National Library of Energy BETA

Sample records for del sol cxs

  1. Sandia Energy - Mesa del Sol Project Is Finalist for International...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Infrastructure Security Renewable Energy Energy Surety Mesa del Sol Energy Facilities Grid Integration Partnership News Distribution Grid Integration News & Events Photovoltaic...

  2. CASA DEL SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirleyEnergyTher i n c i p a l DeInsulation at04-86) (All Previous EditionsOffice of2,CASA DEL

  3. CASA DEL SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirley Ann JacksonDepartment of EnergyResearchers atDayWhenBethanyOnAristidesonBuzMoney andCASA DEL

  4. CASA DEL SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirley Ann JacksonDepartment|Marketing, LLCEfficiency | DepartmentEnergyofC3ECALIFORNIACASA DEL

  5. Reflexiones y alegrías en los 20 años de Sol del Río

    E-Print Network [OSTI]

    Cea, José Roberto

    1993-10-01

    FALL 1993 125 Reflexiones y alegrías en los 20 años de Sol del Río José Roberto Cea En sus inicios, este grupo teatral se llamó Sol del Río 32, ahora es la Compañía Sol del Río. Su fundación fue el 7 de junio de 1973. Han madurado mucho, que la... florecer mejor. Sol del Río ha hecho muchas muy buenas acciones: como mantenerse grupalmente en su trabajo, hacer de este trabajo una profesión de fe y seguridad, lo que les ha permitido hacer espectáculos teatrales que se han mostrado sin rubor alguno...

  6. Sandia Energy - Mesa del Sol Unveils First Smart Grid in the Nation

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust, High-Throughput Analysis ofSampleLignin-Feasting MicrobeMesa del Sol Unveils First Smart

  7. Serie cronolgica de un CME estallando desde el Sol

    E-Print Network [OSTI]

    Christian, Eric

    #12;Serie cronológica de un CME estallando desde el Sol Imagen Compuesta del Sol en luz anaranjado?). Sin embargo, nuestro Sol nos da más que solo una corriente de luz y calor. El Sol nos baña a nosotros y al resto del sistema solar con energía en forma de luz, partículas cargadas eléctricamente y

  8. Sandia Energy - Mesa del Sol

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservation of Fe(II)Geothermal Energy &Water Power&

  9. DE-SOL-0008448

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal GasAdministration Medal01 Sandia National 1 PAGE 1 OF2Guidance to the1NDE-SOL-0008445I,

  10. Nanocrystal/sol-gel nanocomposites

    DOE Patents [OSTI]

    Petruska, Melissa A. (Los Alamos, NM); Klimov, Victor L. (Los Alamos, NM)

    2007-06-05

    The present invention is directed to solid composites including colloidal nanocrystals within a sol-gel host or matrix and to processes of forming such solid composites. The present invention is further directed to alcohol soluble colloidal nanocrystals useful in formation of sol-gel based solid composites.

  11. Nanocrystal/sol-gel nanocomposites

    DOE Patents [OSTI]

    Petruska, Melissa A. (Los Alamos, NM); Klimov, Victor L. (Los Alamos, NM)

    2012-06-12

    The present invention is directed to solid composites including colloidal nanocrystals within a sol-gel host or matrix and to processes of forming such solid composites. The present invention is further directed to alcohol soluble colloidal nanocrystals useful in formation of sol-gel based solid composites

  12. ENERGIA DEL SOL Ts = 5780 K

    E-Print Network [OSTI]

    Batiste, Oriol

    es basa la conversi´o de la radiaci´o solar en calor. #12;TRANSFER`ENCIA DE CALOR PER RADIACI´O Llei a utilitzar-la. Conversi´o en calor Conversi´o directa en electricitat Tractarem primer els principis en que

  13. Sandia Energy » Mesa del Sol

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust, High-ThroughputUpcoming Release of the University of Minnesota's VirtualSandia WinsMesa

  14. CASA DEL SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirleyEnergyTher i n c i p a l DeInsulation at04-86) (All Previous EditionsOffice of2, thetCASA

  15. CASA DEL SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirleyEnergyTher i n c i p a l DeInsulation at04-86) (All Previous EditionsOffice of2,

  16. CASA DEL SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirley Ann JacksonDepartment|Marketing, LLCEfficiency | DepartmentEnergyofC3ECALIFORNIACASA

  17. Sol-gel derived sorbents

    DOE Patents [OSTI]

    Sigman, Michael E.; Dindal, Amy B.

    2003-11-11

    Described is a method for producing copolymerized sol-gel derived sorbent particles for the production of copolymerized sol-gel derived sorbent material. The method for producing copolymerized sol-gel derived sorbent particles comprises adding a basic solution to an aqueous metal alkoxide mixture for a pH.ltoreq.8 to hydrolyze the metal alkoxides. Then, allowing the mixture to react at room temperature for a precalculated period of time for the mixture to undergo an increased in viscosity to obtain a desired pore size and surface area. The copolymerized mixture is then added to an immiscible, nonpolar solvent that has been heated to a sufficient temperature wherein the copolymerized mixture forms a solid upon the addition. The solid is recovered from the mixture, and is ready for use in an active sampling trap or activated for use in a passive sampling trap.

  18. Sol-Gel Deposited Electrochromic Coatings

    E-Print Network [OSTI]

    Ozer, N.

    2010-01-01

    layer, (3) solid electrolyte or ion conductor, (4) ionof inorganic type solid electrolytes [20,21]. An all sol-gel

  19. Hybrid sol-gel optical materials

    DOE Patents [OSTI]

    Zeigler, John M. (Albuquerque, NM)

    1992-01-01

    Hybrid sol-gel materials comprise silicate sols cross-linked with linear polysilane, polygermane, or poly(silane-germane). The sol-gel materials are useful as optical identifiers in tagging and verification applications and, in a different aspect, as stable, visible light transparent non-linear optical materials. Methyl or phenyl silicones, polyaryl sulfides, polyaryl ethers, and rubbery polysilanes may be used in addition to the linear polysilane. The linear polymers cross-link with the sol to form a matrix having high optical transparency, resistance to thermooxidative aging, adherence to a variety of substrates, brittleness, and a resistance to cracking during thermal cycling.

  20. Hybrid sol-gel optical materials

    DOE Patents [OSTI]

    Zeigler, J.M.

    1993-04-20

    Hybrid sol-gel materials comprise silicate sols cross-linked with linear polysilane, polygermane, or poly(silane-germane). The sol-gel materials are useful as optical identifiers in tagging and verification applications and, in a different aspect, as stable, visible light transparent non-linear optical materials. Methyl or phenyl silicones, polyaryl sulfides, polyaryl ethers, and rubbery polysilanes may be used in addition to the linear polysilane. The linear polymers cross-link with the sol to form a matrix having high optical transparency, resistance to thermooxidative aging, adherence to a variety of substrates, brittleness, and a resistance to cracking during thermal cycling.

  1. Hybrid sol-gel optical materials

    DOE Patents [OSTI]

    Zeigler, John M. (Albuquerque, NM)

    1993-01-01

    Hybrid sol-gel materials comprise silicate sols cross-linked with linear polysilane, polygermane, or poly(silane-germane). The sol-gel materials are useful as optical identifiers in tagging and verification applications and, in a different aspect, as stable, visible light transparent non-linear optical materials. Methyl or phenyl silicones, polyaryl sulfides, polyaryl ethers, and rubbery polysilanes may be used in addition to the linear polysilane. The linear polymers cross-link with the sol to form a matrix having high optical transparency, resistance to thermooxidative aging, adherence to a variety of substrates, brittleness, and a resistance to cracking during thermal cycling.

  2. A Solution Route to Thermoelectric Oxide Nanoparticles - A Sol...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    A Solution Route to Thermoelectric Oxide Nanoparticles - A Sol-Gel Process Employing Heterometallic Alkoxides A Solution Route to Thermoelectric Oxide Nanoparticles - A Sol-Gel...

  3. Plexus Sol | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoop Inc Jump to:Newberg,Energy LLC JumpPhono SolarPlexus Sol Jump to: navigation,

  4. AGGIE SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirleyEnergyTher i n c i p a l De p u t y A s s iof1AGGIE SOL The University of California,

  5. AGGIE SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirleyEnergyTher i n c i p a l De p u t y A s s iof1AGGIE SOL The University of California,AGGIE

  6. AGGIE SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirleyEnergyTher i n c i p a l De p u t y A s s iof1AGGIE SOL The University of

  7. AGGIE SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirley Ann JacksonDepartment| Department ofApplianceU.S.Departmentthe(Revision 2)EnergyAGGIE SOL

  8. Sol-gel antireflective coating on plastics

    DOE Patents [OSTI]

    Ashley, C.S.; Reed, S.T.

    1988-01-26

    An antireflection film made from reliquified sol-gel hydrolyzation, condensation polymeric reaction product of a silicon, alkoxides and/or metal alkoxides, or mixtures thereof. The film is particularly useful for coating plastics.

  9. Sol-gel antireflective coating on plastics

    DOE Patents [OSTI]

    Ashley, Carol S. (Albuquerque, NM); Reed, Scott T. (Albuquerque, NM)

    1990-01-01

    An antireflection film made from a reliquified sol-gel hydrolyzation, condensation polymeric reaction product of a silicon, alkoxides and/or metal alkoxides, or mixtures thereof. The film is particularly useful for coating plastics.

  10. Sol-gel method for encapsulating molecules

    DOE Patents [OSTI]

    Brinker, C. Jeffrey (Albuquerque, NM); Ashley, Carol S. (Albuquerque, NM); Bhatia, Rimple (Albuquerque, NM); Singh, Anup K. (San Francisco, CA)

    2002-01-01

    A method for encapsulating organic molecules, and in particular, biomolecules using sol-gel chemistry. A silica sol is prepared from an aqueous alkali metal silicate solution, such as a mixture of silicon dioxide and sodium or potassium oxide in water. The pH is adjusted to a suitably low value to stabilize the sol by minimizing the rate of siloxane condensation, thereby allowing storage stability of the sol prior to gelation. The organic molecules, generally in solution, is then added with the organic molecules being encapsulated in the sol matrix. After aging, either a thin film can be prepared or a gel can be formed with the encapsulated molecules. Depending upon the acid used, pH, and other processing conditions, the gelation time can be from one minute up to several days. In the method of the present invention, no alcohols are generated as by-products during the sol-gel and encapsulation steps. The organic molecules can be added at any desired pH value, where the pH value is generally chosen to achieve the desired reactivity of the organic molecules. The method of the present invention thereby presents a sufficiently mild encapsulation method to retain a significant portion of the activity of the biomolecules, compared with the activity of the biomolecules in free solution.

  11. Neutron detector using sol-gel absorber

    DOE Patents [OSTI]

    Hiller, John M. (Oak Ridge, TN); Wallace, Steven A. (Oak Ridge, TN); Dai, Sheng (Knoxville, TN)

    1999-01-01

    An neutron detector composed of fissionable material having ions of lithium, uranium, thorium, plutonium, or neptunium, contained within a glass film fabricated using a sol-gel method combined with a particle detector is disclosed. When the glass film is bombarded with neutrons, the fissionable material emits fission particles and electrons. Prompt emitting activated elements yielding a high energy electron contained within a sol-gel glass film in combination with a particle detector is also disclosed. The emissions resulting from neutron bombardment can then be detected using standard UV and particle detection methods well known in the art, such as microchannel plates, channeltrons, and silicon avalanche photodiodes.

  12. Duo at Santa Fe's Monte del Sol Charter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    New Mexico Supercomputing Challenge April 21, 2015 Using nanotechnology robots to kill cancer cells LOS ALAMOS, N.M., April 21, 2015-Meghan Hill and Katelynn James of Santa Fe's...

  13. Duo at Santa Fe's Monte del Sol Charter

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalentLaboratory |Sectorfor $1.14 Per1-E Wholesale

  14. Sol-Gel Manufactured Energetic Materials

    DOE Patents [OSTI]

    Simpson, Randall L. (Livermore, CA); Lee, Ronald S. (Livermore, CA); Tillotson, Thomas M. (Tracy, CA); Hrubesh, Lawrence W. (Pleasanton, CA); Swansiger, Rosalind W. (Livermore, CA); Fox, Glenn A. (Livermore, CA)

    2005-05-17

    Sol-gel chemistry is used for the preparation of energetic materials (explosives, propellants and pyrotechnics) with improved homogeneity, and/or which can be cast to near-net shape, and/or made into precision molding powders. The sol-gel method is a synthetic chemical process where reactive monomers are mixed into a solution, polymerization occurs leading to a highly cross-linked three dimensional solid network resulting in a gel. The energetic materials can be incorporated during the formation of the solution or during the gel stage of the process. The composition, pore, and primary particle sizes, gel time, surface areas, and density may be tailored and controlled by the solution chemistry. The gel is then dried using supercritical extraction to produce a highly porous low density aerogel or by controlled slow evaporation to produce a xerogel. Applying stress during the extraction phase can result in high density materials. Thus, the sol-gel method can be used for precision detonator explosive manufacturing as well as producing precision explosives, propellants, and pyrotechnics, along with high power composite energetic materials.

  15. Sol-gel manufactured energetic materials

    DOE Patents [OSTI]

    Simpson, Randall L.; Lee, Ronald S.; Tillotson, Thomas M.; Hrubesh, Lawrence W.; Swansiger, Rosalind W.; Fox, Glenn A.

    2003-12-23

    Sol-gel chemistry is used for the preparation of energetic materials (explosives, propellants and pyrotechnics) with improved homogeneity, and/or which can be cast to near-net shape, and/or made into precision molding powders. The sol-gel method is a synthetic chemical process where reactive monomers are mixed into a solution, polymerization occurs leading to a highly cross-linked three dimensional solid network resulting in a gel. The energetic materials can be incorporated during the formation of the solution or during the gel stage of the process. The composition, pore, and primary particle sizes, gel time, surface areas, and density may be tailored and controlled by the solution chemistry. The gel is then dried using supercritical extraction to produce a highly porous low density aerogel or by controlled slow evaporation to produce a xerogel. Applying stress during the extraction phase can result in high density materials. Thus, the sol-gel method can be used for precision detonator explosive manufacturing as well as producing precision explosives, propellants, and pyrotechnics, along with high power composite energetic materials.

  16. Sol-gel processing with inorganic metal salt precursors

    DOE Patents [OSTI]

    Hu, Zhong-Cheng

    2004-10-19

    Methods for sol-gel processing that generally involve mixing together an inorganic metal salt, water, and a water miscible alcohol or other organic solvent, at room temperature with a macromolecular dispersant material, such as hydroxypropyl cellulose (HPC) added. The resulting homogenous solution is incubated at a desired temperature and time to result in a desired product. The methods enable production of high quality sols and gels at lower temperatures than standard methods. The methods enable production of nanosize sols from inorganic metal salts. The methods offer sol-gel processing from inorganic metal salts.

  17. Documentation EnMetSol 1 Documentation -EnMetSOL

    E-Print Network [OSTI]

    Oldenburg, Carl von Ossietzky Universität

    which provides high quality daylight and solar radiation data for Western and Central Europe. 9th von Ossietzky University of Oldenburg Dr. A. Hammer Date 2014-03-25 #12;Documentation ­ EnMetSol 2 of determining the global radiation at the ground by using data from a geostationary satellite, see [1,2]. We use

  18. SolGen | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page| Open Energy Information Serbia-Enhancing Capacity forSilicium deEnergy Information North| OpenSolutionSolGen Jump

  19. QuantaSol Limited | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoop Inc Jump to:Newberg,Energy LLCALLETE IncScience and Technology CoQuantaSol Limited

  20. SolSolution | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoop Inc JumpHeter Battery TechnologySocovoltaic Systems Jump to:SoftSuisseSolSolution

  1. SolBeam Inc | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION JEnvironmental Jump to:EA EIS ReportEurope GmbH JumpSlough HeatMccoy Geothermal AreaSolBeam Inc

  2. TiSol | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION JEnvironmental Jump to:EA EISTJThin Film Solar Technologies JumpTiSol Jump to: navigation, search

  3. DE-SOL-0008445 Attachment L-4

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal GasAdministration Medal01 Sandia National 1 PAGE 1 OF2Guidance to the1NDE-SOL-0008445

  4. E2SOL LLC | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoopButtePower VenturesInformation9)askDouble Oak,Durra BuildingCane FuelFuelEE2SOL

  5. Sol-gel coatings for optoelectronic devices

    SciTech Connect (OSTI)

    Avellaneda, C.O.; Macedo, M.A.; Florentino, A.O.; Aegerter, M.A. [Univ. of Sao Paulo, Sao Carlos (Brazil). Inst. de Fisica e Quimica

    1994-12-31

    Nb{sub 2}O{sub 5} prepared by a sol-gel process in form of coatings and aerogels are new materials which present interesting properties: (a) The coatings present electrochromic properties and exhibit a blue coloration under Li{sup +} insertion with 100% reversible variation of the optical transmission in the visible and near infrared range between 80% and 200% and have a high chemical stability (tested up to 2,000 cycles). (b) They are semiconductor and present a photoelectric effect when illuminating in the UV region ({lambda} < 360 nm). These films are therefore very promising to be used in electrochromic devices, as electrodes for photoelectrochemical purpose and the development of nanocrystalline solar cell. (c) When prepared in aerogel form, the high BET surface area of the powders is a promising asset to use these new materials for catalytic purposes for air pollution control.

  6. Sol-gel processing of energetic materials

    SciTech Connect (OSTI)

    Tillotson, T.M.; Hrubesh, L.H.; Fox, G.L.; Simpson, R.L.; Lee, R.W.; Swansiger, R.W.; Simpson, L.R.

    1997-08-18

    As part of a new materials effort, we are exploring the use of sol- gel chemistry to manufacture energetic materials. Traditional manufacturing of energetic materials involves processing of granular solids. One application is the production of detonators where powders of energetic material and a binder are typically mixed and compacted at high pressure to make pellets. Performance properties are strongly dependent on particle size distribution, surface area of its constituents, homogeneity of the mix, and void volume. The goal is to produce detonators with fast energy release rate the are insensitive to unintended initiation. In this paper, we report results of our early work in this field of research, including the preparation of detonators from xerogel molding powders and aerogels, comparing the material properties with present state-of-the-art technology.

  7. Sol-gel-derived Epitaxial Nanocomposite Thin Films with Large...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Sol-gel-derived Epitaxial Nanocomposite Thin Films with Large Sharp Magnetoelectric Effect Home Author: B. Liu, T. Sun, J. He, V. P. Dravid Year: 2010 Abstract: Nanostructures of...

  8. Micro-PIXE characterization of interactions between a sol-gel derived bioactive glass and

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    - 1 - Micro-PIXE characterization of interactions between a sol-gel derived bioactive glass the different steps of this bioactivity process via a complete micro-PIXE characterization of a sol- gel derived

  9. Environmental Assessment and Metrics for Solar: Case Study of SolFocus Solar Concentrator Systems

    E-Print Network [OSTI]

    Reich-Weiser, Corinne; Dornfeld, David; Horne, Steve

    2008-01-01

    Assumptions Assembly in India Energy Breakdown t to on3. Energy Breakdown for SolFocus Concentrator System. India

  10. Dgradation et transformation d'un compost ptrolier apport des sols battants et effets sur

    E-Print Network [OSTI]

    Boyer, Edmond

    Dégradation et transformation d'un compost pétrolier apporté à des sols battants et effets sur devenir d'un compost pétrolier après incorporation dans le sol et à appré- cier sa valeur d'amendement. L'expérimentation a été effectuée au laboratoire sur 2 sols de texture limoneuse enrichis en compost selon une dose unique

  11. 3rd ITPA SOL and Divertor Topical Group meeting, St. Petersburg, July 2003 ASDEX Upgrade

    E-Print Network [OSTI]

    3rd ITPA SOL and Divertor Topical Group meeting, St. Petersburg, July 2003 ASDEX Upgrade Arne for power balance A. Kallenbach, 3rd ITPA SOL and Divertor Topical Group meeting, St. Petersburg, July 2003 ms spatial resolution 1-2 mm #12;divertor geometries A. Kallenbach, 3rd ITPA SOL and Divertor Topical

  12. Sol-gel matrices for direct colorimetric detection of analytes

    DOE Patents [OSTI]

    Charych, Deborah H. (Albany, CA); Sasaki, Darryl (Albuquerque, NM); Yamanaka, Stacey (Dallas, TX)

    2000-01-01

    The present invention relates to methods and compositions for the direct detection of analytes using color changes that occur in immobilized biopolymeric material in response to selective binding of analytes to their surface. In particular, the present invention provides methods and compositions related to the encapsulation of biopolymeric material into metal oxide glass using the sol-gel method.

  13. MECHANICAL PROPERTY CHARACTERIZATION OF SOL-GEL DERIVED NANOMATERIALS

    E-Print Network [OSTI]

    Brinker, C. Jeffrey

    mechanical behavior of polysilicate aerogels, prepared using the sol-gel process. Two series of materials were prepared, derivatized with silylating agents, processed into coating solutions, and characterized properties of aerogel thin films were characterized. vi #12;Table of Contents Abstract

  14. Sol-gel chemistry by ring-opening polymerization

    SciTech Connect (OSTI)

    RAHIMIAN,KAMYAR; LOY,DOUGLAS A.

    2000-02-07

    Sol-gel processing of materials is plagued by shrinkage during polymerization of the alkoxide monomers and processing (aging and drying) of the resulting gels. The authors have developed a new class of hybrid organic-inorganic materials based on the solventless ring-opening polymerization (ROP) of monomers bearing the 2,2,5,5-tetramethyl-2,5-disilaoxacyclopentyl group, which permits them to drastically reduce shrinkage in sol-gel processed materials. Because the monomers are polymerized through a chain growth mechanism catalyzed by base rather than the step growth mechanism normally used in sol-gel systems, hydrolysis and condensation products are entirely eliminated. Furthermore, since water is not required for hydrolysis, an alcohol solvent is not necessary. Monomers with two disilaoxacyclopentyl groups, separated by a rigid phenylene group or a more flexible alkylene group, were prepared through disilylation of the corresponding diacetylenes, followed by ring closure and hydrogenation. Anionic polymerization of these materials, either neat or with 2,2,5,5-tetramethyl-2,5-disila-1-oxacyclopentane as a copolymer, affords thermally stable transparent gels with no visible shrinkage. These materials provide an easy route to the introduction of sol-gel type materials in encapsulation of microelectronics, which they have successfully demonstrated.

  15. Aero-Sol-Gel (ASG) Reactor For Nano-Powder Synthesis G. Beaucage, J. Hyeon-Lee, D. J. Kohls

    E-Print Network [OSTI]

    Beaucage, Gregory

    Aero-Sol-Gel (ASG) Reactor For Nano-Powder Synthesis G. Beaucage, J. Hyeon-Lee, D. J. Kohls-structured oxides where sol- gel reactions are carried out in aerosol droplets. This aero-sol-gel reactor (ASG-scale structure and high specific surface areas (100 to 700 m2 /g) [1, 2]. This aero-sol- gel reactor (ASG

  16. Sol-gel polymerization of tetraalkoxygermanium and organotrialkoxygermanium monomers

    SciTech Connect (OSTI)

    Baugher, B.M.; Loy, D.A. [Sandia National Labs., Albuquerque, NM (United States). Properties of Organic Materials Dept.

    1996-12-31

    While the sol-gel polymerizations of tetraalkoxy- and organotrialkoxysilanes have been extensively studied, there have been few reports of similar investigations with the analogous tetraalkoxygermanium and organotrialkoxygermanium compounds. Germanium alkoxides have received less attention due, in part to their higher cost, but also their greater reactivity towards hydrolysis and condensation reactions. Germanium oxide materials are potentially interesting because the Ge-O-Ge linkage is labile (compared with the siloxane bond in silica gels and polysilsequioxanes) opening up the possibility of further chemical modification of the polymeric architecture. This may permit hydrolytic reorganization of germanium oxide networks under relatively mild conditions. In this paper, the authors present the results of investigations of the sol-gel polymerizations of tetraethoxygermanium, tetraisopropoxygermanium, and methyltriethoxy-germanium to afford network materials as both xerogels and aerogels.

  17. Synthesis of zirconium oxide nanoparticle by sol-gel technique

    SciTech Connect (OSTI)

    Lim, H. S.; Ahmad, A.; Hamzah, H. [School of Chemical Science and Food Technology, Faculty of Science and Technology, National University of Malaysia, 43600 Bangi (Malaysia)

    2013-11-27

    Zirconium oxide nanoparticle is synthesized using sol-gel technique. Various mole ratio of ammonia solution and nitric acid relative to zirconium propoxide is added in the reaction to study the effect on the crystallinity and particle size on zirconium oxide particle. Zirconium oxide synthesized with nitric acid have the smallest particle size under FESEM image and show the increasing formation of crystalline tetragonal phase under XRD diffractogram.

  18. Solventless sol-gel chemistry through ring-opening polymerization of bridged disilaoxacyclopentanes

    SciTech Connect (OSTI)

    RAHIMIAN,KAMYAR; LOY,DOUGLAS A.

    2000-04-04

    Disilaoxacyclopentanes have proven to be excellent precursors to sol-gel type materials. These materials have shown promise as precursors for encapsulation and microelectronics applications. The polymers are highly crosslinked and are structurally similar to traditional sol-gels, but unlike typical sol-gels they are prepared without the use of solvents and water, they have low VOC's and show little shrinkage during processing.

  19. Inves Pozo Sol Sociedad Limitada | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QAsource History View NewTexas: Energy ResourcesOrder at 8, 13Renewable PowerMismatch |Inves Pozo Sol Sociedad

  20. Novatec BioSol AG | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QAsource History ViewMayo, Maryland:NPI VenturesNewSt. Louis, Minnesota: EnergyOhio: EnergyNottingham,Novatec BioSol

  1. PaSol Italia SpA | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QAsource History ViewMayo, Maryland:NPIProtectio Program | OpenWisconsin:NewOverPPS EnviroPowered Inc JumpPVMPaSol

  2. DE-SOL-0000332 | netl.doe.gov

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HAB Packet Hanford Advisory Board6/23/2014 Rev. 20 IdahoDE-SOL-0000332

  3. DE-SOL-0003719 | netl.doe.gov

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HAB Packet Hanford Advisory Board6/23/2014 Rev. 20DE-SOL-0003719 -

  4. DE-SOL-0005395 | netl.doe.gov

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HAB Packet Hanford Advisory Board6/23/2014 Rev. 20DE-SOL-0003719

  5. DE-SOL-0006851 | netl.doe.gov

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HAB Packet Hanford Advisory Board6/23/2014 Rev. 20DE-SOL-0003719Site

  6. Consolidated Edison Sol Inc (New Jersey) | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX E LISTStar EnergyLawler,CoalConcordia Electric Coop, IncIllinois)Consolidated Edison Sol

  7. I Sol Ventures GmbH | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX E LISTStar2-0057-EA JumpDuimen RiverScoringUtilities Comm JumpImaging JumpSol Ventures

  8. ConSol (Building Industry Research Alliance) | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoopButtePower Ventures JumpCommercial Jump(Thompson, 1985)(Laney, 2005)ComvergeConSol

  9. Stress effects in sol-gel derived ferroelectric thin films L. Lian and N. R. Sottosa)

    E-Print Network [OSTI]

    Sottos, Nancy R.

    Stress effects in sol-gel derived ferroelectric thin films L. Lian and N. R. Sottosa) Department 26 August 2003; accepted 19 October 2003 Residual stress development during processing of sol investigates the effects of stress on field-induced polarization switching in ferroelectric Pb Zr0.52Ti0.48)O3

  10. Toroidicity in the Tokamak SOL: Effects on Poloidal Asymmetries, Radial Current and the L-H Transition

    E-Print Network [OSTI]

    Toroidicity in the Tokamak SOL: Effects on Poloidal Asymmetries, Radial Current and the L-H Transition

  11. Optical fiber sensor having a sol-gel fiber core and a method of making

    DOE Patents [OSTI]

    Tao, Shiquan; Jindal, Rajeev; Winstead, Christopher; Singh, Jagdish P.

    2006-06-06

    A simple, economic wet chemical procedure is described for making sol-gel fibers. The sol-gel fibers made from this process are transparent to ultraviolet, visible and near infrared light. Light can be guided in these fibers by using an organic polymer as a fiber cladding. Alternatively, air can be used as a low refractive index medium. The sol-gel fibers have a micro pore structure which allows molecules to diffuse into the fiber core from the surrounding environment. Chemical and biochemical reagents can be doped into the fiber core. The sol-gel fiber can be used as a transducer for constructing an optical fiber sensor. The optical fiber sensor having an active sol-gel fiber core is more sensitive than conventional evanescent wave absorption based optical fiber sensors.

  12. Aero-Sol-Gel Synthesis of Nanostructured Silica Jingyu Hyeon-Lee, Gregory Beaucage,*, and Sotiris E. Pratsinis

    E-Print Network [OSTI]

    Beaucage, Gregory

    Aero-Sol-Gel Synthesis of Nanostructured Silica Powders Jingyu Hyeon-Lee, Gregory Beaucage-temperature aero- sol-gel process. Hydrolysis and condensation of tetraethoxysilane (TEOS) and tetramethoxy- silane, an aero-sol- gel technique for production of powders with extremely high specific surface areas at room

  13. Located in downtown Tucson, Armory Park del Sol finds its architectural inspiration in the surrounding

    E-Print Network [OSTI]

    flooring Energy Efficient ~ Photovoltaic electric power generating systems ~ Solar water heaters with on- demand water heater backup ~ Dual pane high efficiency windows ~ Masonry wall superstructure is concrete masonry super structure ~ Termite proof metal studs ~ Copper water lines Easy Access ~ Extra-wide hallways

  14. Best Practices Case Study: John Wesley Miller Companies - Armory Park Del Sol, Tucson, AZ

    SciTech Connect (OSTI)

    2009-10-01

    Case study of John Wesley Miller Companies, who built two net zero energy homes plus 97 other solar homes in Tucson, AZ. Masonry block walls with rigid foam exterior sheathing, rigid foam over the roof deck plus R-38 in the attic, ducts in conditioned space, 4.2 kW and 5.7 kW photovoltaics and solar water heating yielded HERS scores of 0 on the two homes.

  15. Duo at Santa Fe's Monte del Sol Charter School takes top award...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Challenge is open to any New Mexico high-school, middle-school or elementary-school student. More than 240 students representing 64 teams from schools around the state...

  16. Duo at Santa Fe's Monte del Sol Charter School takes top award in 25th

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HAB PacketDieselAbsorption Techniques |Dr.Dr.

  17. Sandia Energy - Mesa del Sol Project Is Finalist for International Smart

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservation of Fe(II)Geothermal Energy &Water Power&Grid Action Network 2014 Award of

  18. Substituent effects on the sol-gel chemistry of organotrialkoxysilanes

    SciTech Connect (OSTI)

    LOY, DOUGLAS A.; BAUGHER, BRIGITTA M.; BAUGHER, COLLEEN R.; SCHNEIDER, DUANE A.; RAHIMIAN, KAMYAR

    2000-05-09

    Silsesquioxanes have been the subject of intensive study in the past and are becoming important again as a vehicle for introducing organic functionalities into hybrid organic-inorganic materials through sol-gel processing. Depending on the application, the target hybrid material may be required to be a highly cross-linked, insoluble gel or a soluble polymer that can be cast as a thin film or coating. The former has applications such as catalyst supports and separations media; the latter is an economically important method for surface modification or compatiblization for applying adhesives or introducing fillers. Polysilsesquioxanes are readily prepared through the hydrolysis and condensation of organotrialkoxysilanes, though organotriaminosilane and organotrihalosilane monomers can also be used. This paper explores the kinetics of the preparation route.

  19. Mayenite Synthesized Using the Citrate Sol-Gel Method

    SciTech Connect (OSTI)

    Ude, Sabina N [ORNL] [ORNL; Rawn, Claudia J [ORNL] [ORNL; Meisner, Roberta A [University of Tennessee (UTK) and Oak Ridge National Laboratory (ORNL)] [University of Tennessee (UTK) and Oak Ridge National Laboratory (ORNL); Kirkham, Melanie J [ORNL] [ORNL; Jones, Gregory L. [University of Tennessee, Knoxville (UTK)] [University of Tennessee, Knoxville (UTK); Payzant, E Andrew [ORNL] [ORNL

    2014-01-01

    A citrate sol-gel method has been used to synthesize mayenite (Ca12Al14O33). X-ray powder diffraction data show that the samples synthesized using the citrate sol-gel method contained CaAl2O4 and CaCO3 along with mayenite when fired ex-situ in air at 800 C but were single phase when fired at 900 C and above. Using high temperature x-ray diffraction, data collected in-situ in air at temperatures of 600 C and below showed only amorphous content; however, data collected at higher temperatures indicated the first phase to crystallize is CaCO3. High temperature x-ray diffraction data collected in 4% H2/96% N2 does not show the presence of CaCO3, and Ca12Al14O33 starts to form around 850 C. In comparison, x-ray powder diffraction data collected ex-situ on samples synthesized using traditional solid-state synthesis shows that single phase was not reached until samples were fired at 1350 C. DTA/TGA data collected either in a nitrogen environment or air on samples synthesized using the citrate gel method suggest the complete decomposition of metastable phases and the formation of mayenite at 900 C, although the phase evolution is very different depending on the environment. Brunauer-Emmett-Teller (BET) measurements showed a slightly higher surface area of 7.4 0.1 m2/g in the citrate gel synthesized samples compared to solid-state synthesized sample with a surface area of 1.61 0.02 m2/g. SEM images show a larger particle size for samples synthesized using the solid-state method compared to those synthesized using the citrate gel method.

  20. Non-Shrinking Sol-Gel Type Polymers by Ring Opening Polymerizations

    SciTech Connect (OSTI)

    Loy, D.A.; Rahimian, K.

    1999-04-05

    We have designed a new class of cyclic siloxane compounds that behave as sol-gel systems when ring open polymerized using a hydroxide base. These monomers polymerize through chain growth polymerization. unlike conventional alkoxysilane sol-gel precursors, to form sol-gel polymers. They do not require solvent or water for polymerization, show no visible shrinkage or cracking during polymerization and are thermally stable. We have successfully utilized these materials in encapsulation of microelectronics. Current efforts are focused toward expanding this family of ROP monomers and optimization of their mechanical properties.

  1. Solventless sol-gel chemistry through ring-opening polymerization of bridged disilaoxacyclopentanes

    SciTech Connect (OSTI)

    RAHIMIAN,KAMYAR; LOY,DOUGLAS A.

    2000-05-01

    Ring-opening polymerization (ROP) of disilaoxacyclopentanes has proven to be an excellent approach to sol-gel type hybrid organic-inorganic materials. These materials have shown promise as precursors for encapsulation and microelectronics applications. The polymers are highly crosslinked and are structurally similar to traditional sol-gels, but unlike typical sol-gels they are prepared by an organic base or Bronsted acid (formic or triflic acid), without the use of solvents and water, they have low VOC's and show little shrinkage during processing.

  2. Ammonia Sensors Based on Doped-Sol-Gel-Tipped Optical Fibers for Catalyst System Diagnostics

    Broader source: Energy.gov [DOE]

    This work focuses on the development and application of optical fibers sensors tip-coated with sol gels that sequester a transducing material whose optical response is sensitive to NH3.

  3. Environmental Assessment and Metrics for Solar: Case Study of SolFocus Solar Concentrator Systems

    E-Print Network [OSTI]

    Reich-Weiser, Corinne; Dornfeld, David; Horne, Steve

    2008-01-01

    International Journal of LCA, vol. 10, no. 1, pp. 85–94,Life-cycle assessment (LCA) is utilized to analyze SolFocussolar systems. A hybrid LCA method- ology is explained that

  4. The physics and chemistry of semiconductor nanocrystals in sol-gel derived optical microcavities

    E-Print Network [OSTI]

    Chan, Yinthai

    2006-01-01

    The incorporation of semiconductor nanocrystals (NCs) into sol-gel derived matrices presents both novel applications as well as a robust platform in which to investigate the nonlinear optical properties of NCs. This thesis ...

  5. Molecular receptors in metal oxide sol-gel materials prepared via molecular imprinting

    DOE Patents [OSTI]

    Sasaki, Darryl Y. (Albuquerque, NM); Brinker, C. Jeffrey (Albuquerque, NM); Ashley, Carol S. (Albuquerque, NM); Daitch, Charles E. (Charlottesville, VA); Shea, Kenneth J. (Irvine, CA); Rush, Daniel J. (Philadelphia, PA)

    2000-01-01

    A method is provided for molecularly imprinting the surface of a sol-gel material, by forming a solution comprised of a sol-gel material, a solvent, an imprinting molecule, and a functionalizing siloxane monomer of the form Si(OR).sub.3-n X.sub.n, wherein n is an integer between zero and three and X is a functional group capable of reacting with the imprinting molecule, evaporating the solvent, and removing the imprinting molecule to form the molecularly imprinted metal oxide sol-gel material. The use of metal oxide sol-gels allows the material porosity, pore size, density, surface area, hardness, electrostatic charge, polarity, optical density, and surface hydrophobicity to be tailored and be employed as sensors and in catalytic and separations operations.

  6. Construccion, calibracion evaluacion del sistema link de alineamiento del espectrometro de muones del experimento CMS

    E-Print Network [OSTI]

    Calderon A T

    Construccion, calibracion evaluacion del sistema link de alineamiento del espectrometro de muones del experimento CMS

  7. Solar Flare Measurements with STIX and MiSolFA

    E-Print Network [OSTI]

    Casadei, Diego

    2014-01-01

    Solar flares are the most powerful events in the solar system and the brightest sources of X-rays, often associated with emission of particles reaching the Earth and causing geomagnetic storms, giving problems to communication, airplanes and even black-outs. X-rays emitted by accelerated electrons are the most direct probe of solar flare phenomena. The Micro Solar-Flare Apparatus (MiSolFA) is a proposed compact X-ray detector which will address the two biggest issues in solar flare modeling. Dynamic range limitations prevent simultaneous spectroscopy with a single instrument of all X-ray emitting regions of a flare. In addition, most X-ray observations so far are inconsistent with the high anisotropy predicted by the models usually adopted for solar flares. Operated at the same time as the STIX instrument of the ESA Solar Orbiter mission, at the next solar maximum (2020), they will have the unique opportunity to look at the same flare from two different directions: Solar Orbiter gets very close to the Sun wit...

  8. Fast-wave Power Flow Along SOL Field Lines In NSTX nd The Associated Power Deposition Profile Across The SOL In Front Of The Antenna

    SciTech Connect (OSTI)

    Perkins, Roy

    2013-06-21

    Fast-wave heating and current drive efficiencies can be reduced by a number of processes in the vicinity of the antenna and in the scrape off layer (SOL). On NSTX from around 25% to more than 60% of the high-harmonic fast-wave power can be lost to the SOL regions, and a large part of this lost power flows along SOL magnetic field lines and is deposited in bright spirals on the divertor floor and ceiling. We show that field-line mapping matches the location of heat deposition on the lower divertor, albeit with a portion of the heat outside of the predictions. The field-line mapping can then be used to partially reconstruct the profile of lost fast-wave power at the midplane in front of the antenna, and the losses peak close to the last closed flux surface (LCFS) as well as the antenna. This profile suggests a radial standing-wave pattern formed by fast-wave propagation in the SOL, and this hypothesis will be tested on NSTX-U. Advanced RF codes must reproduce these results so that such codes can be used to understand this edge loss and to minimize RF heat deposition and erosion in the divertor region on ITER.

  9. Del Black

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HAB Packet HanfordDOEDanielDe novo Design ofDefects LeadDel Black Del

  10. Characterization of Hafnia Powder Prepared from an Oxychloride Sol Gel

    SciTech Connect (OSTI)

    McGilvery, Catriona M. [Imperial College, London; De Gendt, S [Imperial College, London; Payzant, E Andrew [ORNL; MacKenzie, M [Imperial College, London; Craven, A J [Imperial College, London; McComb, D W [Imperial College, London

    2011-01-01

    Hafnium containing compounds are of great importance to the semiconductor industry as a replacement for Si(O,N) with a high- gate dielectric. Whilst Hf is already being incorporated into working devices1, much is still to be understood about it. Here we investigate the crystallisation processes and chemistry of bulk HfO2 powders which will aid in interpretation of reactions and crystallisation events occurring in thin films used as gate dielectrics. Amorphous HfO2 powder was prepared via a sol-gel route using hafnium oxychloride (HfOCl2 xH2O) as a precursor. The powders were subjected to various heat treatments and analysed using x-ray diffraction (XRD) and thermal analysis techniques. It was found that a large change in the crystallisation pathway occurred when the sample was heated in an inert environment compared with in air. Instead of the expected monoclinic phase (m-HfO2), tetragonal HfO2 (t-HfO2) also formed under these conditions and was observed up to temperatures of ~760 C. The t-HfO2 particles, which are less than 30nm in size, eventually transform into m-HfO2 on further heating. Possible mechanisms for the crystallisation of t-HfO2 are discussed. It is proposed that within this temperature range t-HfO2 is stabilised due to the presence of oxygen vacancies in the inert environment, forming by the reduction of HfIV to HfIII. As the crystal grows in size as the temperature increases there are too few oxygen vacancies left in the structure to continue stabilising the t-HfO2 phase and so transformation to m-HfO2 occurs.

  11. Tantalum-Tungsten Oxide Thermite Composite Prepared by Sol-Gel Synthesis and Spark Plasma Sintering

    SciTech Connect (OSTI)

    Cervantes, O; Kuntz, J; Gash, A; Munir, Z

    2009-02-13

    Energetic composite powders consisting of sol-gel derived nanostructured tungsten oxide were produced with various amounts of micrometer-scale tantalum fuel metal. Such energetic composite powders were ignition tested and results show that the powders are not sensitive to friction, spark and/or impact ignition. Initial consolidation experiments, using the High Pressure Spark Plasma Sintering (HPSPS) technique, on the sol-gel derived nanostructured tungsten oxide produced samples with higher relative density than can be achieved with commercially available tungsten oxide. The sol-gel derived nanostructured tungsten oxide with immobilized tantalum fuel metal (Ta - WO{sub 3}) energetic composite was consolidated to a density of 9.17 g.cm{sup -3} or 93% relative density. In addition those parts were consolidated without significant pre-reaction of the constituents, thus the sample retained its stored chemical energy.

  12. A sol-powder coating technique for fabrication of yttria stabilised zirconia

    SciTech Connect (OSTI)

    Wattanasiriwech, Darunee . E-mail: darunee@mfu.ac.th; Wattanasiriwech, Suthee; Stevens, Ron

    2006-08-10

    Yttria stabilised zirconia has been prepared using a simple sol-powder coating technique. The polymeric yttria sol, which was prepared using 1,3 propanediol as a network modifier, was homogeneously mixed with nanocrystalline zirconia powder and it showed a dual function: as a binder which promoted densification and a phase modifier which stabilised zirconia in the tetragonal and cubic phases. Thermal analysis and X-ray diffraction revealed that the polymeric yttria sol which decomposed at low temperature into yttrium oxide could change the m {sup {yields}} t phase transformation behaviour of the zirconia, possibly due to the small particle size and very high surface area of both yttria and zirconia particles allowing rapid alloying. The sintered samples exhibited three crystalline phases: monoclinic, tetragonal and cubic, in which cubic and tetragonal are the major phases. The weight fractions of the individual phases present in the selected specimens were determined using quantitative Rietveld analysis.

  13. Catalytic Porous Ceramic Prepared In-Situ by Sol-Gelation for Butane-to-Syngas Processing

    E-Print Network [OSTI]

    Daraio, Chiara

    Catalytic Porous Ceramic Prepared In-Situ by Sol-Gelation for Butane-to-Syngas Processing­1859, 2009 Keywords: catalytic porous ceramic, butane-to-syngas processing, catalytic foam, sol-gelation, Rh containing cat- alytic Rh/ceria/zirconia nanoparticles is tested by its catalytic performance for butane

  14. Magnetic resonance as a structural probe of a uranium (VI) sol-gel process

    SciTech Connect (OSTI)

    King, C.M.; Thompson, M.C.; Buchanan, B.R. [Westinghouse Savannah River Co., Aiken, SC (United States); King, R.B. [Georgia Univ., Athens, GA (United States). Dept. of Chemistry; Garber, A.R. [South Carolina Univ., Columbia, SC (United States). Dept. of Chemistry

    1989-12-31

    NMR investigations on the ORNL process for sol-gel synthesis of microspherical nuclear fuel (UO{sub 2}), has been useful in sorting out the chemical mechanism in the sol-gel steps. {sup 13}C, {sup 15}N, and {sup 1}H NMR studies on the HMTA gelation agent (Hexamethylene tetramine, C{sub 6}H{sub l2}N{sub 4}) has revealed near quantitative stability of this adamantane-like compound in the sol-Gel process, contrary to its historical role as an ammonia source for gelation from the worldwide technical literature. {sub 17}0 NMR of uranyl (UO{sub 2}{sup ++}) hydrolysis fragments produced in colloidal sols has revealed the selective formation of a uranyl trimer, [(UO{sub 2}){sub 3}({mu}{sub 3}-O)({mu}{sub 2}-OH){sub 3}]{sup +}, induced by basic hydrolysis with the HMTA gelation agent. Spectroscopic results show that trimer condensation occurs during sol-gel processing leading to layered polyanionic hydrous uranium oxides in which HMTAH{sup +} is occluded as an ``intercalation`` cation. Subsequent sol-gel processing of microspheres by ammonia washing results in in-situ ion exchange and formation of a layered hydrous ammonium uranate with a proposed structural formula of (NH{sub 4}){sub 2}[(UO{sub 2}){sub 8}O{sub 4}(OH){sub 10}] {center_dot} 8H{sub 2}0. This compound is the precursor to sintered U0{sub 2} ceramic fuel.

  15. Magnetic resonance as a structural probe of a uranium (VI) sol-gel process

    SciTech Connect (OSTI)

    King, C.M.; Thompson, M.C.; Buchanan, B.R. (Westinghouse Savannah River Co., Aiken, SC (United States)); King, R.B. (Georgia Univ., Athens, GA (United States). Dept. of Chemistry); Garber, A.R. (South Carolina Univ., Columbia, SC (United States). Dept. of Chemistry)

    1989-01-01

    NMR investigations on the ORNL process for sol-gel synthesis of microspherical nuclear fuel (UO{sub 2}), has been useful in sorting out the chemical mechanism in the sol-gel steps. {sup 13}C, {sup 15}N, and {sup 1}H NMR studies on the HMTA gelation agent (Hexamethylene tetramine, C{sub 6}H{sub l2}N{sub 4}) has revealed near quantitative stability of this adamantane-like compound in the sol-Gel process, contrary to its historical role as an ammonia source for gelation from the worldwide technical literature. {sub 17}0 NMR of uranyl (UO{sub 2}{sup ++}) hydrolysis fragments produced in colloidal sols has revealed the selective formation of a uranyl trimer, ((UO{sub 2}){sub 3}({mu}{sub 3}-O)({mu}{sub 2}-OH){sub 3}){sup +}, induced by basic hydrolysis with the HMTA gelation agent. Spectroscopic results show that trimer condensation occurs during sol-gel processing leading to layered polyanionic hydrous uranium oxides in which HMTAH{sup +} is occluded as an intercalation'' cation. Subsequent sol-gel processing of microspheres by ammonia washing results in in-situ ion exchange and formation of a layered hydrous ammonium uranate with a proposed structural formula of (NH{sub 4}){sub 2}((UO{sub 2}){sub 8}O{sub 4}(OH){sub 10}) {center dot} 8H{sub 2}0. This compound is the precursor to sintered U0{sub 2} ceramic fuel.

  16. ELM PARTICLE AND ENERGY TRANSPORT IN THE SOL AND DIVERTOR OF DIII-D

    SciTech Connect (OSTI)

    FENSTERMACHER,ME; LEONARD,AW; SNYDER,PB; BOEDO,JA; COLCHIN,RJ; GROEBNER,RJ; GRAY,DS; GROTH,M; HOLLMANN,E; LASNIER,CJ; OSBORNE,TH; PETRIE,TW; RUDAKOV,DL; TAKAHASHI,H; WATKINS,JG; ZENG,L

    2003-04-01

    A271 ELM PARTICLE AND ENERGY TRANSPORT IN THE SOL AND DIVERTOR OF DIII-D. Results from a series of dedicated experiments measuring the effect of particle and energy pulses from Type-I Edge Localized Modes (ELMs) in the DIII-D scrape-off layer (SOL) and divertor are compared with a simple model of ELM propagation in the boundary plasma. The simple model asserts that the propagation of ELM particle and energy perturbations is dominated by ion parallel convection along SOL fields lines and the recovery from the ELM perturbation is determined by recycling physics. Time scales associated with the initial changes of boundary plasma parameters are expected to be on the order of the ion transit time from the outer midplane, where the ELM instability is initiated, to the divertor targets. To test the model, the ion convection velocity is changed in the experiment by varying the plasma density. At moderate to high density, n{sub e}/n{sub Gr} = 0.5-0.8, the delays in the response of the boundary plasma to the midplane ELM pulses, the density dependence of those delays and other observations are consistent with the model. However, at the lowest densities, n{sub e}/n{sub Gr} {approx} 0.35, small delays between the response sin the two divertors, and changes in the response of the pedestal thermal energy to ELM events, indicate that additional factors including electron conduction in the SOL, the pre-ELM condition of the divertor plasma, and the ratio of ELM instability duration to SOL transit time, may be playing a role. The results show that understanding the response of the SOL and divertor plasmas to ELMs, for various pre-ELM conditions, is just as important to predicting the effect of ELM pulses on the target surfaces of future devices as is predicting the characteristics of the ELM perturbation of the core plasma.

  17. Sol-gel silica films embedding NIR- emitting Yb-quinolinolate complexes

    SciTech Connect (OSTI)

    Figus, Cristiana, E-mail: cristiana.figus@dsf.unica.it; Quochi, Francesco, E-mail: cristiana.figus@dsf.unica.it; Piana, Giacomo; Saba, Michele; Mura, Andrea; Bongiovanni, Giovanni [Dipartimento di Fisica, University of Cagliari, SS 554 Bivio per Sestu, I-09042, Monserrato-Cagliari (Italy); Artizzu, Flavia [Dipartimento di Fisica, University of Cagliari and Dipartimento di Scienze Chimiche e Geologiche, University of Cagliari, SS 554 Bivio per Sestu, I-09042, Monserrato-Cagliari (Italy); Mercuri, Maria Laura; Serpe, Angela; Deplano, Paola [Dipartimento di Scienze Chimiche e Geologiche, University of Cagliari, SS 554 Bivio per Sestu, I-09042, Monserrato-Cagliari (Italy)

    2014-10-21

    Sol-gel silica thin films embedding an ytterbium quinolinolato complex (YbClQ{sub 4}) have been obtained using different alkoxides. Homogeneous, crack- and defect-free thin films of optical quality have been successfully deposited on glass substrate by dip-coating. The silica thin films have been characterized by time-resolved photoluminescence. The luminescence properties of the YbClQ{sub 4} are preserved in silica films prepared through an optimized sol-gel approach. The excited state lifetime of the lanthanide is comparable to those observed in bulk and longer than the corresponding ones in solution.

  18. Sol immobilization technique: a delicate balance between activity, selectivity and stability for gold catalyst

    SciTech Connect (OSTI)

    Villa, Alberto [Universita di Milano, Italy] [Universita di Milano, Italy; Wang, Di [Fritz Haber Institute of the Max Planck Society, Berlin, Germany] [Fritz Haber Institute of the Max Planck Society, Berlin, Germany; Veith, Gabriel M [ORNL] [ORNL; Prati, Laura [Universita di Milano, Italy] [Universita di Milano, Italy

    2013-01-01

    Sol immobilization is a widely used method to prepare gold catalysts. The presence of the protective layer can have a significant influence on catalyst properties by mediating metal-support and reactantmetal interactions. This paper details the effect of a polyvinyl alcohol (PVA) protecting groups on the activity of a supported gold catalysts as well as its selectivity towards glycerol oxidation.

  19. Nanoindentation and adhesion of sol-gel-derived hard coatings on polyester

    E-Print Network [OSTI]

    Cao, Guozhong

    Nanoindentation and adhesion of sol-gel-derived hard coatings on polyester C.M. Chan, G.Z. Cao,a) H coatings on modified polyester substrates. The silica network was modified by incorporating an organic, and mechanical properties of the coatings. Various low-temperature densification techniques were studied

  20. FEATURE ARTICLE Growth of Oxide Nanorod Arrays through Sol Electrophoretic Deposition

    E-Print Network [OSTI]

    Cao, Guozhong

    approaches in sol-gel processing for synthesis of inorganic or inorganic/organic hybrid materials are briefly* Department of Materials Science and Engineering, UniVersity of Washington, Seattle, Washington 98195 Recei, are impor- tant materials for various applications in industry and technol- ogy. This is due to their multi

  1. Multivariate Population Balances via Moment and Monte Carlo Simulation Methods: An Important Sol Reaction Engineering

    E-Print Network [OSTI]

    Multivariate Population Balances via Moment and Monte Carlo Simulation Methods: An Important Sol application of current/future importance, a multivariate description is required, for which the existing, hopefully, motivate a broader attack on important multivariate population balance problems, including those

  2. Europhysics Letters PREPRINT Layering transitions for adsorbing polymers in poor sol-

    E-Print Network [OSTI]

    Rechnitzer, Andrew

    Europhysics Letters PREPRINT Layering transitions for adsorbing polymers in poor sol- vents J, Potts, etc.). PACS. 05.70.fh ­ Thermodynamics. PACS. 61.41.+e ­ Polymers, elastomers, and plastics. Abstract. ­ An infinite hierarchy of layering transitions exists for model polymers in solu- tion under

  3. Investigations of the small-scale thermal behavior of sol-gel thermites.

    SciTech Connect (OSTI)

    Warren, Mial E.; Farrow, Matthew; Tappan, Alexander Smith

    2009-02-01

    Sol-gel thermites, formulated from nanoporous oxides and dispersed fuel particles, may provide materials useful for small-scale, intense thermal sources, but understanding the factors affecting performance is critical prior to use. Work was conducted on understanding the synthesis conditions, thermal treatments, and additives that lead to different performance characteristics in iron oxide sol-gel thermites. Additionally, the safety properties of sol-gel thermites were investigated, especially those related to air sensitivity. Sol-gel thermites were synthesized using a variety of different techniques and there appear to be many viable routes to relatively equivalent thermites. These thermites were subjected to several different thermal treatments under argon in a differential scanning calorimeter, and it was shown that a 65 C hold for up to 200 minutes was effective for the removal of residual solvent, thus preventing boiling during the final thermal activation step. Vacuum-drying prior to this heating was shown to be even more effective at removing residual solvent. The addition of aluminum and molybdenum trioxide (MoO{sub 3}) reduced the total heat release per unit mass upon exposure to air, probably due to a decrease in the amount of reduced iron oxide species in the thermite. For the thermal activation step of heat treatment, three different temperatures were investigated. Thermal activation at 200 C resulted in increased ignition sensitivity over thermal activation at 232 C, and thermal activation at 300 C resulted in non-ignitable material. Non-sol-gel iron oxide did not exhibit any of the air-sensitivity observed in sol-gel iron oxide. In the DSC experiments, no bulk ignition of sol-gel thermites was observed upon exposure to air after thermal activation in argon; however ignition did occur when the material was heated in air after thermal treatment. In larger-scale experiments, up to a few hundred milligrams, no ignition was observed upon exposure to air after thermal activation in vacuum; however ignition by resistively-heated tungsten wire was possible. Thin films of thermite were fabricated using a dispersed mixture of aluminum and iron oxide particles, but ignition and propagation of these films was difficult. The only ignition and propagation observed was in a preheated sample.

  4. Transparent ultralow-density silica aerogels prepared by a two-step sol-gel process

    SciTech Connect (OSTI)

    Tillotson, T.M.; Hrubesh, L.W.

    1991-09-01

    Conventional silica sol-gel chemistry is limited for the production of transparent ultralow-density aerogels because (1) gelation is either slow or unachievable, and (2) even when gelation is achieved, the large pore sizes result in loss of transparency for aerogels <.020 g/cc. We have developed a two-step sol-gel process that circumvents the limitations of the conventional process and allows the formation of ultralow-density gels in a matter of hours. we have found that the gel time is dependent on the catalyst concentration. After supercritical extraction, the aerogels are transparent, uncracked tiles with densities as low as .003 g/cc. 6 figs., 11 refs.

  5. Moisture sensor based on evanescent wave light scattering by porous sol-gel silica coating

    DOE Patents [OSTI]

    Tao, Shiquan; Singh, Jagdish P.; Winstead, Christopher B.

    2006-05-02

    An optical fiber moisture sensor that can be used to sense moisture present in gas phase in a wide range of concentrations is provided, as well techniques for making the same. The present invention includes a method that utilizes the light scattering phenomenon which occurs in a porous sol-gel silica by coating an optical fiber core with such silica. Thus, a porous sol-gel silica polymer coated on an optical fiber core forms the transducer of an optical fiber moisture sensor according to an embodiment. The resulting optical fiber sensor of the present invention can be used in various applications, including to sense moisture content in indoor/outdoor air, soil, concrete, and low/high temperature gas streams.

  6. Energy efficiency dynamometer testing at the 1996 American Tour de Sol

    SciTech Connect (OSTI)

    Sluder, S.; Duoba, M.; Buitrago, C.; Leblanc, N.; Larsen, R.

    1996-08-01

    In 1995, the U.S. Department of Energy through Argonne National Laboratory`s Center for Transportation Research sponsored energy efficiency data collection from the student, private, and professional vehicles during the American Tour de Sol. The American Tour de Sol is a multiple-day road rally event run from New York City to Washington, D.C. As part of this efficiency testing, a number of vehicles were tested on a chassis dynamometer utilizing three common drive cycles: the LA-4, the New York City Cycle, and the Highway Fuel Economy Test. The results demonstrate remarkable efficiency increases over a gasoline control vehicle and significant cycle-sensitivity information. Two series hybrid electric vehicles (HEVs) were shown to have fuel efficiencies which were less sensitive to drive cycle than either a gasoline or an electric vehicle.

  7. Characterization of Sol-gel Encapsulated Proteins using Small-angle Neutron Scattering

    SciTech Connect (OSTI)

    Luo, Guangming [ORNL; Zhang, Qiu [ORNL; Del Castillo, Alexis Rae [ORNL; Urban, Volker S [ORNL; O'Neill, Hugh Michael [ORNL

    2009-01-01

    Entrapment of biomolecules in silica-derived sol-gels has grown into a vibrant area of research since it was originally demonstrated. However, accessing the consequences of entrapment on biomolecules and the gel structure remains a major challenge in characterizing these biohybrid materials. We present the first demonstration that it is possible with small-angle neutron scattering (SANS) to study the conformation of dilute proteins that are entrapped in transparent and dense sol-gels. Using deuterium-labeled green fluorescent protein (GFP) and SANS with contrast variation, we demonstrate that the scattering signatures of the sol-gel and the protein can be separated. Analysis of the scattering curves of the sol-gels using a mass-fractal model shows that the size of the colloidal silica particles and the fractal dimensions of the gels were similar in the absence and presence of protein, demonstrating that GFP did not influence the reaction pathway for the formation of the gel. The major structural difference in the gels was that the pore size was increased 2-fold in the presence of the protein. At the contrast match point for silica, the scattering signal from GFP inside the gel became distinguishable over a wide q range. Simulated scattering curves representing a monomer, end-to-end dimer, and parallel dimer of the protein were calculated and compared to the experimental data. Our results show that the most likely structure of GFP is that of an end-to-end dimer. This approach can be readily applied and holds great potential for the structural characterization of complex biohybrid and other materials.

  8. 2005 Tour de Sol: The Sustainable Energy and Transportation Festival and Competition

    SciTech Connect (OSTI)

    Nancy Hazard

    2005-05-07

    This report gives a summary of the 2005Tour de Sol: The Sustainable Energy and Transportation Festival and Competition. It lists our objectives, what we did, and an analysis of how we met our objectives. An 80-page report with a list of verified print, radio and TV media coverage, and copies of selected news clips and web media coverage is available at the NESEA office for review.

  9. Synthesis of Sol-Gel Matrices for Encapsulation of Enzymes Using an Aqueous Route

    SciTech Connect (OSTI)

    Ashley, C.S.; Bhatia, R.B.; Brinker, C.J.; Harris, T.M.

    1998-11-23

    Sol-gel matrices are promising host materials for potential chemical and biosensor applications. Previous studies have focused on modified sol-gel routes using alkoxides for encapsulation of enzymes. However the formation of alcohol as a byproduct during hydrolysis and condensation reactions poses limitations. We report the immobilization of glucose oxidase and peroxidase in silica prepared by an aqueous route which may provide a more favorable environment for the biomolecules. A two step aqueous sol-gel procedure using sodium silicate as the precursor was developed to encapsulate the enzymes and the dye precursor, o-dianisidine. Glucose oxidase catalyzes the oxidation of glucose to give gluconic acid and hydrogen peroxide. Peroxidase then catalyzes the reaction of the dye precursor with hydrogen peroxide to produce a colored product. The kinetics of the coupled enzymatic reactions were monitored by optical spectroscopy and compared to those occurring in tetramethyl orthosilicate (TMOS) derived silica matrices developed by Yamanaka. Enhanced kinetics in the aqueous silicate matrices were related to differences in the host microstructure as elucidated by microstructural comparisons of the corresponding aerogels.

  10. modelado y analisis del transporte del herbicida glifosato

    E-Print Network [OSTI]

    2001-03-12

    ecuaciones diferenciales acopladas que describen el movimiento del agua y del .... Para calcular los parámetros de la curva de retención del modelo de van ...

  11. Electrophoretically active sol-gel processes to backfill, seal, and/or densify porous, flawed, and/or cracked coatings on electrically conductive material

    DOE Patents [OSTI]

    Panitz, Janda K. (Sandia Park, NM); Reed, Scott T. (Albuquerque, NM); Ashley, Carol S. (Albuquerque, NM); Neiser, Richard A. (Albuquerque, NM); Moffatt, William C. (Albuquerque, NM)

    1999-01-01

    Electrophoretically active sol-gel processes to fill, seal, and/or density porous, flawed, and/or cracked coatings on electrically conductive substrates. Such coatings may be dielectrics, ceramics, or semiconductors and, by the present invention, may have deposited onto and into them sol-gel ceramic precursor compounds which are subsequently converted to sol-gel ceramics to yield composite materials with various tailored properties.

  12. Electrophoretically active sol-gel processes to backfill, seal, and/or densify porous, flawed, and/or cracked coatings on electrically conductive material

    DOE Patents [OSTI]

    Panitz, J.K.; Reed, S.T.; Ashley, C.S.; Neiser, R.A.; Moffatt, W.C.

    1999-07-20

    Electrophoretically active sol-gel processes to fill, seal, and/or density porous, flawed, and/or cracked coatings on electrically conductive substrates. Such coatings may be dielectrics, ceramics, or semiconductors and, by the present invention, may have deposited onto and into them sol-gel ceramic precursor compounds which are subsequently converted to sol-gel ceramics to yield composite materials with various tailored properties. 6 figs.

  13. Multi-machine Comparisons of H-mode Separatrix Densities and Edge Profile Behaviour in the ITPA SOL and Divertor Physics Topical Group

    E-Print Network [OSTI]

    Multi-machine Comparisons of H-mode Separatrix Densities and Edge Profile Behaviour in the ITPA SOL and Divertor Physics Topical Group

  14. Integrated Core-SOL-Divertor Modelling for ITER Including Impurity: Effect of Tungsten on Fusion Performance in H-mode and Hybrid Scenario

    E-Print Network [OSTI]

    Integrated Core-SOL-Divertor Modelling for ITER Including Impurity: Effect of Tungsten on Fusion Performance in H-mode and Hybrid Scenario

  15. Crónica del simulacro: "Los rituales del caos" de Carlos Monsiváis

    E-Print Network [OSTI]

    González Márquez, Andrea

    2012-01-01

    ofrece al parecer de ambos como una estrategia rentable delmercado, la estrategia del caos o del escándalo, garantía

  16. Omnipresencia del paralelismo Objetivos del proyecto

    E-Print Network [OSTI]

    Giménez, Domingo

    -Secundaria Incorporaci´on de contenidos de programaci´on paralela en la rama de tecnolog´ias inform´aticas Facultad;Omnipresencia del paralelismo Objetivos del proyecto Material a desarrollar Programaci´on paralela Para explotar componentes computacionales, para lo que se utiliza la programaci´on paralela. Tipos b´asicos: Dentro de un

  17. Role of uranium(VI) in the ThO/sub 2/-UO/sub 3/ sol-gel process

    SciTech Connect (OSTI)

    Tewari, P.H.; Campbell, A.B.

    1980-11-01

    Increases in pH and temperature of U(VI) solutions enhance adsorption of uranium on ThO/sub 2/ through hydrolysis of U(VI) as evidenced by absorption spectra changes of the solution. Sols of ThO/sub 2/-UO/sub 3/ are formed by adsorption of uranium on ThO/sub 2/. At low pH's (approx. pH 3.0), the sols behave as Newtonian fluids but at higher pH's the sols (especially the concentrated ones) transform into thixotropic gels. The increased adsorption of uranium by ThO/sub 2/ and the increased viscosity of the ThO/sub 2/-UO/sub 3/ sols with pH are related. Increased adsorption of uranium produces rod-shaped UO/sub 3/.2H/sub 2/O on the ThO/sub 2/ surface. These UO/sub 3/ nuclei link ThO/sub 2/ particles to form long rodlike particles. With further increased adsorption of uranium at higher pH's (less than or equal to 3.7), the particles crosslink to produce a structured network giving a thixotropic gel. Adsorption, electron microscopic, electrophoetic mobility, X-ray diffraction, and X-ray photoelectron spectroscopic data are presented to explain the role of U(VI) in the sol-gel process. 6 figures, 1 table.

  18. Setembre del 2012 Qualitat, innovaci,

    E-Print Network [OSTI]

    Verschure, Paul

    Campus del Mar: ciències de la salut i de la vida Campus del Poblenou: comunicació i tecnologies de la

  19. Dielectric function of sol-gel prepared nano-granular zinc oxide by spectroscopic ellipsometry

    SciTech Connect (OSTI)

    Gilliot, Mickaël, E-mail: mickael.gilliot@univ-reims.fr; Hadjadj, Aomar [LISM, Université de Reims Champagne-Ardenne, Reims (France); Eypert, Céline [HORIBA Jobin Yvon S.A.S., Palaiseau (France)

    2013-11-14

    ZnO thin films have been prepared by sol gel and deposited by spin coating. The dielectric function has been determined by spectroscopic ellipsometry. Ellipsometric spectra are inverted by a direct numerical method without using the standard fitting procedures. The obtained dielectric function presents a broad excitonic effect. The dielectric function is studied using Elliot excitonic theory including exciton plus band-to-band Coulomb interactions with standard Lorentzian broadening. A modification of this model dielectric function with independent bound and unbound exciton contributions is empirically proposed to improve modelling of the band gap excitonic peak.

  20. Electroanalytical applications of screen-printable surfactant-induced sol-gel graphite composites

    DOE Patents [OSTI]

    Guadalupe, Ana R. (San Juan, PR); Guo, Yizhu (San Juan, PR)

    2001-05-15

    A process for preparing sol-gel graphite composite electrodes is presented. This process preferably uses the surfactant bis(2-ethylhexyl) sulfosuccinate (AOT) and eliminates the need for a cosolvent, an acidic catalyst, a cellulose binder and a thermal curing step from prior art processes. Fabrication of screen-printed electrodes by this process provides a simple approach for electroanalytical applications in aqueous and nonaqueous solvents. Examples of applications for such composite electrodes produced from this process include biochemical sensors such as disposable, single-use glucose sensors and ligand modified composite sensors for metal ion sensitive sensors.

  1. Performance of electric and hybrid vehicles at the 1995 American Tour de Sol

    SciTech Connect (OSTI)

    Quong, S.; LeBlanc, N.; Buitrago, C.; Duoba, M.; Larsen, R.

    1995-12-31

    Energy consumption and performance data were collected on more than 40 electric and hybrid vehicles during the 1995 American Tour de Sol. At this competition, one electric vehicle drove 229 miles on one charge using nickel metalhydride batteries. The results obtained from the data show that electric vehicle efficiencies reached 9.07 mi./kWh or 70 equivalent mpg of gasoline when compared to the total energy cycle efficiency of electricity and gasoline. A gasoline-fueled 1995 Geo Metro that drove the same route attained 36.4 mpg.

  2. Direct formation of aerogels by sol-gel polymerizations of alkoxysilanes in supercritical carbon dioxide

    SciTech Connect (OSTI)

    Loy, D.A.; Yamanaka, A.; Carpenter, J.P. [Sandia National Labs., Albuquerque, NM (United States); [Univ. of California, Irvine, CA (United States)] [and others

    1997-12-31

    Sol-gel polymerization of alkoxysilanes in supercritical carbon dioxide (SCCD) was used to directly prepare aerogels. Polymerizations of tetramethoxysilane (TMOS) and 1,4-bis(triethoxysilyl)benzene (BESP) were performed by dissolving the monomers and formic acid in supercritical carbon dioxide (SCCD). Monolithic gels were obtained in under 12 hours. The silica and polysilsesquioxane gels were readily dried to afford aerogels by slowly venting the SCCD. The aerogels were high surface area mesoporous materials that were characterized by solid state NMR, SEM, TEM, and gas sorption porosimetry.

  3. Journal of Sol-Gel Science and Technology 36, 183195, 2005 c 2005 Springer Science + Business Media, Inc. Manufactured in the United States.

    E-Print Network [OSTI]

    Cao, Guozhong

    of the electrical double-layer surrounding a particle in a colloidal suspension that is responsible for the electrostatic stabilization of a colloid (left), and the electrophoretic motion and process involved in template an electric field to an electrostatically stabilized sol. Nanoclus- ters dispersed in such a sol would develop

  4. Synthesis of palladium-doped silica nanofibers by sol-gel reaction and electrospinning process

    SciTech Connect (OSTI)

    San, Thiam Hui; Daud, Wan Ramli Wan; Kadhum, Abdul Amir Hassan; Mohamad, Abu Bakar; Kamarudin, Siti Kartom; Shyuan, Loh Kee; Majlan, Edy Herianto [Fuel Cell Institute, Universiti Kebangsaan Malaysia, 43600 UKM Bangi, Selangor (Malaysia); Fuel Cell Institute, Universiti Kebangsaan Malaysia, 43600 UKM Bangi, Selangor, Malaysia and Department of Chemical and Process Engineering, Universiti Kebangsaan Malaysia, 43600 UKM Bangi, Selangor (Malaysia); Fuel Cell Institute, Universiti Kebangsaan Malaysia, 43600 UKM Bangi, Selangor (Malaysia)

    2012-06-29

    Nanofiber is drawing great attention nowadays with their high surface area per volume and flexibility in surface functionalities that make them favorable as a proton exchange membrane in fuel cell application. In this study, incorporation of palladium nanoparticles in silica nanofibers was prepared by combination of a tetraorthosilane (TEOS) sol-gel reaction with electrospinning process. This method can prevent the nanoparticles from aggregation by direct mixing of palladium nanoparticles in silica sol. The as-produced electrospun fibers were thermally treated to remove poly(vinyl pyrrolidone) (PVP) and condensation of silanol in silica framework. PVP is chosen as fiber shaping agent because of its insulting and capping properties for various metal nanoparticles. Scanning electron microscopy (SEM), energy dispersive spectrometer (EDS) and Fourier transform infrared spectroscopy (FTIR) were used to characterize the silica fibers and Pd nanoparticles on the fibers. Spun fibers with average diameter ranged from 100nm to 400nm were obtained at optimum operating condition and distribution of Pd nanoparticles on silica fibers was investigated.

  5. Simulation of tokamak SOL and divertor region including heat flux mitigation by gas puffing

    SciTech Connect (OSTI)

    Park, Jin Woo [Seoul National University, Seoul, S. Korea; Na, Y. S. [Seoul National University, Seoul, S. Korea; Hong, S. H. [National Fusion Research Institute, Daejon, South Korea; Ahn, J.W. [Oak Ridge National Laboratory (ORNL); Kim, D. K. [Agency Def Dev, Taejon, South Korea; Han, Hyunsun [National Fusion Research Institute, Taejon, South Korea; Shim, Seong Bo [Pusan National University, Busan, Korea; Lee, Hae June [Pusan National University, Busan, Korea

    2012-01-01

    Two-dimensional (2D), scrape-off layer (SOL)-divertor transport simulations are performed using the integrated plasma-neutral-impurity code KTRAN developed at Seoul National University. Firstly, the code is applied to reproduce a National Spherical Torus eXperiment (NSTX) discharge by using the prescribed transport coefficients and the boundary conditions obtained from the experiment. The plasma density, the heat flux on the divertor plate, and the D (alpha) emission rate profiles from the numerical simulation are found to follow experimental trends qualitatively. Secondly, predictive simulations are carried out for the baseline operation mode in Korea Superconducting Tokamak Advanced Research (KSTAR) to predict the heat flux on the divertor target plates. The stationary peak heat flux in the KSTAR baseline operation mode is expected to be 6.5 MW/m(2) in the case of an orthogonal divertor. To study the mitigation of the heat flux, we investigated the puffing effects of deuterium and argon gases. The puffing position is assumed to be in front of the strike point at the outer lower divertor plate. In the simulations, mitigation of the peak heat flux at the divertor target plates is found to occur when the gas puffing rate exceeds certain values, similar to 1.0 x 10(20) /s and similar to 5.0 x 10(18) /s for deuterium and argon, respectively. Multi-charged impurity transport is also investigated for both NSTX and KSTAR SOL and divertor regions.

  6. Thio sol-gel process for the synthesis of titanium disulfide

    SciTech Connect (OSTI)

    Sriram, M.A.; Kumta, P.N. (Carnegie Mellon Univ., Pittsburgh, PA (United States). Dept. of Materials Science and Engineering)

    1994-05-01

    Sulfides of transition metals (titanium, molybdenum, vanadium, tungsten, etc.) represent an important class of materials well-known for their catalytic and electrochemical properties. The catalytic properties make them potentially useful in hydrodesulfurization reactions, and their electrochemical response makes them suitable as active cathodes in rechargeable batteries. A thio sol-gel process for the synthesis of titanium disulfide using titanium alkoxide as the metal source is demonstrated. The alkoxide reacts at room temperature with H[sub 2]S to form a precipitate which is a precursor to the sulfide. Through infrared spectroscopy and chemical analysis of the powder and gas chromatographic analysis of the liquid byproducts of the reaction, it is shown that a partially sulfidized alkoxide precursor forms through the displacement of alkoxy groups from the alkoxide by sulfur-bearing thiol groups. This thiolysis reaction is very similar to that which occurs in the case of sol-gel reactions to form oxides. The alkoxy-thiol species then undergo condensation-polymerization by the liberation of H[sub 2]S. When it is heat-treated in H[sub 2]S, this precursor transforms to TiS[sub 2] at [approximately]700 C. Systematic heat treatments have been performed and the formation of TiS[sub 2] has been observed using X-ray diffractometry. The change in the morphology has also been studied using scanning electron microscopy.

  7. Dialkylenecarbonate-Bridged Polysilsesquioxanes. Hybrid Organic Sol-Gels with a Thermally Labile Bridging Group

    SciTech Connect (OSTI)

    Loy, D.A.; Beach, J.V.; Baugher, B.M.; Assink, R.A.; Shea, K.J.; Tran, J.; Small, J.H.

    1999-04-21

    In this paper, we introduce a new approach for altering the properties of bridged polysilsesquioxane xerogels using post-processing modification of the polymeric network. The bridging organic group contains latent functionalities that can be liberated thermally, photochemically, or by chemical means after the gel has been processed to a xerogel. These modifications can produce changes in density, volubility, porosity, and or chemical properties of the material. Since every monomer possesses two latent functional groups, the technique allows for the introduction of high levels of functionality in hybrid organic-inorganic materials. Dialkylenecarbonate-bridged polysilsesquioxane gels were prepared by the sol-gel polymerization of bis(triethoxysilylpropyl)carbonate (1) and bis(triethoxysilylisobutyl)-carbonate (2). Thermal treatment of the resulting non-porous xerogels and aerogels at 300-350 C resulted in quantitative decarboxylation of the dialkylenecarbonate bridging groups to give new hydroxyalkyl and olefinic substituted polysilsesquioxane monolithic xerogels and aerogels that can not be directly prepared through direct sol-gel polymerization of organotrialkoxysilanes.

  8. Communications mensuelles de l'lnstitut International dela Potasse, Berne (Suisse) Science du sol N 5/1981

    E-Print Network [OSTI]

    Sparks, Donald L.

    Communications mensuelles de l'lnstitut International dela Potasse, Berne (Suisse) Section 4 of potassium in sandy soils) D.l.Sparks Professeur-adjoint de chimie-physique du sol, dc!ipartement des publications suivantes: Sparks D.L., Martens D.C., Zelazny L. W.: Plant Uptake and Leaching of applied

  9. PICARD SOL, a new ground-based facility for long-term solar radius measurements: first results

    E-Print Network [OSTI]

    Boyer, Edmond

    PICARD SOL, a new ground-based facility for long-term solar radius measurements: first results M solar radius measured in space and on ground and to better understand and calibrate atmospheric effects observations and corrections for atmospheric refraction, first estimates of the mean solar radius at the five

  10. Dense and optical transparent CdWO4 films by sol-gel processing for scintillation applications

    E-Print Network [OSTI]

    Cao, Guozhong

    using tungstic acid and cadmium nitrate as precursors and hydrogen peroxide as solvent; homogeneous fabrication of dense and optically transparent cadmium tungstate (CWO) films by sol-gel processing, nanostructures, and optical and x-ray scintillation properties are discussed in detail. I. INTRODUCTION Cadmium

  11. Synthesis of Mixed Ceramic MgxZn1-xO Nanofibers via Mg2+ Using Sol-Gel Electrospinning

    E-Print Network [OSTI]

    Khan, Saad A.

    Synthesis of Mixed Ceramic MgxZn1-xO Nanofibers via Mg2+ Doping Using Sol-Gel Electrospinning Yakup the fibers and conversion of ceramic precursors into ceramic nanofibers, and the appearance of a range property, morphology, and porosity of the resulting nonwoven mat. Ceramic electrospun nanofibers

  12. JOURNAL OF MATERIALS SCIENCE LETTERS 21, 2002, 251 255 Organic-inorganic sol-gel coating for corrosion protection

    E-Print Network [OSTI]

    Cao, Guozhong

    JOURNAL OF MATERIALS SCIENCE LETTERS 21, 2002, 251­ 255 Organic-inorganic sol-gel coating or coatings. Through the modification of chemical composition of the coatings, such protec- tive coatings can strength and hydrophobicity. Various organic coatings have been studied for corrosion protection [4

  13. High surface area neodymium phosphate nano particles by modified aqueous sol-gel method

    SciTech Connect (OSTI)

    Sankar, Sasidharan [Materials Division, National Institute for Interdisciplinary Science and Technology, Council of Scientific and Industrial Research, Thiruvananthapuram 695 019, Kerala (India)] [Materials Division, National Institute for Interdisciplinary Science and Technology, Council of Scientific and Industrial Research, Thiruvananthapuram 695 019, Kerala (India); Warrier, Krishna Gopakumar, E-mail: wwarrierkgk@yahoo.co.in [Materials Division, National Institute for Interdisciplinary Science and Technology, Council of Scientific and Industrial Research, Thiruvananthapuram 695 019, Kerala (India); Komban, Rajesh [Institut fuer Chemie, Anorganische Chemie 1, Universitaet Osnabrueck, Barbarastrasse 7, 49069 Osnabrueck (Germany)] [Institut fuer Chemie, Anorganische Chemie 1, Universitaet Osnabrueck, Barbarastrasse 7, 49069 Osnabrueck (Germany)

    2011-12-15

    Graphical abstract: Synthesis of nano rod shaped neodymium phosphate particles with specific surface area as high as 107 m{sup 2} g{sup -1} and particles could be compacted and sintered at as low as 1300 Degree-Sign C to a density of 98.5% (theoretical) with an average grain size of {approx}1 {mu}m. Highlights: Black-Right-Pointing-Pointer Nano size neodymium phosphate is synthesized and characterized using a novel modified aqueous sol gel process. Black-Right-Pointing-Pointer Specific surface area above 100 m{sup 2} g{sup -1} achieved without the addition of any complexing agents. Black-Right-Pointing-Pointer High sintered density reported than the density obtained for powder synthesized through conventional solid state reaction. Black-Right-Pointing-Pointer The particles are nano sized and have rod shape morphology and are retained at higher temperatures. Black-Right-Pointing-Pointer An average grain size of {approx}1 {mu}m obtained for sintered NdPO{sub 4} after thermal etching at 1400 Degree-Sign C. -- Abstract: Synthesis of nano rod shaped neodymium phosphate (NdPO{sub 4}) particles with specific surface area as high as 107 m{sup 2}g{sup -1} and an average length of 50 nm with aspect ratio 5 was achieved using modified sol gel method. Crystallite size calculated from the X-ray diffraction data by applying Scherer equation was 5 nm for the precursor gel after calcination at 400 Degree-Sign C. NdPO{sub 4} was first precipitated from neodymium nitrate solution using phosphoric acid followed by peptization using dilute nitric acid and further gelation in ammonia atmosphere. The calcined gel powders were further characterized by surface area (Brunauer-Emmet-Teller nitrogen adsorption analysis), Transmission electron microscopy, scanning electron microscopy, UV-vis and FT-IR analysis. Transmission electron microscopy confirms the formation of rod like morphology from the sol, gel and the calcined particles in nano size range. These particles could be compacted and sintered at as low as 1300 Degree-Sign C to a density of 98.5% (theoretical) with an average grain size of {approx}1 {mu}m.

  14. Sol-gel synthesis and characterization of tetra-alkoxysilane and bridged-polysilsesquioxane materials in non-polar solvents

    SciTech Connect (OSTI)

    Yamanaka, S.A.; Martino, A.; Kawola, J.S.; Loy, D.A. [Sandia National Laboratories, Albuquerque, NM (United States)

    1996-10-01

    Although the sol-gel method has widely been used for the encapsulation of molecules in porous glass materials, the variety of dopants has been limited by the solvents used in processing. Polar solvents, such as ethanol, methanol or tetrahydrofuran, are typically added as cosolvents to prevent phase separation between the organic metal alkoxide and water. Non-polar solvents are generally not suitable for sol-gel processing since they are immicible with the aqueous phase. Our study increases the availability of solvents that may be used in sol-gel processing and therefore expands the range of molecules suitable for encapsulation. Here, we report a novel method for preparing both silica sol-gel materials and bridged-polysilsesquioxane materials in a non-polar, hydrocarbon solvent. The method involves the formation of an inverse micelle upon addition of the surfactant, didodecyldimethylammonium bromide, to toluene. The dynamic nature of the micelle allows sol-gel reactions to occur between water (soluble in the polar core of the micelle) and the metal alkoxide precursor (soluble in the solvent phase). Materials prepared by this technique have been characterized by nitrogen sorption porosimetry, SEM, solid state {sup 29}Si NMR, TGA and XRD. Photochemical conversion of technetium fluorides and oxyfluorides is largely uninvestigated. Because technetium was introduced into U.S. uranium enrichment plants, decommissioning and decontamination of these plants will involve technetium fluorides and oxyfluorides. Photochemical conversion of such compounds may facilitate waste minimization and cost avoidance goals during plant clean-up. Photochemical fluorination using ultraviolet photolysis of a mixture of fluorine and oxygen gases is an effective means of converting solid, nonvolatile fluorides of fight actinides, such as U, Np, and Pu, into volatile hexafluorides thereby removing surface radioactive contamination.

  15. Organic aerogels from the sol-gel polymerization of phenolic-furfural mixtures

    DOE Patents [OSTI]

    Pekala, R.W.

    1995-12-19

    The sol-gel polymerization of a phenolic-furfural mixture in dilute solution leads to a highly cross-linked network that can be supercritically dried to form a high surface area foam. These porous materials have cell/pore sizes{<=}1000{angstrom}, and although they are dark brown in color, they can be classified as a new type of aerogel. The phenolic-furfural aerogel can be pyrolyzed in an inert atmosphere at 1050 C to produce carbon aerogels. This new aerogel may be used for thermal insulation, chromatographic packing, water filtration, ion-exchange, and carbon electrodes for energy storage devices, such as batteries and double-layer capacitors. 8 figs.

  16. Organic aerogels from the sol-gel polymerization of phenolic-furfural mixtures

    DOE Patents [OSTI]

    Pekala, Richard W. (Pleasant Hill, CA)

    1995-01-01

    The sol-gel polymerization of a phenolic-furfural mixture in dilute solution leads to a highly cross-linked network that can be supercritically dried to form a high surface area foam. These porous materials have cell/pore sizes.ltoreq.1000.ANG., and although they are dark brown in color, they can be classified as a new type of aerogel. The phenolic-furfural aerogel can be pyrolyzed in an inert atmosphere at 1050.degree. C. to produce carbon aerogels. This new aerogel may be used for thermal insulation, chromatographic packing, water filtration, ion-exchange, and carbon electrodes for energy storage devices, such as batteries and double-layer capacitors.

  17. Organic carbon aerogels from the sol-gel polymerization of phenolic-furfural mixtures

    SciTech Connect (OSTI)

    Pekala, Richard W. (Pleasant Hill, CA)

    1998-04-28

    The sol-gel polymerization of a phenolic-furfural mixture in dilute solution leads to a highly cross-linked network that can be supercritically dried to form a high surface area foam. These porous materials have cell/pore sizes .ltoreq.1000 .ANG., and although they are dark brown in color, they can be classified as a new type of aerogel. The phenolic-furfural aerogel can be pyrolyzed in an inert atmosphere at 1050.degree. C. to produce carbon aerogels. This new aerogel may be used for thermal insulation, chromatographic packing, water filtration, ion-exchange, and carbon electrodes for energy storage devices, such as batteries and double-layer capacitors.

  18. Organic carbon aerogels from the sol-gel polymerization of phenolic-furfural mixtures

    DOE Patents [OSTI]

    Pekala, R.W.

    1998-04-28

    The sol-gel polymerization of a phenolic-furfural mixture in dilute solution leads to a highly cross-linked network that can be supercritically dried to form a high surface area foam. These porous materials have cell/pore sizes {<=}1000 {angstrom}, and although they are dark brown in color, they can be classified as a new type of aerogel. The phenolic-furfural aerogel can be pyrolyzed in an inert atmosphere at 1050 C to produce carbon aerogels. This new aerogel may be used for thermal insulation, chromatographic packing, water filtration, ion-exchange, and carbon electrodes for energy storage devices, such as batteries and double-layer capacitors. 8 figs.

  19. Organic aerogels from the sol-gel polymerization of phenolic-furfural mixtures

    DOE Patents [OSTI]

    Pekala, R.W.

    1996-09-17

    The sol-gel polymerization of a phenolic-furfural mixture in dilute solution leads to a highly cross-linked network that can be supercritically dried to form a high surface area foam. These porous materials have cell/pore sizes {<=}1,000{angstrom}, and although they are dark brown in color, they can be classified as a new type of aerogel. The phenolic-furfural aerogel can be pyrolyzed in an inert atmosphere at 1,050 C to produce carbon aerogels. This new aerogel may be used for thermal insulation, chromatographic packing, water filtration, ion-exchange, and carbon electrodes for energy storage devices, such as batteries and double-layer capacitors. 8 figs.

  20. Organic aerogels from the sol-gel polymerization of phenolic-furfural mixtures

    DOE Patents [OSTI]

    Pekala, Richard W. (Pleasant Hill, CA)

    1996-01-01

    The sol-gel polymerization of a phenolic-furfural mixture in dilute solution leads to a highly cross-linked network that can be supercritically dried to form a high surface area foam. These porous materials have cell/pore sizes .ltoreq.1000.ANG., and although they are dark brown in color, they can be classified as a new type of aerogel. The phenolic-furfural aerogel can be pyrolyzed in an inert atmosphere at 1050.degree. C. to produce carbon aerogels. This new aerogel may be used for thermal insulation, chromatographic packing, water filtration, ion-exchange, and carbon electrodes for energy storage devices, such as batteries and double-layer capacitors.

  1. Sol-gel synthesis of hybrid organic-inorganic materials. Hexylene- and phenylene-bridged polysiloxanes

    SciTech Connect (OSTI)

    Loy, D.A.; Jamison, G.M.; Baugher, B.M.; Myers, S.A.; Assink, R.A.; Shea, K.J. [Sandia National Laboratories, Albuquerque, NM (United States)] [Sandia National Laboratories, Albuquerque, NM (United States); [Univ. of California, Irvine, CA (United States)

    1996-03-01

    New highly cross-linked polysiloxanes were prepared by sol-gel polymerization of 1,6-bis(diethoxymethylsilyl)hexane (1) and 1,4-bis(diethoxymethylsilyl)benzene (2). Hydrolysis and condensation of 1 and 2 under acidic and basic conditions with 4 equiv of water led to the rapid formation of hexylene- and phenylene-bridged polysiloxane gels. The dry gels (xerogels) were intractable, insoluble materials that were noticeably hydrophobic, exhibiting no swelling in organic solvents or water. Most of the xerogels were high surface area, mesoporous materials. Hexylene-bridged polysiloxanes prepared under acidic conditions were always nonporous regardless of whether they were processed to afford xerogels or supercritically dried as aerogels. Hexylene-bridged polysiloxanes prepared under basic conditions and all of the phenylene-bridged polysiloxanes were mesoporous with surface areas as high as 1025 m{sup 2}/g. 35 refs., 9 figs., 3 tabs.

  2. Encapsulation of nanoclusters in dried gel materials via an inverse micelle/sol gel synthesis

    SciTech Connect (OSTI)

    Martino, A.; Yamanaka, S.A.; Kawola, J.S.; Showalter, S.K.; Loy, D.A.

    1998-09-29

    A dried gel material sterically entrapping nanoclusters of a catalytically active material and a process to make the material via an inverse micelle/sol-gel synthesis are disclosed. A surfactant is mixed with an apolar solvent to form an inverse micelle solution. A salt of a catalytically active material, such as gold chloride, is added along with a silica gel precursor to the solution to form a mixture. To the mixture are then added a reducing agent for the purpose of reducing the gold in the gold chloride to atomic gold to form the nanoclusters and a condensing agent to form the gel which sterically entraps the nanoclusters. The nanoclusters are normally in the average size range of from 5--10 nm in diameter with a monodisperse size distribution. 1 fig.

  3. Encapsulation of nanoclusters in dried gel materials via an inverse micelle/sol gel synthesis

    SciTech Connect (OSTI)

    Martino, Anthony (Albuquerque, NM); Yamanaka, Stacey A. (Dallas, TX); Kawola, Jeffrey S. (Albuquerque, NM); Showalter, Steven K. (Albuquerque, NM); Loy, Douglas A. (Albuquerque, NM)

    1998-01-01

    A dried gel material sterically entrapping nanoclusters of a catalytically active material and a process to make the material via an inverse micelle/sol-gel synthesis. A surfactant is mixed with an apolar solvent to form an inverse micelle solution. A salt of a catalytically active material, such as gold chloride, is added along with a silica gel precursor to the solution to form a mixture. To the mixture are then added a reducing agent for the purpose of reducing the gold in the gold chloride to atomic gold to form the nanoclusters and a condensing agent to form the gel which sterically entraps the nanoclusters. The nanoclusters are normally in the average size range of from 5-10 nm in diameter with a monodisperse size distribution.

  4. Synthesis and characterization of vinyl-bridged polysilsesquioxane sol-gel materials

    SciTech Connect (OSTI)

    Yamanaka, S.A.; Carpenter, J.P.; McClain, M.D.; Loy, D.A.

    1995-08-01

    Vinyl-bridged polysilsesquioxane gels were formed through the use of sol-gel polymerization methods. Acid- and base-catalyzed samples were prepared from both the pure cis-(l) and pure trans-(2) isomers of 1, 2-bis(triethoxysilyl)ethylene. Gelation times of the two isomers were compared. The trans monomer 2 formed gels within a week while the cis monomer I failed to gel-even after several months. Gelation of 1 could be promoted by the addition of a coordinating metal such as palladium. The resulting cis- and trans- vinyl-bridged polysilsesquioxane gels were then processed either by vacuum drying to afford xerogels or by extracting with supercritical carbon dioxide to afford aerogels. These vinylbridged polysilsesquioxanes were characterized by SEM, nitrogen sorption porosimetry, solid State {sub 29}Si and {sub 13}C NMR and x-ray powder diffraction.

  5. INTRODUCCIN A LOS MODELOS DE REGRESIN LINEAL Los Institutos de Qumica Avanzada de Catalua (IQAC) y del Diagnstico Ambiental y Estudios del Agua (IDAEA) del CSIC

    E-Print Network [OSTI]

    ) y del Diagnóstico Ambiental y Estudios del Agua (IDAEA) del CSIC ofrecen la posibilidad de aumentar

  6. Sol-Clad-Siding and Trans-Lucent-Insulation : curtain wall components for conserving dwelling heat by passive-solar means

    E-Print Network [OSTI]

    Iliesiu, Doru

    1983-01-01

    A prototype for a dwelling heat loss compensator is introduced in this thesis, along with its measured thermal performance and suggestions for its future development. As a heat loss compensator, the Sol-Clad-Siding collects, ...

  7. Setembre del 2012 Qualitat, innovaci,

    E-Print Network [OSTI]

    Geffner, Hector

    Barcelona Campus del Mar: ciències de la salut i de la vida Campus del Poblenou: comunicació i tecnologies Biomedicina Campus del Mar: catàleg de titulacions #12;Campus del Poblenou: comunicació i tecnologies de la

  8. On the sol-gel synthesis of strontium-titanate thin films and the prospects of their use in electronics

    SciTech Connect (OSTI)

    Sohrabi Anaraki, H.; Gaponenko, N. V., E-mail: nik@nano.bsuir.edu.by; Rudenko, M. V.; Guk, A. F.; Zavadskij, S. M.; Golosov, D. A.; Kolosnitsyn, B. S. [Belarusian State University of Informatics and Radioelectronics (Belarus); Kolos, V. V.; Pyatlitskij, A. N.; Turtsevich, A. S. [Integral Enterprise (Belarus)

    2014-12-15

    Strontium-titanate films obtained by the sol-gel technique are deposited onto silicon and silicon/oxide titanium/platinum substrates. The strontium-titanate phase is detected by the method of X-ray diffraction analysis after heat treatment at temperatures of 750 and 800°C. The thickness of the films obtained by the spin-on method increases from 50 to 250 nm as the number of deposited layers is increased and is accompanied with an increase in the grain size in the films. Prospects of the development of the sol-gel technique for the formation of film components of electronic devices based on SrTiO{sub 3} xerogels are discussed.

  9. Dialkylene carbonate-bridged polysilsesquioxanes. Hybrid organic-inorganic sol-gels with a thermally labile bridging group

    SciTech Connect (OSTI)

    Loy, D.A.; Beach, J.V.; Baugher, B.M.; Assink, R.A.; Shea, K.J.; Tran, J.; Small, J.H.

    1999-11-01

    In this paper, the authors introduce a new approach for altering the properties of bridged polysilsesquioxane xerogels using postprocessing modification of the polymeric network. The bridging organic group contains latent functionalities that can be liberated thermally, photochemically, or chemically after the gel has been processed to a xerogel. These modifications can produce changes in density, solubility, porosity, and or chemical properties of the material. Since every monomer possesses two latent functional groups, the technique allows for the introduction of high levels of functionality in hybrid organic-inorganic materials. Dialkylene carbonate-bridged polysilsesquioxane gels were prepared by the sol-gel polymerization of bis(triethoxysilylpropyl) carbonate and bis(triethoxysilylisobutyl) carbonate. Thermal treatment of the resulting nonporous xerogels and aerogels at 300--350 C resulted in quantitative decarboxylation of the dialkylene carbonate bridging groups to give new hydroxyalkyl and olefinic substituted polysilsesquioxane monolithic xerogels and aerogels that cannot be directly prepared through direct sol-gel polymerization of organotrialkoxysilanes.

  10. ANA and GIS zeolite synthesis directly from alumatrane and silatrane by sol-gel process and microwave technique

    E-Print Network [OSTI]

    Gulari, Erdogan

    ANA and GIS zeolite synthesis directly from alumatrane and silatrane by sol-gel process, Na2O and H2O at 1:0.25:3:410, GIS was synthesized at hydrothermal treatment of 3 h at 110 C, while analcium (ANA) was produced at 130 C for 8 h. GIS obtained had 4.55 mm in size while ANA's size was 9

  11. Structural Modification of Sol-Gel Materials through Retro Diels-Alder Reaction

    SciTech Connect (OSTI)

    SHALTOUT,RAAFAT M.; LOY,DOUGLAS A.; MCCLAIN,MARK D.; PRABAKAR,SHESHASAYANA; GREAVES,JOHN; SHEA,KENNETH J.

    1999-12-08

    Hydrolysis and condensation of organically bridged bis-triethoxysilanes, (EtO){sub 3}Si-R-Si(OEt){sub 3}, results in the formation of three dimensional organic/inorganic hybrid networks (Equation 1). Properties of these materials, including porosity, are dependent on the nature of the bridging group, R. Flexible groups (akylene-spacers longer than five carbons in length) polymerize under acidic conditions to give non-porous materials. Rigid groups (such as arylene-, alkynylene-, or alkenylene) form non-porous, microporous, and macroporous gels. In many cases the pore size distributions are quite narrow. One of the motivations for preparing hybrid organic-inorganic materials is to extend the range of properties available with sol-gel systems by incorporating organic groups into the inorganic network. For example, organically modified silica gels arc either prepared by co-polymerizing an organoalkoxysilane with a silica precursor or surface silylating the inorganic gel. This can serve to increase hydrophobicity or to introduce some reactive organic functionality. However, the type and orientation of these organic functionalities is difficult to control. Furthermore, many organoalkoxysilanes can act to inhibitor even prevent gelation, limiting the final density of organic functionalities. We have devised a new route for preparing highly functionalized pores in hybrid materials using bridging groups that are thermally converted into the desired functionalities after the gel has been obtained. In this paper, we present the preparation and characterization of bridged polysilsesquioxanes with Diels-Alder adducts as the bridging groups from the sol-gel polymerization of monomers 2 and 4. The bridging groups are constructed such that the retro Diela-Alder reaction releases the dienes and leaves the dienophiles as integral parts of the network polymers. In the rigid architecture of a xerogel, this loss of organic functionality should liberate sufficient space to modify the overall porosity. Furthermore, the new porosity will be functionalized with the dienophilic olefin bridging group. We also demonstrate that by changing the type of Diels-Alder adduct used as the bridging group, we can change the temperature at which the retro-Diels-Alder reaction will occur.

  12. Structural and optical properties of chromium doped zinc oxide nanoparticles synthesized by sol-gel method

    SciTech Connect (OSTI)

    Naqvi, Syed Mohd. Adnan; Irshad, Kashif; Soleimani, Hassan E-mail: noorhana-yahya@petronas.com.my; Yahya, Noorhana E-mail: noorhana-yahya@petronas.com.my

    2014-10-24

    Nanosized Cr-doped ZnO nano particles were synthesized by facile sol-gel auto combustion method. The structural and optical properties of Cr-doped ZnO nanoparticles have been investigated by XRD and UV-Vis spectroscopy at room temperature for 0% to 8% concentration. X-ray diffraction analysis reveals that the Cr-doped ZnO crystallizes in a single phase polycrystalline nature with wurtzite lattice. With every % of doping, the peaks are shifting scarcely and doping of Cr is possible up to 7%. After that, the last peak vanishes, that signifies its structure is transmuted from 8% doping. The average crystallite size decreases with increase in Cr concentration (i.e. 28.9 nm for 0% to 25.8 nm for 8%). The UV-Vis spectra of the nanoparticles betoken an incrementation in the band gap energy from 3.401, 3.415, 3.431, 3.437,3.453, 3.514,3.521, 3.530 and 3.538 eV respectively, for 0,1, 2, 3, 4, 5, 6, 7 and 8 % doping concentration.

  13. Energy efficiency of electric vehicles at the 1994 American Tour de Sol

    SciTech Connect (OSTI)

    Quong, S.; Duoba, M.; Buitrago, C.; LeBlanc, N.; Larsen, R.

    1994-11-01

    In 1994, the US Department of Energy, through Argonne National Laboratory`s Center for Transportation Research, sponsored energy-efficiency data collection from student, private, and professional electric vehicles during the American Tour de Sol (ATdS). The ATDS is a multiple-day road rally event, from New York City to Philadelphia. During each leg of the event, kilowatt-hour meters measured the efficiency of the electric vehicles (EVs), which averaged from 5.68 to 65.74 km/kWh. In addition to daily energy-usage measurements, some vehicles used a data-acquisition unit to collect second-by-second information. This showed, in one case, that 21% of the total energy was captured in regenerative braking. Some of the vehicles were also tested on a dynamometer for energy-efficiency, acceleration, and steady-state power ratings. This paper also compares the energy efficiency of the vehicles during the road rally to the dynamometer results. In almost all vehicles, there was an increase in energy efficiency when the vehicle was traveling over the road, due to the non-transient duty cycle and efficient driving techniques. The dynamometer testing also showed that some EVs are equal to or better than gasoline vehicles in performance and efficiency.

  14. Transient stress evolution and crystallization in laser-irradiated amorphous titania sol-gel films

    SciTech Connect (OSTI)

    Exarhos, G.J.; Hess, N.J. (Pacific Northwest Lab., Richland, WA (United States)); Wood, S. (Washington State Univ., Pullman, WA (United States). Dept. of Physics)

    1991-10-01

    Amorphous TiO{sub 2} sol-gel films are irreversibly transformed to a crystalline anatase phase when heated to temperatures in excess of 575 K or subjected to intense pulsed or CW laser irradiation. The laser-induced transformation is initiated as a result of impurity absorption and subsequent heating, and results in densification and relative changes in compressive stress of the film. Isothermally annealed films exhibit a decrease in compressive stress as crystallization proceeds while an increase in compressive stress followed by a decrease in stress is observed when crystallization is laser-induced. Raman spectroscopy has been used to characterize the crystallization ingrowth kinetics and is used in this work as a real time probe of both film temperature and localized stress which can be evaluated from shifts in lattice phonon frequencies measured in real time during laser irradiation. The laser not only induces the phase transformation but excites inelastic Raman scattering from which film stress and temperature can be estimated. A second approach for the determination of these parameters requires incorporation of a thin ruby film between the titania and silica substrate. Here, the wavelength shift of the laser-induced ruby fluorescence can be used to quantify interfacial stress; the fluorescence lifetime measurements are used to determine temperature. The advantages and limitations of these techniques for evaluating transient stress and temperature evolution in thin titania films subjected to CW laser irradiation will be discussed.

  15. Synthesis of Yttria-Stabilized Zirconia Aerogels by a Non-Alkoxide Sol-Gel Route

    SciTech Connect (OSTI)

    Chervin, C N; Clapsaddle, B J; Chiu, H W; Gash, A E; Satcher, Jr., J H; Kauzlarich, S M

    2005-02-11

    Homogeneous, nanocrystalline powders of yttria-stabilized zirconia were prepared using a nonalkoxide sol-gel method. Monolithic gels, free of precipitation, were prepared by addition of propylene oxide to aqueous solutions of Zr{sup 4+} and Y{sup 3+} chlorides at room temperature. The gels were dried with supercritical CO{sub 2}(l), resulting in amorphous aerogels that crystallized into cubic stabilized ZrO{sub 2} following calcination at 500 C. The aerogels and resulting crystalline products were characterized using in-situ temperature profile X-ray diffraction, thermal analysis, transmission electron microscopy (TEM), scanning electron microscopy (SEM), and nitrogen adsorption/desorption analysis. TEM and N{sub 2} adsorption/desorption analysis of an aerogel indicated a porous network structure with a high surface area (409 m{sup 2}/g). The crystallized yttria-stabilized zirconia maintained high surface area (159 m{sup 2}/g) upon formation of homogeneous, nanoparticles ({approx}10 nm). Ionic conductivity at 1000 C of sintered YSZ (1500 C, 3 hours) prepared by this method, was 0.13 {+-} 0.02 {Omega}{sup -1} cm{sup -1}. Activation energies for the conduction processes from 1000-550 C and 550-400 C, were 0.95 {+-} 0.09 and 1.12 {+-} 0.05 eV, respectively. This is the first reported synthesis and characterization of yttria-stabilized zirconia via an aerogel precursor.

  16. Thickness controlled sol-gel silica films for plasmonic bio-sensing devices

    SciTech Connect (OSTI)

    Figus, Cristiana Quochi, Francesco Artizzu, Flavia Saba, Michele Marongiu, Daniela Mura, Andrea; Bongiovanni, Giovanni; Floris, Francesco; Marabelli, Franco; Patrini, Maddalena; Fornasari, Lucia; Pellacani, Paola; Valsesia, Andrea

    2014-10-21

    Plasmonics has recently received considerable interest due to its potentiality in many fields as well as in nanobio-technology applications. In this regard, various strategies are required for modifying the surfaces of plasmonic nanostructures and to control their optical properties in view of interesting application such as bio-sensing, We report a simple method for depositing silica layers of controlled thickness on planar plasmonic structures. Tetraethoxysilane (TEOS) was used as silica precursor. The control of the silica layer thickness was obtained by optimizing the sol-gel method and dip-coating technique, in particular by properly tuning different parameters such as pH, solvent concentration, and withdrawal speed. The resulting films were characterized via atomic force microscopy (AFM), Fourier-transform (FT) spectroscopy, and spectroscopic ellipsometry (SE). Furthermore, by performing the analysis of surface plasmon resonances before and after the coating of the nanostructures, it was observed that the position of the resonance structures could be properly shifted by finely controlling the silica layer thickness. The effect of silica coating was assessed also in view of sensing applications, due to important advantages, such as surface protection of the plasmonic structure.

  17. Encapsulation of gold nanoclusters in silica materials via an inverse micelle/sol-gel synthesis

    SciTech Connect (OSTI)

    Martino, A.; Kawola, J.S.; Loy, D.A. [Sandia National Labs., Albuquerque, NM (United States)] [Sandia National Labs., Albuquerque, NM (United States); Yamanaka, S.A. [Texas Instruments, Dallas, TX (United States)] [Texas Instruments, Dallas, TX (United States)

    1997-02-01

    Nanometer-sized gold particles were encapsulated in the micropores of xerogels and aerogels. The synthesis involves the sequential reduction of a gold salt followed by sol-gel processing in an inverse micelle solution. The inverse micelle solution solubilizes the metal salt and provides a microreactor for the nucleation, growth, and stabilization of the nanometer-sized clusters. Hydrolysis and condensation of an added siloxane precursor produces a wet gel embedding the particles. Characterization of the particle size and composition and the particle growth process was completed with transmission electron microscopy (TEM), electron diffraction, and UV-visible absorption spectrometry. Characterization of the gel surface areas was completed with N{sub 2} porosimetry. Material properties determined as a function of the gel precursor (TEOS vs a prehydrolyzed form of TEOS), the water to gel precursor reaction stoichiometry, and surfactant concentration are discussed in terms of the unique solution chemistry occurring in the microheterogeneous inverse micelle solutions. 73 refs., 7 figs., 1 tab.

  18. Encapsulation of metal nanocluster catalysts in silica materials via an inverse micelle/sol-gel synthesis

    SciTech Connect (OSTI)

    Martino, A.; Kawola, J.S.; Yamanaka, S.A.; Loy, D.A.

    1997-05-01

    Nanometer sized metal particles were encapsulated in the micropores of xerogels and aerogels. The synthesis involves the sequential reduction of a metal salt followed by sol-gel processing in an inverse micelle solution. The inverse micelle solution solubilizes the metal salt and provides a micro-reactor for the nucleation, growth, and stabilization of the nanometer sized clusters. Hydrolysis and condensation of an added siloxane precursor produces a wet gel embedding the particles. Characterization of the particle size and composition and the particle growth process was completed with transmission electron microscopy (TEM), electron diffraction, and UV-visible absorption spectrometry. Characterization of the gel surface areas was completed with N{sub 2} porosimetry. Material properties determined as a function of the gel precursor (TEOS vs. a pre-hydrolyzed form of TEOS), the water to gel precursor reaction stoichiometry, and surfactant concentration are discussed in terms of the unique solution chemistry occurring in the micro-heterogeneous inverse micelle solutions. Finally, catalyst development and catalyst activity of the materials are discussed. 1-hexene hydrogenation was chosen as a model reaction.

  19. Development of carbon-metal oxide supercapacitors from sol-gel derived carbon-ruthenium xerogels

    SciTech Connect (OSTI)

    Lin, C.; Ritter, J.A.; Popov, B.N.

    1999-09-01

    There has been increasing interest in electrochemical capacitors as energy storage systems because of their high power density and long cycle life, compared to battery devices. According to the mechanism of energy storage, there are two types of electrochemical capacitors. One type is based on double layer (dl) formation due to charge separation, and the other type is based on a faradaic process due to redox reactions. Sol-gel derived high surface area carbon-ruthenium xerogels were prepared from carbonized resorcinol-formaldehyde resins containing an electrochemically active form of ruthenium oxide. The electrochemical capacitance of these materials increased with an increase in the ruthenium content indicating the presence of pseudocapacitance associated with the ruthenium oxide undergoing reversible faradaic redox reactions. A specific capacitance of 256 F/g (single electrode) was obtained from a carbon xerogel containing 14 wt% Ru, which corresponded to more than 50% utilization of the ruthenium. The double layer accounted for 40% of this capacitance. This material was also electrochemically stable, showing no change in a cyclic voltammogram for over 2,000 cycles.

  20. Structure and chemistry of sol-gel derived transparent silica aerogel

    SciTech Connect (OSTI)

    Tewari, P.H.; Lofftus, K.D.; Hunt, A.J.

    1985-02-01

    Transparent silica aerogels are being studied because of their excellent thermal insulation properties for window glazing materials. The chemistry of the base catalyzed Si(OC/sub 2/H/sub 5/)/sub 4/ sol-gel process to produce transparent aerogels is presented. The results of a factorial design set of experiments are discussed in which five process parameters are simultaneously varied. The goal of these experiments was to optimize the process conditions and to analyze the importance of various parameters in improving the properties of the aerogel. A novel technique of ambient temperature supercritical drying of alcogels is described. In this process, supercritical drying occurs at less than or equal to40/sup 0/C instead of at greater than or equal to270/sup 0/C and greater than or equal to1700 PSI (12 MPa), by substituting CO/sub 2/ for alcohol in the alcogel. The time of drying is reduced from 2 to 3 days to 8 to 10 hours. It is shown that light scattering, microstructural properties and other characteristics of aerogels produced by this process and by the high temperature supercritical drying are similar.

  1. Sol-gel synthesis of mesoporous CaCu{sub 3}Ti{sub 4}O{sub 12} thin films and their gas sensing response

    SciTech Connect (OSTI)

    Parra, R., E-mail: rparra@fi.mdp.edu.a [Instituto de Investigaciones en Ciencia y Tecnologia de Materiales (INTEMA), CONICET-UNMdP, J. B. Justo 4302, B7608FDQ Mar del Plata (Argentina); Savu, R. [Instituto de Quimica, UNESP, Rua F. Degni s/n, 14800-900 Araraquara, SP (Brazil); Ramajo, L.A.; Ponce, M.A. [Instituto de Investigaciones en Ciencia y Tecnologia de Materiales (INTEMA), CONICET-UNMdP, J. B. Justo 4302, B7608FDQ Mar del Plata (Argentina); Varela, J.A. [Instituto de Quimica, UNESP, Rua F. Degni s/n, 14800-900 Araraquara, SP (Brazil); Castro, M.S. [Instituto de Investigaciones en Ciencia y Tecnologia de Materiales (INTEMA), CONICET-UNMdP, J. B. Justo 4302, B7608FDQ Mar del Plata (Argentina); Bueno, P.R. [Instituto de Quimica, UNESP, Rua F. Degni s/n, 14800-900 Araraquara, SP (Brazil); Joanni, E. [Instituto de Quimica, UNESP, Rua F. Degni s/n, 14800-900 Araraquara, SP (Brazil); Centro de Tecnologia da Informacao Renato Archer, Rodovia Dom Pedro I (SP-65) km 143, 6, 13069-901 Campinas, SP (Brazil)

    2010-06-15

    A new sol-gel synthesis procedure of stable calcium copper titanate (CaCu{sub 3}Ti{sub 4}O{sub 12}-CCTO) precursor sols for the fabrication of porous films was developed. The composition of the sol was selected in order to avoid the precipitation of undesired phases; ethanol was used as solvent, acetic acid as modifier and poly(ethyleneglycol) as a linker agent. Films deposited by spin-coating onto oxidized silicon substrates were annealed at 700 {sup o}C. The main phase present in the samples, as detected by X-ray diffraction and Raman spectroscopy, was CaCu{sub 3}Ti{sub 4}O{sub 12}. Scanning electron microscopy analysis showed that mesoporous structures, with thicknesses between 200 and 400 nm, were developed as a result of the processing conditions. The films were tested regarding their sensibility towards oxygen and nitrogen at atmospheric pressure using working temperatures from 200 to 290 {sup o}C. The samples exhibited n-type conductivity, high sensitivity and short response times. These characteristics indicate that CCTO mesoporous structures obtained by sol-gel are suitable for application in gas sensing. - Graphical abstract: A sol-gel synthesis procedure toward stable CaCu{sub 3}Ti{sub 4}O{sub 12}-precursor sols avoiding the precipitation of undesired compounds is proposed. Films deposited by spin-coating onto oxidized silicon substrates were annealed at 700 {sup o}C. The thickness varied between 200 and 400 nm depending on sol composition. The films, tested as gas sensors for O{sub 2}, showed n-type conductivity, good sensitivity and short response times.

  2. Principios del maximo para la ecuacion del telegrafo Rafael Ortega

    E-Print Network [OSTI]

    Arias, Cristina M.

    Principios del m´aximo para la ecuaci´on del tel´egrafo Rafael Ortega Departamento de Matem se refieren a problemas de contorno.1 Han sido obtenidos en sucesivas colaboraciones con A. Robles P´erez

  3. Paul Cockshott, Allin Cottrell Las ideas importantes del socialismo del

    E-Print Network [OSTI]

    Cockshott, W. Paul

    , a finales del siglo vimos la reversión hacia el neoliberalismo. 2 #12;Lo qué propusimos en nuestro libro era

  4. Electrochromism in sol-gel deposited TiO(sub 2) films

    SciTech Connect (OSTI)

    Bell, J.M.; Barczynska, J.; Evans, L.A.; MacDonald, K.A.; Wang, J.; Green, D.C.; Smith, G.B.

    1994-12-31

    Electrochromism in sol-gel deposited TiO{sub 2} films and films containing TiO{sub 2} and WO{sub 3} has been observed. The films are deposited by dip-coating from a precursor containing titanium isopropoxide in ethanol or titanium propoxide in ethanol, and after deposition the films are heat treated to between 250 C and 300 C. The films do not show any signs of crystallinity. However substantial coloration is observed using Li{sup +} ions in a non-aqueous electrolyte, both in pure TiO{sub 2} films and in mixed metal oxide films (WO{sub 3}:TiO{sub 2}), although the voltage required to produce coloration is different in the two cases. Results will be presented detailing the optical switching and charge transport properties of the films during cyclic voltammetry. These results will be used to compare the performance of the TiO{sub 2} films with other electrochromics. The TiO{sub 2} and mixed metal films all color cathodically, and the colored state is a neutral greyish color for TiO{sub 2}, while the bleached state is transparent and colorless. Results on coloration efficiency and the stability under repeated electrochemical cycling will also be presented. The neutral color of the TiO{sub 2} films and mixed-metal films means that electrochromic windows based on TiO{sub 2} may have significant advantages over WO{sub 3}-based windows. A detailed analysis of the optical properties of the colored state of the films will be presented. The dynamics of coloration for these films is also under investigation, and preliminary results will be presented.

  5. Characterization of nanocrystalline ZnO:Al films by sol-gel spin coating method

    SciTech Connect (OSTI)

    Gareso, P. L. Rauf, N. Juarlin, E.; Sugianto,; Maddu, A.

    2014-09-25

    Nanocrystalline ZnO films doped with aluminium by sol-gel spin coating method have been investigated using optical transmittance UV-Vis and X-ray diffraction (X-RD) measurements. ZnO films were prepared using zinc acetate dehydrate (Zn(CH{sub 3}COO){sub 2}@@‡2H{sub 2}O), ethanol, and diethanolamine (DEA) as a starting material, solvent, and stabilizer, respectively. For doped films, AlCl{sub 3} was added to the mixture. The ZnO:Al films were deposited on a transparent conductive oxide (TCO) substrate using spin coating technique at room temperature with a rate of 3000 rpm in 30 sec. The deposited films were annealed at various temperatures from 400°C to 600°C during 60 minutes. The transmittance UV-Vis measurement results showed that after annealing at 400°C, the energy band gap profile of nanocrystalline ZnO:Al film was a blue shift. This indicated that the band gap of ZnO:Al increased after annealing due to the increase of crystalline size. As the annealing temperature increased the bandgap energy was a constant. In addition to this, there was a small oscillation occurring after annealing compared to the as–grown samples. In the case of X-RD measurements, the crystalinity of the films were amorphous before annealing, and after annealing the crystalinity became enhance. Also, X-RD results showed that structure of nanocrystalline ZnO:Al films were hexagonal polycrystalline with lattice parameters are a = 3.290 Å and c = 5.2531 Å.

  6. INTRODUCCIN AL DISEO DE EXPERIMENTOS APLICADO EN LA QUMICA Los Institutos de Qumica Avanzada de Catalua (IQAC) y del Diagnstico Ambiental y Estudios del Agua (IDAEA) del CSIC

    E-Print Network [OSTI]

    Cataluña (IQAC) y del Diagnóstico Ambiental y Estudios del Agua (IDAEA) del CSIC ofrecen la posibilidad de

  7. Optical Fiber Chemical Sensor with Sol-Gel Derived Refractive Material as Transducer for High Temperature Gas Sensing in Clean Coal Technology

    SciTech Connect (OSTI)

    Shiquan Tao

    2006-12-31

    The chemistry of sol-gel derived silica and refractive metal oxide has been systematically studied. Sol-gel processes have been developed for preparing porous silica and semiconductor metal oxide materials. Micelle/reversed micelle techniques have been developed for preparing nanometer sized semiconductor metal oxides and noble metal particles. Techniques for doping metal ions, metal oxides and nanosized metal particles into porous sol-gel material have also been developed. Optical properties of sol-gel derived materials in ambient and high temperature gases have been studied by using fiber optic spectroscopic techniques, such as fiber optic ultraviolet/visible absorption spectrometry, fiber optic near infrared absorption spectrometry and fiber optic fluorescence spectrometry. Fiber optic spectrometric techniques have been developed for investigating the optical properties of these sol-gel derived materials prepared as porous optical fibers or as coatings on the surface of silica optical fibers. Optical and electron microscopic techniques have been used to observe the microstructure, such as pore size, pore shape, sensing agent distribution, of sol-gel derived material, as well as the size and morphology of nanometer metal particle doped in sol-gel derived porous silica, the nature of coating of sol-gel derived materials on silica optical fiber surface. In addition, the chemical reactions of metal ion, nanostructured semiconductor metal oxides and nanometer sized metal particles with gas components at room temperature and high temperatures have also been investigated with fiber optic spectrometric methods. Three classes of fiber optic sensors have been developed based on the thorough investigation of sol-gel chemistry and sol-gel derived materials. The first group of fiber optic sensors uses porous silica optical fibers doped with metal ions or metal oxide as transducers for sensing trace NH{sub 3} and H{sub 2}S in high temperature gas samples. The second group of fiber optic sensors uses sol-gel derived porous silica materials doped with nanometer particles of noble metals in the form of fiber or coating for sensing trace H{sub 2}, NH{sub 3} and HCl in gas samples at for applications ambient temperature. The third classes of fiber optic sensors use sol-gel derived semiconductor metal oxide coating on the surface of silica optical fiber as transducers for selectively sensing H{sub 2}, CH{sub 4} and CO at high temperature. In addition, optical fiber temperature sensors use the fluorescence signal of rare-earth metal ions doped porous silica optical fiber or the optical absorption signal of thermochromic metal oxide materials coated on the surface of silica optical fibers have also been developed for monitoring gas temperature of corrosive gas. Based on the results obtained from this project, the principle of fiber optic sensor techniques for monitoring matrix gas components as well as trace components of coal gasification derived syngas has been established. Prototype sensors for sensing trace ammonia and hydrogen sulfide in gasification derived syngas have been built up in our laboratory and have been tested using gas samples with matrix gas composition similar to that of gasification derived fuel gas. Test results illustrated the feasibility of these sensors for applications in IGCC processes.

  8. Dialkylenecarbonate-Bridged Polysilsesquioxanes. Hybrid Organic-Inorganic Sol-Gels with a Thermally Labile Bridging Group

    SciTech Connect (OSTI)

    Assink, Roger A.; Baugher, Brigitta M.; Beach, James V.; Loy, Douglas A.; Shea, Kenneth J.; Small, James H.; Tran, Joseph

    1999-07-20

    In this paper, we introduce a new approach for altering the properties of bridged polysilsesquioxane xerogels using post-processing mobilization of the polymeric network. The bridging organic group contains latent functionalities that can be liberated thermally, photochemically, or by chemical means after the gel has been processed to a xerogel. These modifications can produce changes in density, volubility, porosity, and or chemical properties of the material. Since every monomer possesses two latent functional groups, the technique allows for the introduction of high levels of functionality in hybrid organic-inorganic materials. Dialkylenecarbonate-bridged polysilsesquioxane gels were prepared by the sol-gel polymerization of bis(triethoxysilylpropyl)carbonate (1) and bis(triethoxysilylisobutyl)-carbonate (2). Thermal treatment of the resulting non-porous xerogels and aerogels at 300-350 C resulted in quantitative decarboxylation of the dialkylenecarbonate bridging groups to give new hydroxyalkyl and olefinic substituted polysilsesquioxane monolithic xerogels and aerogels that can not be directly prepared through direct sol-gel polymerization of organotrialkoxysilanes.

  9. Heat treatment effect on the physical properties of cobalt doped TiO{sub 2} sol–gel materials

    SciTech Connect (OSTI)

    Samet, L., E-mail: lolwasamet@gmail.com [Institut Préparatoires aux Etudes d'Ingénieurs d'El-Manar, Université Tunis El Manar, Campus Universitaire, 2092 El Manar (Tunisia); Laboratoire de Photovoltaique de Semi-conducteur et de Nanostructure, Centre de Recherches et des Technologies de l'Energie, Technopole borj cedria, Bp 95, hammamm lif 2050 (Tunisia); Ben Nasseur, J.; Chtourou, R. [Laboratoire de Photovoltaique de Semi-conducteur et de Nanostructure, Centre de Recherches et des Technologies de l'Energie, Technopole borj cedria, Bp 95, hammamm lif 2050 (Tunisia); March, K.; Stephan, O. [Laboratoire de Physique des Solides, UMR 8502 CNRS - Université Paris-Sud, Bât 510, 91405 Orsay cedex (France)

    2013-11-15

    Cobalt doped and undoped TiO{sub 2} powders have been prepared by sol–gel technique and annealed at temperatures ranging from 400 °C to 1000 °C. The effects of annealing temperature on the structural, morphological and optical properties have been characterized by X-ray diffraction, transmission electron microscopy, electron energy-loss spectroscopy and diffuse reflectance spectroscopy. For all doped samples there is a general reduction of the band gap energy, in comparison with undoped samples prepared in the same conditions. More specifically, experimental results indicate that cobalt doping, occurring as Co{sup 2+} ion insertion into the TiO{sub 2} (Ti{sup 4+}) host lattice, inhibits the growth of the crystallites and delays the phase transformation from anatase to rutile. Moreover, at high temperature, a secondary phase (CoTiO{sub 3}) is found to coexist with highly crystalline rutile. These structural characteristics are discussed in relation with the observed general trends for the optical properties. - Highlights: • Cobalt doped and undoped TiO{sub 2} powders have been prepared by sol–gel route. • Doping makes the band gap narrower. • Doping delays the phase transformation from anatase to rutile. • Doping inhibits the growth of the crystallites. • At high annealing temperature a CoTiO{sub 3} phase coexists with highly crystalline rutile.

  10. Electrochemical characterization of thio sol-gel derived titanium sulfide (TiS{sub 2}) powders with unique morphologies

    SciTech Connect (OSTI)

    Sriram, M.A.; Kumta, P.N. [Carnegie Mellon Univ., Pittsburgh, PA (United States)

    1996-12-31

    A novel thio sol-gel process utilizing titanium alkoxide as the metal source has been used to synthesize TiS{sub 2} powders exhibiting uniquely different morphologies. The pure alkoxide and its partially modified form using benzene sulfonic acid (BSA) have been reacted with H{sub 2}S to yield a solid precursor. Upon heat treatment in flowing H{sub 2}S the precursors were converted to TiS{sub 2} exhibiting distinctly different morphologies. These powders have been characterized for their chemical stoichiometry (using X-ray diffraction). At the same time the sulfide was also prepared using conventional techniques involving the reaction of the individual elements in a sealed evacuated quartz ampoule at elevated temperatures of 500{degrees}C. The morphologies of both, the thio sol-gel derived and conventionally synthesized powders have been compared using scanning electron microscopy (SEM). Preliminary electrochemical tests were also performed by fabricating test cathodes of these materials and using them in {open_quotes}hockey puck{close_quotes} cells incorporating lithium as both the anode and the reference electrodes. These studies were conducted to analyze the effect of the different morphologies of the synthesized powders on their electrochemical performance.

  11. Optical properties of undoped and Mg doped CuCrO{sub 2} powders synthesized by sol-gel route

    SciTech Connect (OSTI)

    Srinivasan, Radhakrishnan; Bolloju, Satish [Department of Chemistry, BITS Pilani Hyderabad Campus, Jawahar Nagar Village, Shamirpet Mandal, R.R.District, Hyderabad - 500 078 (India)

    2014-01-28

    In this work, CuCrO{sub 2} was synthesized by sol-gel method using citric acid as a gelling agent. The different parameters like ratio of citric acid to metal ions, calcination temperature, and duration were studied. A green colored powder with particle size around 300 nm was formed at the calcination temperature of 800 °C for four hours duration. The increase in temperature has a profound impact on crystallite size and in turn effected the optical properties. Band gap of the obtained CuCrO{sub 2} has varied from 2.3 to 1.7 eV by increasing the temperature from 800 °C to 900 °C. Doping studies were performed by introducing Mg{sup 2+} ion to substitute Cr{sup 3+} in CuCrO{sub 2}. X-ray powder diffraction and SEM studies on 2% Mg doped samples indicated a clear formation of side phases. According to the X-ray powder patterns, the reflections from side phases were increasing with the increase in doping concentrations of Mg from 2 to 5%. The side phases were found to be MgCr{sub 2}O{sub 4} spinel and CuO. The band gap has decreased for doped samples in comparison to undoped one. In this paper, sol-gel synthesis and characterization by Xray powder diffraction, SEM studies and UV-Vis-Diffuse Reflectance spectra are presented.

  12. New sol-gel synthetic route to transition and main-group metal oxide aerogels using inorganic salt precursors

    SciTech Connect (OSTI)

    Gash, A E; Tillotson, T M; Satcher Jr, J H; Hrubesh, L W; Simpson, R L

    2000-09-12

    We have developed a new sol-gel route to synthesize several transition and main-group metal oxide aerogels. The approach is straightforward, inexpensive, versatile, and it produces monolithic microporous materials with high surface areas. Specifically, we report the use of epoxides as gelation agents for the sol-gel synthesis of chromia aerogels and xerogels from simple Cr(III) inorganic salts. The dependence of both gel formation and its rate was studied by varying the solvent used, the Cr(III) precursor salt, the epoxide/Cr(III) ratio, as well as the type of epoxide employed. All of these variables were shown to affect the rate of gel formation and provide a convenient control of this parameter. Dried chromia aerogels were characterized by high-resolution transmission electron microscopy (HRTEM) and nitrogen adsorption/desorption analyses, results of which will be presented. Our studies have shown that rigid monolithic gels can be prepared from many different metal ions salts, provided the formal oxidation state of the metal ion is greater than or equal to +3. Conversely, when di-valent transition metal salts are used precipitated solids are the products.

  13. Investigation of hydrolysis and condensation in organically modified sol-gel systems: {sup 29}Si NMR and the INEPT sequence

    SciTech Connect (OSTI)

    Alam, T.M.; Assink, R.A.; Loy, D.A.

    1996-06-01

    The spectral editing properties of the {sup 29}Si NMR INEPT heteronuclear transfer experiment have been utilized for the identification and characterization of hydrolysis and initial condensation products in methyltrimethoxysilane (MTMS) sol-gel materials. {sup 29}Si NMR assignments in MTMS are complicated by a small spectral dispersion ({approximately} 0.5 ppm) and two different {sup 29}Si-{sup 1}H J couplings. By using analytical expressions for the INEPT signal response with multiple heteronuclear J couplings, unambiguous spectral assignments can be made. For this organomethoxysilane the rate of hydrolysis was found to be very rapid and significantly faster than either the water or alcohol producing condensation reactions. The hydrolysis species of both the MTMS monomer and its initial T{sup 1} condensation products follow statistical distributions that can be directly related to the extent of the hydrolysis reactions. The role of the statistical distribution of hydrolysis products on the production and synthetic control of organically modified sol-gels is discussed.

  14. "Infinite energy solutions" Fractal Laplace operator Nonlocal problem & well-posedness Renormalized sol's definition Hints & Proof Renormalized solutions adapted to the

    E-Print Network [OSTI]

    Jeanjean, Louis

    "Infinite energy solutions" Fractal Laplace operator Nonlocal problem & well-posedness Renormalized #12;"Infinite energy solutions" Fractal Laplace operator Nonlocal problem & well-posedness Renormalized sol's definition Hints & Proof Plan of the talk 1 "Infinite energy solutions" for elliptic PDEs 2

  15. Sol-Gel Synthesis of Vanadium Oxide within a Block Copolymer Elsa A. Olivetti, Jong Hak Kim, Donald R. Sadoway, Ayse Asatekin, and Anne M. Mayes*

    E-Print Network [OSTI]

    Sadoway, Donald Robert

    -transparent. Introduction Hybrid organic/inorganic nanocomposite materials are widely being developed for drug delivery,1Sol-Gel Synthesis of Vanadium Oxide within a Block Copolymer Matrix Elsa A. Olivetti, Jong Hak Kim, Donald R. Sadoway, Ayse Asatekin, and Anne M. Mayes* Department of Materials Science and Engineering

  16. Under Review for Publication in ASME J. Solar Energy Engineering SOL-12-1058 Life Estimation of Pressurized-Air Solar-Thermal Receiver Tubes

    E-Print Network [OSTI]

    Cortes, Corinna

    Under Review for Publication in ASME J. Solar Energy Engineering SOL-12-1058 Life Estimation of Pressurized-Air Solar-Thermal Receiver Tubes David K. Fork 1 e-mail: fork@google.com John Fitch e-mail: fitch.ziaei@gmail.com Robert I. Jetter e-mail: bjetter@sbcglobal.net The operational conditions of the solar thermal receiver

  17. Fluctuations in an aging system: absence of effective temperature in the sol-gel transition of a quenched gelatin sample

    E-Print Network [OSTI]

    Antoine Bérut; Artyom Petrosyan; Juan Ruben Gomez-Solano; Sergio Ciliberto

    2015-09-03

    We study the fluctuations of a Brownian micro particle trapped with optical tweezers in a gelatin solution undergoing a fast local temperature quench below the sol-gel transition. Contrary to what was previously reported, we observe no anomalous fluctuations in the particle's position that could be interpreted in terms of an effective temperature. A careful analysis with ensemble averages shows only equilibrium-like properties for the fluctuations, even though the system is clearly aging. We also provide a detailed discussion on possible artifacts that could have been interpreted as an effective temperature, such as the presence of a drift or a mixing in time and ensemble averages in data analysis. These considerations are of general interest when dealing with non-ergodic or non-stationary systems.

  18. Influence of transition metals on the surface acidic properties of titania prepared by sol-gel route

    SciTech Connect (OSTI)

    Shali, N.B. [Department of Applied Chemistry, Cochin University of Science and Technology, Cochin-22, Kerala (India); Sugunan, S. [Department of Applied Chemistry, Cochin University of Science and Technology, Cochin-22, Kerala (India)]. E-mail: ssg@cusat.ac.in

    2007-09-04

    A series of titania catalysts containing chromium, molybdenum as well as tungsten has been prepared by colloidal sol-gel route using metatitanic acid as the precursor. Structural characterization of the prepared catalysts was done with Energy dispersive X-ray analysis, X-ray diffraction, BET surface area and pore volume measurements. The influence of different transition metals like chromium, molybdenum and tungsten on the surface acidic properties of titania is investigated in detail. Two independent methods have been used to study the surface acidity of these catalyst systems: temperature programmed desorption of ammonia which is a measure of total acidity and thermodesorption studies using 2,6-dimethyl pyridine which is a measure of Bronsted acidity. Cumene cracking reaction is carried out over the prepared systems for further characterizing the acidity of the prepared catalysts. Remarkable enhancement in the surface acidity is observed after transition metal incorporation. The catalytic activity of the prepared catalysts was tested towards the dehydrogenation of cyclohexane.

  19. Decision-making in structure solution using Bayesian estimates of map quality: the PHENIX AutoSol wizard

    SciTech Connect (OSTI)

    Terwilliger, Thomas C., E-mail: terwilliger@lanl.gov [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States); Adams, Paul D. [Lawrence Berkeley National Laboratory, One Cyclotron Road, Building 64R0121, Berkeley, CA 94720 (United States); Read, Randy J.; McCoy, Airlie J. [Department of Haematology, University of Cambridge, Cambridge CB2 0XY (United Kingdom); Moriarty, Nigel W.; Grosse-Kunstleve, Ralf W.; Afonine, Pavel V.; Zwart, Peter H. [Lawrence Berkeley National Laboratory, One Cyclotron Road, Building 64R0121, Berkeley, CA 94720 (United States); Hung, Li-Wei [Los Alamos National Laboratory, Los Alamos, NM 87545 (United States)

    2009-06-01

    Ten measures of experimental electron-density-map quality are examined and the skewness of electron density is found to be the best indicator of actual map quality. A Bayesian approach to estimating map quality is developed and used in the PHENIX AutoSol wizard to make decisions during automated structure solution. Estimates of the quality of experimental maps are important in many stages of structure determination of macromolecules. Map quality is defined here as the correlation between a map and the corresponding map obtained using phases from the final refined model. Here, ten different measures of experimental map quality were examined using a set of 1359 maps calculated by re-analysis of 246 solved MAD, SAD and MIR data sets. A simple Bayesian approach to estimation of map quality from one or more measures is presented. It was found that a Bayesian estimator based on the skewness of the density values in an electron-density map is the most accurate of the ten individual Bayesian estimators of map quality examined, with a correlation between estimated and actual map quality of 0.90. A combination of the skewness of electron density with the local correlation of r.m.s. density gives a further improvement in estimating map quality, with an overall correlation coefficient of 0.92. The PHENIX AutoSol wizard carries out automated structure solution based on any combination of SAD, MAD, SIR or MIR data sets. The wizard is based on tools from the PHENIX package and uses the Bayesian estimates of map quality described here to choose the highest quality solutions after experimental phasing.

  20. Facile preparation of apatite-type lanthanum silicate by a new water-based sol–gel process

    SciTech Connect (OSTI)

    Yamagata, Chieko, E-mail: yamagata@ipen.br [Nuclear and Energy Research Institute – Instituto de Pesquisas Energéticas e Nucleares – CCTM (Centro de Ciência e Tecnologia de Materiais), São Paulo (Brazil); Elias, Daniel R.; Paiva, Mayara R.S.; Misso, Agatha M.; Castanho, Sonia R.H. Mello [Nuclear and Energy Research Institute – Instituto de Pesquisas Energéticas e Nucleares – CCTM (Centro de Ciência e Tecnologia de Materiais), São Paulo (Brazil)

    2013-06-01

    Highlights: ? We use a Na{sub 2}SiO{sub 3} waste solution as source of Si. ? We present a simple, rapid and low temperature method of lanthanum silicate apatite preparation. ? TEOS, a high cost reagent, was successfully substituted by a cheap price Na{sub 2}SiO{sub 3}, to obtain pure La{sub 9.56}(SiO{sub 4})6O{sub 2.33} lanthanum silicate apatite. - Abstract: In recent years, apatite-type lanthanum silicates ([Ln{sub 10?x}(XO{sub 4})6O{sub 3–1.5x}] (X = Si or Ge)) have been studied for use in SOFC (solid oxide fuel cells), at low temperature (600–800 °C), due to its ionic conductivity which is higher than that of YSZ (Yttrium Stabilized Zirconia) electrolyte. For this reason they are very promising materials as solid electrolyte for SOFCs. Synthesis of functional nanoparticles is a challenge in the nanotechnology. In this work, apatite-type lanthanum silicate nanoparticles were synthesized by a water-based sol–gel process, i.e., sol–gel technique followed by chemical precipitation of lanthanum hydroxide on the gel of the silica. Na{sub 2}SiO{sub 3} waste solution was used as silica source. Spherical aerogel silica was prepared by acid catalyzed reaction, followed by precipitation of lanthanum hydroxide to obtain the precursor of apatite-type lanthanum silicate. Powders of apatite-type lanthanum silicate achieved from the precursor were characterized by thermal analysis, X-ray diffraction (XRD), scanning electron microscopy (SEM) and specific surface area measurements (BET). The apatite phase was formed at 900 °C.

  1. Hoja informativa sobre la calidad del aire interior

    E-Print Network [OSTI]

    · Moho · Polen · Caspa del pelo de los animales · Humo secundario del tabaco · Formaldehído · Monóxido de

  2. Critical Parameters for Turbulent Transport in the SOL: Mechanism for the L-H Transition and its impact on the H-mode Power Threshold and Density Limit in ITER

    E-Print Network [OSTI]

    Critical Parameters for Turbulent Transport in the SOL: Mechanism for the L-H Transition and its impact on the H-mode Power Threshold and Density Limit in ITER

  3. Impactos del Huracn Isaac en la calidad del agua en Luisiana con MODIS 250m

    E-Print Network [OSTI]

    Gilbes, Fernando

    1 Impactos del Huracán Isaac en la calidad del agua en Luisiana con MODIS 250m Thais J. Alicea lluvias. Por tal razón se quiere estudiar la calidad del agua en el delta del río Mississippi antes imágenes en ENVI. Palabras clave: Calidad del agua, ENVI, Isaac, Luisiana, MODIS

  4. Synthesis of CdS/CdSe core/shell ultra small nanostructures using new microwave assisted ultrasonic sol gel route

    SciTech Connect (OSTI)

    Goswami, Y. C., E-mail: y-goswami@yahoo.com; Kumar, Vijay, E-mail: y-goswami@yahoo.com [School of Physical Sciences, ITM University, Sithouli, Gwalior- 474001 (India); Sharma, Ranjana [Institute of Technology and Management, Sithouli, Gwalior- 474001 (India); Singh, Rajeev [Institute of Information Technology and Management, Sithouli, Gwalior, MP 474001 (India)

    2014-04-24

    Core-shell CdS/CdSe nanostructures have been synthesized by new microwave assisted ultrasonic sol gel route. The solution was obtained by dissolving cadmium acetate and Thiourea in the molar ratio 1:1 in Triethlioamine. The solution was Ultrasonically irradiated by Ultrasonic crystal at 40 Hz for 3 hours at 70°C. The sol was kept for another 24 hours for gel formation. Selenium dioxide was used as a selenium source and added separately. The gel was spin coated on Quartz and Glass slides followed by microwave heat treatment. The samples were characterized by structural morphological and optical characterization. XRD studies confirm the zinc blende phase of the CdS nanoparticles. The mean nanocrystal sizes calculated using Scherrer equation is ?1.2nm. Optical studies show the strong blue shift in the spectra due to very small size of the nanocrystals. TEM and HRTEM confirm the formation of core shell structures.

  5. Fabrication of CeO2 by sol-gel process based on microfluidic technology as an analog preparation of ceramic nuclear fuel microspheres

    E-Print Network [OSTI]

    Ye, Bin; Li, Jiaolong; Zhao, Zichen; Chang, Zhenqi; Serra, Christophe A

    2012-01-01

    Microfluidics integrated with sol-gel processes is introduced in preparing monodispersed MOX nuclear fuel microspheres using nonactive cerium as a surrogate for uranium or plutonium. The detailed information about microfluidic devices and sol-gel processes are provided. The effects of viscosity and flow rate of continuous and dispersed phase on size and size distribution of CeO2 microspheres have been investigated. A comprehensive characterization of the CeO2 microspheres has been conducted, including XRD pattern, SEM, density, size and size distribution. The size of prepared monodisperse particles can be controlled precisely in range of 10{\\mu}m to 1000{\\mu}m and the particle CV is below 3%.

  6. Fabrication of CeO2 by sol-gel process based on microfluidic technology as an analog preparation of ceramic nuclear fuel microspheres

    E-Print Network [OSTI]

    Bin Ye; Jilang Miao; Jiaolong Li; Zichen Zhao; Zhenqi Chang; Christophe A. Serra

    2012-12-15

    Microfluidics integrated with sol-gel processes is introduced in preparing monodispersed MOX nuclear fuel microspheres using nonactive cerium as a surrogate for uranium or plutonium. The detailed information about microfluidic devices and sol-gel processes are provided. The effects of viscosity and flow rate of continuous and dispersed phase on size and size distribution of CeO2 microspheres have been investigated. A comprehensive characterization of the CeO2 microspheres has been conducted, including XRD pattern, SEM, density, size and size distribution. The size of prepared monodisperse particles can be controlled precisely in range of 10{\\mu}m to 1000{\\mu}m and the particle CV is below 3%.

  7. Promote the use of electric and hybrid vehicles through information dissemination & data collection through the NESEA American Tour de Sol. Final project report

    SciTech Connect (OSTI)

    2000-09-12

    A report on information dissemination on alternative fueled vehicles and on efficiency data collected at the NESEA American Tour de Sol is presented. Some of the latest advanced transportation technology vehicles were showcased. Numerous attachments are included, such as the post-event newsletter, press kit, publicity report, results table, technical workshop proceedings, NESEA tour rules and resources, and a paper titled ''Quantifying the fuel use and greenhouse gas reduction potential of electric and hybrid vehicles.''

  8. Orígenes y desarrollo del teatro guatemalteco.

    E-Print Network [OSTI]

    Carrillo, Hugo

    1971-10-01

    , tierra de convulsiones telúricas y políticas sazonada con sangre y melancolía, tierra de ensueño y de esperanza donde las procesiones de Semana Santa, solemnes y suntuosas y los fervorosos ritos indígenas al sol y a las estre llas, contrastan vivamente... labores de esceno grafía. En 1950 el destino le llevó a Puerto Rico donde trabajaba con el Teatro Universitario. Sus éxitos en la escenografía incluyen los trabajos para Los soles truncos (Rene Marqués), Ondina (Carmen Natalia), Veji gantes (Francisco...

  9. Decision-Making in Structure Solution using Bayesian Estimates of Map Quality: The PHENIX AutoSol Wizard

    SciTech Connect (OSTI)

    Terwilliger, T. C.; Adams, P. D.; Read, R. J.; McCoy, A. J.; Moriarty, Nigel W.; Grosse-Kunstleve, R. W.; Afonine, P. V.; Zwart, P. H.; Hung, L.-W.

    2009-03-01

    Estimates of the quality of experimental maps are important in many stages of structure determination of macromolecules. Map quality is defined here as the correlation between a map and the map calculated based on a final refined model. Here we examine 10 different measures of experimental map quality using a set of 1359 maps calculated by reanalysis of 246 solved MAD, SAD, and MIR datasets. A simple Bayesian approach to estimation of map quality from one or more measures is presented. We find that a Bayesian estimator based on the skew of histograms of electron density is the most accurate of the 10 individual Bayesian estimators of map quality examined, with a correlation between estimated and actual map quality of 0.90. A combination of the skew of electron density with the local correlation of rms density gives a further improvement in estimating map quality, with an overall correlation coefficient of 0.92. The PHENIX AutoSol Wizard carries out automated structure solution based on any combination of SAD, MAD, SIR, or MIR datasets. The Wizard is based on tools from the PHENIX package and uses the Bayesian estimates of map quality described here to choose the highest-quality solutions after experimental phasing.

  10. Effects of lithium doping on microstructure, electrical properties, and chemical bonds of sol-gel derived NKN thin films

    SciTech Connect (OSTI)

    Lin, Chun-Cheng; Chen, Chan-Ching; Weng, Chung-Ming; Chu, Sheng-Yuan; Tsai, Cheng-Che

    2015-02-28

    Highly (100/110) oriented lead-free Li{sub x}(Na{sub 0.5}K{sub 0.5}){sub 1?x}NbO{sub 3} (LNKN, x?=?0, 0.02, 0.04, and 0.06) thin films are fabricated on Pt/Ti/SiO{sub 2}/Si substrates via a sol-gel processing method. The lithium (Li) dopants modify the microstructure and chemical bonds of the LNKN films, and therefore improve their electrical properties. The optimal values of the remnant polarization (P{sub r}?=?14.3??C/cm{sup 2}), piezoelectric coefficient (d{sub 33}?=?48.1?pm/V), and leakage current (<10{sup ?5} A/cm{sup 2}) are obtained for a lithium addition of x?=?0.04 (i.e., 4 at.?%). The observation results suggest that the superior electrical properties are the result of an improved crystallization, a larger grain size, and a smoother surface morphology. It is shown that the ion transport mechanism is dominated by an Ohmic behavior under low electric fields and the Poole-Frenkel emission effect under high electric fields.

  11. Encapsulation of biomaterials in porous glass-like matrices prepared via an aqueous colloidal sol-gel process

    DOE Patents [OSTI]

    Liu, Dean-Mo (Richmond, CA); Chen, I-Wei (Swarthmore, PA)

    2001-01-01

    The present invention provides a process for the encapsulation of biologically important proteins into transparent, porous silica matrices by an alcohol-free, aqueous, colloidal sol-gel process, and to the biological materials encapsulated thereby. The process is exemplified by studies involving encapsulated cytochrome c, catalase, myoglobin, and hemoglobin, although non-proteinaceous biomaterials, such as active DNA or RNA fragments, cells or even tissues, may also be encapsulated in accordance with the present methods. Conformation, and hence activity of the biomaterial, is successfully retained after encapsulation as demonstrated by optical characterization of the molecules, even after long-term storage. The retained conformation of the biomaterial is strongly correlated to both the rate of gelation and the subsequent drying speed of the encapsulatng matrix. Moreover, in accordance with this process, gelation is accelerated by the use of a higher colloidal solid concentration and a lower synthesis pH than conventional methods, thereby enhancing structural stability and retained conformation of the biomaterials. Thus, the invention also provides a remarkable improvement in retaining the biological activity of the encapsulated biomaterial, as compared with those involved in conventional alkoxide-based processes. It further provides new methods for the quantitative and qualitative detection of test substances that are reactive to, or catalyzed by, the active, encapsulated biological materials.

  12. Nancy ´77: año del desengaño

    E-Print Network [OSTI]

    Rozental, Geneviè ve

    1977-10-01

    una ciudad conservadora, llegó como una bomba, el Io de Mayo, la noticia de la huelga del personal técnico y adminis trativo. Puesto otra vez en marcha el festival, quedó como cierto malhumor en el ambiente, como un sabor a fiesta aguada. Lo que..., bailes o baile-dramas, cuadros de Violeta Parra, que además de cantante y musicóloga era una pintora ingenua, cuadros del argentino Tito Saubidet a incluso dibujos de los escolares de la región de Nancy sobre el tema de América Latina. En una parte...

  13. Arylene-bridged 2,2,5,5-tetramethyl2,5-disila-1-oxacyclopentanes as precursors to non-shrinking polysiloxanes. A new route to sol-gel type polymers

    SciTech Connect (OSTI)

    Rahimian, K.; Loy, D.A.

    1998-11-01

    Sol-gel chemistry has been the focus of much attention in the design and preparation of highly crosslinked polysiloxane gels. Preparation of sol-gel processed silica or polysilesquioxane gels is carried out by the hydrolysis and condensation of alkoxysilyl monomers, usually in the presence of catalytic acid or base and an excess of water. Removal of the alcohol and water byproducts of the condensation reactions, in addition to the alcohol needed to co-dissolve the hydrophobic monomers with water, leads to substantial shrinkage during drying of the resulting gels. This limits the utility of sol-gel processing for applications requiring net-shape casting of artifacts, crack free coatings, or low vaporous organic contaminants (VOCs). It would be advantageous to have a sol-gel process based on an organosilicon monomer that would not require water as a reactant or produce water and alcohol condensation products and still result in siloxane network polymers capable of forming gels. Here, the authors show the synthesis and preparation of a novel sol-gel monomer which can easily be polymerized by ring opening polymerization to give highly crosslinked polysiloxane gels with no condensation byproducts.

  14. Modelo Hidrulico Operacional del Oeste

    E-Print Network [OSTI]

    Gilbes, Fernando

    Recursos de Agua y el Ambiente de Puerto Rico Universidad de Puerto Rico - Mayagüez Dr. Jorge Rivera Santos elementos envueltos en los sistemas de distribución de agua potable de Miradero y Ponce de León.distribución de agua potable de Miradero y Ponce de León. ·· Simular el funcionamiento del sistema.Simular el

  15. EVOLUZIONE-WEB -1 -Evoluzione del Web

    E-Print Network [OSTI]

    De Antonellis, Valeria

    EVOLUZIONE-WEB - 1 - Evoluzione del Web (fonte prof. Polillo) #12;- 2 - L'evoluzione del web EVOLUZIONE-WEB · Dal primo sito Web (1991) il Web è in continua crescita, e in continua evoluzione tecnologia, il mercato, i comportamenti delle persone · Le fasi della storia del Web: Web 1.0, Web 2.0, il

  16. Capitulo 5 El principio del palomar

    E-Print Network [OSTI]

    Fernández Gallardo, Pablo

    Versi´on prelim inar Cap´itulo 5 El principio del palomar El objetivo de este cap´itulo, que dedicamos al principio del palomar1, es ilustrar las insospechadas aplicaciones de un principio, que en su principio del palomar nos dice que en esa lista hay, con seguridad, dos repetidos. Digamos que son fj(x0) y

  17. Uso del Los SIG en ModelosUso del Los SIG en ModelosUso del Los SIG en Modelos Hidrolgicos y de Calida de Agua

    E-Print Network [OSTI]

    Gilbes, Fernando

    Calida de Agua Uso del Los SIG en Modelos Hidrológicos y de Calida de Agua (Caso de Uso Cuenca del Rió Luis R. Pérez-Alegría PhD P.E.Luis R. Pérez-Alegría PhD P.E. #12;Usos del AguaUsos del AguaUsos del AguaUsos del Agua Navegación Consumo Humano HigieneHigiene PescaRecreación #12;Calidad del Agua

  18. Reapertura del Teatro del Pueblo:´Unir la belleza con la resistencia´

    E-Print Network [OSTI]

    Castillo, Marí a

    1996-10-01

    las energías y esperanzas del nuevo emprendimiento se suman a la fuerza simbólica que guarda su antigua historia. "Llegamos a la reapertura del Teatro del Pueblo por el camino de una larga cadena de solidaridades: hubieron seres, hechos... emprendedores de esta nueva empresa: "Los protagonistas del movimiento del Teatro Independiente, unos a otros se fueron transmitiendo el mismo legado: resistir. Resistir a los autoritarismos de todos los pelajes, al comercialismo, al mal gusto. Vivimos épocas...

  19. Compositori, impresari e pubblico nell’Anello di Ugo Fleres: Un ritratto del mondo musicale operistico alle soglie del Novecento.

    E-Print Network [OSTI]

    Bombara, Daniela

    2013-01-01

    costituisce in quegli anni l’asse portante del programmaitaliano che costituisce l’asse portante del romanzo:

  20. Synthesis of BiSrCa(Y)CuO superconductor from the sol-gel method and the effect of Y substitution

    SciTech Connect (OSTI)

    Menassel, S.; Mosbah, M-F.; Altintas, S. P.; Varilci, A.; Bouaicha, F. [Universite Mentouri. Laboratoire Couches Minces et Interfaces. Route de Ain el Bey - 25017 Constantine (Algeria); Abant Izzet Baysal University. Department of Physics. 14280 Bolu. (Turkey)

    2012-09-06

    Superconducting Bi{sub 2}Sr{sub 2}Ca{sub 1-x}Y{sub x}Cu{sub 2}O{sub 8} ceramics samples have been prepared by Sol-Gel methods using citrate process. The influences of the conditions of preparation of oxide powder compound on structural and superconducting properties have been investigated by X ray diffraction (XRD), Scanning Electron Microscopy (SEM) equipped with EDS. The critical transition temperatures Tc have been determined by resistivity versus temperature measurements. Cell parameters samples were calculated from XRD patterns. The polyacryl amide gel makes the citrate process easier, more rapid and affords the possibility of synthesis of high quality oxide powders.

  1. Self-organized micro-holes on titania based sol-gel films under continuous direct writing with a continuous wave ultraviolet laser

    SciTech Connect (OSTI)

    Bakhti, S.; Destouches, N.; Gamet, E.; Reynaud, S. [University of Lyon, F. 42023 Saint-Etienne (France) [University of Lyon, F. 42023 Saint-Etienne (France); CNRS, UMR 5516, Laboratoire Hubert Curien, 18 Rue Pr. Lauras F-42000 Saint-Etienne (France); University of Saint-Etienne, Jean Monnet, F-42000 Saint-Etienne (France); Balan, L. [Institut de Sciences des Materiaux de Mulhouse, CNRS UMR 7361, Universite de Haute Alsace, 15 rue Jean Starcky, 68057 Mulhouse (France)] [Institut de Sciences des Materiaux de Mulhouse, CNRS UMR 7361, Universite de Haute Alsace, 15 rue Jean Starcky, 68057 Mulhouse (France)

    2013-05-27

    The microstructuring of titania based sol-gel films is investigated by direct writing with a continuous wave ultraviolet laser beam emitting at 244 nm. Depending on the exposure conditions, the films exhibit a volume expansion, a volume shrinkage, a self-shaped delamination, or are damaged. This paper is mainly focused on the regime where spontaneous local delamination occurs, which corresponds to a narrow range of laser irradiances and writing speeds. In this regime, self-organized round-shape micro-holes opened on the substrate are generated.

  2. Directoras de escenas novohispanas del siglo XVII

    E-Print Network [OSTI]

    Chabaud Magnus, Jaime

    1989-10-01

    FALL 1989 111 Directoras de escena novohispanas del siglo XVII* Jaime Chabaud Magnus Contrario al pregón de los lugares comunes, la mujer posee un sitio importante en la historia del teatro mexicano. Dentro del arte dramático colonial la única... figura que conocemos—o más bien mencionamos-hasta la saciedad es Sor Juana Inés de la Cruz. Del siglo XVII en que vivió la autora de Los empeños de una casa, los historiadores dan un salto inconmensurable a la segunda mitad del decimonono, cuando...

  3. Sol–gel auto combustion synthesis of CoFe{sub 2}O{sub 4}/1-methyl-2-pyrrolidone nanocomposite with ethylene glycol: Its magnetic characterization

    SciTech Connect (OSTI)

    Topkaya, R.; Kurtan, U.; Junejo, Y.; Baykal, A.

    2013-09-01

    Graphical abstract: - Highlights: • CoFe{sub 2}O{sub 4} was generated by sol–gel autocombustion using 1-methyl-2-pyrrolidone and ethylene glycol. • The presence of spin-disordered surface layer on magnetic core was established. • A linear dependence of the coercivity on temperature was fitted to Kneller's law. - Abstract: Magnetic nanoparticles were generated by sol–gel auto combustion synthesis of metal salts in the presence of 1-methyl-2-pyrrolidone, a functional solvent and ethylene glycol as usual solvent. The average crystallite size was obtained by using line profile fitting as 11 ± 5 nm. The saturation magnetization value decreases with usage of the ethylene glycol in synthesis. The observed exchange bias effect further confirms the existence of the magnetically ordered core surrounded by spin-disordered surface layer and the ethylene glycol. Square-root temperature dependence of coercivity can be fitted to Kneller's law in the temperature range of 10–400 K. The reduced remanent magnetization values lower than the theoretical value of 0.5 for non-interacting single domain particles indicate the CoFe{sub 2}O{sub 4}-1-methyl-2-pyrrolidone nanocomposite to have uniaxial anisotropy instead of the expected cubic anisotropy according to the Stoner–Wohlfarth model.

  4. Sol–gel auto-combustion synthesis of PVP/CoFe{sub 2}O{sub 4} nanocomposite and its magnetic characterization

    SciTech Connect (OSTI)

    Kurtan, U.; Topkaya, R.; Baykal, A.

    2013-11-15

    Graphical abstract: - Highlights: • The Poly(vinyl pyrrolidone) (PVP) was used as a surface capping agent. • PVP/CoFe{sub 2}O{sub 4} nanocomposite was synthesized by a sol-gel auto-combustion method. • The existence of the spin-disordered surface layer was established. - Abstract: Poly(vinyl pyrrolidone)/CoFe{sub 2}O{sub 4} nanocomposite has been fabricated by a sol–gel auto-combustion method. Poly(vinyl pyrrolidone) was used as a reducing agent as well as a surface capping agent to prevent particle aggregation and stabilize the particles. The average crystallite size estimated from X-ray line profile fitting was found to be 20 ± 7 nm. The high field irreversibility and unsaturated magnetization behaviours indicate the presence of the core–shell structure in the sample. The exchange bias effect observed at 10 K suggests the existence of the magnetically aligned core surrounded by spin-disordered surface layer. The reduced remanent magnetization value of 0.6 at 10 K (higher than the theoretical value of 0.5) shows the PVP/CoFe{sub 2}O{sub 4} nanocomposite to have cubic magnetocrystalline anisotropy according to the Stoner–Wohlfarth model.

  5. Effect of cerium on structure modifications of a hybrid sol–gel coating, its mechanical properties and anti-corrosion behavior

    SciTech Connect (OSTI)

    Cambon, Jean-Baptiste, E-mail: cambon@chimie.ups-tlse.fr [Institut Carnot CIRIMAT, Université de Toulouse, UMR CNRS 5085, 118 Route de Narbonne, 31062 Toulouse Cedex 9 (France)] [Institut Carnot CIRIMAT, Université de Toulouse, UMR CNRS 5085, 118 Route de Narbonne, 31062 Toulouse Cedex 9 (France); Esteban, Julien; Ansart, Florence; Bonino, Jean-Pierre; Turq, Viviane [Institut Carnot CIRIMAT, Université de Toulouse, UMR CNRS 5085, 118 Route de Narbonne, 31062 Toulouse Cedex 9 (France)] [Institut Carnot CIRIMAT, Université de Toulouse, UMR CNRS 5085, 118 Route de Narbonne, 31062 Toulouse Cedex 9 (France); Santagneli, S.H.; Santilli, C.V.; Pulcinelli, S.H. [Departamento F?sico-Química, Instituto de Química, Universidade Estadual Paulista, UNESP, CP 355, 14801-970 Araraquara, SP (Brazil)] [Departamento F?sico-Química, Instituto de Química, Universidade Estadual Paulista, UNESP, CP 355, 14801-970 Araraquara, SP (Brazil)

    2012-11-15

    Highlights: ? New sol–gel routes to replace chromates for corrosion protection of aluminum. ? Effect of cerium concentration on the microstructure of xerogel. ? Electrochemical and mechanical performances of hybrid coating with different cerium contents. ? Good correlation between the different results with an optimal cerium content of 0.01 M. -- Abstract: An organic–inorganic hybrid coating was developed to improve the corrosion resistance of the aluminum alloy AA 2024-T3. Organic and inorganic coatings derived from glycidoxypropyl-trimethoxysilane (GPTMS) and aluminum tri-sec-butoxide Al(O{sup s}Bu){sub 3}, with different cerium contents, were deposited onto aluminum by dip-coating process. Corrosion resistance and mechanical properties were investigated by electrochemical impedance measurements and nano-indentation respectively. An optimal cerium concentration of 0.01 M was evidenced. To correlate and explain the hybrid coating performances in relation to the cerium content, NMR experiments were performed. It has been shown that when the cerium concentration in the hybrid is higher than 0.01 M there are important modifications in the hybrid structure that account for the mechanical properties and anti-corrosion behavior of the sol–gel coating.

  6. Methods for and products of processing nanostructure nitride, carbonitride and oxycarbonitride electrode power materials by utilizing sol gel technology for supercapacitor applications

    DOE Patents [OSTI]

    Huang, Yuhong (West Hills, CA); Wei, Oiang (West Hills, CA); Chu, Chung-tse (Chatsworth, CA); Zheng, Haixing (Oak Park, CA)

    2001-01-01

    Metal nitride, carbonitride, and oxycarbonitride powder with high surface area (up to 150 m.sup.2 /g) is prepared by using sol-gel process. The metal organic precursor, alkoxides or amides, is synthesized firstly. The metal organic precursor is modified by using unhydrolyzable organic ligands or templates. A wet gel is formed then by hydrolysis and condensation process. The solvent in the wet gel is then be removed supercritically to form porous amorphous hydroxide. This porous hydroxide materials is sintered to 725.degree. C. under the ammonia flow and porous nitride powder is formed. The other way to obtain high surface area nitride, carbonitride, and oxycarbonitride powder is to pyrolyze polymerized templated metal amides aerogel in an inert atmosphere. The electrochemical capacitors are prepared by using sol-gel prepared nitride, carbonitride, and oxycarbonitride powder. Two methods are used to assemble the capacitors. Electrode is formed either by pressing the mixture of nitride powder and binder to a foil, or by depositing electrode coating onto metal current collector. The binder or coating is converted into a continuous network of electrode material after thermal treatment to provide enhanced energy and power density. Liquid electrolyte is soaked into porous electrode. The electrochemical capacitor assembly further has a porous separator layer between two electrodes/electrolyte and forming a unit cell.

  7. Photocatalytic degradation of gaseous toluene over TiO{sub 2}-SiO{sub 2} composite nanotubes synthesized by sol-gel with template technique

    SciTech Connect (OSTI)

    Zou, Xuejun [State Key Laboratory of Fine Chemical and Key Laboratory of Industrial Ecology and Environmental Engineering, School of Environmental Sciences and Technology, Dalian University of Technology, Dalian, 116024 (China)] [State Key Laboratory of Fine Chemical and Key Laboratory of Industrial Ecology and Environmental Engineering, School of Environmental Sciences and Technology, Dalian University of Technology, Dalian, 116024 (China); Li, Xinyong, E-mail: xyli@dlut.edu.cn [State Key Laboratory of Fine Chemical and Key Laboratory of Industrial Ecology and Environmental Engineering, School of Environmental Sciences and Technology, Dalian University of Technology, Dalian, 116024 (China) [State Key Laboratory of Fine Chemical and Key Laboratory of Industrial Ecology and Environmental Engineering, School of Environmental Sciences and Technology, Dalian University of Technology, Dalian, 116024 (China); Department of Chemical Engineering, Curtin University, Perth, WA 6845 (Australia); Qu, Zhenping; Zhao, Qidong; Shi, Yong; Chen, Yongying [State Key Laboratory of Fine Chemical and Key Laboratory of Industrial Ecology and Environmental Engineering, School of Environmental Sciences and Technology, Dalian University of Technology, Dalian, 116024 (China)] [State Key Laboratory of Fine Chemical and Key Laboratory of Industrial Ecology and Environmental Engineering, School of Environmental Sciences and Technology, Dalian University of Technology, Dalian, 116024 (China); Tade, Moses [Department of Chemical Engineering, Curtin University, Perth, WA 6845 (Australia)] [Department of Chemical Engineering, Curtin University, Perth, WA 6845 (Australia); Liu, Shaomin, E-mail: shaomin.liu@curtin.edu.au [Department of Chemical Engineering, Curtin University, Perth, WA 6845 (Australia)] [Department of Chemical Engineering, Curtin University, Perth, WA 6845 (Australia)

    2012-02-15

    Graphical abstract: TiO{sub 2}-SiO{sub 2} nanotubes (b) were fabricated by sol-gel method using ZnO nanowires (a) as template. Highlights: Black-Right-Pointing-Pointer A simple method to prepare TiO{sub 2}-SiO{sub 2} nanotubes for photocatalytic toluene removal. Black-Right-Pointing-Pointer The TiO{sub 2}-SiO{sub 2} nanotubes have a small blue shift and higher absorption intensity. Black-Right-Pointing-Pointer The TiO{sub 2}-SiO{sub 2} nanotubes have an enhanced photoactivity in degrading gaseous toluene. -- Abstract: TiO{sub 2}-SiO{sub 2} composite nanotubes were successfully synthesized by a facile sol-gel technique utilizing ZnO nanowires as template. The nanotubes were well characterized by transmission electron microscopy, X-ray photoelectron spectroscopy, X-ray diffraction, Fourier transform infrared spectroscopy, N{sub 2} adsorption-desorption analysis and UV-vis diffuse reflectance spectroscopy. The nanotubular TiO{sub 2}-SiO{sub 2} composite photocatalysts showed diameter of 300-325 nm, fine mesoporous structure and high specific surface area. The results indicated that the degradation efficiency of gaseous toluene could get 65% after 4 h reaction using the TiO{sub 2}-SiO{sub 2} composite as the photocatalyst under UV light illumination, which was higher than that of P25.

  8. Sol–gel synthesis of SnO{sub 2}–MgO nanoparticles and their photocatalytic activity towards methylene blue degradation

    SciTech Connect (OSTI)

    Bayal, Nisha; Jeevanandam, P.

    2013-10-15

    Graphical abstract: - Highlights: • A simple sol–gel method for the synthesis of SnO{sub 2}–MgO nanoparticles is reported. • Band gap of SnO{sub 2} can be tuned by varying the magnesium content in SnO{sub 2}–MgO. • SnO{sub 2}–MgO shows good photocatalytic activity towards degradation of methylene blue. - Abstract: SnO{sub 2}–MgO mixed metal oxide nanoparticles were prepared by a simple sol–gel method. The nanoparticles were characterized by power X-ray diffraction, scanning electron microscopy coupled with energy dispersive X-ray analysis, transmission electron microscopy and UV–vis diffuse reflectance spectroscopy. The XRD results indicate the formation of mixed metal oxide nanoparticles and also a decrease of SnO{sub 2} crystallite size in the mixed metal oxide nanoparticles with increasing magnesium oxide content. The reflectance spectroscopy results show a blue shift of the band gap of SnO{sub 2} in the mixed metal oxide nanoparticles. The photocatalytic activity of the SnO{sub 2}–MgO nanoparticles was tested using the photodegradation of aqueous methylene blue in the presence of sunlight. The results indicate that the mixed metal oxide nanoparticles possess higher efficiency for the photodegradation of methylene blue compared to pure SnO{sub 2} nanoparticles.

  9. DE-SOL-0001379

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalent Bonding Low-Cost Ground8 Gas Hydrate CharacterizationTBD1379 TABLE

  10. DE-SOL-0003641

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalent Bonding Low-Cost Ground8 Gas Hydrate

  11. DE-SOL-0005388

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalent Bonding Low-Cost Ground8 Gas Hydrate12/21/2012 000001 3 1

  12. DE-SOL-0005395

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalent Bonding Low-Cost Ground8 Gas Hydrate12/21/2012 000001 3 15395

  13. DE-SOL-0005388

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    needed for in-depth understanding and analysis of the energy-economic system of the United States, conventional and advanced energy technologies, and energy-related...

  14. DE-SOL-0008448

    National Nuclear Security Administration (NNSA)

    Deterence and Detection, "Design, Integration, Construction, Communication and Engineering 2" Acquisition Letter of Commitment to Accept Key Personnel Position. This letter...

  15. DE-SOL-0008418

    National Nuclear Security Administration (NNSA)

    corrected in amendment 000002. 12. Question 12: RFP Reference: Section L-13 (a) The Internet NNSS website Reading Room, Labor Agreements Question: Will the government release all...

  16. DE-SOL-0005982

    National Nuclear Security Administration (NNSA)

    2 EQUIPMENT - HANDHELD COMPUTER - WIRELESS WHEEL LOAD SYSTEM 1 EQUIPMENT - HEAT STRESS MONITOR 5 EQUIPMENT - HOIST - PORTABLE 1 EQUIPMENT - HOMOGENIZER 1 EQUIPMENT - HPGI 1...

  17. DE-SOL-0008448

    National Nuclear Security Administration (NNSA)

    offeror shall submit evidence to substantiate the authority of the person signing the offer and submit in Volume I of the proposal. CERTIFICATE I, ...

  18. DE-SOL-0005395

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    cross-cutting support to ORD R&D activities. CLIN 1 comprises the following work functions: A. Research Services. Although any of the functions of Research Services may take...

  19. DE-SOL-0008418

    National Nuclear Security Administration (NNSA)

    and effect . 11132015 Signature on File ITEM NO. SUPPLIESSERVICES QUANTITY UNIT UNIT PRICE AMOUNT NAME OF OFFEROR OR CONTRACTOR 2 2 CONTINUATION SHEET REFERENCE NO. OF DOCUMENT...

  20. DE-SOL-0008418

    National Nuclear Security Administration (NNSA)

    and effect . 12102015 Signature on File ITEM NO. SUPPLIESSERVICES QUANTITY UNIT UNIT PRICE AMOUNT NAME OF OFFEROR OR CONTRACTOR 2 3 CONTINUATION SHEET REFERENCE NO. OF DOCUMENT...

  1. DE-SOL-0008418

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal Gas &SCE-SessionsSouthReporteeo | National/%2A en Office of CounterterrorismEvents0/2015

  2. DE-SOL-0008418

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal Gas &SCE-SessionsSouthReporteeo | National/%2A en Office of

  3. DE-SOL-0008418

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal Gas &SCE-SessionsSouthReporteeo | National/%2A en Office ofAmendment 000002 1 Questions

  4. DE-SOL-0008418

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal Gas &SCE-SessionsSouthReporteeo | National/%2A en Office ofAmendment 000002 1

  5. DE-SOL-0008448

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal GasAdministration Medal01 Sandia National 1 PAGE 1 OF2Guidance to

  6. DE-SOL-0008449

    National Nuclear Security Administration (NNSA)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal GasAdministration Medal01 Sandia National 1 PAGE 1 OF2Guidance to [Submit in Volume II,

  7. Curso experimental en qumica biolgica, ambiental y tecnologas relacionadas Los Institutos de Qumica Avanzada de Catalua (IQAC) y de Diagnstico Ambiental y Estudios del Agua (IDAEA) del

    E-Print Network [OSTI]

    Química Avanzada de Cataluña (IQAC) y de Diagnóstico Ambiental y Estudios del Agua (IDAEA) del Consejo

  8. Mecanica celeste: Ecuaciones del movimiento Christian Nitschelm

    E-Print Network [OSTI]

    Nitschelm, Christian

    /O = - OA mV = r mV (4) El c´alculo de la diferencial del momento cin´etico con respecto al tiempo permite

  9. Evaluación del impacto | Open Energy Information

    Open Energy Info (EERE)

    sectores de la economa. Puede ser utilizado para las fuentes de emisin de gases de efecto invernadero tanto del sector elctrico como de los otros sectores. Adems puede...

  10. Roberto Cossa habla del teatro

    E-Print Network [OSTI]

    Magnarelli, Sharon

    1987-04-01

    SPRING 1987 133 Roberto Cossa habla del teatro* Sharon Magnarelli Desde tu punto de vista, ¿cuál de tus obras ha tenido más éxito, no necesariamente económico, sino personal? Yo creo que no podría hablar de una. Nuestro fin de semana lo fue en.... Después otra obra que realmente me dejó mucho fue La nona. Fue un éxito grande de publico, pero también yo hacía seis años que había dejado de escribir. Y la pieza que quizás hoy más se menciona o más se reconoce es El viejo criado. Tú me dijiste que...

  11. Luis Felipe Rodrguez Investigador del centro de

    E-Print Network [OSTI]

    Rodriguez, Luis F.

    antiguos griegos, el Universo se entendía formado a partir de cuatro 348 Dossier elementos: tierra, agua agua está formada por dos átomos del elemento hidrógeno y un átomo del elemento oxígeno. A su vez, el agua está formada por ocho protones, seis neutrones y ocho electrones. En la actualidad se cree que

  12. Mg{sub x}Zn{sub 1-x}O (x = 0-1) films fabricated by sol-gel spin coating

    SciTech Connect (OSTI)

    Caglar, Mujdat [Department of Physics, Faculty of Science, Anadolu University, 26470 Eskisehir (Turkey)] [Department of Physics, Faculty of Science, Anadolu University, 26470 Eskisehir (Turkey); Wu, Junshu; Li, Keyan [Department of Materials Science and Chemical Engineering, School of Chemical Engineering, Dalian University of Technology, Dalian 116012 (China)] [Department of Materials Science and Chemical Engineering, School of Chemical Engineering, Dalian University of Technology, Dalian 116012 (China); Caglar, Yasemin; Ilican, Saliha [Department of Physics, Faculty of Science, Anadolu University, 26470 Eskisehir (Turkey)] [Department of Physics, Faculty of Science, Anadolu University, 26470 Eskisehir (Turkey); Xue, Dongfeng, E-mail: dfxue@chem.dlut.edu.cn [Department of Materials Science and Chemical Engineering, School of Chemical Engineering, Dalian University of Technology, Dalian 116012 (China)] [Department of Materials Science and Chemical Engineering, School of Chemical Engineering, Dalian University of Technology, Dalian 116012 (China)

    2010-03-15

    Mg{sub x}Zn{sub 1-x}O films were deposited onto the glass substrate by a sol-gel spin coating method. The drying and annealing temperatures were 300 and 500 {sup o}C in air. As x varies from 0 to 1, it was observed that the crystal structure is changed from wurtzite ZnO to cubic MgO. The morphology characterizations of these films were observed by scanning electron microscope. The randomly oriented hexagonal nanorods were gown on the glass surface when x = 0 and 0.25, which became disappeared with increasing Mg contents. The optical properties of these films were investigated by room-temperature photoluminescence (PL) and UV-vis absorption spectra, which show that the optical band gap and photoluminescence in the visible and UV regions can be ideally tuned by varying the Mg contents in the Mg{sub x}Zn{sub 1-x}O alloy films.

  13. Effects of diethanolamine on sol–gel–processed Cu{sub 2}ZnSnS{sub 4} photovoltaic absorber thin films

    SciTech Connect (OSTI)

    Kahraman, S. Çetinkaya, S.; Çetinkara, H.A.; Güder, H.S.

    2014-02-01

    Highlights: • DEA content significantly affected the crystal structure and the phase purity. • The films’ crystallite sizes increased with increasing DEA content. • Two different impurity levels were found for each film via R-T characteristics. • Under different illuminations, the n-Si/CZTS exhibited good photo-response. • The light on/off current ratios confirmed the photo-sensitivity of the junction. - Abstract: As a promising solar absorber, the Cu{sub 2}ZnSnS{sub 4} compound has been popular recently for the production of green and economical thin-film solar cells owing to the abundancy and non-toxicity of all the constituents. In this study, we have produced Cu{sub 2}ZnSnS{sub 4} films via the sol–gel technique. As a stabilizer, the effects of the diethanolamine on the properties of the films were investigated. The amount of diethanolamine significantly affected the crystal structure, crystallite sizes and phase purity of the films. X-ray diffraction and Raman spectroscopy analyses confirmed the formation of phase-pure CZTS films. It was found that the film produced by using 2 ml of diethanolamine in sol exhibited pure CZTS phase, compact and dense morphology and enhanced photo-sensitivity. Light on/off current ratio of the n-Si/Cu{sub 2}ZnSnS{sub 4} junction was found to be 47 under 100 mW/cm{sup 2} of illumination. Electrical activation energies of the films were investigated and the variations were attributed to delocalized phonon states generating from the presence of other phases and lattice defects.

  14. La guerra del fin del mundo: historia e invencion en una novela historica 

    E-Print Network [OSTI]

    Loeffler, Lisa Bowe

    1984-01-01

    . No solo la psicologia de los personajes, sino tambien las costumbres descritas responden por completo a la epoca del nove- lists. " Segun su juicio, en este tipo de novela, ". . . lo que interesa realmente es la curiosidad y excentricidad del ambiente... que este escritor utilize los hechos corno ". . . medios para alcanzar verdaderamente la mencionada fidelidad historica que es ". . . la verdad de la psicologfa historica de sus personajes, del hic et nunc (aquf. y ahora) de sus motivaciones...

  15. Modelo Hidrulico Operacional del Oeste de Puerto Rico

    E-Print Network [OSTI]

    Gilbes, Fernando

    Puerto Rico Introducción El Instituto de Investigaciones Sobre Recursos de Agua y el Ambiente de Puerto del Modelo Hidráulico Operacional del Sistema de Distribución de Agua del Oeste de Puerto Rico. El agua. · Reserva Nodos que representan una fuente de agua externa del sistema. · Tanques Nodos con

  16. Instituto de Ciencias del Patrimonio MEMORIA 2012/13

    E-Print Network [OSTI]

    Fitze, Patrick

    Salnés), Guinea, Etiopía, Mongolia, Uruguay y Chile. La estrategia común del Incipit se articula a través

  17. Actuar en asociacin Regin del Gran Atlas, Marruecos

    E-Print Network [OSTI]

    Jóvenes equipos «del Sur» apoyados por el Instituto América Latina · Desarrollo sustentable en Amazonia

  18. UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR

    E-Print Network [OSTI]

    Bor, Gil

    1 UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR ÁLGEBRA II (PROGRAMA DE ESTUDIOS) DR DE GUANAJUATO NOMBRE DE LA ENTIDAD: COLEGIO DEL NIVEL MEDIO SUPERIOR NOMBRE DEL PROGRAMA EDUCATIVO Bachillerato General del Nivel Medio Superior NOMBRE DE LA MATERIA: ALGEBRA II CLAVE: BMAL2-9 NÚMERO DE VERSIÓN

  19. UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR

    E-Print Network [OSTI]

    Bor, Gil

    UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR CÁLCULO DIFERENCIAL (PROGRAMA DE;UNIVERSIDAD DE GUANAJUATO NOMBRE DE LA ENTIDAD: COLEGIO DEL NIVEL MEDIO SUPERIOR NOMBRE DEL PROGRAMA EDUCATIVO Bachillerato General del Nivel Medio Superior NOMBRE DE LA MATERIA: Cálculo Diferencial CLAVE: OMCDI-9 NÚMERO

  20. UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR

    E-Print Network [OSTI]

    Bor, Gil

    UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR INFORMÁTICA APLICADA I (PROGRAMA DE;UNIVERSIDAD DE GUANAJUATO NOMBRE DE LA ENTIDAD: COLEGIO DEL NIVEL MEDIO SUPERIOR NOMBRE DEL PROGRAMA EDUCATIVO Bachillerato General del Nivel Medio Superior NOMBRE DE LA MATERIA: Informática Aplicada I CLAVE: OCIA1

  1. UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR

    E-Print Network [OSTI]

    Bor, Gil

    UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR INFORMÁTICA APLICADA II (PROGRAMA DE;UNIVERSIDAD DE GUANAJUATO NOMBRE DE LA ENTIDAD: COLEGIO DEL NIVEL MEDIO SUPERIOR NOMBRE DEL PROGRAMA EDUCATIVO Bachillerato General del Nivel Medio Superior NOMBRE DE LA MATERIA: Informática Aplicada II CLAVE: OCIA2

  2. UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR

    E-Print Network [OSTI]

    Bor, Gil

    UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR PROBABILIDAD Y ESTADÍSTICA (PROGRAMA DE;UNIVERSIDAD DE GUANAJUATO NOMBRE DE LA ENTIDAD: COLEGIO DEL NIVEL MEDIO SUPERIOR NOMBRE DEL PROGRAMA EDUCATIVO Bachillerato General del Nivel Medio Superior NOMBRE DE LA MATERIA: Probabilidad y Estadística CLAVE: BMPES-8

  3. UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR

    E-Print Network [OSTI]

    Bor, Gil

    UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR GEOMETRÍA Y TRIGONOMETRÍA (PROGRAMA DE;UNIVERSIDAD DE GUANAJUATO NOMBRE DE LA ENTIDAD: COLEGIO DEL NIVEL MEDIO SUPERIOR NOMBRE DEL PROGRAMA EDUCATIVO Bachillerato General del Nivel Medio Superior NOMBRE DE LA MATERIA: GEOMETRÍA Y TRIGONOMETRÍA CLAVE: BMGTR-7

  4. UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR

    E-Print Network [OSTI]

    Bor, Gil

    1 UNIVERSIDAD DE GUANAJUATO COLEGIO DEL NIVEL MEDIO SUPERIOR GEOMETRÍA ANALÍTICA (PROGRAMA DE;2 UNIVERSIDAD DE GUANAJUATO NOMBRE DE LA ENTIDAD: COLEGIO DEL NIVEL MEDIO SUPERIOR NOMBRE DEL PROGRAMA EDUCATIVO Bachillerato General del Nivel Medio Superior NOMBRE DE LA MATERIA: GEOMETRÍA ANALÍTICA CLAVE: BMGAN-9 NÚMERO

  5. Smoothable del Pezzo surfaces with quotient singularities

    E-Print Network [OSTI]

    Hacking, Paul

    Smoothable del Pezzo surfaces with quotient singularities Paul Hacking and Yuri Prokhorov Abstract-01-00395-a, 06-01-72017-MHTI-a and CRDF-RUM, no. 1-2692-MO-05. #12;Paul Hacking and Yuri Prokhorov

  6. CONCENTRADO DE LA INFORMACIN NOMBRE DEL PROYECTO

    E-Print Network [OSTI]

    Bor, Gil

    del senderismo son educativos, recreativos y deportivos, pretendiéndose con él, disfrutar de de vida tradicional, devolviendo al camino el concepto de lugar de encuentro, de intercambio, que en medir el éxito estableciendo indicadores para evaluaciones periódicas. ANTECEDENTES De acuerdo al

  7. Balance del año teatral 1972 en Lima.

    E-Print Network [OSTI]

    Cajiao Salas, Teresa

    1974-10-01

    sectores.6 Buenos ejemplos de este hecho son el Grupo Telba de Barranco, la Asociación del Teatro Experimental de Lince, el grupo teatral de la Compañía de Ahorros de Chorrillos, el grupo de la Comunidad Industrial Petroquímica. Otra observación de... Administración de Negocios y Mercadotecnia y el del Instituto de Administración y Tecnología.7 Al hablar de los grupos universitarios no es posible comentar la actividad teatral en Perú sin destacar en forma muy especial la importante labor que desarrolla y...

  8. PREMIS A LA TRANSFERNCIA DE CONEIXEMENT, convocatria 2013 CANDIDATURES GUANYADORES (Acord del Jurat del Premi del 17 de juliol del 2013)

    E-Print Network [OSTI]

    Departament de Ciències Experimentals i de la Salut �mbit: Comunicació i Tecnologies de la Informació MEMBRES DEL GRUP TECNOLOGIES DELS RECURSOS LING�ÍSTICS: SILVIA ARANO, N�RIA BEL, SANTIAGO BEL, SARA MENDES de Ciències Polítiques i Socials �mbit: Comunicació i Tecnologies de la Informació HERNÁN MORALES

  9. Teatro chileno en la década del 80

    E-Print Network [OSTI]

    Piñ a, Juan André s

    1992-04-01

    SPRING 1992 85 definitiva. Se trata, más bien, de directores "buscadores de textos" y que son capaces de proponer una visión concreta, una estética específica a través del trabajo sostenido con un elenco determinado, con el cual sobre todo sienten... SPRING 1992 85 definitiva. Se trata, más bien, de directores "buscadores de textos" y que son capaces de proponer una visión concreta, una estética específica a través del trabajo sostenido con un elenco determinado, con el cual sobre todo sienten...

  10. Optical sensing elements for nitrogen dioxide (NO.sub.2) gas detection, a sol-gel method for making the sensing elements and fiber optic sensors incorporating nitrogen dioxide gas optical sensing elements

    DOE Patents [OSTI]

    Mechery, Shelly John (Mississippi State, MS); Singh, Jagdish P. (Starkville, MS)

    2007-07-03

    A sensing element, a method of making a sensing element, and a fiber optic sensor incorporating the sensing element are described. The sensor can be used for the quantitative detection of NO.sub.2 in a mixture of gases. The sensing element can be made by incorporating a diazotizing reagent which reacts with nitrous ions to produce a diazo compound and a coupling reagent which couples with the diazo compound to produce an azo dye into a sol and allowing the sol to form an optically transparent gel. The sensing element changes color in the presence of NO.sub.2 gas. The temporal response of the absorption spectrum at various NO.sub.2 concentrations has also been recorded and analyzed. Sensors having different design configurations are described. The sensing element can detect NO.sub.2 gas at levels of parts per billion.

  11. 1 0 N J I T M A G A Z I N E | F A L L 2 0 0 8 At the edge in solAr reseArch

    E-Print Network [OSTI]

    Bieber, Michael

    1 0 N J I T M A G A Z I N E | F A L L 2 0 0 8 At the edge in solAr reseArch The cool, calm water. But that's where NJIT operates one of the world's foremost solar- research facilities, on a narrow causeway jutting a thousand feet into the lake. Big Bear Solar Observatory (BBSO) has produced a wealth of data

  12. cmoves?10 A principios del siglo XIX la astronoma

    E-Print Network [OSTI]

    Rodriguez, Luis F.

    hizo Galileo Galilei a fines de 1612 y #12;11¿cómoves? principios de 1613 aparece un punto de luz que observados en cuatro años. HR 8799 es una estrella parecida al Sol y se encuentra a 130 años-luz de la Tierra detección di- recta? ¿Es lo mismo ver un cuerpo por su luz que inferirlo por la ausencia de luz que puede

  13. CONVOCATORIA A LOS ESTUDIANTES DEL CENTRO DE INVESTIGACIN Y DE ESTUDIOS AVANZADOS DEL INSTITUTO

    E-Print Network [OSTI]

    ) Propuestas basadas en su tema de tesis de posgrado. B) Propuestas con nuevas ideas no relacionadas con su tema de tesis de posgrado. Bases de la convocatoria 1. OBJETO. El objeto de la convocatoria IDi4Biz estudiantes de diferentes posgrados del Cinvestav. 3. APROBACI�N DEL ASESOR DE TESIS. La participación de los

  14. Aprendizajes del Informe Especial (SREX) del IPCC Desastres en Amrica Latina y el Caribe

    E-Print Network [OSTI]

    sus implicaciones para la sociedad y el desarrollo sostenible. El informe considera los efectos del referencia a este documento se debe hacer de la siguiente manera: Alianza Clima y Desarrollo (2012) La adaptación (véase la Figura 1). El informe considera el rol del desarrollo en fomentar la exposición y la

  15. Synthesis, characterization and application of sol-gel derived mesoporous TiO{sub 2} nanoparticles for dye-sensitized solar cells

    SciTech Connect (OSTI)

    Khan, M. Alam; Shaheer Akhtar, M.; Yang, O-Bong [School of Semiconductor and Chemical Engineering, Chonbuk National University, Dukjin Dong, Dukjingu, Jeon-ju (Korea, Republic of)

    2010-12-15

    Nanocrystalline mesoporous titania of anatase crystal phase were prepared by sol-gel route by varying calcination (400 C and 600 C) conditions, and the photo-electrochemical properties were investigated for dye-sensitized solar cell applications. The TTIP precursor in n-heptane solvent with ratio of water to TTIP (5:1) was found to be effective substrate for the working electrodes. The overall conversion efficiency of 7.59% was achieved under 1 sun irradiation with open circuit voltage of 0.77 V, current density of 17.00 mA/cm{sup 2} and FF of 51.12. The high efficiency of the 400 C calcined sample were attributed to its mesopores, high BET surface area (80.1 m{sup 2}/g) and large pore volume of prepared titania substrate which provide better surface for the absorption of dye, improves light harvesting efficiency and better charge injection. The prepared samples were characterized by XRD, small angle XRD, FE-SEM, TEM, IPCE, I-V curve, BET surface area and BJH plot techniques. (author)

  16. Annealing effects on structural, electrical and optical properties of antimony-tinoxide thin films deposited by sol gel dip coating technique

    SciTech Connect (OSTI)

    Lekshmy, S. Sujatha, E-mail: jolly2jolly@gmail.com; Anitha, V. S., E-mail: jolly2jolly@gmail.com; Berlin, I. John, E-mail: jolly2jolly@gmail.com; Joy, K., E-mail: jolly2jolly@gmail.com [Thin film Laboratory, Post Graduate and Research Department of Physics, Mar Ivanios College, Thiruvananthapuram 695 015 (India)

    2014-01-28

    Antimony-doped tin dioxide possess interesting physical and chemical properties. These properties have a wide range of applications such as catalysis and optoelectronic devices. In the present study, antimony-doped tin oxide (SnO2:Sb) thin films were deposited on the quartz substrates by sol-gel dip coating technique. The films were annealed at temperatures 350°C, 550°C and 850°C in air for 2 hours. The structure and surface morphologies were observed by X-ray diffraction (XRD) and Scanning electron microscopy (SEM). XRD patterns shows tetragonal structure for the SnO2:Sb films annealed at different temperatures. Crystallite size increased from 6 to 14 nm as annealing temperature increased from 350°C to 850°C. SEM studies reveals crack free and smooth surface for all the films. The grains are found to be homogenously distributed for films annealed at higher temperature. The electrical conductivity of the films annealed at 350°C and 550°C decreased and increased for the films annealed at 850°C. The optical properties of the films were investigated in the UV-visible-NIR region (200-900 nm) using UV spectra. The transmittance of the films decreased for films annealed at higher temperature. The optical energy band gap values (4.13 eV-4.83 eV) increased with the increase in annealing temperature.

  17. Periodizaciones y cambio de lenguaje: Monsiváis ante la crítica cultural del neoliberalismo

    E-Print Network [OSTI]

    Corona, Ignacio

    2011-01-01

    CRÍTICA CULTURAL DEL NEOLIBERALISMO Ignacio Corona The Ohioel impacto del neoliberalismo en un reciente congresohipotético impacto del neoliberalismo en la literatura es

  18. El uso del lenguaje en los diferentes canales de Internet

    E-Print Network [OSTI]

    Rosso, Paolo

    reflejo de la personalidad del sujeto que lo elabora. La elección de las palabras y el modo en que se

  19. Corpo rigido 1 Dinamica del Corpo Rigido

    E-Print Network [OSTI]

    Roma "La Sapienza", Università di

    o dotato di moto prefissato). L' asse #� 3 viene chiamato asse del sistema e l' asse # â?¢ k â??e chiamato asse fisso. Ovviamente la numerazione degli assi â??e arbitraria. Si definiscono i momenti d pura rotazione: attorno all' asse # â?¢ n, # â?¢ k, #� 3 rispettivamente

  20. Oficina del Rector Manuel Palomar Sanz

    E-Print Network [OSTI]

    Escolano, Francisco

    Oficina del Rector Rector: Manuel Palomar Sanz Secretaría Administrativa: Juana Marco Marco de la Universidad de Alicante, Manuel Palomar, ha recibido esta mañana al Equipo de Fútbol Masculino de Alicante, Manuel Palomar, y el director territorial de Cajamar en Alicante, Francisco Javier Ruiz

  1. Meso-porous ?-Fe{sub 2}O{sub 3} thin films synthesized via the sol-gel process for light-driven water oxidation

    SciTech Connect (OSTI)

    Hamd, Wael; Laberty-Robert, Christel; Sanchez, Clement [Laboratoire de Chimie de la Matiere Condensee de Paris-UMR 7574, Universite Paris 6, College de France, 11 place Marcelin Berthelot 75005, Paris, (France); Cobo, Saioa; Fize, Jennifer; Artero, Vincent [Laboratoire de Chimie et Biologie des Metaux, Universite Grenoble 1, CNRS, CEA, 17 rue des Martyrs 38054, Grenoble Cedex 9, (France); Baldinozzi, Gianguido [SPMS, MFE, CNRS-Ecole Centrale Paris et CEA, DEN, DMN, 91191 Gif-sur-Yvette, (France); Schwartz, Wilfrid; Reymermier, Maryse; Pereira, Alexandre [CEA Institut Liten, DTNM/L2CE, 17 rue des Martyrs 38054, Grenoble Cedex 9, (France); Fontecave, Marc [Laboratoire de Chimie et Biologie des Metaux, Universite Grenoble 1, CNRS, CEA, 17 rue des Martyrs 38054, Grenoble Cedex 9, (France); SPMS, MFE, CNRS-Ecole Centrale Paris et CEA, DEN, DMN, 91191 Gif-sur-Yvette, (France)

    2012-07-01

    This work reports a facile and cost-effective method for synthesizing photoactive ?-Fe{sub 2}O{sub 3} films as well as their performances when used as photoanodes for water oxidation. Transparent ?-Fe{sub 2}O{sub 3} meso-porous films were fabricated by template-directed sol-gel chemistry coupled with the dip-coating approach, followed by annealing at various temperatures from 350 degrees C to 750 degrees C in air. ?-Fe{sub 2}O{sub 3} films were characterized by X-ray diffraction, XPS, FE-SEM and electrochemical measurements. The photoelectrochemical performance of ?-Fe{sub 2}O{sub 3} photoanodes was characterized and optimized through the deposition of Co-based co-catalysts via different methods (impregnation, electro-deposition and photo-electro-deposition). Interestingly, the resulting hematite films heat-treated at relatively low temperature (500 degrees C), and therefore devoid of any extrinsic dopant, achieve light-driven water oxidation under near-to-neutral (pH = 8) aqueous conditions after decoration with a Co catalyst. The onset potential is 0.75 V vs. the reversible hydrogen electrode (RHE), thus corresponding to 450 mV light-induced under potential, although modest photocurrent density values (40 ?Acm{sup -2}) are obtained below 1.23 V vs. RHE. These new materials with a very large interfacial area in contact with the electrolyte and allowing for a high loading of water oxidation catalysts open new avenues for the optimization of photo-electrochemical water splitting. (authors)

  2. Synthesis and Characterization of Self-assembled c-axis Oriented Bi2Sr3Co2Oy Thin Films by the Sol gel Method

    SciTech Connect (OSTI)

    Lei H.; Zhu, X.; Tang, X.; Shi, D.; Jian, H.; Yeoh, W.K.; Zhao, B.; Yang, J.; Li, Q.; Zheng, R.; Dou, S.; Sun, Y.

    2011-08-18

    Bi{sub 2}Sr{sub 3}Co{sub 2}Oy thin films are prepared on SrTiO{sub 3} (100), (110) and (111) single crystal substrates using the sol-gel method. All the thin films are c-axis oriented regardless of the orientation of the substrate suggesting self-assembled c-axis orientation, and X-ray photoelectron spectroscopy results give evidence of coexistence of Co{sup 3+} and Co{sup 2+} ions in the derived films. Transmission electronic microscopy observations reveal that all samples are c-axis oriented with no obvious differences for different samples, and the c-axis lattice constant is determined as 15 {angstrom} suggesting the misfit structure. A phenomenological thermodynamic phase diagram for self-assembled c-axis orientation is established for misfit cobaltate-based films using chemical solution deposition. All samples behave like semiconductors due to the coexistence of Co{sup 3+}/Co{sup 2+} ions, and the resistivity at 350 K is 47, 39 and 17 m{Omega} cm for the thin films on SrTiO{sub 3} (100), (110) and (111), respectively, whereas the Seebeck coefficient at 300 K is 97, 89 and 77 {micro}V K{sup -1}. The successful attainment of Bi{sub 2}Sr{sub 3}Co{sub 2}O{sub y} thin films with self-assembled c-axis orientation will provide an effective prototype for investigation of growth mechanisms in complex oxide thin films with a misfit structure.

  3. Cyclization phenomena in the sol-gel polymerization of {alpha},{omega}-bis(triethoxysilyl)alkanes and incorporation of the cyclic structures into network silsesquioxane polymers

    SciTech Connect (OSTI)

    Loy, D.A.; Carpenter, J.P.; Alam, T.M.; Shaltout, R. [Sandia National Labs., Albuquerque, NM (United States)] [Sandia National Labs., Albuquerque, NM (United States); Dorhout, P.K. [Colorado State Univ., Fort Collins, CO (United States). Dept. of Chemistry] [Colorado State Univ., Fort Collins, CO (United States). Dept. of Chemistry; Greaves, J.; Shea, K.J. [Univ. of California, Irvine, CA (United States). Dept. of Chemistry] [Univ. of California, Irvine, CA (United States). Dept. of Chemistry; Small, J.H. [Los Alamos National Lab., NM (United States). Polymers and Coatings Group] [Los Alamos National Lab., NM (United States). Polymers and Coatings Group

    1999-06-16

    Intramolecular cyclizations during acid-catalyzed sol-gel polymerizations of {alpha},{omega}-bis(triethoxysilyl)alkanes substantially lengthen gel times for monomers with ethylene (1), propylene (2), and butylene (3) bridging groups. These cyclization reactions were found, using mass spectrometry and {sup 29}Si NMR spectroscopy, to lead preferentially to monomeric and dimeric products based on six- and seven-membered disilsesquioxane rings. 1,2-Bis(triethoxysilyl)ethane (1) reacts under acidic conditions to give a bicyclic dimer (5) that is composed of two annelated seven-membered rings. Under the same conditions, 1,3-bis(triethoxysilyl)propane (2), 1,4-bis(triethoxysilyl)butane (3), and Z-1,4-bis(triethoxysilyl)but-2-ene (10) undergo an intramolecular condensation reaction to give the six- and seven-membered cyclic disilsesquioxanes 6, 7, and 11. Subsequently, these cyclic monomers slowly react to form the tricyclic dimers 8, 9, and 12. With NaOH as polymerization catalyst, these cyclic silsesquioxanes readily reacted to afford gels that were shown by CP MAS {sup 29}Si NMR and infrared spectroscopies to retain some cyclic structures. Comparison of the porosity and microstructure of xerogels prepared from the cyclic monomers 6 and 7 with those of gels prepared directly from their acyclic precursors 2 and 3 indicates that the final pore structure of the xerogels is markedly dependent on the nature of the precursor. In addition, despite the fact that the monomeric cyclic disilsesquioxane species cannot be isolated from 1--3 under basic conditions due to their rapid rate of gelation, spectroscopic techniques also detected the presence of the cyclic structures in the resulting polymeric gels.

  4. Cyclization Phenomena in the Sol-Gel Polymerization of a,w-Bis(triethoxysilyl)alkanes and Incorporation of the Cyclic Structures into Network Silsesquioxane Polymers

    SciTech Connect (OSTI)

    Alam, T.M.; Carpenter, J.P.; Dorhout, P.K.; Greaves, J.; Loy, D.A.; Shaltout, R.; Shea, K.J.; Small, J.H.

    1999-01-04

    Intramolecular cyclizations during acid-catalyzed, sol-gel polymerizations of ct,co- bis(tietioxysilyl)aWmes substintidly lengtien gelties formonomers witietiylene- (l), propylene- (2), and butylene-(3)-bridging groups. These cyclizations reactions were found, using mass spectrometry and %i NMR spectroscopy, to lead preferentially to monomeric and dimeric products based on six and seven membered disilsesquioxane rings. 1,2- Bis(triethoxysilyl)ethane (1) reacts under acidic conditions to give a bicyclic drier (5) that is composed of two annelated seven membered rings. Under the same conditions, 1,3- bis(triethoxysilyl)propane (2), 1,4-bis(triethoxysilyl)butane (3), and z-1,4- bis(triethoxysilyl)but-2-ene (10) undergo an intramolecular condensation reaction to give the six membemd and seven membered cyclic disilsesquioxanes 6, 7, and 11. Subsequently, these cyclic monomers slowly react to form the tricyclic dirners 8,9 and 12. With NaOH as polymerization catalyst these cyclic silsesquioxanes readily ~aeted to afford gels that were shown by CP MAS z%i NMR and infr=d spectroscopes to retain some cyclic structures. Comparison of the porosity and microstructwe of xerogels prepared from the cyclic monomers 6 and 7 with gels prepared directly from their acyclic precursors 2 and 3, indicate that the final pore structure of the xerogels is markedly dependent on the nature of the precursor. In addition, despite the fact that the monomeric cyclic disilsesquioxane species can not be isolated from 1-3 under basic conditions due to their rapid rate of gelation, spectroscopic techniques also detected the presence of the cyclic structures in the resulting polymeric gels.

  5. T#tulo del art#culo en la revista Ep#grafe Nombre del autor

    E-Print Network [OSTI]

    Vela-Arevalo, Luz V.

    T#tulo del art#culo en la revista Ep#grafe Nombre LATEXpara la revista Ep#grafe. El contenido de este art#culo muestra es to* *talmente irrelevante, s

  6. Soluzione prova in itinere di Informatica B del 19 novembre 2004 Esercizio n. 1

    E-Print Network [OSTI]

    Amigoni, Francesco

    alla soluzione del compito cui è preposto) e l'efficienza (cioè se perviene alla soluzione del compito

  7. Epgrafe, Revista del Depto. de Matemticas y Fsica de la UAA Modelacin matemtica del control de plagas en un cultivo

    E-Print Network [OSTI]

    Vela-Arevalo, Luz V.

    Epígrafe, Revista del Depto. de Matemáticas y Física de la UAA Modelación matemática del control de

  8. El teatro argentino del año 2000 y el teatro del futuro

    E-Print Network [OSTI]

    Pellettieri, Osvaldo

    2000-10-01

    concepto deconstructivo, con su manejo de la contaminación textual, señaló el advenimiento del intertexto posmoderno en nuestro teatro. Las nociones que Jencks (97) postula para la arquitectura posmoderna pueden emplearse para acercarse al teatro de... incluyen en esta tendencia.10 Ellos, junto a otros creadores, están protagonizando desde los primeros años de la presente década una "nueva entrada al mundo" del teatro argentino. En un ambiente limitado durante mucho tiempo a "vivir con lo nuestro...

  9. Calculo Numerico II. Curso 03/04. La ecuacion del calor 1. Aproximar la solucion del problema

    E-Print Network [OSTI]

    Quirós, Fernando

    C´alculo Num´erico II. Curso 03/04. La ecuaci´on del calor 1. Aproximar la soluci´on del problema discreto. La derivada espacial se discretiza por medio de la aproximaci´on de orden 2 en diferencias la ecuaci´on del calor. 4. Calcular el residuo del esquema salto de rana Un+1 i - Un-1 i 2k = Un i+1

  10. The characteristic of carbon-coated LiFePO{sub 4} as cathode material for lithium ion battery synthesized by sol-gel process in one step heating and varied pH

    SciTech Connect (OSTI)

    Triwibowo, J.; Yuniarti, E.; Suharyadi, E.

    2014-09-25

    This research has been done on the synthesis of carbon coated LiFePO{sub 4} through sol-gel process. Carbon layer serves for improving electronic conductivity, while the variation of pH in the sol-gel process is intended to obtain the morphology of the material that may improve battery performance. LiFePO{sub 4}/C precursors are Li{sub 2}CO{sub 3}, NH{sub 4}H{sub 2}PO{sub 4} and FeC{sub 2}O{sub 4}.H{sub 2}O and citric acid. In the synthesis process, consisting of a colloidal suspension FeC{sub 2}O{sub 4}.H{sub 2}O and distilled water mixed with a colloidal suspension consisting of NH{sub 4}H{sub 2}PO{sub 4}, Li{sub 2}CO{sub 3}, and distilled water. Variations addition of citric acid is used to control the pH of the gel formed by mixing two colloidal suspensions. Sol in this study had a pH of 5, 5.4 and 5.8. The obtained wet gel is further dried in the oven and then sintered at a temperature 700°C for 10 hours. The resulting material is further characterized by XRD to determine the phases formed. The resulting powder morphology is observed through SEM. Specific surface area of the powder was tested by BET, while the electronic conductivity characterized with EIS.

  11. “Releo Mis Papeles del Pasado para Escribir Mi Romance del Porvenir”: Respiración Artificial y El Programa de Refundación del Campo Cultural Argentino

    E-Print Network [OSTI]

    Garibotto, Veró nica; Gó mez, Antonio

    2009-01-01

    estrategias narrativas –la fragmentación del relato, la representación oblicua de la realidad, la alegorización del presente mediante un buceo en el pasado– se propone que la novela de Piglia pone de manifi esto la capacidad del discurso literario de evadir... pasado, plasma su realidad inmediata y, mediante la captura de estos dos momentos, busca impactar sobre el futuro. Como Ossorio, como Raúl –que en los setenta y desde Caracas propone una versión corregida de la historia nacional, en la que en una isla...

  12. Hacia la historia del teatro hispanoamericano

    E-Print Network [OSTI]

    Dauster, Frank

    1993-04-01

    artículo reciente que rechaza de plano el método generacional por ser demasiado mecánico y fácil y por carecer de rigor científico, y luego propone organización en períodos de variada duración, que abarcan hasta cuatro o cinco siglos. Tal sistema de... periodización, además de que peca enormemente de los supuestos vicios del método generacional, no ayuda en absoluto. Ni en literatura ni en sociedad existen períodos estructurales homogéneos de tal duración. Todo período de más de unas cuantas décadas, por...

  13. Structural and electrical properties of the sol-gel prepared Sr{sub 1-x}Er{sub x}SnO{sub 3-{delta}} compounds

    SciTech Connect (OSTI)

    Ouni, S.; Nouri, S. [Unite de Recherche de Chimie des Materiaux et de l'Environnement UR11ES25, ISSBAT, Universite de Tunis ElManar 9, Avenue Dr. Zoheir Safi, 1006 Tunis (Tunisia); Rohlicek, J. [Institute of Physics ASCR, v.v.i, Na Slovance 2, 18221 Prague 8 (Czech Republic); Ben Hassen, R., E-mail: rached.benhassen@fss.rnu.tn [Unite de Recherche de Chimie des Materiaux et de l'Environnement UR11ES25, ISSBAT, Universite de Tunis ElManar 9, Avenue Dr. Zoheir Safi, 1006 Tunis (Tunisia)

    2012-08-15

    Erbium-substituted strontium stannates, with Er content 0{<=}x{<=}0.09, have been prepared by sol-gel method. The solubility limit of Er was found to be about 3%. The influence of temperature and the duration of the calcination, on the confirmation of single phase of Er doped SrSnO{sub 3} were investigated by using X-ray powder diffraction. The distribution of Er{sup 3+} in the crystal structure has been studied. Rietveld refinement of the data revealed that the crystal structure of the representative compound (Sr{sub 0.97}Er{sub 0.03}SnO{sub 3-{delta}}) is orthorhombic perovskite (space group Pbnm). The cell dimensions are: a=5.7152(1) A, b=5.7092(1) A and c=8.0710(2) A. The IR spectroscopy measurements of the samples with x{<=}0.03 were done in a wavelength range 400-2000 cm{sup -1} and confirmed the observed tilting in the SnO{sub 6} octahedra. The transport properties in the system Sr{sub 1-x}Er{sub x}SnO{sub 3-{delta}}, x{<=}0.03, were investigated at high temperature. The Sr{sub 0.97}Er{sub 0.03}SnO{sub 3-{delta}} compound exhibits semiconductive behaviour and the electrical transport mechanism agrees with the non-adiabatic small polaron hopping model between nominal states Sn{sup 4+}/Sn{sup 2+} in the temperature ranges 350-525 and 525-693 K separately. - Graphical abstract: The Sr{sub 0.97}Er{sub 0.03}SnO{sub 3-{delta}} compound exhibits semiconductive behaviour and the electrical transport mechanism agrees with the non-adiabatic small polaron hopping model between nominal states Sn{sup 4+}/Sn{sup 2+}. Highlights: Black-Right-Pointing-Pointer Er showed a maximum solubility of 3 mol% in SrSnO{sub 3} perovskite at 1173 K. Black-Right-Pointing-Pointer SnO{sub 6} octahedra in Sr{sub 1-x}Er{sub x}SnO{sub 3-{delta}} are tilted. Black-Right-Pointing-Pointer The expansion of the cell parameters ascribed to the apparition of Sn{sup 2+} ions. Black-Right-Pointing-Pointer Transport mechanism in Sr{sub 0.97}Er{sub 0.03}SnO{sub 3-{delta}} agrees with the non-adiabatic small polaron hopping model.

  14. Synthesis, characterization of double perovskite Ca{sub 2}MSbO{sub 6} (M = Dy, Fe, Cr, Al) materials via sol–gel auto-combustion and their catalytic properties

    SciTech Connect (OSTI)

    Feraru, S.; Samoila, P.; Borhan, A.I.; Ignat, M.; Iordan, A.R.; Palamaru, M.N.

    2013-10-15

    Double perovskite-type oxide Ca{sub 2}MSbO{sub 6} materials, where M = Dy, Fe, Cr, and Al, were prepared by using the sol–gel auto-combustion method. The role of different B-site cations on their synthesis, structures, morphologies and catalytic properties was investigated. The progress of double-perovskite type structure formation and the disappearance of the organic phases were monitored by infrared absorption spectroscopy (FTIR). Double perovskite oxide structures were evaluated using X-ray diffraction (XRD), while the microstructure of obtained compounds was studied using scanning electron microscopy (SEM). Also, BET surface areas were measured at the liquid nitrogen temperature by nitrogen adsorption. Catalytic properties of the obtained compounds were evaluated by test reaction of hydrogen peroxide decomposition. - Highlights: • Ca{sub 2}MSbO{sub 6} double perovskites were obtained by sol–gel auto-combustion method. • Ca{sub 2}MSbO{sub 6} (M = Dy, Fe, Cr and Al) as catalysts in H{sub 2}O{sub 2} decomposition • Strong relationship between particles' shape, BET area and catalytic performance • Ca{sub 2}FeSbO{sub 6} spherical grains show superior catalytic activity.

  15. Festival Report: XI Muestra Nacional de Teatro Peruano y I Encuentro Interregional de Teatro Peruano del Movimiento de Teatro Independiente del Perú

    E-Print Network [OSTI]

    Ferguson Acosta, Dennis

    1993-10-01

    permitirá que el público limeño se vaya educando con respecto a la riqueza del teatro nacional. Planificado a corto plazo el encuentro sufrió de insuficiente apoyo financiero y de seria desorganización de parte del recién terminado teatro del Museo de la... permitirá que el público limeño se vaya educando con respecto a la riqueza del teatro nacional. Planificado a corto plazo el encuentro sufrió de insuficiente apoyo financiero y de seria desorganización de parte del recién terminado teatro del Museo de la...

  16. DE-SOL-0003641 001

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalent Bonding Low-Cost Ground8 Gas Hydrate12/21/2012 000001 3 1 13. THIS

  17. Sol Inc | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page| Open Energy Information Serbia-Enhancing Capacity forSilicium deEnergy Information North| Open

  18. Sol Solution | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page| Open Energy Information Serbia-Enhancing Capacity forSilicium deEnergy Information North| OpenSolution Jump to:

  19. Sol rios | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page| Open Energy Information Serbia-Enhancing Capacity forSilicium deEnergy Information North| OpenSolution Jumprios

  20. Big Sol - Facilities - Cyclotron Institute

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room News PublicationsAudits & InspectionsBeryllium and ChronicBestBeyond theBid-ListBig

  1. AGGIE SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirley Ann JacksonDepartment| Department ofApplianceU.S.Departmentthe(Revision 2)EnergyAGGIE

  2. AGGIE SOL | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of Natural GasAdjustmentsShirley Ann JacksonDepartment of EnergyResearchers atDay 12: Drive5Leadership at PNNL

  3. El Sexto Festival de Teatro Español del Siglo de Oro

    E-Print Network [OSTI]

    Pé rez-Pisonero, Arturo

    1981-04-01

    no poder aprehender ni la mecánica de la obra, ni la violencia sicológica de los personajes y, por consiguiente, de sus acciones, em prendieron derroteros falsos, ajenos por completo a la mente del autor y del público. Así, una obra como la última... reconocer sus limitaciones así como posibilidades. Huyendo de las grandes obras, no de su valor sino de su dificultad, escogieron para su montaje aquellas comedias que, una vez resuelta la mecánica escénica del enredo, garantizan por su humor el éxito...

  4. Festival Report: VIII Encuentro Nacional de Teatro del CLETA

    E-Print Network [OSTI]

    Frischmann, Donald H.

    1983-10-01

    en plazas públicas de la ciudad de Guadalajara y sus alrededores. Al mismo tiempo, en la Escuela Normal de Atequiza, Jalisco, 78 LATIN AMERICAN THEATRE REVIEW se llevaron a cabo las actividades internas del Encuentro. Hubo ponencias y... impresionó por la obvia preparación experta de sus artistas. Este grupo presentó una obra que denunciaba la manipulación del pueblo por parte del gobierno y sus aliados en los medios masivos de comunicación. Un "mexicano típico" es traído desde el campo a...

  5. Del carnaval como 'metáfora' al teatro de carnaval

    E-Print Network [OSTI]

    Remedi, Gustavo

    2001-04-01

    , obreros textiles," Mauricio Rosencof Por distintas razones, y desde diversos enfoques, en las últimas décadas se ha dedicado considerable atención al tema del cuerpo y de la dimensión material en tanto fundamentos de todo modelo cultural, y en..., barrial, callejero o ambulante, los estudios e historias de teatro (Andrés Castillo, Juan C. Legido, Roger Mirza, Jorge Pignataro, Walter Rela, Stella Santos) continuaron dejando afuera todo aquello que no tomara parte del "circuito del centro," es...

  6. Aprobado por unanimidad, en sesin de Consejo Acadmico de rea del Nivel Medio Superior el 6 de julio del 2004. Entra en vigor ciclo ago-dic 2004. Objetivo del rea

    E-Print Network [OSTI]

    Bor, Gil

    Aprobado por unanimidad, en sesión de Consejo Académico de Área del Nivel Medio Superior el 6 de Matemáticas #12;Aprobado por unanimidad, en sesión de Consejo Académico de Área del Nivel Medio Superior el 6 por unanimidad, en sesión de Consejo Académico de Área del Nivel Medio Superior el 6 de julio del 2004

  7. Expandiendo los límites del teatro: Una entrevista con Astrid Hadad

    E-Print Network [OSTI]

    Alzate, Gastó n

    1997-04-01

    bolero puede verse envuelto en aires prehispánicos o una rumba puede tener influencia del blues o del rock and roll. Tal es el caso de su espectáculo Heavy Nopal (1994), en el que la artista se definió como hija de dos deidades: la Coatlicue y la... bolero puede verse envuelto en aires prehispánicos o una rumba puede tener influencia del blues o del rock and roll. Tal es el caso de su espectáculo Heavy Nopal (1994), en el que la artista se definió como hija de dos deidades: la Coatlicue y la...

  8. La lunga notte del cinema italiano: fascisti ed esquimesi

    E-Print Network [OSTI]

    Villa, Cristina

    2007-01-01

    di Prcdappio. Il 10. In Cinema Robecchi, Alessandro. Quel4. Pilletti, Paolo. Cinema e futiou. Milano: Spirali, 5.La lunga notte del cinema fascisti (Jristiiìci I italiano;

  9. DISCURSO DEL MINISTRO DE RELACIONES EXTERIROES, EMBAJADOR DAVID CHOQUEHUANCA CESPEDES.

    E-Print Network [OSTI]

    Richner, Heinz

    presentación del Libro "El Desarrollo Endógeno Sustentable como interfaz para implementar el Vivir bien en la un desarrollo sostenible sustentable, un desarro

  10. Estructura del Grado en Ingeniera de la Energa (GIE)

    E-Print Network [OSTI]

    Bilbao Arrese, Jesús Mario

    Se incluyen expresamente en el título ETSI US Las 3 menciones del GIE Ahorro y eficiencia energética

  11. La difesa idraulica del territorio 2003 Trieste 10-12 settembre 2003

    E-Print Network [OSTI]

    Cenedese, Claudia

    'apertura fra i due ostacoli, d, il diametro del vortice e y, la distanza del centro del vortice da un asse raggio del cilindro e Y la distanza fra il centro del vortice ed un asse ideale passante per il centro

  12. Centro di Ricerca Il Direttore del Centro di Ricerca Hydro-Eco

    E-Print Network [OSTI]

    Di Pillo, Gianni

    Centro di Ricerca HYDRO-ECO HYDRO-ECO . Il Direttore del Centro di Ricerca Hydro-Eco Visto il D Vista la Delibera del Consiglio del Centro Hydro-Eco del 15/9/2010 Vista la Delibera del Senato Ricerca Hydro-Eco è così composta: Rosario Cantelli Angelo Chianese Paolo De Filippis Stefania Panero

  13. Manuel Galich: La identidad del teatro latinoamericano

    E-Print Network [OSTI]

    Má rceles Daconte, Eduardo

    1984-04-01

    cuando en México se produce esa enorme transformación social que es la Revolución Mexicana a principios del siglo XX y empieza a manifestarse un teatro popular en las carpas o jacalones, como llaman en México, y surgen los cómicos populares, la revista... teatro europeo de la época, como el naturalismo por ejemplo. Tenía que llegar una irreversible conmoción a partir de la segunda década de este siglo con la Revolución Mexicana y después con la Revolución Cubana en 1959, una revolución de verdad porque...

  14. EnerDel | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTIONRobertsdale, AlabamaETEC GmbH JumpEllenville, New York:Corporation JumpEncapEndicottEnerEnerDel Jump

  15. Faces of Science: Sara Del Valle

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HABFES OctoberEvan Racah861 ANNUAL ELECTRICRashi Iyer Faces ofSara Del

  16. Pulte/Del Webb | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION JEnvironmental Jump to:EA EIS Report Url JumpTechnology JumpPrueba 1 JumpDistrict NoPulsarPulte/Del

  17. Incubar del Caribe | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIXsource History View NewGuam:on Openei |source History ViewInQbatortermIncubar del Caribe

  18. Faces of Science: Sara Del Valle

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submitKansasCommunitiesofExtrans -ORGANIZATION FYMicrotransferJoséRashi IyerSara Del

  19. Arquitectura del Sistema de Gestin del ancho de Banda y Proteccin (SGBP) para entornos de redes

    E-Print Network [OSTI]

    Ortega, Eusebi Calle

    posibles rutas de respaldo, teniendo en cuenta los requerimientos de calidad de servicio y de protección de de servicios aquellas redes más dinámicas orientadas a la conexión con garantías de calidad de calidad de servicio (QoS: quality of service) del tráfico. MPLS es la tecnología elegida para el

  20. ALGORITMOS DE OPTIMIZACIN APLICADOS AL SEGUIMIENTO DEL MOVIMIENTO ARTICULAR Y LA DIGITALIZACIN AUTOMTICA DEL

    E-Print Network [OSTI]

    Pantrigo Fernández, Juan José

    ALGORITMOS DE OPTIMIZACI�N APLICADOS AL SEGUIMIENTO DEL MOVIMIENTO ARTICULAR Y LA DIGITALIZACI�N es de naturaleza dinámica, admite la aplicación de algoritmos de estimación secuencial, como los Filtros de Partículas. Desafortunadamente, estos algoritmos no consiguen abordar con éxito problemas de

  1. La Formación Literaria de Agustín Yáñez y Al Filo del Agua: Formación literaria y temperamento

    E-Print Network [OSTI]

    Martínez, José Luis

    1983-01-01

    a A. Y. : Al filo del agua, op. cit. , p. X. Salvador Reyes299. 20. A. Y. : Al filo del agua, p. 113ss. 21. Ibidem, p.de Agustín Yáñez y Al Filo del Agua FORMACIÓN LITERARIA Y

  2. Explorando el papel del intercambio virtual en el desarrollo de la competencia translingüística y transcultural

    E-Print Network [OSTI]

    Rossomondo, Amy E.; Alonso, Maria

    2009-09-01

    El presente artículo ofrece una exploración de los objetivos propuestos para las instituciones postsecundarias en el informe del 2007 del MLA sobre el futuro del estudio de las lenguas extranjeras en el siglo XXI en los ...

  3. Disposizione n. 2437/2014 Prot. n. 0032296 del 30/05/2014

    E-Print Network [OSTI]

    Guidoni, Leonardo

    Finanza e la Contabilità dell'Ateneo, emanato con Decreto Rettorale del 23/07/2002; VISTO il Decreto comma 7-bis del succitato art. 66, che prevede il rimborso, a carico dell'aggiudicatario, del costo

  4. Application to Export Electric Energy OE Docket No. EA-405 Del...

    Energy Savers [EERE]

    Application to Export Electric Energy OE Docket No. EA-405 Del Norte Energy LLC Application to Export Electric Energy OE Docket No. EA-405 Del Norte Energy LLC Application from Del...

  5. Al convegno associata la rappresentazione teatrale del testo

    E-Print Network [OSTI]

    Di Pillo, Gianni

    Roma. Alan Turing's legacy | L'eredità di Alan Turing Roma 12 e 13 Ottobre 2012 Accoglienza dei nell'invenzione del computer Roberto Cordeschi e Guglielmo Tamburrini h. 12.15-13.00 Alan Turing e lAl convegno è associata la rappresentazione teatrale del testo La mela di Alan, dedicata a Alan

  6. Generalized complementing maps Francisco R. RUIZ DEL PORTAL

    E-Print Network [OSTI]

    Ruiz, Jesús M.

    Generalized complementing maps Francisco R. RUIZ DEL PORTAL Departamento de Geometr´ia y Topolog´ia Facultad de Ciencias Matem´aticas Universidad Complutense de Madrid 28040 Madrid, Spain R Portal-00825. 357 #12;F.R. Ruiz del Portal Generalized complementing maps differential version of this degree based

  7. Ionic Liquid and Silica Sol-Gel Composite Materials Doped with N,N,N ',N '-tetra(n-octyl)diglycolamide for Extraction of La3+ and Ba2+

    SciTech Connect (OSTI)

    Bell, Jason R [ORNL; Dai, Sheng [ORNL; Yu, Bo [ORNL; Luo, Huimin [ORNL

    2012-01-01

    Sol-gel processed silica materials which incorporated ionic liquids and tetraoctyldiglycolamide (TODGA) were prepared and used for extraction of La3+ and Ba2+ from aqueous solution. Imidazolium-based ionic liquids, 1-alkyl-3-methylimidazolium bis(trifluoromethane)sulfonimide ([Cnmim][NTf2]) were entrapped in the monolithic composite sorbents. Extraction efficiency was found to be dependent upon both the volume of IL used in the silica matrix, and the alkyl chain length of the IL cation. The silica composite sorbent containing [C8mim][NTf2] exhibited the best extraction efficiency for La3+ and the best separation factor for La3+ / Ba 2+. The results were analyzed by both Langmuir and Freundlich adsorption isotherm models, and the Freundlich model was found to give better fit.

  8. Teoria de la Computacion 1. Encuentre una gramatica libre del contexto para los siguientes lenguajes

    E-Print Network [OSTI]

    Merino, Criel

    ´atica libre del contexto que genere el lenguaje acep- tado por pila vac´ia del aut´omata de pila M = ({q0, q1

  9. MANUAL DE PROCEDIMIENTOS DEL DEPARTAMENTO DE BIOTECNOLOGIA Y BIOINGENIERIA. DISPOSICIONES GENERALES

    E-Print Network [OSTI]

    1 MANUAL DE PROCEDIMIENTOS DEL DEPARTAMENTO DE BIOTECNOLOGIA Y BIOINGENIERIA. DISPOSICIONES del Departamento (http://biotecnologia.cinvestav.mx) CAPITULO I 2.- Para los propósitos de este Manual

  10. Los flujos y reflujos de préstamos sociales y ambientales del Banco Mundial en México

    E-Print Network [OSTI]

    Fox, Jonathan A

    2000-01-01

    de la inversión y del ahorro “al derrumbarse la confianza deLa estrategia para favorecer el ahorro del CAS subraya la

  11. San José de Moro y el Fin de los Mochicas en el Valle de Jequetepeque, Costa Norte del Perú

    E-Print Network [OSTI]

    Castillo Butters, Luis Jaime

    2012-01-01

    al nivel superior de la ocupación Mochica Medio del Áreaal nivel superior de la ocupación Mochica Medio del Área 35.

  12. Temporalidad e historia: hacia una reformulación del marco interpretativo del testimonio posdictatorial

    E-Print Network [OSTI]

    Garibotto, Veró nica

    2010-01-01

    dictadura militar] a la primera persona. Difícilmente podemos abordarlo asistidos por el sistema de mediaciones que una historia más lejana permite elaborar. […] Se trata, más bien, de mantenerse dentro de los límites de un discurso que tiene a la... entrevistas testimoniales, tomas exteriores de Buenos Aires y una serie de dibujos con escenas de la campaña al desierto hacia fines del siglo XIX. Es en la articula- ción de estas imágenes que se organiza la constelación temporal que sostiene la película. En...

  13. Conferenza Nazionale ASITA, L'Aquila, 21 24 ottobre 2008 Stima di movimenti superficiali del terreno e di mappe digitali di

    E-Print Network [OSTI]

    Perissin, Daniele

    riportano i risultati relativi al terremoto del 12 maggio 2008 nella provincia del Sichuan, ricavati dall

  14. Theatre Notes: Segunda Temporada del Teatro Popular de México

    E-Print Network [OSTI]

    1974-04-01

    . Segunda Temporada del Teatro Popular de México El repertorio de la segunda temporada del "Teatro Popular de Mexico" que duró desde septiembre de 1973 hasta enero de 1974, presentó 13 obras por el sistema rotatorio en los teatros de los barrios en la... Ciudad de Mexico. Las obras fueron: El paraje de la luna rota, de Luz María Servin El Gesticulador, de Rodolfo Usigli Las confesiones de Sor Juana, de Margarita Urueta Asesinato de una conciencia, de Luis G. Basurto Los motivos del lobo, de Sergio...

  15. La magia postergada: género fantástico e identidad nacional en la España del XIX

    E-Print Network [OSTI]

    Payán Martín, Juan Jesús

    2015-01-01

    de prácticas culturales derivadas del contacto histórico conestrategias semejantes, derivadas de la negociación respecto

  16. La economa del agua de riego Jos A. Gmez-Limn

    E-Print Network [OSTI]

    Oñate, Juan J.

    #12;La economía del agua de riego en España José A. Gómez-Limón Javier Calatrava Alberto Garrido Caja Rural, Sociedad Cooperatica de Crédito. La economía del agua de riego en España Todos los derechos Directiva Marco de Agua: ¿Un modelo alternativo del uso del agua? Llorenç Avellà, José Carles y Carles

  17. Investigacin Centro de Investigacin y de Estudios Avanzados del Instituto Politcnico Nacional

    E-Print Network [OSTI]

    aplicaciones. Arturo del S. Corazón Sánchez Carmona Ingeniería de procesos para biocombustibles de generaciones

  18. Coordinacin de la Especializacin en Ingeniera del Gas Natural Valle de Sartenejas, Universidad Simn Bolvar,

    E-Print Network [OSTI]

    Vásquez, Carlos

    Coordinación de la Especialización en Ingeniería del Gas Natural Valle de Sartenejas, Universidad DEL GAS NATURAL Grado académico que otorga Especialista en Ingeniería del Gas Natural. Perfil de egresado El egresado de la Especialización del Gas Natural tendrá la competencia para: Manejar y aplicar

  19. Investigacin Centro de Investigacin y de Estudios Avanzados del Instituto Politcnico Nacional

    E-Print Network [OSTI]

    , biodiversidad y funcionamiento de los ecosistemas de arrecifes de coral, privilegiando el estudio del desarrollo

  20. CURSOS DE POSTGRADO DEL CSIC 2008-2009 CIENCIA Y TECNOLOGA DE LOS MATERIALES

    E-Print Network [OSTI]

    : Director: ISABEL SOFIA ASCENSION MONTERO HERRERO ICMMSede del curso: Codirector: 40 02/02/2009Horas

  1. L'ombra del padre. Il caso Calvino

    E-Print Network [OSTI]

    Adami, Stefano

    2010-01-01

    e del successivo 27 n° 4993. Credo opportuno aggiungere cheVice Console di San Remo. Non credo poi fuori luogo di farUn certo Mario Calvino che credo sia Mattia non Mario, e che

  2. MAESTRA EN DESARROLLO Y AMBIENTE Objetivo del programa

    E-Print Network [OSTI]

    Vásquez, Carlos

    ) Transformación del ambiente por la actividad humana 3 Desarrollo sustentable 3 Economía ambiental y de los Pobreza, desigualdad y desarrollo humano 3 El Desarrollo humano y sustentable: principios, conocimientos Líneas de investigación Educación, Interpretación y Psicología Ambiental Desarrollo Sustentable y

  3. EN COOPERACIN En los pases del Sur 41

    E-Print Network [OSTI]

    « Población, salud, desarrollo sustentable en África subsahariana » fue organizada por el IRD, la Agencia, a través principalmente de la instrumentación del convenio sobre el desarrollo sustentable firmado en 2004

  4. La Usina del Lenguaje: Teoría de la Poesía Neobarroca 

    E-Print Network [OSTI]

    De Cuba, Pablo A.

    2013-08-08

    La usina del lenguaje: Teoría de la poesía neobarroca examines one of the most relevant poetry tendencies of the last thirty years: the Neo-baroque. In this dissertation I have endeavored to analyze the works of a number ...

  5. Student Competition: Siting Potential Dams at Camp Del Webb, Utah

    E-Print Network [OSTI]

    Wamser, William Kyle

    2007-11-14

    Siting Potential Dams at Camp Del Webb, Utah Presented By: Kyle Wamser Problem ? Camp Del Webb is Lacking an Onsite Lake ? High Adventure Bases generally need aquatics ? Large lake nearby, but transportation is required ? Possible Solution... hillshade ? Finding Possible Lake Locations ? Added three potential dam sites ? Calculated watersheds ? Extended dams through terrain to prevent runoff on the sides ? Calculated watershed dam elevation, which identified lakes Results...

  6. Ni{sub 0.5}Zn{sub 0.5}Fe{sub 2}O{sub 4} nanoparticles dispersed in a SiO{sub 2} matrix synthesized by sol-gel processing

    SciTech Connect (OSTI)

    Pozo Lopez, G.; Condo, A.M.; Instituto Balseiro, Universidad Nacional de Cuyo, Av. Bustillo 9500, 8400, San Carlos de Bariloche; Consejo Nacional de Investigaciones Cientificas y Tecnicas ; Urreta, S.E.; Silvetti, S.P.; Aguirre, M. del C.; Instituto de Fisica Enrique Gaviola - CONICET

    2012-12-15

    (Ni{sub 0.5}Zn{sub 0.5}Fe{sub 2}O{sub 4})x/(SiO{sub 2})(100 - x) (x = 5, 20 and 50 wt.%) nanocomposites are synthesized by a sol-gel method using tetraethylorthosilicate (TEOS) and metallic nitrates as precursors, and by further annealing the powders for 1 h at 1273 K. X-ray diffraction (XRD), transmission electron microscopy (TEM), room temperature vibrating sample magnetometry (VSM) and SQUID measurements are employed for structural, morphological and magnetic sample characterization. For all the concentrations analyzed, the powder nanocomposites actually consist of spinel NiZn ferrite nanoparticles, dispersed in an amorphous silica matrix. TEM studies reveal different particle size distributions and particle morphologies for the three ferrite contents. The 20 wt.%-NiZn ferrite samples consist of nearly spherical nanoparticles, of about 8 nm, mainly superparamagnetic, well-dispersed in the amorphous silica matrix, while the 5 wt.%-NiZn ferrite samples exhibit a bimodal particle size distribution (5 and 30 nm) of single-domain nanoparticles embedded in the silica. In the 50 wt.%-NiZn ferrite samples, two particle families are observed: small round superparamagnetic nanoparticles of about 8 nm embedded in the amorphous silica matrix and large, non-spherical, ferrimagnetic ones, forming agglomerates outside the matrix. In all the synthesized samples, thickness fringes are observed inside some of the ferrite nanoparticles in dark field images. This contrast is explained using the theory of electron diffraction in a weak beam dark field (WBDF) condition and considering spherical ferrite nanoparticles. A large range of tailored magnetic properties varying the fraction, dispersion and mean size of the ferrimagnetic NiZn ferrite particles is obtained. Room temperature saturation magnetization values are found in the range 3.0-30.4 Am{sup 2}/kg for the different concentration samples. Coercivity values, between 1.9 and 7.6 mT, are more than 50% higher than those measured in powders of pure stoichiometric NiZn ferrite nanoparticles and somewhat higher than those reported for similar NiZn ferrite/SiO{sub 2} nanocomposites also synthesized by sol-gel processes. A correlation between the nanocomposite microstructure and the observed magnetic properties is established. - Highlights: Black-Right-Pointing-Pointer NiZn ferrite/SiO{sub 2} nanocomposites are successfully synthesized by a sol-gel route. Black-Right-Pointing-Pointer Depending on the NiZn ferrite content single or bimodal size distributions result. Black-Right-Pointing-Pointer Coercivity (1.9-7.6 mT) is 50% higher than in stoichiometric NiZn ferrite powders. Black-Right-Pointing-Pointer Microstructure and magnetic properties are correlated.

  7. Vanguardia, raza y nación: una lectura de la negritud de la novela mexicana Panchito Chapopote y del estridentismo a la luz del modernismo brasileño y de Macunaíma

    E-Print Network [OSTI]

    Irizarry, Roberto

    2012-01-01

    y del estridentismo a la luz del modernismo brasileño y dedesenlace argumental. A la luz de dicho panorama narrativo,Panchito Chapopote visto a la luz de Macunaíma : la nación,

  8. Comparison of effectiveness of sub-slab ventilation systems for indoor radon mitigation: A numerical study; Comparaison a l`aide d`un outil numerique de l`efficacite des systemes de ventilation active du sol limitant la penetration du radon dans l`habitat

    SciTech Connect (OSTI)

    Bonnefous, Y.C. [Ecole Nationale des Travaux Publics de l`Etat, 69 - Vaulx en Velin (France). Lab. Sciences de l`Habitat]|[Lawrence Berkeley Lab., CA (United States); Gadgil, A.J. [Lawrence Berkeley Lab., CA (United States); Allard, F. [Institut National des Sciences Appliquees (INSA), 69 - Villeurbanne (France)

    1992-04-01

    The functioning of an active sub-slab ventilation system (SVS) has been studied successfully with the help of a previously evaluated numerical model. The parameters explored are the permeability of the sub-slab and the gravel placed beneath it, the amplitude of applied pressure at the installation point of the system and the functioning method: depressurization or pressurization. The mechanisms contributing to the success of the two systems are identified. This numerical study shows that the presence of a layer of gravel beneath the sub-slab considerably improves the performance of the SVS. Considered separately from the extremely permeable sub-slabs, the depressurization systems perform better than the pressurization systems. 17 refs. [Francais] Le fonctionnement des Systemes de Ventilation active du Sol (SVS) a ete etudie a l`aide d`un outil numerique precedemment evalue avec succes. Les parametres explores sont les permeabilites du sol et du gravier place sous plancher bas, l`amplitude de la pression appliquee au point d`installation du systeme, et le mode de fonctionnement: Depressurisation ou Pressurisation. Les mecanismes contribuant au succes des deux systemes sont identifies. Cette etude numerique montre que la presence d`une couche de gravier sous plancher bas ameliore de facon considerable les performances des SVS. Mis a part le cas des sols extremement permeables, les systemes de Depressurisation ont de meilleures performances que les systemes de Pressurisation. 17 refs.

  9. Structural and dielectric/ferroelectric properties of (La{sub 1-x}Nd{sub x}){sub 2}Ti{sub 2}O{sub 7} synthesized by sol-gel route

    SciTech Connect (OSTI)

    Shao Zhenmian; Saitzek, Sebastien; Roussel, Pascal; Mentre, Olivier; Prihor Gheorghiu, Felicia; Mitoseriu, Liliana; Desfeux, Rachel

    2010-07-15

    A series of compounds with the general formula (La{sub 1-x}Nd{sub x}){sub 2}Ti{sub 2}O{sub 7} (0.0{<=}x{<=}1.0) has been prepared by the sol-gel method. The decomposition of the gel was characterized by thermo-gravimetric analysis coupled to mass spectrometry, indicating the reaction is achieved above 850 {sup o}C. The lattice parameters versus x show an expected decrease in the a and b parameters while c and the {beta} angle remain almost unchanged with respect to the monoclinic symmetry conserved for the full solid solution. Dielectric, piezoelectric and ferroelectric properties were measured on the entire series. - Graphical abstract: XRD patterns of (La{sub 1-x}Nd{sub x}){sub 2}Ti{sub 2}O{sub 7} powders for various x values. The (hkl) peaks positions (with h and k{ne}0) change with x values while the (00l) peaks positions remain unaffected.

  10. Los hijos del terremoto: Imágenes de un recuerdo

    E-Print Network [OSTI]

    Dauster, Frank

    1988-10-01

    FAII.1QR8 5 Los hijos del terremoto: Imágenes de un recuerdo Frank Dauster Una de las tentaciones más frecuentemente vencedoras que sedu cen al estudioso de teatro es la de tratar el texto como si fuera un documento rigurosamente lógico cuyo... figura está en la escena de una manera constante. Es un verdadero tour de force de actuación. La pieza más reciente de Dragún, Hijos del terremoto, que según entendemos se está representando ahora en Buenos Aires con el título Arriba corazón...

  11. Humberto Duvauchelle: 3 décadas como profesional del teatro en Chile

    E-Print Network [OSTI]

    1986-04-01

    144 LATIN AMERICAN THEATRE REVIEW Humberto Duvauchelle: 3 décadas como profesional del teatro en Chile El 22 de noviembre, 1985, el conocido actor nacional cumplió 30 años de Servicio Publico en favor de la cultura y su difusión a todos los... varias obras de autores como Giraudoux, O'Neill, Calderón de la Barca, etc. Integrando al entonces célebre ITUCH (Instituto del Teatro de la Universidad de Chile) ya en la capital fué intérprete allí de una docena de obras, entre otras, Largo viaje...

  12. El concepto del honor en tres dramas de Calderon 

    E-Print Network [OSTI]

    Escabi, Maria Isabel

    1978-01-01

    , secrete ven an@a. Estos dramas tratan el terna del honor conyugal y los celos. Los tres son tragedias y tienen un argumento bastante parecido. En estos el marido que cree que su honor ha sido manchado, se venga de su esposa siguiendo las convenciones... XVII se hara un estudio especial sobre cate terna. Este sera el primer capitulo. En cate se estudiara la diferencia entre el honor y la honra, las caracterrsticas de un caballero noble u honrado, la convencion teatral deli codigo del honor, las...

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    Pellarolo, Silvia

    1997-10-01

    los escritores y actores de Buenos Aires" (18), documentadas por los periódicos de la época, que transcribe el crítico. La primera a la que hace referencia - según datos del periódico La Nación del 17 de mayo de 1895 - fue constituida en el Salón... esta época, cuyas obras de limitadas tiradas eran generalmente distribuidas gratis entre los amigos,3 los $20 por obra de los autores teatrales toman otra perspectiva. Para ubicarnos en los salarios de la época, recurrimos a los datos que da el...

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    laurea in memoria delle vittime del terremoto dell'Aquila patrocinato dall'Ordine Nazionale dei Geologi e dall'Associazione vittime universitarie del terremoto dell'Aquila del 6 aprile 2009. Il Direttore

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    2012-01-01

    III del sur, seguramente derivadas de su coeternidad, sobreencontramos algunas formas derivadas del estilo de MTLF,Mochica Tardío A   formas derivadas de Mochica Medio,

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    de Ita, Fernando

    1992-04-01

    la efervescencia política que se dio en México de 1982 a la fecha. El desgaste del sistema político mexicano se reflejó en muy diversos frentes, entre ellos el cultural, puesto que este aparato nació con el proyecto de modernización que inició el... sistema educativo; charrismo sindical;2 reivindicaciones legítimas del magisterio; y sobre todo, agotamiento del modelo político que venía imponiendo sus reglas desde 1947. La crisis general del país se reflejó en el teatro de los ochenta con el...

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    termodinamica lega la pressione p alla dipendenza dell'energia totale E del sistema dal volume V: p = -E

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    estos datos estimamos una densidad poblacional de 1 individuo por cada 15 km2, lo que sugiere que laTAMAÑO POBLACIONAL Y CONSERVACIÓN DEL JAGUAR EN LA RESERVA DE LA BIOSFERA DE CALAKMUL, CAMPECHE distribución y tamaño poblacional. Actual- mente se le considera una especie amenazada y en peligro de

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    Almeida Naveda, Eduardo

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    Rizk, Beatriz J.

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    luego. El título de algunos de los poemas elegidos y representados finalmente, explícitamente señalan su contenido, sin que tengamos que detenernos en ellos: "el hambre," "la bomba atómica," "el Caribe," "el sueño," "los usureros," "Aviso: Gran Zoo... de trasfondo como un elemento más, o de apuntamiento crítico como en el trabajo presentado por el equipo que dirigió Atahualpa del Cioppo; el texto de los poemas escogidos "Aviso," "Usureros," "Bomba Atómica" y "Cierre" fue cantados por un...

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    Milano-Bicocca, Università

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  17. DE-SOL-0003641 Amendment 002

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    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalent Bonding Low-Cost Ground8 Gas Hydrate12/21/2012 000001 3 1 13.

  18. DE-SOL-0003641 Amendment 003

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration would like submit theCovalent Bonding Low-Cost Ground8 Gas Hydrate12/21/2012 000001 3 1 13.3641

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    E-Print Network [OSTI]

    Ozer, N.

    2010-01-01

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    4. Contract Value: Initial Amount Current or Final Amount* Estimated Cost Fixed Price FeeProfit Total Value *Should reflect any contract value increases...

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    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page| Open Energy Information Serbia-Enhancing Capacity forSilicium deEnergy Information North| OpenSolution Jump

  3. SolFocus | Open Energy Information

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    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page| Open Energy Information Serbia-Enhancing Capacity forSilicium deEnergy Information North| OpenSolution

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    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QAsource History ViewMayo, Maryland:NPIProtectio1975)Energy Technology JumpWilliam County,| OpenEIPrismIntegris

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    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX E LISTStar EnergyLawler,CoalConcordia Electric Coop, IncIllinois)Consolidated

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    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoop Inc JumpHeter Battery Technology CoWanpingSilveiraSmallSmarrSnapping

  7. Sol e Suisse AG | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoop Inc JumpHeter Battery TechnologySocovoltaic Systems Jump to:SoftSuisse AG Jump to:

  8. Sol3g SL | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoop Inc JumpHeter Battery TechnologySocovoltaic Systems Jump to:SoftSuisse AG Jump

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    inquiete po" su contenido politico y social, sino por su poder de pene- tracion en la realidad; y mejor adn si es capaz de voltear ?18 la realidad a revels para mostrar camo es del otro lado. " George McMurray, in his analysis of Garcia Mdrquez and his...-342. Chester C. Christian, Jr. , "Realidad y fantasia: Sociologia de la novela actual en Hispanoam5rica, " MSS, draft, p. 14. Robert G. Mead, Jr. , "After the Boom, " Am5ricas, 30, No. 4, p. 7. 7 Jaime Mejia Duque, El otono del patriarca o crisis de la...

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