal group size which minimizes the total number of tests under various and Verstraeten [13] suggested that testing pools can lower false positive and false negative rates in low

  11. Portable tester for determining gas content within a core sample

    DOE Patents [OSTI]

    Garcia, Jr., Fred (Donora, PA); Schatzel, Steven J. (Bethel Park, PA)

    1998-01-01T23:59:59.000Z

    A portable tester is provided for reading and displaying the pressure of a gas released from a rock core sample stored within a sealed container and for taking a sample of the released pressurized gas for chemical analysis thereof for subsequent use in a modified direct method test which determines the volume of gas and specific type of gas contained within the core sample. The portable tester includes a pair of low and high range electrical pressure transducers for detecting a gas pressure; a pair of low and high range display units for displaying the pressure of the detected gas- a selector valve connected to the low and high range pressure transducers, a selector knob for selecting gas flow to one of the flow paths; control valve having an inlet connection to the sealed container, and outlets connected to: a sample gas canister, a second outlet port connected to the selector valve means for reading the pressure of the gas from the sealed container to either the low range or high range pressure transducers, and a connection for venting gas contained within the sealed container to the atmosphere. A battery is electrically connected to and supplies the power for operating the unit. The pressure transducers, display units, selector and control valve means and the battery is mounted to and housed within a protective casing for portable transport and use.

  12. Biomolecular free energy profiles by a shootingumbrella sampling protocol, ``BOLAS''

    E-Print Network [OSTI]

    Schlick, Tamar

    Biomolecular free energy profiles by a shootingĂ?umbrella sampling protocol, ``BOLAS'' Ravi an efficient technique for computing free energies corresponding to conformational transitions in complex. This makes possible computation of free energy profiles along complex reaction coordinates for biomolecular

  13. Stratified source-sampling techniques for Monte Carlo eigenvalue analysis.

    SciTech Connect (OSTI)

    Mohamed, A.

    1998-07-10T23:59:59.000Z

    In 1995, at a conference on criticality safety, a special session was devoted to the Monte Carlo ''Eigenvalue of the World'' problem. Argonne presented a paper, at that session, in which the anomalies originally observed in that problem were reproduced in a much simplified model-problem configuration, and removed by a version of stratified source-sampling. In this paper, stratified source-sampling techniques are generalized and applied to three different Eigenvalue of the World configurations which take into account real-world statistical noise sources not included in the model problem, but which differ in the amount of neutronic coupling among the constituents of each configuration. It is concluded that, in Monte Carlo eigenvalue analysis of loosely-coupled arrays, the use of stratified source-sampling reduces the probability of encountering an anomalous result over that if conventional source-sampling methods are used. However, this gain in reliability is substantially less than that observed in the model-problem results.

  14. Two samples test for discrete power-law distributions

    E-Print Network [OSTI]

    Bessi, Alessandro

    2015-01-01T23:59:59.000Z

    Power-law distributions occur in wide variety of physical, biological, and social phenomena. In this paper, we propose a statistical hypothesis test based on the log-likelihood ratio to assess whether two samples of discrete data are drawn from the same power-law distribution.

  15. Rapid Screening of Complex Chemical Samples via Capillary Array Analysis

    SciTech Connect (OSTI)

    D. S. Anex; D. W. Neyer

    1998-11-01T23:59:59.000Z

    This report is a summary of the results of a two-year Laboratory-Directed Research and Development (LDRD) project that developed instrumentation and methods for capillary array analysis. During the course of this project, a new capillary array electrochromatography instrument was developed to perform eight simultaneous separations and provide complementary chromatographic information from each column on a single sample.

  16. A TOWED PUMP AND SHIPBOARD FILTERING SYSTEM FOR SAMPLING

    E-Print Network [OSTI]

    ;452: A TOWED PUMP AND SHIPBOARD FILTERING SYSTEM FOR SAMPLING SMALL ZOOPLANKTERS ,.^^»»r, Commissioner BUREAU OF Commercial Fisheries, Donald L. McKernan, Director A TOWED PUMP AND SHIPBOARD FILTERING Performance 13 Discussion 17 Summary 18 Literature cited 19 111 #12;#12;A TOWED PUMP AND SHIPBOARD FILTERING

  17. Robust and Scalable Sampling Algorithms for Network Measurement

    E-Print Network [OSTI]

    Wang, Xiaoming

    2010-10-12T23:59:59.000Z

    application in traffic monitoring, we introduce Discrete RIDE (D-RIDE), which allows one to sample each flow with a geometric random variable. Our numerous simulations and experiments with P2P networks and real Internet traces confirm that these algorithms...

  18. Groundwater and Leachate Monitoring and Sampling at ERDF, CY 2009

    SciTech Connect (OSTI)

    R.L. Weiss, B.L. Lawrence, D.W. Woolery

    2010-07-08T23:59:59.000Z

    This document reports the findings of the groundwater and leachate monitoring and sampling at the Environmental restoration Disposal Facility for calendar year 2009. The purpose of this annual monitoring report is to evaluate the conditions of and identify trends for groundwater beneath the ERDF and report leachate results in fulfillment of the requirements specified in the ERDF ROD and the ERDF Amended ROD.

  19. Blocking Gibbs Sampling in Very Large Probabilistic Expert Systems

    E-Print Network [OSTI]

    of Chicago 1118E 58th St. Chicago IL 60637 kong@galton.uchicago.edu U#11;e Kj#26;rul#11; Aalborg University converges much faster than plain Gibbs sampling for very complex problems. Keywords: probabilistic expert one shall be referred to as plain Gibbs. The evaluation of our blocking-Gibbs method is conducted

  20. Refractor Importance Sampling Haohai Yu and Robert A. van Engelen

    E-Print Network [OSTI]

    van Engelen, Robert A.

    al., 1995] properties that make these meth- ods more attractive compared to exact methods. Stochastic Chain Monte Carlo (MCMC) forms another important group of stochastic sampling algorithms. Examples., 1996, MacKay, 1998, Pearl, 1987, Chavez and Cooper, 1990]. Stratified sam- pling [Bouckaert, 1994