Powered by Deep Web Technologies
Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


1

Overcoming the far-field diffraction limit via absorbance modulation  

E-Print Network [OSTI]

Diffraction limits the resolution of far-field lithography and imaging to about half of the wavelength, which greatly limits the capability of optical techniques. The proposed technique with absorbance modulation aims to ...

Tsai, Hsin-Yu Sidney

2011-01-01T23:59:59.000Z

2

Optimization of proteomic sample preparation procedures for comprehens...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

procedures for comprehensive protein characterization of pathogenic systems. Optimization of proteomic sample preparation procedures for comprehensive protein...

3

Microfluidic DNA sample preparation method and device  

DOE Patents [OSTI]

Manipulation of DNA molecules in solution has become an essential aspect of genetic analyses used for biomedical assays, the identification of hazardous bacterial agents, and in decoding the human genome. Currently, most of the steps involved in preparing a DNA sample for analysis are performed manually and are time, labor, and equipment intensive. These steps include extraction of the DNA from spores or cells, separation of the DNA from other particles and molecules in the solution (e.g. dust, smoke, cell/spore debris, and proteins), and separation of the DNA itself into strands of specific lengths. Dielectrophoresis (DEP), a phenomenon whereby polarizable particles move in response to a gradient in electric field, can be used to manipulate and separate DNA in an automated fashion, considerably reducing the time and expense involved in DNA analyses, as well as allowing for the miniaturization of DNA analysis instruments. These applications include direct transport of DNA, trapping of DNA to allow for its separation from other particles or molecules in the solution, and the separation of DNA into strands of varying lengths.

Krulevitch, Peter A. (Pleasanton, CA); Miles, Robin R. (Danville, CA); Wang, Xiao-Bo (San Diego, CA); Mariella, Raymond P. (Danville, CA); Gascoyne, Peter R. C. (Bellaire, TX); Balch, Joseph W. (Livermore, CA)

2002-01-01T23:59:59.000Z

4

LCLS Equipment Inventory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample Environment: Magnet and6 th7525T HE F IRSTA3LCLS

5

LCLS Prep Lab Images | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample Environment: Magnet and6 th7525T HE FLCLSLCLS Prep Lab

6

Fluidics platform and method for sample preparation and analysis  

DOE Patents [OSTI]

Herein provided are fluidics platform and method for sample preparation and analysis. The fluidics platform is capable of analyzing DNA from blood samples using amplification assays such as polymerase-chain-reaction assays and loop-mediated-isothermal-amplification assays. The fluidics platform can also be used for other types of assays and analyzes. In some embodiments, a sample in a sealed tube can be inserted directly. The following isolation, detection, and analyzes can be performed without a user's intervention. The disclosed platform may also comprises a sample preparation system with a magnetic actuator, a heater, and an air-drying mechanism, and fluid manipulation processes for extraction, washing, elution, assay assembly, assay detection, and cleaning after reactions and between samples.

Benner, W. Henry; Dzenitis, John M.; Bennet, William J.; Baker, Brian R.

2014-08-19T23:59:59.000Z

7

Sample preparation and detection device for infectious agents  

DOE Patents [OSTI]

A sample preparation and analysis device which incorporates both immunoassays and PCR assays in one compact, field-portable microchip. The device provides new capabilities in fluid and particle control which allows the building of a fluidic chip with no moving parts, thus decreasing fabrication cost and increasing the robustness of the device. The device can operate in a true continuous (not batch) mode. The device incorporates magnetohydrodynamic (MHD) pumps to move the fluid through the system, acoustic mixing and fractionation, dielectropheretic (DEP) sample concentration and purification, and on-chip optical detection capabilities.

Miles, Robin R.; Wang, Amy W.; Fuller, Christopher K.; Lemoff, Asuncion V.; Bettencourt, Kerry A.; Yu, June

2003-06-10T23:59:59.000Z

8

Apparatus for preparing a sample for mass spectrometry  

DOE Patents [OSTI]

An apparatus is described for preparing a sample for analysis by a mass spectrometer system. The apparatus has an entry chamber and an ionization chamber separated by a skimmer. A capacitor having two space-apart electrodes followed by one or more ion-imaging lenses is disposed in the ionization chamber. The chamber is evacuated and the capacitor is charged. A valve injects a sample gas in the form of sample pulses into the entry chamber. The pulse is collimated by the skimmer and enters the ionization chamber. When the sample pulse passes through the gap between the electrodes, it discharges the capacitor and is thereby ionized. The ions are focused by the imaging lenses and enter the mass analyzer, where their mass and charge are analyzed. 1 figures.

Villa-Aleman, E.

1994-05-10T23:59:59.000Z

9

Waste minimization in analytical chemistry through innovative sample preparation techniques.  

SciTech Connect (OSTI)

Because toxic solvents and other hazardous materials are commonly used in analytical methods, characterization procedures result in significant and costly amount of waste. We are developing alternative analytical methods in the radiological and organic areas to reduce the volume or form of the hazardous waste produced during sample analysis. For the radiological area, we have examined high-pressure, closed-vessel microwave digestion as a way to minimize waste from sample preparation operations. Heated solutions of strong mineral acids can be avoided for sample digestion by using the microwave approach. Because reactivity increases with pressure, we examined the use of less hazardous solvents to leach selected contaminants from soil for subsequent analysis. We demonstrated the feasibility of this approach by extracting plutonium from a NET reference material using citric and tartaric acids with microwave digestion. Analytical results were comparable to traditional digestion methods, while hazardous waste was reduced by a factor often. We also evaluated the suitability of other natural acids, determined the extraction performance on a wider variety of soil types, and examined the extraction efficiency of other contaminants. For the organic area, we examined ways to minimize the wastes associated with the determination of polychlorinated biphenyls (PCBs) in environmental samples. Conventional methods for analyzing semivolatile organic compounds are labor intensive and require copious amounts of hazardous solvents. For soil and sediment samples, we have a method to analyze PCBs that is based on microscale extraction using benign solvents (e.g., water or hexane). The extraction is performed at elevated temperatures in stainless steel cells containing the sample and solvent. Gas chromatography-mass spectrometry (GC/MS) was used to quantitate the analytes in the isolated extract. More recently, we developed a method utilizing solid-phase microextraction (SPME) for natural water samples. In this SPME technique, a fused-silica fiber coated with a polymeric film is exposed to the sample, extraction is allowed to take place, and then the analytes are thermally desorbed for GC analysis. Unlike liquid-liquid extraction or solid-phase extraction, SPME consumes all of the extracted sample in the analysis, significantly reducing the required sample volume.

Smith, L. L.

1998-05-28T23:59:59.000Z

10

Methodology for Optimal In Situ Alignment and Setting of Bendable Optics for Diffraction-Limited Focusing of Soft X-Rays  

E-Print Network [OSTI]

mirrors, x-rays, x-ray optics, synchrotron radiation,beamline, Kirkpatrick-Baez, metrology of x-ray opticsand Setting of Bendable Optics for Diffraction-Limited

Merthe, Daniel

2013-01-01T23:59:59.000Z

11

Amphiphilic mediated sample preparation for micro-flow cytometry  

DOE Patents [OSTI]

A flow cytometer includes a flow cell for detecting the sample, an oil phase in the flow cell, a water phase in the flow cell, an oil-water interface between the oil phase and the water phase, a detector for detecting the sample at the oil-water interface, and a hydrophobic unit operatively connected to the sample. The hydrophobic unit is attached to the sample. The sample and the hydrophobic unit are placed in an oil and water combination. The sample is detected at the interface between the oil phase and the water phase.

Clague, David S. (Livermore, CA); Wheeler, Elizabeth K. (Livermore, CA); Lee, Abraham P. (Irvine, CA)

2006-07-25T23:59:59.000Z

12

Amphiphilic mediated sample preparation for micro-flow cytometry  

DOE Patents [OSTI]

A flow cytometer includes a flow cell for detecting the sample, an oil phase in the flow cell, a water phase in the flow cell, an oil-water interface between the oil phase and the water phase, a detector for detecting the sample at the oil-water interface, and a hydrophobic unit operatively connected to the sample. The hydrophobic unit is attached to the sample. The sample and the hydrophobic unit are placed in an oil and water combination. The sample is detected at the interface between the oil phase and the water phase.

Clague, David S. (Livermore, CA); Wheeler, Elizabeth K. (Livermore, CA); Lee, Abraham P. (Irvine, CA)

2009-03-17T23:59:59.000Z

13

Sample preparation method for glass welding by ultrashort laser pulses yields higher seam strength  

SciTech Connect (OSTI)

Glass welding by ultrashort laser pulses allows joining without the need of an absorber or a preheating and postheating process. However, cracks generated during the welding process substantially impair the joining strength of the welding seams. In this paper a sample preparation method is described that prevents the formation of cracks. The measured joining strength of samples prepared by this method is substantially higher than previously reported values.

Cvecek, K.; Miyamoto, I.; Strauss, J.; Wolf, M.; Frick, T.; Schmidt, M.

2011-05-01T23:59:59.000Z

14

Chemical composition of esophageal-fistula forage samples as influenced by drying method, salivary leaching and sample preparation  

E-Print Network [OSTI]

in partial fulfillment of the requirement for the degree of YASTER OF' SCI"'NCE, De"ember 1g76 CHEJJICAL COY!POSITION OF ESOPHAGEAL-FISTULA FORAGF SA(vPLES AS INFLUENCED BY DRYING I'METHOD, SALIVARY LEACHING AND SAMPLE PREPARATION A Thesis RAFAEL... ARISTIDES ACOS A-GONZALEZ Approved as to style and content by! (Cha rman o Committee) ((iced of Department) ( I'~iamb r ) Yemb r ) Dcc: mb~+~g~n'jrr ABSTRACT Chemical Composition of Esophageal-Fistula Forage Samples as Influenced by Drying Nethod...

Acosta-Gonzalez, Rafael Aristides

1976-01-01T23:59:59.000Z

15

Enhancing the science return of Mars missions via sample preparation, robotic surface exploration and in orbit fuel production  

E-Print Network [OSTI]

The future of Mars exploration is challenging from multiple points of view. To enhance their science return, future surface probes will most likely be equipped with complex Sample Preparation And Transfer (SPAT) facilities. ...

Lamamy, Julien-Alexandre, 1978-

2004-01-01T23:59:59.000Z

16

EVALUATION OF ARG-1 SAMPLES PREPARED BY CESIUM CARBONATE DISSOLUTION DURING THE ISOLOK SME ACCEPTABILITY TESTING  

SciTech Connect (OSTI)

Evaluation of Defense Waste Processing Facility (DWPF) Chemical Process Cell (CPC) cycle time identified several opportunities to improve the CPC processing time. The Mechanical Systems & Custom Equipment Development (MS&CED) Section of the Savannah River National Laboratory (SRNL) recently completed the evaluation of one of these opportunities - the possibility of using an Isolok sampling valve as an alternative to the Hydragard valve for taking DWPF process samples at the Slurry Mix Evaporator (SME). The use of an Isolok for SME sampling has the potential to improve operability, reduce maintenance time, and decrease CPC cycle time. The SME acceptability testing for the Isolok was requested in Task Technical Request (TTR) HLW-DWPF-TTR-2010-0036 and was conducted as outlined in Task Technical and Quality Assurance Plan (TTQAP) SRNLRP-2011-00145. RW-0333P QA requirements applied to the task, and the results from the investigation were documented in SRNL-STI-2011-00693. Measurement of the chemical composition of study samples was a critical component of the SME acceptability testing of the Isolok. A sampling and analytical plan supported the investigation with the analytical plan directing that the study samples be prepared by a cesium carbonate (Cs{sub 2}CO{sub 3}) fusion dissolution method and analyzed by Inductively Coupled Plasma - Optical Emission Spectroscopy (ICP-OES). The use of the cesium carbonate preparation method for the Isolok testing provided an opportunity for an additional assessment of this dissolution method, which is being investigated as a potential replacement for the two methods (i.e., sodium peroxide fusion and mixed acid dissolution) that have been used at the DWPF for the analysis of SME samples. Earlier testing of the Cs{sub 2}CO{sub 3} method yielded promising results which led to a TTR from Savannah River Remediation, LLC (SRR) to SRNL for additional support and an associated TTQAP to direct the SRNL efforts. A technical report resulting from this work was issued that recommended that the mixed acid method be replaced by the Cs{sub 2}CO{sub 3} method for the measurement of magnesium (Mg), sodium (Na), and zirconium (Zr) with additional testing of the method by DWPF Laboratory being needed before further implementation of the Cs{sub 2}CO{sub 3} method at that laboratory. While the SME acceptability testing of the Isolok does not address any of the open issues remaining after the publication of the recommendation for the replacement of the mixed acid method by the Cs{sub 2}CO{sub 3} method (since those issues are to be addressed by the DWPF Laboratory), the Cs{sub 2}CO{sub 3} testing associated with the Isolok testing does provide additional insight into the performance of the method as conducted by SRNL. The performance is to be investigated by looking to the composition measurement data generated by the samples of a standard glass, the Analytical Reference Glass - 1 (ARG-1), that were prepared by the Cs{sub 2}CO{sub 3} method and included in the SME acceptability testing of the Isolok. The measurements of these samples were presented as part of the study results, but no statistical analysis of these measurements was conducted as part of those results. It is the purpose of this report to provide that analysis, which was supported using JMP Version 7.0.2.

Edwards, T.; Hera, K.; Coleman, C.

2011-12-05T23:59:59.000Z

17

Prepared  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledo SiteTonawandaUniversity21Prepared by Oak Ridge

18

E-Print Network 3.0 - alice photocathode preparation Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

and waveguides - are b e i i produced using MOCVD prepared Ga... examples of optoelectronic devices and OEICs will be discussed and the MOCVD equipment employed to prepare...

19

A comparison of sample preparation methodology in the evaluation of geosynthetic clay liner (GCL) hydraulic conductivity  

SciTech Connect (OSTI)

The method of preparing a single needle-punched GCL product for evaluation of hydraulic conductivity in a flexible wall permeameter was examined. The test protocol utilized for this evaluation was GRI Test Method GCL-2 Permeability of GCLs. The GCL product consisted of bentonite clay material supported by a woven and a non-woven geotextile on either side. The method preparation focused on the procedure for separating the test specimen from the larger sample and whether these methods produced difficulty in generating reliable test data. The methods examined included cutting with a razor knife, scissors, and a circular die with the perimeter of the test area under wet and dry conditions. In order to generate as much data as possible, tests were kept brief. Flow was monitored only long enough to determine whether or not preferential flow paths appeared to be present. The results appear to indicate that any of the methods involved will work. Difficulties arose not from the development of preferential flow paths around the edges of the specimens, but from the loss of bentonite from the edges during handling.

Siebken, J.R. [National Seal Co., Galesburg, IL (United States); Lucas, S. [Albarrie Naue Ltd., Barrie, Ontario (Canada)

1997-11-01T23:59:59.000Z

20

Surface Cleaning Techniques: Ultra-Trace ICP-MS Sample Preparation and Assay of HDPE  

SciTech Connect (OSTI)

The world’s most sensitive radiation detection and assay systems depend upon ultra-low background (ULB) materials to reduce unwanted radiological backgrounds. Herein, we evaluate methods to clean HDPE, a material of interest to ULB systems and the means to provide rapid assay of surface and bulk contamination. ULB level material and ultra-trace level detection of actinide elements is difficult to attain, due to the introduction of contamination from sample preparation equipment such as pipette tips, sample vials, forceps, etc. and airborne particulate. To date, literature available on the cleaning of such polymeric materials and equipment for ULB applications and ultra-trace analyses is limited. For these reasons, a study has been performed to identify an effective way to remove surface contamination from polymers in an effort to provide improved instrumental detection limits. Inductively Coupled Plasma Mass Spectroscopy (ICP-MS) was utilized to assess the effectiveness of a variety of leachate solutions for removal of inorganic uranium and thorium surface contamination from polymers, specifically high density polyethylene (HDPE). HDPE leaching procedures were tested to optimize contaminant removal of thorium and uranium. Calibration curves for thorium and uranium ranged from 15 ppq (fg/mL) to 1 ppt (pg/mL). Detection limits were calculated at 6 ppq for uranium and 7 ppq for thorium. Results showed the most effective leaching reagent to be clean 6 M nitric acid for 72 hour exposures. Contamination levels for uranium and thorium found in the leachate solutions were significant for ultralow level radiation detection applications.

Overman, Nicole R.; Hoppe, Eric W.; Addleman, Raymond S.

2013-06-01T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

Methods for preparing comparative standards and field samples for neutron activation analysis of soil  

SciTech Connect (OSTI)

One of the more difficult problems associated with comparative neutron activation analysis (CNAA) is the preparation of standards which are tailor-made to the desired irradiation and counting conditions. Frequently, there simply is not a suitable standard available commercially, or the resulting gamma spectrum is convoluted with interferences. In a recent soil analysis project, the need arose for standards which contained about 35 elements. In response, a computer spreadsheet was developed to calculate the appropriate amount of each element so that the resulting gamma spectrum is relatively free of interferences. Incorporated in the program are options for calculating all of the irradiation and counting parameters including activity produced, necessary flux/bombardment time, counting time, and appropriate source-to-detector distance. The result is multi-element standards for CNAA which have optimal concentrations. The program retains ease of use without sacrificing capability. In addition to optimized standard production, a novel soil homogenization technique was developed which is a low cost, highly efficient alternative to commercially available homogenization systems. Comparative neutron activation analysis for large scale projects has been made easier through these advancements. This paper contains details of the design and function of the NAA spreadsheet and innovative sample handling techniques.

Glasgow, D.C.; Dyer, F.F.; Robinson, L.

1994-06-01T23:59:59.000Z

22

Adjustable virtual pore-size filter for automated sample preparation using acoustic radiation force  

SciTech Connect (OSTI)

We present a rapid and robust size-based separation method for high throughput microfluidic devices using acoustic radiation force. We developed a finite element modeling tool to predict the two-dimensional acoustic radiation force field perpendicular to the flow direction in microfluidic devices. Here we compare the results from this model with experimental parametric studies including variations of the PZT driving frequencies and voltages as well as various particle sizes and compressidensities. These experimental parametric studies also provide insight into the development of an adjustable 'virtual' pore-size filter as well as optimal operating conditions for various microparticle sizes. We demonstrated the separation of Saccharomyces cerevisiae and MS2 bacteriophage using acoustic focusing. The acoustic radiation force did not affect the MS2 viruses, and their concentration profile remained unchanged. With optimized design of our microfluidic flow system we were able to achieve yields of > 90% for the MS2 with > 80% of the S. cerevisiae being removed in this continuous-flow sample preparation device.

Jung, B; Fisher, K; Ness, K; Rose, K; Mariella, R

2008-05-22T23:59:59.000Z

23

E-Print Network 3.0 - avid radioprobes preparation Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

and plasmids used in this study... of their preparation, by LC-electrospray ionization (ESI)-MSMS on a Thermo Exactive Orbitrap mass spectrometer, using... . Mathematical models...

24

Portable sample preparation and analysis system for micron and sub-micron particle characterization using light scattering and absorption spectroscopy  

DOE Patents [OSTI]

There is provided a method and device for remote sampling, preparation and optical interrogation of a sample using light scattering and light absorption methods. The portable device is a filtration-based device that removes interfering background particle material from the sample matrix by segregating or filtering the chosen analyte from the sample solution or matrix while allowing the interfering background particles to be pumped out of the device. The segregated analyte is then suspended in a diluent for analysis. The device is capable of calculating an initial concentration of the analyte, as well as diluting the analyte such that reliable optical measurements can be made. Suitable analytes include cells, microorganisms, bioparticles, pathogens and diseases. Sample matrixes include biological fluids such as blood and urine, as well as environmental samples including waste water.

Stark, Peter C. (Los Alamos, NM); Zurek, Eduardo (Barranquilla, CO); Wheat, Jeffrey V. (Fort Walton Beach, FL); Dunbar, John M. (Santa Fe, NM); Olivares, Jose A. (Los Alamos, NM); Garcia-Rubio, Luis H. (Temple Terrace, FL); Ward, Michael D. (Los Alamos, NM)

2011-07-26T23:59:59.000Z

25

E-Print Network 3.0 - arca subcrenata prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

in arcA and arcB were consistent with our report that Arc... of NaCl, 1.62 g of CaCl2 2H2O, 1 g of Casamino Acids, and 3 ml of glycerol. Solid media were prepared... ,...

26

The Sample Preparation Laboratories | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary)morphinanInformation Desert Southwest RegionatSearchScheduled System BurstLong Term ScheduleProject IssueCynthia

27

LCLS Sample Preparation Laboratory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-SeriesFlickrinformationPostdocs &JeffIntensitySurface Los5New

28

Universal nucleic acids sample preparation method for cells, spores and their mixture  

DOE Patents [OSTI]

The present invention relates to a method for extracting nucleic acids from biological samples. More specifically the invention relates to a universal method for extracting nucleic acids from unidentified biological samples. An advantage of the presently invented method is its ability to effectively and efficiently extract nucleic acids from a variety of different cell types including but not limited to prokaryotic or eukaryotic cells and/or recalcitrant organisms (i.e. spores). Unlike prior art methods which are focused on extracting nucleic acids from vegetative cell or spores, the present invention effectively extracts nucleic acids from spores, multiple cell types or mixtures thereof using a single method. Important that the invented method has demonstrated an ability to extract nucleic acids from spores and vegetative bacterial cells with similar levels effectiveness. The invented method employs a multi-step protocol which erodes the cell structure of the biological sample, isolates, labels, fragments nucleic acids and purifies labeled samples from the excess of dye.

Bavykin, Sergei (Darien, IL)

2011-01-18T23:59:59.000Z

29

High Throughput Sample Preparation and Analysis for DNA Sequencing, PCR and Combinatorial Screening of Catalysis Based on Capillary Array Technique  

SciTech Connect (OSTI)

Sample preparation has been one of the major bottlenecks for many high throughput analyses. The purpose of this research was to develop new sample preparation and integration approach for DNA sequencing, PCR based DNA analysis and combinatorial screening of homogeneous catalysis based on multiplexed capillary electrophoresis with laser induced fluorescence or imaging UV absorption detection. The author first introduced a method to integrate the front-end tasks to DNA capillary-array sequencers. protocols for directly sequencing the plasmids from a single bacterial colony in fused-silica capillaries were developed. After the colony was picked, lysis was accomplished in situ in the plastic sample tube using either a thermocycler or heating block. Upon heating, the plasmids were released while chromsomal DNA and membrane proteins were denatured and precipitated to the bottom of the tube. After adding enzyme and Sanger reagents, the resulting solution was aspirated into the reaction capillaries by a syringe pump, and cycle sequencing was initiated. No deleterious effect upon the reaction efficiency, the on-line purification system, or the capillary electrophoresis separation was observed, even though the crude lysate was used as the template. Multiplexed on-line DNA sequencing data from 8 parallel channels allowed base calling up to 620 bp with an accuracy of 98%. The entire system can be automatically regenerated for repeated operation. For PCR based DNA analysis, they demonstrated that capillary electrophoresis with UV detection can be used for DNA analysis starting from clinical sample without purification. After PCR reaction using cheek cell, blood or HIV-1 gag DNA, the reaction mixtures was injected into the capillary either on-line or off-line by base stacking. The protocol was also applied to capillary array electrophoresis. The use of cheaper detection, and the elimination of purification of DNA sample before or after PCR reaction, will make this approach an attractive alternative to current methods for genetic analysis and disease diagnosis.

Yonghua Zhang

2002-05-27T23:59:59.000Z

30

Sample M&V Plan from the Texas Workshop: Preparing and Evaluating Measurement and Verification Plans for Energy Performance Contracts in Texas  

E-Print Network [OSTI]

This document contains a sample M&V plan that has been prepared in accordance with the Texas Guidelines for Measurement and Verification for Energy Performance Contracts. This sample M&V plan was extracted from the March 1999 workshop, entitled...

Haberl, J. S.

1999-01-01T23:59:59.000Z

31

Sample Preparation and Characterisation  

E-Print Network [OSTI]

of a 21 4 Cr1Mo power plant steel from Drax Power Station was supplied by National Power plc, it was agitated to prevent the buildup of a layer of bubbles which would provide insulation and reduce the cooling.019 0.015 Table 6.1: Composition of 21 4 Cr1Mo steel; all quantities in wt. %. Data supplied by Bodycote

Cambridge, University of

32

Negligible Sample Heating from Synchrotron Infrared Beam Michael C. Martina  

E-Print Network [OSTI]

Negligible Sample Heating from Synchrotron Infrared Beam Michael C. Martina , Nelly M. Tsvetkovab of Molecular and Cellular Biology, University of California at Davis, USA Infrared (IR) spectroscopy is one can now obtain diffraction-limited spot sizes with high signal intensity in an infrared microscope

33

A Portable Cryo-Plunger for On-Site Intact Cryogenic Microscopy Sample Preparation in Natural Environments  

E-Print Network [OSTI]

in cryo-grid preparation and technological pro- gress in transmission electron microcopy (TEM) instru or propane at 808 K. They applied their technique to aqueous suspensions of biomolecules (Dubochet et al

Knowles, David William

34

Sample Preparation Laboratory Training - Course 204 | Sample Preparation  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 -the Mid-Infrared0 ResourceAwardsSafeguards and SecuritySafety

35

Chemical Resources | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-Series to User Group and Userof a blast-resistant navalChemCam laser Chemical

36

Chemical Inventory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: Vegetation Proposed New Substation SitesStandingtheirCheck In & RegistrationChemicalDropletsChemical

37

Laboratory Access | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-SeriesFlickrinformationPostdocs space control

38

Laboratory Waste | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-SeriesFlickrinformationPostdocs space Combined Routes & Schedules Blue

39

Equipment Inventory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: Vegetation ProposedUsing ZirconiaPolicy and Assistance EnvironmentalEnzymeEnzymeCr1stEquipment Inventory

40

Geoscience Laboratory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-SeriesFlickr Flickr Editor'sshort version)UnveilsGeorgeGeoscience Laboratory

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

Introduction Preparation  

E-Print Network [OSTI]

Introduction Motivation Preparation Notos' Components Results Conclusions and Future Work Building Problem Description and Motivation Preparation Notation, Passive DNS trends and Anchor Classes Notos Reputation Results Conclusions and Future Work Special thanks to: Damballa Passive DNS data, Malware and BL

42

Lucky exposures: diffraction limited astronomical imaging through the atmosphere  

E-Print Network [OSTI]

brightness are circled in red in d). In panels a)—c) the blurring effect of the PSFs re-distributes the flux from the point sources over a wider area of the image leading to a substantial reduction in the peak pixel values in the images. can be improved... to this method as the Lucky Exposures technique. A number of other authors have published results using very similar methods, particularly 1.3. Performance of ground-based high resolution imaging techniques 11 for solar and planetary observations. Observations...

Tubbs, Robert Nigel

2003-11-25T23:59:59.000Z

43

Diffraction-Limited Soft X-Ray Workshop  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: Vegetation Proposed Newcatalyst phasesData FilesShape,Physics DiagnosticsMicrochips. |

44

ALS Workshop Highlights Diffraction-Limited Storage Ring Opportunities  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsrucLasDelivered‰PNGExperience4AJ01) (See95TI07)Operations DuringALSSpectrum PrintUsers'ALS Workshop

45

Correlated Topographic and Spectroscopic Imaging Beyond Diffraction Limit  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: Vegetation Proposed Newcatalyst phases on γ-Al2O3. | EMSLHydrogen andCorrectiveby Atomic

46

Pressurized fluidized-bed hydroretorting of eastern oil shales. Volume 4, Task 5, Operation of PFH on beneficiated shale, Task 6, Environmental data and mitigation analyses and Task 7, Sample procurement, preparation, and characterization: Final report, September 1987--May 1991  

SciTech Connect (OSTI)

The objective of Task 5 (Operation of Pressurized Fluidized-Bed Hydro-Retorting (PFH) on Beneficiated Shale) was to modify the PFH process to facilitate its use for fine-sized, beneficiated Eastern shales. This task was divided into 3 subtasks: Non-Reactive Testing, Reactive Testing, and Data Analysis and Correlations. The potential environment impacts of PFH processing of oil shale must be assessed throughout the development program to ensure that the appropriate technologies are in place to mitigate any adverse effects. The overall objectives of Task 6 (Environmental Data and Mitigation Analyses) were to obtain environmental data relating to PFH and shale beneficiation and to analyze the potential environmental impacts of the integrated PFH process. The task was divided into the following four subtasks. Characterization of Processed Shales (IGT), 6.2. Water Availability and Treatment Studies, 6.3. Heavy Metals Removal and 6.4. PFH Systems Analysis. The objective of Task 7 (Sample Procurement, Preparation, and Characterization) was to procure, prepare, and characterize raw and beneficiated bulk samples of Eastern oil shale for all of the experimental tasks in the program. Accomplishments for these tasks are presented.

Not Available

1992-03-01T23:59:59.000Z

47

Abstracting Preparation  

E-Print Network [OSTI]

Guidelines & Review Manuscript Preparation Submit Your Manuscript Book Reviews Movies & Videos Contact of Biological and Chemical Sciences. Queen Mary, University of London, Mile End Road, London, UK. Abstract Two motive force for energy conversion, providing for metabolism, for active transport, and for synthesis

Allen, John F.

48

Petrographic characterization of Kentucky coals. Final report. Part V. Pyrite size/form/microlithotype distribution in western Kentucky prepared coals and in channel samples from western Kentucky and western Pennsylvania  

SciTech Connect (OSTI)

Pyrite and marcasite distribution has been characterized in several western Kentucky coals, western Pennsylvania coals, and coals from western Kentucky preparation plants using three parameters of size, morphology, and microlithotype association. A classification system was developed to provide a consistent method for recording different pyrite/marcasite types. Sulfides were microscopically measured and placed in one of six size divisions (<5, 5 to 10, 10 to 40, 40 to 75, 75 to 100, or >150..mu..m) rather than absolute size. Five categories (euhedral, framboidal, dendritic, massive, or cleat) describe pyrite/marcasite morphology. The third parameter identifies the microlithotype (vitrite, clarite, inertite, liptite, durite, vitrinertite, trimacerite, or carbominerite) in which the pyrite occurs (not including the measured sulfide). Carbominerite is a mineral/organic association dominated by mineral matter. The percentage of each variable represents the total number of counts per sample and not the volume of pyrite. Throughout the studies, both sulfides are collectively referred to as pyrite unless otherwise specified. This paper describes the different studies which were undertaken to test the usefulness of this pyrite classification system. Systematic trends in pyrite variability were determined for the Springfield coal and Herrin of western Kentucky. Pyrite characterization of the Lower Kittanning coal from western Pennsylvania shows that certain pyrite morphologies can be an expression of the environments deposition of coal bodies. Studies of western Kentucky prepared coals demonstrate that pyrite characterization apparently can provide a method for predicting pyrite behavior and the extent of pyrite removal for specific coals. 77 references, 15 figures, 19 tables.

Frankle, K.A.; Hower, J.C.

1983-01-01T23:59:59.000Z

49

Preparation of Samples for Compositional Analysis: Laboratory...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Institute * Battelle Contract No. DE-AC36-99-GO10337 DISCLAIMER These Standard Biomass Analytical Methods ("Methods") are provided by the National Renewable Energy...

50

Sample preparation system for microfluidic applications  

DOE Patents [OSTI]

An apparatus that couples automated injection with flow feedback to provide nanoliter accuracy in controlling microliter volumes. The apparatus comprises generally a source of hydraulic fluid pressure, a fluid isolator joined to the outlet of the hydraulic pressure source and a flow sensor to provide pressure-driven analyte metering. For operation generally and particularly in microfluidic systems the hydraulic pressure source is typically an electrokinetic (EK) pump that incorporates gasless electrodes. The apparatus is capable of metering sub-microliter volumes at flowrates of 1 100 .mu.L/min into microsystem load pressures of up to 1000 50 psi, respectively. Flowrates can be specified within 0.5 .mu.L/min and volumes as small as 80 nL can be metered.

Mosier, Bruce P. (San Francisco, CA); Crocker, Robert W. (Fremont, CA); Patel, Kamlesh D. (Dublin, CA); Harnett, Cindy K. (Livermore, CA)

2007-05-08T23:59:59.000Z

51

Lithium Isotope Sample Preparation University of Maryland  

E-Print Network [OSTI]

in the chemistries are methanol and ethanol, both ~100%, stored under cabinet #4, in the area marked "organics." It is necessary for the 12 ml Li column chemistry to use Teflon- distilled methanol. The ethanol that is used with ethanol used for removing ink from surfaces is ordinarily kept near the Milli-Q system. cleaning

Mcdonough, William F.

52

Laboratory Equipment & Supplies | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-SeriesFlickrinformationPostdocs space controlAppraisalLaboratory

53

Geoscience Equipment Inventory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: Vegetation ProposedUsingFun with Big Sky Learning FunNeuTel2011 Venezia,Lab George NeilFall Job

54

Geoscience Prep Lab Slideshow | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: Vegetation ProposedUsingFun with Big Sky Learning FunNeuTel2011 Venezia,Lab George NeilFall

55

Available for Checkout Equipment Inventory | Sample Preparation  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth (AOD)ProductssondeadjustsondeadjustAboutScience Program Cumulus Humilis,Technologies Available

56

BCM 1 Equipment Inventory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth (AOD)ProductssondeadjustsondeadjustAboutScience Program CumulusA t i o nLiquids Reserve ClassBBEEBunch1

57

BCM 2 Equipment Inventory | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth (AOD)ProductssondeadjustsondeadjustAboutScience Program CumulusA t i o nLiquids Reserve ClassBBEEBunch12

58

RW Prepared  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledo SiteTonawandaUniversity21Prepared by,..~Y-t7 Ii,r

59

Preparing Your  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 - SeptemberMicroneedles for medical point07.06 AgendaPreparation forTrioxide The

60

Sample introducing apparatus and sample modules for mass spectrometer  

DOE Patents [OSTI]

An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus.

Thompson, Cyril V. (Knoxville, TN); Wise, Marcus B. (Kingston, TN)

1993-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

Sample introducing apparatus and sample modules for mass spectrometer  

DOE Patents [OSTI]

An apparatus for introducing gaseous samples from a wide range of environmental matrices into a mass spectrometer for analysis of the samples is described. Several sample preparing modules including a real-time air monitoring module, a soil/liquid purge module, and a thermal desorption module are individually and rapidly attachable to the sample introducing apparatus for supplying gaseous samples to the mass spectrometer. The sample-introducing apparatus uses a capillary column for conveying the gaseous samples into the mass spectrometer and is provided with an open/split interface in communication with the capillary and a sample archiving port through which at least about 90 percent of the gaseous sample in a mixture with an inert gas that was introduced into the sample introducing apparatus is separated from a minor portion of the mixture entering the capillary discharged from the sample introducing apparatus. 5 figures.

Thompson, C.V.; Wise, M.B.

1993-12-21T23:59:59.000Z

62

Office Automation Document Preparation  

E-Print Network [OSTI]

.2 Distinctions 1.3 Facilities 1.3.1 Document Preparation 1.3.2 Records Management 1.3.3 Communication 1 organizations contemplating the installation of document-preparation systems. * Administrative managersOffice Automation and Document Preparation for the v' University of North Carolina at Chapel Hill

North Carolina at Chapel Hill, University of

63

E-Print Network 3.0 - aberrant class ii Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

the diffraction limit... , but there are situations in which having slightly aberrated optics can provide some relative visual benefits. This fact led Source: Artal, Pablo -...

64

E-Print Network 3.0 - automated sample transfer Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

code) - Prepare sample dilution: o Use stock ... Source: Kaber, David B. - Department of Industrial and Systems Engineering, North Carolina State University Collection:...

65

Preparation of acetaldehyde  

DOE Patents [OSTI]

Disclosed is a process for the preparation of acetaldehyde by the hydrogenation of ketene in the presence of a transition metal hydrogenation catalyst.

Tustin, Gerald Charles (Kingsport, TN); Depew, Leslie Sharon (Kingsport, TN)

1997-10-21T23:59:59.000Z

66

Aerosol preparation of intact lipoproteins  

DOE Patents [OSTI]

A medical diagnostic method and instrumentation system for analyzing noncovalently bonded agglomerated biological particles is described. The method and system comprises: a method of preparation for the biological particles; an electrospray generator; an alpha particle radiation source; a differential mobility analyzer; a particle counter; and data acquisition and analysis means. The medical device is useful for the assessment of human diseases, such as cardiac disease risk and hyperlipidemia, by rapid quantitative analysis of lipoprotein fraction densities. Initially, purification procedures are described to reduce an initial blood sample to an analytical input to the instrument. The measured sizes from the analytical sample are correlated with densities, resulting in a spectrum of lipoprotein densities. The lipoprotein density distribution can then be used to characterize cardiac and other lipid-related health risks.

Benner, W. Henry (Danville, CA); Krauss, Ronald M (Berkeley, CA); Blanche, Patricia J (Berkeley, CA)

2012-01-17T23:59:59.000Z

67

arbitrary sub-diffraction-limit pattern: Topics by E-print Network  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Washington at Seattle, University of 243 Synthesising arbitrary quantum states in a superconduct-ing resonator Computer Technologies and Information Sciences Websites Summary:...

68

Measurement of the separation between atoms beyond diffraction limit RID A-5077-2009  

E-Print Network [OSTI]

the distance of the two atoms via the emitted resonance fluorescence. We define R? as the unit vector in observation direction, and the observation angle #12; as #12;=arcos#1;R? ?r12/r12#2;. The total two-atom steady state resonance fluorescence spectrum S...

Chang, J. T.; Evers, J.; Scully, Marlan O.; Zubairy, M. Suhail

2006-01-01T23:59:59.000Z

69

Optical imaging beyond the diffraction limit via dark states RID A-8711-2009  

E-Print Network [OSTI]

We study the possibility of creating spatial patterns having subwavelength size by using the so-called dark states formed by the interaction between atoms and optical fields. These optical fields have a specified spatial distribution. Our...

Li, Hebin; Sautenkov, Vladimir A.; Kash, Michael M.; Sokolov, Alexei V.; Welch, George R.; Rostovtsev, Yuri V.; Zubairy, M. Suhail; Scully, Marlan O.

2008-01-01T23:59:59.000Z

70

Think about it Preparing for Graduate School  

E-Print Network [OSTI]

Think about it Preparing for Graduate School Selecting Schools to Which You'll Apply Applying for Admittance The G.R.E. Writing Sample Campus Visits Graduate School Programs Your reasons for going to graduate school in English should go beyond simply that you like to read and write, that you like school

Sheridan, Jennifer

71

AUTOMATED, ACCURATE, AND INEXPENSIVE SOLUTION-PREPARATION ON A DIGITAL MICROFLUIDIC BIOCHIP*  

E-Print Network [OSTI]

AUTOMATED, ACCURATE, AND INEXPENSIVE SOLUTION- PREPARATION ON A DIGITAL MICROFLUIDIC BIOCHIP* Tao propose an electrowetting-based "digital" microfluidic biochip design for automated solution-crystallization application. Index Terms: Digital microfluidics, droplets, laboratory automation, sample preparation. I

Chakrabarty, Krishnendu

72

Preparing for the Future  

E-Print Network [OSTI]

tx H2O | pg. 12 Preparing for the Future Story by Kathy Wythe Preparing for the Future University establishes water management degree program Texas A&M University launched an interdisci-plinary water management degree programduring the fall... 2005 semester with 12 stu-dents seeking either master?s or doctorate degrees in water management and hydrologic sciences. The degree program, the first in Texas, includes 42 faculty members in 12 departments from four differ- ent colleges, said Ron...

Wythe, Kathy

2006-01-01T23:59:59.000Z

73

Yeast Immunofluorescence Prepare Cells  

E-Print Network [OSTI]

slide. Resuspend in up to 250 µl SPC buffer to prepare up to 5 slides. #12;Prepare Slide: 11. Use clean 15-well slide(s). Start with 25 µl of 2 mg/ml poly-D-lysine (Sigma P-1024) per slide. Pipet on and then off, leaving a thin film on slide well. Hold at room temperature for 1 minute. Wash slide using

Aris, John P.

74

Offline solid phase microextraction sampling system  

DOE Patents [OSTI]

An offline solid phase microextraction (SPME) sampling apparatus for enabling SPME samples to be taken a number of times from a previously collected fluid sample (e.g. sample atmosphere) stored in a fused silica lined bottle which keeps volatile organics in the fluid sample stable for weeks at a time. The offline SPME sampling apparatus has a hollow body surrounding a sampling chamber, with multiple ports through which a portion of a previously collected fluid sample may be (a) released into the sampling chamber, (b) SPME sampled to collect analytes for subsequent GC analysis, and (c) flushed/purged using a fluidically connected vacuum source and purging fluid source to prepare the sampling chamber for additional SPME samplings of the same original fluid sample, such as may have been collected in situ from a headspace.

Harvey, Chris A. (French Camp, CA)

2008-12-16T23:59:59.000Z

75

Review: Preparing for Climate Change  

E-Print Network [OSTI]

Review: Preparing for Climate Change By Michael D.Stephen, Preparing for Climate Change. A Boston Review Book.alkaline paper. “Climate change is inevitable, but disaster

Kunnas, Jan

2013-01-01T23:59:59.000Z

76

automated sample preparation: Topics by E-print Network  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Websites Summary: of a partial automation since they act on the control part of the vehicle. This increasing automationABV- A Low Speed Automation Project to Study the...

77

Intelligent front-end sample preparation tool using acoustic streaming.  

SciTech Connect (OSTI)

We have successfully developed a nucleic acid extraction system based on a microacoustic lysis array coupled to an integrated nucleic acid extraction system all on a single cartridge. The microacoustic lysing array is based on 36{sup o} Y cut lithium niobate, which couples bulk acoustic waves (BAW) into the microchannels. The microchannels were fabricated using Mylar laminates and fused silica to form acoustic-fluidic interface cartridges. The transducer array consists of four active elements directed for cell lysis and one optional BAW element for mixing on the cartridge. The lysis system was modeled using one dimensional (1D) transmission line and two dimensional (2D) FEM models. For input powers required to lyse cells, the flow rate dictated the temperature change across the lysing region. From the computational models, a flow rate of 10 {micro}L/min produced a temperature rise of 23.2 C and only 6.7 C when flowing at 60 {micro}L/min. The measured temperature changes were 5 C less than the model. The computational models also permitted optimization of the acoustic coupling to the microchannel region and revealed the potential impact of thermal effects if not controlled. Using E. coli, we achieved a lysing efficacy of 49.9 {+-} 29.92 % based on a cell viability assay with a 757.2 % increase in ATP release within 20 seconds of acoustic exposure. A bench-top lysing system required 15-20 minutes operating up to 58 Watts to achieve the same level of cell lysis. We demonstrate that active mixing on the cartridge was critical to maximize binding and release of nucleic acid to the magnetic beads. Using a sol-gel silica bead matrix filled microchannel the extraction efficacy was 40%. The cartridge based magnetic bead system had an extraction efficiency of 19.2%. For an electric field based method that used Nafion films, a nucleic acid extraction efficiency of 66.3 % was achieved at 6 volts DC. For the flow rates we tested (10-50 {micro}L/min), the nucleic acid extraction time was 5-10 minutes for a volume of 50 {micro}L. Moreover, a unique feature of this technology is the ability to replace the cartridges for subsequent nucleic acid extractions.

Cooley, Erika J.; McClain, Jaime L.; Murton, Jaclyn K.; Edwards, Thayne L.; Achyuthan, Komandoor E.; Branch, Darren W.; Clem, Paul Gilbert; Anderson, John Mueller; James, Conrad D.; Smith, Gennifer; Kotulski, Joseph Daniel

2009-09-01T23:59:59.000Z

78

Digital microfluidic sample preparation for biological mass spectrometry   

E-Print Network [OSTI]

The use of mass spectrometry in the biosciences has undergone huge growth in re- cent years due to sustained effort in the development of new ionisation techniques, more powerful mass analysers and better bioinformatic ...

Stokes, Adam A.

2011-06-27T23:59:59.000Z

79

Optimization of proteomic sample preparation procedures for comprehensive  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 - September 2006 The 2002Optics Group (X-ray Science Division) Theprotein

80

BCM1 Prep Lab Slideshow | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth (AOD)ProductssondeadjustsondeadjustAboutScience Program CumulusA t i o nLiquids Reserve ClassBBEEBunch12BCM1

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


81

BCM2 Prep Lab Slideshow | Sample Preparation Laboratories  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth (AOD)ProductssondeadjustsondeadjustAboutScience Program CumulusA t i o nLiquids Reserve

82

Biology Chemistry & Material Science Laboratory 1 | Sample Preparation  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-Series to someone6 M. Babzien,Biological Imaging by Soft X-Ray1.2U.S.

83

Biology Chemistry & Material Science Laboratory 2 | Sample Preparation  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May JunDatastreamsmmcrcalgovInstrumentsruc DocumentationP-Series to someone6 M. Babzien,Biological Imaging by Soft

84

Preparation of vinyl acetate  

DOE Patents [OSTI]

This invention pertains to the preparation of vinyl acetate by contacting a mixture of hydrogen and ketene with a heterogeneous catalyst containing a transition metal to produce acetaldehyde, which is then reacted with ketene in the presence of an acid catalyst to produce vinyl acetate.

Tustin, Gerald Charles (Kingsport, TN); Zoeller, Joseph Robert (Kingsport, TN); Depew, Leslie Sharon (Kingsport, TN)

1998-01-01T23:59:59.000Z

85

Preparation of vinyl acetate  

DOE Patents [OSTI]

This invention pertains to the preparation of vinyl acetate by contacting a mixture of hydrogen and ketene with a heterogeneous catalyst containing a transition metal to produce acetaldehyde, which is then reacted with ketene in the presence of an acid catalyst to produce vinyl acetate.

Tustin, G.C.; Zoeller, J.R.; Depew, L.S.

1998-03-24T23:59:59.000Z

86

CAREER FAIR PREPARATION &  

E-Print Network [OSTI]

, NJ #12;BEFORE THE CAREER FAIR · Prepare A Resume Create a resume using the "RBS Undergraduate New Brunswick Student Handbook" as a guide Have your resume reviewed by a Career Counselor Upload resume to Symplicity - RBS Undergraduate Office New Brunswick's career portal system Print plenty copies of your resume

Lin, Xiaodong

87

Sampling box  

DOE Patents [OSTI]

An air sampling box that uses a slidable filter tray and a removable filter cartridge to allow for the easy replacement of a filter which catches radioactive particles is disclosed.

Phillips, Terrance D. (617 Chestnut Ct., Aiken, SC 29803); Johnson, Craig (100 Midland Rd., Oak Ridge, TN 37831-0895)

2000-01-01T23:59:59.000Z

88

TORIS Data Preparation Guidelines  

SciTech Connect (OSTI)

The objective of this manual is to present guidelines and procedures for the preparation of new data for the Tertiary Oil Recovery Information System (TORIS) data base. TORIS is an analytical system currently maintained by the Department of Energy's (DOE) Bartlesville Project Office. It uses an extensive field- and reservoir-level data base to evaluate the technical and economic recovery potential of specific crude oil reservoirs.

Guinn, H.; Remson, D.

1999-03-11T23:59:59.000Z

89

Preparing for the Unexpected  

E-Print Network [OSTI]

for leaks before continuing service. Inventory ? Account for all livestock, fuels, chemicals, machinery and equipment. Compare this list to the inventory prepared before the incident. 1#24; ? Note any lost livestock, and report to emergency response... the crisis and rely on the public to follow instructions and react quickly. To know exactly what to do if a disaster occurs, you will need to monitor TV, radio or on-line news reports for official news. The health department, county emergency management...

Harris, Janie; Norman, Lisa; Lesikar, Bruce J.; Smith, David

2007-03-26T23:59:59.000Z

90

Thermal oxidation procedure PREPARATION........................................................................................................................................... 2  

E-Print Network [OSTI]

procedure - 2 - Preparation. The preparation procedure sets up the power, gas supplies, cooling water, (DI to check all the supplies. Cooling water Gas supplies Routing DI water for wet oxidation We start........................................................................................................................................... 2 Step 1 Turn on the cooling water

Hochberg, Michael

91

Surface preparation and plating  

SciTech Connect (OSTI)

This chapter covers electroplating and electroless nickel plating since coatings of this type play an important role in diamond turning technology. Items to be discussed include preparation of substrates prior to coating, plating defects such as pits and nodules and their influence on optics, the influence of stress in coatings, plating details for copper, gold, silver, and electroless nickel, and the importance of additives and their influence on grain size and structure of deposits. Some comments are made on future challenges that could be presented to the plating community to further improve the quality of coatings applied for diamond turning purposes. 60 references, 8 figures, 9 tables.

Dini, J.W.; Waldrop, F.B.; Reno, R.W.

1982-10-06T23:59:59.000Z

92

ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION...  

Broader source: Energy.gov (indexed) [DOE]

5: BUDGET PREPARATION, PRESENTATION, AND APPORTIONMENT RECORDS ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION, AND APPORTIONMENT RECORDS Budget and...

93

ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION...  

Broader source: Energy.gov (indexed) [DOE]

5: BUDGET PREPARATION, PRESENTATION, AND APPORTIONMENT ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION, AND APPORTIONMENT Budget and apportionment records...

94

Process for preparing liquid wastes  

DOE Patents [OSTI]

A process for preparing radioactive and other hazardous liquid wastes for treatment by the method of vitrification or melting is provided for.

Oden, Laurance L. (Albany, OR); Turner, Paul C. (Albany, OR); O'Connor, William K. (Lebanon, OR); Hansen, Jeffrey S. (Corvallis, OR)

1997-01-01T23:59:59.000Z

95

CIP Preparation Course Summer 2008  

E-Print Network [OSTI]

CIP Preparation Course Summer 2008 Project Lead: Susan Rose, Ph.D. Office for the Protection, and support needed to prepare for and successfully pass the Certified IRB Professional (CIP) examination, State Law (Marlene) Week 9 (8/11/08) *Pre-post practice test, Q&A, CIP Discussion, Test Strategies

Biederman, Irving

96

Analytical Data Report for Sediment Samples Collected From 200 BP 5 OU, C7514 (299-E28-30) L-Well  

SciTech Connect (OSTI)

This an analytical data report for samples received from BP-5 L Well. This report is being prepared for CHPRC.

Lindberg, Michael J.

2010-06-18T23:59:59.000Z

97

E-Print Network 3.0 - a-exposed atlantic cod Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

98

E-Print Network 3.0 - atlantic cod pineal Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

99

E-Print Network 3.0 - atlantic cod piscidin Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

portions of freshly landed Atlantic cod, Gadus morhua, were either directly stored in ice... during certain seasons. Materials and Methods Sample Preparation Eviscerated...

100

E-Print Network 3.0 - aluminum borate whisker Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

borate whisker Search Powered by Explorit Topic List Advanced Search Sample search results for: aluminum borate whisker Page: << < 1 2 3 4 5 > >> 1 Chemical Preparation of Aluminum...

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

Preparing for Transfer Biological Engineering  

E-Print Network [OSTI]

Environmental Engineering Game Design Industrial Systems & Information Technology Information Science MaterialsPreparing for Transfer Majors: Biological Engineering Chemical Engineering Civil Engineering Computer Science Electrical & Computer Engineering Engineering Physics Environmental Engineering

Walter, M.Todd

102

Microfluidic preparative free-flow isoelectric focusing in a triangular channel: System development and characterization  

E-Print Network [OSTI]

A preparative scale free-flow IEF device is developed and characterized with the aim of addressing needs of molecular biologists working with protein samples on the milligrams and milliliters scale. A triangular-shape ...

Wen, Jian

103

PUBLISHED ONLINE: 11 JANUARY 2009 DOI: 10.1038/NPHYS1158 Diffraction-limited performance and focusing of  

E-Print Network [OSTI]

is an attractive high-brightness X-ray source in its own right, particularly as laser development progresses by the relativistically oscillating plasma surface generated by an ultraintense laser focused onto a solid target. Until such an extreme interaction with increasing laser intensity. Here, we provide the first quantitative evidence

Loss, Daniel

104

Preparation, Characterization, and Catalytic Properties of Tungsten...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Preparation, Characterization, and Catalytic Properties of Tungsten Trioxide Cyclic Trimers on FeO(111)Pt(111). Preparation, Characterization, and Catalytic Properties of Tungsten...

105

Business Owners: Prepare for Utility Disruptions | Department...  

Broader source: Energy.gov (indexed) [DOE]

Utility Disruptions Business Owners: Prepare for Utility Disruptions Business Owners: Prepare for Utility Disruptions Have a plan in place in case a natural disaster or other...

106

PREPARED BY: Regional Freight Data  

E-Print Network [OSTI]

.5% Truck, ocean, rail, air Milled grain products and preparations and bakery products 3.3% Truck, rail instruments and apparatus 3.1% Truck, air Printed products 2.9% Truck, rail, air Nonmetallic mineral products for 60% of Oregon jobs · Transportation and logistics account for 20-25% of product cost · Average

Bertini, Robert L.

107

prepared at INRIA Sophia Antipolis  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Maxime DESCOTEAUX Adviser Rachid Deriche INRIA Sophia Antipolis, France Reviewers Peter Basser NICHD, USA Ayache INRIA Sophia Antipolis, France Habib Benali INSERM / Pitié-Salpêtrière, France Denis Le Bihan

Paris-Sud XI, Université de

108

prepared at INRIA Sophia Antipolis  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Wassermann Advisor Dr. Rachid Deriche INRIA Sophia-Antipolis, France Reviewers Dr. Cyril Poupon CEA Neuro l' INRIA Sophia Antipolis et present´ee ´a l' Universit´e de Nice-Sophia Antipolis ´Ecole Doctorale

Paris-Sud XI, Université de

109

prepared at INRIA Sophia Antipolis  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Sophia Antipolis, France Pr. Val´erie Perrier University of Grenoble, France Dr. Fabrice Wallois;UNIVERSIT ´E NICE-SOPHIA ANTIPOLIS - UFR Sciences ´Ecole Doctorale STIC (Sciences et Technologies de l

Paris-Sud XI, Université de

110

prepared at INRIA Sophia Antipolis  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Voronoi Diagrams and Applications Camille WORMSER Advisors Pr. Jean-Daniel Boissonnat INRIA Sophia Antipolis, France Pr. Mariette Yvinec INRIA Sophia Antipolis, France Reviewers Pr. Aurenhammer Technische

Paris-Sud XI, Université de

111

prepared at INRIA Sophia Antipolis  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia NUNDLOLL Defense date: 30 March 2010. Jury Members Jean Luc GOUZ� INRIA Sophia Antipolis, France Advisor Frédéric GROGNARD INRIA Sophia Antipolis, France Co-advisor Ludovic MAILLERET INRA Sophia Antipolis, France

Paris-Sud XI, Université de

112

prepared at INRIA Sophia Antipolis  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia Antipolis and presented at the University of Nice-Sophia Pr. Rachid Deriche INRIA Sophia Antipolis, France Pr. Olivier Faugeras INRIA Sophia Antipolis, France-Fredrik Westin Harvard University, USA Examiners Pr. Nicholas Ayache INRIA Sophia Antipolis, France Dr. Maher

Paris-Sud XI, Université de

113

Safety Manual Prepared by the  

E-Print Network [OSTI]

IMS Safety Manual Prepared by the IMS Safety Committee January 1991 (revised 1/2009) Institute 2 Introduction 3 IMS Laboratory Safety Reporting Policy 4 IMS Safety Committee 5 Fire Safety and Emergency Procedures 6 First Aid and Emergency Response 8 General Laboratory Safety 10 Chemical Spills

Alpay, S. Pamir

114

Preparation of gas selective membranes  

DOE Patents [OSTI]

Gas separation membranes which possess improved characteristics as exemplified by selectivity and flux may be prepared by coating a porous organic polymer support with a solution or emulsion of a plasticizer and an organic polymer, said coating being effected at subatmospheric pressures in order to increase the penetration depth of the coating material.

Kulprathipanja, S.; Kulkarni, S.S.; Funk, E.W.

1988-06-14T23:59:59.000Z

115

Preparation of gas selective membranes  

DOE Patents [OSTI]

Gas separation membranes which possess improved characteristics as exemplified by selectivity and flux may be prepared by coating a porous organic polymer support with a solution or emulsion of a plasticizer and an organic polymer, said coating being effected at subatmospheric pressures in order to increase the penetration depth of the coating material.

Kulprathipanja, Santi (Hoffman Estates, IL); Kulkarni, Sudhir S. (Hoffman Estates, IL); Funk, Edward W. (Highland Park, IL)

1988-01-01T23:59:59.000Z

116

Arduino Sustainability Project Prepared for  

E-Print Network [OSTI]

Arduino Sustainability Project Prepared for: Dr. Pushkin Kachroo EE 290 UNLV Christian Calvo 2009 by the Arduino microcontroller to satisfy the theme of sustainability. The device I decided to construct is determined by the LDR. The LDR output signal is fed into an analog input of the Arduino. The value is read

Kachroo, Pushkin

117

Preparation of asymmetric porous materials  

DOE Patents [OSTI]

A method for preparing an asymmetric porous material by depositing a porous material film on a flexible substrate, and applying an anisotropic stress to the porous media on the flexible substrate, where the anisotropic stress results from a stress such as an applied mechanical force, a thermal gradient, and an applied voltage, to form an asymmetric porous material.

Coker, Eric N. (Albuquerque, NM)

2012-08-07T23:59:59.000Z

118

RECYCLING RATE STUDY Prepared by  

E-Print Network [OSTI]

NATIONAL RECYCLING RATE STUDY Prepared by: Smith, Bucklin and Associates, Inc. Market Research and Statistics Division Chicago, Illinois July 2003 PRINTED ON RECYCLED PAPER #12;BCI RECYCLING RATE STUDY TABLE ....................................................................................................1 II. METHODOLOGY A. Total Pounds of Lead Recycled from Batteries

Laughlin, Robert B.

119

preparation  

E-Print Network [OSTI]

Uranium can be removed from groundwater by adding an electron donor to the subsurface that stimulates growth of native bacteria, generating conditions that result in precipitation of uranium. The long-term efficacy of this technology is unproven. Numerical modeling results for uranium bioremediation in a shallow, alluvial aquifer are provided to establish a broad framework for understanding processes associated with bioremediation of uranium and to bound conditions under which bioremediation could succeed in the long-term and conditions under which it is likely to fail. The models are benchmarked against experiments conducted at the Rifle, Colorado site. Sensitivity analysis of model parameters were conducted, examining: alternatives to the acetate electron donor (lactate and ethanol), oxygen and nitrate terminal electron acceptors, multiphase flow, density and gas entrapment processes, and hypothetical flood events. Sensitivity of simulated aqueous U(VI) concentrations to process model parameters suggest that groundwater flow rate, uranium bioreduction rate, and sulfate bioreduction parameters exert the most impact on bioremediation effectiveness. The simulated scenarios are used to assess potential performance issues for site conditions and other bioremediation approaches.

Bioremediation Of Uranium In; Shallow Alluvial Aquifers; Shallow Alluvial Aquifers; S. B. Yabusaki; Y. Fang; S. R. Waichler; P. E. Long

120

Prepared  

E-Print Network [OSTI]

The demand for energy continues to grow in North America. Canada plays a key role in balancing the demand and supply requirements. As the conventional oil reserves are declining in the world, there will be an ever-growing need for exploring the oil resources at remote locations including the vast oil sands deposits in the Athabasca region of northern Alberta and deep water. This paper will present an overview of Canada’s conventional oil, oil sands and offshore industry, with primary focus on current production levels, future production forecasts, pipeline issues, and current and potential markets. BUEC 663: NRE Capstone-Group Project

Kaleem Shakir; Mohammed Riaz; Jacob Oommachan

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


121

Preparation and Analysis of Biomass Lignins  

SciTech Connect (OSTI)

Lignin, comprised primarily of three randomly polymerized phenylpropenyl monomers, is, arguably, the second most common organic molecule on earth. In current biorefinery applications, lignin is burned, usually in concentrated pulping or hydrolysis liquor, as a source of process steam and both internal and exported electricity. The aromatic content of lignin makes it a potentially attractive feedstock for highly-valued aromatic chemicals, polymers, and carbon products (graphite, activated carbon, and carbon fiber). Revenue from production of lignin-based chemicals could play a major role in biorefinery profitability if cost-effective methods for lignin separation and purification can be developed. This article presents descriptions of methods for assessing and purifying biorefinery lignins so that they can be evaluated for use as feedstocks for production of chemical products. Areas covered are: 1) initial evaluations of as-received lignin samples (visual, microscopic, separable organics), 2) analysis of common contaminants (bulk and filterable ash and particulate contaminants in liquid and dry lignin samples), 3) preparation of lignins for experimental use as chemical feedstocks (prefiltration, filtration using bench-scale chemical apparatus and larger scale bag filters, one-step lignin precipitation, two-step carbohydrate and lignin precipitation, desalting of dry powdered or precipitated lignin, and lyophilization). These methods have been used successfully at bench-scale to produce the 1 50 kg amounts of wood and grass lignins typically required for bench-scale assessment as chemical feedstocks

Compere, A L [ORNL; Griffith, William {Bill} L [ORNL

2009-01-01T23:59:59.000Z

122

ARTIFACT FORMATION DURING NEUTRALIZATION OF TANK 50 SAMPLES  

SciTech Connect (OSTI)

Degradation products have been identified in the extracts of Tank 50 samples analyzed by semivolatile organic compound analysis (SVOA) using gas chromatography/mass spectrometry (GC/MS). These materials, identified as short chain alkyl alcohols, were formed by acidification during sample preparation. A number of questions were raised about the formation of these and other materials reported in Tank 50 surface samples, and this report serves to address these questions.

Crump, S.; Young, J.

2014-08-01T23:59:59.000Z

123

Preparation of superconductor precursor powders  

DOE Patents [OSTI]

A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic and/or reduced particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of all metals in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products.

Bhattacharya, Raghunath (Littleton, CO)

1998-01-01T23:59:59.000Z

124

Method for preparing ceramic composite  

DOE Patents [OSTI]

A process is disclosed for preparing ceramic composite comprising blending TiC particulates, Al{sub 2}O{sub 3} particulates and nickel aluminide and consolidating the mixture at a temperature and pressure sufficient to produce a densified ceramic composite having fracture toughness equal to or greater than 7 MPa m{sup 1/2}, a hardness equal to or greater than 18 GPa. 5 figs.

Alexander, K.B.; Tiegs, T.N.; Becher, P.F.; Waters, S.B.

1996-01-09T23:59:59.000Z

125

Method for preparing ceramic composite  

DOE Patents [OSTI]

A process for preparing ceramic composite comprising blending TiC particulates, Al.sub.2 O.sub.3 particulates and nickle aluminide and consolidating the mixture at a temperature and pressure sufficient to produce a densified ceramic composite having fracture toughness equal to or greater than 7 MPa m.sup.1/2, a hardness equal to or greater than 18 GPa.

Alexander, Kathleen B. (Oak Ridge, TN); Tiegs, Terry N. (Lenoir City, TN); Becher, Paul F. (Oak Ridge, TN); Waters, Shirley B. (Knoxville, TN)

1996-01-01T23:59:59.000Z

126

The preparation of phosphine tellurides  

E-Print Network [OSTI]

THE PREPARATION OF PHOSPHINE TELLURIDES A Thesis Brian Howard Steeves Submitted to the Graduate C o lie ge of the Texas A@M University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE January 1965 Major Subject...: Chemistry THE PRKPARATLGN GF PHGSPHINE TELLUREDKS Brian Howard Steeves Approved as to style and content by: (Chairman of Com itte ) (Member) (Head of Dep r nt) (Member (Member) (Mem r) January 1965 ACKNOWLEDGMENT I would like to express my sincere...

Steeves, Brian Howard

2012-06-07T23:59:59.000Z

127

Preparation of high purity vanadium  

SciTech Connect (OSTI)

The paper reviews the various reduction and refining methods that have been used to prepare vanadium metal. Earlier work on metallothermic and carbothermic reduction processes is discussed. Recent work on improving the scaling up the aluminothermic reduction process is described in detail. Iron and silicon are first removed from commercial V/sub 2/O/sub 5/ by an ion exchange separation technique and the purified oxide is then exothermically reduced with aluminum metal. The resulting V-Al ingot is heated in a vacuum to 1700/sup 0/C to remove the aluminum and dissolved oxygen, and the sponge is then electron-beam melted to remove residual volatile impurities to yield vanadium metal of 99.98% purity. Precautions taken during each processing stage to minimize carbon, nitrogen and oxygen contamination are described. Metal containing < 50 ppmw each of C, N and O, < 20 ppmw Si, and < 10 ppmw of Fe and Al has been prepared in kilogram quantities by this method. The hardness of the beam melted is 60 to 70 DPH. Experiments designed to scale up the reduction process and to increase the efficiency of the separation and melting steps are described. Various refining techniques that have been applied to the preparation of high purity vanadium are described and comparisons made between the quality of metal obtained by each.

Carlson, O.N.; Burkholder, H.R.; Martsching, G.A.; Schmidt, F.A.

1981-01-01T23:59:59.000Z

128

ESPC IDIQ Contract Sample  

Broader source: Energy.gov [DOE]

Document displays a sample indefinite delivery, indefinite quantity (IDIQ) energy savings performance contract (ESPC).

129

Performance evaluation soil samples utilizing encapsulation technology  

DOE Patents [OSTI]

Performance evaluation soil samples and method of their preparation uses encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration. 1 fig.

Dahlgran, J.R.

1999-08-17T23:59:59.000Z

130

Performance evaluation soil samples utilizing encapsulation technology  

DOE Patents [OSTI]

Performance evaluation soil samples and method of their preparation using encapsulation technology to encapsulate analytes which are introduced into a soil matrix for analysis and evaluation by analytical laboratories. Target analytes are mixed in an appropriate solvent at predetermined concentrations. The mixture is emulsified in a solution of polymeric film forming material. The emulsified solution is polymerized to form microcapsules. The microcapsules are recovered, quantitated and introduced into a soil matrix in a predetermined ratio to form soil samples with the desired analyte concentration.

Dahlgran, James R. (Idaho Falls, ID)

1999-01-01T23:59:59.000Z

131

Stormwater Pollution Prevention Plan Prepared by  

E-Print Network [OSTI]

Stormwater Pollution Prevention Plan Prepared by: Environment, Health, Safety, and Security .....................................................16 3.0 Potential Sources of Pollution

Eisen, Michael

132

PREPARED FOR: The National Renewable Energy Laboratory  

E-Print Network [OSTI]

Wind and solar integration study May 2010 Prepared for NREL by GE Energy 1 River Road Schenectady, New York 12345PREPARED FOR: The National Renewable Energy Laboratory A national laboratory of the U.S. Department of Energy PREPARED BY: GE Energy MAY 2010 WESTERNWIND AND SOLAR INTEGRATION STUDY #12;#12;Western

133

Rain sampling device  

DOE Patents [OSTI]

The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of the precipitation from the chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device. 11 figures.

Nelson, D.A.; Tomich, S.D.; Glover, D.W.; Allen, E.V.; Hales, J.M.; Dana, M.T.

1991-05-14T23:59:59.000Z

134

Rain sampling device  

DOE Patents [OSTI]

The present invention constitutes a rain sampling device adapted for independent operation at locations remote from the user which allows rainfall to be sampled in accordance with any schedule desired by the user. The rain sampling device includes a mechanism for directing wet precipitation into a chamber, a chamber for temporarily holding the precipitation during the process of collection, a valve mechanism for controllably releasing samples of said precipitation from said chamber, a means for distributing the samples released from the holding chamber into vessels adapted for permanently retaining these samples, and an electrical mechanism for regulating the operation of the device.

Nelson, Danny A. (Richland, WA); Tomich, Stanley D. (Richland, WA); Glover, Donald W. (Prosser, WA); Allen, Errol V. (Benton City, WA); Hales, Jeremy M. (Kennewick, WA); Dana, Marshall T. (Richland, WA)

1991-01-01T23:59:59.000Z

135

Chapter 6 List of Preparers  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on Delicious Rank EERE:YearRound-Up fromDepartmentTieCelebrate Earth Day with SecretaryDerivedof&6. LIST OF PREPARERS

136

Procedures for sampling radium-contaminated soils  

SciTech Connect (OSTI)

Two procedures for sampling the surface layer (0 to 15 centimeters) of radium-contaminated soil are recommended for use in remedial action projects. Both procedures adhere to the philosophy that soil samples should have constant geometry and constant volume in order to ensure uniformity. In the first procedure, a ''cookie cutter'' fashioned from pipe or steel plate, is driven to the desired depth by means of a slide hammer, and the sample extracted as a core or plug. The second procedure requires use of a template to outline the sampling area, from which the sample is obtained using a trowel or spoon. Sampling to the desired depth must then be performed incrementally. Selection of one procedure over the other is governed primarily by soil conditions, the cookie cutter being effective in nongravelly soils, and the template procedure appropriate for use in both gravelly and nongravelly soils. In any event, a minimum sample volume of 1000 cubic centimeters is recommended. The step-by-step procedures are accompanied by a description of the minimum requirements for sample documentation. Transport of the soil samples from the field is then addressed in a discussion of the federal regulations for shipping radioactive materials. Interpretation of those regulations, particularly in light of their application to remedial action soil-sampling programs, is provided in the form of guidance and suggested procedures. Due to the complex nature of the regulations, however, there is no guarantee that our interpretations of them are complete or entirely accurate. Preparation of soil samples for radium-226 analysis by means of gamma-ray spectroscopy is described.

Fleischhauer, H.L.

1985-10-01T23:59:59.000Z

137

Electrochemical Behavior and Li Diffusion Study of LiCoO? Thin Film Electrodes Prepared by PLD  

E-Print Network [OSTI]

Preferred c-axis oriented LiCoO? thin films were prepared on the SiO?/Si (SOS) substrates by pulsed laser deposition (PLD). Thin film electrodes without carbon and binder are ideal samples to study the electrochemical ...

Xia, H.

138

COMPUTER SCIENCE SAMPLE PROGRAM  

E-Print Network [OSTI]

COMPUTER SCIENCE SAMPLE PROGRAM (First Math Course MATH 198) This sample program suggests one way CS 181: Foundations of Computer Science II CS 180: Foundations of Computer Science I CS 191

Gering, Jon C.

139

Preparation of superconductor precursor powders  

DOE Patents [OSTI]

A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic and/or reduced particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of all metals in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products. 7 figs.

Bhattacharya, R.

1998-08-04T23:59:59.000Z

140

Preparation of superconductor precursor powders  

DOE Patents [OSTI]

A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals, such as nitrate salts of thallium, barium, calcium, and copper, which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of thallium in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products.

Bhattacharya, Raghunath (Littleton, CO); Blaugher, Richard D. (Evergreen, CO)

1995-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

Preparation of hydrophobic organic aeorgels  

DOE Patents [OSTI]

Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.

Baumann, Theodore F. (Tracy, CA); Satcher, Jr., Joe H. (Patterson, CA); Gash, Alexander E. (Livermore, CA)

2007-11-06T23:59:59.000Z

142

Preparation of hydrophobic organic aeorgels  

DOE Patents [OSTI]

Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.

Baumann, Theodore F.; Satcher Jr., Joe H.; Gash, Alexander E.

2004-10-19T23:59:59.000Z

143

CHARACTERIZATION OF CORE SAMPLE COLLECTED FROM THE SALTSTONE DISPOSAL FACILITY  

SciTech Connect (OSTI)

During the month of September 2008, grout core samples were collected from the Saltstone Disposal Facility, Vault 4, cell E. This grout was placed during processing campaigns in December 2007 from Deliquification, Dissolution and Adjustment Batch 2 salt solution. The 4QCY07 Waste Acceptance Criteria sample collected on 11/16/07 represents the salt solution in the core samples. Core samples were retrieved to initiate the historical database of properties of emplaced Saltstone and to demonstrate the correlation between field collected and laboratory prepared samples. Three samples were collected from three different locations. Samples were collected using a two-inch diameter concrete coring bit. In April 2009, the core samples were removed from the evacuated sample container, inspected, transferred to PVC containers, and backfilled with nitrogen. Samples furthest from the wall were the most intact cylindrically shaped cored samples. The shade of the core samples darkened as the depth of coring increased. Based on the visual inspection, sample 3-3 was selected for all subsequent analysis. The density and porosity of the Vault 4 core sample, 1.90 g/cm{sup 3} and 59.90% respectively, were comparable to values achieved for laboratory prepared samples. X-ray diffraction analysis identified phases consistent with the expectations for hydrated Saltstone. Microscopic analysis revealed morphology features characteristic of cementitious materials with fly ash and calcium silicate hydrate gel. When taken together, the results of the density, porosity, x-ray diffraction analysis and microscopic analysis support the conclusion that the Vault 4, Cell E core sample is representative of the expected waste form.

Cozzi, A.; Duncan, A.

2010-01-28T23:59:59.000Z

144

Preparation and characterization of gradient polymer films  

SciTech Connect (OSTI)

Gradient polymers are multicomponent polymers whose chemical constitution varies with depth in the sample. Although these polymers may possess unique mechanical, optical, and barrier properties they remain relatively unexplored. This work is a study of the preparation of gradient polymers by sequential exposure of films to a diffusing monomer followed by electron beam irradiation. Initial experiments involved immersion of poly(vinyl chloride) (PVC) films in styrene or n-butyl methacrylate (BMA) for various time periods followed by irradiation with 1 or 10 megarads of accelerated electrons. A significant amount of poly(n-butyl methacrylate) (PBMA) formed in PVC/BMA systems, but little polystyrene could be found in the PVC/styrene films. A second set of experiments involved immersion of PVC and polyethylene (PE) films in BMA for 20, 40, 60, and 720 minutes followed by irradiation with 10 megarads of electrons. These films were then characterized using optical microscopy, quantitative transmission Fourier transform infrared spectroscopy (FTIR), and a depth profiling procedure based on quantitative attenuated total reflection (ATR) FTIR. It was concluded that the mechanism of PBMA formation in the polyethylene films was a result of events immediately following irradiation. Atmospheric oxygen diffusing into irradiated films trapped free radicals at the film surfaces. This was followed by storage in an evacuated desiccator where unintentional exposure to BMA vapor took place. This BMA reacted with free radicals that remained within the film cores, polymerizing to PBMA.

Smith, S.C.

1987-01-01T23:59:59.000Z

145

NREL Develops Accelerated Sample Activation Process for Hydrogen Storage Materials (Fact Sheet)  

SciTech Connect (OSTI)

This fact sheet describes NREL's accomplishments in developing a new sample activation process that reduces the time to prepare samples for measurement of hydrogen storage from several days to five minutes and provides more uniform samples. Work was performed by NREL's Chemical and Materials Science Center.

Not Available

2010-12-01T23:59:59.000Z

146

GUM Analysis for TIMS Isotopic Ratios in BEP0 Graphite Qualification Samples, Round 2  

SciTech Connect (OSTI)

In May 2007, one set of three samples from NBL were addressed to Steve Petersen for TIMS analysis, and included BEP0 samples numbered 27008, 30986, and 50846. All cores were trimmed by tooling, and lightly cleaned by CO2 pellet blasting. Small discs were cut from the second set of samples for SIMS analysis, with the remainder of each used for TIMS preparation.

Gerlach, David C.; Heasler, Patrick G.; Reid, Bruce D.

2009-01-01T23:59:59.000Z

147

Nature Methods Minimalistic encapsulated proteomic sample processing applied to copy number  

E-Print Network [OSTI]

Nature Methods Minimalistic encapsulated proteomic sample processing applied to copy number Supplementary Figure 1 Comparison of SILAC-based ratios using different sample processing conditions steps of the iST sample preparation workflow. It further shows how to troubleshoot the method in case

Cai, Long

148

Sample Desorption/Onization From Mesoporous Silica  

DOE Patents [OSTI]

Mesoporous silica is shown to be a sample holder for laser desorption/ionization of mass spectrometry. Supported mesoporous silica was prepared by coating an ethanolic silicate solution having a removable surfactant onto a substrate to produce a self-assembled, ordered, nanocomposite silica thin film. The surfactant was chosen to provide a desired pore size between about 1 nanometer diameter and 50 nanometers diameter. Removal of the surfactant resulted in a mesoporous silica thin film on the substrate. Samples having a molecular weight below 1000, such as C.sub.60 and tryptophan, were adsorbed onto and into the mesoporous silica thin film sample holder and analyzed using laser desorption/ionization mass spectrometry.

Iyer, Srinivas (Los Alamos, NM); Dattelbaum, Andrew M. (Los Alamos, NM)

2005-10-25T23:59:59.000Z

149

PREPARING FOR A SUCCESSFUL EVMS CERTIFICATION  

SciTech Connect (OSTI)

The client, a government agency, requires its contractor to obtain an Earned Value Management System (EVMS) certification that meets the intent of ANSI/EIA-748-B, Earned Value Management Systems. The contractor has extensive experience with certification preparation, having completed two certifications within two years. Information from a previous EVMS certification and internal system surveillances are used to prepare for client-based EVMS certifications and bi-annual surveillances. The contractor also sent members of its group to assist other companies preparing for surveillances and certifications to perform 'Black Hat Reviews.' This paper is a lessons learned on preparing a team for EVMS certification. The information is also applicable for surveillances, since the contractor prepares its team for the surveillance in the same manner as the initial certification. Some of the areas covered include required documents, tracing the data through the systems, Control Account Manager (CAM) preparation, and system verification.

CROWE SL; BASCHE AD

2011-02-09T23:59:59.000Z

150

Sampled data lattice filters  

E-Print Network [OSTI]

SAMPLED DATA LATTICE FILTERS A Thesis by WILLIAM TERRY THRIFT III Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirements for the degree of MASTER OF SCIENCE December 1979 Major Subfect...: Electrical Engineering SAMPLED DATA LATTICE FILTERS A Thesis by WILLIAM TERRY THRIFT III Approved as to style and content by: (Chair an of Committee) (Hea f Department) (Member) (Member) (Member) (Member) December 1979 ABSTRACT Sampled Data...

Thrift, William Terry

1980-01-01T23:59:59.000Z

151

Synthesis and Optical Properties of Sulfide Nanoparticles Prepared...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Optical Properties of Sulfide Nanoparticles Prepared in Dimethylsulfoxide. Synthesis and Optical Properties of Sulfide Nanoparticles Prepared in Dimethylsulfoxide. Abstract: Many...

152

Preparing for Project Implementation Assigning Accountability...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Assigning Accountability for Each Project, April 14, 2010 Preparing for Project Implementation Assigning Accountability for Each Project, April 14, 2010 Assigning Accountability...

153

Document prepared by APIC Bioterrorism Task Force  

E-Print Network [OSTI]

ATTACHMENT Document prepared by APIC Bioterrorism Task Force Judith F. English, Mae Y. Cundiff of civilian populations not recommended. 3. Infection Control Practices for Patient Management Symptomatic

Oliver, Douglas L.

154

Cold Dissolved Saltcake Waste Simulant Development, Preparation, and Analysis  

SciTech Connect (OSTI)

CH2M HILL Hanford Group, Inc. is identifying and developing supplemental process technologies to accelerate the Hanford tank waste cleanup mission. Bulk vitrification, containerized grout, and steam reforming are three technologies under consideration for treatment of the radioactive saltcake wastes in 68 single-shell tanks. To support development and testing of these technologies, Pacific Northwest National Laboratory (PNNL) was tasked with developing a cold dissolved saltcake simulant formulation to be representative of an actual saltcake waste stream, preparing 25- and 100-L batches of the simulant, and analyzing the composition of the batches to ensure conformance to formulation targets. Lacking a defined composition for dissolved actual saltcake waste, PNNL used available tank waste composition information and an equilibrium chemistry model (Environmental Simulation Program [ESP{trademark}]) to predict the concentrations of analytes in solution. Observations of insoluble solids in initial laboratory preparations for the model-predicted formulation prompted reductions in the concentration of phosphate and silicon in the final simulant formulation. The analytical results for the 25- and 100-L simulant batches, prepared by an outside vendor to PNNL specifications, agree within the expected measurement accuracy ({approx}10%) of the target concentrations and are highly consistent for replicate measurements, with a few minor exceptions. In parallel with the production of the 2nd simulant batch (100-L), a 1-L laboratory control sample of the same formulation was carefully prepared at PNNL to serve as an analytical standard. The instrumental analyses indicate that the vendor prepared batches of solution adequately reflect the as-formulated simulant composition. In parallel with the simulant development effort, a nominal 5-M (molar) sodium actual waste solution was prepared at the Hanford Site from a limited number of tank waste samples. Because this actual waste solution w as also to be used for testing the supplemental treatment technologies, the modeled simulant formulation was predicated on the composite of waste samples used to prepare it. Subsequently, the actual waste solution was filtered and pretreated to remove radioactive cesium at PNNL and then analyzed using the same instrumentation and procedures applied to the simulant samples. The overall agreement of measured simulant and actual waste solution compositions is better than {+-}10% for the most concentrated species including sodium, nitrate, hydroxide, carbonate, and nitrite. While the magnitude of the relative difference in the simulant and actual waste composition is large (>20% difference) for a few analytes (aluminum, chromium, fluoride, potassium, and total organic carbon), the absolute differences in concentration are in general not appreciable. Our evaluation is that these differences in simulant and actual waste solutions should have a negligible impact on bulk vitrification and containerized grout process testing, while the impact of the low aluminum concentration on steam reforming is yet to be determined.

Rassat, Scot D.; Mahoney, Lenna A.; Russell, Renee L.; Bryan, Samuel A.; Sell, Rachel L.

2003-05-13T23:59:59.000Z

155

E-Print Network 3.0 - alternative nuclear energy Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Powered by Explorit Topic List Advanced Search Sample search results for: alternative nuclear energy Page: << < 1 2 3 4 5 > >> 1 Preparing Non-nuclear Engineers for the Nuclear...

156

Process for preparing energetic materials  

DOE Patents [OSTI]

Sol-gel chemistry is used for the preparation of energetic materials (explosives, propellants and pyrotechnics) with improved homogeneity, and/or which can be cast to near-net shape, and/or made into precision molding powders. The sol-gel method is a synthetic chemical process where reactive monomers are mixed into a solution, polymerization occurs leading to a highly cross-linked three dimensional solid network resulting in a gel. The energetic materials can be incorporated during the formation of the solution or during the gel stage of the process. The composition, pore, and primary particle sizes, gel time, surface areas, and density may be tailored and controlled by the solution chemistry. The gel is then dried using supercritical extraction to produce a highly porous low density aerogel or by controlled slow evaporation to produce a xerogel. Applying stress during the extraction phase can result in high density materials. Thus, the sol-gel method can be used for precision detonator explosive manufacturing as well as producing precision explosives, propellants, and pyrotechnics, along with high power composite energetic materials.

Simpson, Randall L. (Livermore, CA); Lee, Ronald S. (Livermore, CA); Tillotson, Thomas M. (Tracy, CA; , Hrubesh, Lawrence W. (Pleasanton, CA); Swansiger, Rosalind W. (Livermore, CA); Fox, Glenn A. (Livermore, CA)

2011-12-13T23:59:59.000Z

157

November 21, 2000 PV Lesson Plan 2 Sample Questions & Answers  

E-Print Network [OSTI]

November 21, 2000 PV Lesson Plan 2 ­ Sample Questions & Answers Prepared for the Oregon Million Solar Roofs Coalition By Frank Vignola ­ University of Oregon Solar Radiation Monitoring Lab John Hocken your understanding: 1. The typical voltage of a silicon solar cell is about 0.5 volts; where does

Oregon, University of

158

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING FINAL REPORT  

E-Print Network [OSTI]

REVIEW OF DIESEL PARTICULATE MATTER SAMPLING METHODS FINAL REPORT Prepared by David B. Kittelson of Mechanical Engineering Center for Diesel Research Minneapolis, MN January 14, 1999 #12;01/14/99 Page 2 TABLE ................................................................................................................5 DIESEL ENGINE TECHNOLOGY AND EMISSION REGULATIONS .............................7 PHYSICAL

Minnesota, University of

159

Rehabilitation Services Sample Occupations  

E-Print Network [OSTI]

/Industries Correction Agencies Drug Treatment Centers Addiction Counselor Advocacy Occupations Art Therapist BehavioralRehabilitation Services Sample Occupations Sample Work Settings Child & Day Care Centers Clinics................................ IIB 29-1000 E4 Careers in Counseling and Human Services .........IIB 21-1010 C7 Careers in Health Care

Ronquist, Fredrik

160

Sampling system and method  

DOE Patents [OSTI]

The present disclosure provides an apparatus and method for coupling conduit segments together. A first pump obtains a sample and transmits it through a first conduit to a reservoir accessible by a second pump. The second pump further conducts the sample from the reservoir through a second conduit.

Decker, David L.; Lyles, Brad F.; Purcell, Richard G.; Hershey, Ronald Lee

2013-04-16T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

Biological sample collector  

DOE Patents [OSTI]

A biological sample collector is adapted to a collect several biological samples in a plurality of filter wells. A biological sample collector may comprise a manifold plate for mounting a filter plate thereon, the filter plate having a plurality of filter wells therein; a hollow slider for engaging and positioning a tube that slides therethrough; and a slide case within which the hollow slider travels to allow the tube to be aligned with a selected filter well of the plurality of filter wells, wherein when the tube is aligned with the selected filter well, the tube is pushed through the hollow slider and into the selected filter well to sealingly engage the selected filter well and to allow the tube to deposit a biological sample onto a filter in the bottom of the selected filter well. The biological sample collector may be portable.

Murphy, Gloria A. (French Camp, CA)

2010-09-07T23:59:59.000Z

162

Preparation and characterization of boro-tellurite glasses  

SciTech Connect (OSTI)

Glass samples of the system: xB{sub 2}O{sub 3}?(100?x) TeO{sub 2}; x= 15, 20, 25 and 30 mol% were prepared by melt quenching and characterized by X-ray diffraction, density measurements, Differential Scanning Calorimetry and FTIR spectroscopy. XRD confirmed the amorphous structure of all samples. Density of glasses decreased with increase in B{sub 2}O{sub 3} concentration due to the replacement of heavier TeO{sub 2} with lighter B{sub 2}O{sub 3} whereas the glass transition temperature increased from 339°C to 366°C; the later effect was due to increase in the concentration of stronger B-O bonds in the glass network. FTIR studies found that BO{sub 4} units convert into BO{sub 3} with the addition of B{sub 2}O{sub 3}.

Kaur, Nirmal, E-mail: akphysics@yahoo.com; Khanna, Atul, E-mail: akphysics@yahoo.com [Glass Physics and Sensors Laboratory, Department of Physics, Guru Nanak Dev University, Amritsar-143005, Punjab (India); Krishna, P. S. R. [Solid State Physics Division, Bhabha Atomic Research Centre, Mumbai-400085, Maharashtra (India)

2014-04-24T23:59:59.000Z

163

Method and apparatus for automated processing and aliquoting of whole blood samples for analysis in a centrifugal fast analyzer  

DOE Patents [OSTI]

A rotor and disc assembly for use in a centrifugal fast analyzer. The assembly is designed to process multiple samples of whole blood followed by aliquoting of the resultant serum into precisely measured samples for subsequent chemical analysis. The assembly requires minimal operator involvement with no mechanical pipetting. The system comprises: (1) a whole blood sample disc; (2) a serum sample disc; (3) a sample preparation rotor; and (4) an analytical rotor. The blood sample disc and serum sample disc are designed with a plurality of precision bore capillary tubes arranged in a spoked array. Samples of blood are loaded into the blood sample disc by capillary action and centrifugally discharged into cavities of the sample preparation rotor where separation of serum and solids is accomplished. The serum is loaded into the capillaries of the serum sample disc by capillary action and subsequently centrifugally expelled into cuvettes of the analyticaly rotor for conventional methods. 5 figs.

Burtis, C.A.; Johnson, W.F.; Walker, W.A.

1985-08-05T23:59:59.000Z

164

PREPARATION OF A DRY PRODUCT FROM CONDENSED  

E-Print Network [OSTI]

PREPARATION OF A DRY PRODUCT FROM CONDENSED MENHADEN SOLUBLES Statistical Supplement WOODS HOI CONDENSED MENHADEN SOLUBLES: STATISTICAL ANALYSIS OF THE DATA (Supplement to the Fish and Wildlife Service. Fish and Wildlife Service Research Report k^, Preparation of a Dry Product from Condensed Menhaden

165

NOTICE OF PREPARATION: DRAFT ENVIRONMENTAL IMPACT REPORT  

E-Print Network [OSTI]

NOTICE OF PREPARATION: DRAFT ENVIRONMENTAL IMPACT REPORT DATE: September 25, 2013 TO: Responsible (Trustees) will be the lead agency for the preparation of an environmental impact report (EIR to: CSU Board of Trustees c/o Nicole Carter, Senior Planner SWCA Environmental Consultants 1422

Sze, Lawrence

166

Energy Audit Procedures Prepared for the  

E-Print Network [OSTI]

Energy Audit Procedures Prepared for the U.S. Department of Energy Office of Electricity Delivery Subtask 3.5.1: Residential Energy Efficiency Deliverable 1 Prepared by The University of Hawai or reflect those of the United States Government or any agency thereof. #12;Project Report 1: Energy Audit

167

Preparation of irregular mesoporous hydroxyapatite  

SciTech Connect (OSTI)

An irregular mesoporous hydroxyapatite (meso-HA), Ca{sub 10}(PO{sub 4}){sub 6}(OH){sub 2}, is successfully prepared from Ca(NO{sub 3}){sub 2}.4H{sub 2}O and NH{sub 4}H{sub 2}PO{sub 4} using surfactant cetyltrimethyl ammonium bromide (CTAB) as template. Fourier transform infrared spectroscopy (FTIR) and differential scanning calorimetry (DSC) results reveal that the positive head of CTAB is assembled on the surface precipitated HA and much NH{sub 4}{sup +} is enclosed in precipitated HA before calcination. Field scanning electron microscope (FSEM) reveals that there exist many interconnected pores throughout the HA reticular skeleton. Nitrogen adsorption-desorption experiment exhibits a mesoporous material type IV curve, and pore size distribution calculated from the desorption branch of the isotherms based on Barrett-Joyner-Halenda (BJH) model shows that most pores throughout the HA reticular skeleton are sized at about 40 nm, but the pores are not uniform on the whole, owning to decomposition of the 'organic' CTAB templating structures and ammonium salt enclosed in the precipitated HA. The specific surface area of irregular meso-HA is calculated to be 37.6 m{sup 2}/g according to the Brunauer-Emmett-Teller (BET) equation. Moreover, after polylactic acid/meso-HA (PLA/meso-HA) composites degraded 12 weeks in normal saline at 37 deg. C, the interconnected pores throughout the HA skeleton were enlarged and sized in micron degree, which resemble trabecular bone structure very much.

Wang Hualin [School of Chemical Technology, Hefei University of Technology, Hefei, Anhui 230009 (China)], E-mail: hlwang@hfut.edu.cn; Zhai Linfeng; Li Yanhong; Shi Tiejun [School of Chemical Technology, Hefei University of Technology, Hefei, Anhui 230009 (China)

2008-06-03T23:59:59.000Z

168

Waste classification sampling plan  

SciTech Connect (OSTI)

The purpose of this sampling is to explain the method used to collect and analyze data necessary to verify and/or determine the radionuclide content of the B-Cell decontamination and decommissioning waste stream so that the correct waste classification for the waste stream can be made, and to collect samples for studies of decontamination methods that could be used to remove fixed contamination present on the waste. The scope of this plan is to establish the technical basis for collecting samples and compiling quantitative data on the radioactive constituents present in waste generated during deactivation activities in B-Cell. Sampling and radioisotopic analysis will be performed on the fixed layers of contamination present on structural material and internal surfaces of process piping and tanks. In addition, dose rate measurements on existing waste material will be performed to determine the fraction of dose rate attributable to both removable and fixed contamination. Samples will also be collected to support studies of decontamination methods that are effective in removing the fixed contamination present on the waste. Sampling performed under this plan will meet criteria established in BNF-2596, Data Quality Objectives for the B-Cell Waste Stream Classification Sampling, J. M. Barnett, May 1998.

Landsman, S.D.

1998-05-27T23:59:59.000Z

169

Sample storage/disposal study  

SciTech Connect (OSTI)

Radioactive waste from defense operations has accumulated at the Hanford Site`s underground waste tanks since the late 1940`s. Each tank must be analyzed to determine whether it presents any harm to the workers at the Hanford Site, the public or the environment. Analyses of the waste aids in the decision making process in preparation of future tank waste stabilization procedures. Characterization of the 177 waste tanks on the Hanford Site will produce a large amount of archived material. This also brings up concerns as to how the excess waste tank sample material from 325 and 222-S Analytical Laboratories will be handled. Methods to archive and/or dispose of the waste have been implemented into the 222-S and 325 Laboratory procedures. As the amount of waste characterized from laboratory analysis grows, an examination of whether the waste disposal system will be able to compensate for this increase in the amount of waste needs to be examined. Therefore, the need to find the safest, most economically sound method of waste storage/disposal is important.

Valenzuela, B.D.

1994-09-29T23:59:59.000Z

170

Elimination of ``memory`` from sample handling and inlet system of a mass spectrometer  

DOE Patents [OSTI]

This paper describes a method for preparing the sample handling and inlet system of a mass spectrometer for analysis of a subsequent sample following analysis of a previous sample comprising the flushing of the system interior with supercritical CO{sub 2} and venting the interior. The method eliminates the effect of system ``memory`` on the subsequent analysis, especially following persistent samples such as xenon and krypton.

Chastgner, P.

1991-05-08T23:59:59.000Z

171

A Sensitive Determination of Iodine Species, Including Organoiodine, for Freshwater and Seawater Samples Using High Performance Liquid Chromatography and Spectrophotometric Detection  

E-Print Network [OSTI]

, with minimal sample preparation, compared to existing methods. The method has been successfully applied to determine iodide, iodate as the difference of total inorganic iodide and iodide after reduction of the sample, and organic iodine as the difference...

Schwehr, K. A.; Santschi, P. H.

172

Ninth annual coal preparation, utilization, and environmental control contractors conference: Proceedings  

SciTech Connect (OSTI)

Papers are grouped under the following sessions: compliance technology; high-efficiency preparation; characterization; advanced technologies; alternative fuels; coal utilization; industrial/commercial combustor development; combustion; superclean emission systems; carbon dioxide recovery and reuse; air toxics and fine particulates; air toxics sampling and analysis workshop; and combined poster session. Selected papers have been processed separately for inclusion in the Energy Science and Technology Database.

Not Available

1993-09-01T23:59:59.000Z

173

A Method for the Preparation of NIST Traceable Fossil Fuel Standards with Concentrations  

E-Print Network [OSTI]

at NIST with high accuracy and precision by isotope dilution thermal ionization mass spectrometry and quality control test samples. Unlike calibrants prepared from high purity components, this method enables Abbreviations M bar Calculated concentration of mixture EDXRF Energy Dispersive X-Ray Fluorescence n number

174

Prepare for Exam I Aug. 16. 10:50-12:05  

E-Print Network [OSTI]

problems such as the reliability of a system. Be prepared for Ch 3: (1) Know the definitions of random) Know the definitions of sample space, event, probability, and distribution. (2) Be able to use variable. (2) Be able to find discrete distributions for certain probability models. (3) Be able to find

Zhang, Yu

175

Preparation of a Data Management Plan, Development of the Data Pipeline, and Efficient Archiving  

E-Print Network [OSTI]

Preparation of a Data Management Plan, Development of the Data Pipeline, and Efficient Archiving quality data archive is produced, design archive production into the instrument data pipeline, use PDS major archive design milestones, early generation of sample data, peer review of the pipeline

Waliser, Duane E.

176

Natural Radioactivity of Boron Added Clay Samples  

SciTech Connect (OSTI)

Clay, consisting fine-grained minerals, is an interesting materials and can be used in a variety of different fields especially in dermatology application. Using clay such a field it is important to measure its natural radioactivity. Thus the purpose of this study is to measure {sup 226}Ra, {sup 232}Th and {sup 40}K concentration in clay samples enriched with boron. Three different types of clay samples were prepared where boron is used in different rate. The measurements have been determined using a gamma-ray spectrometry consists of a 3''x3'' NaI(Tl) detector. From the measured activity the radium equivalent activities (Ra{sub eq}), external hazard index (H{sub ex}), absorbed dose rate in air (D) and annual effective dose (AED) have also been obtained.

Akkurt, I.; Guenoglu, K. [Sueleyman Demirel University, Faculty of Arts and Sciences, Dept. of Physics, Isparta (Turkey); Canakcii, H. [Gaziantep University, Engineering Faculty, Civil Engineering Dept., Gaziantep (Turkey); Mavi, B. [Amasya University, Faculty of Arts and Sciences, Dept. of Physics, Amasya (Turkey)

2011-12-26T23:59:59.000Z

177

Water Sample Concentrator  

ScienceCinema (OSTI)

Automated portable device that concentrates and packages a sample of suspected contaminated water for safe, efficient transport to a qualified analytical laboratory. This technology will help safeguard against pathogen contamination or chemical and biolog

Idaho National Laboratory

2010-01-08T23:59:59.000Z

178

Dissolution actuated sample container  

DOE Patents [OSTI]

A sample collection vial and process of using a vial is provided. The sample collection vial has an opening secured by a dissolvable plug. When dissolved, liquids may enter into the interior of the collection vial passing along one or more edges of a dissolvable blocking member. As the blocking member is dissolved, a spring actuated closure is directed towards the opening of the vial which, when engaged, secures the vial contents against loss or contamination.

Nance, Thomas A.; McCoy, Frank T.

2013-03-26T23:59:59.000Z

179

SAMPLING AND ANALYSIS PROTOCOLS  

SciTech Connect (OSTI)

Radiological sampling and analyses are performed to collect data for a variety of specific reasons covering a wide range of projects. These activities include: Effluent monitoring; Environmental surveillance; Emergency response; Routine ambient monitoring; Background assessments; Nuclear license termination; Remediation; Deactivation and decommissioning (D&D); and Waste management. In this chapter, effluent monitoring and environmental surveillance programs at nuclear operating facilities and radiological sampling and analysis plans for remediation and D&D activities will be discussed.

Jannik, T; P Fledderman, P

2007-02-09T23:59:59.000Z

180

Liquid sampling system  

DOE Patents [OSTI]

A conduit extends from a reservoir through a sampling station and back to the reservoir in a closed loop. A jet ejector in the conduit establishes suction for withdrawing liquid from the reservoir. The conduit has a self-healing septum therein upstream of the jet ejector for receiving one end of a double-ended cannula, the other end of which is received in a serum bottle for sample collection. Gas is introduced into the conduit at a gas bleed between the sample collection bottle and the reservoir. The jet ejector evacuates gas from the conduit and the bottle and aspirates a column of liquid from the reservoir at a high rate. When the withdrawn liquid reaches the jet ejector the rate of flow therethrough reduces substantially and the gas bleed increases the pressure in the conduit for driving liquid into the sample bottle, the gas bleed forming a column of gas behind the withdrawn liquid column and interrupting the withdrawal of liquid from the reservoir. In the case of hazardous and toxic liquids, the sample bottle and the jet ejector may be isolated from the reservoir and may be further isolated from a control station containing remote manipulation means for the sample bottle and control valves for the jet ejector and gas bleed. 5 figs.

Larson, L.L.

1984-09-17T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

SLUDGE BATCH 7 PREPARATION TANK 4 AND 12 CHARACTERIZATION  

SciTech Connect (OSTI)

Samples of PUREX sludge from Tank 4 and HM sludge from Tank 12 were characterized in preparation for Sludge Batch 7 (SB7) formulation in Tank 51. SRNL analyses on Tank 4 and Tank 12 were requested in separate Technical Assistance Requests (TAR). The Tank 4 samples were pulled on January 19, 2010 following slurry operations by F-Tank Farm. The Tank 12 samples were pulled on February 9, 2010 following slurry operations by H-Tank Farm. At the Savannah River National Laboratory (SRNL), two 200 mL dip samples of Tank 4 and two 200 mL dip samples of Tank 12 were received in the SRNL Shielded Cells. Each tank's samples were composited into clean 500 mL polyethylene storage bottles and weighed. The composited Tank 4 sample was 428.27 g and the composited Tank 12 sample was 502.15 g. As expected there are distinct compositional differences between Tank 4 and Tank 12 sludges. The Tank 12 slurry is much higher in Al, Hg, Mn, and Th, and much lower in Fe, Ni, S, and U than the Tank 4 slurry. The Tank 4 sludge definitely makes the more significant contribution of S to any sludge batch blend. This S, like that observed during SB6 washing, is best monitored by looking at the total S measured by digesting the sample and analyzing by inductively coupled plasma - atomic emission spectroscopy (ICPAES). Alternatively, one can measure the soluble S by ICP-AES and adjust the value upward by approximately 15% to have a pretty good estimate of the total S in the slurry. Soluble sulfate measurements by ion chromatography (IC) will be biased considerably lower than the actual total S, the difference being due to the non-sulfate soluble S and the undissolved S. Tank 12 sludge is enriched in U-235, and hence samples transferred into SRNL from the Tank Farm will need to be placed on the reportable special nuclear material inventory and tracked for total U per SRNL procedure requirements.

Bannochie, C.; Click, D.; Pareizs, J.

2010-05-21T23:59:59.000Z

182

Coal preparation: The essential clean coal technology  

SciTech Connect (OSTI)

This chapter is a brief introduction to a broad topic which has many highly specialized areas. The aim is to summarize the essential elements of coal preparation and illustrate its important role in facilitating the clean use of coal. Conventional coal preparation is the essential first step in ensuring the economic and environmentally acceptable use of coal. The aim of coal preparation is to produce saleable products of consistent, specified quality which satisfy customer requirements while optimizing the utilization of the coal resource. Coal preparation covers all aspects of preparing coal for the market. It includes size reduction, blending and homogenization and, most importantly, the process of physical beneficiation or washing, which involves separation of undesirable mineral matter from the coal substance itself. Coal preparation can be performed at different levels of sophistication and cost. The degree of coal preparation required is decided by considering the quality of the raw coal, transport costs and, in particular, the coal quality specified by the consumer. However, the cost of coal beneficiation rises rapidly with the complexity of the process and some coal is lost with the waste matter because of process inefficiencies, therefore each situation requires individual study to determine the optimum coal preparation strategy. The necessary expertise is available within APEC countries such as Australia. Coals destined for iron making are almost always highly beneficiated. Physical beneficiation is mostly confined to the higher rank, hard coals, but all other aspects of coal preparation can be applied to subbituminous and lignitic coals to improve their utilization. Also, there are some interesting developments aimed specifically at reducing the water content of lower rank coals.

Cain, D.

1993-12-31T23:59:59.000Z

183

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledo SiteTonawandaUniversity21PreparedRffiS.-SeaGrand

184

Fluid sampling system  

DOE Patents [OSTI]

An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to be decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank. 4 figs.

Houck, E.D.

1994-10-11T23:59:59.000Z

185

Fluid sampling system  

DOE Patents [OSTI]

An fluid sampling system allows sampling of radioactive liquid without spillage. A feed tank is connected to a liquid transfer jet powered by a pumping chamber pressurized by compressed air. The liquid is pumped upwardly into a sampling jet of a venturi design having a lumen with an inlet, an outlet, a constricted middle portion, and a port located above the constricted middle portion. The liquid is passed under pressure through the constricted portion causing its velocity to increase and its pressure to decreased, thereby preventing liquid from escaping. A septum sealing the port can be pierced by a two pointed hollow needle leading into a sample bottle also sealed by a pierceable septum affixed to one end. The bottle is evacuated by flow through the sample jet, cyclic variation in the sampler jet pressure periodically leaves the evacuated bottle with lower pressure than that of the port, thus causing solution to pass into the bottle. The remaining solution in the system is returned to the feed tank via a holding tank.

Houck, Edward D. (Idaho Falls, ID)

1994-01-01T23:59:59.000Z

186

Numerically Efficient Parallel Algorithms Prepared for the  

E-Print Network [OSTI]

Simulation using High Performance Computing Prepared by New Mexico Tech New Mexico Institute of Mining agency thereof. #12;Final Report for Task One Project: Application of High Performance Computing

187

a amework for change Prepared by  

E-Print Network [OSTI]

a amework for change Prepared by the California Air Resources Board for the State of California D. Nichols Chairman, Air Resources Board James N. Goldstene Executive O cer, Air Resources Board_____________________________________ C-138 Industry____________________________________________C-150 Recycling and Waste

188

a amework for change Prepared by  

E-Print Network [OSTI]

a amework for change Prepared by the California Air Resources Board for the State of California D. Nichols Chairman, Air Resources Board James N. Goldstene Executive O cer, Air Resources Board____________________________________________C-150 Recycling and Waste_________________________________ C-158 Forests

189

Viscous sludge sample collector  

DOE Patents [OSTI]

A vertical core sample collection system for viscous sludge. A sample tube's upper end has a flange and is attached to a piston. The tube and piston are located in the upper end of a bore in a housing. The bore's lower end leads outside the housing and has an inwardly extending rim. Compressed gas, from a storage cylinder, is quickly introduced into the bore's upper end to rapidly accelerate the piston and tube down the bore. The lower end of the tube has a high sludge entering velocity to obtain a full-length sludge sample without disturbing strata detail. The tube's downward motion is stopped when its upper end flange impacts against the bore's lower end inwardly extending rim.

Beitel, George A [Richland, WA

1983-01-01T23:59:59.000Z

190

E-Print Network 3.0 - agents design preparation Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Tools... Management: Software development General Terms Design, Security, Standardization Keywords Mobile Agents 1... . SMASH is also designed to address 12;context-based...

191

E-Print Network 3.0 - alloy films prepared Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

of Alloys and Compounds 312 (2000) 238250 www.elsevier.comlocatejallcom Summary: of eutectic alloy amorphous silicon film. (b) SAD pattern of metastable crystal gold near...

192

E-Print Network 3.0 - arylindium reagents prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Reagent 1: Sulfosalicylic Acid Solution, 1,000 ml... Reagent 2: Sulfosalicylic Acid + CaCl2 Solution, 250 ml ... Source: Lebendiker, Mario - Wolfson Centre for Applied Structural...

193

E-Print Network 3.0 - al83fe17 alloys prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Corrosion ... Source: Zheng, Yufeng - Department of Advanced Materials and Nanotechnology, Peking University Collection: Materials Science ; Biology and Medicine 4...

194

E-Print Network 3.0 - alloy particles prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

5 h. Lenticular ... Source: Zheng, Yufeng - Department of Advanced Materials and Nanotechnology, Peking University Collection: Materials Science ; Biology and Medicine 4 JOURNAL...

195

E-Print Network 3.0 - anode catalysts prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

fuel cells, by modifying both the anode and the cathode catalysts that will enable PEM fuel cell... catalyst as a separate phase - as nanoparticles. 2. ... Source: DOE Office of...

196

E-Print Network 3.0 - acid-prepared mesoporous spheres Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

University Collection: Materials Science ; Physics 8 Nitrogen Adsorption in Carbon Aerogels: A Molecular Simulation Study Summary: a molecular model for carbon aerogel in which...

197

E-Print Network 3.0 - actinide target preparation Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

for such materials... ' actinides, to distinguish them from the larger quantities of uranium and plutonium also present in the fuel... to extract and recycle all actinides in...

198

Versatile, automated sample preparation and detection of contaminants and biological materials  

E-Print Network [OSTI]

Contamination of food, water, medicine and ingestible household products is a public health hazard that episodically causes outbreaks worldwide. Existing laboratory methods are often expensive, require a laboratory environment ...

Hoehl, Melanie Margarete

2013-01-01T23:59:59.000Z

199

Robots Help with Sample Preparation and Analysis at UNL Water Sciences Lab  

E-Print Network [OSTI]

to headspace to liquid injection. Paired with the new inert source Agilent 5973, with both electron impact (EI to the Lab's Quattro Micro triple quadrupole mass spectrometer. The Symbiosys Enviro is an automated system and others such as algal toxins that may negatively impact Nebraska's water quality and environment. #12;

Nebraska-Lincoln, University of

200

E-Print Network 3.0 - antifreeze protein prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

with a melting point-freezing point difference... Macrozoarces americanus, all of which produce ... Source: Cheng, Chi-Hing Christina - Department of Animal Biology, University...

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

E-Print Network 3.0 - activated carbons prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Forest carbon projects... straightforward way to sequester carbon and is the simplest carbon sequestration activity to account for in forest... reductions achieved by...

202

E-Print Network 3.0 - automated spike preparation Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

S. Rhode a a... 1994 Abstract A software routine to reconstruct individual spike trains from multi-neuron, single Source: Street, Nick - Department of Computer Science,...

203

E-Print Network 3.0 - acid-g-ethylene glycol prepared Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

of interest in this research were com- plexing poly(methacrylic acid-g-ethylene glycol) hydro- gels... Part Synthesis of Poly(methacrylic acid-g-ethylene glycol) ... Source:...

204

E-Print Network 3.0 - apatite powders prepared Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

a final stage of more... -rock and minerals separates (amphibole, pyroxene, biotite, titanite and apatite) were extracted from ... Source: Siebel, Wolfgang - Institut fr...

205

E-Print Network 3.0 - automatic preparative gas-liquid Sample...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Gas Engineering, West Virginia University Collection: Fossil Fuels 72 Comparison of void fraction correlations for different flow patterns in horizontal and upward inclined...

206

Structural, electrical and dielectric properties of spinel nickel ferrite prepared by soft mechanochemical synthesis  

SciTech Connect (OSTI)

Graphical abstract: - Highlights: • Sintered NiFe{sub 2}O{sub 4} was prepared by a soft mechanochemical route from mixture powders. • XRD and Raman measurements indicate that the prepared samples have spinel structure. • The activation energy ?E are 0.653 and 0.452 eV for NiFe{sub 2}O{sub 4} samples. • Ferrite from Ni(OH){sub 2}/Fe{sub 2}O{sub 3} has lower DC conductivity than from Ni(OH){sub 2}/Fe(OH){sub 3} powders. • The values of dielectric constant of samples NiFe{sub 2}O{sub 4} are 70 and 200, respectively. - Abstract: Nickel ferrite, NiFe{sub 2}O{sub 4} was prepared by a soft mechanochemical route from a mixture of (1) Ni(OH){sub 2} and ?-Fe{sub 2}O{sub 3} and (2) Ni(OH){sub 2} and Fe(OH){sub 3} powders in a planetary ball mill for 25 h. The powder samples were sintered at 1100 °C for 2 h and were characterized by X-ray diffraction (XRD), Raman spectroscopy and scanning electron microscopy (SEM). Impedance spectroscopy techniques were used to study the effect of grain and grain boundary on the electrical properties of the prepared samples. A difference in dielectric constant (?) and dielectric loss tangent (tan ?) of NiFe{sub 2}O{sub 4} samples obtained by the same methods but starting from different initial components was observed.

Lazarevi?, Zorica Ž., E-mail: lzorica@yahoo.com [Institute of Physics, University of Belgrade, P.O. Box 68, Pregrevica 118, Zemun, Belgrade (Serbia); Jovaleki?, ?edomir [The Institute for Multidisciplinary Research, University of Belgrade, Kneza Višeslava 1, Belgrade (Serbia); Sekuli?, Dalibor L. [Faculty of Technical Sciences, University of Novi Sad, Trg Dositeja Obradovi?a 6, Novi Sad (Serbia); Milutinovi?, Aleksandra [Institute of Physics, University of Belgrade, P.O. Box 68, Pregrevica 118, Zemun, Belgrade (Serbia); Baloš, Sebastian; Slankamenac, Miloš [Faculty of Technical Sciences, University of Novi Sad, Trg Dositeja Obradovi?a 6, Novi Sad (Serbia); Rom?evi?, Nebojša Ž. [Institute of Physics, University of Belgrade, P.O. Box 68, Pregrevica 118, Zemun, Belgrade (Serbia)

2013-10-15T23:59:59.000Z

207

Environmental Science: Sample Pathway  

E-Print Network [OSTI]

Environmental Science: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Core GE 100 Intro to Env Science ES 105 Env Earth Science Sophomore Year CGS Core (CGS NS201 will fulfill CAS BI107 & 124) MA 115 Statistics Summer Environmental Internship Junior Year CH 171 Chem for Health Sciences CH

Goldberg, Bennett

208

Preparation and electrocatalytic activity of tungsten carbide and titania nanocomposite  

SciTech Connect (OSTI)

Graphical abstract: The electrocatalytic activity of tungsten carbide and titania nanocomposite is related to the structure, crystal phase and chemical components of the nanocomposite, and is also affected by the property of electrolyte. A synergistic effect exists between tungsten carbide and titania of the composite. Highlights: {yields} Electrocatalytic activity of tungsten carbide and titania nanocomposite with core-shell structure. {yields} Activity is related to the structure, crystal phase and chemical component of the nanocomposite. {yields} The property of electrolyte affects the electrocatalytic activity. {yields} A synergistic effect exists between tungsten carbide and titania of the composite. -- Abstract: Tungsten carbide and titania nanocomposite was prepared by combining a reduced-carbonized approach with a mechanochemical approach. The samples were characterized by X-ray diffraction, transmission electron microscope under scanning mode and X-ray energy dispersion spectrum. The results show that the crystal phases of the samples are composed of anatase, rutile, nonstoichiometry titanium oxide, monotungsten carbide, bitungsten carbide and nonstoichiometry tungsten carbide, and they can be controlled by adjusting the parameters of the reduced-carbonized approach; tungsten carbide particles decorate on the surface of titania support, the diameter of tungsten carbide particle is smaller than 20 nm and that of titania is around 100 nm; the chemical components of the samples are Ti, O, W and C. The electrocatalytic activity of the samples was measured by a cyclic voltammetry with three electrodes. The results indicate that the electrocatalytic activities of the samples are related to their crystal phases and the property of electrolyte in aqueous solution. A synergistic effect between titania and tungsten carbide is reported for the first time.

Hu, Sujuan; Shi, Binbin; Yao, Guoxing [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)] [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China); Li, Guohua, E-mail: nanozjut@zjut.edu.cn [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)] [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China); Ma, Chunan [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)] [State Key Laboratory Breeding Base of Green Chemistry Synthesis Technology, School of Chemical Engineering and Materials Science, Zhejiang University of Technology, Hangzhou 310032 (China)

2011-10-15T23:59:59.000Z

209

DOE Signs Notice to Prepare Environmental Assessment on Proposed...  

Broader source: Energy.gov (indexed) [DOE]

DOE Signs Notice to Prepare Environmental Assessment on Proposed Project with Germany DOE Signs Notice to Prepare Environmental Assessment on Proposed Project with Germany June 30,...

210

President Issues Executive Order Aimed at Preparing for the Impacts...  

Broader source: Energy.gov (indexed) [DOE]

President Issues Executive Order Aimed at Preparing for the Impacts of Climate Change; Tribal Leaders to Serve on Task Force President Issues Executive Order Aimed at Preparing for...

211

EIS-0472: Notice of Intent to Prepare a Programmatic Environmental...  

Energy Savers [EERE]

Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0472: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Uranium Leasing...

212

DOE to Prepare a Supplemental Environmental Impact Statement...  

Energy Savers [EERE]

Prepare a Supplemental Environmental Impact Statement for Proposed Surplus Plutonium Disposition at the Savannah River Site DOE to Prepare a Supplemental Environmental Impact...

213

EIS-0469: Notice of Intent To Prepare an Environmental Impact...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

69: Notice of Intent To Prepare an Environmental Impact Statement and to Conduct Scoping Meetings EIS-0469: Notice of Intent To Prepare an Environmental Impact Statement and to...

214

EIS-0509: Notice of Intent to Prepare Environmental Impact Statement...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

EIS-0509: Notice of Intent to Prepare Environmental Impact Statement EIS-0509: Notice of Intent to Prepare Environmental Impact Statement The Federal Energy Regulatory Commission...

215

EIS-0500: Notice of Intent to Prepare Environmental Impact Statement...  

Energy Savers [EERE]

Notice of Intent to Prepare Environmental Impact Statement EIS-0500: Notice of Intent to Prepare Environmental Impact Statement Crystal Springs Hatchery Program; Bingham, Custer,...

216

EIS-0502: Notice of Intent to Prepare Environmental Impact Statement...  

Energy Savers [EERE]

Notice of Intent to Prepare Environmental Impact Statement EIS-0502: Notice of Intent to Prepare Environmental Impact Statement Hot Springs to Anaconda Transmission Line Rebuild...

217

EIS-0310: Notice of Intent to Prepare a Programmatic Environmental...  

Energy Savers [EERE]

Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0310: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Accomplishing Expanded...

218

EIS-0428: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

28: Notice of Intent to Prepare an Environmental Impact Statement EIS-0428: Notice of Intent to Prepare an Environmental Impact Statement Construction and Startup of the...

219

EIS-0402: Advance Notice of Intent to Prepare an Environmental...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

EIS-0402: Advance Notice of Intent to Prepare an Environmental Impact Statement EIS-0402: Advance Notice of Intent to Prepare an Environmental Impact Statement Remediation of Area...

220

EIS-0510: FERC Notice of Intent to Prepare Environmental Impact...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

510: FERC Notice of Intent to Prepare Environmental Impact Statement EIS-0510: FERC Notice of Intent to Prepare Environmental Impact Statement Calcasieu Pass Project, Cameron...

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

EIS-0481: Notice of Intent to Prepare a Programmatic Environmental...  

Energy Savers [EERE]

81: Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0481: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Engineered High...

222

EIS-0483: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

Notice of Intent to Prepare an Environmental Impact Statement EIS-0483: Notice of Intent to Prepare an Environmental Impact Statement Estes to Flatiron Substation Transmission...

223

EIS-0504: Notice of Intent to Prepare Environmental Impact Statement...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Notice of Intent to Prepare Environmental Impact Statement EIS-0504: Notice of Intent to Prepare Environmental Impact Statement Gulf LNG Liquefaction Project, Jackson County,...

224

EIS-0494: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

94: Notice of Intent to Prepare an Environmental Impact Statement EIS-0494: Notice of Intent to Prepare an Environmental Impact Statement Excelerate Liquefaction Solutions Lavaca...

225

EIS-0481: Notice of Intent to Prepare a Programmatic Environmental...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0481: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Engineered High Energy...

226

EIS-0496: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

6: Notice of Intent to Prepare an Environmental Impact Statement EIS-0496: Notice of Intent to Prepare an Environmental Impact Statement DOE's Western Area Power Administration...

227

EIS-0499: Notice of Intent to Prepare Environmental Impact Statement...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

499: Notice of Intent to Prepare Environmental Impact Statement EIS-0499: Notice of Intent to Prepare Environmental Impact Statement Great Northern Transmission Line Project The...

228

EIS-0491: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

Notice of Intent to Prepare an Environmental Impact Statement EIS-0491: Notice of Intent to Prepare an Environmental Impact Statement Lake Charles Liquefaction Project, Calcasieu...

229

EIS-0510: FERC Notice of Intent to Prepare Environmental Impact...  

Energy Savers [EERE]

FERC Notice of Intent to Prepare Environmental Impact Statement EIS-0510: FERC Notice of Intent to Prepare Environmental Impact Statement Calcasieu Pass Project, Cameron Parish,...

230

EIS-0503: Notice of Intent to Prepare Environmental Impact Statement...  

Energy Savers [EERE]

Notice of Intent to Prepare Environmental Impact Statement EIS-0503: Notice of Intent to Prepare Environmental Impact Statement New England Clean Power Link, Vermont DOE announces...

231

Preparation and Characterisation of Vertically Aligned Carbon Nanotubes.  

E-Print Network [OSTI]

??This thesis presents the preparation of vertically aligned carbon nanotubes using porous anodic alumina templates via thermal chemical vapour deposition. The characteristics of prepared carbon… (more)

Xu, Rui

2010-01-01T23:59:59.000Z

232

Redox Chemistry in Thin Layers of Organometallic Complexes Prepared...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Redox Chemistry in Thin Layers of Organometallic Complexes Prepared Using Ion Soft Landing. Redox Chemistry in Thin Layers of Organometallic Complexes Prepared Using Ion Soft...

233

EIS-0394: Advance Notice of Intent to Prepare an Environmental...  

Energy Savers [EERE]

Advance Notice of Intent to Prepare an Environmental Impact Statement EIS-0394: Advance Notice of Intent to Prepare an Environmental Impact Statement Implementation of the...

234

EIS-0301: Notice of Intent to Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

of Intent to Prepare an Environmental Impact Statement and Notice of Floodplain and Wetlands Involvement EIS-0301: Notice of Intent to Prepare an Environmental Impact Statement...

235

EIS-0390: Notice of Intent to Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

Intent to Prepare an Environmental Impact Statement; Floodplain and Wetlands Involvement; and Public Scoping Meetings EIS-0390: Notice of Intent to Prepare an Environmental Impact...

236

EIS-0409: Notice of Intent to Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

to Prepare an Environmental Impact Statement and Notice of Proposed Floodplain and Wetlands Involvement EIS-0409: Notice of Intent to Prepare an Environmental Impact Statement...

237

EIS-0475: Notice of Intent To Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

5: Notice of Intent To Prepare an Environmental Impact Statement and Notice of Wetlands Involvement EIS-0475: Notice of Intent To Prepare an Environmental Impact Statement and...

238

Decoupled Sampling for Graphics Pipelines  

E-Print Network [OSTI]

We propose a generalized approach to decoupling shading from visibility sampling in graphics pipelines, which we call decoupled sampling. Decoupled sampling enables stochastic supersampling of motion and defocus blur at ...

Ragan-Kelley, Jonathan Millar

239

Fluid sampling apparatus and method  

DOE Patents [OSTI]

Incorporation of a bellows in a sampling syringe eliminates ingress of contaminants, permits replication of amounts and compression of multiple sample injections, and enables remote sampling for off-site analysis. 3 figs.

Yeamans, D.R.

1998-02-03T23:59:59.000Z

240

Soil sampling kit and a method of sampling therewith  

DOE Patents [OSTI]

A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allow an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds.

Thompson, Cyril V. (Knoxville, TN)

1991-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

Soil sampling kit and a method of sampling therewith  

DOE Patents [OSTI]

A soil sampling device and a sample containment device for containing a soil sample is disclosed. In addition, a method for taking a soil sample using the soil sampling device and soil sample containment device to minimize the loss of any volatile organic compounds contained in the soil sample prior to analysis is disclosed. The soil sampling device comprises two close fitting, longitudinal tubular members of suitable length, the inner tube having the outward end closed. With the inner closed tube withdrawn a selected distance, the outer tube can be inserted into the ground or other similar soft material to withdraw a sample of material for examination. The inner closed end tube controls the volume of the sample taken and also serves to eject the sample. The soil sample containment device has a sealing member which is adapted to attach to an analytical apparatus which analyzes the volatile organic compounds contained in the sample. The soil sampling device in combination with the soil sample containment device allows an operator to obtain a soil sample containing volatile organic compounds and minimizing the loss of the volatile organic compounds prior to analysis of the soil sample for the volatile organic compounds. 11 figures.

Thompson, C.V.

1991-02-05T23:59:59.000Z

242

INVESTIGATION OF THE TOTAL ORGANIC HALOGEN ANALYTICAL METHOD AT THE WASTE SAMPLING CHARACTERIZATION FACILITY (WSCF)  

SciTech Connect (OSTI)

Total organic halogen (TOX) is used as a parameter to screen groundwater samples at the Hanford Site. Trending is done for each groundwater well, and changes in TOX and other screening parameters can lead to costly changes in the monitoring protocol. The Waste Sampling and Characterization Facility (WSCF) analyzes groundwater samples for TOX using the United States Environmental Protection Agency (EPA) SW-846 method 9020B (EPA 1996a). Samples from the Soil and Groundwater Remediation Project (S&GRP) are submitted to the WSCF for analysis without information regarding the source of the sample; each sample is in essence a 'blind' sample to the laboratory. Feedback from the S&GRP indicated that some of the WSCF-generated TOX data from groundwater wells had a number of outlier values based on the historical trends (Anastos 2008a). Additionally, analysts at WSCF observed inconsistent TOX results among field sample replicates. Therefore, the WSCF lab performed an investigation of the TOX analysis to determine the cause of the outlier data points. Two causes were found that contributed to generating out-of-trend TOX data: (1) The presence of inorganic chloride in the groundwater samples: at inorganic chloride concentrations greater than about 10 parts per million (ppm), apparent TOX values increase with increasing chloride concentration. A parallel observation is the increase in apparent breakthrough of TOX from the first to the second activated-carbon adsorption tubes with increasing inorganic chloride concentration. (2) During the sample preparation step, excessive purging of the adsorption tubes with oxygen pressurization gas after sample loading may cause channeling in the activated-carbon bed. This channeling leads to poor removal of inorganic chloride during the subsequent wash step with aqueous potassium nitrate. The presence of this residual inorganic chloride then produces erroneously high TOX values. Changes in sample preparation were studied to more effectively remove inorganic chloride from the activated carbon adsorption tubes. With the TOX sample preparation equipment and TOX analyzers at WSCF, the nitrate wash recommended by EPA SW-846 method 9020B was found to be inadequate to remove inorganic chloride interference. Increasing the nitrate wash concentration from 10 grams per liter (g/L) to 100 g/L potassium nitrate and increasing the nitrate wash volume from 3 milliliters (mL) to 10 mL effectively removed the inorganic chloride up to at least 100 ppm chloride in the sample matrix. Excessive purging of the adsorption tubes during sample preparation was eliminated. These changes in sample preparation have been incorporated in the analytical procedure. The results using the revised sample preparation procedure show better agreement of TOX values both for replicate analyses of single samples and for the analysis of replicate samples acquired from the same groundwater well. Furthermore, less apparent column breakthrough now occurs with the revised procedure. One additional modification made to sample preparation was to discontinue the treatment of groundwater samples with sodium bisulfite. Sodium bisulfite is used to remove inorganic chlorine from the sample; inorganic chlorine is not expected to be a constituent in these groundwater samples. Several other factors were also investigated as possible sources of anomalous TOX results: (1) Instrument instability: examination of the history of results for TOX laboratory control samples and initial calibration verification standards indicate good long-term precision for the method and instrument. Determination of a method detection limit of 2.3 ppb in a deionized water matrix indicates the method and instrumentation have good stability and repeatability. (2) Non-linear instrument response: the instrument is shown to have good linear response from zero to 200 parts per billion (ppb) TOX. This concentration range encompasses the majority of samples received at WSCF for TOX analysis. (3) Improper sample preservation: ion-chromatographic analysis of several samples wit

DOUGLAS JG; MEZNARICH HD, PHD; OLSEN JR; ROSS GA; STAUFFER M

2008-09-30T23:59:59.000Z

243

Preparation and screening of crystalline inorganic materials  

DOE Patents [OSTI]

Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc. Once prepared, these materials can be screened for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical, or other properties. Thus, the present invention provides methods for the parallel synthesis and analysis of novel materials having useful properties.

Schultz, Peter G. (La Jolla, CA); Xiang, Xiaodong (Danville, CA); Goldwasser, Isy (Palo Alto, CA); Brice{hacek over (n)}o, Gabriel (Baldwin Park, CA); Sun, Xiao-Dong (Fremont, CA); Wang, Kai-An (Cupertino, CA)

2008-10-28T23:59:59.000Z

244

Northern Marshall Islands radiological survey: sampling and analysis summary  

SciTech Connect (OSTI)

A radiological survey was conducted in the Northern Marshall Islands to document reamining external gamma exposures from nuclear tests conducted at Enewetak and Bikini Atolls. An additional program was later included to obtain terrestrial and marine samples for radiological dose assessment for current or potential atoll inhabitants. This report is the first of a series summarizing the results from the terrestrial and marine surveys. The sample collection and processing procedures and the general survey methodology are discussed; a summary of the collected samples and radionuclide analyses is presented. Over 5400 samples were collected from the 12 atolls and 2 islands and prepared for analysis including 3093 soil, 961 vegetation, 153 animal, 965 fish composite samples (average of 30 fish per sample), 101 clam, 50 lagoon water, 15 cistern water, 17 groundwater, and 85 lagoon sediment samples. A complete breakdown by sample type, atoll, and island is given here. The total number of analyses by radionuclide are 8840 for /sup 241/Am, 6569 for /sup 137/Cs, 4535 for /sup 239 +240/Pu, 4431 for /sup 90/Sr, 1146 for /sup 238/Pu, 269 for /sup 241/Pu, and 114 each for /sup 239/Pu and /sup 240/Pu. A complete breakdown by sample category, atoll or island, and radionuclide is also included.

Robison, W.L.; Conrado, C.L.; Eagle, R.J.; Stuart, M.L.

1981-07-23T23:59:59.000Z

245

Sample holder with optical features  

DOE Patents [OSTI]

A sample holder for holding a sample to be observed for research purposes, particularly in a transmission electron microscope (TEM), generally includes an external alignment part for directing a light beam in a predetermined beam direction, a sample holder body in optical communication with the external alignment part and a sample support member disposed at a distal end of the sample holder body opposite the external alignment part for holding a sample to be analyzed. The sample holder body defines an internal conduit for the light beam and the sample support member includes a light beam positioner for directing the light beam between the sample holder body and the sample held by the sample support member.

Milas, Mirko; Zhu, Yimei; Rameau, Jonathan David

2013-07-30T23:59:59.000Z

246

A comparison of sequential and point sample scouting for arthropods of cotton  

E-Print Network [OSTI]

of Department December 1981 use of infested/damaged sample units whereas the Sterling package was based primarily on undamaged/uninfested sample units. The Rothrock package was based entirely on undamaged or uninfested sample units and resulted... L. Sterling for his guidance and counsel during the course of this study and preparation of the manuscript. The author also wishes to thank Drs. James W. Smith, Jr. , Robert S. Halliwell, and John H. Benedict, for their services on the graduate...

Rothrock, Michael Alan

1981-01-01T23:59:59.000Z

247

Characterization of gels prepared from silicon ethoxide  

E-Print Network [OSTI]

by heating to a high temperature, with low heating rates. Tg and Tc were correlated to water gt alcohol contents in presence of HCI or HF. Aerogels were found to have high pore volume, low bulk density, large pore size, and weak mechanical strength.... Structures of dried gels 2. 3, Densification 13 14 15 19 19 CHAPTER III 3. 1. Raw materials 3. 2. Xerogel preparation 3. 3. Aerogel preparation 3. 4. Characterization of dried gels 3, 4. 1. Mercury porosimetry 3. 4. 2. BET analysis 3. 4, 3...

Yun, Su-Jin

2012-06-07T23:59:59.000Z

248

Method of preparing meso-haloalkylporphyrins  

DOE Patents [OSTI]

Transition metal complexes of meso-haloalkylporphyrins, wherein the haloalkyl groups contain 2 to 8 carbon atoms have been found to be highly effective catalysts for oxidation of alkanes and for the decomposition of hydroperoxides. Also disclosed is a process for the preparation of meso-halocarbyl-porphyrins which comprises contacting a halocarbyl dipyrromethane with a halocarbyl-substituted aldehyde in the presence of an acid granular solid catalyst. Also disclosed is a process for the preparation of meso-halocarbyl-porphyrins which comprises contacting a halocarbyl dipyrromethane with a halocarbyl-substituted aldehyde in the presence of an acid granular solic catalyst.

Wijesekera, Tilak (Glen Mills, PA); Lyons, James E. (Wallingford, PA); Ellis, Jr., Paul E. (Downingtown, PA); Bhinde, Manoj V. (Boothwyn, PA)

1998-01-01T23:59:59.000Z

249

INVESTIGATION OF THE TOTAL ORGANIC HALOGEN ANALYTICAL METHOD AT THE WASTE SAMPLING AND CHARACTERIZATION FACILITY  

SciTech Connect (OSTI)

Total organic halogen (TOX) is used as a parameter to screen groundwater samples at the Hanford Site. Trending is done for each groundwater well, and changes in TOX and other screening parameters can lead to costly changes in the monitoring protocol. The Waste Sampling and Characterization Facility (WSCF) analyzes groundwater samples for TOX using the United States Environmental Protection Agency (EPA) SW-S46 method 9020B (EPA 1996a). Samples from the Soil and Groundwater Remediation Project (SGRP) are submitted to the WSCF for analysis without information regarding the source of the sample; each sample is in essence a ''blind'' sample to the laboratory. Feedback from the SGRP indicated that some of the WSCF-generated TOX data from groundwater wells had a number of outlier values based on the historical trends (Anastos 200Sa). Additionally, analysts at WSCF observed inconsistent TOX results among field sample replicates. Therefore, the WSCF lab performed an investigation of the TOX analysis to determine the cause of the outlier data points. Two causes were found that contributed to generating out-of-trend TOX data: (1) The presence of inorganic chloride in the groundwater samples: at inorganic chloride concentrations greater than about 10 parts per million (ppm), apparent TOX values increase with increasing chloride concentration. A parallel observation is the increase in apparent breakthrough of TOX from the first to the second activated-carbon adsorption tubes with increasing inorganic chloride concentration. (2) During the sample preparation step, excessive purging of the adsorption tubes with oxygen pressurization gas after sample loading may cause channeling in the activated carbon bed. This channeling leads to poor removal of inorganic chloride during the subsequent wash step with aqueous potassium nitrate. The presence of this residual inorganic chloride then produces erroneously high TOX values. Changes in sample preparation were studied to more effectively remove inorganic chloride from the activated-carbon adsorption tubes. With the TOX sample preparation equipment and TOX analyzers at WSCF, the nitrate wash recommended by EPA SW-846 method 9020B was found to be inadequate to remove inorganic chloride interference. Increasing the nitrate wash concentration from 10 grams per liter (g/L) to 100 giL potassium nitrate and increasing the nitrate wash volume from 3 milliliters (mL) to 10 mL effectively removed the inorganic chloride up to at least 100 ppm chloride in the sample matrix. Excessive purging of the adsorption tubes during sample preparation was eliminated. These changes in sample preparation have been incorporated in the analytical procedure. The results using the revised sample preparation procedure show better agreement of TOX values both for replicate analyses of single samples and for the analysis of replicate samples acquired from the same groundwater well. Furthermore, less apparent adsorption tube breakthrough now occurs with the revised procedure. One additional modification made to sample preparation was to discontinue the treatment of groundwater samples with sodium bisulfite. Sodium bisulfite is used to remove inorganic chlorine from the sample; inorganic chlorine is not expected to be a constituent in these groundwater samples. Several other factors were also investigated as possible sources of anomalous TOX results: (1) Instrument instability: examination of the history of results for TOX laboratory control samples and initial calibration verification standards indicate good long-term precision for the method and instrument. Determination of a method detection limit of 2.3 ppb in a deionized water matrix indicates the method and instrumentation have good stability and repeatability. (2) Non-linear instrument response: the instrument is shown to have good linear response from zero to 200 parts per billion (ppb) TOX. This concentration range encompasses the majority of samples received at WSCF for TOX analysis. Linear response was checked using both non-volatile TOX species (trichlorophenol) an

JG DOUGLAS; HK MEZNARICH, PHD; JR OLSEN; GA ROSS PHD; M STAUFFER

2009-02-13T23:59:59.000Z

250

Sample Environment Plans and Progress  

E-Print Network [OSTI]

Sample Environment Plans and Progress at the SNS & HFIR SNS HFIR User Group Meeting American Conference on Neutron Scattering Ottawa, Canada June 26 ­ 30, 2010 Lou Santodonato Sample Environment Group our sample environment capabilities Feedback SHUG meetings User surveys Sample Environment Steering

Pennycook, Steve

251

Process for the preparation of an energetic nitrate ester  

DOE Patents [OSTI]

A process for the preparation of an energetic nitrate ester compound and related intermediates is provided.

Chavez, David E; Naud, Darren L; Hiskey, Michael A

2013-12-17T23:59:59.000Z

252

PREPARATION AND SPECTROSCOPIC PROPERTIES OF THREE NEW ACTINIDE (IV) BOROHYDRIDES  

E-Print Network [OSTI]

uranium tetrakis-borohydrides were prepared by a different reaction which involves the actinide tetrafluoride

Banks, Rodney Howard

2010-01-01T23:59:59.000Z

253

Stack sampling apparatus  

SciTech Connect (OSTI)

An apparatus for obtaining samples from a structure includes a support member, at least one stabilizing member, and at least one moveable member. The stabilizing member has a first portion coupled to the support member and a second portion configured to engage with the structure to restrict relative movement between the support member and the structure. The stabilizing member is radially expandable from a first configuration where the second portion does not engage with a surface of the structure to a second configuration where the second portion engages with the surface of the structure.

Lind, Randall F; Lloyd, Peter D; Love, Lonnie J; Noakes, Mark W; Pin, Francois G; Richardson, Bradley S; Rowe, John C

2014-09-16T23:59:59.000Z

254

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado, Disposal

255

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,

256

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,and

257

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOld

258

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOld

259

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction, Colorado,andOldOld

260

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction,

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofofOxford SiteToledoSampling at the Grand Junction,Groundwater and

262

Sample Changes and Issues  

Annual Energy Outlook 2013 [U.S. Energy Information Administration (EIA)]

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) " ,"ClickPipelines AboutDecemberSteamYear Jan FebThousand Cubic Feet)Year JanC.9.3. Receipts8.160Sample

263

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling at

264

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling at4

265

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C.Green River, Utah, DisposalRulison,Sampling

266

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C. 20545 OCT 28Sacandaga SiteSep NovWater Sampling

267

September 2004 Water Sampling  

Office of Legacy Management (LM)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr May Jun Jul(Summary) "ofEarlyEnergyDepartment ofDepartment ofof EnergyYou$0.C. 20545 OCT 28Sacandaga SiteSep NovWaterSampling

268

Energy Simulation Training Prepared for the  

E-Print Network [OSTI]

`i Natural Energy Institute University of Hawai`i Manoa #12;#12;TABLE OF CONTENTS HNEI FUNDING Program Subtask 3.5.1: Residential Energy Efficiency Deliverable 3 Prepared by The University of Hawai and Earth Science and Technology University of Hawai`i April 2013 #12;Acknowledgement: This material

269

Preparation of a semiconductor thin film  

DOE Patents [OSTI]

A process for the preparation of a semiconductor film. The process comprises depositing nanoparticles of a semiconductor material onto a substrate whose surface temperature during nanoparticle deposition thereon is sufficient to cause substantially simultaneous fusion of the nanoparticles to thereby coalesce with each other and effectuate film growth.

Pehnt, Martin (TuBingen, DE); Schulz, Douglas L. (Denver, CO); Curtis, Calvin J. (Lakewood, CO); Ginley, David S. (Evergreen, CO)

1998-01-01T23:59:59.000Z

270

Leafy Green Preparation and Cooling Study  

E-Print Network [OSTI]

Leafy Green Preparation and Cooling Study Dominique N. Bibbins #12;Background : Leafy Greens z In the past, leafy greens have been the source of food borne-illnesses and outbreaks. z It is important Lasting knowledge of survey practices, procedures, and protocol. #12;Acknowledgements z Laura Green, Ph

271

Process for the preparation of vinyl acetate  

DOE Patents [OSTI]

This invention pertains to the preparation of vinyl acetate by contacting within a contact zone a mixture of ketene and acetaldehyde with an acid catalyst at about one bar pressure and between about 85.degree. and 200.degree. C. and removing the reaction products from the contact zone.

Tustin, Gerald Charles (Kingsport, TN); Zoeller, Joseph Robert (Kingsport, TN); Depew, Leslie Sharon (Kingsport, TN)

1998-01-01T23:59:59.000Z

272

Process for the preparation of vinyl acetate  

DOE Patents [OSTI]

This invention pertains to the preparation of vinyl acetate by contacting within a contact zone a mixture of ketene and acetaldehyde with an acid catalyst at about one bar pressure and between about 85 and 200 C and removing the reaction products from the contact zone.

Tustin, G.C.; Zoeller, J.R.; Depew, L.S.

1998-02-17T23:59:59.000Z

273

Energy Efficient Data Centers Prepared by  

E-Print Network [OSTI]

Board - Equinix · Pacific Gas and Electric Company · New York State Energy Research and DevelopmentEnergy Efficient Data Centers Prepared by William Tschudi, Tengfang Xu, Dale Sartor, Bruce Nordman, Jon Koomey, and Osman Sezgen Environmental Energy Technologies Division Lawrence Berkeley National

274

Methods for preparation of catalytic materials  

SciTech Connect (OSTI)

To establish guidelines for the development of a scientific basis for catalyst preparation is perhaps a very ambitious goal. One would re required first to answer the following rhetorical questions: what are the properties which determine the performance of a catalytic material; how can these properties be introduced, developed, and/or improved during preparation? The answer to these questions involves a comprehensive discussion of the theories of catalysis, which is beyond the scope of this review. The authors will attempt, instead, to provide a rationale for each reader to answer these questions on the basis of his/her own interests. They start the discussion by describing the fundamental steps in producing bulk catalysts and/or catalyst supports. The fundamental processes involved are those derived from traditional three-dimensional chemistry. The topic areas will include single-component and multicomponent metal oxides. Unsupported metallic catalysts are formed by transformations involving physical or chemical processes, and the preparation methods for this class of materials will be discussed next. Attention will then turn to the preparation of supported catalytic materials. The main topics to be discussed will be those related to the interaction between the support and the active phase when they are put together to generate the catalyst. In this approach, the authors exploit the virtually unexplored field of surface, or two-dimensional, physical chemistry. The materials considered include dispersed metals and alloys and composite oxides. 366 refs.

Schwarz, J.A. [Syracuse Univ., NY (United States). Dept. of Chemical Engineering and Materials Science; Contescu, C.; Contescu, A. [Romanian Academy, Bucharest (Romania). Inst. of Physical Chemistry

1995-05-01T23:59:59.000Z

275

Preparation of a semiconductor thin film  

DOE Patents [OSTI]

A process is disclosed for the preparation of a semiconductor film. The process comprises depositing nanoparticles of a semiconductor material onto a substrate whose surface temperature during nanoparticle deposition thereon is sufficient to cause substantially simultaneous fusion of the nanoparticles to thereby coalesce with each other and effectuate film growth.

Pehnt, M.; Schulz, D.L.; Curtis, C.J.; Ginley, D.S.

1998-01-27T23:59:59.000Z

276

prepared at INRIA Sophia-Antipolis  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia-Antipolis and presented at the University of Nice Sophia-Electrodes acquisitions in the retina Hassan NASSER Advisor Pr. Bruno Cessac INRIA Sophia-Antipolis Reviewers Pr. Stefano Statistique de l'ENS Examiners Pr. Pierre Kornprobst INRIA Sophia-Antipolis Pr. Adrián Palacios University

Paris-Sud XI, Université de

277

prepared at INRIA Sophia-Antipolis Mediterranee  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia-Antipolis M´editerran´ee and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation´e-Salp^etri`ere, Paris, France Dr. Pierre Comon I3S / CNRS / University of Nice, France Dr. Rachid Deriche INRIA Sophia

Paris-Sud XI, Université de

278

prepared at Inria Sophia Antipolis -Mediterranee  

E-Print Network [OSTI]

PhD THESIS prepared at Inria Sophia Antipolis - M´editerran´ee and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation. Rachid Deriche, Inria Sophia Antipolis-M´editerran´ee, France Reviewers Dr. Christian Barillot, CNRS

Recanati, Catherine

279

prepared at INRIA Sophia-Antipolis Mediterranee  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia-Antipolis M´editerran´ee and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation Features in Diffusion MRI Jian CHENG Advisers Dr. Rachid Deriche INRIA Sophia Antipolis, France Dr. Tianzi

Paris-Sud XI, Université de

280

prepared at INRIA Sophia Antipolis -Mditerrane  

E-Print Network [OSTI]

PhD THESIS prepared at INRIA Sophia Antipolis - Méditerranée and presented at the University of Nice-Sophia Antipolis Graduate School of Information and Communication Sciences A dissertation INRIA Sophia Antipolis, France Thierry VI�VILLE INRIA Sophia Antipolis, France President Rachid DERICHE

Paris-Sud XI, Université de

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

Test Preparation Options Free Test Prep Websites  

E-Print Network [OSTI]

Test Preparation Options Free Test Prep Websites ACT: http: http://www.collegeboard.com/student/testing/sat/prep_one/test.html http://www.number2.com://testprep.princetonreview.com/CourseSearch/Search.aspx?itemCode=17&productType=F&rid=1&zip=803 02 Test Prep Classes Front Range Community College: Classes

Stowell, Michael

282

CURRICULUM VITAE DATE PREPARED: September 5, 2007  

E-Print Network [OSTI]

CURRICULUM VITAE DATE PREPARED: September 5, 2007 PART I: General Information Education 2000- Organization for Human Brain Mapping (OHBM), Member HMS Curriculum Vitae Page 1 of 14 #12;2005- Society for Neuroscience (SFN), Member HMS Curriculum Vitae Page 2 of 14 #12;Part II: Research, Teaching

Boas, David

283

Photocatalytic methods for preparation of electrocatalyst materials  

DOE Patents [OSTI]

The invention relates to methods of preparing metal particles on a support material, including platinum-containing nanoparticles on a carbon support. Such materials can be used as electrocatalysts, for example as improved electrocatalysts in proton exchange membrane fuel cells (PEM-FCs).

Nwoga, Tochi Tudor; Kawahara, Kazuo; Li, Wen; Song, Yujiang; Shelnutt, John A; Miller, James E; Medforth, Craig John; Ueno, Yukiyoshi; Kawamura, Tetsuo

2013-12-17T23:59:59.000Z

284

Photocatalytic methods for preparation of electrocatalyst materials  

DOE Patents [OSTI]

The invention relates to methods of preparing metal particles on a support material, including platinum-containing nanoparticles on a carbon support. Such materials can be used as electrocatalysts, for example as improved electrocatalysts in polymer electrolyte membrane fuel cells (PEM-FCs).

Li, Wen; Kawamura, Tetsuo; Nagami, Tetsuo; Takahashi, Hiroaki; Muldoon, John; Shelnutt, John A; Song, Yujiang; Miller, James E; Hickner, Michael A; Medforth, Craig

2013-09-24T23:59:59.000Z

285

Data Update for Paxton, MA Prepared for  

E-Print Network [OSTI]

Data Update for Paxton, MA May, 2006 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for May, 2006 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

Massachusetts at Amherst, University of

286

Data Update for Paxton, MA Prepared for  

E-Print Network [OSTI]

Data Update for Paxton, MA June, 2006 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for June, 2006 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

Massachusetts at Amherst, University of

287

Data Update for Paxton, MA Prepared for  

E-Print Network [OSTI]

Data Update for Paxton, MA May, 2005 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for May, 2005 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

Massachusetts at Amherst, University of

288

Data Update for Paxton, MA Prepared for  

E-Print Network [OSTI]

Data Update for Paxton, MA July, 2005 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for July, 2005 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

Massachusetts at Amherst, University of

289

Data Update for Paxton, MA Prepared for  

E-Print Network [OSTI]

Data Update for Paxton, MA June, 2005 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for June, 2005 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

Massachusetts at Amherst, University of

290

Data Update for Paxton, MA Prepared for  

E-Print Network [OSTI]

Data Update for Paxton, MA July, 2006 Prepared for Massachusetts Technology Collaborative, 75 North Drive, Westborough, MA 01581 By Kai Wu Monthly Data Summary for July, 2006 This update summarizes the monthly data results for the Paxton MA monitoring site at 42-18-11.6 N, 71-53-50.9 W per the WSG84

Massachusetts at Amherst, University of

291

Steps in Preparing an Extension Publication.  

E-Print Network [OSTI]

- TDOC Z TA24S.7 B873 , nO.1296 _~J Stepsin Preparing an Extension Publication 1 A . It I University System gncu ura B-1296 ~ Texas Th~ Te~as A&M Extension Daniel C. Pfannstiel, Director '\\.... ~Arvice College Station, Texas 77843... CONTENTS Foreword.. . ......... ........... ........... 3 Approval Procedures for r--- Numbered Publications . ......... ,' . . . . . . . . 4 New Publications. . . . . . . . . . . . . . . . . . . . . .. 4 Reprints and Revisions...

Anonymous,

1980-01-01T23:59:59.000Z

292

The Economic State of Milwaukee, Prepared by  

E-Print Network [OSTI]

The Economic State of Milwaukee, 1990-2008 Prepared by: Center for Economic Development University of Wisconsin-Milwaukee December 2010 For further information contact: Joel Rast UWM Center for Economic of a two-year study by the University of Wisconsin-Milwaukee Center for Economic Development (CED

Saldin, Dilano

293

Process of preparing tritiated porous silicon  

DOE Patents [OSTI]

A process of preparing tritiated porous silicon is described in which porous silicon is equilibrated with a gaseous vapor containing HT/T{sub 2} gas in a diluent for a time sufficient for tritium in the gas phase to replace hydrogen present in the pore surfaces of the porous silicon. 1 fig.

Tam, S.W.

1997-02-18T23:59:59.000Z

294

Process of preparing tritiated porous silicon  

DOE Patents [OSTI]

A process of preparing tritiated porous silicon in which porous silicon is equilibrated with a gaseous vapor containing HT/T.sub.2 gas in a diluent for a time sufficient for tritium in the gas phase to replace hydrogen present in the pore surfaces of the porous silicon.

Tam, Shiu-Wing (Downers Grove, IL)

1997-01-01T23:59:59.000Z

295

Prepared by Ryan T. Kennelly, Economic Analyst  

E-Print Network [OSTI]

Prepared by Ryan T. Kennelly, Economic Analyst Center for Business and Economic Research Lee Business School University of Nevada, Las Vegas October 2012 #12;The Center for Business and Economic new economic indexes for the metropolitan area of Las Vegas, Nevada. We first construct a coincident

Hemmers, Oliver

296

Conventional coal preparation in the United States  

SciTech Connect (OSTI)

Processing of bituminous and anthracite coal is widely practiced in the United States and, as mentioned earlier, about 80 percent of the production of these coals is processed as clean coal in preparation plants. Subbituminous coal is not widely processed, primarily because these low rank raw coals are low in sulfur (0.5 to 1.0 percent) and relatively low in ash (8 to 15 percent). They are also relatively low in heat content due to their high inherent moisture. Lignite coals, to the best of the authors{close_quote} knowledge, are not presently being processed in Conventional Coal Preparation plants. This is due to their unstable nature and putting them in water in a coal preparation plant is likely to cause severe degradation in particle size and add to their already high inherent moisture content. The following are the benefits of clean coal processing: produces a uniform product which can be utilized more efficiently; produces a higher quality product which results in higher efficiency at the power station or the steel mill; reduces sulfur dioxide and other adverse stack emissions during coal firing which is a very important environmental consideration; reduces ash or slag handling costs by the user; reduces shipping costs; and reduces handling and storage costs. Processing any stable raw coal in a coal preparation plant will always produce a higher grade product which is a more efficient and a more environmentally acceptable fuel for use at power stations, steel mills, home heating or industrial boilers.

Beck, M.K.; Taylor, B.

1993-12-31T23:59:59.000Z

297

Fluid sampling tool  

DOE Patents [OSTI]

A fluid sampling tool is described for sampling fluid from a container. The tool has a fluid collecting portion which is drilled into the container wall, thereby affixing it to the wall. The tool may have a fluid extracting section which withdraws fluid collected by the fluid collecting section. The fluid collecting section has a fluted shank with an end configured to drill a hole into a container wall. The shank has a threaded portion for tapping the borehole. The shank is threadably engaged to a cylindrical housing having an inner axial passageway sealed at one end by a septum. A flexible member having a cylindrical portion and a bulbous portion is provided. The housing can be slid into an inner axial passageway in the cylindrical portion and sealed to the flexible member. The bulbous portion has an outer lip defining an opening. The housing is clamped into the chuck of a drill, the lip of the bulbous section is pressed against a container wall until the shank touches the wall, and the user operates the drill. Wall shavings (kerf) are confined in a chamber formed in the bulbous section as it folds when the shank advances inside the container. After sufficient advancement of the shank, an o-ring makes a seal with the container wall. 6 figs.

Garcia, A.R.; Johnston, R.G.; Martinez, R.K.

1999-05-25T23:59:59.000Z

298

PHYSICAL PROPERTY MEASUREMENTS OF LABORATORY PREPARED SALTSTONE GROUT  

SciTech Connect (OSTI)

The Saltstone Production Facility (SPF) built two new Saltstone Disposal Units (SDU), SDU 3 and SDU 5, in 2013. The variable frequency drive (VFD) for the grout transfer hose pump tripped due to high current demand by the motor during the initial radioactive saltstone transfer to SDU 5B on 12/5/2013. This was not observed during clean cap processing on July 5, 2013 to SDU 3A, which is a slightly longer distance from the SPF than is SDU 5B. Saltstone Design Authority (SDA) is evaluating the grout pump performance and capabilities to transfer the grout processed in SPF to SDU 3/5. To assist in this evaluation, grout physical properties are required. At this time, there are no rheological data from the actual SPF so the properties of laboratory prepared samples using simulated salt solution or Tank 50 salt solution will be measured. The physical properties of grout prepared in the laboratory with de-ionized water (DI) and salt solutions were obtained at 0.60 and 0.59 water to premix (W/P) ratios, respectively. The yield stress of the DI grout was greater than any salt grout. The plastic viscosity of the DI grout was lower than all of the salt grouts (including salt grout with admixture). When these physical data were used to determine the pressure drop and fluid horsepower for steady state conditions, the salt grouts without admixture addition required a higher pressure drop and higher fluid horsepower to transport. When 0.00076 g Daratard 17/g premix was added, both the pressure drop and fluid horsepower were below that of the DI grout. Higher concentrations of Daratard 17 further reduced the pressure drop and fluid horsepower. The uncertainty in the single point Bingham Plastic parameters is + 4% of the reported values and is the bounding uncertainty. Two different mechanical agitator mixing protocols were followed for the simulant salt grout, one having a total mixing time of three minutes and the other having a time of 10 minutes. The Bingham Plastic parameters were essentially the same for the salt grout without admixture. When Daratard 17 was added, the Bingham Plastic yield stress increased for the 10 minute mix. The simulant salt used in this task had similar physical properties of the Tank 50 3Q13 salt grout and is recommended for future use, if the salt solution in Tank 50 does not change. The design basis physical properties used to size the pumps and mixers at SPF were obtained from DPST-85-312. The grouts characterized in this report are bounded by the design basis density and Bingham Plastic yield stress. The opposite is true for the plastic viscosity. Steady state pressure drop calculations were performed for the design basis values using the flow rate for the clean cap and salt grouts and they bound the pressure drop of the grouts characterized in this report. A comparison of the lab prepared samples to PI ProcessBook data, specifically average pressure drop, indicate that the lab prepared samples are more viscous in nature than what is processed in the facility. This difference could be due to the applied shear rates which could be lower in the lab as compared to the facility and that fact the SPF added flush water, making this comparison more difficult. A perfunctory review of the PI ProcessBook data was discussed. It may be possible that the frequency that the distributed control system alters the grout pump speed to maintain grout hopper volume can negatively affect the efficiency of the grout pump.

Hansen, E.; Cozzi, A.; Edwards, T.

2014-05-05T23:59:59.000Z

299

Fluid sampling tool  

DOE Patents [OSTI]

The invention includes a rotatable tool for collecting fluid through the wall of a container. The tool includes a fluid collection section with a cylindrical shank having an end portion for drilling a hole in the container wall when the tool is rotated, and a threaded portion for tapping the hole in the container wall. A passageway in the shank in communication with at least one radial inlet hole in the drilling end and an opening at the end of the shank is adapted to receive fluid from the container. The tool also includes a cylindrical chamber affixed to the end of the shank opposite to the drilling portion thereof for receiving and storing fluid passing through the passageway. The tool also includes a flexible, deformable gasket that provides a fluid-tight chamber to confine kerf generated during the drilling and tapping of the hole. The invention also includes a fluid extractor section for extracting fluid samples from the fluid collecting section.

Johnston, Roger G. (Los Alamos, NM); Garcia, Anthony R. E. (Espanola, NM); Martinez, Ronald K. (Santa Cruz, NM)

2001-09-25T23:59:59.000Z

300

Specified assurance level sampling procedure  

SciTech Connect (OSTI)

In the nuclear industry design specifications for certain quality characteristics require that the final product be inspected by a sampling plan which can demonstrate product conformance to stated assurance levels. The Specified Assurance Level (SAL) Sampling Procedure has been developed to permit the direct selection of attribute sampling plans which can meet commonly used assurance levels. The SAL procedure contains sampling plans which yield the minimum sample size at stated assurance levels. The SAL procedure also provides sampling plans with acceptance numbers ranging from 0 to 10, thus, making available to the user a wide choice of plans all designed to comply with a stated assurance level.

Willner, O.

1980-11-01T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

Tank 241-BY-104 vapor sampling and analysis tank characterization report  

SciTech Connect (OSTI)

Tank BY-104 headspace gas and vapor samples were collected and analyzed to help determine the potential risks to tank farm workers due to fugitive emissions from the tank. Tank BY-104 using the vapor sampling system (VSS) on June 24, 1994 by WHC Sampling and Mobile Laboratories. Air from the tank BY-104 headspace was withdrawn via a heated sampling probe mounted in riser 10A, and transferred via heated tubing to the VSS sampling manifold. Sampling media were prepared and analyzed by WHC, Oak Ridge National Laboratories, Pacific Northwest Laboratories, and Oregon Graduate Institute of Science and Technology through a contract with Sandia National Laboratories. The 46 tank air samples and 2 ambient air control samples collected are listed in Table X-1 by analytical laboratory. Table X-1 also lists the 10 trip blanks provided by the laboratories.

Huckaby, J.L.

1995-05-10T23:59:59.000Z

302

Preparation of fullerene/glass composites  

DOE Patents [OSTI]

Synthesis of fullerene/glass composites is described. A direct method for preparing solid solutions of C{sub 60} in silicon dioxide (SiO{sub 2}) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these ``guests`` in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C{sub 60}. Depending upon the preparative procedure, C{sub 60} dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C{sub 60} in a solid glass matrix, is generated by the present method.

Mattes, B.R.; McBranch, D.W.; Robinson, J.M.; Koskelo, A.C.; Love, S.P.

1995-05-30T23:59:59.000Z

303

Novel hard compositions and methods of preparation  

DOE Patents [OSTI]

Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value.

Sheinberg, H.

1981-02-03T23:59:59.000Z

304

Preparation of fullerene/glass composites  

DOE Patents [OSTI]

Synthesis of fullerene/glass composites. A direct method for preparing solid solutions of C.sub.60 in silicon dioxide (SiO.sub.2) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these "guests" in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C.sub.60. Depending upon the preparative procedure, C.sub.60 dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C.sub.60 in a solid glass matrix, is generated by the present method.

Mattes, Benjamin R. (Santa Fe, NM); McBranch, Duncan W. (Santa Fe, NM); Robinson, Jeanne M. (Los Alamos, NM); Koskelo, Aaron C. (Los Alamos, NM); Love, Steven P. (Los Alamos, NM)

1995-01-01T23:59:59.000Z

305

Prepared for the U.S. Department of Energy under Contract DE-AC05-76RL01830  

E-Print Network [OSTI]

panels, battery banks, and sampling units. During an approximate four month performance evaluation periodPNNL-22900 Prepared for the U.S. Department of Energy under Contract DE-AC05-76RL01830 Solar-22900 Solar Powered Radioactive Air Monitoring Stations JM Barnett TL Gervais LE Bisping October 2013

306

Sampling for Bacteria in Wells  

E-Print Network [OSTI]

This publication will instruct you on the proper procedures for collecting a sample from a water well for bacteriological analysis....

Lesikar, Bruce J.

2001-11-15T23:59:59.000Z

307

Sample Residential Program Term Sheet  

Broader source: Energy.gov (indexed) [DOE]

Goal DRAFT U.S. DOE Sample Residential Program Term Sheet - DRAFT Introduction is seeking to develop an energy...

308

Rapid Microwave Preparation of Highly Efficient Ce[superscript 3+]-Substituted Garnet Phosphors for Solid State White Lighting  

SciTech Connect (OSTI)

Ce{sup 3+}-substituted aluminum garnet compounds of yttrium (Y{sub 3}Al{sub 5}O{sub 12}) and lutetium (Lu{sub 3}Al{sub 5}O{sub 12}) - both important compounds in the generation of (In,Ga)N-based solid state white lighting - have been prepared using a simple microwave heating technique involving the use of a microwave susceptor to provide the initial heat source. Carbon used as the susceptor additionally creates a reducing atmosphere around the sample that helps stabilize the desired luminescent compound. High quality, phase-pure materials are prepared within a fraction of the time and using a fraction of the energy required in a conventional ceramic preparation; the microwave technique allows for a reduction of about 95% in preparation time, making it possible to obtain phase pure, Ce{sup 3+}-substituted garnet compounds in under 20 min of reaction time. It is estimated that the overall reduction in energy compared with ceramic routes as practiced in the lab is close to 99%. Conventionally prepared material is compared with material prepared using microwave heating in terms of structure, morphology, and optical properties, including quantum yield and thermal quenching of luminescence. Finally, the microwave-prepared compounds have been incorporated into light-emitting diode 'caps' to test their performance characteristics in a real device, in terms of their photon efficiency and color coordinates.

Birkel, Alexander; Denault, Kristin A.; George, Nathan C.; Doll, Courtney E.; Héry, Bathylle; Mikhailovsky, Alexander A.; Birkel, Christina S.; Hong, Byung-Chul; Seshadri, Ram (UCSB); (Mitsubishi)

2012-04-30T23:59:59.000Z

309

Preparation and structure of hexagonal molybdenum trioxide  

SciTech Connect (OSTI)

The phase widely known as hexagonal MoO/sub 3/ is shown to correspond to the dehydrated and de-ammoniated decamolybdate. The latter material has the ideal stoichiometry NH/sub 4/Mo/sub 5/ O/sub 15/OH x 2H/sub 2/O. Relationships between a variety of materials with the decamolybdate structure are discussed. A novel preparative route to ammonium decamolybdate is described.

Caiger, N.A.; Crouch-Baker, S.; Dickens, P.G.; James, G.S.

1987-04-01T23:59:59.000Z

310

Method for preparing porous metal hydride compacts  

DOE Patents [OSTI]

A method for preparing porous metallic-matrix hydride compacts which can be repeatedly hydrided and dehydrided without disintegration. A mixture of a finely divided metal hydride and a finely divided matrix metal is contacted with a poison which prevents the metal hydride from dehydriding at room temperature and atmospheric pressure. The mixture of matrix metal and poisoned metal hydride is then compacted under pressure at room temperature to form porous metallic-matrix hydride compacts.

Ron, M.; Gruen, D.M.; Mendelsohn, M.H.; Sheft, I.

1980-01-21T23:59:59.000Z

311

LEAM Film Development Test Report Prepared by  

E-Print Network [OSTI]

Solar Test Test Item No. l Film Development Tests Test Item No. 2 Film Development Tests Test Item No. 3~~ ··········~~~ LEAM Film Development Test Report Prepared by: R. Sii'r'...ms ~1 rf\\:'3· ~ ij ATM Film Development Test Report -~~'·.· ··..· .··. . ~...=-~ ~ IWitJY~W ' ~· CONTENTS 1. PURPOSE 2. SCOPE

Rathbun, Julie A.

312

Process for preparing improved silvered glass mirrors  

DOE Patents [OSTI]

Glass mirrors having improved weathering properties are prepared by an improvement in the process for making the mirrors. The glass surface after it has been cleaned but before it is silvered, is contacted with a solution of lanthanide rare earths in addition to a sensitization solution of tin or palladium. The addition of the rare earths produces a mirror which has increased resistance to delamination of the silver from the glass surface in the presence of water.

Buckwalter, C.Q. Jr.

1980-01-28T23:59:59.000Z

313

Method for preparing porous metal hydride compacts  

DOE Patents [OSTI]

A method for preparing porous metallic-matrix hydride compacts which can be repeatedly hydrided and dehydrided without disintegration. A mixture of a finely divided metal hydride and a finely divided matrix metal is contacted with a poison which prevents the metal hydride from dehydriding at room temperature and atmospheric pressure. The mixture of matrix metal and poisoned metal hydride is then compacted under pressure at room temperature to form porous metallic-matrix hydride compacts.

Ron, Moshe (Haifa, IL); Gruen, Dieter M. (Downers Grove, IL); Mendelsohn, Marshall H. (Woodridge, IL); Sheft, Irving (Oak Park, IL)

1981-01-01T23:59:59.000Z

314

Characterization Of Sample HTF-13-13-128  

SciTech Connect (OSTI)

Savannah River Remediation (SRR) has requested that Savannah River National Laboratory (SRNL) characterize a sample of Tank 13 in preparation for Sludge Batch 9 (SB9). A 200 mL sample of Tank 13 was received by SRNL on July 22, 2013 (Tank Farm sample ID HTF-13-13-128). Characterization of the sample to meet the requirements of the request is complete. Results include: visual observations; slurry and supernatant density; weight percent total and insoluble solids; supernatant characterization; total alpha, total beta, and several radionuclide analyses; and elemental analyses of the dried solids. The sample was very fluid. After settling overnight, there was a small layer of solids on the bottom of the sample container (a 250 mL HDPE bottle) with the remainder being clear supernatant. To better show the sludge solids relative to the overall sample, 25 mL of slurry was placed in a graduated cylinder and allowed to settle over a weekend (approximately 90 hours). The sludge layer was at the approximately 4 mL. The small visually observed quantity of insoluble solids was confirmed with a low weight percent insoluble solids of 0.94%.

Pareizs, J. M.

2013-09-25T23:59:59.000Z

315

RAPID DETERMINATION OF RA-226 IN ENVIRONMENTAL SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of {sup 226}Ra in environmental samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used for emergency response or routine sample analyses. The need for rapid analyses in the event of a Radiological Dispersive Device or Improvised Nuclear Device event is well-known. In addition, the recent accident at Fukushima Nuclear Power Plant in March, 2011 reinforces the need to have rapid analyses for radionuclides in environmental samples in the event of a nuclear accident. {sup 226}Ra (T1/2 = 1,620 years) is one of the most toxic of the long-lived alpha-emitters present in the environment due to its long life and its tendency to concentrate in bones, which increases the internal radiation dose of individuals. The new method to determine {sup 226}Ra in environmental samples utilizes a rapid sodium hydroxide fusion method for solid samples, calcium carbonate precipitation to preconcentrate Ra, and rapid column separation steps to remove interferences. The column separation process uses cation exchange resin to remove large amounts of calcium, Sr Resin to remove barium and Ln Resin as a final purification step to remove {sup 225}Ac and potential interferences. The purified {sup 226}Ra sample test sources are prepared using barium sulfate microprecipitation in the presence of isopropanol for counting by alpha spectrometry. The method showed good chemical recoveries and effective removal of interferences. The determination of {sup 226}Ra in environmental samples can be performed in less than 16 h for vegetation, concrete, brick, soil, and air filter samples with excellent quality for emergency or routine analyses. The sample preparation work takes less than 6 h. {sup 225}Ra (T1/2 = 14.9 day) tracer is used and the {sup 225}Ra progeny {sup 217}At is used to determine chemical yield via alpha spectrometry. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory radium particles are effectively digested. The preconcentration and column separation steps can also be applied to aqueous samples with good results.

Maxwell, S.

2012-01-03T23:59:59.000Z

316

Sampling for Beryllium Surface Contamination using Wet, Dry and Alcohol Wipe Sampling  

SciTech Connect (OSTI)

This research project was conducted at the National Nuclear Security Administration's Kansas City Plant, operated by Honeywell Federal Manufacturing and Technologies, in conjunction with the Safety Sciences Department of Central Missouri State University, to compare relative removal efficiencies of three wipe sampling techniques currently used at Department of Energy facilities. Efficiencies of removal of beryllium contamination from typical painted surfaces were tested by wipe sampling with dry Whatman 42 filter paper, with water-moistened (Ghost Wipe) materials, and by methanol-moistened wipes. Test plates were prepared using 100 mm X 15 mm Pyrex Petri dishes with interior surfaces spray painted with a bond coat primer. To achieve uniform deposition over the test plate surface, 10 ml aliquots of solution containing 1 beryllium and 0.1 ml of metal working fluid were transferred to the test plates and subsequently evaporated. Metal working fluid was added to simulate the slight oiliness common on surfaces in metal working shops where fugitive oil mist accumulates over time. Sixteen test plates for each wipe method (dry, water, and methanol) were processed and sampled using a modification of wiping patterns recommended by OSHA Method 125G. Laboratory and statistical analysis showed that methanol-moistened wipe sampling removed significantly more (about twice as much) beryllium/oil-film surface contamination as water-moistened wipes (p< 0.001), which removed significantly more (about twice as much) residue as dry wipes (p <0.001). Evidence for beryllium sensitization via skin exposure argues in favor of wipe sampling with wetting agents that provide enhanced residue removal efficiency.

Kerr, Kent

2004-12-17T23:59:59.000Z

317

HEART SMART NUTRITION Prepare Food Right--Ensure It's Light  

E-Print Network [OSTI]

Lesson 4 HEART SMART NUTRITION Prepare Food Right--Ensure It's Light To prepare foods lower in fat Heart Smart? True or False ______ 1. A cholesterol- free product is also fat-free. True or False

318

Arkansas Preparing for Wind Power | Department of Energy  

Broader source: Energy.gov (indexed) [DOE]

Arkansas Preparing for Wind Power Arkansas Preparing for Wind Power April 15, 2010 - 5:25pm Addthis Joshua DeLung Renowned science fiction author Isaac Asimov once said, "No...

319

RAPID DETERMINATION OF {sup 210} PO IN WATER SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that can be used for emergency response or routine water analyses. If a radiological dispersive device (RDD) event or a radiological attack associated with drinking water supplies occurs, there will be an urgent need for rapid analyses of water samples, including drinking water, ground water and other water effluents. Current analytical methods for the assay of {sup 210}Po in water samples have typically involved spontaneous auto-deposition of {sup 210}Po onto silver or other metal disks followed by counting by alpha spectrometry. The auto-deposition times range from 90 minutes to 24 hours or more, at times with yields that may be less than desirable. If sample interferences are present, decreased yields and degraded alpha spectrums can occur due to unpredictable thickening in the deposited layer. Separation methods have focused on the use of Sr Resin?, often in combination with 210Pb analysis. A new rapid method for {sup 210}Po in water samples has been developed at the Savannah River National Laboratory (SRNL) that utilizes a rapid calcium phosphate co-precipitation method, separation using DGA Resin? (N,N,N?,N? tetraoctyldiglycolamide extractant-coated resin, Eichrom Technologies or Triskem-International), followed by rapid microprecipitation of {sup 210}Po using bismuth phosphate for counting by alpha spectrometry. This new method can be performed quickly with excellent removal of interferences, high chemical yields and very good alpha peak resolution, eliminating any potential problems with the alpha source preparation for emergency or routine samples. A rapid sequential separation method to separate {sup 210} Po and actinide isotopes was also developed. This new approach, rapid separation with DGA Resin plus microprecipitation for alpha source preparation, is a significant advance in radiochemistry for the rapid determination of {sup 210}Po.

Maxwell, S.

2013-05-22T23:59:59.000Z

320

advanced coal preparation: Topics by E-print Network  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

... 15 1.6.2 Implement advanced clean coal technologies for production of energy products ... 15 An SAIC Report Prepared...

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

Post-Award Deliverables Sample (Second Part of Sample Deliverables...  

Broader source: Energy.gov (indexed) [DOE]

Task Orders (IDIQ Attachment. J-4) Sample Statement of Work - Standard Service Offerings for Contractor-Identified Project ESPC TASK ORDER REQUEST FOR PROPOSAL (TO RFP) TEMPLATE...

322

AGAROSE GEL PREPARATION AND DNA QUANTIFICATION  

E-Print Network [OSTI]

/µL concentration from the stock solution available 2. E.g., Promega, comes in a concentration of 450 ng/µL solution, to make a 2 ng/µL (prepare: Stock lambda (450 ng/µL) = 4.45 µL 3:1 buffer (TE:5X dye) = 995.55µL StoreL of each lambda (10, 25, 50ng) in the first 3 wells, which will serve as standards. 5. Take 1 µL of total

Gill, Kulvinder

323

Process for preparing silicon carbide foam  

DOE Patents [OSTI]

A method of preparing near net shape, monolithic, porous SiC foams is disclosed. Organosilicon precursors are used to produce polymeric gels by thermally induced phase separation, wherein, a sufficiently concentrated solution of an organosilicon polymer is cooled below its solidification temperature to form a gel. Following solvent removal from the gel, the polymer foam is pretreated in an oxygen plasma in order to raise its glass transition temperature. The pretreated foam is then pyrolyzed in an inert atmosphere to form a SiC foam. 9 figs.

Whinnery, L.L.; Nichols, M.C.; Wheeler, D.R.; Loy, D.A.

1997-09-16T23:59:59.000Z

324

Process for preparing silicon carbide foam  

DOE Patents [OSTI]

A method of preparing near net shape, monolithic, porous SiC foams is disclosed. Organosilicon precursors are used to produce polymeric gels by thermally induced phase separation, wherein, a sufficiently concentrated solution of an organosilicon polymer is cooled below its solidification temperature to form a gel. Following solvent removal from the gel, the polymer foam is pretreated in an oxygen plasma in order to raise its glass transition temperature. The pretreated foam is then pyrolized in an inert atmosphere to form a SiC foam.

Whinnery, LeRoy Louis (Livermore, CA); Nichols, Monte Carl (Livermore, CA); Wheeler, David Roger (Albuquerque, NM); Loy, Douglas Anson (Albuquerque, NM)

1997-01-01T23:59:59.000Z

325

Improved method for preparing rare earth sesquichalcogenides  

DOE Patents [OSTI]

An improved method for the preparation of high purity rare earth sesquichalcogenides is described. The rare earth, as one or more pieces of the metal, is sealed under a vacuum with a stoichiometric amount of sulfur or selenium and a small amount of iodine into a quartz reaction vessel. The sealed vessel is then heated to above the vaporization temperature of the chalcogen and below the melting temperature of the rare earth metal and maintained until the product has been formed. The iodine is then vaporized off leaving a pure product. The rare earth sulfides and selenides thus formed are useful as semiconductors and as thermoelectric generators. 3 tables.

Takeshita, T.; Beaudry, B.J.; Gschneidner, K.A. Jr.

1982-04-14T23:59:59.000Z

326

Method for preparing high purity vanadium  

DOE Patents [OSTI]

A method for preparing high purity vanadium having a low silicon content has been developed. Vanadium pentoxide is reduced with a stoichiometric, or slightly deficient amount of aluminum to produce a vanadium-aluminum alloy containing an excess of oxygen. Silicon is removed by electron-beam melting the alloy under oxidizing conditions to promote the formation of SiO which is volatile at elevated temperatures. Excess oxygen is removed by heating the alloy in the presence of calcium metal to form calcium oxide.

Schmidt, Frederick (Ames, IA); Carlson, O. Norman (Ames, IA)

1986-09-09T23:59:59.000Z

327

Method for preparing high purity vanadium  

DOE Patents [OSTI]

A method for preparing high purity vanadium having a low silicon content has been developed. Vanadium pentoxide is reduced with a stoichiometric, or slightly deficient amount of aluminum to produce a vanadium-aluminum alloy containing an excess of oxygen. Silicon is removed by electron-beam melting the alloy under oxidizing conditions to promote the formation of SiO which is volatile at elevated temperatures. Excess oxygen is removed by heating the alloy in the presence of calcium metal to form calcium oxide.

Schmidt, F.; Carlson, O.N.

1984-05-16T23:59:59.000Z

328

Preparation of thorium-uranium gel spheres  

SciTech Connect (OSTI)

Ceramic oxide spheres with diameters of 15 to 1500 ..mu..m are being evaluated for fabrication of power reactor fuel rods. (Th,U)O/sub 2/ spheres can be prepared by internal or external chemical gelation of nitrate solutions or oxide sols. Two established external gelation techniques were tested but proved to be unsatisfactory for the intended application. Established internal gelation techniques for UO/sub 2/ spheres were applied with minor modifications to make 75% ThO/sub 2/-25% UO/sub 2/ spheres that sinter to diameters of 200 to 1400 ..mu..m (99% T.D.).

Spence, R.D.; Haas, P.A.

1980-01-01T23:59:59.000Z

329

Preparation of diallyl phthalate prepolymer solutions  

SciTech Connect (OSTI)

A process is claimed for preparing prepolymers of a diallyl phthalate at room temperature. The process is characterized by the fact that the solution of a diallyl phthalate alone or a diallyl phthalate and another copolymerizable monomer, in a liquid ketone at ambient temperature, is heated in the presence of a free radical-forming catalyst, preferably hydrogen peroxide, as well as in the presence of a small amount of a strong acid until at least 60% and advantageously at least 90% of the monomer initially present has been converted to the prepolymer.

Not Available

1982-12-01T23:59:59.000Z

330

Method to prepare nanoparticles on porous mediums  

DOE Patents [OSTI]

A method to prepare porous medium decorated with nanoparticles involves contacting a suspension of nanoparticles in an ionic liquid with a porous medium such that the particles diffuse into the pores of the medium followed by heating the resulting composition to a temperature equal to or greater than the thermal decomposition temperature of the ionic liquid resulting in the removal of the liquid portion of the suspension. The nanoparticles can be a metal, an alloy, or a metal compound. The resulting compositions can be used as catalysts, sensors, or separators.

Vieth, Gabriel M. (Knoxville, TN) [Knoxville, TN; Dudney, Nancy J. (Oak Ridge, TN) [Oak Ridge, TN; Dai, Sheng (Knoxville, TN) [Knoxville, TN

2010-08-10T23:59:59.000Z

331

Conductive ceramic composition and method of preparation  

DOE Patents [OSTI]

A ceramic anode composition is formed of a multivalent metal oxide or oxygenate such as an alkali metal, transition metal oxygenate. The anode is prepared as a non-stoichiometric crystalline structure by reaction and conditioning in a hydrogen gas cover containing minor proportions of carbon dioxide and water vapor. The structure exhibits a single phase and substantially enhanced electrical conductivity over that of the corresponding stoichiometric structure. Unexpectedly, such oxides and oxygenates are found to be stable in the reducing anode fuel gas of a molten carbonate fuel cell.

Smith, James L. (Lemont, IL); Kucera, Eugenia H. (Downers Grove, IL)

1991-01-01T23:59:59.000Z

332

Preparation of Papers for AIAA Technical Conferences  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 - SeptemberMicroneedles for medical point07.06 AgendaPreparation for a

333

Preparation, Characterization, and Catalytic Properties of Tungsten  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 - SeptemberMicroneedles for medical point07.06 AgendaPreparation forTrioxide Cyclic

334

Preparation of reactive beta-dicalcium silicate  

DOE Patents [OSTI]

This invention relates to the preparation of fine particles of reactive beta-dicalcium silicate by means of a solid state process which comprises firing a mixture of calcium sulfate, silica and a reducing additive selected from the group consisting of calcium sulfide, carbon, carbon monoxide, methane and hydrogen, at a temperature of about 850.degree.-1000.degree. C. A carrier gas such as nitrogen or carbon dioxide may also be added, if desired. A high concentration of sulfur dioxide is a by-product of this process.

Shen, Ming-Shing (Laramie, WY, NJ); Chen, James M. (Rahway, NJ); Yang, Ralph T. (Amherst, NY)

1982-01-01T23:59:59.000Z

335

Preparation of reactive beta-dicalcium silicate  

DOE Patents [OSTI]

This invention relates to the preparation of fine particles of reactive beta-dicalcium silicate by means of a solid state process which comprises firing a mixture of calcium sulfate, silica, and a reducing additive selected from the group consisting of calcium sulfide, carbon, carbon monoxide, methane, and hydrogen, at a temperature of about 850 to 1000/sup 0/C. A carrier gas such as nitrogen or carbon dioxide may also be added, if desired. A high concentration of sulfur dioxide is a by-product of this process.

Shen, M.S.; Chen, J.M.; Yang, R.T.

1980-02-28T23:59:59.000Z

336

Conductive ceramic composition and method of preparation  

DOE Patents [OSTI]

A ceramic anode composition is formed of a multivalent metal oxide or oxygenate such as an alkali metal, transition metal oxygenate. The anode is prepared as a non-stoichiometric crystalline structure by reaction and conditioning in a hydrogen gas cover containing minor proportions of carbon dioxide and water vapor. The structure exhibits a single phase and substantially enhanced electrical conductivity over that of the corresponding stoichiometric structure. Unexpectedly, such oxides and oxygenates are found to be stable in the reducing anode fuel gas of a molten carbonate fuel cell. 4 figures.

Smith, J.L.; Kucera, E.H.

1991-04-16T23:59:59.000Z

337

Analysis Of The Tank 6F Final Characterization Samples-2012  

SciTech Connect (OSTI)

The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm-243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

Oji, L. N.; Diprete, D. P.; Coleman, C. J.; Hay, M. S.; Shine, E. P.

2012-09-27T23:59:59.000Z

338

ANALYSIS OF THE TANK 6F FINAL CHARACTERIZATION SAMPLES-2012  

SciTech Connect (OSTI)

The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm-243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

Oji, L.; Diprete, D.; Coleman, C.; Hay, M.; Shine, G.

2012-06-28T23:59:59.000Z

339

Analysis of the Tank 6F Final Characterization Samples-2012  

SciTech Connect (OSTI)

The Savannah River National Laboratory (SRNL) was requested by Savannah River Remediation (SRR) to provide sample preparation and analysis of the Tank 6F final characterization samples to determine the residual tank inventory prior to grouting. Fourteen residual Tank 6F solid samples from three areas on the floor of the tank were collected and delivered to SRNL between May and August 2011. These Tank 6F samples were homogenized and combined into three composite samples based on a proportion compositing scheme and the resulting composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 6F composite samples include bulk density and water leaching of the solids to account for water soluble components. The composite Tank 6F samples were analyzed and the data reported in triplicate. Sufficient quality assurance standards and blanks were utilized to demonstrate adequate characterization of the Tank 6F samples. The main evaluation criteria were target detection limits specified in the technical task request document. While many of the target detection limits were met for the species characterized for Tank 6F some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The isotopes whose detection limits were not met in all cases included Sn-126, Sb-126, Sb-126m, Eu-152, Cm- 243 and Cf-249. SRNL, in conjunction with the customer, reviewed all of these cases and determined that the impacts of not meeting the target detection limits were acceptable. Based on the analyses of variance (ANOVA) for the inorganic constituents of Tank 6F, all the inorganic constituents displayed heterogeneity. The inorganic results demonstrated consistent differences across the composite samples: lowest concentrations for Composite Sample 1, intermediate-valued concentrations for Composite Sample 2, and highest concentrations for Composite Sample 3. The Hg and Mo results suggest possible measurement outliers. However, the magnitudes of the differences between the Hg 95% upper confidence limit (UCL95) results with and without the outlier and the magnitudes of the differences between the Mo UCL95 results with and without the outlier do not appear to have practical significance. It is recommended to remove the potential measurement outliers. Doing so is conservative in the sense of producing a higher UCL95 for Hg and Mo than if the potential outliers were included in the calculations. In contrast to the inorganic results, most of the radionuclides did not demonstrate heterogeneity among the three Tank 6F composite sample characterization results.

Oji, L. N.; Diprete, D. P.; Coleman, C. J.; Hay, M. S.; Shine, E. P.

2013-01-31T23:59:59.000Z

340

Characterization Results For The 2013 HTF 3H Evaporator Overhead Samples  

SciTech Connect (OSTI)

This report tabulates the radiochemical analysis of the 3H evaporator overhead sample for {sup 137}Cs, {sup 90}Sr, and {sup 129}I to meet the requirements in the Effluent Treatment Project (ETP) Waste Acceptance Criteria (WAC) (rev. 6). This report identifies the sample receipt date, preparation method, and analysis performed in the accumulation of the listed values. All data was found to be within the ETP WAC (rev. 6) specification for the Waste Water Collection Tanks (WWCT).

Washington, A. L. II

2013-12-04T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Method for the concentration and separation of actinides from biological and environmental samples  

DOE Patents [OSTI]

A method and apparatus for the quantitative recover of actinide values from biological and environmental sample by passing appropriately prepared samples in a mineral acid solution through a separation column of a dialkyl(phenyl)-N,N-dialylcarbamoylmethylphosphine oxide dissolved in tri-n-butyl phosphate on an inert substrate which selectively extracts the actinide values. The actinide values can be eluted either as a group or individually and their presence quantitatively detected by alpha counting. 3 figs.

Horwitz, E.P.; Dietz, M.L.

1989-05-30T23:59:59.000Z

342

Acceptance sampling using judgmental and randomly selected samples  

SciTech Connect (OSTI)

We present a Bayesian model for acceptance sampling where the population consists of two groups, each with different levels of risk of containing unacceptable items. Expert opinion, or judgment, may be required to distinguish between the high and low-risk groups. Hence, high-risk items are likely to be identifed (and sampled) using expert judgment, while the remaining low-risk items are sampled randomly. We focus on the situation where all observed samples must be acceptable. Consequently, the objective of the statistical inference is to quantify the probability that a large percentage of the unsampled items in the population are also acceptable. We demonstrate that traditional (frequentist) acceptance sampling and simpler Bayesian formulations of the problem are essentially special cases of the proposed model. We explore the properties of the model in detail, and discuss the conditions necessary to ensure that required samples sizes are non-decreasing function of the population size. The method is applicable to a variety of acceptance sampling problems, and, in particular, to environmental sampling where the objective is to demonstrate the safety of reoccupying a remediated facility that has been contaminated with a lethal agent.

Sego, Landon H.; Shulman, Stanley A.; Anderson, Kevin K.; Wilson, John E.; Pulsipher, Brent A.; Sieber, W. Karl

2010-09-01T23:59:59.000Z

343

Adaptive Sampling for Environmental Robotics  

E-Print Network [OSTI]

186, 2003. S. Thrun, “Robotics Mapping: A survey”, Exploringtechnique to environmental robotics applications includingSampling for Environmental Robotics Mohammad Rahimi †,‡‡ ,

Mohammad Rahimi; Richard Pon; Deborah Estrin; William J. Kaiser; Mani Srivastava; Gaurav S. Sukhatme

2003-01-01T23:59:59.000Z

344

Sample Residential Program Term Sheet  

Broader source: Energy.gov [DOE]

A sample for defining and elaborating on the specifics of a clean energy loan program. Author: U.S. Department of Energy

345

Homeowner Soil Sample Information Form  

E-Print Network [OSTI]

Homeowners should submit this form with their soil samples when requesting a soil test from the Texas A&M Soil Testing Laboratory....

Provin, Tony

2007-04-11T23:59:59.000Z

346

Novel hard compositions and methods of preparation  

DOE Patents [OSTI]

Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value. Photomicrographs show that the shapes of the grains of the alloy mixture with which the minor amount of carbide (or carbide-formers) is mixed are radically altered from large, rounded to small, very angular by the addition of the carbide. Superiority of one of these hard compositions of matter over cobalt-bonded tungsten carbide for ultra-high pressure anvil applications was demonstrated. 3 figs.

Sheinberg, H.

1983-08-23T23:59:59.000Z

347

Novel hard compositions and methods of preparation  

DOE Patents [OSTI]

Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value. Photomicrographs show that the shapes of the grains of the alloy mixture with which the minor amount of carbide (or carbide-formers) is mixed are radically altered from large, rounded to small, very angular by the addition of the carbide. Superiority of one of these hard compositions of matter over cobalt-bonded tungsten carbide for ultra-high pressure anvil applications was demonstrated.

Sheinberg, Haskell (Los Alamos, NM)

1983-08-23T23:59:59.000Z

348

Guide to preparing SAND reports and other communication products.  

SciTech Connect (OSTI)

This guide describes the R&A process, Common Look and Feel requirements, and preparation and publishing procedures for communication products at Sandia National Laboratories. Samples of forms and examples of published communications products are provided. This guide takes advantage of the wealth of material now available on the Web as a resource. Therefore, it is best viewed as an electronic document. If some of the illustrations are too small to view comfortably, you can enlarge them on the screen as needed. The format of this document is considerably different than that usually expected of a SAND Report. It was selected to permit the large number of illustrations and examples to be placed closer to the text that references them. In the case of forms, covers, and other items that are included as examples, a link to the Web is provided so that you can access the items and download them for use. This guide details the processes for producing a variety of communication products at Sandia National Laboratories. Figure I-1 shows the general publication development process. Because extensive supplemental material is available from Sandia on the internal web or from external sources (Table I-1), the guide has been shortened to make it easy to find information that you need.

Not Available

2011-09-01T23:59:59.000Z

349

Defining And Characterizing Sample Representativeness For DWPF Melter Feed Samples  

SciTech Connect (OSTI)

Representative sampling is important throughout the Defense Waste Processing Facility (DWPF) process, and the demonstrated success of the DWPF process to achieve glass product quality over the past two decades is a direct result of the quality of information obtained from the process. The objective of this report was to present sampling methods that the Savannah River Site (SRS) used to qualify waste being dispositioned at the DWPF. The goal was to emphasize the methodology, not a list of outcomes from those studies. This methodology includes proven methods for taking representative samples, the use of controlled analytical methods, and data interpretation and reporting that considers the uncertainty of all error sources. Numerous sampling studies were conducted during the development of the DWPF process and still continue to be performed in order to evaluate options for process improvement. Study designs were based on use of statistical tools applicable to the determination of uncertainties associated with the data needs. Successful designs are apt to be repeated, so this report chose only to include prototypic case studies that typify the characteristics of frequently used designs. Case studies have been presented for studying in-tank homogeneity, evaluating the suitability of sampler systems, determining factors that affect mixing and sampling, comparing the final waste glass product chemical composition and durability to that of the glass pour stream sample and other samples from process vessels, and assessing the uniformity of the chemical composition in the waste glass product. Many of these studies efficiently addressed more than one of these areas of concern associated with demonstrating sample representativeness and provide examples of statistical tools in use for DWPF. The time when many of these designs were implemented was in an age when the sampling ideas of Pierre Gy were not as widespread as they are today. Nonetheless, the engineers and statisticians used carefully thought out designs that systematically and economically provided plans for data collection from the DWPF process. Key shared features of the sampling designs used at DWPF and the Gy sampling methodology were the specification of a standard for sample representativeness, an investigation that produced data from the process to study the sampling function, and a decision framework used to assess whether the specification was met based on the data. Without going into detail with regard to the seven errors identified by Pierre Gy, as excellent summaries are readily available such as Pitard [1989] and Smith [2001], SRS engineers understood, for example, that samplers can be biased (Gy?s extraction error), and developed plans to mitigate those biases. Experiments that compared installed samplers with more representative samples obtained directly from the tank may not have resulted in systematically partitioning sampling errors into the now well-known error categories of Gy, but did provide overall information on the suitability of sampling systems. Most of the designs in this report are related to the DWPF vessels, not the large SRS Tank Farm tanks. Samples from the DWPF Slurry Mix Evaporator (SME), which contains the feed to the DWPF melter, are characterized using standardized analytical methods with known uncertainty. The analytical error is combined with the established error from sampling and processing in DWPF to determine the melter feed composition. This composition is used with the known uncertainty of the models in the Product Composition Control System (PCCS) to ensure that the wasteform that is produced is comfortably within the acceptable processing and product performance region. Having the advantage of many years of processing that meets the waste glass product acceptance criteria, the DWPF process has provided a considerable amount of data about itself in addition to the data from many special studies. Demonstrating representative sampling directly from the large Tank Farm tanks is a difficult, if not unsolvable enterprise due to li

Shine, E. P.; Poirier, M. R.

2013-10-29T23:59:59.000Z

350

Comparison of different pressing techniques for the preparation of n-type silicon-germanium thermoelectric alloys  

SciTech Connect (OSTI)

Improvements to state-of-the-art Si{sub 80}Ge{sub 20} thermoelectric alloys have been observed in laboratory-scale samples by the powder metallurgy techniques of mechanical alloying and hot pressing. Incorporating these improvements in large scale compacts for the production of thermoelectric generator elements is the next step in achieving higher efficiency RTGs. This paper discusses consolidation of large quantities of mechanically alloyed powders into production size compacts. Differences in thermoelectric properties are noted between the compacts prepared by the standard technique of hot uniaxial pressing and hot isostatic pressing. Most significant is the difference in carrier concentration between the alloys prepared by the two consolidation techniques.

Harringa, J.L.; Cook, B.A.

1996-06-01T23:59:59.000Z

351

Ambient pressure process for preparing aerogel thin films reliquified sols useful in preparing aerogel thin films  

DOE Patents [OSTI]

A method for preparing aerogel thin films by an ambient-pressure, continuous process. The method of this invention obviates the use of an autoclave and is amenable to the formation of thin films by operations such as dip coating. The method is less energy intensive and less dangerous than conventional supercritical aerogel processing techniques.

Brinker, Charles Jeffrey (Albuquerque, NM); Prakash, Sai Sivasankaran (Minneapolis, MN)

1999-01-01T23:59:59.000Z

352

ANALYSIS OF THE TANK 5F FINAL CHARATERIZATION SAMPLES-2011  

SciTech Connect (OSTI)

The Savannah River National Laboratory (SRNL) was requested by SRR to provide sample preparation and analysis of the Tank 5F final characterization samples to determine the residual tank inventory prior to grouting. Two types of samples were collected and delivered to SRNL: floor samples across the tank and subsurface samples from mounds near risers 1 and 5 of Tank 5F. These samples were taken from Tank 5F between January and March 2011. These samples from individual locations in the tank (nine floor samples and six mound Tank 5F samples) were each homogenized and combined in a given proportion into 3 distinct composite samples to mimic the average composition in the entire tank. These Tank 5F composite samples were analyzed for radiological, chemical and elemental components. Additional measurements performed on the Tank 5F composite samples include bulk density and water leaching of the solids to account for water soluble species. With analyses for certain challenging radionuclides as the exception, all composite Tank 5F samples were analyzed and reported in triplicate. The target detection limits for isotopes analyzed were based on customer desired detection limits as specified in the technical task request documents. SRNL developed new methodologies to meet these target detection limits and provide data for the extensive suite of components. While many of the target detection limits were met for the species characterized for Tank 5F, as specified in the technical task request, some were not met. In a few cases, the relatively high levels of radioactive species of the same element or a chemically similar element precluded the ability to measure some isotopes to low levels. The Technical Task Request allows that while the analyses of these isotopes is needed, meeting the detection limits for these isotopes is a lower priority than meeting detection limits for the other specified isotopes. The isotopes whose detection limits were not met in all cases included the following: Al-26, Sn-126, Sb-126, Sb-126m, Eu-152 and Cf-249. SRNL, in conjunction with the plant customer, reviewed all these cases and determined that the impacts were negligible.

Oji, L.; Diprete, D.; Coleman, C.; Hay, M.

2012-01-20T23:59:59.000Z

353

Database Sampling with Functional Dependencies  

E-Print Network [OSTI]

Database Sampling with Functional Dependencies Jes´us Bisbal, Jane Grimson Department of Computer there is a need to prototype the database which the applications will use when in operation. A prototype database can be built by sampling data from an existing database. Including relevant semantic information when

Riera, Jesús Bisbal

354

HYDRAULIC CONDUCTIVITY OF SALTSTONE FORMULATED USING 1Q11, 2Q11 AND 3Q11 TANK 50 SLURRY SAMPLES  

SciTech Connect (OSTI)

As part of the Saltstone formulation work requested by Waste Solidification Engineering (WSE), Savannah River National Laboratory (SRNL) was tasked with preparing Saltstone samples for fresh property analysis and hydraulic conductivity measurements using actual Tank 50 salt solution rather than simulated salt solution. Samples of low level waste salt solution collected from Tank 50H during the first, second, and third quarters of 2011 were used to formulate the Saltstone samples. The salt solution was mixed with premix (45 wt % slag, 45 wt % fly ash, and 10 wt % cement), in a ratio consistent with facility operating conditions during the quarter of interest. The fresh properties (gel, set, bleed) of each mix were evaluated and compared to the recommended acceptance criteria for the Saltstone Production Facility. ASTM D5084-03, Method C was used to measure the hydraulic conductivity of the Saltstone samples. The hydraulic conductivity of Saltstone samples prepared from 1Q11 and 2Q11 samples of Tank 50H is 4.2E-9 cm/sec and 2.6E-9 cm/sec, respectively. Two additional 2Q11 and one 3Q11 sample were not successfully tested due to the inability to achieve stable readings during saturation and testing. The hydraulic conductivity of the samples made from Tank 50H salt solution compare well to samples prepared with simulated salt solution and cured under similar conditions (1.4E-9 - 4.9E-8 cm/sec).

Reigel, M.; Nichols, R.

2012-06-27T23:59:59.000Z

355

Sample push-out fixture  

DOE Patents [OSTI]

This invention generally relates to the remote removal of pelletized samples from cylindrical containment capsules. V-blocks are used to receive the samples and provide guidance to push out rods. Stainless steel liners fit into the v-channels on the v-blocks which permits them to be remotely removed and replaced or cleaned to prevent cross contamination between capsules and samples. A capsule holder securely holds the capsule while allowing manual up/down and in/out movement to align each sample hole with the v-blocks. Both end sections contain identical v-blocks; one that guides the drive out screw and rods or manual push out rods and the other to receive the samples as they are driven out of the capsule.

Biernat, John L. (Scotia, NY)

2002-11-05T23:59:59.000Z

356

Remotely prepared entanglement: a quantum web page  

E-Print Network [OSTI]

In quantum teleportation, an unknown quantum state is transmitted from one party to another using only local operations and classical communication, at the cost of shared entanglement. Is it possible similarly, using an $N$ party entangled state, to have the state retrievable by {\\it any} of the $N-1$ possible receivers? If the receivers cooperate, and share a suitable state, this can be done reliably. The $N$ party GHZ is one such state; I derive a large class of such states, and show that they are in general not equivalent to the GHZ. I also briefly discuss the problem where the parties do not cooperate, and the relationship to multipartite entanglement quantification. I define a new set of entanglement monotones, the entanglements of preparation.

Todd A. Brun

2001-07-05T23:59:59.000Z

357

Method of preparing composite superconducting wire  

DOE Patents [OSTI]

An improved method of preparing composite multifilament superconducting wire of Nb.sub.3 Sn in a copper matrix which eliminates the necessity of coating the drawn wire with tin. A generalized cylindrical billet of an alloy of copper containing at least 15 weight percent niobium, present in the copper as discrete, randomly distributed and oriented dendritic-shaped particles, is provided with at least one longitudinal opening which is filled with tin to form a composite drawing rod. The drawing rod is then drawn to form a ductile composite multifilament wire containing a filament of tin. The ductile wire containing the tin can then be wound into magnet coils or other devices before heating to diffuse the tin through the wire to react with the niobium forming Nb.sub.3 Sn. Also described is an improved method for making large billets of the copper-niobium alloy by consumable-arc casting.

Verhoeven, John D. (Ames, IA); Gibson, Edwin D. (Ames, IA); Finnemore, Douglas K. (Ames, IA); Ostenson, Jerome E. (Ames, IA); Schmidt, Frederick A. (Ames, IA); Owen, Charles V. (Ames, IA)

1985-08-06T23:59:59.000Z

358

Preparation of stable crude oil transport emulsions  

SciTech Connect (OSTI)

A process for preparing an oil-in-water emulsion for pipeline transmission is described comprising: (a) shearing and mixing statically, without any dynamic shearing and mixing preceding or following the shearing and mixing statically, a hydrocarbon with an emulsifying composition comprising water and a minor amount of an emulsifying agent at a temperature of from about 100/sup 0/F. to about 200/sup 0/F. to form an oil-in-water emulsion having a viscosity sufficiently low for pipeline transmission, wherein the amount of water in the oil-in-water emulsion is from about 15% to about 60% by weight, and wherein the emulsifying agent is used in an amount sufficient to assist in the formation of the oil-in-water emulsion that is sufficiently stable for pipeline transmission; and wherein the emulsifying agent comprises about 50 percent by weight of an ethoxylated nonyl phenol compound.

Gregoli, A.A.; Hamshar, J.A.; Olah, A.M.; Riley, C.J.; Rimmer, D.P.

1988-02-16T23:59:59.000Z

359

Guide to preparing SAND reports. Revised  

SciTech Connect (OSTI)

This guide contains basic information needed to produce a SAND report. Its guidelines reflect DOE regulation and Sandia policy. The guide includes basic writing instructions in an annotated sample report; guidance for organization, format, and layout of reports produced by line organizations; and information about conference papers, journal articles, and brochures. The appendixes contain sections on Sandia`s preferred usage, equations, references, copyrights and permissions, and publishing terms.

Locke, T.K. [ed.

1996-04-01T23:59:59.000Z

360

Sample rotating turntable kit for infrared spectrometers  

DOE Patents [OSTI]

An infrared spectrometer sample rotating turntable kit has a rotatable sample cup containing the sample. The infrared spectrometer has an infrared spectrometer probe for analyzing the sample and the rotatable sample cup is adapted to receive the infrared spectrometer probe. A reflectance standard is located in the rotatable sample cup. A sleeve is positioned proximate the sample cup and adapted to receive the probe. A rotator rotates the rotatable sample cup. A battery is connected to the rotator.

Eckels, Joel Del (Livermore, CA); Klunder, Gregory L. (Oakland, CA)

2008-03-04T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

Sample Business Plan Framework 3  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

362

Sample Business Plan Framework 2  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

363

Sample Business Plan Framework 4  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

364

Sample Business Plan Framework 1  

Broader source: Energy.gov [DOE]

U.S. Department of Energy Better Buildings Neighborhood Program: Sample Business Plan Framework 1: A program seeking to continue operations in the post-grant period as a not-for-profit (NGO) entity.

365

Sampling based on local bandwidth  

E-Print Network [OSTI]

The sampling of continuous-time signals based on local bandwidth is considered in this thesis. In an intuitive sense, local bandwidth refers to the rate at which a signal varies locally. One would expect that signals should ...

Wei, Dennis

2007-01-01T23:59:59.000Z

366

The beryllium quandary: will the lower exposure limits spur new developments in sampling and analysis?  

SciTech Connect (OSTI)

At the time this article was written, new rulemakings were under consideration at OSHA and the U.S. Department of Energy (DOE) that would propose changes to occupational exposure limits for beryllium. Given these developments, it’s a good time to review the tools and methods available to IHs for assessing beryllium air and surface contamination in the workplace—what’s new and different, and what’s tried and true. The article discusses limit values and action levels for beryllium, problematic aspects of beryllium air sampling, sample preparation, sample analysis, and data evaluation.

Brisson, Michael

2013-06-03T23:59:59.000Z

367

Depth-discrete sampling port  

DOE Patents [OSTI]

A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

Pemberton, Bradley E. (Aiken, SC); May, Christopher P. (Columbia, MD); Rossabi, Joseph (Aiken, SC); Riha, Brian D. (Augusta, GA); Nichols, Ralph L. (North Augusta, SC)

1999-01-01T23:59:59.000Z

368

Depth-discrete sampling port  

DOE Patents [OSTI]

A sampling port is provided which has threaded ends for incorporating the port into a length of subsurface pipe. The port defines an internal receptacle which is in communication with subsurface fluids through a series of fine filtering slits. The receptacle is in further communication through a bore with a fitting carrying a length of tubing there which samples are transported to the surface. Each port further defines an additional bore through which tubing, cables, or similar components of adjacent ports may pass.

Pemberton, Bradley E. (Aiken, SC); May, Christopher P. (Columbia, MD); Rossabi, Joseph (Aiken, SC); Riha, Brian D. (Augusta, GA); Nichols, Ralph L. (North Augusta, SC)

1998-07-07T23:59:59.000Z

369

Guide to preparing SAND reports and other communication products : version 2.0.  

SciTech Connect (OSTI)

This guide describes the R&A process, Common Look and Feel requirements, and preparation and publishing procedures for communication products at Sandia National Laboratories. Samples of forms and examples of published communications products are provided. This guide details the processes for producing a variety of communication products at Sandia National Laboratories. Figure I-1 shows the general publication development process. Because extensive supplemental material is available from Sandia on the internal Web or from external sources (Table I-1), the guide has been shortened to make it easy to find information that you need.

Johnson, Debra M.; Brittenham, Phillip W.

2005-12-01T23:59:59.000Z

370

Hanford Waste Vitrification Plant full-scale feed preparation testing with water and process simulant slurries  

SciTech Connect (OSTI)

The Hanford Waste Vitrification Plant was intended to convert selected, pretreated defense high-level waste and transuranic waste from the Hanford Site into a borosilicate glass. A full-scale testing program was conducted with nonradioactive waste simulants to develop information for process and equipment design of the feed-preparation system. The equipment systems tested included the Slurry Receipt and Adjustment Tank, Slurry Mix Evaporator, and Melter-Feed Tank. The areas of data generation included heat transfer (boiling, heating, and cooling), slurry mixing, slurry pumping and transport, slurry sampling, and process chemistry. 13 refs., 129 figs., 68 tabs.

Gaskill, J.R.; Larson, D.E.; Abrigo, G.P. [and others] [and others

1996-03-01T23:59:59.000Z

371

Preparation and in situ Characterization of Surfaces Using Soft...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

in situ Characterization of Surfaces Using Soft-Landing in a Fourier Transform Ion Cyclotron Resonance Mass Preparation and in situ Characterization of Surfaces Using Soft-Landing...

372

Student Design Competition Guide to Project Preparation and Submittal...  

Broader source: Energy.gov (indexed) [DOE]

Guide to Project Preparation and Submittal DOE Challenge Home Student Competition Procuring Architectural and Engineering Services for Energy Efficiency and Sustainability...

373

EIS-0402: Amended Notice of Intent to Prepare an Environmental...  

Energy Savers [EERE]

to prepare an environmental impact statement (EIS) for cleanup of Area IV, including the Energy Technology Engineering Center (ETEC), as well as the Northern Buffer Zone of the...

374

activated carbon preparation: Topics by E-print Network  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

mesoporous carbon-based composites for confinement of Eue Mesoporous polymer-carbon composite (CMPEICMK-3) materials were successfully prepared. After Eu(III) ions were loaded...

375

activated carbon prepared: Topics by E-print Network  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

mesoporous carbon-based composites for confinement of Eue Mesoporous polymer-carbon composite (CMPEICMK-3) materials were successfully prepared. After Eu(III) ions were loaded...

376

Preparations of rare earth-iron alloys by thermite reduction  

DOE Patents [OSTI]

An improved method for the preparation of high-purity rare earth-iron alloys by the aluminothermic reduction of a mixture of rare earth and iron fluorides.

Schmidt, Frederick A. (Ames, IA); Peterson, David T. (Ames, IA); Wheelock, John T. (Nevada, IA)

1986-09-16T23:59:59.000Z

377

BPA Fact Sheet - Preparing for reliability entity registration...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Preparing for reliability entity registration Based on the NERC Functional Model The Energy Policy Act of 2005 (EPAct 2005) strongly emphasized reliability of the nation's bulk...

378

EIS-0355: Notice of Intent to Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

and Notice of Floodplain and Wetlands Involvement Remediation of the Moab Uranium Mill Tailings Site in Grand County, UT DOE announces its intent to prepare an Environmental...

379

Virginia, Maryland teams prepare for Regional Middle School Science...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Virginia, Maryland teams prepare for Regional Middle School Science Bowl March 3, 2005 The Department of Energy's Jefferson Lab, in Newport News, Va., hosts the VirginiaMaryland...

380

Jefferson Lab's Science Education Website Helps Students Prepare...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Jefferson Lab's Science Education Website Helps Students Prepare for Upcoming Standards of Learning Tests April 12, 2004 Usage of Jefferson Lab's Science Education website is...

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

RUS Bulletin 1794A-601: Preparing an Environmental Report for...  

Open Energy Info (EERE)

601: Preparing an Environmental Report for an Environmental Assessment Jump to: navigation, search OpenEI Reference LibraryAdd to library PermittingRegulatory Guidance -...

382

ATP: polynucleotide adenylyltransferase enzyme and method of preparation thereof  

DOE Patents [OSTI]

The invention relates to ATP: polynucleotide adenylyltransferase enzyme and a method for its preparation comprising extraction from monocotyledonous plant tissue and chromatographic separation.

Mans, Rusty J. (Gainesville, FL)

1987-01-01T23:59:59.000Z

383

Dominican Republic-Support for the Preparation of National Climate...  

Open Energy Info (EERE)

National Climate Change Strategy Jump to: navigation, search Name Dominican Republic-Argentina-Support for the Preparation of National Climate Change Strategy AgencyCompany...

384

Bay Bridge Lights Presentation prepared by Zoon Engineering  

Energy Savers [EERE]

2015 BAY BRIDGE LIGHTS Presentation prepared by Zoon Engineering Presentation Outline Lighting of the New East Span of the Bay Bridge Brief Over view Lighting Facts ...

385

EIS-0498: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

Notice of Intent to Prepare an Environmental Impact Statement Magnolia Liquefied Natural Gas Project, Calcasieu Parish, Louisiana The Federal Energy Regulatory Commission...

386

Jefferson Lab Website Offers Preparation Help For Virginia Standards...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Preparation Help For Virginia Standards of Learning Tests NEWPORT NEWS, Va., April 27, 2009 - Along with the return of warm weather and blooming flowers, another sure sign of...

387

ORNL staff help students prepare for FIRST LEGO League competition...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

staff help students prepare for FIRST LEGO League competition Brian Peters, right, a design engineer for nuclear systems with US ITER at Oak Ridge National Laboratory, works with...

388

p-Type transparent conducting oxides and methods for preparation  

DOE Patents [OSTI]

A facile, low temperature and low pressure method for the preparation of a wide range of phase pure ABO.sub.2 compositions.

Shahriari, Dean Y. (Evanston, IL); Barnabe, Antoine (Toulouse, FR); Mason, Thomas O. (Evanston, IL); Poeppelmeier, Kenneth R. (Evanston, IL)

2011-05-31T23:59:59.000Z

389

RUS Bulletin 1794-A-600: Preparing an Environmental Report for...  

Open Energy Info (EERE)

RUS Bulletin 1794-A-600: Preparing an Environmental Report for Categorically Excluded Projects Jump to: navigation, search OpenEI Reference LibraryAdd to library Permitting...

390

EIS-0361: Notice of Intent to Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

West Virginia The U.S. Department of Energy (DOE) announces its intent to prepare an Environmental Impact Statement (EIS) to assess the potential environmental impacts of a...

391

EIS-0269: Notice of Intent to Prepare a Programmatic Environmental...  

Energy Savers [EERE]

EIS-0269: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Alternative Strategies for the Long-Term Management and Use of Depleted Uranium Hexafluoride,...

392

EIS-0463: Notice of Intent to Prepare an Environmental Impact...  

Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

an Environmental Impact Statement and Conduct Public Scoping Meetings Presidential Permit Application for Northern Pass Transmission, New Hampshire Notice of Intent To Prepare...

393

Surveillance Guides - PTS 13.2 Packaging and Preparation for...  

Broader source: Energy.gov (indexed) [DOE]

Facility Representative RL Facility Representative Program April 10, 1995 Surveillance Guide PTS 13.2 Revision 0 Packaging and Preparation for Shipment Page 1 of...

394

EIS-0323: Notice of Intent to Prepare a Supplemental Environmental...  

Broader source: Energy.gov (indexed) [DOE]

Project in California The Western Area Power Administration (Western), Department of Energy (DOE), intends to prepare a Supplemental Environmental Impact Statement (SEIS) to...

395

Controlled environment vitrification system for preparation of liquids  

DOE Patents [OSTI]

A system is described for preparing specimens in a controlled environment to insure that a liquid or partially liquid specimen is maintained in its original state while it is being prepared, and once prepared the specimen is vitrified or solidified with minimal alteration of its microstructure. The controlled environment is provided within a chamber where humidity and temperature can be controlled precisely while the specimen is prepared. The specimen is mounted on a plunger and a shutter controlled opening is opened substantially simultaneously with release of the plunger so the specimen is propelled through the shutter into an adjacent cryogenic bath. 7 figs.

Bellare, J.R.; Davis, H.T.; Scriven, L.E. II; Talmon, Y.

1988-06-28T23:59:59.000Z

396

Advanced Post-Combustion CO2 Capture Prepared for the  

E-Print Network [OSTI]

Advanced Post-Combustion CO2 Capture Prepared for the Clean Air Task Force under a grant from...................................................................................... 3 2. Current Status of Post-Combustion Capture

397

EIS-0403: Notice of Intent to Prepare a Programmatic Environmental...  

Broader source: Energy.gov (indexed) [DOE]

EIS-0403: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Solar Energy Development in Six Southwestern States The Agencies have determined that a...

398

Nevada National Security Site Groundwater Program Prepares for...  

Energy Savers [EERE]

the site in preparation for an independent peer review of the historic underground test area, Frenchman Flat. In August 2010, the peer review panel found model projections to...

399

EIS-0366: Notice of Intent to Prepare a Programmatic Environmental...  

Broader source: Energy.gov (indexed) [DOE]

of Intent to Prepare a Programmatic Environmental Impact Statement Implementation of the Carbon Sequestration Program The U.S. Department of Energy (DOE) announces its intent to...

400

Final Guidance on Improving the Process for Preparing Efficient...  

Broader source: Energy.gov (indexed) [DOE]

the Process for Preparing Efficient and Timely Environmental Reviews under the National Environmental Policy Act. The National Environmental Policy Act (NEPA) and CEQ Regulations...

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

EIS-0429: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

Statement EIS-0429: Notice of Intent to Prepare an Environmental Impact Statement Construction and Startup of the Indiana Gasification, LLC, Industrial Gasification Facility in...

402

EIS-0432: Notice of Intent to Prepare an Environmental Impact...  

Energy Savers [EERE]

to Prepare an Environmental Impact Statement Federal Loan Guarantee to Support the Construction and Startup of the Medicine Bow Fuel & Power Coal-to-Liquid Facility in Carbon...

403

EIS-0389: Notice of Intent To Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

Environmental Impact Statement and Conduct Scoping Meetings; Notice of Floodplain and Wetlands Involvement EIS-0389: Notice of Intent To Prepare an Environmental Impact Statement...

404

EIS-0395: Notice of Intent to Prepare an Environmental Impact...  

Broader source: Energy.gov (indexed) [DOE]

Impact Statement and to Conduct Public Scoping Meetings and Notice of Floodplain and Wetlands Involvement EIS-0395: Notice of Intent to Prepare an Environmental Impact Statement...

405

Public Scoping for Preparation of a Programmatic Environmental Impact  

E-Print Network [OSTI]

0 Public Scoping for Preparation of a Programmatic Environmental Impact Statement for the Deepwater........................................................................................................................................1 III. Natural Resources Damage Assessment..........................................................................................................................7 VIII. Environmental Consequences of Restoration Types

406

Copper- and silver-zirconia aerogels: Preparation, structural properties and catalytic behavior in methanol synthesis from carbon dioxide  

SciTech Connect (OSTI)

Copper- and silver-zirconia aerogels containing 10 at% IB metal were prepared from tetra-n-butoxy zirconium(IV) and IB metal acetates using the solution sol-gel method and ensuring high-temperature (HT) and low-temperature (LT) supercritical drying, respectively. The influence of preparation parameters and calcination on the structural and catalytic properties of the aerogels for the synthesis of methanol from carbon dioxide and hydrogen was investigated. After calcination in air at 573 K, the catalysts had BET surface areas in the range of 100--143 m{sup 2}/g (Cu/ZrO{sub 2}) and 77--125 m{sup 2}/g (Ag/ZrO{sub 2}), respectively. Due to the reductive alcoholic atmosphere during high-temperature supercritical drying, metallic copper and silver existed in all raw HT-aerogels. The mean size of the copper crystallites wa/s 30 nm. The silver crystallite size for the HT-aerogel prepared with nitric acid was 10 nm, whereas for samples prepared with acetic acid it was 5--7 nm. Calcination in air at 573 K led to the formation of highly dispersed amorphous copper oxide and silver. Comparing the catalytic behavior of the calcined copper-zirconia aerogels with corresponding xerogels prepared by coprecipitation revealed highest activity for the LT-aerogel, whereas the HT-aerogels were least active. In contrast, similar catalytic behavior was observed for the differently dried silver-zirconia samples. Generally, CO{sub 2}-conversion of the copper-zirconia samples. Generally, CO{sub 2}-conversion of the copper-zirconia aerogels was markedly higher than that of the corresponding silver-zirconia aerogels, whereas methanol selectivity was similar.

Koeppel, R.A.; Stoecker, C.; Baiker, A. [Swiss Federal Inst. of Technology, Zuerich (Switzerland). Lab. of Technical Chemistry] [Swiss Federal Inst. of Technology, Zuerich (Switzerland). Lab. of Technical Chemistry

1998-10-25T23:59:59.000Z

407

Headspace vapor characterization of Hanford Waste Tank 241-T-110: Results from samples collected on August 31, 1995. Tank Vapor Characterization Project  

SciTech Connect (OSTI)

This report describes the results of vapor samples taken from the headspace of waste storage tank 241-T-110 (Tank T-110) at the Hanford Site in Washington State. Pacific Northwest National Laboratory (PNNL) contracted with Westinghouse Hanford Company (WHC) to provide sampling devices and analyze samples for inorganic and organic analytes collected from the tank headspace and ambient air near the tank. The analytical work was performed by the PNNL Vapor Analytical Laboratory (VAL) by the Tank Vapor Characterization Project. Work performed was based on a sample and analysis plan (SAP) prepared by WHC. The SAP provided job-specific instructions for samples, analyses, and reporting. The SAP for this sample job was {open_quotes}Vapor Sampling and Analysis Plan{close_quotes}, and the sample job was designated S5056. Samples were collected by WHC on August 31, 1995, using the Vapor Sampling System (VSS), a truck-based sampling method using a heated probe inserted into the tank headspace.

McVeety, B.D.; Thomas, B.L.; Evans, J.C. [and others

1996-05-01T23:59:59.000Z

408

Preparation and Characterization of Graphene Oxide Paper  

SciTech Connect (OSTI)

Free-standing paper-like or foil-like materials are an integral part of our technological society. Their uses include protective layers, chemical filters, components of electrical batteries or supercapacitors, adhesive layers, electronic or optoelectronic components, and molecular storage. Inorganic 'paper-like' materials based on nanoscale components such as exfoliated vermiculite or mica platelets have been intensively studied and commercialized as protective coatings, high-temperature binders, dielectric barriers and gas-impermeable membranes. Carbon-based flexible graphite foils composed of stacked platelets of expanded graphite have long been used in packing and gasketing applications because of their chemical resistivity against most media, superior sealability over a wide temperature range, and impermeability to fluids. The discovery of carbon nanotubes brought about bucky paper, which displays excellent mechanical and electrical properties that make it potentially suitable for fuel cell and structural composite applications. Here we report the preparation and characterization of graphene oxide paper, a free-standing carbon-based membrane material made by flow-directed assembly of individual graphene oxide sheets. This new material outperforms many other paper-like materials in stiffness and strength. Its combination of macroscopic flexibility and stiffness is a result of a unique interlocking-tile arrangement of the nanoscale graphene oxide sheets.

Dikin,D.; Stankovich, S.; Zimney, E.; Piner, R.; Dommett, G.; Evmenenko, G.; Nguyen, S.; Ruoff, R.

2007-01-01T23:59:59.000Z

409

Method of preparation of removable syntactic foam  

DOE Patents [OSTI]

Easily removable, environmentally safe, low-density, syntactic foams are disclosed which are prepared by mixing insoluble microballoons with a solution of water and/or alcohol-soluble polymer to produce a pourable slurry, optionally vacuum filtering the slurry in varying degrees to remove unwanted solvent and solute polymer, and drying to remove residual solvent. The properties of the foams can be controlled by the concentration and physical properties of the polymer, and by the size and properties of the microballoons. The suggested solute polymers are non-toxic and soluble in environmentally safe solvents such as water or low-molecular weight alcohols. The syntactic foams produced by this process are particularly useful in those applications where ease of removability is beneficial, and could find use in packaging recoverable electronic components, in drilling and mining applications, in building trades, in art works, in the entertainment industry for special effects, in manufacturing as temporary fixtures, in agriculture as temporary supports and containers and for delivery of fertilizer, in medicine as casts and splints, as temporary thermal barriers, as temporary protective covers for fragile objects, as filters for particulate matter, which matter may be easily recovered upon exposure to a solvent, as in-situ valves (for one-time use) which go from maximum to minimum impedance when solvent flows through, and for the automatic opening or closing of spring-loaded, mechanical switches upon exposure to a solvent, among other applications. 1 fig.

Arnold, C. Jr.; Derzon, D.K.; Nelson, J.S.; Rand, P.B.

1995-07-11T23:59:59.000Z

410

Method for preparing high purity vanadium  

SciTech Connect (OSTI)

A method is described of preparing high-purity, low-silicon vanadium metal from vanadium pentoxide containing silicon, iron and other impurities comprising: mixing the vanadium pentoxide with aluminum to form a reaction mixture, the quantity of aluminum in the mixture being from about stoichiometric to about 10% deficient in the amount necessary to completely reduce the vanadium pentoxide to vanadium metal: heating the mixture under reducing conditions to a temperature sufficient to react the mixture to reduce the vanadium pentoxide and form a vanadium-aluminum alloy containing silicon, iron and from about 0.6 to about 3 weight percent oxygen; heating the alloy under reduced pressure to a temperature sufficient to vaporize the aluminum and iron in the alloy and to react the silicon with some of the oxygen to form volatile silicon monoxide which vaporizes away from the alloy thereby removing aluminum, iron, silicon and some of the oxygen from the vanadium metal, and heating the vanadium metal in the presence of calcium metal to a temperature and for a period of time sufficient for the oxygen to diffuse from the vanadium and react with the calcium to form calcium oxide, thereby removing oxygen from the vanadium metal, forming a high-purity, low-silicon vanadium metal.

Schmidt, F.; Carlson, O.N.

1986-09-09T23:59:59.000Z

411

Preparation for upgrading western subbituminous coal  

SciTech Connect (OSTI)

The objective of this project was to establish the physical and chemical characteristics of western coal and determine the best preparation technologies for upgrading this resource. Western coal was characterized as an abundant, easily mineable, clean, low-sulfur coal with low heating value, high moisture, susceptibility to spontaneous ignition, and considerable transit distances from major markets. Project support was provided by the Morgantown Energy Technology Center (METC) of the US Department of Energy (DOE). The research was conducted by the Western Research Institute, (WRI) in Laramie, Wyoming. The project scope of work required the completion of four tasks: (1) project planning, (2) literature searches and verbal contacts with consumers and producers of western coal, (3) selection of the best technologies to upgrade western coal, and (4) identification of research needed to develop the best technologies for upgrading western coals. The results of this research suggest that thermal drying is the best technology for upgrading western coals. There is a significant need for further research in areas involving physical and chemical stabilization of the dried coal product. Excessive particle-size degradation and resulting dustiness, moisture reabsorption, and high susceptibility to spontaneous combustion are key areas requiring further research. Improved testing methods for the determination of equilibrium moisture and susceptibility to spontaneous ignition under various ambient conditions are recommended.

Grimes, R.W.; Cha, C.Y.; Sheesley, D.C.

1990-11-01T23:59:59.000Z

412

Method of preparation of removable syntactic foam  

DOE Patents [OSTI]

Easily removable, environmentally safe, low-density, syntactic foams are disclosed which are prepared by mixing insoluble microballoons with a solution of water and/or alcohol-soluble polymer to produce a pourable slurry, optionally vacuum filtering the slurry in varying degrees to remove unwanted solvent and solute polymer, and drying to remove residual solvent. The properties of the foams can be controlled by the concentration and physical properties of the polymer, and by the size and properties of the microballoons. The suggested solute polymers are non-toxic and soluble in environmentally safe solvents such as water or low-molecular weight alcohols. The syntactic foams produced by this process are particularly useful in those applications where ease of removability is beneficial, and could find use in packaging recoverable electronic components, in drilling and mining applications, in building trades, in art works, in the entertainment industry for special effects, in manufacturing as temporary fixtures, in agriculture as temporary supports and containers and for delivery of fertilizer, in medicine as casts and splints, as temporary thermal barriers, as temporary protective covers for fragile objects, as filters for particulate matter, which matter may be easily recovered upon exposure to a solvent, as in-situ valves (for one-time use) which go from maximum to minimum impedance when solvent flows through, and for the automatic opening or closing of spring-loaded, mechanical switches upon exposure to a solvent, among other applications.

Arnold, Jr., Charles (Albuquerque, NM); Derzon, Dora K. (Albuquerque, NM); Nelson, Jill S. (Albuquerque, NM); Rand, Peter B. (Albuquerque, NM)

1995-01-01T23:59:59.000Z

413

Surface electronic structure for various surface preparations of Nb-doped SrTiO{sub 3} (001)  

SciTech Connect (OSTI)

High-resolution angle-resolved photoemission spectroscopy (ARPES) was used to study the surface electronic structure of Nb-doped SrTiO{sub 3} (STO) single crystals prepared using a variety of surface preparations. ARPES measurements show that simple degreasing with subsequent anneal in vacuum is not an adequate surface preparation of STO, rather, preparations consisting of etching with buffered HF or HCl, and to a lesser extent, simple water leaching resulted in surfaces with much less disorder. A non-dispersing, mid-gap state was found ?800 meV above the top of the valence band for samples which underwent etching. This mid-gap state is not present for vacuum-annealed and water-leached samples, as well as for STO thin films grown using molecular beam epitaxy. Theoretical modeling using density functional theory suggests that this mid-gap state is not related to the SrO- and TiO{sub 2}-terminated surfaces, but rather, is due to a partial hydrogenation of the STO surface that occurs during etching.

Hatch, Richard C.; Fredrickson, Kurt D.; Choi, Miri; Lin, Chungwei; Seo, Hosung; Posadas, Agham B.; Demkov, Alexander A. [Department of Physics, The University of Texas at Austin, Austin, Texas 78712 (United States)] [Department of Physics, The University of Texas at Austin, Austin, Texas 78712 (United States)

2013-09-14T23:59:59.000Z

414

Reference Potential source Data type Sampling site Type of samples Number of samples Method of source  

E-Print Network [OSTI]

samples for Saharan dust from Libya back trajectory analysis Kandler et al. 2009 PSA NAF-2 Illite NAF-4 Illite/kaolinite ratio Chlorite/kaolinite ratio Carbonate content Libya (here: central

Meskhidze, Nicholas

415

Characterization Data Package for Containerized Sludge Samples Collected from Engineered Container SCS-CON-210  

SciTech Connect (OSTI)

This data package contains the K Basin sludge characterization results obtained by Pacific Northwest National Laboratory during processing and analysis of four sludge core samples collected from Engineered Container SCS-CON-210 in 2010 as requested by CH2M Hill Plateau Remediation Company. Sample processing requirements, analytes of interest, detection limits, and quality control sample requirements are defined in the KBC-33786, Rev. 2. The core processing scope included reconstitution of a sludge core sample distributed among four to six 4-L polypropylene bottles into a single container. The reconstituted core sample was then mixed and subsampled to support a variety of characterization activities. Additional core sludge subsamples were combined to prepare a container composite. The container composite was fractionated by wet sieving through a 2,000 micron mesh and a 500-micron mesh sieve. Each sieve fraction was sampled to support a suite of analyses. The core composite analysis scope included density determination, radioisotope analysis, and metals analysis, including the Waste Isolation Pilot Plant Hazardous Waste Facility Permit metals (with the exception of mercury). The container composite analysis included most of the core composite analysis scope plus particle size distribution, particle density, rheology, and crystalline phase identification. A summary of the received samples, core sample reconstitution and subsampling activities, container composite preparation and subsampling activities, physical properties, and analytical results are presented. Supporting data and documentation are provided in the appendices. There were no cases of sample or data loss and all of the available samples and data are reported as required by the Quality Assurance Project Plan/Sampling and Analysis Plan.

Fountain, Matthew S.; Fiskum, Sandra K.; Baldwin, David L.; Daniel, Richard C.; Bos, Stanley J.; Burns, Carolyn A.; Carlson, Clark D.; Coffey, Deborah S.; Delegard, Calvin H.; Edwards, Matthew K.; Greenwood, Lawrence R.; Neiner, Doinita; Oliver, Brian M.; Pool, Karl N.; Schmidt, Andrew J.; Shimskey, Rick W.; Sinkov, Sergey I.; Snow, Lanee A.; Soderquist, Chuck Z.; Thompson, Christopher J.; Trang-Le, Truc LT; Urie, Michael W.

2013-09-10T23:59:59.000Z

416

Preparation of bitumen and kerogen through microwave assisted extraction and digestion  

SciTech Connect (OSTI)

Microwave procedures are replacing Soxhlet and ultrasonic extractions in many applications and are also finding widespread use in acid digestion procedures. In microwave extractions solvent choice is not dictated by boiling point considerations, so the choice of solvent(s) can be made based on polarity. It is possible to operate at temperatures above the solvent boiling point and at increased pressures. As a result these extractions are characterized by high solvent efficiency, small sample size, low solvent volumes, and short extraction times. These characteristics are ideal for bitumen extractions. Similarly, in digestion procedures, a high recovery yield is obtained in a minimum time using smaller volumes of acids. We report a convenient procedure for preparation of both bitumen and kerogen from shale samples based on a study of the efficiency of a series of solvents of varying polarity for bitumen recovery and testing of acid composition and volumes at different microwave powers and digestion times.

Dickneider, T.A.; Martin, S. [Univ. of Scranton, PA (United States)

1996-12-31T23:59:59.000Z

417

Influence of Surface Preparation on Scanning Kelvin Probe Microscopy and Electron Backscatter Diffraction Analysis of Cross Sections of CdTe/CdS Solar Cells  

SciTech Connect (OSTI)

Electron backscatter diffraction (EBSD) provides information on the crystallographic structure of a sample, while scanning Kelvin probe microscopy (SKPM) provides information on its electrical properties. The advantage of these techniques is their high spatial resolution, which cannot be attained with any other techniques. However, because these techniques analyze the top layers of the sample, surface or cross section features directly influence the results of the measurements, and sample preparation is a main step in the analysis. In this work we investigated different methods to prepare cross sections of CdTe/CdS solar cells for EBSD and SKPM analyses. We observed that procedures used to prepare surfaces for EBSD are not suitable to prepare cross sections, and we were able to develop a process using polishing and ion-beam milling. This process resulted in very good results and allowed us to reveal important aspects of the cross section of the CdTe films. For SKPM, polishing and a light ion-beam milling resulted in cross sections that provided good data. We were able to observe the depletion region on the CdTe film and the p-n junction as well as the interdiffusion layer between CdTe and CdS. However, preparing good-quality cross sections for SKPM is not a reproducible process, and artifacts are often observed.

Moutinho, H. R.; Dhere, R. G.; Jiang, C. S.; Al-Jassim, M. M.

2011-01-01T23:59:59.000Z

418

1. Prepare 200g of each protein sample in SDS-page loading buffer. 2. Load sample, flanked by prestained molecular weight markers onto a 10% acrylamide gel,  

E-Print Network [OSTI]

. 4. Remove supernatant and wash gel bands 2-3x 15' in 500µL 50:50 acetonitrile:100mM ammonium bicarbonate. 5. Remove supernatant and add 50 µL acetonitrile to completely dry gel band (should turn opaque). Remove acetonitrile and speed vac for ~5 minutes or until slices are completely dry. 6. Resuspend a 20µg

Cravatt, Benjamin

419

RAPID SEPARATION OF ACTINIDES AND RADIOSTRONTIUM IN VEGETATION SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of actinides and radiostrontium in vegetation samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used in emergency response situations or for routine analysis. The actinides in vegetation method utilizes a rapid sodium hydroxide fusion method, a lanthanum fluoride matrix removal step, and a streamlined column separation process with stacked TEVA, TRU and DGA Resin cartridges. Lanthanum was separated rapidly and effectively from Am and Cm on DGA Resin. Alpha emitters are prepared using rare earth microprecipitation for counting by alpha spectrometry. The purified {sup 90}Sr fractions are mounted directly on planchets and counted by gas flow proportional counting. The method showed high chemical recoveries and effective removal of interferences. The actinide and {sup 90}Sr in vegetation sample analysis can be performed in less than 8 h with excellent quality for emergency samples. The rapid fusion technique is a rugged sample digestion method that ensures that any refractory actinide particles or vegetation residue after furnace heating is effectively digested.

Maxwell, S.

2010-06-01T23:59:59.000Z

420

Anthrax Sampling and Decontamination: Technology Trade-Offs  

SciTech Connect (OSTI)

The goal of this project was to answer the following questions concerning response to a future anthrax release (or suspected release) in a building: 1. Based on past experience, what rules of thumb can be determined concerning: (a) the amount of sampling that may be needed to determine the extent of contamination within a given building; (b) what portions of a building should be sampled; (c) the cost per square foot to decontaminate a given type of building using a given method; (d) the time required to prepare for, and perform, decontamination; (e) the effectiveness of a given decontamination method in a given type of building? 2. Based on past experience, what resources will be spent on evaluating the extent of contamination, performing decontamination, and assessing the effectiveness of the decontamination in abuilding of a given type and size? 3. What are the trade-offs between cost, time, and effectiveness for the various sampling plans, sampling methods, and decontamination methods that have been used in the past?

Price, Phillip N.; Hamachi, Kristina; McWilliams, Jennifer; Sohn, Michael D.

2008-09-12T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

Preparation and photocatalytic properties of AgI–SnO{sub 2} nano-composites  

SciTech Connect (OSTI)

Highlights: ? AgI–SnO{sub 2} nano-composites have been successfully synthesized. ? As-prepared AgI–SnO{sub 2} nano-composites own the excellent visible light photocatalytic activity. ? As-prepared AgI–SnO{sub 2} nano-composites own the excellent stability. - Abstract: AgI doped SnO{sub 2} nano-composites were prepared by the chemical coprecipitation method and were characterized by the X-ray diffraction, transmission electron microscopy and X-ray photoelectron spectroscopy. Results showed that main of the I{sup ?} ions remained in the AgI lattice which is highly dispersed in the system. The photo-catalytic experiments performed under visible light irradiation using methylene blue as the pollutant revealed that not only the photo-catalytic activity but also the stability of SnO{sub 2} based photocatalyst could be improved by introduction of an appropriate amount of AgI, and the result was further supported by the UV–Vis diffuse reflection spectra and the electron spin-resonance spectra. Among all of the samples, AgI–SnO{sub 2} nano-composite with 2At% AgI exhibited the best catalytic efficiency and stability.

Wen, Biao; Wang, Xiao-Hui; Lu, Juan; Cao, Jia-Lei [College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou 215021 (China); Wang, Zuo-Shan, E-mail: zuoshanwang@suda.edu.cn [College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou 215021 (China); State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081 (China)

2013-05-15T23:59:59.000Z

422

A facile method for the preparation of Eu{sup 2+}-doped nanocrystalline BaFCl  

SciTech Connect (OSTI)

Graphical abstract: - Highlights: • A facile co-precipitation method for the preparation of Eu{sup 2+}-doped BaFCl. • Reduction of Eu{sup 3+} to Eu{sup 2+} by zinc granular under nitrogen flow. • Photoluminescence and cathodoluminescence spectroscopy of the as-prepared BaFCl:Eu{sup 2+}. • Temperature dependent photoluminescence properties of Eu{sup 2+} ions in BaFCl. - Abstract: A facile method for the preparation of Eu{sup 2+}-doped BaFCl is reported. The method is based on the co-precipitation of aqueous solutions of BaCl{sub 2} and NH{sub 4}F to yield BaFCl. The doping by europium in the 2+ oxidation state is realized by the reduction of Eu{sup 3+} to Eu{sup 2+} employing granular zinc in the BaCl{sub 2} solution under nitrogen. Powder X-ray diffraction and electron microscopy have been used to confirm the BaFCl phase and photoluminescence, in the temperature range of 2.5–290 K, and room-temperature cathodoluminescence spectra have been measured to characterize the Eu{sup 2+} ions in the sample.

Wang, Xianglei; Liu, Zhiqiang [School of Physical, Environmental and Mathematical Sciences, The University of New South Wales, UNSW Canberra (ADFA), Canberra, ACT 2600 (Australia); Stevens-Kalceff, Marion A. [School of Physics and Electron Microscope Unit, Mark Wainwright Analytical Centre, The University of New South Wales, Sydney, NSW 2052 (Australia); Riesen, Hans, E-mail: h.riesen@adfa.edu.au [School of Physical, Environmental and Mathematical Sciences, The University of New South Wales, UNSW Canberra (ADFA), Canberra, ACT 2600 (Australia)

2013-10-15T23:59:59.000Z

423

A Pilot Project in Preparation of an Aerodynamic Optimization Workshop  

E-Print Network [OSTI]

A Pilot Project in Preparation of an Aerodynamic Optimization Workshop with Lessons Learned John C-scale Aerodynamic Optimization Workshop. Three independent optimization efforts were conducted concurrently, each in the preparation of a possible future workshop on aerodynamic shape optimization. 1.0 Introduction During AIAA

Jameson, Antony

424

Formulation and method for preparing gels comprising hydrous hafnium oxide  

DOE Patents [OSTI]

Formulations useful for preparing hydrous hafnium oxide gels contain a metal salt including hafnium, an acid, an organic base, and a complexing agent. Methods for preparing gels containing hydrous hafnium oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including hafnium, an acid, an organic base, and a complexing agent.

Collins, Jack L; Hunt, Rodney D; Montgomery, Frederick C

2013-08-06T23:59:59.000Z

425

Formulation and method for preparing gels comprising hydrous cerium oxide  

DOE Patents [OSTI]

Formulations useful for preparing hydrous cerium oxide gels contain a metal salt including cerium, an organic base, and a complexing agent. Methods for preparing gels containing hydrous cerium oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including cerium, an organic base, and a complexing agent.

Collins, Jack L; Chi, Anthony

2013-05-07T23:59:59.000Z

426

u DATA PREPARATION FOR DATA SHICHAO ZHANG and CHENGQI ZHANG  

E-Print Network [OSTI]

u DATA PREPARATION FOR DATA MINING SHICHAO ZHANG and CHENGQI ZHANG Faculty of Information of Science andTechnology, Kowloon, Hong Kong, China Data preparation is a fundamental stage of data analysis. While a lot of low-quality information is available in various data sources and on the Web, many

Yang, Qiang

427

Formulation and method for preparing gels comprising hydrous aluminum oxide  

SciTech Connect (OSTI)

Formulations useful for preparing hydrous aluminum oxide gels contain a metal salt including aluminum, an organic base, and a complexing agent. Methods for preparing gels containing hydrous aluminum oxide include heating a formulation to a temperature sufficient to induce gel formation, where the formulation contains a metal salt including aluminum, an organic base, and a complexing agent.

Collins, Jack L.

2014-06-17T23:59:59.000Z

428

Notice of Preparation, Comments, and Scoping Meeting Transcript  

E-Print Network [OSTI]

DRAFT ENVIRONMENTAL IMPACT REPORT Project Title: Richmond Bay Campus 2013 Long Range Development Plan of the California Environmental Quality Act (CEQA), this Notice of Preparation is hereby sent to inform you that UC is preparing a Draft Environmental Impact Report (EIR) on the RBC 2013 LRDP and Phase 1 development. The EIR

Lee, Jason R.

429

REPORT ON THE ANALYSIS OF WAC SAMPLES FROM EVAPORATOR OVERHEADS FOR 2011  

SciTech Connect (OSTI)

This report tabulates the chemical analysis of the 3H, 2H and 2F evaporator overhead samples including the inorganic, organic, and radionuclide species according the ETP WAC (rev.4). In addition, the physical properties including pH, total suspended solids, and average particle size are listed for each sample. The report identifies all sample receipt dates, preparation methods, and analyses completed to accumulate these values. All values were found to be within the ETP WAC specifications for WWCT except for the {sup 137}Cs concentration for the 2F sample which was slightly above the limit ({approx}5%). However, tank farm personnel sample each tank overhead for beta/gamma prior to transfer using a pulse height analyzer and these field readings were all well within limits. Additional actions will be taken to help understand the reason in the discrepancy of the field measurement versus laboratory analysis.

Washington, A.

2012-03-29T23:59:59.000Z

430

Inertial impaction air sampling device  

DOE Patents [OSTI]

An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

Dewhurst, K.H.

1987-12-10T23:59:59.000Z

431

Spent nuclear fuel sampling strategy  

SciTech Connect (OSTI)

This report proposes a strategy for sampling the spent nuclear fuel (SNF) stored in the 105-K Basins (105-K East and 105-K West). This strategy will support decisions concerning the path forward SNF disposition efforts in the following areas: (1) SNF isolation activities such as repackaging/overpacking to a newly constructed staging facility; (2) conditioning processes for fuel stabilization; and (3) interim storage options. This strategy was developed without following the Data Quality Objective (DQO) methodology. It is, however, intended to augment the SNF project DQOS. The SNF sampling is derived by evaluating the current storage condition of the SNF and the factors that effected SNF corrosion/degradation.

Bergmann, D.W.

1995-02-08T23:59:59.000Z

432

Inertial impaction air sampling device  

DOE Patents [OSTI]

An inertial impactor to be used in an air sampling device for collection of respirable size particles in ambient air which may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry.

Dewhurst, Katharine H. (13150 Wenonah SE. Apt. 727, Albuquerque, NM 87123)

1990-01-01T23:59:59.000Z

433

Inertial impaction air sampling device  

DOE Patents [OSTI]

An inertial impactor is designed which is to be used in an air sampling device for collection of respirable size particles in ambient air. The device may include a graphite furnace as the impaction substrate in a small-size, portable, direct analysis structure that gives immediate results and is totally self-contained allowing for remote and/or personal sampling. The graphite furnace collects suspended particles transported through the housing by means of the air flow system, and these particles may be analyzed for elements, quantitatively and qualitatively, by atomic absorption spectrophotometry. 3 figs.

Dewhurst, K.H.

1990-05-22T23:59:59.000Z

434

Sample Licensing Agreements | Partnerships | ORNL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 -the Mid-Infrared0 ResourceAwardsSafeguards and SecuritySafety Salt LakeSampleSample

435

Tank 241-BY-110 vapor sampling and analysis tank characterization report  

SciTech Connect (OSTI)

Tank BY-110 headspace gas and vapor samples were collected and analyzed to help determine the potential risks to tank farm workers due to fugitive emissions from the tank. Tank BY-110 is on the Ferrocyanide Watch List. Samples were collected from Tank BY-110 using the vapor sampling system (VSS) on November 11, 1994 by WHC Sampling and Mobile Laboratories. The tank headspace temperature was determined to be 27 C. Air from the Tank BY-110 headspace was withdrawn via a 7.9 m-long heated sampling probe mounted in riser 12B, and transferred via heated tubing to the VSS sampling manifold. All heated zones of the VSS were maintained at approximately 50 C. Sampling media were prepared and analyzed by WHC, Oak Ridge National Laboratories, and Pacific Northwest Laboratories. The 40 tank air samples and 2 ambient air control samples collected are listed in Table X-1 by analytical laboratory. Table X-1 also lists the 14 trip blanks and 2 field blanks that accompanied the samples.

Huckaby, J.L.

1995-05-10T23:59:59.000Z

436

Tank 241-BY-108 vapor sampling and analysis tank characterization report  

SciTech Connect (OSTI)

Tank BY-108 headspace gas and vapor samples were collected and analyzed to help determine the potential risks to tank farm workers due to fugitive emissions from the tank. Tank BY-108 is on the Ferrocyanide Watch List. Samples were collected from Tank BY-108 using the vapor sampling system (VSS) on october 27, 1994 by WHC Sampling and Mobile Laboratories. The tank headspace temperature was determined to be 25.7 C. Air from the Tank BY-108 headspace was withdrawn via a 7.9 m-long heated sampling probe mounted in riser 1, and transferred via heated tubing to the VSS sampling manifold. All heated zones of the VSS were maintained at approximately 50 C. Sampling media were prepared and analyzed by WHC, Oak Ridge National Laboratories, and Pacific Northwest Laboratories. The 40 tank air samples and 2 ambient air control samples collected are listed in Table X-1 by analytical laboratory. Table X-1 also lists the 14 trip blanks and 2 field blanks that accompanied the samples.

Huckaby, J.L.

1995-05-10T23:59:59.000Z

437

Mechanical sampling systems for coal quality control in Romanian power plants  

SciTech Connect (OSTI)

According to ISO 1988 samples must be taken from moving currents by using certain mechanical devices, and, only, exceptionally, by an understanding between party`s, by manually sampling. The principal requirements when designing and constructing a mechanical sampling system are that: it shall be capable of collecting and preparing increments or samples, as the case may be, that are free from relevant bias; it shall maintain this capability under all such conditions of sampling that are stipulated in the relevant specifications and without necessitating that sampling be interrupted for cleaning or maintenance. Actually, coal quality control in Romanian power plants are usually performed by a manual system. In order to meet ISO 1988 requirements, RENEL-GSCI (formerly ICEMENERG) has designed and achieved a falling stream sampler with cutter bucket in accordance with ISO 9411-1 (solid mineral fuels - Mechanical sampling from moving stream) provisions. This device has been installed in the Oradea 2 cogeneration power plant in the coal falling stream at the end of the belt conveyor. When the mechanical sampling installation was commissioned, experiments to check for precision and bias had been out for the installation as a whole. The method of checking for bias was by comparison with stopped-belt sampling. The mechanical sampling device is still under testing. The paper presents the result obtained during the preliminary test period in order to certify the mechanical sampler.

Matei, M. [Romanian Electricity Authority, Bucharest (Romania). Study, Research and Engineering Group

1998-12-31T23:59:59.000Z

438

Waste tank characterization sampling limits  

SciTech Connect (OSTI)

This document is a result of the Plant Implementation Team Investigation into delayed reporting of the exotherm in Tank 241-T-111 waste samples. The corrective actions identified are to have immediate notification of appropriate Tank Farm Operations Shift Management if analyses with potential safety impact exceed established levels. A procedure, WHC-IP-0842 Section 12.18, ``TWRS Approved Sampling and Data Analysis by Designated Laboratories`` (WHC 1994), has been established to require all tank waste sampling (including core, auger and supernate) and tank vapor samples be performed using this document. This document establishes levels for specified analysis that require notification of the appropriate shift manager. The following categories provide numerical values for analysis that may indicate that a tank is either outside the operating specification or should be evaluated for inclusion on a Watch List. The information given is intended to translate an operating limit such as heat load, expressed in Btu/hour, to an analysis related limit, in this case cesium-137 and strontium-90 concentrations. By using the values provided as safety flags, the analytical laboratory personnel can notify a shift manager that a tank is in potential violation of an operating limit or that a tank should be considered for inclusion on a Watch List. The shift manager can then take appropriate interim measures until a final determination is made by engineering personnel.

Tusler, L.A.

1994-09-02T23:59:59.000Z

439

Sample Internship Posting Department Name  

E-Print Network [OSTI]

Sample Internship Posting Department Name: Internship Title: Location: Description of Organization are examples from other internship postings Interns will: · Analyze potential investments · Shadow team members(s) in ________ is desirable For a list of majors see http://admissions.vanderbilt.edu/major Internship Period: The following

Bordenstein, Seth

440

Environmental surveillance master sampling schedule  

SciTech Connect (OSTI)

This document contains the planned 1994 schedules for routine collection of samples for the Surface Environmental Surveillance Project (SESP), Drinking Water Project, and Ground-Water Surveillance Project. Samples are routinely collected for the SESP and analyzed to determine the quality of air, surface water, soil, sediment, wildlife, vegetation, foodstuffs, and farm products at Hanford Site and surrounding communities. The responsibility for monitoring the onsite drinking water falls outside the scope of the SESP. The Hanford Environmental Health Foundation is responsible for monitoring the nonradiological parameters as defined in the National Drinking Water Standards while PNL conducts the radiological monitoring of the onsite drinking water. PNL conducts the drinking water monitoring project concurrent with the SESP to promote efficiency and consistency, utilize the expertise developed over the years, and reduce costs associated with management, procedure development, data management, quality control and reporting. The ground-water sampling schedule identifies ground-water sampling events used by PNL for environmental surveillance of the Hanford Site.

Bisping, L.E.

1994-02-01T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


441

Environmental Analysis & Policy: Sample Pathway  

E-Print Network [OSTI]

Environmental Analysis & Policy: Sample Pathway Semester I Semester II Freshman Year CGS Core CGS Sustainable Development OR Spring GE 425 U.S. Environmental Policy (Senior) GE 309 Intermediate Env Analysis (Fall) EAP Elective Summer Environmental Internship Senior Year GE 420 Env Policy Analysis 4 th Semester

Goldberg, Bennett

442

AUTOMATING GROUNDWATER SAMPLING AT HANFORD  

SciTech Connect (OSTI)

Until this past October, Fluor Hanford managed Hanford's integrated groundwater program for the U.S. Department of Energy (DOE). With the new contract awards at the Site, however, the CH2M HILL Plateau Remediation Company (CHPRC) has assumed responsibility for the groundwater-monitoring programs at the 586-square-mile reservation in southeastern Washington State. These programs are regulated by the Resource Conservation and Recovery Act (RCRA) and the Comprehensive Environmental Response Compensation and Liability Act (CERCLA). The purpose of monitoring is to track existing groundwater contamination from past practices, as well as other potential contamination that might originate from RCRA treatment, storage, and disposal (TSD) facilities. An integral part of the groundwater-monitoring program involves taking samples of the groundwater and measuring the water levels in wells scattered across the site. More than 1,200 wells are sampled each year. Historically, field personnel or 'samplers' have been issued pre-printed forms that have information about the well(s) for a particular sampling evolution. This information is taken from the Hanford Well Information System (HWIS) and the Hanford Environmental Information System (HEIS)--official electronic databases. The samplers used these hardcopy forms to document the groundwater samples and well water-levels. After recording the entries in the field, the samplers turned the forms in at the end of the day and the collected information was posted onto a spreadsheet that was then printed and included in a log book. The log book was then used to make manual entries of the new information into the software application(s) for the HEIS and HWIS databases. This is a pilot project for automating this tedious process by providing an electronic tool for automating water-level measurements and groundwater field-sampling activities. The automation will eliminate the manual forms and associated data entry, improve the accuracy of the information recorded, and enhance the efficiency and sampling capacity of field personnel. The goal of the effort is to eliminate 100 percent of the manual input to the database(s) and replace the management of paperwork by the field and clerical personnel with an almost entirely electronic process. These activities will include the following: scheduling the activities of the field teams, electronically recording water-level measurements, electronically logging and filing Groundwater Sampling Reports (GSR), and transferring field forms into the site-wide Integrated Document Management System (IDMS).

CONNELL CW; HILDEBRAND RD; CONLEY SF; CUNNINGHAM DE

2009-01-16T23:59:59.000Z

443

Preparation of activated carbon from sorghum pith and its structural and electrochemical properties  

SciTech Connect (OSTI)

Research highlights: {yields} Sorghum pith as the cost effective raw material for activated carbon preparation. {yields} Physicochemical method/KOH activation for preparation of activated carbon is inexpensive. {yields} Activated carbon having lower surface area surprisingly delivered a higher specific capacitance. {yields} Treated at 500 {sup o}C activated carbon exceeds maximum specific capacitances of 320.6 F/g at 10 mV/s. -- Abstract: The cost effective activated carbon (AC) has been prepared from sorghum pith by NaOH activation at various temperatures, including 300 {sup o}C (AC1), 400 {sup o}C (AC2) and 500 {sup o}C (AC3) for the electrodes in electric double layer capacitor (EDLC) applications. The amorphous nature of the samples has been observed from X-ray diffraction and Raman spectral studies. Subsequently, the surface functional groups, surface morphology, pore diameter and specific surface area have been identified through FT-IR, SEM, histogram and N{sub 2} adsorption/desorption isotherm methods. The electrochemical characterization of AC electrodes has been examined using cyclic voltammetry technique in the potential range of -0.1-1.2 V in 1.0 M H{sub 2}SO{sub 4} electrolyte at different scan rates (10, 20, 30, 40, 50 and 100 mV/s). The maximum specific capacitances of 320.6 F/g at 10 mV/s and 222.1 F/g at 100 mV/s have been obtained for AC3 electrode when compared with AC1 and AC2 electrodes. Based on the characterization studies, it has been inferred that the activated carbon prepared from sorghum pith may be one of the innovative carbon electrode materials for EDLC applications.

Senthilkumar, S.T.; Senthilkumar, B. [Solid State Ionics and Energy Devices Laboratory, Department of Physics, Bharathiar University, Coimbatore 641046 (India)] [Solid State Ionics and Energy Devices Laboratory, Department of Physics, Bharathiar University, Coimbatore 641046 (India); Balaji, S. [Materials Laboratory, Thiagarajar Advanced Research Center, Thiagarajar College of Engineering, Madurai 625015 (India)] [Materials Laboratory, Thiagarajar Advanced Research Center, Thiagarajar College of Engineering, Madurai 625015 (India); Sanjeeviraja, C. [Department of Physics, Alagappa University, Karaikudi 630003 (India)] [Department of Physics, Alagappa University, Karaikudi 630003 (India); Kalai Selvan, R., E-mail: selvankram@buc.edu.in [Solid State Ionics and Energy Devices Laboratory, Department of Physics, Bharathiar University, Coimbatore 641046 (India)

2011-03-15T23:59:59.000Z

444

Hanford Site Environmental Surveillance Master Sampling Schedule  

SciTech Connect (OSTI)

This document contains the CY2000 schedules for the routine collection of samples for the Surface Environmental Surveillance Project (SESP) and Drinking Water Monitoring Project. Each section includes sampling locations, sample types, and analyses to be performed.

Bisping, Lynn E.

2000-01-27T23:59:59.000Z

445

A World without Sample Preparation: Developing Rapid Uranium Isotope Measurement Capabilities by Resonance Ionization Mass Spectrometry (RIMS)  

SciTech Connect (OSTI)

We are developing highly sensitive, highly discriminating laser-based techniques for rapid determination of isotopic compositions. Rapid command of such information is critical to assessment of the origin and history of nuclear materials, particularly in post-detonation scenarios.

Knight, K B; Hutcheon, I D; Isselhardt, B H; Savina, M R; Prussin, S G

2009-06-08T23:59:59.000Z

446

Experimental: Sample Preparation TiO2 compact (TiO2comp) anatase films (0.1  

E-Print Network [OSTI]

) solar cells by an embossing technique to increase light harvesting and electron percolation.biancardo@risoe.dk Working principle of ETA solar cells: light irradiation (1) produce excitation (2) of the absorber (Abs 20 kgcm-2). Experimental: Device Testing Sun simulation was provided by a solar simulator KHS Solar

447

Tank farm backlog soil sample analysis plan  

SciTech Connect (OSTI)

This document describes the measures to collect samples, perform testing on samples, and make decisions to obtain a Contained- in Determination for tank farms backlog soil.

Ahlers, J.D., Westinghouse Hanford

1996-07-17T23:59:59.000Z

448

Zero-valent iron nanoparticles preparation  

SciTech Connect (OSTI)

Graphical abstract: Zero-valent iron nanoparticles were synthesized by hydrogenating [Fe[N(Si(CH{sub 3}){sub 3}){sub 2}]{sub 2}] at room temperature and a pressure of 3 atm. The synthesized nanoparticles were spherical and had diameters less than 5 nm. Highlights: ? Zero-valent iron nanoparticles were synthesized by hydrogenating [Fe[N(Si(CH{sub 3}){sub 3}){sub 2}]{sub 2}]. ? The conditions of reaction were at room temperature and a pressure of 3 atm. ? The synthesized nanoparticles were spherical and had diameters less than 5 nm. -- Abstract: Zero-valent iron nanoparticles were synthesized by hydrogenating [Fe[N(Si(CH{sub 3}){sub 3}){sub 2}]{sub 2}] at room temperature and a pressure of 3 atm. To monitor the reaction, a stainless steel pressure reactor lined with PTFE and mechanically stirred was designed. This design allowed the extraction of samples at different times, minimizing the perturbation in the system. In this way, the shape and the diameter of the nanoparticles produced during the reaction were also monitored. The results showed the production of zero-valent iron nanoparticles that were approximately 5 nm in diameter arranged in agglomerates. The agglomerates grew to 900 nm when the reaction time increased up to 12 h; however, the diameter of the individual nanoparticles remained almost the same. During the reaction, some byproducts constituted by amino species acted as surfactants; therefore, no other surfactants were necessary.

Oropeza, S. [Instituto Politécnico Nacional, ESIQIE, UPALM, Edificio Z-6, Primer Piso, C.P. 07738, Col. San Pedro Zacatenco, México D.F. (Mexico)] [Instituto Politécnico Nacional, ESIQIE, UPALM, Edificio Z-6, Primer Piso, C.P. 07738, Col. San Pedro Zacatenco, México D.F. (Mexico); Corea, M., E-mail: mcoreat@yahoo.com.mx [Instituto Politécnico Nacional, ESIQIE, UPALM, Edificio Z-6, Primer Piso, C.P. 07738, Col. San Pedro Zacatenco, México D.F. (Mexico); Gómez-Yáñez, C. [Instituto Politécnico Nacional, ESIQIE, UPALM, Edificio Z-6, Primer Piso, C.P. 07738, Col. San Pedro Zacatenco, México D.F. (Mexico)] [Instituto Politécnico Nacional, ESIQIE, UPALM, Edificio Z-6, Primer Piso, C.P. 07738, Col. San Pedro Zacatenco, México D.F. (Mexico); Cruz-Rivera, J.J. [Universidad Autónoma de San Luis Potosí, Instituto de Metalurgia, Sierra Leona 550, San Luis Potosí, C.P. 78210 (Mexico)] [Universidad Autónoma de San Luis Potosí, Instituto de Metalurgia, Sierra Leona 550, San Luis Potosí, C.P. 78210 (Mexico); Navarro-Clemente, M.E., E-mail: mnavarroc@ipn.mx [Instituto Politécnico Nacional, ESIQIE, UPALM, Edificio Z-6, Primer Piso, C.P. 07738, Col. San Pedro Zacatenco, México D.F. (Mexico)

2012-06-15T23:59:59.000Z

449

Adaptive Sampling in Hierarchical Simulation  

SciTech Connect (OSTI)

We propose an adaptive sampling methodology for hierarchical multi-scale simulation. The method utilizes a moving kriging interpolation to significantly reduce the number of evaluations of finer-scale response functions to provide essential constitutive information to a coarser-scale simulation model. The underlying interpolation scheme is unstructured and adaptive to handle the transient nature of a simulation. To handle the dynamic construction and searching of a potentially large set of finer-scale response data, we employ a dynamic metric tree database. We study the performance of our adaptive sampling methodology for a two-level multi-scale model involving a coarse-scale finite element simulation and a finer-scale crystal plasticity based constitutive law.

Knap, J; Barton, N R; Hornung, R D; Arsenlis, A; Becker, R; Jefferson, D R

2007-07-09T23:59:59.000Z

450

Environmental surveillance master sampling schedule  

SciTech Connect (OSTI)

Environmental surveillance of the Hanford Site and surrounding areas is conducted by the Pacific Northwest Laboratory (PNL) for the US Department of Energy (DOE). This document contains the planned schedule for routine sample collection for the Surface Environmental Surveillance Project (SESP) and Ground-Water Monitoring Project. Samples for radiological analyses include Air-Particulate Filter, gases and vapor; Water/Columbia River, Onsite Pond, Spring, Irrigation, and Drinking; Foodstuffs/Animal Products including Whole Milk, Poultry and Eggs, and Beef; Foodstuffs/Produce including Leafy Vegetables, Vegetables, and Fruit; Foodstuffs/Farm Products including Wine, Wheat and Alfalfa; Wildlife; Soil; Vegetation; and Sediment. Direct Radiation Measurements include Terrestrial Locations, Columbia River Shoreline Locations, and Onsite Roadway, Railway and Aerial, Radiation Surveys.

Bisping, L E

1992-01-01T23:59:59.000Z

451

Tank 241-BY-105 vapor sampling and analysis tank characterization report  

SciTech Connect (OSTI)

Tank BY-105 headspace gas and vapor samples were collected and analyzed to help determine the potential risks to tank farm workers due to fugitive emissions from the tank. Tank BY-105 is on the Ferrocyanide Watch List. Samples were collected from Tank BY-105 using the vapor sampling system (VSS) on July 7, 1994 by WHC Sampling and Mobile Laboratories. The tank headspace temperature was determined to be 26 C. Air from the Tank BY-105 headspace was withdrawn via a heated sampling probe mounted in riser 10A, and transferred via heated tubing to the VSS sampling manifold. All heated zones of the VSS were maintained at approximately 65 C. Sampling media were prepared and analyzed by WHC, Oak Ridge National Laboratories, Pacific Northwest Laboratories, and Oregon Graduate Institute of Science and Technology through a contract with Sandia National Laboratories. The 46 tank air samples and 2 ambient air control samples collected are listed in Table X-1 by analytical laboratory. Table X-1 also lists the 10 trip blanks provided by the laboratories.

Huckaby, J.L.

1995-05-10T23:59:59.000Z

452

Tank 241-BY-106 vapor sampling and analysis tank characterization report  

SciTech Connect (OSTI)

Tank BY-106 headspace gas and vapor samples were collected and analyzed to help determine the potential risks to tank farm workers due to fugitive emissions from the tank. Tank BY-106 is on the Ferrocyanide Watch List. Samples were collected from Tank BY-106 using the vapor sampling system (VSS) on July 8, 1994 by WHC Sampling and Mobile Laboratories. The tank headspace temperature was determined to be 27 C. Air from the Tank BY-106 headspace was withdrawn via a heated sampling probe mounted in riser 10B, and transferred via heated tubing to the VSS sampling manifold. All heated zones of the VSS were maintained at approximately 65 C. Sampling media were prepared and analyzed by WHC, Oak Ridge National Laboratories, Pacific Northwest Laboratories, and Oregon Graduate Institute of Science and Technology through a contract with Sandia National Laboratories. The 46 tank air samples and 2 ambient air control samples collected are listed in Table X-1 by analytical laboratory. Table X-1 also lists the 10 trip blanks provided by the laboratories.

Huckaby, J.L.

1995-05-10T23:59:59.000Z

453

Tank 241-C-101 vapor sampling and analysis tank characterization report  

SciTech Connect (OSTI)

Tank C-101 headspace gas and vapor samples were collected and analyzed to help determine the potential risks of fugitive emissions to tank farm workers. Gas and vapor samples from the Tank C-101 headspace were collected on July 7, 1994 using the in situ sampling (ISS) method, and again on September 1, 1994 using the more robust vapor sampling system (VSS). Gas and vapor concentrations in Tank C-101 are influenced by its connections to other tanks and its ventilation pathways. At issue is whether the organic vapors in Tank C-101 are from the waste in that tank, or from Tanks C-102 or C-103. Tank C-103 is on the Organic Watch List; the other two are not. Air from the Tank C-101 headspace was withdrawn via a 7.9-m long heated sampling probe mounted in riser 8, and transferred via heated tubing to the VSS sampling manifold. The tank headspace temperature was determined to be 34.0 C, and all heated zones of the VSS were maintained at approximately 50 C. Sampling media were prepared and analyzed by WHC, Oak Ridge National Laboratories, Pacific Northwest Laboratories, and Oregon Graduate Institute of Science and Technology through a contract with Sandia National Laboratories. The 39 tank air samples and 2 ambient air control samples collected are listed in Table X-1 by analytical laboratory. Table X-1 also lists the 14 trip blanks and 2 field blanks provided by the laboratories.

Huckaby, J.L.

1995-05-31T23:59:59.000Z

454

Rock Sampling | Open Energy Information  

Open Energy Info (EERE)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data CenterFranconia, Virginia:FAQ < RAPID Jump to: navigation, searchVirginia BlueRiverwoods,Rock Sampling Details Activities (18) Areas

455

INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING DISTRIBUTION, AND POPULATION  

E-Print Network [OSTI]

INCOHERENCE AND THE PARAMETRIC TEST FRAMEWORK: MISCONCEIVED RELATIONSHIPS AMONG SAMPLE, SAMPLING Keywords: Parametric test, sample, population, sampling distributions Parametric tests are frequently parametric tests, nor hold beliefs that are consistent with that framework. The parametric test framework

Yu, Alex

456

Method for loading lipsomes with ionizable phosphorylated hydrophobic compounds, pharmaceutical preparations and a method for administering the preparations  

DOE Patents [OSTI]

A method of entrapping ionizable compounds, preferably phosphorylated hydrophobic compounds, into liposomes having transmembrane gradients is disclosed. The procedures involve forming liposomes in an acidic medium or a basic medium, adding to the acidic medium a cationic compound or to the basic medium an anionic compound and then adding a base to the cationic-containing medium or an acid to the anionic-containing medium, thereby inducing the ionizable compound into the liposomes` internal aqueous phase. The compound-entrapped liposomes prepared in accordance with the disclosed methods may be used as pharmaceutical preparations. Methods of administering such pharmaceutical preparations are also disclosed. 2 figs.

Mehlhorn, R.J.

1998-10-27T23:59:59.000Z

457

Method for loading lipsomes with ionizable phosphorylated hydrophobic compounds, pharmaceutical preparations and a method for administering the preparations  

DOE Patents [OSTI]

A method of entrapping ionizable compounds, preferably phosphorylated hydrophobic compounds, into liposomes having transmembrane gradients is disclosed. The procedures involve forming liposomes in an acidic medium or a basic medium, adding to the acidic medium a cationic compound or to the basic medium an anionic compound and then adding a base to the cationic-containing medium or an acid to the anionic-containing medium, thereby inducing the ionizable compound into the liposomes' internal aqueous phase. The compound-entrapped liposomes prepared in accordance with the disclosed methods may be used as pharmaceutical preparations. Methods of administering such pharmaceutical preparations are also disclosed.

Mehlhorn, Rolf Joachim (Richmond, CA)

1998-10-27T23:59:59.000Z

458

STAFFREPORT Prepared for the Bioenergy Interagency Working Group  

E-Print Network [OSTI]

STAFFREPORT Prepared for the Bioenergy Interagency Working Group: Air Resources Board 2010 2009 PROGRESS TO PLAN BIOENERGY ACTION PLAN FOR CALIFORNIA CALIFORNIA ENERGY COMMISSION #12, and et. al. 2010. 2009 Progress to Plan Bioenergy Action Plan for California. California Energy

459

Jefferson Lab's Science Education Website Helps Students Prepare...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

is the "Who Wants to Win 1,000,000 Math and Science Quiz Jefferson Lab's Science Education Website Helps Students Prepare for Upcoming Standards of Learning Tests April 7,...

460

Hamilton Truck Route Study Prepared for the City of Hamilton  

E-Print Network [OSTI]

Hamilton Truck Route Study Prepared for the City of Hamilton March 2012 #12;#12;Hamilton Truck and Logistics McMaster University Hamilton, Ontario March 2012 mitl.mcmaster.ca #12;#12;McMaster Institute

Haykin, Simon

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Appendix A. Notice of Inquiry: Preparation of Report to Congress...  

Office of Environmental Management (EM)

of Report to Congress on Price-Anderson Act. 62 Federal Register 68,272 (December 31, 1997) Appendix A. Notice of Inquiry: Preparation of Report to Congress on Price-Anderson...

462

Preparations of rare earth-iron alloys by thermite reduction  

DOE Patents [OSTI]

Disclosed is an improved method for the preparation of high-purity rare earth-iron alloys by the aluminothermic reduction of a mixture of rare earth and iron fluorides.

Schmidt, F.A.; Peterson, D.T.; Wheelock, J.T.

1985-10-28T23:59:59.000Z

463

Career Preparation for Handicapped Adolescents: A Matter of Appropriate Education  

E-Print Network [OSTI]

A complete individualization concept is presented as the avenue to achieve "appropriate education" for handicapped adolescents. Exemplified within the context of the educational goal of career preparation, this concept ...

Clark, Gary M.

1980-01-01T23:59:59.000Z

464

Data Preparation Process for the Buildings Performance Database  

SciTech Connect (OSTI)

The Buildings Performance Database (BPD) includes empirically measured data from a variety of data sources with varying degrees of data quality and data availability. The purpose of the data preparation process is to maintain data quality within the database and to ensure that all database entries have sufficient data for meaningful analysis and for the database API. Data preparation is a systematic process of mapping data into the Building Energy Data Exchange Specification (BEDES), cleansing data using a set of criteria and rules of thumb, and deriving values such as energy totals and dominant asset types. The data preparation process takes the most amount of effort and time therefore most of the cleansing process has been automated. The process also needs to adapt as more data is contributed to the BPD and as building technologies over time. The data preparation process is an essential step between data contributed by providers and data published to the public in the BPD.

Walter, Travis; Dunn, Laurel; Mercado, Andrea; Brown, Richard E.; Mathew, Paul

2014-06-30T23:59:59.000Z

465

RAPID SEPARATION METHOD FOR ACTINIDES IN EMERGENCY SOIL SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of actinides in soil and sediment samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used for samples up to 2 grams in emergency response situations. The actinides in soil method utilizes a rapid sodium hydroxide fusion method, a lanthanum fluoride soil matrix removal step, and a streamlined column separation process with stacked TEVA, TRU and DGA Resin cartridges. Lanthanum was separated rapidly and effectively from Am and Cm on DGA Resin. Vacuum box technology and rapid flow rates are used to reduce analytical time. Alpha sources are prepared using cerium fluoride microprecipitation for counting by alpha spectrometry. The method showed high chemical recoveries and effective removal of interferences. This new procedure was applied to emergency soil samples received in the NRIP Emergency Response exercise administered by the National Institute for Standards and Technology (NIST) in April, 2009. The actinides in soil results were reported within 4-5 hours with excellent quality.

Maxwell, S.; Culligan, B.; Noyes, G.

2009-11-09T23:59:59.000Z

466

Methods and apparatuses for preparing upgraded pyrolysis oil  

DOE Patents [OSTI]

Methods and apparatuses for preparing upgraded pyrolysis oil are provided herein. In an embodiment, a method of preparing upgraded pyrolysis oil includes providing a biomass-derived pyrolysis oil stream having an original oxygen content. The biomass-derived pyrolysis oil stream is hydrodeoxygenated under catalysis in the presence of hydrogen to form a hydrodeoxygenated pyrolysis oil stream comprising a cyclic paraffin component. At least a portion of the hydrodeoxygenated pyrolysis oil stream is dehydrogenated under catalysis to form the upgraded pyrolysis oil.

Brandvold, Timothy A; Baird, Lance Awender; Frey, Stanley Joseph

2013-10-01T23:59:59.000Z

467

Glass flask air sample analysis through Gas Chromatography in India: Implications for constraining CO2 surface fluxes  

E-Print Network [OSTI]

for an air inlet (equipped with a 7µm filter), a pump and a battery placed below the ON/OFF button, a flow to the site measurements, they are prepared and evacuated. We pump and heat the flasks. During pumping the temperature is +60 dc. Flasks are pumped for 72 hours. Outlook Air sampling started at two new stations, Cape

468

ANALYSIS OF VAPORS FROM METHYLENE CHLORIDE EXTRACTS OF NUCLEAR GRADE HEPA FILTER FIBERGLASS SAMPLES  

SciTech Connect (OSTI)

While several organic compounds were detected in the vapor samples used in the reenactment of the preparation of mounts from the extracts of nuclear grade high-efficiency particulate air filter fiberglass samples, the most significant species present in the samples were methylene chloride, phenol, phenol-d6, and 2-fluorophenol. These species were all known to be present in the extracts, but were expected to have evaporated during the preparation of the mounts, as the mounts appeared to be dry before any vapor was collected. These species were present at the following percentages of their respective occupational exposure limits: methylene chloride, 2%; phenol, 0.4%; and phenol-d6, 0.6%. However, there is no established limit for 2-fluorophenol. Several other compounds were detected at low levels for which, as in the case of 2-fluorophenol, there are no established permissible exposure limits. These compounds include 2-chlorophenol; N-nitroso-1-propanamine; 2-fluoro-1,1{prime}-biphenyl; 1,2-dihydroacenaphthylene; 2,5-cyclohexadiene-1,4-dione,2,6-bis(1,1-dimethylethyl); trimethyl oxirane; n-propylpropanamine; 2-(Propylamino)ethanol; 4-methoxy-1-butene; 6-methyl-5-hepten-2-one; and 3,4-dimethylpyridine. Some of these were among those added as surrogates or spike standards as part ofthe Advanced Technologies and Laboratories International, Inc. preparation ofthe extract of the HEPA filter media and are indicated as such in the data tables in Section 2, Results; other compounds found were not previously known to be present. The main inorganic species detected (sulfate, sodium, and sulfur) are also consistent with species added in the preparation of the methylene chloride extract of the high-efficiency particulate air sample.

FRYE JM; ANASTOS HL; GUTIERREZ FC

2012-06-07T23:59:59.000Z

469

Low temperature synthesis of nanocrystalline magnesium aluminate with high surface area by surfactant assisted precipitation method: Effect of preparation conditions  

SciTech Connect (OSTI)

Highlights: ? MgAl{sub 2}O{sub 4} showed a high surface area and nanocrystalline structure. ? Addition of polymeric surfactant affected the structural properties of MgAl{sub 2}O{sub 4}. ? MgAl{sub 2}O{sub 4} prepared with surfactant showed a hollow cylindrical shape. -- Abstract: A surfactant assisted co-precipitation method was employed for the low temperature synthesis of magnesium aluminate spinel with nanocrystalline size and high specific surface area. Pluronic P123 triblock copolymer and ammonia solution were used as surfactant and precipitation agent, respectively. The prepared samples were characterized by thermal gravimetric and differential thermal gravimetric analyses (TG/DTG), X-ray diffraction (XRD), N{sub 2} adsorption (BET) and transmission electron microscopy (TEM) techniques. The effects of several process parameters such as refluxing temperature, refluxing time, pH, P123 to metals mole ratio (P123/metals) and calcination temperature on the structural properties of the samples were investigated. The obtained results showed that, among the process parameters pH and refluxing temperature have a significant effect on the structural properties of samples. The results revealed that increase in pH from 9.5 to 11 and refluxing temperature from 40 °C to 80 °C increased the specific surface area of prepared samples in the range of 157–188 m{sup 2} g{sup ?1} and 162–184 m{sup 2} g{sup ?1}, respectively. The XRD analysis showed the single-phase MgAl{sub 2}O{sub 4} was formed at 700 °C.

Mosayebi, Zeinab [Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan (Iran, Islamic Republic of)] [Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan (Iran, Islamic Republic of); Rezaei, Mehran, E-mail: rezaei@kashanu.ac.ir [Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan (Iran, Islamic Republic of) [Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan (Iran, Islamic Republic of); Catalyst and Advanced Materials Research Laboratory, Chemical Engineering Department, Faculty of Engineering, University of Kashan, Kashan (Iran, Islamic Republic of); Hadian, Narges [Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan (Iran, Islamic Republic of)] [Institute of Nanoscience and Nanotechnology, University of Kashan, Kashan (Iran, Islamic Republic of); Kordshuli, Fazlollah Zareie [Shiraz Petrochemical Co., Shiraz (Iran, Islamic Republic of)] [Shiraz Petrochemical Co., Shiraz (Iran, Islamic Republic of); Meshkani, Fereshteh [Catalyst and Advanced Materials Research Laboratory, Chemical Engineering Department, Faculty of Engineering, University of Kashan, Kashan (Iran, Islamic Republic of)] [Catalyst and Advanced Materials Research Laboratory, Chemical Engineering Department, Faculty of Engineering, University of Kashan, Kashan (Iran, Islamic Republic of)

2012-09-15T23:59:59.000Z

470

Sample introduction apparatus for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

Van den Engh, Ger (Seattle, WA)

1998-01-01T23:59:59.000Z

471

Sample introduction system for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

Engh, G. van den

1997-02-11T23:59:59.000Z

472

Sample introduction system for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning, HPLC tubing and fittings may be used in a manner which facilitates removing of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it.

Van den Engh, Ger (Seattle, WA)

1997-01-01T23:59:59.000Z

473

Sample introduction apparatus for a flow cytometer  

DOE Patents [OSTI]

A sample introduction system for a flow cytometer allows easy change of sample containers such as test tubes and facilitates use in high pressure environments. The sample container includes a cap having a pressure supply chamber and a sample container attachment cavity. A sample container may be automatically positioned into the attachment cavity so as to sealably engage the end of the sample container as its outer surface. This positioning may be accomplished through some sample introduction mechanism. To facilitate cleaning HPLC tubing and fittings may be used in a manner which facilitates removable of the entire tubing from both the nozzle container and other sample container cap to permit its replacement to avoid contamination. The sample container support may include horizontal stops which loosely limit the movement of the sample container and thus avoid further stresses upon it. 3 figs.

Van den Engh, G.

1998-03-10T23:59:59.000Z

474

Synchronized sampling improves fault location  

SciTech Connect (OSTI)

Transmission line faults must be located accurately to allow maintenance crews to arrive at the scene and repair the faulted section as soon as possible. Rugged terrain and geographical layout cause some sections of power transmission lines to be difficult to reach. In the past, a variety of fault location algorithms were introduced as either an add-on feature in protective relays or stand-alone implementation in fault locators. In both cases, the measurements of current and voltages were taken at one terminal of a transmission line only. Under such conditions, it may become difficult to determine the fault location accurately, since data from other transmission line ends are required for more precise computations. In the absence of data from the other end, existing algorithms have accuracy problems under several circumstances, such as varying switching and loading conditions, fault infeed from the other end, and random value of fault resistance. Most of the one-end algorithms were based on estimation of voltage and current phasors. The need to estimate phasors introduces additional difficulty in high-speed tripping situations where the algorithms may not be fast enough in determining fault location accurately before the current signals disappear due to the relay operation and breaker opening. This article introduces a unique concept of high-speed fault location that can be implemented either as a simple add-on to the digital fault recorders (DFRs) or as a stand-alone new relaying function. This advanced concept is based on the use of voltage and current samples that are synchronously taken at both ends of a transmission line. This sampling technique can be made readily available in some new DFR designs incorporating receivers for accurate sampling clock synchronization using the satellite Global Positioning System (GPS).

Kezunovic, M. [Texas A and M Univ., College Station, TX (United States)] [Texas A and M Univ., College Station, TX (United States); Perunicic, B. [Lamar Univ., Beaumont, TX (United States)] [Lamar Univ., Beaumont, TX (United States)

1995-04-01T23:59:59.000Z

475

Licensing Guide and Sample License  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmospheric Optical Depth7-1D: VegetationEquipment Surfaces and Interfaces Sample6, 2011 LawrenceE CAnalytical InstrumentationEnergy

476

Sample Environments at Sector 30  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE:1 First Use of Energy for All Purposes (Fuel and Nonfuel),Feet) Year Jan Feb Mar Apr MayAtmosphericNuclear Security Administration the1 -the Mid-Infrared0 ResourceAwardsSafeguards and SecuritySafety Salt LakeSample

477

CARRIER PREPARATION BUILDING MATERIALS HANDLING SYSTEM DESCRIPTION DOCUMENT  

SciTech Connect (OSTI)

The Carrier Preparation Building Materials Handling System receives rail and truck shipping casks from the Carrier/Cask Transport System, and inspects and prepares the shipping casks for return to the Carrier/Cask Transport System. Carrier preparation operations for carriers/casks received at the surface repository include performing a radiation survey of the carrier and cask, removing/retracting the personnel barrier, measuring the cask temperature, removing/retracting the impact limiters, removing the cask tie-downs (if any), and installing the cask trunnions (if any). The shipping operations for carriers/casks leaving the surface repository include removing the cask trunnions (if any), installing the cask tie-downs (if any), installing the impact limiters, performing a radiation survey of the cask, and installing the personnel barrier. There are four parallel carrier/cask preparation lines installed in the Carrier Preparation Building with two preparation bays in each line, each of which can accommodate carrier/cask shipping and receiving. The lines are operated concurrently to handle the waste shipping throughputs and to allow system maintenance operations. One remotely operated overhead bridge crane and one remotely operated manipulator is provided for each pair of carrier/cask preparation lines servicing four preparation bays. Remotely operated support equipment includes a manipulator and tooling and fixtures for removing and installing personnel barriers, impact limiters, cask trunnions, and cask tie-downs. Remote handling equipment is designed to facilitate maintenance, dose reduction, and replacement of interchangeable components where appropriate. Semi-automatic, manual, and backup control methods support normal, abnormal, and recovery operations. Laydown areas and equipment are included as required for transportation system components (e.g., personnel barriers and impact limiters), fixtures, and tooling to support abnormal and recovery operations. The Carrier Preparation Building Materials Handling System interfaces with the Cask/Carrier Transport System to move the carriers to and from the system. The Carrier Preparation Building System houses the equipment and provides the facility, utility, safety, communications, and auxiliary systems supporting operations and protecting personnel.

E.F. Loros

2000-06-28T23:59:59.000Z

478

TRU waste-sampling program  

SciTech Connect (OSTI)

As part of a TRU waste-sampling program, Los Alamos National Laboratory retrieved and examined 44 drums of /sup 238/Pu- and /sup 239/Pu-contaminated waste. The drums ranged in age from 8 months to 9 years. The majority of drums were tested for pressure, and gas samples withdrawn from the drums were analyzed by a mass spectrometer. Real-time radiography and visual examination were used to determine both void volumes and waste content. Drum walls were measured for deterioration, and selected drum contents were reassayed for comparison with original assays and WIPP criteria. Each drum tested at atmospheric pressure. Mass spectrometry revealed no problem with /sup 239/Pu-contaminated waste, but three 8-month-old drums of /sup 238/Pu-contaminated waste contained a potentially hazardous gas mixture. Void volumes fell within the 81 to 97% range. Measurements of drum walls showed no significant corrosion or deterioration. All reassayed contents were within WIPP waste acceptance criteria. Five of the drums opened and examined (15%) could not be certified as packaged. Three contained free liquids, one had corrosive materials, and one had too much unstabilized particulate. Eleven drums had the wrong (or not the most appropriate) waste code. In many cases, disposal volumes had been inefficiently used. 2 refs., 23 figs., 7 tabs.

Warren, J.L.; Zerwekh, A.

1985-08-01T23:59:59.000Z

479

A nuclear magnetic resonance study of hydrogen in battery and chemically prepared material  

SciTech Connect (OSTI)

Solid-state magic-angle-spinning nuclear magnetic resonance studies have been undertaken on positive plate material from lead-acid batteries and on samples of both pure ..cap alpha..-PbO/sub 2/ and pure ..beta..-PbO/sub 2/ prepared by nonelectrochemical methods. Battery positive plate samples contain protons in two different surface and near surface configurations. One of these proton species is associated with mobile, isolated, adsorbed hydroxyl groups, and/or water molecules that can be removed by outgassing. The other proton species is not removed by outgassing; it probably corresponds to water molecules and/of closely spaced hydroxyl groups trapped on internal crystal surfaces. The proton species present in fresh (uncycled) positive plate material are not significantly different in either configuration or abundance from those in extensively cycled samples. Thus, it is unlikely that decline in battery capacity with cycling service is associated with a change in the hydrogen content of PbO/sub 2/.

Hill, R.J.; Jessel, A.M.

1987-06-01T23:59:59.000Z

480

Field emission from gadolinium silicide prepared by ion implantation with electron beam annealing  

SciTech Connect (OSTI)

A silicon-based field emission cathode, the rare earth silicide GdSi{sub 2} was prepared by implanting Gd ions into silicon using a metal vapor vacuum arc ion source and subsequently annealed by electron beam. For as-implanted samples, turn-on field was about 21 V/{mu}m at a current density of 1 {mu}A/cm{sup 2} and a field emission current density of 1 mA/cm{sup 2} was reached at an applied field of 34 V/{mu}m. After annealing, the turn-on field could be as low as 9 V/{mu}m and the current density of 1 mA/cm{sup 2} can be reached at an applied field of 14 V/{mu}m. X-ray diffraction with x-ray photoelectron spectroscopy analyses and atomic force microscopy were used to characterize microstructure changes of the samples. The results showed that these excellent field emission characteristics were attributed to the GdSi{sub 2} compounds formed in the samples. The field emission mechanism was discussed in terms of Fowler-Nordheim (FN) theory. It was found that FN plots could be divided into two segments obviously, and this was perhaps because of the thermal effect in the process of field emission.

Duan, H. G.; Xie, E. Q.; Ye, F. [School of Physical Science and Technology, Lanzhou University, Lanzhou 730000 (China)

2007-03-15T23:59:59.000Z

Note: This page contains sample records for the topic "diffraction-limited sample preparation" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


481

ANALYSIS OF SAMPLES FROM TANK 5F CHEMICAL CLEANING  

SciTech Connect (OSTI)

The Savannah River Site (SRS) is preparing Tank 5F for closure. The first step in preparing the tank for closure is mechanical sludge removal. Following mechanical sludge removal, SRS performed chemical cleaning with oxalic acid to remove the sludge heel. Personnel are currently assessing the effectiveness of the chemical cleaning. SRS personnel collected liquid samples during chemical cleaning and submitted them to Savannah River National Laboratory (SRNL) for analysis. Following chemical cleaning, they collected a solid sample (also known as 'process sample') and submitted it to SRNL for analysis. The authors analyzed these samples to assess the effectiveness of the chemical cleaning process. The conclusions from this work are: (1) With the exception of iron, the dissolution of sludge components from Tank 5F agreed with results from the actual waste demonstration performed in 2007. The fraction of iron removed from Tank 5F by chemical cleaning was significantly less than the fraction removed in the SRNL demonstrations. The likely cause of this difference is the high pH following the first oxalic acid strike. (2) Most of the sludge mass remaining in the tank is iron and nickel. (3) The remaining sludge contains approximately 26 kg of barium, 37 kg of chromium, and 37 kg of mercury. (4) Most of the radioactivity remaining in the residual material is beta emitters and {sup 90}Sr. (5) The chemical cleaning removed more than {approx} 90% of the uranium isotopes and {sup 137}Cs. (6) The chemical cleaning removed {approx} 70% of the neptunium, {approx} 83% of the {sup 90}Sr, and {approx} 21% of the {sup 60}Co. (7) The chemical cleaning removed less than 10% of the plutonium, americium, and curium isotopes. (8) The chemical cleaning removed more than 90% of the aluminium, calcium, and sodium from the tank. (9) The cleaning operations removed 61% of lithium, 88% of non-radioactive strontium, and 65% of zirconium. The {sup 90}Sr and non-radioactive strontium were measured by different methods, and the differences in the fraction removed are not statistically significant. (10) Chemical cleaning removed 10-50% of the barium, chromium, iron, magnesium, manganese, and silicon. (11) Chemical cleaning removed only {approx}1% of the nickel.

Poirier, M.; Fink, S.

2011-03-07T23:59:59.000Z

482

Effect of different intravenous iron preparations on lymphocyte intracellular reactive oxygen species generation and subpopulation survival.  

E-Print Network [OSTI]

IV iron compounds induced greater intracellular ROS generation,IV iron preparations on intracellular reactive oxygen species generationIV iron preparations on intracellular immune cell ROS generation

Gupta, Ajay; Zhuo, Jiaying; Zha, Junli; Reddy, Srinivasa; Olp, Jonathan; Pai, Amy

2010-01-01T23:59:59.000Z

483

EIS-0082-S2: Notice of Intent to Prepare a Supplemental Environmental...  

Office of Environmental Management (EM)

082-S2: Notice of Intent to Prepare a Supplemental Environmental Impact Statement EIS-0082-S2: Notice of Intent to Prepare a Supplemental Environmental Impact Statement...

484

EIS-0236: Notice of Intent to Prepare a Supplement to the Programmatic...  

Energy Savers [EERE]

: Notice of Intent to Prepare a Supplement to the Programmatic Environmental Impact Statement EIS-0236: Notice of Intent to Prepare a Supplement to the Programmatic Environmental...

485

Method and apparatus for data sampling  

DOE Patents [OSTI]

A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium.

Odell, Daniel M. C. (Aiken, SC)

1994-01-01T23:59:59.000Z

486

Method and apparatus for data sampling  

DOE Patents [OSTI]

A method and apparatus for sampling radiation detector outputs and determining event data from the collected samples is described. The method uses high speed sampling of the detector output, the conversion of the samples to digital values, and the discrimination of the digital values so that digital values representing detected events are determined. The high speed sampling and digital conversion is performed by an A/D sampler that samples the detector output at a rate high enough to produce numerous digital samples for each detected event. The digital discrimination identifies those digital samples that are not representative of detected events. The sampling and discrimination also provides for temporary or permanent storage, either serially or in parallel, to a digital storage medium. 6 figures.

Odell, D.M.C.

1994-04-19T23:59:59.000Z

487

Fluid sampling system for a nuclear reactor  

DOE Patents [OSTI]

A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump. 1 fig.

Lau, L.K.; Alper, N.I.

1994-11-22T23:59:59.000Z

488

Fluid sampling system for a nuclear reactor  

DOE Patents [OSTI]

A system of extracting fluid samples, either liquid or gas, from the interior of a nuclear reactor containment utilizes a jet pump. To extract the sample fluid, a nonradioactive motive fluid is forced through the inlet and discharge ports of a jet pump located outside the containment, creating a suction that draws the sample fluid from the containment through a sample conduit connected to the pump suction port. The mixture of motive fluid and sample fluid is discharged through a return conduit to the interior of the containment. The jet pump and means for removing a portion of the sample fluid from the sample conduit can be located in a shielded sample grab station located next to the containment. A non-nuclear grade active pump can be located outside the grab sampling station and the containment to pump the nonradioactive motive fluid through the jet pump.

Lau, Louis K. (Monroeville, PA); Alper, Naum I. (Monroeville, PA)

1994-01-01T23:59:59.000Z

489

Preparation, characterization and catalytic properties of MCM-48 supported tungstophosphoric acid mesoporous materials for green synthesis of benzoic acid  

SciTech Connect (OSTI)

MCM-48 and tungstophosphoric acid (HPW) were prepared and applied for the synthesis of HPW/MCM-48 mesoporous materials. The characterization results showed that HPW/MCM-48 obtained retained the typical mesopore structure of MCM-48, and the textural parameters decreased with the increase loading of HPW. The catalytic oxidation results of benzyl alcohol and benzaldehyde with 30% H{sub 2}O{sub 2} indicated that HPW/MCM-48 was an efficient catalyst for the green synthesis of benzoic acid. Furthermore, 35 wt% HPW/MCM-48 sample showed the highest activity under the reaction conditions. Highlights: • 5–45 wt% HPW/MCM-48 mesoporous catalysts were prepared and characterized. • Their catalytic activities for the green synthesis of benzoic acid were investigated. • HPW/MCM-48 was approved to be an efficient catalyst. • 5 wt% HPW/MCM-48 exhibited the highest catalytic activity.

Wu, Hai-Yan; Zhang, Xiao-Li; Chen, Xi; Chen, Ya; Zheng, Xiu-Cheng, E-mail: zhxch@zzu.edu.cn

2014-03-15T23:59:59.000Z

490

Evaporator Feed Qualification Analysis Of Tank 38H And 43H Samples: January 2010 Through April 2013  

SciTech Connect (OSTI)

This report provides the results of analyses that focused on the chemical species that pertain to the sodium aluminosilicate formation potential for archived Tank 38H and 43H subsurface samples from January 2010 through April 2013. Analyses included warm acid strike preparation followed by analysis of silicon, aluminum, and sodium and water dilution preparation followed by analysis for anions. The Tank 43H and 38H supernatant liquid silicon measurements for the January 2010 through April 2013 time period exhibit a slight increasing trend. Over this time period, the silicon concentration in the Tank 43H and Tank 38H samples averaged 179 mg/L and 235 mg/L, respectively. Comparison of Tank 43H sample results from 2005 through April 2013 to the previously developed process control models indicates that the current formation of sodium aluminosilicate in the 2H system is due to the seeded direct precipitation of cancrinite and sodalite.

Martino, C. J.; Coleman, C. J.

2013-08-21T23:59:59.000Z

491

Preparation and characterization of V/TiO{sub 2} nanocatalyst with magnetic nucleus of iron  

SciTech Connect (OSTI)

Graphical abstract: - Highlights: • Fe-V/TiO{sub 2} nanocatalyst is prepared. • Combination of sol–gel and wetness impregnation methods. • Facile separation of catalyst from medium by magnet. - Abstract: A magnetic composite containing V/TiO{sub 2} was prepared by combination of sol–gel and wetness impregnation methods. The effects of synthesis temperature, different weight percents of Fe supported on TiO{sub 2}, vanadium loading and the heating rate of calcination on the structure and morphology of nanocatalyst were investigated. The optimum conditions for synthesized catalyst were 40 wt.% of Fe, 15 wt.% of V and synthesis temperature equal to 30 °C. Characterization of catalyst is carried out using XRD, TGA, DSC, SEM, FTIR and N{sub 2} physisorption measurements. The magnetic character of nanocatalyst was measured using VSM, which showed the typical paramagnetic behavior of sample at room temperature with a saturation magnetization value equal to 8.283 emu/g. The nanocatalyst has a particle size about 56 nm and can easily be separated from medium by a magnet.

Feyzi, Mostafa; Rafiee, Hamid Reza, E-mail: rafieehr@yahoo.com; Ranjbar, Shahram; Jafari, Fataneh; Safari, Banafsheh

2013-11-15T23:59:59.000Z

492

ALARA ASSESSMENT OF SETTLER SLUDGE SAMPLING METHODS  

SciTech Connect (OSTI)

The purpose of this assessment is to compare underwater and above water settler sludge sampling methods to determine if the added cost for underwater sampling for the sole purpose of worker dose reductions is justified. Initial planning for sludge sampling included container, settler and knock-out-pot (KOP) sampling. Due to the significantly higher dose consequence of KOP sludge, a decision was made to sample KOP underwater to achieve worker dose reductions. Additionally, initial plans were to utilize the underwater sampling apparatus for settler sludge. Since there are no longer plans to sample KOP sludge, the decision for underwater sampling for settler sludge needs to be revisited. The present sampling plan calls for spending an estimated $2,500,000 to design and construct a new underwater sampling system (per A21 C-PL-001 RevOE). This evaluation will compare and contrast the present method of above water sampling to the underwater method that is planned by the Sludge Treatment Project (STP) and determine if settler samples can be taken using the existing sampling cart (with potentially minor modifications) while maintaining doses to workers As Low As Reasonably Achievable (ALARA) and eliminate the need for costly redesigns, testing and personnel retraining.

NELSEN LA

2009-01-30T23:59:59.000Z

493

Sample Residential Program Term Sheet | Department of Energy  

Broader source: Energy.gov (indexed) [DOE]

Sample Residential Program Term Sheet Sample Residential Program Term Sheet A sample for defining and elaborating on the specifics of a clean energy loan program. Sample...

494

An introduction to boson-sampling  

E-Print Network [OSTI]

Boson-sampling is a simplified model for quantum computing that may hold the key to implementing the first ever post-classical quantum computer. Boson-sampling is a non-universal quantum computer that is significantly more straightforward to build than any universal quantum computer proposed so far. We begin this chapter by motivating boson-sampling and discussing the history of linear optics quantum computing. We then summarize the boson-sampling formalism, discuss what a sampling problem is, explain why boson-sampling is easier than linear optics quantum computing, and discuss the Extended Church-Turing thesis. Next, sampling with other classes of quantum optical states is analyzed. Finally, we discuss the feasibility of building a boson-sampling device using existing technology.

Bryan T. Gard; Keith R. Motes; Jonathan P. Olson; Peter P. Rohde; Jonathan P. Dowling

2014-06-26T23:59:59.000Z

495

Principles for Sampling Airborne Radioactivity from Stacks  

SciTech Connect (OSTI)

This book chapter describes the special processes involved in sampling the airborne effluents from nuclear faciities. The title of the book is Radioactive Air Sampling Methods. The abstract for this chapter was cleared as PNNL-SA-45941.

Glissmeyer, John A.

2010-10-18T23:59:59.000Z

496

General Sample Submission Form University of Utah  

E-Print Network [OSTI]

in all applicable information as completely as possible Sample Information Sample ID / Description/MS/MS (FTMS) ______ Maldi/FTMS ______ Maldi/ToF ______ ESI/MS ______ ESI/FTMS _____ Location and Staff MS file

Hill, Chris

497

Sample holder for X-ray diffractometry  

DOE Patents [OSTI]

A sample holder for use with X-ray diffractometers with the capability to rotate the sample, as well as to adjust the position of the sample in the x, y, and z directions. Adjustment in the x direction is accomplished through loosening set screws, moving a platform, and retightening the set screws. Motion translators are used for adjustment in the y and z directions. An electric motor rotates the sample, and receives power from the diffractometer.

Hesch, Victor L. (Los Alamos, NM)

1992-01-01T23:59:59.000Z

498

E-Print Network 3.0 - air pollution sampling Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

sampling Search Powered by Explorit Topic List Advanced Search Sample search results for: air pollution sampling Page: << < 1 2 3 4 5 > >> 1 griculture is in the spotlight as a...

499

Electron microscopy study of NiW/Al{sub 2}O{sub 3}-F(x) sulfided catalysts prepared using oxisalt and thiosalt precursors  

SciTech Connect (OSTI)

Two different series of sulfided NiW catalysts supported on alumina modified with different amounts of fluoride, in the range 0.0-2.5 wt%, have been prepared by using two different tungsten precursor salts: ammonium metatungstate and ammonium tetrathiotungstate. Samples of both catalyst series have been examined by the use of high-resolution electron microscopy. For the oxisalt-prepared catalysts the results indicate that fluoride incorporation increases the size of WS{sub 2} crystallites but has little effect on the number of layers. On the other hand, the change of precursor salt significantly influences the stacking of WS{sub 2} crystallites without greatly affecting their size. The thiosalt method of preparation also leads to an excess of sulfur in the catalysts, which is distributed in a nonhomogeneous way. 16 refs., 13 figs., 2 tabs.

Ramirez, J.; Castillo, P.; Benitez, A. [Universidad Autonoma de Mexico City (Mexico)] [and others] [Universidad Autonoma de Mexico City (Mexico); and others

1996-01-01T23:59:59.000Z

500

RAPID SEPARATION METHOD FOR ACTINIDES IN EMERGENCY AIR FILTER SAMPLES  

SciTech Connect (OSTI)

A new rapid method for the determination of actinides and strontium in air filter samples has been developed at the Savannah River Site Environmental Lab (Aiken, SC, USA) that can be used in emergency response situations. The actinides and strontium in air filter method utilizes a rapid acid digestion method and a streamlined column separation process with stacked TEVA, TRU and Sr Resin cartridges. Vacuum box technology and rapid flow rates are used to reduce analytical time. Alpha emitters are prepared using cerium fluoride microprecipitation for counting by alpha spectrometry. The purified {sup 90}Sr fractions are mounted directly on planchets and counted by gas flow proportional counting. The method showed high chemical recoveries and effective removal of interferences. This new procedure was applied to emergency air filter samples received in the NRIP Emergency Response exercise administered by the National Institute for Standards and Technology (NIST) in April, 2009. The actinide and {sup 90}Sr in air filter results were reported in {approx}4 hours with excellent quality.

Maxwell, S.; Noyes, G.; Culligan, B.

2010-02-03T23:59:59.000Z