Sample records for diffraction-limited sample preparation

  1. PreparationSampleGuide:StartQuickISX Sample Preparation Guide

    E-Print Network [OSTI]

    straining the sample through a 70 micron nylon mesh strainer. If sample aggregation is a problem, we suggest

  2. Overcoming the far-field diffraction limit via absorbance modulation

    E-Print Network [OSTI]

    Tsai, Hsin-Yu Sidney

    2011-01-01T23:59:59.000Z

    Diffraction limits the resolution of far-field lithography and imaging to about half of the wavelength, which greatly limits the capability of optical techniques. The proposed technique with absorbance modulation aims to ...

  3. Preparation of Samples for Compositional Analysis: Laboratory...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    in the analysis. Procedures are listed that are suitable for the preparation of biomass feedstocks and a variety of biomass-derived materials. Representative sampling of biomass...

  4. Optimization of proteomic sample preparation procedures for comprehens...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    procedures for comprehensive protein characterization of pathogenic systems. Optimization of proteomic sample preparation procedures for comprehensive protein...

  5. Microfluidic DNA sample preparation method and device

    DOE Patents [OSTI]

    Krulevitch, Peter A. (Pleasanton, CA); Miles, Robin R. (Danville, CA); Wang, Xiao-Bo (San Diego, CA); Mariella, Raymond P. (Danville, CA); Gascoyne, Peter R. C. (Bellaire, TX); Balch, Joseph W. (Livermore, CA)

    2002-01-01T23:59:59.000Z

    Manipulation of DNA molecules in solution has become an essential aspect of genetic analyses used for biomedical assays, the identification of hazardous bacterial agents, and in decoding the human genome. Currently, most of the steps involved in preparing a DNA sample for analysis are performed manually and are time, labor, and equipment intensive. These steps include extraction of the DNA from spores or cells, separation of the DNA from other particles and molecules in the solution (e.g. dust, smoke, cell/spore debris, and proteins), and separation of the DNA itself into strands of specific lengths. Dielectrophoresis (DEP), a phenomenon whereby polarizable particles move in response to a gradient in electric field, can be used to manipulate and separate DNA in an automated fashion, considerably reducing the time and expense involved in DNA analyses, as well as allowing for the miniaturization of DNA analysis instruments. These applications include direct transport of DNA, trapping of DNA to allow for its separation from other particles or molecules in the solution, and the separation of DNA into strands of varying lengths.

  6. Flow Cytometry Instrument Policy & Penalties Sample Preparation

    E-Print Network [OSTI]

    Noble, James S.

    the integrity of the instrument, all samples must be filtered with a 40 µm mesh cell strainer just before

  7. Overcoming the Diffraction Limit Using Multiple Light Scattering in a Highly Disordered Medium

    E-Print Network [OSTI]

    Choi, Youngwoon

    We report that disordered media made of randomly distributed nanoparticles can be used to overcome the diffraction limit of a conventional imaging system. By developing a method to extract the original image information ...

  8. Preparation of Samples for Light Microscopy Simple Wax Seal

    E-Print Network [OSTI]

    Fygenson, Deborah Kuchnir

    Preparation of Samples for Light Microscopy Simple Wax Seal Materials - Slide - Cover Slip - Paraffin Wax Candle - Pasteur Pipette (suggested size 5 3/4 inch) - Matches Preparation of the Slide - You may want to protect the work surface from melted wax. We use a sheet of aluminum foil taped

  9. Fluidics platform and method for sample preparation and analysis

    DOE Patents [OSTI]

    Benner, W. Henry; Dzenitis, John M.; Bennet, William J.; Baker, Brian R.

    2014-08-19T23:59:59.000Z

    Herein provided are fluidics platform and method for sample preparation and analysis. The fluidics platform is capable of analyzing DNA from blood samples using amplification assays such as polymerase-chain-reaction assays and loop-mediated-isothermal-amplification assays. The fluidics platform can also be used for other types of assays and analyzes. In some embodiments, a sample in a sealed tube can be inserted directly. The following isolation, detection, and analyzes can be performed without a user's intervention. The disclosed platform may also comprises a sample preparation system with a magnetic actuator, a heater, and an air-drying mechanism, and fluid manipulation processes for extraction, washing, elution, assay assembly, assay detection, and cleaning after reactions and between samples.

  10. Repetitive petawatt-class laser with near-diffraction-limited focal spot and transform-limited pulse duration

    E-Print Network [OSTI]

    Umstadter, Donald

    Repetitive petawatt-class laser with near-diffraction-limited focal spot and transform-loop feedback control systems in the temporal and spatial domains are used to yield Fourier-transform acceleration and x-ray generation. Keywords: petawatt, diffraction limited, transform limited, spatial

  11. Sample preparation and detection device for infectious agents

    DOE Patents [OSTI]

    Miles, Robin R.; Wang, Amy W.; Fuller, Christopher K.; Lemoff, Asuncion V.; Bettencourt, Kerry A.; Yu, June

    2003-06-10T23:59:59.000Z

    A sample preparation and analysis device which incorporates both immunoassays and PCR assays in one compact, field-portable microchip. The device provides new capabilities in fluid and particle control which allows the building of a fluidic chip with no moving parts, thus decreasing fabrication cost and increasing the robustness of the device. The device can operate in a true continuous (not batch) mode. The device incorporates magnetohydrodynamic (MHD) pumps to move the fluid through the system, acoustic mixing and fractionation, dielectropheretic (DEP) sample concentration and purification, and on-chip optical detection capabilities.

  12. Apparatus for preparing a sample for mass spectrometry

    DOE Patents [OSTI]

    Villa-Aleman, Eliel (Aiken, SC)

    1994-01-01T23:59:59.000Z

    An apparatus for preparing a sample for analysis by a mass spectrometer system. The apparatus has an entry chamber and an ionization chamber separated by a skimmer. A capacitor having two space-apart electrodes followed by one or more ion-imaging lenses is disposed in the ionization chamber. The chamber is evacuated and the capacitor is charged. A valve injects a sample gas in the form of sample pulses into the entry chamber. The pulse is collimated by the skimmer and enters the ionization chamber. When the sample pulse passes through the gap between the electrodes, it discharges the capacitor and is thereby ionized. The ions are focused by the imaging lenses and enter the mass analyzer, where their mass and charge are analyzed.

  13. Apparatus for preparing a sample for mass spectrometry

    DOE Patents [OSTI]

    Villa-Aleman, E.

    1994-05-10T23:59:59.000Z

    An apparatus is described for preparing a sample for analysis by a mass spectrometer system. The apparatus has an entry chamber and an ionization chamber separated by a skimmer. A capacitor having two space-apart electrodes followed by one or more ion-imaging lenses is disposed in the ionization chamber. The chamber is evacuated and the capacitor is charged. A valve injects a sample gas in the form of sample pulses into the entry chamber. The pulse is collimated by the skimmer and enters the ionization chamber. When the sample pulse passes through the gap between the electrodes, it discharges the capacitor and is thereby ionized. The ions are focused by the imaging lenses and enter the mass analyzer, where their mass and charge are analyzed. 1 figures.

  14. Waste minimization in analytical chemistry through innovative sample preparation techniques.

    SciTech Connect (OSTI)

    Smith, L. L.

    1998-05-28T23:59:59.000Z

    Because toxic solvents and other hazardous materials are commonly used in analytical methods, characterization procedures result in significant and costly amount of waste. We are developing alternative analytical methods in the radiological and organic areas to reduce the volume or form of the hazardous waste produced during sample analysis. For the radiological area, we have examined high-pressure, closed-vessel microwave digestion as a way to minimize waste from sample preparation operations. Heated solutions of strong mineral acids can be avoided for sample digestion by using the microwave approach. Because reactivity increases with pressure, we examined the use of less hazardous solvents to leach selected contaminants from soil for subsequent analysis. We demonstrated the feasibility of this approach by extracting plutonium from a NET reference material using citric and tartaric acids with microwave digestion. Analytical results were comparable to traditional digestion methods, while hazardous waste was reduced by a factor often. We also evaluated the suitability of other natural acids, determined the extraction performance on a wider variety of soil types, and examined the extraction efficiency of other contaminants. For the organic area, we examined ways to minimize the wastes associated with the determination of polychlorinated biphenyls (PCBs) in environmental samples. Conventional methods for analyzing semivolatile organic compounds are labor intensive and require copious amounts of hazardous solvents. For soil and sediment samples, we have a method to analyze PCBs that is based on microscale extraction using benign solvents (e.g., water or hexane). The extraction is performed at elevated temperatures in stainless steel cells containing the sample and solvent. Gas chromatography-mass spectrometry (GC/MS) was used to quantitate the analytes in the isolated extract. More recently, we developed a method utilizing solid-phase microextraction (SPME) for natural water samples. In this SPME technique, a fused-silica fiber coated with a polymeric film is exposed to the sample, extraction is allowed to take place, and then the analytes are thermally desorbed for GC analysis. Unlike liquid-liquid extraction or solid-phase extraction, SPME consumes all of the extracted sample in the analysis, significantly reducing the required sample volume.

  15. Amphiphilic mediated sample preparation for micro-flow cytometry

    DOE Patents [OSTI]

    Clague, David S. (Livermore, CA); Wheeler, Elizabeth K. (Livermore, CA); Lee, Abraham P. (Irvine, CA)

    2006-07-25T23:59:59.000Z

    A flow cytometer includes a flow cell for detecting the sample, an oil phase in the flow cell, a water phase in the flow cell, an oil-water interface between the oil phase and the water phase, a detector for detecting the sample at the oil-water interface, and a hydrophobic unit operatively connected to the sample. The hydrophobic unit is attached to the sample. The sample and the hydrophobic unit are placed in an oil and water combination. The sample is detected at the interface between the oil phase and the water phase.

  16. Amphiphilic mediated sample preparation for micro-flow cytometry

    DOE Patents [OSTI]

    Clague, David S. (Livermore, CA); Wheeler, Elizabeth K. (Livermore, CA); Lee, Abraham P. (Irvine, CA)

    2009-03-17T23:59:59.000Z

    A flow cytometer includes a flow cell for detecting the sample, an oil phase in the flow cell, a water phase in the flow cell, an oil-water interface between the oil phase and the water phase, a detector for detecting the sample at the oil-water interface, and a hydrophobic unit operatively connected to the sample. The hydrophobic unit is attached to the sample. The sample and the hydrophobic unit are placed in an oil and water combination. The sample is detected at the interface between the oil phase and the water phase.

  17. Robots Help with Sample Preparation and Analysis at UNL Water Sciences Lab

    E-Print Network [OSTI]

    Nebraska-Lincoln, University of

    Robots Help with Sample Preparation and Analysis at UNL Water Sciences Lab By Daniel Snow, Ph of compounds. The other robotic system recently installed is a Spark Holland Symbiosys Environ coupled

  18. Sample preparation method for glass welding by ultrashort laser pulses yields higher seam strength

    SciTech Connect (OSTI)

    Cvecek, K.; Miyamoto, I.; Strauss, J.; Wolf, M.; Frick, T.; Schmidt, M.

    2011-05-01T23:59:59.000Z

    Glass welding by ultrashort laser pulses allows joining without the need of an absorber or a preheating and postheating process. However, cracks generated during the welding process substantially impair the joining strength of the welding seams. In this paper a sample preparation method is described that prevents the formation of cracks. The measured joining strength of samples prepared by this method is substantially higher than previously reported values.

  19. Analytical Chemistry Laboratory (ACL) procedure compendium. Volume 2, Sample preparation methods

    SciTech Connect (OSTI)

    Not Available

    1993-08-01T23:59:59.000Z

    This volume contains the interim change notice for sample preparation methods. Covered are: acid digestion for metals analysis, fusion of Hanford tank waste solids, water leach of sludges/soils/other solids, extraction procedure toxicity (simulate leach in landfill), sample preparation for gamma spectroscopy, acid digestion for radiochemical analysis, leach preparation of solids for free cyanide analysis, aqueous leach of solids for anion analysis, microwave digestion of glasses and slurries for ICP/MS, toxicity characteristic leaching extraction for inorganics, leach/dissolution of activated metal for radiochemical analysis, extraction of single-shell tank (SST) samples for semi-VOC analysis, preparation and cleanup of hydrocarbon- containing samples for VOC and semi-VOC analysis, receiving of waste tank samples in onsite transfer cask, receipt and inspection of SST samples, receipt and extrusion of core samples at 325A shielded facility, cleaning and shipping of waste tank samplers, homogenization of solutions/slurries/sludges, and test sample preparation for bioassay quality control program.

  20. Methodology for Optimal In Situ Alignment and Setting of Bendable Optics for Diffraction-Limited Focusing of Soft X-Rays

    E-Print Network [OSTI]

    Merthe, Daniel

    2013-01-01T23:59:59.000Z

    mirrors, x-rays, x-ray optics, synchrotron radiation,beamline, Kirkpatrick-Baez, metrology of x-ray opticsand Setting of Bendable Optics for Diffraction-Limited

  1. Impact of sample preparation on mineralogical analysis of zero-valent iron reactive barrier materials

    SciTech Connect (OSTI)

    Phillips, Debra Helen [ORNL; Gu, Baohua [ORNL; Watson, David B [ORNL; Roh, Yul [ORNL

    2003-03-01T23:59:59.000Z

    Permeable reactive barriers (PRBs) of zero-valent iron (Fe{sup 0}) are increasingly being used to remediate contaminated ground water. Corrosion of Fe{sup 0} filings and the formation of precipitates can occur when the PRB material comes in contact with ground water and may reduce the lifespan and effectiveness of the barrier. At present, there are no routine procedures for preparing and analyzing the mineral precipitates from Fe{sup 0} PRB material. These procedures are needed because mineralogical composition of corrosion products used to interpret the barrier processes can change with iron oxidation and sample preparation. The objectives of this study were (i) to investigate a method of preparing Fe{sup 0} reactive barrier material for mineralogical analysis by X-ray diffraction (XRD), and (ii) to identify Fe mineral phases and rates of transformations induced by different mineralogical preparation techniques. Materials from an in situ Fe{sup 0} PRB were collected by undisturbed coring and processed for XRD analysis after different times since sampling for three size fractions and by various drying treatments. We found that whole-sample preparation for analysis was necessary because mineral precipitates occurred within the PRB material in different size fractions of the samples. Green rusts quickly disappeared from acetone-dried samples and were not present in air-dried and oven-dried samples. Maghemite/magnetite content increased over time and in oven-dried samples, especially after heating to 105 C. We conclude that care must be taken during sample preparation of Fe{sup 0} PRB material, especially for detection of green rusts, to ensure accurate identification of minerals present within the barrier system.

  2. Chemical composition of esophageal-fistula forage samples as influenced by drying method, salivary leaching and sample preparation

    E-Print Network [OSTI]

    Acosta-Gonzalez, Rafael Aristides

    1976-01-01T23:59:59.000Z

    in partial fulfillment of the requirement for the degree of YASTER OF' SCI"'NCE, De"ember 1g76 CHEJJICAL COY!POSITION OF ESOPHAGEAL-FISTULA FORAGF SA(vPLES AS INFLUENCED BY DRYING I'METHOD, SALIVARY LEACHING AND SAMPLE PREPARATION A Thesis RAFAEL... ARISTIDES ACOS A-GONZALEZ Approved as to style and content by! (Cha rman o Committee) ((iced of Department) ( I'~iamb r ) Yemb r ) Dcc: mb~+~g~n'jrr ABSTRACT Chemical Composition of Esophageal-Fistula Forage Samples as Influenced by Drying Nethod...

  3. Method and apparatus for the preparation of liquid samples for determination of boron

    DOE Patents [OSTI]

    Siemer, Darryl D. (Idaho Falls, ID)

    1986-01-01T23:59:59.000Z

    A method and apparatus for the preparation of a liquid sample for the quantitative determination of boron by flame photometry. The sample is combined in a vessel with sulfuric acid, and an excess of methanol is added thereto. The methanol reacts with any boron present in the sample to form trimethyl borate which is volatilized by the heat of reaction between the excess methanol and sulfuric acid. The volatilized trimethyl borate is withdrawn from the vessel by either a partial vacuum or a positive pressure and is rapidly transferred to a standard flame photometer. The method is free of interference from typical boron concomitants.

  4. Applied Focused Ion Beam Techniques for Sample Preparation of Astromaterials for Integrated Nano-Analysis

    SciTech Connect (OSTI)

    Graham, G A; Teslich, N E; Kearsley, A T; Stadermann, F J; Stroud, R M; Dai, Z R; Ishii, H A; Hutcheon, I D; Bajt, S; Snead, C J; Weber, P K; Bradley, J P

    2007-02-20T23:59:59.000Z

    Sample preparation is always a critical step in study of micrometer sized astromaterials available for study in the laboratory, whether their subsequent analysis is by electron microscopy or secondary ion mass spectrometry. A focused beam of gallium ions has been used to prepare electron transparent sections from an interplanetary dust particle, as part of an integrated analysis protocol to maximize the mineralogical, elemental, isotopic and spectroscopic information extracted from one individual particle. In addition, focused ion beam techniques have been employed to extract cometary residue preserved on the rims and walls of micro-craters in 1100 series aluminum foils that were wrapped around the sample tray assembly on the Stardust cometary sample collector. Non-ideal surface geometries and inconveniently located regions of interest required creative solutions. These include support pillar construction and relocation of a significant portion of sample to access a region of interest. Serial sectioning, in a manner similar to ultramicrotomy, is a significant development and further demonstrates the unique capabilities of focused ion beam microscopy for sample preparation of astromaterials.

  5. Investigation of stimulated raman scattering using short-pulse diffraction limited laser beam near the instability threshold

    SciTech Connect (OSTI)

    Kline, John L [Los Alamos National Laboratory; Montgomery, David S [Los Alamos National Laboratory; Flippo, Kirk A [Los Alamos National Laboratory; Rose, Harvey A [Los Alamos National Laboratory; Yin, L [Los Alamos National Laboratory; Albright, B J [Los Alamos National Laboratory; Johnson, R P [Los Alamos National Laboratory; Shimada, T [Los Alamos National Laboratory; Bowers, K [Los Alamos National Laboratory; Rousseaux, C [CEA; Tassin, V [CEA; Baton, S D [FRANCE; Amiranoff, F [FRANCE; Hardin, R A [WEST VIRGINIA UNIV

    2008-01-01T23:59:59.000Z

    Short pulse laser plasma interaction experiments using diffraction limited beams provide an excellent platform to investigate the fundamental physics of Stimulated Raman Scattering. Detailed understanding of these laser plasma instabilities impacts the current inertial confinement fusion ignition designs and could potentially impact fast ignition when higher energy lasers are used with longer pulse durations ( > 1 kJ and> 1 ps). Using short laser pulses, experiments can be modeled over the entire interaction time of the laser using particle-in-cell codes to validate our understanding quantitatively. Experiments have been conducted at the Trident laser facility and the LULI (Laboratoire pour l'Utilisation des Lasers Intenses) to investigate stimulated Raman scattering near the threshold of the instability using 527 nm and 1059 nm laser light respectively with 1.5-3.0 ps pulses. In both experiments, the interaction beam was focused into a pre-ionized He gas-jet plasma. Measurements of the reflectivity as a function of intensity and k{lambda}{sub D} were completed at the Trident laser facility. At LULI, a 300 fs Thomson scattering probe is used to directly measure the density fluctuations of the driven electron plasma and ion acoustic waves. Work is currently underway comparing the results of the experiments with simulations using the VPIC [K. J. Bowers, et at., Phys. Plasmas, 15 055703 (2008)] particle-in-cell code. Details of the experimental results are presented in this manuscript.

  6. Enhancing the science return of Mars missions via sample preparation, robotic surface exploration and in orbit fuel production

    E-Print Network [OSTI]

    Lamamy, Julien-Alexandre, 1978-

    2004-01-01T23:59:59.000Z

    The future of Mars exploration is challenging from multiple points of view. To enhance their science return, future surface probes will most likely be equipped with complex Sample Preparation And Transfer (SPAT) facilities. ...

  7. A comparison of sample preparation methodology in the evaluation of geosynthetic clay liner (GCL) hydraulic conductivity

    SciTech Connect (OSTI)

    Siebken, J.R. [National Seal Co., Galesburg, IL (United States); Lucas, S. [Albarrie Naue Ltd., Barrie, Ontario (Canada)

    1997-11-01T23:59:59.000Z

    The method of preparing a single needle-punched GCL product for evaluation of hydraulic conductivity in a flexible wall permeameter was examined. The test protocol utilized for this evaluation was GRI Test Method GCL-2 Permeability of GCLs. The GCL product consisted of bentonite clay material supported by a woven and a non-woven geotextile on either side. The method preparation focused on the procedure for separating the test specimen from the larger sample and whether these methods produced difficulty in generating reliable test data. The methods examined included cutting with a razor knife, scissors, and a circular die with the perimeter of the test area under wet and dry conditions. In order to generate as much data as possible, tests were kept brief. Flow was monitored only long enough to determine whether or not preferential flow paths appeared to be present. The results appear to indicate that any of the methods involved will work. Difficulties arose not from the development of preferential flow paths around the edges of the specimens, but from the loss of bentonite from the edges during handling.

  8. Toward a Fieldable Atomic Mass Spectrometer for Safeguards Applications: Sample Preparation and Ionization

    SciTech Connect (OSTI)

    Barinaga, Charles J.; Hager, George J.; Hart, Garret L.; Koppenaal, David W.; Marcus, R. Kenneth; Jones, Sarah MH; Manard, Benjamin T.

    2014-10-31T23:59:59.000Z

    The International Atomic Energy Agency’s (IAEA’s) long-term research and development plan calls for the development of new methods to detect misuse at nuclear fuel cycle facilities such as reprocessing and enrichment plants. At enrichment plants, for example, the IAEA’s contemporary safeguards approaches are based on a combination of routine and random inspections that include collection of UF6 samples from in-process material and selected cylinders for subsequent analyses. These analyses include destructive analysis (DA) in a laboratory (typically by mass spectrometry [MS]) for isotopic characterization, and environmental sampling (ES) for subsequent laboratory elemental and isotopic analysis (also both typically by MS). One area of new method development includes moving this kind of isotope ratio analytical capability for DA and ES activities into the field. Some of the reasons for these developments include timeliness of results, avoidance of hazardous material shipments, and guidance for additional sample collecting. However, this capability does not already exist for several reasons, such as that most lab-based chemical and instrumental methods rely on laboratory infrastructure (highly trained staff, power, space, hazardous material handling, etc.) and require significant amounts of consumables (power, compressed gases, etc.). In addition, there are no currently available, fieldable instruments for atomic or isotope ratio analysis. To address these issues, Pacific Northwest National Laboratory (PNNL) and collaborator, Clemson University, are studying key areas that limit the fieldability of isotope ratio mass spectrometry for atomic ions: sample preparation and ionization, and reducing the physical size of a fieldable mass spectrometer. PNNL is seeking simple and robust techniques that could be effectively used by inspectors who may have no expertise in analytical MS. In this report, we present and describe the preliminary findings for three candidate techniques: matrix-assisted laser desorption/ionization (MALDI) MS, liquid sampling-atmospheric pressure glow discharge (LS-APGD), and laser ablation/ionization (LAI) MS at atmospheric pressure. Potential performance metrics for these techniques will be presented, including detectability, response, isotope ratio accuracy and precision, and ease of use.

  9. Surface Cleaning Techniques: Ultra-Trace ICP-MS Sample Preparation and Assay of HDPE

    SciTech Connect (OSTI)

    Overman, Nicole R.; Hoppe, Eric W.; Addleman, Raymond S.

    2013-06-01T23:59:59.000Z

    The world’s most sensitive radiation detection and assay systems depend upon ultra-low background (ULB) materials to reduce unwanted radiological backgrounds. Herein, we evaluate methods to clean HDPE, a material of interest to ULB systems and the means to provide rapid assay of surface and bulk contamination. ULB level material and ultra-trace level detection of actinide elements is difficult to attain, due to the introduction of contamination from sample preparation equipment such as pipette tips, sample vials, forceps, etc. and airborne particulate. To date, literature available on the cleaning of such polymeric materials and equipment for ULB applications and ultra-trace analyses is limited. For these reasons, a study has been performed to identify an effective way to remove surface contamination from polymers in an effort to provide improved instrumental detection limits. Inductively Coupled Plasma Mass Spectroscopy (ICP-MS) was utilized to assess the effectiveness of a variety of leachate solutions for removal of inorganic uranium and thorium surface contamination from polymers, specifically high density polyethylene (HDPE). HDPE leaching procedures were tested to optimize contaminant removal of thorium and uranium. Calibration curves for thorium and uranium ranged from 15 ppq (fg/mL) to 1 ppt (pg/mL). Detection limits were calculated at 6 ppq for uranium and 7 ppq for thorium. Results showed the most effective leaching reagent to be clean 6 M nitric acid for 72 hour exposures. Contamination levels for uranium and thorium found in the leachate solutions were significant for ultralow level radiation detection applications.

  10. Methods for preparing comparative standards and field samples for neutron activation analysis of soil

    SciTech Connect (OSTI)

    Glasgow, D.C.; Dyer, F.F.; Robinson, L.

    1994-06-01T23:59:59.000Z

    One of the more difficult problems associated with comparative neutron activation analysis (CNAA) is the preparation of standards which are tailor-made to the desired irradiation and counting conditions. Frequently, there simply is not a suitable standard available commercially, or the resulting gamma spectrum is convoluted with interferences. In a recent soil analysis project, the need arose for standards which contained about 35 elements. In response, a computer spreadsheet was developed to calculate the appropriate amount of each element so that the resulting gamma spectrum is relatively free of interferences. Incorporated in the program are options for calculating all of the irradiation and counting parameters including activity produced, necessary flux/bombardment time, counting time, and appropriate source-to-detector distance. The result is multi-element standards for CNAA which have optimal concentrations. The program retains ease of use without sacrificing capability. In addition to optimized standard production, a novel soil homogenization technique was developed which is a low cost, highly efficient alternative to commercially available homogenization systems. Comparative neutron activation analysis for large scale projects has been made easier through these advancements. This paper contains details of the design and function of the NAA spreadsheet and innovative sample handling techniques.

  11. Audit of the Union Valley sample preparation facility at Oak Ridge

    SciTech Connect (OSTI)

    NONE

    1997-11-07T23:59:59.000Z

    This audit was initiated to determine if the US DOE`s acquisition of the Union Valley Sample Preparation Facility (UVSPF) was necessary and cost effective. To accomplish the audit objective, four actions were taken: (1) review of applicable laws and regulations, (2) analysis of procurement files for the lease and interviews of Department and contractor officials, (3) evaluation of facility justifications, and (4) assessment of workload and staffing requirements of Lockheed Martin Energy Systems` Analytical Services Organization. The audit found that Energy Systems did not base the acquisition of the UVSPF on valid mission requirements. This occurred because Energy Systems did not follow Department procedures in planning and developing the lease, and the Department approved the lease without adequate justification. It was recommended that the Manager, Oak Ridge Operations Office: (1) direct Energy Systems to follow Department policies and procedures and base acquisitions of property on valid mission requirements and an analysis of all viable alternatives; (2) direct project managers to follow Department orders and require approvals of construction projects and property leases to include (a) verification that projects are essential to meet mission requirements and (b) analysis of all viable alternatives; and (3) direct Energy Systems to give the required 365-day notice and discontinue the lease. The audit also found that Energy Systems restricted the location of the UVSPF without establishing a programmatic need for the restriction. The restriction gave an Energy Systems subcontractor a competitive advantage and may have caused the Department to pay more than necessary for the facility. It was recommended that the Manager, Oak Ridge Operations Office, direct Energy Systems to discontinue the practice of restricting facility locations unless they are justified to meet mission requirements. The audit concluded that the UVSPF was not necessary.

  12. Portable sample preparation and analysis system for micron and sub-micron particle characterization using light scattering and absorption spectroscopy

    DOE Patents [OSTI]

    Stark, Peter C. (Los Alamos, NM); Zurek, Eduardo (Barranquilla, CO); Wheat, Jeffrey V. (Fort Walton Beach, FL); Dunbar, John M. (Santa Fe, NM); Olivares, Jose A. (Los Alamos, NM); Garcia-Rubio, Luis H. (Temple Terrace, FL); Ward, Michael D. (Los Alamos, NM)

    2011-07-26T23:59:59.000Z

    There is provided a method and device for remote sampling, preparation and optical interrogation of a sample using light scattering and light absorption methods. The portable device is a filtration-based device that removes interfering background particle material from the sample matrix by segregating or filtering the chosen analyte from the sample solution or matrix while allowing the interfering background particles to be pumped out of the device. The segregated analyte is then suspended in a diluent for analysis. The device is capable of calculating an initial concentration of the analyte, as well as diluting the analyte such that reliable optical measurements can be made. Suitable analytes include cells, microorganisms, bioparticles, pathogens and diseases. Sample matrixes include biological fluids such as blood and urine, as well as environmental samples including waste water.

  13. Flat Polishing for TEM sample preparation Things you will need to buy or borrow

    E-Print Network [OSTI]

    Devoret, Michel H.

    with sample Thickness adjustment knob #12;4 Mounting the sample 6. Crystal bond wax melts nicely at 150C, so flake of wax on it. Let the wax melt, then push your sample into it. Use just a small flake of wax. You don't want wax all over the holder. 7. Place the sample holder into the polishing puck, and retract

  14. LCLS Sample Preparation Laboratory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office of Science (SC)Integrated Codes |Is Your Home asLCLS Experimental Run Schedules Check-In |

  15. The Sample Preparation Laboratories | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOnItemResearch >Internship Program The NIF andPoints ofProject Home ProjectTheCynthia

  16. A Super-high Angular Resolution Principle for Coded-mask X-ray Imaging Beyond the Diffraction Limit of Single Pinhole

    E-Print Network [OSTI]

    Chen Zhang; Shuang Nan Zhang

    2008-06-25T23:59:59.000Z

    High angular resolution X-ray imaging is always demanded by astrophysics and solar physics, which can be realized by coded-mask imaging with very long mask-detector distance in principle. Previously the diffraction-interference effect has been thought to degrade coded-mask imaging performance dramatically at low energy end with very long mask-detector distance. In this work the diffraction-interference effect is described with numerical calculations, and the diffraction-interference cross correlation reconstruction method (DICC) is developed in order to overcome the imaging performance degradation. Based on the DICC, a super-high angular resolution principle (SHARP) for coded-mask X-ray imaging is proposed. The feasibility of coded mask imaging beyond the diffraction limit of single pinhole is demonstrated with simulations. With the specification that the mask element size of 50* 50 square micrometers and the mask-detector distance of 50 m, the achieved angular resolution is 0.32 arcsec above about 10 keV, and 0.36 arcsec at 1.24 keV where diffraction can not be neglected. The on-axis source location accuracy is better than 0.02 arcsec. Potential applications for solar observations and wide-field X-ray monitors are also shortly discussed.

  17. High Throughput Sample Preparation and Analysis for DNA Sequencing, PCR and Combinatorial Screening of Catalysis Based on Capillary Array Technique

    SciTech Connect (OSTI)

    Yonghua Zhang

    2002-05-27T23:59:59.000Z

    Sample preparation has been one of the major bottlenecks for many high throughput analyses. The purpose of this research was to develop new sample preparation and integration approach for DNA sequencing, PCR based DNA analysis and combinatorial screening of homogeneous catalysis based on multiplexed capillary electrophoresis with laser induced fluorescence or imaging UV absorption detection. The author first introduced a method to integrate the front-end tasks to DNA capillary-array sequencers. protocols for directly sequencing the plasmids from a single bacterial colony in fused-silica capillaries were developed. After the colony was picked, lysis was accomplished in situ in the plastic sample tube using either a thermocycler or heating block. Upon heating, the plasmids were released while chromsomal DNA and membrane proteins were denatured and precipitated to the bottom of the tube. After adding enzyme and Sanger reagents, the resulting solution was aspirated into the reaction capillaries by a syringe pump, and cycle sequencing was initiated. No deleterious effect upon the reaction efficiency, the on-line purification system, or the capillary electrophoresis separation was observed, even though the crude lysate was used as the template. Multiplexed on-line DNA sequencing data from 8 parallel channels allowed base calling up to 620 bp with an accuracy of 98%. The entire system can be automatically regenerated for repeated operation. For PCR based DNA analysis, they demonstrated that capillary electrophoresis with UV detection can be used for DNA analysis starting from clinical sample without purification. After PCR reaction using cheek cell, blood or HIV-1 gag DNA, the reaction mixtures was injected into the capillary either on-line or off-line by base stacking. The protocol was also applied to capillary array electrophoresis. The use of cheaper detection, and the elimination of purification of DNA sample before or after PCR reaction, will make this approach an attractive alternative to current methods for genetic analysis and disease diagnosis.

  18. Comparison of SW-846 method 3051 and SW-846 method 7471A for the preparation of solid waste samples for mercury determination

    SciTech Connect (OSTI)

    Giaquinto, J.M.; Essling, A.M.; Keller, J.M.

    1996-08-01T23:59:59.000Z

    This report describes experimental studies to evaluate the use of EPA SW-846 method 3051 for preparation and dissolution of solid samples for Hg analysis. The study showed that the method is effective in dissolution of four sample types without significant loss of Hg. Based on results of this study, method 3051 was used for analysis of high radioactive waste samples to obtain results for a number of RCRA regulated metals without the need to utilize a separate sample preparation method (EPA SW-846 method 7471A) specific only for Hg.

  19. Sample M&V Plan from the Texas Workshop: Preparing and Evaluating Measurement and Verification Plans for Energy Performance Contracts in Texas

    E-Print Network [OSTI]

    Haberl, J. S.

    1999-01-01T23:59:59.000Z

    This document contains a sample M&V plan that has been prepared in accordance with the Texas Guidelines for Measurement and Verification for Energy Performance Contracts. This sample M&V plan was extracted from the March 1999 workshop, entitled...

  20. Sample Preparation and Characterisation

    E-Print Network [OSTI]

    Cambridge, University of

    supplied by Corus RD&T. These were from creep tests, and comprised a screw-thread, which was used to hold.49 0.011 0.009 11.15 Mo Ni Nb V W 0.85 0.34 0.01 0.28 0.02 Table 6.2: Composition of creep-tested steel Fracture surface Screw thread Gauge Figure 6.1: Failed creep test specimen. The arrows show the position

  1. A Portable Cryo-Plunger for On-Site Intact Cryogenic Microscopy Sample Preparation in Natural Environments

    E-Print Network [OSTI]

    Knowles, David William

    in cryo-grid preparation and technological pro- gress in transmission electron microcopy (TEM) instru or propane at 808 K. They applied their technique to aqueous suspensions of biomolecules (Dubochet et al

  2. Negligible Sample Heating from Synchrotron Infrared Beam Michael C. Martina

    E-Print Network [OSTI]

    Negligible Sample Heating from Synchrotron Infrared Beam Michael C. Martina , Nelly M. Tsvetkovab of Molecular and Cellular Biology, University of California at Davis, USA Infrared (IR) spectroscopy is one can now obtain diffraction-limited spot sizes with high signal intensity in an infrared microscope

  3. Sample Preparation Laboratory Training - Course 204 | Sample Preparation

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level:Energy: Grid Integration Redefining What's PossibleRadiation Protection245C Unlimited ReleaseWelcome ton6 th US/German

  4. Chemical Resources | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625govInstrumentstdmadapInactiveVisiting the TWPSuccessAlamosCharacterization of SelectiveBrownFirst martianChemical

  5. Laboratory Access | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office of Science (SC)Integrated Codes |Is Your Home asLCLS ExperimentalFiveVentureFrontiers inAccess

  6. Laboratory Waste | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office of Science (SC)Integrated Codes |Is Your Home asLCLSLaboratory Directors LaboratoryPlanning

  7. Chemical Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office511041clothAdvanced Materials Advanced. C o w l i t z CPlasma of the Rotating 2015Analysis ofChemical

  8. Equipment Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOEThe Bonneville Power AdministrationField8,Dist. Category UC-l 1, 13 DE@Energy Innovation

  9. Geoscience Laboratory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office of Science (SC) Environmental AssessmentsGeoffrey CampbelllongApplyingGeorge T.Geoscience Laboratory

  10. LANSCE | Lujan Center | Chemical & Sample Prep

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Chemical & Sample Preparation For general questions, please contact the Lujan Center Chemical and Sample Preparation Laboratory responsible: Charles Kelsey | ckelsey@lanl.gov |...

  11. Pressurized fluidized-bed hydroretorting of eastern oil shales. Volume 4, Task 5, Operation of PFH on beneficiated shale, Task 6, Environmental data and mitigation analyses and Task 7, Sample procurement, preparation, and characterization: Final report, September 1987--May 1991

    SciTech Connect (OSTI)

    Not Available

    1992-03-01T23:59:59.000Z

    The objective of Task 5 (Operation of Pressurized Fluidized-Bed Hydro-Retorting (PFH) on Beneficiated Shale) was to modify the PFH process to facilitate its use for fine-sized, beneficiated Eastern shales. This task was divided into 3 subtasks: Non-Reactive Testing, Reactive Testing, and Data Analysis and Correlations. The potential environment impacts of PFH processing of oil shale must be assessed throughout the development program to ensure that the appropriate technologies are in place to mitigate any adverse effects. The overall objectives of Task 6 (Environmental Data and Mitigation Analyses) were to obtain environmental data relating to PFH and shale beneficiation and to analyze the potential environmental impacts of the integrated PFH process. The task was divided into the following four subtasks. Characterization of Processed Shales (IGT), 6.2. Water Availability and Treatment Studies, 6.3. Heavy Metals Removal and 6.4. PFH Systems Analysis. The objective of Task 7 (Sample Procurement, Preparation, and Characterization) was to procure, prepare, and characterize raw and beneficiated bulk samples of Eastern oil shale for all of the experimental tasks in the program. Accomplishments for these tasks are presented.

  12. Introduction Preparation

    E-Print Network [OSTI]

    Introduction Motivation Preparation Notos' Components Results Conclusions and Future Work Building Problem Description and Motivation Preparation Notation, Passive DNS trends and Anchor Classes Notos Reputation Results Conclusions and Future Work Special thanks to: Damballa Passive DNS data, Malware and BL

  13. Lucky exposures: diffraction limited astronomical imaging through the atmosphere

    E-Print Network [OSTI]

    Tubbs, Robert Nigel

    2003-11-25T23:59:59.000Z

    brightness are circled in red in d). In panels a)—c) the blurring effect of the PSFs re-distributes the flux from the point sources over a wider area of the image leading to a substantial reduction in the peak pixel values in the images. can be improved... to this method as the Lucky Exposures technique. A number of other authors have published results using very similar methods, particularly 1.3. Performance of ground-based high resolution imaging techniques 11 for solar and planetary observations. Observations...

  14. ALS Workshop Highlights Diffraction-Limited Storage Ring Opportunities

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office of ScienceandMesa del(ANL-IN-03-032)8Li (59AJ76) (See theDoctoral Fellowship inALSALSALSALSUsers'ALS

  15. ALS Workshop Highlights Diffraction-Limited Storage Ring Opportunities

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office of ScienceandMesa del(ANL-IN-03-032)8Li (59AJ76) (See theDoctoral Fellowship

  16. ALS Workshop Highlights Diffraction-Limited Storage Ring Opportunities

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOnItemResearch >InternshipDepartmentNeutrino-Induced1ALSALS RevealsALS Workshop

  17. Diffraction-Limited Soft X-Ray Workshop

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOEThe Bonneville Power AdministrationField Campaign: Potential ApplicationYu,

  18. Lithium Isotope Sample Preparation University of Maryland

    E-Print Network [OSTI]

    Mcdonough, William F.

    in the chemistries are methanol and ethanol, both ~100%, stored under cabinet #4, in the area marked "organics." It is necessary for the 12 ml Li column chemistry to use Teflon- distilled methanol. The ethanol that is used with ethanol used for removing ink from surfaces is ordinarily kept near the Milli-Q system. cleaning

  19. Sample preparation system for microfluidic applications

    DOE Patents [OSTI]

    Mosier, Bruce P. (San Francisco, CA); Crocker, Robert W. (Fremont, CA); Patel, Kamlesh D. (Dublin, CA); Harnett, Cindy K. (Livermore, CA)

    2007-05-08T23:59:59.000Z

    An apparatus that couples automated injection with flow feedback to provide nanoliter accuracy in controlling microliter volumes. The apparatus comprises generally a source of hydraulic fluid pressure, a fluid isolator joined to the outlet of the hydraulic pressure source and a flow sensor to provide pressure-driven analyte metering. For operation generally and particularly in microfluidic systems the hydraulic pressure source is typically an electrokinetic (EK) pump that incorporates gasless electrodes. The apparatus is capable of metering sub-microliter volumes at flowrates of 1 100 .mu.L/min into microsystem load pressures of up to 1000 50 psi, respectively. Flowrates can be specified within 0.5 .mu.L/min and volumes as small as 80 nL can be metered.

  20. 7 SAMPLING AND PREPARATION FOR LABORATORY MEASUREMENTS

    E-Print Network [OSTI]

    . Scanning is an evaluation technique performed by moving a portable radiation detection instrument time. Commonly used radiation detection and measuring equipment for radiological survey field

  1. Laboratory Equipment & Supplies | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office of Science (SC)Integrated Codes |Is Your Home asLCLSLaboratory Directors Laboratory Directors

  2. LCLS Equipment Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOEThe Bonneville PowerCherries 82981-1cnHigh SchoolIn12electron 9 5 - -/e),,s - 6157Bioenergy09913 35 FEL789LCLS

  3. LCLS Prep Lab Images | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOEThe Bonneville PowerCherries 82981-1cnHigh SchoolIn12electron 9 5 - -/e),,s - 6157Bioenergy09913

  4. Available for Checkout Equipment Inventory | Sample Preparation

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office511041cloth DocumentationProductsAlternativeOperationalAugust AugustInstruments on the

  5. BCM 1 Equipment Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office511041cloth DocumentationProductsAlternativeOperationalAugust Nazim Ali Bharmal, Comparisons ofBBQ - Is1

  6. BCM 2 Equipment Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office511041cloth DocumentationProductsAlternativeOperationalAugust Nazim Ali Bharmal, Comparisons ofBBQ - Is12

  7. Geoscience Equipment Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOEThe Bonneville Power AdministrationField8,Dist.Newof EnergyFundingGeneGenomeGeoffreyGeorge A.Fall Job

  8. Geoscience Prep Lab Slideshow | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOEThe Bonneville Power AdministrationField8,Dist.Newof EnergyFundingGeneGenomeGeoffreyGeorge A.Fall

  9. Petrographic characterization of Kentucky coals. Final report. Part V. Pyrite size/form/microlithotype distribution in western Kentucky prepared coals and in channel samples from western Kentucky and western Pennsylvania

    SciTech Connect (OSTI)

    Frankle, K.A.; Hower, J.C.

    1983-01-01T23:59:59.000Z

    Pyrite and marcasite distribution has been characterized in several western Kentucky coals, western Pennsylvania coals, and coals from western Kentucky preparation plants using three parameters of size, morphology, and microlithotype association. A classification system was developed to provide a consistent method for recording different pyrite/marcasite types. Sulfides were microscopically measured and placed in one of six size divisions (<5, 5 to 10, 10 to 40, 40 to 75, 75 to 100, or >150..mu..m) rather than absolute size. Five categories (euhedral, framboidal, dendritic, massive, or cleat) describe pyrite/marcasite morphology. The third parameter identifies the microlithotype (vitrite, clarite, inertite, liptite, durite, vitrinertite, trimacerite, or carbominerite) in which the pyrite occurs (not including the measured sulfide). Carbominerite is a mineral/organic association dominated by mineral matter. The percentage of each variable represents the total number of counts per sample and not the volume of pyrite. Throughout the studies, both sulfides are collectively referred to as pyrite unless otherwise specified. This paper describes the different studies which were undertaken to test the usefulness of this pyrite classification system. Systematic trends in pyrite variability were determined for the Springfield coal and Herrin of western Kentucky. Pyrite characterization of the Lower Kittanning coal from western Pennsylvania shows that certain pyrite morphologies can be an expression of the environments deposition of coal bodies. Studies of western Kentucky prepared coals demonstrate that pyrite characterization apparently can provide a method for predicting pyrite behavior and the extent of pyrite removal for specific coals. 77 references, 15 figures, 19 tables.

  10. TANK 5 SAMPLING

    SciTech Connect (OSTI)

    Vrettos, N; William Cheng, W; Thomas Nance, T

    2007-11-26T23:59:59.000Z

    Tank 5 at the Savannah River Site has been used to store high level waste and is currently undergoing waste removal processes in preparation for tank closure. Samples were taken from two locations to determine the contents in support of Documented Safety Analysis (DSA) development for chemical cleaning. These samples were obtained through the use of the Drop Core Sampler and the Snowbank Sampler developed by the Engineered Equipment & Systems (EES) group of the Savannah River National Laboratory (SRNL).

  11. Food Preparation Unit Preparation Materials and

    E-Print Network [OSTI]

    brush, potato masher, peeler, strainer, and steamer basket. · Food and kitchen equipment for preparation

  12. Sampling box

    DOE Patents [OSTI]

    Phillips, Terrance D. (617 Chestnut Ct., Aiken, SC 29803); Johnson, Craig (100 Midland Rd., Oak Ridge, TN 37831-0895)

    2000-01-01T23:59:59.000Z

    An air sampling box that uses a slidable filter tray and a removable filter cartridge to allow for the easy replacement of a filter which catches radioactive particles is disclosed.

  13. Use of Electrodeposition for Sample Preparation and Rejection Rate Prediction for Assay of Electroformed Ultra High Purity Copper for 232Th and 238U Prior to Inductively Coupled Plasma Mass Spectrometry (ICP/MS)

    SciTech Connect (OSTI)

    Hoppe, Eric W.; Aalseth, Craig E.; Brodzinski, Ronald L.; Day, Anthony R.; Farmer, Orville T.; Hossbach, Todd W.; McIntyre, Justin I.; Miley, Harry S.; Mintzer, Esther E.; Seifert, Allen; Smart, John E.; Warren, Glen A.

    2008-07-01T23:59:59.000Z

    The search for neutrinoless double beta decay in 76Ge has driven the need for ultra-low background Ge detectors shielded by electroformed copper of ultra-high radiopurity (<0.1µBq/kg). Although electrodeposition processes are almost sophisticated enough to produce copper of this purity, to date there are no methods sensitive enough to assay it. Inductively-coupled plasma mass spectrometry (ICP/MS) can detect thorium and uranium at femtogram levels, but in the past, this assay has been hindered by high copper concentrations in the sample. Electrodeposition of copper samples removes copper from the solution while selectively concentrating thorium and uranium contaminants to be assayed by ICP/MS. Spiking 232Th and 238U into the plating bath simulates low purity copper and allows for the calculation of the electrochemical rejection rate of thorium and uranium in the electroplating system. This rejection value will help to model plating bath chemistry.

  14. Offline solid phase microextraction sampling system

    DOE Patents [OSTI]

    Harvey, Chris A. (French Camp, CA)

    2008-12-16T23:59:59.000Z

    An offline solid phase microextraction (SPME) sampling apparatus for enabling SPME samples to be taken a number of times from a previously collected fluid sample (e.g. sample atmosphere) stored in a fused silica lined bottle which keeps volatile organics in the fluid sample stable for weeks at a time. The offline SPME sampling apparatus has a hollow body surrounding a sampling chamber, with multiple ports through which a portion of a previously collected fluid sample may be (a) released into the sampling chamber, (b) SPME sampled to collect analytes for subsequent GC analysis, and (c) flushed/purged using a fluidically connected vacuum source and purging fluid source to prepare the sampling chamber for additional SPME samplings of the same original fluid sample, such as may have been collected in situ from a headspace.

  15. Office Automation Document Preparation

    E-Print Network [OSTI]

    North Carolina at Chapel Hill, University of

    .2 Distinctions 1.3 Facilities 1.3.1 Document Preparation 1.3.2 Records Management 1.3.3 Communication 1 organizations contemplating the installation of document-preparation systems. * Administrative managersOffice Automation and Document Preparation for the v' University of North Carolina at Chapel Hill

  16. International perspectives on coal preparation

    SciTech Connect (OSTI)

    NONE

    1997-12-31T23:59:59.000Z

    The report consists of the vugraphs from the presentations which covered the following topics: Summaries of the US Department of Energy`s coal preparation research programs; Preparation trends in Russia; South African coal preparation developments; Trends in hard coal preparation in Germany; Application of coal preparation technology to oil sands extraction; Developments in coal preparation in China; and Coal preparation in Australia.

  17. automated sample preparation: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Websites Summary: of a partial automation since they act on the control part of the vehicle. This increasing automationABV- A Low Speed Automation Project to Study the...

  18. Intelligent front-end sample preparation tool using acoustic streaming.

    SciTech Connect (OSTI)

    Cooley, Erika J.; McClain, Jaime L.; Murton, Jaclyn K.; Edwards, Thayne L.; Achyuthan, Komandoor E.; Branch, Darren W.; Clem, Paul Gilbert; Anderson, John Mueller; James, Conrad D.; Smith, Gennifer; Kotulski, Joseph Daniel

    2009-09-01T23:59:59.000Z

    We have successfully developed a nucleic acid extraction system based on a microacoustic lysis array coupled to an integrated nucleic acid extraction system all on a single cartridge. The microacoustic lysing array is based on 36{sup o} Y cut lithium niobate, which couples bulk acoustic waves (BAW) into the microchannels. The microchannels were fabricated using Mylar laminates and fused silica to form acoustic-fluidic interface cartridges. The transducer array consists of four active elements directed for cell lysis and one optional BAW element for mixing on the cartridge. The lysis system was modeled using one dimensional (1D) transmission line and two dimensional (2D) FEM models. For input powers required to lyse cells, the flow rate dictated the temperature change across the lysing region. From the computational models, a flow rate of 10 {micro}L/min produced a temperature rise of 23.2 C and only 6.7 C when flowing at 60 {micro}L/min. The measured temperature changes were 5 C less than the model. The computational models also permitted optimization of the acoustic coupling to the microchannel region and revealed the potential impact of thermal effects if not controlled. Using E. coli, we achieved a lysing efficacy of 49.9 {+-} 29.92 % based on a cell viability assay with a 757.2 % increase in ATP release within 20 seconds of acoustic exposure. A bench-top lysing system required 15-20 minutes operating up to 58 Watts to achieve the same level of cell lysis. We demonstrate that active mixing on the cartridge was critical to maximize binding and release of nucleic acid to the magnetic beads. Using a sol-gel silica bead matrix filled microchannel the extraction efficacy was 40%. The cartridge based magnetic bead system had an extraction efficiency of 19.2%. For an electric field based method that used Nafion films, a nucleic acid extraction efficiency of 66.3 % was achieved at 6 volts DC. For the flow rates we tested (10-50 {micro}L/min), the nucleic acid extraction time was 5-10 minutes for a volume of 50 {micro}L. Moreover, a unique feature of this technology is the ability to replace the cartridges for subsequent nucleic acid extractions.

  19. Digital microfluidic sample preparation for biological mass spectrometry 

    E-Print Network [OSTI]

    Stokes, Adam A.

    2011-06-27T23:59:59.000Z

    The use of mass spectrometry in the biosciences has undergone huge growth in re- cent years due to sustained effort in the development of new ionisation techniques, more powerful mass analysers and better bioinformatic ...

  20. BCM1 Prep Lab Slideshow | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office511041cloth DocumentationProductsAlternativeOperationalAugust Nazim Ali Bharmal, Comparisons ofBBQ -

  1. BCM2 Prep Lab Slideshow | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOE Office511041cloth DocumentationProductsAlternativeOperationalAugust Nazim Ali Bharmal, Comparisons ofBBQ -BCM2

  2. Biology Chemistry & Material Science Laboratory 1 | Sample Preparation

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625govInstrumentstdmadapInactiveVisiting the TWP TWPAlumniComplexMaterialProductionBiological

  3. Biology Chemistry & Material Science Laboratory 2 | Sample Preparation

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625govInstrumentstdmadapInactiveVisiting the TWP TWPAlumniComplexMaterialProductionBiologicalLaboratories

  4. Preparation of acetaldehyde

    DOE Patents [OSTI]

    Tustin, G.C.; Depew, L.S.

    1997-10-21T23:59:59.000Z

    Disclosed is a process for the preparation of acetaldehyde by the hydrogenation of ketene in the presence of a transition metal hydrogenation catalyst.

  5. Method for preparing Pb-. beta. ''-alumina ceramic

    DOE Patents [OSTI]

    Hellstrom, E.E.

    1984-08-30T23:59:59.000Z

    A process is disclosed for preparing impermeable, polycrystalline samples of Pb-..beta..''-alumina ceramic from Na-..beta..''-alumina ceramic by ion exchange. The process comprises two steps. The first step is a high-temperature vapor phase exchange of Na by K, followed by substitution of Pb for K by immersing the sample in a molten Pb salt bath. The result is a polycrystalline Pb-..beta..''-alumina ceramic that is substantially crack-free.

  6. Aerosol preparation of intact lipoproteins

    DOE Patents [OSTI]

    Benner, W. Henry (Danville, CA); Krauss, Ronald M (Berkeley, CA); Blanche, Patricia J (Berkeley, CA)

    2012-01-17T23:59:59.000Z

    A medical diagnostic method and instrumentation system for analyzing noncovalently bonded agglomerated biological particles is described. The method and system comprises: a method of preparation for the biological particles; an electrospray generator; an alpha particle radiation source; a differential mobility analyzer; a particle counter; and data acquisition and analysis means. The medical device is useful for the assessment of human diseases, such as cardiac disease risk and hyperlipidemia, by rapid quantitative analysis of lipoprotein fraction densities. Initially, purification procedures are described to reduce an initial blood sample to an analytical input to the instrument. The measured sizes from the analytical sample are correlated with densities, resulting in a spectrum of lipoprotein densities. The lipoprotein density distribution can then be used to characterize cardiac and other lipid-related health risks.

  7. Think about it Preparing for Graduate School

    E-Print Network [OSTI]

    Sheridan, Jennifer

    Think about it Preparing for Graduate School Selecting Schools to Which You'll Apply Applying for Admittance The G.R.E. Writing Sample Campus Visits Graduate School Programs Your reasons for going to graduate school in English should go beyond simply that you like to read and write, that you like school

  8. North Sea Whitefish Survey: 2012 Prepared by

    E-Print Network [OSTI]

    ;2 Executive summary The North Sea Whitefish (NSW) survey sailed on 03 June 2012, fishing operations beganNorth Sea Whitefish Survey: 2012 Prepared by Chris Darby, Danny Normandale, Marta Soffker, Samantha samples were collected from cod, haddock and whiting for age determination. In 2009, throughout the survey

  9. AUTOMATED, ACCURATE, AND INEXPENSIVE SOLUTION-PREPARATION ON A DIGITAL MICROFLUIDIC BIOCHIP*

    E-Print Network [OSTI]

    Chakrabarty, Krishnendu

    AUTOMATED, ACCURATE, AND INEXPENSIVE SOLUTION- PREPARATION ON A DIGITAL MICROFLUIDIC BIOCHIP* Tao propose an electrowetting-based "digital" microfluidic biochip design for automated solution-crystallization application. Index Terms: Digital microfluidics, droplets, laboratory automation, sample preparation. I

  10. Measurement of the separation between atoms beyond diffraction limit RID A-5077-2009

    E-Print Network [OSTI]

    Chang, J. T.; Evers, J.; Scully, Marlan O.; Zubairy, M. Suhail

    2006-01-01T23:59:59.000Z

    ;7#4; E. Betzig, Opt. Lett. 20, 237 #1;1995#2;. #3;8#4; C. Hettich et al., Science 298, 385 #1;2002#2;. #3;9#4; R. H. Dicke, Phys. Rev. 93, 99 #1;1954#2;. #3;10#4; Z. Ficek and S. Swain, Quantum Interference and Coherence #1;Springer, Berlin, 2005..., and M. S. Zubairy, Phys. Rev. A 65, 043819 #1;2002#2;; M. Sahrai, H. Tajalli, K. T. Kapale, and M. S. Zubairy, ibid. 72, 013820 #1;2005#2;. #3;15#4; J. Eschner et al., Nature #1;London#2; 413, 495 #1;2001#2;; G. R. Guth?rleinet al., Nature #1;London...

  11. Optical imaging beyond the diffraction limit via dark states RID A-8711-2009

    E-Print Network [OSTI]

    Li, Hebin; Sautenkov, Vladimir A.; Kash, Michael M.; Sokolov, Alexei V.; Welch, George R.; Rostovtsev, Yuri V.; Zubairy, M. Suhail; Scully, Marlan O.

    2008-01-01T23:59:59.000Z

    We study the possibility of creating spatial patterns having subwavelength size by using the so-called dark states formed by the interaction between atoms and optical fields. These optical fields have a specified spatial distribution. Our...

  12. arbitrary sub-diffraction-limit pattern: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Washington at Seattle, University of 243 Synthesising arbitrary quantum states in a superconduct-ing resonator Computer Technologies and Information Sciences Websites Summary:...

  13. Sampling diffusive transition paths

    E-Print Network [OSTI]

    F. Miller III, Thomas

    2009-01-01T23:59:59.000Z

    Sampling di?usive transition paths Thomas F. Miller III ?the algorithm to sample the transition path ensemble for thedynamics I. INTRODUCTION Transition path sampling (TPS) is a

  14. Guide to preparing SAND Reports and other communication products.

    SciTech Connect (OSTI)

    Not Available

    2009-02-01T23:59:59.000Z

    This guide describes the R&A process, Common Look and Feel requirements, and preparation and publishing procedures for communication products at Sandia National Laboratories. Samples of forms and examples of published communications products are provided.

  15. Sampling and analyses report for postburn sampling at the RM1 UCG Site, Hanna, Wyoming

    SciTech Connect (OSTI)

    Crader, S.E.

    1989-06-01T23:59:59.000Z

    Between June 22, 1989 and June 26, 1989, Western Research Institute (WRI) completed the second quarterly Rocky Mountain 1 Underground Coal Gasification (RM1 UCG) site groundwater monitoring for the year 1989. This quarterly sample outing represents the third sampling since the completion of the RM1 groundwater restoration. Background material and the sampling and analytical procedures associated with this task are described in the `Rocky Mountain 1 Postburn Groundwater Monitoring Quality Assurance Plan`, prepared by the U.S. DOE.

  16. EXPORT CONTROLS PREPARED BY

    E-Print Network [OSTI]

    Sorin, Eric J.

    EXPORT CONTROLS MANUAL PREPARED BY: Office of General Counsel The California State University SEPTEMBER 2012 #12; Export Controls Manual Table of Contents I. INTRODUCTION ......................................................................................................... 1 II. HISTORY OF EXPORT CONTROLS

  17. Preparation of ethylenediamine dinitrate

    DOE Patents [OSTI]

    Lee, K.

    1984-05-17T23:59:59.000Z

    Method for the preparation of ethylenediamine dinitrate. Ethylenediamine dinitrate, a useful explosive, may readily be prepared by solvent extraction of nitrate ion from an acidic aqueous solution thereof using a high-molecular-weight, water-insoluble amine dissolved in an organic solvent, and reacting the resulting oraganic solution with ethylenediamine. The process of the instant invention avoids the use of concentrated nitric acid, as is currently practiced, resulting in a synthesis which is far less hazardous, especially for large quantities of the explosive, and more efficient.

  18. Preparation of ethylenediamine dinitrate

    DOE Patents [OSTI]

    Lee, Kien-yin (Los Alamos, NM)

    1985-01-01T23:59:59.000Z

    Method for the preparation of ethylenediamine dinitrate. Ethylenediamine dinitrate, a useful explosive, may readily be prepared by solvent extraction of nitrate ion from an acidic aqueous solution thereof using a high-molecular-weight, water-insoluble amine dissolved in an organic solvent, and reacting the resulting organic solution with ethylenediamine. The process of the instant invention avoids the use of concentrated nitric acid, as is currently practiced, resulting in a synthesis which is far less hazardous especially for large quantities of the explosive, and more efficient.

  19. E-Print Network 3.0 - a-exposed atlantic cod Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

  20. E-Print Network 3.0 - atlantic cod pineal Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

  1. E-Print Network 3.0 - atlantic cod piscidin Sample Search Results

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

  2. Preparation of graphitic articles

    DOE Patents [OSTI]

    Phillips, Jonathan; Nemer, Martin; Weigle, John C.

    2010-05-11T23:59:59.000Z

    Graphitic structures have been prepared by exposing templates (metal, metal-coated ceramic, graphite, for example) to a gaseous mixture that includes hydrocarbons and oxygen. When the template is metal, subsequent acid treatment removes the metal to yield monoliths, hollow graphitic structures, and other products. The shapes of the coated and hollow graphitic structures mimic the shapes of the templates.

  3. Preparation of vinyl acetate

    DOE Patents [OSTI]

    Tustin, G.C.; Zoeller, J.R.; Depew, L.S.

    1998-03-24T23:59:59.000Z

    This invention pertains to the preparation of vinyl acetate by contacting a mixture of hydrogen and ketene with a heterogeneous catalyst containing a transition metal to produce acetaldehyde, which is then reacted with ketene in the presence of an acid catalyst to produce vinyl acetate.

  4. Experiments: Preparation and Measurement

    E-Print Network [OSTI]

    Neumaier, Arnold

    the experimental set­up und the results of performing the experiment. Again, this is part of human cultureExperiments: Preparation and Measurement by Arnold Neumaier, Vienna March 1996 Abstract Introduction Experiments, properly arranged, provide information about a physical system by suitable

  5. ESPC IDIQ Contract Sample

    Broader source: Energy.gov [DOE]

    Document displays a sample indefinite delivery, indefinite quantity (IDIQ) energy savings performance contract (ESPC).

  6. TORIS Data Preparation Guidelines

    SciTech Connect (OSTI)

    Guinn, H.; Remson, D.

    1999-03-11T23:59:59.000Z

    The objective of this manual is to present guidelines and procedures for the preparation of new data for the Tertiary Oil Recovery Information System (TORIS) data base. TORIS is an analytical system currently maintained by the Department of Energy's (DOE) Bartlesville Project Office. It uses an extensive field- and reservoir-level data base to evaluate the technical and economic recovery potential of specific crude oil reservoirs.

  7. Rain sampling device

    DOE Patents [OSTI]

    Nelson, D.A.; Tomich, S.D.; Glover, D.W.; Allen, E.V.; Hales, J.M.; Dana, M.T.

    1991-05-14T23:59:59.000Z

    The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of the precipitation from the chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device. 11 figures.

  8. Rain sampling device

    DOE Patents [OSTI]

    Nelson, Danny A. (Richland, WA); Tomich, Stanley D. (Richland, WA); Glover, Donald W. (Prosser, WA); Allen, Errol V. (Benton City, WA); Hales, Jeremy M. (Kennewick, WA); Dana, Marshall T. (Richland, WA)

    1991-01-01T23:59:59.000Z

    The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of said precipitation from said chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device.

  9. Thermal oxidation procedure PREPARATION........................................................................................................................................... 2

    E-Print Network [OSTI]

    Hochberg, Michael

    procedure - 2 - Preparation. The preparation procedure sets up the power, gas supplies, cooling water, (DI to check all the supplies. Cooling water Gas supplies Routing DI water for wet oxidation We start........................................................................................................................................... 2 Step 1 Turn on the cooling water

  10. COMPUTER SCIENCE SAMPLE PROGRAM

    E-Print Network [OSTI]

    Gering, Jon C.

    COMPUTER SCIENCE SAMPLE PROGRAM (First Math Course MATH 198) This sample program suggests one way CS 181: Foundations of Computer Science II CS 180: Foundations of Computer Science I CS 191

  11. Preparation of tungsten oxide

    DOE Patents [OSTI]

    Bulian, Christopher J. (Yankton, SD); Dye, Robert C. (Los Alamos, NM); Son, Steven F. (Los Alamos, NM); Jorgensen, Betty S. (Jemez Springs, NM); Perry, W. Lee (Jemez Springs, NM)

    2009-09-22T23:59:59.000Z

    Tungsten trioxide hydrate (WO.sub.3.H.sub.2O) was prepared from a precursor solution of ammonium paratungstate in concentrated aqueous hydrochloric acid. The precursor solution was rapidly added to water, resulting in the crash precipitation of a yellow white powder identified as WO.sub.3.H.sub.2O nanosized platelets by x-ray diffraction and scanning electron microscopy. Annealing of the powder at 200.degree. C. provided cubic phase WO.sub.3 nanopowder, and at 400.degree. C. provided WO.sub.3 nanopowder as a mixture of monoclinic and orthorhombic phases.

  12. Surface preparation and plating

    SciTech Connect (OSTI)

    Dini, J.W.; Waldrop, F.B.; Reno, R.W.

    1982-10-06T23:59:59.000Z

    This chapter covers electroplating and electroless nickel plating since coatings of this type play an important role in diamond turning technology. Items to be discussed include preparation of substrates prior to coating, plating defects such as pits and nodules and their influence on optics, the influence of stress in coatings, plating details for copper, gold, silver, and electroless nickel, and the importance of additives and their influence on grain size and structure of deposits. Some comments are made on future challenges that could be presented to the plating community to further improve the quality of coatings applied for diamond turning purposes. 60 references, 8 figures, 9 tables.

  13. REMOTE REFURBISHMENT OF THE METALLOGRAPHY PREPARATION BOX AT THE INL

    SciTech Connect (OSTI)

    Adam B. Robinson; R. Paul Lind

    2010-09-01T23:59:59.000Z

    One of the most utilized hot cell capabilities at the Idaho National Laboratory is referred to as the containment box. This is where all destructive examination samples are prepared for analysis. This one window box is contained within the much larger Hot Fuels Examination Facility which consists of a 21x10x8 meter hot cell with an inert argon atmosphere. The refurbishment of this box entailed removing of all sample preparation equipment and support systems, as well as the design and installation of new preparation equipment. The new equipment consists of low and high speed saws, grinding and polishing equipment, water recirculation systems, and sample storage units. This paper includes the details of this refurbishment.

  14. Performance evaluation soil samples utilizing encapsulation technology

    DOE Patents [OSTI]

    Dahlgran, J.R.

    1999-08-17T23:59:59.000Z

    Performance evaluation soil samples and method of their preparation uses encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration. 1 fig.

  15. Performance evaluation soil samples utilizing encapsulation technology

    DOE Patents [OSTI]

    Dahlgran, James R. (Idaho Falls, ID)

    1999-01-01T23:59:59.000Z

    Performance evaluation soil samples and method of their preparation using encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration.

  16. ARTIFACT FORMATION DURING NEUTRALIZATION OF TANK 50 SAMPLES

    SciTech Connect (OSTI)

    Crump, S.; Young, J.

    2014-08-01T23:59:59.000Z

    Degradation products have been identified in the extracts of Tank 50 samples analyzed by semivolatile organic compound analysis (SVOA) using gas chromatography/mass spectrometry (GC/MS). These materials, identified as short chain alkyl alcohols, were formed by acidification during sample preparation. A number of questions were raised about the formation of these and other materials reported in Tank 50 surface samples, and this report serves to address these questions.

  17. Procedures for sampling radium-contaminated soils

    SciTech Connect (OSTI)

    Fleischhauer, H.L.

    1985-10-01T23:59:59.000Z

    Two procedures for sampling the surface layer (0 to 15 centimeters) of radium-contaminated soil are recommended for use in remedial action projects. Both procedures adhere to the philosophy that soil samples should have constant geometry and constant volume in order to ensure uniformity. In the first procedure, a ''cookie cutter'' fashioned from pipe or steel plate, is driven to the desired depth by means of a slide hammer, and the sample extracted as a core or plug. The second procedure requires use of a template to outline the sampling area, from which the sample is obtained using a trowel or spoon. Sampling to the desired depth must then be performed incrementally. Selection of one procedure over the other is governed primarily by soil conditions, the cookie cutter being effective in nongravelly soils, and the template procedure appropriate for use in both gravelly and nongravelly soils. In any event, a minimum sample volume of 1000 cubic centimeters is recommended. The step-by-step procedures are accompanied by a description of the minimum requirements for sample documentation. Transport of the soil samples from the field is then addressed in a discussion of the federal regulations for shipping radioactive materials. Interpretation of those regulations, particularly in light of their application to remedial action soil-sampling programs, is provided in the form of guidance and suggested procedures. Due to the complex nature of the regulations, however, there is no guarantee that our interpretations of them are complete or entirely accurate. Preparation of soil samples for radium-226 analysis by means of gamma-ray spectroscopy is described.

  18. IDENTIFICATION Your Sample Box

    E-Print Network [OSTI]

    Liskiewicz, Maciej

    to Virginia Tech Soil Testing Lab, 145 Smyth Hall (MC 0465), 185 Ag Quad Ln, Blacksburg VA 24061, in sturdy, K, Ca, Mg, Zn, Mn, Cu, Fe, B, and soluble salts) NoCharge $16.00 Organic Matter $4.00 $6.00 Fax with soil sample and form; make check or money order payable to "Treasurer, Virginia Tech." COST PER SAMPLE

  19. Sampling system and method

    DOE Patents [OSTI]

    Decker, David L.; Lyles, Brad F.; Purcell, Richard G.; Hershey, Ronald Lee

    2013-04-16T23:59:59.000Z

    The present disclosure provides an apparatus and method for coupling conduit segments together. A first pump obtains a sample and transmits it through a first conduit to a reservoir accessible by a second pump. The second pump further conducts the sample from the reservoir through a second conduit.

  20. Rehabilitation Services Sample Occupations

    E-Print Network [OSTI]

    Ronquist, Fredrik

    /Industries Correction Agencies Drug Treatment Centers Addiction Counselor Advocacy Occupations Art Therapist BehavioralRehabilitation Services Sample Occupations Sample Work Settings Child & Day Care Centers Clinics................................ IIB 29-1000 E4 Careers in Counseling and Human Services .........IIB 21-1010 C7 Careers in Health Care

  1. Process for preparing liquid wastes

    DOE Patents [OSTI]

    Oden, Laurance L. (Albany, OR); Turner, Paul C. (Albany, OR); O'Connor, William K. (Lebanon, OR); Hansen, Jeffrey S. (Corvallis, OR)

    1997-01-01T23:59:59.000Z

    A process for preparing radioactive and other hazardous liquid wastes for treatment by the method of vitrification or melting is provided for.

  2. Energy Fuels REnergy Fuels R PreparePrepare

    E-Print Network [OSTI]

    PrePre Energy Fuels REnergy Fuels R PreparePrepare Energy Fuels REnergy Fuels R 44 Union B44 Union 80228 Telephone: (303) 980-0540 Fax: (303) 985-2080 www.golder.com OFFICES ACROSS AFRICA, ASIA, AUSTRALIA, EUROPE, NORTH AMERICA AND SOUTH AMERICA TAILINGS CELL DESIGN REPORT PIÑON RIDGE PROJECT MONTROSE

  3. Waste classification sampling plan

    SciTech Connect (OSTI)

    Landsman, S.D.

    1998-05-27T23:59:59.000Z

    The purpose of this sampling is to explain the method used to collect and analyze data necessary to verify and/or determine the radionuclide content of the B-Cell decontamination and decommissioning waste stream so that the correct waste classification for the waste stream can be made, and to collect samples for studies of decontamination methods that could be used to remove fixed contamination present on the waste. The scope of this plan is to establish the technical basis for collecting samples and compiling quantitative data on the radioactive constituents present in waste generated during deactivation activities in B-Cell. Sampling and radioisotopic analysis will be performed on the fixed layers of contamination present on structural material and internal surfaces of process piping and tanks. In addition, dose rate measurements on existing waste material will be performed to determine the fraction of dose rate attributable to both removable and fixed contamination. Samples will also be collected to support studies of decontamination methods that are effective in removing the fixed contamination present on the waste. Sampling performed under this plan will meet criteria established in BNF-2596, Data Quality Objectives for the B-Cell Waste Stream Classification Sampling, J. M. Barnett, May 1998.

  4. PRTR ion exchange vault column sampling

    SciTech Connect (OSTI)

    Cornwell, B.C.

    1995-03-14T23:59:59.000Z

    This report documents ion exchange column sampling and Non Destructive Assay (NDA) results from activities in 1994, for the Plutonium Recycle Test Reactor (PRTR) ion exchange vault. The objective was to obtain sufficient information to prepare disposal documentation for the ion exchange columns found in the PRTR Ion exchange vault. This activity also allowed for the monitoring of the liquid level in the lower vault. The sampling activity contained five separate activities: (1) Sampling an ion exchange column and analyzing the ion exchange media for purpose of waste disposal; (2) Gamma and neutron NDA testing on ion exchange columns located in the upper vault; (3) Lower vault liquid level measurement; (4) Radiological survey of the upper vault; and (5) Secure the vault pending waste disposal.

  5. Sample Desorption/Onization From Mesoporous Silica

    DOE Patents [OSTI]

    Iyer, Srinivas (Los Alamos, NM); Dattelbaum, Andrew M. (Los Alamos, NM)

    2005-10-25T23:59:59.000Z

    Mesoporous silica is shown to be a sample holder for laser desorption/ionization of mass spectrometry. Supported mesoporous silica was prepared by coating an ethanolic silicate solution having a removable surfactant onto a substrate to produce a self-assembled, ordered, nanocomposite silica thin film. The surfactant was chosen to provide a desired pore size between about 1 nanometer diameter and 50 nanometers diameter. Removal of the surfactant resulted in a mesoporous silica thin film on the substrate. Samples having a molecular weight below 1000, such as C.sub.60 and tryptophan, were adsorbed onto and into the mesoporous silica thin film sample holder and analyzed using laser desorption/ionization mass spectrometry.

  6. The preparation and analysis of ammonia base sulfite pulping liquor

    E-Print Network [OSTI]

    Honstead, John Frederick

    1950-01-01T23:59:59.000Z

    much better check between results obtained by two different operators testing the same sample, and using the Palm- rose method. In a mill the liquor is test d b? shift men as the liquor is being prepared, and also by technicians in the laboratory...

  7. CHARACTERIZATION OF CORE SAMPLE COLLECTED FROM THE SALTSTONE DISPOSAL FACILITY

    SciTech Connect (OSTI)

    Cozzi, A.; Duncan, A.

    2010-01-28T23:59:59.000Z

    During the month of September 2008, grout core samples were collected from the Saltstone Disposal Facility, Vault 4, cell E. This grout was placed during processing campaigns in December 2007 from Deliquification, Dissolution and Adjustment Batch 2 salt solution. The 4QCY07 Waste Acceptance Criteria sample collected on 11/16/07 represents the salt solution in the core samples. Core samples were retrieved to initiate the historical database of properties of emplaced Saltstone and to demonstrate the correlation between field collected and laboratory prepared samples. Three samples were collected from three different locations. Samples were collected using a two-inch diameter concrete coring bit. In April 2009, the core samples were removed from the evacuated sample container, inspected, transferred to PVC containers, and backfilled with nitrogen. Samples furthest from the wall were the most intact cylindrically shaped cored samples. The shade of the core samples darkened as the depth of coring increased. Based on the visual inspection, sample 3-3 was selected for all subsequent analysis. The density and porosity of the Vault 4 core sample, 1.90 g/cm{sup 3} and 59.90% respectively, were comparable to values achieved for laboratory prepared samples. X-ray diffraction analysis identified phases consistent with the expectations for hydrated Saltstone. Microscopic analysis revealed morphology features characteristic of cementitious materials with fly ash and calcium silicate hydrate gel. When taken together, the results of the density, porosity, x-ray diffraction analysis and microscopic analysis support the conclusion that the Vault 4, Cell E core sample is representative of the expected waste form.

  8. CITIZENSHIP NOW! EXAM PREPARATION HANDBOOK

    E-Print Network [OSTI]

    Qiu, Weigang

    CITIZENSHIP NOW! EXAM PREPARATION HANDBOOK #12;washington oregon nevada idaho montananorthdakota to offer targeted programs--Si Se Puede!, a joint education initiative between CUNY and the Consulate NOW! EXAM PREPARATION HANDBOOK #12;T he City University of New York is the nation's largest urban

  9. Sample Changes and Issues

    Annual Energy Outlook 2013 [U.S. Energy Information Administration (EIA)]

    EIA-914 Survey and HPDI. Figure 2 shows how this could change apparent production. The blue line shows the reported sample production as it would normally be reported under the...

  10. Water Sample Concentrator

    ScienceCinema (OSTI)

    Idaho National Laboratory

    2010-01-08T23:59:59.000Z

    Automated portable device that concentrates and packages a sample of suspected contaminated water for safe, efficient transport to a qualified analytical laboratory. This technology will help safeguard against pathogen contamination or chemical and biolog

  11. Dissolution actuated sample container

    DOE Patents [OSTI]

    Nance, Thomas A.; McCoy, Frank T.

    2013-03-26T23:59:59.000Z

    A sample collection vial and process of using a vial is provided. The sample collection vial has an opening secured by a dissolvable plug. When dissolved, liquids may enter into the interior of the collection vial passing along one or more edges of a dissolvable blocking member. As the blocking member is dissolved, a spring actuated closure is directed towards the opening of the vial which, when engaged, secures the vial contents against loss or contamination.

  12. SAMPLING AND ANALYSIS PROTOCOLS

    SciTech Connect (OSTI)

    Jannik, T; P Fledderman, P

    2007-02-09T23:59:59.000Z

    Radiological sampling and analyses are performed to collect data for a variety of specific reasons covering a wide range of projects. These activities include: Effluent monitoring; Environmental surveillance; Emergency response; Routine ambient monitoring; Background assessments; Nuclear license termination; Remediation; Deactivation and decommissioning (D&D); and Waste management. In this chapter, effluent monitoring and environmental surveillance programs at nuclear operating facilities and radiological sampling and analysis plans for remediation and D&D activities will be discussed.

  13. Liquid sampling system

    DOE Patents [OSTI]

    Larson, L.L.

    1984-09-17T23:59:59.000Z

    A conduit extends from a reservoir through a sampling station and back to the reservoir in a closed loop. A jet ejector in the conduit establishes suction for withdrawing liquid from the reservoir. The conduit has a self-healing septum therein upstream of the jet ejector for receiving one end of a double-ended cannula, the other end of which is received in a serum bottle for sample collection. Gas is introduced into the conduit at a gas bleed between the sample collection bottle and the reservoir. The jet ejector evacuates gas from the conduit and the bottle and aspirates a column of liquid from the reservoir at a high rate. When the withdrawn liquid reaches the jet ejector the rate of flow therethrough reduces substantially and the gas bleed increases the pressure in the conduit for driving liquid into the sample bottle, the gas bleed forming a column of gas behind the withdrawn liquid column and interrupting the withdrawal of liquid from the reservoir. In the case of hazardous and toxic liquids, the sample bottle and the jet ejector may be isolated from the reservoir and may be further isolated from a control station containing remote manipulation means for the sample bottle and control valves for the jet ejector and gas bleed. 5 figs.

  14. Liquid sampling system

    DOE Patents [OSTI]

    Larson, Loren L. (Idaho Falls, ID)

    1987-01-01T23:59:59.000Z

    A conduit extends from a reservoir through a sampling station and back to the reservoir in a closed loop. A jet ejector in the conduit establishes suction for withdrawing liquid from the reservoir. The conduit has a self-healing septum therein upstream of the jet ejector for receiving one end of a double-ended cannula, the other end of which is received in a serum bottle for sample collection. Gas is introduced into the conduit at a gas bleed between the sample collection bottle and the reservoir. The jet ejector evacuates gas from the conduit and the bottle and aspirates a column of liquid from the reservoir at a high rate. When the withdrawn liquid reaches the jet ejector the rate of flow therethrough reduces substantially and the gas bleed increases the pressure in the conduit for driving liquid into the sample bottle, the gas bleed forming a column of gas behind the withdrawn liquid column and interrupting the withdrawal of liquid from the reservoir. In the case of hazardous and toxic liquids, the sample bottle and the jet ejector may be isolated from the reservoir and may be further isolated from a control station containing remote manipulation means for the sample bottle and control valves for the jet ejector and gas bleed.

  15. Sample storage/disposal study

    SciTech Connect (OSTI)

    Valenzuela, B.D.

    1994-09-29T23:59:59.000Z

    Radioactive waste from defense operations has accumulated at the Hanford Site`s underground waste tanks since the late 1940`s. Each tank must be analyzed to determine whether it presents any harm to the workers at the Hanford Site, the public or the environment. Analyses of the waste aids in the decision making process in preparation of future tank waste stabilization procedures. Characterization of the 177 waste tanks on the Hanford Site will produce a large amount of archived material. This also brings up concerns as to how the excess waste tank sample material from 325 and 222-S Analytical Laboratories will be handled. Methods to archive and/or dispose of the waste have been implemented into the 222-S and 325 Laboratory procedures. As the amount of waste characterized from laboratory analysis grows, an examination of whether the waste disposal system will be able to compensate for this increase in the amount of waste needs to be examined. Therefore, the need to find the safest, most economically sound method of waste storage/disposal is important.

  16. Fluid sampling system

    DOE Patents [OSTI]

    Houck, E.D.

    1994-10-11T23:59:59.000Z

    An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to be decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank. 4 figs.

  17. Fluid sampling system

    DOE Patents [OSTI]

    Houck, Edward D. (Idaho Falls, ID)

    1994-01-01T23:59:59.000Z

    An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank.

  18. Microfluidic preparative free-flow isoelectric focusing in a triangular channel: System development and characterization

    E-Print Network [OSTI]

    Wen, Jian

    A preparative scale free-flow IEF device is developed and characterized with the aim of addressing needs of molecular biologists working with protein samples on the milligrams and milliliters scale. A triangular-shape ...

  19. Viscous sludge sample collector

    DOE Patents [OSTI]

    Beitel, George A [Richland, WA

    1983-01-01T23:59:59.000Z

    A vertical core sample collection system for viscous sludge. A sample tube's upper end has a flange and is attached to a piston. The tube and piston are located in the upper end of a bore in a housing. The bore's lower end leads outside the housing and has an inwardly extending rim. Compressed gas, from a storage cylinder, is quickly introduced into the bore's upper end to rapidly accelerate the piston and tube down the bore. The lower end of the tube has a high sludge entering velocity to obtain a full-length sludge sample without disturbing strata detail. The tube's downward motion is stopped when its upper end flange impacts against the bore's lower end inwardly extending rim.

  20. Experimental Scattershot Boson Sampling

    E-Print Network [OSTI]

    Marco Bentivegna; Nicolò Spagnolo; Chiara Vitelli; Fulvio Flamini; Niko Viggianiello; Ludovico Latmiral; Paolo Mataloni; Daniel J. Brod; Ernesto F. Galvão; Andrea Crespi; Roberta Ramponi; Roberto Osellame; Fabio Sciarrino

    2015-05-14T23:59:59.000Z

    Boson Sampling is a computational task strongly believed to be hard for classical computers, but efficiently solvable by orchestrated bosonic interference in a specialised quantum computer. Current experimental schemes, however, are still insufficient for a convincing demonstration of the advantage of quantum over classical computation. A new variation of this task, Scattershot Boson Sampling, leads to an exponential increase in speed of the quantum device, using a larger number of photon sources based on parametric downconversion. This is achieved by having multiple heralded single photons being sent, shot by shot, into different random input ports of the interferometer. Here we report the first Scattershot Boson Sampling experiments, where six different photon-pair sources are coupled to integrated photonic circuits. We employ recently proposed statistical tools to analyse our experimental data, providing strong evidence that our photonic quantum simulator works as expected. This approach represents an important leap toward a convincing experimental demonstration of the quantum computational supremacy.

  1. Ammonia Results Review for Retained Gas Sampling

    SciTech Connect (OSTI)

    Mahoney, Lenna A.

    2000-09-20T23:59:59.000Z

    This report was prepared as part of a task supporting the deployment of the retained gas sampler (RGS) system in Flammable Gas Watch List Tanks. The emphasis of this report is on presenting supplemental information about the ammonia measurements resulting from retained gas sampling of Tanks 241-AW-101, A-101, AN-105, AN-104, AN-103, U-103, S-106, BY-101, BY-109, SX-106, AX-101, S-102, S-111, U-109, and SY-101. This information provides a better understanding of the accuracy of past RGS ammonia measurements, which will assist in determining flammable and toxicological hazards.

  2. GUM Analysis for TIMS Isotopic Ratios in BEP0 Graphite Qualification Samples, Round 2

    SciTech Connect (OSTI)

    Gerlach, David C.; Heasler, Patrick G.; Reid, Bruce D.

    2009-01-01T23:59:59.000Z

    In May 2007, one set of three samples from NBL were addressed to Steve Petersen for TIMS analysis, and included BEP0 samples numbered 27008, 30986, and 50846. All cores were trimmed by tooling, and lightly cleaned by CO2 pellet blasting. Small discs were cut from the second set of samples for SIMS analysis, with the remainder of each used for TIMS preparation.

  3. Preparing for Transfer Biological Engineering

    E-Print Network [OSTI]

    Walter, M.Todd

    Environmental Engineering Game Design Industrial Systems & Information Technology Information Science MaterialsPreparing for Transfer Majors: Biological Engineering Chemical Engineering Civil Engineering Computer Science Electrical & Computer Engineering Engineering Physics Environmental Engineering

  4. Preparation of waste oil for analysis to determine hazardous metals

    SciTech Connect (OSTI)

    Essling, A.M.; Huff, D.R.; Huff, E.A.; Fox, I.M.; Graczyk, D.G.

    1995-07-01T23:59:59.000Z

    Two methods for preparing waste-oil samples to permit measurement of their metals content were evaluated. For this evaluation, metals-in-oil standard reference materials were prepared by each method and the resulting solutions were analyzed for 20 metals, including those (As, Ba, Cd, Cr, Pb, Hg, Se, and Ag) regulated as hazardous under the Resource Conservation and Recovery Act. One preparation method involved combustion of the waste oil under oxygen at 25 atm pressure, as described in the American Society for Testing and Materials test method E926-88. As we applied it, this method gave recoveries well under 90% for most of the metals that we examined and, hence, proved unsatisfactory for routine application to waste-oil analysis. With the other method, nitric acid decomposition in a sealed vessel heated with microwave energy (analogous to US Environmental Protection Agency Method 3051), recoveries of all 20 metal contaminants were within 90 to 110% of the certified values. This microwave digestion procedure was also more efficient since it allowed six samples to be prepared together, whereas the oxygen combustion approach allowed processing of only one sample at a time.

  5. Environmental Science: Sample Pathway

    E-Print Network [OSTI]

    Goldberg, Bennett

    Environmental Science: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Core GE 100 & 124) MA 115 Statistics Summer Environmental Internship Junior Year CH 171 Chem for Health Sciences CH in Environmental Sciences is 17 courses. Courses taken to satisfy CAS major requirements (required, principal, core

  6. Observation of coupled plasmon-polariton modes of plasmon waveguides for electromagnetic energy transport below the diffraction limit

    E-Print Network [OSTI]

    Southern California, University of

    Observation of coupled plasmon-polariton modes of plasmon waveguides for electromagnetic energy the influence of optical near-field interactions on the dipole surface plasmon resonance of Au nanoparticles, the resonance energies of the collective plasmon-polariton modes are determined for longitudinal and transverse

  7. The Scattering Polarization of the Sr I 4607 ÅLine at the Diffraction Limit Resolution of a 1-m Telescope

    E-Print Network [OSTI]

    Javier Trujillo Bueno; Nataliya Shchukina

    2007-06-15T23:59:59.000Z

    One of the greatest challenges in solar and stellar physics in coming years will be to observe the Second Solar Spectrum with a spatial resolution significantly better than 1 arcsec. This type of scattering polarization observations would probably allow us to discover hitherto unknown aspects of the Sun's hidden magnetism. Here we report on some theoretical predictions for the photospheric line of Sr I at 4607 \\AA, which we have obtained by solving the three-dimensional (3D) radiative transfer problem of scattering line polarization in a realistic hydrodynamical model of the solar photosphere. We have taken into account not only the anisotropy of the radiation field in the 3D medium and the Hanle effect of a tangled magnetic field, but also the symmetry breaking effects caused by the horizontal atmospheric inhomogeneities produced by the solar surface convection. Interestingly, the Q/I and U/I linear polarization signals of the emergent spectral line radiation have sizable values and fluctuations, even at the very center of the solar disk where we meet the forward scattering case. The ensuing small-scale patterns in Q/I and U/I turn out to be sensitive to the assumed magnetic field model, and are of great diagnostic value. We argue that it should be possible to observe them with the help of a 1-m telescope equipped with adaptive optics and a suitable polarimeter.

  8. November 21, 2000 PV Lesson Plan 2 Sample Questions & Answers

    E-Print Network [OSTI]

    Oregon, University of

    November 21, 2000 PV Lesson Plan 2 ­ Sample Questions & Answers Prepared for the Oregon Million a single PV cell produces; so how can you get the amperage that you need? 4. You want to run your small CD player that requires 17 Watts. If you have a 12% efficient PV array operating about noon on a sunny day

  9. REVIEW OF DIESEL PARTICULATE MATTER SAMPLING FINAL REPORT

    E-Print Network [OSTI]

    Minnesota, University of

    REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS FINAL REPORT Prepared by David B. Kittelson of Mechanical Engineering Center for Diesel Research Minneapolis, MN January 14, 1999 #12;01/14/99 Page 2 TABLE ................................................................................................................5 DIESEL ENGINE TECHNOLOGY AND EMISSION REGULATIONS .............................7 PHYSICAL

  10. Natural Radioactivity of Boron Added Clay Samples

    SciTech Connect (OSTI)

    Akkurt, I.; Guenoglu, K. [Sueleyman Demirel University, Faculty of Arts and Sciences, Dept. of Physics, Isparta (Turkey); Canakcii, H. [Gaziantep University, Engineering Faculty, Civil Engineering Dept., Gaziantep (Turkey); Mavi, B. [Amasya University, Faculty of Arts and Sciences, Dept. of Physics, Amasya (Turkey)

    2011-12-26T23:59:59.000Z

    Clay, consisting fine-grained minerals, is an interesting materials and can be used in a variety of different fields especially in dermatology application. Using clay such a field it is important to measure its natural radioactivity. Thus the purpose of this study is to measure {sup 226}Ra, {sup 232}Th and {sup 40}K concentration in clay samples enriched with boron. Three different types of clay samples were prepared where boron is used in different rate. The measurements have been determined using a gamma-ray spectrometry consists of a 3''x3'' NaI(Tl) detector. From the measured activity the radium equivalent activities (Ra{sub eq}), external hazard index (H{sub ex}), absorbed dose rate in air (D) and annual effective dose (AED) have also been obtained.

  11. Preparation, Characterization, and Catalytic Properties of Tungsten...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Preparation, Characterization, and Catalytic Properties of Tungsten Trioxide Cyclic Trimers on FeO(111)Pt(111). Preparation, Characterization, and Catalytic Properties of Tungsten...

  12. Business Owners: Prepare for Utility Disruptions | Department...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Utility Disruptions Business Owners: Prepare for Utility Disruptions Business Owners: Prepare for Utility Disruptions Have a plan in place in case a natural disaster or other...

  13. Characterization of sampling cyclones

    E-Print Network [OSTI]

    Moore, Murray Edward

    1986-01-01T23:59:59.000Z

    Farland, who' provided an excellent opportunity for the enhancement of my engineering career. To Dr. Best for his patient snd competent assistance in this project. To Dr. Parish who gave his service to my graduate committee. To Bob DeOtte and Carlos Ortiz... in air sampling standards, several different samplers have been developed which utilize either inertial impaction or cyclonic flow fractionation techniques. For example, a 10 pm cutpoint size selective inlet was developed by McFarland, Ortiz...

  14. Post-Award Deliverables Sample (Second Part of Sample Deliverables...

    Broader source: Energy.gov (indexed) [DOE]

    samplereptgrqmts.doc More Documents & Publications ESPC Sample Deliverables for Task Orders (IDIQ Attachment. J-4) Sample Statement of Work - Standard Service Offerings for...

  15. Decoupled Sampling for Graphics Pipelines

    E-Print Network [OSTI]

    Ragan-Kelley, Jonathan Millar

    We propose a generalized approach to decoupling shading from visibility sampling in graphics pipelines, which we call decoupled sampling. Decoupled sampling enables stochastic supersampling of motion and defocus blur at ...

  16. Fluid sampling apparatus and method

    DOE Patents [OSTI]

    Yeamans, David R. (Los Alamos, NM)

    1998-01-01T23:59:59.000Z

    Incorporation of a bellows in a sampling syringe eliminates ingress of contaminants, permits replication of amounts and compression of multiple sample injections, and enables remote sampling for off-site analysis.

  17. Fluid sampling apparatus and method

    DOE Patents [OSTI]

    Yeamans, D.R.

    1998-02-03T23:59:59.000Z

    Incorporation of a bellows in a sampling syringe eliminates ingress of contaminants, permits replication of amounts and compression of multiple sample injections, and enables remote sampling for off-site analysis. 3 figs.

  18. Soil sampling kit and a method of sampling therewith

    DOE Patents [OSTI]

    Thompson, Cyril V. (Knoxville, TN)

    1991-01-01T23:59:59.000Z

    A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allow an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds.

  19. Soil sampling kit and a method of sampling therewith

    DOE Patents [OSTI]

    Thompson, C.V.

    1991-02-05T23:59:59.000Z

    A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allows an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds. 11 figures.

  20. OVERVIEW OF BERYLLIUM SAMPLING AND ANALYSIS

    SciTech Connect (OSTI)

    Brisson, M

    2009-04-01T23:59:59.000Z

    Because of its unique properties as a lightweight metal with high tensile strength, beryllium is widely used in applications including cell phones, golf clubs, aerospace, and nuclear weapons. Beryllium is also encountered in industries such as aluminium manufacturing, and in environmental remediation projects. Workplace exposure to beryllium particulates is a growing concern, as exposure to minute quantities of anthropogenic forms of beryllium may lead to sensitization and to chronic beryllium disease, which can be fatal and for which no cure is currently known. Furthermore, there is no known exposure-response relationship with which to establish a 'safe' maximum level of beryllium exposure. As a result, the current trend is toward ever lower occupational exposure limits, which in turn make exposure assessment, both in terms of sampling and analysis, more challenging. The problems are exacerbated by difficulties in sample preparation for refractory forms of beryllium, such as beryllium oxide, and by indications that some beryllium forms may be more toxic than others. This chapter provides an overview of sources and uses of beryllium, health risks, and occupational exposure limits. It also provides a general overview of sampling, analysis, and data evaluation issues that will be explored in greater depth in the remaining chapters. The goal of this book is to provide a comprehensive resource to aid personnel in a wide variety of disciplines in selecting sampling and analysis methods that will facilitate informed decision-making in workplace and environmental settings.

  1. NID Copper Sample Analysis

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Zhu, Zihua

    2011-09-12T23:59:59.000Z

    The current focal point of the nuclear physics program at PNNL is the MAJORANA DEMONSTRATOR, and the follow-on Tonne-Scale experiment, a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0???). This experiment requires the use of germanium isotopically enriched in 76Ge. The MAJORANA DEMONSTRATOR is a DOE and NSF funded project with a major science impact. The DEMONSTRATOR will utilize 76Ge from Russia, but for the Tonne-Scale experiment it is hoped that an alternate technology, possibly one under development at Nonlinear Ion Dynamics (NID), will be a viable, US-based, lower-cost source of separated material. Samples of separated material from NID require analysis to determine the isotopic distribution and impurities. DOE is funding NID through an SBIR grant for development of their separation technology for application to the Tonne-Scale experiment. The Environmental Molecular Sciences facility (EMSL), a DOE user facility at PNNL, has the required mass spectroscopy instruments for making isotopic measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR and for the development of the future separation technology required for the Tonne-Scale experiment. A sample of isotopically separated copper was provided by NID to PNNL in January 2011 for isotopic analysis as a test of the NID technology. The results of that analysis are reported here. A second sample of isotopically separated copper was provided by NID to PNNL in August 2011 for isotopic analysis as a test of the NID technology. The results of that analysis are also reported here.

  2. Germanium-76 Sample Analysis

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Engelhard, Mark H.; Zhu, Zihua

    2011-04-01T23:59:59.000Z

    The MAJORANA DEMONSTRATOR is a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0???). The DEMONSTRATOR will utilize 76Ge from Russia, and the first one gram sample was received from the supplier for analysis on April 24, 2011. The Environmental Molecular Sciences facility, a DOE user facility at PNNL, was used to make the required isotopic and chemical purity measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR. The results of this first analysis are reported here.

  3. Stack sampling apparatus

    DOE Patents [OSTI]

    Lind, Randall F; Lloyd, Peter D; Love, Lonnie J; Noakes, Mark W; Pin, Francois G; Richardson, Bradley S; Rowe, John C

    2014-09-16T23:59:59.000Z

    An apparatus for obtaining samples from a structure includes a support member, at least one stabilizing member, and at least one moveable member. The stabilizing member has a first portion coupled to the support member and a second portion configured to engage with the structure to restrict relative movement between the support member and the structure. The stabilizing member is radially expandable from a first configuration where the second portion does not engage with a surface of the structure to a second configuration where the second portion engages with the surface of the structure.

  4. Draft Sample Collection Instrument

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels DataDepartment of Energy Your Density Isn't Your Destiny:Revised Finding of No53197E T ADRAFTJanuaryDominionDowDepartmentPublic5 5Sample

  5. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA group currentBradleyTableSelling7 AugustAFRICAN3u ;;;::Sampling at the Sherwood,

  6. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA groupTuba City, Arizona, DisposalFourthN V O 1CentralGroundwater,Sampling at the

  7. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA groupTuba City, Arizona, DisposalFourthN V O 1CentralGroundwater,Sampling at the4

  8. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA groupTuba City, Arizona, DisposalFourthN V O 1CentralGroundwater,Sampling at

  9. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA groupTuba City, Arizona, DisposalFourthN V O 1CentralGroundwater,Sampling

  10. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA groupTuba City, Arizona, DisposalFourthN V O 1CentralGroundwater,SamplingTuba

  11. September 2004 Water Sampling

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA groupTuba City, Arizona, DisposalFourthN V O 1CentralGroundwater,SamplingTubaand

  12. NID Copper Sample Analysis

    SciTech Connect (OSTI)

    Kouzes, Richard T.; Zhu, Zihua

    2011-02-01T23:59:59.000Z

    The current focal point of the nuclear physics program at PNNL is the MAJORANA DEMONSTRATOR, and the follow-on Tonne-Scale experiment, a large array of ultra-low background high-purity germanium detectors, enriched in 76Ge, designed to search for zero-neutrino double-beta decay (0???). This experiment requires the use of germanium isotopically enriched in 76Ge. The DEMONSTRATOR will utilize 76Ge from Russia, but for the Tonne-Scale experiment it is hoped that an alternate technology under development at Nonlinear Ion Dynamics (NID) will be a viable, US-based, lower-cost source of separated material. Samples of separated material from NID require analysis to determine the isotopic distribution and impurities. The MAJORANA DEMONSTRATOR is a DOE and NSF funded project with a major science impact. DOE is funding NID through an SBIR grant for development of their separation technology for application to the Tonne-Scale experiment. The Environmental Molecular Sciences facility (EMSL), a DOE user facility at PNNL, has the required mass spectroscopy instruments for making these isotopic measurements that are essential to the quality assurance for the MAJORANA DEMONSTRATOR and for the development of the future separation technology required for the Tonne-Scale experiment. A sample of isotopically separated copper was provided by NID to PNNL for isotopic analysis as a test of the NID technology. The results of that analysis are reported here.

  13. Sample holder with optical features

    DOE Patents [OSTI]

    Milas, Mirko; Zhu, Yimei; Rameau, Jonathan David

    2013-07-30T23:59:59.000Z

    A sample holder for holding a sample to be observed for research purposes, particularly in a transmission electron microscope (TEM), generally includes an external alignment part for directing a light beam in a predetermined beam direction, a sample holder body in optical communication with the external alignment part and a sample support member disposed at a distal end of the sample holder body opposite the external alignment part for holding a sample to be analyzed. The sample holder body defines an internal conduit for the light beam and the sample support member includes a light beam positioner for directing the light beam between the sample holder body and the sample held by the sample support member.

  14. Recovery of coal fines from preparation plant effluents

    SciTech Connect (OSTI)

    Choudhry, V. (Praxis Engineers, Inc., Milpitas, CA (USA)); Khan, L. (Illinois State Geological Survey, Champaign, IL (USA)); Yang, D. (Michigan Technological Univ., Houghton, MI (USA))

    1990-01-01T23:59:59.000Z

    The objectives of this project are to test and demonstrate the feasibility of recovering the coal fines which are currently disposed of with plant effluent streams in order to produce a fine clean coal product. This product can then be blended with the coarse clean coal from the preparation plant. Recovery of carbonaceous material from the effluent streams will be effected by means of Michigan Technological University's static tube flotation process in conjunction with pyrite depressants. This process has been successfully demonstrated on a number of coals to reject 85% of the pyritic sulfur and recover 90% of the Btu value. The process parameters will be modified to accept preparation plant effluents in order to produce a low-ash, low-sulfur clean coal product that at a minimum is compatible with the quality requirements of the plant clean coal. This report covers the first quarter of the project. The main activities during this period were the drafting of a project work plan and the collection of four coal preparation plant effluent samples for testing. Effluent slurry samples were collected from four operating preparation plants in Illinois and shipped to Michigan Technological University for experimental work.

  15. Elimination of ``memory`` from sample handling and inlet system of a mass spectrometer

    DOE Patents [OSTI]

    Chastgner, P.

    1991-05-08T23:59:59.000Z

    This paper describes a method for preparing the sample handling and inlet system of a mass spectrometer for analysis of a subsequent sample following analysis of a previous sample comprising the flushing of the system interior with supercritical CO{sub 2} and venting the interior. The method eliminates the effect of system ``memory`` on the subsequent analysis, especially following persistent samples such as xenon and krypton.

  16. Method and apparatus for automated processing and aliquoting of whole blood samples for analysis in a centrifugal fast analyzer

    DOE Patents [OSTI]

    Burtis, C.A.; Johnson, W.F.; Walker, W.A.

    1985-08-05T23:59:59.000Z

    A rotor and disc assembly for use in a centrifugal fast analyzer. The assembly is designed to process multiple samples of whole blood followed by aliquoting of the resultant serum into precisely measured samples for subsequent chemical analysis. The assembly requires minimal operator involvement with no mechanical pipetting. The system comprises: (1) a whole blood sample disc; (2) a serum sample disc; (3) a sample preparation rotor; and (4) an analytical rotor. The blood sample disc and serum sample disc are designed with a plurality of precision bore capillary tubes arranged in a spoked array. Samples of blood are loaded into the blood sample disc by capillary action and centrifugally discharged into cavities of the sample preparation rotor where separation of serum and solids is accomplished. The serum is loaded into the capillaries of the serum sample disc by capillary action and subsequently centrifugally expelled into cuvettes of the analyticaly rotor for conventional methods. 5 figs.

  17. Method and apparatus for automated processing and aliquoting of whole blood samples for analysis in a centrifugal fast analyzer

    DOE Patents [OSTI]

    Burtis, Carl A. (Oak Ridge, TN); Johnson, Wayne F. (Loudon, TN); Walker, William A. (Knoxville, TN)

    1988-01-01T23:59:59.000Z

    A rotor and disc assembly for use in a centrifugal fast analyzer. The assembly is designed to process multiple samples of whole blood followed by aliquoting of the resultant serum into precisely measured samples for subsequent chemical analysis. The assembly requires minimal operator involvement with no mechanical pipetting. The system comprises (1) a whole blood sample disc, (2) a serum sample disc, (3) a sample preparation rotor, and (4) an analytical rotor. The blood sample disc and serum sample disc are designed with a plurality of precision bore capillary tubes arranged in a spoked array. Samples of blood are loaded into the blood sample disc in capillary tubes filled by capillary action and centrifugally discharged into cavities of the sample preparation rotor where separation of serum and solids is accomplished. The serum is loaded into the capillaries of the serum sample disc by capillary action and subsequently centrifugally expelled into cuvettes of the analytical rotor for analysis by conventional methods.

  18. prepared at INRIA Sophia Antipolis

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Maxime DESCOTEAUX Adviser Rachid Deriche INRIA Sophia Antipolis, France Reviewers Peter Basser NICHD, USA Ayache INRIA Sophia Antipolis, France Habib Benali INSERM / Pitié-Salpêtrière, France Denis Le Bihan

  19. prepared at INRIA Sophia Antipolis

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Wassermann Advisor Dr. Rachid Deriche INRIA Sophia-Antipolis, France Reviewers Dr. Cyril Poupon CEA Neuro l' INRIA Sophia Antipolis et present´ee ´a l' Universit´e de Nice-Sophia Antipolis ´Ecole Doctorale

  20. prepared at INRIA Sophia Antipolis

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Sophia Antipolis, France Pr. Val´erie Perrier University of Grenoble, France Dr. Fabrice Wallois;UNIVERSIT ´E NICE-SOPHIA ANTIPOLIS - UFR Sciences ´Ecole Doctorale STIC (Sciences et Technologies de l

  1. prepared at INRIA Sophia Antipolis

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Voronoi Diagrams and Applications Camille WORMSER Advisors Pr. Jean-Daniel Boissonnat INRIA Sophia Antipolis, France Pr. Mariette Yvinec INRIA Sophia Antipolis, France Reviewers Pr. Aurenhammer Technische

  2. prepared at INRIA Sophia Antipolis

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia NUNDLOLL Defense date: 30 March 2010. Jury Members Jean Luc GOUZ� INRIA Sophia Antipolis, France Advisor Frédéric GROGNARD INRIA Sophia Antipolis, France Co-advisor Ludovic MAILLERET INRA Sophia Antipolis, France

  3. prepared at INRIA Sophia Antipolis

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Pr. Rachid Deriche INRIA Sophia Antipolis, France Pr. Olivier Faugeras INRIA Sophia Antipolis, France-Fredrik Westin Harvard University, USA Examiners Pr. Nicholas Ayache INRIA Sophia Antipolis, France Dr. Maher

  4. Preparation of gas selective membranes

    DOE Patents [OSTI]

    Kulprathipanja, S.; Kulkarni, S.S.; Funk, E.W.

    1988-06-14T23:59:59.000Z

    Gas separation membranes which possess improved characteristics as exemplified by selectivity and flux may be prepared by coating a porous organic polymer support with a solution or emulsion of a plasticizer and an organic polymer, said coating being effected at subatmospheric pressures in order to increase the penetration depth of the coating material.

  5. Preparation of gas selective membranes

    DOE Patents [OSTI]

    Kulprathipanja, Santi (Hoffman Estates, IL); Kulkarni, Sudhir S. (Hoffman Estates, IL); Funk, Edward W. (Highland Park, IL)

    1988-01-01T23:59:59.000Z

    Gas separation membranes which possess improved characteristics as exemplified by selectivity and flux may be prepared by coating a porous organic polymer support with a solution or emulsion of a plasticizer and an organic polymer, said coating being effected at subatmospheric pressures in order to increase the penetration depth of the coating material.

  6. RECYCLING RATE STUDY Prepared by

    E-Print Network [OSTI]

    Laughlin, Robert B.

    NATIONAL RECYCLING RATE STUDY Prepared by: Smith, Bucklin and Associates, Inc. Market Research and Statistics Division Chicago, Illinois July 2003 PRINTED ON RECYCLED PAPER #12;BCI RECYCLING RATE STUDY TABLE ....................................................................................................1 II. METHODOLOGY A. Total Pounds of Lead Recycled from Batteries

  7. JOURNAL AUTHORS SURVEY Prepared by

    E-Print Network [OSTI]

    Stevenson, Paul

    JISC/OSI JOURNAL AUTHORS SURVEY Report Prepared by Key Perspectives Ltd 48 Old Coach Road, Playing behind its development 4 2.2 Models and definitions of open access 8 2.2.1 Open access journals 8 2 4.1 Respondent profiles 18 4.2 Awareness of open access journals 18 4.2.1 Extent and longevity

  8. Prepared by: Environmental Design & Research,

    E-Print Network [OSTI]

    Oh, Kwang W.

    Architecture and Engineering, P.C. (edr) 217 Montgomery St., Suite 1000 Syracuse, New York 13202 P. 315 Broadway Albany, New York 12246 Contact: Ms. Peggy McSorley Phone: (518) 320-3200 Prepared By: edr Companies (edr) 217 Montgomery Street, Suite 1000 Syracuse, New York 13202 Contact: Patrick Heaton Phone

  9. Photochemical preparation of plutonium pentafluoride

    DOE Patents [OSTI]

    Rabideau, Sherman W. (Los Alamos, NM); Campbell, George M. (Los Alamos, NM)

    1987-01-01T23:59:59.000Z

    The novel compound plutonium pentafluoride may be prepared by the photodissociation of gaseous plutonium hexafluoride. It is a white solid of low vapor pressure, which consists predominantly of a face-centered cubic structure with a.sub.o =4.2709.+-.0.0005 .ANG..

  10. Preparation of asymmetric porous materials

    DOE Patents [OSTI]

    Coker, Eric N. (Albuquerque, NM)

    2012-08-07T23:59:59.000Z

    A method for preparing an asymmetric porous material by depositing a porous material film on a flexible substrate, and applying an anisotropic stress to the porous media on the flexible substrate, where the anisotropic stress results from a stress such as an applied mechanical force, a thermal gradient, and an applied voltage, to form an asymmetric porous material.

  11. Sample Environment Plans and Progress

    E-Print Network [OSTI]

    Pennycook, Steve

    Sample Environment Plans and Progress at the SNS & HFIR SNS HFIR User Group Meeting American Conference on Neutron Scattering Ottawa, Canada June 26 ­ 30, 2010 Lou Santodonato Sample Environment Group our sample environment capabilities Feedback SHUG meetings User surveys Sample Environment Steering

  12. Fluid sampling tool

    DOE Patents [OSTI]

    Johnston, Roger G. (Los Alamos, NM); Garcia, Anthony R. E. (Espanola, NM); Martinez, Ronald K. (Santa Cruz, NM)

    2001-09-25T23:59:59.000Z

    The invention includes a rotatable tool for collecting fluid through the wall of a container. The tool includes a fluid collection section with a cylindrical shank having an end portion for drilling a hole in the container wall when the tool is rotated, and a threaded portion for tapping the hole in the container wall. A passageway in the shank in communication with at least one radial inlet hole in the drilling end and an opening at the end of the shank is adapted to receive fluid from the container. The tool also includes a cylindrical chamber affixed to the end of the shank opposite to the drilling portion thereof for receiving and storing fluid passing through the passageway. The tool also includes a flexible, deformable gasket that provides a fluid-tight chamber to confine kerf generated during the drilling and tapping of the hole. The invention also includes a fluid extractor section for extracting fluid samples from the fluid collecting section.

  13. preparation

    E-Print Network [OSTI]

    Bioremediation Of Uranium In; Shallow Alluvial Aquifers; Shallow Alluvial Aquifers; S. B. Yabusaki; Y. Fang; S. R. Waichler; P. E. Long

    Uranium can be removed from groundwater by adding an electron donor to the subsurface that stimulates growth of native bacteria, generating conditions that result in precipitation of uranium. The long-term efficacy of this technology is unproven. Numerical modeling results for uranium bioremediation in a shallow, alluvial aquifer are provided to establish a broad framework for understanding processes associated with bioremediation of uranium and to bound conditions under which bioremediation could succeed in the long-term and conditions under which it is likely to fail. The models are benchmarked against experiments conducted at the Rifle, Colorado site. Sensitivity analysis of model parameters were conducted, examining: alternatives to the acetate electron donor (lactate and ethanol), oxygen and nitrate terminal electron acceptors, multiphase flow, density and gas entrapment processes, and hypothetical flood events. Sensitivity of simulated aqueous U(VI) concentrations to process model parameters suggest that groundwater flow rate, uranium bioreduction rate, and sulfate bioreduction parameters exert the most impact on bioremediation effectiveness. The simulated scenarios are used to assess potential performance issues for site conditions and other bioremediation approaches.

  14. Prepared

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645 3,625 1,006 492 742EnergyOn AprilA groupTuba City, Arizona,Site Operations Guide Doc. No.GS05:orPOST-REMEDIAL

  15. Literature Building Mold Sampling Report

    E-Print Network [OSTI]

    Krstic, Miroslav

    Industrial Hygiene San Diego, CA Prepared By: Date: April 6, 2009 Karen G. Shockley, CIH #6766 #12;Literature and information obtained during a three site visits by Aurora Industrial Hygiene, Inc. (Aurora) to the property

  16. Specified assurance level sampling procedure

    SciTech Connect (OSTI)

    Willner, O.

    1980-11-01T23:59:59.000Z

    In the nuclear industry design specifications for certain quality characteristics require that the final product be inspected by a sampling plan which can demonstrate product conformance to stated assurance levels. The Specified Assurance Level (SAL) Sampling Procedure has been developed to permit the direct selection of attribute sampling plans which can meet commonly used assurance levels. The SAL procedure contains sampling plans which yield the minimum sample size at stated assurance levels. The SAL procedure also provides sampling plans with acceptance numbers ranging from 0 to 10, thus, making available to the user a wide choice of plans all designed to comply with a stated assurance level.

  17. Sampling for Bacteria in Wells 

    E-Print Network [OSTI]

    Lesikar, Bruce J.

    2001-11-15T23:59:59.000Z

    Sampling for Bacteria in Wells E-126 11/01 Water samples for bacteria tests must always be col- lected in a sterile container. The procedure for collect- ing a water sample is as follows: 1. Obtain a sterile container from a Health Department... immediately after collecting water sample. Refrigerate the sample and transport it to the laborato- ry (in an ice chest) as soon after collection as possible (six hours is best, but up to 30 hours). Many labs will not accept bacteria samples on Friday so check...

  18. Preparation of superconductor precursor powders

    DOE Patents [OSTI]

    Bhattacharya, Raghunath (Littleton, CO)

    1998-01-01T23:59:59.000Z

    A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic and/or reduced particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of all metals in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products.

  19. Method for preparing ceramic composite

    DOE Patents [OSTI]

    Alexander, K.B.; Tiegs, T.N.; Becher, P.F.; Waters, S.B.

    1996-01-09T23:59:59.000Z

    A process is disclosed for preparing ceramic composite comprising blending TiC particulates, Al{sub 2}O{sub 3} particulates and nickel aluminide and consolidating the mixture at a temperature and pressure sufficient to produce a densified ceramic composite having fracture toughness equal to or greater than 7 MPa m{sup 1/2}, a hardness equal to or greater than 18 GPa. 5 figs.

  20. Method for preparing ceramic composite

    DOE Patents [OSTI]

    Alexander, Kathleen B. (Oak Ridge, TN); Tiegs, Terry N. (Lenoir City, TN); Becher, Paul F. (Oak Ridge, TN); Waters, Shirley B. (Knoxville, TN)

    1996-01-01T23:59:59.000Z

    A process for preparing ceramic composite comprising blending TiC particulates, Al.sub.2 O.sub.3 particulates and nickle aluminide and consolidating the mixture at a temperature and pressure sufficient to produce a densified ceramic composite having fracture toughness equal to or greater than 7 MPa m.sup.1/2, a hardness equal to or greater than 18 GPa.

  1. Preparation of high purity vanadium

    SciTech Connect (OSTI)

    Carlson, O.N.; Burkholder, H.R.; Martsching, G.A.; Schmidt, F.A.

    1981-01-01T23:59:59.000Z

    The paper reviews the various reduction and refining methods that have been used to prepare vanadium metal. Earlier work on metallothermic and carbothermic reduction processes is discussed. Recent work on improving the scaling up the aluminothermic reduction process is described in detail. Iron and silicon are first removed from commercial V/sub 2/O/sub 5/ by an ion exchange separation technique and the purified oxide is then exothermically reduced with aluminum metal. The resulting V-Al ingot is heated in a vacuum to 1700/sup 0/C to remove the aluminum and dissolved oxygen, and the sponge is then electron-beam melted to remove residual volatile impurities to yield vanadium metal of 99.98% purity. Precautions taken during each processing stage to minimize carbon, nitrogen and oxygen contamination are described. Metal containing < 50 ppmw each of C, N and O, < 20 ppmw Si, and < 10 ppmw of Fe and Al has been prepared in kilogram quantities by this method. The hardness of the beam melted is 60 to 70 DPH. Experiments designed to scale up the reduction process and to increase the efficiency of the separation and melting steps are described. Various refining techniques that have been applied to the preparation of high purity vanadium are described and comparisons made between the quality of metal obtained by each.

  2. 3 - DJ : sampling as design

    E-Print Network [OSTI]

    Patel, Sayjel Vijay

    2015-01-01T23:59:59.000Z

    3D Sampling is introduced as a new spatial craft that can be applied to architectural design, akin to how sampling is applied in the field of electronic music. Through the development of 3-DJ, a prototype design software, ...

  3. Automated LEPS (low-energy photon spectrometry) system using a robotic sample changer

    SciTech Connect (OSTI)

    Delmastro, J.R.; Wade, M.A.; Dykes, F.W. (Westinghouse Idaho Nuclear Company, Idaho Falls (USA)); Lewis, A.L. (ARAMCO, Dhahran (Saudi Arabia))

    1989-11-01T23:59:59.000Z

    At the Idaho Chemical Processing Plant, effluent waste streams are regularly monitored for {sup 129}I. After sample preparation, a filter paper containing the separated radioiodine is mounted on an aluminum backing card for ease in handling. The card is loaded onto a low-energy photon detector and counted for {approximately}2 h with a Nuclear Data ND6700 spectrometer. After the counting is complete, the ND6700 system analyzes the spectrum to determine the quantity of {sup 129}I in the sample. The {sup 129}I in a typical waste stream sample is determined by counting four separate samples, i.e., duplicates of the waste stream sample, a blank, and an unknown quality control sample. The need arose to process large numbers of these samples. To improve sample throughput and permit unattended counting of these samples, a totally automated low-energy photon spectrometry (LEPS) system was developed to perform all the sample handling and analysis operations.

  4. Sampling for Bacteria in Wells

    E-Print Network [OSTI]

    Lesikar, Bruce J.

    2001-11-15T23:59:59.000Z

    Sampling for Bacteria in Wells E-126 11/01 Water samples for bacteria tests must always be col- lected in a sterile container. The procedure for collect- ing a water sample is as follows: 1. Obtain a sterile container from a Health Department...

  5. ON ADAPTIVE SAMPLING Philippe Flajolet

    E-Print Network [OSTI]

    Flajolet, Philippe

    . We analyze the storage/accuracy trade--off of an adaptive sampling algorithm due to Wegman that makes. Wegman [11] has proposed an interesting alternative solution to that problem based on Adaptive Sampling 4. 2 Wegman's Adaptive Sampling Method The problem discussed here is the following. We are given

  6. Spectral Thompson Sampling Tomas Kocak

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    Spectral Thompson Sampling Tom´as Koc´ak SequeL team INRIA Lille - Nord Europe France Michal Valko Thompson Sampling (TS) has surged a lot of interest due to its good empirical performance, in particular that our algorithm is com- petitive on both synthetic and real-world data. 1 Introduction Thompson Sampling

  7. Forensic Applications of Light-Element Stable Isotope Ratios of Ricinus communis Seeds and Ricin Preparations

    SciTech Connect (OSTI)

    Kreuzer, Helen W.; West, Jason B.; Ehleringer, James

    2013-01-01T23:59:59.000Z

    Seeds of the castor plant Ricinus communis, also known as castor beans, are of forensic interest because they are the source of the poison ricin. We have tested whether stable isotope ratios of castor seeds and ricin prepared by various methods can be used as a forensic signature. We collected over 300 castor seed samples from locations around the world and measured the C, N, O, and H stable isotope ratios of the whole seeds, oil, and three types of ricin preparations. Our results demonstrate that N isotope ratios can be used to correlate ricin prepared by any of these methods to source seeds. Further, stable isotope ratios distinguished >99% of crude and purified ricin protein samples in pair-wise comparison tests. Stable isotope ratios therefore constitute a valuable forensic signature for ricin preparations.

  8. Method of surface preparation of niobium

    DOE Patents [OSTI]

    Srinivasan-Rao, Triveni (Shoreham, NY); Schill, John F. (Ridge, NY)

    2003-01-01T23:59:59.000Z

    The present invention is for a method of preparing a surface of niobium. The preparation method includes polishing, cleaning, baking and irradiating the niobium surface whereby the resulting niobium surface has a high quantum efficiency.

  9. Preparing for Project Implementation Assigning Accountability...

    Broader source: Energy.gov (indexed) [DOE]

    Assigning Accountability for Each Project (April 14, 2010) More Documents & Publications Preparing for Project Implementation after an Energy Assessment...

  10. Stormwater Pollution Prevention Plan Prepared by

    E-Print Network [OSTI]

    Eisen, Michael

    Stormwater Pollution Prevention Plan Prepared by: Environment, Health, Safety, and Security .....................................................16 3.0 Potential Sources of Pollution

  11. ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION...

    Broader source: Energy.gov (indexed) [DOE]

    RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION, AND APPORTIONMENT ADMINISTRATIVE RECORDS SCHEDULE 23: RECORDS COMMON TO MOST OFFICES Administrative Management Records...

  12. Prepared by Heather Wilcox Feb. 22, 2009

    E-Print Network [OSTI]

    Worden, Alexandra Z.

    in an autoclaved glass bottle (we pre- autoclave the bottle). Aliquots of SUCROSE LYSIS BUFFER can be prepared

  13. PREPARED FOR: The National Renewable Energy Laboratory

    E-Print Network [OSTI]

    Wind and solar integration study May 2010 Prepared for NREL by GE Energy 1 River Road Schenectady, New York 12345PREPARED FOR: The National Renewable Energy Laboratory A national laboratory of the U.S. Department of Energy PREPARED BY: GE Energy MAY 2010 WESTERNWIND AND SOLAR INTEGRATION STUDY #12;#12;Western

  14. Introduction Sample preparation is an essential step for all three main

    E-Print Network [OSTI]

    Lebendiker, Mario

    -PAGE analysis of proteins extracted from Escherichia coli cells. BL21 DE3 pLysS cells were harvested-B Reagent diluted 1:5 in water. Likewise, the whole bacterial protein extracts were diluted 1:5 in water of efficiently extracting proteins from cells is essen- tial. The use of mild detergents to disrupt cells

  15. Versatile, automated sample preparation and detection of contaminants and biological materials

    E-Print Network [OSTI]

    Hoehl, Melanie Margarete

    2013-01-01T23:59:59.000Z

    Contamination of food, water, medicine and ingestible household products is a public health hazard that episodically causes outbreaks worldwide. Existing laboratory methods are often expensive, require a laboratory environment ...

  16. How to Prepare Your Abstract

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level: National5Sales for4,645U.S. DOEThe Bonneville PowerCherries 82981-1cnHigh School football Highdefault SignInstitute / TexasA4. U.S. to Prepare

  17. A comparison of sequential and point sample scouting for arthropods of cotton

    E-Print Network [OSTI]

    Rothrock, Michael Alan

    1981-01-01T23:59:59.000Z

    of Department December 1981 use of infested/damaged sample units whereas the Sterling package was based primarily on undamaged/uninfested sample units. The Rothrock package was based entirely on undamaged or uninfested sample units and resulted... L. Sterling for his guidance and counsel during the course of this study and preparation of the manuscript. The author also wishes to thank Drs. James W. Smith, Jr. , Robert S. Halliwell, and John H. Benedict, for their services on the graduate...

  18. Preparation of superconductor precursor powders

    DOE Patents [OSTI]

    Bhattacharya, R.

    1998-08-04T23:59:59.000Z

    A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic and/or reduced particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of all metals in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products. 7 figs.

  19. Preparation of superconductor precursor powders

    DOE Patents [OSTI]

    Bhattacharya, Raghunath (Littleton, CO); Blaugher, Richard D. (Evergreen, CO)

    1995-01-01T23:59:59.000Z

    A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals, such as nitrate salts of thallium, barium, calcium, and copper, which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of thallium in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products.

  20. Preparation of hydrophobic organic aeorgels

    DOE Patents [OSTI]

    Baumann, Theodore F.; Satcher Jr., Joe H.; Gash, Alexander E.

    2004-10-19T23:59:59.000Z

    Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.

  1. Preparation of hydrophobic organic aeorgels

    SciTech Connect (OSTI)

    Baumann, Theodore F. (Tracy, CA); Satcher, Jr., Joe H. (Patterson, CA); Gash, Alexander E. (Livermore, CA)

    2007-11-06T23:59:59.000Z

    Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.

  2. National Coal Council Presentation/Prepared Remarks | Department...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    National Coal Council PresentationPrepared Remarks National Coal Council PresentationPrepared Remarks National Coal Council PresentationPrepared Remarks More Documents &...

  3. A perspective on the status of coal research from shipments of samples

    SciTech Connect (OSTI)

    Vorres, K.S. [Argonne National Lab., IL (United States); Kruse, C.W. [Illinois State Geological Survey, Champaign, IL (United States); Nater, K.A. [deGrote Vos, Zeeweg 37, 1753 BB St. Martenzee, NL (Netherlands); Glick, D.C.; Davis, A. [Pennsylvania State Univ., University Park, PA (United States). Coal and Organic Petrology Labs.

    1993-12-31T23:59:59.000Z

    Research on all aspects of coal research, at least for more small scale work, involves the use of samples at the beginning of experimental work. Most research workers for smaller scale work do not collect their own coal samples, but rather order them from a group of sample suppliers. The number of suppliers meeting the major needs in the US, as well as for the world, is not very large. An examination of the shipments of samples from each of these suppliers will give an interesting insight into the general trends in volume of work in the field. The suppliers involved in this study include the Argonne Premium Coal Sample Program, the Illinois Basin Coal Sample Program, the SBN and the several groups of samples from the Pennsylvania State University Coal Sample Bank. Each of these supplies a different number of samples in varying quantities. The quantities and variety of samples is important to the individual worker in selecting a supplier. The type of work to be done frequently affects the quantities and choice of sample, which in turn affects the choice of supplier. In general these data indicate that researchers realize the advantages of acquiring samples from centralized sample banks. These advantages include a lower cost than would be incurred from individual sampling and preparation; availability of analyzed samples; preservation of samples and the possibility of comparing results with others who have worked on the same samples.

  4. Acceptance sampling using judgmental and randomly selected samples

    SciTech Connect (OSTI)

    Sego, Landon H.; Shulman, Stanley A.; Anderson, Kevin K.; Wilson, John E.; Pulsipher, Brent A.; Sieber, W. Karl

    2010-09-01T23:59:59.000Z

    We present a Bayesian model for acceptance sampling where the population consists of two groups, each with different levels of risk of containing unacceptable items. Expert opinion, or judgment, may be required to distinguish between the high and low-risk groups. Hence, high-risk items are likely to be identifed (and sampled) using expert judgment, while the remaining low-risk items are sampled randomly. We focus on the situation where all observed samples must be acceptable. Consequently, the objective of the statistical inference is to quantify the probability that a large percentage of the unsampled items in the population are also acceptable. We demonstrate that traditional (frequentist) acceptance sampling and simpler Bayesian formulations of the problem are essentially special cases of the proposed model. We explore the properties of the model in detail, and discuss the conditions necessary to ensure that required samples sizes are non-decreasing function of the population size. The method is applicable to a variety of acceptance sampling problems, and, in particular, to environmental sampling where the objective is to demonstrate the safety of reoccupying a remediated facility that has been contaminated with a lethal agent.

  5. (Recovery of coal fines from preparation plant effluents)

    SciTech Connect (OSTI)

    Choudhry, V. (Praxis Engineers, Inc., Milpitas, CA (USA)); Khan, L. (Illinois State Geological Survey, Champaign, IL (USA)); Yang, D. (Michigan Technological Univ., Houghton, MI (USA))

    1991-01-01T23:59:59.000Z

    The objectives of this project are to test and demonstrate the feasibility of recovering coal fines which are currently disposed of with plant effluent streams, in order to produce a fine clean coal product. This product can then be blended with the coarse clean coal from the preparation plant. Recovery of coal from the effluent stream samples will be effected by means of Michigan Technological University's static tube flotation process. This process has been successfully demonstrated on a number of raw coals to reject 85% of the pyritic sulfur and recover 90% of the combustible matter. The process parameters will be modified so that this technology can be applied to preparation plant effluents in order to recover a low-ash, low-sulfur clean coal that is, at a minimum, compatible with the quality of the clean coal currently produced from the preparation plant. The main activities during this period were setting up the static tube test unit to conduct the experimental work as outlined in the project work plan. The first of four effluent slurry samples collected from four operating Illinois preparation plants was tested at Michigan Technological University. The first batch of tests resulted in a clean coal containing 7.5% ash at 94.5% combustible matter recovery. Another test aimed at lowering the ash further analyzed at 3.0% ash and 0.92% total sulfur. In addition, analyses of particle size distribution and sink-float testing of the +200 mesh material were undertaken as a part of the effluent characterization work. 5 tabs.

  6. Sample Residential Program Term Sheet

    Broader source: Energy.gov [DOE]

    A sample for defining and elaborating on the specifics of a clean energy loan program. Author: U.S. Department of Energy

  7. IWTU Process Sample Analysis Report

    SciTech Connect (OSTI)

    Nick Soelberg

    2013-04-01T23:59:59.000Z

    CH2M-WG Idaho (CWI) requested that Battelle Energy Alliance (BEA) analyze various samples collected during June – August 2012 at the Integrated Waste Treatment Facility (IWTU). Samples of IWTU process materials were collected from various locations in the process. None of these samples were radioactive. These samples were collected and analyzed to provide more understanding of the compositions of various materials in the process during the time of the process shutdown that occurred on June 16, 2012, while the IWTU was in the process of nonradioactive startup.

  8. Defining And Characterizing Sample Representativeness For DWPF Melter Feed Samples

    SciTech Connect (OSTI)

    Shine, E. P.; Poirier, M. R.

    2013-10-29T23:59:59.000Z

    Representative sampling is important throughout the Defense Waste Processing Facility (DWPF) process, and the demonstrated success of the DWPF process to achieve glass product quality over the past two decades is a direct result of the quality of information obtained from the process. The objective of this report was to present sampling methods that the Savannah River Site (SRS) used to qualify waste being dispositioned at the DWPF. The goal was to emphasize the methodology, not a list of outcomes from those studies. This methodology includes proven methods for taking representative samples, the use of controlled analytical methods, and data interpretation and reporting that considers the uncertainty of all error sources. Numerous sampling studies were conducted during the development of the DWPF process and still continue to be performed in order to evaluate options for process improvement. Study designs were based on use of statistical tools applicable to the determination of uncertainties associated with the data needs. Successful designs are apt to be repeated, so this report chose only to include prototypic case studies that typify the characteristics of frequently used designs. Case studies have been presented for studying in-tank homogeneity, evaluating the suitability of sampler systems, determining factors that affect mixing and sampling, comparing the final waste glass product chemical composition and durability to that of the glass pour stream sample and other samples from process vessels, and assessing the uniformity of the chemical composition in the waste glass product. Many of these studies efficiently addressed more than one of these areas of concern associated with demonstrating sample representativeness and provide examples of statistical tools in use for DWPF. The time when many of these designs were implemented was in an age when the sampling ideas of Pierre Gy were not as widespread as they are today. Nonetheless, the engineers and statisticians used carefully thought out designs that systematically and economically provided plans for data collection from the DWPF process. Key shared features of the sampling designs used at DWPF and the Gy sampling methodology were the specification of a standard for sample representativeness, an investigation that produced data from the process to study the sampling function, and a decision framework used to assess whether the specification was met based on the data. Without going into detail with regard to the seven errors identified by Pierre Gy, as excellent summaries are readily available such as Pitard [1989] and Smith [2001], SRS engineers understood, for example, that samplers can be biased (Gy?s extraction error), and developed plans to mitigate those biases. Experiments that compared installed samplers with more representative samples obtained directly from the tank may not have resulted in systematically partitioning sampling errors into the now well-known error categories of Gy, but did provide overall information on the suitability of sampling systems. Most of the designs in this report are related to the DWPF vessels, not the large SRS Tank Farm tanks. Samples from the DWPF Slurry Mix Evaporator (SME), which contains the feed to the DWPF melter, are characterized using standardized analytical methods with known uncertainty. The analytical error is combined with the established error from sampling and processing in DWPF to determine the melter feed composition. This composition is used with the known uncertainty of the models in the Product Composition Control System (PCCS) to ensure that the wasteform that is produced is comfortably within the acceptable processing and product performance region. Having the advantage of many years of processing that meets the waste glass product acceptance criteria, the DWPF process has provided a considerable amount of data about itself in addition to the data from many special studies. Demonstrating representative sampling directly from the large Tank Farm tanks is a difficult, if not unsolvable enterprise due to li

  9. SST Sample Characterization Analysis of Archive Samples 102-C, 105-C, and 106-C

    SciTech Connect (OSTI)

    Hara, F. T.; Kaye, J. H.; Steele, R. T.; Stromatt, R. W.; Thomas, D. L.; Urie, M. W.

    1990-04-01T23:59:59.000Z

    A substantial effort is planned to be initiated at the Hanford Site regarding the characterization of 149 single-shell tanks (SSTs) containing the byproducts of reprocessing during the 1950s and 1960s. Sampling and analysis, in distinct phases, are planned to involve laboratory investigations to determine both chemical and radionuclide inventories, so that waste disposal decisions can be developed. During 1989, trial analyses were performed on four archived samples from SSTs at the Pacific Northwest Laboratory using established U.S. Environmental Protection Agency (EPA) protocols and radiochemical procedures. The analysis of the archived SST waste material provides three important types of data for use in planning Phase I-A and Phase 1-B sample analysis. The types of data served as input to I) fi na 1 i zing the waste samp 1 e analysis procedures and methods and identify where procedure developmen~ may be needed, 2) evaluating the impact of normal paraffin hydrocarbon (NPH) lubricant {used in field sampling) on extracting inorganics or radionuclides from the SST sample, and 3) identifying trends in amounts of occupational radiation exposure expected from performing the various analysis procedures. Overall, the results are qualitative in nature, and the conclusions given are to be used with appropriate respect for the limitations of small amounts of data from four samples used in development processes. The results of the Phase I-A and I-B sample analysis will provide essential data for method performance for use in finalizing Phase I-C planning and methods development scope. Section 2.0, Inorganic Analysis, encompasses sample preparation, sample analysis, identification of methods performance limitations, and possible alternatives. Performance of the inorganic analytical methods was evaluated and changes were made to some of the procedures. In some cases, inductively coupled plasma-atomic emission spectroscopy (referred to in this report as ICP) did not provide the levels of accuracy and precision usually required for EPA work due to interference by other elements. In these cases, other methods are suggested as appropriate for trial as alternatives. In all cases, duplicates, spikes, and blanks were used to establish performance of the methods for the specific waste matrix. Results focused on problems in using the methods tested on the samples, the suitability of the ICP method of determining EP Toxicity metal ions and 22 EPA pollutant metal ions, and the suitability of cold vapor atomic absorption (CVAA) for mercury determinations. Problems areas identified are ICP spectral corrections, poor reproducibility from water leach and EP Toxicity methods, and adjustments needed for mercury analysis by CVAA. Section 3.0, Organics Analysis, details two screening procedures [total organic carbon (TOC) and gas chromatography (GC)], extraction procedures and related problems, surrogate spiking to test extraction efficiencies and matrix effects, and semivolatile organics via GC/mass spectroscopy (MS). The results show that the GC/MS is vulnerable to fouling and overload and that a combination of dilution and perhaps acidification are required to provide acceptable results. NPH and silicone-based lubricants from the sampling process impact the semivolatile analysis; however, with some modification the semivolatile method based on EPA SOW 288 can be used. Section 4.0, Radionuclide Analysis, evaluates procedures used to measure the radionuclides that might be found in the SST tank waste samples and establishes the level of accuracy and precision that can be expected. These data reveal that additional procedure development is needed in order to measure all of the radionuclides listed in Table 4-14 of the Waste Characterization Plan. In addition, the archive samples analyzed may not be representative of the tank population and considerable adaptation of the radiochemical procedures may be necessary to perform the desired measurements. NPH tests were conducted to determine whether the NPH from the field sampling process extracted significan

  10. Sampling for Beryllium Surface Contamination using Wet, Dry and Alcohol Wipe Sampling

    SciTech Connect (OSTI)

    Kerr, Kent

    2004-12-17T23:59:59.000Z

    This research project was conducted at the National Nuclear Security Administration's Kansas City Plant, operated by Honeywell Federal Manufacturing and Technologies, in conjunction with the Safety Sciences Department of Central Missouri State University, to compare relative removal efficiencies of three wipe sampling techniques currently used at Department of Energy facilities. Efficiencies of removal of beryllium contamination from typical painted surfaces were tested by wipe sampling with dry Whatman 42 filter paper, with water-moistened (Ghost Wipe) materials, and by methanol-moistened wipes. Test plates were prepared using 100 mm X 15 mm Pyrex Petri dishes with interior surfaces spray painted with a bond coat primer. To achieve uniform deposition over the test plate surface, 10 ml aliquots of solution containing 1 beryllium and 0.1 ml of metal working fluid were transferred to the test plates and subsequently evaporated. Metal working fluid was added to simulate the slight oiliness common on surfaces in metal working shops where fugitive oil mist accumulates over time. Sixteen test plates for each wipe method (dry, water, and methanol) were processed and sampled using a modification of wiping patterns recommended by OSHA Method 125G. Laboratory and statistical analysis showed that methanol-moistened wipe sampling removed significantly more (about twice as much) beryllium/oil-film surface contamination as water-moistened wipes (p< 0.001), which removed significantly more (about twice as much) residue as dry wipes (p <0.001). Evidence for beryllium sensitization via skin exposure argues in favor of wipe sampling with wetting agents that provide enhanced residue removal efficiency.

  11. Detection of Acetone Processing of Castor Bean Mash for Forensic Investigation of Ricin Preparation Methods

    SciTech Connect (OSTI)

    Kreuzer-Martin, Helen W.; Wahl, Jon H.; Metoyer, Candace N.; Colburn, Heather A.; Wahl, Karen L.

    2010-07-01T23:59:59.000Z

    The toxic protein ricin is of concern as a potential biological threat agent (BTA) Recently, several samples of ricin have been seized in connection with biocriminal activity. Analytical methods are needed that enable federal investigators to determine how the samples were prepared, to match seized samples to potential source materials, and to identify samples that may have been prepared by the same method using the same source materials. One commonly described crude ricin preparation method is acetone extraction of crushed castor beans. Here we describe the use of solid-phase microextraction and headspace analysis of crude ricin preparation samples to determine whether they were processed by acetone extraction. In all cases, acetone-extracted bean mash could be distinguished from un-extracted mash or mash extracted with other organic solvents. Statistical analysis showed that storage in closed containers for up to 109 days had no effect on acetone signal intensity. Signal intensity in acetone-extracted mash decreased during storage in open containers, but extracted mash could still be distinguished from un-extracted mash after 94 days.

  12. Characterization Of Sample HTF-13-13-128

    SciTech Connect (OSTI)

    Pareizs, J. M.

    2013-09-25T23:59:59.000Z

    Savannah River Remediation (SRR) has requested that Savannah River National Laboratory (SRNL) characterize a sample of Tank 13 in preparation for Sludge Batch 9 (SB9). A 200 mL sample of Tank 13 was received by SRNL on July 22, 2013 (Tank Farm sample ID HTF-13-13-128). Characterization of the sample to meet the requirements of the request is complete. Results include: visual observations; slurry and supernatant density; weight percent total and insoluble solids; supernatant characterization; total alpha, total beta, and several radionuclide analyses; and elemental analyses of the dried solids. The sample was very fluid. After settling overnight, there was a small layer of solids on the bottom of the sample container (a 250 mL HDPE bottle) with the remainder being clear supernatant. To better show the sludge solids relative to the overall sample, 25 mL of slurry was placed in a graduated cylinder and allowed to settle over a weekend (approximately 90 hours). The sludge layer was at the approximately 4 mL. The small visually observed quantity of insoluble solids was confirmed with a low weight percent insoluble solids of 0.94%.

  13. Hazard Sampling Dialog General Layout

    E-Print Network [OSTI]

    Zhang, Tao

    1 Hazard Sampling Dialog General Layout The dialog's purpose is to display information about the hazardous material being sampled by the UGV so either the system or the UV specialist can identify the risk level of the hazard. The dialog is associated with the hazmat reading icons (Table 1). Components

  14. Database Sampling with Functional Dependencies

    E-Print Network [OSTI]

    Riera, Jesús Bisbal

    Database Sampling with Functional Dependencies Jes´us Bisbal, Jane Grimson Department of Computer there is a need to prototype the database which the applications will use when in operation. A prototype database can be built by sampling data from an existing database. Including relevant semantic information when

  15. BLOOD SAMPLING SYSTEM TROUBLESHOOTING TIPS

    E-Print Network [OSTI]

    Kay, Mark A.

    SAFESET TM BLOOD SAMPLING SYSTEM SAFESETTM TROUBLESHOOTING TIPS TO PREVENT BLOOD BACKING UP IN LINE that all air bubbles have been eliminated when priming o Invert and tap blood sampling ports to remove air volume o Reinfuse the patient's blood slowly, no faster than 1mL per second, by pressing the plunger back

  16. Sample push-out fixture

    DOE Patents [OSTI]

    Biernat, John L. (Scotia, NY)

    2002-11-05T23:59:59.000Z

    This invention generally relates to the remote removal of pelletized samples from cylindrical containment capsules. V-blocks are used to receive the samples and provide guidance to push out rods. Stainless steel liners fit into the v-channels on the v-blocks which permits them to be remotely removed and replaced or cleaned to prevent cross contamination between capsules and samples. A capsule holder securely holds the capsule while allowing manual up/down and in/out movement to align each sample hole with the v-blocks. Both end sections contain identical v-blocks; one that guides the drive out screw and rods or manual push out rods and the other to receive the samples as they are driven out of the capsule.

  17. PREPARING FOR A SUCCESSFUL EVMS CERTIFICATION

    SciTech Connect (OSTI)

    CROWE SL; BASCHE AD

    2011-02-09T23:59:59.000Z

    The client, a government agency, requires its contractor to obtain an Earned Value Management System (EVMS) certification that meets the intent of ANSI/EIA-748-B, Earned Value Management Systems. The contractor has extensive experience with certification preparation, having completed two certifications within two years. Information from a previous EVMS certification and internal system surveillances are used to prepare for client-based EVMS certifications and bi-annual surveillances. The contractor also sent members of its group to assist other companies preparing for surveillances and certifications to perform 'Black Hat Reviews.' This paper is a lessons learned on preparing a team for EVMS certification. The information is also applicable for surveillances, since the contractor prepares its team for the surveillance in the same manner as the initial certification. Some of the areas covered include required documents, tracing the data through the systems, Control Account Manager (CAM) preparation, and system verification.

  18. Adiabatic state preparation study of methylene

    SciTech Connect (OSTI)

    Veis, Libor, E-mail: libor.veis@jh-inst.cas.cz; Pittner, Ji?í, E-mail: jiri.pittner@jh-inst.cas.cz [J. Heyrovský Institute of Physical Chemistry, Academy of Sciences of the Czech Republic, v.v.i., Dolejškova 3, 18223 Prague 8 (Czech Republic)

    2014-06-07T23:59:59.000Z

    Quantum computers attract much attention as they promise to outperform their classical counterparts in solving certain type of problems. One of them with practical applications in quantum chemistry is simulation of complex quantum systems. An essential ingredient of efficient quantum simulation algorithms are initial guesses of the exact wave functions with high enough fidelity. As was proposed in Aspuru-Guzik et al. [Science 309, 1704 (2005)], the exact ground states can in principle be prepared by the adiabatic state preparation method. Here, we apply this approach to preparation of the lowest lying multireference singlet electronic state of methylene and numerically investigate preparation of this state at different molecular geometries. We then propose modifications that lead to speeding up the preparation process. Finally, we decompose the minimal adiabatic state preparation employing the direct mapping in terms of two-qubit interactions.

  19. The application of Graphene as a sample support in Transmission Electron Microscopy

    E-Print Network [OSTI]

    Pantelic, R S; Kaiser, U; Stahlberg, H

    2012-01-01T23:59:59.000Z

    Transmission electron microscopy has witnessed rampant development and surging point resolution over the past few years. The improved imaging performance of modern electron microscopes shifts the bottleneck for image contrast and resolution to sample preparation. Hence, it is increasingly being realized that the full potential of electron microscopy will only be realized with the optimization of current sample preparation techniques. Perhaps the most recognized issues are background signal and noise contributed by sample supports, sample charging and instability. Graphene provides supports of single atom thickness, extreme physical stability, periodic structure, and ballistic electrical conductivity. As an increasing number of applications adapting graphene to their benefit emerge, we discuss the unique capabilities afforded by the use of graphene as a sample support for electron microscopy.

  20. Cold Dissolved Saltcake Waste Simulant Development, Preparation, and Analysis

    SciTech Connect (OSTI)

    Rassat, Scot D.; Mahoney, Lenna A.; Russell, Renee L.; Bryan, Samuel A.; Sell, Rachel L.

    2003-05-13T23:59:59.000Z

    CH2M HILL Hanford Group, Inc. is identifying and developing supplemental process technologies to accelerate the Hanford tank waste cleanup mission. Bulk vitrification, containerized grout, and steam reforming are three technologies under consideration for treatment of the radioactive saltcake wastes in 68 single-shell tanks. To support development and testing of these technologies, Pacific Northwest National Laboratory (PNNL) was tasked with developing a cold dissolved saltcake simulant formulation to be representative of an actual saltcake waste stream, preparing 25- and 100-L batches of the simulant, and analyzing the composition of the batches to ensure conformance to formulation targets. Lacking a defined composition for dissolved actual saltcake waste, PNNL used available tank waste composition information and an equilibrium chemistry model (Environmental Simulation Program [ESP{trademark}]) to predict the concentrations of analytes in solution. Observations of insoluble solids in initial laboratory preparations for the model-predicted formulation prompted reductions in the concentration of phosphate and silicon in the final simulant formulation. The analytical results for the 25- and 100-L simulant batches, prepared by an outside vendor to PNNL specifications, agree within the expected measurement accuracy ({approx}10%) of the target concentrations and are highly consistent for replicate measurements, with a few minor exceptions. In parallel with the production of the 2nd simulant batch (100-L), a 1-L laboratory control sample of the same formulation was carefully prepared at PNNL to serve as an analytical standard. The instrumental analyses indicate that the vendor prepared batches of solution adequately reflect the as-formulated simulant composition. In parallel with the simulant development effort, a nominal 5-M (molar) sodium actual waste solution was prepared at the Hanford Site from a limited number of tank waste samples. Because this actual waste solution w as also to be used for testing the supplemental treatment technologies, the modeled simulant formulation was predicated on the composite of waste samples used to prepare it. Subsequently, the actual waste solution was filtered and pretreated to remove radioactive cesium at PNNL and then analyzed using the same instrumentation and procedures applied to the simulant samples. The overall agreement of measured simulant and actual waste solution compositions is better than {+-}10% for the most concentrated species including sodium, nitrate, hydroxide, carbonate, and nitrite. While the magnitude of the relative difference in the simulant and actual waste composition is large (>20% difference) for a few analytes (aluminum, chromium, fluoride, potassium, and total organic carbon), the absolute differences in concentration are in general not appreciable. Our evaluation is that these differences in simulant and actual waste solutions should have a negligible impact on bulk vitrification and containerized grout process testing, while the impact of the low aluminum concentration on steam reforming is yet to be determined.

  1. RAPID DETERMINATION OF RA-226 IN ENVIRONMENTAL SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.

    2012-01-03T23:59:59.000Z

    A new rapid method for the determination of {sup 226}Ra in environmental samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used for emergency response or routine sample analyses. The need for rapid analyses in the event of a Radiological Dispersive Device or Improvised Nuclear Device event is well-known. In addition, the recent accident at Fukushima Nuclear Power Plant in March, 2011 reinforces the need to have rapid analyses for radionuclides in environmental samples in the event of a nuclear accident. {sup 226}Ra (T1/2 = 1,620 years) is one of the most toxic of the long-lived alpha-emitters present in the environment due to its long life and its tendency to concentrate in bones, which increases the internal radiation dose of individuals. The new method to determine {sup 226}Ra in environmental samples utilizes a rapid sodium hydroxide fusion method for solid samples, calcium carbonate precipitation to preconcentrate Ra, and rapid column separation steps to remove interferences. The column separation process uses cation exchange resin to remove large amounts of calcium, Sr Resin to remove barium and Ln Resin as a final purification step to remove {sup 225}Ac and potential interferences. The purified {sup 226}Ra sample test sources are prepared using barium sulfate microprecipitation in the presence of isopropanol for counting by alpha spectrometry. The method showed good chemical recoveries and effective removal of interferences. The determination of {sup 226}Ra in environmental samples can be performed in less than 16 h for vegetation, concrete, brick, soil, and air filter samples with excellent quality for emergency or routine analyses. The sample preparation work takes less than 6 h. {sup 225}Ra (T1/2 = 14.9 day) tracer is used and the {sup 225}Ra progeny {sup 217}At is used to determine chemical yield via alpha spectrometry. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory radium particles are effectively digested. The preconcentration and column separation steps can also be applied to aqueous samples with good results.

  2. HYDRAULIC CEMENT PREPARATION FROM LURGI SPENT SHALE

    E-Print Network [OSTI]

    Mehta, P.K.

    2013-01-01T23:59:59.000Z

    Investigations on hydraulic cement from spent oil shale,"April 16-18, 1980 HYDRAULIC CEMENT PREPARATION FROM LURGIpressi ve b strength, MPa this cement in moist environments.

  3. Methods for preparation of cyclopentadienyliron (II) arenes

    DOE Patents [OSTI]

    Keipert, S.J.

    1991-10-22T23:59:59.000Z

    Two improved methods for preparation of compounds with the structure shown in the equation, [(Cp)--Fe--(Ar)][sup +][sub b]X[sup b[minus

  4. Recommendations for the Preparation of Environmental Assessments...

    Energy Savers [EERE]

    and Environmental Impact Statements Second Edition This second edition of the "Green Book" was issued by DOE to assist preparers and reviewers of NEPA documents, with the...

  5. MA 159 Final Exam Memo/Preparation

    E-Print Network [OSTI]

    Owen Davis

    2007-11-17T23:59:59.000Z

    MA 159 Final Exam Memo/Preparation. Monday, December 10 – 10:20 AM (2 hour exam). In Lambert Fieldhouse. **Note the early time and have double and ...

  6. Remote preparation of an atomic quantum memory

    E-Print Network [OSTI]

    Wenjamin Rosenfeld; Stefan Berner; Juergen Volz; Markus Weber; Harald Weinfurter

    2006-08-29T23:59:59.000Z

    Storage and distribution of quantum information are key elements of quantum information processing and quantum communication. Here, using atom-photon entanglement as the main physical resource, we experimentally demonstrate the preparation of a distant atomic quantum memory. Applying a quantum teleportation protocol on a locally prepared state of a photonic qubit, we realized this so-called remote state preparation on a single, optically trapped 87Rb atom. We evaluated the performance of this scheme by the full tomography of the prepared atomic state, reaching an average fidelity of 82%.

  7. ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION...

    Energy Savers [EERE]

    SCHEDULE 5: BUDGET PREPARATION, PRESENTATION, AND APPORTIONMENT Budget and apportionment records include the various files accumulated in the course of formulating the budget for...

  8. Document prepared by APIC Bioterrorism Task Force

    E-Print Network [OSTI]

    Oliver, Douglas L.

    ATTACHMENT Document prepared by APIC Bioterrorism Task Force Judith F. English, Mae Y. Cundiff of civilian populations not recommended. 3. Infection Control Practices for Patient Management Symptomatic

  9. RAPID DETERMINATION OF {sup 210} PO IN WATER SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.

    2013-05-22T23:59:59.000Z

    A new rapid method for the determination of {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that can be used for emergency response or routine water analyses. If a radiological dispersive device (RDD) event or a radiological attack associated with drinking water supplies occurs, there will be an urgent need for rapid analyses of water samples, including drinking water, ground water and other water effluents. Current analytical methods for the assay of {sup 210}Po in water samples have typically involved spontaneous auto-deposition of {sup 210}Po onto silver or other metal disks followed by counting by alpha spectrometry. The auto-deposition times range from 90 minutes to 24 hours or more, at times with yields that may be less than desirable. If sample interferences are present, decreased yields and degraded alpha spectrums can occur due to unpredictable thickening in the deposited layer. Separation methods have focused on the use of Sr Resin?, often in combination with 210Pb analysis. A new rapid method for {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that utilizes a rapid calcium phosphate co-precipitation method, separation using DGA Resin? (N,N,N?,N? tetraoctyldiglycolamide extractant-coated resin, Eichrom Technologies or Triskem-International), followed by rapid microprecipitation of {sup 210}Po using bismuth phosphate for counting by alpha spectrometry. This new method can be performed quickly with excellent removal of interferences, high chemical yields and very good alpha peak resolution, eliminating any potential problems with the alpha source preparation for emergency or routine samples. A rapid sequential separation method to separate {sup 210} Po and actinide isotopes was also developed. This new approach, rapid separation with DGA Resin plus microprecipitation for alpha source preparation, is a significant advance in radiochemistry for the rapid determination of {sup 210}Po.

  10. Preparation and characterization of boro-tellurite glasses

    SciTech Connect (OSTI)

    Kaur, Nirmal, E-mail: akphysics@yahoo.com; Khanna, Atul, E-mail: akphysics@yahoo.com [Glass Physics and Sensors Laboratory, Department of Physics, Guru Nanak Dev University, Amritsar-143005, Punjab (India); Krishna, P. S. R. [Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai-400085, Maharashtra (India)

    2014-04-24T23:59:59.000Z

    Glass samples of the system: xB{sub 2}O{sub 3}?(100?x) TeO{sub 2}; x= 15, 20, 25 and 30 mol% were prepared by melt quenching and characterized by X-ray diffraction, density measurements, Differential Scanning Calorimetry and FTIR spectroscopy. XRD confirmed the amorphous structure of all samples. Density of glasses decreased with increase in B{sub 2}O{sub 3} concentration due to the replacement of heavier TeO{sub 2} with lighter B{sub 2}O{sub 3} whereas the glass transition temperature increased from 339°C to 366°C; the later effect was due to increase in the concentration of stronger B-O bonds in the glass network. FTIR studies found that BO{sub 4} units convert into BO{sub 3} with the addition of B{sub 2}O{sub 3}.

  11. Sample Business Plan Framework 3

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  12. Sample Business Plan Framework 2

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  13. Sample Business Plan Framework 4

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  14. Sample Business Plan Framework 1

    Broader source: Energy.gov [DOE]

    U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

  15. Process for preparing energetic materials

    DOE Patents [OSTI]

    Simpson, Randall L. (Livermore, CA); Lee, Ronald S. (Livermore, CA); Tillotson, Thomas M. (Tracy, CA; , Hrubesh, Lawrence W. (Pleasanton, CA); Swansiger, Rosalind W. (Livermore, CA); Fox, Glenn A. (Livermore, CA)

    2011-12-13T23:59:59.000Z

    Sol-gel chemistry is used for the preparation of energetic materials (explosives, propellants and pyrotechnics) with improved homogeneity, and/or which can be cast to near-net shape, and/or made into precision molding powders. The sol-gel method is a synthetic chemical process where reactive monomers are mixed into a solution, polymerization occurs leading to a highly cross-linked three dimensional solid network resulting in a gel. The energetic materials can be incorporated during the formation of the solution or during the gel stage of the process. The composition, pore, and primary particle sizes, gel time, surface areas, and density may be tailored and controlled by the solution chemistry. The gel is then dried using supercritical extraction to produce a highly porous low density aerogel or by controlled slow evaporation to produce a xerogel. Applying stress during the extraction phase can result in high density materials. Thus, the sol-gel method can be used for precision detonator explosive manufacturing as well as producing precision explosives, propellants, and pyrotechnics, along with high power composite energetic materials.

  16. Analysis Of The Tank 6F Final Characterization Samples-2012

    SciTech Connect (OSTI)

    Oji, L. N.; Diprete, D. P.; Coleman, C. J.; Hay, M. S.; Shine, E. P.

    2012-09-27T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm-243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

  17. ANALYSIS OF THE TANK 6F FINAL CHARACTERIZATION SAMPLES-2012

    SciTech Connect (OSTI)

    Oji, L.; Diprete, D.; Coleman, C.; Hay, M.; Shine, G.

    2012-06-28T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm-243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

  18. Analysis of the Tank 6F Final Characterization Samples-2012

    SciTech Connect (OSTI)

    Oji, L. N.; Diprete, D. P.; Coleman, C. J.; Hay, M. S.; Shine, E. P.

    2013-01-31T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm- 243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

  19. UWMadison Department of Geography Guidelines for Preparation of the Senior Honors Thesis

    E-Print Network [OSTI]

    Wisconsin at Madison, University of

    1 UWMadison Department of Geography Guidelines for Preparation of the Senior Honors Thesis q. Use only one side of the paper. q The text must be doublespaced, with paragraphs clearly indented, Wisconsin" and, under that, the date. (See the sample at the end of these guidelines.) o Affirmation

  20. A Method for the Preparation of NIST Traceable Fossil Fuel Standards with Concentrations

    E-Print Network [OSTI]

    at NIST with high accuracy and precision by isotope dilution thermal ionization mass spectrometry and quality control test samples. Unlike calibrants prepared from high purity components, this method enables Abbreviations M bar Calculated concentration of mixture EDXRF Energy Dispersive X-Ray Fluorescence n number

  1. Ninth annual coal preparation, utilization, and environmental control contractors conference: Proceedings

    SciTech Connect (OSTI)

    Not Available

    1993-09-01T23:59:59.000Z

    Papers are grouped under the following sessions: compliance technology; high-efficiency preparation; characterization; advanced technologies; alternative fuels; coal utilization; industrial/commercial combustor development; combustion; superclean emission systems; carbon dioxide recovery and reuse; air toxics and fine particulates; air toxics sampling and analysis workshop; and combined poster session. Selected papers have been processed separately for inclusion in the Energy Science and Technology Database.

  2. Prepare for Exam I Aug. 16. 10:50-12:05

    E-Print Network [OSTI]

    Zhang, Yu

    problems such as the reliability of a system. Be prepared for Ch 3: (1) Know the definitions of random) Know the definitions of sample space, event, probability, and distribution. (2) Be able to use variable. (2) Be able to find discrete distributions for certain probability models. (3) Be able to find

  3. Guidelines for Manuscript Preparation Purdue University Press

    E-Print Network [OSTI]

    Ginzel, Matthew

    Guidelines for Manuscript Preparation Purdue University Press The editing of your book or essay will be considerably faster and less costly if you follow a few guidelines for manuscript preparation. Double-space all the space bar to indent paragraphs. Do not type anything in all caps. Do include page numbers in your

  4. Energy Audit Procedures Prepared for the

    E-Print Network [OSTI]

    Energy Audit Procedures Prepared for the U.S. Department of Energy Office of Electricity Delivery Subtask 3.5.1: Residential Energy Efficiency Deliverable 1 Prepared by The University of Hawai or reflect those of the United States Government or any agency thereof. #12;Project Report 1: Energy Audit

  5. Exam Preparation Identifying Levels of Learning

    E-Print Network [OSTI]

    , proposed a six-level model of learning, with each level requiring a different type of cognitive processingSee over Exam Preparation Identifying Levels of Learning When you are preparing for an exam, understand, apply, analyze, evaluate, and create. Understanding these levels and the types of exam questions

  6. PREPARED FOR: The National Renewable Energy Laboratory

    E-Print Network [OSTI]

    by GE Energy 1 River Road Schenectady, New York 12345 Technical Monitor: Debra Lew Prepared under Acker, Karin Wadsack, Carson Pete, Jason Kemper and Mark Bielecki State University of New YorkPREPARED FOR: The National Renewable Energy Laboratory A national laboratory of the U.S. Department

  7. NOTICE OF PREPARATION: DRAFT ENVIRONMENTAL IMPACT REPORT

    E-Print Network [OSTI]

    Sze, Lawrence

    NOTICE OF PREPARATION: DRAFT ENVIRONMENTAL IMPACT REPORT DATE: September 25, 2013 TO: Responsible (Trustees) will be the lead agency for the preparation of an environmental impact report (EIR to: CSU Board of Trustees c/o Nicole Carter, Senior Planner SWCA Environmental Consultants 1422

  8. Sampling Report for August 15, 2014 WIPP Samples

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels DataDepartment of Energy Your Density Isn'tOrigin ofEnergy atLLC - FE DKT. 10-160-LNG - ORDERSTATE0-1ofEnergy SampleSample of

  9. Reference Potential source Data type Sampling site Type of samples Number of samples Method of source

    E-Print Network [OSTI]

    Meskhidze, Nicholas

    samples for Saharan dust from Libya back trajectory analysis Kandler et al. 2009 PSA NAF-2 Illite NAF-4 Illite/kaolinite ratio Chlorite/kaolinite ratio Carbonate content Libya (here: central

  10. CTBTO Contractor Laboratory Test Sample Production Report

    SciTech Connect (OSTI)

    Bob Hague; Tracy Houghton; Nick Mann; Matt Watrous

    2013-08-01T23:59:59.000Z

    In October 2012 scientists from both Idaho National Laboratory (INL) and the CTBTO contact laboratory at Seibersdorf, Austria designed a system and capability test to determine if the INL could produce and deliver a short lived radio xenon standard in time for the standard to be measured at the CTBTO contact laboratory at Seibersdorf, Austria. The test included sample standard transportation duration and potential country entrance delays at customs. On October 23, 2012 scientists at the Idaho National Laboratory (INL) prepared and shipped a Seibersdorf contract laboratory supplied cylinder. The canister contained 1.0 scc of gas that consisted of 70% xenon and 30% nitrogen by volume. The t0 was October 24, 2012, 1200 ZULU. The xenon content was 0.70 +/ 0.01 scc at 0 degrees C. The 133mXe content was 4200 +/ 155 dpm per scc of stable xenon on t0 (1 sigma uncertainty). The 133Xe content was 19000 +/ 800 dpm per scc of stable xenon on t0 (1 sigma uncertainty).

  11. SLUDGE BATCH 7 PREPARATION TANK 4 AND 12 CHARACTERIZATION

    SciTech Connect (OSTI)

    Bannochie, C.; Click, D.; Pareizs, J.

    2010-05-21T23:59:59.000Z

    Samples of PUREX sludge from Tank 4 and HM sludge from Tank 12 were characterized in preparation for Sludge Batch 7 (SB7) formulation in Tank 51. SRNL analyses on Tank 4 and Tank 12 were requested in separate Technical Assistance Requests (TAR). The Tank 4 samples were pulled on January 19, 2010 following slurry operations by F-Tank Farm. The Tank 12 samples were pulled on February 9, 2010 following slurry operations by H-Tank Farm. At the Savannah River National Laboratory (SRNL), two 200 mL dip samples of Tank 4 and two 200 mL dip samples of Tank 12 were received in the SRNL Shielded Cells. Each tank's samples were composited into clean 500 mL polyethylene storage bottles and weighed. The composited Tank 4 sample was 428.27 g and the composited Tank 12 sample was 502.15 g. As expected there are distinct compositional differences between Tank 4 and Tank 12 sludges. The Tank 12 slurry is much higher in Al, Hg, Mn, and Th, and much lower in Fe, Ni, S, and U than the Tank 4 slurry. The Tank 4 sludge definitely makes the more significant contribution of S to any sludge batch blend. This S, like that observed during SB6 washing, is best monitored by looking at the total S measured by digesting the sample and analyzing by inductively coupled plasma - atomic emission spectroscopy (ICPAES). Alternatively, one can measure the soluble S by ICP-AES and adjust the value upward by approximately 15% to have a pretty good estimate of the total S in the slurry. Soluble sulfate measurements by ion chromatography (IC) will be biased considerably lower than the actual total S, the difference being due to the non-sulfate soluble S and the undissolved S. Tank 12 sludge is enriched in U-235, and hence samples transferred into SRNL from the Tank Farm will need to be placed on the reportable special nuclear material inventory and tracked for total U per SRNL procedure requirements.

  12. Sample rotating turntable kit for infrared spectrometers

    DOE Patents [OSTI]

    Eckels, Joel Del (Livermore, CA); Klunder, Gregory L. (Oakland, CA)

    2008-03-04T23:59:59.000Z

    An infrared spectrometer sample rotating turntable kit has a rotatable sample cup containing the sample. The infrared spectrometer has an infrared spectrometer probe for analyzing the sample and the rotatable sample cup is adapted to receive the infrared spectrometer probe. A reflectance standard is located in the rotatable sample cup. A sleeve is positioned proximate the sample cup and adapted to receive the probe. A rotator rotates the rotatable sample cup. A battery is connected to the rotator.

  13. ANALYSIS OF THE TANK 5F FINAL CHARACTERIZATION SAMPLES-2011

    SciTech Connect (OSTI)

    Oji, L.; Diprete, D.; Coleman, C.; Hay, M.

    2012-08-03T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by SRR to provide sample preparation and analysis of the Tank 5F final characterization samples to determine the residual tank inventory prior to grouting. Two types of samples were collected and delivered to SRNL: floor samples across the tank and subsurface samples from mounds near risers 1 and 5 of Tank 5F. These samples were taken from Tank 5F between January and March 2011. These samples from individual locations in the tank (nine floor samples and six mound Tank 5F samples) were each homogenized and combined in a given proportion into 3 distinct composite samples to mimic the average composition in the entire tank. These Tank 5F composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 5F composite samples include bulk density and water leaching of the solids to account for water soluble species. With analyses for certain challenging radionuclides as the exception, all composite Tank 5F samples were analyzed and reported in triplicate. The target detection limits for isotopes analyzed were based on customer desired detection limits as specified in the technical task request documents. SRNL developed new methodologies to meet these target detection limits and provide data for the extensive suite of components. While many of the target detection limits were met for the species characterized for Tank 5F, as specified in the technical task request, some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The Technical Task Request allows that while the analyses of these isotopes is needed, meeting the detection limits for these isotopes is a lower priority than meeting detection limits for the other specified isotopes. The isotopes whose detection limits were not met in all cases included the following: Al-26, Sn-126, Sb-126, Sb-126m, Eu-152 and Cf-249. SRNL, in conjunction with the plant customer, reviewed all these cases and determined that the impacts were negligible.

  14. Analysis Of The Tank 5F Final Characterization Samples-2011

    SciTech Connect (OSTI)

    Oji, L. N.; Diprete, D.; Coleman, C. J.; Hay, M. S.

    2012-09-27T23:59:59.000Z

    The Savannah River National Laboratory (SRNL) was requested by SRR to provide sample preparation and analysis of the Tank 5F final characterization samples to determine the residual tank inventory prior to grouting. Two types of samples were collected and delivered to SRNL: floor samples across the tank and subsurface samples from mounds near risers 1 and 5 of Tank 5F. These samples were taken from Tank 5F between January and March 2011. These samples from individual locations in the tank (nine floor samples and six mound Tank 5F samples) were each homogenized and combined in a given proportion into 3 distinct composite samples to mimic the average composition in the entire tank. These Tank 5F composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 5F composite samples include bulk density and water leaching of the solids to account for water soluble species. With analyses for certain challenging radionuclides as the exception, all composite Tank 5F samples were analyzed and reported in triplicate. The target detection limits for isotopes analyzed were based on customer desired detection limits as specified in the technical task request documents. SRNL developed new methodologies to meet these target detection limits and provide data for the extensive suite of components. While many of the target detection limits were met for the species characterized for Tank 5F, as specified in the technical task request, some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The Technical Task Request allows that while the analyses of these isotopes is needed, meeting the detection limits for these isotopes is a lower priority than meeting detection limits for the other specified isotopes. The isotopes whose detection limits were not met in all cases included the following: Al-26, Sn-126, Sb-126, Sb-126m, Eu-152 and Cf-249. SRNL, in conjunction with the plant customer, reviewed all these cases and determined that the impacts were negligible.

  15. Inertial impaction air sampling device

    DOE Patents [OSTI]

    Dewhurst, K.H.

    1987-12-10T23:59:59.000Z

    An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

  16. Inertial impaction air sampling device

    DOE Patents [OSTI]

    Dewhurst, K.H.

    1990-05-22T23:59:59.000Z

    An inertial impactor is designed which is to be used in an air sampling device for collection of respirable size particles in ambient air. The device may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

  17. Spent nuclear fuel sampling strategy

    SciTech Connect (OSTI)

    Bergmann, D.W.

    1995-02-08T23:59:59.000Z

    This report proposes a strategy for sampling the spent nuclear fuel (SNF) stored in the 105-K Basins (105-K East and 105-K West). This strategy will support decisions concerning the path forward SNF disposition efforts in the following areas: (1) SNF isolation activities such as repackaging/overpacking to a newly constructed staging facility; (2) conditioning processes for fuel stabilization; and (3) interim storage options. This strategy was developed without following the Data Quality Objective (DQO) methodology. It is, however, intended to augment the SNF project DQOS. The SNF sampling is derived by evaluating the current storage condition of the SNF and the factors that effected SNF corrosion/degradation.

  18. Characterization Results For The 2013 HTF 3H Evaporator Overhead Samples

    SciTech Connect (OSTI)

    Washington, A. L. II

    2013-12-04T23:59:59.000Z

    This report tabulates the radiochemical analysis of the 3H evaporator overhead sample for {sup 137}Cs, {sup 90}Sr, and {sup 129}I to meet the requirements in the Effluent Treatment Project (ETP) Waste Acceptance Criteria (WAC) (rev. 6). This report identifies the sample receipt date, preparation method, and analysis performed in the accumulation of the listed values. All data was found to be within the ETP WAC (rev. 6) specification for the Waste Water Collection Tanks (WWCT).

  19. Method for the concentration and separation of actinides from biological and environmental samples

    DOE Patents [OSTI]

    Horwitz, E. Philip (Naperville, IL); Dietz, Mark L. (Tucson, AZ)

    1989-01-01T23:59:59.000Z

    A method and apparatus for the quantitative recover of actinide values from biological and environmental sample by passing appropriately prepared samples in a mineral acid solution through a separation column of a dialkyl(phenyl)-N,N-dialylcarbamoylmethylphosphine oxide dissolved in tri-n-butyl phosphate on an inert substrate which selectively extracts the actinide values. The actinide values can be eluted either as a group or individually and their presence quantitatively detected by alpha counting.

  20. Method for the concentration and separation of actinides from biological and environmental samples

    DOE Patents [OSTI]

    Horwitz, E.P.; Dietz, M.L.

    1989-05-30T23:59:59.000Z

    A method and apparatus for the quantitative recover of actinide values from biological and environmental sample by passing appropriately prepared samples in a mineral acid solution through a separation column of a dialkyl(phenyl)-N,N-dialylcarbamoylmethylphosphine oxide dissolved in tri-n-butyl phosphate on an inert substrate which selectively extracts the actinide values. The actinide values can be eluted either as a group or individually and their presence quantitatively detected by alpha counting. 3 figs.

  1. Methods and Materials Sample Collection

    E-Print Network [OSTI]

    by Greenwood (1958). A 1.5-inch (3.8 em) mesh liner was laced into the cod end to retain small specimens which reported that Alaska pollock \\yas the principal species taken by these Japanese fisheries. However from flatfish samples collected in 1949 were reported by Mosher (1954); the Soviet collections of 1957

  2. Sample Internship Posting Department Name

    E-Print Network [OSTI]

    Bordenstein, Seth

    Sample Internship Posting Department Name: Internship Title: Location: Description of Organization are examples from other internship postings Interns will: · Analyze potential investments · Shadow team members(s) in ________ is desirable For a list of majors see http://admissions.vanderbilt.edu/major Internship Period: The following

  3. Waste tank characterization sampling limits

    SciTech Connect (OSTI)

    Tusler, L.A.

    1994-09-02T23:59:59.000Z

    This document is a result of the Plant Implementation Team Investigation into delayed reporting of the exotherm in Tank 241-T-111 waste samples. The corrective actions identified are to have immediate notification of appropriate Tank Farm Operations Shift Management if analyses with potential safety impact exceed established levels. A procedure, WHC-IP-0842 Section 12.18, ``TWRS Approved Sampling and Data Analysis by Designated Laboratories`` (WHC 1994), has been established to require all tank waste sampling (including core, auger and supernate) and tank vapor samples be performed using this document. This document establishes levels for specified analysis that require notification of the appropriate shift manager. The following categories provide numerical values for analysis that may indicate that a tank is either outside the operating specification or should be evaluated for inclusion on a Watch List. The information given is intended to translate an operating limit such as heat load, expressed in Btu/hour, to an analysis related limit, in this case cesium-137 and strontium-90 concentrations. By using the values provided as safety flags, the analytical laboratory personnel can notify a shift manager that a tank is in potential violation of an operating limit or that a tank should be considered for inclusion on a Watch List. The shift manager can then take appropriate interim measures until a final determination is made by engineering personnel.

  4. Licensing Guide and Sample License

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    TEI:HNOL06Y TRANSFER WORKIN6 6ROUP Lic:eniing Guide and Sample Lic:enie ICan.u City Plan I OFermilab OAK RIDGE Nuioul.

  5. Environmental Analysis & Policy: Sample Pathway

    E-Print Network [OSTI]

    Goldberg, Bennett

    Environmental Analysis & Policy: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Sustainable Development OR Spring GE 425 U.S. Environmental Policy (Senior) GE 309 Intermediate Env Analysis (Fall) EAP Elective Summer Environmental Internship Senior Year GE 420 Env Policy Analysis 4 th Semester

  6. Quantum rejection sampling Maris Ozols

    E-Print Network [OSTI]

    Cerf, Nicolas

    generation prob- lem. We exhibit an algorithm, which we call quantum rejec- tion sampling, and analyze its technical innovation is an extension of the automorphism principle to continuous groups that arise or to redistribute to lists, requires prior specific permission and/or a fee. ITCS '12, January 08 - 10, 2012

  7. AUTOMATING GROUNDWATER SAMPLING AT HANFORD

    SciTech Connect (OSTI)

    CONNELL CW; HILDEBRAND RD; CONLEY SF; CUNNINGHAM DE

    2009-01-16T23:59:59.000Z

    Until this past October, Fluor Hanford managed Hanford's integrated groundwater program for the U.S. Department of Energy (DOE). With the new contract awards at the Site, however, the CH2M HILL Plateau Remediation Company (CHPRC) has assumed responsibility for the groundwater-monitoring programs at the 586-square-mile reservation in southeastern Washington State. These programs are regulated by the Resource Conservation and Recovery Act (RCRA) and the Comprehensive Environmental Response Compensation and Liability Act (CERCLA). The purpose of monitoring is to track existing groundwater contamination from past practices, as well as other potential contamination that might originate from RCRA treatment, storage, and disposal (TSD) facilities. An integral part of the groundwater-monitoring program involves taking samples of the groundwater and measuring the water levels in wells scattered across the site. More than 1,200 wells are sampled each year. Historically, field personnel or 'samplers' have been issued pre-printed forms that have information about the well(s) for a particular sampling evolution. This information is taken from the Hanford Well Information System (HWIS) and the Hanford Environmental Information System (HEIS)--official electronic databases. The samplers used these hardcopy forms to document the groundwater samples and well water-levels. After recording the entries in the field, the samplers turned the forms in at the end of the day and the collected information was posted onto a spreadsheet that was then printed and included in a log book. The log book was then used to make manual entries of the new information into the software application(s) for the HEIS and HWIS databases. This is a pilot project for automating this tedious process by providing an electronic tool for automating water-level measurements and groundwater field-sampling activities. The automation will eliminate the manual forms and associated data entry, improve the accuracy of the information recorded, and enhance the efficiency and sampling capacity of field personnel. The goal of the effort is to eliminate 100 percent of the manual input to the database(s) and replace the management of paperwork by the field and clerical personnel with an almost entirely electronic process. These activities will include the following: scheduling the activities of the field teams, electronically recording water-level measurements, electronically logging and filing Groundwater Sampling Reports (GSR), and transferring field forms into the site-wide Integrated Document Management System (IDMS).

  8. Structural, electrical and dielectric properties of spinel nickel ferrite prepared by soft mechanochemical synthesis

    SciTech Connect (OSTI)

    Lazarevi?, Zorica Ž., E-mail: lzorica@yahoo.com [Institute of Physics, University of Belgrade, P.O. Box 68, Pregrevica 118, Zemun, Belgrade (Serbia); Jovaleki?, ?edomir [The Institute for Multidisciplinary Research, University of Belgrade, Kneza Višeslava 1, Belgrade (Serbia); Sekuli?, Dalibor L. [Faculty of Technical Sciences, University of Novi Sad, Trg Dositeja Obradovi?a 6, Novi Sad (Serbia); Milutinovi?, Aleksandra [Institute of Physics, University of Belgrade, P.O. Box 68, Pregrevica 118, Zemun, Belgrade (Serbia); Baloš, Sebastian; Slankamenac, Miloš [Faculty of Technical Sciences, University of Novi Sad, Trg Dositeja Obradovi?a 6, Novi Sad (Serbia); Rom?evi?, Nebojša Ž. [Institute of Physics, University of Belgrade, P.O. Box 68, Pregrevica 118, Zemun, Belgrade (Serbia)

    2013-10-15T23:59:59.000Z

    Graphical abstract: - Highlights: • Sintered NiFe{sub 2}O{sub 4} was prepared by a soft mechanochemical route from mixture powders. • XRD and Raman measurements indicate that the prepared samples have spinel structure. • The activation energy ?E are 0.653 and 0.452 eV for NiFe{sub 2}O{sub 4} samples. • Ferrite from Ni(OH){sub 2}/Fe{sub 2}O{sub 3} has lower DC conductivity than from Ni(OH){sub 2}/Fe(OH){sub 3} powders. • The values of dielectric constant of samples NiFe{sub 2}O{sub 4} are 70 and 200, respectively. - Abstract: Nickel ferrite, NiFe{sub 2}O{sub 4} was prepared by a soft mechanochemical route from a mixture of (1) Ni(OH){sub 2} and ?-Fe{sub 2}O{sub 3} and (2) Ni(OH){sub 2} and Fe(OH){sub 3} powders in a planetary ball mill for 25 h. The powder samples were sintered at 1100 °C for 2 h and were characterized by X-ray diffraction (XRD), Raman spectroscopy and scanning electron microscopy (SEM). Impedance spectroscopy techniques were used to study the effect of grain and grain boundary on the electrical properties of the prepared samples. A difference in dielectric constant (?) and dielectric loss tangent (tan ?) of NiFe{sub 2}O{sub 4} samples obtained by the same methods but starting from different initial components was observed.

  9. Preparing for Hurricane Irene: Follow Local Direction

    Broader source: Energy.gov [DOE]

    Hurricane Irene is heading towards the East Coast, and while the extent of its impact is not yet known, those who may be effected (even inland areas), should get prepared and follow the direction...

  10. Is Your Plant Prepared for a Hurricane?

    SciTech Connect (OSTI)

    Not Available

    2006-07-01T23:59:59.000Z

    This DOE Industrial Technologies Program BestPractices fact sheet lists resources for manufacturers and steps they can take to prepare for the devastating winds and floods caused by hurricanes.

  11. a amework for change Prepared by

    E-Print Network [OSTI]

    october 2008 Pursuant to AB 32 e California Global Warming Solutions Act of 2006 Climate Change Proposed______________________________________________C-131 Green Buildings_____________________________________ C-138 Industrya amework for change Prepared by the California Air Resources Board for the State of California

  12. INTERNATIONAL TRAVEL REIMBURSEMENT REQUEST Date: Dept: Preparer

    E-Print Network [OSTI]

    El Karoui, Noureddine

    INTERNATIONAL TRAVEL REIMBURSEMENT REQUEST Date: Dept: Preparer: UC Employee Student Vendor Other: Name: Emp/Stu/Ven ID: Address: City/ST/Zip: E-Mail: Phone: US Citizen/Permanent Resident? Yes No Fax

  13. International Particle Accelerator Community Prepares for May...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    International Particle Accelerator Community Prepares for May 3-8 Gathering in Richmond NEWPORT NEWS, VA - April 29, 2015 - Scientists, engineers and students from across U.S. and...

  14. Numerically Efficient Parallel Algorithms Prepared for the

    E-Print Network [OSTI]

    Simulation using High Performance Computing Prepared by New Mexico Tech New Mexico Institute of Mining agency thereof. #12;Final Report for Task One Project: Application of High Performance Computing

  15. Process for the preparation of organoclays

    DOE Patents [OSTI]

    Chaiko, David J. (Naperville, IL)

    2003-01-01T23:59:59.000Z

    A method for preparing organoclays from smectites for use as rheological control agents and in the preparation of nanocomposites. Typically, the clay is dispersed in water, and a substantially monomolecular layer of a water soluble polymer is applied to the surfaces of the clay. A surfactant is also applied to the clay to modify the surface hydrophilic/hydrophobic balance of the clay, and the organoclay is separated out for subsequent use.

  16. Process for the preparation of organoclays

    DOE Patents [OSTI]

    Chaiko, David J.

    2004-11-23T23:59:59.000Z

    A method for preparing organoclays for use as rheological control agents and in the preparation of nanocomposites. Typically, the clay is dispersed in water, and a specific amount of polymeric hydrotrope, ranging from 0.1 to 15 weight percent relative to the weight of the clay, is adsorbed onto the clay surface. Quaternary amine exchange is also performed on the clay to modify the surface hydrophilic/lipophilic balance (HLB) of the clay.

  17. Remote State Preparation for Quantum Fields

    E-Print Network [OSTI]

    Ran Ber; Erez Zohar

    2015-01-07T23:59:59.000Z

    Remote state preparation is generation of a desired state by a remote observer. In spite of causality, it is well known, according to the Reeh-Schlieder theorem, that it is possible for relativistic quantum field theories, and a "physical" process achieving this task, involving superoscillatory functions, has recently been introduced. In this work we deal with non-relativistic fields, and show that remote state preparation is also possible for them, hence generalizing the Reeh-Schlieder theorem.

  18. Preparation and electrocatalytic activity of tungsten carbide and titania nanocomposite

    SciTech Connect (OSTI)

    Hu, Sujuan; Shi, Binbin; Yao, Guoxing [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)] [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China); Li, Guohua, E-mail: nanozjut@zjut.edu.cn [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)] [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China); Ma, Chunan [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)] [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)

    2011-10-15T23:59:59.000Z

    Graphical abstract: The electrocatalytic activity of tungsten carbide and titania nanocomposite is related to the structure, crystal phase and chemical components of the nanocomposite, and is also affected by the property of electrolyte. A synergistic effect exists between tungsten carbide and titania of the composite. Highlights: {yields} Electrocatalytic activity of tungsten carbide and titania nanocomposite with core-shell structure. {yields} Activity is related to the structure, crystal phase and chemical component of the nanocomposite. {yields} The property of electrolyte affects the electrocatalytic activity. {yields} A synergistic effect exists between tungsten carbide and titania of the composite. -- Abstract: Tungsten carbide and titania nanocomposite was prepared by combining a reduced-carbonized approach with a mechanochemical approach. The samples were characterized by X-ray diffraction, transmission electron microscope under scanning mode and X-ray energy dispersion spectrum. The results show that the crystal phases of the samples are composed of anatase, rutile, nonstoichiometry titanium oxide, monotungsten carbide, bitungsten carbide and nonstoichiometry tungsten carbide, and they can be controlled by adjusting the parameters of the reduced-carbonized approach; tungsten carbide particles decorate on the surface of titania support, the diameter of tungsten carbide particle is smaller than 20 nm and that of titania is around 100 nm; the chemical components of the samples are Ti, O, W and C. The electrocatalytic activity of the samples was measured by a cyclic voltammetry with three electrodes. The results indicate that the electrocatalytic activities of the samples are related to their crystal phases and the property of electrolyte in aqueous solution. A synergistic effect between titania and tungsten carbide is reported for the first time.

  19. Environmental surveillance master sampling schedule

    SciTech Connect (OSTI)

    Bisping, L E

    1992-01-01T23:59:59.000Z

    Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the US Department of Energy (DOE). This document contains the planned schedule for routine sample collection for the Surface Environmental Surveillance Project (SESP) and Ground-Water Monitoring Project. Samples for radiological analyses include Air-Particulate Filter, gases and vapor; Water/Columbia River, Onsite Pond, Spring, Irrigation, and Drinking; Foodstuffs/Animal Products including Whole Milk, Poultry and Eggs, and Beef; Foodstuffs/Produce including Leafy Vegetables, Vegetables, and Fruit; Foodstuffs/Farm Products including Wine, Wheat and Alfalfa; Wildlife; Soil; Vegetation; and Sediment. Direct Radiation Measurements include Terrestrial Locations, Columbia River Shoreline Locations, and Onsite Roadway, Railway and Aerial, Radiation Surveys.

  20. Adaptive Sampling in Hierarchical Simulation

    SciTech Connect (OSTI)

    Knap, J; Barton, N R; Hornung, R D; Arsenlis, A; Becker, R; Jefferson, D R

    2007-07-09T23:59:59.000Z

    We propose an adaptive sampling methodology for hierarchical multi-scale simulation. The method utilizes a moving kriging interpolation to significantly reduce the number of evaluations of finer-scale response functions to provide essential constitutive information to a coarser-scale simulation model. The underlying interpolation scheme is unstructured and adaptive to handle the transient nature of a simulation. To handle the dynamic construction and searching of a potentially large set of finer-scale response data, we employ a dynamic metric tree database. We study the performance of our adaptive sampling methodology for a two-level multi-scale model involving a coarse-scale finite element simulation and a finer-scale crystal plasticity based constitutive law.

  1. HYDRAULIC CONDUCTIVITY OF SALTSTONE FORMULATED USING 1Q11, 2Q11 AND 3Q11 TANK 50 SLURRY SAMPLES

    SciTech Connect (OSTI)

    Reigel, M.; Nichols, R.

    2012-06-27T23:59:59.000Z

    As part of the Saltstone formulation work requested by Waste Solidification Engineering (WSE), Savannah River National Laboratory (SRNL) was tasked with preparing Saltstone samples for fresh property analysis and hydraulic conductivity measurements using actual Tank 50 salt solution rather than simulated salt solution. Samples of low level waste salt solution collected from Tank 50H during the first, second, and third quarters of 2011 were used to formulate the Saltstone samples. The salt solution was mixed with premix (45 wt % slag, 45 wt % fly ash, and 10 wt % cement), in a ratio consistent with facility operating conditions during the quarter of interest. The fresh properties (gel, set, bleed) of each mix were evaluated and compared to the recommended acceptance criteria for the Saltstone Production Facility. ASTM D5084-03, Method C was used to measure the hydraulic conductivity of the Saltstone samples. The hydraulic conductivity of Saltstone samples prepared from 1Q11 and 2Q11 samples of Tank 50H is 4.2E-9 cm/sec and 2.6E-9 cm/sec, respectively. Two additional 2Q11 and one 3Q11 sample were not successfully tested due to the inability to achieve stable readings during saturation and testing. The hydraulic conductivity of the samples made from Tank 50H salt solution compare well to samples prepared with simulated salt solution and cured under similar conditions (1.4E-9 - 4.9E-8 cm/sec).

  2. New Training Resource Prepares Rescuers for Hydrogen and Fuel...

    Office of Environmental Management (EM)

    Training Resource Prepares Rescuers for Hydrogen and Fuel Cell Emergencies New Training Resource Prepares Rescuers for Hydrogen and Fuel Cell Emergencies April 21, 2015 - 11:26am...

  3. Student Design Competition Guide to Project Preparation and Submittal...

    Energy Savers [EERE]

    Design Competition Guide to Project Preparation and Submittal Student Design Competition Guide to Project Preparation and Submittal, from the U.S. Department of Energy's Zero...

  4. apatite powders prepared: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    , and thermal properties of Nafion powders prepared by high-energy ball milling of pellets is given. Nafion powders prepared in this manner exhibit thermal behavior similar...

  5. Secretary Steven Chu's Remarks as Prepared for Delivery at the...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Chu's Remarks as Prepared for Delivery at the Polytechnic Institute of New York University Secretary Steven Chu's Remarks as Prepared for Delivery at the Polytechnic Institute...

  6. EA-1947: Notice of Intent to Prepare an Environmental Assessment...

    Energy Savers [EERE]

    Notice of Intent to Prepare an Environmental Assessment and Cancellation of an Environmental Impact Statement EA-1947: Notice of Intent to Prepare an Environmental Assessment and...

  7. EIS-0496: Notice of Intent to Prepare an Environmental Impact...

    Energy Savers [EERE]

    6: Notice of Intent to Prepare an Environmental Impact Statement EIS-0496: Notice of Intent to Prepare an Environmental Impact Statement DOE's Western Area Power Administration...

  8. EIS-0481: Notice of Intent to Prepare a Programmatic Environmental...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0481: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Engineered High Energy...

  9. EIS-0500: Notice of Intent to Prepare Environmental Impact Statement...

    Energy Savers [EERE]

    Notice of Intent to Prepare Environmental Impact Statement EIS-0500: Notice of Intent to Prepare Environmental Impact Statement Crystal Springs Hatchery Program; Bingham, Custer,...

  10. EIS-0481: Notice of Intent to Prepare a Programmatic Environmental...

    Energy Savers [EERE]

    81: Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0481: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Engineered High...

  11. Redox Chemistry in Thin Layers of Organometallic Complexes Prepared...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Redox Chemistry in Thin Layers of Organometallic Complexes Prepared Using Ion Soft Landing. Redox Chemistry in Thin Layers of Organometallic Complexes Prepared Using Ion Soft...

  12. Student Competition Prepares the Next Generation of Wind Energy...

    Broader source: Energy.gov (indexed) [DOE]

    Competition Prepares the Next Generation of Wind Energy Entrepreneurs Student Competition Prepares the Next Generation of Wind Energy Entrepreneurs April 11, 2013 - 11:32am Addthis...

  13. President Issues Executive Order Aimed at Preparing for the Impacts...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Issues Executive Order Aimed at Preparing for the Impacts of Climate Change; Tribal Leaders to Serve on Task Force President Issues Executive Order Aimed at Preparing for the...

  14. EIS-0394: Advance Notice of Intent to Prepare an Environmental...

    Energy Savers [EERE]

    Advance Notice of Intent to Prepare an Environmental Impact Statement EIS-0394: Advance Notice of Intent to Prepare an Environmental Impact Statement Implementation of the...

  15. EM's Richland Operations Office Marks Milestone in Preparing...

    Office of Environmental Management (EM)

    Richland Operations Office Marks Milestone in Preparing its Highest-Risk Facility for Demolition EM's Richland Operations Office Marks Milestone in Preparing its Highest-Risk...

  16. Microsoft Word - JWS Sample.doc

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    7 SAMPLE ONLY REV2021005 SAMPLE ONLY Joint Work Statement For CRADA No. Sample BETWEEN U. S. Department of Energy Naval Petroleum Reserve No. 3 Rocky Mountain Oilfield Testing...

  17. RAPID SEPARATION OF ACTINIDES AND RADIOSTRONTIUM IN VEGETATION SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.

    2010-06-01T23:59:59.000Z

    A new rapid method for the determination of actinides and radiostrontium in vegetation samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used in emergency response situations or for routine analysis. The actinides in vegetation method utilizes a rapid sodium hydroxide fusion method, a lanthanum fluoride matrix removal step, and a streamlined column separation process with stacked TEVA, TRU and DGA Resin cartridges. Lanthanum was separated rapidly and effectively from Am and Cm on DGA Resin. Alpha emitters are prepared using rare earth microprecipitation for counting by alpha spectrometry. The purified {sup 90}Sr fractions are mounted directly on planchets and counted by gas flow proportional counting. The method showed high chemical recoveries and effective removal of interferences. The actinide and {sup 90}Sr in vegetation sample analysis can be performed in less than 8 h with excellent quality for emergency samples. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory actinide particles or vegetation residue after furnace heating is effectively digested.

  18. Anthrax Sampling and Decontamination: Technology Trade-Offs

    SciTech Connect (OSTI)

    Price, Phillip N.; Hamachi, Kristina; McWilliams, Jennifer; Sohn, Michael D.

    2008-09-12T23:59:59.000Z

    The goal of this project was to answer the following questions concerning response to a future anthrax release (or suspected release) in a building: 1. Based on past experience, what rules of thumb can be determined concerning: (a) the amount of sampling that may be needed to determine the extent of contamination within a given building; (b) what portions of a building should be sampled; (c) the cost per square foot to decontaminate a given type of building using a given method; (d) the time required to prepare for, and perform, decontamination; (e) the effectiveness of a given decontamination method in a given type of building? 2. Based on past experience, what resources will be spent on evaluating the extent of contamination, performing decontamination, and assessing the effectiveness of the decontamination in abuilding of a given type and size? 3. What are the trade-offs between cost, time, and effectiveness for the various sampling plans, sampling methods, and decontamination methods that have been used in the past?

  19. The beryllium quandary: will the lower exposure limits spur new developments in sampling and analysis?

    SciTech Connect (OSTI)

    Brisson, Michael

    2013-06-03T23:59:59.000Z

    At the time this article was written, new rulemakings were under consideration at OSHA and the U.S. Department of Energy (DOE) that would propose changes to occupational exposure limits for beryllium. Given these developments, it’s a good time to review the tools and methods available to IHs for assessing beryllium air and surface contamination in the workplace—what’s new and different, and what’s tried and true. The article discusses limit values and action levels for beryllium, problematic aspects of beryllium air sampling, sample preparation, sample analysis, and data evaluation.

  20. Synchronized sampling improves fault location

    SciTech Connect (OSTI)

    Kezunovic, M. [Texas A and M Univ., College Station, TX (United States)] [Texas A and M Univ., College Station, TX (United States); Perunicic, B. [Lamar Univ., Beaumont, TX (United States)] [Lamar Univ., Beaumont, TX (United States)

    1995-04-01T23:59:59.000Z

    Transmission line faults must be located accurately to allow maintenance crews to arrive at the scene and repair the faulted section as soon as possible. Rugged terrain and geographical layout cause some sections of power transmission lines to be difficult to reach. In the past, a variety of fault location algorithms were introduced as either an add-on feature in protective relays or stand-alone implementation in fault locators. In both cases, the measurements of current and voltages were taken at one terminal of a transmission line only. Under such conditions, it may become difficult to determine the fault location accurately, since data from other transmission line ends are required for more precise computations. In the absence of data from the other end, existing algorithms have accuracy problems under several circumstances, such as varying switching and loading conditions, fault infeed from the other end, and random value of fault resistance. Most of the one-end algorithms were based on estimation of voltage and current phasors. The need to estimate phasors introduces additional difficulty in high-speed tripping situations where the algorithms may not be fast enough in determining fault location accurately before the current signals disappear due to the relay operation and breaker opening. This article introduces a unique concept of high-speed fault location that can be implemented either as a simple add-on to the digital fault recorders (DFRs) or as a stand-alone new relaying function. This advanced concept is based on the use of voltage and current samples that are synchronously taken at both ends of a transmission line. This sampling technique can be made readily available in some new DFR designs incorporating receivers for accurate sampling clock synchronization using the satellite Global Positioning System (GPS).

  1. Tank farm backlog soil sample analysis plan

    SciTech Connect (OSTI)

    Ahlers, J.D., Westinghouse Hanford

    1996-07-17T23:59:59.000Z

    This document describes the measures to collect samples, perform testing on samples, and make decisions to obtain a Contained- in Determination for tank farms backlog soil.

  2. Radioactive Samples / Materials at the APS

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Radioactive Samples Materials at the APS The use of radioactive samples requires additional information for review and approval. All proposed experiments involving...

  3. Gas Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page onYou are now leaving Energy.gov You are now leaving Energy.gov You are being directedAnnualPropertyd8c-a9ae-f8521cbb8489InformationFrenchtown, NewG22 JumpGas Sampling Jump to:

  4. Sample Licensing Agreements | Partnerships | ORNL

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level:Energy: Grid Integration Redefining What's PossibleRadiation Protection245C Unlimited ReleaseWelcome ton6 th US/German Workshop onSample

  5. Sample Retention Incentive Service Agreement

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels DataDepartment of Energy Your Density Isn'tOrigin ofEnergy atLLC - FE DKT. 10-160-LNG - ORDERSTATE0-1ofEnergy Sample Employee:

  6. Soil Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page onYou are now leaving Energy.gov You are now leaving Energy.gov You are beingZealand Jump to:Ezfeedflag JumpID-f < RAPID‎ |RippeyInformationSoda Springs, Idaho:Soil Sampling Jump

  7. Groundwater Sampling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page onYou are now leaving Energy.gov You are now leaving Energy.gov You are8COaBulkTransmissionSitingProcess.pdfGetec AG| Open Energy Information 2000)2004) |1978) |Groundwater Sampling

  8. Preparation and screening of crystalline inorganic materials

    DOE Patents [OSTI]

    Schultz, Peter G. (La Jolla, CA); Xiang, Xiaodong (Danville, CA); Goldwasser, Isy (Palo Alto, CA); Brice{hacek over (n)}o, Gabriel (Baldwin Park, CA); Sun, Xiao-Dong (Fremont, CA); Wang, Kai-An (Cupertino, CA)

    2008-10-28T23:59:59.000Z

    Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc. Once prepared, these materials can be screened for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical, or other properties. Thus, the present invention provides methods for the parallel synthesis and analysis of novel materials having useful properties.

  9. Remote state preparation of spatial qubits

    E-Print Network [OSTI]

    M. A. Solís-Prosser; L. Neves

    2011-08-17T23:59:59.000Z

    We study the quantum communication protocol of remote state preparation (RSP) for pure states of qubits encoded in single photons transmitted through a double slit, the so-called spatial qubits. Two measurement strategies that one can adopt to remotely prepare the states are discussed. The first strategy is the well-known spatial postselection, where a single-pixel detector measures the transverse position of the photon between the focal and the image plane of a lens. The second strategy, proposed by ourselves, is a generalized measurement divided into two steps: the implementation of a two-outcome positive operator-valued measurement (POVM) followed by the spatial postselection at the focal plane of the lens by a two-pixel detector in each output of the POVM. In both cases we analyze the effects of the finite spatial resolution of the detectors over three figures of merit of the protocol, namely, the probability of preparation, the fidelity and purity of the remotely prepared states. It is shown that our strategy improves these figures compared with spatial postselection, at the expense of increasing the classical communication cost as well as the required experimental resources. In addition, we present a modified version of our strategy for RSP of spatial qudits which is able to prepare arbitrary pure states, unlike spatial postselection alone. We expect that our study may also be extended for RSP of the angular spectrum of a single-photon field as an alternative for quantum teleportation which requires very inefficient nonlinear interactions.

  10. Apparatus for sectioning demountable semiconductor samples

    DOE Patents [OSTI]

    Sopori, Bhushan L. (Scottsdale, AZ); Wolf, Abraham (Sun City West, AZ)

    1984-01-01T23:59:59.000Z

    Apparatus for use during polishing and sectioning operations of a ribbon sample is described. The sample holder includes a cylinder having an axially extending sample cavity terminated in a first funnel-shaped opening and a second slot-like opening. A spring-loaded pressure plunger is located adjacent the second opening of the sample cavity for frictional engagement of the sample prior to introduction of a molding medium in the sample cavity. A heat softenable molding medium is inserted in the funnel-shaped opening, to surround the sample. After polishing, the heater is energized to allow draining of the molding medium from the sample cavity. During manual polishing, the second end of the sample holder is inserted in a support ring which provides mechanical support as well as alignment of the sample holder during polishing. A gauge block for measuring the protrusion of a sample beyond the second wall of the holder is also disclosed.

  11. Nanocrystalline Complex Oxides Prepared by Mechanochemical Reactions

    SciTech Connect (OSTI)

    Sepelak, V. [Institute of Nanotechnology, Karlsruhe Institute of Technology, Herrmann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany); On leave from the Slovak Academy of Sciences, Watsonova 45, 04353 Kosice (Slovakia); Bergmann, I. [VOLKSWAGEN AG, 38436 Wolfsburg (Germany); Indris, S. [Institute of Nanotechnology, Karlsruhe Institute of Technology, Herrmann-von-Helmholtz-Platz 1, 76344 Eggenstein-Leopoldshafen (Germany); Subrt, J. [Institute of Inorganic Chemistry, Academy of Sciences of Czech Republic, 25068 Rez (Czech Republic); Heitjans, P. [Institute of Physical Chemistry and Electrochemistry, Leibniz University Hannover, Callinstrasse 3-3A, 30167 Hannover (Germany); Becker, K.-D. [Institute of Physical and Theoretical Chemistry, Braunschweig University of Technology, Hans-Sommer-Strasse 10, 38106 Braunschweig (Germany)

    2010-07-13T23:59:59.000Z

    The preparation of complex oxides by the conventional solid-state (ceramic) route requires a number of stages, including homogenization of the powder precursors, compaction of the reactants, and finally prolonged heat treatment at considerably elevated temperatures under controlled oxygen fugacity. One goal of modern materials research and development has been to identify simpler processing schemes that do not rely upon high-temperature treatments for inducing solid-state reactions. At present, mechanochemical methods become widely used for the preparation of nanocrystalline materials due to their relative simplicity and availability. In this work, selected examples of the preparation of nanoscale complex oxides via single-step mechanochemical routes are presented. Nuclear spectroscopic methods are employed to follow the mechanically induced formation of nanooxides and to characterize the nonequilibrium structural state of the resulting nanophases at the atomic level.

  12. Characterization Data Package for Containerized Sludge Samples Collected from Engineered Container SCS-CON-210

    SciTech Connect (OSTI)

    Fountain, Matthew S.; Fiskum, Sandra K.; Baldwin, David L.; Daniel, Richard C.; Bos, Stanley J.; Burns, Carolyn A.; Carlson, Clark D.; Coffey, Deborah S.; Delegard, Calvin H.; Edwards, Matthew K.; Greenwood, Lawrence R.; Neiner, Doinita; Oliver, Brian M.; Pool, Karl N.; Schmidt, Andrew J.; Shimskey, Rick W.; Sinkov, Sergey I.; Snow, Lanee A.; Soderquist, Chuck Z.; Thompson, Christopher J.; Trang-Le, Truc LT; Urie, Michael W.

    2013-09-10T23:59:59.000Z

    This data package contains the K Basin sludge characterization results obtained by Pacific Northwest National Laboratory during processing and analysis of four sludge core samples collected from Engineered Container SCS-CON-210 in 2010 as requested by CH2M Hill Plateau Remediation Company. Sample processing requirements, analytes of interest, detection limits, and quality control sample requirements are defined in the KBC-33786, Rev. 2. The core processing scope included reconstitution of a sludge core sample distributed among four to six 4-L polypropylene bottles into a single container. The reconstituted core sample was then mixed and subsampled to support a variety of characterization activities. Additional core sludge subsamples were combined to prepare a container composite. The container composite was fractionated by wet sieving through a 2,000 micron mesh and a 500-micron mesh sieve. Each sieve fraction was sampled to support a suite of analyses. The core composite analysis scope included density determination, radioisotope analysis, and metals analysis, including the Waste Isolation Pilot Plant Hazardous Waste Facility Permit metals (with the exception of mercury). The container composite analysis included most of the core composite analysis scope plus particle size distribution, particle density, rheology, and crystalline phase identification. A summary of the received samples, core sample reconstitution and subsampling activities, container composite preparation and subsampling activities, physical properties, and analytical results are presented. Supporting data and documentation are provided in the appendices. There were no cases of sample or data loss and all of the available samples and data are reported as required by the Quality Assurance Project Plan/Sampling and Analysis Plan.

  13. INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING DISTRIBUTION, AND POPULATION

    E-Print Network [OSTI]

    Yu, Alex

    INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING Keywords: Parametric test, sample, population, sampling distributions Parametric tests are frequently parametric tests, nor hold beliefs that are consistent with that framework. The parametric test framework

  14. Method of preparing meso-haloalkylporphyrins

    DOE Patents [OSTI]

    Wijesekera, Tilak (Glen Mills, PA); Lyons, James E. (Wallingford, PA); Ellis, Jr., Paul E. (Downingtown, PA); Bhinde, Manoj V. (Boothwyn, PA)

    1998-01-01T23:59:59.000Z

    Transition metal complexes of meso-haloalkylporphyrins, wherein the haloalkyl groups contain 2 to 8 carbon atoms have been found to be highly effective catalysts for oxidation of alkanes and for the decomposition of hydroperoxides. Also disclosed is a process for the preparation of meso-halocarbyl-porphyrins which comprises contacting a halocarbyl dipyrromethane with a halocarbyl-substituted aldehyde in the presence of an acid granular solid catalyst. Also disclosed is a process for the preparation of meso-halocarbyl-porphyrins which comprises contacting a halocarbyl dipyrromethane with a halocarbyl-substituted aldehyde in the presence of an acid granular solic catalyst.

  15. Characterization of gels prepared from silicon ethoxide

    E-Print Network [OSTI]

    Yun, Su-Jin

    1990-01-01T23:59:59.000Z

    by heating to a high temperature, with low heating rates. Tg and Tc were correlated to water gt alcohol contents in presence of HCI or HF. Aerogels were found to have high pore volume, low bulk density, large pore size, and weak mechanical strength.... Structures of dried gels 2. 3, Densification 13 14 15 19 19 CHAPTER III 3. 1. Raw materials 3. 2. Xerogel preparation 3. 3. Aerogel preparation 3. 4. Characterization of dried gels 3, 4. 1. Mercury porosimetry 3. 4. 2. BET analysis 3. 4, 3...

  16. Characterization of gels prepared from silicon ethoxide 

    E-Print Network [OSTI]

    Yun, Su-Jin

    1990-01-01T23:59:59.000Z

    by heating to a high temperature, with low heating rates. Tg and Tc were correlated to water gt alcohol contents in presence of HCI or HF. Aerogels were found to have high pore volume, low bulk density, large pore size, and weak mechanical strength.... Structures of dried gels 2. 3, Densification 13 14 15 19 19 CHAPTER III 3. 1. Raw materials 3. 2. Xerogel preparation 3. 3. Aerogel preparation 3. 4. Characterization of dried gels 3, 4. 1. Mercury porosimetry 3. 4. 2. BET analysis 3. 4, 3...

  17. PREPARATION AND SPECTROSCOPIC PROPERTIES OF THREE NEW ACTINIDE (IV) BOROHYDRIDES

    E-Print Network [OSTI]

    Banks, Rodney Howard

    2010-01-01T23:59:59.000Z

    uranium tetrakis-borohydrides were prepared by a different reaction which involves the actinide tetrafluoride

  18. Process for the preparation of an energetic nitrate ester

    DOE Patents [OSTI]

    Chavez, David E; Naud, Darren L; Hiskey, Michael A

    2013-12-17T23:59:59.000Z

    A process for the preparation of an energetic nitrate ester compound and related intermediates is provided.

  19. "Dedicated to Maximizing Planetary Sample Science

    E-Print Network [OSTI]

    Rathbun, Julie A.

    that evaluated sample mass with regards to previous Apollo Program surface activity, scientific productivity and environmentally sensitive samples. (2) This geological sample mass exceeds that of the Apollo 17 mission by only that of the Apollo Program to demonstrate we have progressed beyond Apollo. (3) Using the Apollo sample containers

  20. Diffraction-limited ultrasensitive molecular nano-arrays with singular nano-cone Yunshan Wang, Ting-Chou Chang, Paul R. Stoddart, and Hsueh-Chia Chang

    E-Print Network [OSTI]

    Chang, Hsueh-Chia

    Wang, Ting-Chou Chang, Paul R. Stoddart, and Hsueh-Chia Chang Citation: Biomicrofluidics 8, 021101-arrays with singular nano-cone scattering Yunshan Wang,1 Ting-Chou Chang,1 Paul R. Stoddart,2 and Hsueh-Chia Chang1 1

  1. Sample introduction apparatus for a flow cytometer

    DOE Patents [OSTI]

    Van den Engh, Ger (Seattle, WA)

    1998-01-01T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

  2. Sample introduction system for a flow cytometer

    DOE Patents [OSTI]

    Engh, G. van den

    1997-02-11T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

  3. Sample introduction system for a flow cytometer

    DOE Patents [OSTI]

    Van den Engh, Ger (Seattle, WA)

    1997-01-01T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

  4. Sample introduction apparatus for a flow cytometer

    DOE Patents [OSTI]

    Van den Engh, G.

    1998-03-10T23:59:59.000Z

    A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

  5. PHYSICAL PROPERTY MEASUREMENTS OF LABORATORY PREPARED SALTSTONE GROUT

    SciTech Connect (OSTI)

    Hansen, E.; Cozzi, A.; Edwards, T.

    2014-05-05T23:59:59.000Z

    The Saltstone Production Facility (SPF) built two new Saltstone Disposal Units (SDU), SDU 3 and SDU 5, in 2013. The variable frequency drive (VFD) for the grout transfer hose pump tripped due to high current demand by the motor during the initial radioactive saltstone transfer to SDU 5B on 12/5/2013. This was not observed during clean cap processing on July 5, 2013 to SDU 3A, which is a slightly longer distance from the SPF than is SDU 5B. Saltstone Design Authority (SDA) is evaluating the grout pump performance and capabilities to transfer the grout processed in SPF to SDU 3/5. To assist in this evaluation, grout physical properties are required. At this time, there are no rheological data from the actual SPF so the properties of laboratory prepared samples using simulated salt solution or Tank 50 salt solution will be measured. The physical properties of grout prepared in the laboratory with de-ionized water (DI) and salt solutions were obtained at 0.60 and 0.59 water to premix (W/P) ratios, respectively. The yield stress of the DI grout was greater than any salt grout. The plastic viscosity of the DI grout was lower than all of the salt grouts (including salt grout with admixture). When these physical data were used to determine the pressure drop and fluid horsepower for steady state conditions, the salt grouts without admixture addition required a higher pressure drop and higher fluid horsepower to transport. When 0.00076 g Daratard 17/g premix was added, both the pressure drop and fluid horsepower were below that of the DI grout. Higher concentrations of Daratard 17 further reduced the pressure drop and fluid horsepower. The uncertainty in the single point Bingham Plastic parameters is + 4% of the reported values and is the bounding uncertainty. Two different mechanical agitator mixing protocols were followed for the simulant salt grout, one having a total mixing time of three minutes and the other having a time of 10 minutes. The Bingham Plastic parameters were essentially the same for the salt grout without admixture. When Daratard 17 was added, the Bingham Plastic yield stress increased for the 10 minute mix. The simulant salt used in this task had similar physical properties of the Tank 50 3Q13 salt grout and is recommended for future use, if the salt solution in Tank 50 does not change. The design basis physical properties used to size the pumps and mixers at SPF were obtained from DPST-85-312. The grouts characterized in this report are bounded by the design basis density and Bingham Plastic yield stress. The opposite is true for the plastic viscosity. Steady state pressure drop calculations were performed for the design basis values using the flow rate for the clean cap and salt grouts and they bound the pressure drop of the grouts characterized in this report. A comparison of the lab prepared samples to PI ProcessBook data, specifically average pressure drop, indicate that the lab prepared samples are more viscous in nature than what is processed in the facility. This difference could be due to the applied shear rates which could be lower in the lab as compared to the facility and that fact the SPF added flush water, making this comparison more difficult. A perfunctory review of the PI ProcessBook data was discussed. It may be possible that the frequency that the distributed control system alters the grout pump speed to maintain grout hopper volume can negatively affect the efficiency of the grout pump.

  6. REPORT ON THE ANALYSIS OF WAC SAMPLES FROM EVAPORATOR OVERHEADS FOR 2011

    SciTech Connect (OSTI)

    Washington, A.

    2012-03-29T23:59:59.000Z

    This report tabulates the chemical analysis of the 3H, 2H and 2F evaporator overhead samples including the inorganic, organic, and radionuclide species according the ETP WAC (rev.4). In addition, the physical properties including pH, total suspended solids, and average particle size are listed for each sample. The report identifies all sample receipt dates, preparation methods, and analyses completed to accumulate these values. All values were found to be within the ETP WAC specifications for WWCT except for the {sup 137}Cs concentration for the 2F sample which was slightly above the limit ({approx}5%). However, tank farm personnel sample each tank overhead for beta/gamma prior to transfer using a pulse height analyzer and these field readings were all well within limits. Additional actions will be taken to help understand the reason in the discrepancy of the field measurement versus laboratory analysis.

  7. Pi sampling: a methodical and flexible approach to initial macromolecular crystallization screening

    SciTech Connect (OSTI)

    Gorrec, Fabrice, E-mail: fgorrec@mrc-lmb.cam.ac.uk; Palmer, Colin M.; Lebon, Guillaume; Warne, Tony [MRC Laboratory of Molecular Biology, Hills Road, Cambridge CB2 0QH (United Kingdom)

    2011-05-01T23:59:59.000Z

    Pi sampling, derived from the incomplete factorial approach, is an effort to maximize the diversity of macromolecular crystallization conditions and to facilitate the preparation of 96-condition initial screens. The Pi sampling method is derived from the incomplete factorial approach to macromolecular crystallization screen design. The resulting ‘Pi screens’ have a modular distribution of a given set of up to 36 stock solutions. Maximally diverse conditions can be produced by taking into account the properties of the chemicals used in the formulation and the concentrations of the corresponding solutions. The Pi sampling method has been implemented in a web-based application that generates screen formulations and recipes. It is particularly adapted to screens consisting of 96 different conditions. The flexibility and efficiency of Pi sampling is demonstrated by the crystallization of soluble proteins and of an integral membrane-protein sample.

  8. Hurricane Season 2006: Preparation is your

    E-Print Network [OSTI]

    Wood, Stephen L.

    Hurricane Season 2006: Preparation is your first step to SAFETY 2005 Hurricanes NAME CATEGORY Cindy A HURRICANE WATCH,issued for your part of the coast, indicates the possibility that you could experience hurricane conditions within 36 hours. This watch should trigger your disaster plan,and protective measures

  9. Retsch PM400 ball mill Nanoparticle preparation

    E-Print Network [OSTI]

    Anderson, Scott L.

    the presence of a low binding energy boride species (CexBy) XPS Catalyst Coated, Unoxidized Boron NanoparticlesRetsch PM400 ball mill pump Nanoparticle preparation Ball Milling Method Physically grind micron are coated with various ligands/capping agents to promote suspension in a variety of fuels and/or to protect

  10. Prepared by Ryan T. Kennelly, Economic Analyst

    E-Print Network [OSTI]

    Hemmers, Oliver

    Prepared by Ryan T. Kennelly, Economic Analyst Center for Business and Economic Research Lee Business School University of Nevada, Las Vegas October 2012 #12;The Center for Business and Economic new economic indexes for the metropolitan area of Las Vegas, Nevada. We first construct a coincident

  11. Technical Note Graphene: Substrate preparation and introduction

    E-Print Network [OSTI]

    Technical Note Graphene: Substrate preparation and introduction Radosav S. Pantelic a , Ji Won Suk September 2010 Accepted 4 October 2010 Available online xxxx Keywords: Graphene Graphene oxide Cryo the transfer of continuous, single-layer, pristine graphene to standard Quan- tifoil TEM grids. We compare

  12. Preparation of a semiconductor thin film

    DOE Patents [OSTI]

    Pehnt, M.; Schulz, D.L.; Curtis, C.J.; Ginley, D.S.

    1998-01-27T23:59:59.000Z

    A process is disclosed for the preparation of a semiconductor film. The process comprises depositing nanoparticles of a semiconductor material onto a substrate whose surface temperature during nanoparticle deposition thereon is sufficient to cause substantially simultaneous fusion of the nanoparticles to thereby coalesce with each other and effectuate film growth.

  13. Assessment Update 2009 Prepared: July 27, 2009

    E-Print Network [OSTI]

    Maxwell, Bruce D.

    1 Assessment Update 2009 Prepared: July 27, 2009 CHBE assessment activities during AY 2008 Thresholds Details of Assessment Activities Inputs Assessment Threshold Response Review The Faculty tightened) Safety in Senior Design Reports: I viewed the Coal Bed Methane Water Treatment Project and the Coal

  14. Leafy Green Preparation and Cooling Study

    E-Print Network [OSTI]

    Leafy Green Preparation and Cooling Study Dominique N. Bibbins #12;Background : Leafy Greens z In the past, leafy greens have been the source of food borne-illnesses and outbreaks. z It is important Lasting knowledge of survey practices, procedures, and protocol. #12;Acknowledgements z Laura Green, Ph

  15. Data Update for Paxton, MA Prepared for

    E-Print Network [OSTI]

    Massachusetts at Amherst, University of

    Data Update for Paxton, MA May, 2006 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for May, 2006 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

  16. Data Update for Paxton, MA Prepared for

    E-Print Network [OSTI]

    Massachusetts at Amherst, University of

    Data Update for Paxton, MA June, 2006 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for June, 2006 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

  17. Data Update for Paxton, MA Prepared for

    E-Print Network [OSTI]

    Massachusetts at Amherst, University of

    Data Update for Paxton, MA May, 2005 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for May, 2005 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

  18. Data Update for Paxton, MA Prepared for

    E-Print Network [OSTI]

    Massachusetts at Amherst, University of

    Data Update for Paxton, MA July, 2005 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for July, 2005 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

  19. Data Update for Paxton, MA Prepared for

    E-Print Network [OSTI]

    Massachusetts at Amherst, University of

    Data Update for Paxton, MA June, 2005 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for June, 2005 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

  20. Data Update for Paxton, MA Prepared for

    E-Print Network [OSTI]

    Massachusetts at Amherst, University of

    Data Update for Paxton, MA July, 2006 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for July, 2006 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

  1. Elizabeth Alison Thompson a. Professional Preparation

    E-Print Network [OSTI]

    Borenstein, Elhanan

    Elizabeth Alison Thompson a. Professional Preparation Instutution Major Degree Year Cambridge Proceedings 70) Five most closely related Koepke, H. A., and Thompson, E. A. (2013) Efficient identification of equivalences in dynamic graphs and pedigree structures. Journal of Computational Biology 20: 551-570. Thompson

  2. Preparation of III-V semiconductor nanocrystals

    DOE Patents [OSTI]

    Alivisatos, A.P.; Olshavsky, M.A.

    1996-04-09T23:59:59.000Z

    Nanometer-scale crystals of III-V semiconductors are disclosed. They are prepared by reacting a group III metal source with a group V anion source in a liquid phase at elevated temperature in the presence of a crystallite growth terminator such as pyridine or quinoline. 4 figs.

  3. Energy Simulation Training Prepared for the

    E-Print Network [OSTI]

    `i Natural Energy Institute University of Hawai`i Manoa #12;#12;TABLE OF CONTENTS HNEI FUNDING Program Subtask 3.5.1: Residential Energy Efficiency Deliverable 3 Prepared by The University of Hawai and Earth Science and Technology University of Hawai`i April 2013 #12;Acknowledgement: This material

  4. Test Preparation Options Free Test Prep Websites

    E-Print Network [OSTI]

    Stowell, Michael

    Test Preparation Options Free Test Prep Websites ACT: http: http://www.collegeboard.com/student/testing/sat/prep_one/test.html http://www.number2.com://testprep.princetonreview.com/CourseSearch/Search.aspx?itemCode=17&productType=F&rid=1&zip=803 02 Test Prep Classes Front Range Community College: Classes

  5. Preparation of a semiconductor thin film

    DOE Patents [OSTI]

    Pehnt, Martin (TuBingen, DE); Schulz, Douglas L. (Denver, CO); Curtis, Calvin J. (Lakewood, CO); Ginley, David S. (Evergreen, CO)

    1998-01-01T23:59:59.000Z

    A process for the preparation of a semiconductor film. The process comprises depositing nanoparticles of a semiconductor material onto a substrate whose surface temperature during nanoparticle deposition thereon is sufficient to cause substantially simultaneous fusion of the nanoparticles to thereby coalesce with each other and effectuate film growth.

  6. Glacier Recession Prepared by Joni L. Kincaid

    E-Print Network [OSTI]

    Glacier Recession Prepared by Joni L. Kincaid for the Advancing Geospatial Skills in Science funded by the National Science Foundation's GK-12 Program. Spring, 2007 #12;Glacier: a large mass of ice Line Glacier How do glaciers form? Glaciers form in locations where the snow does not melt over

  7. Photocatalytic methods for preparation of electrocatalyst materials

    DOE Patents [OSTI]

    Nwoga, Tochi Tudor; Kawahara, Kazuo; Li, Wen; Song, Yujiang; Shelnutt, John A; Miller, James E; Medforth, Craig John; Ueno, Yukiyoshi; Kawamura, Tetsuo

    2013-12-17T23:59:59.000Z

    The invention relates to methods of preparing metal particles on a support material, including platinum-containing nanoparticles on a carbon support. Such materials can be used as electrocatalysts, for example as improved electrocatalysts in proton exchange membrane fuel cells (PEM-FCs).

  8. Photocatalytic methods for preparation of electrocatalyst materials

    DOE Patents [OSTI]

    Li, Wen; Kawamura, Tetsuo; Nagami, Tetsuo; Takahashi, Hiroaki; Muldoon, John; Shelnutt, John A; Song, Yujiang; Miller, James E; Hickner, Michael A; Medforth, Craig

    2013-09-24T23:59:59.000Z

    The invention relates to methods of preparing metal particles on a support material, including platinum-containing nanoparticles on a carbon support. Such materials can be used as electrocatalysts, for example as improved electrocatalysts in polymer electrolyte membrane fuel cells (PEM-FCs).

  9. Energy Efficient Data Centers Prepared by

    E-Print Network [OSTI]

    Board - Equinix · Pacific Gas and Electric Company · New York State Energy Research and DevelopmentEnergy Efficient Data Centers Prepared by William Tschudi, Tengfang Xu, Dale Sartor, Bruce Nordman, Jon Koomey, and Osman Sezgen Environmental Energy Technologies Division Lawrence Berkeley National

  10. prepared at INRIA Sophia-Antipolis

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia-Antipolis and presented at the University of Nice Sophia-Electrodes acquisitions in the retina Hassan NASSER Advisor Pr. Bruno Cessac INRIA Sophia-Antipolis Reviewers Pr. Stefano Statistique de l'ENS Examiners Pr. Pierre Kornprobst INRIA Sophia-Antipolis Pr. Adrián Palacios University

  11. prepared at INRIA Sophia-Antipolis Mediterranee

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia-Antipolis M´editerran´ee and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation´e-Salp^etri`ere, Paris, France Dr. Pierre Comon I3S / CNRS / University of Nice, France Dr. Rachid Deriche INRIA Sophia

  12. prepared at Inria Sophia Antipolis -Mediterranee

    E-Print Network [OSTI]

    Recanati, Catherine

    PhD THESIS prepared at Inria Sophia Antipolis - M´editerran´ee and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation. Rachid Deriche, Inria Sophia Antipolis-M´editerran´ee, France Reviewers Dr. Christian Barillot, CNRS

  13. prepared at INRIA Sophia-Antipolis Mediterranee

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia-Antipolis M´editerran´ee and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation Features in Diffusion MRI Jian CHENG Advisers Dr. Rachid Deriche INRIA Sophia Antipolis, France Dr. Tianzi

  14. prepared at INRIA Sophia Antipolis -Mditerrane

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    PhD THESIS prepared at INRIA Sophia Antipolis - Méditerranée and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation INRIA Sophia Antipolis, France Thierry VI�VILLE INRIA Sophia Antipolis, France President Rachid DERICHE

  15. PREPARING THE VIRTUAL CLASSROOM FOR DISTANCE DELIVERY

    E-Print Network [OSTI]

    Dyer, Bill

    of humans and their companion domestic animals and livestock. Students learn that there are certain "at riskPREPARING THE VIRTUAL CLASSROOM FOR DISTANCE DELIVERY: MEDICAL-VETERINARY ENTOMOLOGY CLINICS laboratory," library materials, conventional lectures and the 43 virtual patients in the clinics

  16. Process for the preparation of vinyl acetate

    DOE Patents [OSTI]

    Tustin, G.C.; Zoeller, J.R.; Depew, L.S.

    1998-02-17T23:59:59.000Z

    This invention pertains to the preparation of vinyl acetate by contacting within a contact zone a mixture of ketene and acetaldehyde with an acid catalyst at about one bar pressure and between about 85 and 200 C and removing the reaction products from the contact zone.

  17. Prepared for: Michigan Department of Natural Resources

    E-Print Network [OSTI]

    Notre Dame, University of

    Prepared for: Michigan Department of Natural Resources Natural Heritage Grants Program and USDA DISTRIBUTIONS IN GOGEBIC COUNTY, MICHIGAN Dr. Karen E. Francl University of Notre Dame Environmental Research October 2005 #12;2 Abstract This project sought to provide valuable data for the Michigan Herp Atlas

  18. Original article Preparation and radical scavenging activity

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    reaction could be applied to prepare casein antioxidant peptides with higher activity equivalent antioxidant capacity (TEAC). Analysis showed that all casein plasteins had improved radical / radical scavenging activity / antioxidant ­ 9.6% ; : 500 U 30 °C 50% 5.6 h 6 2 1,1- -2

  19. Drug delivery Preparation of Monodisperse Biodegradable Polymer

    E-Print Network [OSTI]

    Prentiss, Mara

    Drug delivery Preparation of Monodisperse Biodegradable Polymer Microparticles Using a Microfluidic Flow-Focusing Device for Controlled Drug Delivery Qiaobing Xu, Michinao Hashimoto, Tram T. Dang, Todd microparticles have broad utility as vehicles for drug delivery and form the basis of several therapies approved

  20. Process of preparing tritiated porous silicon

    DOE Patents [OSTI]

    Tam, S.W.

    1997-02-18T23:59:59.000Z

    A process of preparing tritiated porous silicon is described in which porous silicon is equilibrated with a gaseous vapor containing HT/T{sub 2} gas in a diluent for a time sufficient for tritium in the gas phase to replace hydrogen present in the pore surfaces of the porous silicon. 1 fig.

  1. Preparation of III-V semiconductor nanocrystals

    DOE Patents [OSTI]

    Alivisatos, A. Paul (Berkeley, CA); Olshavsky, Michael A. (Brunswick, OH)

    1996-01-01T23:59:59.000Z

    Nanometer-scale crystals of III-V semiconductors are disclosed, They are prepared by reacting a group III metal source with a group V anion source in a liquid phase at elevated temperature in the presence of a crystallite growth terminator such as pyridine or quinoline.

  2. Process of preparing tritiated porous silicon

    DOE Patents [OSTI]

    Tam, Shiu-Wing (Downers Grove, IL)

    1997-01-01T23:59:59.000Z

    A process of preparing tritiated porous silicon in which porous silicon is equilibrated with a gaseous vapor containing HT/T.sub.2 gas in a diluent for a time sufficient for tritium in the gas phase to replace hydrogen present in the pore surfaces of the porous silicon.

  3. North Sea Whitefish Survey: 2010 Prepared by

    E-Print Network [OSTI]

    ;Executive summary The North Sea Whitefish (NSW) survey sailed on 31 May 2010, fishing operations began on 1North Sea Whitefish Survey: 2010 Prepared by Chris Darby, Danny Normandale, Matthew Parker the first two surveys are encouraging. The NSW recorded a good range of ages for all target species in all

  4. North Sea Whitefish Survey: 2011 Prepared by

    E-Print Network [OSTI]

    ;Executive summary The North Sea Whitefish (NSW) survey sailed on 11 June 2011, fishing operations beganNorth Sea Whitefish Survey: 2011 Prepared by Chris Darby, Danny Normandale, Matthew Parker the three NSW surveys are starting to provide a valuable evaluation of the dynamics of the three target

  5. 1. Prepare 200g of each protein sample in SDS-page loading buffer. 2. Load sample, flanked by prestained molecular weight markers onto a 10% acrylamide gel,

    E-Print Network [OSTI]

    Cravatt, Benjamin

    . 4. Remove supernatant and wash gel bands 2-3x 15' in 500µL 50:50 acetonitrile:100mM ammonium bicarbonate. 5. Remove supernatant and add 50 µL acetonitrile to completely dry gel band (should turn opaque). Remove acetonitrile and speed vac for ~5 minutes or until slices are completely dry. 6. Resuspend a 20µg

  6. RAPID SEPARATION METHOD FOR ACTINIDES IN EMERGENCY SOIL SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.; Culligan, B.; Noyes, G.

    2009-11-09T23:59:59.000Z

    A new rapid method for the determination of actinides in soil and sediment samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used for samples up to 2 grams in emergency response situations. The actinides in soil method utilizes a rapid sodium hydroxide fusion method, a lanthanum fluoride soil matrix removal step, and a streamlined column separation process with stacked TEVA, TRU and DGA Resin cartridges. Lanthanum was separated rapidly and effectively from Am and Cm on DGA Resin. Vacuum box technology and rapid flow rates are used to reduce analytical time. Alpha sources are prepared using cerium fluoride microprecipitation for counting by alpha spectrometry. The method showed high chemical recoveries and effective removal of interferences. This new procedure was applied to emergency soil samples received in the NRIP Emergency Response exercise administered by the National Institute for Standards and Technology (NIST) in April, 2009. The actinides in soil results were reported within 4-5 hours with excellent quality.

  7. Method and apparatus for data sampling

    DOE Patents [OSTI]

    Odell, Daniel M. C. (Aiken, SC)

    1994-01-01T23:59:59.000Z

    A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium.

  8. Method and apparatus for data sampling

    DOE Patents [OSTI]

    Odell, D.M.C.

    1994-04-19T23:59:59.000Z

    A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples is described. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium. 6 figures.

  9. Fluid sampling system for a nuclear reactor

    DOE Patents [OSTI]

    Lau, Louis K. (Monroeville, PA); Alper, Naum I. (Monroeville, PA)

    1994-01-01T23:59:59.000Z

    A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump.

  10. Fluid sampling system for a nuclear reactor

    DOE Patents [OSTI]

    Lau, L.K.; Alper, N.I.

    1994-11-22T23:59:59.000Z

    A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump. 1 fig.

  11. Rapid Microwave Preparation of Highly Efficient Ce[superscript 3+]-Substituted Garnet Phosphors for Solid State White Lighting

    SciTech Connect (OSTI)

    Birkel, Alexander; Denault, Kristin A.; George, Nathan C.; Doll, Courtney E.; Héry, Bathylle; Mikhailovsky, Alexander A.; Birkel, Christina S.; Hong, Byung-Chul; Seshadri, Ram (UCSB); (Mitsubishi)

    2012-04-30T23:59:59.000Z

    Ce{sup 3+}-substituted aluminum garnet compounds of yttrium (Y{sub 3}Al{sub 5}O{sub 12}) and lutetium (Lu{sub 3}Al{sub 5}O{sub 12}) - both important compounds in the generation of (In,Ga)N-based solid state white lighting - have been prepared using a simple microwave heating technique involving the use of a microwave susceptor to provide the initial heat source. Carbon used as the susceptor additionally creates a reducing atmosphere around the sample that helps stabilize the desired luminescent compound. High quality, phase-pure materials are prepared within a fraction of the time and using a fraction of the energy required in a conventional ceramic preparation; the microwave technique allows for a reduction of about 95% in preparation time, making it possible to obtain phase pure, Ce{sup 3+}-substituted garnet compounds in under 20 min of reaction time. It is estimated that the overall reduction in energy compared with ceramic routes as practiced in the lab is close to 99%. Conventionally prepared material is compared with material prepared using microwave heating in terms of structure, morphology, and optical properties, including quantum yield and thermal quenching of luminescence. Finally, the microwave-prepared compounds have been incorporated into light-emitting diode 'caps' to test their performance characteristics in a real device, in terms of their photon efficiency and color coordinates.

  12. Bayesian Statistics Stochastic Simulation -Gibbs sampling

    E-Print Network [OSTI]

    Wright, Francis

    Bayesian Statistics Stochastic Simulation - Gibbs sampling Bayesian Statistics - an Introduction Dr Pettit Bayesian Statistics - an Introduction #12;Bayesian Statistics Stochastic Simulation - Gibbs sampling What is Bayesian Statistics? Bayes Theorem The Likelihood Principle Mixtures of conjugate priors

  13. Curve sampling and geometric conditional simulation

    E-Print Network [OSTI]

    Fan, Ayres C. (Ayres Chee), 1978-

    2008-01-01T23:59:59.000Z

    The main objective of this thesis is the development and exploitation of techniques to generate geometric samples for the purpose of image segmentation. A sampling-based approach provides a number of benefits over existing ...

  14. An introduction to boson-sampling

    E-Print Network [OSTI]

    Bryan T. Gard; Keith R. Motes; Jonathan P. Olson; Peter P. Rohde; Jonathan P. Dowling

    2014-06-26T23:59:59.000Z

    Boson-sampling is a simplified model for quantum computing that may hold the key to implementing the first ever post-classical quantum computer. Boson-sampling is a non-universal quantum computer that is significantly more straightforward to build than any universal quantum computer proposed so far. We begin this chapter by motivating boson-sampling and discussing the history of linear optics quantum computing. We then summarize the boson-sampling formalism, discuss what a sampling problem is, explain why boson-sampling is easier than linear optics quantum computing, and discuss the Extended Church-Turing thesis. Next, sampling with other classes of quantum optical states is analyzed. Finally, we discuss the feasibility of building a boson-sampling device using existing technology.

  15. Principles for Sampling Airborne Radioactivity from Stacks

    SciTech Connect (OSTI)

    Glissmeyer, John A.

    2010-10-18T23:59:59.000Z

    This book chapter describes the special processes involved in sampling the airborne effluents from nuclear faciities. The title of the book is Radioactive Air Sampling Methods. The abstract for this chapter was cleared as PNNL-SA-45941.

  16. Preparation of fullerene/glass composites

    DOE Patents [OSTI]

    Mattes, B.R.; McBranch, D.W.; Robinson, J.M.; Koskelo, A.C.; Love, S.P.

    1995-05-30T23:59:59.000Z

    Synthesis of fullerene/glass composites is described. A direct method for preparing solid solutions of C{sub 60} in silicon dioxide (SiO{sub 2}) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these ``guests`` in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C{sub 60}. Depending upon the preparative procedure, C{sub 60} dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C{sub 60} in a solid glass matrix, is generated by the present method.

  17. Preparation of fullerene/glass composites

    DOE Patents [OSTI]

    Mattes, Benjamin R. (Santa Fe, NM); McBranch, Duncan W. (Santa Fe, NM); Robinson, Jeanne M. (Los Alamos, NM); Koskelo, Aaron C. (Los Alamos, NM); Love, Steven P. (Los Alamos, NM)

    1995-01-01T23:59:59.000Z

    Synthesis of fullerene/glass composites. A direct method for preparing solid solutions of C.sub.60 in silicon dioxide (SiO.sub.2) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these "guests" in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C.sub.60. Depending upon the preparative procedure, C.sub.60 dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C.sub.60 in a solid glass matrix, is generated by the present method.

  18. Remote State Preparation of Mental Information

    E-Print Network [OSTI]

    Patrizio E. Tressoldi; Andrei Khrennikov

    2012-07-26T23:59:59.000Z

    The aim of this paper is to define in theoretical terms and summarise the available experimental evidence that physical and mental "objects", if considered "information units", may present similar classical and quantum models of communication beyond their specific characteristics. Starting with the Remote State Preparation protocol, a variant of the Teleportation protocol, for which formal models and experimental evidence are already available in quantum mechanics, we outline a formal model applied to mental information we defined Remote State Preparation of Mental Information (RSPMI), and we summarise the experimental evidence supporting the feasibility of a RSPMI protocol. The available experimental evidence offers strong support to the possibility of real communication at distance of mental information promoting the integration between disciplines that have as their object of knowledge different aspects of reality, both physical and the mental, leading to a significant paradigm shift in cognitive and information science.

  19. Novel hard compositions and methods of preparation

    DOE Patents [OSTI]

    Sheinberg, H.

    1981-02-03T23:59:59.000Z

    Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value.

  20. Method for preparing porous metal hydride compacts

    DOE Patents [OSTI]

    Ron, M.; Gruen, D.M.; Mendelsohn, M.H.; Sheft, I.

    1980-01-21T23:59:59.000Z

    A method for preparing porous metallic-matrix hydride compacts which can be repeatedly hydrided and dehydrided without disintegration. A mixture of a finely divided metal hydride and a finely divided matrix metal is contacted with a poison which prevents the metal hydride from dehydriding at room temperature and atmospheric pressure. The mixture of matrix metal and poisoned metal hydride is then compacted under pressure at room temperature to form porous metallic-matrix hydride compacts.

  1. Method for preparing porous metal hydride compacts

    DOE Patents [OSTI]

    Ron, Moshe (Haifa, IL); Gruen, Dieter M. (Downers Grove, IL); Mendelsohn, Marshall H. (Woodridge, IL); Sheft, Irving (Oak Park, IL)

    1981-01-01T23:59:59.000Z

    A method for preparing porous metallic-matrix hydride compacts which can be repeatedly hydrided and dehydrided without disintegration. A mixture of a finely divided metal hydride and a finely divided matrix metal is contacted with a poison which prevents the metal hydride from dehydriding at room temperature and atmospheric pressure. The mixture of matrix metal and poisoned metal hydride is then compacted under pressure at room temperature to form porous metallic-matrix hydride compacts.

  2. Process for preparing improved silvered glass mirrors

    DOE Patents [OSTI]

    Buckwalter, C.Q. Jr.

    1980-01-28T23:59:59.000Z

    Glass mirrors having improved weathering properties are prepared by an improvement in the process for making the mirrors. The glass surface after it has been cleaned but before it is silvered, is contacted with a solution of lanthanide rare earths in addition to a sensitization solution of tin or palladium. The addition of the rare earths produces a mirror which has increased resistance to delamination of the silver from the glass surface in the presence of water.

  3. Preparation of nanostructured materials having improved ductility

    DOE Patents [OSTI]

    Zhao, Yonghao; Zhu, Yuntian T.

    2010-04-20T23:59:59.000Z

    A method for preparing a nanostructured aluminum alloy involves heating an aluminum alloy workpiece at temperature sufficient to produce a single phase coarse grained aluminum alloy, then refining the grain size of the workpiece at a temperature at or below room temperature, and then aging the workpiece to precipitate second phase particles in the nanosized grains of the workpiece that increase the ductility without decreasing the strength of the workpiece.

  4. ANALYSIS OF SAMPLES FROM TANK 5F CHEMICAL CLEANING

    SciTech Connect (OSTI)

    Poirier, M.; Fink, S.

    2011-03-07T23:59:59.000Z

    The Savannah River Site (SRS) is preparing Tank 5F for closure. The first step in preparing the tank for closure is mechanical sludge removal. Following mechanical sludge removal, SRS performed chemical cleaning with oxalic acid to remove the sludge heel. Personnel are currently assessing the effectiveness of the chemical cleaning. SRS personnel collected liquid samples during chemical cleaning and submitted them to Savannah River National Laboratory (SRNL) for analysis. Following chemical cleaning, they collected a solid sample (also known as 'process sample') and submitted it to SRNL for analysis. The authors analyzed these samples to assess the effectiveness of the chemical cleaning process. The conclusions from this work are: (1) With the exception of iron, the dissolution of sludge components from Tank 5F agreed with results from the actual waste demonstration performed in 2007. The fraction of iron removed from Tank 5F by chemical cleaning was significantly less than the fraction removed in the SRNL demonstrations. The likely cause of this difference is the high pH following the first oxalic acid strike. (2) Most of the sludge mass remaining in the tank is iron and nickel. (3) The remaining sludge contains approximately 26 kg of barium, 37 kg of chromium, and 37 kg of mercury. (4) Most of the radioactivity remaining in the residual material is beta emitters and {sup 90}Sr. (5) The chemical cleaning removed more than {approx} 90% of the uranium isotopes and {sup 137}Cs. (6) The chemical cleaning removed {approx} 70% of the neptunium, {approx} 83% of the {sup 90}Sr, and {approx} 21% of the {sup 60}Co. (7) The chemical cleaning removed less than 10% of the plutonium, americium, and curium isotopes. (8) The chemical cleaning removed more than 90% of the aluminium, calcium, and sodium from the tank. (9) The cleaning operations removed 61% of lithium, 88% of non-radioactive strontium, and 65% of zirconium. The {sup 90}Sr and non-radioactive strontium were measured by different methods, and the differences in the fraction removed are not statistically significant. (10) Chemical cleaning removed 10-50% of the barium, chromium, iron, magnesium, manganese, and silicon. (11) Chemical cleaning removed only {approx}1% of the nickel.

  5. Visual Sample Plan Version 3.0

    E-Print Network [OSTI]

    PNNL-14970 Visual Sample Plan Version 3.0 User's Guide N. L. Hassig R. O. Gilbert J. E. Wilson B. A-14970 Visual Sample Plan Version 3.0 User's Guide N. L. Hassig R. O. Gilbert J. E. Wilson B. A Sample Plan (VSP) Version 3.0 and provides instructions for using the software. VSP selects

  6. Elemental Analyses of Hanford Surface Neutron Moisture Measurement Calibration Standard Samples

    SciTech Connect (OSTI)

    Watson, W.T., Westinghouse Hanford

    1996-07-31T23:59:59.000Z

    Elemental analyses have been performed on twenty samples taken from the moisture standards prepared to use in performing experimental calibrations of the surface neutron moisture measurement system. These standards consisted of mixtures of sand, hydrated alumina, and boron carbide. Elemental analyses were performed primarily to discover the quantities of any strong thermal neutron absorbers that may have been present in the mixture in unknown trace quantities.

  7. ANALYSIS OF VAPORS FROM METHYLENE CHLORIDE EXTRACTS OF NUCLEAR GRADE HEPA FILTER FIBERGLASS SAMPLES

    SciTech Connect (OSTI)

    FRYE JM; ANASTOS HL; GUTIERREZ FC

    2012-06-07T23:59:59.000Z

    While several organic compounds were detected in the vapor samples used in the reenactment of the preparation of mounts from the extracts of nuclear grade high-efficiency particulate air filter fiberglass samples, the most significant species present in the samples were methylene chloride, phenol, phenol-d6, and 2-fluorophenol. These species were all known to be present in the extracts, but were expected to have evaporated during the preparation of the mounts, as the mounts appeared to be dry before any vapor was collected. These species were present at the following percentages of their respective occupational exposure limits: methylene chloride, 2%; phenol, 0.4%; and phenol-d6, 0.6%. However, there is no established limit for 2-fluorophenol. Several other compounds were detected at low levels for which, as in the case of 2-fluorophenol, there are no established permissible exposure limits. These compounds include 2-chlorophenol; N-nitroso-1-propanamine; 2-fluoro-1,1{prime}-biphenyl; 1,2-dihydroacenaphthylene; 2,5-cyclohexadiene-1,4-dione,2,6-bis(1,1-dimethylethyl); trimethyl oxirane; n-propylpropanamine; 2-(Propylamino)ethanol; 4-methoxy-1-butene; 6-methyl-5-hepten-2-one; and 3,4-dimethylpyridine. Some of these were among those added as surrogates or spike standards as part ofthe Advanced Technologies and Laboratories International, Inc. preparation ofthe extract of the HEPA filter media and are indicated as such in the data tables in Section 2, Results; other compounds found were not previously known to be present. The main inorganic species detected (sulfate, sodium, and sulfur) are also consistent with species added in the preparation of the methylene chloride extract of the high-efficiency particulate air sample.

  8. Arkansas Preparing for Wind Power | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    Arkansas Preparing for Wind Power Arkansas Preparing for Wind Power April 15, 2010 - 5:25pm Addthis Joshua DeLung Renowned science fiction author Isaac Asimov once said, "No...

  9. Microsoft PowerPoint - Preparing for IAEA Data Reporting (10...

    National Nuclear Security Administration (NNSA)

    URENCO Limited Preparing for IAEA Data Reporting (10 CFR 75) 1 Carol Wormington - URENCO USA Preparing for IAEA Data Reporting (10 CFR 75) * We were YKO, an NRC Licensee 2 * YKO...

  10. Solar Ready Vets: Preparing Our Veterans to Join the Growing...

    Office of Environmental Management (EM)

    Solar Ready Vets: Preparing Our Veterans to Join the Growing Solar Workforce Solar Ready Vets: Preparing Our Veterans to Join the Growing Solar Workforce April 6, 2015 - 2:27pm...

  11. Sample sizes for confidence limits for reliability.

    SciTech Connect (OSTI)

    Darby, John L.

    2010-02-01T23:59:59.000Z

    We recently performed an evaluation of the implications of a reduced stockpile of nuclear weapons for surveillance to support estimates of reliability. We found that one technique developed at Sandia National Laboratories (SNL) under-estimates the required sample size for systems-level testing. For a large population the discrepancy is not important, but for a small population it is important. We found that another technique used by SNL provides the correct required sample size. For systems-level testing of nuclear weapons, samples are selected without replacement, and the hypergeometric probability distribution applies. Both of the SNL techniques focus on samples without defects from sampling without replacement. We generalized the second SNL technique to cases with defects in the sample. We created a computer program in Mathematica to automate the calculation of confidence for reliability. We also evaluated sampling with replacement where the binomial probability distribution applies.

  12. advanced coal preparation: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    ... 15 1.6.2 Implement advanced clean coal technologies for production of energy products ... 15 An SAIC Report Prepared...

  13. Experimental: Sample Preparation TiO2 compact (TiO2comp) anatase films (0.1

    E-Print Network [OSTI]

    state device based on the wealth of knowledge housed in the field of Dye Sensitized Solar Cells (20 min, 110 °C). Cell geometries : (1) ITO/TiO2comp/PbS/Pedot/Au (2) ITO/TiO2comp/TiO2nps and Development of Extremely Thin Absorber Solid State Solar Cells Matteo Biancardo*, Frederik Krebs The Danish

  14. Phenotypic Data Collection and Sample Preparation for Genomics of Wood Formation and Cellulosic Biomass Traits in Sunflower: Ames, IA location.

    SciTech Connect (OSTI)

    Marek, Laura F.

    2011-06-17T23:59:59.000Z

    Three fields were planted in Ames in 2010, two association mapping fields, N3 and A, and a recombinant inbred line field, N13. Phenotype data and images were transferred to UGA to support genetic and genomic analyses of woody biomass-related traits.

  15. Glass flask air sample analysis through Gas Chromatography in India: Implications for constraining CO2 surface fluxes

    E-Print Network [OSTI]

    for an air inlet (equipped with a 7µm filter), a pump and a battery placed below the ON/OFF button, a flow to the site measurements, they are prepared and evacuated. We pump and heat the flasks. During pumping the temperature is +60 dc. Flasks are pumped for 72 hours. Outlook Air sampling started at two new stations, Cape

  16. Uncertainty and sampling issues in tank characterization

    SciTech Connect (OSTI)

    Liebetrau, A.M.; Pulsipher, B.A.; Kashporenko, D.M. [and others

    1997-06-01T23:59:59.000Z

    A defensible characterization strategy must recognize that uncertainties are inherent in any measurement or estimate of interest and must employ statistical methods for quantifying and managing those uncertainties. Estimates of risk and therefore key decisions must incorporate knowledge about uncertainty. This report focuses statistical methods that should be employed to ensure confident decision making and appropriate management of uncertainty. Sampling is a major source of uncertainty that deserves special consideration in the tank characterization strategy. The question of whether sampling will ever provide the reliable information needed to resolve safety issues is explored. The issue of sample representativeness must be resolved before sample information is reliable. Representativeness is a relative term but can be defined in terms of bias and precision. Currently, precision can be quantified and managed through an effective sampling and statistical analysis program. Quantifying bias is more difficult and is not being addressed under the current sampling strategies. Bias could be bounded by (1) employing new sampling methods that can obtain samples from other areas in the tanks, (2) putting in new risers on some worst case tanks and comparing the results from existing risers with new risers, or (3) sampling tanks through risers under which no disturbance or activity has previously occurred. With some bound on bias and estimates of precision, various sampling strategies could be determined and shown to be either cost-effective or infeasible.

  17. Air sampling in the workplace. Final report

    SciTech Connect (OSTI)

    Hickey, E.E.; Stoetzel, G.A.; Strom, D.J.; Cicotte, G.R. [Pacific Northwest Lab., Richland, WA (United States); Wiblin, C.M. [Advanced Systems Technology, Inc., Atlanta, GA (United States); McGuire, S.A. [Nuclear Regulatory Commission, Washington, DC (United States). Div. of Regulatory Applications

    1993-09-01T23:59:59.000Z

    This report provides technical information on air sampling that will be useful for facilities following the recommendations in the NRC`s Regulatory Guide 8.25, Revision 1, ``Air sampling in the Workplace.`` That guide addresses air sampling to meet the requirements in NRC`s regulations on radiation protection, 10 CFR Part 20. This report describes how to determine the need for air sampling based on the amount of material in process modified by the type of material, release potential, and confinement of the material. The purposes of air sampling and how the purposes affect the types of air sampling provided are discussed. The report discusses how to locate air samplers to accurately determine the concentrations of airborne radioactive materials that workers will be exposed to. The need for and the methods of performing airflow pattern studies to improve the accuracy of air sampling results are included. The report presents and gives examples of several techniques that can be used to evaluate whether the airborne concentrations of material are representative of the air inhaled by workers. Methods to adjust derived air concentrations for particle size are described. Methods to calibrate for volume of air sampled and estimate the uncertainty in the volume of air sampled are described. Statistical tests for determining minimum detectable concentrations are presented. How to perform an annual evaluation of the adequacy of the air sampling is also discussed.

  18. RAPID SEPARATION METHOD FOR ACTINIDES IN EMERGENCY AIR FILTER SAMPLES

    SciTech Connect (OSTI)

    Maxwell, S.; Noyes, G.; Culligan, B.

    2010-02-03T23:59:59.000Z

    A new rapid method for the determination of actinides and strontium in air filter samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used in emergency response situations. The actinides and strontium in air filter method utilizes a rapid acid digestion method and a streamlined column separation process with stacked TEVA, TRU and Sr Resin cartridges. Vacuum box technology and rapid flow rates are used to reduce analytical time. Alpha emitters are prepared using cerium fluoride microprecipitation for counting by alpha spectrometry. The purified {sup 90}Sr fractions are mounted directly on planchets and counted by gas flow proportional counting. The method showed high chemical recoveries and effective removal of interferences. This new procedure was applied to emergency air filter samples received in the NRIP Emergency Response exercise administered by the National Institute for Standards and Technology (NIST) in April, 2009. The actinide and {sup 90}Sr in air filter results were reported in {approx}4 hours with excellent quality.

  19. Conductive ceramic composition and method of preparation

    DOE Patents [OSTI]

    Smith, James L. (Lemont, IL); Kucera, Eugenia H. (Downers Grove, IL)

    1991-01-01T23:59:59.000Z

    A ceramic anode composition is formed of a multivalent metal oxide or oxygenate such as an alkali metal, transition metal oxygenate. The anode is prepared as a non-stoichiometric crystalline structure by reaction and conditioning in a hydrogen gas cover containing minor proportions of carbon dioxide and water vapor. The structure exhibits a single phase and substantially enhanced electrical conductivity over that of the corresponding stoichiometric structure. Unexpectedly, such oxides and oxygenates are found to be stable in the reducing anode fuel gas of a molten carbonate fuel cell.

  20. Method for preparing high purity vanadium

    DOE Patents [OSTI]

    Schmidt, Frederick (Ames, IA); Carlson, O. Norman (Ames, IA)

    1986-09-09T23:59:59.000Z

    A method for preparing high purity vanadium having a low silicon content has been developed. Vanadium pentoxide is reduced with a stoichiometric, or slightly deficient amount of aluminum to produce a vanadium-aluminum alloy containing an excess of oxygen. Silicon is removed by electron-beam melting the alloy under oxidizing conditions to promote the formation of SiO which is volatile at elevated temperatures. Excess oxygen is removed by heating the alloy in the presence of calcium metal to form calcium oxide.

  1. Method for preparing high purity vanadium

    DOE Patents [OSTI]

    Schmidt, F.; Carlson, O.N.

    1984-05-16T23:59:59.000Z

    A method for preparing high purity vanadium having a low silicon content has been developed. Vanadium pentoxide is reduced with a stoichiometric, or slightly deficient amount of aluminum to produce a vanadium-aluminum alloy containing an excess of oxygen. Silicon is removed by electron-beam melting the alloy under oxidizing conditions to promote the formation of SiO which is volatile at elevated temperatures. Excess oxygen is removed by heating the alloy in the presence of calcium metal to form calcium oxide.

  2. Preparation of thorium-uranium gel spheres

    SciTech Connect (OSTI)

    Spence, R.D.; Haas, P.A.

    1980-01-01T23:59:59.000Z

    Ceramic oxide spheres with diameters of 15 to 1500 ..mu..m are being evaluated for fabrication of power reactor fuel rods. (Th,U)O/sub 2/ spheres can be prepared by internal or external chemical gelation of nitrate solutions or oxide sols. Two established external gelation techniques were tested but proved to be unsatisfactory for the intended application. Established internal gelation techniques for UO/sub 2/ spheres were applied with minor modifications to make 75% ThO/sub 2/-25% UO/sub 2/ spheres that sinter to diameters of 200 to 1400 ..mu..m (99% T.D.).

  3. Preparation of reactive beta-dicalcium silicate

    DOE Patents [OSTI]

    Shen, Ming-Shing (Laramie, WY, NJ); Chen, James M. (Rahway, NJ); Yang, Ralph T. (Amherst, NY)

    1982-01-01T23:59:59.000Z

    This invention relates to the preparation of fine particles of reactive beta-dicalcium silicate by means of a solid state process which comprises firing a mixture of calcium sulfate, silica and a reducing additive selected from the group consisting of calcium sulfide, carbon, carbon monoxide, methane and hydrogen, at a temperature of about 850.degree.-1000.degree. C. A carrier gas such as nitrogen or carbon dioxide may also be added, if desired. A high concentration of sulfur dioxide is a by-product of this process.

  4. Preparation of reactive beta-dicalcium silicate

    DOE Patents [OSTI]

    Shen, M.S.; Chen, J.M.; Yang, R.T.

    1980-02-28T23:59:59.000Z

    This invention relates to the preparation of fine particles of reactive beta-dicalcium silicate by means of a solid state process which comprises firing a mixture of calcium sulfate, silica, and a reducing additive selected from the group consisting of calcium sulfide, carbon, carbon monoxide, methane, and hydrogen, at a temperature of about 850 to 1000/sup 0/C. A carrier gas such as nitrogen or carbon dioxide may also be added, if desired. A high concentration of sulfur dioxide is a by-product of this process.

  5. Steps in Preparing an Extension Publication.

    E-Print Network [OSTI]

    Anonymous,

    1980-01-01T23:59:59.000Z

    for fiscal affairs. The next step is the assignment of a purchase order number by the fiscal office, after which the entire manuscript file is sent to the associate editor publications. Publications approval data are record ed in the publications office...- TDOC Z TA24S.7 B873 , nO.1296 _~J Stepsin Preparing an Extension Publication 1 A . It I University System gncu ura B-1296 ~ Texas Th~ Te~as A&M Extension Daniel C. Pfannstiel, Director '\\.... ~Arvice College Station, Texas 77843...

  6. AGAROSE GEL PREPARATION AND DNA QUANTIFICATION

    E-Print Network [OSTI]

    Gill, Kulvinder

    /µL concentration from the stock solution available 2. E.g., Promega, comes in a concentration of 450 ng/µL solution, to make a 2 ng/µL (prepare: Stock lambda (450 ng/µL) = 4.45 µL 3:1 buffer (TE:5X dye) = 995.55µL StoreL of each lambda (10, 25, 50ng) in the first 3 wells, which will serve as standards. 5. Take 1 µL of total

  7. Process for preparing silicon carbide foam

    DOE Patents [OSTI]

    Whinnery, L.L.; Nichols, M.C.; Wheeler, D.R.; Loy, D.A.

    1997-09-16T23:59:59.000Z

    A method of preparing near net shape, monolithic, porous SiC foams is disclosed. Organosilicon precursors are used to produce polymeric gels by thermally induced phase separation, wherein, a sufficiently concentrated solution of an organosilicon polymer is cooled below its solidification temperature to form a gel. Following solvent removal from the gel, the polymer foam is pretreated in an oxygen plasma in order to raise its glass transition temperature. The pretreated foam is then pyrolyzed in an inert atmosphere to form a SiC foam. 9 figs.

  8. Process for preparing silicon carbide foam

    DOE Patents [OSTI]

    Whinnery, LeRoy Louis (Livermore, CA); Nichols, Monte Carl (Livermore, CA); Wheeler, David Roger (Albuquerque, NM); Loy, Douglas Anson (Albuquerque, NM)

    1997-01-01T23:59:59.000Z

    A method of preparing near net shape, monolithic, porous SiC foams is disclosed. Organosilicon precursors are used to produce polymeric gels by thermally induced phase separation, wherein, a sufficiently concentrated solution of an organosilicon polymer is cooled below its solidification temperature to form a gel. Following solvent removal from the gel, the polymer foam is pretreated in an oxygen plasma in order to raise its glass transition temperature. The pretreated foam is then pyrolized in an inert atmosphere to form a SiC foam.

  9. Improved method for preparing rare earth sesquichalcogenides

    DOE Patents [OSTI]

    Takeshita, T.; Beaudry, B.J.; Gschneidner, K.A. Jr.

    1982-04-14T23:59:59.000Z

    An improved method for the preparation of high purity rare earth sesquichalcogenides is described. The rare earth, as one or more pieces of the metal, is sealed under a vacuum with a stoichiometric amount of sulfur or selenium and a small amount of iodine into a quartz reaction vessel. The sealed vessel is then heated to above the vaporization temperature of the chalcogen and below the melting temperature of the rare earth metal and maintained until the product has been formed. The iodine is then vaporized off leaving a pure product. The rare earth sulfides and selenides thus formed are useful as semiconductors and as thermoelectric generators. 3 tables.

  10. Conductive ceramic composition and method of preparation

    DOE Patents [OSTI]

    Smith, J.L.; Kucera, E.H.

    1991-04-16T23:59:59.000Z

    A ceramic anode composition is formed of a multivalent metal oxide or oxygenate such as an alkali metal, transition metal oxygenate. The anode is prepared as a non-stoichiometric crystalline structure by reaction and conditioning in a hydrogen gas cover containing minor proportions of carbon dioxide and water vapor. The structure exhibits a single phase and substantially enhanced electrical conductivity over that of the corresponding stoichiometric structure. Unexpectedly, such oxides and oxygenates are found to be stable in the reducing anode fuel gas of a molten carbonate fuel cell. 4 figures.

  11. Method to prepare nanoparticles on porous mediums

    DOE Patents [OSTI]

    Vieth, Gabriel M. (Knoxville, TN) [Knoxville, TN; Dudney, Nancy J. (Oak Ridge, TN) [Oak Ridge, TN; Dai, Sheng (Knoxville, TN) [Knoxville, TN

    2010-08-10T23:59:59.000Z

    A method to prepare porous medium decorated with nanoparticles involves contacting a suspension of nanoparticles in an ionic liquid with a porous medium such that the particles diffuse into the pores of the medium followed by heating the resulting composition to a temperature equal to or greater than the thermal decomposition temperature of the ionic liquid resulting in the removal of the liquid portion of the suspension. The nanoparticles can be a metal, an alloy, or a metal compound. The resulting compositions can be used as catalysts, sensors, or separators.

  12. Preparing for Hurricane Season | Department of Energy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative1 First Use of Energy for All Purposes (Fuel and Nonfuel), 2002; Level:Energy: Grid Integration Redefining What's Possible forPortsmouth/Paducah ProjectPRE-AWARD ACCOUNTINGQuantitative hiRXand ThePreparing for

  13. Comparison of different pressing techniques for the preparation of n-type silicon-germanium thermoelectric alloys

    SciTech Connect (OSTI)

    Harringa, J.L.; Cook, B.A.

    1996-06-01T23:59:59.000Z

    Improvements to state-of-the-art Si{sub 80}Ge{sub 20} thermoelectric alloys have been observed in laboratory-scale samples by the powder metallurgy techniques of mechanical alloying and hot pressing. Incorporating these improvements in large scale compacts for the production of thermoelectric generator elements is the next step in achieving higher efficiency RTGs. This paper discusses consolidation of large quantities of mechanically alloyed powders into production size compacts. Differences in thermoelectric properties are noted between the compacts prepared by the standard technique of hot uniaxial pressing and hot isostatic pressing. Most significant is the difference in carrier concentration between the alloys prepared by the two consolidation techniques.

  14. LCLS Proposal Preparation and Review Process Guidelines 10/8/11 LCLS Proposal Preparation and Review Process Guidelines

    E-Print Network [OSTI]

    Wechsler, Risa H.

    LCLS Proposal Preparation and Review Process Guidelines ­ 10/8/11 LCLS Proposal Preparation and Review Process Guidelines Proposal Preparation The technical capabilities of the LCLS are developing rapidly. LCLS operations will continue to evolve over the next few years, and we appreciate

  15. 100 Area Columbia River sediment sampling

    SciTech Connect (OSTI)

    Weiss, S.G. [Westinghouse Hanford Co., Richland, WA (United States)

    1993-09-08T23:59:59.000Z

    Forty-four sediment samples were collected from 28 locations in the Hanford Reach of the Columbia River to assess the presence of metals and man-made radionuclides in the near shore and shoreline settings of the Hanford Site. Three locations were sampled upriver of the Hanford Site plutonium production reactors. Twenty-two locations were sampled near the reactors. Three locations were sampled downstream of the reactors near the Hanford Townsite. Sediment was collected from depths of 0 to 6 in. and between 12 to 24 in. below the surface. Samples containing concentrations of metals exceeding the 95 % upper threshold limit values (DOE-RL 1993b) are considered contaminated. Contamination by arsenic, chromium, copper, lead, and zinc was found. Man-made radionuclides occur in all samples except four collected opposite the Hanford Townsite. Man-made radionuclide concentrations were generally less than 1 pCi/g.

  16. Argonne Premium Coal Sample Bank The Argonne Premium Coal (APC) Sample Bank can supply

    E-Print Network [OSTI]

    Maranas, Costas

    Argonne Premium Coal Sample Bank Background Overview T The Argonne Premium Coal (APC) Sample Bank can supply researchers with highly uniform, well-protected coal samples unexposed to oxygen. Researchers investigating coal structure, properties, and behavior can benefit greatly from these samples

  17. Proper Oil Sampling Intervals and Sample Collection Techniques Gasoline/Diesel/Natural Gas Engines

    E-Print Network [OSTI]

    Proper Oil Sampling Intervals and Sample Collection Techniques Gasoline/Diesel/Natural Gas Engines: · Oil samples can be collected during oil changes. Follow manufacturers recommendations on frequency (hours, mileage, etc) of oil changes. · Capture a sample from the draining oil while the oil is still hot

  18. APPROPRIATE ZOOPLANKTON SAMPLING METHODOLOGY FOR OTEC SITES

    E-Print Network [OSTI]

    Commins, M.L.

    2014-01-01T23:59:59.000Z

    Thermal Energy Conversion (OTEC) sites. Participants J.Zooplankton Sampling for OTEC Sites t~thodology Edited bywho gave an overview of the OTEC program, and the policies

  19. Workplace Charging Challenge: Sample Workplace Charging Policy...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    guidelines used by one Workplace Charging Challenge partner to keep their program running safe and successfully. Sample Workplace Charging Policy More Documents & Publications...

  20. Colling Wipe Samples for VX Analysis

    SciTech Connect (OSTI)

    Koester, C; Hoppes, W G

    2010-02-11T23:59:59.000Z

    This standard operating procedure (SOP) provides uniform procedures for the collection of wipe samples of VX residues from surfaces. Personnel may use this procedure to collect and handle wipe samples in the field. Various surfaces, including building materials (wood, metal, tile, vinyl, etc.) and equipment, may be sampled based on this procedure. The purpose of such sampling is to determine whether or not the relevant surfaces are contaminated, to determine the extent of their contamination, to evaluate the effectiveness of decontamination procedures, and to determine the amount of contaminant that might present as a contact hazard.

  1. Guide to preparing SAND reports and other communication products.

    SciTech Connect (OSTI)

    Not Available

    2011-09-01T23:59:59.000Z

    This guide describes the R&A process, Common Look and Feel requirements, and preparation and publishing procedures for communication products at Sandia National Laboratories. Samples of forms and examples of published communications products are provided. This guide takes advantage of the wealth of material now available on the Web as a resource. Therefore, it is best viewed as an electronic document. If some of the illustrations are too small to view comfortably, you can enlarge them on the screen as needed. The format of this document is considerably different than that usually expected of a SAND Report. It was selected to permit the large number of illustrations and examples to be placed closer to the text that references them. In the case of forms, covers, and other items that are included as examples, a link to the Web is provided so that you can access the items and download them for use. This guide details the processes for producing a variety of communication products at Sandia National Laboratories. Figure I-1 shows the general publication development process. Because extensive supplemental material is available from Sandia on the internal web or from external sources (Table I-1), the guide has been shortened to make it easy to find information that you need.

  2. Preparation and properties of polyvinyl alcohol microspheres

    SciTech Connect (OSTI)

    Campbell, J.H.; Grens, J.Z.; Poco, J.F.; Ives, B.H.

    1986-06-01T23:59:59.000Z

    Polyvinyl alcohol (PVA) microspheres, having a size range of approx.150- to 250-..mu..m diameter with 1- to 5-..mu..m wall thickness, have been fabricated using a solution droplet technique. The spheres were developed for possible use on the Lawrence Livermore National Laboratory (LLNL) Inertial Confinement Fusion (ICF) Program. PVA, a polymer chosen based on earlier survey work carried out at KMS Fusion, Inc., has good strength, low hydrogen permeability, is optically transparent, and water soluble. The latter property makes it safe and easy to use in our droplet generator system. A unique dual-orifice droplet generator was used to prepare the spheres. The droplet generator operating conditions and the column processing parameters were chosen using results from our 1-D model calculations as a guide. The polymer microsphere model is an extension of the model we developed to support the glass sphere production. After preparation, the spheres were physically characterized for surface quality, sphericity, wall thickness (and uniformity), and size. We also determined the buckling pressure for both uncoated and CH-coated spheres. Radiation stability to beta decay (from tritium) was evaluated by exposing the spheres to a 7-keV electron beam. The results from these and other physical property measurements are presented in this report.

  3. Novel hard compositions and methods of preparation

    DOE Patents [OSTI]

    Sheinberg, Haskell (Los Alamos, NM)

    1983-08-23T23:59:59.000Z

    Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value. Photomicrographs show that the shapes of the grains of the alloy mixture with which the minor amount of carbide (or carbide-formers) is mixed are radically altered from large, rounded to small, very angular by the addition of the carbide. Superiority of one of these hard compositions of matter over cobalt-bonded tungsten carbide for ultra-high pressure anvil applications was demonstrated.

  4. Preparation of certain m-aminophenols and the use thereof for preparation of laser dyes

    DOE Patents [OSTI]

    Hammond, P.R.

    1983-12-29T23:59:59.000Z

    Methods are provided for making certain m-aminophenols using a sulfonation/alkali fusion procedure. The aminophenols are key intermediates in the synthesis of dyes, particularly efficient, stable dyes for laser application. Preparations of some rhodamine and phenoxazone dyes from the m-aminophenols are described.

  5. Ambient pressure process for preparing aerogel thin films reliquified sols useful in preparing aerogel thin films

    DOE Patents [OSTI]

    Brinker, Charles Jeffrey (Albuquerque, NM); Prakash, Sai Sivasankaran (Minneapolis, MN)

    1999-01-01T23:59:59.000Z

    A method for preparing aerogel thin films by an ambient-pressure, continuous process. The method of this invention obviates the use of an autoclave and is amenable to the formation of thin films by operations such as dip coating. The method is less energy intensive and less dangerous than conventional supercritical aerogel processing techniques.

  6. Evaporator Feed Qualification Analysis Of Tank 38H And 43H Samples: January 2010 Through April 2013

    SciTech Connect (OSTI)

    Martino, C. J.; Coleman, C. J.

    2013-08-21T23:59:59.000Z

    This report provides the results of analyses that focused on the chemical species that pertain to the sodium aluminosilicate formation potential for archived Tank 38H and 43H subsurface samples from January 2010 through April 2013. Analyses included warm acid strike preparation followed by analysis of silicon, aluminum, and sodium and water dilution preparation followed by analysis for anions. The Tank 43H and 38H supernatant liquid silicon measurements for the January 2010 through April 2013 time period exhibit a slight increasing trend. Over this time period, the silicon concentration in the Tank 43H and Tank 38H samples averaged 179 mg/L and 235 mg/L, respectively. Comparison of Tank 43H sample results from 2005 through April 2013 to the previously developed process control models indicates that the current formation of sodium aluminosilicate in the 2H system is due to the seeded direct precipitation of cancrinite and sodalite.

  7. SAMPLE: software for VAX FORTRAN execution timing

    SciTech Connect (OSTI)

    Lowe, L.H.

    1983-01-01T23:59:59.000Z

    SAMPLE is a set of subroutines in use at the Los Alamos National Laboratory for collecting CPU timings of various FORTRAN program sections - usually individual subroutines. These measurements have been useful in making programs run faster. The presentation includes a description of the software and examples of its use. The software is available on the directory (SAMPLE) of the VAX SIG tape.

  8. EML Surface Air Sampling Program, 1989 data

    SciTech Connect (OSTI)

    Larsen, R.J.; Sanderson, C.G.

    1991-08-01T23:59:59.000Z

    Measurements of the concentrations of specific atmospheric radionuclides in air filter samples collected for the Environmental Measurements Laboratory`s Surface Air Sampling Program (SASP) during 1989 indicate that anthropogenic radionuclides, in both hemispheres, were at or below the lower limits of detection for the analytical and sampling techniques that were used to measure them. During 1989, the occasional detection of {sup 137}Cs in some air filter samples may have resulted from resuspension of previously deposited debris. The naturally occurring radioisotopes that we measure, {sup 7}Be and {sup 210}Pb, continue to be detected in most air filter samples. The 1989 annual mean concentrations of {sup 7}Be at many of the sites were lower than those previously reported during the last decade. Possible changes in the atmospheric production of {sup 7}Be, variations in atmospheric circulation and precipitation patterns, as well as modifications to our sampling procedure many all have contributed to this observed trend. Short-term variations in the concentrations of {sup 7}Be and {sup 210}Pb continued to be observed at many sites at which weekly air filter samples were analyzed. These short-term fluctuations probably resulted from variations in meteorological factors. The data from our quality control samples indicate that the reliability of the air filter measurements are acceptable for their intended application.

  9. EML Surface Air Sampling Program, 1989 data

    SciTech Connect (OSTI)

    Larsen, R.J.; Sanderson, C.G.

    1991-08-01T23:59:59.000Z

    Measurements of the concentrations of specific atmospheric radionuclides in air filter samples collected for the Environmental Measurements Laboratory's Surface Air Sampling Program (SASP) during 1989 indicate that anthropogenic radionuclides, in both hemispheres, were at or below the lower limits of detection for the analytical and sampling techniques that were used to measure them. During 1989, the occasional detection of {sup 137}Cs in some air filter samples may have resulted from resuspension of previously deposited debris. The naturally occurring radioisotopes that we measure, {sup 7}Be and {sup 210}Pb, continue to be detected in most air filter samples. The 1989 annual mean concentrations of {sup 7}Be at many of the sites were lower than those previously reported during the last decade. Possible changes in the atmospheric production of {sup 7}Be, variations in atmospheric circulation and precipitation patterns, as well as modifications to our sampling procedure many all have contributed to this observed trend. Short-term variations in the concentrations of {sup 7}Be and {sup 210}Pb continued to be observed at many sites at which weekly air filter samples were analyzed. These short-term fluctuations probably resulted from variations in meteorological factors. The data from our quality control samples indicate that the reliability of the air filter measurements are acceptable for their intended application.

  10. Disc valve for sampling erosive process streams

    DOE Patents [OSTI]

    Mrochek, J.E.; Dinsmore, S.R.; Chandler, E.W.

    1984-08-16T23:59:59.000Z

    This is a patent for a disc-type, four-port sampling valve for service with erosive high temperature process streams. Inserts and liners of ..cap alpha..-silicon carbide respectively, in the faceplates and in the sampling cavities, limit erosion while providing lubricity for a smooth and precise operation. 1 fig.

  11. Atmospheric sampling glow discharge ionization source

    DOE Patents [OSTI]

    McLuckey, S.A.; Glish, G.L.

    1989-07-18T23:59:59.000Z

    An atmospheric sampling glow discharge ionization source that can be used in combination with an analytical instrument which operates at high vacuum, such as a mass spectrometer. The atmospheric sampling glow discharge ionization source comprises a chamber with at least one pair of electrodes disposed therein, an inlet for a gaseous sample to be analyzed and an outlet communicating with an analyzer which operates at subatmospheric pressure. The ionization chamber is maintained at a pressure below atmospheric pressure, and a voltage difference is applied across the electrodes to induce a glow discharge between the electrodes, so that molecules passing through the inlet are ionized by the glow discharge and directed into the analyzer. The ionization source accepts the sample under atmospheric pressure conditions and processes it directly into the high vacuum instrument, bridging the pressure gap and drawing off unwanted atmospheric gases. The invention also includes a method for analyzing a gaseous sample using the glow discharge ionization source described above. 3 figs.

  12. Recovery of coal from preparation plant effluents using a packed column

    SciTech Connect (OSTI)

    Choudhry, V.; Khan, L.; Yang, D.; Banerjee, D.D.

    1993-12-31T23:59:59.000Z

    The feasibility of recovering coal from coal preparation plant waste (or effluent) streams at the pilot scale using the packed column flotation process is demonstrated. In Phase I of the project, a total of four effluent samples were tested at the bench scale with the objective of recovering low-ash, low-sulfur clean coal products that were, at a minimum, compatible with the quality of the clean coal produced by the preparation plants supplying the waste stream samples. Phase II of the project comprised demonstration of the technology at the pilot scale using a 4-in. I.D. {times} 20-ft tall column installed at the Applied Laboratory of the Illinois State Geological Survey. A large effluent sample was conducted, consisting of particle size distribution, proximate and complete analyses, and batch froth flotation testing. Ash, total and pyritic sulfur, and calorific value of the effluent sample were also determined. The effluent feed sample contained 50-55% ash and 2.2% total sulfur. Confirmatory tests were conducted at Michigan Technological University using a bench-scale packed column. A product containing 5.4% ash was obtained at 97.5% ash rejection and 71.8% combustible matter recovery. Changing the process operating parameters allowed the quality of the product to be controlled such that its ash content ranged between 6 and 10%, with combustible matter recoveries in the 71-77% range. Pilot testing was conducted using a test matrix designed to study the effects of primary variables (feed rate, percent solids, and reagent dosage) and operating variables (air rate, wash water, and pulp level) with the objective of optimizing the process performance. Feed rates of 20-108 lb/hour were tested, with very good performance being obtained at a feed rate of 32 lb/hour (374 lb/h/ft{sup 2}).

  13. Making coal burnable: preparation and use

    SciTech Connect (OSTI)

    Rittenhouse, R.C.

    1985-06-01T23:59:59.000Z

    This paper offers several different views on the tools available to boost the burnability of coal. One view of making coal burnable and for better emissions control lies in the combustion process. One approach is fluidized bed combustion and the two choices within this technology are atmospheric (AFBC) and pressurized (PFBC). Several tests are being conducted to develop the slagging combustor technology for direct conversion from oil to coal. Some advantages listed for this method are a simple retrofit, low particulate, NO/sub x/ and SO/sub 2/ emissions, no modification for burning pulverized coal or coal/water slurry, no ash and no moving parts. Another method discussed is coal blending. The industrial and utility coal burning demand, combined with vacillating regulatory situations, reveals a need for coal users to be ever more alert to fuel price and availability. Technologies in the three areas of application -- coal preparation/cleaning, combustion, and emissions control -- offer an endless array of combinations.

  14. Remotely prepared entanglement: a quantum web page

    E-Print Network [OSTI]

    Todd A. Brun

    2001-07-05T23:59:59.000Z

    In quantum teleportation, an unknown quantum state is transmitted from one party to another using only local operations and classical communication, at the cost of shared entanglement. Is it possible similarly, using an $N$ party entangled state, to have the state retrievable by {\\it any} of the $N-1$ possible receivers? If the receivers cooperate, and share a suitable state, this can be done reliably. The $N$ party GHZ is one such state; I derive a large class of such states, and show that they are in general not equivalent to the GHZ. I also briefly discuss the problem where the parties do not cooperate, and the relationship to multipartite entanglement quantification. I define a new set of entanglement monotones, the entanglements of preparation.

  15. Method of preparing composite superconducting wire

    DOE Patents [OSTI]

    Verhoeven, John D. (Ames, IA); Gibson, Edwin D. (Ames, IA); Finnemore, Douglas K. (Ames, IA); Ostenson, Jerome E. (Ames, IA); Schmidt, Frederick A. (Ames, IA); Owen, Charles V. (Ames, IA)

    1985-08-06T23:59:59.000Z

    An improved method of preparing composite multifilament superconducting wire of Nb.sub.3 Sn in a copper matrix which eliminates the necessity of coating the drawn wire with tin. A generalized cylindrical billet of an alloy of copper containing at least 15 weight percent niobium, present in the copper as discrete, randomly distributed and oriented dendritic-shaped particles, is provided with at least one longitudinal opening which is filled with tin to form a composite drawing rod. The drawing rod is then drawn to form a ductile composite multifilament wire containing a filament of tin. The ductile wire containing the tin can then be wound into magnet coils or other devices before heating to diffuse the tin through the wire to react with the niobium forming Nb.sub.3 Sn. Also described is an improved method for making large billets of the copper-niobium alloy by consumable-arc casting.

  16. Expediting Groundwater Sampling at Hanford and Making It Safer - 13158

    SciTech Connect (OSTI)

    Connell, Carl W. Jr.; Conley, S.F.; Carr, Jennifer S.; Schatz, Aaron L. [CH2M HILL Plateau Remediation Company, P.O. Box 1600, Richland, WA 99352 (United States)] [CH2M HILL Plateau Remediation Company, P.O. Box 1600, Richland, WA 99352 (United States); Brown, W.L. [Lockheed Martin Systems Information, P.O. Box 950, Richland, WA 99352 (United States)] [Lockheed Martin Systems Information, P.O. Box 950, Richland, WA 99352 (United States); Hildebrand, R. Douglas [Department of Energy - Richland Operations Office, 825 Jadwin Ave., Richland, WA 99352 (United States)] [Department of Energy - Richland Operations Office, 825 Jadwin Ave., Richland, WA 99352 (United States)

    2013-07-01T23:59:59.000Z

    The CH2M HILL Plateau Remediation Company (CHPRC) manages the groundwater monitoring programs at the Department of Energy's 586-square-mile Hanford site in southeastern Washington state. These programs are regulated by the Resource Conservation and Recovery Act (RCRA), the Comprehensive Environmental Response Compensation and Liability Act (CERCLA), and the Atomic Energy Act (AEA). The purpose of monitoring is to track existing groundwater contamination from past practices, as well as other potential contamination that might originate from RCRA treatment, storage, and disposal (TSD) facilities. An integral part of the groundwater-monitoring program involves taking samples of the groundwater and measuring the water levels in wells scattered across the site. Each year, more than 1,500 wells are accessed for a variety of reasons. Historically, the monitoring activities have been very 'people intensive'. Field personnel or 'samplers' have been issued pre-printed forms showing information about the well(s) for a particular sampling evolution. This information is taken from two official electronic databases: the Hanford Well Information System (HWIS) and the Hanford Environmental Information System (HEIS). The samplers traditionally used these hardcopy forms to document the groundwater samples and well water-levels. After recording the entries in the field, the samplers turned the forms in at the end of the day and other personnel posted the collected information. In Automating Groundwater Sampling at Hanford (HNF-38542-FP Revision 0, Presented at Waste Management 2009 Conference, March 1 - March 5, 2009, Phoenix, AZ), we described the methods, tools, and techniques that would be used in automating the activities associated with measuring water levels. The Field Logging and Electronic Data Gathering (FLEDG) application/database that automates collecting the water-level measurement data has now been implemented at Hanford. In addition to eliminating the need to print out documents, the system saves three-to-four man days each month for the field personnel taking the measurements and the scientists and administrators managing the data and the documentation. After the information has received technical review, FLEDG automatically updates the database for water-level measurements and loads the document management system with the completed sampling report. Due to safety considerations, access to wells is conditional. A spreadsheet with appropriate data not only lists the wells that are cleared for work, but also the safety personnel who must be present before work can start. This spreadsheet is used in planning daily activities. Daily plans are structured to ensure that the wells to be sampled are cleared for work and the appropriate safety personnel have been assigned and are present before the work starts. Historically, the spreadsheets have been prepared manually, and as a result, are potentially subject to human error. However, a companion database application has been developed to work with FLEDG - making the entire sampling process more efficient and safer for personnel. The Well Access List - Electronic, WAL-E, is a database that contains much the same information that was previously manually loaded into the spread sheet. In addition, WAL-E contains a managed work-flow application that shows the access requirements and allows for appropriate reviews of the compiled well. Various CHPRC organizations, including Industrial Hygiene, RADCON, and Well Maintenance and Sample Administration are able to enter and review the wells added or deleted from the WAL-E database. The FLEDG system then accesses this database information to identify appropriate support personnel and provide safety requirements to field personnel. In addition, WAL-E offers the assurance that wells have appropriate locks and are correctly labeled and electrically grounded as required, before well activities begin. This feature is an extremely important aspect of the FLEDG/WAL-E system because it adds another safety check to the work evolution and reduces the pote

  17. Automated collection and processing of environmental samples

    DOE Patents [OSTI]

    Troyer, Gary L. (Richland, WA); McNeece, Susan G. (Richland, WA); Brayton, Darryl D. (Richland, WA); Panesar, Amardip K. (Kennewick, WA)

    1997-01-01T23:59:59.000Z

    For monitoring an environmental parameter such as the level of nuclear radiation, at distributed sites, bar coded sample collectors are deployed and their codes are read using a portable data entry unit that also records the time of deployment. The time and collector identity are cross referenced in memory in the portable unit. Similarly, when later recovering the collector for testing, the code is again read and the time of collection is stored as indexed to the sample collector, or to a further bar code, for example as provided on a container for the sample. The identity of the operator can also be encoded and stored. After deploying and/or recovering the sample collectors, the data is transmitted to a base processor. The samples are tested, preferably using a test unit coupled to the base processor, and again the time is recorded. The base processor computes the level of radiation at the site during exposure of the sample collector, using the detected radiation level of the sample, the delay between recovery and testing, the duration of exposure and the half life of the isotopes collected. In one embodiment, an identity code and a site code are optically read by an image grabber coupled to the portable data entry unit.

  18. Reference samples for water-related programs in the US Environmental Protection Agency

    SciTech Connect (OSTI)

    Winter, J.A.

    1985-06-01T23:59:59.000Z

    The Environmental Monitoring and Support Laboratory at Cincinnati provides quality assurance (QA) support for US Environmental Protection Agency (EPA) water-related programs. Two important segments of this support are the Quality Control Sample Program, which furnishes samples of known concentrations for use as independent checks on intralaboratory QA activities, and the EPA's Repository for Toxic and Hazardous Materials, which provides calibration standards and spiking solutions for trace organic analyses of interest to the Agency. Each series contains one or more analytes, with true or reference values. The samples and standards are prepared as stable concentrated solutions in all-glass ampuls for dilution to volume, and analyses by EPA, its contractors and grantees, and other federal, state, and local agencies. 1 reference, 6 tables.

  19. Guide to preparing SAND reports and other communication products : version 2.0.

    SciTech Connect (OSTI)

    Johnson, Debra M.; Brittenham, Phillip W.

    2005-12-01T23:59:59.000Z

    This guide describes the R&A process, Common Look and Feel requirements, and preparation and publishing procedures for communication products at Sandia National Laboratories. Samples of forms and examples of published communications products are provided. This guide details the processes for producing a variety of communication products at Sandia National Laboratories. Figure I-1 shows the general publication development process. Because extensive supplemental material is available from Sandia on the internal Web or from external sources (Table I-1), the guide has been shortened to make it easy to find information that you need.

  20. A comparison of the nutrition of home-prepared and commercial diets for dogs 

    E-Print Network [OSTI]

    Streiff, Erin Leigh

    2001-01-01T23:59:59.000Z

    fulfillment of the requirements for the degree of MASTER OF SCIENCE Approved as to style and content by: John E. Bauer (Co-Chair of Committee) Q. Rosema alzem 1 (Me r) Stephen B. Smith (Co-Chair of Committee) John E. Bauer (Chair of Nutrition...-Chairs of Advisory Committee: Dr. John E. Bauer Dr. Stephen B. Smith The objective of this study was to compare the nutrition of home-prepared and commercial diets in dogs. In order to do this, weighed food records, laboratory analysis of food samples, and serum...

  1. Hanford Waste Vitrification Plant full-scale feed preparation testing with water and process simulant slurries

    SciTech Connect (OSTI)

    Gaskill, J.R.; Larson, D.E.; Abrigo, G.P. [and others] [and others

    1996-03-01T23:59:59.000Z

    The Hanford Waste Vitrification Plant was intended to convert selected, pretreated defense high-level waste and transuranic waste from the Hanford Site into a borosilicate glass. A full-scale testing program was conducted with nonradioactive waste simulants to develop information for process and equipment design of the feed-preparation system. The equipment systems tested included the Slurry Receipt and Adjustment Tank, Slurry Mix Evaporator, and Melter-Feed Tank. The areas of data generation included heat transfer (boiling, heating, and cooling), slurry mixing, slurry pumping and transport, slurry sampling, and process chemistry. 13 refs., 129 figs., 68 tabs.

  2. Copper- and silver-zirconia aerogels: Preparation, structural properties and catalytic behavior in methanol synthesis from carbon dioxide

    SciTech Connect (OSTI)

    Koeppel, R.A.; Stoecker, C.; Baiker, A. [Swiss Federal Inst. of Technology, Zuerich (Switzerland). Lab. of Technical Chemistry] [Swiss Federal Inst. of Technology, Zuerich (Switzerland). Lab. of Technical Chemistry

    1998-10-25T23:59:59.000Z

    Copper- and silver-zirconia aerogels containing 10 at% IB metal were prepared from tetra-n-butoxy zirconium(IV) and IB metal acetates using the solution sol-gel method and ensuring high-temperature (HT) and low-temperature (LT) supercritical drying, respectively. The influence of preparation parameters and calcination on the structural and catalytic properties of the aerogels for the synthesis of methanol from carbon dioxide and hydrogen was investigated. After calcination in air at 573 K, the catalysts had BET surface areas in the range of 100--143 m{sup 2}/g (Cu/ZrO{sub 2}) and 77--125 m{sup 2}/g (Ag/ZrO{sub 2}), respectively. Due to the reductive alcoholic atmosphere during high-temperature supercritical drying, metallic copper and silver existed in all raw HT-aerogels. The mean size of the copper crystallites wa/s 30 nm. The silver crystallite size for the HT-aerogel prepared with nitric acid was 10 nm, whereas for samples prepared with acetic acid it was 5--7 nm. Calcination in air at 573 K led to the formation of highly dispersed amorphous copper oxide and silver. Comparing the catalytic behavior of the calcined copper-zirconia aerogels with corresponding xerogels prepared by coprecipitation revealed highest activity for the LT-aerogel, whereas the HT-aerogels were least active. In contrast, similar catalytic behavior was observed for the differently dried silver-zirconia samples. Generally, CO{sub 2}-conversion of the copper-zirconia samples. Generally, CO{sub 2}-conversion of the copper-zirconia aerogels was markedly higher than that of the corresponding silver-zirconia aerogels, whereas methanol selectivity was similar.

  3. Spectroscopic diagnostics for bacteria in biologic sample

    DOE Patents [OSTI]

    El-Sayed, Mostafa A. (Atlanta, GA); El-Sayed, Ivan H. (Somerville, MA)

    2002-01-01T23:59:59.000Z

    A method to analyze and diagnose specific bacteria in a biologic sample using spectroscopy is disclosed. The method includes obtaining the spectra of a biologic sample of a non-infected patient for use as a reference, subtracting the reference from the spectra of an infected sample, and comparing the fingerprint regions of the resulting differential spectrum with reference spectra of bacteria in saline. Using this diagnostic technique, specific bacteria can be identified sooner and without culturing, bacteria-specific antibiotics can be prescribed sooner, resulting in decreased likelihood of antibiotic resistance and an overall reduction of medical costs.

  4. Visual Sample Plan (VSP) - FIELDS Integration

    SciTech Connect (OSTI)

    Pulsipher, Brent A.; Wilson, John E.; Gilbert, Richard O.; Hassig, Nancy L.; Carlson, Deborah K.; Bing-Canar, John; Cooper, Brian; Roth, Chuck

    2003-04-19T23:59:59.000Z

    Two software packages, VSP 2.1 and FIELDS 3.5, are being used by environmental scientists to plan the number and type of samples required to meet project objectives, display those samples on maps, query a database of past sample results, produce spatial models of the data, and analyze the data in order to arrive at defensible decisions. VSP 2.0 is an interactive tool to calculate optimal sample size and optimal sample location based on user goals, risk tolerance, and variability in the environment and in lab methods. FIELDS 3.0 is a set of tools to explore the sample results in a variety of ways to make defensible decisions with quantified levels of risk and uncertainty. However, FIELDS 3.0 has a small sample design module. VSP 2.0, on the other hand, has over 20 sampling goals, allowing the user to input site-specific assumptions such as non-normality of sample results, separate variability between field and laboratory measurements, make two-sample comparisons, perform confidence interval estimation, use sequential search sampling methods, and much more. Over 1,000 copies of VSP are in use today. FIELDS is used in nine of the ten U.S. EPA regions, by state regulatory agencies, and most recently by several international countries. Both software packages have been peer-reviewed, enjoy broad usage, and have been accepted by regulatory agencies as well as site project managers as key tools to help collect data and make environmental cleanup decisions. Recently, the two software packages were integrated, allowing the user to take advantage of the many design options of VSP, and the analysis and modeling options of FIELDS. The transition between the two is simple for the user – VSP can be called from within FIELDS, automatically passing a map to VSP and automatically retrieving sample locations and design information when the user returns to FIELDS. This paper will describe the integration, give a demonstration of the integrated package, and give users download instructions and software requirements for running the integrated package.

  5. Gas sampling system for a mass spectrometer

    DOE Patents [OSTI]

    2003-12-30T23:59:59.000Z

    The present invention relates generally to a gas sampling system, and specifically to a gas sampling system for transporting a hazardous process gas to a remotely located mass spectrometer. The gas sampling system includes a capillary tube having a predetermined capillary length and capillary diameter in communication with the supply of process gas and the mass spectrometer, a flexible tube surrounding and coaxial with the capillary tube intermediate the supply of process gas and the mass spectrometer, a heat transfer tube surrounding and coaxial with the capillary tube, and a heating device in communication the heat transfer tube for substantially preventing condensation of the process gas within the capillary tube.

  6. Disc valve for sampling erosive process streams

    DOE Patents [OSTI]

    Mrochek, J.E.; Dinsmore, S.R.; Chandler, E.W.

    1986-01-07T23:59:59.000Z

    A four-port disc valve is described for sampling erosive, high temperature process streams. A rotatable disc defining opposed first and second sampling cavities rotates between fired faceplates defining flow passageways positioned to be alternatively in axial alignment with the first and second cavities. Silicon carbide inserts and liners composed of [alpha] silicon carbide are provided in the faceplates and in the sampling cavities to limit erosion while providing lubricity for a smooth and precise operation when used under harsh process conditions. 1 fig.

  7. Vapor port and groundwater sampling well

    DOE Patents [OSTI]

    Hubbell, J.M.; Wylie, A.H.

    1996-01-09T23:59:59.000Z

    A method and apparatus have been developed for combining groundwater monitoring wells with unsaturated-zone vapor sampling ports. The apparatus allows concurrent monitoring of both the unsaturated and the saturated zone from the same well at contaminated areas. The innovative well design allows for concurrent sampling of groundwater and volatile organic compounds (VOCs) in the vadose (unsaturated) zone from a single well, saving considerable time and money. The sample tubes are banded to the outer well casing during installation of the well casing. 10 figs.

  8. Vapor port and groundwater sampling well

    DOE Patents [OSTI]

    Hubbell, Joel M. (Idaho Falls, ID); Wylie, Allan H. (Idaho Falls, ID)

    1996-01-01T23:59:59.000Z

    A method and apparatus has been developed for combining groundwater monitoring wells with unsaturated-zone vapor sampling ports. The apparatus allows concurrent monitoring of both the unsaturated and the saturated zone from the same well at contaminated areas. The innovative well design allows for concurrent sampling of groundwater and volatile organic compounds (VOCs) in the vadose (unsaturated) zone from a single well, saving considerable time and money. The sample tubes are banded to the outer well casing during installation of the well casing.

  9. Structural and spectroscopic analyses of europium doped yttrium oxyfluoride powders prepared by combustion synthesis

    SciTech Connect (OSTI)

    Rakov, Nikifor [PG-Ciência dos Materiais, Universidade Federal do Vale do São Francisco, 48902-300 Juazeiro, BA (Brazil)] [PG-Ciência dos Materiais, Universidade Federal do Vale do São Francisco, 48902-300 Juazeiro, BA (Brazil); Guimarães, R. B.; Maciel, Glauco S. [Instituto de Física, Universidade Federal Fluminense, 24210-346 Niterói, RJ (Brazil)] [Instituto de Física, Universidade Federal Fluminense, 24210-346 Niterói, RJ (Brazil); Lozano B, W. [Departamento de Física, Universidade Federal de Pernambuco, 50670-901 Recife, PE (Brazil)] [Departamento de Física, Universidade Federal de Pernambuco, 50670-901 Recife, PE (Brazil)

    2013-07-28T23:59:59.000Z

    A facile widely spread technique employed to produce low-cost high-yield oxide powders, combustion synthesis, was used to prepare yttrium oxyfluoride crystalline ceramic powders. The structure of the powders was analyzed by X-ray powder diffraction and Rietveld refinement. Samples heat treated at 700 °C had a predominance of vernier orthorhombic Y{sub 6}O{sub 5}F{sub 8} phase, while samples heat treated at 800 °C crystallized in stoichiometric rhombohedral YOF phase. The samples were doped with luminescent europium trivalent ions (Eu{sup 3+}) in different concentrations (1–15 wt.%) and Judd-Ofelt theory was used to probe the distortion from the inversion symmetry of the local crystal field and the degree of covalency between the rare-earth ion and the surrounding ligands. The luminescence lifetime was measured and the luminescence quantum efficiency (LQE) was estimated. We observed that Eu{sup 3+}:Y{sub 6}O{sub 5}F{sub 8} samples presented higher LQE in spite of the larger local crystal field anisotropy found for Eu{sup 3+}:YOF samples.

  10. Guide to preparing SAND reports. Revised

    SciTech Connect (OSTI)

    Locke, T.K. [ed.

    1996-04-01T23:59:59.000Z

    This guide contains basic information needed to produce a SAND report. Its guidelines reflect DOE regulation and Sandia policy. The guide includes basic writing instructions in an annotated sample report; guidance for organization, format, and layout of reports produced by line organizations; and information about conference papers, journal articles, and brochures. The appendixes contain sections on Sandia`s preferred usage, equations, references, copyrights and permissions, and publishing terms.

  11. Surface electronic structure for various surface preparations of Nb-doped SrTiO{sub 3} (001)

    SciTech Connect (OSTI)

    Hatch, Richard C.; Fredrickson, Kurt D.; Choi, Miri; Lin, Chungwei; Seo, Hosung; Posadas, Agham B.; Demkov, Alexander A. [Department of Physics, The University of Texas at Austin, Austin, Texas 78712 (United States)] [Department of Physics, The University of Texas at Austin, Austin, Texas 78712 (United States)

    2013-09-14T23:59:59.000Z

    High-resolution angle-resolved photoemission spectroscopy (ARPES) was used to study the surface electronic structure of Nb-doped SrTiO{sub 3} (STO) single crystals prepared using a variety of surface preparations. ARPES measurements show that simple degreasing with subsequent anneal in vacuum is not an adequate surface preparation of STO, rather, preparations consisting of etching with buffered HF or HCl, and to a lesser extent, simple water leaching resulted in surfaces with much less disorder. A non-dispersing, mid-gap state was found ?800 meV above the top of the valence band for samples which underwent etching. This mid-gap state is not present for vacuum-annealed and water-leached samples, as well as for STO thin films grown using molecular beam epitaxy. Theoretical modeling using density functional theory suggests that this mid-gap state is not related to the SrO- and TiO{sub 2}-terminated surfaces, but rather, is due to a partial hydrogenation of the STO surface that occurs during etching.

  12. Innovative coke oven gas cleaning system for retrofit applications. Environmental Monitoring program. Volume 1 - sampling progrom report. Baseline Sampling Program report

    SciTech Connect (OSTI)

    Stuart, L.M.

    1994-05-27T23:59:59.000Z

    Bethlehem Steel Corporation (BSC), in conjunction with the Department of Energy (DOE) is conducting a Clean Coal Technology (CCT) project at its Sparrows Point, Maryland Coke Oven Plant. This innovative coke oven gas cleaning system combines several existing technologies into an integrated system for removing impurities from Coke Oven Gas (COG) to make it an acceptable fuel. DOE provided cost-sharing under a Cooperative Agreement with BSC. This Cooperative Agreement requires BSC to develop and conduct and Environmental Monitoring Plan for the Clean Coal Technology project and to report the status of the EMP on a quarterly basis. It also requires the preparation of a final report on the results of the Baseline Compliance and Supplemental Sampling Programs that are part of the EMP and which were conducted prior to the startup of the innovative coke oven gas cleaning system. This report is the Baseline Sampling Program report.

  13. EIS-0463: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    an Environmental Impact Statement and Conduct Public Scoping Meetings Presidential Permit Application for Northern Pass Transmission, New Hampshire Notice of Intent To Prepare...

  14. Surveillance Guides - PTS 13.2 Packaging and Preparation for...

    Broader source: Energy.gov (indexed) [DOE]

    Facility Representative RL Facility Representative Program April 10, 1995 Surveillance Guide PTS 13.2 Revision 0 Packaging and Preparation for Shipment Page 1 of...

  15. Charge Retention by Gold Clusters on Surfaces Prepared Using...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    soft landing of mass-selected ions. Ligand-stabilized gold clusters were prepared in methanol solution by reduction of chloro(triphenylphosphine)gold(I) with borane...

  16. Optimized Pump Systems Save Coal Preparation Plant Money and...

    Broader source: Energy.gov (indexed) [DOE]

    study describes how Peabody Holding Company was able to improve the performance of a coal slurry pumping system at its Randolph Coal Preparation plant. Using a systematic...

  17. Advanced Post-Combustion CO2 Capture Prepared for the

    E-Print Network [OSTI]

    Advanced Post-Combustion CO2 Capture Prepared for the Clean Air Task Force under a grant from...................................................................................... 3 2. Current Status of Post-Combustion Capture

  18. EIS-0361: Notice of Intent to Prepare an Environmental Impact...

    Broader source: Energy.gov (indexed) [DOE]

    West Virginia The U.S. Department of Energy (DOE) announces its intent to prepare an Environmental Impact Statement (EIS) to assess the potential environmental impacts of a...

  19. EIS-0402: Amended Notice of Intent to Prepare an Environmental...

    Office of Environmental Management (EM)

    2008 notice of intent to prepare an environmental impact statement (EIS) for cleanup of Area IV, including the Energy Technology Engineering Center (ETEC), as well as the...

  20. EIS-0323: Notice of Intent to Prepare a Supplemental Environmental...

    Broader source: Energy.gov (indexed) [DOE]

    Project in California The Western Area Power Administration (Western), Department of Energy (DOE), intends to prepare a Supplemental Environmental Impact Statement (SEIS) to...

  1. Preparations of rare earth-iron alloys by thermite reduction

    DOE Patents [OSTI]

    Schmidt, Frederick A. (Ames, IA); Peterson, David T. (Ames, IA); Wheelock, John T. (Nevada, IA)

    1986-09-16T23:59:59.000Z

    An improved method for the preparation of high-purity rare earth-iron alloys by the aluminothermic reduction of a mixture of rare earth and iron fluorides.

  2. EIS-0434: Notice of Intent To Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Impact Statement and to Conduct Scoping Meetings EIS-0434: Notice of Intent To Prepare an Environmental Impact Statement and to Conduct Scoping Meetings Hualapai Valley Solar...

  3. EIS-0440: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Impact Statement and Conduct Scoping Meetings EIS-0440: Notice of Intent to Prepare an Environmental Impact Statement and Conduct Scoping Meetings Construction and Operation of...

  4. EIS-0403: Notice of Intent to Prepare a Programmatic Environmental...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Environmental Impact Statement EIS-0403: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Solar Energy Development in Six Southwestern States The...

  5. Virginia, Maryland teams prepare for Regional Middle School Science...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Virginia, Maryland teams prepare for Regional Middle School Science Bowl March 3, 2005 The Department of Energy's Jefferson Lab, in Newport News, Va., hosts the VirginiaMaryland...

  6. EIS-0310: Notice of Intent to Prepare a Programmatic Environmental...

    Office of Environmental Management (EM)

    Isotope Production Missions in the United States, Including the Role of the Fast Flux Test Facility The Secretary of Energy recently announced DOE's intent to prepare a...

  7. Jefferson Lab's Science Education Website Helps Students Prepare...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Jefferson Lab's Science Education Website Helps Students Prepare for Upcoming Standards of Learning Tests April 12, 2004 Usage of Jefferson Lab's Science Education website is...

  8. RUS Bulletin 1794A-601: Preparing an Environmental Report for...

    Open Energy Info (EERE)

    601: Preparing an Environmental Report for an Environmental Assessment Jump to: navigation, search OpenEI Reference LibraryAdd to library PermittingRegulatory Guidance -...

  9. The radioactive Substances (Prepared Uranium Thorium Compounds) Exemption Order 1962 

    E-Print Network [OSTI]

    Joseph, Keith

    1962-01-01T23:59:59.000Z

    STATUTORY INSTRUMENTS 1962 No. 2711 ATOMIC ENERGY AND RADIOACI1VE SUBSTANCES The Radioactive Substances (prepared Uranium and Thorium Compounds) Exemption Order 1962...

  10. EIS-0269: Notice of Intent to Prepare a Programmatic Environmental...

    Office of Environmental Management (EM)

    EIS-0269: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Alternative Strategies for the Long-Term Management and Use of Depleted Uranium Hexafluoride,...

  11. Dominican Republic-Support for the Preparation of National Climate...

    Open Energy Info (EERE)

    National Climate Change Strategy Jump to: navigation, search Name Dominican Republic-Argentina-Support for the Preparation of National Climate Change Strategy AgencyCompany...

  12. Bay Bridge Lights Presentation prepared by Zoon Engineering

    Energy Savers [EERE]

    2015 BAY BRIDGE LIGHTS Presentation prepared by Zoon Engineering Presentation Outline Lighting of the New East Span of the Bay Bridge Brief Over view Lighting Facts ...

  13. EIS-0366: Notice of Intent to Prepare a Programmatic Environmental...

    Broader source: Energy.gov (indexed) [DOE]

    Implementation of the Carbon Sequestration Program The U.S. Department of Energy (DOE) announces its intent to prepare a Programmatic Environmental Impact Statement (PEIS) to...

  14. EIS-0396: Advance Notice of Intent o Prepare an Environmental...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    EIS-0396: Advance Notice of Intent o Prepare an Environmental Impact Statement Global Nuclear Energy Partnership Technology Demonstration Program Advance Notice of Intent To...

  15. EIS-0510: FERC Notice of Intent to Prepare Environmental Impact...

    Broader source: Energy.gov (indexed) [DOE]

    impacts of the Calcasieu Pass Project, a proposed liquefied natural gas (LNG) export terminal in Cameron Parish, Louisiana. DOE is a cooperating agency in preparing the EIS. DOE,...

  16. activated carbon preparation: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    mesoporous carbon-based composites for confinement of Eue Mesoporous polymer-carbon composite (CMPEICMK-3) materials were successfully prepared. After Eu(III) ions were loaded...

  17. activated carbon prepared: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    mesoporous carbon-based composites for confinement of Eue Mesoporous polymer-carbon composite (CMPEICMK-3) materials were successfully prepared. After Eu(III) ions were loaded...

  18. activated carbons prepared: Topics by E-print Network

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    mesoporous carbon-based composites for confinement of Eue Mesoporous polymer-carbon composite (CMPEICMK-3) materials were successfully prepared. After Eu(III) ions were loaded...

  19. Early science runs prepare Sequoia for national security missions...

    National Nuclear Security Administration (NNSA)

    Early science runs prepare Sequoia for national security missions | National Nuclear Security Administration Facebook Twitter Youtube Flickr RSS People Mission Managing the...

  20. Controlled remote state preparation via partially entangled quantum channel

    E-Print Network [OSTI]

    Chun Wang; Zhi Zeng; Xi-Han Li

    2014-12-30T23:59:59.000Z

    We propose two controlled remote state preparation protocols via partially entangled channels. One prepares a single-qubit state and the other prepares a two-qubit state. Different from other controlled remote state preparation schemes which also utilize partially entangled channels, neither auxiliary qubits nor two-qubit unitary transformations are required in our schemes and the success probabilities are independent of the coefficients of the quantum channel. The success probabilities are 50% and 25% for arbitrary single-qubit states and two-qubit states, respectively. We also show that the success probabilities can reach 100% for restricted classes of states.