National Library of Energy BETA

Sample records for batch analytical batch

  1. Batch Jobs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room News PublicationsAudits & Inspections AuditsBarbara McClintock andBasics BasicsBasilBatch

  2. Example Hopper Batch Scripts

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    batch system must wait for the desired big memory nodes to become available. Running Hybrid MPIOpenMP Applications Hybrid MPIOpenMP Example: New Recommendations (recommended)...

  3. Thermal Analysis of Waste Glass Batches: Effect of Batch Makeup...

    Office of Scientific and Technical Information (OSTI)

    Book: Thermal Analysis of Waste Glass Batches: Effect of Batch Makeup on Gas-Evolving Reactions Citation Details In-Document Search Title: Thermal Analysis of Waste Glass Batches:...

  4. Data-driven batch schuduling

    SciTech Connect (OSTI)

    Bent, John [Los Alamos National Laboratory; Denehy, Tim [GOOGLE; Arpaci - Dusseau, Remzi [UNIV OF WISCONSIN; Livny, Miron [UNIV OF WISCONSIN; Arpaci - Dusseau, Andrea C [NON LANL

    2009-01-01

    In this paper, we develop data-driven strategies for batch computing schedulers. Current CPU-centric batch schedulers ignore the data needs within workloads and execute them by linking them transparently and directly to their needed data. When scheduled on remote computational resources, this elegant solution of direct data access can incur an order of magnitude performance penalty for data-intensive workloads. Adding data-awareness to batch schedulers allows a careful coordination of data and CPU allocation thereby reducing the cost of remote execution. We offer here new techniques by which batch schedulers can become data-driven. Such systems can use our analytical predictive models to select one of the four data-driven scheduling policies that we have created. Through simulation, we demonstrate the accuracy of our predictive models and show how they can reduce time to completion for some workloads by as much as 80%.

  5. Transferring Data from Batch Jobs at NERSC

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    from Batch Jobs Transferring Data from Batch Jobs Examples Once you are set up for automatic authentication (see HPSS Passwords) you can access HPSS within batch scripts. You...

  6. Submitting Batch Jobs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservation ofAlbuquerque|SensitiveAprilPhotonStructureStudentsSubmitting Batch Jobs

  7. Example Batch Scripts

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HABFES OctoberEvan Racah Evan Racah 1517546Has Evidence Example Batch

  8. NDA BATCH 2009-7

    SciTech Connect (OSTI)

    Lawrence Livermore National Laboratory

    2009-10-30

    The testing facility is LLNL plutonium facility segmented gamma scanner. 100% of the radioassay data in the batch data report is reviewed.

  9. Progressing batch hydrolysis process

    DOE Patents [OSTI]

    Wright, J.D.

    1985-01-10

    A progressive batch hydrolysis process is disclosed for producing sugar from a lignocellulosic feedstock. It comprises passing a stream of dilute acid serially through a plurality of percolation hydrolysis reactors charged with feed stock, at a flow rate, temperature and pressure sufficient to substantially convert all the cellulose component of the feed stock to glucose. The cooled dilute acid stream containing glucose, after exiting the last percolation hydrolysis reactor, serially fed through a plurality of pre-hydrolysis percolation reactors, charged with said feedstock, at a flow rate, temperature and pressure sufficient to substantially convert all the hemicellulose component of said feedstock to glucose. The dilute acid stream containing glucose is cooled after it exits the last prehydrolysis reactor.

  10. Batch compositions for cordierite ceramics

    DOE Patents [OSTI]

    Hickman, David L. (Big Flats, NY)

    1994-07-26

    Ceramic products consisting principally of cordierite and a method for making them are provided, the method employing batches comprising a mineral component and a chemical component, the mineral component comprising clay and talc and the chemical component consisting essentially of a combination of the powdered oxides, hydroxides, or hydrous oxides of magnesium, aluminum and silicon. Ceramics made by extrusion and firing of the batches can exhibit low porosity, high strength and low thermal expansion coefficients.

  11. NDA BATCH 2002-02

    SciTech Connect (OSTI)

    Lawrence Livermore National Laboratory

    2009-12-09

    QC sample results (daily background checks, 20-gram and 100-gram SGS drum checks) were within acceptable criteria established by WIPP's Quality Assurance Objectives for TRU Waste Characterization. Replicate runs were performed on 5 drums with IDs LL85101099TRU, LL85801147TRU, LL85801109TRU, LL85300999TRU and LL85500979TRU. All replicate measurement results are identical at the 95% confidence level as established by WIPP criteria. Note that the batch covered 5 weeks of SGS measurements from 23-Jan-2002 through 22-Feb-2002. Data packet for SGS Batch 2002-02 generated using gamma spectroscopy with the Pu Facility SGS unit is technically reasonable. All QC samples are in compliance with established control limits. The batch data packet has been reviewed for correctness, completeness, consistency and compliance with WIPP's Quality Assurance Objectives and determined to be acceptable. An Expert Review was performed on the data packet between 28-Feb-02 and 09-Jul-02 to check for potential U-235, Np-237 and Am-241 interferences and address drum cases where specific scan segments showed Se gamma ray transmissions for the 136-keV gamma to be below 0.1 %. Two drums in the batch showed Pu-238 at a relative mass ratio more than 2% of all the Pu isotopes.

  12. EFFECT OF GLASS-BATCH MAKEUP ON...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    rate of heat-transfer from molten glass to the batch blanket and the kinetics of various chemical reactions and phase transitions jointly control the batch- to-glass conversion...

  13. Batch-mode Supervised Learning Linear regression

    E-Print Network [OSTI]

    Wehenkel, Louis

    Batch-mode Supervised Learning Linear regression Applied inductive learning - Lecture 3 Louis (& Pierre Geurts)AIA... (1/19) #12;Batch-mode Supervised Learning Linear regression Batch-mode Supervised Learning Linear regression Least mean square error solution Regularization and algorithmics Residual

  14. Adding coal dust to coal batch

    SciTech Connect (OSTI)

    V.S. Shved; A.V.Berezin [OAO Koks, Kemerovo (Russian Federation)

    2009-05-15

    The granulometric composition of coke dust from the dry-slaking machine is determined. The influence of additions of 3-7% coke dust on the quality of industrial coking batch and the coke obtained by box coking is estimated. Adding 1% coke dust to coking batch does not markedly change the coke quality. Industrial equipment for the supply of dry-slaking dust to the batch is described.

  15. CASCADE OPTIMIZATION AND CONTROL OF BATCH REACTORS

    E-Print Network [OSTI]

    Jutan, Arthur

    CASCADE OPTIMIZATION AND CONTROL OF BATCH REACTORS Xiangming Hua, Sohrab Rohani and Arthur Jutan ajutan@uwo.ca Abstract: In this study, a cascade closed-loop optimization and control strategy for batch reactor. Using model reduction a cascade system is developed, which can effectively combine optimization

  16. Method and apparatus for melting glass batch

    DOE Patents [OSTI]

    Fassbender, Alexander G. (Kennewick, WA); Walkup, Paul C. (Richland, WA); Mudge, Lyle K. (Richland, WA)

    1988-01-01

    A glass melting system involving preheating, precalcining, and prefluxing of batch materials prior to injection into a glass furnace. The precursors are heated by convection rather than by radiation in present furnaces. Upon injection into the furnace, batch materials are intimately coated with molten flux so as to undergo or at least begin the process of dissolution reaction prior to entering the melt pool.

  17. Biological Hydrogen Production Measured in Batch Anaerobic

    E-Print Network [OSTI]

    Biological Hydrogen Production Measured in Batch Anaerobic Respirometers B R U C E E . L O G A N The biological production of hydrogen from the fermentation of different substrates was examined in batch tests product for a sugar (4). The accumulation of hydrogen and other degradation byproducts during fermen

  18. Analysis and Control of Heteroazeotropic Batch Distillation

    E-Print Network [OSTI]

    Skogestad, Sigurd

    , called an entrainer, has to be added to facilitate separation and enhance distillation. When a heavy entrainer is added continuously in the top section of the batch column the process is called extractive batch distillation. When an entrainer is added batchwise to the original mixture we simply call

  19. Dynamic Control of Serial-batch Processing Systems 

    E-Print Network [OSTI]

    Cerekci, Abdullah

    2010-01-14

    ......................... 133 APPENDIX C: PAIRED-T TEST RESULTS FOR CHAPTER V .......................... 144 VITA ......................................................................................................................... 154 ix LIST OF FIGURES FIGURE... processor?s queue to improve the performance of the batch processor. 6 The assumptions relating to the serial-batch processor system are as follows: There are N incompatible product types being processed by the serial-batch processor system. Batch...

  20. Your Unanswered Questions…. Answered- Batch 2

    Broader source: Energy.gov [DOE]

    Secretary Chu hosted an online town hall to discuss President Obama's clean energy innovation agenda -- and while he was able to answer about 10 questions submitted online during the event, we received more than 200! Here is our second batch of questions and answers.

  1. Batch” Kinetics in Flow: Online IR Analysis and Continuous Control

    E-Print Network [OSTI]

    Moore, Jason S.

    Currently, kinetic data is either collected under steady-state conditions in flow or by generating time-series data in batch. Batch experiments are generally considered to be more suitable for the generation of kinetic ...

  2. Batch load anaerobic digestion of dairy manure 

    E-Print Network [OSTI]

    Egg, Richard P

    1979-01-01

    and medium size dairy operations unless the pro- cess can be made more efficient or some other economic benefit can be derived from the manure. A recent study indicated that a batch load process might be more efficient in waste stabilization and biogas... rate of biogas production was 0. 69 liters biogas/liter digester/ day. This volumetric biogas production increased with increasing influent total solids concentration. Influent concentration had little effect on other biogas production parameters...

  3. Uranium and Strontium Batch Sorption and Diffusion Kinetics into...

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Uranium and Strontium Batch Sorption and Diffusion Kinetics into Mesoporous Silica Friday, February 27, 2015 Figure 1 Figure 1. Transmission electron microscopy images of (A)...

  4. TANK 50 BATCH 0 SALTSTONE FORMULATION CONFIRMATION

    SciTech Connect (OSTI)

    Langton, C.

    2006-06-05

    Savannah River National Laboratory (SRNL) personnel were requested to confirm the Tank 50 Batch 0 grout formulation per Technical Task Request, SSF-TTR-2006-0001 (task 1 of 2) [1]. Earlier Batch 0 formulation testing used a Tank 50 sample collected in September 2005 and is described elsewhere [2]. The current testing was performed using a sample of Tank 50 waste collected in May 2006. This work was performed according to the Technical Task and Quality Assurance Plan (TT/QAP), WSRC-RP-2006-00594 [3]. The salt solution collected from Tank 50 in May 2006 contained approximately 3 weight percent more solids than the sample collected in September 2005. The insoluble solids took longer to settle in the new sample which was interpreted as indicating finer particles in the current sample. The saltstone formulation developed for the September 2005 Tank 50 Batch 0 sample was confirmed for the May 2006 sample with one minor exception. Saltstone prepared with the Tank 50 sample collected in May 2006 required 1.5 times more Daratard 17 set retarding admixture than the saltstone prepared with the September In addition, a sample prepared with lower shear mixing (stirring with a spatula) had a higher plastic viscosity (57 cP) than samples made with higher shear mixing in a blender (23cP). The static gel times of the saltstone slurries made with low shear mixing were also shorter ({approx}32 minutes) than those for comparable samples made in the blender ({approx}47 minutes). The addition of the various waste streams (ETP, HEU-HCAN, and GPE-HCAN) to Tank 50 from September 2005 to May 2006 has increased the amount of set retarder, Daratard 17, required for processing saltstone slurries through the Saltstone facility. If these streams are continued to be added to Tank 50, the quantity of admixtures required to maintain the same processing conditions for the Saltstone facility will probably change and additional testing is recommended to reconfirm the Tank 50 Saltstone formulation.

  5. Real-time Dynamic Optimization of Batch Crystallization Processes

    E-Print Network [OSTI]

    Van den Hof, Paul

    process. The seeded fed-batch crystallizer is represented by a nonlinear moment model. An optimal controlReal-time Dynamic Optimization of Batch Crystallization Processes Ali Mesbah, , Alex N. Kalbasenka-time implementations of the proposed strategy reveal the effectiveness of closed-loop optimal control

  6. MODEL-BASED OPTIMAL OPERATION OF SEEDED BATCH CRYSTALLISATION PROCESSES

    E-Print Network [OSTI]

    Van den Hof, Paul

    .mesbah@tudelft.nl Dynamic optimization is applied for optimal control of a semi-industrial batch crystallisation process of the open-loop optimal control due to plant-model mismatch, unmeasured process disturbances, irreproducibleMODEL-BASED OPTIMAL OPERATION OF SEEDED BATCH CRYSTALLISATION PROCESSES A. Mesbah1, 2 , J. Landlust

  7. MELTING OF GLASS BATCH: MODEL FOR MULTIPLE OVERLAPPING GAS-EVOLVING...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: MELTING OF GLASS BATCH: MODEL FOR MULTIPLE OVERLAPPING GAS-EVOLVING REACTIONS Citation Details In-Document Search Title: MELTING OF GLASS BATCH: MODEL FOR MULTIPLE...

  8. CHOP: Performance Optimization for Batched Schema Evolution 1

    E-Print Network [OSTI]

    Claypool, Kajal

    of schema evolution primitives as well as for the merging of database modifications of primitivesCHOP: Performance Optimization for Batched Schema Evolution 1 Kajal T. Claypool, Elke A on Schema Evolution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 1.2 Our Proposed

  9. Dynamic Control for Batch Process Systems Using Stochastic Utility Evaluation 

    E-Print Network [OSTI]

    Park, Hongsuk

    2012-10-19

    Most research studies in the batch process control problem are focused on optimizing system performance. The methods address the problem by minimizing single criterion such as cycle time and tardiness, or bi-criteria such ...

  10. Batch polymerization of styrene initiated by alkyl lithiums 

    E-Print Network [OSTI]

    Desai, Rashmi R

    1970-01-01

    BATCH POLYYIERIZATION OF STYRENE INITIATED BY ALKYL LITHIUMS A Thesis by RASHMI R. DESAI Submitted to the Graduate College of Texas ASM University partial fulfillment of the requirement for the degree of MASTER OF SCIFNCE May 1970 Major... Subject: Chemical Fngineering BATCH POLYMERI2ATION OF STYRENE INITIATED BY ALKYL LITHIUMS A Thesis by RASHMI R. DESAI Approved as to style and content by: / . I ?ii' (Chairman of Committee) (Head of Depar tment) ( ember) (Member) May 1970 111...

  11. Temperature effects on seawater batch activated sludge systems 

    E-Print Network [OSTI]

    Wigley, Henry Albert

    1972-01-01

    TEMPERATURE EFFECTS ON SEAMATER BATCH ACTIVATED SLUDGE SYSTEMS A Thesis by HENRY ALBERT WIGLEY, JR. Submitted to the Graduate Colleqe of Texas A&M University in partial fulfillment of the requirement for the deqree of MASTER OF SCIENCE May... 1972 Major Subject: Civil Engineerinq TEMPERATURE EFFECTS ON SEAWATER BATCH ACTIVATED SLUDGE SYSTEMS A Thesis by HENRY ALBERT WIGLEY, JR. Approved as to style and content by: C ai rman o ommi ttee Head of D partmen Member Member May 1972...

  12. SLUDGE BATCH VARIABILITY STUDY WITH FRIT 418

    SciTech Connect (OSTI)

    Johnson, F.; Edwards, T.

    2010-11-29

    The Defense Waste Processing Facility (DWPF) initiated processing Sludge Batch 6 (SB6) in the summer of 2010. In support of processing, the Savannah River National Laboratory (SRNL) provided a recommendation to utilize Frit 418 to process SB6. This recommendation was based on assessments of the compositional projections for SB6 available at the time from the Liquid Waste Organization (LWO) and SRNL (using a model-based approach). To support qualification of SB6, SRNL executed a variability study to assess the applicability of the current durability models for SB6. The durability models were assessed over the expected Frit 418-SB6 composition range. Seventeen glasses were selected for the variability study based on the sludge projections used in the frit recommendation. Five of the glasses are based on the centroid of the compositional region, spanning a waste loading (WL) range of 32 to 40%. The remaining twelve glasses are extreme vertices (EVs) of the sludge region of interest for SB6 combined with Frit 418 and are all at 36% WL. These glasses were fabricated and characterized using chemical composition analysis, X-ray diffraction (XRD) and the Product Consistency Test (PCT). After initiating the SB6 variability study, the measured composition of the SB6 Tank 51 qualification glass produced at the SRNL Shielded Cells Facility indicated that thorium was present in the glass at an appreciable concentration (1.03 wt%), which made it a reportable element for SB6. This concentration of ThO{sub 2} resulted in a second phase of experimental studies. Five glasses were formulated that were based on the centroid of the new sludge compositional region combined with Frit 418, spanning a WL range of 32 to 40%. These glasses were fabricated and characterized using chemical composition analysis and the PCT. Based on the measured PCT response, all of the glasses (with and without thorium) were acceptable with respect to the Environmental Assessment (EA) reference glass regardless of thermal history. All of the normalized boron releases were less than 1 g/L. While all of the targeted glass compositions were predictable with respect to the Product Composition Control System (PCCS) models for durability, a small number of the measured glass compositions were located outside of the lower prediction limit indicating poorer durability than what was actually measured. These unpredictable glasses were in the same lithium metaborate (LM) preparation block during the chemical analyses, which resulted in measured compositions that were not representative of the target compositions. A review of the data did not indicate a clear cause for the problem. Re-digestion and re-measurement of three glasses from this preparation block yielded glass compositions closer to the target values and predicted PCT responses within the PCCS model uncertainty. Therefore, it is believed that the glasses were correctly fabricated and the targeted compositions are closer representations of the true compositions. Per the requirements of the DWPF Glass Product Control Program, the PCCS durability models have been shown to be applicable for the SB6/Frit 418 glass system. PCT results from the glasses fabricated as part of the variability study were shown to be predictable and/or acceptable with respect to the DWPF PCCS models. In addition, the inclusion of ThO{sub 2} was shown to have minimal impact on the acceptability and predictability of the variability study glasses.

  13. Batch Mode Stochastic-Based Robust Dynamic Resource Allocation

    E-Print Network [OSTI]

    Maciejewski, Anthony A.

    Batch Mode Stochastic-Based Robust Dynamic Resource Allocation in a Heterogeneous Computing System in system parameters is common. Robustness can be defined as the degree to which a system can function in data size and content. Determining a resource allocation that accounts for this uncertainty

  14. REPORTABLE RADIONUCLIDES IN DWPF SLUDGE BATCH 7A (MACROBATCH 8)

    SciTech Connect (OSTI)

    Reboul, S.; Diprete, D.; Click, D.; Bannochie, C.

    2011-12-20

    The Waste Acceptance Product Specifications (WAPS) 1.2 require that the waste producer 'shall report the curie inventory of radionuclides that have half-lives longer than 10 years and that are, or will be, present in concentrations greater than 0.05 percent of the total inventory for each waste type indexed to the years 2015 and 3115.' As part of the strategy to meet WAPS 1.2, the Defense Waste Processing Facility (DWPF) will report for each waste type all radionuclides that have half-lives longer than 10 years and contribute greater than 0.01 percent of the total curie inventory from the time of production through the 1100 year period from 2015 through 3115. The initial list of radionuclides to be reported is based on the design-basis glass identified in the Waste Form Compliance Plan (WCP) and Waste Form Qualification Report. However, it is required that the list be expanded if other radionuclides with half-lives greater than 10 years are identified that meet the 'greater than 0.01% of the curie inventory' criterion. Specification 1.6 of the WAPS, International Atomic Energy Agency Safeguards Reporting for High Level Waste (HLW), requires that the ratio by weights of the following uranium and plutonium isotopes be reported: U-233, U-234, U-235, U-236, and U-238; and Pu-238, Pu-239, Pu-240, Pu-241, and Pu-242. Therefore, the complete list of reportable radionuclides must also include these sets of U and Pu isotopes - and the U and Pu isotopic mass distributions must be identified. The DWPF receives HLW sludge slurry from Savannah River Site (SRS) Tank 40. For Sludge Batch 7a (SB7a), the waste in Tank 40 contained a blend of the heel from Sludge Batch 6 (SB6) and the Sludge Batch 7 (SB7) material transferred to Tank 40 from Tank 51. This sludge blend is also referred to as Macrobatch 8. Laboratory analyses of a Tank 40 sludge sample were performed to quantify the concentrations of pertinent radionuclides in the SB7a waste. Subsequently, radiological decay and in-growth were calculated over the time period from 2015 to 3115. This provided a basis for characterizing the radionuclide content of SB7a over time and for identifying the 'reportable radionuclides.' Details of the characterization methodology and the analytical results are the focus of this report. This work was performed at the request of the Waste Solidification Engineering Department of Savannah River Remediation, initiated via Technical Task Request (TTR) HLW-DWPF-TTR-2010-0031. A minor revision in the reporting requirements was requested via a subsequent email communication. The work was conducted in accordance with the protocols identified in Task Technical and Quality Assurance Plan SRNL-RP-2010-01218 and Analytical Study Plan SRNL-RP-2010-01219. All of the raw data related to this scope have been recorded in laboratory notebook SRNL-NB-2011-00061. The overall goal of this task was to characterize the radionuclide content of the SB7a waste sufficiently to meet the WAPS and DWPF reporting requirements. The specific objectives were: (1) Quantify the current concentrations of all radionuclides impacting (or potentially-impacting) the total curie content between calendar years 2011 and 3115. Also quantify the current concentrations of other radionuclides specifically requested in the TTR or required by the WAPS. (2) Calculate future concentrations of decayed and in-grown radionuclides impacting the total curie content between calendar years 2015 and 3115; (3) Identify as 'reportable' all radionuclides contributing {ge} 0.01% of the total curie content from 2015 to 3115 and having half-lives {ge} 10 years.

  15. HIGH LEVEL WASTE SLUDGE BATCH 4 VARIABILITY STUDY

    SciTech Connect (OSTI)

    Fox, K; Tommy Edwards, T; David Peeler, D; David Best, D; Irene Reamer, I; Phyllis Workman, P

    2006-10-02

    The Defense Waste Processing Facility (DWPF) is preparing for vitrification of High Level Waste (HLW) Sludge Batch 4 (SB4) in early FY2007. To support this process, the Savannah River National Laboratory (SRNL) has provided a recommendation to utilize Frit 503 for vitrifying this sludge batch, based on the composition projection provided by the Liquid Waste Organization on June 22, 2006. Frit 418 was also recommended for possible use during the transition from SB3 to SB4. A critical step in the SB4 qualification process is to demonstrate the applicability of the durability models, which are used as part of the DWPF's process control strategy, to the glass system of interest via a variability study. A variability study is an experimentally-driven assessment of the predictability and acceptability of the quality of the vitrified waste product that is anticipated from the processing of a sludge batch. At the DWPF, the durability of the vitrified waste product is not directly measured. Instead, the durability is predicted using a set of models that relate the Product Consistency Test (PCT) response of a glass to the chemical composition of that glass. In addition, a glass sample is taken during the processing of that sludge batch, the sample is transmitted to SRNL, and the durability is measured to confirm acceptance. The objective of a variability study is to demonstrate that these models are applicable to the glass composition region anticipated during the processing of the sludge batch - in this case the Frit 503 - SB4 compositional region. The success of this demonstration allows the DWPF to confidently rely on the predictions of the durability/composition models as they are used in the control of the DWPF process.

  16. A batch reactor heat recovery challenge problem Johannes Jschke, Sigurd Skogestad

    E-Print Network [OSTI]

    Skogestad, Sigurd

    A batch reactor heat recovery challenge problem Johannes Jäschke, Sigurd Skogestad Department a challenge problem for maximizing the heat recovery in a heat exchanger network connected to a set of batch

  17. pV3 Batch User's Reference Manual for use with the following workstations

    E-Print Network [OSTI]

    Peraire, Jaime

    pV3 Batch User's Reference Manual Rev. 2.05 for use with the following workstations: Compaq ALPHAs. 2 #12;Contents 1 Introduction 4 2 pV3 Batch Server 5 2.1 Batch Server Startup.4 Advanced Programming . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7 3 pV3 Post

  18. Batch drilling program cuts time, costs for Liuhua development

    SciTech Connect (OSTI)

    Gray, G.E.; Hall, K.H.; Mu, H.C.

    1996-08-12

    The efficiency of batch drilling operations and the appropriate use of technology, teamwork, and thorough planning helped cut several days off the time to drill each of 10 subsea wells for the Liuhua 11-1 development project in the South China Sea. The overall development program calls for drilling and completing 20 subsea horizontal wells. The rig-of-opportunity phase was the initial phase of this development and used a contract rig to establish the subsea wellhead array and initiate drilling of the development wells. The wellhead array was the first critical step. It was the foundation for the building block construction process used to create Liuhua`s subsea production system on the seabed. The paper discusses conductor operations, batch drilling operations, surface hole section, intermediate and production hole sections, the ten wells, application of technology, and overall results.

  19. Tank 40 Final Sludge Batch 8 Chemical Characterization Results

    SciTech Connect (OSTI)

    Bannochie, Christopher J.

    2013-09-19

    A sample of Sludge Batch 8 (SB8) was pulled from Tank 40 in order to obtain radionuclide inventory analyses necessary for compliance with the Waste Acceptance Product Specifications (WAPS). The SB8 WAPS sample was also analyzed for chemical composition, including noble metals, and fissile constituents, and these results are reported here. These analyses along with the WAPS radionuclide analyses will help define the composition of the sludge in Tank 40 that is currently being fed to the Defense Waste Processing Facility (DWPF) as SB8. At SRNL, the 3-L Tank 40 SB8 sample was transferred from the shipping container into a 4-L high density polyethylene bottle and solids were allowed to settle. Supernate was then siphoned off and circulated through the shipping container to complete the transfer of the sample. Following thorough mixing of the 3-L sample, a 553 g sub-sample was removed. This sub-sample was then utilized for all subsequent slurry sample preparations. Eight separate aliquots of the slurry were digested, four with HNO{sub 3}/HCl (aqua regia) in sealed Teflon(r) vessels and four with NaOH/Na{sub 2}O{sub 2} (alkali or peroxide fusion) using Zr crucibles. Two Analytical Reference Glass - 1 (ARG-1) standards were digested along with a blank for each preparation. Each aqua regia digestion and blank was diluted to 1:100 mL with deionized water and submitted to Analytical Development (AD) for inductively coupled plasma - atomic emission spectroscopy (ICP-AES) analysis, inductively coupled plasma - mass spectrometry (ICP-MS) analysis, atomic absorption spectroscopy (AA) for As and Se, and cold vapor atomic absorption spectroscopy (CV-AA) for Hg. Equivalent dilutions of the alkali fusion digestions and blank were submitted to AD for ICP-AES analysis. Tank 40 SB8 supernate was collected from a mixed slurry sample in the SRNL Shielded Cells and submitted to AD for ICP-AES, ion chromatography (IC), total base/free OH-/other base, total inorganic carbon/total organic carbon (TIC/TOC) analyses. Weighted dilutions of slurry were submitted for IC, TIC/TOC, and total base/free OH-/other base analyses. Activities for U-233, U-235, and Pu-239 were determined from the ICP-MS data for the aqua regia digestions of the Tank 40 WAPS slurry using the specific activity of each isotope. The Pu-241 value was determined from a Pu-238/-241 method developed by SRNL AD and previously described.

  20. Microsoft Word - FINAL Rocky Flats LBNL report Batch #1.docx

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal Gas &SCE-SessionsSouthReport for the t-) S/,,5 'a C O M P R EH2 UMTRCAthe First Batch of

  1. Increased CPC batch size study for Tank 42 sludge in the Defense Waste Processing Facility

    SciTech Connect (OSTI)

    Daniel, W.E.

    2000-01-06

    A series of experiments have been completed at TNX for the sludge-only REDOX adjusted flowsheet using Tank 42 sludge simulant in response to the Technical Task Request HLW/DWPT/TTR-980013 to increase CPC batch sizes. By increasing the initial SRAT batch size, a melter feed batch at greater waste solids concentration can be prepared and thus increase melter output per batch by about one canister. The increased throughput would allow DWPF to dispose of more waste in a given time period thus shortening the overall campaign.

  2. FLOWSHEET FOR ALUMINUM REMOVAL FROM SLUDGE BATCH 6

    SciTech Connect (OSTI)

    Pike, J; Jeffrey Gillam, J

    2008-12-17

    Samples of Tank 12 sludge slurry show a substantially larger fraction of aluminum than originally identified in sludge batch planning. The Liquid Waste Organization (LWO) plans to formulate Sludge Batch 6 (SB6) with about one half of the sludge slurry in Tank 12 and one half of the sludge slurry in Tank 4. LWO identified aluminum dissolution as a method to mitigate the effect of having about 50% more solids in High Level Waste (HLW) sludge than previously planned. Previous aluminum dissolution performed in a HLW tank in 1982 was performed at approximately 85 C for 5 days and dissolved nearly 80% of the aluminum in the sludge slurry. In 2008, LWO successfully dissolved 64% of the aluminum at approximately 60 C in 46 days with minimal tank modifications and using only slurry pumps as a heat source. This report establishes the technical basis and flowsheet for performing an aluminum removal process in Tank 51 for SB6 that incorporates the lessons learned from previous aluminum dissolution evolutions. For SB6, aluminum dissolution process temperature will be held at a minimum of 65 C for at least 24 days, but as long as practical or until as much as 80% of the aluminum is dissolved. As planned, an aluminum removal process can reduce the aluminum in SB6 from about 84,500 kg to as little as 17,900 kg with a corresponding reduction of total insoluble solids in the batch from 246,000 kg to 131,000 kg. The extent of the reduction may be limited by the time available to maintain Tank 51 at dissolution temperature. The range of dissolution in four weeks based on the known variability in dissolution kinetics can range from 44 to more than 80%. At 44% of the aluminum dissolved, the mass reduction is approximately 1/2 of the mass noted above, i.e., 33,300 kg of aluminum instead of 66,600 kg. Planning to reach 80% of the aluminum dissolved should allow a maximum of 81 days for dissolution and reduce the allowance if test data shows faster kinetics. 47,800 kg of the dissolved aluminum will be stored in Tank 8 and 21,000 kg will be stored in saltcake via evaporation. Up to 77% of the total aluminum planned for SB6 may be removed via aluminum dissolution. Storage of the aluminum-laden supernate in Tank 8 will require routine evaluation of the free hydroxide concentration in order to maintain aluminum in solution. Periodic evaluation will be established on concurrent frequency with corrosion program samples as previously established for aluminum-laden supernate from SB5 that is stored in Tank 11.

  3. STATISTICAL EVALUATION OF SMALL SCALE MIXING DEMONSTRATION SAMPLING AND BATCH TRANSFER PERFORMANCE - 12093

    SciTech Connect (OSTI)

    GREER DA; THIEN MG

    2012-01-12

    The ability to effectively mix, sample, certify, and deliver consistent batches of High Level Waste (HLW) feed from the Hanford Double Shell Tanks (DST) to the Waste Treatment and Immobilization Plant (WTP) presents a significant mission risk with potential to impact mission length and the quantity of HLW glass produced. DOE's Tank Operations Contractor, Washington River Protection Solutions (WRPS) has previously presented the results of mixing performance in two different sizes of small scale DSTs to support scale up estimates of full scale DST mixing performance. Currently, sufficient sampling of DSTs is one of the largest programmatic risks that could prevent timely delivery of high level waste to the WTP. WRPS has performed small scale mixing and sampling demonstrations to study the ability to sufficiently sample the tanks. The statistical evaluation of the demonstration results which lead to the conclusion that the two scales of small DST are behaving similarly and that full scale performance is predictable will be presented. This work is essential to reduce the risk of requiring a new dedicated feed sampling facility and will guide future optimization work to ensure the waste feed delivery mission will be accomplished successfully. This paper will focus on the analytical data collected from mixing, sampling, and batch transfer testing from the small scale mixing demonstration tanks and how those data are being interpreted to begin to understand the relationship between samples taken prior to transfer and samples from the subsequent batches transferred. An overview of the types of data collected and examples of typical raw data will be provided. The paper will then discuss the processing and manipulation of the data which is necessary to begin evaluating sampling and batch transfer performance. This discussion will also include the evaluation of the analytical measurement capability with regard to the simulant material used in the demonstration tests. The paper will conclude with a discussion of the analysis results illustrating the relationship between the pre-transfer samples and the batch transfers, which support the recommendation regarding the need for a dedicated feed sampling facility.

  4. Uranium Adsorption on Granular Activated Carbon – Batch Testing

    SciTech Connect (OSTI)

    Parker, Kent E.; Golovich, Elizabeth C.; Wellman, Dawn M.

    2013-09-26

    The uranium adsorption performance of two activated carbon samples (Tusaar Lot B-64, Tusaar ER2-189A) was tested using unadjusted source water from well 299-W19-36. These batch tests support ongoing performance optimization efforts to use the best material for uranium treatment in the Hanford Site 200 West Area groundwater pump-and-treat system. A linear response of uranium loading as a function of the solution-to-solid ratio was observed for both materials. Kd values ranged from ~380,000 to >1,900,000 ml/g for the B-64 material and ~200,000 to >1,900,000 ml/g for the ER2-189A material. Uranium loading values ranged from 10.4 to 41.6 ?g/g for the two Tusaar materials.

  5. Admission Control and Pricing in a Queue with Batch Arrivals Utku Yildirim John J. Hasenbein1

    E-Print Network [OSTI]

    Hasenbein, John

    , for example, setting the price high enough such that it is not advantageous for the incoming batch to enter for a revenue maximizing controller. Keywords: batch queues, pricing, admission control, Markov decision and that paper lists various real life examples where pricing might be helpful to control a queue. Naor [15

  6. SLUDGE BATCH 7 PREPARATION TANK 4 AND 12 CHARACTERIZATION

    SciTech Connect (OSTI)

    Bannochie, C.; Click, D.; Pareizs, J.

    2010-05-21

    Samples of PUREX sludge from Tank 4 and HM sludge from Tank 12 were characterized in preparation for Sludge Batch 7 (SB7) formulation in Tank 51. SRNL analyses on Tank 4 and Tank 12 were requested in separate Technical Assistance Requests (TAR). The Tank 4 samples were pulled on January 19, 2010 following slurry operations by F-Tank Farm. The Tank 12 samples were pulled on February 9, 2010 following slurry operations by H-Tank Farm. At the Savannah River National Laboratory (SRNL), two 200 mL dip samples of Tank 4 and two 200 mL dip samples of Tank 12 were received in the SRNL Shielded Cells. Each tank's samples were composited into clean 500 mL polyethylene storage bottles and weighed. The composited Tank 4 sample was 428.27 g and the composited Tank 12 sample was 502.15 g. As expected there are distinct compositional differences between Tank 4 and Tank 12 sludges. The Tank 12 slurry is much higher in Al, Hg, Mn, and Th, and much lower in Fe, Ni, S, and U than the Tank 4 slurry. The Tank 4 sludge definitely makes the more significant contribution of S to any sludge batch blend. This S, like that observed during SB6 washing, is best monitored by looking at the total S measured by digesting the sample and analyzing by inductively coupled plasma - atomic emission spectroscopy (ICPAES). Alternatively, one can measure the soluble S by ICP-AES and adjust the value upward by approximately 15% to have a pretty good estimate of the total S in the slurry. Soluble sulfate measurements by ion chromatography (IC) will be biased considerably lower than the actual total S, the difference being due to the non-sulfate soluble S and the undissolved S. Tank 12 sludge is enriched in U-235, and hence samples transferred into SRNL from the Tank Farm will need to be placed on the reportable special nuclear material inventory and tracked for total U per SRNL procedure requirements.

  7. SLUDGE BATCH 7B QUALIFICATION ACTIVITIES WITH SRS TANK FARM SLUDGE

    SciTech Connect (OSTI)

    Pareizs, J.; Click, D.; Lambert, D.; Reboul, S.

    2011-11-16

    Waste Solidification Engineering (WSE) has requested that characterization and a radioactive demonstration of the next batch of sludge slurry - Sludge Batch 7b (SB7b) - be completed in the Shielded Cells Facility of the Savannah River National Laboratory (SRNL) via a Technical Task Request (TTR). This characterization and demonstration, or sludge batch qualification process, is required prior to transfer of the sludge from Tank 51 to the Defense Waste Processing Facility (DWPF) feed tank (Tank 40). The current WSE practice is to prepare sludge batches in Tank 51 by transferring sludge from other tanks. Discharges of nuclear materials from H Canyon are often added to Tank 51 during sludge batch preparation. The sludge is washed and transferred to Tank 40, the current DWPF feed tank. Prior to transfer of Tank 51 to Tank 40, SRNL typically simulates the Tank Farm and DWPF processes with a Tank 51 sample (referred to as the qualification sample). With the tight schedule constraints for SB7b and the potential need for caustic addition to allow for an acceptable glass processing window, the qualification for SB7b was approached differently than past batches. For SB7b, SRNL prepared a Tank 51 and a Tank 40 sample for qualification. SRNL did not receive the qualification sample from Tank 51 nor did it simulate all of the Tank Farm washing and decanting operations. Instead, SRNL prepared a Tank 51 SB7b sample from samples of Tank 7 and Tank 51, along with a wash solution to adjust the supernatant composition to the final SB7b Tank 51 Tank Farm projections. SRNL then prepared a sample to represent SB7b in Tank 40 by combining portions of the SRNL-prepared Tank 51 SB7b sample and a Tank 40 Sludge Batch 7a (SB7a) sample. The blended sample was 71% Tank 40 (SB7a) and 29% Tank 7/Tank 51 on an insoluble solids basis. This sample is referred to as the SB7b Qualification Sample. The blend represented the highest projected Tank 40 heel (as of May 25, 2011), and thus, the highest projected noble metals content for SB7b. Characterization was performed on the Tank 51 SB7b samples and SRNL performed DWPF simulations using the Tank 40 SB7b material. This report documents: (1) The preparation and characterization of the Tank 51 SB7b and Tank 40 SB7b samples. (2) The performance of a DWPF Chemical Process Cell (CPC) simulation using the SB7b Tank 40 sample. The simulation included a Sludge Receipt and Adjustment Tank (SRAT) cycle, where acid was added to the sludge to destroy nitrite and reduce mercury, and a Slurry Mix Evaporator (SME) cycle, where glass frit was added to the sludge in preparation for vitrification. The SME cycle also included replication of five canister decontamination additions and concentrations. Processing parameters were based on work with a nonradioactive simulant. (3) Vitrification of a portion of the SME product and characterization and durability testing (as measured by the Product Consistency Test (PCT)) of the resulting glass. (4) Rheology measurements of the SRAT receipt, SRAT product, and SME product. This program was controlled by a Task Technical and Quality Assurance Plan (TTQAP), and analyses were guided by an Analytical Study Plan. This work is Technical Baseline Research and Development (R&D) for the DWPF. It should be noted that much of the data in this document has been published in interoffice memoranda. The intent of this technical report is bring all of the SB7b related data together in a single permanent record and to discuss the overall aspects of SB7b processing.

  8. Sample Results from Routine Salt Batch 7 Samples

    SciTech Connect (OSTI)

    Peters, T.

    2015-05-13

    Strip Effluent Hold Tank (SEHT) and Decontaminated Salt Solution Hold Tank (DSSHT) samples from several of the “microbatches” of Integrated Salt Disposition Project (ISDP) Salt Batch (“Macrobatch”) 7B have been analyzed for 238Pu, 90Sr, 137Cs, Inductively Coupled Plasma Emission Spectroscopy (ICPES), and Ion Chromatography Anions (IC-A). The results from the current microbatch samples are similar to those from earlier samples from this and previous macrobatches. The Actinide Removal Process (ARP) and the Modular Caustic-Side Solvent Extraction Unit (MCU) continue to show more than adequate Pu and Sr removal, and there is a distinct positive trend in Cs removal, due to the use of the Next Generation Solvent (NGS). The Savannah River National Laboratory (SRNL) notes that historically, most measured Concentration Factor (CF) values during salt processing have been in the 12-14 range. However, recent processing gives CF values closer to 11. This observation does not indicate that the solvent performance is suffering, as the Decontamination Factor (DF) has still maintained consistently high values. Nevertheless, SRNL will continue to monitor for indications of process upsets. The bulk chemistry of the DSSHT and SEHT samples do not show any signs of unusual behavior.

  9. Methods for batch fabrication of cold cathode vacuum switch tubes

    DOE Patents [OSTI]

    Walker, Charles A. (Albuquerque, NM); Trowbridge, Frank R. (Albuquerque, NM)

    2011-05-10

    Methods are disclosed for batch fabrication of vacuum switch tubes that reduce manufacturing costs and improve tube to tube uniformity. The disclosed methods comprise creating a stacked assembly of layers containing a plurality of adjacently spaced switch tube sub-assemblies aligned and registered through common layers. The layers include trigger electrode layer, cathode layer including a metallic support/contact with graphite cathode inserts, trigger probe sub-assembly layer, ceramic (e.g. tube body) insulator layer, and metallic anode sub-assembly layer. Braze alloy layers are incorporated into the stacked assembly of layers, and can include active metal braze alloys or direct braze alloys, to eliminate costs associated with traditional metallization of the ceramic insulator layers. The entire stacked assembly is then heated to braze/join/bond the stack-up into a cohesive body, after which individual switch tubes are singulated by methods such as sawing. The inventive methods provide for simultaneously fabricating a plurality of devices as opposed to traditional methods that rely on skilled craftsman to essentially hand build individual devices.

  10. SLUDGE BATCH 6/TANK 51 SIMULANT CHEMICAL PROCESS CELL SIMULATIONS

    SciTech Connect (OSTI)

    Koopman, David; Best, David

    2010-04-28

    Qualification simulant testing was completed to determine appropriate processing conditions and assumptions for the Sludge Batch 6 (SB6) Shielded Cells demonstration of the DWPF flowsheet using the qualification sample from Tank 51 for SB6 after SRNL washing. It was found that an acid addition window of 105-139% of the DWPF acid equation (100-133% of the Koopman minimum acid equation) gave acceptable Sludge Receipt and Adjustment Tank (SRAT) and Slurry Mix Evaporator (SME) results for nitrite destruction and hydrogen generation. Hydrogen generation occurred continuously after acid addition in three of the four tests. The three runs at 117%, 133%, and 150% stoichiometry (Koopman) were all still producing around 0.1 lb hydrogen/hr at DWPF scale after 42 hours of boiling in the SRAT. The 150% acid run reached 110% of the DWPF SRAT limit of 0.65 lb H{sub 2}/hr, and the 133% acid run reached 75% of the DWPF SME limit of 0.223 lb H{sub 2}/hr. Conversely, nitrous oxide generation was subdued compared to previous sludge batches, staying below 25 lb/hr in all four tests or about a fourth as much as in comparable SB4 testing. Two other processing issues were noted. First, incomplete mercury suspension impacted mercury stripping from the SRAT slurry. This led to higher SRAT product mercury concentrations than targeted (>0.45 wt% in the total solids). Associated with this issue was a general difficulty in quantifying the mass of mercury in the SRAT vessel as a function of time, especially as acid stoichiometry increased. About ten times more mercury was found after drying the 150% acid SME product to powder than was indicated by the SME product sample results. Significantly more mercury was also found in the 133% acid SME product samples than was found during the SRAT cycle sampling. It appears that mercury is segregating from the bulk slurry in the SRAT vessel, as mercury amalgam deposits for example, and is not being resuspended by the agitators. The second processing issue was significant ammonium ion formation as the acid stoichiometry was increased due to the high noble metal-high mercury feed conditions. Ammonium ion was found partitioned between the SRAT product slurry and the condensate from the lab-scale off-gas chiller downstream of the SRAT condenser. The ammonium ion was produced from nitrate ion by formic acid. Formate losses increased with increasing acid stoichiometry reaching 40% at the highest stoichiometry tested. About a third of the formate loss at higher acid stoichiometries appeared to be due to ammonia formation. The full extent of ammonia formation was not determined in these tests, since uncondensed ammonia vapor was not quantified; but total formation was bounded by the combined loss of nitrite and nitrate. Nitrate losses during ammonia formation led to nitrite-to-nitrate conversion values that were negative in three of the four tests. The negative results were an artifact of the calculation that assumes negligible SRAT nitrate losses. The sample data after acid addition indicated that some of the initial nitrite was converted to nitrate, so the amount of nitrate destroyed included nitrite converted to nitrate plus some of the added nitrate from the sludge and nitric acid. It is recommended that DWPF investigate the impact of SME product ammonium salts on melter performance (hydrogen, redox). It was recommended that the SB6 Shielded Cells qualification run be performed at 115% acid stoichiometry and allow about 35 hours of boiling for mercury stripping at the equivalent of a 5,000 lb/hr boil-up rate.

  11. Tc-99 Adsorption on Selected Activated Carbons - Batch Testing Results

    SciTech Connect (OSTI)

    Mattigod, Shas V.; Wellman, Dawn M.; Golovich, Elizabeth C.; Cordova, Elsa A.; Smith, Ronald M.

    2010-12-01

    CH2M HILL Plateau Remediation Company (CHPRC) is currently developing a 200-West Area groundwater pump-and-treat system as the remedial action selected under the Comprehensive Environmental Response, Compensation, and Liability Act Record of Decision for Operable Unit (OU) 200-ZP-1. This report documents the results of treatability tests Pacific Northwest National Laboratory researchers conducted to quantify the ability of selected activated carbon products (or carbons) to adsorb technetium-99 (Tc-99) from 200-West Area groundwater. The Tc-99 adsorption performance of seven activated carbons (J177601 Calgon Fitrasorb 400, J177606 Siemens AC1230AWC, J177609 Carbon Resources CR-1240-AW, J177611 General Carbon GC20X50, J177612 Norit GAC830, J177613 Norit GAC830, and J177617 Nucon LW1230) were evaluated using water from well 299-W19-36. Four of the best performing carbons (J177606 Siemens AC1230AWC, J177609 Carbon Resources CR-1240-AW, J177611 General Carbon GC20X50, and J177613 Norit GAC830) were selected for batch isotherm testing. The batch isotherm tests on four of the selected carbons indicated that under lower nitrate concentration conditions (382 mg/L), Kd values ranged from 6,000 to 20,000 mL/g. In comparison. Under higher nitrate (750 mg/L) conditions, there was a measureable decrease in Tc-99 adsorption with Kd values ranging from 3,000 to 7,000 mL/g. The adsorption data fit both the Langmuir and the Freundlich equations. Supplemental tests were conducted using the two carbons that demonstrated the highest adsorption capacity to resolve the issue of the best fit isotherm. These tests indicated that Langmuir isotherms provided the best fit for Tc-99 adsorption under low nitrate concentration conditions. At the design basis concentration of Tc 0.865 µg/L(14,700 pCi/L), the predicted Kd values from using Langmuir isotherm constants were 5,980 mL/g and 6,870 mL/g for for the two carbons. These Kd values did not meet the target Kd value of 9,000 mL/g. Tests conducted to ascertain the effects of changing pH showed that at pH values of 6.5 and 7.5, no significant differences existed in Tc-adsorption performance for three of the carbons, but the fourth carbon performed better at pH 7.5. When the pH was increased to 8.5, a slight decline in performance was observed for all carbons. Tests conducted to ascertain the temperature effect on Tc-99 adsorption indicated that at 21 ºC, 27 ºC, and 32 ºC there were no significant differences in Tc-99 adsorption for three of the carbons. The fourth carbon showed a noticeable decline in Tc-99 adsorption performance with increasing temperature. The presence of volatile organic compounds (VOCs) in the source water did not significantly affect Tc-99 adsorption on either of two carbons tested. Technetium-99 adsorption differed by less than 15% with or without VOCs present in the test water, indicating that Tc-99 adsorption would not be significantly affected if VOCs were removed from the water prior to contact with carbon.

  12. Batch Enzymatic Hydrolysis of Pretreated Corn Stover and Improvements with Countercurrent Saccharification 

    E-Print Network [OSTI]

    Liang, Chao

    2015-07-29

    Enzymatic saccharification of non-food biomass, such as lignocellulose, can produce sugars. Sugars are the common feedstock for bioethanol, which can be substituted for transportation fuel and address the shortage of fossil fuels. Traditional batch...

  13. Progress in Multi-Batch Slip Stacking in the Fermilab Main Injector and Future Plans

    SciTech Connect (OSTI)

    Seiya, K.; Chase, B.; Dey, J.; Joireman, P.; Kourbanis, I.; Reid, J.; /Fermilab

    2008-04-01

    The multi-batch slip stacking has been used for operations since January, 2008 and effectively increased proton intensity to the NuMI target by 50% in a Main Injector (MI) cycle. The MI accepts 11 batches at injection energy from the Booster, and sends two batches to antiproton production and nine to the NuMI beam line. The total beam power in a cycle was increased to 340 kW on average. We have been doing beam studies in order to increase the beam power to 400 kW and to control the beam loss. We will also discuss 12 batch slip stacking scheme which is going to be used for future neutrino experiments.

  14. Site Selection for Concrete Batch Plant to Support Plutonium Disposition Facilities at the Savannah River Site

    SciTech Connect (OSTI)

    Wike, L.D.

    2001-06-15

    WSRC conducted a site selection study to identify, assess, and rank candidate sites for an onsite concrete batch plant at the Savannah River Site in the vicinity of F-Area.

  15. Uranium Adsorption on Ion-Exchange Resins - Batch Testing

    SciTech Connect (OSTI)

    Mattigod, Shas V.; Golovich, Elizabeth C.; Wellman, Dawn M.; Cordova, Elsa A.; Smith, Ronald M.

    2010-12-01

    The uranium adsorption performance of five resins (Dowex 1, Dowex 21K 16-30 [fresh], Dowex 21K 16-30 [regenerated], Purofine PFA600/4740, and ResinTech SIR-1200) were tested using unspiked, nitrate-spiked, and nitrate-spiked/pH adjusted source water from well 299-W19-36. These batch tests were conducted in support of a resin selection process in which the best resin to use for uranium treatment in the 200-West Area groundwater pump-and-treat system will be identified. The results from these tests are as follows: • The data from the high-nitrate (1331 mg/L) tests indicated that Dowex 1, Dowex 21K 16-30 (fresh), Purofine PFA600/4740, and ResinTech SIR-1200 all adsorbed uranium similarly well with Kd values ranging from ~15,000 to 95,000 ml/g. All four resins would be considered suitable for use in the treatment system based on uranium adsorption characteristics. • Lowering the pH of the high nitrate test conditions from 8.2 to 7.5 did not significantly change the uranium adsorption isotherms for the four tested resins. The Kd values for these four resins under high nitrate (1338 mg/L), lower pH (7.5) ranged from ~15,000 to 80,000 ml/g. • Higher nitrate concentrations greatly reduced the uranium adsorption on all four resins. Tests conducted with unspiked (no amendments; nitrate at 337 mg/L and pH at 8.2) source water yielded Kd values for Dowex 1, Dowex 21K 16-30 (fresh), Purofine PFA600/4740, and ResinTech SIR-1200 resins ranging from ~800,000 to >3,000,000 ml/g. These values are about two orders of magnitude higher than the Kd values noted from tests conducted using amended source water. • Compared to the fresh resin, the regenerated Dowex 21K 16-30 resin exhibited significantly lower uranium-adsorption performance under all test conditions. The calculated Kd values for the regenerated resin were typically an order of magnitude lower than the values calculated for the fresh resin. • Additional testing using laboratory columns is recommended to better resolve differences between the adsorption abilities of the resins and to develop estimates of uranium loading on the resins. By determining the quantity of uranium that each resin can adsorb and the time required to reach various levels of loading, resin lifetime in the treatment system can be estimated.

  16. Production of branched-chain alcohols by recombinant Ralstonia eutropha in fed-batch cultivation

    SciTech Connect (OSTI)

    Fei, Q; Brigham, CJ; Lu, JN; Fu, RZ; Sinskey, AJ

    2013-09-01

    Branched-chain alcohols are considered promising green energy sources due to their compatibility with existing infrastructure and their high energy density. We utilized a strain of Ralstonia eutropha capable of producing branched-chain alcohols and examined its production in flask cultures. In order to increase isobutanol and 3-methyl-1-butanol (isoamyl alcohol) productivity in the engineered strain, batch, fed-batch, and two-stage fed-batch cultures were carried out in this work. The effects of nitrogen source concentration on branched-chain alcohol production were investigated under four different initial concentrations in fermenters. A maximum 380 g m(-3) of branched-chain alcohol production was observed with 2 kg m(-3) initial NH4Cl concentration in batch cultures. A pH-stat control strategy was utilized to investigate the optimum carbon source amount fed during fed-batch cultures for higher cell density. In cultures of R. eutropha strains that did not produce polyhydroxyalkanoate or branched-chain alcohols, a maximum cell dry weight of 36 kg m(-3) was observed using a fed-batch strategy, when 10 kg m(-3) carbon source was fed into culture medium. Finally, a total branched-chain alcohol titer of 790 g m(-3), the highest branched-chain alcohol yield of 0.03 g g(-1), and the maximum branched-chain alcohol productivity of 8.23 g m(-3) h(-1) were obtained from the engineered strain Re2410/pJL26 in a two-stage fed-batch culture system with pH-stat control. Isobutanol made up over 95% (mass fraction) of the total branched-chain alcohols titer produced in this study. (C) 2013 Published by Elsevier Ltd.

  17. ANALYSIS OF DWPF SLUDGE BATCH 7A (MACROBATCH 8) POUR STREAM SAMPLES

    SciTech Connect (OSTI)

    Johnson, F.

    2012-05-01

    The Defense Waste Processing Facility (DWPF) began processing Sludge Batch 7a (SB7a), also referred to as Macrobatch 8 (MB8), in June 2011. SB7a is a blend of the heel of Tank 40 from Sludge Batch 6 (SB6) and the SB7a material that was transferred to Tank 40 from Tank 51. SB7a was processed using Frit 418. During processing of each sludge batch, the DWPF is required to take at least one glass sample to meet the objectives of the Glass Product Control Program (GPCP), which is governed by the DWPF Waste Compliance Plan, and to complete the necessary Production Records so that the final glass product may be disposed of at a Federal Repository. Three pour stream glass samples and two Melter Feed Tank (MFT) slurry samples were collected while processing SB7a. These additional samples were taken during SB7a to understand the impact of antifoam and the melter bubblers on glass redox chemistry. The samples were transferred to the Savannah River National Laboratory (SRNL) where they were analyzed. The following conclusions were drawn from the analytical results provided in this report: (1) The sum of oxides for the official SB7a pour stream glass is within the Product Composition Control System (PCCS) limits (95-105 wt%). (2) The average calculated Waste Dilution Factor (WDF) for SB7a is 2.3. In general, the measured radionuclide content of the official SB7a pour stream glass is in good agreement with the calculated values from the Tank 40 dried sludge results from the SB7a Waste Acceptance Program Specification (WAPS) sample. (3) As in previous pour stream samples, ruthenium and rhodium inclusions were detected by Scanning Electron Microscopy-Electron Dispersive Spectroscopy (SEM-EDS) in the official SB7a pour stream sample. (4) The Product Consistency Test (PCT) results indicate that the official SB7a pour stream glass meets the waste acceptance criteria for durability with a normalized boron release of 0.64 g/L, which is an order of magnitude less than the Environmental Assessment (EA) glass. (5) The measured density of the SB7a pour stream glass was 2.7 g/cm{sup 3}. (6) The Fe{sup 2+}/{Sigma}Fe ratios of the SB7a pour stream samples were in the range of 0.04-0.13, while the MFT sample glasses prepared by SRNL were in the range of 0.02-0.04.

  18. ANALYSIS OF DWPF SLUDGE BATCH 6 (MACROBATCH 7) POUR STREAM GLASS SAMPLES

    SciTech Connect (OSTI)

    Johnson, F.

    2012-01-20

    The Defense Waste Processing Facility (DWPF) began processing Sludge Batch 6 (SB6), also referred to as Macrobatch 7 (MB7), in June 2010. SB6 is a blend of the heel of Tank 40 from Sludge Batch 5 (SB5), H-Canyon Np transfers and SB6 that was transferred to Tank 40 from Tank 51.1 SB6 was processed using Frit 418. Sludge is received into the DWPF Chemical Processing Cell (CPC) and is processed through the Sludge Receipt and Adjustment Tank (SRAT) and Slurry Mix Evaporator Tank (SME). The treated sludge slurry is then transferred to the Melter Feed Tank (MFT) and fed to the melter. During processing of each sludge batch, the DWPF is required to take at least one glass sample to meet the objectives of the Glass Product Control Program (GPCP) and to complete the necessary Production Records so that the final glass product may be disposed of at a Federal Repository. The DWPF requested various analyses of radioactive glass samples obtained from the melter pour stream during processing of SB6 as well as reduction/oxidation (REDOX) analysis of MFT samples to determine the impact of Argon bubbling. Sample analysis followed the Task Technical and Quality Assurance Plan (TTQAP) and an Analytical Study Plan (ASP). Four Pour Stream (PS) glass samples and two MFT slurry samples were delivered to the Savannah River National Laboratory (SRNL) from the DWPF. Table 1-1 lists the sample information for each pour stream glass sample. SB6 PS3 (S03472) was selected as the official pour stream sample for SB6 and full analysis was requested. This report details the visual observations of the as-received SB6 PS No.3 glass sample as well as results for the chemical composition, Product Consistency Test (PCT), radionuclide content, noble metals, and glass density. REDOX results will be provided for all four pour stream samples and vitrified samples of MFT-558 and MFT-568A. Where appropriate, data from other pour stream samples will be provided.

  19. Analysis Of The Sludge Batch 7b (Macrobatch 9) DWPF Pour Stream Glass Sample

    SciTech Connect (OSTI)

    Johnson, F. C.; Crawford, C. L.; Pareizs, J. M.

    2013-11-18

    The Defense Waste Processing Facility (DWPF) began processing Sludge Batch 7b (SB7b), also referred to as Macrobatch 9 (MB9), in January 2012. SB7b is a blend of the heel of Tank 40 from Sludge Batch 7a (SB7a) and the SB7b material that was transferred to Tank 40 from Tank 51. SB7b was processed using Frit 418. During processing of each sludge batch, the DWPF is required to take at least one glass sample to meet the objectives of the Glass Product Control Program (GPCP), which is governed by the DWPF Waste Form Compliance Plan, and to complete the necessary Production Records so that the final glass product may be disposed of at a Federal Repository. Two pour stream glass samples were collected while processing SB7b. The samples were transferred to the Savannah River National Laboratory (SRNL) where one was analyzed and the other was archived. The following conclusions were drawn from the analytical results provided in this report: The sum of oxides for the official SB7b pour stream glass is within the Product Composition Control System (PCCS) limits (95-105 wt%); The average calculated Waste Dilution Factor (WDF) for SB7b is 2.3. In general, the measured radionuclide content of the official SB7b pour stream glass is in good agreement with the calculated values from the Tank 40 dried sludge results from the SB7b Waste Acceptance Program Specification (WAPS) sample; As in previous pour stream samples, ruthenium and rhodium inclusions were detected by Scanning Electron Microscopy-Electron Dispersive Spectroscopy (SEM-EDS) in the SB7b pour stream sample; The Product Consistency Test (PCT) results indicate that the official SB7b pour stream glass meets the waste acceptance criteria for durability with a normalized boron release of 0.8 g/L, which is an order of magnitude less than the Environmental Assessment (EA) glass; The measured density of the SB7b pour stream glass was 2.70 g/cm{sup 3}; The Fe{sup 2+}/?Fe ratio of the SB7b pour stream samples was 0.07.

  20. Results Of Initial Analyses Of The Salt (Macro) Batch 9 Tank 21H Qualification Samples

    SciTech Connect (OSTI)

    Peters, T.

    2015-10-08

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H in support of qualification of Interim Salt Disposition Project (ISDP) Salt (Macro) Batch 9 for processing through the Actinide Removal Process (ARP) and the Modular Caustic-Side Solvent Extraction Unit (MCU). This document reports the initial results of the analyses of samples of Tank 21H. Analysis of the Tank 21H Salt (Macro) Batch 9 composite sample indicates that the material does not display any unusual characteristics. Further results on the chemistry and other tests will be issued in the future.

  1. Results of initial analyses of the salt (macro) batch 9 tank 21H qualification samples

    SciTech Connect (OSTI)

    Peters, T. B.

    2015-10-01

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H in support of qualification of Interim Salt Disposition Project (ISDP) Salt (Macro) Batch 9 for processing through the Actinide Removal Process (ARP) and the Modular Caustic-Side Solvent Extraction Unit (MCU). This document reports the initial results of the analyses of samples of Tank 21H. Analysis of the Tank 21H Salt (Macro) Batch 9 composite sample indicates that the material does not display any unusual characteristics or observations, such as floating solids, the presence of large amount of solids, or unusual colors. Further results on the chemistry and other tests will be issued in the future.

  2. Batch polymerization of styrene initiated by n-butyl lithium in a cyclohexane solvent 

    E-Print Network [OSTI]

    Landon, Thomas Rodman

    1971-01-01

    Committee ea Depa tment Mem er Mem er em er August 1971 ABSTRACT Batch Polymerization of Styrene Initiated by N-Butyl Lithium in Cyclohexane Solvent. (August 19 71) Thomas Rodman Landon, B, S. , Te x as A (&M Un i ve rs i ty Directed by: Dr.... Rayford G. Anthony Styrene is polymerized by n-butyl lithium with cyclo- hexane as the solvent. The polymerization is carried out in an isothermal batch reactors at three temperature 30, 40, and 50'C. The proposed reaction proceeds by a homo- geneous...

  3. Batch polymerization of styrene initiated by n-butyllithium in benzene 

    E-Print Network [OSTI]

    Tanlak, Tayfun

    1975-01-01

    BATCH POLYMERIZATION OF STYRENE INITIATED BY n-BUTYLLITHIUM IN BENZENE A Thesis by TAYFUN TANLAK Submitted to the Graduate Co'l1ege of Texas Anil University in partial fu1fi11ment of the requirement for the degree cf MASTER OF SCIENCE... August 1975 Major Subject: Chemica1 Engineering BATCH POLYMERIZATION OF STYRENE INITIATED BY n-BUTYLLITHIUM IN BENZENE A Thesis by TAYFUN TANLAK Approved as to style and content by: Chairman of Committee Head Department Member ~ /z'1tup Member...

  4. Directed batch assembly of three-dimensional helical nanobelts through angular winding and electroplating

    E-Print Network [OSTI]

    Sun, Yu

    and electroplating This article has been downloaded from IOPscience. Please scroll down to see the full text article of three-dimensional helical nanobelts through angular winding and electroplating D J Bell1 , T E Bauert1. In a subsequent Au electroplating step, contacts are electroformed and the batch assembly is completed, while

  5. Batch-mode vs Online-mode Supervised Learning Motivations for Artificial Neural Networks

    E-Print Network [OSTI]

    Wehenkel, Louis

    Batch-mode vs Online-mode Supervised Learning Motivations for Artificial Neural Networks Linear ANN-mode vs Online-mode Supervised Learning Motivations for Artificial Neural Networks Linear ANN Models for Artificial Neural Networks Linear ANN Models Single neuron models Single layer models Nonlinear ANN Models

  6. Transfer-Free Batch Fabrication of Large-Area Suspended Graphene Membranes

    E-Print Network [OSTI]

    Zettl, Alex

    heightened for the preparation of sus- pended graphene structures to ascertain graphene's fundamentalTransfer-Free Batch Fabrication of Large- Area Suspended Graphene Membranes Benjami´n Alema of the predicted properties arising from the two-dimensional nature of graphene1 4 can be obscured or altered

  7. NESTED BATCH MODE LEARNING AND STOCHASTIC OPTIMIZATION WITH AN APPLICATION TO SEQUENTIAL

    E-Print Network [OSTI]

    Powell, Warren B.

    . optimal learning, materials science, sequential design of experiments, decision making, dynamicNESTED BATCH MODE LEARNING AND STOCHASTIC OPTIMIZATION WITH AN APPLICATION TO SEQUENTIAL MULTI-STAGE TESTING IN MATERIALS SCIENCE YINGFEI WANG, KRISTOFER G. REYES, KEITH A. BROWN§, CHAD A. MIRKIN

  8. Design and Optimization of Condenser and Centrifuge Units for Enhancement of a Batch Vacuum Frying System 

    E-Print Network [OSTI]

    Pandey, Akhilesh

    2011-02-22

    A batch vacuum frying system, which processes fruits and vegetables, includes a frying pan, a surface-condenser, and a vacuum pump. With health and safety issues in mind, this research focused on developing a modified surface-condenser to prevent...

  9. Microbial Fuel Cells In this experiment, a batch mixed culture microbial fuel cell with Shewanella

    E-Print Network [OSTI]

    Fay, Noah

    Microbial Fuel Cells Abstract In this experiment, a batch mixed culture microbial fuel cell conditions under nitrogen gas. In the microbial fuel cell with Shewanella putrefaciens sp. 200 as catalysisM at pH=7. Introduction Microbial fuel cells (MFC) are systems that take advantage of certain

  10. APPLIED MICROBIAL AND CELL PHYSIOLOGY Electricity production from xylose in fed-batch

    E-Print Network [OSTI]

    to ethanol production from pentoses is energy production using a microbial fuel cell (MFC). An MFCAPPLIED MICROBIAL AND CELL PHYSIOLOGY Electricity production from xylose in fed-batch and continuous-flow microbial fuel cells Liping Huang & Bruce E. Logan Received: 23 March 2008 /Revised: 30 May

  11. On the Social Welfare of Mechanisms for Repeated Batch Matching Elliot Anshelevich

    E-Print Network [OSTI]

    Anshelevich, Elliot

    in the market for the next round. This setting models several scenarios of interest, includ- ing many job of work on analyzing single rounds of markets that clear in batches as well as on designing and an compatibility dominate. There is now a signifi- cant literature on market design for achieving various differ

  12. Control of incident irradiance on a batch operated flat-plate photobioreactor

    E-Print Network [OSTI]

    Pilon, Laurent

    microalgae growth rate. Then, the feed-forward inversion control scheme adjusted the incident irradiance biomass and lipid productivity in microalgae cultivation. The present approach can rapidly identify and productivity of microalgae. This was illustrated with Nannochloropsis oculata batch grown in a flat-plate PBR

  13. Production Leveling (Heijunka) Implementation in a Batch Production System: a Case Study

    E-Print Network [OSTI]

    Boyer, Edmond

    of Production Leveling outside automotive networks. Additionally, one can question whether Lean Manufacturing, Department of Manufacturing, GETEQ Research Group, Caixa Postal 476, Campus Universitário, Trindade, 88040 on a subsidiary of a multinational enterprise located on Brazil, which manufacturing processes comprise batch

  14. Hybrid Batch Bayesian Optimization Javad Azimi AZIMI@EECS.OREGONSTATE.EDU

    E-Print Network [OSTI]

    Fern, Xiaoli Zhang

    motivating application we try to optimize the power output of nano-enhanced Microbial Fuel Cells (MFCs). MFCsHybrid Batch Bayesian Optimization Javad Azimi AZIMI@EECS.OREGONSTATE.EDU Oregon State University Abstract Bayesian Optimization (BO) aims at optimizing an unknown function that is costly to evaluate. We

  15. Supplementary Analysis For: The sva package for removing batch effects and other unwanted variation in

    E-Print Network [OSTI]

    Leek, Jeffrey

    Storey3 1 Johns Hopkins Bloomberg School of Public Health 2 Boston University 3 Princeton University the data from an ExpressionSet 1 2 Applying the fsva function to remove batch effects for prediction 2 1) > library(sva) > library(bladderbatch) 1 #12;> library(RColorBrewer) > data(bladderdata) > library

  16. Greedy Algorithm for Scheduling Batch Plants with Sequence-Dependent Changeovers

    E-Print Network [OSTI]

    Grossmann, Ignacio E.

    of multistage batch plants with a large number of orders and sequence-dependent changeovers. Such problems marketplace can only be ensured if companies optimize the various functions within their supply chain with many related optimization problems, such as maintenance planning, energy and inventory optimization

  17. Nitrogen removal via nitrite in a sequencing batch reactor treating sanitary landfill leachate

    E-Print Network [OSTI]

    Nitrogen removal via nitrite in a sequencing batch reactor treating sanitary landfill leachate, for the automation of a bench-scale SBR treating leachate generated in old landfills. Attention was given confirm the effectiveness of the nitrite route for nitrogen removal optimisation in leachate treatment

  18. Intelligent monitoring system for long-term control of Sequencing Batch Reactors

    E-Print Network [OSTI]

    -scale Sequencing Batch Reactor (SBR) treating nitrogen-rich wastewater (sanitary landfill leachate). The paper). Leachate generated in old landfills is a high-strength wastewater and is characterized by a low COD monitoring tool for adjusting the phase length and COD addition in SBRs treating sanitary landfill leachate

  19. Optimisation of sanitary landfill leachate treatment in a sequencing batch reactor

    E-Print Network [OSTI]

    Optimisation of sanitary landfill leachate treatment in a sequencing batch reactor A. Spagni, S was operated for almost three years in an attempt to optimise the treatment of leachates generated in old and N removal were usually higher than 98% and 90%, respectively, whereas COD (of the leachate) removal

  20. Utilizing Green Energy Prediction to Schedule Mixed Batch and Service Jobs in Data Centers

    E-Print Network [OSTI]

    Simunic, Tajana

    Utilizing Green Energy Prediction to Schedule Mixed Batch and Service Jobs in Data Centers Baris on using immediately available green energy to supplement the non- renewable, or brown energy at the cost of canceling and rescheduling jobs whenever the green energy availability is too low [16]. In this paper we

  1. DETERMINATION OF REPORTABLE RADIONUCLIDES FOR DWPF SLUDGE BATCH 4 MACROBATCH 5

    SciTech Connect (OSTI)

    Bannochie, C; Ned Bibler, N; David Diprete, D

    2008-05-30

    The Waste Acceptance Product Specifications (WAPS)1 1.2 require that 'The Producer shall report the inventory of radionuclides (in Curies) that have half-lives longer than 10 years and that are, or will be, present in concentrations greater than 0.05 percent of the total inventory for each waste type indexed to the years 2015 and 3115'. As part of the strategy to meet WAPS 1.2, the Defense Waste Processing Facility (DWPF) will report for each waste type, all radionuclides (with half-lives greater than 10 years) that have concentrations greater than 0.01 percent of the total inventory from time of production through the 1100 year period from 2015 through 3115. The initial listing of radionuclides to be included is based on the design-basis glass as identified in the Waste Form Compliance Plan (WCP)2 and Waste Form Qualification Report (WQR)3. However, it is required that this list be expanded if other radionuclides with half-lives greater than 10 years are identified that may meet the greater than 0.01% criterion for Curie content. Specification 1.6 of the WAPS, International Atomic Energy Agency (IAEA) Safeguards Reporting for High Level Waste (HLW), requires that the ratio by weights of the following uranium and plutonium isotopes be reported: U-233, U-234, U-235, U-236, U-238, Pu-238, Pu-239, Pu-240, Pu-241, and Pu-242. Therefore, the complete set of reportable radionuclides must also include this set of U and Pu isotopes. The DWPF is receiving radioactive sludge slurry from HLW Tank 40. The radioactive sludge slurry in Tank 40 is a blend of the previous contents of Tank 40 (Sludge Batch 3) and the sludge that was transferred to Tank 40 from Tank 51. The blend of sludge from Tank 51 and Tank 40 defines Sludge Batch 4 (also referred to as Macrobatch 5 (MB5)). This report develops the list of reportable radionuclides and associated activities and determines the radionuclide activities as a function of time. The DWPF will use this list and the activities as one of the inputs for the development of the Production Records that relate to the radionuclide inventory. This work was initiated through Task Technical Request HLW/DWPF/TTR-2005-0034; Rev. 0 entitled Sludge Batch 4 SRNL Shielded Cells Testing4. Specifically, this report details results from performing, in part, Subtask 3 of the TTR and, in part, meets Deliverable 7 of the TTR. The work was performed following the Technical Task and Quality Assurance Plan (TTQAP), WSRC-RP-2006-00310, Rev. 15 and Analytical Study Plan (ASP), WSRC-RP-2006-00458, Rev. 16. In order to determine the reportable radionuclides for Sludge Batch 4 (SB4) (Macro Batch 5 (MB5)), a list of radioisotopes that may meet the criteria as specified by the Department of Energy's (DOE) WAPS was developed. All radioactive U-235 fission products and all radioactive activation products that could be in the SRS HLW were considered. In addition, all U and Pu isotopes identified in WAPS 1.6 were included in the list. This list was then evaluated and some isotopes excluded from the projection calculations. Based on measurements and analytical detection limits, twenty-nine radionuclides have been identified as reportable for DWPF SB4 (MB5) as specified by WAPS 1.2. The 29 reportable nuclides are: Ni-59; Ni-63; Se-79; Sr-90; Zr-93; Nb-93m; Tc-99; Sn-126; Cs-137; Sm-151; U-233; U-234; Np-237; U-238; Pu-238; Pu-239; Pu-240; Am-241; Pu-241; Pu-242; Am-242m; Am-243; Cm-244; Cm-245; Cm-246; Cm-247; Bk-247; Cm-248; and Cf-251. The WCP and WQR require that all of radionuclides present in the Design Basis glass be considered as the initial set of reportable radionuclides. For SB4 (MB5), all of the radionuclides in the Design Basis glass are reportable except for three radionuclides: Pd-107, Cs-135, and Th-230. At no time through the calendar year 3115 did any of these three radionuclides contribute to more than 0.01% of the radioactivity on a Curie basis. Two additional uranium isotopes (U-235 and -236) must be added to the list of reportable radionuclides in order to meet WAPS 1.6. All of the Pu isotopes and other U isoto

  2. SLUDGE WASHING AND DEMONSTRATION OF THE DWPF FLOWSHEET IN THE SRNL SHIELDED CELLS FOR SLUDGE BATCH 7A QUALIFICATION

    SciTech Connect (OSTI)

    Pareizs, J.; Billings, A.; Click, D.

    2011-07-08

    Waste Solidification Engineering (WSE) has requested that characterization and a radioactive demonstration of the next batch of sludge slurry (Sludge Batch 7a*) be completed in the Shielded Cells Facility of the Savannah River National Laboratory (SRNL) via a Technical Task Request (TTR). This characterization and demonstration, or sludge batch qualification process, is required prior to transfer of the sludge from Tank 51 to the Defense Waste Processing Facility (DWPF) feed tank (Tank 40). The current WSE practice is to prepare sludge batches in Tank 51 by transferring sludge from other tanks. Discharges of nuclear materials from H Canyon are often added to Tank 51 during sludge batch preparation. The sludge is washed and transferred to Tank 40, the current DWPF feed tank. Prior to transfer of Tank 51 to Tank 40, SRNL simulates the Tank Farm and DWPF processes with a Tank 51 sample (referred to as the qualification sample). Sludge Batch 7a (SB7a) is composed of portions of Tanks 4, 7, and 12; the Sludge Batch 6 heel in Tank 51; and a plutonium stream from H Canyon. SRNL received the Tank 51 qualification sample (sample ID HTF-51-10-125) following sludge additions to Tank 51. This report documents: (1) The washing (addition of water to dilute the sludge supernate) and concentration (decanting of supernate) of the SB7a - Tank 51 qualification sample to adjust sodium content and weight percent insoluble solids to Tank Farm projections. (2) The performance of a DWPF Chemical Process Cell (CPC) simulation using the washed Tank 51 sample. The simulation included a Sludge Receipt and Adjustment Tank (SRAT) cycle, where acid was added to the sludge to destroy nitrite and reduce mercury, and a Slurry Mix Evaporator (SME) cycle, where glass frit was added to the sludge in preparation for vitrification. The SME cycle also included replication of five canister decontamination additions and concentrations. Processing parameters were based on work with a non-radioactive simulant. (3) Vitrification of a portion of the SME product and characterization and durability testing (as measured by the Product Consistency Test (PCT)) of the resulting glass. (4) Rheology measurements of the initial slurry samples and samples after each phase of CPC processing. This program was controlled by a Task Technical and Quality Assurance Plan (TTQAP), and analyses were guided by an Analytical Study Plan. This work is Technical Baseline Research and Development (R&D) for the DWPF. It should be noted that much of the data in this document has been published in interoffice memoranda. The intent of this technical report is bring all of the SB7a related data together in a single permanent record and to discuss the overall aspects of SB7a processing.

  3. Characterization Of The As-Received Sludge Batch 9 Qualification Sample (Htf-51-15-81)

    SciTech Connect (OSTI)

    Pareizs, J.

    2015-09-30

    Savannah River National Laboratory (SRNL) personnel have been requested to qualify the next sludge batch (Sludge Batch 9 – SB9) for processing at the Defense Waste Processing Facility (DWPF). To accomplish this task, Savannah River Remediation (SRR) has sent SRNL a 3-L slurried sample of Tank 51H (HTF-51-15-81) to be characterized, washed, and then used in a lab-scale demonstration of the DWPF flowsheet (potentially after combining with Tank 40H sludge). This report documents the first steps of the qualification process – characterization of the as-received Tank 51H qualification sample. These results will be used to support a reprojection of SB9 by SRR from which final Tank 51H washing, frit development, and Chemical Processing Cell (CPC) activities will be based.

  4. SRS SLUDGE BATCH QUALIFICATION AND PROCESSING; HISTORICAL PERSPECTIVE AND LESSONS LEARNED

    SciTech Connect (OSTI)

    Cercy, M.; Peeler, D.; Stone, M.

    2013-09-25

    This report provides a historical overview and lessons learned associated with the SRS sludge batch (SB) qualification and processing programs. The report covers the framework of the requirements for waste form acceptance, the DWPF Glass Product Control Program (GPCP), waste feed acceptance, examples of how the program complies with the specifications, an overview of the Startup Program, and a summary of continuous improvements and lessons learned. The report includes a bibliography of previous reports and briefings on the topic.

  5. Evaluation of methods of mixing lime in bituminous paving mixtures in batch and drum plants 

    E-Print Network [OSTI]

    Button, Joseph Wade

    1984-01-01

    . Lime was added in the pugmill of the batch plant, on the cold feed belt, and through the fines feeder of the drum mix plant. The asphalt and aggregates used were characterized in the laboratory. Asphalt concrete mixture tests included laboratory... Maria Road 14 3 Laboratory Test Program for All Mixtures 17 Process by which Lime Slurry was Added to the Individual Aggregates on the Cold Feed Belt Overall Average Air Void Content of Laboratory Mixed and Compacted Samples 19 27 Resilient...

  6. Removal of aqueous rinsable flux residues in a batch spray dishwater

    SciTech Connect (OSTI)

    Slanina, J.T.

    1992-02-01

    An alkaline detergent solution used in an industrial dishwasher was evaluated to remove aqueous rinsable flux residues on printed wiring boards (PWBs) after hot air solder leveling and hot oil solder dip and leveling. The dishwasher, a batch cleaning process, was compared to an existing conveyorized aqueous cleaning process. The aqueous soluble flux residues from both soldering processes were removed with a solution of a mild alkaline detergent dissolved in hot deionized (DI) water.

  7. Analysis Of DWPF Sludge Batch 7a (Macrobatch 8) Pour Stream Samples

    SciTech Connect (OSTI)

    Johnson, F. C.; Pareizs, J. M.

    2012-10-24

    The Defense Waste Processing Facility (DWPF) began processing Sludge Batch 7a (SB7a), also referred to as Macrobatch 8 (MB8), in June 2011. SB7a is a blend of the heel of Tank 40 from Sludge Batch 6 (SB6) and the SB7a material that was transferred to Tank 40 from Tank 51. SB7a was processed using Frit 418. During processing of each sludge batch, the DWPF is required to take at least one glass sample to meet the objectives of the Glass Product Control Program (GPCP), which is governed by the DWPF Waste Compliance Plan, and to complete the necessary Production Records so that the final glass product may be disposed of at a Federal Repository. Three pour stream glass samples and two Melter Feed Tank (MFT) slurry samples were collected while processing SB7a. These additional samples were taken during SB7a to understand the impact of antifoam and the melter bubblers on glass redox chemistry. The samples were transferred to the Savannah River National Laboratory (SRNL) where they were analyzed.

  8. Small Scale Mixing Demonstration Batch Transfer and Sampling Performance of Simulated HLW - 12307

    SciTech Connect (OSTI)

    Jensen, Jesse; Townson, Paul; Vanatta, Matt

    2012-07-01

    The ability to effectively mix, sample, certify, and deliver consistent batches of High Level Waste (HLW) feed from the Hanford Double Shell Tanks (DST) to the Waste treatment Plant (WTP) has been recognized as a significant mission risk with potential to impact mission length and the quantity of HLW glass produced. At the end of 2009 DOE's Tank Operations Contractor, Washington River Protection Solutions (WRPS), awarded a contract to EnergySolutions to design, fabricate and operate a demonstration platform called the Small Scale Mixing Demonstration (SSMD) to establish pre-transfer sampling capacity, and batch transfer performance data at two different scales. This data will be used to examine the baseline capacity for a tank mixed via rotational jet mixers to transfer consistent or bounding batches, and provide scale up information to predict full scale operational performance. This information will then in turn be used to define the baseline capacity of such a system to transfer and sample batches sent to WTP. The Small Scale Mixing Demonstration (SSMD) platform consists of 43'' and 120'' diameter clear acrylic test vessels, each equipped with two scaled jet mixer pump assemblies, and all supporting vessels, controls, services, and simulant make up facilities. All tank internals have been modeled including the air lift circulators (ALCs), the steam heating coil, and the radius between the wall and floor. The test vessels are set up to simulate the transfer of HLW out of a mixed tank, and collect a pre-transfer sample in a manner similar to the proposed baseline configuration. The collected material is submitted to an NQA-1 laboratory for chemical analysis. Previous work has been done to assess tank mixing performance at both scales. This work involved a combination of unique instruments to understand the three dimensional distribution of solids using a combination of Coriolis meter measurements, in situ chord length distribution measurements, and electro-resistive tomography. This current work utilized the same instruments to monitor simulated waste transfers. This paper will discuss some of the scaling compromises when it came to the scaled sampling system design, handling of large quantities of material for sampling, and present data for the discuss of likely behavior of the full scale DST based on scaling correlations using a scale ratio exponent (SRE) from 0.25 to 0.45 and the behavior observed in the SSMD platform. This does not establish a scaling factor for DST mixing using paired jet mixers but is an attempt to envelope the likely performance ranges in terms of certification sampling bias, certification sample root-mean-square-deviation, and bath to batch relative standard deviation. (authors)

  9. Batch Jobs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room News PublicationsAudits & Inspections AuditsBarbara McClintock andBasics BasicsBasil Lalli

  10. Batch Jobs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room News PublicationsAudits & Inspections AuditsBarbara McClintock andBasics BasicsBasil

  11. Evaluation of ISDP Batch 2 Qualification Compliance to 512-S, DWPF, Tank Farm, and Saltstone Waste Acceptance Criteria

    SciTech Connect (OSTI)

    Shafer, A.

    2010-05-05

    The purpose of this report is to document the acceptability of the second macrobatch (Salt Batch 2) of Tank 49H waste to H Tank Farm, DWPF, and Saltstone for operation of the Interim Salt Disposition Project (ISDP). Tank 49 feed meets the Waste Acceptance Criteria (WAC) requirements specified by References 11, 12, and 13. Salt Batch 2 material is qualified and ready to be processed through ARP/MCU to the final disposal facilities.

  12. DETERMINATION OF REPORTABLE RADIONUCLIDES FOR DWPF SLUDGE BATCH 5 (MACROBATCH 6)

    SciTech Connect (OSTI)

    Bannochie, C.; Bibler, N.; Diprete, D.

    2010-02-04

    The Waste Acceptance Product Specifications (WAPS) 1.2 require that ''The Producer shall report the inventory of radionuclides (in Curies) that have half-lives longer than 10 years and that are, or will be, present in concentrations greater than 0.05 percent of the total inventory for each waste type indexed to the years 2015 and 3115''. As part of the strategy to comply with WAPS 1.2, the Defense Waste Processing Facility (DWPF) will report for each waste type, all radionuclides (with half-lives greater than 10 years) that have concentrations greater than 0.01 percent of the total inventory from time of production through the 1100 year period from 2015 through 3115. The initial listing of radionuclides to be included is based on the design-basis glass as identified in the Waste Form Compliance Plan (WCP) and Waste Form Qualification Report (WQR). However, it is required that this list be expanded if other radionuclides with half-lives greater than 10 years are identified that may meet the greater than 0.01% criterion for Curie content. Specification 1.6 of the WAPS, International Atomic Energy Agency (IAEA) Safeguards Reporting for High Level Waste (HLW), requires that the ratio by weights of the following uranium and plutonium isotopes be reported: U-233, U-234, U-235, U-236, U-238, Pu-238, Pu-239, Pu-240, Pu-241, and Pu-242. Therefore, the complete set of reportable radionuclides must also include this set of U and Pu isotopes. The DWPF is receiving radioactive sludge slurry from HLW Tank 40. The radioactive sludge slurry in Tank 40 is a blend of the heel from Tank 40 (Sludge Batch 4 (SB4)), Sludge Batch 5 (SB5) that was transferred to Tank 40 from Tank 51, and H-Canyon Np transfers completed after the start of processing. The blend of sludge in Tank 40 is also referred to as Macrobatch 6 (MB6). This report develops the list of reportable radionuclides and associated activities and determines the radionuclide activities as a function of time. The DWPF will use this list and the activities as one of the inputs for the development of the Production Records that relate to the radionuclide inventory. This work was initiated through Technical Task Request (TTR) HLW-DWPF-TTR-2008-0010; Rev. 2 entitled Sludge Batch 5 SRNL Shielded Cells Testing. Specifically, this report details results from performing Subtask II, 5 of the TTR and, in part, meets Deliverable 7 of the TTR. The work was performed following the Task Technical and Quality Assurance Plan (TTQAP), WSRC-RP-2008-00137, Rev. 2 and Analytical Study Plan (ASP), WSRC-RP-2008-00138, Rev. 2. In order to determine the reportable radionuclides for SB5 (MB6), a list of radioisotopes that may meet the criteria as specified by the Department of Energy's (DOE) WAPS was developed. All radioactive U-235 fission products and all radioactive activation products that could be in the SRS HLW were considered. In addition, all U and Pu isotopes identified in WAPS 1.6 were included in the list. This list was then evaluated and some isotopes excluded from the projection calculations. Based on measurements and analytical detection limits, twenty-six radionuclides have been identified as reportable for DWPF SB5 as specified by WAPS 1.2. The 26 reportable radionuclides are: Cl-36, Ni-59, Ni-63, Sr-90, Zr-93, Nb-93m, Tc-99, Sn-126, Cs-137, Sm-151, U-233, U-234, Np-237, U-238, Pu-238, Pu-239, Pu-240, Am-241, Pu-241, Pu-242, Am-242m, Am-243, Cm-244, Cm-245, Cm-246, Cf-251. Chlorine-36 is reported for the first time based on the upper bounding activity determined from the aqua regia digested sludge slurry. The WCP and WQR require that all of radionuclides present in the Design Basis glass be considered as the initial set of reportable radionuclides. For SB5 (MB6), all of the radionuclides in the Design Basis glass are reportable except for four radionuclides: Se-79, Pd-107, Cs-135, and Th-230. At no time through the year 3115 did any of these three radionuclides contribute to more than 0.01% of the radioactivity on a Curie basis. Two additional uranium isotopes (U-235 and -236) must be added to

  13. DETERMINATION OF REPORTABLE RADIONUCLIDES FOR DWPF SLUDGE BATCH 6 (MACROBATCH 7)

    SciTech Connect (OSTI)

    Bannochie, C.; Diprete, D.

    2011-06-01

    The Waste Acceptance Product Specifications (WAPS) 1.2 require that 'The Producer shall report the inventory of radionuclides (in Curies) that have half-lives longer than 10 years and that are, or will be, present in concentrations greater than 0.05 percent of the total inventory for each waste type indexed to the years 2015 and 3115'. As part of the strategy to comply with WAPS 1.2, the Defense Waste Processing Facility (DWPF) will report for each waste type, all radionuclides (with half-lives greater than 10 years) that have concentrations greater than 0.01 percent of the total inventory from time of production through the 1100 year period from 2015 through 3115. The initial listing of radionuclides to be included is based on the design-basis glass as identified in the Waste Form Compliance Plan (WCP) and Waste Form Qualification Report (WQR). However, it is required that this list be expanded if other radionuclides with half-lives greater than 10 years are identified that may meet the greater than 0.01% criterion for Curie content. Specification 1.6 of the WAPS, International Atomic Energy Agency (IAEA) Safeguards Reporting for High Level Waste (HLW), requires that the ratio by weights of the following uranium and plutonium isotopes be reported: U-233, U-234, U-235, U-236, U-238, Pu-238, Pu-239, Pu-240, Pu-241, and Pu-242. Therefore, the complete set of reportable radionuclides must also include this set of U and Pu isotopes. The DWPF is receiving radioactive sludge slurry from HLW Tank 40. The radioactive sludge slurry in Tank 40 is a blend of the heel from Sludge Batch 5 (SB5) with H-Canyon Np transfers completed after the start of processing SB5, and Sludge Batch 6 (SB6) that was transferred to Tank 40 from Tank 51. The blend of sludge in Tank 40 is also referred to as Macrobatch 7 (MB7). This report develops the list of reportable radionuclides and associated activities as a function of time. The DWPF will use this list and the activities as one of the inputs for the development of the Production Records that relate to radionuclide inventory. This work was initiated through Technical Task Request (TTR) HLW-DWPF-TTR-2009-0014; Rev. 2 entitled Sludge Batch 6 SRNL Shielded Cells Testing. Specifically, this report details results from performing Subtask III, Item 2 of the TTR and, in part, meets Deliverable 7 of the TTR. The work was performed following the Task Technical and Quality Assurance Plan (TTQAP), SRNL-RP-2009-00473, Rev. 15 and Analytical Study Plan (ASP), SRNL-RP-2009-00474, Rev. 1. In order to determine the reportable radionuclides for SB6 (MB7), a list of radioisotopes that may meet the criteria as specified by the Department of Energy's (DOE) WAPS was developed. All radioactive U-235 fission products and all radioactive activation products that could be in the SRS HLW were considered. In addition, all U and Pu isotopes identified in WAPS 1.6 were included in the list. This list was then evaluated and some isotopes were excluded from the projection calculations. Based on measurements and analytical detection limits, 30 radionuclides have been identified as reportable for DWPF SB6 as specified by WAPS 1.2. The WCP and WQR require that all of the radionuclides present in the Design Basis glass be considered as the initial set of reportable radionuclides. For SB6, all of the radionuclides in the Design Basis glass are reportable except for three radionuclides: Pd-107, Cs-135, and Th-230. At no time during the 1100-year period between 2015 and 3115 did any of these three radionuclides contribute to more than 0.01% of the radioactivity on a Curie basis. Two additional uranium isotopes (U-235 and -236) must be added to the list of reportable radionuclides in order to meet WAPS 1.6. All of the Pu isotopes (Pu-238, -239, -240, -241, and -242) and other U isotopes (U-233, -234, and -238) identified in WAPS 1.6 were already determined to be reportable according to WAPS 1.2 This brings the total number of reportable radionuclides for SB6 to 32. The radionuclide measurements made for SB6 are the most extensive condu

  14. Determination Of Reportable Radionuclides For DWPF Sludge Batch 7B (Macrobatch 9)

    SciTech Connect (OSTI)

    Crawford, C. L.; DiPrete, D. P.

    2013-08-22

    The Waste Acceptance Product Specifications (WAPS) 1.2 require that “The Producer shall report the inventory of radionuclides (in Curies) that have half-lives longer than 10 years and that are, or will be, present in concentrations greater than 0.05 percent of the total inventory for each waste type indexed to the years 2015 and 3115”. As part of the strategy to comply with WAPS 1.2, the Defense Waste Processing Facility (DWPF) will report for each waste type, all radionuclides (with half-lives greater than 10 years) that have concentrations greater than 0.01 percent of the total inventory from time of production through the 1100 year period from 2015 through 3115. The initial listing of radionuclides to be included is based on the design-basis glass as identified in the Waste Form Compliance Plan (WCP) and Waste Form Qualification Report (WQR). However, it is required that this list be expanded if other radionuclides with half-lives greater than 10 years are identified that may meet the greater than 0.01% criterion for Curie content. Specification 1.6 of the WAPS, International Atomic Energy Agency (IAEA) Safeguards Reporting for High Level Waste (HLW), requires that the ratio by weights of the following uranium and plutonium isotopes be reported: U-233, U-234, U-235, U-236, U-238, Pu-238, Pu-239, Pu-240, Pu-241, and Pu-242. Therefore, the complete set of reportable radionuclides must also include this set of U and Pu isotopes. The DWPF is receiving radioactive sludge slurry from HLW Tank 40. The radioactive sludge slurry in Tank 40 is a blend of the heel from Sludge Batch 7a (SB7a) and Sludge Batch 7b (SB7b) that was transferred to Tank 40 from Tank 51. The blend of sludge in Tank 40 is also referred to as Macrobatch 9 (MB9). This report develops the list of reportable radionuclides and associated activities as a function of time. The DWPF will use this list and the activities as one of the inputs for the development of the Production Records that relate to radionuclide inventory. This work was initiated through Technical Task Request (TTR) HLW-DWPF-TTR-2011-0004; Rev. 0 entitled Sludge Batch 7b Qualification Studies. Specifically, this report details results from performing Subtask II, Item 2 of the TTR and, in part, meets Deliverable 6 of the TTR. The work was performed following the Task Technical and Quality Assurance Plan (TTQAP), SRNL-RP-2011-00247, Rev. 0 and Analytical Study Plan (ASP), SRNL-RP-2011-00248, Rev. 0. In order to determine the reportable radionuclides for SB7b (MB9), a list of radioisotopes that may meet the criteria as specified by the Department of Energy’s (DOE) WAPS was developed. All radioactive U-235 fission products and all radioactive activation products that could be in the SRS HLW were considered. In addition, all U and Pu isotopes identified in WAPS 1.6 were included in the list. This list was then evaluated and some isotopes were excluded from the projection calculations. Based on measurements and analytical detection limits, 27 radionuclides have been identified as reportable for DWPF SB7b as specified by WAPS 1.2. The WCP and WQR require that all of the radionuclides present in the Design Basis glass be considered as the initial set of reportable radionuclides. For SB7b, all of the radionuclides in the Design Basis glass are reportable except for three radionuclides: Pd-107, Cs-135, and Th-230. At no time during the 1100-year period between 2015 and 3115 did any of these three radionuclides contribute to more than 0.01% of the radioactivity on a Curie basis. Two additional uranium isotopes (U-235 and -236) must be added to the list of reportable radionuclides in order to meet WAPS 1.6. All of the Pu isotopes (Pu-238, -239, -240, -241, and -242) and other U isotopes (U-233, -234, and -238) identified in WAPS 1.6 were already determined to be reportable according to WAPS 1.2 This brings the total number of reportable radionuclides for SB7b to 29. The radionuclide measurements made for SB7b are similar to those performed in the previous SB7a MB8 work. Some method development/refine

  15. DETERMINATION OF REPORTABLE RADIONUCLIDES FOR DWPF SLUDGE BATCH 7B (MACROBATCH 9)

    SciTech Connect (OSTI)

    Crawford, C. L.; Diprete, D. P.

    2014-05-01

    The Waste Acceptance Product Specifications (WAPS) 1.2 require that “The Producer shall report the inventory of radionuclides (in Curies) that have half-lives longer than 10 years and that are, or will be, present in concentrations greater than 0.05 percent of the total inventory for each waste type indexed to the years 2015 and 3115”. As part of the strategy to comply with WAPS 1.2, the Defense Waste Processing Facility (DWPF) will report for each waste type, all radionuclides (with half-lives greater than 10 years) that have concentrations greater than 0.01 percent of the total inventory from time of production through the 1100 year period from 2015 through 3115. The initial listing of radionuclides to be included is based on the design-basis glass as identified in the Waste Form Compliance Plan (WCP) and Waste Form Qualification Report (WQR). However, it is required that this list be expanded if other radionuclides with half-lives greater than 10 years are identified that may meet the greater than 0.01% criterion for Curie content. Specification 1.6 of the WAPS, International Atomic Energy Agency (IAEA) Safeguards Reporting for High Level Waste (HLW), requires that the ratio by weights of the following uranium and plutonium isotopes be reported: U-233, U-234, U-235, U-236, U-238, Pu-238, Pu-239, Pu-240, Pu-241, and Pu- 242. Therefore, the complete set of reportable radionuclides must also include this set of U and Pu isotopes. The DWPF is receiving radioactive sludge slurry from HLW Tank 40. The radioactive sludge slurry in Tank 40 is a blend of the heel from Sludge Batch 7a (SB7a) and Sludge Batch 7b (SB7b) that was transferred to Tank 40 from Tank 51. The blend of sludge in Tank 40 is also referred to as Macrobatch 9 (MB9). This report develops the list of reportable radionuclides and associated activities as a function of time. The DWPF will use this list and the activities as one of the inputs for the development of the Production Records that relate to radionuclide inventory. This work was initiated through Technical Task Request (TTR) HLW-DWPF-TTR-2011-0004; Rev. 0 entitled Sludge Batch 7b Qualification Studies. Specifically, this report details results from performing Subtask II, Item 2 of the TTR and, in part, meets Deliverable 6 of the TTR. The work was performed following the Task Technical and Quality Assurance Plan (TTQAP), SRNL-RP-2011-00247, Rev. 0 and Analytical Study Plan (ASP), SRNL-RP-2011-00248, Rev. 0. In order to determine the reportable radionuclides for SB7b (MB9), a list of radioisotopes that may meet the criteria as specified by the Department of Energy’s (DOE) WAPS was developed. All radioactive U- 235 fission products and all radioactive activation products that could be in the SRS HLW were considered. In addition, all U and Pu isotopes identified in WAPS 1.6 were included in the list. This list was then evaluated and some isotopes were excluded from the projection calculations. Based on measurements and analytical detection limits, 27 radionuclides have been identified as reportable for DWPF SB7b as specified by WAPS 1.2. The WCP and WQR require that all of the radionuclides present in the Design Basis glass be considered as the initial set of reportable radionuclides. For SB7b, all of the radionuclides in the Design Basis glass are reportable except for three radionuclides: Pd-107, Cs-135, and Th-230. At no time during the 1100- year period between 2015 and 3115 did any of these three radionuclides contribute to more than 0.01% of the radioactivity on a Curie basis. Two additional uranium isotopes (U-235 and -236) must be added to the list of reportable radionuclides in order to meet WAPS 1.6. All of the Pu isotopes (Pu-238, -239, -240, -241, and -242) and other U isotopes (U-233, -234, and -238) identified in WAPS 1.6 were already determined to be reportable according to WAPS 1.2 This brings the total number of reportable radionuclides for SB7b to 29. The radionuclide measurements made for SB7b are similar to those performed in the previous SB7a MB8 work. Some method development/ref

  16. SLUDGE WASHING AND DEMONSTRATION OF THE DWPF FLOWSHEET IN THE SRNL SHIELDED CELLS FOR SLUDGE BATCH 6 QUALIFICATION

    SciTech Connect (OSTI)

    Pareizs, J.; Pickenheim, B.; Bannochie, C.; Billings, A.; Bibler, N.; Click, D.

    2010-10-01

    Prior to initiating a new sludge batch in the Defense Waste Processing Facility (DWPF), Savannah River National Laboratory (SRNL) is required to simulate this processing, including Chemical Process Cell (CPC) simulation, waste glass fabrication, and chemical durability testing. This report documents this simulation for the next sludge batch, Sludge Batch 6 (SB6). SB6 consists of Tank 12 material that has been transferred to Tank 51 and subjected to Low Temperature Aluminum Dissolution (LTAD), Tank 4 sludge, and H-Canyon Pu solutions. Following LTAD and the Tank 4 addition, Liquid Waste Operations (LWO) provided SRNL a 3 L sample of Tank 51 sludge for SB6 qualification. Pu solution from H Canyon was also received. SB6 qualification included washing the sample per LWO plans/projections (including the addition of Pu from H Canyon), DWPF CPC simulations, waste glass fabrication (vitrification), and waste glass characterization and chemical durability evaluation. The following are significant observations from this demonstration. Sludge settling improved slightly as the sludge was washed. SRNL recommended (and the Tank Farm implemented) one less wash based on evaluations of Tank 40 heel projections and projections of the glass composition following transfer of Tank 51 to Tank 40. Thorium was detected in significant quantities (>0.1 wt % of total solids) in the sludge. In past sludge batches, thorium has been determined by Inductively Coupled Plasma-Mass Spectroscopy (ICP-MS), seen in small quantities, and reported with the radionuclides. As a result of the high thorium, SRNL-AD has added thorium to their suite of Inductively Coupled Plasma-Atomic Emission Spectroscopy (ICP-AES) elements. The acid stoichiometry for the DWPF Sludge Receipt and Adjustment Tank (SRAT) processing of 115%, or 1.3 mol acid per liter of SRAT receipt slurry, was adequate to accomplish some of the goals of SRAT processing: nitrite was destroyed to below 1,000 mg/kg and mercury was removed to below the DWPF target with 750 g of steam per g of mercury. However, rheological properties did not improve and were above the design basis. Hydrogen generation rates did not exceed DWPF limits during the SRAT and Slurry Mix Evaporator (SME) cycles. However, hydrogen generation during the SRAT cycle approached the DWPF limit. The glass fabricated with the Tank 51 SB6 SME product and Frit 418 was acceptable with respect to chemical durability as measured by the Product Consistency Test (PCT). The PCT response was also predictable by the current durability models of the DWPF Product Composition Control System (PCCS). It should be noted, however, that in the first attempt to make glass from the SME product, the contents of the fabrication crucible foamed over. This may be a result of the SME product's REDOX (Reduction/Oxidation - Fe{sup 2+}/{Sigma}Fe) of 0.08 (calculated from SME product analytical results). The following are recommendations drawn from this demonstration. In this demonstration, at the request of DWPF, SRNL caustic boiled the SRAT contents prior to acid addition to remove water (to increase solids concentration). During the nearly five hours of caustic boiling, 700 ppm of antifoam was required to control foaming. SRNL recommends that DWPF not caustic boil/concentrate SRAT receipt prior to acid addition until further studies can be performed to provide a better foaming control strategy or a new antifoam is developed for caustic boiling. Based on this set of runs and a recently completed demonstration with the SB6 Waste Acceptance Product Specifications (WAPS) sample, it is recommended that DWPF not add formic acid at the design addition rate of two gallons per minute for this sludge batch. A longer acid addition time appears to be helpful in allowing slower reaction of formic acid with the sludge and possibly decreases the chance of a foam over during acid addition.

  17. Batch methods for enriching trace impurities in hydrogen gas for their further analysis

    DOE Patents [OSTI]

    Ahmed, Shabbir; Lee, Sheldon H.D.; Kumar, Romesh; Papdias, Dionissios D.

    2014-07-15

    Provided herein are batch methods and devices for enriching trace quantities of impurities in gaseous mixtures, such as hydrogen fuel. The methods and devices rely on concentrating impurities using hydrogen transport membranes wherein the time period for concentrating the sample is calculated on the basis of optimized membrane characteristics, comprising its thickness and permeance, with optimization of temperature, and wherein the enrichment of trace impurities is proportional to the pressure ratio P.sub.hi/P.sub.lo and the volume ratio V.sub.1/V.sub.2, with following detection of the impurities using commonly-available detection methods.

  18. Batch polymerization of styrene and isoprene by n-butyl lithium initiator 

    E-Print Network [OSTI]

    Hasan, Sayeed

    1970-01-01

    BATCN ?OLYMERIZATION OF STYRENE AND ISO?RENE BY n-BUTYL LITHIUM INITIATOR A Thesis SAYEED IIASAV Submitted to the Graduate College of Texas A&M University in partial fulfillment of the requirement for the d pre of IJASTER OF SCIFNCE... ler) CP3 MV gse P . January 1970 9&ZS&8 ABSTRACT Batch Polymerization of Styrene and Isoprene By n-Butyl Lithium Initiator. (January 1970) Sayeed 1Iasan, B. Sc. , East Pakistan University of Engineering and Technology, Dacca Directed by: Dr...

  19. Selective batch crushing in the coal-preparation shop at OAO NTMK

    SciTech Connect (OSTI)

    N.A. Berkutov; Yu.V. Stepanov; P.V. Shtark; L.A. Makhortova; N.K. Popova; D.A. Koshkarov; N.V. Tsarev [OAO Nizhnetagil'skii Metallurgicheskii Kombinat (NTMK)(Russian Federation)

    2007-05-15

    In September 2004, after reconstruction at OAO Nizhnetagil'skii Metallurgicheskii Kombinat (NTMK), blast furnace 6 went into operation for the production of vanadium from hot metal. At the startup of furnace 6, besides optimising its composition; it was decided to restore selective crushing of the coal batch using pneumatic and mechanical separation in the third unit of the coal preparation shop. Additional increase in the mechanical strength of coke by 1.5-2.0% was predicted with a 0.5-1.0% decrease in wear.

  20. Determination Of Reportable Radionuclides For DWPF Sludge Batch 7B (Macrobatch 9)

    SciTech Connect (OSTI)

    Crawford, C. L.; Diprete, D. P.

    2012-12-17

    The DWPF is receiving radioactive sludge slurry from HLW Tank 40. The radioactive sludge slurry in Tank 40 is a blend of the heel from Sludge Batch 7a (SB7a) and Sludge Batch 7b (SB7b) that was transferred to Tank 40 from Tank 51. The blend of sludge in Tank 40 is also referred to as Macrobatch 9 (MB9). This report develops the list of reportable radionuclides and associated activities as a function of time. Twenty-seven radionuclides have been identified as reportable for DWPF SB7b. Each of these radionuclides has a half-life greater than ten years and contributes more than 0.01% of the radioactivity on a Curie basis at some point from production through the 1100 year period between 2015 and 3115. For SB7b, all of the radionuclides in the Design Basis glass are reportable except for three radionuclides: Pd-107, Cs-135, and Th-230. At no time during the 1100- year period between 2015 and 3115 did any of these three radionuclides contribute to more than 0.01% of the radioactivity on a Curie basis. The radionuclide measurements made for SB7b are the most extensive conducted to date. Some method development/refinement occurred during the conduct of these measurements, leading to lower detection limits and more accurate measurement of some isotopes than was previously possible.

  1. Kinetic model for quartz and spinel dissolution during melting of high-level-waste glass batch

    SciTech Connect (OSTI)

    Pokorny, Richard; Rice, Jarrett A.; Crum, Jarrod V.; Schweiger, Michael J.; Hrma, Pavel R.

    2013-07-24

    The dissolution of quartz particles and the growth and dissolution of crystalline phases during the conversion of batch to glass potentially affects both the glass melting process and product quality. Crystals of spinel exiting the cold cap to molten glass below can be troublesome during the vitrification of iron-containing high-level wastes. To estimate the distribution of quartz and spinel fractions within the cold cap, we used kinetic models that relate fractions of these phases to temperature and heating rate. Fitting the model equations to data showed that the heating rate, apart from affecting quartz and spinel behavior directly, also affects them indirectly via concurrent processes, such as the formation and motion of bubbles. Because of these indirect effects, it was necessary to allow one kinetic parameter (the pre-exponential factor) to vary with the heating rate. The resulting kinetic equations are sufficiently simple for the detailed modeling of batch-to-glass conversion as it occurs in glass melters. The estimated fractions and sizes of quartz and spinel particles as they leave the cold cap, determined in this study, will provide the source terms needed for modeling the behavior of these solid particles within the flow of molten glass in the melter.

  2. INTERPRETATION OF AT-LINE SPECTRA FROM AFS-2 BATCH #3 FERROUS SULFAMATE TREATMENT

    SciTech Connect (OSTI)

    Kyser, E.; O'Rourke, P.

    2013-12-10

    Spectra from the “at-line” spectrometer were obtained during the ferrous sulfamate (FS) valence adjustment step of AFS-2 Batch #3 on 9/18/2013. These spectra were analyzed by mathematical principal component regression (PCR) techniques to evaluate the effectiveness of this treatment. Despite the complications from Pu(IV), we conclude that all Pu(VI) was consumed during the FS treatment, and that by the end of the treatment, about 85% was as Pu(IV) and about 15% was as Pu(III). Due to the concerns about the “odd” shape of the Pu(IV) peak and the possibility of this behavior being observed in the future, a follow-up sample was sent to SRNL to investigate this further. Analysis of this sample confirmed the previous results and concluded that it “odd” shape was due to an intermediate acid concentration. Since the spectral evidence shows complete reduction of Pu(VI) we conclude that it is appropriate to proceed with processing of this the batch of feed solution for HB-Line including the complexation of the fluoride with aluminum nitrate.

  3. Verification Of The Defense Waste Processing Facility's (DWPF) Process Digestion Methods For The Sludge Batch 8 Qualification Sample

    SciTech Connect (OSTI)

    Click, D. R.; Edwards, T. B.; Wiedenman, B. J.; Brown, L. W.

    2013-03-18

    This report contains the results and comparison of data generated from inductively coupled plasma – atomic emission spectroscopy (ICP-AES) analysis of Aqua Regia (AR), Sodium Peroxide/Sodium Hydroxide Fusion Dissolution (PF) and Cold Chem (CC) method digestions and Cold Vapor Atomic Absorption analysis of Hg digestions from the DWPF Hg digestion method of Sludge Batch 8 (SB8) Sludge Receipt and Adjustment Tank (SRAT) Receipt and SB8 SRAT Product samples. The SB8 SRAT Receipt and SB8 SRAT Product samples were prepared in the SRNL Shielded Cells, and the SRAT Receipt material is representative of the sludge that constitutes the SB8 Batch or qualification composition. This is the sludge in Tank 51 that is to be transferred into Tank 40, which will contain the heel of Sludge Batch 7b (SB7b), to form the SB8 Blend composition.

  4. An experimental system for the n-butyl-lithium initiated polymerization of styrene in a multi-sampled batch reactor 

    E-Print Network [OSTI]

    Cox, James Harvey

    1974-01-01

    AN EXPERIMENTAL SYSTEM FOR THE n-BUTYLLITHIUM INITIATED POLYMERIZATION OF STYRENE IN A MULTI-SAMPLED BATCH REACTOR A Thesis by JAMES HARVEY COX, JR. Submitted to the Graduate College of Texas A&M University in partial fulfillment... of the requirement for the degree of MASTER OF SCIENCE May 1974 Ma]or Subject: Chemical Engineering AN EXPERIMENTAL SYSTEM FOR THE n-BUTYLLITHIUM INITIATED POLYMERIZATION OF STYRENE IN A MULTI-SAMPLED BATCH REACTOR A Thesis by JAMES HARVEY COX, JR. Approved...

  5. Analysis of tank 23H samples in support of salt batch planning

    SciTech Connect (OSTI)

    Hay, M. S.; Coleman, C. J.; Diprete, D. P.

    2015-08-14

    Savannah River Remediation obtained three samples from different heights within Tank 23H. The samples were analyzed by Savannah River National Laboratory to support salt batch planning. The results from the analysis indicate the top two samples from the tank appear similar in composition. The lowest sample from the tank contained significantly more solids and a more concentrated salt solution. The filtered supernate from the bottom sample showed ~60% lower Sr-90 and Pu-238 concentrations than the decanted (unfiltered) supernate results which may indicate the presence of some small amount of entrained solid particles in the decanted sample. The mercury concentrations measured in the filtered supernate were fairly low for all three samples ranging from 11.2 to 42.3 mg/L.

  6. Numerical model for the vacuum pyrolysis of scrap tires in batch reactors

    SciTech Connect (OSTI)

    Yang, J.; Tanguy, P.A.; Roy, C.

    1995-06-01

    A quantitative model for scrap tire pyrolysis in a batch scale reactor developed comprises the following basic phenomena: conduction inside tire particles; conduction, convection, and radiation between the feedstock particles or between the fluids and the particles; tire pyrolysis reaction; exothermicity and endothermicity caused by tire decomposition and volatilization; and the variation of the composition and the thermal properties of tire particles. This model was used to predict the transient temperature and density distributions in the bed of particles, the volatile product evolution rate, the mass change, the energy consumption during the pyrolysis process, and the pressure history in a tire pyrolysis reactor with a load of 1 kg. The model predictions agree well with independent experimental data.

  7. DWPF coupled feed flowsheet material balance with batch one sludge and copper nitrate catalyst

    SciTech Connect (OSTI)

    Choi, A.S.

    1993-09-28

    The SRTC has formally transmitted a recommendation to DWPF to replace copper formate with copper nitrate as the catalyst form during precipitate hydrolysis [1]. The SRTC was subsequently requested to formally document the technical bases for the recommendation. A memorandum was issued on August 23, 1993 detailing the activities (and responsible individuals) necessary to address the impact of this change in catalyst form on process compatibility, safety, processibility environmental impact and product glass quality [2]. One of the activities identified was the preparation of a material balance in which copper nitrate is substituted for copper formate and the identification of key comparisons between this material balance and the current Batch 1 sludge -- Late Wash material balance [3].

  8. AUTOMATED BATCH CHARACTERIZATION OF ICF SHELLS WITH VISION-ENABLED OPTICAL MICROSCOPE SYSTEM

    SciTech Connect (OSTI)

    HUANG,H; STEPHENS,R.B; HILL,D.W; LYON,C; NIKROO,A; STEINMAN,D.A

    2003-06-01

    OAK-B135 Inertial Confinement Fusion (ICF) shells are mesoscale objects with nano-scale dimensional and nano-surface finish requirements. Currently, the shell dimensions are measured by white-light interferometry and an image analysis method. These two methods complement each other and give a rather complete data set on a single shell. The process is, however, labor intensive. They have developed an automation routine to fully characterize a shell in one shot and perform unattended batch measurements. The method is useful to the ICF program both for production screening and for full characterization. It also has potential for Inertial Fusion Energy (IFE) power plant where half a million shells need to be processed daily.

  9. JOURNAL OF MICROELECTROMECHANICAL SYSTEMS, VOL. 10, NO. 1, MARCH 2001 25 Batch Transfer of LIGA Microstructures by Selective

    E-Print Network [OSTI]

    Lin, Liwei

    Microstructures by Selective Electroplating and Bonding Li-Wei Pan and Liwei Lin Abstract--A flip-chip, batch demonstrated by selective electroplating and bonding. Single layer LIGA microstructures with thickness of 200 m of bonding via electroplating. After the selective bonding process, the originally fixed microstructures

  10. A mathematical model for batch and continuous thickening of flocculated suspensions in vessels with varying cross-section

    E-Print Network [OSTI]

    Karlsen, Kenneth Hvistendahl

    A mathematical model for batch and continuous thickening of flocculated suspensions in vessels of continuous thickening of flocculated suspensions in an ideal cylindrical thickener is extended to vessels having varying cross-section, including divergent or convergent conical vessels. The purpose

  11. Three-Dimensional Flow and Thermal Structures in Glass Melting Furnaces. Part II: Effect of Batch and Bubbles.

    E-Print Network [OSTI]

    Pilon, Laurent

    Three-Dimensional Flow and Thermal Structures in Glass Melting Furnaces. Part II: Effect of Batch and thermal structure in glass melting furnaces with a throat. The effects of the following parameters This is a second part of a study concerned with the three-dimensional natural circulation in glass melting furnaces

  12. 1. Batch reaction experiment Cu, Ni and Zn show increased concentrations with the addition of CO2,

    E-Print Network [OSTI]

    capacity by pressure relief, or from CO2-Enhanced Oil Recovery. Currently, produced waters from oil and gas sandstone shows that total concen- trations of the eight metals of interest are low ( 30 g/g), with leached%) are also low. Figure 2. Batch experiment metal concentrations through time for Captain, Cormorant

  13. VERIFICATION OF THE DEFENSE WASTE PROCESSING FACILITY'S (DWPF) PROCESS DIGESTION METHOD FOR THE SLUDGE BATCH 7A QUALIFICATION SAMPLE

    SciTech Connect (OSTI)

    Click, D.; Edwards, T.; Jones, M.; Wiedenman, B.

    2011-03-14

    For each sludge batch that is processed in the Defense Waste Processing Facility (DWPF), the Savannah River National Laboratory (SRNL) performs confirmation of the applicability of the digestion method to be used by the DWPF lab for elemental analysis of Sludge Receipt and Adjustment Tank (SRAT) receipt samples and SRAT product process control samples. DWPF SRAT samples are typically dissolved using a room temperature HF-HNO{sub 3} acid dissolution (i.e., DWPF Cold Chem Method, see DWPF Procedure SW4-15.201) and then analyzed by inductively coupled plasma - atomic emission spectroscopy (ICP-AES). This report contains the results and comparison of data generated from performing the Aqua Regia (AR), Sodium peroxide/Hydroxide Fusion (PF) and DWPF Cold Chem (CC) method digestions of Sludge Batch 7a (SB7a) SRAT Receipt and SB7a SRAT Product samples. The SB7a SRAT Receipt and SB7a SRAT Product samples were prepared in the SRNL Shielded Cells, and the SRAT Receipt material is representative of the sludge that constituates the SB7a Batch or qualification composition. This is the sludge in Tank 51 that is to be transferred into Tank 40, which will contain the heel of Sludge Batch 6 (SB6), to form the Sb7a Blend composition.

  14. Pipeline and Batch Sharing in Grid Workloads Douglas Thain, John Bent, Andrea C. Arpaci-Dusseau, Remzi H. Arpaci-Dusseau, and Miron Livny

    E-Print Network [OSTI]

    Arpaci-Dusseau, Remzi

    Pipeline and Batch Sharing in Grid Workloads Douglas Thain, John Bent, Andrea C. Arpaci Abstract We present a study of six batch-pipelined scientific workloads that are candidates for execution characterizes workloads composed of pipelines of sequential processes that use file storage for communication

  15. SJSU Information Support Services Run Batch Contracts for Temporary Faculty info-support@sjsu.edu, 408-924-1530 Page 1

    E-Print Network [OSTI]

    Su, Xiao

    page displays. 5. Term: Use the lookup button to search the appropriate term. 6. Due Date: (optional data that exists in the system for the temporary faculty will appear on the Contract Appointment letter/Terms. 2. Click Batch Contracts for T. Faculty. The Batch Process for TF Contract search page displays. 3

  16. THE SLUDGE BATCH 7A GLASS VARIABILITY STUDY WITH FRIT 418 AND FRIT 702

    SciTech Connect (OSTI)

    Peeler, D.; Edwards, T.

    2011-03-24

    The Defense Waste Processing Facility (DWPF) is preparing to initiate processing of Sludge Batch 7a (SB7a) in May 2011. To support qualification of SB7a, the Savannah River National Laboratory (SRNL) was requested to execute a variability study (VS) to assess the applicability of the current Product Composition Control System (PCCS) durability models for the Frit 418-SB7a compositional region of interest. The objective of this study was to demonstrate applicability of the current durability models to the SB7a compositional region of interest and acceptability of the SB7a glasses with respect to the Environmental Assessment (EA) glass in terms of durability as defined by the Product Consistency Test (PCT). To support programmatic objectives, twenty-eight SB7a glasses were selected based on the nominal sludge projections used to support the frit recommendation. Twenty-three of the SB7a VS glasses were based on the use of Frit 418, while 5 glasses were based on the use of Frit 702. Frit 702 was also identified as a viable candidate for SB7a, especially if SO{sub 4} concentrations are found to be higher than anticipated. Frit 702 has shown a higher SO{sub 4} retention capability as compared to Frit 418. With respect to acceptability, the PCT results of the SB7a-VS glasses are acceptable relative to the EA glass regardless of thermal history (quenched or canister centerline cooled) or compositional view (target or measured). More specifically, all of the SB7a glasses have normalized boron release values (NL [B]) less than 0.9 g/L as compared to the benchmark NL [B] value for EA of 16.695 g/L. With respect to the applicability of the current durability models to the SB7a VS compositional region of interest, all of the study glasses (based on target compositions) lie within the 95% confidence intervals of the model predictions. When model applicability is based on the measured compositions, all of the SB7a VS glasses are predictable with the exception of SB7aVS-02 and SB7aVS-06. Although the NL [B] values of these two glasses range from 0.66 to 0.73 g/L (considered very acceptable), the PCT responses are not considered predictable by the current durability models. The current durability models are conservative for these glasses since they are more durable than predicted by the models. These two glasses are extreme vertices (EV) based compositions coupled with Frit 418 at 36% WL and target the maximum Na{sub 2}O content (15.01 wt% Na{sub 2}O) of the SB7a VS glasses. Higher alkali glasses for which the model overpredicts the PCT response have been observed previously in the Sludge Batch 3 (SB3) Phase 1 VS and the Sludge Batch 6 (SB6) VS.

  17. Completing Pre-Pilot Tasks To Scale Up Biomass Fractionation Pretreatment Apparatus From Batch To Continuous

    SciTech Connect (OSTI)

    Dick Wingerson

    2004-12-15

    PureVision Technology, Inc. (PureVision) was the recipient of a $200,000 Invention and Innovations (I&I) grant from the U. S. Department of Energy (DOE) to complete prepilot tasks in order to scale up its patented biomass fractionation pretreatment apparatus from batch to continuous processing. The initial goal of the I&I program, as detailed in PureVision's original application to the DOE, was to develop the design criteria to build a small continuous biomass fractionation pilot apparatus utilizing a retrofitted extruder with a novel screw configuration to create multiple reaction zones, separated by dynamic plugs within the reaction chamber that support the continuous counter-flow of liquids and solids at elevated temperature and pressure. Although the ultimate results of this 27-month I&I program exceeded the initial expectations, some of the originally planned tasks were not completed due to a modification of direction in the program. PureVision achieved its primary milestone by establishing the design criteria for a continuous process development unit (PDU). In addition, PureVision was able to complete the procurement, assembly, and initiate shake down of the PDU at Western Research Institute (WRI) in Laramie, WY during August 2003 to February 2004. During the month of March 2004, PureVision and WRI performed initial testing of the continuous PDU at WRI.

  18. Batch Microreactor Studies of Lignin Depolymerization by Bases. 1. Alcohol Solvents

    SciTech Connect (OSTI)

    MILLER, JAMES E.; EVANS, LINDSEY; LITTLEWOLF, ALICIA; TRUDELL, DANIEL E.

    2002-05-01

    Biomass feedstocks contain roughly 10-30% lignin, a substance that can not be converted to fermentable sugars. Hence, most schemes for producing biofuels (ethanol) assume that the lignin coproduct will be utilized as boiler fuel to provide heat and power to the process. However, the chemical structure of lignin suggests that it will make an excellent high value fuel additive, if it can be broken down into smaller molecular units. From fiscal year 1997 through fiscal year 2001, Sandia National Laboratories was a participant in a cooperative effort with the National Renewable Energy Laboratory and the University of Utah to develop and scale a base catalyzed depolymerization (BCD) process for lignin conversion. SNL's primary role in the effort was to utilize rapidly heated batch microreactors to perform kinetic studies, examine the reaction chemistry, and to develop alternate catalyst systems for the BCD process. This report summarizes the work performed at Sandia during FY97 and FY98 with alcohol based systems. More recent work with aqueous based systems will be summarized in a second report.

  19. Method for automatically evaluating a transition from a batch manufacturing technique to a lean manufacturing technique

    DOE Patents [OSTI]

    Ivezic, Nenad; Potok, Thomas E.

    2003-09-30

    A method for automatically evaluating a manufacturing technique comprises the steps of: receiving from a user manufacturing process step parameters characterizing a manufacturing process; accepting from the user a selection for an analysis of a particular lean manufacturing technique; automatically compiling process step data for each process step in the manufacturing process; automatically calculating process metrics from a summation of the compiled process step data for each process step; and, presenting the automatically calculated process metrics to the user. A method for evaluating a transition from a batch manufacturing technique to a lean manufacturing technique can comprise the steps of: collecting manufacturing process step characterization parameters; selecting a lean manufacturing technique for analysis; communicating the selected lean manufacturing technique and the manufacturing process step characterization parameters to an automatic manufacturing technique evaluation engine having a mathematical model for generating manufacturing technique evaluation data; and, using the lean manufacturing technique evaluation data to determine whether to transition from an existing manufacturing technique to the selected lean manufacturing technique.

  20. Determination of actinides in environmental samples with ICP-MS and automated batch preconcentration

    SciTech Connect (OSTI)

    Crain, J.S.; Smith, L.L.; Alvaradao, J.A. [Argonne National Laboratory, IL (United States)] [and others

    1994-12-31

    Thorium, uranium, and uranium progeny (e.g., {sup 226}Ra) were isolated from a variety of natural water matrices (well, spring, lake, river, and tap waters) using automated batch separation and a proprietary chelating resin. Minimal sample treatment was required in advance of the chemical separation procedure, i.e., samples were acidified, enriched isotopes were added and equilibrated, and, in certain cases, samples were filtered to remove biomass and other particulate matter. Major elemental constituents (e.g., Mg and Ca) were removed by the chemical separation. The isolated actinides and their detectable progeny were then determined using isotope dilution inductively coupled plasma-mass spectrometry combined with ultrasonic nebulization; flow injection was also used to improve sample utilization efficiency and increase the practical limit of preconcentration. Preconcentration factors of ca. 50 were achievable, thereby allowing determination of the isotopes TA interest at concentrations below 1 pg/L (i.e., 1 pCi/L of {sup 226}Ra). The internal and external reproducibility of these measurements will be described, as will their comparability to results obtained by radiochemical means. The authors will also discuss the utility of this procedure for environmental surveillance and the examination of uranium series disequilibria in natural aqueous systems.

  1. Power/Performance Trade-offs of Small Batched LU Based Solvers on GPUs

    SciTech Connect (OSTI)

    Villa, Oreste; Fatica, Massimiliano; Gawande, Nitin A.; Tumeo, Antonino

    2013-08-26

    In this paper we propose and analyze a set of batched linear solvers for small matrices on Graphic Processing Units (GPUs), evaluating the various alternatives depending on the size of the systems to solve. We discuss three different solutions that operate with different level of parallelization and GPU features. The first, exploiting the CUBLAS library, manages matrices of size up to 32x32 and employs Warp level (one matrix, one Warp) parallelism and shared memory. The second works at Thread-block level parallelism (one matrix, one Thread-block), still exploiting shared memory but managing matrices up to 76x76. The third is Thread level parallel (one matrix, one thread) and can reach sizes up to 128x128, but it does not exploit shared memory and only relies on the high memory bandwidth of the GPU. The first and second solution only support partial pivoting, the third one easily supports partial and full pivoting, making it attractive to problems that require greater numerical stability. We analyze the trade-offs in terms of performance and power consumption as function of the size of the linear systems that are simultaneously solved. We execute the three implementations on a Tesla M2090 (Fermi) and on a Tesla K20 (Kepler).

  2. RASTtk: A modular and extensible implementation of the RAST algorithm for building custom annotation pipelines and annotating batches of genomes

    SciTech Connect (OSTI)

    Brettin, Thomas; Davis, James J.; Disz, Terry; Edwards, Robert A.; Gerdes, Svetlana; Olsen, Gary J.; Olson, Robert; Overbeek, Ross; Parrello, Bruce; Pusch, Gordon D.; Shukla, Maulik; Thomason, III, James A.; Stevens, Rick; Vonstein, Veronika; Wattam, Alice R.; Xia, Fangfang

    2015-02-10

    The RAST (Rapid Annotation using Subsystem Technology) annotation engine was built in 2008 to annotate bacterial and archaeal genomes. It works by offering a standard software pipeline for identifying genomic features (i.e., protein-encoding genes and RNA) and annotating their functions. Recently, in order to make RAST a more useful research tool and to keep pace with advancements in bioinformatics, it has become desirable to build a version of RAST that is both customizable and extensible. In this paper, we describe the RAST tool kit (RASTtk), a modular version of RAST that enables researchers to build custom annotation pipelines. RASTtk offers a choice of software for identifying and annotating genomic features as well as the ability to add custom features to an annotation job. RASTtk also accommodates the batch submission of genomes and the ability to customize annotation protocols for batch submissions. This is the first major software restructuring of RAST since its inception.

  3. RASTtk: A modular and extensible implementation of the RAST algorithm for building custom annotation pipelines and annotating batches of genomes

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Brettin, Thomas; Davis, James J.; Disz, Terry; Edwards, Robert A.; Gerdes, Svetlana; Olsen, Gary J.; Olson, Robert; Overbeek, Ross; Parrello, Bruce; Pusch, Gordon D.; et al

    2015-02-10

    The RAST (Rapid Annotation using Subsystem Technology) annotation engine was built in 2008 to annotate bacterial and archaeal genomes. It works by offering a standard software pipeline for identifying genomic features (i.e., protein-encoding genes and RNA) and annotating their functions. Recently, in order to make RAST a more useful research tool and to keep pace with advancements in bioinformatics, it has become desirable to build a version of RAST that is both customizable and extensible. In this paper, we describe the RAST tool kit (RASTtk), a modular version of RAST that enables researchers to build custom annotation pipelines. RASTtk offersmore »a choice of software for identifying and annotating genomic features as well as the ability to add custom features to an annotation job. RASTtk also accommodates the batch submission of genomes and the ability to customize annotation protocols for batch submissions. This is the first major software restructuring of RAST since its inception.« less

  4. SLUDGE BATCH 5 ACCEPTANCE EVALUATION RADIONUCLIDE CONCENTRATIONS IN TANK 51 SB5 QUALIFICATION SAMPLE PREPARED AT SRNL

    SciTech Connect (OSTI)

    Bannochie, C; Ned Bibler, N; David Diprete, D

    2008-07-28

    Presented in this report are radionuclide concentrations required as part of the program of qualifying Sludge Batch Five (SB5) for processing in the Defense Waste Processing Facility (DWPF). Part of this SB5 material is currently in Tank 51 being washed and prepared for transfer to Tank 40. The acceptance evaluation needs to be completed prior to the transfer of the material in Tank 51 to Tank 40 to complete the formation of SB5. The sludge slurry in Tank 40 has already been qualified for DWPF and is currently being processed as SB4. The radionuclide concentrations were measured or estimated in the Tank 51 SB5 Qualification Sample prepared at Savannah River National Laboratory (SRNL). This sample was prepared from the three liter sample of Tank 51 sludge slurry taken on March 21, 2008. The sample was delivered to SRNL where it was initially characterized in the Shielded Cells. Under direction of the Liquid Waste Organization it was then modified by five washes, six decants, an addition of Pu/Be from Canyon Tank 16.4, and an addition of NaNO2. This final slurry now has a composition expected to be similar to that of the slurry in Tank 51 after final preparations have been made for transfer of that slurry to Ta Determining the radionuclide concentrations in this Tank 51 SB5 Qualification Sample is part of the work requested in Technical Task Request (TTR) No. HLW-DWPF-TTR-2008-0010. The work with this qualification sample is covered by a Task Technical and Quality Assurance Plan and an Analytical Study Plan. The radionuclides included in this report are needed for the DWPF Radiological Program Evaluation, the DWPF Waste Acceptance Criteria (TSR/WAC) Evaluation, and the DWPF Solid Waste Characterization Program (TTR Task 2). Radionuclides required to meet the Waste Acceptance Product Specifications (TTR Task 5) will be measured at a later date after the slurry from Tank 51 has been transferred to Tank 40. Then a sample of the as-processed SB5 will be taken and transferred to SRNL for measurement of these radionuclides. Data presented in this report represents the measured or estimated radionuclide concentrations obtained from several standard and special analytical methods performed by Analytical Development (AD) personnel within SRNL. The method for I-129 measurement in sludge is described in detail. Most of these methods were performed on solutions resulting from the dissolutions of the slurry samples. Concentrations are given for twenty-nine radionuclides along with total alpha and beta activity. Values for total gamma and total gamma plus beta activities are also calculated. Results also indicate that 98% of the Tc-99 and 92% of the I-129 that could have been in this sludge batch have been removed by chemical processing steps in the SRS Canyons or Tank Farm.

  5. Large batch dimensional metrology demonstrated in the example of a LIGA fabricated spring.

    SciTech Connect (OSTI)

    Aigeldinger, Georg; Skala, Dawn M.; Ceremuga, Joseph T.

    2004-04-01

    Deep x-ray lithography in combination with electroforming is capable of producing high precision metal parts in small lot series. This study deals with a high aspect ratio structure with overall dimensions on the order of 10 mm x 7 mm x 1.5 mm, with the smallest line width being 150 {micro}m. The lateral deviation from the design is to be kept to a minimum, preferably below 5 {micro}m. To ensure adequate quality control, a semi-automated metrology technique has been established to measure all parts. While the paper will give a brief overview of all involved techniques, it focuses on the method to measure the top and bottom of the parts and the top of geometries following the process. The instrument used is a View Engineering Voyager V6x12 microscope, which is fully programmable. The microscope allows direct measurement of geometries but also is capable of saving all captured data as point clouds. These point clouds play a central role when evaluating part geometry. After measuring the part, the point cloud is compared to the computer aided design (CAD) contour of the part, using a commercially available software package. The challenge of proper edge lighting on a nickel alloy part is evaluated by varying lighting conditions systematically. Results of two conditions are presented along with a set of optimized parameters. With the introduced set of tools, process flow can be monitored by measuring geometries, e.g. linewidths in every step of the process line. An example for such analysis is given. After delivery of a large batch of parts, extensive numbers of datasets were available allowing the evaluation of the variation of part geometries. Discussed in detail is the deviation from part top to part bottom geometries indicating swelling of the PMMA mold in the electroplating bath.

  6. NEPHELINE FORMATION STUDY FOR SLUDGE BATCH 4: PHASE 3 EXPERIMENTAL RESULTS

    SciTech Connect (OSTI)

    Fox, K

    2006-05-01

    This Phase 3 study was undertaken to complement the previous phases of the nepheline formation studies1, 2 by continuing the investigation into the ability of the nepheline discriminator to predict the occurrence of nepheline crystallization in Sludge Batch 4 (SB4) glasses and into the impact of such phases on the durability of the SB4 glasses. The Phase 3 study had two primary objectives. The first was to continue to demonstrate the ability of the discriminator value to adequately predict the nepheline formation potential for specific glass systems of interest. The second was to generate additional data that have a high probability of supporting the SB4 variability study. To support these two objectives, sixteen glasses were selected based on the most recent SB4 compositional projection, Case 15C Blend 1.3 Four different frits were included, based on previous assessments of projected operating windows and melt rate,4, 5 with four WLs selected for each frit. Eight of these frit-sludge combinations covered WLs which tightly bound the nepheline discriminator value of 0.62, with the intent of refining this value to a level of confidence where it can be incorporated into offline administrative controls and/or the Process Composition Control System (PCCS) to support Slurry Mix Evaporator (SME) acceptability decisions. The remaining eight frit-sludge combinations targeted lower WLs (35 and 40%) and were prepared and analyzed to contribute needed data to the ComPro database6 to support a potential variability study for SB4.

  7. SLUDGE WASHING AND DEMONSTRATION OF THE DWPF FLOWSHEET IN THE SRNL SHIELDED CELLS FOR SLUDGE BATCH 5 QUALIFICATION

    SciTech Connect (OSTI)

    Pareizs, J; Cj Bannochie, C; Damon Click, D; Dan Lambert, D; Michael Stone, M; Bradley Pickenheim, B; Amanda Billings, A; Ned Bibler, N

    2008-11-10

    Sludge Batch 5 (SB5) is predominantly a combination of H-modified (HM) sludge from Tank 11 that underwent aluminum dissolution in late 2007 to reduce the total mass of sludge solids and aluminum being fed to the Defense Waste Processing Facility (DWPF) and Purex sludge transferred from Tank 7. Following aluminum dissolution, the addition of Tank 7 sludge and excess Pu to Tank 51, Liquid Waste Operations (LWO) provided the Savannah River National Laboratory (SRNL) a 3-L sample of Tank 51 sludge for SB5 qualification. SB5 qualification included washing the sample per LWO plans/projections (including the addition of a Pu/Be stream from H Canyon), DWPF Chemical Process Cell (CPC) simulations, waste glass fabrication (vitrification), and waste glass chemical durability evaluation. This report documents: (1) The washing (addition of water to dilute the sludge supernatant) and concentration (decanting of supernatant) of the Tank 51 qualification sample to adjust sodium content and weight percent insoluble solids to Tank Farm projections. (2) The performance of a DWPF CPC simulation using the washed Tank 51 sample. This includes a Sludge Receipt and Adjustment Tank (SRAT) cycle, where acid is added to the sludge to destroy nitrite and remove mercury, and a Slurry Mix Evaporator (SME) cycle, where glass frit is added to the sludge in preparation for vitrification. The SME cycle also included replication of five canister decontamination additions and concentrations. Processing parameters for the CPC processing were based on work with a non radioactive simulant. (3) Vitrification of a portion of the SME product and Product Consistency Test (PCT) evaluation of the resulting glass. (4) Rheology measurements of the initial slurry samples and samples after each phase of CPC processing. This work is controlled by a Task Technical and Quality Assurance Plan (TTQAP) , and analyses are guided by an Analytical Study Plan. This work is Technical Baseline Research and Development (R&D) for the DWPF.

  8. Problem 13.2 From our output below, we can see that the batch factor is significant with p-value .004.

    E-Print Network [OSTI]

    Marzban, Caren

    (x, y, pch = 1, cex = 2, col = "red", lwd = 2) 2 #12;STAT 421 Homework 10 -2 -1 0 1 2 -0.100.000.10 13$fitted.values[model$residuals > 0.05] y = model$residuals[model$residuals > 0.05] points(x, y, pch = 1, cex = 2, col = "red", lwd.05] points(x, y, pch = 1, cex = 2, col = "red", lwd = 2) 1 2 3 4 5 -0.100.000.10 Fitted Values vs batch Batch

  9. SLUDGE BATCH 6 ACCEPTANCE EVALUATION: RADIONUCLIDE CONCENTRATIONS IN TANK 51 SB6 QUALIFICATION SAMPLE PREPARED AT SRNL

    SciTech Connect (OSTI)

    Bannochie, C.; Bibler, N.; Diprete, D.

    2010-05-21

    Presented in this report are radionuclide concentrations required as part of the program of qualifying Sludge Batch Six (SB6) for processing in the Defense Waste Processing Facility (DWPF). The SB6 material is currently in Tank 51 being washed and prepared for transfer to Tank 40. The acceptance evaluation needs to be completed prior to the transfer of the material in Tank 51 to Tank 40. The sludge slurry in Tank 40 has already been qualified for DWPF and is currently being processed as SB5. The radionuclide concentrations were measured or estimated in the Tank 51 SB6 Qualification Sample prepared at Savannah River National Laboratory (SRNL). This sample was prepared from the three liter sample of Tank 51 sludge slurry (HTF-51-09-110) taken on October 8, 2009. The sample was delivered to SRNL where it was initially characterized in the Shielded Cells. Under the direction of the Liquid Waste Organization it was then modified by eight washes, nine decants, an addition of Pu from Canyon Tank 16.3, and an addition of NaNO{sub 2}. This final slurry now has a composition expected to be similar to that of the slurry in Tank 51 after final preparations have been made for transfer of that slurry to Tank 40. Determining the radionuclide concentrations in this Tank 51 SB6 Qualification Sample is part of the work requested in Technical Task Request (TTR) No. HLW-DWPF-TTR-2009-0014. The work with this qualification sample is covered by a Task Technical and Quality Assurance Plan and an Analytical Study Plan. The radionuclides included in this report are needed for the DWPF Radiological Program Evaluation, the DWPF Waste Acceptance Criteria (TSR/WAC) Evaluation, and the DWPF Solid Waste Characterization Program (TTR Task I.2). Radionuclides required to meet the Waste Acceptance Product Specifications (TTR Task II.2.) will be measured at a later date after the slurry from Tank 51 has been transferred to Tank 40. Then a sample of the as-processed SB6 will be taken and transferred to SRNL for measurement of these radionuclides. The results presented in this report are those necessary for DWPF to assess if the Tank 51 SB6 sample prepared at SRNL meets the requirements for the DWPF Radiological Program Evaluation, the DWPF Waste Acceptance Criteria evaluation, and the DWPF Solid Waste Characterization Program. The sample is the same as that on which the chemical composition was reported. Concentrations are given for thirty-four radionuclides along with total alpha and beta activity. Values for total gamma and total gamma plus beta activities are also calculated. Results also indicate that 99% of the Tc-99 and at least 90% of the I-129 that could have been in this sludge batch have been removed by chemical processing steps in the SRS Canyons or Tank Farm.

  10. Sludge Washing And Demonstration Of The DWPF Flowsheet In The SRNL Shielded Cells For Sludge Batch 8 Qualification

    SciTech Connect (OSTI)

    Pareizs, J. M.; Crawford, C. L.

    2013-04-26

    The current Waste Solidification Engineering (WSE) practice is to prepare sludge batches in Tank 51 by transferring sludge from other tanks to Tank 51. Tank 51 sludge is washed and transferred to Tank 40, the current Defense Waste Processing Facility (DWPF) feed tank. Prior to transfer of Tank 51 to Tank 40, the Savannah River National Laboratory (SRNL) typically simulates the Tank Farm and DWPF processes using a Tank 51 sample (referred to as the qualification sample). WSE requested the SRNL to perform characterization on a Sludge Batch 8 (SB8) sample and demonstrate the DWPF flowsheet in the SRNL shielded cells for SB8 as the final qualification process required prior to SB8 transfer from Tank 51 to Tank 40. A 3-L sample from Tank 51 (the SB8 qualification sample; Tank Farm sample HTF-51-12-80) was received by SRNL on September 20, 2012. The as-received sample was characterized prior to being washed. The washed material was further characterized and used as the material for the DWPF process simulation including a Sludge Receipt and Adjustment Tank (SRAT) cycle, a Slurry Mix Evaporator (SME) cycle, and glass fabrication and chemical durability measurements.

  11. SUMMARY REPORT FOR THE ANALYSIS OF THE SLUDGE BATCH 6 (MACROBATCH 7) DWPF POUR STREAM GLASS SAMPLE FOR CANISTER S03472

    SciTech Connect (OSTI)

    Johnson, F.

    2012-01-23

    In order to comply with the Waste Acceptance Specifications in Sludge Batch 6 (Macrobatch 7), Savannah River National Laboratory personnel performed characterization analyses on the Defense Waste Processing Facility (DWPF) pour stream glass sample collected while filling canister S03472. This report summarizes results of the characterization, which indicate that the DWPF produced glass that is significantly more durable than the Environmental Assessment glass. Results and further details are documented in 'Analysis of DWPF Sludge Batch 6 (Macrobatch 7) Pour Stream Glass Samples,' SRNL-STI-2011-00555.

  12. SUMMARY REPORT FOR THE ANALYSIS OF THE SLUDGE BATCH 7A (MACROBATCH 8) DWPF POUR STREAM GLASS SAMPLE FOR CANISTER S03619

    SciTech Connect (OSTI)

    Johnson, F.

    2012-05-01

    In order to comply with the Waste Acceptance Specifications in Sludge Batch 7a (Macrobatch 8), Savannah River National Laboratory personnel characterized the Defense Waste Processing Facility (DWPF) pour stream glass sample collected while filling canister S03619. This report summarizes the results of the compositional analysis for reportable oxides and radionuclides, and the normalized Product Consistency Test (PCT) results. The PCT responses indicate that the DWPF produced glass that is significantly more durable than the Environmental Assessment glass. Results and further details are documented in 'Analysis of DWPF Sludge Batch 7a (Macrobatch 8) Pour Stream Samples,' SRNL-STI-2012-00017.

  13. CRC DEPLETION CALCULATIONS FOR THE NON-RODDED ASSEMBLIES IN BATCHES 1, 2, AND 3 OF CRYSTAL RIVER UNIT 3

    SciTech Connect (OSTI)

    Kenneth D. Wright

    1997-07-29

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain non-rodded fuel assemblies from batches 1, 2, and 3 of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for Commercial Reactor Critical (CRC) evaluations to support development of the disposal criticality methodology. A non-rodded assembly is one which never contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) during its irradiation history. The objective of this analysis is to provide SAS2H generated isotopic compositions for each fuel assembly's depleted fuel and depleted burnable poison materials. These SAS2H generated isotopic compositions are acceptable for use in CRC benchmark reactivity calculations containing the various fuel assemblies.

  14. CRC DEPLETION CALCULATIONS FOR THE RODDED ASSEMBLIES IN BATCHES 1, 2, 3, AND 1X OF CRYSTAL RIVER UNIT 3

    SciTech Connect (OSTI)

    Kenneth D. Wright

    1997-09-03

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain rodded fuel assemblies from batches 1, 2, 3, and 1X of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for Commercial Reactor Critical (CRC) evaluations to support the development of the disposal criticality methodology. A rodded assembly is one that contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) for some period of time during its irradiation history. The objective of this analysis is to provide SAS2H calculated isotopic compositions of depleted fuel and depleted burnable poison for each fuel assembly to be used in subsequent CRC reactivity calculations containing the fuel assemblies.

  15. CRC DEPLETION CALCULATIONS FOR THE NON-RODDED ASSEMBLIES IN BATCHES 4 AND 5 OF CRYSTAL RIVER UNIT 3

    SciTech Connect (OSTI)

    Kenneth D. Wright

    1997-07-30

    The purpose of this design analysis is to document the SAS2H depletion calculations of certain non-rodded fuel assemblies from batches 4 and 5 of the Crystal River Unit 3 pressurized water reactor (PWR) that are required for commercial Reactor Critical (CRC) evaluations to support the development of the disposal criticality methodology. A non-rodded assembly is one which never contains a control rod assembly (CRA) or an axial power shaping rod assembly (APSRA) during its irradiation history. The objective of this analysis is to provide SAS2H generated isotopic compositions for each fuel assembly's depleted fuel and depleted burnable poison materials. These SAS2H generated isotopic compositions are acceptable for use in CRC benchmark reactivity calculations containing the various fuel assemblies.

  16. Coal fly ash interaction with environmental fluids: Geochemical and strontium isotope results from combined column and batch leaching experiments

    SciTech Connect (OSTI)

    Brubaker, Tonya M.; Stewart, Brian W.; Capo, Rosemary C.; Schroeder, Karl T.; Chapman, Elizabeth C.; Spivak-Birndorf, Lev J.; Vesper, Dorothy J.; Cardone, Carol R.; Rohar, Paul C.

    2013-05-01

    The major element and Sr isotope systematics and geochemistry of coal fly ash and its interactions with environmental waters were investigated using laboratory flow-through column leaching experiments (sodium carbonate, acetic acid, nitric acid) and sequential batch leaching experiments (water, acetic acid, hydrochloric acid). Column leaching of Class F fly ash samples shows rapid release of most major elements early in the leaching procedure, suggesting an association of these elements with soluble and surface bound phases. Delayed release of certain elements (e.g., Al, Fe, Si) signals gradual dissolution of more resistant silicate or glass phases as leaching continues. Strontium isotope results from both column and batch leaching experiments show a marked increase in {sup 87}Sr/{sup 86}Sr ratio with continued leaching, yielding a total range of values from 0.7107 to 0.7138. For comparison, the isotopic composition of fluid output from a fly ash impoundment in West Virginia falls in a narrow range around 0.7124. The experimental data suggest the presence of a more resistant, highly radiogenic silicate phase that survives the combustion process and is leached after the more soluble minerals are removed. Strontium isotopic homogenization of minerals in coal does not always occur during the combustion process, despite the high temperatures encountered in the boiler. Early-released Sr tends to be isotopically uniform; thus the Sr isotopic composition of fly ash could be distinguishable from other sources and is a useful tool for quantifying the possible contribution of fly ash leaching to the total dissolved load in natural surface and ground waters.

  17. Development Of A Macro-Batch Qualification Strategy For The Hanford Tank Waste Treatment And Immobilization Plant

    SciTech Connect (OSTI)

    Herman, Connie C.

    2013-09-30

    The Savannah River National Laboratory (SRNL) has evaluated the existing waste feed qualification strategy for the Hanford Tank Waste Treatment and Immobilization Plant (WTP) based on experience from the Savannah River Site (SRS) Defense Waste Processing Facility (DWPF) waste qualification program. The current waste qualification programs for each of the sites are discussed in the report to provide a baseline for comparison. Recommendations on strategies are then provided that could be implemented at Hanford based on the successful Macrobatch qualification strategy utilized at SRS to reduce the risk of processing upsets or the production of a staged waste campaign that does not meet the processing requirements of the WTP. Considerations included the baseline WTP process, as well as options involving Direct High Level Waste (HLW) and Low Activity Waste (LAW) processing, and the potential use of a Tank Waste Characterization and Staging Facility (TWCSF). The main objectives of the Hanford waste feed qualification program are to demonstrate compliance with the Waste Acceptance Criteria (WAC), determine waste processability, and demonstrate unit operations at a laboratory scale. Risks to acceptability and successful implementation of this program, as compared to the DWPF Macro-Batch qualification strategy, include: Limitations of mixing/blending capability of the Hanford Tank Farm; The complexity of unit operations (i.e., multiple chemical and mechanical separations processes) involved in the WTP pretreatment qualification process; The need to account for effects of blending of LAW and HLW streams, as well as a recycle stream, within the PT unit operations; and The reliance on only a single set of unit operations demonstrations with the radioactive qualification sample. This later limitation is further complicated because of the 180-day completion requirement for all of the necessary waste feed qualification steps. The primary recommendations/changes include the following: Collection and characterization of samples for relevant process analytes from the tanks to be blended during the staging process; Initiation of qualification activities earlier in the staging process to optimize the campaign composition through evaluation from both a processing and glass composition perspective; Definition of the parameters that are important for processing in the WTP facilities (unit operations) across the anticipated range of wastes and as they relate to qualification-scale equipment; Performance of limited testing with simulants ahead of the waste feed qualification sample demonstration as needed to determine the available processing window for that campaign; and Demonstration of sufficient mixing in the staging tank to show that the waste qualification sample chemical and physical properties are representative of the transfers to be made to WTP. Potential flowcharts for derivatives of the Hanford waste feed qualification process are also provided in this report. While these recommendations are an extension of the existing WTP waste qualification program, they are more in line with the processes currently performed for SRS. The implementation of these processes at SRS has been shown to offer flexibility for processing, having identified potential processing issues ahead of the qualification or facility processing, and having provided opportunity to optimize waste loading and throughput in the DWPF.

  18. SJSU Information Support Services Run Batch Contracts for Temporary TAs and GAs info-support@sjsu.edu, 408-924-1530 Page 1

    E-Print Network [OSTI]

    Su, Xiao

    -support@sjsu.edu, 408-924-1530 Page 4 The TF Batch Contract page displays. 5. Term: Use the lookup button to search the appropriate term. 6. Due Date: (Optional.) Enter due date. 7. Dean's Name: Enter your Dean's name. 8. Enter letter/Terms and Conditions page. This section demonstrates how to generate and print the teaching

  19. Integration of the Uncertainties of Anion and TOC Measurements into the Flammability Control Strategy for Sludge Batch 8 at the DWPF

    SciTech Connect (OSTI)

    Edwards, T. B.

    2013-03-14

    The Savannah River National Laboratory (SRNL) has been working with the Savannah River Remediation (SRR) Defense Waste Processing Facility (DWPF) in the development and implementation of a flammability control strategy for DWPF’s melter operation during the processing of Sludge Batch 8 (SB8). SRNL’s support has been in response to technical task requests that have been made by SRR’s Waste Solidification Engineering (WSE) organization. The flammability control strategy relies on measurements that are performed on Slurry Mix Evaporator (SME) samples by the DWPF Laboratory. Measurements of nitrate, oxalate, formate, and total organic carbon (TOC) standards generated by the DWPF Laboratory are presented in this report, and an evaluation of the uncertainties of these measurements is provided. The impact of the uncertainties of these measurements on DWPF’s strategy for controlling melter flammability also is evaluated. The strategy includes monitoring each SME batch for its nitrate content and its TOC content relative to the nitrate content and relative to the antifoam additions made during the preparation of the SME batch. A linearized approach for monitoring the relationship between TOC and nitrate is developed, equations are provided that integrate the measurement uncertainties into the flammability control strategy, and sample calculations for these equations are shown to illustrate the impact of the uncertainties on the flammability control strategy.

  20. Batch Strategies for Maximizing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 OutreachProductswsicloudwsiclouddenDVA N C E D B L O OLaura BeaneCardwell,Production1358 ApprovedImportanceBassiu

  1. Batch Strategies for Maximizing

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 OutreachProductswsicloudwsiclouddenDVA N C E D B L O OLaura BeaneCardwell,Production1358 ApprovedImportanceBassiut

  2. Submitting Batch Jobs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservation ofAlbuquerque|SensitiveAprilPhotonStructureStudents

  3. Batch Script Examples

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room News PublicationsAudits & Inspections AuditsBarbara McClintock andBasics

  4. Example Batch Scripts

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HABFES OctoberEvan Racah Evan Racah 1517546Has Evidence Example

  5. Example Batch Scripts

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HABFES OctoberEvan Racah Evan Racah 1517546Has Evidence ExampleExample

  6. Example batch scripts

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HABFES OctoberEvan Racah Evan Racah 1517546Has Evidence ExampleExample

  7. Running Interactive Batch Jobs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservation of Fe(II) byMultidayAlumni > The Energy MaterialsRooftop SolarRoyRun

  8. Parallel Batch Scripts

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformationJesseworkSURVEYI/O Streams forOrhanTheoreticalSecurity Complex3

  9. SLUDGE BATCH 7 ACCEPTANCE EVALUATION: RADIONUCLIDE CONCENTRATIONS IN TANK 51 SB7 QUALIFICATION SAMPLE PREPARED AT SRNL

    SciTech Connect (OSTI)

    Pareizs, J.; Hay, M.

    2011-02-22

    Presented in this report are radionuclide concentrations required as part of the program of qualifying Sludge Batch Seven (SB7) for processing in the Defense Waste Processing Facility (DWPF). The SB7 material is currently in Tank 51 being washed and prepared for transfer to Tank 40. The acceptance evaluation needs to be completed prior to the transfer of the material in Tank 51 to Tank 40. The sludge slurry in Tank 40 has already been qualified for DWPF and is currently being processed as SB6. The radionuclide concentrations were measured or estimated in the Tank 51 SB7 Qualification Sample prepared at Savannah River National Laboratory (SRNL). This sample was prepared from the three liter qualification sample of Tank 51 sludge slurry (HTF-51-10-125) received on September 18, 2010. The sample was delivered to SRNL where it was initially characterized in the Shielded Cells. With consultation from the Liquid Waste Organization, the qualification sample was then modified by several washes and decants, which included addition of Pu from H Canyon and sodium nitrite per the Tank Farm corrosion control program. This final slurry now has a composition expected to be similar to that of the slurry in Tank 51 after final preparations have been made for transfer of that slurry to Tank 40. Determining the radionuclide concentrations in this Tank 51 SB7 Qualification Sample is part of the work requested in Technical Task Request (TTR) No. HLW-DWPF-TTR-2010-0031. The radionuclides included in this report are needed for the DWPF Radiological Program Evaluation, the DWPF Waste Acceptance Criteria (TSR/WAC) Evaluation, and the DWPF Solid Waste Characterization Program (TTR Task I.2). Radionuclides required to meet the Waste Acceptance Product Specifications (TTR Task III.2.) will be measured at a later date after the slurry from Tank 51 has been transferred to Tank 40. Then a sample of the as-processed SB7 will be taken and transferred to SRNL for measurement of these radionuclides. The results presented in this report are those necessary for DWPF to assess if the Tank 51 SB7 sample prepared at SRNL meets the requirements for the DWPF Radiological Program Evaluation, the DWPF Waste Acceptance Criteria evaluation, and the DWPF Solid Waste Characterization Program. Concentrations are given for thirty-four radionuclides along with total alpha and beta activity. Values for total gamma and total gamma plus beta activities are also calculated.

  10. SLUDGE BATCH 7 (SB7) WASHING DEMONSTRATION TO DETERMINE SULFATE/OXALATE REMOVAL EFFICIENCY AND SETTLING BEHAVIOR

    SciTech Connect (OSTI)

    Reboul, S.; Click, D.; Lambert, D.

    2010-12-10

    To support Sludge Batch 7 (SB7) washing, a demonstration of the proposed Tank Farm washing operation was performed utilizing a real-waste test slurry generated from Tank 4, 7, and 12 samples. The purpose of the demonstration was twofold: (1) to determine the settling time requirements and washing strategy needed to bring the SB7 slurry to the desired endpoint; and (2) to determine the impact of washing on the chemical and physical characteristics of the sludge, particularly those of sulfur content, oxalate content, and rheology. Seven wash cycles were conducted over a four month period to reduce the supernatant sodium concentration to approximately one molar. The long washing duration was due to the slow settling of the sludge and the limited compaction. Approximately 90% of the sulfur was removed through washing, and the vast majority of the sulfur was determined to be soluble from the start. In contrast, only about half of the oxalate was removed through washing, as most of the oxalate was initially insoluble and did not partition to the liquid phase until the latter washes. The final sulfur concentration was 0.45 wt% of the total solids, and the final oxalate concentration was 9,900 mg/kg slurry. More oxalate could have been removed through additional washing, although the washing would have reduced the supernatant sodium concentration.The yield stress of the final washed sludge (35 Pa) was an order of magnitude higher than that of the unwashed sludge ({approx}4 Pa) and was deemed potentially problematic. The high yield stress was related to the significant increase in insoluble solids that occurred ({approx}8 wt% to {approx}18 wt%) as soluble solids and water were removed from the slurry. Reduction of the insoluble solids concentration to {approx}14 wt% was needed to reduce the yield stress to an acceptable level. However, depending on the manner that the insoluble solids adjustment was performed, the final sodium concentration and extent of oxalate removal would be prone to change. As such, the strategy for completing the final wash cycle is integral to maintaining the proper balance of chemical and physical requirements.

  11. Summary Report For The Analysis Of The Sludge Batch 7b (Macrobatch 9) DWPF Pour Stream Glass Sample For Canister S04023

    SciTech Connect (OSTI)

    Johnson, F. C.

    2013-11-18

    In order to comply with the Defense Waste Processing Facility (DWPF) Waste Form Compliance Plan for Sluldge Batch 7b, Savannah River National Laboratory (SRNL) personnel characterized the Defense Waste Processing Facility (DWPF) pour stream (PS) glass sample collected while filling canister S04023. This report summarizes the results of the compositional analysis for reportable oxides and radionuclides and the normalized Product Consistency Test (PCT) results. The PCT responses indicate that the DWPF produced glass that is significantly more durable than the Environmental Assessment glass.

  12. Short contact time direct coal liquefaction using a novel batch reactor. Quarterly technical progress report, September 15, 1995--January 15, 1996

    SciTech Connect (OSTI)

    Klein, M.T.; Calkins, W.H.; Huang, He

    1996-01-26

    The objective of this research is to optimize the design and operation of the bench scale batch reactor (SCTBR) f or coal liquefaction at short contact times (0.01 to 10 minutes or longer). Additional objectives are to study the kinetics of direct coal liquefaction particularly at short reaction times, and to investigate the role of the organic oxygen components of coal and their reaction pathways during liquefaction. Many of those objectives have already been achieved and others are still in progress. This quarterly report covers further progress toward those objectives.

  13. ELIMINATION OF THE CHARACTERIZATION OF DWPF POUR STREAM SAMPLE AND THE GLASS FABRICATION AND TESTING OF THE DWPF SLUDGE BATCH QUALIFICATION SAMPLE

    SciTech Connect (OSTI)

    Amoroso, J.; Peeler, D.; Edwards, T.

    2012-05-11

    A recommendation to eliminate all characterization of pour stream glass samples and the glass fabrication and Product Consistency Test (PCT) of the sludge batch qualification sample was made by a Six-Sigma team chartered to eliminate non-value-added activities for the Defense Waste Processing Facility (DWPF) sludge batch qualification program and is documented in the report SS-PIP-2006-00030. That recommendation was supported through a technical data review by the Savannah River National Laboratory (SRNL) and is documented in the memorandums SRNL-PSE-2007-00079 and SRNL-PSE-2007-00080. At the time of writing those memorandums, the DWPF was processing sludge-only waste but, has since transitioned to a coupled operation (sludge and salt). The SRNL was recently tasked to perform a similar data review relevant to coupled operations and re-evaluate the previous recommendations. This report evaluates the validity of eliminating the characterization of pour stream glass samples and the glass fabrication and Product Consistency Test (PCT) of the sludge batch qualification samples based on sludge-only and coupled operations. The pour stream sample has confirmed the DWPF's ability to produce an acceptable waste form from Slurry Mix Evaporator (SME) blending and product composition/durability predictions for the previous sixteen years but, ultimately the pour stream analysis has added minimal value to the DWPF's waste qualification strategy. Similarly, the information gained from the glass fabrication and PCT of the sludge batch qualification sample was determined to add minimal value to the waste qualification strategy since that sample is routinely not representative of the waste composition ultimately processed at the DWPF due to blending and salt processing considerations. Moreover, the qualification process has repeatedly confirmed minimal differences in glass behavior from actual radioactive waste to glasses fabricated from simulants or batch chemicals. In contrast, the variability study has significantly added value to the DWPF's qualification strategy. The variability study has evolved to become the primary aspect of the DWPF's compliance strategy as it has been shown to be versatile and capable of adapting to the DWPF's various and diverse waste streams and blending strategies. The variability study, which aims to ensure durability requirements and the PCT and chemical composition correlations are valid for the compositional region to be processed at the DWPF, must continue to be performed. Due to the importance of the variability study and its place in the DWPF's qualification strategy, it will also be discussed in this report. An analysis of historical data and Production Records indicated that the recommendation of the Six Sigma team to eliminate all characterization of pour stream glass samples and the glass fabrication and PCT performed with the qualification glass does not compromise the DWPF's current compliance plan. Furthermore, the DWPF should continue to produce an acceptable waste form following the remaining elements of the Glass Product Control Program; regardless of a sludge-only or coupled operations strategy. If the DWPF does decide to eliminate the characterization of pour stream samples, pour stream samples should continue to be collected for archival reasons, which would allow testing to be performed should any issues arise or new repository test methods be developed.

  14. Comparison of different liquid anaerobic digestion effluents as inocula and nitrogen sources for solid-state batch anaerobic digestion of corn stover

    SciTech Connect (OSTI)

    Xu Fuqing; Shi Jian; Lv Wen; Yu Zhongtang; Li Yebo

    2013-01-15

    Highlights: Black-Right-Pointing-Pointer Compared methane production of solid AD inoculated with different effluents. Black-Right-Pointing-Pointer Food waste effluent (FWE) had the largest population of acetoclastic methanogens. Black-Right-Pointing-Pointer Solid AD inoculated with FWE produced the highest methane yield at F/E ratio of 4. Black-Right-Pointing-Pointer Dairy waste effluent (DWE) was rich of cellulolytic and xylanolytic bacteria. Black-Right-Pointing-Pointer Solid AD inoculated with DWE produced the highest methane yield at F/E ratio of 2. - Abstract: Effluents from three liquid anaerobic digesters, fed with municipal sewage sludge, food waste, or dairy waste, were evaluated as inocula and nitrogen sources for solid-state batch anaerobic digestion of corn stover in mesophilic reactors. Three feedstock-to-effluent (F/E) ratios (i.e., 2, 4, and 6) were tested for each effluent. At an F/E ratio of 2, the reactor inoculated by dairy waste effluent achieved the highest methane yield of 238.5 L/kgVS{sub feed}, while at an F/E ratio of 4, the reactor inoculated by food waste effluent achieved the highest methane yield of 199.6 L/kgVS{sub feed}. The microbial population and chemical composition of the three effluents were substantially different. Food waste effluent had the largest population of acetoclastic methanogens, while dairy waste effluent had the largest populations of cellulolytic and xylanolytic bacteria. Dairy waste also had the highest C/N ratio of 8.5 and the highest alkalinity of 19.3 g CaCO{sub 3}/kg. The performance of solid-state batch anaerobic digestion reactors was closely related to the microbial status in the liquid anaerobic digestion effluents.

  15. Coupled alkai fieldspar dissolution and secondary mineral precipatation in batch systems-2: New experiments with supercritical CO2 and implications for carbon sequestration

    SciTech Connect (OSTI)

    Lu, Peng; Fu, Qi; Seyfried, William E. Jr.; Hedges, Sheila W. [U.S. DOE; Soong, Yee [U.S. DOE; Jones, Kyle; Zhua, Chen

    2013-01-01

    In order to evaluate the extent of CO{sub 2}–water–rock interactions in geological formations for C sequestration, three batch experiments were conducted on alkali feldspars–CO{sub 2}–brine interactions at 150–200 °C and 300 bars. The elevated temperatures were necessary to accelerate the reactions to facilitate attainable laboratory measurements. Temporal evolution of fluid chemistry was monitored by major element analysis of in situ fluid samples. SEM, TEM and XRD analysis of reaction products showed extensive dissolution features (etch pits, channels, kinks and steps) on feldspars and precipitation of secondary minerals (boehmite, kaolinite, muscovite and paragonite) on feldspar surfaces. Therefore, these experiments have generated both solution chemistry and secondary mineral identity. The experimental results show that partial equilibrium was not attained between secondary minerals and aqueous solutions for the feldspar hydrolysis batch systems. Evidence came from both solution chemistry (supersaturation of the secondary minerals during the entire experimental duration) and metastable co-existence of secondary minerals. The slow precipitation of secondary minerals results in a negative feedback in the dissolution–precipitation loop, reducing the overall feldspar dissolution rates by orders of magnitude. Furthermore, the experimental data indicate the form of rate laws greatly influence the steady state rates under which feldspar dissolution took place. Negligence of both the mitigating effects of secondary mineral precipitation and the sigmoidal shape of rate–?G{sub r} relationship can overestimate the extent of feldspar dissolution during CO{sub 2} storage. Finally, the literature on feldspar dissolution in CO{sub 2}-charged systems has been reviewed. The data available are insufficient and new experiments are urgently needed to establish a database on feldspar dissolution mechanism, rates and rate laws, as well as secondary mineral information at CO{sub 2} storage conditions.

  16. Report for Batch Leach Analyses on Sediments at 100-HR-3 Operable Unit, Boreholes C7620, C7621, C7622, C7623, C7626, C7627, C7628, C7629, C7630, and C7866. Revision 1.

    SciTech Connect (OSTI)

    Lindberg, Michael J.

    2012-04-25

    This is a revision to a previously released report. This revision contains additional analytical results for the sample with HEIS number B2H4X7. Between November 4, 2010 and October 26, 2011 sediment samples were received from 100-HR-3 Operable Unit for geochemical studies. The analyses for this project were performed at the 331 building located in the 300 Area of the Hanford Site. The analyses were performed according to Pacific Northwest National Laboratory (PNNL) approved procedures and/or nationally recognized test procedures. The data sets include the sample identification numbers, analytical results, estimated quantification limits (EQL), and quality control data. The preparatory and analytical quality control requirements, calibration requirements, acceptance criteria, and failure actions are defined in the on-line QA plan 'Conducting Analytical Work in Support of Regulatory Programs' (CAW). This QA plan implements the Hanford Analytical Services Quality Assurance Requirements Documents (HASQARD) for PNNL. Samples were received with a chain of custody (COC) and were analyzed according to the sample identification numbers supplied by the client. All Samples were refrigerated upon receipt until prepared for analysis. All samples were received with custody seals intact unless noted in the Case Narrative. Holding time is defined as the time from sample preparation to the time of analyses. The prescribed holding times were met for all analytes unless noted in the Case Narrative. All reported analytical results meet the requirements of the CAW or client specified SOW unless noted in the case narrative. Due to the requirements of the statement of work and sampling events in the field, the 28 day and the 48 hr requirements cannot be met. The statement of work requires samples to be selected at the completion of the borehole. It is not always possible to complete a borehole and have the samples shipped to the laboratory within the hold time requirements. Duplicate RPD for Uranium 238 (38.9%) was above the acceptance limit (35) in 1E05003-DUP1 for ICPMS-Tc-U-WE The sample result is less than 10 times the detection limits. Duplicate recoveries are not applicable to this analyte. Duplicate RPD for Silver 107 (68.2%) was above the acceptance limit (35) in 2C06004-DUP1 for ICPMS-RCRA-AE The sample result is less than 10 times the detection limits. Duplicate recoveries are not applicable to this analyte. Matrix Spike Recovery for Chromium, Hexavalent (48.8%) was outside acceptance limits (75-125) in 1E23001-MS1 for Hexavalent Chromium/Soil. Potential Matrix interference. Sample results associated with this batch are below the EQL. There should be no impact to the data as reported. Matrix Spike Recovery for Chromium, Hexavalent (50.2%) was outside acceptance limits (75-125) in 2B22010-MS1 for Hexavalent Chromium/Soil. Potential Matrix interference. Sample results associated with this batch are below the EQL. There should be no impact to the data as reported.

  17. DESTRUCTION OF TETRAPHENYLBORATE IN TANK 48H USING WET AIR OXIDATION BATCH BENCH SCALE AUTOCLAVE TESTING WITH ACTUAL RADIOACTIVE TANK 48H WASTE

    SciTech Connect (OSTI)

    Adu-Wusu, K; Paul Burket, P

    2009-03-31

    Wet Air Oxidation (WAO) is one of the two technologies being considered for the destruction of Tetraphenylborate (TPB) in Tank 48H. Batch bench-scale autoclave testing with radioactive (actual) Tank 48H waste is among the tests required in the WAO Technology Maturation Plan. The goal of the autoclave testing is to validate that the simulant being used for extensive WAO vendor testing adequately represents the Tank 48H waste. The test objective was to demonstrate comparable test results when running simulated waste and real waste under similar test conditions. Specifically: (1) Confirm the TPB destruction efficiency and rate (same reaction times) obtained from comparable simulant tests, (2) Determine the destruction efficiency of other organics including biphenyl, (3) Identify and quantify the reaction byproducts, and (4) Determine off-gas composition. Batch bench-scale stirred autoclave tests were conducted with simulated and actual Tank 48H wastes at SRNL. Experimental conditions were chosen based on continuous-flow pilot-scale simulant testing performed at Siemens Water Technologies Corporation (SWT) in Rothschild, Wisconsin. The following items were demonstrated as a result of this testing. (1) Tetraphenylborate was destroyed to below detection limits during the 1-hour reaction time at 280 C. Destruction efficiency of TPB was > 99.997%. (2) Other organics (TPB associated compounds), except biphenyl, were destroyed to below their respective detection limits. Biphenyl was partially destroyed in the process, mainly due to its propensity to reside in the vapor phase during the WAO reaction. Biphenyl is expected to be removed in the gas phase during the actual process, which is a continuous-flow system. (3) Reaction byproducts, remnants of MST, and the PUREX sludge, were characterized in this work. Radioactive species, such as Pu, Sr-90 and Cs-137 were quantified in the filtrate and slurry samples. Notably, Cs-137, boron and potassium were shown as soluble as a result of the WAO reaction. (4) Off-gas composition was measured in the resulting gas phase from the reaction. Benzene and hydrogen were formed during the reaction, but they were reasonably low in the off-gas at 0.096 and 0.0063 vol% respectively. Considering the consistency in replicating similar test results with simulated waste and Tank 48H waste under similar test conditions, the results confirm the validity of the simulant for other WAO test conditions.

  18. Submitting Batch Jobs on Carver

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    mpirun -np 8 .mpiwrapped Such wrapper codes can be similarly prepared in other languages such as C or C++. Actually, the python example above can be considered as one...

  19. Transferring Data from Batch Jobs

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservationBio-Inspired Solar FuelTechnologyTel:FebruaryEIA'sTrainingActivity

  20. Using the PDSF Batch System

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservationBio-Inspired SolarAbout /Two0 -Using supercritical carbon dioxide as a UsingSystem

  1. Supporting Multiple Workloads, Batch Systems,

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorking With Livermore National LabSupplier ToolboxSupport

  2. Report for Batch Leach Analyses on Sediments at 100-FR-3 Operable Unit, Boreholes C7790, C7791, and C7792

    SciTech Connect (OSTI)

    Lindberg, Michael J.

    2011-03-01

    This is a data report for CHPRC for the 100-FR-3 operable unit. Between August 15, 2010 and December 2, 2010 sediment samples were received from the 100-FR-3 Operable Unit for geochemical studies. The analyses for this project were performed at the 325 building located in the 300 Area of the Hanford Site. The analyses were performed according to Pacific Northwest National Laboratory (PNNL) approved procedures and/or nationally recognized test procedures. The data sets include the sample identification numbers, analytical results, estimated quantification limits (EQL), and quality control data. The preparatory and analytical quality control requirements, calibration requirements, acceptance criteria, and failure actions are defined in the on-line QA plan 'Conducting Analytical Work in Support of Regulatory Programs' (CAW). This QA plan implements the Hanford Analytical Services Quality Assurance Requirements Documents (HASQARD) for PNNL.

  3. SLUDGE BATCH 6 PHASE II FLOWSHEET SIMULATIONS

    SciTech Connect (OSTI)

    Koopman, D.; Best, D.

    2010-03-30

    Two Sludge Receipt and Adjustment Tank (SRAT) runs were used to demonstrate that a fairly wide window of acid stoichiometry was available for processing SB6 Phase II flowsheet simulant (Tank 40 simulant) while still meeting the dual goals of acceptable nitrate destruction and controlled hydrogen generation. Phase II was an intermediate flowsheet study for the projected composition of Tank 40 after transfer of SB6/Tank 51 sludge to the heel of SB5. The composition was based on August 2009 projections. A window of about 50% in total acid was found between acceptable nitrite destruction and excessive hydrogen generation.

  4. Batch fabrication of precision miniature permanent magnets

    DOE Patents [OSTI]

    Christenson, Todd R. (Albuquerque, NM); Garino, Terry J. (Albuquerque, NM); Venturini, Eugene L. (Albuquerque, NM)

    2002-01-01

    A new class of processes for fabrication of precision miniature rare earth permanent magnets is disclosed. Such magnets typically have sizes in the range 0.1 to 10 millimeters, and dimensional tolerances as small as one micron. Very large magnetic fields can be produced by such magnets, lending to their potential application in MEMS and related electromechanical applications, and in miniature millimeter-wave vacuum tubes. This abstract contains simplifications, and is supplied only for purposes of searching, not to limit or alter the scope or meaning of any claims herein.

  5. Batch extracting process using magneticparticle held solvents

    DOE Patents [OSTI]

    Nunez, Luis (Elmhurst, IL); Vandergrift, George F. (Bolingbrook, IL)

    1995-01-01

    A process for selectively removing metal values which may include catalytic values from a mixture containing same, wherein a magnetic particle is contacted with a liquid solvent which selectively dissolves the metal values to absorb the liquid solvent onto the magnetic particle. Thereafter the solvent-containing magnetic particles are contacted with a mixture containing the heavy metal values to transfer metal values into the solvent carried by the magnetic particles, and then magnetically separating the magnetic particles. Ion exchange resins may be used for selective solvents.

  6. A batch fabricated biomimetic dry adhesive

    E-Print Network [OSTI]

    Northen, Michael T; Turner, K L

    2005-01-01

    nano-structures as dry adhesives J. Adhesion Sci. Technol.al 2003 Microfabricated adhesive mimicking gecko foot-hairfabricated biomimetic dry adhesive Michael T Northen 1,3 and

  7. A batch fabricated biomimetic dry adhesive

    E-Print Network [OSTI]

    Northen, Michael T; Turner, K L

    2005-01-01

    emerging ?eld of microelectromechanical systems (MEMS) hasproduced. The microelectromechanical systems (MEMS)-based

  8. A batch fabricated biomimetic dry adhesive

    E-Print Network [OSTI]

    Northen, Michael T; Turner, K L

    2005-01-01

    emerging ?eld of microelectromechanical systems (MEMS) hasbeen produced. The microelectromechanical systems (MEMS)-

  9. Atlas Sodium Automated Batch Synthesis System

    E-Print Network [OSTI]

    Subramanian, Venkat

    and a target temperature · Temperature can be controlled by monitoring the hotplate temperature or by monitoring the reaction temperature with the temperature probe *Note that reaction temperatures tend resistant temperature probe, an optional pH probe, and a syringe pump with 2 glass syringes (5mL and 0.5m

  10. ESTIMATING THE ASYMPTOTIC VARIANCE WITH BATCH MEANS

    E-Print Network [OSTI]

    Whitt, Ward

    Research Stanford University Stanford, CA 94305­4022 and Ward Whitt AT&T Bell Laboratories Murray Hill, NJ

  11. ESTIMATING THE ASYMPTOTIC VARIANCE WITH BATCH MEANS

    E-Print Network [OSTI]

    Whitt, Ward

    Research Stanford University Stanford, CA 94305-4022 and Ward Whitt AT&T Bell Laboratories Murray Hill, NJ

  12. Thermal Analysis of Waste Glass Batches: Effect of Batch Makeup on

    Office of Scientific and Technical Information (OSTI)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefieldSulfateSciTechtail.Theory of rare Kaon and Pion decays Citation Details In-Document SearchGas-Evolving

  13. Microsoft PowerPoint - NMMSS Strategy_Analytical Approach for...

    National Nuclear Security Administration (NNSA)

    Unmatched Exports and Domestic Activity Log Unmatched Items to Transit Matching Matrix Transit Matching Matrix Identify Matches using transaction details Batch Action Date...

  14. MULTI-BATCH SELF-ASSEMBLY FOR MICROSYSTEM INTEGRATION

    E-Print Network [OSTI]

    process, surface modification techniques, and electroplating as a post-assembly process, for the purpose, reductive desorption, electroplating, microsystem integration Introduction Recent developments in the area of micro components onto a substrate. In addition, electroplating as a post assembly process is used

  15. Using design of experiments to improve a batch chemical process

    E-Print Network [OSTI]

    Hill, Andrew, S.M. (Andrew James). Massachusetts Institute of Technology

    2010-01-01

    Novartis Vaccines and Diagnostics has made a strong commitment to manufacturing seasonal influenza vaccines through their cell culture technology called Optaflu®. The goal of this project is to improve overall process yield ...

  16. Apparatus and method for batch-wire continuous pumping

    DOE Patents [OSTI]

    Fassbender, Alexander G. (West Richland, WA)

    1996-01-01

    The apparatus of the present invention contains at least one pressure vessel having a separator defining two chambers within each pressure vessel. The separator slideably seals the two chambers. Feedstock is placed within a second chamber adjoining the first chamber via a feedstock pump operating in a high volume low head mode. A pressurizer operates in a low volume high pressure mode to pressurize the working fluid and the feedstock in the pressure vessels to a process operating pressure. A circulating pump operates in a high volume, low head mode to circulate feedstock through the process. A fourth pump is used for moving feedstock and product at a pressure below the process operating pressure.

  17. MEMS design rule checking: a batch approach for remote operation

    SciTech Connect (OSTI)

    Yarberry, V.R.

    1998-01-01

    This paper describes a design rule checking (DRC) tool developed as an aid for designing microelectromechanical structures (MEMS) using AutoCAD running on a Windows NT workstation. The application suite, MEMSdrc, consists of: a graphical user interface integrated into AutoCAD to invoke DRC, translation and interface software to communicate with a commercial IC layout design checking software package, and routines to interactively display and review the results. The user interface provides the capability to select a checking window area and specific DRC rules to be applied to the design. The MEMS structures, defined as 2D AutoCAD geometry are translated first into DXF format, then to GDSII format. A remote process transfers the files to a Unix workstation where Mentor Graphics ICverify is invoked to perform the layout design rule checks. Upon completion, the results are translated into DXF geometry and returned back to the Windows NT workstation to be overlaid onto the original design. A set of icons are provided for the user to interactively review the results inside of AutoCAD using a first/next/previous technique.

  18. Batch extracting process using magnetic particle held solvents

    DOE Patents [OSTI]

    Nunez, L.; Vandergrift, G.F.

    1995-11-21

    A process is described for selectively removing metal values which may include catalytic values from a mixture containing same, wherein a magnetic particle is contacted with a liquid solvent which selectively dissolves the metal values to absorb the liquid solvent onto the magnetic particle. Thereafter the solvent-containing magnetic particles are contacted with a mixture containing the heavy metal values to transfer metal values into the solvent carried by the magnetic particles, and then magnetically separating the magnetic particles. Ion exchange resins may be used for selective solvents. 5 figs.

  19. Simultaneous Batching and Scheduling Using Dynamic Decomposition on a Grid

    E-Print Network [OSTI]

    Mangasarian, Olvi L.

    , in the petroleum sector, scheduling problems arise in the transportation and unloading of crude oil from pipelines, the transfer to storage tanks and the charge for each crude oil distillation unit. In basic chemical

  20. Batch image processing in synaptic membrane biology Donal Stewart1

    E-Print Network [OSTI]

    Millar, Andrew J.

    vesicle recycling function [2, 3]. The goal of this type of imaging is to record the changes. Aggregate assays: Multiple replicates of the same assay are then aggregated to provide mean and standard error ROI intensity pro- files for synapse behaviour. protocol being tested. The aggregated result

  1. List of Accepted Summer Interns (2013) May-June Batch

    E-Print Network [OSTI]

    2013-01-01

    .-K. Chou Narai**** Chin*** (THAILAND) Dr. George T.F. Wong MCB Sand*** Satap****(INDIA) Dr. Cheng** Sah** (INDIA) Dr. Yeng-Long Chen Sanch*** Bis*** (INDIA) Dr. Chia-Fu Chou Sach** Vi*** Mul** (INDIA**** (PHILIPPINES) Dr. Paul E. Verslues HEN** AKR*** DO** (GHANA) KA* SYUA* L** (MALAYSIA) Dr. Pei-Wen Hsiao Mu

  2. Batching Work and Rework Processes with Limited Deterioration of Reworkables

    E-Print Network [OSTI]

    Magdeburg, Universität

    processes belongs to the broad field of reverse logistics which deals with all kinds of reuse processes

  3. Using Sleepers to Manage Batch Access to HPSS

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservationBio-Inspired SolarAbout /Two0 - 19PortalStatusUserUserHomeUsing

  4. Effect of furnace operating conditions on alkali vaporization, batch

    Office of Scientific and Technical Information (OSTI)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefieldSulfate Reducing(Journal Article) | SciTech ConnectExperimentsGAMMA-RAYNp, Pu, and Am):carryover,

  5. Uranium and Strontium Batch Sorption and Diffusion Kinetics into Mesoporous

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorking With WIPPfinalUnexpectedofWyko NT33004. Uranium4.Silica | Stanford

  6. Using The Batch System: Univa Grid Engine (UGE)

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust,Field-effectWorking WithTelecentric viewing system for light collectionEnergy

  7. Controlled Multi-Batch Self-Assembly of Micro Devices Xiaorong Xiong

    E-Print Network [OSTI]

    is prepared with hydrophobic alkanethiol-coated gold binding sites. To perform assembly, a hydrocarbon oil be assembled to a single substrate sequentially. As a post assembly proce- dure, electroplating is incorporated), electroplating of tin and lead alloy, surface energy and surface tension force simulation and binding site de

  8. Iodine Adsorption on Ion-Exchange Resins and Activated Carbons– Batch Testing

    SciTech Connect (OSTI)

    Parker, Kent E.; Golovich, Elizabeth C.; Wellman, Dawn M.

    2014-09-30

    Iodine sorption onto seven resins and six carbon materials was evaluated using water from well 299-W19-36 on the Hanford Site. These materials were tested using a range of solution-to-solid ratios. The test results are as follows: • The efficacy of the resin and granular activated carbon materials was less than predicted based on manufacturers’ performance data. It is hypothesized that this is due to the differences in speciation previously determined for Hanford groundwater. • The sorption of iodine is affected by the iodine species in the source water. Iodine loading on resins using source water ranged from 1.47 to 1.70 µg/g with the corresponding Kd values from 189.9 to 227.0 mL/g. The sorption values when the iodine is converted to iodide ranged from 2.75 to 5.90 µg/g with the corresponding Kd values from 536.3 to 2979.6 mL/g. It is recommended that methods to convert iodine to iodide be investigated in fiscal year (FY) 2015. • The chemicals used to convert iodine to iodate adversely affected the sorption of iodine onto the carbon materials. Using as-received source water, loading and Kd values ranged from 1.47 to 1.70 µg/g and 189.8 to 226.3 mL/g respectively. After treatment, loading and Kd values could not be calculated because there was little change between the initial and final iodine concentration. It is recommended the cause of the decrease in iodine sorption be investigated in FY15. • In direct support of CH2M HILL Plateau Remediation Company, Pacific Northwest National Laboratory has evaluated samples from within the 200W pump and treat bioreactors. As part of this analysis, pictures taken within the bioreactor reveal a precipitate that, based on physical properties and known aqueous chemistry, is hypothesized to be iron pyrite or chalcopyrite, which could affect iodine adsorption. It is recommended these materials be tested at different solution-to-solid ratios in FY15 to determine their effect on iodine sorption.

  9. Power Generation in Fed-Batch Microbial Fuel Cells as a Function

    E-Print Network [OSTI]

    . The performance of conventional anaerobic treatment processes, such as anaerobic digestion, are adversely affected domestic wastewater (4), ocean sediments (10), animal wastes (11), and anaerobic sewage sludge (5, 12

  10. Production of Cellulase on Mixtures of Xylose and Cellulose in a Fed-Batch Process

    E-Print Network [OSTI]

    California at Riverside, University of

    Energy Research Institute, Golden, Colorado 80401 Accepted forpublication May 79, 1989 Cellulase received attention for renewable production of fuels from cellulosics because of the high selectivity for enzyme production, provided the motivation for studying enzyme production on a mixture of xylose

  11. Tank 37H Salt Removal Batch Process and Salt Dissolution Mixing Study

    SciTech Connect (OSTI)

    Kwon, K.C.

    2001-09-18

    Tank 30H is the receipt tank for concentrate from the 3H Evaporator. Tank 30H has had problems, such as cooling coil failure, which limit its ability to receive concentrate from the 3H Evaporator. SRS High Level Waste wishes to use Tank 37H as the receipt tank for the 3H Evaporator concentrate. Prior to using Tank 37H as the 3H Evaporator concentrate receipt tank, HLW must remove 50 inches of salt cake from the tank. They requested SRTC to evaluate various salt removal methods for Tank 37H. These methods include slurry pumps, Flygt mixers, the modified density gradient method, and molecular diffusion.

  12. CONTINUOSLY STIRRED TANK REACTOR PARAMETERS THAT AFFECT SLUDGE BATCH 6 SIMULANT PROPERTIES

    SciTech Connect (OSTI)

    Newell, J.; Lambert, D.; Stone, M.; Fernandez, A.

    2010-05-28

    The High Level Radioactive Waste (HLW) Sludge in Savannah River Site (SRS) waste tanks was produced over a period of over 60 years by neutralizing the acidic waste produced in the F and H Separations Canyons with sodium hydroxide. The HLW slurries have been stored at free hydroxide concentrations above 1 M to minimize the corrosion of the carbon steel waste tanks. Sodium nitrite is periodically added as a corrosion inhibitor. The resulting waste has been subjected to supernate evaporation to minimize the volume of the stored waste. In addition, some of the waste tanks experienced high temperatures so some of the waste has been at elevated temperatures. Because the waste is radioactive, the waste is transforming through the decay of shorter lived radioactive species and the radiation damage that the decay releases. The goal of the Savannah River National Laboratory (SRNL) simulant development program is to develop a method to produce a sludge simulant that matches both the chemical and physical characteristics of the HLW without the time, temperature profile, chemical or radiation exposure of that of the real waste. Several different approaches have been taken historically toward preparing simulated waste slurries. All of the approaches used in the past dozen years involve some precipitation of the species using similar chemistry to that which formed the radioactive waste solids in the tank farm. All of the approaches add certain chemical species as commercially available insoluble solid compounds. The number of species introduced in this manner, however, has varied widely. All of the simulant preparation approaches make the simulated aqueous phase by adding the appropriate ratios of various sodium salts. The simulant preparation sequence generally starts with an acidic pH and ends up with a caustic pH (typically in the 10-12 range). The current method for making sludge simulant involves the use of a temperature controlled continuously stirred tank reactor (CSTR). Precipitated MnO{sub 2} is combined with metal nitrates and fed into the CSTR. The metals are precipitated by a caustic NaOH stream. The rates at which these streams are added allows for pH adjustment of the mixture. A graphical representation of this process is given in Figure 1. In using the CSTR method for developing simulant, there are various parameters that can be adjusted in order to effectuate a physical change in the resulting simulant: pH, temperature, mixing speed, and flow rate. How will changing these parameters affect the physical properties of the sludge simulant? The ability to determine which parameter affects a particular property could allow one to develop a simulant that would better match the physical characteristics of HLW sludge.

  13. XXII ICTAM, 2529 August 2008, Adelaide, Australia THE PREVALENCE OF GHOST RODS IN BATCH MIXER DESIGNS

    E-Print Network [OSTI]

    Balasuriya, Sanjeeva

    . It is well known (see, e.g., [1, 2]) that laminar fluid flows can stir the fluid effectively, provided the stirring that correspondingly takes place in the fluid. It has been recognized that flow structures. INTRODUCTION In this paper we are concerned with the laminar mixing of a viscous fluid in a container

  14. The application of value stream management principles in a batch production environment

    E-Print Network [OSTI]

    Allison, Daniel J

    2004-01-01

    The need for continuous improvement within a value stream is very necessary in today's business environment and can be one of the key sources of competitive advantage. As a company learns and implements the tools and ...

  15. ACooperative MultiAgent System for Plan Generation in Batch Manufacturing

    E-Print Network [OSTI]

    Fu, Yongjian

    blending plan, i.e., the proportion of raw materials used in making the product. Traditionally blending. However, the optimal blending plan for a particular task usually requires the knowledge of raw materials inventory. It takes much time for experts to learn about the huge amount of information about raw materials

  16. A Cooperative Multi-Agent System for Plan Generation in Batch Manufacturing

    E-Print Network [OSTI]

    Fu, Yongjian

    blending plan, i.e., the proportion of raw materials used in making the product. Traditionally blending. However, the optimal blending plan for a particular task usually requires the knowledge of raw materials inventory. It takes much time for experts to learn about the huge amount of information about raw materials

  17. Chemical Reduction of PCE by Zero Valent Iron Colloids Batch and Column Experiments

    E-Print Network [OSTI]

    Cirpka, Olaf Arie

    -Tests: Source Remediation Partners · Undesired side reaction between nZVI and water: anaerobic corrosion Loss also in greater depth and underneath buildings - Applicable to large range of contaminants (chlorinated hydrocarbons, heavy metals, pesticides etc.) NAPASAN-Particle Flakes D50 = 900 nm aS = 1.3 m²/g Thickness ~ 70

  18. LIPID PRODUCTION BY DUNALIELLA SALINA IN BATCH CULTURE: EFFECTS OF NITROGEN LIMITATION AND LIGHT INTENSITY

    SciTech Connect (OSTI)

    Weldy, C.S.; Huesemann, M.

    2007-01-01

    Atmospheric carbon dioxide (CO2) concentrations are increasing and may cause unknown deleterious environmental effects if left unchecked. The Intergovernmental Panel on Climate Change (IPCC) has predicted in its latest report a 2°C to 4°C increase in global temperatures even with the strictest CO2 mitigation practices. Global warming can be attributed in large part to the burning of carbon-based fossil fuels, as the concentration of atmospheric CO2 is directly related to the burning of fossil fuels. Biofuels which do not add CO2 to the atmosphere are presently generated primarily from terrestrial plants, i.e., ethanol from corn grain and biodiesel from soybean oil. The production of biofuels from terrestrial plants is severely limited by the availability of fertile land. Lipid production from microalgae and its corresponding biodiesel production have been studied since the late 1970s but large scale production has remained economically infeasible due to the large costs of sterile growing conditions required for many algal species. This study focuses on the potential of the halophilic microalgae species Dunaliella salina as a source of lipids and subsequent biodiesel production. The lipid production rates under high light and low light as well as nitrogen suffi cient and nitrogen defi cient culture conditions were compared for D. salina cultured in replicate photobioreactors. The results show (a) cellular lipid content ranging from 16 to 44% (wt), (b) a maximum culture lipid concentration of 450mg lipid/L, and (c) a maximum integrated lipid production rate of 46mg lipid/L culture*day. The high amount of lipids produced suggests that D. salina, which can be mass-cultured in non-sterile outdoor ponds, has strong potential to be an economically valuable source for renewable oil and biodiesel production.

  19. Tank 49H salt batch supernate qualification for ARP/MCU

    SciTech Connect (OSTI)

    Nash, C. A.; Peters, T.; Fink, S.; Foster, T.

    2008-08-25

    This report covers the laboratory testing and analyses of Tank 49H Qualification Sample Sets A and C, performed in support of initial radioactive operations of Actinide Removal Process (ARP) and Modular Caustic-Side Solvent Extraction Unit (MCU). Major goals of this work include checking that Tank 49H was well mixed after the last receipt of Tank 23H, characterizing Tank 49H supernate after solids are settled so that its composition can be compared to waste acceptance and hazard criteria, verifying actinide and strontium adsorption with a small scale test using monosodium titanate (MST) and filtration, checking MCU solvent performance when applied to the liquid produced from MST contact, and verifying that in-tank settling after a minimum of 30 days was at least as good or better at reducing solids content after a Tank 49H to Tank 50H transfer occurred than what was observed in less time in the lab. The first four items were covered by Sample Set A. The fifth item was covered by Sample Set C, which had several analyses after compositing as required in the nuclear criticality safety evaluation (NCSE).

  20. Batch Scheduling of Recurrent Applications for Energy Savings on Mobile Phones 

    E-Print Network [OSTI]

    Marina, Mahesh; Calder, Matthew

    Recurrent applications that mostly run in the background are a significant source of power consumption on battery-limited mobile phones. We highlight the pitfalls of scheduling such applications independently without ...

  1. Countercurrent Enzymatic Saccharification of Lignocellulosic Biomass and Improvements Over Batch Operation 

    E-Print Network [OSTI]

    Zentay, Agustin Nicholas

    2014-05-05

    Transportation fuels are the major driver for fossil fuel production, a burden that many countries have tried to ease by blending fossil fuels with biofuel substitutes such as ethanol. Current U.S. ethanol production relies ...

  2. Finding limiting flows of batch extractive distillation with interval Erika R. Fritsa,b*

    E-Print Network [OSTI]

    Csendes, Tibor

    ., Hungary, e-mail: ufo@mail.bme.hu b HAS ­ BUTE Research Group of Technical Chemistry, H-1521 Budapest, P

  3. Decision Making for Batch Manufacturing Sites under Uncertainty Andreas A. Linninger and Aninda Chakraborty

    E-Print Network [OSTI]

    Linninger, Andreas A.

    in the overall plant design. Keywords Robust Policy, Cost Effective Policy, Flexibility Index Introduction Chakraborty Laboratory for Product and Process Design Department of Chemical Engineering, University, amount as well as composition. Pharmaceutical and fine chemical production distinguishes itself also

  4. Batch-microfabricated miniaturized planar arrays of Langmuir probes for reentry plasma diagnostics and nanosatellites

    E-Print Network [OSTI]

    Field, Ella Suzanne

    2011-01-01

    One of the most important technical goals in spacecraft design is maintaining the vehicle's integrity under the extreme conditions encountered during reentry to the Earth's atmosphere. When a hypersonic vehicle travels ...

  5. Elucidating the solid, liquid and gaseous products from batch pyrolysis of cotton-gin trash. 

    E-Print Network [OSTI]

    Aquino, Froilan Ludana

    2009-05-15

    and 30 min settings, however, the HV of char was low and almost similar to the HV of CGT. A maximum gas yield of 40 wt.% was measured at 800°C and 60 min and the highest liquid yield of 30 wt.% was determined at 800°C and 30 min. In the modified pyrolysis...

  6. Asymmetric Batch Incremental View Maintenance Hao He Junyi Xie Jun Yang Hai Yu

    E-Print Network [OSTI]

    Yang, Jun

    because of some index. We ex- ploit such asymmetries using an unconventional strategy that selectively hour," and "re- port total gasoline sales in North Carolina if the oil price has changed by more than

  7. Batch kernel SOM and related Laplacian methods for social network analysis 1

    E-Print Network [OSTI]

    Rossi, Fabrice

    Large graphs are natural mathematical models for describing the structure of the data in a wide variety on the spectral analysis of the graph. The proposed method is used to explore the structure of a medieval social network modeled through a weighted graph that has been directly built from a large corpus of agrarian

  8. Batch Splitting in an Assembly Scheduling Environment Satyaki Ghosh Dastidar Rakesh Nagi1

    E-Print Network [OSTI]

    Nagi, Rakesh

    and the diversity of the product mix has made the production planning and scheduling more complex. In the current and setup costs, and timely delivery. Although there have been advances in production control techniques A classical approach in production planning and scheduling is to derive a Master Production Schedule (MPS

  9. Genetic algorithm based task reordering to improve the performance of batch scheduled massively parallel scientific applications

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Sankaran, Ramanan; Angel, Jordan; Brown, W. Michael

    2015-04-08

    The growth in size of networked high performance computers along with novel accelerator-based node architectures has further emphasized the importance of communication efficiency in high performance computing. The world's largest high performance computers are usually operated as shared user facilities due to the costs of acquisition and operation. Applications are scheduled for execution in a shared environment and are placed on nodes that are not necessarily contiguous on the interconnect. Furthermore, the placement of tasks on the nodes allocated by the scheduler is sub-optimal, leading to performance loss and variability. Here, we investigate the impact of task placement on themore »performance of two massively parallel application codes on the Titan supercomputer, a turbulent combustion flow solver (S3D) and a molecular dynamics code (LAMMPS). Benchmark studies show a significant deviation from ideal weak scaling and variability in performance. The inter-task communication distance was determined to be one of the significant contributors to the performance degradation and variability. A genetic algorithm-based parallel optimization technique was used to optimize the task ordering. This technique provides an improved placement of the tasks on the nodes, taking into account the application's communication topology and the system interconnect topology. As a result, application benchmarks after task reordering through genetic algorithm show a significant improvement in performance and reduction in variability, therefore enabling the applications to achieve better time to solution and scalability on Titan during production.« less

  10. Machine-Generated Algorithms, Proofs and Software for the Batch Verification of Digital Signature Schemes

    E-Print Network [OSTI]

    International Association for Cryptologic Research (IACR)

    , including pseudocode and diagrams. All experiments were also re-run using the RELIC pairing library. We

  11. A mathematical model of batch and continuous microbial cultures exhibiting sequential removal characteristics 

    E-Print Network [OSTI]

    Catchings, Ronald Curtis

    1972-01-01

    in incomplete conbustion of the ketone samples and therefore and inaccurate carbon response. In the latter part of Experiment 3-3, after 300 minutes, the TOC obtained from the gas chromatograph was higher than that obtained from the TCA. This also occurred...

  12. The effect of SO2 on mineral carbonation in batch tests

    SciTech Connect (OSTI)

    Summers, Cathy A.; Dahlin, David C.; Ochs, Thomas L.

    2004-01-01

    CO2 sequestration is a key element of future emission-free fossil-fueled power plants. Other constituents of flue gas must also be captured and rendered innocuous. Contemporary power plants remove SOx from exit gases, but next-generation plants may simultaneously treat CO2, SOx, and other pollutants. Pioneering tests at the U.S. Department of Energy's Albany Research Center investigated the combined treatment of CO2 and SO2 in a mineral-carbonation process. SO2 was removed from the gas stream, and as a small fraction of the total volume of mineralizing gas, it did not inhibit the carbonation reaction. The results indicate that this approach to CO2 sequestration could be used to treat multiple pollutants.

  13. Sorption of four triarylmethane dyes in a sandy soil determined by batch and column experiments

    E-Print Network [OSTI]

    Flury, Markus

    techniques. The four dyes, C.I. Food Blue 2 (Brilliant Blue FCF), C.I. Food Green 3, C.I. Acid Blue 7, and C.I. Acid Green 9, were all from the class of triarylmethnane dyes. Adsorption isotherms were determined than C.I. Acid Green 9 and Acid Blue 7. The former two dyes contain three sulfonic acid groups while

  14. A Wireless Batch Sealed Absolute Capacitive Pressure Sensor Orhan Akar1

    E-Print Network [OSTI]

    Akin, Tayfun

    -etch stop technique. Fabricated devices measure 2.6x1.6 mm 2 in size and houses 24 turns of gold. Furthermore, the sensor can be operated using a passive telemetry approach [4-7], as discussed later. Sensor should be as small as possible, usually in the range of 1-2µm. The capacitor gap should also house

  15. Please use "gres" settings in your batch scripts

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration wouldMass mapSpeeding access| DepartmentPeerFederalPlatinumtake the 2011 user surveyPlease use

  16. MELTING OF GLASS BATCH: MODEL FOR MULTIPLE OVERLAPPING GAS-EVOLVING

    Office of Scientific and Technical Information (OSTI)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefieldSulfate Reducing(Journalspectroscopy ofArticle) |management (Patent)SciTechSciTech ConnectREACTIONS

  17. Mendel at NERSC - Supporting Multiple Workloads, Batch Systems, and Compute Environments on a Single Linux Cluster

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration wouldMass map shines light on dark matter By SarahMODELINGMeetingsMembranesMemorial DayCUG 2013

  18. Three-Dimensional Flow and Thermal Structure in Glass Melting Furnaces. Part II: Effect of Batch and Bubbles

    E-Print Network [OSTI]

    Pilon, Laurent; Zhao, Guochang; Viskanta, Raymond

    2002-01-01

    properties of soda-lime solicate glass of composition 74 SiOwas retained for ?H melt for soda-lime silicate glass having

  19. Optimal synthesis for the minimum time control problems of fed-batch bioprocesses for growth functions with two maxima

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    volume (representing a completely full tank). The optimal synthesis for this problem has been obtained) Departamento de Matem´atica, Universidad T´ecnica Federico Santa Mar´ia, Avenida Espa~na 1680, Valpara´iso´ia, Avenida Espa~na 1680, Valpara´iso, Chile (fran- cis.mairet@usm.cl) 1 hal-00655534,version3-2Apr2012 #12

  20. Optimal synthesis for the minimum time control problems of fed-batch bioprocesses for growth functions with two maxima

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    volume (representing a completely full tank). The optimal synthesis for this problem has been obtained) Departamento de Matem´atica, Universidad T´ecnica Federico Santa Mar´ia, Avenida Espa~na 1680, Valpara´iso´ia, Avenida Espa~na 1680, Valpara´iso, Chile (fran- cis.mairet@usm.cl) 1 hal-00655534,version2-31Dec2011 #12

  1. Analysis of the performance and criteria for rational design of a sequencing batch reactor for xenobiotic removal

    E-Print Network [OSTI]

    Daugulis, Andrew J.

    Portillo 21, 00128 Rome, Italy c Water Research Institute, C.N.R., Via Salaria km 29.300, 00015 Modeling Xenobiotics Bioremediation a b s t r a c t Substrate toxicity can impose operability challenges [4­6]. In bioremediation processes, substrate inhibition is a common feature, and in such cases

  2. Transformation of Ferulic Acid to Vanillin Using a Fed-Batch SolidLiquid Two-Phase Partitioning Bioreactor

    E-Print Network [OSTI]

    Daugulis, Andrew J.

    stage extraction into methanol or other organic solvents used in food industry, simultaneously of the most widely used flavor chemicals in the food, cosmetics, and pharmaceutical industries

  3. A Fast Batched Cholesky Factorization on a GPU Tingxing Dong, Azzam Haidar, Stanimire Tomov, and Jack Dongarra

    E-Print Network [OSTI]

    Dongarra, Jack

    the double precision as an example to describe how we implemented, though other precisions, including single, single complex and double complex are also implemented. A. Non-blocked Cholesky factorization 2.5 BLAS. Note that caching is possible because of the small panel sizes. The performance

  4. Fixed bed gasification studies on coal-feedlot biomass and coal-chicken litter biomass under batch mode operation 

    E-Print Network [OSTI]

    Priyadarsan, Soyuz

    2002-01-01

    &M University Boiler Burner Laboratory, and was fired with a) coal, b) feedlot biomass (FB), c) chicken litter biomass (LB), d) high ash feedlot biomass (HFB), e) coal: FB blend (CFB), f) coal: LB blend (CLB), g) coal: HFB blend (CHFB), and h) LB: HFB blend...

  5. Using batch experiments to quantify the potential of North Sea saline aquifers to leach contaminants upon injection of CO2

    E-Print Network [OSTI]

    contaminants upon injection of CO2 Kit Carruthers MSc, Dr. Mark Wilkinson, Dr. Katriona Edlmann · Saline aquifer CO2 storage limited by water and pore compressibilities · Pressure relief via water production · CO2 acidifies water upon dissolution, promoting leaching of heavy metals into solution

  6. Bearing Analytics

    Broader source: Energy.gov [DOE]

    Bearing Analytics is a leading-edge equipment monitoring company aimed at pioneering a new era in industrial bearing condition monitoring. Our objective is to consolidate the needs of customers, environment, and manufacturers to improve asset management and energy efficiency capabilities one bearing at a time.

  7. THE ROLE OF ARCHAEAL METHANOGENS IN BIOMINERALIZATION AND METAL CYCLING: FROM THE MICROSCOPIC TO THE GLOBAL SCALE

    E-Print Network [OSTI]

    Kenward, Paul Alexander

    2010-12-16

    ........................................................................................................................................47 Batch reactors ..................................................................................................................47 Mineralogy and imaging....................................................................... .................................................................102 Batch Reactors................................................................................................................102 Geochemical analysis...

  8. Data Analytics

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home Room NewsInformation Current HAB Packet HanfordDOEDaniel Shechtman andDark FiberAnalytics Data

  9. Storm Water Analytical Period

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Individual Permit Storm Water Analytical Period Storm Water Analytical Period The Individual Permit authorizes the discharge of storm water associated with historical industrial...

  10. Stable Isotope Characterization of TICs/TIMs: Analytical Progress Report

    SciTech Connect (OSTI)

    Volpe, A M; Singleton, M J

    2009-06-05

    We measured twelve alkali cyanide samples that were also sent to ORNL and PNNL collaborators. While results indicate distinct {delta}{sup 13}C and {delta}{sup 15}N values that would be useful to signature studies, the alkali cyanides, especially NaCN, show chemical breakdown during storage that will influence forensic analysis. Carbon and nitrogen stable isotopic compositions of raw materials used to synthesis TETS were measured. Results indicate wide ranges in {delta}{sup 13}C and {delta}{sup 15}N values. Using these raw materials, LLNL scientists synthesized three batches of TETS following published procedures. Stable isotopic measurements of TETS synthesis products indicates nitrogen ({var_epsilon} {sup 15}N = -1.7 to -0.8) and carbon ({var_epsilon} {sup 13}C = -1.0 to -0.1) fractionation during production.

  11. Analyte separation utilizing temperature programmed desorption of a preconcentrator mesh

    DOE Patents [OSTI]

    Linker, Kevin L. (Albuquerque, NM); Bouchier, Frank A. (Albuquerque, NM); Theisen, Lisa (Albuquerque, NM); Arakaki, Lester H. (Edgewood, NM)

    2007-11-27

    A method and system for controllably releasing contaminants from a contaminated porous metallic mesh by thermally desorbing and releasing a selected subset of contaminants from a contaminated mesh by rapidly raising the mesh to a pre-determined temperature step or plateau that has been chosen beforehand to preferentially desorb a particular chemical specie of interest, but not others. By providing a sufficiently long delay or dwell period in-between heating pulses, and by selecting the optimum plateau temperatures, then different contaminant species can be controllably released in well-defined batches at different times to a chemical detector in gaseous communication with the mesh. For some detectors, such as an Ion Mobility Spectrometer (IMS), separating different species in time before they enter the IMS allows the detector to have an enhanced selectivity.

  12. (0.2 and 0.02 wt%, respectively) onto glass in a batch reactor reveals Ni peaks at their appropriate binding

    E-Print Network [OSTI]

    Long, Bernard

    matter (OM) is not clear. We assessed the effect of in situ exposure time to oxic conditions between alkyl carbon present in protein and nonprotein structures. There is an inverse relation between penetration into pore waters divided by sediment accumulation rate (3). Such an "oxygen effect" is explained

  13. Conveying Cycle-Time Analysis in Pneumatic Conveying: A Study of Relationship between Batching & Convey Cycles in Powder & Bulk Handling Systems

    E-Print Network [OSTI]

    Aghdaie, Bahman

    2008-12-19

    The purpose of this project is to develop methods for calculating the instantaneous convey rates for pneumatic conveying systems. Process and systems engineers are often faced with the question of calculating or verifying the required conveying...

  14. Comparison of microwaves to fluidized sand baths for heating tubular reactors for hydrothermal and dilute acid batch pretreatment of corn stover

    E-Print Network [OSTI]

    California at Riverside, University of

    heated pretreatment led to faster xylan, lignin, and acetyl removal as well as ear- lier xylan technology was developed in 1940's driven by military needs and was later intro- duced into civilian markets

  15. [clc] Kinetic and stoichiometric characterization of organoautotrophic growth of Ralstonia eutropha on formic acid in fed-batch and continuous cultures

    E-Print Network [OSTI]

    Grunwald, Stephan

    Formic acid, acting as both carbon and energy source, is a safe alternative to a carbon dioxide, hydrogen and dioxygen mix for studying the conversion of carbon through the Calvin–Benson–Bassham (CBB) cycle into value-added ...

  16. Extraction of uranium(VI) by N,N-di-(2-ethylhexyl)isobutyramide (DEHIBA): from the batch experimental data to the countercurrent process

    SciTech Connect (OSTI)

    Miguirditchian, M.; Sorel, C.; Cames, B.; Bisel, I.; Baron, P.

    2008-07-01

    The selective separation of uranium(VI) in the first cycle of the GANEX process is operated by a hydrometallurgical process using a monoamide extractant DEHiBA (N,N-di-(2-ethylhexyl)isobutyramide). Distribution ratios of uranium(VI) and nitric acid in 1 M DEHiBA/HTP were determined with macro-concentrations of uranium, and the experimental data were modelled by taking into account the activity coefficients of the constituents in aqueous phases. A flowsheet was designed and tested in a countercurrent process in laboratory-scale mixer-settlers on a surrogate U(VI)/HNO 3 feed. More than 99.999% of the uranium was recovered. (authors)

  17. R E S E A R C H A R T I C L E Batch and continuous culture-based selection strategiesforacetic

    E-Print Network [OSTI]

    Wagner, Andreas

    . Abstract Acetic acid tolerance of Saccharomyces cerevisiae is crucial for the production of bioethanol

  18. Batch and Flow Photochemical Benzannulations Based on the Reaction of Ynamides and Diazo Ketones. Application to the Synthesis of Polycyclic Aromatic and Heteroaromatic Compounds

    E-Print Network [OSTI]

    Willumstad, Thomas P.

    Highly substituted polycyclic aromatic and heteroaromatic compounds are produced via a two-stage tandem benzannulation/cyclization strategy. The initial benzannulation step proceeds via a pericyclic cascade mechanism ...

  19. [1] M. Litzkow, M. Livny, "Experience With the Condor Distributed Batch System," Proc. of the IEEE Workshop on Experimental Distributed Systems, Huntsville, Al., October 1990.

    E-Print Network [OSTI]

    McKeown, Nick

    for Computing Machinery. [11] Y. Artsy, R. Finkel, "Designing a process migration facility: the Charlotte. Ousterhout, "Transparent process migration: Design alternatives and the Sprite implementation," Software System Principles, pages 5­12, Austin, Tx., November 1987. The Association for Computing Machinery. [6] R

  20. ResourceSharing Models with StateDependent Arrivals of Batches Gagan L. Choudhury, 1 Kin K. Leung 2 and Ward Whitt 3

    E-Print Network [OSTI]

    Whitt, Ward

    . Leung 2 and Ward Whitt 3 AT&T Bell Laboratories October 7, 1994 ________________ 1 AT&T Bell, Murray Hill, NJ 07974­0636; email: wow@research.att.com #12; Abstract We recently developed a new

  1. Analytical mass spectrometry. Abstracts

    SciTech Connect (OSTI)

    Not Available

    1990-12-31

    This 43rd Annual Summer Symposium on Analytical Chemistry was held July 24--27, 1990 at Oak Ridge, TN and contained sessions on the following topics: Fundamentals of Analytical Mass Spectrometry (MS), MS in the National Laboratories, Lasers and Fourier Transform Methods, Future of MS, New Ionization and LC/MS Methods, and an extra session. (WET)

  2. Analytical mass spectrometry

    SciTech Connect (OSTI)

    Not Available

    1990-01-01

    This 43rd Annual Summer Symposium on Analytical Chemistry was held July 24--27, 1990 at Oak Ridge, TN and contained sessions on the following topics: Fundamentals of Analytical Mass Spectrometry (MS), MS in the National Laboratories, Lasers and Fourier Transform Methods, Future of MS, New Ionization and LC/MS Methods, and an extra session. (WET)

  3. Analytical Chemistry Applied Mathematics

    E-Print Network [OSTI]

    Heller, Barbara

    Architecture Information Technology & Management Integrated Building Delivery Landscape Architecture ManagementAnalytical Chemistry Applied Mathematics Architectural Engineering Architecture Architecture Electricity Markets Environmental Engineering Food Process Engineering Food Safety & Technology

  4. Web Analytics and Statistics

    Office of Energy Efficiency and Renewable Energy (EERE)

    EERE uses Google Analytics to capture statistics on its websites. These statistics help website managers measure and report on users, sessions, most visited pages, and more. The Web Template...

  5. Analysis And Analyticity

    E-Print Network [OSTI]

    Schick, Theodore W. Jr.

    229 ANALYSIS AND ANALYTICITY THEODORE W. SCHICK, JR. In this paper, I attempt to solve the paradox of analysis by eliminating certain ambiguities that have have plagued theories of property-identity and proposition-identity. The paradox...229 ANALYSIS AND ANALYTICITY THEODORE W. SCHICK, JR. In this paper, I attempt to solve the paradox of analysis by eliminating certain ambiguities that have have plagued theories of property-identity and proposition-identity. The paradox...

  6. An Analytic Holographic Superconductor

    E-Print Network [OSTI]

    Christopher P. Herzog

    2011-01-16

    We investigate a holographic superconductor that admits an analytic treatment near the phase transition. In the dual 3+1 dimensional field theory, the phase transition occurs when a scalar operator of scaling dimension two gets a vacuum expectation value. We calculate current-current correlation functions along with the speed of second sound near the critical temperature. We also make some remarks about critical exponents. An analytic treatment is possible because an underlying Heun equation describing the zero mode of the phase transition has a polynomial solution. Amusingly, the treatment here may generalize for an order parameter with any integer spin, and we propose a Lagrangian for a spin two holographic superconductor.

  7. Fields with analytic structure

    E-Print Network [OSTI]

    2011-05-06

    analytic functions” are the strictly convergent power series over A (i.e. the elements of ... standard models of the theory of Qp in the language with symbols for the .... We call the family B a real Weierstrass system if the following conditions

  8. Industrial Analytics Corporation

    SciTech Connect (OSTI)

    Industrial Analytics Corporation

    2004-01-30

    The lost foam casting process is sensitive to the properties of the EPS patterns used for the casting operation. In this project Industrial Analytics Corporation (IAC) has developed a new low voltage x-ray instrument for x-ray radiography of very low mass EPS patterns. IAC has also developed a transmitted visible light method for characterizing the properties of EPS patterns. The systems developed are also applicable to other low density materials including graphite foams.

  9. Analytic Feminism: A Brief Introduction

    E-Print Network [OSTI]

    Cudd, Ann E.

    1995-01-01

    This essay introduces the subject of this special issue by offering a characterization of analytic feminism in terms of its context, methods, and problem areas. I argue that analytic feminism is a legitimate sub-field both of feminism...

  10. STRICTLY CONVERGENT ANALYTIC STRUCTURES 1 ...

    E-Print Network [OSTI]

    2015-02-03

    STRICTLY CONVERGENT ANALYTIC STRUCTURES. RAF CLUCKERS1 AND LEONARD LIPSHITZ2. Abstract. We give conclusive answers to some questions

  11. The Analytical Sciences Digital Library (ASDL)

    E-Print Network [OSTI]

    Larive, Cynthia K.

    2009-01-01

    Analytical Sciences Digital Library (http://www.asdlib.org).Analytical Sciences Digital Library (ASDL) Cynthia K. LariveAnalytical Sciences Digital Library (ASDL) is a collection

  12. Laser ablation in analytical chemistry - A review

    E-Print Network [OSTI]

    Russo, Richard E.; Mao, Xianglei; Liu, Haichen; Gonzalez, Jhanis; Mao, Samuel S.

    2001-01-01

    Encyclopedia of Analytical Chemistry, John Wiley & Sons,applications in analytical chemistry. Matrix independentLaser Ablation in Analytical Chemistry - A Review Richard E.

  13. The Analytical Sciences Digital Library (ASDL)

    E-Print Network [OSTI]

    Larive, Cynthia K.

    2009-01-01

    sciences include analytical chemistry, and other disciplinesis Professor of Analytical Chemistry at the University ofregistered users are analytical chemistry faculty members at

  14. Analytical laboratory quality audits

    SciTech Connect (OSTI)

    Kelley, William D.

    2001-06-11

    Analytical Laboratory Quality Audits are designed to improve laboratory performance. The success of the audit, as for many activities, is based on adequate preparation, precise performance, well documented and insightful reporting, and productive follow-up. Adequate preparation starts with definition of the purpose, scope, and authority for the audit and the primary standards against which the laboratory quality program will be tested. The scope and technical processes involved lead to determining the needed audit team resources. Contact is made with the auditee and a formal audit plan is developed, approved and sent to the auditee laboratory management. Review of the auditee's quality manual, key procedures and historical information during preparation leads to better checklist development and more efficient and effective use of the limited time for data gathering during the audit itself. The audit begins with the opening meeting that sets the stage for the interactions between the audit team and the laboratory staff. Arrangements are worked out for the necessary interviews and examination of processes and records. The information developed during the audit is recorded on the checklists. Laboratory management is kept informed of issues during the audit so there are no surprises at the closing meeting. The audit report documents whether the management control systems are effective. In addition to findings of nonconformance, positive reinforcement of exemplary practices provides balance and fairness. Audit closure begins with receipt and evaluation of proposed corrective actions from the nonconformances identified in the audit report. After corrective actions are accepted, their implementation is verified. Upon closure of the corrective actions, the audit is officially closed.

  15. Data Mining and Business Analytics

    E-Print Network [OSTI]

    Data Mining and Business Analytics CertifiCate Programs spears school of business oklahoma state university #12;e ach year, students enrolled in the OSU Graduate Certificate in Business Data Mining program compete in a national data mining shootout competition at the annual analytics (data mining) conference

  16. ANALYTIC COMPLETION (DRAFT) CHARLES REZK

    E-Print Network [OSTI]

    Rezk, Charles

    ANALYTIC COMPLETION (DRAFT) CHARLES REZK Abstract. This is an expository treatment of what we call "analytic completion" of R- modules, which is a kind of completion defined in terms of quotients of power series modules. It is closely related to the left derived functors of adic completion, in which guise

  17. Biological Upgrading of Sugars Presentation for BETO 2015 Project...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Hyd.- Fermentor Glucose utilization (total) 98% 80% 100% Lipid content 59% 60% 57% Volumetric productivity (gL-hr) at 72 h 0.05 (batch culture) 0.18 (batch culture) 0.29 (batch...

  18. Functionalized magnetic nanoparticle analyte sensor

    SciTech Connect (OSTI)

    Yantasee, Wassana; Warner, Maryin G; Warner, Cynthia L; Addleman, Raymond S; Fryxell, Glen E; Timchalk, Charles; Toloczko, Mychailo B

    2014-03-25

    A method and system for simply and efficiently determining quantities of a preselected material in a particular solution by the placement of at least one superparamagnetic nanoparticle having a specified functionalized organic material connected thereto into a particular sample solution, wherein preselected analytes attach to the functionalized organic groups, these superparamagnetic nanoparticles are then collected at a collection site and analyzed for the presence of a particular analyte.

  19. This

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Batches designed to simulate nuclear high-level waste glass were compressed into pellets that were heated at 5 Kmin and photographed. Three types of batches were prepared,...

  20. Design of hot extrusion molding device for the continuous production of pharmaceutical tablets

    E-Print Network [OSTI]

    Zampierollo, Giorgio (Giorgio Romano)

    2010-01-01

    Currently, pharmaceutical tablets are manufactured in large batch operations that have inefficiencies associated with the stopping, re-configuration and testing between batches. Continuous manufacturing has the potential ...

  1. Analytical Chemistry Laboratory | Argonne National Laboratory

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Chemistry Laboratory provides a broad range of analytical chemistry support services to the scientific and engineering programs. AnalyticalChemistryLaboratoryfactsheet...

  2. Visualization and Analytics Software at NERSC

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Analytics Data, Visualization, and Analytics AVSExpress AVSExpress includes functionality for data visualization and analysis, image processing and data display. It uses a...

  3. Hydrogen Fuel Quality - Focus: Analytical Methods Development...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    Fuel Quality - Focus: Analytical Methods Development & Hydrogen Fuel Quality Results Hydrogen Fuel Quality - Focus: Analytical Methods Development & Hydrogen Fuel Quality Results...

  4. [Task 1.] Biodenitrification of low nitrate solar pond waters using sequencing batch reactors. [Task 2.] Solidification/stabilization of high strength and biodenitrified heavy metal sludges with a Portland cement/flyash system

    SciTech Connect (OSTI)

    Figueroa, L.; Cook, N.E.; Siegrist, R.L.; Mosher, J.; Terry, S.; Canonico, S.

    1995-09-22

    Process wastewater and sludges were accumulated on site in solar evaporation ponds during operations at the Department of Energy's Rocky Flats Plant (DOE/RF). Because of the extensive use of nitric acid in the processing of actinide metals, the process wastewater has high concentrations of nitrate. Solar pond waters at DOE/RF contain 300-60,000 mg NO{sub 3}{sup {minus}}/L. Additionally, the pond waters contain varying concentrations of many other aqueous constituents, including heavy metals, alkali salts, carbonates, and low level radioactivity. Solids, both from chemical precipitation and soil material deposition, are also present. Options for ultimate disposal of the pond waters are currently being evaluated and include stabilization and solidification (S/S) by cementation. Removal of nitrates can enhance a wastes amenability to S/S, or can be a unit operation in another treatment scheme. Nitrate removal is also a concern for other sources of pollution at DOE/RF, including contaminated groundwater collected by interceptor trench systems. Finally, nitrate pollution is a problem at many other DOE facilities where actinide metals were processed. The primary objective of this investigation was to optimize biological denitrification of solar pond waters with nitrate concentrations of 300--2,100 mg NO{sub 3}{sup {minus}}/L to below the drinking water standard of 45 mg NO{sub 3}{sup {minus}}/L (10 mg N/L). The effect of pH upon process stability and denitrification rate was determined. In addition, the effect Cr(VI) on denitrification and fate of Cr(VI) in the presence of denitrifying bacteria was evaluated.

  5. Paper to be presented at AutMoNet 2007 IWA Conference, Gent (B), 5 7 Sept. 2007. Intelligent monitoring system for long-term control of Sequencing Batch

    E-Print Network [OSTI]

    (SBR) treating nitrogen-rich wastewater (sanitary landfill leachate). The paper describes) as indirect process indicators (see e.g. Pavseli et al., 2001; Spagni et al., 2001). Leachate generated in old length and COD addition in SBRs treating sanitary landfill leachate. This research is the result

  6. Analytic equivalence of geometric transitions

    E-Print Network [OSTI]

    Michele Rossi

    2014-08-28

    In this paper \\emph{analytic equivalence} of geometric transition is defined in such a way that equivalence classes of geometric transitions turn out to be the \\emph{arrows} of the \\cy web. Then it seems natural and useful, both from the mathematical and physical point of view, look for privileged arrows' representatives, called \\emph{canonical models}, laying the foundations of an \\emph{analytic} classification of geometric transitions. At this purpose a numerical invariant, called \\emph{bi--degree}, summarizing the topological, geometric and physical changing properties of a geometric transition, is defined for a large class of geometric transitions.

  7. Search & Analytics in Web Archives

    E-Print Network [OSTI]

    Waldmann, Uwe

    Search & Analytics in Web Archives Klaus Berberich References [1] S. Bedathur, K. Berberich, J, ECIR 2010 [3] K. Berberich: " Temporal Search in Web Archives, PhD Thesis, Saarland University, 2010 been identified. Motivation & Overview Web archives such as the Internet Archive or newspaper archives

  8. Analytical Plan for Roman Glasses

    SciTech Connect (OSTI)

    Strachan, Denis M.; Buck, Edgar C.; Mueller, Karl T.; Schwantes, Jon M.; Olszta, Matthew J.; Thevuthasan, Suntharampillai; Heeren, Ronald M.

    2011-01-01

    Roman glasses that have been in the sea or underground for about 1800 years can serve as the independent “experiment” that is needed for validation of codes and models that are used in performance assessment. Two sets of Roman-era glasses have been obtained for this purpose. One set comes from the sunken vessel the Iulia Felix; the second from recently excavated glasses from a Roman villa in Aquileia, Italy. The specimens contain glass artifacts and attached sediment or soil. In the case of the Iulia Felix glasses quite a lot of analytical work has been completed at the University of Padova, but from an archaeological perspective. The glasses from Aquileia have not been so carefully analyzed, but they are similar to other Roman glasses. Both glass and sediment or soil need to be analyzed and are the subject of this analytical plan. The glasses need to be analyzed with the goal of validating the model used to describe glass dissolution. The sediment and soil need to be analyzed to determine the profile of elements released from the glass. This latter need represents a significant analytical challenge because of the trace quantities that need to be analyzed. Both pieces of information will yield important information useful in the validation of the glass dissolution model and the chemical transport code(s) used to determine the migration of elements once released from the glass. In this plan, we outline the analytical techniques that should be useful in obtaining the needed information and suggest a useful starting point for this analytical effort.

  9. Analyte detection using an active assay

    DOE Patents [OSTI]

    Morozov, Victor (Manassas, VA); Bailey, Charles L. (Cross Junction, VA); Evanskey, Melissa R. (Potomac Falls, VA)

    2010-11-02

    Analytes using an active assay may be detected by introducing an analyte solution containing a plurality of analytes to a lacquered membrane. The lacquered membrane may be a membrane having at least one surface treated with a layer of polymers. The lacquered membrane may be semi-permeable to nonanalytes. The layer of polymers may include cross-linked polymers. A plurality of probe molecules may be arrayed and immobilized on the lacquered membrane. An external force may be applied to the analyte solution to move the analytes towards the lacquered membrane. Movement may cause some or all of the analytes to bind to the lacquered membrane. In cases where probe molecules are presented, some or all of the analytes may bind to probe molecules. The direction of the external force may be reversed to remove unbound or weakly bound analytes. Bound analytes may be detected using known detection types.

  10. Analytic bounds on transmission probabilities

    E-Print Network [OSTI]

    Boonserm, Petarpa

    2009-01-01

    We develop some new analytic bounds on transmission probabilities (and the related reflection probabilities and Bogoliubov coefficients) for generic one-dimensional scattering problems. To do so we rewrite the Schrodinger equation for some complicated potential whose properties we are trying to investigate in terms of some simpler potential whose properties are assumed known, plus a (possibly large) "shift" in the potential. Doing so permits us to extract considerable useful information without having to exactly solve the full scattering problem.

  11. BIOCHEMISTRY Analytical Biochemistry 361 (2007) 287293

    E-Print Network [OSTI]

    2007-01-01

    ANALYTICAL BIOCHEMISTRY Analytical Biochemistry 361 (2007) 287­293 www- engineering yet there is a relative paucity of assays available for simple, stable and reproducible applica- tions in membrane biochemistry, transfection, and immuni- zation protocols

  12. Arguments for an Alternative Account of Analyticity

    E-Print Network [OSTI]

    Sexton, Clark Alan

    2009-11-09

    This dissertation presents an alternative account of analyticity, as well as arguments for that account. Although an analysis and interpretation of previous accounts of analyticity are presented, the focus is on the analysis of, and the arguments...

  13. The Analytical Sciences Digital Library (ASDL)

    E-Print Network [OSTI]

    Larive, Cynthia K.

    2009-01-01

    computations, electrochemistry, instrumen- tation, massand “Analytical electrochemistry: a laboratory manual” [14].T (2008) Analyical electrochemistry: a laboratory manual,

  14. Optimal Demand Bidding for Time-Shiftable Loads Hamed Mohsenian-Rad, Senior Member, IEEE

    E-Print Network [OSTI]

    Mohsenian-Rad, Hamed

    ], [6], intelligent pools [7], irrigation pumps [8], water heaters [9], batch processes in data centers

  15. SUSS PM 5 Analytic Probe

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power AdministrationRobust, High-Throughput Analysis of Protein1-0845*RV6STATDecember 2, 2014 Jose,SUSS PM 5 Analytic

  16. Renewable Analytics | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION JEnvironmental Jump to:EA EIS Report UrlNM-b <Refurbished ProjectsInformationEnergyAnalytics

  17. Appendix C Analytical Chemistry Data

    Office of Legacy Management (LM)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield Municipal Gas &SCE-SessionsSouthReport for the WeldonB10081278MaywoodWayne Analytical Chemistry

  18. Analytical Modeling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION J APPENDIX ECoop IncIowaWisconsin: EnergyYork Jump to:HempsteadtemporalAnalytical Modeling Jump to:

  19. Analytical Tools | Department of Energy

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on Delicious Rank EERE: Alternative Fuels DataEnergy Webinar:I Due Date Adv.Alison MarkovitzAmped Up!Analytical Tools

  20. Big Data Analytics in Financial Statement

    E-Print Network [OSTI]

    ;Demographic and Weather Big Data · OfficeMax personalizes online landing pages based on customerBig Data Analytics in Financial Statement Audits Min Cao Roman Chychyla Trevor Stewart February 26th, 2015 #12;Big Data Analytics · Big Data analytics is the process of inspecting, cleaning

  1. A BRIEF HISTORY THE ANALYTICAL CHEMISTRY DIVISION

    E-Print Network [OSTI]

    #12;#12;A BRIEF HISTORY THE ANALYTICAL CHEMISTRY DIVISION OF OAK RIDGE NATIONAL LABORATORY 1950 hiembers of the Chemistry Division R-on: J. A. Swartout In ra: Transfer of Personnel to Analytical Analytical Chemistry Division under Dr. M. T. Kelley, effective immediately; C. L. Burros and Group L. T

  2. Analytical applications for delayed neutrons

    SciTech Connect (OSTI)

    Eccleston, G.W.

    1983-01-01

    Analytical formulations that describe the time dependence of neutron populations in nuclear materials contain delayed-neutron dependent terms. These terms are important because the delayed neutrons, even though their yields in fission are small, permit control of the fission chain reaction process. Analytical applications that use delayed neutrons range from simple problems that can be solved with the point reactor kinetics equations to complex problems that can only be solved with large codes that couple fluid calculations with the neutron dynamics. Reactor safety codes, such as SIMMER, model transients of the entire reactor core using coupled space-time neutronics and comprehensive thermal-fluid dynamics. Nondestructive delayed-neutron assay instruments are designed and modeled using a three-dimensional continuous-energy Monte Carlo code. Calculations on high-burnup spent fuels and other materials that contain a mix of uranium and plutonium isotopes require accurate and complete information on the delayed-neutron periods, yields, and energy spectra. A continuing need exists for delayed-neutron parameters for all the fissioning isotopes.

  3. Notes 04. Elements of analytical dynamics. 

    E-Print Network [OSTI]

    San Andres, Luis

    2008-01-01

    Elements of Analytical Mechanics ? 2008 Luis San Andr?s 1 MEEN 617 - Handout 4a ELEMENTS OF ANALYTICAL MECHANICS Newton's laws (Euler's fundamental principles of motion) are formulated for a single particle and easily extended to systems of particles.... This method is also valid for continuous systems, and in which case not only the equations of motion are obtained but also the associated (natural) boundary conditions. MEEN 617 - Handout 4 Elements of Analytical Mechanics ? 2008 Luis San Andr?s 2...

  4. Method of identity analyte-binding peptides

    DOE Patents [OSTI]

    Kauvar, L.M.

    1990-10-16

    A method for affinity chromatography or adsorption of a designated analyte utilizes a paralog as the affinity partner. The immobilized paralog can be used in purification or analysis of the analyte; the paralog can also be used as a substitute for antibody in an immunoassay. The paralog is identified by screening candidate peptide sequences of 4--20 amino acids for specific affinity to the analyte. 5 figs.

  5. Smart Microfabricated Preconcentrator (and Other Micro Analytical...

    Office of Scientific and Technical Information (OSTI)

    Smart Microfabricated Preconcentrator (and Other Micro Analytical Detection Components&Systems). Citation Details In-Document Search Title: Smart Microfabricated Preconcentrator...

  6. Analytic Challenges to Valuing Energy Storage

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    analytical task. Market Conditions - Markets are continually evolving, and the long-term value of energy storage is difficult to capture. Niche markets have emerged, but...

  7. Transesterification: Laboratory Analytical Procedure (LAP) Van...

    Office of Scientific and Technical Information (OSTI)

    Wychen, S.; Laurens, L. M. L. 09 BIOMASS FUELS; 59 BASIC BIOLOGICAL SCIENCES BIOMASS; ALGAE; LABORATORY ANALYTICAL PROCEDURES; LAPS; TOTAL LIPIDS; FATTY ACID METHYL ESTERS; FAME;...

  8. Investigation and Analytical Description of Acoustic Production...

    Office of Scientific and Technical Information (OSTI)

    Journal Article: Investigation and Analytical Description of Acoustic Production by Magneto-Acoustic Mixing Technology Citation Details In-Document Search This content will become...

  9. Development of Analytical Methodology for Neurochemical Investigations

    E-Print Network [OSTI]

    Fischer, David John

    2010-01-25

    David J. Fischer Department of Pharmaceutical Chemistry University of Kansas Neurochemical Applications of Microchip Electrophoresis The development of sensitive and selective analytical tools has facilitated the investigation ...

  10. Storage option an Analytic approach

    E-Print Network [OSTI]

    Dmitry Lesnik

    2012-05-28

    The mathematical problem of the static storage optimisation is formulated and solved by means of a variational analysis. The solution obtained in implicit form is shedding light on the most important features of the optimal exercise strategy. We show how the solution depends on different constraint types including carry cost and cycling constraint. We investigate the relation between intrinsic and stochastic solutions. In particular we give another proof that the stochastic problem has a "bang-bang" optimal exercise strategy. We also show why the optimal stochastic exercise decision is always close to the intrinsic one. In the second half we develop a perturbation analysis to solve the stochastic optimisation problem. The obtained approximate solution allows us to estimate the time value of the storage option. In particular we find an answer to rather academic question of asymptotic time value for the mean reversion parameter approaching zero or infinity. We also investigate the differences between swing and storage problems. The analytical results are compared with numerical valuations and found to be in a good agreement.

  11. Contained radiological analytical chemistry module

    DOE Patents [OSTI]

    Barney, David M. (Scotia, NY)

    1989-01-01

    A system which provides analytical determination of a plurality of water chemistry parameters with respect to water samples subject to radiological contamination. The system includes a water sample analyzer disposed within a containment and comprising a sampling section for providing predetermined volumes of samples for analysis; a flow control section for controlling the flow through the system; and a gas analysis section for analyzing samples provided by the sampling system. The sampling section includes a controllable multiple port valve for, in one position, metering out sample of a predetermined volume and for, in a second position, delivering the material sample for analysis. The flow control section includes a regulator valve for reducing the pressure in a portion of the system to provide a low pressure region, and measurement devices located in the low pressure region for measuring sample parameters such as pH and conductivity, at low pressure. The gas analysis section which is of independent utility provides for isolating a small water sample and extracting the dissolved gases therefrom into a small expansion volume wherein the gas pressure and thermoconductivity of the extracted gas are measured.

  12. Contained radiological analytical chemistry module

    DOE Patents [OSTI]

    Barney, David M. (Scotia, NY)

    1990-01-01

    A system which provides analytical determination of a plurality of water chemistry parameters with respect to water samples subject to radiological contamination. The system includes a water sample analyzer disposed within a containment and comprising a sampling section for providing predetermined volumes of samples for analysis; a flow control section for controlling the flow through the system; and a gas analysis section for analyzing samples provided by the sampling system. The sampling section includes a controllable multiple port valve for, in one position, metering out sample of a predetermined volume and for, in a second position, delivering the material sample for analysis. The flow control section includes a regulator valve for reducing the pressure in a portion of the system to provide a low pressure region, and measurement devices located in the low pressure region for measuring sample parameters such as pH and conductivity, at low pressure. The gas analysis section which is of independent utility provides for isolating a small water sample and extracting the dissolved gases therefrom into a small expansion volume wherein the gas pressure and thermoconductivity of the extracted gas are measured.

  13. Method and apparatus for detecting an analyte

    DOE Patents [OSTI]

    Allendorf, Mark D. (Pleasanton, CA); Hesketh, Peter J. (Atlanta, GA)

    2011-11-29

    We describe the use of coordination polymers (CP) as coatings on microcantilevers for the detection of chemical analytes. CP exhibit changes in unit cell parameters upon adsorption of analytes, which will induce a stress in a static microcantilever upon which a CP layer is deposited. We also describe fabrication methods for depositing CP layers on surfaces.

  14. Achieving Continuous Manufacturing: Technologies and Approaches for Synthesis, Workup, and Isolation of Drug Substance

    E-Print Network [OSTI]

    the different considerations for developing continuous processes compared with batch. In addition, through scale-up and into full scale production. The impact of continuous manufacture on drug substance analytical technologies (PAT) for real-time dynamic control of continuous processes. Develop modeling

  15. Hanford analytical sample projections 1996--2001

    SciTech Connect (OSTI)

    Joyce, S.M.

    1996-06-26

    This document summarizes the biannual Hanford sample projections for fiscal years 1996 to 2001. Sample projections are based on inputs submitted to Analytical Services covering Environmental Restoration, Tank Waste Remediation Systems (TWRS), Solid Waste, Liquid Effluents, Spent Nuclear Fuels, Transition Projects, Analytical Services, Site Monitoring, and Industrial Hygiene. This information will be used by Hanford Analytical Services to assure that laboratories and resources are available and effectively utilized to meet these documented needs. Sample projections are categorized by radiation level, protocol, sample matrix and Program. Analyses requirements are also presented.

  16. Sensor for detecting and differentiating chemical analytes

    DOE Patents [OSTI]

    Yi, Dechang (Metuchen, NJ); Senesac, Lawrence R. (Knoxville, TN); Thundat, Thomas G. (Knoxville, TN)

    2011-07-05

    A sensor for detecting and differentiating chemical analytes includes a microscale body having a first end and a second end and a surface between the ends for adsorbing a chemical analyte. The surface includes at least one conductive heating track for heating the chemical analyte and also a conductive response track, which is electrically isolated from the heating track, for producing a thermal response signal from the chemical analyte. The heating track is electrically connected with a voltage source and the response track is electrically connected with a signal recorder. The microscale body is restrained at the first end and the second end and is substantially isolated from its surroundings therebetween, thus having a bridge configuration.

  17. Analytical Layer Planning for Nanometer VLSI Designs 

    E-Print Network [OSTI]

    Chang, Chi-Yu

    2012-10-19

    i ANALYTICAL LAYER PLANNING FOR NANOMETER VLSI DESIGNS A Thesis by CHI-YU CHANG Submitted to the Office of Graduate Studies of Texas A&M University in partial fulfillment of the requirements for the degree of MASTER... OF SCIENCE August 2012 Major Subject: Electrical Engineering ii ANALYTICAL LAYER PLANNING FOR NANOMETER VLSI DESIGNS A Thesis by CHI-YU CHANG Submitted to the Office of Graduate Studies of Texas A&M University in partial...

  18. Preconcentration and separation of analytes in microchannels

    DOE Patents [OSTI]

    Hatch, Anson (Tracy, CA); Singh, Anup K. (Danville, CA); Herr, Amy E. (Fremont, CA); Throckmorton, Daniel J. (Tracy, CA)

    2010-11-09

    Disclosed herein are methods and devices for preconcentrating and separating analytes such as proteins and polynucleotides in microchannels. As disclosed, at least one size-exclusion polymeric element is adjacent to processing area or an assay area in a microchannel which may be porous polymeric element. The size-exclusion polymeric element may be used to manipulate, e.g. concentrate, analytes in a sample prior to assaying in the assay area.

  19. An Analytical Approach for Tail-Pipe Emissions Estimation with...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    An Analytical Approach for Tail-Pipe Emissions Estimation with Coupled Engine and Aftertreatment System An Analytical Approach for Tail-Pipe Emissions Estimation with Coupled...

  20. SASSI Analytical Methods Compared with SHAKE Results | Department...

    Office of Environmental Management (EM)

    with SHAKE Results SASSI Analytical Methods Compared with SHAKE Results Structural Mechanics - SRS October 4, 2011 SASSI Analytical Methods Compared with SHAKE Results More...

  1. DOE National Analytical Management Program Draws Global Interest

    Broader source: Energy.gov [DOE]

    CARLSBAD, N.M. – The National Analytical Management Program (NAMP), which coordinates analytical services and capabilities throughout DOE, has garnered global interest.

  2. Big Data and Analytics at Work | GE Global Research

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    time analytics is required At GE we keep pace with these trends via the Industrial Internet, a highly connected ecosystem of intelligent machines, advanced analytics and people...

  3. Current Analytical Chemistry, 2005, 1, 103-119 103 Porphyrin Based Affinity Interactions: Analytical Applications with Special

    E-Print Network [OSTI]

    Miksik, Ivan

    Current Analytical Chemistry, 2005, 1, 103-119 103 Porphyrin Based Affinity Interactions in analytical chemistry as well. Spectropho- tometric, potentiometric and voltammetric methods for the analysis: Analytical Applications with Special Reference to Open Tubular Capillary Electrochromatography Zdenek Deyl*,1

  4. Peterson Building - 8 

    E-Print Network [OSTI]

    Unknown

    2009-01-01

    Compressive Strengths by Age. . . . . . . . . . . . . . . . 159 Bias Factor for Splitting Tensile Strength (Using Best Fit Equation). . . . . . . . . . . 160 Figure 4. 26. Failures of Modulus of Rupture Specimens. Figure 4. 27. Quantile Plots for Modulus.... Creep Test for Batches Al l-A12. Figure B. 22. Creep Test for Batches BS-B6. Figure B. 23. Creep Test for Batches B9-B10. Figure B. 24. Creep Test for Batches B13-B14. Figure B. 25. Creep Test for Batches C7-C8. Figure B. 26. Creep Test for Batches...

  5. SAAF: SANS data Analysis using Analytical Functions

    SciTech Connect (OSTI)

    Zhao, Jinkui [ORNL

    2011-01-01

    The recently completed Extended Q-Range Small Angle Scattering Diffractometer (EQ-SANS) has put the focus on its software needs with renewed urgency. In a series of efforts, we aim at providing a complete set of software solutions on the EQ-SANS instrument. These programs include initial data processing, data correction and reduction, analytical model fitting to the scattering data, Monte Carlo simulation for structure determination, and virtual instrument simulation for experiment planning. SAAF is one such program for analytical data modeling. It takes the reduced EQ-SANS data and allows users to fit the data to analytical models. These models are easy to write. They can either be user written, or from the pre-supplied model library.

  6. Analytical Chemistry Core Capability Assessment - Preliminary Report

    SciTech Connect (OSTI)

    Barr, Mary E. [Los Alamos National Laboratory; Farish, Thomas J. [Los Alamos National Laboratory

    2012-05-16

    The concept of 'core capability' can be nebulous one. Even at a fairly specific level, where core capability equals maintaining essential services, it is highly dependent upon the perspective of the requestor. Samples are submitted to analytical services because the requesters do not have the capability to conduct adequate analyses themselves. Some requests are for general chemical information in support of R and D, process control, or process improvement. Many analyses, however, are part of a product certification package and must comply with higher-level customer quality assurance requirements. So which services are essential to that customer - just those for product certification? Does the customer also (indirectly) need services that support process control and improvement? And what is the timeframe? Capability is often expressed in terms of the currently utilized procedures, and most programmatic customers can only plan a few years out, at best. But should core capability consider the long term where new technologies, aging facilities, and personnel replacements must be considered? These questions, and a multitude of others, explain why attempts to gain long-term consensus on the definition of core capability have consistently failed. This preliminary report will not try to define core capability for any specific program or set of programs. Instead, it will try to address the underlying concerns that drive the desire to determine core capability. Essentially, programmatic customers want to be able to call upon analytical chemistry services to provide all the assays they need, and they don't want to pay for analytical chemistry services they don't currently use (or use infrequently). This report will focus on explaining how the current analytical capabilities and methods evolved to serve a variety of needs with a focus on why some analytes have multiple analytical techniques, and what determines the infrastructure for these analyses. This information will be useful in defining a roadmap for what future capability needs to look like.

  7. 100-B/C Target Analyte List Development for Soil

    SciTech Connect (OSTI)

    R.W. Ovink

    2010-03-18

    This report documents the process used to identify source area target analytes in support of the 100-B/C remedial investigation/feasibility study addendum to DOE/RL-2008-46. This report also establishes the analyte exclusion criteria applicable for 100-B/C use and the analytical methods needed to analyze the target analytes.

  8. Guide to Savannah River Laboratory Analytical Services Group

    SciTech Connect (OSTI)

    Not Available

    1990-04-01

    The mission of the Analytical Services Group (ASG) is to provide analytical support for Savannah River Laboratory Research and Development Programs using onsite and offsite analytical labs as resources. A second mission is to provide Savannah River Site (SRS) operations with analytical support for nonroutine material characterization or special chemical analyses. The ASG provides backup support for the SRS process control labs as necessary.

  9. Nonlinear mechanical and poromechanical analyses: comparison with analytical solutions

    E-Print Network [OSTI]

    Boyer, Edmond

    analytical solutions exist in the field of geomechanics. This is an important step before evaluating

  10. Support for Scalable Analytics over Databases and Data-Streams

    E-Print Network [OSTI]

    Laptev, Nikolay Pavlovich

    2012-01-01

    blogs, social medias and Internet searches. ‘Big Data Analytics’ is now recognized as an emerging technology

  11. CRAIG G. FRASER"' LAGRANGE'S ANALYTICAL MATHEMATICS,

    E-Print Network [OSTI]

    Fraser, Craig

    CRAIG G. FRASER"' LAGRANGE'S ANALYTICAL MATHEMATICS, ITS CARTESIAN ORIGINS AND RECEPTION IN COMTE to the mathematical methods developed in the preceding century by Euler and Lagrange. In the course of his discussion. . . . All his mathematical compositions are remarkable for a singular elegance, by the symmetry of forms

  12. Analytical theory of multipass crystal extraction

    SciTech Connect (OSTI)

    Biryukov, V.; Murphy, C.T.

    1997-10-01

    An analytical theory for the efficiency of particle extraction from an accelerator by means of a bent crystal is proposed. The theory agrees with all the measurements performed in the broad energy range of 14 to 900 GeV, where the efficiency range also spans over two decades, from {approximately}0.3% to {approximately}30%.

  13. Enhancing Power Grid Stability through Analytics

    E-Print Network [OSTI]

    Lakoba, Taras I.

    Enhancing Power Grid Stability through Analytics: Information is Power, and Power is Information no dummies). · But... many challenges in the North American power grid revolve around coordinating? Power is Information · Refrain in many quarters of the power grid today says that we must "extract

  14. Software Analytics: Achievements and Challenges Dongmei Zhang

    E-Print Network [OSTI]

    Xie, Tao

    Software Analytics: Achievements and Challenges Dongmei Zhang Microsoft Research Asia Beijing, USA Email: xie@csc.ncsu.edu Abstract--A huge wealth of various data exist in the practice of software development. Further rich data are produced by modern software and services in operation, many of which tend

  15. Analytical Study of Thermonuclear Reaction Probability Integrals

    E-Print Network [OSTI]

    M. A. Chaudhry; H. J. Haubold; A. M. Mathai

    2000-01-16

    An analytic study of the reaction probability integrals corresponding to the various forms of the slowly varying cross-section factor $S(E)$ is attempted. Exact expressions for reaction probability integrals are expressed in terms of the extended gamma functions.

  16. Cardiogram: Visual Analytics for Automotive Engineers

    E-Print Network [OSTI]

    Cardiogram: Visual Analytics for Automotive Engineers Michael Sedlmair1, Petra Isenberg2, Dominikus that sup- ports automotive engineers in debugging masses of traces each consisting of millions of recorded-critical networks to be error-free has become a major task and challenge for automotive engi- neers. To overcome

  17. Using data analytics to streamline healthcare costs

    E-Print Network [OSTI]

    Using data analytics to streamline healthcare costs The STFC Hartree Centre has helped Albatross Financial Solutions optimise the patient cost benchmarking service it provides to NHS Trusts, helping them to validate and predict costs more accurately and establish best practices. Challenge Most of us will contract

  18. An Analytical Solution on Convective and Diffusive Transport of Analyte in Laminar Flow of Microfluidic Slit

    E-Print Network [OSTI]

    Chen, X.

    Microfluidic devices could find applications in many areas, such as BioMEMs, miniature fuel cells and microfluidic cooling of electronic circuitry. One of the important considerations of microfluidic device in analytical ...

  19. Technosocial Predictive Analytics for Illicit Nuclear Trafficking

    SciTech Connect (OSTI)

    Sanfilippo, Antonio P.; Butner, R. Scott; Cowell, Andrew J.; Dalton, Angela C.; Haack, Jereme N.; Kreyling, Sean J.; Riensche, Roderick M.; White, Amanda M.; Whitney, Paul D.

    2011-03-29

    Illicit nuclear trafficking networks are a national security threat. These networks can directly lead to nuclear proliferation, as state or non-state actors attempt to identify and acquire nuclear weapons-related expertise, technologies, components, and materials. The ability to characterize and anticipate the key nodes, transit routes, and exchange mechanisms associated with these networks is essential to influence, disrupt, interdict or destroy the function of the networks and their processes. The complexities inherent to the characterization and anticipation of illicit nuclear trafficking networks requires that a variety of modeling and knowledge technologies be jointly harnessed to construct an effective analytical and decision making workflow in which specific case studies can be built in reasonable time and with realistic effort. In this paper, we explore a solution to this challenge that integrates evidentiary and dynamic modeling with knowledge management and analytical gaming, and demonstrate its application to a geopolitical region at risk.

  20. Analytical model for Stirling cycle machine design

    E-Print Network [OSTI]

    Formosa, Fabien; 10.1016/j.enconman.2010.02.010

    2013-01-01

    In order to study further the promising free piston Stirling engine architecture, there is a need of an analytical thermodynamic model which could be used in a dynamical analysis for preliminary design. To aim at more realistic values, the models have to take into account the heat losses and irreversibilities on the engine. An analytical model which encompasses the critical flaws of the regenerator and furthermore the heat exchangers effectivenesses has been developed. This model has been validated using the whole range of the experimental data available from the General Motor GPU-3 Stirling engine prototype. The effects of the technological and operating parameters on Stirling engine performance have been investigated. In addition to the regenerator influence, the effect of the cooler effectiveness is underlined.

  1. Electrospray ion source with reduced analyte electrochemistry

    DOE Patents [OSTI]

    Kertesz, Vilmos [Knoxville, TN; Van Berkel, Gary [Clinton, TN

    2011-08-23

    An electrospray ion (ESI) source and method capable of ionizing an analyte molecule without oxidizing or reducing the analyte of interest. The ESI source can include an emitter having a liquid conduit, a working electrode having a liquid contacting surface, a spray tip, a secondary working electrode, and a charge storage coating covering partially or fully the liquid contacting surface of the working electrode. The liquid conduit, the working electrode and the secondary working electrode can be in liquid communication. The electrospray ion source can also include a counter electrode proximate to, but separated from, said spray tip. The electrospray ion source can also include a power system for applying a voltage difference between the working electrodes and a counter-electrode. The power system can deliver pulsed voltage changes to the working electrodes during operation of said electrospray ion source to minimize the surface potential of the charge storage coating.

  2. Comparison of open source visual analytics toolkits.

    SciTech Connect (OSTI)

    Crossno, Patricia Joyce; Harger, John R.

    2010-11-01

    We present the results of the first stage of a two-stage evaluation of open source visual analytics packages. This stage is a broad feature comparison over a range of open source toolkits. Although we had originally intended to restrict ourselves to comparing visual analytics toolkits, we quickly found that very few were available. So we expanded our study to include information visualization, graph analysis, and statistical packages. We examine three aspects of each toolkit: visualization functions, analysis capabilities, and development environments. With respect to development environments, we look at platforms, language bindings, multi-threading/parallelism, user interface frameworks, ease of installation, documentation, and whether the package is still being actively developed.

  3. Electrospray ion source with reduced analyte electrochemistry

    DOE Patents [OSTI]

    Kertesz, Vilmos; Van Berkel, Gary J

    2013-07-30

    An electrospray ion (ESI) source and method capable of ionizing an analyte molecule without oxidizing or reducing the analyte of interest. The ESI source can include an emitter having a liquid conduit, a working electrode having a liquid contacting surface, a spray tip, a secondary working electrode, and a charge storage coating covering partially or fully the liquid contacting surface of the working electrode. The liquid conduit, the working electrode and the secondary working electrode can be in liquid communication. The electrospray ion source can also include a counter electrode proximate to, but separated from, said spray tip. The electrospray ion source can also include a power system for applying a voltage difference between the working electrodes and a counter-electrode. The power system can deliver pulsed voltage changes to the working electrodes during operation of said electrospray ion source to minimize the surface potential of the charge storage coating.

  4. Small Scale Cosmological Perturbations: An Analytic Approach

    E-Print Network [OSTI]

    Wayne Hu; Naoshi Sugiyama

    1996-04-19

    Through analytic techniques verified by numerical calculations, we establish general relations between the matter and cosmic microwave background (CMB) power spectra and their dependence on cosmological parameters on small scales. Fluctuations in the CMB, baryons, cold dark matter (CDM), and neutrinos receive a boost at horizon crossing. Baryon drag on the photons causes alternating acoustic peak heights in the CMB and is uncovered in its bare form under the photon diffusion scale. Decoupling of the photons at last scattering and of the baryons at the end of the Compton drag epoch, freezes the diffusion-damped acoustic oscillations into the CMB and matter power spectra at different scales. We determine the dependence of the respective acoustic amplitudes and damping lengths on fundamental cosmological parameters. The baryonic oscillations, enhanced by the velocity overshoot effect, compete with CDM fluctuations in the present matter power spectrum. We present new exact analytic solutions for the cold dark matter fluctuations in the presence of a growth- inhibiting radiation {\\it and} baryon background. Combined with the acoustic contributions and baryonic infall into CDM potential wells, this provides a highly accurate analytic form of the small-scale transfer function in the general case.

  5. Experimental and analytical study of rotating cavitation

    SciTech Connect (OSTI)

    Kamijo, Kenjiro; Shimura, Takashi; Tsujimoto, Yoshinobu [National Aerospace Lab., Miyagi (Japan). Kakuda Research Center

    1994-12-31

    This paper describes experimental and analytical results of rotating cavitation. There are four major sections in this paper. The first section presents the main characteristics of rotating cavitation which was found in the inducer test using a water tunnel. The second section describes the rotating cavitation which occurred in the development test of an LE-7 liquid oxygen pump for the H-II rocket. Also described in this section is how the rotating cavitation was suppressed. The rotating cavitation was the cause of both super synchronous shaft vibration and an unstable head coefficient curve. The third section presents how the theory of rotating cavitation was developed. The final section shows the measured cavitation compliance and mass flow gain factor of the LE-7 pump inducer for comparison of the experimental and analytical results of the rotating cavitation of the LE-7 pump inducer. Almost all the information presented in this paper has already been reported by Kamijo et al. (1977, 1980, 1993, 1993) and by Shimura (1993). In the present paper, the authors attempt to combine and give a clear overview of the experimental and analytical results described in the previous papers to systematically show their experience and findings on rotating cavitation.

  6. Solar Water Heaters | Department of Energy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    The batch collector is a large box holding a tank and covered with a glaze that faces the sun. Water is heated in this tank, and another pipe takes the heated water from the batch...

  7. Using Hybrid MPI and OpenMP on Hopper and Edison

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    aprun -n 16 -N 2 -S 1 -d 12 a.out Please refer to sample batch scripts for running hybrid MPIOpenMP jobs on the Edison Example Batch Scripts webpage. Notice the different...

  8. CONTAMINATION OF GROUNDWATER BY ORGANIC POLLUTANTS LEACHED FROM IN-SITU SPENT SHALE

    E-Print Network [OSTI]

    Amy, Gary L.

    2013-01-01

    Variables , , , , , , Groundwater Pollution Potential of In-temperature of 80°C. Groundwater batch experiments exam:tn:1 spent shale at 20°C Groundwater batch experiments exam:tn:

  9. Request queues for interactive clients in a shared file system of a parallel computing system

    DOE Patents [OSTI]

    Bent, John M.; Faibish, Sorin

    2015-08-18

    Interactive requests are processed from users of log-in nodes. A metadata server node is provided for use in a file system shared by one or more interactive nodes and one or more batch nodes. The interactive nodes comprise interactive clients to execute interactive tasks and the batch nodes execute batch jobs for one or more batch clients. The metadata server node comprises a virtual machine monitor; an interactive client proxy to store metadata requests from the interactive clients in an interactive client queue; a batch client proxy to store metadata requests from the batch clients in a batch client queue; and a metadata server to store the metadata requests from the interactive client queue and the batch client queue in a metadata queue based on an allocation of resources by the virtual machine monitor. The metadata requests can be prioritized, for example, based on one or more of a predefined policy and predefined rules.

  10. Bench Scale Integration Presentation for BETO 2015 Project Peer...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    bioconversion scalemethod Bench scale Batch Pilot scale Fed-batch Bioconversion Volumetric Productivity (gL-hr) 0.29 0.4 Lipid Content (wt%) 57% 60% Glucose to Product total...

  11. A list of acronyms, abbreviations, symbols, and notation is given in Appendix A. A list of definitions is given in Appendix B

    E-Print Network [OSTI]

    values used in site-specific contaminant transport and risk assessment calculations. Issues regarding-situ batch method, (3) labor

  12. Raman spectroscopy of complex defined media: biopharmaceutical applications

    E-Print Network [OSTI]

    Ram, Rajeev J.

    , grown in shake flasks in batch fermentation mode, using Raman spectroscopy and explicit model glutamine, glutamate, glucose, la

  13. Annals of Mathematics and Artificial Intelligence (2005) 43: 134 Springer 2004 On SAT instance classes and a method for reliable

    E-Print Network [OSTI]

    Stallmann, Matt

    2005-01-01

    of hardware components such as lightbulbs, A/C units, etc. A batch of N replicated hardware components

  14. Attached Scientific Processors for Chemical Computations: A Report to the Chemistry Community

    E-Print Network [OSTI]

    Ostlund, Neil S.

    2012-01-01

    chemistry the AP-120B is better dedicated to the batch execution of long computationally intensive jobs.

  15. BEopt Optimization Tool and National Residential Efficiency Measures...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    response * HPXML export * Schedule wizard * Output visualization * Batch simulations * Library manager * ... Heating Cooling Lighting Appliances Other Efficiency PVSHW Energy Use...

  16. Untitled Document

    National Nuclear Security Administration (NNSA)

    Radionuclide Retardation Measurements of Batch-Sorption Distribution Coefficients for Barium, Cesium, Selenium, Strontium, Uranium, Plutonium, and Neptunium, Submittal 12...

  17. On Jentzsch sets of functions analytic in the unit disc

    E-Print Network [OSTI]

    2015-10-14

    On Jentzsch sets of functions analytic in the. unit disc. Alexandre Eremenko. Sometime 1993. Dear Lee: Let f be an analytic function in the unit disc U = {z : |z|

  18. Modern Data Architectures for Scalable Analytics | ornl.gov

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Modern Data Architectures for Scalable Analytics Apr 14 2014 11:00 AM - 12:00 PM Arjun Shankar, Computational Data Analytics Group, ORNL Computer Sciences and Engineering Division...

  19. Analytic models of plausible gravitational lens potentials

    SciTech Connect (OSTI)

    Baltz, Edward A.; Marshall, Phil; Oguri, Masamune, E-mail: eabaltz@slac.stanford.edu, E-mail: pjm@physics.ucsb.edu, E-mail: oguri@slac.stanford.edu [Kavli Institute for Particle Astrophysics and Cosmology, Stanford University, PO Box 20450, MS29, Stanford, CA 94309 (United States)] [Kavli Institute for Particle Astrophysics and Cosmology, Stanford University, PO Box 20450, MS29, Stanford, CA 94309 (United States)

    2009-01-15

    Gravitational lenses on galaxy scales are plausibly modelled as having ellipsoidal symmetry and a universal dark matter density profile, with a Sersic profile to describe the distribution of baryonic matter. Predicting all lensing effects requires knowledge of the total lens potential: in this work we give analytic forms for that of the above hybrid model. Emphasising that complex lens potentials can be constructed from simpler components in linear combination, we provide a recipe for attaining elliptical symmetry in either projected mass or lens potential. We also provide analytic formulae for the lens potentials of Sersic profiles for integer and half-integer index. We then present formulae describing the gravitational lensing effects due to smoothly-truncated universal density profiles in cold dark matter model. For our isolated haloes the density profile falls off as radius to the minus fifth or seventh power beyond the tidal radius, functional forms that allow all orders of lens potential derivatives to be calculated analytically, while ensuring a non-divergent total mass. We show how the observables predicted by this profile differ from that of the original infinite-mass NFW profile. Expressions for the gravitational flexion are highlighted. We show how decreasing the tidal radius allows stripped haloes to be modelled, providing a framework for a fuller investigation of dark matter substructure in galaxies and clusters. Finally we remark on the need for finite mass halo profiles when doing cosmological ray-tracing simulations, and the need for readily-calculable higher order derivatives of the lens potential when studying catastrophes in strong lenses.

  20. Analytical models of relativistic accretion disks

    E-Print Network [OSTI]

    Viacheslav V. Zhuravlev

    2015-09-24

    We present not a literature review but a description, as detailed and consistent as possible, of two analytic models of disk accretion onto a rotating black hole: a standard relativistic disk and a twisted relativistic disk. Although one of these models is much older than the other, both are of topical current interest for black hole studies. The way the exposition is presented, the reader with only a limited knowledge of general relativity and relativistic hydrodynamics can --- with little or no use of additional sources -- gain good insight into many technical details lacking in the original papers.

  1. Analytical solutions to matrix diffusion problems

    SciTech Connect (OSTI)

    Kekäläinen, Pekka

    2014-10-06

    We report an analytical method to solve in a few cases of practical interest the equations which have traditionally been proposed for the matrix diffusion problem. In matrix diffusion, elements dissolved in ground water can penetrate the porous rock surronuding the advective flow paths. In the context of radioactive waste repositories this phenomenon provides a mechanism by which the area of rock surface in contact with advecting elements is greatly enhanced, and can thus be an important delay mechanism. The cases solved are relevant for laboratory as well for in situ experiments. Solutions are given as integral representations well suited for easy numerical solution.

  2. Analytical laboratory and mobile sampling platform

    SciTech Connect (OSTI)

    Stetzenbach, K.; Smiecinski, A.

    1996-04-30

    This is the final report for the Analytical Laboratory and Mobile Sampling Platform project. This report contains only major findings and conclusions resulting from this project. Detailed reports of all activities performed for this project were provided to the Project Office every quarter since the beginning of the project. This report contains water chemistry data for samples collected in the Nevada section of Death Valley National Park (Triangle Area Springs), Nevada Test Site springs, Pahranagat Valley springs, Nevada Test Site wells, Spring Mountain springs and Crater Flat and Amargosa Valley wells.

  3. Photovoltaic Degradation Rates -- An Analytical Review

    SciTech Connect (OSTI)

    Jordan, D. C.; Kurtz, S. R.

    2012-06-01

    As photovoltaic penetration of the power grid increases, accurate predictions of return on investment require accurate prediction of decreased power output over time. Degradation rates must be known in order to predict power delivery. This article reviews degradation rates of flat-plate terrestrial modules and systems reported in published literature from field testing throughout the last 40 years. Nearly 2000 degradation rates, measured on individual modules or entire systems, have been assembled from the literature, showing a median value of 0.5%/year. The review consists of three parts: a brief historical outline, an analytical summary of degradation rates, and a detailed bibliography partitioned by technology.

  4. Analytical mesoscale modeling of aeolian sand transport

    E-Print Network [OSTI]

    Marc Lämmel; Anne Meiwald; Klaus Kroy

    2014-05-03

    We analyze the mesoscale structure of aeolian sand transport, based on a recently developed two-species continuum model. The calculated sand flux and important average characteristics of the grain trajectories are found to be in remarkable agreement with field and wind-tunnel data. We conclude that the essential mesoscale physics is insensitive to unresolved details on smaller scales and well captured by the coarse-grained analytical model, thus providing a sound basis for precise and numerically efficient mesoscale modeling of aeolian structure formation.

  5. NREL: Measurements and Characterization - Analytical Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantityBonneville Power Administration wouldMass map shines lightGeospatial Toolkit The GeospatialSolar Energy The(35.93Analytical

  6. Category:Analytical Modeling | Open Energy Information

    Open Energy Info (EERE)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Home Page on Google Bookmark EERE: Alternative Fuels Data Center Home Page on QA:QA J-E-1 SECTION JEnvironmentalBowerbank,Cammack Village,8199089°,Analytical Modeling Jump to: navigation, search

  7. Analytical Approaches Towards Understanding Structure-Property

    Office of Scientific and Technical Information (OSTI)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity of NaturalDukeWakefield MunicipalTechnicalInformation4563AbuseConnect Technicalofand PuConnect Analytic

  8. Scientific Achievement Analytical Transmission Electron Microscopy

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach Home RoomPreservation ofAlbuquerque| StanfordOffice of ScienceDiscovered theAnalytical Transmission

  9. Linear differential elimination for analytic functions W. Plesken, D. Robertz

    E-Print Network [OSTI]

    Robertz, Daniel

    Linear differential elimination for analytic functions W. Plesken, D. Robertz Abstract This paper provides methods to decide whether a given analytic function of several complex variables is a linear the function (sin x)2 is a linear combination of the form f1(x)·(cos(x+y))2 +f2(y)·cos(2x+y) with analytic

  10. One Statistician's Perspectives on Statistics and "Big Data" Analytics

    E-Print Network [OSTI]

    Vardeman, Stephen B.

    One Statistician's Perspectives on Statistics and "Big Data" Analytics Some (Ultimately 2014 Vardeman (Iowa State University) Perspectives on "Big Data" Analytics July 2014 1 / 16 #12;My/modern-multivariate-statistical-learning/ Vardeman (Iowa State University) Perspectives on "Big Data" Analytics July 2014 2 / 16 #12;Some (Indirect

  11. Analyte sensing mediated by adapter/carrier molecules

    DOE Patents [OSTI]

    Bayley, Hagan (College Station, TX); Braha, Orit (College Station, TX); Gu, LiQun (Bryan, TX)

    2002-07-30

    This invention relates to an improved method and system for sensing of one or more analytes. A host molecule, which serves as an adapter/carrier, is used to facilitate interaction between the analyte and the sensor element. A detectable signal is produced reflecting the identity and concentration of analyte present.

  12. To cite this this version Shewani, Anil and Horgue, Pierre and Pommier, Sbastien and Debenest, Grald and Lefebvre, Xavier and

    E-Print Network [OSTI]

    Mailhes, Corinne

    a solid leach bed in dry batch anaerobic digestion processes. (2015) Bioresource Technology, vol. 178. pp batch anaerobic digestion processes Anil Shewani a,b,c,f , Pierre Horgue d,e , Sébastien Pommier a experimental dynamic water retention. Keywords: Dry batch anaerobic digestion Leachate percolation Water

  13. Transactions of the ASABE Vol. 49(1): 107-112 E 2006 American Society of Agricultural and Biological Engineers ISSN 0001-2351 107

    E-Print Network [OSTI]

    He, Brian

    batch and existing continuous-flow processes requires the use of a much higher excess alcohol, typically was about 3 min, which is 20 to 30 times shorter than in typical batch processes. The productivity of the RD than that of batch and existing continuous-flow processes. Keywords. Biodiesel, Canola oil, Fatty acid

  14. Road Transportable Analytical Laboratory system. Phase 1

    SciTech Connect (OSTI)

    Finger, S.M.; Keith, V.F.; Spertzel, R.O.; De Avila, J.C.; O`Donnell, M.; Vann, R.L.

    1993-09-01

    This developmental effort clearly shows that a Road Transportable Analytical Laboratory System is a worthwhile and achievable goal. The RTAL is designed to fully analyze (radioanalytes, and organic and inorganic chemical analytes) 20 samples per day at the highest levels of quality assurance and quality control. It dramatically reduces the turnaround time for environmental sample analysis from 45 days (at a central commercial laboratory) to 1 day. At the same time each RTAL system will save the DOE over $12 million per year in sample analysis costs compared to the costs at a central commercial laboratory. If RTAL systems were used at the eight largest DOE facilities (at Hanford, Savannah River, Fernald, Oak Ridge, Idaho, Rocky Flats, Los Alamos, and the Nevada Test Site), the annual savings would be $96,589,000. The DOE`s internal study of sample analysis needs projects 130,000 environmental samples requiring analysis in FY 1994, clearly supporting the need for the RTAL system. The cost and time savings achievable with the RTAL system will accelerate and improve the efficiency of cleanup and remediation operations throughout the DOE complex.

  15. Visual Analytics for Power Grid Contingency Analysis

    SciTech Connect (OSTI)

    Wong, Pak C.; Huang, Zhenyu; Chen, Yousu; Mackey, Patrick S.; Jin, Shuangshuang

    2014-01-20

    Contingency analysis is the process of employing different measures to model scenarios, analyze them, and then derive the best response to remove the threats. This application paper focuses on a class of contingency analysis problems found in the power grid management system. A power grid is a geographically distributed interconnected transmission network that transmits and delivers electricity from generators to end users. The power grid contingency analysis problem is increasingly important because of both the growing size of the underlying raw data that need to be analyzed and the urgency to deliver working solutions in an aggressive timeframe. Failure to do so may bring significant financial, economic, and security impacts to all parties involved and the society at large. The paper presents a scalable visual analytics pipeline that transforms about 100 million contingency scenarios to a manageable size and form for grid operators to examine different scenarios and come up with preventive or mitigation strategies to address the problems in a predictive and timely manner. Great attention is given to the computational scalability, information scalability, visual scalability, and display scalability issues surrounding the data analytics pipeline. Most of the large-scale computation requirements of our work are conducted on a Cray XMT multi-threaded parallel computer. The paper demonstrates a number of examples using western North American power grid models and data.

  16. Summative Mass Analysis of Algal Biomass - Integration of Analytical Procedures: Laboratory Analytical Procedure (LAP)

    SciTech Connect (OSTI)

    Laurens, L. M. L.

    2013-12-01

    This procedure guides the integration of laboratory analytical procedures to measure algal biomass constituents in an unambiguous manner and ultimately achieve mass balance closure for algal biomass samples. Many of these methods build on years of research in algal biomass analysis.

  17. DroidAnalytics: A Signature Based Analytic System to Collect, Extract, Analyze and Associate Android Malware

    E-Print Network [OSTI]

    Lui, John C.S.

    Android Malware Min Zheng, Mingshen Sun, John C.S. Lui Computer Science & Engineering Department android malware. The system facilitates analysts to retrieve, associate and reveal malicious logics at the "opcode level". We demonstrate the efficacy of DroidAnalytics using 150,368 Android applications

  18. The QCD phase diagram from analytic continuation

    E-Print Network [OSTI]

    Bellwied, R; Fodor, Z; Günther, J; Katz, S D; Ratti, C; Szabo, K K

    2015-01-01

    We present the crossover line between the quark gluon plasma and the hadron gas phases for small real chemical potentials. First we determine the effect of imaginary values of the chemical potential on the transition temperature using lattice QCD simulations. Then we use various formulas to perform an analytic continuation to real values of the baryo-chemical potential. Our data set maintains strangeness neutrality to match the conditions of heavy ion physics. The systematic errors are under control up to $\\mu_B\\approx 300$ MeV. For the curvature of the transition line we find that there is an approximate agreement between values from three different observables: the chiral susceptibility, chiral condensate and strange quark susceptibility. The continuum extrapolation is based on $N_t=$ 10, 12 and 16 lattices. By combining the analysis for these three observables we find, for the curvature, the value $\\kappa = 0.0149 \\pm 0.0021$.

  19. Sky coverage of orbital detectors. Analytical approach

    E-Print Network [OSTI]

    Diego Casadei

    2005-12-28

    Orbital detectors without pointing capability have to keep their field of view axis laying on their orbital plane, to observe the largest sky fraction. A general approach to estimate the exposure of each sky element for such detectors is a valuable tool in the R&D phase of a project, when the detector characteristics are still to be fixed. An analytical method to estimate the sky exposure is developed, which makes only few very reasonable approximations. The formulae obtained with this method are used to compute the histogram of the sky exposure of a hypothetical gamma-ray detector installed on the ISS. The C++ code used in this example is freely available on the http://cern.ch/casadei/software.html web page.

  20. Analytical Improvements in PV Degradation Rate Determination

    SciTech Connect (OSTI)

    Jordan, D. C.; Kurtz, S. R.

    2011-02-01

    As photovoltaic (PV) penetration of the power grid increases, it becomes vital to know how decreased power output may affect cost over time. In order to predict power delivery, the decline or degradation rates must be determined accurately. For non-spectrally corrected data several complete seasonal cycles (typically 3-5 years) are required to obtain reasonably accurate degradation rates. In a rapidly evolving industry such a time span is often unacceptable and the need exists to determine degradation rates accurately in a shorter period of time. Occurrence of outliers and data shifts are two examples of analytical problems leading to greater uncertainty and therefore to longer observation times. In this paper we compare three methodologies of data analysis for robustness in the presence of outliers, data shifts and shorter measurement time periods.

  1. Analytical Form of Forces in Hydrophobic Collapse

    E-Print Network [OSTI]

    J. Chakrabarti; Suman Dutta

    2015-05-29

    We calculate analytically the forces between two solvophobic solutes, considering a model system. We show that the effective interaction forces between two solvophobic solutes, mediated by the solvent, is attractive for short ranges, which decreases linearly with surface-to-surface separation s between the solutes and repulsive in the long range falling off as 1 / s 4 . The attraction originates from the unbalanced Laplace force at the liquid-gas interface, generated by the repulsive interaction with the solvent particles, around the solutes at small s. The long range part arises due to unbalanced osmotic pressure. We illustrate the calculations for the Lennard-Jones solvent. We discuss the general implication of our results in the context of hydrophobic collapse.

  2. ANALYTICAL SOLUTIONS OF SINGULAR ISOTHERMAL QUADRUPOLE LENS

    SciTech Connect (OSTI)

    Chu Zhe; Lin, W. P.; Yang Xiaofeng E-mail: linwp@shao.ac.cn

    2013-06-20

    Using an analytical method, we study the singular isothermal quadrupole (SIQ) lens system, which is the simplest lens model that can produce four images. In this case, the radial mass distribution is in accord with the profile of the singular isothermal sphere lens, and the tangential distribution is given by adding a quadrupole on the monopole component. The basic properties of the SIQ lens have been studied in this Letter, including the deflection potential, deflection angle, magnification, critical curve, caustic, pseudo-caustic, and transition locus. Analytical solutions of the image positions and magnifications for the source on axes are derived. We find that naked cusps will appear when the relative intensity k of quadrupole to monopole is larger than 0.6. According to the magnification invariant theory of the SIQ lens, the sum of the signed magnifications of the four images should be equal to unity, as found by Dalal. However, if a source lies in the naked cusp, the summed magnification of the left three images is smaller than the invariant 1. With this simple lens system, we study the situations where a point source infinitely approaches a cusp or a fold. The sum of the magnifications of the cusp image triplet is usually not equal to 0, and it is usually positive for major cusps while negative for minor cusps. Similarly, the sum of magnifications of the fold image pair is usually not equal to 0 either. Nevertheless, the cusp and fold relations are still equal to 0 in that the sum values are divided by infinite absolute magnifications by definition.

  3. SAMPLE RESULTS FROM THE INTEGRATED SALT DISPOSITION PROGRAM MACROBATCH 4 TANK 21H QUALIFICATION SAMPLES

    SciTech Connect (OSTI)

    Peters, T.; Fink, S.

    2011-06-22

    Savannah River National Laboratory (SRNL) analyzed samples from Tank 21H to qualify them for use in the Integrated Salt Disposition Program (ISDP) Batch 4 processing. All sample results agree with expectations based on prior analyses where available. No issues with the projected Salt Batch 4 strategy are identified. This revision includes additional data points that were not available in the original issue of the document, such as additional plutonium results, the results of the monosodium titanate (MST) sorption test and the extraction, scrub strip (ESS) test. This report covers the revision to the Tank 21H qualification sample results for Macrobatch (Salt Batch) 4 of the Integrated Salt Disposition Program (ISDP). A previous document covers initial characterization which includes results for a number of non-radiological analytes. These results were used to perform aluminum solubility modeling to determine the hydroxide needs for Salt Batch 4 to prevent the precipitation of solids. Sodium hydroxide was then added to Tank 21 and additional samples were pulled for the analyses discussed in this report. This work was specified by Task Technical Request and by Task Technical and Quality Assurance Plan (TTQAP).

  4. Analytic Torsion of Z_2-graded Elliptic Complexes

    E-Print Network [OSTI]

    Varghese Mathai; Siye Wu

    2010-04-10

    We define analytic torsion of Z_2-graded elliptic complexes as an element in the graded determinant line of the cohomology of the complex, generalizing most of the variants of Ray-Singer analytic torsion in the literature. It applies to a myriad of new examples, including flat superconnection complexes, twisted analytic and twisted holomorphic torsions, etc. The definition uses pseudo-differential operators and residue traces. We also study properties of analytic torsion for Z_2-graded elliptic complexes, including the behavior under variation of the metric. For compact odd dimensional manifolds, the analytic torsion is independent of the metric, whereas for even dimensional manifolds, a relative version of the analytic torsion is independent of the metric. Finally, the relation to topological field theories is studied.

  5. Analytic Torsion of Z_2-graded Elliptic Complexes

    E-Print Network [OSTI]

    Mathai, Varghese

    2010-01-01

    We define analytic torsion of Z_2-graded elliptic complexes as an element in the graded determinant line of the cohomology of the complex, generalizing most of the variants of Ray-Singer analytic torsion in the literature. It applies to a myriad of new examples, including flat superconnection complexes, twisted analytic and twisted holomorphic torsions, etc. The definition uses pseudo-differential operators and residue traces. We also study properties of analytic torsion for Z_2-graded elliptic complexes, including the behavior under variation of the metric. For compact odd dimensional manifolds, the analytic torsion is independent of the metric, whereas for even dimensional manifolds, a relative version of the analytic torsion is independent of the metric. Finally, the relation to topological field theories is studied.

  6. Mathematica and Fortran programs for various analytic QCD couplings

    E-Print Network [OSTI]

    Cesar Ayala; Gorazd Cvetic

    2014-11-06

    We outline here the motivation for the existence of analytic QCD models, i.e., QCD frameworks in which the running coupling $A(Q^2)$ has no Landau singularities. The analytic (holomorphic) coupling $A(Q^2)$ is the analog of the underlying pQCD coupling $a(Q^2) \\equiv \\alpha_s(Q^2)/\\pi$, and any such $A(Q^2)$ defines an analytic QCD model. We present the general construction procedure for the couplings $A_{\

  7. Analytical Craftsmanship-Evaluation and Analysis of Consumer Perceptions

    E-Print Network [OSTI]

    Papalambros, Panos

    Analytical Craftsmanship- Evaluation and Analysis of Consumer Perceptions by Lara J. Sherefkin ingredients of good interior design pretty much down pat: ergonomics, safety, functionality and convenience

  8. Analytical Development and Support Presentation for BETO 2015...

    Office of Energy Efficiency and Renewable Energy (EERE) Indexed Site

    * Bt-D. Pretreatment Processing Timeline Budget Barriers * Rapid prediction models and analytical work facilitated partnerships with: * INL * Shell * Toyota * DuPont *...

  9. Waste Treatment and Immobilization Plant (WTP) Analytical Laboratory...

    Office of Environmental Management (EM)

    2 Technology Readiness Assessment for the Waste Treatment and Immobilization Plant (WTP) Analytical Laboratory, Balance of Facilities and LAW Waste Vitrification Facilities L....

  10. Analytical Modeling At Lightning Dock Geothermal Area (Brook...

    Open Energy Info (EERE)

    Geothermal Area Exploration Technique Analytical Modeling Activity Date 1978 Usefulness useful DOE-funding Unknown Exploration Basis Assessing the accessible energy in known...

  11. OCIO Technology Summit: Data Analytics | Department of Energy

    Broader source: Energy.gov (indexed) [DOE]

    Cyber Innovation OCIO Technology Summit: Data Analytics OCIO Technology Summit: High Performance Computing SunShot Grand Challenge Summit: Bright Outlook to Achieve SunShot Goal...

  12. Biodiesel Utilization: Update on Recent Analytical Techniques (Presentation)

    SciTech Connect (OSTI)

    Alleman, T. L.; Fouts, L.; Luecke, J.; Thornton, M.; McAlpin, C.

    2009-05-01

    To understand and increase the use of biodiesel, analytical methods need to be shared and compared to ensure that accurate data are gathered on this complex fuel.

  13. An Analytical Framework for Long Term Policy for Commercial Deployment...

    Open Energy Info (EERE)

    An Analytical Framework for Long Term Policy for Commercial Deployment and Innovation in Carbon Capture and Sequestration Technology in the United States Jump to: navigation,...

  14. Visual Analytics for Roof Savings Calculator Ensembles

    SciTech Connect (OSTI)

    Jones, Chad [University of California, Davis] [University of California, Davis; New, Joshua Ryan [ORNL] [ORNL; Sanyal, Jibonananda [ORNL] [ORNL; Ma, Kwan-Liu [University of California, Davis] [University of California, Davis

    2012-01-01

    The Roof Savings Calculator (RSC) has been deployed for DOE as an industry-consensus, web-based tool for easily running complex building energy simulations. These simulations allow both homeowners and experts to determine building-specific cost and energy savings for modern roof and attic technologies. Using a database of over 3 million RSC simulations for different combinations of parameters, we have built a visual analytics tool to assist in the exploration and identification of features in the data. Since the database contains multiple variables, both categorical and continuous, we employ a coordinated multi-view approach that allows coordinated feature exploration through multiple visualizations at once. The main component of our system, a parallel coordinates view, has been adapted to handle large-scale, mixed data types as are found in RSC simulations. Other visualizations include map coordinated plots, high dynamic range (HDR) line plot rendering, and an intuitive user interface. We demonstrate these techniques with several use cases that have helped identify software and parametric simulation issues.

  15. Analytic torsion, vortices and positive Ricci curvature

    E-Print Network [OSTI]

    Berman, Robert J

    2010-01-01

    We characterize the global maximizers of a certain non-local functional defined on the space of all positively curved metrics on an ample line bundle L over a Kahler manifold X. This functional is an adjoint version, introduced by Berndtsson, of Donaldson's L-functional and generalizes the Ding-Tian functional whose critical points are Kahler-Einstein metrics of positive Ricci curvature. Applications to (1) analytic torsions on Fano manifolds (2) Chern-Simons-Higgs vortices on tori and (3) Kahler geometry are given. In particular, proofs of conjectures of (1) Gillet-Soul\\'e and Fang (concerning the regularized determinant of Dolbeault Laplacians on the two-sphere) (2) Tarantello and (3) Aubin (concerning Moser-Trudinger type inequalities) in these three settings are obtained. New proofs of some results in Kahler geometry are also obtained, including a lower bound on Mabuchi's K-energy and the uniqueness result for Kahler-Einstein metrics on Fano manifolds of Bando-Mabuchi. This paper is a substantially extend...

  16. Data Intensive Architecture for Scalable Cyber Analytics

    SciTech Connect (OSTI)

    Olsen, Bryan K.; Johnson, John R.; Critchlow, Terence J.

    2011-12-19

    Cyber analysts are tasked with the identification and mitigation of network exploits and threats. These compromises are difficult to identify due to the characteristics of cyber communication, the volume of traffic, and the duration of possible attack. In this paper, we describe a prototype implementation designed to provide cyber analysts an environment where they can interactively explore a month’s worth of cyber security data. This prototype utilized On-Line Analytical Processing (OLAP) techniques to present a data cube to the analysts. The cube provides a summary of the data, allowing trends to be easily identified as well as the ability to easily pull up the original records comprising an event of interest. The cube was built using SQL Server Analysis Services (SSAS), with the interface to the cube provided by Tableau. This software infrastructure was supported by a novel hardware architecture comprising a Netezza TwinFin® for the underlying data warehouse and a cube server with a FusionIO drive hosting the data cube. We evaluated this environment on a month’s worth of artificial, but realistic, data using multiple queries provided by our cyber analysts. As our results indicate, OLAP technology has progressed to the point where it is in a unique position to provide novel insights to cyber analysts, as long as it is supported by an appropriate data intensive architecture.

  17. Guided Text Search Using Adaptive Visual Analytics

    SciTech Connect (OSTI)

    Steed, Chad A; Symons, Christopher T; Senter, James K; DeNap, Frank A

    2012-10-01

    This research demonstrates the promise of augmenting interactive visualizations with semi- supervised machine learning techniques to improve the discovery of significant associations and insights in the search and analysis of textual information. More specifically, we have developed a system called Gryffin that hosts a unique collection of techniques that facilitate individualized investigative search pertaining to an ever-changing set of analytical questions over an indexed collection of open-source documents related to critical national infrastructure. The Gryffin client hosts dynamic displays of the search results via focus+context record listings, temporal timelines, term-frequency views, and multiple coordinate views. Furthermore, as the analyst interacts with the display, the interactions are recorded and used to label the search records. These labeled records are then used to drive semi-supervised machine learning algorithms that re-rank the unlabeled search records such that potentially relevant records are moved to the top of the record listing. Gryffin is described in the context of the daily tasks encountered at the US Department of Homeland Security s Fusion Center, with whom we are collaborating in its development. The resulting system is capable of addressing the analysts information overload that can be directly attributed to the deluge of information that must be addressed in the search and investigative analysis of textual information.

  18. Laser fusion and glass forming of high iron bearing SiO2-CaO-Fe2O3 batches (Fusin y vitrificacin por lser de vidrios SiO2-CaO-Fe2O3 con altas cantidades de hierro)

    E-Print Network [OSTI]

    Vásquez, Carlos

    , 90 sec. Apparent density of samples: 1,93 & 2,11 gr. /cm3 Laser CO2 RefractoryBrick Mirror Laser CO2, showing a rippling phenomenon. It was possible to take advantage of this foaming effect for separating pressing of 5 gr samples Precharge: 5 ton, 1 min. Charge: 15, 20, 25 and 30 ton, 3 min Exposure to Laser CO

  19. Deep Sludge Gas Release Event Analytical Evaluation

    SciTech Connect (OSTI)

    Sams, Terry L.

    2013-08-15

    Long Abstract. Full Text. The purpose of the Deep Sludge Gas Release Event Analytical Evaluation (DSGRE-AE) is to evaluate the postulated hypothesis that a hydrogen GRE may occur in Hanford tanks containing waste sludges at levels greater than previously experienced. There is a need to understand gas retention and release hazards in sludge beds which are 200 -300 inches deep. These sludge beds are deeper than historical Hanford sludge waste beds, and are created when waste is retrieved from older single-shell tanks (SST) and transferred to newer double-shell tanks (DST).Retrieval of waste from SSTs reduces the risk to the environment from leakage or potential leakage of waste into the ground from these tanks. However, the possibility of an energetic event (flammable gas accident) in the retrieval receiver DST is worse than slow leakage. Lines of inquiry, therefore, are (1) can sludge waste be stored safely in deep beds; (2) can gas release events (GRE) be prevented by periodically degassing the sludge (e.g., mixer pump); or (3) does the retrieval strategy need to be altered to limit sludge bed height by retrieving into additional DSTs? The scope of this effort is to provide expert advice on whether or not to move forward with the generation of deep beds of sludge through retrieval of C-Farm tanks. Evaluation of possible mitigation methods (e.g., using mixer pumps to release gas, retrieving into an additional DST) are being evaluated by a second team and are not discussed in this report. While available data and engineering judgment indicate that increased gas retention (retained gas fraction) in DST sludge at depths resulting from the completion of SST 241-C Tank Farm retrievals is not expected and, even if gas releases were to occur, they would be small and local, a positive USQ was declared (Occurrence Report EM-RP--WRPS-TANKFARM-2012-0014, "Potential Exists for a Large Spontaneous Gas Release Event in Deep Settled Waste Sludge"). The purpose of this technical report is to (1) present and discuss current understandings of gas retention and release mechanisms for deep sludge in U.S. Department of Energy (DOE) complex waste storage tanks; and (2) to identify viable methods/criteria for demonstrating safety relative to deep sludge gas release events (DSGRE) in the near term to support the Hanford C-Farm retrieval mission. A secondary purpose is to identify viable methods/criteria for demonstrating safety relative to DSGREs in the longer term to support the mission to retrieve waste from the Hanford Tank Farms and deliver it to the Waste Treatment and Immobilization Plant (WTP). The potential DSGRE issue resulted in the declaration of a positive Unreviewed Safety Question (USQ). C-Farm retrievals are currently proceeding under a Justification for Continued Operation (JCO) that only allows tanks 241-AN-101 and 241-AN-106 sludge levels of 192 inches and 195 inches, respectively. C-Farm retrievals need deeper sludge levels (approximately 310 inches in 241-AN-101 and approximately 250 inches in 241-AN-106). This effort is to provide analytical data and justification to continue retrievals in a safe and efficient manner.

  20. PHYLOGENOMICS AND POPULATION GENOMICS: MODDELS, ALGORITHMS, AND ANALYTICAL TOOLS

    E-Print Network [OSTI]

    Rosenberg, Noah

    PHYLOGENOMICS AND POPULATION GENOMICS: MODDELS, ALGORITHMS, AND ANALYTICAL TOOLS LUAY K. NAKHLEH on relationships among species themselves. The two fields share a number of overlapping tools, as well as similar analytical tools for assessing properties of the algorithms. We are pleased to present five papers

  1. Analytic Verification at NASA A View from the Trenches

    E-Print Network [OSTI]

    Jipsen, Peter

    Analytic Verification at NASA A View from the Trenches Willem C. Visser July 31, 1999 Autonomous software is considered a major enabling technology for NASA in order to achieve the goal of their slogan Software Engineering 2 (ASE) group at NASA Ames Research Center is developing analytic verification

  2. Sol-gel matrices for direct colorimetric detection of analytes

    DOE Patents [OSTI]

    Charych, Deborah H. (Albany, CA); Sasaki, Darryl (Albuquerque, NM); Yamanaka, Stacey (Dallas, TX)

    2000-01-01

    The present invention relates to methods and compositions for the direct detection of analytes using color changes that occur in immobilized biopolymeric material in response to selective binding of analytes to their surface. In particular, the present invention provides methods and compositions related to the encapsulation of biopolymeric material into metal oxide glass using the sol-gel method.

  3. Using analytic continuation for the hadronic vacuum polarization computation

    SciTech Connect (OSTI)

    Feng, Xu; Hashimoto, Shoji; Hotzel, Grit; Jansen, Karl; Petschlies, Marcus; Renner Dru B

    2014-11-01

    We present two examples of applications of the analytic continuation method for computing the hadronic vacuum polarization function in space- and time-like momentum regions. These examples are the Adler function and the leading order hadronic contribution to the muon anomalous magnetic moment. We comment on the feasibility of the analytic continuation method and provide an outlook for possible further applications.

  4. The Building Adapter: Towards Quickly Applying Building Analytics at Scale

    E-Print Network [OSTI]

    Weimer, Westley

    The Building Adapter: Towards Quickly Applying Building Analytics at Scale Dezhi Hong1 , Hongning}@virginia.edu, jjortiz@us.ibm.com ABSTRACT Building analytics can produce substantial energy savings in commercial buildings by automatically detecting waste- ful or incorrect operations. However, a new building's sens- ing

  5. Pulse propagation in tapered granular chains: An analytic study

    E-Print Network [OSTI]

    Upendra Harbola; Alexandre Rosas; Massimiliano Esposito; Katja Lindenberg

    2009-05-27

    We study pulse propagation in one-dimensional tapered chains of spherical granules. Analytic results for the pulse velocity and other pulse features are obtained using a binary collision approximation. Comparisons with numerical results show that the binary collision approximation provides quantitatively accurate analytic results for these chains.

  6. Micro-Architecture Independent Analytical Processor Performance and Power Modeling

    E-Print Network [OSTI]

    Eeckhout, Lieven

    Micro-Architecture Independent Analytical Processor Performance and Power Modeling Sam Van den models that allow us to produce performance and power estimates across a large design space almost models. In this work we present a micro-architecture independent profiler and associated analytical

  7. PSERC 98-21 "Analytic and Experimentally-Derived

    E-Print Network [OSTI]

    PSERC 98-21 "Analytic and Experimentally-Derived Estimates of Market Power in Deregulated, January 5-8, 1999nd "Analytic and Experimentally-Derived Estimates of Market Power in Deregulated constraints or load characteristics, or retail customers facing suppliers or marketing agents having more than

  8. Business Analytics: The Past, Present and Future of

    E-Print Network [OSTI]

    Grossmann, Ignacio E.

    Tepper School of Business, Carnegie Mellon University 1 #12;THE PAST 2 #12;Example 1: A New Model? Sensitivity Implement Solution 14 #12;The Business Analytics Process Identify a Problem Formulate a Model Data Embed data process in model 15 #12;Operations Research/Business Analytics It is really what

  9. How Policy Analytics Leads to Changes "in the Culture"

    E-Print Network [OSTI]

    of Boats to Boat Stations ·Container Inspection at Ports ·Sports Stadium Security ·Nuclear DetectionHow Policy Analytics Leads to Changes "in the Culture": Examples from "Homeland Security" Fred security ·In each case, policy analytics (data-driven modeling and simulation) led to changes in policy

  10. Existing technology transfer report: analytical capabilities. Volume 1

    SciTech Connect (OSTI)

    Tewari, K.C.

    1984-06-01

    The overall objective of the on-going analytical efforts was to develop in-house expertise and analytical capability for the analysis of coal and coal-derived products in support of SRC-I process technology. The approach taken and work accomplished involved: identification of test methods and associated equipment; review and implementation of analytical facility plan; evaluation of existing instrumentation; evaluation and purchase of new instruments; training of laboratory personnel; validation or development of analytical methods; development of standard product work-up methods; and development of analytical protocol for detailed characterization of SRC-I solid and liquid products. Expertise in analytical chemistry was developed by organizing historical knowledge and assimilating new knowledge as it became available from inside and outside research facilities and the chemical literature. The data were then used to define analytical methods, instrumentation, space, staff needed to create a functional coal analysis laboratory. This report summarizes the direction and progress of the analytical development efforts during the period 1974 to 1980. 2 references, 5 figures.

  11. Analytical extraction of the recombination zone location in organic

    E-Print Network [OSTI]

    Tessler, Nir

    Analytical extraction of the recombination zone location in organic light-emitting diodes from emission patterns produced by organic LEDs (OLEDs). The method is based on derivation of the closed-form expressions for OLED-radiated power developed in previous work and formulation of the analytical relations

  12. ANALYTICAL CHEMISTRY AND MEASUREMENT SCIENCE (What Has DOE Done For Analytical Chemistry?) CONF-8904181--1

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    AFDC Printable Version Share this resource Send a link to EERE: Alternative Fuels Data Center Home Page to someone by E-mail Share EERE: Alternative Fuels Data Center Home Page on Facebook Tweet about EERE: Alternative Fuels Data Center Home Page on Twitter Bookmark EERE: Alternative Fuels Data Center Homesum_a_epg0_fpd_mmcf_m.xls" ,"Available from WebQuantity ofkandz-cm11 Outreach HomeA Better Anode Design to Improve4AJ01) (See Energy Level79AJ01)19^560AMERICA'S, . - - ANALYTICAL

  13. Analytical Chemistry Laboratory progress report for FY 1985

    SciTech Connect (OSTI)

    Green, D.W.; Heinrich, R.R.; Jensen, K.J.

    1985-12-01

    The Analytical Chemistry Laboratory is a full-cost-recovery service center, with the primary mission of providing a broad range of technical support services to the scientific and engineering programs at ANL. In addition, ACL conducts a research program in analytical chemistry, works on instrumental and methods development, and provides analytical services for governmental, educational, and industrial organizations. The ACL handles a wide range of analytical problems, from routine standard analyses to unique problems that require significant development of methods and techniques. The purpose of this report is to summarize the technical and administrative activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year 1985 (October 1984 through September 1985). This is the second annual report for the ACL. 4 figs., 1 tab.

  14. Existing technology transfer report: analytical capabilities. Appendix B. Volume 3

    SciTech Connect (OSTI)

    Tewari, K.C.

    1984-06-01

    The overall objective of the on-going analytical efforts was to develop in-house expertise and analytical capability for the analysis of coal and coal-derived products in support of SRC-I process technology. The approach taken and work accomplished involved: identification of test methods and associated equipment; review and implementation of analytical facility plan; evaluation of existing instrumentation; evaluation and purchase of new instruments; training of laboratory personnel; validation or development of analytical methods; development of standard product work-up methods and development of analytical protocol for detailed characterization of SRC-I solid and liquid products. This volume contains Appendix B with the following attachments: solvent separation procedure A; Wilsonville solvent separation procedure, distillation separation procedure; solvent separation modified Wilsonville Procedure W; statistical comparison of 3 solvent separation procedures; methods development for column chromatography, and application of gas chromatography to characterization of a hydrogen donor solvent; and high performance liquid chromatographic procedure.

  15. Analytical Characterization of the Thorium Nitrate Stockpile

    SciTech Connect (OSTI)

    Mattus, CH

    2003-12-30

    For several years, Oak Ridge National Laboratory (ORNL) has been supporting the Defense Logistics Agency-Defense National Stockpile Center with stewardship of a thorium nitrate (ThN) stockpile. The effort for fiscal year 2002 was to prepare a sampling and analysis plan and to use the activities developed in the plan to characterize the ThN stockpile. The sampling was performed in June and July 2002 by RWE NUKEM with oversight by ORNL personnel. The analysis was performed by Southwest Research Institute of San Antonio, Texas, and data validation was performed by NFT, Inc., of Oak Ridge, Tennessee. Of the {approx} 21,000 drums in the stockpile, 99 were sampled and 53 were analyzed for total metals composition, radiological constituents (using alpha and gamma spectrometry), and oxidizing characteristics. Each lot at the Curtis Bay Depot was sampled. Several of the samples were also analyzed for density. The average density of the domestic ThN was found to be 1.89 {+-} 0.08 g/cm{sup 3}. The oxidizer test was performed following procedures issued by the United Nations in 1999. Test results indicated that none of the samples tested was a Division 5.1 oxidizer per Department of Transportation definition. The samples were analyzed for total metals following the U.S. Environmental Protection Agency methods SW-846-6010B and 6020 (EPA 2003) using a combination of inductively coupled plasma--atomic emission spectroscopy and inductively coupled plasma--mass spectroscopy techniques. The results were used to compare the composition of the eight Resource Conservation and Recovery Act metals present in the sample (arsenic, barium, cadmium, chromium, lead, mercury, selenium, and silver) to regulatory limits. None of the samples was found to be hazardous for toxicity characteristics. The radiological analyses confirmed, when possible, the results obtained by the inductively coupled plasma analyses. These results--combined with the historical process knowledge acquired on the material and the results of previous tests--classified the ThN as low-level radioactive waste for disposal purposes. This characterization was necessary to continue the efforts associated with disposition of the material at the Nevada Test Site, Mercury, Nevada. With the current work presented in this report, the analytical characterization phase is completed for this source material stockpile.

  16. DEVELOPMENT OF AN ANTIFOAM TRACKING SYSTEM AS AN OPTION TO SUPPORT THE MELTER OFF-GAS FLAMMABILITY CONTROL STRATEGY AT THE DWPF

    SciTech Connect (OSTI)

    Edwards, T.; Lambert, D.

    2014-08-27

    The Savannah River National Laboratory (SRNL) has been working with the Savannah River Remediation (SRR) Defense Waste Processing Facility (DWPF) in the development and implementation of an additional strategy for confidently satisfying the flammability controls for DWPF’s melter operation. An initial strategy for implementing the operational constraints associated with flammability control in DWPF was based upon an analytically determined carbon concentration from antifoam. Due to the conservative error structure associated with the analytical approach, its implementation has significantly reduced the operating window for processing and has led to recurrent Slurry Mix Evaporator (SME) and Melter Feed Tank (MFT) remediation. To address the adverse operating impact of the current implementation strategy, SRR issued a Technical Task Request (TTR) to SRNL requesting the development and documentation of an alternate strategy for evaluating the carbon contribution from antifoam. The proposed strategy presented in this report was developed under the guidance of a Task Technical and Quality Assurance Plan (TTQAP) and involves calculating the carbon concentration from antifoam based upon the actual mass of antifoam added to the process assuming 100% retention. The mass of antifoam in the Additive Mix Feed Tank (AMFT), in the Sludge Receipt and Adjustment Tank (SRAT), and in the SME is tracked by mass balance as part of this strategy. As these quantities are monitored, the random and bias uncertainties affecting their values are also maintained and accounted for. This report documents: 1) the development of an alternate implementation strategy and associated equations describing the carbon concentration from antifoam in each SME batch derived from the actual amount of antifoam introduced into the AMFT, SRAT, and SME during the processing of the batch. 2) the equations and error structure for incorporating the proposed strategy into melter off-gas flammability assessments. Sample calculations of the system are also included in this report. Please note that the system developed and documented in this report is intended as an alternative to the current, analytically-driven system being utilized by DWPF; the proposed system is not intended to eliminate the current system. Also note that the system developed in this report to track antifoam mass in the AMFT, SRAT, and SME will be applicable beyond just Sludge Batch 8. While the model used to determine acceptability of the SME product with respect to melter off-gas flammability controls must be reassessed for each change in sludge batch, the antifoam mass tracking methodology is independent of sludge batch composition and as such will be transferable to future sludge batches.

  17. Analytical and micromagnetic study of a Neel domain wall 

    E-Print Network [OSTI]

    Rivkin, K.; Romanov, K.; Abanov, Artem; Adamov, Y.; Saslow, W. M.

    2008-01-01

    For ferromagnets with exchange, dipolar interaction, and uniaxial anisotropy, by both analytic methods and micromagnetic simulations we study Neel domain walls in thin ferromagnetic strips of finite width. Comparison of the numerical results...

  18. Analytics for Power Grid Distribution Reliability in New York City

    E-Print Network [OSTI]

    Rudin, Cynthia

    We summarize the first major effort to use analytics for preemptive maintenance and repair of an electrical distribution network. This is a large-scale multiyear effort between scientists and students at Columbia University ...

  19. Data Analytics Methods in Wind Turbine Design and Operations 

    E-Print Network [OSTI]

    Lee, Giwhyun

    2013-05-22

    This dissertation develops sophisticated data analytic methods to analyze structural loads on, and power generation of, wind turbines. Wind turbines, which convert the kinetic energy in wind into electrical power, are operated within stochastic...

  20. Shimadzu Center for Advanced Analytical Chemistry Instrument Description

    E-Print Network [OSTI]

    Chrzanowski, Thomas H.

    Shimadzu Center for Advanced Analytical Chemistry Instrument Description LCMS-8080 High PerformanceImagingandDocumentation Instrument Fall 2013 Allegra 25R Beckman Coulter Refrigerated Centrifuge Fall 2013 Center for Environmental

  1. Analytical study of a control algorithm based on emotional processing 

    E-Print Network [OSTI]

    Chandra, Manik

    2007-04-25

    Dennis L. O?Neal December 2005 Major Subject: Mechanical Engineering iii ABSTRACT Analytical Study of a Control Algorithm Based on Emotional Processing. (December 2005) Manik Chandra, B. Tech., Indian Institute of Technology Kanpur...

  2. Interlaboratory Analytical Comparison Study to Support Deepwater Horizon

    E-Print Network [OSTI]

    R. Kucklick Analytical Chemistry Division Material Measurement Laboratory National Institute tissue QA10TIS01 reported here. In this exercise, selected polycyclic aromatic hydrocarbons (PAHs have collected environmental samples for hydrocarbon analysis and submitted them to different

  3. Towards Building an Analytics Platform in the Cloud

    E-Print Network [OSTI]

    Kim, Minkyong

    the barrier for the creation, deployment, scaling and maintenance of next generation analytic workloads and manufacturing, into optimization of logistic processes such as supply chain operations, and to human centric

  4. Motion planning with an analytic risk cost for holonomic vehicles

    E-Print Network [OSTI]

    Hover, Franz S.

    We present a robust motion planning algorithm for a holonomic mobile robot that incorporates the risk of collisions directly in the cost function. This deterministic algorithm uses analytic predictions of the path-following ...

  5. Analytical modeling of contaminant transport and horizontal well hydraulics 

    E-Print Network [OSTI]

    Park, Eungyu

    2004-09-30

    transport from one-, two-, and three-dimensional finite sources in a finite-thickness aquifer using Green's function method. A library of unpublished analytical solutions with different finite source geometry is provided. A graphically integrated software...

  6. Arithmetic and analytic properties of finite field hypergeometric functions

    E-Print Network [OSTI]

    Lennon, Catherine (Catherine Ann)

    2011-01-01

    The intent of this thesis is to provide a detailed study of the arithmetic and analytic properties of Gaussian (finite field) hypergeometric series. We present expressions for the number of F,-points on certain families ...

  7. A Novel Analytical Model for Flexure-based Proportion Compliant

    E-Print Network [OSTI]

    Li, Yangmin

    A Novel Analytical Model for Flexure-based Proportion Compliant Mechanisms Qiaoling Meng Yangmin model for flexure-based proportion compliant mechanisms. The displacement and stiffness calculations geometric and material properties of the compliant mechanism. Displacement proportion, input stiffness

  8. Light trapping limits in plasmonic solar cells: an analytical investigation

    E-Print Network [OSTI]

    Sheng, Xing

    We analytically investigate the light trapping performance in plasmonic solar cells with Si/metallic structures. We consider absorption enhancements for surface plasmon polaritons (SPPs) at planar Si/metal interfaces and ...

  9. IT Project Prioritization Leveraging the Analytical Hierarchy Process (AHP)

    E-Print Network [OSTI]

    Freeze, Eric P.

    2015-12-18

    is to develop and exercise an Analytical Hierarchy Process (AHP) model that aids in project prioritization. The AHP is a mathematical decision-making tool that helps standardize the decision-making process while bringing transparency and defensibility...

  10. Probing metal nanoparticles and assemblies with analytical ultracentrifugation

    E-Print Network [OSTI]

    Carney, Randy (Randy Patrick)

    2010-01-01

    Analytical Ultracentrifugation (AUC) is a powerful tool to obtain statistically relevant size and shape measurements for macromolecular systems. Metal nanoparticles coated by a ligand shell of thiolated molecules provide ...

  11. Big Data Big Talent The Master's in Business Analytics program starting Spring 2015 is designed to

    E-Print Network [OSTI]

    Huang, Haiying

    Business Analytics Big Data Big Talent The Master's in Business Analytics program starting Spring Intelligence Web and Social Analytics Big Data Analytics Python for Data Analytics Forecasting Applied 2015 is designed to create an empowered workforce that understands how data - regardless of size

  12. Analytics over Large-Scale Multidimensional Data: The Big Data Revolution!

    E-Print Network [OSTI]

    Song, Il-Yeol

    Analytics over Large-Scale Multidimensional Data: The Big Data Revolution! Alfredo Cuzzocrea ICAR in the field of analytics over big data, and we extend the discussion to analytics over big multidimensional, Management, Performance, Theory Keywords Analytics over Big Data, Analytics over Big Multidimensional Data

  13. Ultrasonic analyte concentration and application in flow cytometry

    DOE Patents [OSTI]

    Kaduchak, Gregory (Los Alamos, NM); Goddard, Greg (Los Alamos, NM); Salzman, Gary (White Rock, NM); Sinha, Dipen (Los Alamos, NM); Martin, John C. (Los Alamos, NM); Kwiatkowski, Christopher (Los Alamos, NM); Graves, Steven (San Juan Pueblo, NM)

    2008-03-11

    The present invention includes an apparatus and corresponding method for concentrating analytes within a fluid flowing through a tube using acoustic radiation pressure. The apparatus includes a function generator that outputs a radio frequency electrical signal to a transducer that transforms the radio frequency electric signal to an acoustic signal and couples the acoustic signal to the tube. The acoustic signal is converted within the tube to acoustic pressure that concentrates the analytes within the fluid.

  14. Ultrasonic analyte concentration and application in flow cytometry

    DOE Patents [OSTI]

    Kaduchak, Gregory; Goddard, Greg; Salzman, Gary; Sinha, Dipen; Martin, John C.; Kwiatkowski, Christopher; Graves, Steven

    2014-07-22

    The present invention includes an apparatus and corresponding method for concentrating analytes within a fluid flowing through a tube using acoustic radiation pressure. The apparatus includes a function generator that outputs a radio frequency electrical signal to a transducer that transforms the radio frequency electric signal to an acoustic signal and couples the acoustic signal to the tube. The acoustic signal is converted within the tube to acoustic pressure that concentrates the analytes within the fluid.

  15. Analytical Chemistry Laboratory Progress Report for FY 1994

    SciTech Connect (OSTI)

    Green, D.W.; Boparai, A.S.; Bowers, D.L. [and others

    1994-12-01

    The purpose of this report is to summarize the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year (FY) 1994 (October 1993 through September 1994). This annual report is the eleventh for the ACL and describes continuing effort on projects, work on new projects, and contributions of the ACL staff to various programs at ANL. The Analytical Chemistry Laboratory is a full-cost-recovery service center, with the primary mission of providing a broad range of analytical chemistry support services to the scientific and engineering programs at ANL. The ACL also has a research program in analytical chemistry, conducts instrumental and methods development, and provides analytical services for governmental, educational, and industrial organizations. The ACL handles a wide range of analytical problems. Some routine or standard analyses are done, but it is common for the Argonne programs to generate unique problems that require significant development of methods and adaption of techniques to obtain useful analytical data. The ACL has four technical groups -- Chemical Analysis, Instrumental Analysis, Organic Analysis, and Environmental Analysis -- which together include about 45 technical staff members. Talents and interests of staff members cross the group lines, as do many projects within the ACL. The Chemical Analysis Group uses wet- chemical and instrumental methods for elemental, compositional, and isotopic determinations in solid, liquid, and gaseous samples and provides specialized analytical services. Major instruments in this group include an ion chromatograph (IC), an inductively coupled plasma/atomic emission spectrometer (ICP/AES), spectrophotometers, mass spectrometers (including gas-analysis and thermal-ionization mass spectrometers), emission spectrographs, autotitrators, sulfur and carbon determinators, and a kinetic phosphorescence uranium analyzer.

  16. Ultrasonic analyte concentration and application in flow cytometry

    DOE Patents [OSTI]

    Kaduchak, Gregory; Goddard, Greg; Salzman, Gary; Sinha, Dipen; Martin, John C.; Kwiatkowski, Christopher; Graves, Steven

    2015-07-07

    The present invention includes an apparatus and corresponding method for concentrating analytes within a fluid flowing through a tube using acoustic radiation pressure. The apparatus includes a function generator that outputs a radio frequency electrical signal to a transducer that transforms the radio frequency electric signal to an acoustic signal and couples the acoustic signal to the tube. The acoustic signal is converted within the tube to acoustic pressure that concentrates the analytes within the fluid.

  17. Quality assurance management plan (QAPP) special analytical support (SAS)

    SciTech Connect (OSTI)

    LOCKREM, L.L.

    1999-05-20

    It is the policy of Special Analytical Support (SAS) that the analytical aspects of all environmental data generated and processed in the laboratory, subject to the Environmental Protection Agency (EPA), U.S. Department of Energy or other project specific requirements, be of known and acceptable quality. It is the intention of this QAPP to establish and assure that an effective quality controlled management system is maintained in order to meet the quality requirements of the intended use(s) of the data.

  18. Analytical Chemistry Laboratory. Progress report for FY 1996

    SciTech Connect (OSTI)

    Green, D.W.; Boparai, A.S.; Bowers, D.L.

    1996-12-01

    The purpose of this report is to summarize the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year (FY) 1996. This annual report is the thirteenth for the ACL. It describes effort on continuing and new projects and contributions of the ACL staff to various programs at ANL. The ACL operates in the ANL system as a full-cost-recovery service center, but has a mission that includes a complementary research and development component: The Analytical Chemistry Laboratory will provide high-quality, cost-effective chemical analysis and related technical support to solve research problems of our clients -- Argonne National Laboratory, the Department of Energy, and others -- and will conduct world-class research and development in analytical chemistry and its applications. Because of the diversity of research and development work at ANL, the ACL handles a wide range of analytical chemistry problems. Some routine or standard analyses are done, but the ACL usually works with commercial laboratories if our clients require high-volume, production-type analyses. It is common for ANL programs to generate unique problems that require significant development of methods and adaption of techniques to obtain useful analytical data. Thus, much of the support work done by the ACL is very similar to our applied analytical chemistry research.

  19. Statistically qualified neuro-analytic failure detection method and system

    DOE Patents [OSTI]

    Vilim, Richard B. (Aurora, IL); Garcia, Humberto E. (Idaho Falls, ID); Chen, Frederick W. (Naperville, IL)

    2002-03-02

    An apparatus and method for monitoring a process involve development and application of a statistically qualified neuro-analytic (SQNA) model to accurately and reliably identify process change. The development of the SQNA model is accomplished in two stages: deterministic model adaption and stochastic model modification of the deterministic model adaptation. Deterministic model adaption involves formulating an analytic model of the process representing known process characteristics, augmenting the analytic model with a neural network that captures unknown process characteristics, and training the resulting neuro-analytic model by adjusting the neural network weights according to a unique scaled equation error minimization technique. Stochastic model modification involves qualifying any remaining uncertainty in the trained neuro-analytic model by formulating a likelihood function, given an error propagation equation, for computing the probability that the neuro-analytic model generates measured process output. Preferably, the developed SQNA model is validated using known sequential probability ratio tests and applied to the process as an on-line monitoring system. Illustrative of the method and apparatus, the method is applied to a peristaltic pump system.

  20. Theory and Applications of NMR to Problems in Material Science and Analytical Chemistry

    E-Print Network [OSTI]

    Agarwal, Arun

    2010-01-01

    in the field of analytical chemistry and material science isin Material Science and Analytical Chemistry A Dissertation490. Van Geet, A. L. Analytical Chemistry 1970, 42, 679-680.

  1. Novel Analytical Methods for Examining Biomolecular Complexes Using Electrospray Ionization Mass Spectrometry

    E-Print Network [OSTI]

    Flick, Tawnya Grace

    2012-01-01

    Annual Review of Analytical Chemistry; Annual Reviews: PaloD. ; Aebersold, R. Analytical Chemistry 2000, 72, 1112-1118.S. ; Amster, I. J. Analytical Chemistry 2006, 78, 3417-3423.

  2. Content Development Policy: Chemical Engineering & Analytical Science 1 The University of Manchester Library

    E-Print Network [OSTI]

    Abrahams, I. David

    Content Development Policy: Chemical Engineering & Analytical Science 1 The University of Manchester Library Content Development Policy Chemical Engineering & Analytical Science Monday, 30 April 2012 Contents Content Development Policy Chemical Engineering & Analytical Science

  3. Characterization of solids deposited on the modular caustic-side solvent extraction unit (MCU) coalescer media removed in May and October 2014

    SciTech Connect (OSTI)

    Fondeur, F. F.

    2015-10-01

    During routine maintenance, the coalescers utilized in the Modular Caustic-Side Solvent Extraction Unit (MCU) processing of Salt Batch 6 and a portion of Salt Batch 7 were sampled and submitted to the Savannah River National Laboratory (SRNL) for characterization, for the purpose of identifying solid phase constituents that may be accumulating in these coalescers. Specifically, two samples were received and characterized: A decontaminated salt solution (DSS) coalescer sample and a strip effluent (SE) coalescer sample. Aliquots of the samples were analyzed by XRD, Fourier Transform Infrared (FTIR) Spectroscopy, SEM, and EDS. Other aliquots of the samples were leached in acid solution, and the leachates were analyzed by ICP-AES. In addition, modeling was performed to provide a basis for comparison of the analytical results.

  4. SAMPLE RESULTS FROM THE INTEGRATED SALT DISPOSITION PROGRAM MACROBATCH 5 TANK 21H QUALIFICATION MST, ESS AND PODD SAMPLES

    SciTech Connect (OSTI)

    Peters, T.; Fink, S.

    2012-04-24

    Savannah River National Laboratory (SRNL) performed experiments on qualification material for use in the Integrated Salt Disposition Program (ISDP) Batch 5 processing. This qualification material was a composite created from recent samples from Tank 21H and archived samples from Tank 49H to match the projected blend from these two tanks. Additionally, samples of the composite were used in the Actinide Removal Process (ARP) and extraction-scrub-strip (ESS) tests. ARP and ESS test results met expectations. A sample from Tank 21H was also analyzed for the Performance Objectives Demonstration Document (PODD) requirements. SRNL was able to meet all of the requirements, including the desired detection limits for all the PODD analytes. This report details the results of the Actinide Removal Process (ARP), Extraction-Scrub-Strip (ESS) and Performance Objectives Demonstration Document (PODD) samples of Macrobatch (Salt Batch) 5 of the Integrated Salt Disposition Program (ISDP).

  5. Analytical Chemistry Laboratory progress report for FY 1984

    SciTech Connect (OSTI)

    Green, D.W.; Heinrich, R.R.; Jensen, K.J.; Stetter, J.R.

    1985-03-01

    Technical and administrative activities of the Analytical Chemistry Laboratory (ACL) are reported for fiscal year 1984. The ACL is a full-cost-recovery service center, with the primary mission of providing a broad range of technical support services to the scientific and engineering programs at ANL. In addition, ACL conducts a research program in analytical chemistry, works on instrumental and methods development, and provides analytical services for governmental, educational, and industrial organizations. The ACL is administratively within the Chemical Technology Division, the principal user, but provides technical support for all of the technical divisions and programs at ANL. The ACL has three technical groups - Chemical Analysis, Instrumental Analysis, and Organic Analysis. Under technical activities 26 projects are briefly described. Under professional activities, a list is presented for publications and reports, oral presentations, awards and meetings attended. 6 figs., 2 tabs.

  6. Infrared freezing of Euclidean observables and analyticity in perturbative QCD

    E-Print Network [OSTI]

    Irinel Caprini; Jan Fischer

    2006-12-21

    The renormalization-group improved finite order expansions of the QCD observables have an unphysical singularity in the Euclidean region, due to the Landau pole of the running coupling. Recently it was claimed that, by using a modified Borel representation, the leading one-chain term in a skeleton expansion of the Euclidean QCD observables is finite and continuous across the Landau pole, and then exhibits an infrared freezing behaviour, vanishing at $Q^2=0$. In the present paper we show, using for illustration the Adler-${\\cal D}$ function, that the above Borel prescription violates the causality properties expressed by energy-plane analyticity: the function ${\\cal D}(Q^2)$ thus defined is the boundary value of a piecewise analytic function in the complex plane, instead of being a standard analytic function. So, the price to be paid for the infrared freezing of Euclidean QCD observables is the loss of a fundamental property of local quantum field theory.

  7. Semi-analytic results for quasi-normal frequencies

    E-Print Network [OSTI]

    Skakala, Jozef

    2010-01-01

    The last decade has seen considerable interest in the quasi-normal frequencies [QNFs] of black holes (and even wormholes), both asymptotically flat and with cosmological horizons. There is wide agreement that the QNFs are often of the form omega_n = (offset) + i n (gap), though some authors have encountered situations where this behaviour seems to fail. To get a better understanding of the general situation we consider a semi-analytic model based on a piecewise Eckart (Poeschl--Teller) potential, allowing for different heights and different rates of exponential falloff in the two asymptotic directions. This model is sufficiently general to capture and display key features of the black hole QNFs while simultaneously being analytically tractable, at least for asymptotically large imaginary parts of the QNFs. We shall derive an appropriate "quantization condition" for the asymptotic QNFs, and extract as much analytic information as possible. In particular, we shall explicitly verify that the (offset)+ i n (gap) ...

  8. Web-based Visual Analytics for Extreme Scale Climate Science

    SciTech Connect (OSTI)

    Steed, Chad A [ORNL; Evans, Katherine J [ORNL; Harney, John F [ORNL; Jewell, Brian C [ORNL; Shipman, Galen M [ORNL; Smith, Brian E [ORNL; Thornton, Peter E [ORNL; Williams, Dean N. [Lawrence Livermore National Laboratory (LLNL)

    2014-01-01

    In this paper, we introduce a Web-based visual analytics framework for democratizing advanced visualization and analysis capabilities pertinent to large-scale earth system simulations. We address significant limitations of present climate data analysis tools such as tightly coupled dependencies, ineffi- cient data movements, complex user interfaces, and static visualizations. Our Web-based visual analytics framework removes critical barriers to the widespread accessibility and adoption of advanced scientific techniques. Using distributed connections to back-end diagnostics, we minimize data movements and leverage HPC platforms. We also mitigate system dependency issues by employing a RESTful interface. Our framework embraces the visual analytics paradigm via new visual navigation techniques for hierarchical parameter spaces, multi-scale representations, and interactive spatio-temporal data mining methods that retain details. Although generalizable to other science domains, the current work focuses on improving exploratory analysis of large-scale Community Land Model (CLM) and Community Atmosphere Model (CAM) simulations.

  9. Analytical effective tensor for flow-through composites

    DOE Patents [OSTI]

    Sviercoski, Rosangela De Fatima (Los Alamos, NM)

    2012-06-19

    A machine, method and computer-usable medium for modeling an average flow of a substance through a composite material. Such a modeling includes an analytical calculation of an effective tensor K.sup.a suitable for use with a variety of media. The analytical calculation corresponds to an approximation to the tensor K, and follows by first computing the diagonal values, and then identifying symmetries of the heterogeneity distribution. Additional calculations include determining the center of mass of the heterogeneous cell and its angle according to a defined Cartesian system, and utilizing this angle into a rotation formula to compute the off-diagonal values and determining its sign.

  10. Random free fermions: An analytical example of eigenstate thermalization

    E-Print Network [OSTI]

    Magan, Javier M

    2015-01-01

    Having analytical instances of the Eigenstate Thermalization Hypothesis (ETH) is of obvious interest, both for fundamental and applied reasons. This is generically a hard task, due to the belief that non-linear interactions are basic ingredients of the thermalization mechanism. In this article we proof that random gaussian free fermions satisfy ETH in the multiparticle sector, by analytically computing the correlations and entanglement entropies of the theory. With the explicit construction at hand, we finally comment on the differences between fully random Hamiltonians and random Gaussian systems, and on the connection between chaotic energy spectra and ETH.

  11. Analytic calculation of 1-jettiness in DIS at O (?s)

    DOE Public Access Gateway for Energy & Science Beta (PAGES Beta)

    Kang, Daekyoung; Los Alamos National Lab.; Lee, Christopher; Stewart, Iain W.

    2014-11-24

    We present an analytic O(?s) calculation of cross sections in deep inelastic scattering (DIS) dependent on an event shape, 1-jettiness, that probes final states with one jet plus initial state radiation. This is the first entirely analytic calculation for a DIS event shape cross section at this order. We present results for the differential and cumulative 1-jettiness cross sections, and express both in terms of structure functions dependent not only on the usual DIS variables x, Q 2 but also on the 1-jettiness ?. Combined with previous results for log resummation, predictions are obtained over the entire range of themore »1-jettiness distribution.« less

  12. anQCD: Fortran programs for couplings at complex momenta in various analytic QCD models

    E-Print Network [OSTI]

    Ayala, Cesar

    2015-01-01

    We provide three Fortran programs which evaluate the QCD analytic (holomorphic) couplings $\\mathcal{A}_{\

  13. Extended Analytical Physics 1, 750:116 Spring Semester 2015

    E-Print Network [OSTI]

    Gustafsson, Torgny

    or life in general. Reading Completed by Reading Physics the First Science (T) Pages College Physics (OExtended Analytical Physics 1, 750:116 Spring Semester 2015 Course Web Home Page: http://www.physics Learning Center Tel. (848) 445-8757 Tel. (848) 445-3123 Email: brahmia@physics.rutgers.edu Workshop Leaders

  14. Analytical chemistry methods for metallic core components: Revision March 1985

    SciTech Connect (OSTI)

    Not Available

    1985-03-01

    This standard provides analytical chemistry methods for the analysis of alloys used to fabricate core components. These alloys are 302, 308, 316, 316-Ti, and 321 stainless steels and 600 and 718 Inconels and they may include other 300-series stainless steels.

  15. Deepest Regression in Analytical Chemistry P. J. Rousseeuw,a

    E-Print Network [OSTI]

    Van Aelst, Stefan

    Deepest Regression in Analytical Chemistry P. J. Rousseeuw,a , S. Van Aelst,a , B. Rambalib , and J Recently the concept of regression depth has been introduced [1]. The deepest regression (DR) is a method for linear regression which is defined as the fit with the best depth relative to the data. In this paper we

  16. 100-K Target Analyte List Development for Soil

    SciTech Connect (OSTI)

    Ovink, R.

    2012-09-18

    This report documents the process used to identify source area target analytes in support of the 100-K Area remedial investigation/feasibility study (RI/FS) addendum to the Integrated 100 Area Remedial Investigation/Feasibility Study Work Plan (DOE/RL-2008-46, Rev. 0).

  17. Risk Analytics for Estimating and Validating Magnitude of Earthquake Losses

    E-Print Network [OSTI]

    Rau-Chaplin, Andrew

    Risk Analytics for Estimating and Validating Magnitude of Earthquake Losses A. Astoul, C. Filliter-time estimation and visualisation of insured losses incurred due to earthquakes is presented. The system incorporates a model for estimating losses due to earthquakes in near real-time and a geo

  18. Analytic design and solutions for resonance domain diffractive optical elements

    E-Print Network [OSTI]

    Friesem, Asher A.

    Analytic design and solutions for resonance domain diffractive optical elements Michael A. Golub. INTRODUCTION Diffractive optical elements (DOEs) are usually designed and characterized with scalar diffraction, 2006 (Doc. ID 72721); published February 14, 2007 A model for designing and analyzing complicated

  19. Analytical Target Cascading in Aircraft Design James Allison(1)

    E-Print Network [OSTI]

    Papalambros, Panos

    preliminary design. Top level system targets are cascaded through all elements in the hierarchy element design specifications have been obtained, the individual design tasks may be completedAnalytical Target Cascading in Aircraft Design James Allison(1) , David Walsh(2) , Michael

  20. Interlaboratory Analytical Comparison Study to Support Deepwater Horizon

    E-Print Network [OSTI]

    . Kucklick Analytical Chemistry Division Material Measurement Laboratory National Institute of Standards, crude oil QA10OIL01 reported here. In this exercise, selected polycyclic aromatic hydrocarbons (PAHs will be required. In addition, numerous other entities have collected environmental samples for hydrocarbon

  1. Interlaboratory Analytical Comparison Study to Support Deepwater Horizon

    E-Print Network [OSTI]

    and John R. Kucklick Analytical Chemistry Division Material Measurement Laboratory National Institute, marine sediment QA10SED01 reported here. In this exercise, selected polycyclic aromatic hydrocarbons for hydrocarbon analysis and submitted them to different laboratories throughout the country. In the past

  2. The case against specialized graph analytics engines University of Wisconsin

    E-Print Network [OSTI]

    Willett, Rebecca

    the performance perspec- tive. We present Grail ­ a syntactic layer for querying graph in a vertex-centric way compare Grail to GraphLab and Giraph, and examine the performance implications of using Grail, showing.e. Grail) that presents such a syntactic mapping layer. We present how graph analytics queries using

  3. Analytical Chemistry Laboratory progress report for FY 1999

    SciTech Connect (OSTI)

    Green, D. W.; Boparai, A. S.; Bowers, D. L.; Graczyk, D. G.

    2000-06-15

    This report summarizes the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year (FY) 1999 (October 1998 through September 1999). This annual progress report, which is the sixteenth in this series for the ACL, describes effort on continuing projects, work on new projects, and contributions of the ACL staff to various programs at ANL.

  4. Analytical Chemistry Laboratory progress report for FY 1998.

    SciTech Connect (OSTI)

    Boparai, A. S.; Bowers, D. L.; Graczyk, D. G.; Green, D. W.; Lindahl, P. C.

    1999-03-29

    This report summarizes the activities of the Analytical Chemistry Laboratory (ACL) at Argonne National Laboratory (ANL) for Fiscal Year (FY) 1998 (October 1997 through September 1998). This annual progress report, which is the fifteenth in this series for the ACL, describes effort on continuing projects, work on new projects, and contributions of the ACL staff to various programs at ANL.

  5. "Machine learning for big data analytics in biomedicine"

    E-Print Network [OSTI]

    Zhigilei, Leonid V.

    "Machine learning for big data analytics in biomedicine" Yanjun (Jane) Qi Assistant Professor yq2h-learning techniques on important challenges in biomedicine, especially those dealing with enormous data sets. Taking on Data Mining (ICDM) · Y. Qi, et al,(2009) "Systematic prediction of human membrane receptor interactions

  6. FIELDS WITH ANALYTIC STRUCTURE 1. Introduction We begin ...

    E-Print Network [OSTI]

    2008-04-17

    that comprises, to our knowledge, all principle, previously studied, analytic structures on Henselian ... subject matter of this paper and thank the University of Leuven and Purdue University for support ..... Since this is a fundamental property, and the ideas of the proof are .... These terms can be handled by induction on n. D.

  7. Proportional Fair Scheduling: Analytical Insight under Rayleigh Fading Environment

    E-Print Network [OSTI]

    Leung, Kin K.

    Proportional Fair Scheduling: Analytical Insight under Rayleigh Fading Environment Erwu Liu and Kin to the constraint of proportional fairness amongst users. The proportional fair scheduling (PFS) algorithm, but also it applies to various kinds of network scenarios. Keywords-proportional fair scheduling, gaussian

  8. Analytical Analysis of Data and Decision Fusion in Sensor Networks

    E-Print Network [OSTI]

    Terwilliger, Mark

    Analytical Analysis of Data and Decision Fusion in Sensor Networks Zille Huma Kamal, Mohammad Ali Michigan University Kalamazoo, MI, USA Abstract - MEMS technology has improved such that the capabilities of large sensor devices can now be encompassed in devices that are the size of a penny. These resource

  9. Analytic Results for Higgs Production in Bottom Fusion

    E-Print Network [OSTI]

    Kemal J. Ozeren

    2010-10-14

    We evaluate analytically the cross section for Higgs production plus one jet through bottom quark fusion. By considering the small pT limit we derive expressions for the resummation coefficients governing the structure of large logarithms, and compare these expressions with those available in the literature.

  10. 100-F Target Analyte List Development for Soil

    SciTech Connect (OSTI)

    Ovink, R.

    2012-09-18

    This report documents the process used to identify source area target analytes in support of the 100-F Area remedial investigation/feasibility study (RI/FS) addendum to the Integrated 100 Area Remedial Investigation/Feasibility Study Work Plan (DOE/RL-2008-46, Rev. 0).

  11. Decision Analytic Modelling in the Economic Evaluation of

    E-Print Network [OSTI]

    Oakley, Jeremy

    Decision Analytic Modelling in the Economic Evaluation of Health Technologies A Consensus Statement when used for the economic evaluation of health technologies; there is limited guidanceforgoodmodelling developed in the context of broader healthcare and economic evaluations, for which ex- plicit guidelines

  12. Letters to Analytical Chemistry Heat-Associated Field Distortion in

    E-Print Network [OSTI]

    Krylov, Sergey

    for Research on Biomolecular Interactions, York University, Toronto, Ontario M3J 1P3, Canada Electro is a well pronounced phenomenon that can be a potential source of errors and instabilities in electro.) are moved by an electric field in an electrolyte, are widely used in analytical sciences.1 Electro- phoresis

  13. Integrating Renewable Energy Using Data Analytics Systems: Challenges and Opportunities

    E-Print Network [OSTI]

    California at Berkeley, University of

    Integrating Renewable Energy Using Data Analytics Systems: Challenges and Opportunities Andrew and intermittent nature of many renewable energy sources makes integrating them into the electric grid challenging-following loads adjust their power consumption to match the avail- able renewable energy supply. We show Internet

  14. A fundamental study on analyte adsorption onto metallophthalocyanines

    E-Print Network [OSTI]

    Tran, Ngoc L.

    2008-01-01

    MD simulations for the ZnPc-TEA complex. Finally, N.L. Trananalyte E FePc E FePc=analyte TEA TMA TMP UHV US-PP VASP vs.Schematic of the lowest energy, optimized TEA-ZnPc binding

  15. ELECTROMOTION 2009 3D Analytical Calculation of Forces between

    E-Print Network [OSTI]

    Paris-Sud XI, Université de

    Co or NdFeB, the designers can use magnets owning a really rigid magnetization. They are the magnets whichELECTROMOTION 2009 1 3D Analytical Calculation of Forces between Linear Halbach-Type Permanent Magnet Arrays H. Allag1,2 , J-P. Yonnet1 and M. E. H. Latreche2 1- Laboratoire de Génie Electrique de

  16. Groundwater Management Tools: Analytical Procedure and Case Studies

    E-Print Network [OSTI]

    Hickman, Mark

    Groundwater Management Tools: Analytical Procedure and Case Studies MAF Technical Paper No: 2003 and Forestry #12;i Contents Page Executive Summary v Introduction 1 Section A ­ Groundwater Management: Best 2 2.2. Groundwater Budgets 2 2.3. Dynamic Storage 2 3. Scale of Abstraction Effects 3 4. Limitations

  17. Harmonic Functions are Real Analytic1 On this very short note we prove that harmonic functions are real analytic functions.

    E-Print Network [OSTI]

    Cabral, Marco

    Harmonic Functions are Real Analytic1 On this very short note we prove that harmonic functions prove Lemma 1 using the mean value property of harmonic functions, Green's theorem and the maximum principle. Lemma 1 (estimate on first derivative) Suppose w is harmonic in Rn , > 0, y and B

  18. Analytical and semi-analytical solutions of horizontal well capture times under no-ow and constant-head boundaries

    E-Print Network [OSTI]

    Zhan, Hongbin

    for oil and gas production in the past decade [15,21]. Extensive studies on pressure anal- ysis-head. The third scenario is recovery from a low-permeability layer bounded above and below by much higher developed analytical solutions of the transient and steady-state gas pressure and the steady-state stream

  19. Direct-Contact Process Water Heating 

    E-Print Network [OSTI]

    Hamann, M. R.

    2006-01-01

    Frequency Days/yr Annual Vol. (mcf) % A1 Batch 90,500 lbs per batch 4 batches/week 80,681 0.6% A2 Batch 200,000 lbs per batch 3 batches/day 200 2,139,594 15.4% Filters (50,000 lbs/hr/filter) 2 Sewer 50,000 lbs/hr/filter 18 hrs/day 200 6,418,781 46....1% Filters (25,000 lbs/hr/filter) 1 Sewer 25,000 lbs/hr/filter 19 hrs/day 200 1,604,695 11.5% Drum Washers 3 Sewer 25,000 lbs/hr/filter 20 hrs/day 150 3,610,564 26.0% Wet Scrubbers 4 Sewer 1 gpm/scrubber 21 hrs/day 200 57,615 0.4% 13,911,930 ANALYSIS...

  20. Analytical Modelling of a Plucked Piezoelectric Bimorph for Energy Harvesting

    E-Print Network [OSTI]

    Pozzi, Michele

    2012-01-01

    Energy harvesting (EH) is a multidisciplinary research area, involving physics, materials science and engineering, with the objective of providing renewable sources of sufficient power to operate targeted low-power applications. Piezoelectric transducers are often used for vibrational, inertial and direct movement EH. One problem is that, due to the stiffness of the most common material (PZT) and typically useful sizes, intrinsic resonant frequencies are normally high, whereas the available power is often concentrated at low frequencies. The aim of the plucking technique of frequency up-conversion, also known as "pizzicato" excitation, is to bridge this frequency gap. In this paper, the technique is modelled analytically. The analytical model is developed starting from the Euler-Bernoulli beam equations modified for piezoelectric coupling. A system of differential equations and associated initial conditions are derived which describe the free vibration of a piezoelectric bimorph in the last part of the plucki...

  1. Analytic models of supercomputer performance in multiprogramming environments

    SciTech Connect (OSTI)

    Menasce, D.A. ); Almeida, V.A.F. )

    1989-01-01

    Supercomputers run multiprogrammed time-sharing operating systems, so their facilities can be shared by many local and remote users. Therefore, it is important to be able to assess the performance of supercomputers and multiprogrammed environments. Analytic models based on Queueing Networks (QNs) and Stochastic Petri Nets (SPNs) are used in this paper with two purposes: to evaluate the performance of supercomputers in multiprogrammed environments, and to compare, performance-wise, conventional supercomputer architectures with a novel architecture proposed here. It is shown, with the aid of the analytic models, that the proposed architecture is preferable performance-wise over the existing conventional supercomputer architectures. A three-level workload characterization model for supercomputers is presented. Input data for the numerical examples discussed here are extracted from the well-known Los Alamos benchmark, and the results are validated by simulation.

  2. Analytical calculation of neutral transport and its effect on ions

    SciTech Connect (OSTI)

    Calvin, M.D.; Hazeltine, R.D.; Valanju, P.M.; Solano, E.R. (Texas Univ., Austin, TX (USA). Inst. for Fusion Studies Texas Univ., Austin, TX (USA). Fusion Research Center)

    1991-06-01

    We analytically calculate the neutral particle distribution and its effects on ion heat and momentum transport in three-dimensional plasmas with arbitrary temperature and density profiles. A general variational principle taking advantage of the simplicity of the charge-exchange (CX) operator is derived to solve self-consistently the neutral-plasma interaction problem. To facilitate an extremal solution, we use the short CX mean-free-path ({lambda}{sub x}) ordering. Further, a non-variational, analytical solution providing a full set of transport coefficient is derived by making the realistic assumption that the product of the CX cross section with relative velocity is constant. The effects of neutrals on plasma energy loss and rotation appear in simple, sensible forms. We find that neutral viscosity dominates ion viscosity everywhere, and in the edge region by a large factor. 13 refs.

  3. SciDAC Visualization and Analytics Center for Enabling Technologies

    SciTech Connect (OSTI)

    Joy, Kenneth I.

    2014-09-14

    This project focuses on leveraging scientific visualization and analytics software technology as an enabling technology for increasing scientific productivity and insight. Advances in computational technology have resulted in an "information big bang," which in turn has created a significant data understanding challenge. This challenge is widely acknowledged to be one of the primary bottlenecks in contemporary science. The vision for our Center is to respond directly to that challenge by adapting, extending, creating when necessary and deploying visualization and data understanding technologies for our science stakeholders. Using an organizational model as a Visualization and Analytics Center for Enabling Technologies (VACET), we are well positioned to be responsive to the needs of a diverse set of scientific stakeholders in a coordinated fashion using a range of visualization, mathematics, statistics, computer and computational science and data management technologies.

  4. Quantitative analytical model for magnetic reconnection in hall magnetohydrodynamics

    SciTech Connect (OSTI)

    Simakov, Andrei N

    2008-01-01

    Magnetic reconnection is of fundamental importance for laboratory and naturally occurring plasmas. Reconnection usually develops on time scales which are much shorter than those associated with classical collisional dissipation processes, and which are not fully understood. While such dissipation-independent (or 'fast') reconnection rates have been observed in particle and Hall magnetohydrodynamics (MHD) simulations and predicted analytically in electron MHD, a quantitative analytical theory of fast reconnection valid for arbitrary ion inertial lengths d{sub i} has been lacking. Here we propose such a theory without a guide field. The theory describes two-dimensional magnetic field diffusion regions, provides expressions for the reconnection rates, and derives a formal criterion for fast reconnection in terms of dissipation parameters and di. It also demonstrates that both open X-point and elongated diffusion regions allow dissipation-independent reconnection and reveals a possibility of strong dependence of the reconnection rates on d{sub i}.

  5. Quality control and statistical process control for nuclear analytical measurements

    SciTech Connect (OSTI)

    Seymour, R.; Sergent, F.; Clark, W.H.C.; Gleason, G.

    1993-12-31

    The same driving forces that are making businesses examine quality control of manufacturing processes are making laboratories reevaluate their quality control programs. Increased regulation (accountability), global competitiveness (profitability), and potential for litigation (defensibility) are the principal driving forces behind the development and implementation of QA/QC programs in the nuclear analytical laboratory. Both manufacturing and scientific quality control can use identical statistical methods, albeit with some differences in the treatment of the measured data. Today, the approaches to QC programs are quite different for most analytical laboratories as compared with manufacturing sciences. This is unfortunate because the statistical process control methods are directly applicable to measurement processes. It is shown that statistical process control methods can provide many benefits for laboratory QC data treatment.

  6. Analytic expression for poloidal flow velocity in the banana regime

    SciTech Connect (OSTI)

    Taguchi, M. [College of Industrial Technology, Nihon University, Narashino 275-8576 (Japan)

    2013-01-15

    The poloidal flow velocity in the banana regime is calculated by improving the l = 1 approximation for the Fokker-Planck collision operator [M. Taguchi, Plasma Phys. Controlled Fusion 30, 1897 (1988)]. The obtained analytic expression for this flow, which can be used for general axisymmetric toroidal plasmas, agrees quite well with the recently calculated numerical results by Parker and Catto [Plasma Phys. Controlled Fusion 54, 085011 (2012)] in the full range of aspect ratio.

  7. MAR flow mapping of Analytical Chemistry Operations (Preliminary Report)

    SciTech Connect (OSTI)

    Barr, Mary E. [Los Alamos National Laboratory; Farish, Thomas J. [Los Alamos National Laboratory

    2012-06-13

    The recently released Supplemental Directive, NA-1 SD 1027, updates the radionuclide threshold values in DOE-STD-1027-92 CN1 to reflect the use of modern parameters for dose conversion factors and breathing rates. The directive also corrects several arithmetic errors within the original standard. The result is a roughly four-fold increase in the amount of weapons-grade nuclear material allowed within a designated radiological facility. Radiological laboratory space within the recently constructed Radiological Laboratory Office and Utility Building (RLUOB) is slated to house selected analytical chemistry support activities in addition to small-scale actinide R&D activities. RLUOB is within the same facility operations envelope as TA-55. Consolidation of analytical chemistry activities to RLUOB and PF-4 offers operational efficiency improvements relative to the current pre-CMRR plans of dividing these activities between RLUOB, PF-4, and CMR. RLUOB is considered a Radiological Facility under STD-1027 - 'Facilities that do not meet or exceed Category 3 threshold criteria but still possess some amount of radioactive material may be considered Radiological Facilities.' The supplemental directive essentially increases the allowable material-at-risk (MAR) within radiological facilities from 8.4 g to 38.6 g for {sup 239}Pu. This increase in allowable MAR provides a unique opportunity to establish additional analytical chemistry support functions in RLUOB without negatively impacting either R&D activities or facility operations. Individual radiological facilities are tasked to determine MAR limits (up to the Category 3 thresholds) appropriate to their operational conditions. This study presents parameters that impact establishing MAR limits for RLUOB and an assessment of how various analytical chemistry support functions could operate within the established MAR limits.

  8. Experimental and Analytical Research on Fracture Processes in ROck

    SciTech Connect (OSTI)

    Herbert H.. Einstein; Jay Miller; Bruno Silva

    2009-02-27

    Experimental studies on fracture propagation and coalescence were conducted which together with previous tests by this group on gypsum and marble, provide information on fracturing. Specifically, different fracture geometries wsere tested, which together with the different material properties will provide the basis for analytical/numerical modeling. INitial steps on the models were made as were initial investigations on the effect of pressurized water on fracture coalescence.

  9. SRC-I Demonstration Plant Analytical Laboratory. Final technical report

    SciTech Connect (OSTI)

    Hamilton, R.F.; Klusaritz, M.; Maroulis, P.J.; Moyer, J.D.; Parees, D.M.; Skinner, R.W.; Sydlik, E.; Tewari, K.C.; Tiedge, W.F.; Znaimer, S.

    1983-09-01

    This report describes planning and methods development activities to establish an SRC-I Coal Liquefaction Demonstration Plant analytical laboratory. Laboratory requirements are listed and methods qualification/development activities are described for the following areas: microanalytical carbon, hydrogen, chlorine, nitrogen, and sulfur procedures; ash determination; GC/MS and GC/FID analyses; metals analyses; and GC-simulated distillation. 2 references, 64 figures, 108 tables.

  10. Math 151 -Practice Exam 2 Problem 1 Find dy

    E-Print Network [OSTI]

    that the unit price of manufacturing x batches of paper towels is p(x) = 412 - 1 3 x2 #12;(a) What answer in part (b) to approximate the additional revenue from selling 2 extra batches in addition of manufacturing x batches of flibbertigibbets is p(x) = 20.1 - 0.02x and the total cost is C(x) = 150 + 0.1x. (a

  11. JOVIAN STRATOSPHERE AS A CHEMICAL TRANSPORT SYSTEM: BENCHMARK ANALYTICAL SOLUTIONS

    SciTech Connect (OSTI)

    Zhang Xi; Shia Runlie; Yung, Yuk L.

    2013-04-20

    We systematically investigated the solvable analytical benchmark cases in both one- and two-dimensional (1D and 2D) chemical-advective-diffusive systems. We use the stratosphere of Jupiter as an example but the results can be applied to other planetary atmospheres and exoplanetary atmospheres. In the 1D system, we show that CH{sub 4} and C{sub 2}H{sub 6} are mainly in diffusive equilibrium, and the C{sub 2}H{sub 2} profile can be approximated by modified Bessel functions. In the 2D system in the meridional plane, analytical solutions for two typical circulation patterns are derived. Simple tracer transport modeling demonstrates that the distribution of a short-lived species (such as C{sub 2}H{sub 2}) is dominated by the local chemical sources and sinks, while that of a long-lived species (such as C{sub 2}H{sub 6}) is significantly influenced by the circulation pattern. We find that an equator-to-pole circulation could qualitatively explain the Cassini observations, but a pure diffusive transport process could not. For slowly rotating planets like the close-in extrasolar planets, the interaction between the advection by the zonal wind and chemistry might cause a phase lag between the final tracer distribution and the original source distribution. The numerical simulation results from the 2D Caltech/JPL chemistry-transport model agree well with the analytical solutions for various cases.

  12. Focused analyte spray emission apparatus and process for mass spectrometric analysis

    DOE Patents [OSTI]

    Roach, Patrick J. (Kennewick, WA); Laskin, Julia (Richland, WA); Laskin, Alexander (Richland, WA)

    2012-01-17

    An apparatus and process are disclosed that deliver an analyte deposited on a substrate to a mass spectrometer that provides for trace analysis of complex organic analytes. Analytes are probed using a small droplet of solvent that is formed at the junction between two capillaries. A supply capillary maintains the droplet of solvent on the substrate; a collection capillary collects analyte desorbed from the surface and emits analyte ions as a focused spray to the inlet of a mass spectrometer for analysis. The invention enables efficient separation of desorption and ionization events, providing enhanced control over transport and ionization of the analyte.

  13. Life-Cycle Assessment of Concrete: Decision-Support Tool and Case Study Application

    E-Print Network [OSTI]

    Gursel, Aysegul Petek

    2014-01-01

    waste from concrete batching involves mixer washout, sludgesof washout, the volume of returned concrete, and the amountwashout, truck wash off, etc. ) for ready-mixed concrete

  14. Search for: All records | SciTech Connect

    Office of Scientific and Technical Information (OSTI)

    using second-harmonic generation (SHG) imaging and X-ray powder diffraction and (iv) production of millilitres of rhodopsin crystal suspension in batches for serial...

  15. The Impact of Control Technology on the Demand Response Potential of California Industrial Refrigerated Facilities Final Report

    E-Print Network [OSTI]

    Scott, Doug

    2014-01-01

    Finished goods freezing Automatic plate Cryogenic PreparedFinished goods freezing Batch cabinet Cryogenic Processedgoods freezing Straight spiral belt Cryogenic Prepared food

  16. Li and Mn uptake data from initial set of imprinted polymers

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Susanna Ventura

    2015-03-27

    Batch tests of crosslinked lithium and manganese imprinted polymers of variable composition to assess their ability to extract lithium and manganese from synthetic brines at T=45C .

  17. Estudiossobrebiodegradacindemicrocontaminantesorgnicosemergentes Estudio sobre biodegradacin de

    E-Print Network [OSTI]

    Politècnica de Catalunya, Universitat

    ÍNDICE ANTECEDENTES OBJETIVO LABORATORIO: Ensayos Batch Objetivos específicos. Materiales y metodología 1 pesticidas, fertilizantes, fangos de depuradora en agricultura; efluentes industriales, ganaderos

  18. Summary - Flowsheet for the Hanford Waste Treatment Plant

    Office of Environmental Management (EM)

    and effectiveness of cesium-137 monitoring. The control strategy for the LAW Vitrification Facility will likely lead to mis-batching of melter feed. Difficult to remove...

  19. Uranium Processing Facility Site Readiness Subproject Completed...

    National Nuclear Security Administration (NNSA)

    sediment basin, installation of a vehicle arresting system gate, construction of a new portal, establishment of a concrete batch plant and building the construction support...

  20. Lithium uptake data of lithium imprinted polymers

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Susanna Ventura

    2015-12-04

    Batch tests of lithium imprinted polymers of variable composition to assess their ability to extract lithium from synthetic brines at T=45C. Initial selectivity data are included

  1. PILOT PLANT STUDIES OF THE BIOCONVERSION OF CELLULOSE AND PRODUCTION OF ETHANOL. REPORT OF WORK PROGRESS, JAN. 31, 1977

    E-Print Network [OSTI]

    Wilke, C.R.

    2010-01-01

    investigations of both batch and semicontinuous recycle operations,investigation, it was frequently observed that rapid cellulase production was obtained when continuous operation

  2. March 2, 2010

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    has been heaviest in 6 months, loaded to capacity at times (1000 jobs) Outages: A few problems with some individual batch nodes but otherwise nothing. Upcoming downtimes: None....

  3. 2nd Annual DOE-ERSP PI Meeting: Abstracts

    E-Print Network [OSTI]

    Hazen, Terry C.

    2007-01-01

    that has been resident in Rocky Flats, Colorado, soils for ~Batch incubations of Rocky Flats soils with glucose showstatic columns filled with Rocky Flats soils showed little

  4. Search for: All records | DOE PAGES

    Office of Scientific and Technical Information (OSTI)

    at 48 hours during the five day experiment, concurrent with a shiftmore in amino acid metabolism. We also report that Y. lipolytica secretes disaccharides early in batch...

  5. 4th Annual DOE-ERSP PI Meeting: Abstracts

    E-Print Network [OSTI]

    Hazen, Terry C.

    2009-01-01

    to adhere to hematite and goethite. Two adhesion-deficientUO 2 by ferrihydrite, goethite, and hematite-coated quartzof batch experiments with goethite as the electron acceptor,

  6. OSTI, US Dept of Energy, Office of Scientific and Technical Informatio...

    Office of Scientific and Technical Information (OSTI)

    STIP Product Type AnnouncementTransmission Options Procedure Booksmonographs Web version of AN 241.1 Harvesting (OSTI-to-Site) Batch Upload (Site-to-OSTI) A...

  7. Across the Pond Newsletter Issue 2

    Office of Environmental Management (EM)

    glass processing and throughput. e UK and US have common interests in the thermodynamics and kinetics of glass batch reactions, e ect of melter parameters such as...

  8. This

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Dissolution retardation of solid silica during glass-batch melting Pavel Hrma , Jos Marcial Pacific Northwest National Laboratory, 99352 Richland, Washington, USA a b s t r a...

  9. Using PDSF Job Arrays

    Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

    Using Job Arrays Using Job Arrays Job arrays have many advantages, including reduced load on the batch system, faster job submission, and easier job management. If you find...

  10. Review of the Hanford Site Waste Treatment and Immobilization...

    Broader source: Energy.gov (indexed) [DOE]

    project requirements for entrained air, slump, and temperature. Concrete was sampled for molding of cylinders for unconfined compression testing. Review of the concrete batch...

  11. Understanding colloidal quantum dot excitation with solution photon correlation fourier spectroscopy

    E-Print Network [OSTI]

    Heathcote, S. Leigh (Stephanie Leigh)

    2015-01-01

    Colloidal quantum dots (CQDs) have useful absorption and emission properties but exist in inhomogenous batches. Solution photon correlation fourier spectroscopy (S-PCFS) combines interferometry with fluorescence correlation ...

  12. Testing the ecological stability of ectomycorrhizal symbiosis: effects of heat, ash and mycorrhizal colonization on Pinus muricata seedling performance

    E-Print Network [OSTI]

    Peay, Kabir G.; Bruns, Thomas D.; Garbelotto, Matteo

    2010-01-01

    batch was subjected to heat treatments modified from Izzo etof the seedlings from each heat treatment were then randomlyresults show that heat treatments (which increase mineral N

  13. Li and Mn uptake data from initial set of imprinted polymers

    DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

    Susanna Ventura

    Batch tests of crosslinked lithium and manganese imprinted polymers of variable composition to assess their ability to extract lithium and manganese from synthetic brines at T=45C .

  14. In-Situ Bioremediation of Perchlorate in Groundwater and Soil

    E-Print Network [OSTI]

    Jin, Liyan

    2012-01-01

    2.24 Perchlorate in the leachate from different batch modeto drain. Collected leachate was analyzed for perchlorate,collected in the leachate, little or no perchlorate

  15. Esterification kinetics of triglycerides in n-hexane catalyzed by an immobilized lipase 

    E-Print Network [OSTI]

    Gomez Ruiz, Alejandro

    1998-01-01

    . The reaction was then run in a fixed bed flow reactor and the reactor performance was predicted using the batch reactor kinetics....

  16. Fate of Endogenous Steroid Hormones in Runoff from Cattle Feedlots

    E-Print Network [OSTI]

    Mansell, David Scott

    2012-01-01

    estrogens at activated sludge sewage treatment plants and inestrogens by activated sludge in batch experiments. Waterexperiments with activated sludge. Sci. Total Environ. 225:

  17. Microsoft PowerPoint - Closing Summary_Brian Horn_Pete Dessaules...

    National Nuclear Security Administration (NNSA)

    and obligations - Mission and programmatic planning - Commerce - Safety and health - Licensingcompliance Transmit matching issues, e.g., - Batch ID 2 Summary...

  18. Microsoft PowerPoint - Recent NMSS Interactions with Foreign...

    National Nuclear Security Administration (NNSA)

    - Japan - Taiwan 2 How industry reports an export Example 1, the export of fuel assemblies 3 Number of Lines License Number Header Gross Weight Line Number Batch...

  19. Computational Geosciences Improved Semi-Analytical Simulation of Geological Carbon Sequestration

    E-Print Network [OSTI]

    Bau, Domenico A.

    Computational Geosciences Improved Semi-Analytical Simulation of Geological Carbon Sequestration of Geological Carbon Sequestration Article Type: Manuscript Keywords: Semi-Analytical Modeling; Iterative Methods; Geological Carbon Sequestration; Injection Site Assessment Corresponding Author: Brent Cody

  20. SINGULAR LEVI-FLAT REAL ANALYTIC HYPERSURFACES By DANIEL BURNS and XIANGHONG GONG

    E-Print Network [OSTI]

    Gong, Xianghong

    SINGULAR LEVI-FLAT REAL ANALYTIC HYPERSURFACES By DANIEL BURNS and XIANGHONG GONG Abstract. We #12;24 DANIEL BURNS AND XIANGHONG GONG Let M be a real analytic hypersurface defined by r = 0