National Library of Energy BETA

Sample records for determination metallographic preparation

  1. Single Crystal Preparation for High-Pressure Experiments in the...

    Office of Scientific and Technical Information (OSTI)

    Our sample preparation steps include cutting, classical metallographic polishing, and laser ablation. The key to our new process is the preservation of crystallinity during cutting ...

  2. Determination of Ideal Broth Formulations Needed to Prepare Hydrous Hafnium Oxide Microspheres via the Internal Gelation Process

    SciTech Connect (OSTI)

    Collins, Jack Lee; Hunt, Rodney Dale; Simmerman, S. G.

    2009-02-01

    A simple test-tube methodology was used to determine optimum process parameters for preparing hydrous hafnium oxide microspheres by the internal gelation process. Broth formulations of hafnyl chloride [HfOCl{sub 2}], hexamethylenetetramine, and urea were found that can be used to prepare hydrous hafnium oxide gel spheres in the temperature range of 70-90 C. A few gel-forming runs were made in which microspheres were prepared with some of these formulations in order to equate the test-tube gelation times with actual gelation times. These preparations confirmed that the test-tube methodology is reliable for determining the ideal broths.

  3. Method and apparatus for the preparation of liquid samples for determination of boron

    DOE Patents [OSTI]

    Siemer, D.D.

    A method and apparatus are described for the preparation of a liquid sample for the quantitative determination of boron by flame photometry. The sample is combined in a vessel with sulfuric acid, and an excess of methanol is added thereto. The methanol reacts with any boron present in the sample to form trimethyl borate which is volatilized by the heat of reaction between the excess methanol and sulfuric acid. The volatilized trimethyl borate is withdrawn from the vessel by either a partial vacuum or a positive pressure and is rapidly transferred to a standard flame photometer. The method is free of interference from typical boron concomitants.

  4. Method and apparatus for the preparation of liquid samples for determination of boron

    DOE Patents [OSTI]

    Siemer, Darryl D.

    1986-01-01

    A method and apparatus for the preparation of a liquid sample for the quantitative determination of boron by flame photometry. The sample is combined in a vessel with sulfuric acid, and an excess of methanol is added thereto. The methanol reacts with any boron present in the sample to form trimethyl borate which is volatilized by the heat of reaction between the excess methanol and sulfuric acid. The volatilized trimethyl borate is withdrawn from the vessel by either a partial vacuum or a positive pressure and is rapidly transferred to a standard flame photometer. The method is free of interference from typical boron concomitants.

  5. CX-004444: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Metallographic Preparation (Section, Mount, Grind, Polish and Optical Metallography) of a U308 Glass Coated Nickel-BaseCX(s) Applied: B3.6Date: 10/29/2010Location(s): Aiken, South CarolinaOffice(s): Savannah River Operations Office

  6. CX-004790: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Metallographic Preparation (Section, Mount, Grind, Polish and Optical Metallography) of a U308 (Depleted Uranium) Glass Coated Nickel-BaseCX(s) Applied: B3.6Date: 10/29/2010Location(s): Aiken, South CarolinaOffice(s): Savannah River Operations Office

  7. NGSI FY15 Final Report. Innovative Sample Preparation for in-Field Uranium Isotopic Determinations

    SciTech Connect (OSTI)

    Yoshida, Thomas M.; Meyers, Lisa

    2015-11-10

    Our FY14 Final Report included an introduction to the project, background, literature search of uranium dissolution methods, assessment of commercial off the shelf (COTS) automated sample preparation systems, as well as data and results for dissolution of bulk quantities of uranium oxides, and dissolution of uranium oxides from swipe filter materials using ammonium bifluoride (ABF). Also, discussed were reaction studies of solid ABF with uranium oxide that provided a basis for determining the ABF/uranium oxide dissolution mechanism. This report details the final experiments for optimizing dissolution of U3O8 and UO2 using ABF and steps leading to development of a Standard Operating Procedure (SOP) for dissolution of uranium oxides on swipe filters.

  8. Microwave-assisted sample preparation of coal and coal fly ash for subsequent metal determination

    SciTech Connect (OSTI)

    Srogi, K.

    2007-01-15

    The aim of this paper is to review microwave-assisted digestion of coal and coal fly ash. A brief description of microwave heating principles is presented. Microwave-assisted digestion appears currently to be the most popular preparation technique, possibly due to the comparatively rapid sample preparation and the reduction of contamination, compared to the conventional hot-plate digestion methods.

  9. Determination

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Determinants of Household Use of Selected Energy Star Appliances May 2016 Independent Statistics & Analysis www.eia.gov U.S. Department of Energy Washington, DC 20585 U.S. Energy Information Administration | Determinants of Household Use of Selected Energy Star Appliances i This report was prepared by the U.S. Energy Information Administration (EIA), the statistical and analytical agency within the U.S. Department of Energy. By law, EIA's data, analyses, and forecasts are independent of

  10. Comparison of SW-846 method 3051 and SW-846 method 7471A for the preparation of solid waste samples for mercury determination

    SciTech Connect (OSTI)

    Giaquinto, J.M.; Essling, A.M.; Keller, J.M.

    1996-08-01

    This report describes experimental studies to evaluate the use of EPA SW-846 method 3051 for preparation and dissolution of solid samples for Hg analysis. The study showed that the method is effective in dissolution of four sample types without significant loss of Hg. Based on results of this study, method 3051 was used for analysis of high radioactive waste samples to obtain results for a number of RCRA regulated metals without the need to utilize a separate sample preparation method (EPA SW-846 method 7471A) specific only for Hg.

  11. Crack growth rates and metallographic examinations of Alloy 600 and Alloy 82/182 from field components and laboratory materials tested in PWR environments.

    SciTech Connect (OSTI)

    Alexandreanu, B.; Chopra, O. K.; Shack, W. J.

    2008-05-05

    In light water reactors, components made of nickel-base alloys are susceptible to environmentally assisted cracking. This report summarizes the crack growth rate results and related metallography for field and laboratory-procured Alloy 600 and its weld alloys tested in pressurized water reactor (PWR) environments. The report also presents crack growth rate (CGR) results for a shielded-metal-arc weld of Alloy 182 in a simulated PWR environment as a function of temperature between 290 C and 350 C. These data were used to determine the activation energy for crack growth in Alloy 182 welds. The tests were performed by measuring the changes in the stress corrosion CGR as the temperatures were varied during the test. The difference in electrochemical potential between the specimen and the Ni/NiO line was maintained constant at each temperature by adjusting the hydrogen overpressure on the water supply tank. The CGR data as a function of temperature yielded activation energies of 252 kJ/mol for a double-J weld and 189 kJ/mol for a deep-groove weld. These values are in good agreement with the data reported in the literature. The data reported here and those in the literature suggest that the average activation energy for Alloy 182 welds is on the order of 220-230 kJ/mol, higher than the 130 kJ/mol commonly used for Alloy 600. The consequences of using a larger value of activation energy for SCC CGR data analysis are discussed.

  12. Metallographic autopsies of full-scale ITER prototype cable-in-conduit conductors after full cyclic testing in SULTAN: III. The importance of strand surface roughness in long twist pitch conductors

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Sanabria, Charlie; Lee, Peter J.; Starch, William; Devred, Arnaud; Larbalestier, David C.

    2016-05-31

    As part of the ITER conductor qualification process, 3 m long Cable-in-Conduit Conductors (CICCs) were tested at the SULTAN facility under conditions simulating ITER operation so as to establish the current sharing temperature, Tcs, as a function of multiple full Lorentz force loading cycles. After a comprehensive evaluation of both the Toroidal Field (TF) and the Central Solenoid (CS) conductors, it was found that Tcs degradation was common in long twist pitch TF conductors while short twist pitch CS conductors showed some Tcs increase. However, one kind of TF conductors containing superconducting strand fabricated by the Bochvar Institute of Inorganicmore » Materials (VNIINM) avoided Tcs degradation despite having long twist pitch. In our earlier metallographic autopsies of long and short twist pitch CS conductors, we observed a substantially greater transverse strand movement under Lorentz force loading for long twist pitch conductors, while short twist pitch conductors had negligible transverse movement. With help from the literature, we concluded that the transverse movement was not the source of Tcs degradation but rather an increase of the compressive strain in the Nb3Sn filaments possibly induced by longitudinal movement of the wires. Like all TF conductors this TF VNIINM conductor showed large transverse motions under Lorentz force loading, but Tcs actually increased, as in all short twist pitch CS conductors. We here propose that the high surface roughness of the VNIINM strand may be responsible for the suppression of the compressive strain enhancement (characteristic of long twist pitch conductors). Furthermore, it appears that increasing strand surface roughness could improve the performance of long twist pitch CICCs.« less

  13. Holding fixture for metallographic mount polishing

    DOE Patents [OSTI]

    Barth, C.H.; Cramer, C.E.

    1997-12-30

    A fixture is described for holding mounted specimens for polishing, having an arm; a body attached to one end of the arm, the body having at least one flange having an opening to accommodate a mounted specimen; and a means applying pressure against the outer surface of the mounted specimen to hold the specimen in contact with the polishing surface. 3 figs.

  14. Holding fixture for metallographic mount polishing

    DOE Patents [OSTI]

    Barth, Clyde H.; Cramer, Charles E.

    1997-01-01

    A fixture for holding mounted specimens for polishing, having an arm; a body attached to one end of the arm, the body having at least one flange having an opening to accommodate a mounted specimen; and a means applying pressure against the outer surface of the mounted specimen to hold the specimen in contact with the polishing surface.

  15. RW Prepared

    Office of Legacy Management (LM)

    r tz s /r;1 RW Prepared by Oak Ridge Associated Un iversities Prepared for Division of Remedial Action Projects U.S. Department of Energy C O M P R E H E N S I V E R A D I O L O G I C A L S U R V E Y O F F - S I T E P R O P E R T Y B N I A G A R A F A L L S S T O R A G E S I T E L E W I S T O N , N E W Y O R K J . D . B E R G E R R a d i o l o g i c a l S i t e A s s e s s m e n t p r o g r a m Manpower Education, Research, and Training Division FINAL REPORT M a y 1 9 8 4 COMPREEENSIVE

  16. LCLS Sample Preparation Laboratory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    LCLS Sample Preparation Laboratory Kayla Zimmerman | (650) 926-6281 Lisa Hammon, LCLS Lab Coordinator Welcome to the LCLS Sample Preparation Laboratory. This small general use wet lab is located in Rm 109 of the Far Experimental Hall near the MEC, CXI, and XCS hutches. It conveniently serves all LCLS hutches and is available for final stage sample preparation. Due to space limitations, certain types of activities may be restricted and all access must be scheduled in advance. User lab bench

  17. Coal Preparation Plant Simulation

    Energy Science and Technology Software Center (OSTI)

    1992-02-25

    COALPREP assesses the degree of cleaning obtained with different coal feeds for a given plant configuration and mode of operation. It allows the user to simulate coal preparation plants to determine an optimum plant configuration for a given degree of cleaning. The user can compare the performance of alternative plant configurations as well as determine the impact of various modes of operation for a proposed configuration. The devices that can be modelled include froth flotationmore » devices, washers, dewatering equipment, thermal dryers, rotary breakers, roll crushers, classifiers, screens, blenders and splitters, and gravity thickeners. The user must specify the plant configuration and operating conditions and a description of the coal feed. COALPREP then determines the flowrates within the plant and a description of each flow stream (i.e. the weight distribution, percent ash, pyritic sulfur and total sulfur, moisture, BTU content, recoveries, and specific gravity of separation). COALPREP also includes a capability for calculating the cleaning cost per ton of coal. The IBM PC version contains two auxiliary programs, DATAPREP and FORLIST. DATAPREP is an interactive preprocessor for creating and editing COALPREP input data. FORLIST converts carriage-control characters in FORTRAN output data to ASCII line-feed (X''0A'') characters.« less

  18. Coal Preparation Plant Simulation

    Energy Science and Technology Software Center (OSTI)

    1992-02-25

    COALPREP assesses the degree of cleaning obtained with different coal feeds for a given plant configuration and mode of operation. It allows the user to simulate coal preparation plants to determine an optimum plant configuration for a given degree of cleaning. The user can compare the performance of alternative plant configurations as well as determine the impact of various modes of operation for a proposed configuration. The devices that can be modelled include froth flotationmore » devices, washers, dewatering equipment, thermal dryers, rotary breakers, roll crushers, classifiers, screens, blenders and splitters, and gravity thickeners. The user must specify the plant configuration and operating conditions and a description of the coal feed. COALPREP then determines the flowrates within the plant and a description of each flow stream (i.e. the weight distribution, percent ash, pyritic sulfur and total sulfur, moisture, BTU content, recoveries, and specific gravity of separation). COALPREP also includes a capability for calculating the cleaning cost per ton of coal.« less

  19. The Sample Preparation Laboratories | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Cynthia Patty 1 Sam Webb 2 John Bargar 3 Arizona 4 Chemicals 5 Team Work 6 Bottles 7 Glass 8 Plan Ahead! See the tabs above for Laboratory Access and forms you'll need to complete. Equipment and Chemicals tabs detail resources already available on site. Avoid delays! Hazardous materials use may require a written Standard Operating Procedure (SOP) before you work. Check the Chemicals tab for more information. The Sample Preparation Laboratories The Sample Preparation Laboratories provide wet lab

  20. International perspectives on coal preparation

    SciTech Connect (OSTI)

    1997-12-31

    The report consists of the vugraphs from the presentations which covered the following topics: Summaries of the US Department of Energy`s coal preparation research programs; Preparation trends in Russia; South African coal preparation developments; Trends in hard coal preparation in Germany; Application of coal preparation technology to oil sands extraction; Developments in coal preparation in China; and Coal preparation in Australia.

  1. EIS-0403: Notice of Intent to Prepare a Programmatic Environmental...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    EIS-0403: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Solar Energy Development in Six Southwestern States The Agencies have determined that a...

  2. Sandia National Laboratories: Research: Facilities: Technology...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    this, we apply spectroscopic and diffraction techniques, light and electron microscopy, metallographic preparation, surface analysis, chemical analysis, thermal analysis, and...

  3. Preparation of acetaldehyde

    DOE Patents [OSTI]

    Tustin, G.C.; Depew, L.S.

    1997-10-21

    Disclosed is a process for the preparation of acetaldehyde by the hydrogenation of ketene in the presence of a transition metal hydrogenation catalyst.

  4. PREPARATION OF NEPTUNIUM HEXAFLUORIDE

    DOE Patents [OSTI]

    Seaborg, G.T.; Brown, H.S.

    1961-05-01

    A method is described for preparing neptunium hexafluoride by treating the lower fluorides of neptunium, such as neptunium tetrafluoride and trifluoride, with fluorine at elevated temperatures.

  5. Geoscience Laboratory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    preparation and other relatively straight-forward laboratory manipulations. These include buffer preparations, solid sample grinding, solution concentration, filtration, and...

  6. Metallographic analysis of irradiated RERTR-3 fuel test specimens.

    SciTech Connect (OSTI)

    Meyer, M. K.; Hofman, G. L.; Strain, R. V.; Clark, C. R.; Stuart, J. R.

    2000-11-08

    The RERTR-3 irradiation test was designed to investigate the irradiation behavior of aluminum matrix U-MO alloy dispersion fuels under high-temperature, high-fission-rate conditions. Initial postirradiation examination of RERTR-3 fuel specimens has concentrated on binary U-MO atomized fuels. The rate of matrix aluminum depletion was found to be higher than predictions based on low temperature irradiation data. Wavelength Dispersive X-ray Spectroscopy (WDS) indicates that aluminum is present in the interior of the fuel particles. WDS data is supported by a mass and volume balance calculation performed on the basis of image analysis results. The depletion of matrix aluminum seems to have no detrimental effects on fuel performance under the conditions tested to date.

  7. PROPOSAL PREPARATION INSTRUCTIONS

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Contract No. DE-AC27-08RV14800 Modification No. A015 PROPOSAL PREPARATION INSTRUCTIONS 1. ... in response to the modification of the contract which defines work that will be funded ...

  8. PROPOSAL PREPARATION INSTRUCTIONS

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Contract No. DE-AC27-08RV14800 Modification No. A015 PROPOSAL PREPARATION INSTRUCTIONS 1. INTRODUCTION This document contains instructions to the contractor for the preparation of a proposal in response to the modification of the contract which defines work that will be funded by and performed under the provisions of the American Recovery and Reinvestment Act (Recovery Act). The contractor shall provide a written proposal consisting of a Technical Proposal and a Cost and Fee Proposal. The

  9. Preparation of hydrophobic coatings

    DOE Patents [OSTI]

    Branson, Eric D.; Shah, Pratik B.; Singh, Seema; Brinker, C. Jeffrey

    2009-02-03

    A method for preparing a hydrophobic coating by preparing a precursor sol comprising a metal alkoxide, a solvent, a basic catalyst, a fluoroalkyl compound and water, depositing the precursor sol as a film onto a surface, such as a substrate or a pipe, heating, the film and exposing the film to a hydrophobic silane compound to form a hydrophobic coating with a contact angle greater than approximately 150.degree.. The contact angle of the film can be controlled by exposure to ultraviolet radiation to reduce the contact angle and subsequent exposure to a hydrophobic silane compound to increase the contact angle.

  10. Preparation of ethylenediamine dinitrate

    DOE Patents [OSTI]

    Lee, K.

    1984-05-17

    Method for the preparation of ethylenediamine dinitrate. Ethylenediamine dinitrate, a useful explosive, may readily be prepared by solvent extraction of nitrate ion from an acidic aqueous solution thereof using a high-molecular-weight, water-insoluble amine dissolved in an organic solvent, and reacting the resulting oraganic solution with ethylenediamine. The process of the instant invention avoids the use of concentrated nitric acid, as is currently practiced, resulting in a synthesis which is far less hazardous, especially for large quantities of the explosive, and more efficient.

  11. Preparation of Draft RODs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Preparation for Warmer Temperatures Preparation for Warmer Temperatures April 2, 2014 - 11:05am Addthis Ceiling fans are a great way to efficiently cool your house in the summer. | Photo courtesy of ©iStockphoto.com/Solidago Ceiling fans are a great way to efficiently cool your house in the summer. | Photo courtesy of ©iStockphoto.com/Solidago Erik Hyrkas Erik Hyrkas Media Relations Specialist, Office of Energy Efficiency & Renewable Energy How can I participate? Find out more ways to

  12. Preparation of ethylenediamine dinitrate

    DOE Patents [OSTI]

    Lee, Kien-yin (Los Alamos, NM)

    1985-01-01

    Method for the preparation of ethylenediamine dinitrate. Ethylenediamine dinitrate, a useful explosive, may readily be prepared by solvent extraction of nitrate ion from an acidic aqueous solution thereof using a high-molecular-weight, water-insoluble amine dissolved in an organic solvent, and reacting the resulting organic solution with ethylenediamine. The process of the instant invention avoids the use of concentrated nitric acid, as is currently practiced, resulting in a synthesis which is far less hazardous especially for large quantities of the explosive, and more efficient.

  13. Cori Phase II Preparations

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Announcements » Cori Phase II Preparations Cori Phase II Preparations May 9, 2016 by Rebecca Hartman-Baker We expect the first cabinets of Cori Phase II to arrive in CRT/Wang Hall on the LBL campus in July. NERSC personnel will immediately get to work on bringing the machine into production. Before the machine can be released to the NERSC user community, a number of tasks must be completed, some of which will have a direct impact on NERSC users. We've created the Cori Phase II Schedule page to

  14. Method for preparing superconductors

    DOE Patents [OSTI]

    Dahlgren, Shelley D.

    1976-01-01

    A superconductor having an equiaxed fine grain beta-tungsten crystalline structure found to have improved high field critical current densities is prepared by sputter-depositing superconductive material onto a substrate cooled to below 200.degree. C. and heat-treating the deposited material.

  15. Process for preparing radiopharmaceuticals

    DOE Patents [OSTI]

    Barak, Morton; Winchell, Harry S.

    1977-01-04

    A process for the preparation of technetium-99m labeled pharmaceuticals is disclosed. The process comprises initially isolating technetium-99m pertechnetate by adsorption upon an adsorbent packing in a chromatographic column. The technetium-99m is then eluted from the packing with a biological compound to form a radiopharmaceutical.

  16. Preparation of graphitic articles

    DOE Patents [OSTI]

    Phillips, Jonathan; Nemer, Martin; Weigle, John C.

    2010-05-11

    Graphitic structures have been prepared by exposing templates (metal, metal-coated ceramic, graphite, for example) to a gaseous mixture that includes hydrocarbons and oxygen. When the template is metal, subsequent acid treatment removes the metal to yield monoliths, hollow graphitic structures, and other products. The shapes of the coated and hollow graphitic structures mimic the shapes of the templates.

  17. Preparation of vinyl acetate

    DOE Patents [OSTI]

    Tustin, G.C.; Zoeller, J.R.; Depew, L.S.

    1998-03-24

    This invention pertains to the preparation of vinyl acetate by contacting a mixture of hydrogen and ketene with a heterogeneous catalyst containing a transition metal to produce acetaldehyde, which is then reacted with ketene in the presence of an acid catalyst to produce vinyl acetate.

  18. Preparation of uranium nitride

    DOE Patents [OSTI]

    Potter, Ralph A.; Tennery, Victor J.

    1976-01-01

    A process for preparing actinide-nitrides from massive actinide metal which is suitable for sintering into low density fuel shapes by partially hydriding the massive metal and simultaneously dehydriding and nitriding the dehydrided portion. The process is repeated until all of the massive metal is converted to a nitride.

  19. Porous electrode preparation method

    DOE Patents [OSTI]

    Arons, R.M.; Dusek, J.T.

    1983-10-18

    A porous sintered plaque is provided with a bimodal porosity that is especially well suited for use as an electrode within a molten carbonate fuel cell. The coarse porosity is sufficient for admitting gases into contact with the reaction surfaces while the fine porosity is wetted with and retains molten electrolyte on the reaction sites. The electrode structure is prepared by providing a very fine powder of such as nickel oxide and blending the powder with a suitable decomposable binder to form a solid mass. The mass is comminuted into agglomerate size particles substantially larger than the fine oxide particles and formed into a cohesive compact for subsequent sintering. Sintering is carried out at sufficient conditions to bind the agglomerates together into a porous structure having both coarse and fine porosity. Where lithiated nickel oxide cathodes are prepared, the sintering conditions can be moderate enough to retain substantial quantities of lithium within the electrode for adequate conductivity. 2 figs.

  20. Porous electrode preparation method

    DOE Patents [OSTI]

    Arons, Richard M.; Dusek, Joseph T.

    1983-01-01

    A porous sintered plaque is provided with a bimodal porosity that is especially well suited for use as an electrode within a molten carbonate fuel cell. The coarse porosity is sufficient for admitting gases into contact with the reaction surfaces while the fine porosity is wetted with and retains molten electrolyte on the reaction sites. The electrode structure is prepared by providing a very fine powder of such as nickel oxide and blending the powder with a suitable decomposable binder to form a solid mass. The mass is comminuted into agglomerate size particles substantially larger than the fine oxide particles and formed into a cohesive compact for subsequent sintering. Sintering is carried out at sufficient conditions to bind the agglomerates together into a porous structure having both coarse and fine porosity. Where lithiated nickel oxide cathodes are prepared, the sintering conditions can be moderate enough to retain substantial quantities of lithium within the electrode for adequate conductivity.

  1. PREPARATION OF URANIUM HEXAFLUORIDE

    DOE Patents [OSTI]

    Lawroski, S.; Jonke, A.A.; Steunenberg, R.K.

    1959-10-01

    A process is described for preparing uranium hexafluoride from carbonate- leach uranium ore concentrate. The briquetted, crushed, and screened concentrate is reacted with hydrogen fluoride in a fluidized bed, and the uranium tetrafluoride formed is mixed with a solid diluent, such as calcium fluoride. This mixture is fluorinated with fluorine and an inert diluent gas, also in a fluidized bed, and the uranium hexafluoride obtained is finally purified by fractional distillation.

  2. TORIS Data Preparation Guidelines

    SciTech Connect (OSTI)

    Guinn, H.; Remson, D.

    1999-03-11

    The objective of this manual is to present guidelines and procedures for the preparation of new data for the Tertiary Oil Recovery Information System (TORIS) data base. TORIS is an analytical system currently maintained by the Department of Energy's (DOE) Bartlesville Project Office. It uses an extensive field- and reservoir-level data base to evaluate the technical and economic recovery potential of specific crude oil reservoirs.

  3. Preparation of fibrous palladium

    SciTech Connect (OSTI)

    Silver, G.L.; Seabaugh, P.W.; Leahy, B.T.; Werkmeister, D.W.; Martin, F.S.; Friedlander, H.N.

    1988-06-15

    Acrylic fibers (pan fibers) absorb palladium from a hot solution of palladium nitrate in nitric acid. When palladium-loaded acrylic fibers are burned, fibers consisting of palladium and palladium oxide are formed. Reduction of this mixture with hydrogen produces fibers of palladium metal. The fibers may be compressed into pellets which offer less resistance to flowing hydrogen than similar pellets prepared by compressing commercial palladium powder. 9 refs., 12 figs., 5 tabs.

  4. Interim Action Determination

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Interim Action Determination Processing of Plutonium Materials from the DOE Standard 3013 Surveillance Program in H-Canyon at the Savannah River Site The Department of Energy (DOE) is preparing the Surplus Plutonium Disposition Supplemental Environmental Impact Statement (SPD SEIS, DOE/EIS-0283-S2). DOE is evaluating alternatives for disposition of non-pit plutonium that is surplus to the national security needs of the United States. Although the Deputy Secretary of Energy approved Critical

  5. Preparation of tungsten oxide

    DOE Patents [OSTI]

    Bulian, Christopher J.; Dye, Robert C.; Son, Steven F.; Jorgensen, Betty S.; Perry, W. Lee

    2009-09-22

    Tungsten trioxide hydrate (WO.sub.3.H.sub.2O) was prepared from a precursor solution of ammonium paratungstate in concentrated aqueous hydrochloric acid. The precursor solution was rapidly added to water, resulting in the crash precipitation of a yellow white powder identified as WO.sub.3.H.sub.2O nanosized platelets by x-ray diffraction and scanning electron microscopy. Annealing of the powder at 200.degree. C. provided cubic phase WO.sub.3 nanopowder, and at 400.degree. C. provided WO.sub.3 nanopowder as a mixture of monoclinic and orthorhombic phases.

  6. PREPARATION OF URANIUM TRIOXIDE

    DOE Patents [OSTI]

    Buckingham, J.S.

    1959-09-01

    The production of uranium trioxide from aqueous solutions of uranyl nitrate is discussed. The uranium trioxide is produced by adding sulfur or a sulfur-containing compound, such as thiourea, sulfamic acid, sulfuric acid, and ammonium sulfate, to the uranyl solution in an amount of about 0.5% by weight of the uranyl nitrate hexahydrate, evaporating the solution to dryness, and calcining the dry residue. The trioxide obtained by this method furnished a dioxide with a considerably higher reactivity with hydrogen fluoride than a trioxide prepared without the sulfur additive.

  7. Fusion Science to Prepare

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    DIII-D Explorations of Fusion Science to Prepare for ITER and FNSF Dr. Richard Buttery General Atomics Tuesday, Dec 10, 2013 - 11:00AM MBG AUDITORIUM Refreshments at 10:45AM The PrinceTon Plasma Physics laboraTory is a U.s. DeParTmenT of energy faciliTy Recent DIII-D research has provided significant new in- formation for the physics basis of key scientific issues for successful operation of ITER and future steady state fu- sion tokamaks, including control of edge localized modes (ELMs), plasma

  8. Method to prepare Semtex

    SciTech Connect (OSTI)

    Alcaraz, A; Dougan, A

    2006-11-26

    This procedure requires the binder and uncoated RDX be prepared in separate steps, see Figure 1: (1) The binder and dye are mixed by agitation with a water-insoluble organic solvent (e.g., toluene), I; (2) The RDX/PETN is agitated thoroughly with water, II; (3) The binder solution I is added to the RDX/water mixture at II with thorough mixing to form a slurry III; (4) In the next step the solvent is distilled off at IV leaving resulting granules; (5) The next step is followed by filtration at V, which may be done by vacuum; (6) The composition is then dried at VI to a dough-like consistency.

  9. Process for preparing liquid wastes

    DOE Patents [OSTI]

    Oden, Laurance L.; Turner, Paul C.; O'Connor, William K.; Hansen, Jeffrey S.

    1997-01-01

    A process for preparing radioactive and other hazardous liquid wastes for treatment by the method of vitrification or melting is provided for.

  10. Chemical Resources | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Chemical Resources Chemical Inventory All Sample Preparation Labs are stocked with an assortment of common solvents, acids, bases, buffers, and other reagents. See our Chemical ...

  11. Comparison of preparation techniques for nuclear materials for transmission electron microscopy (TEM)

    SciTech Connect (OSTI)

    Aitkaliyeva, Assel; Madden, James W.; Miller, Brandon D; Cole, James I; Gan, Jian

    2015-04-01

    Preparation of highly radioactive and irradiated nuclear fuels and materials for transmission electron microscopy (TEM) is conjoined with a set of unique challenges, including but not limited to personnel radiation exposure and contamination. The paper evaluates three specimen preparation techniques for preparation of irradiated materials and determines which technique yields to the most reliable characterization of radiation damage microstructure. Various specimen preparation artifacts associated with each technique are considered and ways of minimizing these artifacts are addressed.

  12. Business Owners: Prepare for Utility Disruptions | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Utility Disruptions Business Owners: Prepare for Utility Disruptions Business Owners: Prepare for Utility Disruptions Have a plan in place in case a natural disaster or other hazard knocks out your business's electricity or natural gas service. Identify energy utilities-The utilities that are absolutely necessary to running your business. How might a disaster impact the availability of those utilities? Determine backup options-Contact your utility companies to discuss potential backup options,

  13. Sample Preparation Laboratory Training - Course 204 | Sample Preparation

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Laboratories Sample Preparation Laboratory Training - Course 204 Who Should Attend This course is mandatory for: SLAC employees and non-employees who need unescorted access to SSRL or LCLS Sample Preparation Laboratories Note: This course may be taken in lieu of Course 199, Laboratory CHP training for SLAC employees. Prerequisites 115 - General Employee Radiological Training (GERT) Take Training Please see the notes section below for information on how to take this training. Course Details

  14. Method for preparation of polysilanes

    DOE Patents [OSTI]

    Zeigler, John M.

    1991-01-01

    High molecular weight polysilanes are prepared using highly non-chain-transferring solvents. Certain alloys of sodium can also be used to advantage with such solvents. The high molecular weights are achievable even in the commercially preferred "normal" addition procedure.

  15. Business Owners: Prepare for Utility Disruptions | Department...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Utility Disruptions Business Owners: Prepare for Utility Disruptions Business Owners: Prepare for Utility Disruptions Have a plan in place in case a natural disaster or other ...

  16. Prepared

    Office of Legacy Management (LM)

    ... November 1982. Oak Ridge Operations, U.S. Atomic Energy Commission, Radiation Survey and ... T.E. Myrick, et. al., Preliminary Results of the Ground-Level Gamma-Ray Scanning Survey of ...

  17. Photochemical preparation of plutonium pentafluoride

    DOE Patents [OSTI]

    Rabideau, Sherman W.; Campbell, George M.

    1987-01-01

    The novel compound plutonium pentafluoride may be prepared by the photodissociation of gaseous plutonium hexafluoride. It is a white solid of low vapor pressure, which consists predominantly of a face-centered cubic structure with a.sub.o =4.2709.+-.0.0005 .ANG..

  18. PREPARATION OF HALIDES OF PLUTONIUM

    DOE Patents [OSTI]

    Garner, C.S.; Johns, I.B.

    1958-09-01

    A dry chemical method is described for preparing plutonium halides, which consists in contacting plutonyl nitrate with dry gaseous HCl or HF at an elevated temperature. The addition to the reaction gas of a small quantity of an oxidizing gas or a reducing gas will cause formation of the tetra- or tri-halide of plutonium as desired.

  19. Preparation of gas selective membranes

    DOE Patents [OSTI]

    Kulprathipanja, S.; Kulkarni, S.S.; Funk, E.W.

    1988-06-14

    Gas separation membranes which possess improved characteristics as exemplified by selectivity and flux may be prepared by coating a porous organic polymer support with a solution or emulsion of a plasticizer and an organic polymer, said coating being effected at subatmospheric pressures in order to increase the penetration depth of the coating material.

  20. Preparation of high purity phosphorus

    DOE Patents [OSTI]

    Rupp, Arthur F.; Woo, David V.

    1981-01-01

    High purity phosphorus and phosphorus compounds are prepared by first reacting H.sub.3 PO.sub.4 with a lead compound such as PbO to form Pb.sub.3 (PO.sub.4).sub.2. The Pb.sub.3 (PO.sub.4).sub.2 is reduced with H.sub.2 at a temperature sufficient to form gaseous phosphorus which can be recovered as a high purity phosphorus product. Phosphorus compounds can be easily prepared by reacting the phosphorus product with gaseous reactants. For example, the phosphorus product is reacted with gaseous Cl.sub.2 to form PCl.sub.5. PCl.sub.5 is reduced to PCl.sub.3 by contacting it in the gaseous phase with solid elemental phosphorus. POCl.sub.3 can be prepared by contacting PCl.sub.5 in the gaseous phase with solid P.sub.2 O.sub.5. The general process is particularly suitable for the preparation of radiophosphorus compounds.

  1. 2009 coal preparation buyer's guide

    SciTech Connect (OSTI)

    2009-04-15

    The guide contains brief descriptions and contact details of 926 US companies supplying coal preparation equipment who exhibited at the 26th annual Coal Prep exhibition and conference, 28-30 April - May 2009, in Lexington, KY, USA. An index of categories of equipment available from the manufacturers is included.

  2. Method for preparing actinide nitrides

    DOE Patents [OSTI]

    Bryan, G.H.; Cleveland, J.M.; Heiple, C.R.

    1975-12-01

    Actinide nitrides, and particularly plutonium and uranium nitrides, are prepared by reacting an ammonia solution of an actinide compound with an ammonia solution of a reactant or reductant metal, to form finely divided actinide nitride precipitate which may then be appropriately separated from the solution. The actinide nitride precipitate is particularly suitable for forming nuclear fuels.

  3. Preparation of asymmetric porous materials

    DOE Patents [OSTI]

    Coker, Eric N.

    2012-08-07

    A method for preparing an asymmetric porous material by depositing a porous material film on a flexible substrate, and applying an anisotropic stress to the porous media on the flexible substrate, where the anisotropic stress results from a stress such as an applied mechanical force, a thermal gradient, and an applied voltage, to form an asymmetric porous material.

  4. PROCESS OF PREPARING URANIUM CARBIDE

    DOE Patents [OSTI]

    Miller, W.E.; Stethers, H.L.; Johnson, T.R.

    1964-03-24

    A process of preparing uranium monocarbide is de scribed. Uranium metal is dissolved in cadmium, zinc, cadmium-- zinc, or magnesium-- zinc alloy and a small quantity of alkali metal is added. Addition of stoichiometric amounts of carbon at 500 to 820 deg C then precipitates uranium monocarbide. (AEC)

  5. Preparation of RCRA contingency plans

    SciTech Connect (OSTI)

    Not Available

    1992-07-01

    The purpose of this guidance is to assist Department of Energy (DOE) field personnel in the preparation of Resource Conservation and Recovery Act (RCRA) contingency plans as set forth in 40 CFR 264/265 Subpart D and 270.42. The guidance will assist personnel in evaluating and ensuring facility compliance with the contingency plan requirements.

  6. Process for preparing fluorine-18

    DOE Patents [OSTI]

    Winchell, Harry S.; Wells, Dale K.; Lamb, James F.; Beaudry, Samuel B.

    1976-09-21

    An improved process for preparation of fluorine-18 by a neon (deuteron, alpha particle) fluorine-18 nuclear reaction in a non-reactive enclosed reaction zone wherein a ultrapure product is recovered by heating the reaction zone to a high temperature and removing the product with an inert gas.

  7. Preparation of gas selective membranes

    DOE Patents [OSTI]

    Kulprathipanja, Santi; Kulkarni, Sudhir S.; Funk, Edward W.

    1988-01-01

    Gas separation membranes which possess improved characteristics as exemplified by selectivity and flux may be prepared by coating a porous organic polymer support with a solution or emulsion of a plasticizer and an organic polymer, said coating being effected at subatmospheric pressures in order to increase the penetration depth of the coating material.

  8. Preparation of superconductor precursor powders

    DOE Patents [OSTI]

    Bhattacharya, Raghunath

    1998-01-01

    A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic and/or reduced particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of all metals in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products.

  9. Porous-electrode preparation method

    DOE Patents [OSTI]

    Arons, R.M.; Dusek, J.T.

    1981-09-17

    A porous sintered plaque is provided with a bimodal porosity that is especially well suited for use as an electrode within a molten carbonate fuel cell. The coarse porosity is sufficient for admitting gases into contact with the reaction surfaces while the fine porosity is wetted with and retains molten electrolyte on the reaction sites. The electrode structure is prepared by providing a very fine powder such as nickel oxide and blending the powder with a suitable decomposable binder to form a solid mass. The mass is comminuted into agglomerate size particles substantially larger than the fine oxide particles and formed into a cohesive compact for subsequent sintering. Sintering is carried out at sufficient conditions to bind the agglomerates together into a porous structure having both coarse and fine porosity. Where lithiated nickel oxide cathodes are prepared, the sintering conditions can be moderate enough to retain substantial quantities of lithium within the electrode for adequate conductivity.

  10. PREPARATION OF REFRACTORY OXIDE CRYSTALS

    DOE Patents [OSTI]

    Grimes, W.R.; Shaffer, J.H.; Watson, G.M.

    1962-11-13

    A method is given for preparing uranium dioxide, thorium oxide, and beryllium oxide in the form of enlarged individual crystals. The surface of a fused alkali metal halide melt containing dissolved uranium, thorium, or beryllium values is contacted with a water-vapor-bearing inert gas stream at a rate of 5 to 10 cubic centimeters per minute per square centimeter of melt surface area. Growth of individual crystals is obtained by prolonged contact. Beryllium oxide-coated uranium dioxide crystals are prepared by disposing uranium dioxide crystals 5 to 20 microns in diameter in a beryllium-containing melt and contacting the melt with a water-vapor-bearing inert gas stream in the same manner. (AEC)

  11. Method for preparing ceramic composite

    DOE Patents [OSTI]

    Alexander, Kathleen B.; Tiegs, Terry N.; Becher, Paul F.; Waters, Shirley B.

    1996-01-01

    A process for preparing ceramic composite comprising blending TiC particulates, Al.sub.2 O.sub.3 particulates and nickle aluminide and consolidating the mixture at a temperature and pressure sufficient to produce a densified ceramic composite having fracture toughness equal to or greater than 7 MPa m.sup.1/2, a hardness equal to or greater than 18 GPa.

  12. Method for preparing ceramic composite

    DOE Patents [OSTI]

    Alexander, K.B.; Tiegs, T.N.; Becher, P.F.; Waters, S.B.

    1996-01-09

    A process is disclosed for preparing ceramic composite comprising blending TiC particulates, Al{sub 2}O{sub 3} particulates and nickel aluminide and consolidating the mixture at a temperature and pressure sufficient to produce a densified ceramic composite having fracture toughness equal to or greater than 7 MPa m{sup 1/2}, a hardness equal to or greater than 18 GPa. 5 figs.

  13. Preparation Of Energy Storage Materials

    DOE Patents [OSTI]

    Li, Lin Song (Los Alamos, NM); Jia, Quanxi (Los Alamos, NM)

    2003-12-02

    A process is provided for the preparation of a metallic oxide composite including mixing an aqueous solution of a water-soluble metal compound and colloidal silica, depositing the mixture upon a substrate, heating the mixture-coated substrates at temperatures from about 150.degree. C. to about 300.degree. C. for time sufficient to form a metallic oxide film, and, removing the silica from the metallic oxide film whereby a porous metal oxide structure is formed.

  14. Preparation of energy storage materials

    DOE Patents [OSTI]

    Li, Lin Song (Los Alamos, NM); Jia, Quanxi (Los Alamos, NM)

    2003-01-01

    A process is provided for the preparation of a metallic oxide composite including mixing an aqueous solution of a water-soluble metal compound and colloidal silica, depositing the mixture upon a substrate, heating the mixture-coated substrates at temperatures from about 150.degree. C. to about 300.degree. C. for time sufficient to form a metallic oxide film, and, removing the silica from the metallic oxide film whereby a porous metal oxide structure is formed.

  15. Method of preparing metallocene compounds

    DOE Patents [OSTI]

    Rosenblum, Myron; Matchett, Stephen A.

    1992-01-01

    This invention describes a novel method of preparing metallocene compounds. The invention is based on synthesis of novel bis cyclopentadienides that, under appropriate conditions, will either encapsulate a transition metal to produce a metallocene such as ferrocene, or ferrocene derivative, or will yield a polymeric metallocene. Compounds produced by this process are useful as catalysts in propulsion systems, or as anti-knock compounds in gasolines.

  16. How to Prepare Your Abstract

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Prepare Your Abstract The abstract should provide a brief overview of your entire research. The abstract briefly states the research problem or purpose of the research (Introduction), how the problem was studied (Methods), what was discovered (Results), and how the results might be interpreted (Discussions and Conclusions). Acronyms may be used in an abstract, however they should be spelled out the first time they are used. Abstracts should be concise and descriptive. Symposium Abstract Format

  17. Method of surface preparation of niobium

    DOE Patents [OSTI]

    Srinivasan-Rao, Triveni; Schill, John F.

    2003-01-01

    The present invention is for a method of preparing a surface of niobium. The preparation method includes polishing, cleaning, baking and irradiating the niobium surface whereby the resulting niobium surface has a high quantum efficiency.

  18. Method for preparing radiopharmaceutical complexes

    DOE Patents [OSTI]

    Jones, Alun G.; Davison, Alan; Abrams, Michael J.

    1989-05-02

    A method for preparing radiopharmaceutical complexes that are substantially free of the reaction materials used to produce the radiopharmaceutical complex is disclosed. The method involves admixing in a suitable first solvent in a container a target seeking ligand or salt or metal adduct thereof, a radionuclide label, and a reducing agent for said radionuclide, thereby forming said radiopharmaceutical complex; coating the interior walls of the container with said pharmaceutical complex; discarding the solvent containing by-products and unreacted starting reaction materials; and removing the radiopharmaceutical complex from said walls by dissolving it in a second solvent, thereby obtaining said radiopharmaceutical complex substantially free of by-products and unreacted starting materials.

  19. Preparation for upgrading western subbituminous coal

    SciTech Connect (OSTI)

    Grimes, R.W.; Cha, C.Y.; Sheesley, D.C.

    1990-11-01

    The objective of this project was to establish the physical and chemical characteristics of western coal and determine the best preparation technologies for upgrading this resource. Western coal was characterized as an abundant, easily mineable, clean, low-sulfur coal with low heating value, high moisture, susceptibility to spontaneous ignition, and considerable transit distances from major markets. Project support was provided by the Morgantown Energy Technology Center (METC) of the US Department of Energy (DOE). The research was conducted by the Western Research Institute, (WRI) in Laramie, Wyoming. The project scope of work required the completion of four tasks: (1) project planning, (2) literature searches and verbal contacts with consumers and producers of western coal, (3) selection of the best technologies to upgrade western coal, and (4) identification of research needed to develop the best technologies for upgrading western coals. The results of this research suggest that thermal drying is the best technology for upgrading western coals. There is a significant need for further research in areas involving physical and chemical stabilization of the dried coal product. Excessive particle-size degradation and resulting dustiness, moisture reabsorption, and high susceptibility to spontaneous combustion are key areas requiring further research. Improved testing methods for the determination of equilibrium moisture and susceptibility to spontaneous ignition under various ambient conditions are recommended.

  20. Preparation and Issuance of Test Reports

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    3 Revision 1 Effective June 2008 Preparation and Issuance of Test Reports Prepared by Electric Transportation Applications Prepared by: _______________________________ Date:__________ Garrett Beauregard Approved by: _________________________________________________ Date: _______________ Donald B. Karner Procedure ETA-GAC003 Revision 1 2 ©2006 Electric Transportation Applications All Rights Reserved Table of Contents 1 Objective

  1. Preparation of superconductor precursor powders

    DOE Patents [OSTI]

    Bhattacharya, R.

    1998-08-04

    A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic and/or reduced particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of all metals in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products. 7 figs.

  2. Preparation of superconductor precursor powders

    DOE Patents [OSTI]

    Bhattacharya, Raghunath; Blaugher, Richard D.

    1995-01-01

    A process for the preparation of a precursor metallic powder composition for use in the subsequent formation of a superconductor. The process comprises the steps of providing an electrodeposition bath comprising an electrolyte medium and a cathode substrate electrode, and providing to the bath one or more soluble salts of one or more respective metals, such as nitrate salts of thallium, barium, calcium, and copper, which are capable of exhibiting superconductor properties upon subsequent appropriate treatment. The bath is continually energized to cause the metallic particles formed at the electrode to drop as a powder from the electrode into the bath, and this powder, which is a precursor powder for superconductor production, is recovered from the bath for subsequent treatment. The process permits direct inclusion of thallium in the preparation of the precursor powder, and yields an amorphous product mixed on an atomic scale to thereby impart inherent high reactivity. Superconductors which can be formed from the precursor powder include pellet and powder-in-tube products.

  3. Preparation of hydrophobic organic aeorgels

    DOE Patents [OSTI]

    Baumann, Theodore F.; Satcher, Jr., Joe H.; Gash, Alexander E.

    2007-11-06

    Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.

  4. Preparation of hydrophobic organic aeorgels

    DOE Patents [OSTI]

    Baumann, Theodore F.; Satcher, Jr., Joe H.; Gash, Alexander E.

    2004-10-19

    Synthetic methods for the preparation of hydrophobic organics aerogels. One method involves the sol-gel polymerization of 1,3-dimethoxybenzene or 1,3,5-trimethoxybenzene with formaldehyde in non-aqueous solvents. Using a procedure analogous to the preparation of resorcinol-formaldehyde (RF) aerogels, this approach generates wet gels that can be dried using either supercritical solvent extraction to generate the new organic aerogels or air dried to produce an xerogel. Other methods involve the sol-gel polymerization of 1,3,5 trihydroxy benzene (phloroglucinol) or 1,3 dihydroxy benzene (resorcinol) and various aldehydes in non-aqueous solvents. These methods use a procedure analogous to the one-step base and two-step base/acid catalyzed polycondensation of phloroglucinol and formaldehyde, but the base catalyst used is triethylamine. These methods can be applied to a variety of other sol-gel precursors and solvent systems. These hydrophobic organics aerogels have numerous application potentials in the field of material absorbers and water-proof insulation.

  5. Explosive double salts and preparation

    DOE Patents [OSTI]

    Cady, Howard H.; Lee, Kien-yin

    1984-01-01

    Applicants have discovered a new composition of matter which is an explosive addition compound of ammonium nitrate (AN) and diethylenetriamine trinitrate (DETN) in a 50:50 molar ratio. The compound is stable over extended periods of time only at temperatures higher than 46.degree. C., decomposing to a fine-grained eutectic mixture (which is also believed to be new) of AN and DETN at temperatures lower than 46.degree. C. The compound of the invention has an x-ray density of 1.61 g/cm.sup.3, explodes to form essentially only gaseous products, has higher detonation properties (i.e., detonation velocity and pressure) than those of any mechanical mixture having the same density and composition as the compound of the invention, is a quite insensitive explosive material, can be cast at temperatures attainable by high pressure steam, and is prepared from inexpensive ingredients. Methods of preparing the compound of the invention and the fine-grained eutectic composition of the invention are given.

  6. Safety assessment of discharge chute isolation barrier preparation and installation

    SciTech Connect (OSTI)

    Meichle, R.H.

    1994-09-29

    The safety assessment is made for the activities for the preparation and installation of the discharge chute isolation barriers. The safety assessment includes a hazard assessment and comparison of potential accidents/events to those addressed by the current safety basis documentation. No significant hazards were identified. An evaluation against the USQ evaluation questions were made and the determination made that the activities do not represent a USQ. Hazard categorization techniques were used to provide a basis for readiness review classification.

  7. PREPARATION OF REFRACTORY OXIDE MICROSPHERE

    DOE Patents [OSTI]

    Haws, C.C. Jr.

    1963-09-24

    A method is described of preparing thorium oxide in the form of fused spherical particles about 1 to 2 microns in diameter. A combustible organic solution of thorium nitrate containing additive metal values is dispersed into a reflected, oxygen-fed flame at a temperature above the melting point of the resulting oxide. The metal additive is aluminum at a proportion such as to provide 1 to 10 weight per cent aluminum oxide in the product, silicon at the same proportion, or beryllium at a proportion of 12 to 25 weight per cent beryllium oxide in the product. A minor proportion of uranium values may also be provided in the solution. The metal additive lowers the oxide melting point and allows fusion and sphere formation in conventional equipment. The product particles are suitable for use in thorium oxide slurries for nuclear reactors. (AEC)

  8. Prepares Overset Grids for Processing

    Energy Science and Technology Software Center (OSTI)

    1998-04-22

    Many large and complex computational problems require multiple, structured, generically overlapped (overset) grids to obtain numerical solutions in a timely manner. BREAKUP significantly reduces required compute times by preparing overset grids for processing on massively parallel computers. BREAKUP subdivides the original grids for use on a user-specified number of parallel processors. Grid-to-grid and intragrid communications are maintained in the parallel environment via connectivity tables generated by BREAKUP. The subgrids are formed to be statically loadmore » balanced and to incur a minimum of communication between the subgrids. When the output of BREAKUP is submitted to an appropriately modified flow solver, subgrid solutions will be updated simultaneously. This contrasts to the much less efficient solution method of updating each original grid sequentially as done in the past.« less

  9. Aerosol preparation of intact lipoproteins

    DOE Patents [OSTI]

    Benner, W. Henry; Krauss, Ronald M; Blanche, Patricia J

    2012-01-17

    A medical diagnostic method and instrumentation system for analyzing noncovalently bonded agglomerated biological particles is described. The method and system comprises: a method of preparation for the biological particles; an electrospray generator; an alpha particle radiation source; a differential mobility analyzer; a particle counter; and data acquisition and analysis means. The medical device is useful for the assessment of human diseases, such as cardiac disease risk and hyperlipidemia, by rapid quantitative analysis of lipoprotein fraction densities. Initially, purification procedures are described to reduce an initial blood sample to an analytical input to the instrument. The measured sizes from the analytical sample are correlated with densities, resulting in a spectrum of lipoprotein densities. The lipoprotein density distribution can then be used to characterize cardiac and other lipid-related health risks.

  10. PREPARATION OF DIBASIC ALUMINUM NITRATE

    DOE Patents [OSTI]

    Gresky, A.T.; Nurmi, E.O.; Foster, D.L.; Wischow, R.P.; Savolainen, J.E.

    1960-04-01

    A method is given for the preparation and recovery of basic aluminum nltrates having an OH: Al ratio of at least two, comprising two steps. First, metallic aluminum is dissolved in aqueous Al(NO/sub 3/)/sub 3/, in the presence of a small quantity of elemental or ionic mercury, to increase its Al: NO/sub 3/ ratio into the range 1 to 1.2. The resulting aqueous solution is then added to an excess of a special organic solvent, typically a mixture of five parts methanol and six parts diethyl ether, whereupon the basic aluminum nitrate, e.g. Al/sub 6/(OH)/sub 13/-(NO/sub 3/)/sub 5/, recoverably precipitates.

  11. National Coal Council Presentation/Prepared Remarks | Department...

    Broader source: Energy.gov (indexed) [DOE]

    National Coal Council PresentationPrepared Remarks More Documents & Publications MESQUITE REFF West PresentationPrepared Remarks RETECH PresentationPrepared Remarks...

  12. Executive Order 13653-Preparing the United States for the Impacts...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    53-Preparing the United States for the Impacts of Climate Change Executive Order 13653-Preparing the United States for the Impacts of Climate Change Executive Order 13653-Preparing ...

  13. PREPARING FOR A SUCCESSFUL EVMS CERTIFICATION

    SciTech Connect (OSTI)

    CROWE SL; BASCHE AD

    2011-02-09

    The client, a government agency, requires its contractor to obtain an Earned Value Management System (EVMS) certification that meets the intent of ANSI/EIA-748-B, Earned Value Management Systems. The contractor has extensive experience with certification preparation, having completed two certifications within two years. Information from a previous EVMS certification and internal system surveillances are used to prepare for client-based EVMS certifications and bi-annual surveillances. The contractor also sent members of its group to assist other companies preparing for surveillances and certifications to perform 'Black Hat Reviews.' This paper is a lessons learned on preparing a team for EVMS certification. The information is also applicable for surveillances, since the contractor prepares its team for the surveillance in the same manner as the initial certification. Some of the areas covered include required documents, tracing the data through the systems, Control Account Manager (CAM) preparation, and system verification.

  14. Process for preparing energetic materials

    DOE Patents [OSTI]

    Simpson, Randall L.; Lee, Ronald S.; Tillotson, Thomas M.; Swansiger, Rosalind W.; Fox, Glenn A.

    2011-12-13

    Sol-gel chemistry is used for the preparation of energetic materials (explosives, propellants and pyrotechnics) with improved homogeneity, and/or which can be cast to near-net shape, and/or made into precision molding powders. The sol-gel method is a synthetic chemical process where reactive monomers are mixed into a solution, polymerization occurs leading to a highly cross-linked three dimensional solid network resulting in a gel. The energetic materials can be incorporated during the formation of the solution or during the gel stage of the process. The composition, pore, and primary particle sizes, gel time, surface areas, and density may be tailored and controlled by the solution chemistry. The gel is then dried using supercritical extraction to produce a highly porous low density aerogel or by controlled slow evaporation to produce a xerogel. Applying stress during the extraction phase can result in high density materials. Thus, the sol-gel method can be used for precision detonator explosive manufacturing as well as producing precision explosives, propellants, and pyrotechnics, along with high power composite energetic materials.

  15. Methods for preparation of cyclopentadienyliron (II) arenes

    DOE Patents [OSTI]

    Keipert, S.J.

    1991-10-22

    Two improved methods for preparation of compounds with the structure shown in the equation, [(Cp)--Fe--(Ar)][sup +][sub b]X[sup b[minus

  16. Novel Materials Preparation & Processing Methodologies | The...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    reactive or toxic components such as the rare earth metals, Mg-based and RE containing ... in the preparation, purification, and fabrication of metallic elements and alloys. ...

  17. Preparation Of Nonreactor Nuclear Facility Documented Safety...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    9-2014, Preparation Of Nonreactor Nuclear Facility Documented Safety Analysis by Website Administrator This Department of Energy (DOE) Standard (STD), DOE-STD-3009-2014, describes...

  18. Preparing Guyana's REDD+ Participation: Developing Capacities...

    Open Energy Info (EERE)

    Workshop, Guidemanual Website http:unfccc.intfilesmethod Country Guyana UN Region Latin America and the Caribbean References Preparing Guyana's REDD+ Participation1...

  19. State Awards for Energy Emergency Preparation

    Broader source: Energy.gov [DOE]

    List of States receiving awards from the Energy Emergency Preparation project under the American Recovery and Reinvestment Act alphabetically by State including the amount of Recovery Act funding.

  20. ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION...

    Office of Environmental Management (EM)

    ADMINISTRATIVE RECORDS SCHEDULE 5: BUDGET PREPARATION, PRESENTATION, AND APPORTIONMENT RECORDS Budget and apportionment records include the various files accumulated in the course ...

  1. Recommendations for the Preparation of Environmental Assessments...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Recommendations for the Preparation of Environmental Assessments and Environmental Impact Statements Second Edition This second edition of the "Green Book" was issued by DOE to ...

  2. Preparing for Project Implementation Assigning Accountability...

    Broader source: Energy.gov (indexed) [DOE]

    Assigning Accountability for Each Project (April 14, 2010) (598.01 KB) More Documents & Publications Preparing for Project Implementation after an Energy Assessment

  3. Preparing for Project Implementation Announcing "the PRIZE",...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    July 14, 2010 8 - Preparing for Project Implementation Announcing "the PRIZE" Save Energy Now LEADER Web Conference Project Implementation Seminar Series Save Energy Now LEADER Web ...

  4. Preparations Underway for the 2015 National Environmental Justice...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Preparations Underway for the 2015 National Environmental Justice Conference & Training Program Preparations Underway for the 2015 National Environmental Justice Conference & ...

  5. PREPARATIONS UNDERWAY FOR THE 2014 NATIONAL ENVIRONMENTAL JUSTICE...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    PREPARATIONS UNDERWAY FOR THE 2014 NATIONAL ENVIRONMENTAL JUSTICE CONFERENCE & TRAINING PROGRAM PREPARATIONS UNDERWAY FOR THE 2014 NATIONAL ENVIRONMENTAL JUSTICE CONFERENCE & ...

  6. Modular microfluidic system for biological sample preparation

    DOE Patents [OSTI]

    Rose, Klint A.; Mariella, Jr., Raymond P.; Bailey, Christopher G.; Ness, Kevin Dean

    2015-09-29

    A reconfigurable modular microfluidic system for preparation of a biological sample including a series of reconfigurable modules for automated sample preparation adapted to selectively include a) a microfluidic acoustic focusing filter module, b) a dielectrophoresis bacteria filter module, c) a dielectrophoresis virus filter module, d) an isotachophoresis nucleic acid filter module, e) a lyses module, and f) an isotachophoresis-based nucleic acid filter.

  7. Tritioacetylating reagents and processes for preparation thereof

    DOE Patents [OSTI]

    Saljoughian, Manoucher; Morimoto, Hiromi; Williams, Philip G.; Than, Chit

    2000-01-01

    Novel acetylating and tritioacetylating reagents suitable for preparation of nonlabelled and radiolabelled organic compounds. N-acetoxynaphthalimide, N-tritioacetoxyphthalimide, N-tritioacetoxysuccinimide, N-tritioacetoxynaphthalimide and processes of their preparation. The invention also concerns synthesis of nonlabelled acetylated and tritioacetylated organic compounds from precursors containing a free --NH.sub.2, --SH or --OH group.

  8. EIS-0472: Notice of Intent to Prepare a Programmatic Environmental Impact

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Statement | Department of Energy Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0472: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Uranium Leasing Program Programmatic Environmental Impact Statement The underlying purpose and need for agency action is that, in support of the Energy Policy Act of 2005 (Public Law 109-58), which emphasized the reestablishment of nuclear power (Sections 601 through 657), DOE needs to determine the

  9. Fundamentals of preparative and nonlinear chromatography

    SciTech Connect (OSTI)

    Guiochon, Georges A; Felinger, Attila; Katti, Anita; Shirazi, Dean G

    2006-02-01

    The second edition of Fundamentals of Preparative and Nonlinear Chromatography is devoted to the fundamentals of a new process of purification or extraction of chemicals or proteins widely used in the pharmaceutical industry and in preparative chromatography. This process permits the preparation of extremely pure compounds satisfying the requests of the US Food and Drug Administration. The book describes the fundamentals of thermodynamics, mass transfer kinetics, and flow through porous media that are relevant to chromatography. It presents the models used in chromatography and their solutions, discusses the applications made, describes the different processes used, their numerous applications, and the methods of optimization of the experimental conditions of this process.

  10. Alkylidenediquinocyclopropanes and Diarylcyclopropenes and method for preparation

    DOE Patents [OSTI]

    West, Robert C.; Beyer, Douglas E.; Komatsu, Koichi

    1979-01-01

    Alkylidenediquinocyclopropanes and diarylcyclopropenes and the preparation of the former by oxidation of the latter and which are characterized by low energy electronic absorption, pronounced dichroism and characteristic specular reflectance.

  11. Preparation and Electrochemical Properties of Nanoporous Transparent...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    properties have been prepared using an interpenetrating inorganic-organic hybrid sol-gel approach. UV-Vis and X-ray photoelectron spectroscopic studies were carried out on...

  12. METHOD OF PREPARING UF$sub 6$

    DOE Patents [OSTI]

    Davidson, R.; Fried, S.

    1959-10-27

    A method is described of preparing uraniurn hexafluoride without the use of fluorine gas by reacting uraniurn tetrafluoride with oxygen gas under rigorously anhydrous conditions at 600 to 1300 deg K within a pre-fluorinated nickel vessel.

  13. Is Your Plant Prepared for a Hurricane?

    SciTech Connect (OSTI)

    2006-07-01

    This DOE Industrial Technologies Program BestPractices fact sheet lists resources for manufacturers and steps they can take to prepare for the devastating winds and floods caused by hurricanes.

  14. Preparing for Hurricane Irene: Follow Local Direction

    Broader source: Energy.gov [DOE]

    Hurricane Irene is heading towards the East Coast, and while the extent of its impact is not yet known, those who may be effected (even inland areas), should get prepared and follow the direction...

  15. Process for the preparation of organoclays

    DOE Patents [OSTI]

    Chaiko, David J.

    2004-11-23

    A method for preparing organoclays for use as rheological control agents and in the preparation of nanocomposites. Typically, the clay is dispersed in water, and a specific amount of polymeric hydrotrope, ranging from 0.1 to 15 weight percent relative to the weight of the clay, is adsorbed onto the clay surface. Quaternary amine exchange is also performed on the clay to modify the surface hydrophilic/lipophilic balance (HLB) of the clay.

  16. Process for the preparation of organoclays

    DOE Patents [OSTI]

    Chaiko, David J.

    2003-01-01

    A method for preparing organoclays from smectites for use as rheological control agents and in the preparation of nanocomposites. Typically, the clay is dispersed in water, and a substantially monomolecular layer of a water soluble polymer is applied to the surfaces of the clay. A surfactant is also applied to the clay to modify the surface hydrophilic/hydrophobic balance of the clay, and the organoclay is separated out for subsequent use.

  17. Return on investment (ROI) proposal preparation guide

    SciTech Connect (OSTI)

    VALERO, O.J.

    1998-10-09

    The ROI Proposal Preparation Guide is a tool to assist Hanford waste generators in preparing ROI proposal forms for submittal to Department of Energy, Richland Operations Office (DOE/RL) for funding. The guide describes the requirements for submitting an ROI proposal and provides examples of completed ROI forms. The intent is to assist waste generators in identifying projects that meet the criteria, provide information necessary to complete the ROI forms, and submit a proposal that is eligible to receive funding.

  18. Preparing for Hurricane Season | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Preparing for Hurricane Season Preparing for Hurricane Season June 1, 2015 - 9:49am Addthis Patricia A. Hoffman Patricia A. Hoffman Assistant Secretary, Office of Electricity Delivery & Energy Reliability Hurricane season in the Atlantic begins today and will last through November 30. As the lead Federal agency responsible for coordinating the response to major energy disruptions, the Department of Energy works closely with other Federal agencies, State, local and tribal governments, and our

  19. REFF West Presentation/Prepared Remarks | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    REFF West Presentation/Prepared Remarks REFF West Presentation/Prepared Remarks REFF West Presentation/Prepared Remarks (798.43 KB) More Documents & Publications RETECH Presentation/Prepared Remarks Presentation: DOE Loan Programs REFF West Presentation/Prepared Remarks Powering New Markets: Utility-scale Photovoltaic Solar

  20. Are You Prepared for a Blackout? | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Prepared for a Blackout? Are You Prepared for a Blackout? August 24, 2012 - 2:23pm Addthis Earlier this week, Lynn talked about how you could prepare for a blackout. It's always...

  1. Preparation and screening of crystalline inorganic materials

    DOE Patents [OSTI]

    Schultz, Peter G.; Xiang, Xiaodong; Goldwasser, Isy; Brice{hacek over }o, Gabriel; Sun, Xiao-Dong; Wang, Kai-An

    2008-10-28

    Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc. Once prepared, these materials can be screened for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical, or other properties. Thus, the present invention provides methods for the parallel synthesis and analysis of novel materials having useful properties.

  2. Method for Preparing Nanoporous Cell-Scaled Reaction Vessels...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Return to Search Method for Preparing Nanoporous Cell-Scaled Reaction Vessels Oak Ridge ... reactions at the microscale level. *Cell-mimicking structures can be prepared as ...

  3. EIS-0485: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare an Environmental Impact Statement EIS-0485: Notice of Intent to Prepare an Environmental Impact Statement Interconnection of the Grande Prairie Wind ...

  4. Preparation and purification of ionic liquids and precursors

    DOE Patents [OSTI]

    Burrell, Anthony K.; Warner, Benjamin P.; McCleskey, T. Mark; Agrawal, Anoop

    2010-07-27

    Substantially pure ionic liquids and ionic liquid precursors were prepared. The substantially pure ionic liquid precursors were used to prepare substantially pure ionic liquids.

  5. Secretary Steven Chu's Remarks as Prepared for Delivery to the...

    Office of Environmental Management (EM)

    Secretary Steven Chu's Remarks as Prepared for Delivery to the DOE Tribal Summit Secretary Steven Chu's Remarks as Prepared for Delivery to the DOE Tribal Summit Secretary Steven...

  6. Memorandum Guidance for the Preparation of Department of Energy...

    Energy Savers [EERE]

    Guidance for the Preparation of Department of Energy (DOE) Annual Site Environmental reports (ASERs) for Calendar Year 2014 Memorandum Guidance for the Preparation of Department of ...

  7. Guidance for Preparation of the 2014 Department of Energy Annual...

    Office of Environmental Management (EM)

    Guidance for Preparation of the 2014 Department of Energy Annual Site Environmental Reports Guidance for Preparation of the 2014 Department of Energy Annual Site Environmental ...

  8. Diesel HCCI with External Mixture Preparation | Department of...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    with External Mixture Preparation Diesel HCCI with External Mixture Preparation 2004 Diesel Engine Emissions Reduction (DEER) Conference Presentation: The Ohio State University PDF ...

  9. NREL: Climate Neutral Research Campuses - Preparing a Plan and...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Preparing a Plan and Setting Priorities At this stage of formulating a climate action ... The resulting plan can be goal driven or finance driven. In preparing climate action ...

  10. EIS-0464: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare an Environmental Impact Statement Lake Charles Carbon Capture and Sequestration Project, Lake Charles, LA Notice of Intent To Prepare an...

  11. Preparation of lithium-ion battery anodes using lignin (Journal...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Preparation of lithium-ion battery anodes using lignin Citation Details In-Document Search Title: Preparation of lithium-ion battery anodes using lignin Authors:...

  12. EIS-0396: Notice of Intent to Prepare a Programmatic Environmental...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare a Programmatic Environmental Impact Statement EIS-0396: Notice of Intent to Prepare a Programmatic Environmental Impact Statement Global Nuclear Energy ...

  13. Hydrogen Transport Properties of Palladium Film Prepared by Colloidal...

    Office of Scientific and Technical Information (OSTI)

    Transport Properties of Palladium Film Prepared by Colloidal Spray Deposition Citation Details In-Document Search Title: Hydrogen Transport Properties of Palladium Film Prepared by ...

  14. EIS-0388: Notice of Intent to Prepare an Environmental Impact...

    Broader source: Energy.gov (indexed) [DOE]

    Notice of Intent to Prepare a Supplemental Environmental Impact Statement EIS-0238-S1: Notice of Intent to Prepare a Supplemental Environmental Impact Statement to the Final...

  15. EIS-0396: Advance Notice of Intent o Prepare an Environmental...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Prepare an Environmental Impact Statement EIS-0396: Advance Notice of Intent o Prepare an Environmental Impact Statement Global Nuclear Energy Partnership Technology Demonstration...

  16. Savannah River Site: Plutonium Preparation Project (PuPP) at...

    Energy Savers [EERE]

    Site: Plutonium Preparation Project (PuPP) at Savannah River Site Savannah River Site: Plutonium Preparation Project (PuPP) at Savannah River Site Full Document and Summary ...

  17. EIS-0399: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare an Environmental Impact Statement EIS-0399: Notice of Intent to Prepare an Environmental Impact Statement Presidential Permit Application for Montana ...

  18. A Versatile Synthetic Route for the Preparation of Titanium Metal...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    A Versatile Synthetic Route for the Preparation of Titanium Metal-Organic Frameworks ... A Versatile Synthetic Route for the Preparation of Titanium Metal-Organic Frameworks. ...

  19. EIS-0288: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare an Environmental Impact Statement EIS-0288: Notice of Intent ... prepare an Environmental Impact Statement (EIS) for the production of tritium using one or ...

  20. EIS-0444: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Statement EIS-0444: Notice of Intent to Prepare an Environmental Impact Statement Texas Clean Energy Project, Ector County, Texas Notice of Intent to Prepare an Environmental...

  1. ETA-HAC003 - Preparation and Issuance of Test Reports

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Effective November 1, 2004 "Preparation and Issuance of Test Reports" Prepared by Electric ... Review and approval of test documentation shall be in accordance with ETA- HAC04, "Review ...

  2. ETA-NAC003 - Preparation and Issuance of Test Reports

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Preparation and Issuance of Test Reports Prepared by Electric Transportation Applications ... Review and approval of test documentation shall be in accordance with ETA- NAC004, "Review ...

  3. ETA-HIAC03 - Preparation and Issuance of Test Reports

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Preparation and Issuance of Test Reports Prepared by Electric Transportation Applications ... Review and approval of test documentation shall be in accordance with ETA- HIAC04, "Review ...

  4. EIS-0402: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare an Environmental Impact Statement Energy Technology Engineering Center (ETEC) Cleanup By the Numbers EIS-0402: Advance Notice of Intent to Prepare an

  5. Argentina-Support for the Preparation of National Climate Change...

    Open Energy Info (EERE)

    Argentina-Support for the Preparation of National Climate Change Strategy Jump to: navigation, search Name UNDP-Argentina Regional Programme for LAC - Support for the preparation...

  6. Dominican Republic-Support for the Preparation of National Climate...

    Open Energy Info (EERE)

    Support for the Preparation of National Climate Change Strategy Jump to: navigation, search Name Dominican Republic-Argentina-Support for the Preparation of National Climate Change...

  7. Secretary Steven Chu's Remarks as Prepared for Delivery at the...

    Energy Savers [EERE]

    Pomona College Commencement Secretary Steven Chu's Remarks as Prepared for Delivery at the Pomona College Commencement May 15, 2011 - 1:04pm Addthis Remarks as Prepared for ...

  8. DOE Efforts in Preparing and Improving First Response Capabilities...

    Office of Environmental Management (EM)

    Efforts in Preparing and Improving First Response Capabilities and Performance through Drills and Exercises DOE Efforts in Preparing and Improving First Response Capabilities and...

  9. EERE Success Story-New Training Resource Prepares Rescuers for...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Training Resource Prepares Rescuers for Hydrogen and Fuel Cell Emergencies EERE Success Story-New Training Resource Prepares Rescuers for Hydrogen and Fuel Cell Emergencies April ...

  10. EIS-0390: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Intent to Prepare an Environmental Impact Statement; Floodplain and Wetlands Involvement; and Public Scoping Meetings EIS-0390: Notice of Intent to Prepare an Environmental Impact...

  11. EIS-0409: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    to Prepare an Environmental Impact Statement and Notice of Proposed Floodplain and Wetlands Involvement EIS-0409: Notice of Intent to Prepare an Environmental Impact Statement...

  12. EIS-0496: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare an Environmental Impact Statement EIS-0496: Notice of Intent to Prepare an Environmental Impact Statement DOE's Western Area Power Administration ...

  13. EIS-0503: Notice of Intent to Prepare Environmental Impact Statement...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare Environmental Impact Statement EIS-0503: Notice of Intent to Prepare Environmental Impact Statement New England Clean Power Link, Vermont DOE announces ...

  14. EIS-0513: FERC Supplemental Notice of Intent to Prepare Environmental...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Supplemental Notice of Intent to Prepare Environmental Impact Statement EIS-0513: FERC Supplemental Notice of Intent to Prepare Environmental Impact Statement Jacksonville Project, ...

  15. EIS-0407: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    : Notice of Intent to Prepare an Environmental Impact Statement EIS-0407: Notice of Intent to Prepare an Environmental Impact Statement Abengoa Biorefinery Project Near Hugoton, ...

  16. EIS-0447: Notice of Intent to Prepare an Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare an Environmental Impact Statement and Conduct Public Scoping Meetings EIS-0447: Notice of Intent to Prepare an Environmental Impact Statement and ...

  17. EIS-0513: FERC Notice of Intent to Prepare Environmental Impact...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Notice of Intent to Prepare Environmental Impact Statement EIS-0513: FERC Notice of Intent to Prepare Environmental Impact Statement Jacksonville Project, Jacksonville, Florida The ...

  18. EIS-0502: Notice of Intent to Prepare Environmental Impact Statement...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    2: Notice of Intent to Prepare Environmental Impact Statement EIS-0502: Notice of Intent to Prepare Environmental Impact Statement Hot Springs to Anaconda Transmission Line Rebuild ...

  19. Preparing the Lab for workforce needs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Preparing for a Power Outage Preparing for a Power Outage September 25, 2015 - 10:39am Addthis What is your plan for when the power goes out? We've got some preparedness tips. | Energy Department Photo. What is your plan for when the power goes out? We've got some preparedness tips. | Energy Department Photo. Allison Lantero Allison Lantero Digital Content Specialist, Office of Public Affairs September is National Preparedness month. Each week of September, FEMA's website Ready.gov will focus on

  20. Process for preparing active oxide powders

    DOE Patents [OSTI]

    Berard, Michael F.; Hunter, Jr., Orville; Shiers, Loren E.; Dole, Stephen L.; Scheidecker, Ralph W.

    1979-02-20

    An improved process for preparing active oxide powders in which cation hydroxide gels, prepared in the conventional manner are chemically dried by alternately washing the gels with a liquid organic compound having polar characteristics and a liquid organic compound having nonpolar characteristics until the mechanical water is removed from the gel. The water-free cation hydroxide is then contacted with a final liquid organic wash to remove the previous organic wash and speed drying. The dried hydroxide treated in the conventional manner will form a highly sinterable active oxide powder.

  1. Surface preparation of adhesively bonded joints

    SciTech Connect (OSTI)

    Hogg, I.C.; Janardhana, M.N.

    1993-12-31

    For the bonding of structures, it is essential that correct surface preparation is completed to ensure both a reliable and a durable bond. In a controlled environment this can be achieved easily, but difficulties can occur in the field. This paper is a compilation of research completed in the area of surface preparation for the bonding of aluminum and graphite epoxy composites. Finite element analysis software MSC/NASTRAN has been used to investigate the effect of adhesion on the strength and failure characteristics of a single lap joint.

  2. Method of preparing meso-haloalkylporphyrins

    DOE Patents [OSTI]

    Wijesekera, Tilak; Lyons, James E.; Ellis, Jr., Paul E.; Bhinde, Manoj V.

    1998-01-01

    Transition metal complexes of meso-haloalkylporphyrins, wherein the haloalkyl groups contain 2 to 8 carbon atoms have been found to be highly effective catalysts for oxidation of alkanes and for the decomposition of hydroperoxides. Also disclosed is a process for the preparation of meso-halocarbyl-porphyrins which comprises contacting a halocarbyl dipyrromethane with a halocarbyl-substituted aldehyde in the presence of an acid granular solid catalyst. Also disclosed is a process for the preparation of meso-halocarbyl-porphyrins which comprises contacting a halocarbyl dipyrromethane with a halocarbyl-substituted aldehyde in the presence of an acid granular solic catalyst.

  3. Interim Action Determination

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Processing of Plutonium Materials from the DOE Standard 3013 Surveillance Program in H-Canyon at the Savannah River Site The Department of Energy (DOE) is preparing the Surplus Plutonium Disposition Supplemental Environmental Impact Statement (SPD SEIS, DOE/EIS-0283-S2). DOE is evaluating alternatives for disposition of non-pit plutonium that is surplus to the national security needs of the United States. Although the Deputy Secretary of Energy approved Critical Decision 1 A, Revised Preferred

  4. Preparation of III-V semiconductor nanocrystals

    DOE Patents [OSTI]

    Alivisatos, A.P.; Olshavsky, M.A.

    1996-04-09

    Nanometer-scale crystals of III-V semiconductors are disclosed. They are prepared by reacting a group III metal source with a group V anion source in a liquid phase at elevated temperature in the presence of a crystallite growth terminator such as pyridine or quinoline. 4 figs.

  5. Preparation of III-V semiconductor nanocrystals

    DOE Patents [OSTI]

    Alivisatos, A. Paul; Olshavsky, Michael A.

    1996-01-01

    Nanometer-scale crystals of III-V semiconductors are disclosed, They are prepared by reacting a group III metal source with a group V anion source in a liquid phase at elevated temperature in the presence of a crystallite growth terminator such as pyridine or quinoline.

  6. Process of preparing tritiated porous silicon

    DOE Patents [OSTI]

    Tam, Shiu-Wing

    1997-01-01

    A process of preparing tritiated porous silicon in which porous silicon is equilibrated with a gaseous vapor containing HT/T.sub.2 gas in a diluent for a time sufficient for tritium in the gas phase to replace hydrogen present in the pore surfaces of the porous silicon.

  7. Process of preparing tritiated porous silicon

    DOE Patents [OSTI]

    Tam, S.W.

    1997-02-18

    A process of preparing tritiated porous silicon is described in which porous silicon is equilibrated with a gaseous vapor containing HT/T{sub 2} gas in a diluent for a time sufficient for tritium in the gas phase to replace hydrogen present in the pore surfaces of the porous silicon. 1 fig.

  8. Preparation and characterization of palladium particles

    SciTech Connect (OSTI)

    Silver, G.L.; Leahy, B.T.; Martin, F.S.

    1989-02-15

    Palladium particles were prepared by burning palladium loaded ion exchange resins and reducing the combustion products with hydrogen gas. The particles can be compressed into pellets. Properties of the pellets, such as resistance to the flow of hydrogen gas and rate of exchange with deuterium, have been measured. 2 refs., 16 figs., 17 tabs.

  9. Process for the preparation of vinyl acetate

    DOE Patents [OSTI]

    Tustin, G.C.; Zoeller, J.R.; Depew, L.S.

    1998-02-17

    This invention pertains to the preparation of vinyl acetate by contacting within a contact zone a mixture of ketene and acetaldehyde with an acid catalyst at about one bar pressure and between about 85 and 200 C and removing the reaction products from the contact zone.

  10. Process for the preparation of vinyl acetate

    DOE Patents [OSTI]

    Tustin, Gerald Charles; Zoeller, Joseph Robert; Depew, Leslie Sharon

    1998-01-01

    This invention pertains to the preparation of vinyl acetate by contacting within a contact zone a mixture of ketene and acetaldehyde with an acid catalyst at about one bar pressure and between about 85.degree. and 200.degree. C. and removing the reaction products from the contact zone.

  11. PREPARATION OF URANIUM-ALUMINUM ALLOYS

    DOE Patents [OSTI]

    Moore, R.H.

    1962-09-01

    A process is given for preparing uranium--aluminum alloys from a solution of uranium halide in an about equimolar molten alkali metal halide-- aluminum halide mixture and excess aluminum. The uranium halide is reduced and the uranium is alloyed with the excess aluminum. The alloy and salt are separated from each other. (AEC)

  12. Preparation of a semiconductor thin film

    DOE Patents [OSTI]

    Pehnt, Martin; Schulz, Douglas L.; Curtis, Calvin J.; Ginley, David S.

    1998-01-01

    A process for the preparation of a semiconductor film. The process comprises depositing nanoparticles of a semiconductor material onto a substrate whose surface temperature during nanoparticle deposition thereon is sufficient to cause substantially simultaneous fusion of the nanoparticles to thereby coalesce with each other and effectuate film growth.

  13. Preparation of a semiconductor thin film

    DOE Patents [OSTI]

    Pehnt, M.; Schulz, D.L.; Curtis, C.J.; Ginley, D.S.

    1998-01-27

    A process is disclosed for the preparation of a semiconductor film. The process comprises depositing nanoparticles of a semiconductor material onto a substrate whose surface temperature during nanoparticle deposition thereon is sufficient to cause substantially simultaneous fusion of the nanoparticles to thereby coalesce with each other and effectuate film growth.

  14. Photocatalytic methods for preparation of electrocatalyst materials

    DOE Patents [OSTI]

    Nwoga, Tochi Tudor; Kawahara, Kazuo; Li, Wen; Song, Yujiang; Shelnutt, John A; Miller, James E; Medforth, Craig John; Ueno, Yukiyoshi; Kawamura, Tetsuo

    2013-12-17

    The invention relates to methods of preparing metal particles on a support material, including platinum-containing nanoparticles on a carbon support. Such materials can be used as electrocatalysts, for example as improved electrocatalysts in proton exchange membrane fuel cells (PEM-FCs).

  15. Photocatalytic methods for preparation of electrocatalyst materials

    DOE Patents [OSTI]

    Li, Wen; Kawamura, Tetsuo; Nagami, Tetsuo; Takahashi, Hiroaki; Muldoon, John; Shelnutt, John A; Song, Yujiang; Miller, James E; Hickner, Michael A; Medforth, Craig

    2013-09-24

    The invention relates to methods of preparing metal particles on a support material, including platinum-containing nanoparticles on a carbon support. Such materials can be used as electrocatalysts, for example as improved electrocatalysts in polymer electrolyte membrane fuel cells (PEM-FCs).

  16. Preparing Low-emission and Climate-Resilient Development Strategies...

    Open Energy Info (EERE)

    contentundpenhomeourworkenvironmentandenergyfo Cost: Free Language: English Preparing Low-Emission and Climate-Resilient Development Strategies (LECRDS) -...

  17. Process for the preparation of an energetic nitrate ester

    DOE Patents [OSTI]

    Chavez, David E; Naud, Darren L; Hiskey, Michael A

    2013-12-17

    A process for the preparation of an energetic nitrate ester compound and related intermediates is provided.

  18. RETECH Presentation/Prepared Remarks | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    RETECH Presentation/Prepared Remarks RETECH Presentation/Prepared Remarks RETECH Presentation/Prepared Remarks (1.1 MB) More Documents & Publications REFF West Presentation/Prepared Remarks DOE-LPO_Email-Update_001_Through_11 LPO_BROCHURE_CSP

  19. Preparing for Project Implementation before an Energy Assessment

    Broader source: Energy.gov [DOE]

    This presentation covers the essential steps to help an organization prepare for an energy assessment.

  20. 2011 Tribal Summit - Secretary Chu's Prepared Remarks | Department of

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Energy - Secretary Chu's Prepared Remarks 2011 Tribal Summit - Secretary Chu's Prepared Remarks Tribal Summit - Secretary Chu's Prepared Remarks SECRETARY STEVEN CHU'S REMARKS AS PREPARED FOR DELIVERY TO THE DOE TRIBAL SUMMIT (40.12 KB) More Documents & Publications Secretary Steven Chu's Remarks as Prepared for Delivery to the DOE Tribal Summit 2011 Secretary Chu's Letter to Tribal Leaders Before the Senate Committee on Indian Affairs

  1. Preparing for the Quality Control Inspector Certification Exam | Department

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    of Energy Preparing for the Quality Control Inspector Certification Exam Preparing for the Quality Control Inspector Certification Exam This presentation, prepared by the Building Performance Center and the Washington Department of Commerce, identifies how individuals can better prepare for the Home Energy Professional Quality Control Inspector Certification Exam. preparing_for_the_qci_ exam_4_18_14.pptx (17.26 MB) More Documents & Publications QCI Exam Test-Taking Tips from Community

  2. Preparation of environmental analyses for synfuel and unconventional gas technologies

    SciTech Connect (OSTI)

    Reed, R.M.

    1982-09-01

    Government agencies that offer financial incentives to stimulate the commercialization of synfuel and unconventional gas technologies usually require an analysis of environmental impacts resulting from proposed projects. This report reviews potentially significant environmental issues associated with a selection of these technologies and presents guidance for developing information and preparing analyses to address these issues. The technologies considered are western oil shale, tar sand, coal liquefaction and gasification, peat, unconventional gas (western tight gas sands, eastern Devonian gas shales, methane from coal seams, and methane from geopressured aquifers), and fuel ethanol. Potentially significant issues are discussed under the general categories of land use, air quality, water use, water quality, biota, solid waste disposal, socioeconomics, and health and safety. The guidance provided in this report can be applied to preparation and/or review of proposals, environmental reports, environmental assessments, environmental impact statements, and other types of environmental analyses. The amount of detail required for any issue discussed must, by necessity, be determined on a case-by-case basis.

  3. Preparation and characterization of tritium targets. [Titanium tritide

    SciTech Connect (OSTI)

    Ramey, D.W.; Adair, H.L.

    1982-01-01

    The Isotope Research Materials Laboratory (IRML) of the Oak Ridge National Laboratory (ORNL) prepares tritium targets that are used to produce an intense beam of 14.5 MeV neutrons by the /sup 3/H(/sup 2/H,/sup 1/n)/sup 4/He reaction. The intense beams of 14.5 MeV neutrons are used in programs involving cancer research, materials evaluation, and materials identification. The tritium targets required by researchers have ranged in size from 1-cm diam to 50-cm diam and have contained from 3.7 x 10/sup 4/ MBq to 2.2 x 10/sup 8/ MBq of tritium. Important parameters in the performance of tritium targets, when bombarded with deuterons, include target lifetime and neutron output. These parameters are heavily dependent on the host metal layer used to form the tritide compound and the gas-to-metal loading of the host material. Fabrication procedures used in preparing titanium tritide targets with subsequent gas-to-metal determinations are described.

  4. Safety assessment of discharge chute isolation barrier preparation and installation

    SciTech Connect (OSTI)

    Meichle, R.H.

    1994-10-21

    This analysis examines activities associated with the installation of isolation barriers in the K Basins at the Hanford Reservation. This revision adds evaluation of barrier drops on stored fuel and basin floor, identifies fuel which will be moved and addresses criticality issues with sludge. The safety assessment is made for the activities for the preparation and installation of the discharge chute isolation barriers. The safety assessment includes a hazard assessment and comparisons of potential accidents/events to those addressed by the current safety basis documentation. No significant hazards were identified. An evaluation against the USQ evaluation questions was made and the determination made that the activities do not represent a USQ. Hazard categorization techniques were used to provide a basis for readiness review classifications.

  5. Novel hard compositions and methods of preparation

    DOE Patents [OSTI]

    Sheinberg, H.

    1981-02-03

    Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value.

  6. Preparation of fullerene/glass composites

    DOE Patents [OSTI]

    Mattes, B.R.; McBranch, D.W.; Robinson, J.M.; Koskelo, A.C.; Love, S.P.

    1995-05-30

    Synthesis of fullerene/glass composites is described. A direct method for preparing solid solutions of C{sub 60} in silicon dioxide (SiO{sub 2}) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these ``guests`` in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C{sub 60}. Depending upon the preparative procedure, C{sub 60} dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C{sub 60} in a solid glass matrix, is generated by the present method.

  7. Preparation of fullerene/glass composites

    DOE Patents [OSTI]

    Mattes, Benjamin R.; McBranch, Duncan W.; Robinson, Jeanne M.; Koskelo, Aaron C.; Love, Steven P.

    1995-01-01

    Synthesis of fullerene/glass composites. A direct method for preparing solid solutions of C.sub.60 in silicon dioxide (SiO.sub.2) glass matrices by means of sol-gel chemistry is described. In order to produce highly concentrated fullerene-sol-gel-composites it is necessary to increase the solubility of these "guests" in a delivery solvent which is compatible with the starter sol (receiving solvent). Sonication results in aggregate disruption by treatment with high frequency sound waves, thereby accelerating the rate of hydrolysis of the alkoxide precursor, and the solution process for the C.sub.60. Depending upon the preparative procedure, C.sub.60 dispersed within the glass matrix as microcrystalline domains, or dispersed as true molecular solutions of C.sub.60 in a solid glass matrix, is generated by the present method.

  8. Method of preparing silicon from sodium fluosilicate

    DOE Patents [OSTI]

    Schmidt, Frederick A.; Rehbein, David; Chiotti, Premo

    1984-01-01

    A process for preparing high purity silicon metal from Na.sub.2 SiF.sub.6 (sodium fluosilicate). The sodium fluosilicate is heated to decomposition temperature to form NaF, which retains most of the impurities, and gaseous SiF.sub.4. The SiF.sub.4 is then reduced by the bomb reduction method using a reductant having a low packing density.

  9. Preparation of nitrogen-doped carbon tubes

    DOE Patents [OSTI]

    Chung, Hoon Taek; Zelenay, Piotr

    2015-12-22

    A method for synthesizing nitrogen-doped carbon tubes involves preparing a solution of cyanamide and a suitable transition metal-containing salt in a solvent, evaporating the solvent to form a solid, and pyrolyzing the solid under an inert atmosphere under conditions suitable for the production of nitrogen-doped carbon tubes from the solid. Pyrolyzing for a shorter period of time followed by rapid cooling resulted in a tubes with a narrower average diameter.

  10. Preparation of nanostructured materials having improved ductility

    DOE Patents [OSTI]

    Zhao, Yonghao; Zhu, Yuntian T.

    2010-04-20

    A method for preparing a nanostructured aluminum alloy involves heating an aluminum alloy workpiece at temperature sufficient to produce a single phase coarse grained aluminum alloy, then refining the grain size of the workpiece at a temperature at or below room temperature, and then aging the workpiece to precipitate second phase particles in the nanosized grains of the workpiece that increase the ductility without decreasing the strength of the workpiece.

  11. Geoscience Equipment Inventory | Sample Preparation Laboratories

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Geoscience Equipment Inventory « Geoscience Laboratory Title Equipment Type Description Coy Anaerobic Chamber Inert Atmosphere Chamber Coy anaerobic chamber (Type C, model 7100-000) with auto airlock for wet and dry sample preparations, 5% H2/95% N2 mix atmosphere, and auto injection system. Fisher Scientific General Purpose Refrigerator Temperature Control Fisher Scientific General Purpose refrigerator. Fisher Scientific Isotemp Freezer Temperature Control Fisher Scientific Isotemp Freezer.

  12. Process for preparing a liquid fuel composition

    DOE Patents [OSTI]

    Singerman, Gary M.

    1982-03-16

    A process for preparing a liquid fuel composition which comprises liquefying coal, separating a mixture of phenols from said liquefied coal, converting said phenols to the corresponding mixture of anisoles, subjecting at least a portion of the remainder of said liquefied coal to hydrotreatment, subjecting at least a portion of said hydrotreated liquefied coal to reforming to obtain reformate and then combining at least a portion of said anisoles and at least a portion of said reformate to obtain said liquid fuel composition.

  13. Arc Casting Intermetallic Alloy (Materials Preparation Center)

    SciTech Connect (OSTI)

    2010-01-01

    Arc casting of intermetallic (La-Ni-Sn) AB5 alloy used for metal hydride hydrogen storage. Upon solidification the Sn is partially rejected and increases in concentration in the remaining liquid. Upon completing solidification there is a great deal of internal stress in the ingot. As the ingot cools further the stress is relieved. This material was cast at the Ames Laboratorys Materials Preparation Center http://www.mpc.ameslab.gov

  14. Method for preparing Pb-. beta. ''-alumina ceramic

    DOE Patents [OSTI]

    Hellstrom, E.E.

    1984-08-30

    A process is disclosed for preparing impermeable, polycrystalline samples of Pb-..beta..''-alumina ceramic from Na-..beta..''-alumina ceramic by ion exchange. The process comprises two steps. The first step is a high-temperature vapor phase exchange of Na by K, followed by substitution of Pb for K by immersing the sample in a molten Pb salt bath. The result is a polycrystalline Pb-..beta..''-alumina ceramic that is substantially crack-free.

  15. PREPARATION OF SPHERICAL URANIUM DIOXIDE PARTICLES

    DOE Patents [OSTI]

    Levey, R.P. Jr.; Smith, A.E.

    1963-04-30

    This patent relates to the preparation of high-density, spherical UO/sub 2/ particles 80 to 150 microns in diameter. Sinterable UO/sub 2/ powder is wetted with 3 to 5 weight per cent water and tumbled for at least 48 hours. The resulting spherical particles are then sintered. The sintered particles are useful in dispersion-type fuel elements for nuclear reactors. (AEC)

  16. Process for preparing improved silvered glass mirrors

    DOE Patents [OSTI]

    Buckwalter, C.Q. Jr.

    1980-01-28

    Glass mirrors having improved weathering properties are prepared by an improvement in the process for making the mirrors. The glass surface after it has been cleaned but before it is silvered, is contacted with a solution of lanthanide rare earths in addition to a sensitization solution of tin or palladium. The addition of the rare earths produces a mirror which has increased resistance to delamination of the silver from the glass surface in the presence of water.

  17. PREPARATION OF ACTINIDE-ALUMINUM ALLOYS

    DOE Patents [OSTI]

    Moore, R.H.

    1962-09-01

    BS>A process is given for preparing alloys of aluminum with plutonium, uranium, and/or thorium by chlorinating actinide oxide dissolved in molten alkali metal chloride with hydrochloric acid, chlorine, and/or phosgene, adding aluminum metal, and passing air and/or water vapor through the mass. Actinide metal is formed and alloyed with the aluminum. After cooling to solidification, the alloy is separated from the salt. (AEC)

  18. WET METHOD OF PREPARING PLUTONIUM TRIBROMIDE

    DOE Patents [OSTI]

    Davidson, N.R.; Hyde, E.K.

    1958-11-11

    S> The preparation of anhydrous plutonium tribromide from an aqueous acid solution of plutonium tetrabromide is described, consisting of adding a water-soluble volatile bromide to the tetrabromide to provide additional bromide ions sufficient to furnish an oxidation-reduction potential substantially more positive than --0.966 volt, evaporating the resultant plutonium tribromides to dryness in the presence of HBr, and dehydrating at an elevated temperature also in the presence of HBr.

  19. Method for preparing porous metal hydride compacts

    DOE Patents [OSTI]

    Ron, Moshe; Gruen, Dieter M.; Mendelsohn, Marshall H.; Sheft, Irving

    1981-01-01

    A method for preparing porous metallic-matrix hydride compacts which can be repeatedly hydrided and dehydrided without disintegration. A mixture of a finely divided metal hydride and a finely divided matrix metal is contacted with a poison which prevents the metal hydride from dehydriding at room temperature and atmospheric pressure. The mixture of matrix metal and poisoned metal hydride is then compacted under pressure at room temperature to form porous metallic-matrix hydride compacts.

  20. Process for preparing improved silvered glass mirrors

    DOE Patents [OSTI]

    Buckwalter, Jr., Charles Q. (Benton, WA)

    1981-01-01

    Glass mirrors having improved weathering properties are prepared by an improvement in the process for making the mirrors. The glass surface after it has been cleaned but before it is silvered, is contacted with a solution of lanthanide rare earths in addition to a sensitization solution of tin or palladium. The addition of the rare earths produces a mirror which has increased resistance to delamination of the silver from the glass surface in the presence of water.

  1. CX-007664: Categorical Exclusion Determination | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    64: Categorical Exclusion Determination CX-007664: Categorical Exclusion Determination Sample Analysis of Savannah River Site Tank Farm Chemical Cleaning CX(s) Applied: B3.6 Date: 11/18/2011 Location(s): South Carolina Offices(s): Savannah River Operations Office The Savannah River Site Tank Farm is preparing Waste Tanks for closure. As part of the closure process they will collect solid and liquid samples from the tanks and submit them to Savannah River National Laboratory for analysis.

  2. CX-014313: Categorical Exclusion Determination | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    13: Categorical Exclusion Determination CX-014313: Categorical Exclusion Determination Development of Dual Purpose Organic Semiconductor Thin Films for Polymer Interface and Electrostatic Applications CX(s) Applied: B3.6 Date: 08/20/2015 Location(s): South Carolina Offices(s): Savannah River Operations Office Sample preparation techniques such as surface and sample modification/deposition and self-assembled monolayer formation will be performed. Sample modification/deposition, self-assembled

  3. CX-010274: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Analytical Sample Preparation Laboratory CX(s) Applied: B3.6 Date: 05/22/2013 Location(s): Oregon Offices(s): National Energy Technology Laboratory

  4. CX-010615: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Analytical Sample Preparation Laboratory CX(s) Applied: B3.6 Date: 07/18/2013 Location(s): Oregon Offices(s): National Energy Technology Laboratory

  5. CX-012606: Categorical Exclusion Determination

    Office of Energy Efficiency and Renewable Energy (EERE)

    Preparing of Environmental Samples for Analysis CX(s) Applied: B3.6Date: 41810 Location(s): South CarolinaOffices(s): Savannah River Operations Office

  6. CX-009850: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Pittsburgh Nanomaterials Preparation Lab CX(s) Applied: B3.6 Date: 01/29/2013 Location(s): Pennsylvania Offices(s): National Energy Technology Laboratory

  7. CX-012620: Categorical Exclusion Determination

    Broader source: Energy.gov [DOE]

    Grout Preparation CX(s) Applied: B3.6Date: 41799 Location(s): South CarolinaOffices(s): Savannah River Operations Office

  8. Temperature determination using pyrometry

    DOE Patents [OSTI]

    Breiland, William G.; Gurary, Alexander I.; Boguslavskiy, Vadim

    2002-01-01

    A method for determining the temperature of a surface upon which a coating is grown using optical pyrometry by correcting Kirchhoff's law for errors in the emissivity or reflectance measurements associated with the growth of the coating and subsequent changes in the surface thermal emission and heat transfer characteristics. By a calibration process that can be carried out in situ in the chamber where the coating process occurs, an error calibration parameter can be determined that allows more precise determination of the temperature of the surface using optical pyrometry systems. The calibration process needs only to be carried out when the physical characteristics of the coating chamber change.

  9. SOLAR '97 CONFERENCE: MANUSCRIPT PREPARATION INSTRUCTIONS

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    IMPROVEMENT AND VALIDATION OF A TRANSIENT MODEL TO PREDICT PHOTOVOLTAIC MODULE TEMPERATURE ... after irradiance, in determining the performance of a typical photovoltaic (PV) system. ...

  10. NEPA Determination Complete

    Broader source: Energy.gov [DOE]

    DOE has determined that this proposed project is a major Federal action that may significantly affect the quality of the human environment. To comply with the National Environmental Policy Act ...

  11. Solids mass flow determination

    DOE Patents [OSTI]

    Macko, Joseph E.

    1981-01-01

    Method and apparatus for determining the mass flow rate of solids mixed with a transport fluid to form a flowing mixture. A temperature differential is established between the solids and fluid. The temperature of the transport fluid prior to mixing, the temperature of the solids prior to mixing, and the equilibrium temperature of the mixture are monitored and correlated in a heat balance with the heat capacities of the solids and fluid to determine the solids mass flow rate.

  12. System Software: A Necessary but Ill-prepared Hero. (Conference...

    Office of Scientific and Technical Information (OSTI)

    System Software: A Necessary but Ill-prepared Hero. Citation Details In-Document Search Title: System Software: A Necessary but Ill-prepared Hero. Abstract not provided. Authors: ...

  13. EIS-0375: Notice of Intent to Prepare an Environmental Impact...

    Energy Savers [EERE]

    75: Notice of Intent to Prepare an Environmental Impact Statement EIS-0375: Notice of Intent to Prepare an Environmental Impact Statement Disposal of Greater-than-Class C Low-Level...

  14. Preparing the Nuclear Security Science Minds of Tomorrow | National...

    National Nuclear Security Administration (NNSA)

    Preparing the Nuclear Security Science Minds of Tomorrow Tuesday, December 17, 2013 - 10:28am Preparing the Nuclear Security Science Minds of Tomorrow On a recent Saturday at the ...

  15. Executive Order -- Preparing the United States for the Impacts...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Order -- Preparing the United States for the Impacts of Climate Change Executive Order -- Preparing the United States for the Impacts of Climate Change 2013climatechange.eo.rel.p...

  16. EIS-0394: Notice of Intent to Prepare an Environmental Impact...

    Energy Savers [EERE]

    Notice of Intent to Prepare an Environmental Impact Statement EIS-0394: Notice of Intent to Prepare ... and the DOE NEPA implementing procedures (10 CFR part 1021), to assess the ...

  17. Office of River Protection Prepares for Critical Waste Treatment...

    Office of Environmental Management (EM)

    Prepares for Critical Waste Treatment Plant Testing Office of River Protection Prepares for Critical Waste Treatment Plant Testing May 16, 2016 - 12:40pm Addthis Workers remove the ...

  18. West Valley Demonstration Project Prepares to Relocate High-Level...

    Office of Environmental Management (EM)

    Prepares to Relocate High-Level Waste West Valley Demonstration Project Prepares to Relocate High-Level Waste December 24, 2013 - 12:00pm Addthis The West Valley Demonstration ...

  19. Process for preparing silicon carbide foam

    DOE Patents [OSTI]

    Whinnery, LeRoy Louis; Nichols, Monte Carl; Wheeler, David Roger; Loy, Douglas Anson

    1997-01-01

    A method of preparing near net shape, monolithic, porous SiC foams is disclosed. Organosilicon precursors are used to produce polymeric gels by thermally induced phase separation, wherein, a sufficiently concentrated solution of an organosilicon polymer is cooled below its solidification temperature to form a gel. Following solvent removal from the gel, the polymer foam is pretreated in an oxygen plasma in order to raise its glass transition temperature. The pretreated foam is then pyrolized in an inert atmosphere to form a SiC foam.

  20. Process for preparing silicon carbide foam

    DOE Patents [OSTI]

    Whinnery, L.L.; Nichols, M.C.; Wheeler, D.R.; Loy, D.A.

    1997-09-16

    A method of preparing near net shape, monolithic, porous SiC foams is disclosed. Organosilicon precursors are used to produce polymeric gels by thermally induced phase separation, wherein, a sufficiently concentrated solution of an organosilicon polymer is cooled below its solidification temperature to form a gel. Following solvent removal from the gel, the polymer foam is pretreated in an oxygen plasma in order to raise its glass transition temperature. The pretreated foam is then pyrolyzed in an inert atmosphere to form a SiC foam. 9 figs.

  1. Preparation of Clay Brick Using Coal Waste

    SciTech Connect (OSTI)

    Yoo, Jung W.; Jung, Jin H.; Kim, Jae M.; Lee, Sung M.; Kim, Hyung T.

    2004-03-31

    A great deal of coal waste produced during the development of a mine was accumulated around the mine, which caused many problems such as traffic, acid mine drainage and damage of forest and scenery. Carbon in the coal waste helps calcination of the brick even at low temperature. Considering the reuse of natural waste and energy saving, clay brick was prepared using coal waste under various conditions, including particle size, amount of coal waste mixed, calcination temperature and pressing pressure. The specimens were characterized by XRD, SEM and TG-DTA and interpreted in terms of water absorption and compressive strength.

  2. METHOD OF PREPARING A CERAMIC FUEL ELEMENT

    DOE Patents [OSTI]

    Ross, W.T.; Bloomster, C.H.; Bardsley, R.E.

    1963-09-01

    A method is described for preparing a fuel element from -325 mesh PuO/ sub 2/ and -20 mesh UO/sub 2/, and the steps of screening --325 mesh UO/sub 2/ from the -20 mesh UO/sub 2/, mixing PuO/sub 2/ with the --325 mesh UO/sub 2/, blending this mixture with sufficient --20 mesh UO/sub 2/ to obtain the desired composition, introducing the blend into a metal tube, repeating the procedure until the tube is full, and vibrating the tube to compact the powder are included. (AEC)

  3. Hydrocarbon synthesis catalyst and method of preparation

    DOE Patents [OSTI]

    Sapienza, Richard S.; Sansone, Michael J.; Slegeir, William A. R.

    1983-08-02

    A catalyst for the synthesis of hydrocarbons from carbon monoxide and hydrogen composed of palladium or platinum and cobalt supported on a solid phase is disclosed. The catalyst is prepared by heating a heterogeneous component of the palladium or platinum deposited on the solid support in a solution of cobalt carbonyl or precursors thereof. The catalyst exhibits excellent activity, stability in air, and produces highly desirable product fractions even with dilute gaseous reactants. The catalyst is preferably used in dilute slurry form, which is desirable from a heat transfer standpoint.

  4. Hydrocarbon synthesis catalyst and method of preparation

    DOE Patents [OSTI]

    Sapienza, R.S.; Sansone, M.J.; Slegeir, W.A.R.

    1983-08-02

    A catalyst for the synthesis of hydrocarbons from carbon monoxide and hydrogen composed of palladium or platinum and cobalt supported on a solid phase is disclosed. The catalyst is prepared by heating a heterogeneous component of the palladium or platinum deposited on the solid support in a solution of cobalt carbonyl or precursors thereof. The catalyst exhibits excellent activity, stability in air, and produces highly desirable product fractions even with dilute gaseous reactants. The catalyst is preferably used in dilute slurry form, which is desirable from a heat transfer standpoint. 9 figs.

  5. Preparation of reactive beta-dicalcium silicate

    DOE Patents [OSTI]

    Shen, M.S.; Chen, J.M.; Yang, R.T.

    1980-02-28

    This invention relates to the preparation of fine particles of reactive beta-dicalcium silicate by means of a solid state process which comprises firing a mixture of calcium sulfate, silica, and a reducing additive selected from the group consisting of calcium sulfide, carbon, carbon monoxide, methane, and hydrogen, at a temperature of about 850 to 1000/sup 0/C. A carrier gas such as nitrogen or carbon dioxide may also be added, if desired. A high concentration of sulfur dioxide is a by-product of this process.

  6. Conductive ceramic composition and method of preparation

    DOE Patents [OSTI]

    Smith, James L.; Kucera, Eugenia H.

    1991-01-01

    A ceramic anode composition is formed of a multivalent metal oxide or oxygenate such as an alkali metal, transition metal oxygenate. The anode is prepared as a non-stoichiometric crystalline structure by reaction and conditioning in a hydrogen gas cover containing minor proportions of carbon dioxide and water vapor. The structure exhibits a single phase and substantially enhanced electrical conductivity over that of the corresponding stoichiometric structure. Unexpectedly, such oxides and oxygenates are found to be stable in the reducing anode fuel gas of a molten carbonate fuel cell.

  7. Method for preparing high purity vanadium

    DOE Patents [OSTI]

    Schmidt, Frederick; Carlson, O. Norman

    1986-09-09

    A method for preparing high purity vanadium having a low silicon content has been developed. Vanadium pentoxide is reduced with a stoichiometric, or slightly deficient amount of aluminum to produce a vanadium-aluminum alloy containing an excess of oxygen. Silicon is removed by electron-beam melting the alloy under oxidizing conditions to promote the formation of SiO which is volatile at elevated temperatures. Excess oxygen is removed by heating the alloy in the presence of calcium metal to form calcium oxide.

  8. Method for preparing high purity vanadium

    DOE Patents [OSTI]

    Schmidt, F.; Carlson, O.N.

    1984-05-16

    A method for preparing high purity vanadium having a low silicon content has been developed. Vanadium pentoxide is reduced with a stoichiometric, or slightly deficient amount of aluminum to produce a vanadium-aluminum alloy containing an excess of oxygen. Silicon is removed by electron-beam melting the alloy under oxidizing conditions to promote the formation of SiO which is volatile at elevated temperatures. Excess oxygen is removed by heating the alloy in the presence of calcium metal to form calcium oxide.

  9. METHOD OF PREPARING COATED REFRACTORY WARE

    DOE Patents [OSTI]

    Perlman, M.L.; Lipkin, D.; Weissman, S.I.

    1959-07-21

    A method is presented for preparing a dense, refractory coating on a vessel adapted to the handling of molten metals such as uranium and plutonium. According to the invention, the inner surface of a heat stable container formed of a refractory metal of either niobium, molybdenum, tantalum, or tungsten is coated with molten thorium within 10 minutes so as to present alloying with the refractory metal and then exposed to a reactive atmosphere of nitrogen at a temperature of about 1750 deg for 30 minutes to form a refractory thorium nitride coating.

  10. METHOD OF PREPARING POLONIUM-BORON SOURCES

    DOE Patents [OSTI]

    Birden, J.H.

    1959-08-01

    An improved technique is described for preparation of a polonium-boron neutron source. A selected amount of Po-210 is vaporized into a thin walled nickel container, then the desired amcunt of boron powder is added. After sealing the container, it is heated quickly by induction heating to vaporize the Po-210 and deposit it in the still cool boron powder. The unit is then quickly cooled to prevent revaporization of the Po-210 from the boron. The build-up of neutron emission may be followed by means of a neutron counter in order to terminate the heating at the optimum level of neutron yield.

  11. LANSCE | Lujan Center | Biology Preparation Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Biology Preparation Laboratory The Lujan Center Biolab offers a variety of capabilities. 1) Biodeuteration Lab (BDL) We run a protein expression lab for perdeuteration of user proteins. We offer full perdeuteration (~99%) using our algal-based media for bacterial growth. We also have M9 minimal media made in D2O for expression of up to ~85% perdeuteration. Users can use our lab in person or mail-in a plasmid for us to express for them. We also have standard protein expression equipment:

  12. Preparation of reactive beta-dicalcium silicate

    DOE Patents [OSTI]

    Shen, Ming-Shing (Laramie, WY, NJ); Chen, James M. (Rahway, NJ); Yang, Ralph T. (Amherst, NY)

    1982-01-01

    This invention relates to the preparation of fine particles of reactive beta-dicalcium silicate by means of a solid state process which comprises firing a mixture of calcium sulfate, silica and a reducing additive selected from the group consisting of calcium sulfide, carbon, carbon monoxide, methane and hydrogen, at a temperature of about 850.degree.-1000.degree. C. A carrier gas such as nitrogen or carbon dioxide may also be added, if desired. A high concentration of sulfur dioxide is a by-product of this process.

  13. Method for preparing a thick film conductor

    DOE Patents [OSTI]

    Nagesh, Voddarahalli K.; Fulrath, deceased, Richard M.

    1978-01-01

    A method for preparing a thick film conductor which comprises providing surface active glass particles, mixing the surface active glass particles with a thermally decomposable organometallic compound, for example, a silver resinate, and then decomposing the organometallic compound by heating, thereby chemically depositing metal on the glass particles. The glass particle mixture is applied to a suitable substrate either before or after the organometallic compound is thermally decomposed. The resulting system is then fired in an oxidizing atmosphere, providing a microstructure of glass particles substantially uniformly coated with metal.

  14. Resin catalysts and method of preparation

    DOE Patents [OSTI]

    Smith, Jr., Lawrence A.

    1986-01-01

    Heat stabilized catalyst compositions are prepared from nuclear sulfonic acid, for example, macroporous crosslinked polyvinyl aromatic compounds containing sulfonic acid groups are neutralized with a metal of Al, Fe, Zn, Cu, Ni, ions or mixtures and alkali, alkaline earth metals or ammonium ions by contacting the resin containing the sulfonic acid with aqueous solutions of the metals salts and alkali, alkaline earth metal or ammonium salts. The catalysts have at least 50% of the sulfonic acid groups neutralized with metal ions and the balance of the sulfonic acid groups neutralized with alkali, alkaline earth ions or ammonium ions.

  15. METHOD OF PREPARING URANIUM PENTA-FLUORIDE

    DOE Patents [OSTI]

    Hobbs, W.E.

    1962-05-22

    This invention relates to a method for the preparation of UF/sub 5/, Gaseous UF/sub 6/ and gaseous HBr are contacted under anhydrous conditions and at a UF/sub 6/-to-HBr molar ratio of at least approximately 1.7. Beta UF/sub 5/ is obtained at a reaction temperature under 125 deg C, alpha UF5 at a temperature over 1505 deg C, and a mixture of the alpha and beta forms at intermediate (125 te 150 DELTA Etemperatures. (AEC)

  16. Improved method for preparing rare earth sesquichalcogenides

    DOE Patents [OSTI]

    Takeshita, T.; Beaudry, B.J.; Gschneidner, K.A. Jr.

    1982-04-14

    An improved method for the preparation of high purity rare earth sesquichalcogenides is described. The rare earth, as one or more pieces of the metal, is sealed under a vacuum with a stoichiometric amount of sulfur or selenium and a small amount of iodine into a quartz reaction vessel. The sealed vessel is then heated to above the vaporization temperature of the chalcogen and below the melting temperature of the rare earth metal and maintained until the product has been formed. The iodine is then vaporized off leaving a pure product. The rare earth sulfides and selenides thus formed are useful as semiconductors and as thermoelectric generators. 3 tables.

  17. Method to prepare nanoparticles on porous mediums

    DOE Patents [OSTI]

    Vieth, Gabriel M [Knoxville, TN; Dudney, Nancy J [Oak Ridge, TN; Dai, Sheng [Knoxville, TN

    2010-08-10

    A method to prepare porous medium decorated with nanoparticles involves contacting a suspension of nanoparticles in an ionic liquid with a porous medium such that the particles diffuse into the pores of the medium followed by heating the resulting composition to a temperature equal to or greater than the thermal decomposition temperature of the ionic liquid resulting in the removal of the liquid portion of the suspension. The nanoparticles can be a metal, an alloy, or a metal compound. The resulting compositions can be used as catalysts, sensors, or separators.

  18. METHOD OF PREPARING RADIOACTIVE CESIUM SOURCES

    DOE Patents [OSTI]

    Quinby, T.C.

    1963-12-17

    A method of preparing a cesium-containing radiation source with physical and chemical properties suitable for high-level use is presented. Finely divided silica is suspended in a solution containing cesium, normally the fission-product isotope cesium 137. Sodium tetraphenyl boron is then added to quantitatively precipitate the cesium. The cesium-containing precipitate is converted to borosilicate glass by heating to the melting point and cooling. Up to 60 weight percent cesium, with a resulting source activity of up to 21 curies per gram, is incorporated in the glass. (AEC)

  19. Conductive ceramic composition and method of preparation

    DOE Patents [OSTI]

    Smith, J.L.; Kucera, E.H.

    1991-04-16

    A ceramic anode composition is formed of a multivalent metal oxide or oxygenate such as an alkali metal, transition metal oxygenate. The anode is prepared as a non-stoichiometric crystalline structure by reaction and conditioning in a hydrogen gas cover containing minor proportions of carbon dioxide and water vapor. The structure exhibits a single phase and substantially enhanced electrical conductivity over that of the corresponding stoichiometric structure. Unexpectedly, such oxides and oxygenates are found to be stable in the reducing anode fuel gas of a molten carbonate fuel cell. 4 figures.

  20. Resin catalysts and method of preparation

    DOE Patents [OSTI]

    Smith, L.A. Jr.

    1986-12-16

    Heat stabilized catalyst compositions are prepared from nuclear sulfonic acid, for example, macroporous crosslinked polyvinyl aromatic compounds containing sulfonic acid groups are neutralized with a metal of Al, Fe, Zn, Cu, Ni, ions or mixtures and alkali, alkaline earth metals or ammonium ions by contacting the resin containing the sulfonic acid with aqueous solutions of the metals salts and alkali, alkaline earth metal or ammonium salts. The catalysts have at least 50% of the sulfonic acid groups neutralized with metal ions and the balance of the sulfonic acid groups neutralized with alkali, alkaline earth ions or ammonium ions.

  1. Preparation of porous lanthanum phosphate with templates

    SciTech Connect (OSTI)

    Onoda, Hiroaki; Ishima, Yuya; Takenaka, Atsushi; Tanaka, Isao

    2009-08-05

    Malonic acid, propionic acid, glycine, n-butylamine, and urea were added to the preparation of lanthanum phosphate from lanthanum nitrate and phosphoric acid solutions. All additives were taken into lanthanum phosphate particles. The additives that have a basic site were easy to contain in precipitates. The addition of templates improved the specific surface area of lanthanum phosphate. The amount of pore, with radius smaller than 4 nm, increased with the addition of templates. The remained additives had influence on the acidic properties of lanthanum phosphate.

  2. Rapid determination of actinides in seawater samples

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Maxwell, Sherrod L.; Culligan, Brian K.; Hutchison, Jay B.; Utsey, Robin C.; McAlister, Daniel R.

    2014-03-09

    A new rapid method for the determination of actinides in seawater samples has been developed at the Savannah River National Laboratory. The actinides can be measured by alpha spectrometry or inductively-coupled plasma mass spectrometry. The new method employs novel pre-concentration steps to collect the actinide isotopes quickly from 80 L or more of seawater. Actinides are co-precipitated using an iron hydroxide co-precipitation step enhanced with Ti+3 reductant, followed by lanthanum fluoride co-precipitation. Stacked TEVA Resin and TRU Resin cartridges are used to rapidly separate Pu, U, and Np isotopes from seawater samples. TEVA Resin and DGA Resin were used tomore » separate and measure Pu, Am and Cm isotopes in seawater volumes up to 80 L. This robust method is ideal for emergency seawater samples following a radiological incident. It can also be used, however, for the routine analysis of seawater samples for oceanographic studies to enhance efficiency and productivity. In contrast, many current methods to determine actinides in seawater can take 1–2 weeks and provide chemical yields of ~30–60 %. This new sample preparation method can be performed in 4–8 h with tracer yields of ~85–95 %. By employing a rapid, robust sample preparation method with high chemical yields, less seawater is needed to achieve lower or comparable detection limits for actinide isotopes with less time and effort.« less

  3. Data Preparation Process for the Buildings Performance Database |

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Department of Energy Preparation Process for the Buildings Performance Database Data Preparation Process for the Buildings Performance Database Data Preparation Process for the Buildings Performance Database, from the U.S. Department of Energy's Office of Energy Efficiency and Renewable Energy, and Lawrence Berkeley Laboratory. Data Preparation for BPD (August 2015) (1.73 MB) More Documents & Publications BEDES Dictionary 1.0 Data Contribution Best Practices Guide EISA 432 Compliance

  4. Preparation for Facility Operations RM | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Preparation for Facility Operations RM Preparation for Facility Operations RM The objective of this Standard Review Plan (SRP) on Preparation for Facility Operations is to provide consistency guidance to evaluate the effectiveness of the final project closure of major construction projects for transition from Critical Decision-4 (CD-4) to facility operations. Preparation for Facility Operations RM (356.48 KB) More Documents & Publications Code of Record Standard Review Plan (SRP) Standard

  5. Detection of Acetone Processing of Castor Bean Mash for Forensic Investigation of Ricin Preparation Methods

    SciTech Connect (OSTI)

    Kreuzer-Martin, Helen W.; Wahl, Jon H.; Metoyer, Candace N.; Colburn, Heather A.; Wahl, Karen L.

    2010-07-01

    The toxic protein ricin is of concern as a potential biological threat agent (BTA) Recently, several samples of ricin have been seized in connection with biocriminal activity. Analytical methods are needed that enable federal investigators to determine how the samples were prepared, to match seized samples to potential source materials, and to identify samples that may have been prepared by the same method using the same source materials. One commonly described crude ricin preparation method is acetone extraction of crushed castor beans. Here we describe the use of solid-phase microextraction and headspace analysis of crude ricin preparation samples to determine whether they were processed by acetone extraction. In all cases, acetone-extracted bean mash could be distinguished from un-extracted mash or mash extracted with other organic solvents. Statistical analysis showed that storage in closed containers for up to 109 days had no effect on acetone signal intensity. Signal intensity in acetone-extracted mash decreased during storage in open containers, but extracted mash could still be distinguished from un-extracted mash after 94 days.

  6. Novel hard compositions and methods of preparation

    DOE Patents [OSTI]

    Sheinberg, Haskell

    1983-08-23

    Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value. Photomicrographs show that the shapes of the grains of the alloy mixture with which the minor amount of carbide (or carbide-formers) is mixed are radically altered from large, rounded to small, very angular by the addition of the carbide. Superiority of one of these hard compositions of matter over cobalt-bonded tungsten carbide for ultra-high pressure anvil applications was demonstrated.

  7. Novel hard compositions and methods of preparation

    DOE Patents [OSTI]

    Sheinberg, H.

    1983-08-23

    Novel very hard compositions of matter are prepared by using in all embodiments only a minor amount of a particular carbide (or materials which can form the carbide in situ when subjected to heat and pressure); and no strategic cobalt is needed. Under a particular range of conditions, densified compositions of matter of the invention are prepared having hardnesses on the Rockwell A test substantially equal to the hardness of pure tungsten carbide and to two of the hardest commercial cobalt-bonded tungsten carbides. Alternately, other compositions of the invention which have slightly lower hardnesses than those described above in one embodiment also possess the advantage of requiring no tungsten and in another embodiment possess the advantage of having a good fracture toughness value. Photomicrographs show that the shapes of the grains of the alloy mixture with which the minor amount of carbide (or carbide-formers) is mixed are radically altered from large, rounded to small, very angular by the addition of the carbide. Superiority of one of these hard compositions of matter over cobalt-bonded tungsten carbide for ultra-high pressure anvil applications was demonstrated. 3 figs.

  8. New hydroprocessing catalysts prepared from molecular complexes

    SciTech Connect (OSTI)

    Ho, T.C.

    1994-12-31

    Current commercial hydroprocessing catalysts are transition metal sulfides (TMS) based on Group 8 and 11 metals. They are prepared by dispersing MoO{sub 3} and a promoter metal oxide, either CoO or NiO, on {gamma}-Al{sub 2}O{sub 3} or SiO{sub 2}-modified Al{sub 2}O{sub 3}. This is followed by sulfiding with a sulfur-bearing stream such as H{sub 2}S at high temperatures. The thus formed MoS{sub 2} crystallites are the backbone of the working catalysts. A potentially fruitful approach to new catalysts would be to molecularly incorporate promoter metals into the structure of MoS{sub 2} edge planes. As a first step, it would seem reasonable to exploit the use of heterometallic metal sulfur complexes as hydroprocessing catalyst precursors. The authors have developed several families of new catalysts along this line. In this paper the authors restrict themselves to the metal amine thiomolybdate-derived catalysts. Specifically, they give an overview of the performance of the bulk (unsupported) FeMo sulfide prepared from MAT. This low-surface-area catalyst shows a high HDN-to-HDS volumetric activity ratio and is also active for HDA. While most of the results are taken from their previous publications, some new results are reported here.

  9. Experience in preparing fuel for combustion

    SciTech Connect (OSTI)

    Rude, J.

    1995-09-01

    The key phase seems to be that wood is the ORIGINAL FUEL. Certainly as man discovered fire, it was the most obvious as well as abundantly available fuel and it burned very well because man was smart enough to select the dry wood once he understood the basics of combustion. As the needs started to go beyond the most elementary, designs for burning ideal fuels were pretty well perfected, however, the burning of less ideal fuels still remain a challenge. To provide plant steam requirements by burning waste that must be disposed of anyway can reduce operating cost considerably. For most of us involved in producing steam, the experience we have with fuels such as bark, wood waste, sludge, and miscellaneous forms of solid combustible waste material, are a result of burning these fuels in an existing boiler supposedly designed for wood waste or possibly a combination of wood and other fuels such as coal, oil, or gas. For a supplier of fuel preparation systems, the typical application involves the sizing, cleaning, and drying of wood waste, and sludge from a pulp and/or paper mill. Other forms of combustible waste are dealt with occasionally and after proper preparation fired in the combustion system for the purpose of generating hot gas and/or steam for the plant process.

  10. Ethylenediamine salt of 5-nitrotetrazole and preparation

    DOE Patents [OSTI]

    Lee, Kien-yin; Coburn, Michael D.

    1985-01-01

    Ethylenediamine salt of 5-nitrotetrazole and preparation. This salt has been found to be useful as an explosive alone and in eutectic mixtures with ammonium nitrate and/or other explosive compounds. Its eutectic with ammonium nitrate has been demonstrated to behave in a similar manner to a monomolecular explosive such as TNT, and is less sensitive than the pure salt. Moreover, this eutectic mixture, which contains 87.8 mol % of ammonium nitrate, is close to the CO.sub.2 -balanced composition of 90 mol %, and has a relatively low melting point of 110.5 C. making it readily castable. The ternary eutectic system containing the ethylenediamine salt of 5-nitrotetrazole, ammonium nitrate and ethylenediamine dinitrate has a eutectic temperature of 89.5 C. and gives a measured detonation pressure of 24.8 GPa, which is 97.6% of the calculated value. Both the pure ethylenediamine salt and its known eutectic compounds behave in substantially ideal manner. Methods for the preparation of the salt are described.