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Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
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they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
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1

Small Angle X-Ray Scattering Detector  

DOE Patents [OSTI]

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., qmax/qmin approx=lO0.

Hessler, Jan P.

2004-06-15T23:59:59.000Z

2

Small Angle X-Ray Scattering Detector  

DOE Patents [OSTI]

A detector for time-resolved small-angle x-ray scattering includes a nearly constant diameter, evacuated linear tube having an end plate detector with a first fluorescent screen and concentric rings of first fiber optic bundles for low angle scattering detection and an annular detector having a second fluorescent screen and second fiber optic bundles concentrically disposed about the tube for higher angle scattering detection. With the scattering source, i.e., the specimen under investigation, located outside of the evacuated tube on the tube's longitudinal axis, scattered x-rays are detected by the fiber optic bundles, to each of which is coupled a respective photodetector, to provide a measurement resolution, i.e., dq/q, where q is the momentum transferred from an incident x-ray to an x-ray scattering specimen, of 2% over two (2) orders of magnitude in reciprocal space, i.e., q.sub.max /q.sub.min.congruent.100.

Hessler, Jan P. (Downers Grove, IL)

2004-06-15T23:59:59.000Z

3

Small Angle X-ray Scattering (SAXS) Laboratory Learning Experiences  

E-Print Network [OSTI]

.A. & Svergun D.I. (1987). Structure Analysis by Small-Angle X-Ray and Neutron Scattering. NY: Plenum PressSmall Angle X-ray Scattering (SAXS) Laboratory Learning Experiences o - Use of small angle X-ray scattering instrumentation o - Programs that you will use SAXS (BRUKER AXS) PRIMUS (Konarev, Volkov, Koch

Meagher, Mary

4

E-Print Network 3.0 - angle x-ray scattering Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

2008Standard Operating Procedure Title: Small Angle X-ray Scattering... approved: December 26 2009 Small Angle X-ray Scattering, Rotating Anode PURPOSE: This Standard...

5

Small angle neutron scattering and small angle X-ray scattering studies of platinum-loaded carbon foams  

Science Journals Connector (OSTI)

The morphology of carbon nanofoam samples comprising platinum nanoparticles dispersed in the matrix was characterized by small angle neutron scattering (SANS) and small angle X-ray scattering (SAXS) techniques. R...

P. U. Sastry; V. K. Aswal; A. G. Wagh

2008-11-01T23:59:59.000Z

6

Materials Small-angle X-ray Scattering (SAXS) | Stanford Synchrotron  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Materials Small-angle X-ray Scattering (SAXS) Materials Small-angle X-ray Scattering (SAXS) Small Angle X-ray Scattering for Materials Science Small-angle X-ray scattering (SAXS) is a well-established characterization method for microstructure investigations in various materials. It probes electron density differences to give information about structural inhomogeneities from the near atomic scale (1 nm) to the micron scale (1 000 nm). The method involves measuring the scattered X-ray intensity as a function of (typically small) scattering angles and is generally performed in transmission. SAXS is used to characterize the size scale of inhomogeneities (e.g. pores, inclusions, second phase regions) in polymer blends, micro-emulsions, geological materials, bones, cements and ceramics. Instrumentation

7

Micellar structure from comparison of X-ray and neutron small-angle scattering  

E-Print Network [OSTI]

249 Micellar structure from comparison of X-ray and neutron small-angle scattering T. Zemb and P according to the method developed by Hayter and Penfold. Both X-ray and neutron scattering signals, or by a combination of both. It has been shown recent- ly [1, 2] that it is possible in neutron scattering studies

Boyer, Edmond

8

Analysis of Intrinsically Disordered Proteins by Small-Angle X-ray Scattering  

Science Journals Connector (OSTI)

Small-angle scattering of X-rays (SAXS) is a method for the low-resolution structural characterization of biological macromolecules in solution. The technique is highly complementary to the high-resolution method...

Pau Bernad; Dmitri I. Svergun

2012-01-01T23:59:59.000Z

9

Beyond simple small-angle X-ray scattering: developments in online complementary techniques and sample environments  

Science Journals Connector (OSTI)

Possibilities in auxiliary technique combinations with small- and wide-angle X ray scattering are described, as well as more complicated sample environments used in X-ray and neutron scattering.

Bras, W.

2014-09-23T23:59:59.000Z

10

Investigating increasingly complex macromolecular systems with small-angle X-ray scattering  

Science Journals Connector (OSTI)

A review of recent and ongoing development and results within the field of biological solution small-angle X-ray scattering (BioSAXS), with a focus on the increasing complexity of biological samples, data collection and data evaluation strategies.

Vestergaard, B.

2014-10-21T23:59:59.000Z

11

Small-Angle X-ray Scattering Using Coherent Undulator Radiation at the ESRF  

Science Journals Connector (OSTI)

A high-coherent-flux X-ray beam for small-angle-scattering studies has been produced and analyzed at the Tro?ka beamline of the European Synchrotron Radiation Facility. The statistics of a static speckle pattern are used to characterize the coherence properties.

Abernathy, D.L.

1998-01-01T23:59:59.000Z

12

Wide angle x-ray scattering of proteins : effect of beam exposure on protein integrity.  

SciTech Connect (OSTI)

Wide-angle X-ray scattering patterns from proteins in solution contain information relevant to the determination of protein fold. At relevant scattering angles, however, these data are weak, and the degree to which they might be used to categorize the fold of a protein is unknown. Preliminary work has been performed at the BioCAT insertion-device beamline at the Advanced Photon Source which demonstrates that one can collect X-ray scattering data from proteins in solution to spacings of at least 2.2 {angstrom} (q = 2.8 {angstrom}-1). These data are sensitive to protein conformational states, and are in good agreement with the scattering predicted by the program CRYSOL using the known three-dimensional atomic coordinates of the protein. An important issue in the exploitation of this technique as a tool for structural genomics is the extent to which the high intensity of X-rays available at third-generation synchrotron sources chemically or structurally damage proteins. Various data-collection protocols have been investigated demonstrating conditions under which structural degradation of even sensitive proteins can be minimized, making this technique a viable tool for protein fold categorization, the study of protein folding, unfolding, protein-ligand interactions and domain movement.

Fischetti, R. F.; Rodi, D. J.; Mirza, A.; Makowski, L.; Illinois Inst. of Tech.

2003-01-01T23:59:59.000Z

13

Characterization of porous materials using combined small-angle X-ray and neutron scattering techniques  

SciTech Connect (OSTI)

A combination of ultra small angle X-ray scattering (USAXS) and ultra small angle neutron scattering (USANS) is used to characterize porous materials. The analysis methods yield quantitative information, including the mean skeletal chord length, mean pore chord length, skeletal density, and composition. A mixed cellulose ester (MCE) membrane with a manufacturer-labeled pore size of 0.1 {mu}m was used as a model to elucidate the specifics of the method. Four approaches describing four specific scenarios (different known parameters and form of the scattering data) are compared. Pore chords determined using all four approaches are in good agreement with the scanning electron microscopy estimates but are larger than the manufacturer's nominal pore size. Our approach also gives the average chord of the skeletal solid (struts) of the membrane, which is also consistent for all four approaches. Combined data from USAXS and USANS gives the skeletal density and the strut composition.

Hu, Naiping; Borkar, Neha; Kohls, Doug; Schaefer, Dale W. (UCIN)

2014-09-24T23:59:59.000Z

14

Time Resolved Collapse of a Folding Protein Observed with Small Angle X-Ray Scattering  

SciTech Connect (OSTI)

High-intensity, ''pink'' beam from an undulator was used in conjunction with microfabricated rapid-fluid mixing devices to monitor the early events in protein folding with time resolved small angle x-ray scattering. This Letter describes recent work on the protein bovine {beta} -lactoglobulin where collapse from an expanded to a compact set of states was directly observed on the millisecond time scale. The role of chain collapse, one of the initial stages of protein folding, is not currently understood. The characterization of transient, compact states is vital in assessing the validity of theories and models of the folding process.

Pollack, L.; Tate, M. W.; Finnefrock, A. C.; Kalidas, C.; Trotter, S.; Darnton, N. C.; Lurio, L.; Austin, R. H.; Batt, C. A.; Gruner, S. M. (and others)

2001-05-21T23:59:59.000Z

15

Time-Resolved Small-Angle X-ray Scattering Studies Revealed Three Kinetic  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

June 2010 June 2010 Time-Resolved Small-Angle X-ray Scattering Studies Revealed Three Kinetic Stages of a T=4 Virus Maturation Most eukaryotic viruses, including HIV, influenza and herpes viruses, undergo maturation when transitioning from the noninfectious provirion to the infectious virion. Maturation processes involve reorganization of viral quaternary structure to defend viral gene from the cellular defense mechanism and lead to effective transfection. Nudaurelia capensis omega virus, NwV, is a T=4, non-enveloped, icosahedral, single strand RNA virus, where T is the triangulation number defining an icosahedral lattice of the virus capsid structure. Virus like particles (VLPs) of NwV exhibit large pH-dependent conformational changes (LCC) when the procapsid, purified at pH=7.6, (~480 Å) is exposed to pH=5.0, resulting in ~400 Å particles (Figure 1). In response to the LCC, an auto-proteolysis occurs in which each of 240 subunits is cleaved at Asn570-Phe571 (1). We investigated this pH-induced maturation by equilibrium and time-resolved small angle X-ray scattering (SAXS) at SSRL beam line 4-2.

16

Eur. J. Biochem. 85, 529-534 (1978) X-Ray and Neutron Small-Angle Scattering Studies  

E-Print Network [OSTI]

Eur. J. Biochem. 85, 529-534 (1978) X-Ray and Neutron Small-Angle Scattering Studies of the Complex-ray and neutron scattering techniques. In this work, we concentrated mainly on radius of gyration analyses and a neutron scattering experiment is performed in 21-Iz0 solvent. This decrease simply reflects the fact

17

Characterization of the Binding of Gallium, Platinum, and Uranium to Pseudomonas fluorescens by Small-Angle X-Ray Scattering and Transmission Electron Microscopy  

Science Journals Connector (OSTI)

...that combined small-angle neutron scattering and small-angle X-ray scattering...by small-angle X-ray and neutron scattering. Plenum Press, New York...of biological structures by neutron scattering from solution. Rep. Prog...

Susan Krueger; Gregory J. Olson; David Johnsonbaugh; T. J. Beveridge

1993-12-01T23:59:59.000Z

18

Sodium Humate Solution Studied with Small-Angle X-Ray Scattering  

Science Journals Connector (OSTI)

...Survey, Denver, Colorado 80225 Denver Research Center, Marathon Oil Company, Littleton, Colorado 80120 Small-angle x-ray...L. SUTULA B. J. WIGINTON Denver Research Center, Marathon Oil Company, Littleton, Colorado 80120 The possibility...

R. L. Wershaw; P. J. Burcar; C. L. Sutula; B. J. Wiginton

1967-09-22T23:59:59.000Z

19

Ostwald ripening of cobalt precipitates in silica aerogels? An ultra-small-angle X-ray scattering study  

Science Journals Connector (OSTI)

Silica aerogels were doped with cobalt, reduced, and studied with ultra-small-angle X-ray scattering. A scattering pattern rich in structure extends over nearly four orders of magnitude in q space, covering real space from 5 to 3000 ?, exposing micropores, mesopores and macropores for all aerogels.

Braun, A.

2005-01-19T23:59:59.000Z

20

Small angle neutron and X-ray scattering studies of carbons prepared using inorganic templates  

SciTech Connect (OSTI)

Small angle neutron (SANS) and X-ray (SAXS) scattering analyses of carbons derived from organic-loaded inorganic template materials, used as anodes in lithium ion cells, have been performed. Two clays were used as templates to load the organic precursors, pillared montmorrillonite (PILC), a layered silicate clay whose sheets have been permanently propped open by sets of thermally stable molecular props, and sepiolite, a natural channeled clay. Five different organic precursors were used to load the PILC: pyrene, styrene, pyrene/trioxane copolymer, ethylene and propylene, whereas only propylene and ethylene were used to load sepiolite. Pyrolysis took place at 700{degrees}C under nitrogen. Values such as hole radius, fractal dimension, cutoff length and density of the final carbons will be compared as a function of the clay and carbon precursors.

Sandi, G.; Thiyagarajan, P.; Winans, R.E.; Carrado, K.A.

1997-09-01T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


21

Small-angle x-ray scattering studies on nonionic microemulsions  

Science Journals Connector (OSTI)

The microstructure in a [n-dodecyltetraoxyethylene glycol monoether (C12E4)]-water-hexadecane system was investigated by the small-angle x-ray scattering (SAXS) technique for various surfactant concentrations and solution temperatures at a constant ratio of water and hexadecane (1:1 by weight). At 25 C, a sharp distinct peak was observed in the SAXS curves. On the basis of the analysis of the surfactant concentration dependence of the peak position, it was concluded that a lamella structure had been formed. At 45 C, the scattering curves showed a single, broad peak. With increasing C12E4 concentration, the peak position shifted toward higher angles. An analysis of the peak position suggested that oil-in-water (O-W) -type microemulsion droplets had been formed. At lower surfactant concentrations, the possibilities, that W-O droplets had been formed and that a bicontinuous structure had been constructed at the intermediate concentrations, were pointed out. The scattering profiles were not in contradiction with the theoretical ones for spheres if the polydispersity was considered. From a consideration of the peak position, which is related to the interparticle distance through the Bragg equation, it was suggested that the (spherical) droplets were distributed in a more or less ordered manner, probably in fcc or bcc symmetry, and not in simple-cubic symmetry. The radius and the aggregation number of the droplet were estimated to be about 1317 A? and 351400, respectively, depending on the surfactant concentration.

Tsuyoshi Shimobouji; Hideki Matsuoka; Norio Ise; Hideo Oikawa

1989-04-15T23:59:59.000Z

22

Spatially-resolved small-angle x-ray scattering studies of soot inception and growth.  

SciTech Connect (OSTI)

The high spectral brilliance of x-rays produced at the Basic Energy Sciences Synchrotron Radiation Center of Argonne's Advanced Photon Source allows us to perform small-angle x-ray scattering (SAXS) measurements of the distributions of soot particles in flames. SAXS provides an in situ probe of the size and distribution of particles in the region between 1 and 100 nm. Detailed measurements on a propylene/air diffusion flame allow us to extract a spatially dependent background, which occurs in gas-phase combustion systems, and to perform Abel inversions, which provide the radial dependence of the scattering intensity. A bimodal distribution of soot particles is needed to describe our results. The radial behavior of the two modes of this distribution implies that the chemistry and fluid dynamics are strongly coupled in this simple diffusion flame. The larger particles of this distribution correspond to the previously observed primary particles, which have a relatively complex radial dependence. Midway between the fuel source and the widest part of the flame the primary particles have a mean radius of 6 nm or less and their concentration is symmetrically distributed about the flame front. At the widest part of the flame, two distinct distributions of primary particles are observed. Near the center of the flame the particles have a mean radius of 10 nm and a polydispersity of 0.3 and beyond a transition region they have a mean radius of 21 nm and a polydispersity of 0.2. The smaller particles, which require additional experiments before they can be identified, correspond either to soot nuclei, PAH species such as naphthalene, and/or disordered carbons with graphitic basal planes.

Hessler, J. P.; Seifert, S.; Winans, R. E.

2002-07-17T23:59:59.000Z

23

Studies of protein structure in solution and protein folding using synchrotron small-angle x-ray scattering  

SciTech Connect (OSTI)

Synchrotron small angle x-ray scattering (SAXS) has been applied to the structural study of several biological systems, including the nitrogenase complex, the heat shock cognate protein (hsc70), and lysozyme folding. The structural information revealed from the SAXS experiments is complementary to information obtained by other physical and biochemical methods, and adds to our knowledge and understanding of these systems.

Chen, Lingling

1996-04-01T23:59:59.000Z

24

Contribution of synchrotron radiation to small-angle X-ray scattering studies in hard condensed matter  

Science Journals Connector (OSTI)

Synchrotron radiation, by virtue of its special beam characteristics, has revived interest in small-angle X-ray scattering for hard condensed matter and materials science. New techniques have been developed and new scientific themes tackled, ranging from metallurgy to nanotechnology.

Simon, J.-P.

2007-01-20T23:59:59.000Z

25

Simbol-X Mirror Module Thermal Shields: II-Small Angle X-Ray Scattering Measurements  

SciTech Connect (OSTI)

The formation flight configuration of the Simbol-X mission implies that the X-ray mirror module will be open to Space on both ends. In order to reduce the power required to maintain the thermal stability and, therefore, the high angular resolution of the shell optics, a thin foil thermal shield will cover the mirror module. Different options are presently being studied for the foil material of these shields. We report results of an experimental investigation conducted to verify that the scattering of X-rays, by interaction with the thin foil material of the thermal shield, will not significantly affect the performances of the telescope.

Barbera, M. [Universita degli Studi di Palermo, Dip. di Scienze Fisiche ed Astronomiche, Palermo (Italy); Istituto Nazionale di Astrofisica-Osservatorio Astronomico di Palermo G.S. Vaiana, Palermo (Italy); Ayers, T. [Luxel Corporation, Friday Harbor (WA) (United States); Collura, A. [Istituto Nazionale di Astrofisica-Osservatorio Astronomico di Palermo G.S. Vaiana, Palermo (Italy); Nasillo, G. [Universita degli Studi di Palermo, Centro Grandi Apparecchiature, Palermo (Italy); Pareschi, G.; Tagliaferri, G. [Istituto Nazionale di Astrofisica-Osservatorio Astronomico di Brera, Merate (Italy)

2009-05-11T23:59:59.000Z

26

Combining Single-Molecule Optical Trapping and Small-Angle X-Ray Scattering Measurements to Compute the Persistence Length of a Protein  

E-Print Network [OSTI]

and purification For small-angle x-ray scattering and circular dichroism ER/K a-helix sequences from the myosin VICombining Single-Molecule Optical Trapping and Small-Angle X-Ray Scattering Measurements to Compute. In this study, we quantify this flexibility in terms of persistence length, namely the length scale over which

Spudich, James A.

27

E-Print Network 3.0 - anomalous small-angle x-ray Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

2008Standard Operating Procedure Title: Small Angle X-ray Scattering... approved: December 26 2009 Small Angle X-ray Scattering, Rotating Anode PURPOSE: This Standard...

28

Performance of a high-resolution, synchrotron-based, small-angle x-ray scattering instrument  

SciTech Connect (OSTI)

We describe the construction and performance of a small-angle x-ray scattering (SAXS) instrument which we have used on several beam lines at the National Synchrotron Light Source. The analyzer crystal was a channel cut Si(1,1,1) designed for use at {lambda}=1.54 A with a measured efficiency of 60{percent} and an angular resolution full width at half maximum of 0.001{degree}. In the case of strongly scattering samples (i.e., powders), momentum transfer {ital q} between 1{times}10{sup {minus}4} A{lt}{ital q}{lt}0.1 A{sup {minus}1} could be studied with over eight decades of dynamic intensity range. We demonstrate the versatility of this instrument by performing scattering experiments on a variety of spherical latex samples spanning the size range from 50 to 800 nm, liquid crystal samples with sharp, asymmetrical Bragg peaks, and metal clusters with sizes less than 10 nm. Small-angle x-ray scattering data for the larger polystyrene samples is compared with light scattering data and theoretical structure factors, and the relative roles of instrument smearing, sample polydispersity, and interparticle interference are elucidated. In the case of the liquid crystal samples, the high resolution of the instrument allows structural features to be observed that were previously obscured by the instrumental resolution in other small-angle neutron and synchroton-based Kratky camera data taken on the same samples. {copyright} {ital 1996 American Institute of Physics.}

Wilcoxon, J.P.; Craft, S.A. [Nanostructured Materials Division, Sandia National Laboratories, Albuquerque, New Mexico 87185 (United States)] [Nanostructured Materials Division, Sandia National Laboratories, Albuquerque, New Mexico 87185 (United States); Thurston, T.R. [Physics Department, Brookhaven National Laboratory, Upton, New York 11973 (United States)] [Physics Department, Brookhaven National Laboratory, Upton, New York 11973 (United States)

1996-09-01T23:59:59.000Z

29

New reactor dedicated to in operando studies of model catalysts by means of surface x-ray diffraction and grazing incidence small angle x-ray scattering  

SciTech Connect (OSTI)

A new experimental setup has been developed to enable in situ studies of catalyst surfaces during chemical reactions by means of surface x-ray diffraction (SXRD) and grazing incidence small angle x-ray scattering. The x-ray reactor chamber was designed for both ultrahigh-vacuum (UHV) and reactive gas environments. A laser beam heating of the sample was implemented; the sample temperature reaches 1100 K in UHV and 600 K in the presence of reactive gases. The reactor equipment allows dynamical observations of the surface with various, perfectly mixed gases at controlled partial pressures. It can run in two modes: as a bath reactor in the pressure range of 1-1000 mbars and as a continuous flow cell for pressure lower than 10{sup -3} mbar. The reactor is connected to an UHV preparation chamber also equipped with low energy electron diffraction and Auger spectroscopy. This setup is thus perfectly well suited to extend in situ studies to more complex surfaces, such as epitaxial films or supported nanoparticles. It offers the possibility to follow the chemically induced changes of the morphology, the structure, the composition, and growth processes of the model catalyst surface during exposure to reactive gases. As an example the Pd{sub 8}Ni{sub 92}(110) surface structure was followed by SXRD under a few millibars of hydrogen and during butadiene hydrogenation while the reaction was monitored by quadrupole mass spectrometry. This experiment evidenced the great sensitivity of the diffracted intensity to the subtle interaction between the surface atoms and the gas molecules.

Saint-Lager, M.-C.; Bailly, A.; Dolle, P.; Baudoing-Savois, R.; Taunier, P.; Garaudee, S.; Cuccaro, S.; Douillet, S.; Geaymond, O.; Perroux, G.; Tissot, O.; Micha, J.-S.; Ulrich, O.; Rieutord, F. [Institut Neel, CNRS and Universite Joseph Fourier, BP 166, F-38042 Grenoble Cedex 9 (France); CEA/DRFMC, 17 rue des Martyrs, 38054 Grenoble Cedex 9 (France)

2007-08-15T23:59:59.000Z

30

Small angle x-ray scattering study of fluctuations in 1-propanol-water and 2-propanol-water systems  

SciTech Connect (OSTI)

Small-angle x-ray scattering (SAXS) measurements have been carried out on the 1-propanol (NPA)-water system and on the 2-propanol (IPA)-water system at 20{degree}C. In the NPA-water system, the zero angle intensity, the concentration fluctuation, the Kirkwood-Buff parameters, and Debye's correlation lengths have been determined at various concentrations. In the IPA-water system, the zero angle intensity and Debye's correlation lengths have also been determined. In both the NPA-water and IPA-water systems, all obtained parameters have maxima at about 0.2 of the mole fraction of alcohol. In terms of these parameters, the mixing state of the NPA-water and IPA-water systems is discussed and compared with that of the TBA-water system.

Hayashi, Hisashi; Nishikawa, Keiko; Iijima, Takao (Gakushuin Univ., Tokyo (Japan))

1990-10-18T23:59:59.000Z

31

Wide angle X-ray scattering study of the layering in three of the Argonne premium coals  

Science Journals Connector (OSTI)

Using wide angle X-ray scattering methods, the phase interference curves and the inter-layer structure curves of thee of the Argonne Premium Coals were measured. These analyses indicate the inter-layer structuring is rank dependent. In the sub-bituminous coal (WyodakAnderson), the number of layers in the average short-range structural domain is ca. 2.3, with the average inter-layer distance being 4.1. For Pittsburgh #8 coal, the average inter-layer distance decreases slightly, to 4.0, while the number of layers in the average short-range structural domain increases to ca. 3. For the more mature Pocahontas #3, a low-volatile bituminous coal, the inter-layer distance decreases to 3.7, and the average short-range structural domain contains 4.55 layers.

D.L. Wertz; J.L. Quin

2000-01-01T23:59:59.000Z

32

In-situ small-angle X-ray scattering study of the precipitation behavior in a Fe-25 at.%Co-9 at.%Mo alloy  

SciTech Connect (OSTI)

Fe-Co-Mo alloys show extraordinary mechanical properties which make them potential candidates for various high-performance applications. In the present study, for the first time, the precipitation behavior in a Fe-25 at.%Co-9 at.%Mo alloy was studied by small-angle X-ray scattering using high-energy synchrotron radiation. The specimens were isothermally aged in an in-situ furnace. The small-angle X-ray scattering patterns showed scaling behavior and were evaluated by employing a model function from the literature. This approach provides information about the characteristic length scale and the volume fraction of the precipitates in the alloy.

Zickler, Gerald A. [Department of Physical Metallurgy and Materials Testing, Montanuniversitaet Leoben, Franz-Josef-Strasse 18, A-8700 Leoben (Austria); Christian Doppler Laboratory for Early Stages of Precipitation, Montanuniversitaet Leoben, Franz-Josef-Strasse 18, A-8700 Leoben (Austria)], E-mail: gerald.zickler@mu-leoben.at; Eidenberger, Elisabeth [Department of Physical Metallurgy and Materials Testing, Montanuniversitaet Leoben, Franz-Josef-Strasse 18, A-8700 Leoben (Austria); Leitner, Harald [Department of Physical Metallurgy and Materials Testing, Montanuniversitaet Leoben, Franz-Josef-Strasse 18, A-8700 Leoben (Austria); Christian Doppler Laboratory for Early Stages of Precipitation, Montanuniversitaet Leoben, Franz-Josef-Strasse 18, A-8700 Leoben (Austria); Stergar, Erich; Clemens, Helmut [Department of Physical Metallurgy and Materials Testing, Montanuniversitaet Leoben, Franz-Josef-Strasse 18, A-8700 Leoben (Austria); Staron, Peter; Lippmann, Thomas; Schreyer, Andreas [GKSS Research Center Geesthacht, Max-Planck-Strasse 1, D-21502 Geesthacht (Germany)

2008-12-15T23:59:59.000Z

33

Combined sampler robot and high-performance liquid chromatography: a fully automated system for biological small-angle X-ray scattering experiments at the Synchrotron SOLEIL SWING beamline  

Science Journals Connector (OSTI)

A prototype was developed to perform online purification and automatic loading of protein solutions at a small-angle X-ray scattering beamline.

David, G.

2009-09-08T23:59:59.000Z

34

Critical opalescence points to thermodynamic instability: relevance to small-angle X-ray scattering of resorcinol-formaldehyde gel formation at low pH  

Science Journals Connector (OSTI)

In situ small-angle X-ray scattering exhibits a non-monotonic evolution during the formation of resorcinol-formaldehyde gels. The data can be analyzed in terms of critical fluctuations, which points to a reaction-induced phase separation process.

Gommes, C.J.

2008-06-06T23:59:59.000Z

35

Design and characterization of an undulator beamline optimized for small-angle coherent X-ray scattering at the Advanced Photon Source  

Science Journals Connector (OSTI)

The design of an undulator beamline at the Advanced Photon Source optimized for performing coherent small-angle X-ray scattering is described. The beamline has been characterized by measuring and analysing static speckle patterns from isotropically disordered samples. The measured speckle widths and amplitudes are compared with a theory described herein and found to be in good agreement with its predictions.

Sandy, A.R.

1999-11-01T23:59:59.000Z

36

AN EFFICIENT PARALLEL GPU EVALUATION OF SMALL ANGLE X-RAY SCATTERING PROFILES  

E-Print Network [OSTI]

the scat- tering curve from a condensation of a gas of "dummy beads" to an experi-ray Scattering (SAXS) provides information on the excess electron density of the sample versus the surrounding of the experiment. For this procedure to be successful, an efficient procedure for both sampling protein structures

Hamelryck, Thomas

37

Molecular structures of fluid phase phosphatidylglycerol bilayers as determined by small angle neutron and X-ray scattering  

E-Print Network [OSTI]

neutron and X-ray scattering Jianjun Pan a, , Frederick A. Heberle a , Stephanie Tristram-Nagle b Matter Division, Neutron Sciences Directorate, Oak Ridge National Laboratory, Oak Ridge, TN 378316100 Institute for Neutron Sciences, Oak Ridge National Laboratory, Oak Ridge, TN 378316453, USA e Canadian

Nagle, John F.

38

Sub-second Morphological Changes in Nafion during Water Uptake Detected by Small-Angle X-Ray Scattering  

SciTech Connect (OSTI)

The ability of Nafion membrane to absorb water rapidly and create a network of hydrated interconnected water domains provides this material with an unmatched ability to conduct ions through a chemically and mechanically robust membrane. The morphology and composition of these hydrated membranes significantly affects their transport properties and performance. This work demonstrates that differences in interfacial interactions between the membranes exposed to vapor or liquid water can cause significant changes in kinetics of water uptake. In-situ small-angle X-ray scattering (SAXS) experiments captured the rapid swelling of the membrane in liquid water with nanostructure rearrangement on the order of seconds. For membranes in contact with water vapor, morphological changes are four-orders-of-magnitude slower than in liquid water, suggesting that interfacial resistance limits the penetration of water into the membrane. Also, upon water absorption from liquid water, a structural rearrangement from a distribution of spherical and cylindrical domains to exclusively cylindrical-like domains is suggested. These differences in water-uptake kinetics and morphology provide a new perspective into Schroeders Paradox, which dictates different water contents for vaporand liquid-equilibrated ionomers at unit activity. The findings of this work provide critical insights into the fast kinetics of water absorption of Nafion membrane, which can aid in the design of energy conversion devices that operate under frequent changes in environmental conditions.

Kusoglu, Ahmet; Modestino, Miguel A.; Hexemer, Alexander; Segalman, Rachel A.; Weber, Adam Z.

2011-09-30T23:59:59.000Z

39

Protein Folding Dynamics Detected By Time-Resolved Synchrotron X-ray Small-Angle Scattering Technique  

SciTech Connect (OSTI)

The polypeptide collapse is an essential dynamics in protein folding. To understand the mechanism of the collapse, in situ observation of folding by various probes is necessary. The changes in secondary and tertiary structures in the folding process of globular proteins, whose chain lengths are less than 300 polypeptides, were observed by circular dichrosim and intrinsic fluorescence spectroscopies, respectively. On the other hand, those in protein compactness could be only detected by using time-resolved synchrotron x-ray small-angle scattering technique. The observed dynamics for several proteins with different topologies suggested a common folding mechanism termed 'collapse and search' dynamics, in which the polypeptide collapse precedes the formation of the native contact formation. In 'collapse and search' dynamics, the most outstanding feature lied in the compactness of the initial intermediates. The collapsed intermediates demonstrated the scaling relationship between radius of gyration (Rg) and chain length with a scaling exponent of 0.35 {+-} 0.11, which is close to the value (1/3) predicted by mechano-statistical theory for the collapsed globules of polymers in poor solvent. Thus, it was suggested that the initial collapse is caused by the coil-globule transition of polymers. Since the collapse is essential to the folding of larger proteins, further investigations on the collapse likely lead to an important insight into the protein folding phenomena.

Fujisawa, Tetsuro; Takahashi, Satoshi [RIKEN Harima Institute, SPring-8 Center, Laboratory for Biometal Science, Hyogo 679-5148 (Japan); Institute for Protein Research, Osaka University Suita Osaka 565-0871/CREST, JST (Japan)

2007-03-30T23:59:59.000Z

40

Characterization of Nanoclay Orientation in Polymer Nanocomposite Film by Small-angle X-ray Scattering  

SciTech Connect (OSTI)

The orientation distribution of layer-shaped nanoclays (e.g. organoclays and pristine clays) dispersed in a polymer matrix is an important parameter to control the properties of polymer nanocomposites. In this study, we demonstrate that the use of multi-directional 2-D small-angleX-rayscattering (SAXS) can quantitatively describe the orientation distribution of organoclays (e.g. Cloisite C20A) in melt-pressed nanocompositefilms, containing ethylene-vinyl acetate (EVA) copolymers as polymer matrices. Different weight fractions of organoclays were used to alter the orientation profile of nanocompositefilms, in which the dispersion and morphology of organoclays were also characterized by complementary 2-D and 3-D transmission electron microscopy (TEM). All nanocomposites exhibited mixed intercalation/exfoliation clay morphology, where the intercalated structure possessed partial orientation parallel to the in-plane direction of the film. The higher content of the clay loading showed a higher clay orientation. A simple analytical scheme for SAXS data analysis to determine the orientation parameter (P{sub 2}) was demonstrated, the results of which are in agreement with the gas permeation properties of the nanocompositefilms.

P Nawani; C Burger; L Rong; B Chu; B Hsiao; A Tsou; W Weng

2011-12-31T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


41

EXPRESSION, PURIFICATION, AND SMALL ANGLE X-RAY SCATTERING OF DNA REPLICATION AND REPAIR PROTEINS FROM THE HYPERTHERMOPHILE SULFOLOBUS SOLFATARICUS  

SciTech Connect (OSTI)

Vital molecular processes such as DNA replication, transcription, translation, and maintenance occur through transient protein interactions. Elucidating the mechanisms by which these protein complexes and interactions function could lead to treatments for diseases related to DNA damage and cell division control. In the recent decades since its introduction as a third domain, Archaea have shown to be simpler models for complicated eukaryotic processes such as DNA replication, repair, transcription, and translation. Sulfolobus solfataricus is one such model organism. A hyperthermophile with an optimal growth temperature of 80C, Sulfolobus protein-protein complexes and transient protein interactions should be more stable at moderate temperatures, providing a means to isolate and study their structure and function. Here we provide the initial steps towards characterizing three DNA-related Sulfolobus proteins with small angle X-ray scattering (SAXS): Sso0257, a cell division control and origin recognition complex homolog, Sso0768, the small subunit of the replication factor C, and Sso3167, a Mut-T like protein. SAXS analysis was performed at multiple concentrations for both short and long exposure times. The Sso0257 sample was determined to be either a mixture of monomeric and dimeric states or a population of dynamic monomers in various conformational states in solution, consistent with a fl exible winged helix domain. Sso0768 was found to be a complex mixture of multimeric states in solution. Finally, molecular envelope reconstruction from SAXS data for Sso3167 revealed a novel structural component which may function as a disordered to ordered region in the presence of its substrates and/or protein partners.

Patterson, S.M.; Hatherill, J.R.; Hammel, M.; Hura, G.L.; Tainer, J.A.; Yannone, S.M.

2008-01-01T23:59:59.000Z

42

13 - X-ray and Neutron Scattering  

Science Journals Connector (OSTI)

Abstract This chapter describes the use of neutrons and X-rays as probes in the study of structural and dynamic properties of metallic materials. Crystalline materials are characterized by their diffraction peaks related to their average crystallographic structure. In real crystals, locally displaced atoms and chemically (or isotopically for neutrons) different species may lead not only to changes of peak shapes and positions, but also to additional (diffuse) scattering between Bragg peak, including scattering around the primary beam (small-angle scattering). All these features can be used to extract information about the state of a sample, its compositional and structural variations on a scale depending on the scattering, in static and time-resolved kinetic studies. Energy-resolved scattering also offers an insight into solid-state dynamics on a microscopic scale. Some of the most important methods will be described and illustrated by instructive examples. The presentation offers a combined view of neutron and X-ray scattering, with the necessary simplifications dictated by space limitations. The special properties of thermal neutrons and of hard X-rays (now widely available at synchrotron radiation sources), their mutual combination, and combinations with other methods, in particular electron microscopy, offer ample opportunity to better understand and control materials properties. After a brief introduction to scattering from real crystals and some general ideas about long-range strains and Bragg peaks, the vicinity of Bragg peaks (displacement scattering at large scattering angles), the scattering far away from Bragg peaks (chemical heterogeneities, short-range order), and, in greater detail, small-angle scattering (which is not sensitive to the extent of crystallinity, but to nanoscale variations of chemical composition and of magnetization, precipitation) will be described, along with classical and more recent applications related to short-range ordering and precipitation in bulk and nanostructured alloys. Some other fields are only briefly addressed (grazing-incidence studies of surfaces, radiography, absorption spectroscopies, coherent X-rays). The final section offers some information on the influence of defects on lattice dynamics and on (slow) diffusive motion in materials.

Gernot Kostorz

2014-01-01T23:59:59.000Z

43

Insights into Montmorillonite Nanoclay Based ex Situ Nanocomposites from SEBS and Modified SEBS by Small-Angle X-ray Scattering and Modulated DSC Studies  

Science Journals Connector (OSTI)

Insights into Montmorillonite Nanoclay Based ex Situ Nanocomposites from SEBS and Modified SEBS by Small-Angle X-ray Scattering and Modulated DSC Studies ... (1-3) These polymer?clay nanocomposites possess superior properties to conventional microcomposites due to maximized interfacial adhesion and finely dispersed nanoclays distributed all through the polymer matrix. ... TEM image of AA6SEBS-MT4 nanocomposite (Figure 6l) indicates that MT nanoclays are dispersed well with lamellar microphase separated morphology which is regained on addition of the MT nanoclay. ...

Anirban Ganguly; Anil K. Bhowmick; Yongjin Li

2008-07-22T23:59:59.000Z

44

Small-angle neutron scattering and neutron reflectometry  

Science Journals Connector (OSTI)

Diffraction methods, interpreted loosely, could be applied to the techniques of wide-angle X-ray scattering, small-angle X-ray scattering, electron diffraction, small-angle neutron scattering, small-angle light s...

R. W. Richards

1993-01-01T23:59:59.000Z

45

Agglomeration and sintering in annealed FePt nanoparticle assemblies studied by small angle neutron scattering and x-ray diffraction  

Science Journals Connector (OSTI)

In this work we give a detailed account of complementary small angle neutron scattering and x-ray diffraction studies of polymer mediated, self-assembled FePt nanoparticle arrays as a function of annealing temperature. The combination of these two techniques provides significantly greater physical insight than is available using either individually. Since both methods integrate over a large number of particles statistically meaningful data can be obtained in contrast to imaging techniques where typically only small areas are analyzed. The data show that the median particle size increases with annealing at temperatures of 580C and above. The data also demonstrate that the distribution of particle diameters is significant and increases with annealing temperature. These results allow a comprehensive structural model of the annealed assemblies to be developed in terms of particle sintering and agglomeration. This enhanced understanding will allow new strategies to be pursued in realizing the potential of nanoparticle assemblies as a monodispersed data storage medium.

T. Thomson; S. L. Lee; M. F. Toney; C. D. Dewhurst; F. Y. Ogrin; C. J. Oates; S. Sun

2005-08-19T23:59:59.000Z

46

Crystal Structures and Small-angle X-ray Scattering Analysis of UDP-galactopyranose Mutase from the Pathogenic Fungus Aspergillus fumigatus  

SciTech Connect (OSTI)

UDP-galactopyranose mutase (UGM) is a flavoenzyme that catalyzes the conversion of UDP-galactopyranose to UDP-galactofuranose, which is a central reaction in galactofuranose biosynthesis. Galactofuranose has never been found in humans but is an essential building block of the cell wall and extracellular matrix of many bacteria, fungi, and protozoa. The importance of UGM for the viability of many pathogens and its absence in humans make UGM a potential drug target. Here we report the first crystal structures and small-angle x-ray scattering data for UGM from the fungus Aspergillus fumigatus, the causative agent of aspergillosis. The structures reveal that Aspergillus UGM has several extra secondary and tertiary structural elements that are not found in bacterial UGMs yet are important for substrate recognition and oligomerization. Small-angle x-ray scattering data show that Aspergillus UGM forms a tetramer in solution, which is unprecedented for UGMs. The binding of UDP or the substrate induces profound conformational changes in the enzyme. Two loops on opposite sides of the active site move toward each other by over 10 {angstrom} to cover the substrate and create a closed active site. The degree of substrate-induced conformational change exceeds that of bacterial UGMs and is a direct consequence of the unique quaternary structure of Aspergillus UGM. Galactopyranose binds at the re face of the FAD isoalloxazine with the anomeric carbon atom poised for nucleophilic attack by the FAD N5 atom. The structural data provide new insight into substrate recognition and the catalytic mechanism and thus will aid inhibitor design.

Dhatwalia, Richa; Singh, Harkewal; Oppenheimer, Michelle; Karr, Dale B.; Nix, Jay C.; Sobrado, Pablo; Tanner, John J. (Missouri); (LBNL); (VPI-SU)

2012-05-14T23:59:59.000Z

47

Impact of Ferrocene on the Structure of Diesel Exhaust Soot as Probed with Wide-Angle X-ray Scattering and C(1s) NEXAFS Spectroscopy  

SciTech Connect (OSTI)

We report on the structure of a set of diesel exhaust samples that were obtained from reference diesel fuel and diesel fuel mixed with ferrocene. Characterization was carried out with X-ray absorption spectroscopy (C(1s) NEXAFS) and wide-angle X-ray scattering (WAXS). The reference diesel soot shows a pronounced graphite-like microstructure and molecular structure, with a strong (0 0 2) graphite Bragg reflex and a strong aromatic C{double_bond}C resonance at 285 eV. The mineral matter in the reference soot could be identified as Fe{sub 2}O{sub 3} hematite. The soot specimen from the diesel mixed with ferrocene has an entirely different structure and lacks significantly in graphite-like characteristics. NEXAFS spectra of such soot barely show aromatics but pronounced contributions from aliphatic structures. WAXS patterns show almost no intensity at the Bragg (0 0 2) reflection of graphite, but a strong aliphatic {gamma}-side band. The iron from the ferrocene transforms to Fe{sub 2}O{sub 3} maghemite.

Braun,A.; Huggins, F.; Kelly, K.; Mun, B.; Ehrlich, S.; Huffman, G.

2006-01-01T23:59:59.000Z

48

Nonlinear X-ray Compton Scattering  

E-Print Network [OSTI]

X-ray scattering is a weak linear probe of matter. It is primarily sensitive to the position of electrons and their momentum distribution. Elastic X-ray scattering forms the basis of atomic structural determination while inelastic Compton scattering is often used as a spectroscopic probe of both single-particle excitations and collective modes. X-ray free-electron lasers (XFELs) are unique tools for studying matter on its natural time and length scales due to their bright and coherent ultrashort pulses. However, in the focus of an XFEL the assumption of a weak linear probe breaks down, and nonlinear light-matter interactions can become ubiquitous. The field can be sufficiently high that even non-resonant multiphoton interactions at hard X-rays wavelengths become relevant. Here we report the observation of one of the most fundamental nonlinear X-ray-matter interactions, the simultaneous Compton scattering of two identical photons producing a single photon at nearly twice the photon energy. We measure scattered...

Fuchs, Matthias; Chen, Jian; Ghimire, Shambhu; Shwartz, Sharon; Kozina, Michael; Jiang, Mason; Henighan, Thomas; Bray, Crystal; Ndabashimiye, Georges; Bucksbaum, P H; Feng, Yiping; Herrmann, Sven; Carini, Gabriella; Pines, Jack; Hart, Philip; Kenney, Christopher; Guillet, Serge; Boutet, Sebastien; Williams, Garth; Messerschmidt, Marc; Seibert, Marvin; Moeller, Stefan; Hastings, Jerome B; Reis, David A

2015-01-01T23:59:59.000Z

49

Simulation of the shape of chaperonins using the small-angle x-ray scattering curves and torus form factor  

SciTech Connect (OSTI)

The inverse scattering problem has been solved for protein complexes whose surfaces can be described by a set of the simplest doubly connected surfaces in the uniform approximation (a scattering potential inside the molecule is a constant). Solutions of two proteins-well-known GroEL bacterial chaperonin and poor-studied bacteriophage chaperonin, which is a product of 146 gene (gp146)-were taken for the experiment. The shapes of protein complexes have been efficiently reconstructed from the experimental scattering curves. The shell method, the method of the rotation of amino acid sequences with the use of the form factor of an amino acid, and the method of seeking the model parameters of a protein complex with the preliminarily obtained form factor of the model have been used to reconstruct the shape of these particles.

Amarantov, S. V., E-mail: amarantov_s@mail.ru [Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation); Naletova, I. N. [Moscow State University, Belozerskii Institute of Molecular Biology and Bioorganic Chemistry (Russian Federation); Kurochkina, L. P. [Russian Academy of Sciences, Shemyakin-Ovchinnikov Institute of Bioorganic Chemistry (Russian Federation)

2011-08-15T23:59:59.000Z

50

Characterization of the Decaheme c-type Cytochrome OmcA in Solution and on Hematite Surfaces by Small Angle X-ray Scattering and Neutron Reflectometry  

SciTech Connect (OSTI)

The outer membrane protein OmcA is an 85 kDa decaheme c-type cytochrome located on the surface of the dissimilatory metal reducing bacterium Shewanella oneidensis MR-1. It is assumed to mediate electron shuttling, generated by the bacteria s metabolism, to extracellular acceptors that include solid metal oxides such as hematite ( -Fe2O3). To investigate the mechanism by which OmcA interacts with hematite, we purified OmcA and characterized its solution structure by small angle X-ray scattering (SAXS) and its interaction with hematite by neutron reflectometry (NR). SAXS results showed that OmcA is a monomer that adopts a flat ellipsoidal shape with a dimension of 3.4 9.0 6.5 nm3. Changes in redox state affect OmcA conformation. In addition, OmcA interacts with small organic ligands known to act as electron shuttle molecules, such as flavin mononucleotide (FMN), resulting in the formation of high molecular weight assemblies. A model system, developed using NR to study the interaction of OmcA with hematite, shows that OmcA forms a well-defined monomolecular layer on hematite surfaces. This allows OmcA to preferentially interact with hematite in a conformation that maximizes its contact area with the mineral surface. Overall, these results provide experimental and quantitative evidence for OmcA reduction of solid metal oxides involving both direct and indirect mechanisms.

Johs, Alexander [ORNL; Shi, Liang [ORNL; Droubay, Timothy [Pacific Northwest National Laboratory (PNNL); Ankner, John Francis [ORNL; Liang, Liyuan [ORNL

2010-01-01T23:59:59.000Z

51

HIGH BRILLIANCE X-RAY SCATTERING FOR  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

BRILLIANCE X-RAY SCATTERING FOR BRILLIANCE X-RAY SCATTERING FOR LIFE SCIENCES (LIX) Group Leader: Lin Yang Proposal Team: O. Bilsel 1 , B. Hsiao 2 , H. Huang 3 , T. Irving 4 , A. Menzel 5 , L. Pollack 6 , C. Riekel 7 , J. Rubert 8 , H. Tsuruta 9 , L. Yang 10 1 University of Massachusetts, 2 Stony Brook University, 3 Rice University, 4 IIT, 5SLS, 6 Cornell University, 7 European Synchrotron Radiation Facility, 8 NEU, 9 Stanford Synchrotron Radiation Lightsource, 10 Brookhaven National Laboratory TECHNIQUES AND CAPABILITIES APPLICATIONS ADDITIONAL INFORMATION * Energy range 2-20keV using undulator source. Simultaneous SAXS/WAXS to cover 0.003-3Å -1 at 12keV with 1 micron spot size * Time-resolved solution scattering with resolution of (1) microseconds to milliseconds using continuous-flow mixing (5µm x 10µm spot size) and (2) milliseconds using stopped-

52

Characterization of the Decaheme c-Type Cytochrome OmcA in Solution and on Hematite Surfaces by Small Angle X-Ray Scattering and Neutron Reflectometry  

SciTech Connect (OSTI)

The outer membrane protein OmcA is an 85 kDa decaheme c-type cytochrome located on the surface of the dissimilatory metal-reducing bacterium Shewanella oneidensis MR-1. It is assumed to mediate shuttling of electrons to extracellular acceptors that include solid metal oxides such as hematite (a-Fe2O3). No information is yet available concerning OmcA structure in physiologically relevant conditions such as aqueous environments. We purified OmcA and characterized its solution structure by small angle x-ray scattering (SAXS), and its interaction at the hematite-water interface by neutron reflectometry. SAXS showed that OmcA is a monomer that adopts a flat ellipsoidal shape with an overall dimension of 34 x 90 x 65A? 3. To our knowledge, we obtained the first direct evidence that OmcA undergoes a redox state-dependent conformational change in solution whereby reduction decreases the overall length of OmcA by ~7 A? (the maximum dimension was 96 A? for oxidized OmcA, and 89 A? for NADH and dithionite-reduced OmcA). OmcA was also found to physically interact with electron shuttle molecules such as flavin mononucleotide, resulting in the formation of high-molecular-weight assemblies. Neutron reflectometry showed that OmcA forms a well-defined monomolecular layer on hematite surfaces, where it assumes an orientation that maximizes its contact area with the mineral surface. These novel insights into the molecular structure of OmcA in solution, and its interaction with insoluble hematite and small organic ligands, demonstrate the fundamental structural bases underlying OmcAs role in mediating redox processes.

Johs, Alexander; Shi, Liang; Droubay, Timothy C.; Ankner, John F.; Liang, L.

2010-06-16T23:59:59.000Z

53

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscop...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Refinement Friday, September 28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray...

54

Edible oil structures at low and intermediate concentrations. II. Ultra-small angle X-ray scattering of in situ tristearin solids in triolein  

SciTech Connect (OSTI)

Ultra-small angle X-ray scattering has been used for the first time to elucidate, in situ, the aggregation structure of a model edible oil system. The three-dimensional nano- to micro-structure of tristearin solid particles in triolein solvent was investigated using 5, 10, 15, and 20% solids. Three different sample preparation procedures were investigated: two slow cooling rates of 0.5/min, case 1 (22 days of storage at room temperature) and case 2 (no storage), and one fast cooling of 30/min, case 3 (no storage). The length scale investigated, by using the Bonse-Hart camera at beamline ID-15D at the Advanced Photon Source, Argonne National Laboratory, covered the range from 300? to 10??m. The unified fit and the Guinier-Porod models in the Irena software were used to fit the data. The former was used to fit 3 structural levels. Level 1 structures showed that the primary scatterers were essentially 2-dimensional objects for the three cases. The scatterers possessed lateral dimensions between 1000 and 4300?. This is consistent with the sizes of crystalline nanoplatelets present which were observed using cryo-TEM. Level 2 structures were aggregates possessing radii of gyration, R{sub g2} between 1800? and 12000? and fractal dimensions of either D{sub 2}=1 for case 3 or 1.8?D{sub 2}?2.1 for case 1 and case 2. D{sub 2}?=?1 is consistent with unaggregated 1-dimensional objects. 1.8???D{sub 2}???2.1 is consistent with these 1-dimensional objects (below) forming structures characteristic of diffusion or reaction limited cluster-cluster aggregation. Level 3 structures showed that the spatial distribution of the level 2 structures was uniform, on the average, for case 1, with fractal dimension D{sub 3}?3 while for case 2 and case 3 the fractal dimension was D{sub 3}?2.2, which suggested that the large-scale distribution had not come to equilibrium. The Guinier-Porod model showed that the structures giving rise to the aggregates with a fractal dimension given by D{sub 2} in the unified fit level 2 model were cylinders described by the parameter s?1 in the Guinier-Porod model. The size of the base of these cylinders was in agreement with the cryo-TEM observations as well as with the results of the level 1 unified fit model. By estimating the size of the nanoplatelets and understanding the structures formed via their aggregation, it will be possible to engineer novel lipids systems that embody desired functional characteristics.

Peyronel, Fernanda; Marangoni, Alejandro G. [Food Science Department, University of Guelph, Guelph, Ontario N1G 2W1 (Canada); Ilavsky, Jan [Advanced Photon Source, Argonne National Laboratory, 9700S Cass Ave., Bldg. 434D, Argonne, Illinois 60439 (United States); Mazzanti, Gianfranco [Department of Process Engineering and Applied Science, Dalhousie University, Halifax, Nova Scotia B3H 4R2 (Canada); Pink, David A. [Food Science Department, University of Guelph, Guelph, Ontario N1G 2W1 (Canada); Physics Department, St. Francis Xavier University, Antigonish, Nova Scotia B2G 2W5 (Canada)

2013-12-21T23:59:59.000Z

55

Neutron and X-ray Scattering Study of Magnetic Manganites  

E-Print Network [OSTI]

Neutron and X-ray Scattering Study of Magnetic Manganites Graeme Eoin Johnstone A Thesis submitted are performed using a variety of neutron scattering and x-ray scattering techniques. The electronic ground for analysing the results of the polarised neutron scattering experiment. There are a large number of people who

Boothroyd, Andrew

56

Introduction to Neutron and X-Ray Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Scattering Studies of Thin Scattering Studies of Thin Polymer Films Introduction to Neutron and X-Ray Scattering Sunil K. Sinha UCSD/LANL Acknowledgements: Prof. R.Pynn( Indiana U.) Prof. M.Tolan (U. Dortmund) Wilhelm Conrad Röntgen 1845-1923 1895: Discovery of X-Rays 1901 W. C. Röntgen in Physics for the discovery of x-rays. 1914 M. von Laue in Physics for x-ray diffraction from crystals. 1915 W. H. Bragg and W. L. Bragg in Physics for crystal structure determination. 1917 C. G. Barkla in Physics for characteristic radiation of elements. 1924 K. M. G. Siegbahn in Physics for x-ray spectroscopy. 1927 A. H. Compton in Physics for scattering of x-rays by electrons. 1936 P. Debye in Chemistry for diffraction of x-rays and electrons in gases.

57

Nanostructure of a-Si:H and related alloys by small-angle scattering of neutrons and X-rays: Annual technical progress report: May 22, 1998 -- May 21, 1999  

SciTech Connect (OSTI)

This report describes work being performed to provide details of the microstructure in high-quality hydrogenated amorphous silicon and related alloys on the nanometer scale. The materials under study are being prepared by state-of-the-art deposition methods, as well as by new and emerging deposition techniques. The purpose is to establish the role of nanostructural features in controlling opto-electronic and photovoltaic properties. The approach centers around the use of the uncommon technique of small-angle scattering of both X-rays (SAXS) and neutrons (SANS). SAXS has already been established as highly sensitive to microvoids and columnar-like microstructure. A major goal of this research is to establish the sensitivity of SANS to the hydrogen nanostructure. Conventional X-ray diffraction techniques are being used to examine medium-range order and microcrystallinity, particularly near the boundary between amorphous and microcrystalline material.

Williamson, D. L.

1999-12-21T23:59:59.000Z

58

Twelfth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Twelfth National School on Neutron and X-ray Scattering June 12 � June 26, 2010 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

59

National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

National School on Neutron and X-ray Scattering May 30 � June 13, 2009 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

60

National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

15th National School on Neutron and X-ray Scattering August 10 - 24, 2013 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


61

Fourteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Fourteenth National School on Neutron and X-ray Scattering August 12 - 25, 2012 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major Ridge National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang

Pennycook, Steve

62

Thirteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Thirteenth National School on Neutron and X-ray Scattering June 11 ­ June 25, 2011 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

63

Sixteenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Sixteenth National School on Neutron and X-ray Scattering June 14-28, 2014 at Argonne National of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major's Neutron Scattering Science Division. Scientific Directors: Suzanne G.E. te Velthuis, Esen Ercan Alp

Pennycook, Steve

64

Tenth National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Tenth National School on Neutron and X-ray Scattering September 24 - October 11, 2008 at Argonne of the National School on Neutron and X-ray Scattering is to educate graduate students on the utilization of major National Laboratory's Neutron Scattering Science Division. Scientific Directors: Jonathan C. Lang, Suzanne

Pennycook, Steve

65

Inelastic X-ray and Nuclear Resonant Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

... Search About User Information News & Events Science & Education Beamlines Divisions Argonne Home > Advanced Photon Source > Inelastic X-ray and Nuclear Resonant Scattering...

66

X-ray Diffuse Scattering Measurements of Nucleation Dynamics...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-ray Diffuse Scattering Measurements of Nucleation Dynamics at Femtosecond Resolution Real-time measurement and control of the non-equilibrium properties of materials represents...

67

Incoherent x-ray scattering in single molecule imaging  

E-Print Network [OSTI]

Imaging of the structure of single proteins or other biomolecules with atomic resolution would be enormously beneficial to structural biology. X-ray free-electron lasers generate highly intense and ultrashort x-ray pulses, providing a route towards imaging of single molecules with atomic resolution. The information on molecular structure is encoded in the coherent x-ray scattering signal. In contrast to crystallography there are no Bragg reflections in single molecule imaging, which means the coherent scattering is not enhanced. Consequently, a background signal from incoherent scattering deteriorates the quality of the coherent scattering signal. This background signal cannot be easily eliminated because the spectrum of incoherently scattered photons cannot be resolved by usual scattering detectors. We present an ab initio study of incoherent x-ray scattering from individual carbon atoms, including the electronic radiation damage caused by a highly intense x-ray pulse. We find that the coherent scattering pa...

Slowik, Jan Malte; Dixit, Gopal; Jurek, Zoltan; Santra, Robin

2014-01-01T23:59:59.000Z

68

Photon Sciences | Beamlines | IXS: Inelastic X-ray Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

IXS: Inelastic X-ray Scattering IXS: Inelastic X-ray Scattering Poster | Fact Sheet | Preliminary Design Report Scientific Scope Many hot topics related to the high frequency dynamics of condensed matter require both a narrower and steeper resolution function and access to a broader dynamic range than what are currently available. This represents a sort of "no man's land" that falls right in the dynamic gap lying between the high frequency spectroscopies, such as inelastic x-ray scattering (IXS), and the low frequency ones. New IXS spectrometers with improved energy and momentum resolutions would be required to fill this gap. To achieve this goal, a new x-ray optics concept for both the monochromatization and energy analysis of x-rays will be implemented at the NSLS-II Inelastic X-ray Scattering beamline. This solution exploits the

69

HIV-1 Tat membrane interactions probed using X-ray and neutron scattering, CD spectroscopy and MD simulations  

E-Print Network [OSTI]

HIV-1 Tat membrane interactions probed using X-ray and neutron scattering, CD spectroscopy and MD translocation, were provided by wide-angle X-ray scattering (WAXS) and neutron scattering. CD spectroscopy for Neutron Research, 100 Bureau Drive, Stop 6102, Gaithersburg, MD 20899, United States d CHESS, Cornell

Nagle, John F.

70

Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Probing Spatial, Electronic Structures with X-ray Scattering, Spectroscopic Techniques Wednesday, September 5, 2012 - 10:45am SLAC, Bldg. 137, Room 226 Gang Chen Seminar: Structures at atomic scales are traditionally determined through X-ray crystallography that amplifies scattering intensities by introducing spatial periodicity. For amorphous materials and many macromolecules, such as viruses, proteins and biofilms, it is hard to determine structures due to their incapability to crystallize or change of configuration during crystallization. In this talk, I will present the application of X-ray reflectivity and a newly developed fluctuation X-ray scattering technique to study the structures of lipid membranes and randomly oriented nanoparticles. Three different types of domain registrations occurring with

71

Studies in Small Angle Scattering Techniques  

E-Print Network [OSTI]

. Knud Møllenbach Abstract. Small angle scattering of neutrons, x-rays and y-rays are found among scattering as well as small angle y-ray diffraction. The study of neutron scat- tering from formations limit of the neutron diffractometer 20 3. SMALL ANGLE SCATTERING INSTRUMENTS 22 3.1. The double crystal

72

Structured x-ray beams from twisted electrons by inverse Compton scattering of laser light  

E-Print Network [OSTI]

The inverse Compton scattering of laser light on high-energetic twisted electrons is investigated with the aim to construct spatially structured x-ray beams. In particular, we analyze how the properties of the twisted electrons, such as the topological charge and aperture angle of the electron Bessel beam, affects the energy and angular distribution of scattered x-rays. We show that with suitably chosen initial twisted electron states one can synthesize tailor-made x-ray beam profiles with a well-defined spatial structure, in a way not possible with ordinary plane-wave electron beams.

Seipt, D; Fritzsche, S

2014-01-01T23:59:59.000Z

73

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Resonant Soft X-Ray Scattering - Combining Structural with Spectroscopic Refinement Friday, September 28, 2012 - 10:00am SLAC, Bldg. 137, Room 322 SSRL Presents Kevin Stone X-ray absorption spectroscopy has become an important tool in understanding the electronic structure of materials. Resonant absorption edges in the soft x-ray regime are especially interesting as they allow the study of the lighter elements, such as in organic or organo-metallic substances, as well as important L-edges of the 3d transition metals important in magnetic and oxide systems. Measurements of soft x-ray absorption spectra are inherently surface sensitive, and are plagued by issues such as extinction (in electron yield measurements) or self absorption (in fluorescence yield

74

New Directions in X-ray Scattering - SSRL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

6, 2006 A summary of the workshop on New Directions in X-ray Scattering On Dec 6th, we held a day long workshop to solicit user input on the new directions that the SSRL...

75

Magnetism studies using resonant, coherent, x-ray scattering...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Magnetism studies using resonant, coherent, x-ray scattering Monday, September 10, 2012 - 10:00am SLAC, Bldg. 137, Room 226 Keoki Seu Seminar: With the advent of free electron...

76

Generation of first hard X-ray pulse at Tsinghua Thomson Scattering X-ray Source  

SciTech Connect (OSTI)

Tsinghua Thomson Scattering X-ray Source (TTX) is the first-of-its-kind dedicated hard X-ray source in China based on the Thomson scattering between a terawatt ultrashort laser and relativistic electron beams. In this paper, we report the experimental generation and characterization of the first hard X-ray pulses (51.7 keV) via head-on collision of an 800 nm laser and 46.7 MeV electron beams. The measured yield is 1.0 Multiplication-Sign 10{sup 6} per pulse with an electron bunch charge of 200 pC and laser pulse energy of 300 mJ. The angular intensity distribution and energy spectra of the X-ray pulse are measured with an electron-multiplying charge-coupled device using a CsI scintillator and silicon attenuators. These measurements agree well with theoretical and simulation predictions. An imaging test using the X-ray pulse at the TTX is also presented.

Du Yingchao; Yan Lixin; Hua Jianfei; Du Qiang; Zhang Zhen; Li Renkai; Qian Houjun; Huang Wenhui; Chen Huaibi; Tang Chuanxiang [Accelerator Laboratory, Department of Engineering Physics, Tsinghua University, Beijing 100084 (China); Key Laboratory of Particle and Radiation Imaging, Tsinghua University, Ministry of Education, Beijing 100084 (China); Key Laboratory of High Energy Radiation Imaging Fundamental Science for National Defense, Tsinghua University, Beijing 100084 (China)

2013-05-15T23:59:59.000Z

77

X-ray Raman scattering study of aligned polyfluorene  

E-Print Network [OSTI]

We present a non-resonant inelastic x-ray scattering study at the carbon K-edge on aligned poly[9,9-bis(2-ethylhexyl)-fluorene-2,7-diyl] and show that the x-ray Raman scattering technique can be used as a practical alternative to x-ray absorption measurements. We demonstrate that this novel method can be applied to studies on aligned $\\pi$-conjugated polymers complementing diffraction and optical studies. Combining the experimental data and a very recently proposed theoretical scheme we demonstrate a unique property of x-ray Raman scattering by performing the symmetry decomposition on the density of unoccupied electronic states into $s$- and $p$-type symmetry contributions.

S. Galambosi; M. Knaapila; J. A. Soininen; K. Nyg\\aard; S. Huotari; F. Galbrecht; U. Scherf; A. P. Monkman; K. Hmlinen

2006-08-29T23:59:59.000Z

78

High performance x-ray anti-scatter grid  

DOE Patents [OSTI]

Disclosed are an x-ray anti-scatter grid for x-ray imaging, particularly for screening mammography, and method for fabricating same, x-rays incident along a direct path pass through a grid composed of a plurality of parallel or crossed openings, microchannels, grooves, or slots etched in a substrate, such as silicon, having the walls of the microchannels or slots coated with a high opacity material, such as gold, while x-rays incident at angels with respect to the slots of the grid, arising from scatter, are blocked. The thickness of the substrate is dependent on the specific application of the grid, whereby a substrate of the grid for mammography would be thinner than one for chest radiology. Instead of coating the walls of the slots, such could be filed with an appropriate liquid, such as mercury. 4 Figs.

Logan, C.M.

1995-05-23T23:59:59.000Z

79

Structural characterization of Green River oil-shale at high-pressure using pair distribution function analysis and small angle x-ray scattering.  

SciTech Connect (OSTI)

The compression behavior of a silicate-rich oil shale from the Green River formation in the pressure range 0.0-2.4 GPa was studied using in situ high pressure X-ray pair distribution function (PDF) measurements for the sample contained within a Paris-Edinburgh cell. The real-space local structural information in the PDF, G(r), was used to evaluate the compressibility of the oil shale. Specifically, the pressure-induced reduction in the medium- to long-range atom distances (6-20 {angstrom}) yielded an average sample compressibility corresponding to a bulk modulus of ca. 61-67 GPa. A structural model consisting of a three phase mixture of the principal crystalline oil shale components (quartz, albite and Illite) provided a good fit to the ambient pressure PDF data (R 30.7%). Indeed the features in the PDF beyond 6 {angstrom}, were similarly well fit by a single phase model of the highest symmetry, highly crystalline quartz component.

Locke, D. R.; Chupas, P. J.; Chapman, K. W.; Pugmire, R. J.; Winans, R. E.; Univ. of Utah

2008-01-01T23:59:59.000Z

80

Dense Plasma X-ray Scattering: Methods and Applications  

SciTech Connect (OSTI)

We have developed accurate x-ray scattering techniques to measure the physical properties of dense plasmas. Temperature and density are inferred from inelastic x-ray scattering data whose interpretation is model-independent for low to moderately coupled systems. Specifically, the spectral shape of the non-collective Compton scattering spectrum directly reflects the electron velocity distribution. In partially Fermi degenerate systems that have been investigated experimentally in laser shock-compressed beryllium, the Compton scattering spectrum provides the Fermi energy and hence the electron density. We show that forward scattering spectra that observe collective plasmon oscillations yield densities in agreement with Compton scattering. In addition, electron temperatures inferred from the dispersion of the plasmon feature are consistent with the ion temperature sensitive elastic scattering feature. Hence, theoretical models of the static ion-ion structure factor and consequently the equation of state of dense matter can be directly tested.

Glenzer, S H; Lee, H J; Davis, P; Doppner, T; Falcone, R W; Fortmann, C; Hammel, B A; Kritcher, A L; Landen, O L; Lee, R W; Munro, D H; Redmer, R; Weber, S

2009-08-19T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


81

Self-similarity during growth of the Au/TiO{sub 2}(110) model catalyst as seen by the scattering of x-rays at grazing-angle incidence  

SciTech Connect (OSTI)

The growth of gold nanoparticles on TiO{sub 2}(110) was investigated in situ by grazing incidence x-ray scattering techniques. The in-plane diffraction showed complex epitaxial relationships with a preferential alignment of dense gold direction along the bridging oxygen rows of TiO{sub 2}(110) ([110]{sub Au} parallel [001]{sub TiO{sub 2}}) with a low lattice mismatch. Whatever the growth temperature (T=300,600 K), two nearly equiproportional epitaxial planes, i.e., (111){sub Au} parallel (110){sub TiO{sub 2}} and (112){sub Au} parallel (110){sub TiO{sub 2}}, were observed. The small angle scattering from the nanoparticles was analyzed using a truncated sphere shape with models [R. Lazzari, F. Leroy, and G. Renaud, Phys. Rev. B 76, 125411 (2007)] that account for (i) multiple scattering effects due to the graded profile of refraction index in the normal direction and (ii) the correlation between the particle spacing and sizes. At the beginning of the growth, gold particles are pinned on defects and grow through a diffusion-limited mechanism. However, coalescence does not occur via a static mechanism. It rather involves surface diffusion of clusters. It proceeds through a self-similar mechanism, not only on the size distribution but also on the spatial ordering. Particle locations, which are no longer controlled by the randomness of nucleation centers, become dominated by the correlation between the particle size and its influence area. A strong link between island height and radius indicates that particles are close to equilibrium. Indeed, the value derived for contact angle (adhesion energy) compares well with tabulated data. In addition, the cluster size before the onset of coalescence compares with that of the gold particles at the maximum of catalytic activity for the oxidation of CO.

Lazzari, Remi; Jupille, Jacques [Institut des NanoSciences de Paris, Universites Pierre et Marie Curie (Paris 6) et Denis Diderot (Paris 7), CNRS UMR 7588 Campus Boucicaut, 140 Rue de Lourmel, 75015 Paris (France); Renaud, Gilles [Nanostructures et Rayonnement Synchrotron, Service de Physique des Materiaux et Microstructures, Departement de Recherche Fondamentale sur la Matiere Condensee, Commissariat a l'Energie Atomique, 17 Avenue des Martyrs, F-38054 Grenoble, Cedex 9 (France); Leroy, Frederic [Centre de Recherche en Matiere Condensee et NanoSciences, CNRS-UPR 7281, Campus de Luminy Case 913, 13288 Marseille Cedex 09 (France)

2007-09-15T23:59:59.000Z

82

Neutron and X-Ray Scattering - Argonne National Laboratories, Materials  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Home Home Neutron and X-Ray Scattering Neutron and X-ray Scattering Science Recent advances in neutron and x-ray scattering instrumentation at major DOE facilities such as the Spallation Neutron Source and Advanced Photon Source provide unprecedented insights into complex phenomena in bulk and interfacial materials. The vision of our group is to harness the complementarity of neutrons and x-rays to study how materials respond on a range of length and time scales to phase competition, so that we can learn to control emergent behavior and generate functional properties in energy-related materials. We use neutrons and x-rays to investigate the structure and dynamics of bulk and interfacial materials with properties that are useful for energy applications, such as superconductivity, magnetism and thermoelectricity. Phase competition can generate or enhance such properties, but it is extremely challenging to characterize fluctuations in the competing order, whether in bulk disordered materials, or artificial heterostructures. Our goal is to utilize efficient techniques that we have been developing for measuring nanoscale phase fluctuations, both static and dynamic, to enable the rational design of new materials for energy within MSD.

83

Accepted Manuscript Using Small Angle Solution Scattering Data in Xplor-NIH Structure Calcula-  

E-Print Network [OSTI]

and wide angle X-ray and small angle neutron scattering for biomolecular structure calculation using and wide angle X-ray scattering (SAXS/WAXS) and small angle neutron scattering (SANS) data, on the otherAccepted Manuscript Using Small Angle Solution Scattering Data in Xplor-NIH Structure Calcula

Clore, G. Marius

84

MeV-Energy X Rays from Inverse Compton Scattering with Laser-Wakefield Accelerated Electrons  

Science Journals Connector (OSTI)

We report the generation of MeV x rays using an undulator and accelerator that are both driven by the same 100-terawatt laser system. The laser pulse driving the accelerator and the scattering laser pulse are independently optimized to generate a high energy electron beam (>200??MeV) and maximize the output x-ray brightness. The total x-ray photon number was measured to be ?1107, the source size was 5???m, and the beam divergence angle was ?10??mrad. The x-ray photon energy, peaked at 1MeV (reaching up to 4MeV), exceeds the thresholds of fundamental nuclear processes (e.g., pair production and photodisintegration).

S. Chen; N. D. Powers; I. Ghebregziabher; C. M. Maharjan; C. Liu; G. Golovin; S. Banerjee; J. Zhang; N. Cunningham; A. Moorti; S. Clarke; S. Pozzi; D. P. Umstadter

2013-04-10T23:59:59.000Z

85

X-ray and neutron scattering from nano-mgantic clusters | The...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-ray and neutron scattering from nano-mgantic clusters The student will participate in hands on X-ray scattering experiments on bio-inspired inorganic materials (i.e., magnetic...

86

High Resolution X-Ray Scattering at Sector 3, Advanced Photon...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Sector 3 Beamlines Staff Publications Conferences IXN group Sector 3 : High Resolution X-ray Scattering Sector 3 is operated by the Inelastic X-ray Nuclear Resonant Scattering...

87

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Wednesday, 30 May 2012 00:00 In principle, tri-block copolymers...

88

Diffuse scattering of hard x rays from rough surfaces  

Science Journals Connector (OSTI)

The diffuse scattering of hard x rays from rough solid surfaces has been measured and described quantitatively in terms of an improved distorted-wave Born approximation. The rough surface is characterized by the rms roughness ?, the height-height correlation length ?, and the roughness exponent h. The value for ? is in excellent agreement with that deduced from reflectivity. The significance of the parameters ?, ?, and h is tested by comparison with the results obtained from scanning force mircoscopy.

Wolfgang Weber and Bruno Lengeler

1992-09-15T23:59:59.000Z

89

National School on Neutron and X-ray Scattering August 10-24, 2013  

E-Print Network [OSTI]

National School on Neutron and X-ray Scattering August 10-24, 2013 Argonne National Laboratory National Laboratory 3:15 ­ 3:30 Break #12;National School on Neutron and X-ray Scattering August 10 Dinner Week 1 wrap-up Picnic #12;National School on Neutron and X-ray Scattering August 10-24, 2012 Oak

Kemner, Ken

90

CHEMICAL APPLICATIONS OF INELASTIC X-RAY SCATTERING  

SciTech Connect (OSTI)

Inelastic x-ray scattering (IXS), complementary to other more established inelastic scattering probes, such as light scattering, electron scattering, and neutron scattering, is becoming an important experimental technique in the study of elementary excitations in condensed matters. Over the past decade, IXS with total energy resolution of few meV has been achieved, and is being used routinely in the study of phonon dispersions in solids and liquids as well as dynamics in disordered and biological systems. In the study of electronic excitations, IXS with total energy resolution on the order of 100 meV to 1 eV is gaining wider applications also. For example, IXS has been used to study collective excitations of valence electrons, single electron excitations of valence electrons, as well as core electron excitations. In comparison with the alternative scattering techniques mentioned above, IXS has several advantages. First, IXS probes the full momentum transfer range of the dielectric response of the sample, whereas light scattering is limited to very small momentum transfers, and electron scattering suffers the effects of multiple scattering at large momentum transfers. Second, since IXS measures the bulk properties of the sample it is not surface sensitive, therefore it does not require special preparation of the sample. The greater flexibility in sample conditions and environments makes IXS an ideal probe in the study of liquids and samples under extreme temperature, pressure, and magnetic field. Third, the tunability of synchrotron radiation sources enables IXS to exploit element specificity and resonant enhancement of scattering cross sections. Fourth, IXS is unique in the study of dynamics of liquids and amorphous solids because it can probe the particular region of energy-momentum transfer phase space, which is inaccessible to inelastic neutron scattering. On the other hand, the main disadvantages of IXS are the small cross sections and the strong absorption of x-rays in high Z elements.

HAYASHI,H.; UDAGAWA,Y.; GILLET,J.M.; CALIEBE,W.A.; KAO,C.C.

2001-08-01T23:59:59.000Z

91

2011 U.S. National School on Neutron and X-ray Scattering  

SciTech Connect (OSTI)

The 13th annual U.S. National School on Neutron and X-ray Scattering was held June 11 to 25, 2011, at both Oak Ridge and Argonne National Laboratories. This school brought together 65 early career graduate students from 56 different universities in the US and provided them with a broad introduction to the techniques available at the major large-scale neutron and synchrotron x-ray facilities. This school is focused primarily on techniques relevant to the physical sciences, but also touches on cross-disciplinary bio-related scattering measurements. During the school, students received lectures by over 30 researchers from academia, industry, and national laboratories and participated in a number of short demonstration experiments at Argonne's Advanced Photon Source (APS) and Oak Ridge's Spallation neutron Source (SNS) and High Flux Isotope Reactor (HFIR) facilities to get hands-on experience in using neutron and synchrotron sources. The first week of this year's school was held at Oak Ridge National Lab, where Lab director Thom Mason welcomed the students and provided a shitorical perspective of the neutron and x-ray facilities both at Oak Ridge and Argonne. The first few days of the school were dedicated to lectures laying out the basics of scattering theory and the differences and complementarity between the neutron and x-ray probes given by Sunil Sinha. Jack Carpenter provided an introduction into how neutrons are generated and detected. After this basic introduction, the students received lectures each morning on specific techniques and conducted demonstration experiments each afternoon on one of 15 different instruments at either the SNS or HFIR. Some of the topics covered during this week of the school included inelastic neutron scattering by Bruce Gaulin, x-ray and neutron reflectivity by Chuck Majkrazak, small-angle scattering by Volker Urban, powder diffraction by Ashfia Huq and diffuse scattering by Gene Ice.

Lang, Jonathan [Argonne National Laboratory (ANL); te Vethuis, Suzanne [Argonne National Laboratory (ANL); Ekkebus, Allen E [ORNL; Chakoumakos, Bryan C [ORNL; Budai, John D [ORNL

2012-01-01T23:59:59.000Z

92

National School on Neutron and X-ray Scattering June 14-28, 2014  

E-Print Network [OSTI]

National School on Neutron and X-ray Scattering June 14-28, 2014 Argonne National Laboratory:00 Dinner Dinner Dinner Dinner Week 1 wrap-up Picnic #12;National School on Neutron and X-ray Scattering Restaurant 9:45 - 10:45 Lecture Interaction of X-rays and Neutrons with Matter Roger Pynn University

Kemner, Ken

93

Large-scale Nanostructure Simulations from X-ray Scattering Data On Graphics Processor Clusters  

SciTech Connect (OSTI)

X-ray scattering is a valuable tool for measuring the structural properties of materialsused in the design and fabrication of energy-relevant nanodevices (e.g., photovoltaic, energy storage, battery, fuel, and carbon capture andsequestration devices) that are key to the reduction of carbon emissions. Although today's ultra-fast X-ray scattering detectors can provide tremendousinformation on the structural properties of materials, a primary challenge remains in the analyses of the resulting data. We are developing novelhigh-performance computing algorithms, codes, and software tools for the analyses of X-ray scattering data. In this paper we describe two such HPCalgorithm advances. Firstly, we have implemented a flexible and highly efficient Grazing Incidence Small Angle Scattering (GISAXS) simulation code based on theDistorted Wave Born Approximation (DWBA) theory with C++/CUDA/MPI on a cluster of GPUs. Our code can compute the scattered light intensity from any givensample in all directions of space; thus allowing full construction of the GISAXS pattern. Preliminary tests on a single GPU show speedups over 125x compared tothe sequential code, and almost linear speedup when executing across a GPU cluster with 42 nodes, resulting in an additional 40x speedup compared to usingone GPU node. Secondly, for the structural fitting problems in inverse modeling, we have implemented a Reverse Monte Carlo simulation algorithm with C++/CUDAusing one GPU. Since there are large numbers of parameters for fitting in the in X-ray scattering simulation model, the earlier single CPU code required weeks ofruntime. Deploying the AccelerEyes Jacket/Matlab wrapper to use GPU gave around 100x speedup over the pure CPU code. Our further C++/CUDA optimization deliveredan additional 9x speedup.

Sarje, Abhinav; Pien, Jack; Li, Xiaoye; Chan, Elaine; Chourou, Slim; Hexemer, Alexander; Scholz, Arthur; Kramer, Edward

2012-01-15T23:59:59.000Z

94

Neutron and X-ray Scattering Studies of Strongly Correlated Electron Systems  

E-Print Network [OSTI]

Neutron and X-ray Scattering Studies of Strongly Correlated Electron Systems Russell A. Ewings 2008 #12;Abstract Neutron and X-ray Scattering Studies of Strongly Correlated Electron Systems Russell-ray scattering and neutron scattering experiments on several strongly correlated transition metal oxides

Boothroyd, Andrew

95

Air-core grid for scattered x-ray rejection  

DOE Patents [OSTI]

The invention is directed to a grid used in x-ray imaging applications to block scattered radiation while allowing the desired imaging radiation to pass through, and to process for making the grid. The grid is composed of glass containing lead oxide, and eliminates the spacer material used in prior known grids, and is therefore, an air-core grid. The glass is arranged in a pattern so that a large fraction of the area is open allowing the imaging radiation to pass through. A small pore size is used and the grid has a thickness chosen to provide high scatter rejection. For example, the grid may be produced with a 200 {micro}m pore size, 80% open area, and 4 mm thickness. 2 figs.

Logan, C.M.; Lane, S.M.

1995-10-03T23:59:59.000Z

96

Lipid Bilayer Structure Determined by the Simultaneous Analysis of Neutron and X-Ray Scattering Data  

E-Print Network [OSTI]

Lipid Bilayer Structure Determined by the Simultaneous Analysis of Neutron and X-Ray Scattering) and dipalmitoylphosphatidylcholine (DPPC) bilayers by simultaneously analyzing x-ray and neutron scattering data. The neutron data electron and neutron scattering density profiles. A key result of the analysis is the molecular surface

Nagle, John F.

97

Resonant soft x-ray scattering: elemental/chemical specific probe...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant soft x-ray scattering: elementalchemical specific probe of reciprocal space and ordered structure Wednesday, October 15, 2014 - 3:00pm SLAC, Redtail Hawk Conference Room...

98

X-ray and neutron scattering studies on some nanoscale structures in molecular biology.  

E-Print Network [OSTI]

??Scattering of X-rays and neutrons has been applied to the study of nanostructures with interesting biological functions. The systems studied were the protein calmodulin and (more)

Ikonen, Teemu

2007-01-01T23:59:59.000Z

99

Determination of interfacial roughness using X-ray scattering  

SciTech Connect (OSTI)

Crystal truncation rod (CTR) scattering is shown to be a powerful technique for determining interfacial roughness non-destructively. By measuring the decay of scattering away from a Bragg reflection in the surface direction an rms roughness of the surface or interface can be extracted. The authors obtain rms roughness values with an accuracy of {+-} 0.1 {angstrom}. Sensitivity to lateral length scale roughness ranges from the wavelength of the x-rays to between 1,000--10,000 {angstrom} depending on the instrument function and the specific truncation rod. The influence of different cleans, as well as the thermal oxidation process, on the Si-SiO{sub 2} interface is investigated. A hot water treatment prior to the thermal oxidation is shown to roughen the Si-SiO{sub 2} interface. CTR scattering results also show a smoothing of the interface as a result of the oxidation process even for as little as 60 {angstrom} of thermal oxidation. Comparison between AFM and CTR scattering gives a consistent picture of the relative roughness of the wafers, although the absolute numbers do not agree. The differences in the absolute values can be explained by the lateral roughness scale that the two techniques measure, indicating that it is at periodicities below {approx} 100 {angstrom} that the increased roughness observed by the x-ray is found. Crystal truncation rods are shown to be perpendicular to the surface and not along the crystallographic axes of a miscut crystal. It is shown that for a crystal terminated by a regular step array both an atomistic and a continuum description of CTR scattering give identical results. Furthermore, the atomistic approach is used to show that a diamond cubic surface with a miscut is inherently rough. Even for a small miscut the tilt of the CTR with respect to the crystallographic axes results in complications for measuring the rod intensity. The authors present schemes for determining the exact position of the CTR in reciprocal space and for measuring the miscut of a single crystal. These methods were applied to the measurement of CTR intensities of silicon(001) wafers with miscuts of 0.1 and 4 degrees.

Munkholm, A.

1997-05-01T23:59:59.000Z

100

Solution-Phase Structure of an Artificial Foldamer:? X-ray Scattering Study  

Science Journals Connector (OSTI)

Foldamers provide important insights into the fundamentals of noncovalent folding, which is of primary importance for understanding biological systems and developing novel self-assembling materials. ... This work was supported by the National Science Foundation under Grant CHE 03-45254 (J.S.M.) and by the Division of Chemical Sciences, Office of Basic Energy Sciences, DOE under Grant DE-FG02-99ER14999 (M.R.W.). ... Small-angle scattering (SAS) of x-rays and neutrons is a fundamental tool in the study of biol. ...

Richard F. Kelley; Boris Rybtchinski; Matthew T. Stone; Jeffrey S. Moore; Michael R. Wasielewski

2007-03-17T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


101

The Role of Surface X-ray Scattering in Electrocatalysis  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

3 3 N. M. Markovi , LBNL and C. A. Lucas, University of Liverpool Ecological and political realities have moved discussions of, and advances in, fuel cell technology into mainstream public awareness. Electrocatalysis, the science of modifying the overall rates of electrochemical reactions so that selectivity, yield and efficiency are maximized, is the work from which those advances spring. Studies in electrocatalysis have resulted in highly selective multicomponent gas mixture sensors, human blood component sensors, new electrocatalysts for oxidation/reduction of inorganic and organic pollutants in air and water, as well as better electrocatalysts for the fuel cell conversion of renewable and fossil fuels to electrical work. Studies of the mechanisms by which these catalysts operate have been advanced through development of in-situ surface x-ray scattering (SXS) techniques. SXS capabilities at SSRL were recently used to investigate the interface structure of an ultrathin COad (adsorbed carbon monoxide) overlayer on platinum. This work has elevated the macroscopic description of the COad state at the solid-liquid interface to a microscopic level and enabled the relation between the reactivity and the interfacial structure of COad/Pt to be understood.

102

Doppler effects in resonant x-ray Raman scattering  

Science Journals Connector (OSTI)

Theory for Doppler effects in resonant x-ray Raman scattering (RXS) is presented. It is shown that the electron Doppler effect is important in nonradiative RXS for decay transitions between continuum nuclear states lying above the dissociation threshold, and that the averaging of the RXS cross section over molecular orientations can lead to strong non-Lorentzian broadenings of the atomiclike resonances. The Doppler effect is found to give a unique possibility to distinguish dissociating identical atoms, because different peaks correspond to atoms with opposite Doppler shifts. Spectral features of the atomiclike profile are predicted and analyzed. Strong oscillations of the RXS cross section will occur as a consequence of the interference of the Auger electrons. Due to the Doppler effect and the interference, the atomiclike profile can be associated with supernarrow spectral features, the width of which goes below the lifetime broadening and is practically independent of the spectral distribution of the incident radiation. As another consequence of the oscillations and strong anisotropy caused by the interference, we predict parity selection rules for Auger decay transitions in both bound and dissociative systems. The corresponding experiments can be realized by measurements of resonant Auger of surface adsorbed molecules and for molecules by the electron-ion coincidence technique.

Faris Gelmukhanov; Hans gren; Pawe? Sa?ek

1998-04-01T23:59:59.000Z

103

Wide-angle point-to-point x-ray imaging with almost arbitrarily large angles of incidence  

SciTech Connect (OSTI)

The paper describes a new scheme for wide-angle point-to-point x-ray imaging with almost arbitrarily large angles of incidence by a matched pair of spherically bent crystals to eliminate the astigmatism, which is a well-known imaging error of spherical mirrors. In addition to x rays, the scheme should be applicable to a very broad spectrum of the electromagnetic radiation, including microwaves, infrared and visible light, as well as UV and extreme UV radiation, if the crystals are replaced with appropriate spherical reflectors. The scheme may also be applicable to the imaging with ultrasound.

Bitter, M.; Hill, K. W.; Scott, S.; Feder, R. [Princeton Plasma Physics Laboratory, Princeton, New Jersey 08543 (United States); Ko, Jinseok; Ince-Cushman, A.; Rice, J. E. [Plasma Science and Fusion Center, Cambridge, Massachusetts 02139 (United States)

2008-10-15T23:59:59.000Z

104

Small-Angle Neutron Scattering Studies of Charged Carboxyl-Terminated Dendrimers in Solutions  

E-Print Network [OSTI]

Small-Angle Neutron Scattering Studies of Charged Carboxyl-Terminated Dendrimers in Solutions Q. R-angle neutron scattering was used to characterize the solution behavior of charged carboxylic acid terminated- copy,16 small-angle X-ray scattering,17 and small-angle neutron scattering (SANS),18-25 have been used

Dubin, Paul D.

105

A Miniature Maxthal Furnace for X-ray Spectroscopy and Scattering Experiments up to 1200 degrees C  

SciTech Connect (OSTI)

We have built a new small furnace to perform high temperature studies up to 1200 deg. C in vacuum or in oxygen atmosphere. This furnace was originally used as a catalytic reactor optimized for the in situ X-ray Absorption Spectroscopy experiments on beamline ID24. It has now been redesigned for use on the ESRF beamline ID01 for in situ Grazing Incidence Small Angle X-ray Scattering experiments. For these experiments high mechanical stability of the sample holder is necessary to keep the alignment of the sample during heating.

Gorges, Bernard; Vitoux, Hugo; Redondo, Pablo; Carbone, Gerardina [ESRF, BP220 38043 Grenoble CEDEX (France); Mocouta, Cristian [SOLEIL -BP48 91192 Gif-sur-Yvette CEDEX (France); Guilera, Gemma [ALBA CELLS 08290 Cerdanoyla Del Valles Barcelona (Spain)

2010-06-23T23:59:59.000Z

106

Protein folding and protein metallocluster studies using synchrotron small angler X-ray scattering  

SciTech Connect (OSTI)

Proteins, biological macromolecules composed of amino-acid building blocks, possess unique three dimensional shapes or conformations which are intimately related to their biological function. All of the information necessary to determine this conformation is stored in a protein`s amino acid sequence. The problem of understanding the process by which nature maps protein amino-acid sequences to three-dimensional conformations is known as the protein folding problem, and is one of the central unsolved problems in biophysics today. The possible applications of a solution are broad, ranging from the elucidation of thousands of protein structures to the rational modification and design of protein-based drugs. The scattering of X-rays by matter has long been useful as a tool for the characterization of physical properties of materials, including biological samples. The high photon flux available at synchrotron X-ray sources allows for the measurement of scattering cross-sections of dilute and/or disordered samples. Such measurements do not yield the detailed geometrical information available from crystalline samples, but do allow for lower resolution studies of dynamical processes not observable in the crystalline state. The main focus of the work described here has been the study of the protein folding process using time-resolved small-angle x-ray scattering measurements. The original intention was to observe the decrease in overall size which must accompany the folding of a protein from an extended conformation to its compact native state. Although this process proved too fast for the current time-resolution of the technique, upper bounds were set on the probable compaction times of several small proteins. In addition, an interesting and unexpected process was detected, in which the folding protein passes through an intermediate state which shows a tendency to associate. This state is proposed to be a kinetic molten globule folding intermediate.

Eliezer, D.

1994-06-01T23:59:59.000Z

107

High-pressure structural studies of dysprosium using angle-dispersive x-ray diffraction  

SciTech Connect (OSTI)

We present structural results under pressure for elemental dysprosium (Dy) up to 87 GPa using in situ angle-dispersive x-ray diffraction measurements with synchrotron x rays and a diamond-anvil cell. Dy exhibits the structural transition sequence, hP2{yields}hR9{yields}hP4{yields}distorted cF4, from Rietveld full-profile refinements. Clear evidence is documented for the high-pressure distorted cF4 phase observed above 45 GPa to be an orthorhombic oS8 (Cmmm) structure for Dy in the lanthanide phase diagram.

Shen Yongrong; Kumar, Ravhi S.; Cornelius, Andrew L.; Nicol, Malcolm F. [Department of Physics and High Pressure Science and Engineering Center, University of Nevada Las Vegas, Las Vegas, Nevada 89154-4002 (United States)

2007-02-01T23:59:59.000Z

108

Acquisition of an In-House X-ray Scattering Facility for Nanostructure Characterization and Student Training  

SciTech Connect (OSTI)

This equipment grant was specifically dedicated to the development of a "state of the art" x-ray scattering facility...

Schuller, Ivan K [UC San Diego

2013-08-02T23:59:59.000Z

109

Photon Sciences | Beamlines | CSX: Coherent Soft X-ray Scattering and  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

CSX: Coherent Soft X-ray Scattering and polarization CSX: Coherent Soft X-ray Scattering and polarization X-Ray 1 Poster | X-Ray 2 Poster | Fact Sheet | Preliminary Design Report Scientific Scope The Coherent Soft X-ray Scattering and Polarization (CSX) beamline design (source and optics) has been optimized to the NSLS-II parameters to provide the highest possible flux for experiments requiring either high coherence or full control of the polarization. Beamline Description The CSX beamline will be served by two identical EPU49 sources. Both EPUs are planned to operate in a canted geometry with opposite circular polarization for fast polarization switching experiments at the full polarization control (PC) branch. The EPUs will also be able to operate "phased" as a single device for high coherent flux experiments at the

110

16th National School on Neutron and X-ray Scattering  

ScienceCinema (OSTI)

Students talk about their experience at the 16th National School on Neutron and X-ray Scattering, or NXS 2014. Jointly conducted by Oak Ridge and Argonne national laboratories, NXS immerses graduate students in national user facilities to learn in a hands-on environment how to use neutrons and X-rays in their research.

Chakoumakos, Bryan; Achilles, Cherie; Cybulskis, Viktor; Gilbert, Ian

2014-07-23T23:59:59.000Z

111

16th National School on Neutron and X-ray Scattering  

SciTech Connect (OSTI)

Students talk about their experience at the 16th National School on Neutron and X-ray Scattering, or NXS 2014. Jointly conducted by Oak Ridge and Argonne national laboratories, NXS immerses graduate students in national user facilities to learn in a hands-on environment how to use neutrons and X-rays in their research.

Chakoumakos, Bryan; Achilles, Cherie; Cybulskis, Viktor; Gilbert, Ian

2014-07-02T23:59:59.000Z

112

Search for Photon-Photon Elastic Scattering in the X-ray Region  

E-Print Network [OSTI]

We report the first results of a search for real photon-photon scattering using X rays. A novel system is developed to split and collide X-ray pulses by applying interferometric techniques. A total of $6.5\\times10^{5}$ pulses (each containing about $10^{11}$ photons) from an X-ray Free-Electron Laser are injected into the system. No scattered events are observed, and an upper limit of $1.7\\times 10^{-24}$ ${\\rm m^{2}}$ (95% C.L.) is obtained on the photon-photon elastic scattering cross section at 6.5 keV.

T. Inada; T. Yamaji; S. Adachi; T. Namba; S. Asai; T. Kobayashi; K. Tamasaku; Y. Tanaka; Y. Inubushi; K. Sawada; M. Yabashi; T. Ishikawa

2014-04-18T23:59:59.000Z

113

X Ray Scattering | U.S. DOE Office of Science (SC)  

Office of Science (SC) Website

X Ray Scattering X Ray Scattering Materials Sciences and Engineering (MSE) Division MSE Home About Research Areas Energy Frontier Research Centers (EFRCs) DOE Energy Innovation Hubs BES Funding Opportunities The Computational Materials and Chemical Sciences Network (CMCSN) Theoretical Condensed Matter Physics Scientific Highlights Reports and Activities Principal Investigators' Meetings BES Home Research Areas X Ray Scattering Print Text Size: A A A RSS Feeds FeedbackShare Page This activity supports basic research on the fundamental interactions of photons with matter to achieve an understanding of atomic, electronic, and magnetic structures and excitations and their relationships to materials properties. The main emphasis is on x-ray scattering, spectroscopy, and imaging research, primarily at major BES-supported user facilities.

114

The Step Roughening of the Cu(113) Surface: A Grazing Incidence X-Ray Scattering Study  

Science Journals Connector (OSTI)

In conjunction with the development of high brilliance synchrotron sources, the grazing incidence x-ray scattering (GIXS) technique is emerging as an important structural probe for surface and interface studies [...

K. S. Liang; E. B. Sirota; K. L. DAmico; G. J. Hughes

1988-01-01T23:59:59.000Z

115

National School on Neutron and X-Ray Scattering Held at APS&IPNS  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

August 14th, 2000 National School on Neutron and X-Ray Scattering Held at APS & IPNS During the two-week period of August 14-26, 2000 Argonne National Laboratory once again hosted...

116

Safety & Security Guidelines Annual U.S. National School on Neutron and X-ray Scattering  

E-Print Network [OSTI]

Safety & Security Guidelines 15th Annual U.S. National School on Neutron and X-ray Scattering-574-4600. Neutron Sciences User Programs and Outreach Office Oak Ridge National Laboratory #12;

117

National School on Neutron and X-ray Scattering | Argonne National...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Questions Program Details NX School Partners Contact education@anl.gov National School on Neutron & X-ray Scattering June 14-28, 2014 About the School The main purpose of the...

118

Inelastic X-Ray Scattering at Sector 30, Advanced Photon Source  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

synchrotron radiation produced at the APS to study a wide variety of complex materials with inelastic x-ray scattering. Please feel free to explore our site and learn more...

119

Observation of correlated X-ray scattering at atomic resolution  

Science Journals Connector (OSTI)

...order, such as proteins in solution...to study such disordered matter. The...X-rays from an ensemble of identical...signal from an ensemble in three dimensions...experiments on disordered ensembles-such as proteins in solution-may...

2014-01-01T23:59:59.000Z

120

X-ray resonant magnetic scattering from structurally and magnetically rough interfaces in multilayered systems. I. Specular reflectivity  

E-Print Network [OSTI]

X-ray resonant magnetic scattering from structurally and magnetically rough interfaces formulation of x-ray resonant magnetic scattering from rough surfaces and interfaces is given for specular/Fe multilayer. DOI: 10.1103/PhysRevB.68.224409 PACS number s : 75.70.Cn, 61.10.Kw I. INTRODUCTION X-ray

Haskel, Daniel

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


121

X-ray dark-field imaging modeling * F. Pfeiffer,2  

E-Print Network [OSTI]

X-ray dark-field imaging modeling W. Cong,1, * F. Pfeiffer,2 M. Bech,2 and G. Wang1 1 Biomedical-field images are formed from x-ray small-angle scattering signals. The small-angle scattering signals to describe the relationship between x-ray small-angle scattering coefficients of an object and dark

Wang, Ge

122

International Conference on Surface X-ray and Neutron Scattering (SXNS-11)  

SciTech Connect (OSTI)

The 11th International Surface X-ray and Neutron Scattering (SXNS) Conference was held on July 13-17, 2010, on the Northwestern University (NU) campus, in Evanston Illinois and hosted by the NU Materials Research Science and Engineering Center. This biennial conference brought together a community of 164 attendees from 16 countries. The field now makes use of a broad range of new experimental capabilities that have been made possible through the development of increasingly brilliant X-ray and neutron sources around the world, including third generation synchrotron sources, neutron reactor and spallation sources, as well as the recent development of X-ray lasers.

Michael J. Bedzyk

2011-06-17T23:59:59.000Z

123

Measurements of Ionic Structure in Shock Compressed Lithium Hydride from Ultrafast X-Ray Thomson Scattering  

SciTech Connect (OSTI)

We present the first ultrafast temporally, spectrally, and angularly resolved x-ray scattering measurements from shock-compressed matter. The experimental spectra yield the absolute elastic and inelastic scattering intensities from the measured density of free electrons. Laser-compressed lithium-hydride samples are well characterized by inelastic Compton and plasmon scattering of a K-alpha x-ray probe providing independent measurements of temperature and density. The data show excellent agreement with the total intensity and structure when using the two-species form factor and accounting for the screening of ion-ion interactions.

Kritcher, A. L. [L-399, Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551 (United States); Department of Nuclear Engineering, University of California Berkeley, Berkeley, California 94709 (United States); Neumayer, P.; Doeppner, T.; Landen, O. L.; Glenzer, S. H. [L-399, Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551 (United States); Brown, C. R. D. [Department of Physics, Imperial College, London SW7 2AZ (United Kingdom); AWE plc., Aldermaston, Reading, RG7 4PR (United Kingdom); Davis, P. [L-399, Lawrence Livermore National Laboratory, P.O. Box 808, Livermore, California 94551 (United States); Department of Physics, University of California Berkeley, Berkeley, California 94709 (United States); Falcone, R. W.; Lee, H. J. [Department of Physics, University of California Berkeley, Berkeley, California 94709 (United States); Gericke, D. O.; Vorberger, J.; Wuensch, K. [CFSA, Department of Physics, University of Warwick, Coventry CV4 7AL (United Kingdom); Gregori, G. [Department of Physics, Oxford University, Oxford OX1 3PU (United Kingdom); Holst, B.; Redmer, R. [Universitaet Rostock, Institut fuer Physik, D-18051 Rostock (Germany); Morse, E. C. [Department of Nuclear Engineering, University of California Berkeley, Berkeley, California 94709 (United States); Pelka, A.; Roth, M. [Institut fuer Kernphysik, Technische Universitaet Darmstadt, Darmstadt (Germany)

2009-12-11T23:59:59.000Z

124

Fabrication of high-throughput critical-angle X-ray transmission gratings for wavelength-dispersive spectroscopy  

E-Print Network [OSTI]

The development of the critical-angle transmission (CAT) grating seeks both an order of magnitude improvement in the effective area, and a factor of three increase in the resolving power of future space-based, soft x-ray ...

Bruccoleri, Alexander Robert

2013-01-01T23:59:59.000Z

125

Demonstration of Successful X-ray Thomson Scattering Using Picosecond K-(alpha) X-ray Sources for the Characterization of Dense Heated Matter  

SciTech Connect (OSTI)

We discuss the first successful K-{alpha} x-ray Thomson scattering experiment from solid density plasmas for use as a diagnostic in determining the temperature, density, and ionization state of warm dense matter with picosecond resolution. The development of this source as a diagnostic and stringent requirements for successful K-{alpha} x-ray Thomson scattering are addressed. Data for the experimental techniques described in this paper [1] suggest the capability of single shot characterization of warm dense matter and the ability to use this scattering source at future Free Electron Lasers (FEL) where comparable scattering signal levels are predicted.

Kritcher, A; Neumayer, P; Lee, H J; Doeppner, T; Falcone, R; Glenzer, S; Morse, E C

2008-05-05T23:59:59.000Z

126

THE HARD X-RAY SPECTRUM OF NGC 1365: SCATTERED LIGHT, NOT BLACK HOLE SPIN  

SciTech Connect (OSTI)

Active galactic nuclei (AGNs) show excess X-ray emission above 10 keV compared with extrapolation of spectra from lower energies. Risaliti et al. have recently attempted to model the hard X-ray excess in the type 1.8 AGN NGC 1365, concluding that the hard excess most likely arises from Compton-scattered reflection of X-rays from an inner accretion disk close to the black hole. Their analysis disfavored a model in which the hard excess arises from a high column density of circumnuclear gas partially covering a primary X-ray source, despite such components being required in the NGC 1365 data below 10 keV. Using a Monte Carlo radiative transfer approach, we demonstrate that this conclusion is invalidated by (1) use of slab absorption models, which have unrealistic transmission spectra for partial covering gas, (2) neglect of the effect of Compton scattering on transmitted spectra, and (3) inadequate modeling of the spectrum of scattered X-rays. The scattered spectrum is geometry-dependent and, for high global covering factors, may dominate above 10 keV. We further show that, in models of circumnuclear gas, the suppression of the observed hard X-ray flux by reprocessing may be no larger than required by the ''light bending'' model invoked for inner disk reflection, and the expected emission line strengths lie within the observed range. We conclude that the time-invariant ''red wing'' in AGN X-ray spectra is probably caused by continuum transmitted through and scattered from circumnuclear gas, not by highly redshifted line emission, and that measurement of black hole spin is not possible.

Miller, L. [Department of Physics, Oxford University, Denys Wilkinson Building, Keble Road, Oxford OX1 3RH (United Kingdom); Turner, T. J. [Department of Physics, University of Maryland Baltimore County, Baltimore, MD 21250 (United States)

2013-08-10T23:59:59.000Z

127

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi Center 091 Chemistry Bldg. / College Park, MD 20742  

E-Print Network [OSTI]

X-ray Crystallographic Center (XCC) User Registration Form Peter Y. Zavalij X-ray Crystallographi. or advisor confirmation e-mail X-ray Diffractometer that will be used: User Level and Status Smart Apex2X'Pert Pro MRD (Reflectivity & low angles) Xeuss (Small/Wide Angle X-ray Scattering) Submitting user ­ only

Thirumalai, Devarajan

128

X-Ray Radiation from Nonlinear Thomson Scattering of an Intense Femtosecond Laser on Relativistic Electrons in a Helium Plasma  

E-Print Network [OSTI]

X-Ray Radiation from Nonlinear Thomson Scattering of an Intense Femtosecond Laser on Relativistic laser beam on plasma electrons. A collimated x-ray radiation with a broad continuous spectrum peaked by the ultraintense laser fields. The results show the existence of several physical mecha- nisms for the x-ray

Umstadter, Donald

129

SSRL School 2007 on Hard X-ray Scattering Techniques in MES  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

May 15-17, 2007 SSRL School on Hard X-ray Scattering Techniques in Materials and Environmental Sciences Group photo taken at the SSRL School on Hard X-ray Scattering Techniques in Materials and Environmental Sciences. A large, printable version of this group image is available via clicking on the image. Overview: Modern synchrotron-based X-ray scattering (SR-XRS) techniques offer the ability to probe nano- and atomic-scale structures and order/disorder relationships that critically govern the properties of advanced technological and environmental materials. The high collimation, intensity, and tunability of SR allow the investigation of a wide range of materials, including thin films and interfaces, nanoparticles, amorphous materials, solutions, hydrated and disordered bacteriogenic minerals,

130

SOFT INELASTIC X-RAY SCATTERING (SIX) Group Leader: Ignace Jarrige  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

INELASTIC X-RAY SCATTERING (SIX) INELASTIC X-RAY SCATTERING (SIX) Group Leader: Ignace Jarrige 1 Proposal Team: D. Arena 1 , A. Baron 2 , Y. Cai 1 , Y.-D. Chuang 3 , F. de Groot 4 , J. Guo 3 , J.P. Hill 1 , S. Hulbert 1 , C. McGuinness 5 , R. Reininger 9 , J.E. Rubenson 6 , C. Sanchez-Hanke 1 , T. Schmitt 7 , K. Smith 8 1 Brookhaven National Laboratory, 2 SPring-8, 3 Lawrence Berkeley Laboratory, 4 Utrecht University, 5 Trinity College Dublin, 6 Uppsala University, 7 Paul Scherrer Institute, 8 Boston University, 9 Argonne National Laboratory TECHNIQUE AND CAPABILITIES APPLICATIONS ADDITIONAL INFORMATION * Resonant inelastic x-ray scattering (RIXS) at unprecedented resolution (10 meV @ 1000 eV) to revolutionize study of low energy excitations in many important materials. * Continuously tunable momentum transfer (q) to study the

131

An EXAFS spectroscopic study of solvates of copper(I) and copper(II) in acetonitrile, dimethyl sulfoxide, pyridine, and tetrahydrothiophene solutions and a large-angle X-ray scattering study of the copper(II) acetonitrile solvate in solution  

SciTech Connect (OSTI)

X-ray absorption edge and EXAFS spectra of the acetonitrile, dimethyl sulfoxide, pyridine and tetrahydrothiophene solvated copper(I) ions and the acetonitrile and dimethyl sulfoxide solvated copper(II) ions have been measured in solution. Analysis reveals that the copper(I) solvates are most probably tetrahedral, and the following Cu-solvate bond distances have been found: Cu-N = 1.99(2) [angstrom] in acetonitrile, Cu-O = 2.09(4) [angstrom] in dimethyl sulfoxide, Cu-N = 2.06(1) [angstrom] in pyridine, and Cu-S = 2.30(1) [angstrom] in tetrahydrothiophene. The copper(II) solvates are most probably Jahn-Teller distorted octahedrons, and the following equatorial Cu-solvate bond distances have been found: Cu-N = 1.99(1) [angstrom] in acetonitrile, and Cu-O = 1.98(1) [angstrom] in dimethyl sulfoxide. An 1.0 M solution of copper(II) trifluoromethanesulfonate in acetonitrile has been studied by means of the large-angle X-ray scattering technique, and the following Cu-N and Cu-C distances have been found for the Cu(CH[sub 3]CN)[sub 4][sup 2][sup +] complex: 1.99(1) and 3.12(1) [angstrom], respectively. No solvate molecules in the axial positions could however be seen by any of the technique used. The structure of the tetraaquacopper(I) ion has been assumed to be tetrahedral, and from a correlation between the difference in bond length between the copper(I) and copper(II) solvates and the disproportionation constants of copper(I) in the solvent, the Cu-O bond distance is predicted to be approximately 0.14 [angstrom] longer than the equatorial Cu-O distances in the Jahn-Teller distorted hexaaquacopper(II) complex, thus about 2.13 [angstrom].

Persson, I. (Swedish Univ. of Agricultural Sciences, Uppsala (Sweden)); Penner-Hahn, J.E. (Univ. of Michigan, Ann Arbor (United States) Stanford Univ., CA (United States)); Hodgson, K.O. (Univ. of Michigan, Ann Arbor (United States))

1993-05-26T23:59:59.000Z

132

Elasticity of single-crystalline graphite: Inelastic x-ray scattering study Alexey Bosak and Michael Krisch  

E-Print Network [OSTI]

. IXS overcomes the intrinsic difficulties of inelastic neutron scattering INS -- namely, sample sizeElasticity of single-crystalline graphite: Inelastic x-ray scattering study Alexey Bosak of the five independent elastic moduli of single-crystalline graphite, using inelastic x-ray scattering IXS

Nabben, Reinhard

133

Structural and dynamical studies of superacids and superacidic solutions using neutron and high energy X-ray scattering.  

E-Print Network [OSTI]

?? The diffusive motions of the Brnsted superacid, hydrogen fluoride, have been studied using quasielastic neutron scattering. Neutron and high energy X-ray diffraction measurements on (more)

Molaison, Jamie John

2006-01-01T23:59:59.000Z

134

High-quality quartz single crystals for high-energy-resolution inelastic X-ray scattering analyzers  

Science Journals Connector (OSTI)

High-quality quartz (-SiO2) crystals are characterized, and their use for inelastic X-ray scattering analyzers is presented and discussed.

H?nnicke, M.G.

2013-06-07T23:59:59.000Z

135

Exact limiting relation between the structure factors in neutron and x-ray scattering  

E-Print Network [OSTI]

The ratio of the static matter structure factor measured in experiments on coherent X-ray scattering to the static structure factor measured in experiments on neutron scattering is considered. It is shown theoretically that this ratio in the long-wavelength limit is equal to the nucleus charge at arbitrary thermodynamic parameters of a pure substance (the system of nuclei and electrons, where interaction between particles is pure Coulomb) in a disordered equilibrium state. This result is the exact relation of the quantum statistical mechanics. The experimental verification of this relation can be done in the long wavelength X-ray and neutron experiments.

V. B. Bobrov; S. A. Trigger; S. N. Skovorod'ko

2010-07-11T23:59:59.000Z

136

High energy resolution inelastic x-ray scattering at the SRI-CAT  

SciTech Connect (OSTI)

This report is a combination of vugraphs and two papers. The vugraphs give information on the beamline at the APS for IXS and the science addressable by IXS. They also cover the 10 milli-eV resolution spectrometer and the 200 milli-eV resolution spectrometer. The first paper covers the performance of the focusing Ge(444) backscattering analyzers for the inelastic x-ray scattering. The second paper discusses inelastic x-ray scattering from TiC and Ti single crystals.

Macrander, A.T.

1996-08-01T23:59:59.000Z

137

Spatial frequency spectrum of the x-ray scatter distribution in CBCT projections  

SciTech Connect (OSTI)

Purpose: X-ray scatter is a source of significant image quality loss in cone-beam computed tomography (CBCT). The use of Monte Carlo (MC) simulations separating primary and scattered photons has allowed the structure and nature of the scatter distribution in CBCT to become better elucidated. This work seeks to quantify the structure and determine a suitable basis function for the scatter distribution by examining its spectral components using Fourier analysis.Methods: The scatter distribution projection data were simulated using a CBCT MC model based on the EGSnrc code. CBCT projection data, with separated primary and scatter signal, were generated for a 30.6 cm diameter water cylinder [single angle projection with varying axis-to-detector distance (ADD) and bowtie filters] and two anthropomorphic phantoms (head and pelvis, 360 projections sampled every 1, with and without a compensator). The Fourier transform of the resulting scatter distributions was computed and analyzed both qualitatively and quantitatively. A novel metric called the scatter frequency width (SFW) is introduced to determine the scatter distribution's frequency content. The frequency content results are used to determine a set basis functions, consisting of low-frequency sine and cosine functions, to fit and denoise the scatter distribution generated from MC simulations using a reduced number of photons and projections. The signal recovery is implemented using Fourier filtering (low-pass Butterworth filter) and interpolation. Estimates of the scatter distribution are used to correct and reconstruct simulated projections.Results: The spatial and angular frequencies are contained within a maximum frequency of 0.1 cm{sup ?1} and 7/(2?) rad{sup ?1} for the imaging scenarios examined, with these values varying depending on the object and imaging setup (e.g., ADD and compensator). These data indicate spatial and angular sampling every 5 cm and ?/7 rad (?25) can be used to properly capture the scatter distribution, with reduced sampling possible depending on the imaging scenario. Using a low-pass Butterworth filter, tuned with the SFW values, to denoise the scatter projection data generated from MC simulations using 10{sup 6} photons resulted in an error reduction of greater than 85% for the estimating scatter in single and multiple projections. Analysis showed that the use of a compensator helped reduce the error in estimating the scatter distribution from limited photon simulations by more than 37% when compared to the case without a compensator for the head and pelvis phantoms. Reconstructions of simulated head phantom projections corrected by the filtered and interpolated scatter estimates showed improvements in overall image quality.Conclusions: The spatial frequency content of the scatter distribution in CBCT is found to be contained within the low frequency domain. The frequency content is modulated both by object and imaging parameters (ADD and compensator). The low-frequency nature of the scatter distribution allows for a limited set of sine and cosine basis functions to be used to accurately represent the scatter signal in the presence of noise and reduced data sampling decreasing MC based scatter estimation time. Compensator induced modulation of the scatter distribution reduces the frequency content and improves the fitting results.

Bootsma, G. J. [Department of Medical Biophysics, University of Toronto, Toronto, Ontario M5G 2M9, Canada and Radiation Medicine Program, Princess Margaret Hospital, Toronto, Ontario M5G 2M9 (Canada)] [Department of Medical Biophysics, University of Toronto, Toronto, Ontario M5G 2M9, Canada and Radiation Medicine Program, Princess Margaret Hospital, Toronto, Ontario M5G 2M9 (Canada); Verhaegen, F. [Department of Radiation Oncology (MAASTRO), GROW School for Oncology and Developmental Biology, Maastricht University Medical Center, Maastricht 6201 BN (Netherlands) [Department of Radiation Oncology (MAASTRO), GROW School for Oncology and Developmental Biology, Maastricht University Medical Center, Maastricht 6201 BN (Netherlands); Department of Oncology, Medical Physics Unit, McGill University, Montreal, Quebec H3G 1A4 (Canada); Jaffray, D. A. [Department of Medical Biophysics, University of Toronto, Toronto, Ontario M5G 2M9 (Canada) [Department of Medical Biophysics, University of Toronto, Toronto, Ontario M5G 2M9 (Canada); Radiation Medicine Program, Princess Margaret Hospital, Toronto, Ontario M5G 2M9 (Canada); Ontario Cancer Institute, Princess Margaret Hospital, Toronto, Ontario M5G 2M9 (Canada); Department of Radiation Oncology, University of Toronto, Toronto, Ontario M5G 2M9 (Canada)

2013-11-15T23:59:59.000Z

138

X-ray Scattering Reveals Unusual Growth of Lead on Silicon  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-ray Scattering Reveals Unusual Growth of Lead on Silicon X-ray Scattering Reveals Unusual Growth of Lead on Silicon Most thin films grow on substrates in only three ways: layer by layer, formation of atomic islands, or layers followed by islands. The particular growth mode that a given material will follow crucially depends on the relative magnitudes of the surface energy of the film versus the interfacial energy of the film on the substrate. Recently, a team of researchers from the University of Illinois, Academica Sinica in Taiwan, Georgia Tech, and the City University of Hong Kong has discovered a remarkable anomaly. By means of real-time x-ray scattering measurements, the researchers found that lead films grown on silicon adopt a completely novel pattern of growth. X-ray diffraction images taken with a CCD camera during growth of Pb films on Si(111). The interference fringes yield information about island height and layer thickness. Fig. 1. X-ray diffraction images taken with a CCD camera during growth of Pb films on Si(111). The interference fringes yield information about island height and layer thickness.

139

A time-resolved x-ray scattering experiment for the study of phase transitions and crystallization processes in metallic alloys  

SciTech Connect (OSTI)

An experimental setup to perform high-resolution time-resolved X-ray scattering has been commissioned on the side station of beamline 8-ID at the Advanced Photon Source. A Peltier-cooled diode detector array covering an angle range of 20 degrees is mounted on a 4-circle goniometer and is used to temporally resolve X-ray scattering patterns with a resolution up to 10 ms. Metallic ribbon samples can be quickly heated and cooled from temperatures up to 500 C inside a furnace with controllable atmosphere and equipped with a beryllium window. A description of the setup is presented along with actual results showing time-resolved phase transitions and crystallization processes in AlYNi metallic alloys. These results demonstrate the power of this technique to investigate complex crystallization processes as well as the versatility of this time-resolved X-ray scattering spectrometer.

Pelletier, J. F.; Sutton, M.; Altounian, Z.; Saini, S.; Luriom L. B.; Sandy, A. R.; Lumma, D.; Borthwick, M. A.; Falus, P.; Mochrie, S. G. J.; Stephenson, G. B.

1999-10-29T23:59:59.000Z

140

E-Print Network 3.0 - angle scattering restraints Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Characterization of Assemblies from Summary: , San Francisco 2001), small-angle X-ray and neutron scattering (KochQB3 et al., 2003), site... subcomplex) are first purified by...

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


141

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering Resonant Soft X-Ray Scattering of Tri-Block Copolymers Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Wednesday, 30 May 2012 00:00 In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

142

Kevin Yager on the Nanoscience of Studying Scattered X-Rays  

SciTech Connect (OSTI)

Kevin Yager, a scientist at Brookhaven Lab's Center for Functional Nanomaterials, discusses his research on materials spanning just billionths of a meter. Yager specializes in making new materials through meticulously guided self-assembly and probing nanoscale structures with a technique called x-ray scattering.

Yager; Kevin

2014-03-31T23:59:59.000Z

143

X-ray scattering study of the average polycyclic aromatic unit in Ledo coal  

Science Journals Connector (OSTI)

Through an X-ray scattering analysis, the short-range structural features, the relationship(s) between the aryl/alkyl carbon ratio, and the size of the average polycyclic aromatic unit in Ledo coal from Makum coalfield, Assam, India, are elucidated.

Boruah, R.K.

2008-01-16T23:59:59.000Z

144

THE SCATTERED X-RAY HALO AROUND NOVA CYGNI 1992: TESTING A MODEL FOR INTERSTELLAR DUST  

E-Print Network [OSTI]

and Jonathan C. Tan Princeton University Observatory, Peyton Hall, Princeton, NJ 08544; draine@astro.princeton.edu, jt@astro.princeton.edu Received 2002 August 15; accepted 2003 May 13 ABSTRACT We use published ROSAT of emission from an O-Ne white dwarf plus a thermal plasma, and X-ray scattering is calculated for a dust

Draine, Bruce T.

145

Alamethicin in lipid bilayers: Combined use of X-ray scattering and MD simulations Jianjun Pan a  

E-Print Network [OSTI]

Alamethicin in lipid bilayers: Combined use of X-ray scattering and MD simulations Jianjun Pan of Biological Sciences, Carnegie Mellon University, Pittsburgh, PA 15213, USA d Canadian Neutron Beam Centre:1PC with varying amounts of alamethicin (Alm). We combine the use of X-ray diffuse scattering

Nagle, John F.

146

E-Print Network 3.0 - angle x-ray studies Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

work as a preionization source... of with and without applying x-ray photons to the HF laser. Since dose rate of the cw x-ray generator is easily Source: Ecole Polytechnique,...

147

HipGISAXS: a high-performance computing code for simulating grazing-incidence X-ray scattering data  

Science Journals Connector (OSTI)

A new massively parallel code for simulation of a grazing-incidence X-ray scattering experiment has been developed. The sample modeling flexibility enables users to simulate scattering patterns for a wide variety of nanostructures and morphologies.

Chourou, S.T.

2013-11-07T23:59:59.000Z

148

Magnetic x-ray scattering at the M{sub 5} absorption edge of Ho  

SciTech Connect (OSTI)

Magnetic x-ray scattering from thin Ho-metal films at M{sub 5} resonance reveals atomic scattering lengths up to 200r{sub 0}--i.e., of the same order of magnitude as predicted theoretically by Hannon et al. [Phys. Rev. Lett. 61, 1245 (1988)]. The photon-energy dependence of first- and second-order magnetic satellites allows a straightforward identification of circular and linear dichroic contributions. A direct comparison to magnetic neutron scattering demonstrates the potential of the method for studies of complex magnetic structures in ultrathin films and highly diluted materials.

Ott, H.; Schierle, E.; Grigoriev, A. Yu.; Kaindl, G.; Weschke, E. [Institut fuer Experimentalphysik, Freie Universitaet Berlin, Arnimallee 14, D-14195 Berlin-Dahlem (Germany); Schuessler-Langeheine, C. [Institut fuer Experimentalphysik, Freie Universitaet Berlin, Arnimallee 14, D-14195 Berlin-Dahlem (Germany); II. Physikalisches Institut, Universitaet zu Koeln, Zuelpicher Str. 77, D-50937 Koeln (Germany); Leiner, V. [Institut fuer Experimentalphysik/Festkoerperphysik, Ruhr-Universitaet Bochum, D-44780 Bochum (Germany); Institut fuer Werkstoffforschung, WFN, GKSS Forschungszentrum, D-21502 Geesthacht (Germany); Zabel, H. [Institut fuer Experimentalphysik/Festkoerperphysik, Ruhr-Universitaet Bochum, D-44780 Bochum (Germany)

2006-09-01T23:59:59.000Z

149

An In-vacuum Diffractometer for Resonant elastic Soft X-ray Scattering  

SciTech Connect (OSTI)

We describe the design, construction, and performance of a 4-circle in-vacuum diffractometer for resonant elastic soft x-ray scattering. The diffractometer, installed on the resonant elastic and inelastic x-ray scattering beamline at the Canadian Light Source, includes 9 in-vacuum motions driven by in-vacuum stepper motors and operates in ultra-high vacuum at base pressure of 2 x 10{sup -10} Torr. Cooling to a base temperature of 18 K is provided with a closed-cycle cryostat. The diffractometer includes a choice of 3 photon detectors: a photodiode, a channeltron, and a 2D sensitive channelplate detector. Along with variable slit and filter options, these detectors are suitable for studying a wide range of phenomena having both weak and strong diffraction signals. Example measurements of diffraction and reflectivity in Nd-doped (La,Sr){sub 2}CuO{sub 4} and thin film (Ga,Mn)As are shown.

D Hawthorn; F He; L Venema; H Davis; A Achkar; J Zhang; R Sutarto; H Wadati; A Radi; et al.

2011-12-31T23:59:59.000Z

150

E-Print Network 3.0 - angle x-ray sky Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Pulsars... you'd . . . Active Galactic . . . X-ray binaries Pulsars and relatives Gamma-ray bursts Gravitational Source: Phinney, E. Sterl - Division of Physics, Mathematics and...

151

Structure and dynamics of cadmium telluride studied by x-ray and inelastic neutron scattering  

SciTech Connect (OSTI)

We present a combined study of density functional theory, x-ray diffraction, and inelastic neutron scattering examining the temperature dependent structure and lattice dynamics of commercially available cadmium telluride. A subtle change in the structure is evinced near 80~K, which manifests also in the measured phonon density of states. There is no change to the long-range ordered structure. The implications of the change in relation to structural defects are discussed.

Niedziela, Jennifer L [ORNL; Stone, Matthew B [ORNL

2014-01-01T23:59:59.000Z

152

Chirality-induced `forbidden' reflections in X-ray resonant scattering  

Science Journals Connector (OSTI)

It is shown that additional Bragg reflections can appear in resonant near-edge X-ray diffraction exclusively owing to the local chirality associated with the left-right asymmetric environment of scattering atoms. This effect occurs even in centrosymmetric crystals, which are not gyrotropic in optics, and some realistic examples are considered in detail (-Fe2O3, LiNbO3 etc.).

Dmitrienko, V.E.

2001-10-26T23:59:59.000Z

153

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

154

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

155

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

156

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

157

Resonant Soft X-Ray Scattering of Tri-Block Copolymers  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print Resonant Soft X-Ray Scattering of Tri-Block Copolymers Print In principle, tri-block copolymers (tri-BCPs), consisting of three chemically distinct polymers covalently joined together at the ends of each polymer chain, can serve as scaffolds and templates for fabricating a vast number of nanostructures. While quantitatively understanding the details of the morphology and the manner in which the different blocks interact with surfaces and interfaces is critical to success, previous experiments have been few. Now, an international team from the United States, Korea, and Japan has succeeded in combining resonant soft x-ray scattering (RSoXS) at ALS Beamline 11.0.1 with transmission electron microscopy tomography (TEMT) and other techniques to unambiguously determine morphologies comprising two nested hexagonally packed arrays of nanoscopic, cylindrical microdomains in the bulk and a core-shell nanostructure in a thin film. Not only has this work revealed a new phase of ABC tri-block copolymer with complicated morphology, it has illustrated the importance of RSoXS as a unique, powerful tool for examining complex, multi-component systems that could not be characterized with conventional methods.

158

Scattering Theory When an x-ray beam (or neutron or light) passes through a material with  

E-Print Network [OSTI]

Scattering Theory When an x-ray beam (or neutron or light) passes through a material radiation is scattered in directions that differ from that of the incident beam. Scattering arises since x of scattered radiation resulting from this process bears a direct relationship to the structure (the pattern

Beaucage, Gregory

159

Effective Long-Range Attraction between Protein Molecules in Solutions Studied by Small Angle Neutron Scattering  

E-Print Network [OSTI]

Neutron Scattering Yun Liu,1 Emiliano Fratini,2 Piero Baglioni,1,2 Wei-Ren Chen,1 and Sow-Hsin Chen1,* 1, Italy (Received 8 February 2005; published 8 September 2005) Small angle neutron scattering intensity neutron and x-ray scattering investigations of proteins suggest the presence of a short-range attractive

Chen, Sow-Hsin

160

Probing Ag nanoparticle surface oxidation in contact with (in)organics: an X-ray scattering and fluorescence yield approach  

Science Journals Connector (OSTI)

An advanced characterization approach to spatially resolve the reactions occurring at the interface between silver nanoparticles and a simple aqueous system is presented. Both phase and chemical distributions were obtained from X-ray scattering and fluorescence yield techniques.

Levard, C.

2011-10-06T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


161

Compact x-ray source based on burst-mode inverse Compton scattering at 100kHz  

E-Print Network [OSTI]

A design for a compact x-ray light source (CXLS) with flux and brilliance orders of magnitude beyond existing laboratory scale sources is presented. The source is based on inverse Compton scattering of a high brightness ...

Bessuille, J.

162

Raman scattering and X-ray diffraction study of the thermal decomposition of an ettringite-group crystal  

Science Journals Connector (OSTI)

...?A Raman scattering and X-ray diffraction study of the thermal decomposition of a naturally occurring, ettringite-group crystal is presented. Raman spectra, ... previous studies that reported higher temperatur...

S. K. Deb; M. H. Manghnani; K. Ross; R. A. Livingston

2003-02-01T23:59:59.000Z

163

E-Print Network 3.0 - angle x-ray absorption Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND Summary: in the atomic and molecular constituents of the atmosphere, and 2) the absorption of incident...

164

E-Print Network 3.0 - angle x-ray diffraction Sample Search Results  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

; Materials Science 60 Page 12 CHESS News Magazine 2005 FacilityHighlight Impact of a Future Energy Recovery Linac Summary: -rolled Aluminum SR X-ray diffraction. Map grain...

165

Z .Reviews in Molecular Biotechnology 74 2000 207 231 X-ray and neutron surface scattering for studying  

E-Print Network [OSTI]

Z .Reviews in Molecular Biotechnology 74 2000 207 231 X-ray and neutron surface scattering,U , Tonya L. Kuhlb , Joyce Y. Wongc , Gregory S. Smitha,1 a Manuel Lujan Jr. Neutron Scattering Center is defined as the Zratio of the number of particles neutrons or .photons elastically and specularly scattered

Kuhl, Tonya L.

166

New X-ray Scattering Facility at Ris National Laboratory Jens Wenzel Andreasen, Dag Werner Breiby, Martin Drews, Martin Meedom Nielsen  

E-Print Network [OSTI]

New X-ray Scattering Facility at Risø National Laboratory Jens Wenzel Andreasen, Dag Werner Breiby, DK-4000 Roskilde, Denmark The new X-ray facility at the Danish Polymer Centre, Risø National

167

Inelastic X-ray scattering experiments on B[subscript 4]C under high static pressures  

SciTech Connect (OSTI)

Boron K-edge inelastic X-ray scattering experiments were performed on clean B{sub 4}C and shock impact recovered boron carbide up to 30 GPa and at ambient temperature to understand the pressure induced bonding changes. The spectral features corresponding to the boron site in the interlinking chain remained unchanged up to 30 GPa. The results of our experiments indicate that pressure induces less distortion to the boron sites and the local amorphization observed in the previous reports are due to the rearrangement of carbon atoms under extreme conditions without affecting the boron environment.

Kumar, Ravhi S.; Dandekar, Dattatraya; Leithe-Jasper, Andres; Tanaka, Takaho; Xiao, Yuming; Chow, Paul; Nicol, Malcolm F.; Cornelius, Andrew L. (UNLV); (MXPL-M); (CIW); (USARL)

2010-05-04T23:59:59.000Z

168

Soft x-ray coherent scattering: Instrument and methods at ESRF ID08  

SciTech Connect (OSTI)

An experimental setup has been developed to perform soft x-ray coherent scattering at beamline ID08 of the European Synchrotron Radiation Facility. An intense coherent beam was obtained by filtering the primary beam with the monochromator and a circular pinhole. A pinhole holder with motorized translations was installed inside the UHV chamber of the diffractometer. The scattered intensity was recorded in reflection geometry with a back-illuminated charge coupled device camera. As a demonstration we report experimental results of resonant magnetic scattering using coherent beam. The degree of coherence is evaluated, and it is shown that, while the vertical coherence is much higher than the horizontal one at the source, the situation is reversed at the diffractometer. The intensity of the coherent beam is also discussed.

Beutier, Guillaume; Marty, Alain; Livet, Frederic; Laan, Gerrit van der; Stanescu, Stefan; Bencok, Peter [DRFMC, SP2M, CEA Grenoble, 17 avenue des Martyrs, 38054 Grenoble Cedex (France); LTPCM, INPG-UJF-CNRS, BP 75, 38402 St. Martin d'Heres (France); Magnetic Spectroscopy Group, Daresbury Laboratory, Warrington WA4 4AD (United Kingdom); ESRF, 6 rue Jules Horowitz, BP 220, 38043 Grenoble Cedex (France)

2007-09-15T23:59:59.000Z

169

Models to analyze small-angle neutron scattering from unilamellar lipid vesicles Norbert Kucerka* and John F. Nagle  

E-Print Network [OSTI]

Models to analyze small-angle neutron scattering from unilamellar lipid vesicles Norbert Kucerka from small-angle neutron scattering of unilamellar vesicles. DOI: 10.1103/PhysRevE.69.051903 PACS discrete diffraction peaks that occur for multilamellar arrays, the scattering of x rays or neutrons from

Nagle, John F.

170

X-ray resonant exchange scattering of rare-earth nickel borocarbides  

SciTech Connect (OSTI)

The purpose of this thesis is to investigate the systematics of the microscopic magnetic order within a series of isostructural compounds and, at the same, to develop the relatively young experimental method of x-ray resonant exchange scattering (XRES). In this thesis, the author presents XRES studies of several rare-earth nickel borocarbides, RNi{sub 2}B{sub 2}C. He shows that XRES, similar to the neutron techniques, allows the determination of the orientation of the magnetic moment by measuring the Q-dependence of the scattered intensity of magnetic Bragg reflections. As samples in this study, he chose the recently discovered family of rare-earth nickel borocarbides, RNi{sub 2}B{sub 2}C, which display a wide variety of magnetic structures. Furthermore, in several of these materials, long range magnetic order coexists with superconductivity over some temperature range.

Detlefs, C.

1997-10-08T23:59:59.000Z

171

Supplementary data for HIV-1 Tat membrane interaction probed using X-ray and neutron scattering, CD, and MD simulations  

E-Print Network [OSTI]

1 Supplementary data for HIV-1 Tat membrane interaction probed using X-ray and neutron scattering- spacing are linearly related. Figure S3. Neutron scattering from stacks of DOPC:DOPE (3:1)/Tat, x=0 of Physics, Rensselaer Polytechnic Institute, 110 Eighth Street, Troy, NY 12180, 3 NIST Center for Neutron

Nagle, John F.

172

Flat panel X-ray detector with reduced internal scattering for improved attenuation accuracy and dynamic range  

DOE Patents [OSTI]

An x-ray detector is disclosed that has had all unnecessary material removed from the x-ray beam path, and all of the remaining material in the beam path made as light and as low in atomic number as possible. The resulting detector is essentially transparent to x-rays and, thus, has greatly reduced internal scatter. The result of this is that x-ray attenuation data measured for the object under examination are much more accurate and have an increased dynamic range. The benefits of this improvement are that beam hardening corrections can be made accurately, that computed tomography reconstructions can be used for quantitative determination of material properties including density and atomic number, and that lower exposures may be possible as a result of the increased dynamic range.

Smith, Peter D. (Santa Fe, NM); Claytor, Thomas N. (White Rock, NM); Berry, Phillip C. (Albuquerque, NM); Hills, Charles R. (Los Alamos, NM)

2010-10-12T23:59:59.000Z

173

E-Print Network 3.0 - accurate x-ray scattering Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

RMS. Figure 8. Example x-ray images taken with a 2 scanning... X-ray imaging tests of Constellation-X SXT mirror segment pairs ... Source: Christian, Eric - Laboratory for High...

174

X-Ray Interactions with Matter from the Center for X-Ray Optics (CXRO)  

DOE Data Explorer [Office of Scientific and Technical Information (OSTI)]

The primary interactions of low-energy x-rays within condensed matter, viz. photoabsorption and coherent scattering, are described for photon energies outside the absorption threshold regions by using atomic scattering factors. The atomic scattering factors may be accurately determined from the atomic photoabsorption cross sections using modified Kramers-Kronig dispersion relations. From a synthesis of the currently available experimental data and recent theoretical calculations for photoabsorption, the angle-independent, forward-scattering components of the atomic scattering factors have been thus semiempirically determined and tabulated here for 92 elements and for the region 50-30,000 eV. Atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction. The incoherent scattering contributions that become significant for the light elements at the higher photon energies are similarly determined. The basic x-ray interaction relations that are used in applied x-ray physics are presented here in terms of the atomic scattering factors. The bulk optical constants are also related to the atomic scattering factors. These atomic and optical relations are applied to the detailed calculation of the reflectivity characteristics of a series of practical x-ray mirror, multilayer, and crystal monochromators. Comparisons of the results of this semiempirical,"atom-like", description of x-ray interactions for the low-energy region with those of experiment and ab initio theory are presented.

Henke, B.L.; Gullikson, E.M.; Davis, J.C.

175

National School on Neutron and X-ray Scattering Building 223 Auditorium, Room B002 September 24 -October 11, 2008 Argonne National Laboratory  

E-Print Network [OSTI]

National School on Neutron and X-ray Scattering Building 223 Auditorium, Room B002 September 24 (HFIR) Neutron Scattering Science Division Oak Ridge Laboratory 10:15 - 10:30 Break 9:30 - 9:45 Break 10 School on Neutron and X-ray Scattering Building 8600, Main Lobby September 24 - October 11, 2008 Oak

Pennycook, Steve

176

Changes in the Atomic Structure through Glass Transition Observed by X-Ray Scattering  

SciTech Connect (OSTI)

The glass transition involves a minor change in the internal energy, and yet the physical and mechanical properties of a glass change dramatically. In order to determine the evolution of the atomic structure through the glass transition, we employed in-situ synchrotron X-ray scattering measurements as a function of temperature on a model material: Zr-Cu-Al metallic glass. We found that the thermal expansion at the atomic level is smaller than the macroscopic thermal expansion, and significantly increases above the glass transition temperature. The observed changes in the pair-distribution function (PDF) are explained in terms of the fluctuations in the local atomic volume and their change through the glass transition.

Egami, Takeshi [ORNL

2012-01-01T23:59:59.000Z

177

In Situ Synchrotron Based X-ray Fluorescence and Scattering Measurements During Atomic Layer Deposition: Initial Growth of HfO2 on Si and Ge Substrates  

SciTech Connect (OSTI)

The initial growth of HfO{sub 2} was studied by means of synchrotron based in situ x-ray fluorescence (XRF) and grazing incidence small angle x-ray scattering (GISAXS). HfO{sub 2} was deposited by atomic layer deposition (ALD) using tetrakis(ethylmethylamino)hafnium and H{sub 2}O on both oxidized and H-terminated Si and Ge surfaces. XRF quantifies the amount of deposited material during each ALD cycle and shows an inhibition period on H-terminated substrates. No inhibition period is observed on oxidized substrates. The evolution of film roughness was monitored using GISAXS. A correlation is found between the inhibition period and the onset of surface roughness.

K Devloo-Casier; J Dendooven; K Ludwig; G Lekens; J DHaen; C Detavernier

2011-12-31T23:59:59.000Z

178

Comment on X-Ray Inelastic Scattering of Li Metal in the Region of Intermediate Momentum Transfer  

Science Journals Connector (OSTI)

The observation of a peak near the Fermi energy in the x-ray inelastic scattering spectrum of lithium has been variously explained as resulting from optical transitions in lithium, and as being attributable to an "oil-Mylar" protective cover. A new experiment sensitive to the surface impurities of the scattering sample and insensitive to instrumental distortion demonstrates that the observed feature is not due to oil or Mylar but rather arises from the lithium scattering process.

N. G. Alexandropoulos and G. G. Cohen

1975-10-27T23:59:59.000Z

179

Structural Model of the 50 S Subunit of Escherichia coli Ribosomes from Solution Scattering: I. X-ray Synchroton Radiation Study  

Science Journals Connector (OSTI)

The application of new methods of small-angle scattering data interpretation to a contrast variation study of the 50 S ribosomal subunit of Escherichia coli in solution is described. The experimental X-ray data from contrast variation with sucrose are analysed in terms of the basic functions in real and the scattering curves from the volume inaccessible to sucrose and from the regions inside this volume occupied mainly by RNA and by proteins are obtained. From these curves models of the shape of the 50 S subunit and its RNA-rich core are evaluated. These two shapes are positioned so that their difference, which approximates the volume occupied by the proteins, produces a scattering curve which is in good agreement with the scattering from the protein moiety.

D.I. Svergun; M.H.J. Koch; I.N. Serdyuk

1994-01-01T23:59:59.000Z

180

Large angle solid state position sensitive x-ray detector system  

DOE Patents [OSTI]

A method and apparatus for x-ray measurement of certain properties of a solid material are disclosed. In distinction to known methods and apparatus, this invention employs a specific fiber-optic bundle configuration, termed a reorganizer, itself known for other uses, for coherently transmitting visible light originating from the scintillation of diffracted x-radiation from the solid material gathered along a substantially one dimensional linear arc, to a two-dimensional photo-sensor array. The two-dimensional photodetector array, with its many closely packed light sensitive pixels, is employed to process the information contained in the diffracted radiation and present the information in the form of a conventional x-ray diffraction spectrum. By this arrangement, the angular range of the combined detector faces may be increased without loss of angular resolution. Further, the prohibitively expensive coupling together of a large number of individual linear diode photodetectors, which would be required to process signals generated by the diffracted radiation, is avoided. 7 figs.

Kurtz, D.S.; Ruud, C.O.

1998-03-03T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


181

Large angle solid state position sensitive x-ray detector system  

DOE Patents [OSTI]

A method and apparatus are disclosed for x-ray measurement of certain properties of a solid material. In distinction to known methods and apparatus, this invention employs a specific fiber-optic bundle configuration, termed a reorganizer, itself known for other uses, for coherently transmitting visible light originating from the scintillation of diffracted x-radiation from the solid material gathered along a substantially one dimensional linear arc, to a two-dimensional photo-sensor array. The two-dimensional photodetector array, with its many closely packed light sensitive pixels, is employed to process the information contained in the diffracted radiation and present the information in the form of a conventional x-ray diffraction spectrum. By this arrangement, the angular range of the combined detector faces may be increased without loss of angular resolution. Further, the prohibitively expensive coupling together of a large number of individual linear diode photodetectors, which would be required to process signals generated by the diffracted radiation, is avoided. 7 figs.

Kurtz, D.S.; Ruud, C.O.

1998-07-21T23:59:59.000Z

182

Large angle solid state position sensitive x-ray detector system  

DOE Patents [OSTI]

A method and apparatus for x-ray measurement of certain properties of a solid material. In distinction to known methods and apparatus, this invention employs a specific fiber-optic bundle configuration, termed a reorganizer, itself known for other uses, for coherently transmitting visible light originating from the scintillation of diffracted x-radiation from the solid material gathered along a substantially one dimensional linear arc, to a two-dimensional photo-sensor array. The two-dimensional photodetector array, with its many closely packed light sensitive pixels, is employed to process the information contained in the diffracted radiation and present the information in the form of a conventional x-ray diffraction spectrum. By this arrangement, the angular range of the combined detector faces may be increased without loss of angular resolution. Further, the prohibitively expensive coupling together of a large number of individual linear diode photodetectors, which would be required to process signals generated by the diffracted radiation, is avoided.

Kurtz, David S. (State College, PA); Ruud, Clay O. (State College, PA)

1998-01-01T23:59:59.000Z

183

Structural investigation of liquid acetic acid by neutron scattering, DFT calculations and molecular dynamics simulations. Complementarity to x-ray scattering results  

Science Journals Connector (OSTI)

Abstract Neutron scattering experiments have been performed on fully deuterated liquid acetic acid (AA) at room temperature and atmospheric pressure. The scattering data are analyzed to yield the structure factor SM(Q), the molecular form factor F1(Q) and the pair correlation function g(r). To describe the intermolecular arrangement of the liquid, we have considered two dimers and two trimers, involving the isomer cis, already described in our x-ray scattering study. Neutron scattering data show that the local order of the liquid is well described by linear and ring cis trimers. Complementarity with recent x-ray results is then highlighted. Using four force fields, MD simulations show that x-ray and neutron scattering data are better reproduced by both OPLS-AA1 and OPLS-AA2 potentials.

Sonia Fathi; Salah Bouazizi; Sahbi Trabelsi; Miguel Angel Gonzalez; Mohamed Bahri; Salah Nasr; Marie-Claire Bellissent-Funel

2014-01-01T23:59:59.000Z

184

Cost-effective upgrade of a focusing system for inelastic X-ray scattering experiments under high pressure  

Science Journals Connector (OSTI)

This paper describes a scheme utilizing a set of low-cost and compact Kirkpatrick-Baez mirrors for upgrading the optical system of the Taiwan Inelastic X-ray Scattering beamline at SPring-8 for high-pressure experiments using diamond-anvil cells. The scheme as implemented improves the focus to 13 m 16 m with transmission of up to 72%.

Huang, C.-Y.

2007-12-18T23:59:59.000Z

185

Sound velocities of compressed Fe3C from simultaneous synchrotron X-ray diffraction and nuclear resonant scattering measurements  

Science Journals Connector (OSTI)

A recently installed X-ray diffraction facility that is integrated with existing nuclear resonant scattering set-ups at Sector 3 of the Advanced Photon Source at Argonne National Laboratory is introduced. Its applications for measuring the sound velocities of compressed Fe3C are reported.

Gao, L.

2009-09-16T23:59:59.000Z

186

Damage of amorphous carbon induced by soft x-ray femtosecond pulses above and below the critical angle  

SciTech Connect (OSTI)

We present results of damage studies conducted at the Free Electron LASer in Hamburg (FLASH) facility with 13.5 nm (91.8 eV) and 7 nm (177.1 eV) radiations. The laser beam was focused on a sample of 890-nm-thick amorphous carbon coated on a silicon wafer mimicking a x-ray mirror. The fluence threshold for graphitization was determined for different grazing angles above and below the critical angle. The observed angular dependence of F{sub th} is explained by the variation in absorption depth and reflectivity. Moreover, the absorbed local dose needed for the phase transition leading to graphitization is shown to vary with the radiation wavelength.

Chalupsky, J.; Hajkova, V.; Burian, T.; Juha, L.; Vysin, L. [Institute of Physics, Academy of Sciences of the Czech Republic, Na Slovance 2, 182 21 Prague 8 (Czech Republic); Altapova, V.; Sinn, H.; Tschentscher, Th.; Gaudin, J. [European XFEL, DESY, Notkestr., 85 D-22607 Hamburg (Germany); Gleeson, A. J. [CCRLC Daresbury Laboratory, Warrington, Cheshire WA4 4AD (United Kingdom); Jurek, M.; Sobierajski, R. [Institute of Physics, Polish Academy of Sciences, Al. Lotnikow 32/46, PL-02-668 Warsaw (Poland); Stoermer, M. [GKSS-Forschungszentrum Geesthacht GmbH, Max-Planck-Strasse, 1 21502 Geesthach (Germany); Tiedtke, K.; Toleikis, S.; Wabnitz, H. [HASYLAB/DESY, Notkestr., 85 D-22607 Hamburg (Germany)

2009-07-20T23:59:59.000Z

187

Narrowband inverse Compton scattering x-ray sources at high laser intensities  

E-Print Network [OSTI]

Narrowband x- and gamma-ray sources based on the inverse Compton scattering of laser pulses suffer from a limitation of the allowed laser intensity due to the onset of nonlinear effects that increase their bandwidth. It has been suggested that laser pulses with a suitable frequency modulation could compensate this ponderomotive broadening and reduce the bandwidth of the spectral lines, which would allow to operate narrowband Compton sources in the high-intensity regime. In this paper we, therefore, present the theory of nonlinear Compton scattering in a frequency modulated intense laser pulse. We systematically derive the optimal frequency modulation of the laser pulse from the scattering matrix element of nonlinear Compton scattering, taking into account the electron spin and recoil. We show that, for some particular scattering angle, an optimized frequency modulation completely cancels the ponderomotive broadening for all harmonics of the backscattered light. We also explore how sensitive this compensation ...

Seipt, D; Surzhykov, A; Fritzsche, S

2014-01-01T23:59:59.000Z

188

X-Ray Diamond Anvil Cell Facility at NSLS: 2010 Progress Report  

E-Print Network [OSTI]

X-Ray Diamond Anvil Cell Facility at NSLS: 2010 Progress Report Zhiqiang ChenZhiqiang Chen Stony) Powder X-ray Diffraction, Total Scattering Pair-Distributiony , g Function (PDF) under high P and high, yield strength, amorphization, texturing, compressibility Hydrothermal DAC (Bassett) Angle Dispersive X-ray

Duffy, Thomas S.

189

Neutron and X-ray Scattering Techniques have proved so successful in condensed matter studies that a wide variety of sample environments have been developed in consquence. Many  

E-Print Network [OSTI]

Foreword Neutron and X-ray Scattering Techniques have proved so successful in condensed matter whose function is to develop and optimise the techniques appropriate to neutron scattering. Since other neutron and X-ray research centres have similar technical support groups, it was felt timely to unité

Boyer, Edmond

190

Commissioning of a Soft X-ray Beamline PF-BL-16A with a Variable-Included-Angle Varied-Line-Spacing Grating Monochromator  

SciTech Connect (OSTI)

The design and commissioning of a new soft X-ray beamline, BL-16A, at the Photon Factory is presented. The beamline consists of a pre-focusing mirror, an entrance slit, a variable-included-angle varied-line-spacing plane grating monochromator, and a post-focusing system as usual, and provides circularly and linearly polarized soft X rays in the energy range 200-1500 eV with an APPLE-II type undulator. The commissioning procedure for the beamline optics is described in detail, especially the check of the focal position for the zero-th order and diffracted X rays.

Amemiya, Kenta; Toyoshima, Akio; Kikuchi, Takashi; Kosuge, Takashi; Nigorikawa, Kazuyuki; Sumii, Ryohei; Ito, Kenji [Institute of Materials Structure Science, High Energy Accelerator Research Organization, 1-1 Oho, Tsukuba, Ibaraki 305-0801 (Japan)

2010-06-23T23:59:59.000Z

191

Spectrum bandwidth narrowing of Thomson scattering X-rays with energy chirped electron beams from laser wakefield acceleration  

SciTech Connect (OSTI)

We study incoherent Thomson scattering between an ultrashort laser pulse and an electron beam accelerated from a laser wakefield. The energy chirp effects of the accelerated electron beam on the final radiation spectrum bandwidth are investigated. It is found that the scattered X-ray radiation has the minimum spectrum width and highest intensity as electrons are accelerated up to around the dephasing point. Furthermore, it is proposed that the electron acceleration process inside the wakefield can be studied by use of 90 Thomson scattering. The dephasing position and beam energy chirp can be deduced from the intensity and bandwidth of the scattered radiation.

Xu, Tong; Chen, Min, E-mail: minchen@sjtu.edu.cn; Li, Fei-Yu; Yu, Lu-Le [Key Laboratory for Laser Plasmas (Ministry of Education), Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China)] [Key Laboratory for Laser Plasmas (Ministry of Education), Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China); Sheng, Zheng-Ming, E-mail: zmsheng@sjtu.edu.cn [Key Laboratory for Laser Plasmas (Ministry of Education), Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China) [Key Laboratory for Laser Plasmas (Ministry of Education), Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China); SUPA, Department of Physics, University of Strathclyde, Glasgow G4 0NG (United Kingdom); Zhang, Jie [Key Laboratory for Laser Plasmas (Ministry of Education), Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China) [Key Laboratory for Laser Plasmas (Ministry of Education), Department of Physics and Astronomy, Shanghai Jiao Tong University, Shanghai 200240 (China); Beijing National Laboratory of Condensed Matter Physics, Institute of Physics, CAS, Beijing 100190 (China)

2014-01-06T23:59:59.000Z

192

Simulations of Microchannel Plate Sensitivity to <20 keV X-rays as a Function of Energy and Incident Angle  

SciTech Connect (OSTI)

We present results of Monte Carlo simulations of microchannel plate (MCP) response to x-rays in the 250 eV to 20 keV energy range as a function of both x-ray energy and impact angle. The model is based on the model presented in Rochau et al. (2006). However, while the Rochau et al. (2006) model was two-dimensional, and their results only went to 5 keV, our results have been expanded to 20 keV, and our model has been incorporated into a three-dimensional Monte Carlo MCP model that we have developed over the past several years (Kruschwitz et al. 2011). X-ray penetration through multiple MCP pore walls is increasingly important above 5 keV. The effect of x-ray penetration through multiple pores on MCP performance was studied and is presented.

Kruschwitz, Craig [NSTec; Wu, M. [SNL; Rochau, G. A. [SNL

2013-06-13T23:59:59.000Z

193

X-ray and Neutron Scattering Studies of Methyl Iodide and Hydrogen Confined in Porous Media.  

E-Print Network [OSTI]

??X-ray diffraction was used to study the liquid - solid phase transition and structure of methyl iodide confined in porous GelTech glass, with 25, 50 (more)

Glanville, Yvonne

2005-01-01T23:59:59.000Z

194

Three-dimensional reconstruction of liquid phases in disordered mesopores using in situ small-angle scattering  

Science Journals Connector (OSTI)

In situ synchrotron small-angle X-ray scattering is used to investigate wetting transitions of liquids confined in disordered mesoporous materials. A plurigaussian stochastic model is proposed, which enables one to analyze the data in terms of changing interface areas, contact angle and triple-line length.

Gommes, C.J.

2013-03-14T23:59:59.000Z

195

Local structure of amorphous \\{MO50Ni50\\} determined by anomalous x-ray scattering using synchroton radiation  

Science Journals Connector (OSTI)

Anomalous (resonance) x-ray scattering technique using synchrotron radiation was applied to determine the compositionally resolved local structure of sputter deposited amorphous Mo50Ni50. The local environments of Mo atoms and Ni atoms were found to be significantly different from each other, but similar to the corresponding local environments in crystalline MoNi. The results compare favorably with those of the EXAFS measurement.

S. Aur; D. Kofalt; Y. Waseda; T. Egami; R. Wang; H.S. Chen; Boon-Keng Teo

1983-01-01T23:59:59.000Z

196

Short-range and long-range order of phyllomanganate nanoparticles determined using high-energy X-ray scattering  

Science Journals Connector (OSTI)

High-energy X-ray scattering data from turbostratic phyllomanganate nanosheets are analyzed in real-space by pair distribution function analysis and in reciprocal space by the Bragg-rod method and the Debye equation. The elastic deformation of the two-dimensional nanocrystals is modeled with (1) a new empirical strain function in Bragg-rod calculations and (2) explicit spherical and cylindrical mandrels implemented in the Debye equation.

Manceau, A.

2013-01-17T23:59:59.000Z

197

Ion distributions at charged aqueous surfaces: Synchrotron X-ray scattering studies  

SciTech Connect (OSTI)

Surface sensitive synchrotron X-ray scattering studies were performed to obtain the distribution of monovalent ions next to a highly charged interface at room temperature. To control surface charge density, lipids, dihexadecyl hydrogen-phosphate (DHDP) and dimysteroyl phosphatidic acid (DMPA), were spread as monolayer materials at the air/water interface, containing CsI at various concentrations. Five decades in bulk concentrations (CsI) are investigated, demonstrating that the interfacial distribution is strongly dependent on bulk concentration. We show that this is due to the strong binding constant of hydronium H3O+ to the phosphate group, leading to proton-transfer back to the phosphate group and to a reduced surface charge. Using anomalous reflectivity off and at the L3 Cs+ resonance, we provide spatial counterion (Cs+) distributions next to the negatively charged interfaces. The experimental ion distributions are in excellent agreement with a renormalized surface charge Poisson-Boltzmann theory for monovalent ions without fitting parameters or additional assumptions. Energy Scans at four fixed momentum transfers under specular reflectivity conditions near the Cs+ L3 resonance were conducted on 10-3 M CsI with DHDP monolayer materials on the surface. The energy scans exhibit a periodic dependence on photon momentum transfer. The ion distributions obtained from the analysis are in excellent agreement with those obtained from anomalous reflectivity measurements, providing further confirmation to the validity of the renormalized surface charge Poisson-Boltzmann theory for monovalent ions. Moreover, the dispersion corrections f0 and f00 for Cs+ around L3 resonance, revealing the local environment of a Cs+ ion in the solution at the interface, were extracted simultaneously with output of ion distributions.

Bu, Wei

2009-08-15T23:59:59.000Z

198

Neutron and x-ray scattering studies of the metallurgical condition and residual stresses in Weldalite welds  

SciTech Connect (OSTI)

Weldalite is a lithium-containing aluminum alloy which is being considered for aerospace applications because its favorable strength-to-weight ratio. Successful welding of this alloy depends on the control of the metallurgical condition and residual stresses in the heat affected zone. Neutron and x-ray scattering methods of residual stress measurement were applied to plasma arc welds made in aluminum-lithium alloy test panels as part of an evaluation of materials for use in welded structures. In the course of these studies discrepancies between x-ray and neutron results from the heat affected zone (HAZ) of the weld were found. Texture changes and recovery from the cold work, indicated in peak widths, were found in the HAZ as well. The consideration of x-ray and neutron results leads to the conclusion that there is a change in solute composition which modifies the d-spacings in the HAZ which affects the neutron diffraction determination of residual stresses. The composition changes give the appearance of significant compressive strains in the HAZ. This effect and sharp gradients in the texture give severe anomalies in the neutron measurement of residual stress. The use of combined x-ray and neutron techniques and the solution to the minimizing of the neutron diffraction anomalies are discussed.

Spooner, S. [Oak Ridge National Lab., TN (United States); Pardue, E.B.S. [Technology for Energy Corp., Knoxville, TN (United States)

1995-12-31T23:59:59.000Z

199

Local density profiles in thin films and multilayers from diffuse x-ray and neutron scattering  

SciTech Connect (OSTI)

We develop a technique to determine local density profiles in conformally rough thin films and multilayers for which conventional reflectometry does not work. The main idea is to integrate the total scattered intensity for a given vertical momentum transfer over the parallel momentum transfer. Probing Fourier space globally results in a local probe in real space and the integrated intensity is proportional to the local reflectivity of the surface. We also discuss the influence of a finite range of integration as well as sample inhomogeneities, such as nonconformity of the roughness. This technique is limited to situations where the kinematic Born approximation is sufficient to describe the scattering process. However, in certain cases, the technique can be used in the vicinity of the critical angle of total external reflection as well.

Rauscher, M.; Reichert, H.; Engemann, S.; Dosch, H. [Max-Planck-Institut fuer Metallforschung, Heisenbergstrasse 3, 70569 Stuttgart (Germany); and Institut fuer Theoretische und Angewandte Physik, Universitaet Stuttgart, Pfaffenwaldring 57, 70569 Stuttgart (Germany)

2005-11-15T23:59:59.000Z

200

Simulating x-ray Thomson scattering signals from high-density, millimetre-scale plasmas at the National Ignition Facility  

SciTech Connect (OSTI)

We have developed a model for analysing x-ray Thomson scattering data from high-density, millimetre-scale inhomogeneous plasmas created during ultra-high pressure implosions at the National Ignition Facility in a spherically convergent geometry. The density weighting of the scattered signal and attenuation of the incident and scattered x-rays throughout the target are included using radial profiles of the density, opacity, ionization state, and temperature provided by radiation-hydrodynamics simulations. These simulations show that the scattered signal is strongly weighted toward the bulk of the shocked plasma and the Fermi degenerate material near the ablation front. We show that the scattered signal provides a good representation of the temperature of this highly nonuniform bulk plasma and can be determined to an accuracy of ca. 15% using typical data analysis techniques with simple 0D calculations. On the other hand, the mean ionization of the carbon in the bulk is underestimated. We suggest that this discrepancy is due to the convolution of scattering profiles from different regions of the target. Subsequently, we discuss modifications to the current platform to minimise the impact of inhomogeneities, as well as opacity, and also to enable probing of conditions more strongly weighted toward the compressed core.

Chapman, D. A., E-mail: david.chapman@awe.co.uk [Plasma Physics Group, Radiation Physics Department, AWE plc, Reading RG7 4PR (United Kingdom); Centre for Fusion, Space and Astrophysics, University of Warwick, Coventry CV4 7AL (United Kingdom); Kraus, D.; Falcone, R. W. [Department of Physics, University of California, Berkeley, California 94720 (United States); Kritcher, A. L.; Bachmann, B.; Collins, G. W.; Gaffney, J. A.; Hawreliak, J. A.; Landen, O. L.; Le Pape, S.; Ma, T.; Nilsen, J.; Pak, A.; Swift, D. C.; Dppner, T. [Lawrence Livermore National Laboratory, Livermore, California 94550 (United States); Gericke, D. O. [Centre for Fusion, Space and Astrophysics, University of Warwick, Coventry CV4 7AL (United Kingdom); Glenzer, S. H. [SLAC National Accelerator Laboratory, Menlo Park, California 94309 (United States); Guymer, T. M. [Plasma Physics Group, Radiation Physics Department, AWE plc, Reading RG7 4PR (United Kingdom); Neumayer, P. [Gesellschaft fr Schwerionenforschung, 64291 Darmstadt (Germany); Redmer, R. [Institut fr Physik, Universitt Rostock, 18051 Rostock (Germany); and others

2014-08-15T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


201

Evidence for the Importance of Resonance Scattering in X-Ray Emission Line Profiles of the O Star Zeta Puppis  

SciTech Connect (OSTI)

We fit the Doppler profiles of the He-like triplet complexes of O VII and N VI in the X-ray spectrum of the O star {zeta} Pup, using XMM-Newton RGS data collected over {approx} 400 ks of exposure. We find that they cannot be well fit if the resonance and intercombination lines are constrained to have the same profile shape. However, a significantly better fit is achieved with a model incorporating the effects of resonance scattering, which causes the resonance line to become more symmetric than the intercombination line for a given characteristic continuum optical depth {tau}{sub *}. We discuss the plausibility of this hypothesis, as well as its significance for our understanding of Doppler profiles of X-ray emission lines in O stars.

Leutenegger, M.A.; /Columbia U.; Owocki, S.P.; /Bartol Research Inst.; Kahn, S.M.; /KIPAC, Menlo Park; Paerels, F.B.S.; /Columbia U.

2006-10-10T23:59:59.000Z

202

2-D X-Ray Focusing by Circular Phase Bragg-Fresnel Lenses at a Bragg Angle Close to ?/2  

Science Journals Connector (OSTI)

Two-dimensional focusing of hard X-rays has been accomplished for the first time by means of a phase Bragg-Fresnel lens with efficiency close to 40%. Images of the radiation region of a conventional X-ray tube...

V. V. Aristov; Yu. A. Basov; A. A. Snigirev; M. Belakhovsky

1992-01-01T23:59:59.000Z

203

Performance of spherically focusing Ge(444) backscattering analyzers for inelastic x-ray scattering  

SciTech Connect (OSTI)

A spectrometer designed to use an undulator source and having targeted resolutions of 0.01 eV in one mode of use and 0.2 eV in another will operate at the APS. We report here on analyzers that we have, constructed for use on this spectrometer for 0.2-eV resolution. We have tested them at NSLS beamline X21 using focused wiggler radiation and at CHESS using radiation from the CHESS-ANL undulator. Analyzers were constructed by gluing and pressing 90-mm-diameter, (111) oriented Ge wafers into concave glass forms having a radius near 1 m. An overall inelastic scattering resolution of 0.3 eV using the (444) reflection was demonstrated at CHESS. Recent results at X21 revealed a useful diameter of 74 mm at an 870 Bragg angle.

Macrander, A.T.; Kushnir, V.I.; Blasdell, R.C.

1994-08-01T23:59:59.000Z

204

Tunable X-ray source  

DOE Patents [OSTI]

A method for the production of X-ray bunches tunable in both time and energy level by generating multiple photon, X-ray, beams through the use of Thomson scattering. The method of the present invention simultaneously produces two X-ray pulses that are tunable in energy and/or time.

Boyce, James R. (Williamsburg, VA)

2011-02-08T23:59:59.000Z

205

Week 2 AGENDA: National School on Neutron and X-ray Scattering page 1 of 5 Oak Ridge National Laboratory [9/30/08  

E-Print Network [OSTI]

Week 2 AGENDA: National School on Neutron and X-ray Scattering page 1 of 5 Oak Ridge National Ridge National Laboratory Dean Myles, Director ORNL Neutron Scattering Science Division 1 GROUPS [A,B,C,D,E,F,G,H,I] Iran Thomas Auditorium Lecture Inelastic Neutron Scattering R. Osborn, ANL ALL

Pennycook, Steve

206

Low-Angle Neutron Scattering  

Science Journals Connector (OSTI)

A set of techniques that can be used to find the size of a particle in solution or to find the size or spacing of internal regions that can be distinguished by different neutron scattering power, such as the prot...

Jan W. Gooch

2011-01-01T23:59:59.000Z

207

X-Ray Scattering from Sodium-Doped Polyacetylene: Incommensurate-Commensurate and Order-Disorder Transformations  

Science Journals Connector (OSTI)

X-ray scattering carried out in situ during electrochemical doping indicates an unusual sequence of structural transitions. On doping to ?6-7 mole%, lightly doped regions coexist with a discommensurate-domain channel structure. As the Na concentration increases, the density of domain walls decreases. When the discommensuration density falls to zero, the Na channels form a commensurate 33 superlattice with respect to the (average) triangular lattice of (CH)x chains. At still higher concentrations, the Na lattice becomes unstable and transforms into a disordered "fluid" phase within the ordered polyacetylene structure.

M. Winokur; Y. B. Moon; A. J. Heeger; J. Barker; D. C. Bott; H. Shirakawa

1987-06-01T23:59:59.000Z

208

Neutron-Proton Scattering at Small Angles  

Science Journals Connector (OSTI)

24 May 1955 research-article Neutron-Proton Scattering at Small Angles...Thresher R. G. P. Voss R. Wilson Neutron-proton scattering has been measured from 6 to 61 5 degrees c.m. for neutrons of effective energy 105 3 and 137 5...

1955-01-01T23:59:59.000Z

209

E-Print Network 3.0 - anomalous x-ray scattering Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

structure based on anomalous scattering andor isomorphous... of the handedness of the constellation of anomalous scatterers will never lead to correctly interpretable...

210

Center for X-Ray Optics, 1992  

SciTech Connect (OSTI)

This report discusses the following topics: Center for X-Ray Optics; Soft X-Ray Imaging wit Zone Plate Lenses; Biological X-Ray microscopy; Extreme Ultraviolet Lithography for Nanoelectronic Pattern Transfer; Multilayer Reflective Optics; EUV/Soft X-ray Reflectometer; Photoemission Microscopy with Reflective Optics; Spectroscopy with Soft X-Rays; Hard X-Ray Microprobe; Coronary Angiography; and Atomic Scattering Factors.

Not Available

1993-08-01T23:59:59.000Z

211

High energy x-ray scattering studies of the local order in liquid Al  

SciTech Connect (OSTI)

The x-ray structure factors and densities for liquid aluminum from 1123 K to 1273 K have been measured using the beamline electrostatic levitator. Atomic structures as a function of temperature have been constructed from the diffraction data with reverse Monte Carlo simulations. An analysis of the local atomic structures in terms of the Honeycutt-Andersen indices indicates a high degree of icosahedral and distorted icosahedral order, a modest amount of body-centered cubic order, and marginal amounts of face-centered cubic and hexagonal close-packed order.

Mauro, N.A.; Bendert, J.C.; Vogt, A.J.; Gewin, J.M.; Kelton, K.F. (WU)

2012-10-23T23:59:59.000Z

212

Magnetic X-Ray Scattering Study of GdCo2Ge2 and NdCo2Ge2  

SciTech Connect (OSTI)

The results of magnetic x-ray resonant exchange scattering (XRES) experiments are important to the development of an understanding of magnetic interactions in materials. The advantages of high Q resolution, polarization analysis, and the ability to study many different types of materials make it a vital tool in the field of condensed matter physics. Though the concept of XRES was put forth by Platzman and Tzoar in 1970, the technique did not gain much attention until the work of Gibbs and McWhan et al. in 1988. Since then, the technique of XRES has grown immensely in use and applicability. Researchers continue to improve upon the procedure and detection capabilities in order to study magnetic materials of all kinds. The XRES technique is particularly well suited to studying the rare earth metals because of the energy range involved. The resonant L edges of these elements fall between 5-10 KeV. Resonant and nonresonant x-ray scattering experiments were performed in order to develop an understanding of the magnetic ordering in GdCo{sub 2}Ge{sub 2} and NdCo{sub 2}Ge{sub 2}.

William Good

2002-08-27T23:59:59.000Z

213

X-ray Diffraction Laboratory: Department of Chemistry Texas A & M University  

E-Print Network [OSTI]

, Rotating Anode Page: 1 of 5 Approved: JHR 1/8/2009 SOP: SOPSAXSLA Last date revised: December 26 2009 Date approved: December 26 2009 Small Angle X-ray Scattering, Rotating Anode PURPOSE: This Standard Operating

Meagher, Mary

214

Characterization of Metallurgical Chars by Small Angle Neutron Scattering  

Science Journals Connector (OSTI)

Characterization of Metallurgical Chars by Small Angle Neutron Scattering ... Small angle scattering measures the intensity I(q) of scattered neutrons as a function of scattering angle ? from the input beam, or alternatively, as a function of the scattering vector q:? q = |q| = (4?/?) sin(?/2), where ? is the wavelength of the incident wave. ...

I. Snook; I. Yarovsky; H. J. M. Hanley; M. Y. Lin; D. Mainwaring; H. Rogers; P. Zulli

2002-08-06T23:59:59.000Z

215

The Fourier transform in X-ray and electron scattering of hydrogenlike atoms  

Science Journals Connector (OSTI)

The author shows the mathematical aspects of the Fourier transform (FT) that make possible the conversion of scattering data into chemically important functions.

Jeffrey A. Foley

1991-01-01T23:59:59.000Z

216

Peculiarities of the correlation functions, X-ray and neutron scattering in BaTiO{sub 3}  

SciTech Connect (OSTI)

Based on molecular-dynamics (MD) simulations, we have calculated the static and dynamic correlation functions in a BaTiO{sub 3} crystal. The static correlation functions have been used to study the peculiarities of diffuse scattering in barium titanate showing the experimentally observed anomalous planes. Based on time-dependent pair correlation functions, we have calculated the phonon spectra of BaTiO{sub 3} and studied the central peak of inelastic scattering. The phonon frequencies calculated by the MD method agree well with those obtained previously in the quasi-harmonic approximation. We show that the central peak of inelastic scattering is associated mainly with the soft optic mode and has the same symmetry. The large anisotropy in the displacements of atoms in the soft mode allows the presence of peculiarities in both X-ray scattering and EXAFS spectroscopy to be explained. The characteristic shape of the EXAFS spectra is shown to be explained by the quasi-one-dimensional motion of the oxygen ions in the cubic lattice of BaTiO{sub 3}. Our calculation of triple correlation functions shows that the titanium atom in the described model oscillates around the cubic cell center. Explaining the experimental data that have caused disagreement about the nature of the phase transition in BaTiO{sub 3} using the developed model gives grounds to treat the phase transition in barium titanate as a displacive one.

Matsko, N. L., E-mail: matsko@lpi.ru; Maksimov, E. G.; Lepeshkin, S. V. [Russian Academy of Sciences, Lebedev Physical Institute (Russian Federation)

2012-08-15T23:59:59.000Z

217

Phonon dispersion of graphite by inelastic x-ray scattering * J. Maultzsch,1, E. Dobardzi,2 S. Reich,3 I. Milosevi,2 M. Damnjanovi,2 A. Bosak,4 M. Krisch,4 and  

E-Print Network [OSTI]

quality. It has been partly measured by inelastic neutron scattering INS , electron- energy lossPhonon dispersion of graphite by inelastic x-ray scattering M. Mohr,1, * J. Maultzsch,1, E-plane phonon dispersion of graphite obtained from inelastic x-ray scattering, including the optical

Nabben, Reinhard

218

Synchrotron x-ray scattering investigations of oxygen-induced nucleation in a Zr-based glass-forming alloy.  

SciTech Connect (OSTI)

The metallic glass-forming alloy VIT-105 (Zr{sub 52.5}Cu{sub 17.9}Ni{sub 14.6}Al{sub 10}Ti{sub 5}) was used to study the effect of oxygen on nucleation. Ex situ synchrotron X-ray scattering experiments performed on as-cast samples showed that oxygen leads to the formation of tetragonal and/or cubic phases, depending on oxygen content. The samples crystallized into either a primitive tetragonal phase or the so-called fcc 'big cube' phase in a glassy matrix. A subsequent discussion on the role of oxygen in heterogeneous nucleation in Zr-based bulk metallic glasses is presented.

Wall, J. J.; Almer, J. D.; Vogel, S. C.; Liaw, P. K.; Choo, H.; Liu, C. T.; LANL; Univ. of Tennessee; ORNL

2009-01-01T23:59:59.000Z

219

Beam Measurement of 11.424 GHz X-Band Linac for Compton Scattering X-ray Source  

SciTech Connect (OSTI)

An inverse Compton scattering X-ray source for medical applications, consisting of an X-band (11.424 GHz) linac and Q-switched Nd:YAG laser, is currently being developed at the University of Tokyo. This system uses an X-band 3.5-cell thermionic cathode RF gun for electron beam generation. We can obtain a multi-bunch electron beam with this gun. The beam is accelerated to 30 MeV by a traveling-wave accelerating tube. So far, we have verified stable beam generation (around 2.3 MeV) by using the newly designed RF gun and we have succeeded in beam transportation to a beam dump.

Natsui, Takuya; Mori, Azusa; Masuda, Hirotoshi; Uesaka, Mitsuru [Nuclear Professional School, School of Engineering, University of Tokyo, 22-2 Shirane-shirakata, Tokai, Naka, Ibaraki 319-1188 (Japan); Sakamoto, Fumito [Akita National College of Technology, 1-1 Iijima-bunkyo, Akita city, Akita 011-8511 (Japan)

2010-11-04T23:59:59.000Z

220

Acoustic plasmons and doping evolution of Mott physics in resonant inelastic x-ray scattering from cuprate superconductors  

SciTech Connect (OSTI)

By incorporating a long-range Coulomb interaction into the framework of the one-band Hubbard model, they delineate how the low-energy plasmon around 1 eV, which is a universal feature of the charge dynamics of the cuprates, manifests itself in the resonant inelastic x-ray scattering (RIXS) spectra. The long-range Coulomb interaction in the doped system control sthe form of the intraband RIXS dispersion near the Brillouin zone center around the {Gamma} point. The out-of-plane momentum transfer component q{sub z} is found to play a key role in determining whether or not the RIXS spectrum shows a plasmon-related gap at {Gamma}.

Markiewicz, R.S.; Hasan, M.Z.; Bansil, A.; (NEU); (Princeton)

2010-01-28T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


221

From ultra-high vacuum to the electrochemical interface : x-ray scattering studies of model electrocatalysts.  

SciTech Connect (OSTI)

In-situ surface X-ray scattering (SXS) has become a powerful probe of the atomic structure at the metal-electrolyte interface. In this paper we describe an experiment in which a Pt(111) sample is prepared under ultra-high vacuum (UHV) conditions to have a p(2 x 2) oxygen layer adsorbed on the surface. The surface is then studied using SXS under UHV conditions before successive transfer to a bulk water environment and then to the electrochemical environment (0.1 M KOH solution) under an applied electrode potential. The Pt surface structure is examined in detail using crystal truncation rod (CTR) measurements under these different conditions. Finally, some suggestions for future experiments on alloy materials, using the same methodology, are proposed and discussed in relation to previous results.

Lucas, C. A.; Cormack, M.; Gallagher, M. E.; Brownrigg, A.; Thompson, P.; Fowler, B.; Grunder, Y.; Roy, J.; Stamenkovic, V.; Markovic, N. M.; Materials Science Division; Univ. of Liverpool; European Synchrotron Radiation Facility

2008-08-01T23:59:59.000Z

222

Prototype grooved and spherically bent Si backscattering crystal analyzer for meV resolution inelastic x-ray scattering  

SciTech Connect (OSTI)

The high-order backscattering reflections from single crystals of silicon have mrad rocking curve widths that can be exploited to produce meV energy-resolution focusing analyzer crystals for use in inelastic x-ray scattering experiments at third-generation synchrotron sources. The first generation of these analyzers has been limited in efficiency principally by slope and/or figure errors. We calculate the effect of slope errors on the theoretical energy resolution and focus spot size of a typical analyzer design using a ray-tracing code to ensure that there are no unforeseen contributions to the energy resolution and efficiency. We also present measurements of the slope errors of the atomic planes for a prototype, spherically bent, strain-relief grooved analyzer as proof that it is in principle possible to obtain the slope and figure error limits required for a high efficiency meV resolution backscattering crystal.

Blasdell, R.C.; Macrander, A.T. (Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439-4814 (United States))

1995-02-01T23:59:59.000Z

223

Optimization of a coherent soft x-ray beamline for coherent scattering experiments at NSLS-II  

SciTech Connect (OSTI)

The coherent soft x-ray and full polarization control (CSX) beamline at the National Synchrotron Light Source - II (NSLS-II) will deliver 1013 coherent photons per second in the energy range of 0.2-2 keV with a resolving power of 2000. The source, a dual elliptically polarizing undulator (EPU), and beamline optics should be optimized to deliver the highest possible coherent flux in a 10-30 {micro}m spot for use in coherent scattering experiments. Using the computer code Synchrotron Radiation Workshop (SRW), we simulate the photon source and focusing optics in order to investigate the conditions which provide the highest usable coherent intensity on the sample. In particular, we find that an intermediate phasing magnet is needed to correct for the relative phase between the two EPUs and that the optimum phase setting produces a spectrum in which the desired wavelength is slightly red-shifted thus requiring a larger aperture than originally anticipated. This setting is distinct from that which produces an on-axis spectrum similar to a single long undulator. Furthermore, partial coherence calculations, utilizing a multiple electron approach, indicate that a high degree of spatial coherence is still obtained at the sample location when such an aperture is used. The aperture size which maximizes the signal-to-noise ratio of a double-slit experiment is explored. This combination of high coherence and intensity is ideally suited for x-ray ptychography experiments which reconstruct the scattering density from micro-diffraction patterns. This technique is briefly reviewed and the effects on the image quality of proximity to the beamline focus are explored.

Shapiro D.; Chubar, O.; Kaznatcheev, K.; Reininger, R.; Sanchez-Hanke, C.; Wang, S.

2011-08-21T23:59:59.000Z

224

National School on Neutron and X-ray Scattering Oak Ridge National Laboratory June 12-26, 2010 Oak Ridge, Tennessee  

E-Print Network [OSTI]

National School on Neutron and X-ray Scattering Oak Ridge National Laboratory June 12-26, 2010 Oak ------------------------------------------------------------------------------- SCHEDULE FOR SATURDAY, JUNE 19, 2010 School participants arrive in Oak Ridge, TN and check in at the Comfort Inn. Dinner hosted by Oak Ridge National Laboratory

Pennycook, Steve

225

Temporal synchronization of GHz repetition rate electron and laser pulses for the optimization of a compact inverse-Compton scattering x-ray source  

E-Print Network [OSTI]

The operation of an inverse-Compton scattering source of x-rays or gamma-rays requires the precision alignment and synchronization of highly focused electron bunches and laser pulses at the collision point. The arrival times of electron and laser pulses must be synchronized with picosecond precision. We have developed an RF synchronization technique that reduces the initial timing uncertainty from 350 ps to less than 2 ps, greatly reducing the parameter space to be optimized while commissioning the x-ray source. We describe the technique and present measurements of its performance.

Hadmack, Michael R; Madey, John M J; Kowalczyk, Jeremy M D

2014-01-01T23:59:59.000Z

226

Dissolution dynamics of the calcite-water interface observed in situ by glancing-incidence X-ray scattering  

SciTech Connect (OSTI)

Glancing-incidence X-ray scattering measurements made at the National Synchrotron Light Source were used to investigate dissolution dynamics in situ at the calcite-water interface. The relation between calcite saturation state and roughness of the calcite (1014) cleavage surface as a function of time was examined during pH titrations of an initially calcite-saturated solution. Systematic variations in roughness were observed as a function of saturation state as pH was titrated to values below that of calcite saturation. Different steady-state values of roughness were evident at fixed values of {Delta}G{sub r}, and these were correlated with the extent of undersaturation. A significant increase in roughness begins to occur with increasing undersaturation at a {Delta}G{sub r} value of approximately {minus}2.0 kcal/mol. The dissolution rate corresponding to this increase is about 1.5 x 10{sup 7} mmol/cm {center_dot} sec. This increase in roughness is attributed to a transition in the principal rate-determining dissolution mechanism, and is consistent with both powder-reaction studies of dissolution kinetics and single-crystal dissolution studies by atomic force microscopy. These data indicate some important potential applications of GIXS in the study of mineral-water interface geochemistry.

Sturchio, N.C.; Chiarello, R.P.

1995-06-02T23:59:59.000Z

227

Ris-R-747(EN) Neutron and X-Ray Diffraction  

E-Print Network [OSTI]

describes X-ray and neutron scattering experiments per- formed on two examples of modulated structures is divided in three parts. A single crystal elastic neutron scattering experiment between 4.2 and 115 K has shift across the layers. A small-angle neutron scattering experiment has been performed on the mag

228

Small-angle neutron scattering study of high-pressure sintered detonation nanodiamonds  

SciTech Connect (OSTI)

The structure of detonation diamonds sintered at a high pressure (7 GPa) and temperatures of 1200-1700 Degree-Sign C has been investigated by small-angle neutron scattering. It is shown that sintering leads to an increase in the particle size from 6 to 30 nm and established that this increase is due to the chainlike oriented attachment of particles. This study supplements the oriented-attachment model, which was suggested based on the X-ray diffraction spectra of detonation nanodiamonds (DNDs) sintered under the same conditions.

Kidalov, S. V.; Shakhov, F. M., E-mail: fedor.shakhov@mail.ioffe.ru [Ioffe Physical-Technical Institute of the Russian Academy of Sciences (Russian Federation); Lebedev, V. T.; Orlova, D. N.; Grushko, Yu. S. [Russian Academy of Sciences, Konstantinov St. Petersburg Nuclear Physics Institute (Russian Federation)

2011-12-15T23:59:59.000Z

229

X-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND  

E-Print Network [OSTI]

with the occurrence of solar X-ray flare, when light travel time delay is accounted, suggesting that X-rays fromX-RAY EMISSION FROM PLANETS AND COMETS: RELATIONSHIP WITH SOLAR X-RAYS AND SOLAR WIND ANIL BHARDWAJ Flight center, Greenbelt, MD 20771, USA Scattering of solar X-ray radiation mainly produces the non

?stgaard, Nikolai

230

4.3.2.3 Small angle X-ray and neutron scattering  

Science Journals Connector (OSTI)

This document is part of Subvolume C Spectroscopic and Kinetic Data. Physical Data I of Volume 1 Nucleic Acids of Landolt-Brnstein - Group VII Biophysics.

H. Eisenberg

1990-01-01T23:59:59.000Z

231

Influence of the multiple scattering of relativistic electrons on the line width of backward Parametric X-ray Radiation in the absence of photo absorption  

E-Print Network [OSTI]

The multiple scattering effect on the line width of backward Parametric X-ray Radiation (PXR) in the extremely Bragg geometry, produced by low energy relativistic electrons traversing a single crystal, is discussed. It is shown that there exist conditions, when the influence of photo absorption on the line width can be neglected, and the only multiple scattering process of relativistic electrons in crystal leads to the broadening of backward PXR lines. Based on the obtained theoretical results, the line width broadening of backward PXR, caused by the multiple scattering of 30 MeV and 50 MeV relativistic electrons in a Si crystal of varying thicknesses, is numerically obtained.

Tabrizi, Mehdi

2015-01-01T23:59:59.000Z

232

E-Print Network 3.0 - angle neutron diffractometer Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

(300 - 2000 K) X-ray reflectometer (under installation) Small and Ultra Small Angle Neutron Scattering... (at)ipta.demokritos.gr 2106503712 2106533431 Large Scale...

233

Cosmic Ray Pitch Angle Scattering Through 90 o  

E-Print Network [OSTI]

Cosmic Ray Pitch Angle Scattering Through 90 o G.M. Felice 1 and R.M. Kulsrud 2 Princeton Plasma­ lar attention to the problem of particle scattering through the # = cos -1 (v # /v) = 90 o pitch angle their pitch angle by mirror interaction with long wavelength waves generated by the # # 0 particles. We match

234

Structural and magnetic properties of transition metal substituted BaFe{sub 2}As{sub 2} compounds studied by x-ray and neutron scattering  

SciTech Connect (OSTI)

The purpose of my dissertation is to understand the structural and magnetic properties of the newly discovered FeAs-based superconductors and the interconnection between superconductivity, antiferromagnetism, and structure. X-ray and neutron scattering techniques are powerful tools to directly observe the structure and magnetism in this system. I used both xray and neutron scattering techniques on di#11;erent transition substituted BaFe2As2 compounds in order to investigate the substitution dependence of structural and magnetic transitions and try to understand the connections between them.

Kim, Min Gyu [Ames Laboratory

2012-08-28T23:59:59.000Z

235

A More Informative Approach for Characterization of Polymer Monolithic Phases: Small Angle Neutron Scattering/Ultrasmall Angle Neutron Scattering  

Science Journals Connector (OSTI)

A More Informative Approach for Characterization of Polymer Monolithic Phases: Small Angle Neutron Scattering/Ultrasmall Angle Neutron Scattering ... Scattered neutrons were detected with a 64 cm 64 cm two-dimensional position sensitive detector with 128 128 pixels and 0.5 cm resolution per pixel. ...

Kathleen M. Ford; Brian G. Konzman; Judith F. Rubinson

2011-11-08T23:59:59.000Z

236

Theoretical treatments of the bound-free contribution and experimental best practice in X-ray Thomson scattering from warm dense matter  

SciTech Connect (OSTI)

By comparison with high-resolution synchrotron x-ray experimental results, we assess several theoretical treatments for the bound-free (core-electron) contribution to x-ray Thomson scattering (i.e., also known as nonresonant inelastic x-ray scattering). We identify an often overlooked source of systematic error in the plane-wave form factor approximation (PWFFA) used in the inference of temperature, ionization state, and free electron density in some laser-driven compression studies of warm dense matter. This error is due to a direct violation of energy conservation in the PWFFA. We propose an improved practice for the bound-free term that will be particularly relevant for XRTS experiments performed with somewhat improved energy resolution at the National Ignition Facility or the Linac Coherent Light Source. Our results raise important questions about the accuracy of state variable determination in XRTS studies, given that the limited information content in low-resolution XRTS spectra does not strongly constrain the models of electronic structure being used to fit the spectra.

Mattern, Brian A.; Seidler, Gerald T. [Department of Physics, University of Washington, Seattle, Washington 98195-1560 (United States)

2013-02-15T23:59:59.000Z

237

Aspherical refractive lenses for small-angle neutron scattering  

Science Journals Connector (OSTI)

This paper discusses the testing and simulation of aspherical neutron lenses as focusing elements for small-angle neutron scattering and their transparency with respect to thermal diffuse scattering.

Frielinghaus, H.

2009-06-20T23:59:59.000Z

238

Hydrogen absorption in epitaxial W/Nb(001) and polycrystalline Fe/Nb(110) multilayers studied in-situ by X-ray/neutron scattering techniques and X-ray absorption spectroscopy  

SciTech Connect (OSTI)

Hydrogen can be absorbed in large quantities by 100 {angstrom} thin Nb layers embedded in epitaxial W/Nb and polycrystalline Fe/Nb multilayers. The solubility and the hydrogen-induced structural changes of the host lattice are explored in-situ by small-angle neutron/X-ray reflectometry and high-angle diffraction. These measurements reveal for both systems that the relative out-of-plane expansion of the Nb layers is considerably larger than the relative increase of the Nb interplanar spacing indicating two distinctly different mechanisms of hydrogen absorption. In Fe/Nb multilayers, hydrogen expands the Nb interplanar spacing in a continuous way as function of the external pressure. In contrast, the Nb lattice expansion is discontinuous in epitaxial W/Nb multilayers: A jump in the Nb(002) Bragg reflection position occurs at a critical hydrogen pressure of 1 mbar. In-situ EXAFS spectroscopy also exhibits an irreversible expansion of the Nb lattice in the film plane for p{sub H{sub 2}}> 1 mbar. This can be regarded as a structural phase transition from an exclusively out-of-plane to a three-dimensionally expanded state at low and high hydrogen pressures, respectively.

Klose, F.; Rehm, C.; Fieber-Erdmann, M.; Holub-Krappe, E.; Bleif, H. J.; Sowers, H.; Goyette, R.; Troger, L.; Maletta, H.

1999-11-02T23:59:59.000Z

239

E-Print Network 3.0 - angle scattering studies Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Search Sample search results for: angle scattering studies Page: << < 1 2 3 4 5 > >> 1 Neutron Scattering in Polymer Micelle Characterization Summary: scattering Small Angle...

240

Reflection soft X-ray microscope and method  

DOE Patents [OSTI]

A reflection soft X-ray microscope is provided by generating soft X-ray beams, condensing the X-ray beams to strike a surface of an object at a predetermined angle, and focusing the X-ray beams reflected from the surface onto a detector, for recording an image of the surface or near surface features of the object under observation.

Suckewer, Szymon (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ); Rosser, Roy (Princeton, NJ)

1993-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


241

X-ray Imaging Workshop  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Imaging and Spectro-microscopy: Imaging and Spectro-microscopy: the Present and the Future Stanford Synchrotron Radiation Laboratory October 8-9, 2002 Organizers: John Miao & Keith Hodgson A workshop on "X-ray Imaging and Spectro-microscopy: the Present and the Future" was held on October 8-9, 2002. This workshop, organized by John Miao (SSRL) and Keith Hodgson (SSRL) provided a forum to discuss the scientific applications of a variety of imaging and spectro-microscopic techniques, including photoemission electron microscopy (PEEM), angle resolved photoemission spectroscopy (ARPES), coherent diffraction imaging, x-ray microscopy, micro-tomography, holographic imaging, and x-ray micro-probe. Twelve invited speakers discussed the important scientific applications of these techniques, and also predicted the future scientific directions with the advance of instrumentation and x-ray sources. The workshop was well attended with over fifty registered attendees.

242

X-ray Diffraction (XRD) 1.0 What is X-ray Diffraction  

E-Print Network [OSTI]

X-ray Diffraction (XRD) · 1.0 What is X-ray Diffraction · 2.0 Basics of Crystallography · 3.0 Production of X-rays · 4.0 Applications of XRD · 5.0 Instrumental Sources of Error · 6.0 Conclusions #12 why the cleavage faces of crystals appear to reflect X-ray beams at certain angles of incidence (theta

Moeck, Peter

243

Foams As Viewed by Small-Angle Neutron Scattering  

Science Journals Connector (OSTI)

Foams As Viewed by Small-Angle Neutron Scattering ... For wet foams, we met other difficulties, common to any strongly scattering system:? a part of the scattered beam is collected in the central cells along with the transmitted beam; this can spoil the transmission measurements. ...

Monique A. V. Axelos; Franois Bou

2003-07-04T23:59:59.000Z

244

Improvement of data treatment in small-angle neutron scattering  

Science Journals Connector (OSTI)

General equations are given for background subtraction of SANS treatment, which account for large scattering angles () and allow the extraction of the scattering due to the sample when the later is inside a container that displays a spurious scattering signal. Several calibration methods to determine the inherent sample backgrounds are also described.

Br?let, A.

2007-01-12T23:59:59.000Z

245

X-ray Crystallographic, Scanning Microprobe X-ray Diffraction, and Cross-Polarized/Magic Angle Spinning [superscript 13]C NMR Studies of the Structure of Cellulose III[subscript II  

SciTech Connect (OSTI)

The X-ray crystallographic structure of cellulose III{sub II} is characterized by disorder; the unit cell (space group P2{sub 1}; a = 4.45 {angstrom}, b = 7.64 {angstrom}, c = 10.36 {angstrom}, {alpha} = {beta} = 90{sup o}, {gamma} = 106.96{sup o}) is occupied by one chain that is the average of statistically disordered antiparallel chains. {sup 13}C CP/MAS NMR studies reveal the presence of three distinct molecular conformations that can be interpreted as a mixture of two different crystal forms, one equivalent to cellulose III{sub I}, and another with two independent glucosyl conformations in the asymmetric unit. Both X-ray crystallographic and {sup 13}C NMR spectroscopic results are consistent with an aggregated microdomain structure for cellulose III{sub II}. This structure can be generated from a new crystal form (space group P2{sub 1}; a = 4.45 {angstrom}, b = 14.64 {angstrom}, c = 10.36 {angstrom}, {alpha} = {beta} = 90{sup o}, {gamma} = 90.05{sup o}; two crystallographically independent and antiparallel chains; gt hydroxymethyl groups) by multiple dislocation defects. These defects produce microdomains of the new crystal form and cellulose III{sub I} that scanning microprobe diffraction studies show are distributed consistently through the cellulose III{sub II} fiber.

Wada, Masahisa; Heux, Laurent; Nishiyama, Yoshiharu; Langan, Paul; (U of Tokyo); (CNRS-CRMD); (LANL)

2009-03-16T23:59:59.000Z

246

Small-angle scattering in a marginal Fermi liquid  

Science Journals Connector (OSTI)

We study the magnetotransport properties of a model of small-angle scattering in a marginal Fermi liquid. Such a model has been proposed by Varma and Abrahams [Phys. Rev. Lett. 86, 4652 (2001)] to account for the anomalous temperature dependence of in-plane magnetotransport properties of the high-Tc cuprates. We study the resistivity, Hall angle, and magnetoresistance using both analytical and numerical techniques. We find that small-angle scattering only generates a difference in temperature dependence between the inverse Hall angle and the resistivity near particle-hole symmetric Fermi surfaces where the conventional Hall term vanishes. The magnetoresistance always shows Kohlers rule behavior.

E. C. Carter and A. J. Schofield

2002-12-17T23:59:59.000Z

247

Sure, a textbook can tell you about Bragg's Law and the x-ray absorption energies for any element in the periodic table, but it can't tell you how to plan and carry out an x-ray scattering experiment at one of the 50 or so synchrotron radiation facilitie  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Report Report SSRL 6 th Annual School on Synchrotron X-ray Scattering Techniques in Materials and Environmental Sciences: Theory and Application SSRL SR-XRS participants. Synchrotron-based X-ray scattering (SR-XRS) techniques offer the ability to probe nano- and atomic-scale structure that dictates the properties of advanced technological and environmental materials. Important materials studied at the Stanford Synchrotron Radiation Lightsource (SSRL) include organic and inorganic thin films and interfaces, nanoparticles, complex oxides, solutions, polymers, minerals and poorly crystalline materials. Good planning and a good working knowledge of beam lines and techniques are required to successfully conduct SR-XRS measurements. This sixth annual School at SSRL on Synchrotron X-ray

248

A combined fit of total scattering and extended x-ray absorption fine structure data for local-structure determination in crystalline materials  

SciTech Connect (OSTI)

Reverse Monte Carlo (RMC) refinements of local structure using a simultaneous fit of X-ray/neutron total scattering and extended X-ray absorption fine structure (EXAFS) data were developed to incorporate an explicit treatment of both single- and multiple-scattering contributions to EXAFS. The refinement algorithm, implemented as an extension to the public domain computer software RMCProfile, enables accurate modeling of EXAFS over distances encompassing several coordination shells around the absorbing species. The approach was first tested on Ni, which exhibits extensive multiple scattering in EXAFS, and then applied to perovskite-like SrAl{sub 1/2}Nb{sub 1/2}O{sub 3}. This compound crystal1izes with a cubic double-perovskite structure but presents a challenge for local-structure determination using a total pair-distribution function (PDF) alone because of overlapping peaks of the constituent partial PDFs (e.g. Al-O and Nb-O or Sr-O and O-O). The results obtained here suggest that the combined use of the total scattering and EXAFS data provides sufficient constraints for RMC refinements to recover fine details of local structure in complex perovskites. Among other results, it was found that the probability density distribution for Sr in SrAl{sub 1/2}Nb{sub 1/2}O{sub 3} adopts T{sub d} point-group symmetry for the Sr sites, determined by the ordered arrangement of Al and Nb, as opposed to a spherical distribution commonly assumed in traditional Rietveld refinements.

Proffen, Thomas E [Los Alamos National Laboratory; Krayzman, Victor [NIST; Levin, Igor [NIST; Tucker, Matt [ISIS, UK

2009-01-01T23:59:59.000Z

249

Concepts in spin echo small-angle neutron scattering  

Science Journals Connector (OSTI)

Two-dimensional spin echo small-angle neutron scattering experiments are proposed for the direct measurement of the vector-length distribution function. Interpretation of the correlation function from one-dimensional experiments is also presented.

Zhao, J.

2001-09-25T23:59:59.000Z

250

Toward a Taxonomy of the Denatured State: Small Angle Scattering Studies of Unfolded Proteins  

SciTech Connect (OSTI)

Despite the critical role the unfolded state plays in defining protein folding kinetics and thermodynamics (Berg et al., 2002; Dunker, 2002; Shortle, 2002; Wright and Dyson, 2002), our understanding of its detailed structure remains rather rudimentary; the heterogeneity of the unfolded ensemble renders difficult or impossible its study by traditional, atomic-level structural methods. Consequently, recent years have seen a significant expansion of small-angle X-ray and neutron scattering (SAXS and SANS, respectively) techniques that provide direct, albeit rotationally and time-averaged, measures of the geometric properties of the unfolded ensemble. These studies have reached a critical mass, allowing us for the first time to define general observations regarding the nature of the geometry - and possibly the chemistry and physics - of unfolded proteins.

Millett, I.S.; Doniach, S.; Plaxco, K.W. (Stanford); (UCSB)

2005-02-15T23:59:59.000Z

251

Place-exchange mechanism of Pt (111) oxidation/reduction as observed by synchrotron X-ray scattering  

SciTech Connect (OSTI)

Structural changes in the Pt(111) single crystal surface associated with incipient electrochemical oxidation/reduction were studied by {ital in}{ital situ} synchrotron x-ray reflectivity. It was shown that lifting of Pt atoms of the surface layer occurs, substantiating the long-standing hypothesis of a place-exchange mechanism for solution/metal interface oxidation. It was also shown that, for a charge transfer of {approx_lt}1.7 e{sup -}/Pt atom, the initially flat surface structure could be recovered by electrochemical reduction. In constrast, the surface was irreversibly roughened for amounts of charge transfer exceeding {approx}1.7 e{sup -}/Pt, but the roughening involved only the atoms in the top layer of the original flat surface. A detailed mechanism is proposed for the place-exchange mechanism and the subsequent roughening of the electrode surface.

You, H.; Nagy, Z.; Zurawski, D.J.; Chiarello, R.P.

1996-07-01T23:59:59.000Z

252

X-ray microscopy using grazing-incidence reflection optics  

SciTech Connect (OSTI)

The Kirkpatrick-Baez microscopes are described along with their role as the workhorse of the x-ray imaging devices. This role is being extended with the development of a 22X magnification Kirkpatrick-Baez x-ray microscope with multilayer x-ray mirrors. These mirrors can operate at large angles, high x-ray energies, and have a narrow, well defined x-ray energy bandpass. This will make them useful for numerous experiments. However, where a large solid angle is needed, the Woelter microscope will still be necessary and the technology needed to build them will be useful for many other types of x-ray optics.

Price, R.H.

1981-08-06T23:59:59.000Z

253

Structure and photoinduced structural changes in a-As2S3 films: A study by differential anomalous x-ray scattering  

Science Journals Connector (OSTI)

Differential anomalous x-ray-scattering experiments were carried out on two samples, annealed and photodarkened a-As2S3 films of 4 ?m in thickness. Two x-ray energies were chosen. One is 11 859 eV, just below the arsenic K edge; the other is 11 700 eV, below the edge by 167 eV. The study of the structure and photoinduced reversible structural changes in the a-As2S3 films show that the first sharp diffraction peak (FSDP) is related to intermediate-range correlations. These correlations extend as far as 7.0 . Beyond 7.0 , however, the structure in radial distribution function tends to the average atomic density. The FSDP is dominated by the arsenic-related atomic correlations, especially As-As atomic correlation. After photodarkening, the structure overall in both the short and intermediate ranges moves to a more disordered state. The photoinduced structural changes involve changes of the As-As atomic pair correlation in the intermediate range as illustrated by the comparisons of the changes between the annealed and photodarkened a-As2S3 films in the FSDPs and the differential structure factors.

Weiqing Zhou; D. E. Sayers; M. A. Paesler; B. Bouchet-Fabre; Q. Ma; D. Raoux

1993-01-01T23:59:59.000Z

254

The scanning soft X-ray microscope at Hasylab: imaging and spectroscopy of photoelectrons, photoluminescence, desorbed ions, reflected, scattered and transmitted light  

Science Journals Connector (OSTI)

The scanning soft X-ray microscope operating at Hasylab/Desy has been developed to combine lateral and temporal resolution, tunability and various conventional spectroscopy techniques. Different mirror optics are used to form a microprobe in the energy range 151500 eV. A grazing incidence ellipsoidal mirror provides a resolution of 1 ?m over the entire energy range, and in the vacuum ultraviolet region below 30 eV, 0.15 ?m can be achieved with a Pt-coated Schwarzschild objective. Due to the large working distance of the optics used, the detection and analysis of several surface signals are comparatively simple. Detectors and spectrometers for photoelectrons, luminescence, fluorescence, desorbed ions, reflected, scattered and transmitted light are built in permanently into the microscope. Furthermore, some combinations of the different methods can be used for simultaneous measurements. In this paper the technical developments of recent years are described. A short representation of some exemplary applications will give an insight into the work of our group and illustrate the characteristics of the microscope. The following topics are discussed: cross-luminescence of barium fluoride, visible luminescence and degradation of porous silicon, photoluminescence of ceramics, chemical contrast in photoemission spectroscopy, and Bragg reflection as a contrast mechanism in X-ray microscopy.

J Voss

1997-01-01T23:59:59.000Z

255

Small-Angle Proton-Proton Scattering at 20 Mev  

Science Journals Connector (OSTI)

The differential cross section for the scattering of 19.8-Mev protons by protons has been measured for angles between 18 and 35 in the center-of-mass system, detection being by photographic emulsion placed in a scattering camera. Cross sections were measured simultaneously at all angles and azimuths. A run with analyzing slits closed served to evaluate the small slit-edge correction. The accuracy of the cross-section measurements is approximately 2.5% at all angles except 18, where the accuracy is about 3%.

Herbert N. Royden and Byron T. Wright

1959-01-01T23:59:59.000Z

256

Variation of Q with energy in mosaic analyzers for inelastic x-ray measurements  

SciTech Connect (OSTI)

Curved mosaic graphite analyzers have been used for many years for inelastic scattering measurements with both conventional x-ray sources as well as synchrotron sources (1). The trend in recent years has been to use spherically bent perfect crystal analyzers to collect large solid angles with high energy resolution. Although, these spherical analyzers achieve excellent energy resolution, the large solid angle limits the Q resolution. For cylindrically bent mosaic graphite, it is possible to obtain good energy and Q resolution simultaneously, while maintaining a large solid angle by collecting a range of energies dispersed along a linear position detector. However, if the mosaic spread of the crystal is less than the acceptance angle subtended in the scattering plane, the energy spectrum from a mosaic analyzer as collected in a linear detector will have Q varying with energy. The resolution and the variation in Q with energy along a linear detector are discussed in relation to inelastic x-ray scattering measurements.

Tischler, J. Z.; Larson, B. C. [Solid State Division, Oak Ridge National Laboratory, Oak Ridge, Tennessee 37831-6030 (United States); Zschack, Paul [Univ. of Illinois, UNICAT, Bldg. 438D, Argonne National Lab., Argonne, Illinois 60439-4863 (United States)

1997-07-01T23:59:59.000Z

257

Resolving Conflicting Crystallographic and NMR Models for Solution-State DNA with Solution X-ray Diffraction  

Science Journals Connector (OSTI)

We report on synchrotron-based high-angle X-ray solution scattering measured to 2 resolution for two synthetic DNA sequences for which there are conflicting X-ray crystal and solution NMR models. ... Herein, we report on synchrotron-based high-angle X-ray solution scattering measured to 2 resolution for two synthetic DNA sequences for which there are numerous conflicting X-ray crystal and solution NMR models. ... The crystal structure of the synthetic DNA dodecamer d(CpGpCpGpApApTpTpCpGpCpG) was refined to a residual error of R = 17.8% at 1.9- resoln. ...

Xiaobing Zuo; David M. Tiede

2004-12-10T23:59:59.000Z

258

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate  

E-Print Network [OSTI]

X-ray-induced phase transformation in congruent and vapor-transport-equilibrated lithium tantalate an effect of a partially reversible x-ray-induced increase of diffuse x-ray scattering in both congruent been attributed to x-ray-induced decay of the ferroelectric phase at room temperature. The x-ray

Byer, Robert L.

259

Multiple-scattering calculations of the uranium {ital L}{sub 3}-edge x-ray-absorption near-edge structure  

SciTech Connect (OSTI)

A theoretical study of the uranium {ital L}{sub 3}-edge x-ray absorption near-edge structure (XANES) is presented for several uranium compounds, including oxides, intermetallics, uranyl fluoride, and {alpha}-uranium. Calculations were performed using FEFF6, an {ital ab} {ital initio} multiple-scattering (MS) code that includes the most important features of current theories. The results, which account for both the fine structure {chi} and the atomiclike background {mu}{sub 0} of the absorption coefficient {mu}, are compared to new and previously measured experimental spectra, reavealing very good agreement for most systems. For several compounds, a more detailed theoretical analysis determined the influence of cluster size and scattering order upon the calculated spectra. Results indicate that MS paths and scattering paths that include rather distant atoms make significant contributions for UO{sub 2}, whereas XANES for crystals with lower symmetry and density can be modeled using only shorter single-scattering paths. In most cases, assumption of a screened final state in the calculation gives better agreement with experiment than use of an unscreened final state. The successful modeling of spectra for a variety of different uranium compounds, with differing spectral features, indicates that the semirelativistic treatment of XANES used here is adequate even for heavy elements. The well-known resonance, observed experimentally for uranyl (UO{sub 2}{sup 2+}) compounds {approx}15 eV above the white line, is successfully modeled here for the first time, using multiple-scattering paths within the O-U-O axial bonds. Overlapping muffin-tin spheres were required in the calculation, probably as a result of the short uranyl axial bonds.

Hudson, E.A. [Glenn T. Seaborg Institute for Transactinium Science, Lawrence Livermore National Laboratory, University of California, Livermore, California 94551 (United States)] [Glenn T. Seaborg Institute for Transactinium Science, Lawrence Livermore National Laboratory, University of California, Livermore, California 94551 (United States); Rehr, J.J. [Department of Physics, University of Washington, Seattle, Washington 98195 (United States)] [Department of Physics, University of Washington, Seattle, Washington 98195 (United States); Bucher, J.J. [Chemical Sciences Division, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States)] [Chemical Sciences Division, Lawrence Berkeley National Laboratory, Berkeley, California 94720 (United States)

1995-11-15T23:59:59.000Z

260

Earth X-ray albedo for cosmic X-ray background radiation in the 1--1000 keV band  

E-Print Network [OSTI]

We present calculations of the reflection of the cosmic X-ray background (CXB) by the Earth's atmosphere in the 1--1000 keV energy range. The calculations include Compton scattering and X-ray fluorescent emission and are based on a realistic chemical composition of the atmosphere. Such calculations are relevant for CXB studies using the Earth as an obscuring screen (as was recently done by INTEGRAL). The Earth's reflectivity is further compared with that of the Sun and the Moon -- the two other objects in the Solar system subtending a large solid angle on the sky, as needed for CXB studies.

E. Churazov; S. Sazonov; R. Sunyaev; M. Revnivtsev

2008-02-11T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


261

SANS -Small Angle Neutron Scattering Tcnica de difrao  

E-Print Network [OSTI]

SANS - Small Angle Neutron Scattering Técnica de difração informações sobre tamanho e forma de- Neutrons are created in the centre of the target station when the beam of high energy protons collides by evaporating nuclear particles, mainly neutrons, in all directions. Each proton produces approximately 15

Loh, Watson

262

A high-resolution large-acceptance analyzer for X-ray fluorescence and Raman spectroscopy  

SciTech Connect (OSTI)

A newly designed multi-crystal X-ray spectrometer and its applications in the fields of X-ray fluorescence and X-ray Raman spectroscopy are described. The instrument is based on 8 spherically curved Si crystals, each with a 3.5 inch diameter form bent to a radius of 86 cm. The crystals are individually aligned in the Rowland geometry capturing a total solid angle of 0.07 sr. The array is arranged in a way that energy scans can be performed by moving the whole instrument, rather than scanning each crystal by itself. At angles close to back scattering the energy resolution is between 0.3 and 1 eV depending on the beam dimensions at the sample. The instrument is mainly designed for X-ray absorption and fluorescence spectroscopy of transition metals in dilute systems such as metalloproteins. First results of the Mn K{beta} (3p -> 1s) emission in photosystem II are shown. An independent application of the instrument is the technique of X-ray Raman spectroscopy which can address problems similar to those in traditional soft X-ray absorption spectroscopies, and initial results are presented.

Bergmann, Uwe; Cramer, Stephen P.

2001-08-02T23:59:59.000Z

263

Total reflection inelastic x-ray scattering from a 10 nm thick La{sub 0.6}Sr{sub 0.2}CoO{sub 3} thin film.  

SciTech Connect (OSTI)

To study equilibrium changes in composition, valence, and electronic structure near the surface and into the bulk, we demonstrate the use of a new approach, total-reflection inelastic x-ray scattering, as a sub-keV spectroscopy capable of depth profiling chemical changes in thin films with nanometer resolution. By comparing data acquired under total x-ray reflection and penetrating conditions, we are able to separate the O K-edge spectra from a 10 nm La{sub 0.6}Sr{sub 0.4}CoO{sub 3} thin film from that of the underlying SrTiO{sub 3} substrate. With a smaller wavelength probe than comparable soft x-ray absorption measurements, we also describe the ability to easily access dipole-forbidden final states, using the dramatic evolution of the La N{sub 4,5} edge with momentum transfer as an example.

Fister, T. T.; Fong, D. D.; Eastman, J. A.; Iddir, H.; Zapol, P.; Fuoss, P. H.; Balasubramanian, M.; Gordon, R. A.; Balasubramaniam, K. R.; Salvador, P. A.; Simon Fraser Univ.; Carnegie Mellon Univ.

2011-01-18T23:59:59.000Z

264

Investigations of anisotropy of the electronic density in KC8 by synchroton X-ray Compton scattering  

Science Journals Connector (OSTI)

Extensive experiments have been performed to determine the electronic behavior of the outer alkali electron in the stage one heavy alkali metal GIC to test both available band structure calculations (1,2). The discrepancy in the experimental results is very large, leading to prediction of large (3,5) or small (4) charge transfer. Within impulse approximation, the Compton profiles are used to determine the electron momentum distribution of the solid along selected directions. As it works in momentum space, the inelastic scattering is a very sensitive test of the ground-state calculated wave-functions. Compton profiles have been measured, using the high resolution spectrometer from the LURE synchroton source, with intercalated HOPG samples. The special features of the conduction band of KC8 are discussed in comparison with theoretical band structure calculations (1,2). For more accurate check, we need the theoretical Compton profiles based on calculated wave-functions.

G. Loupias; J. Chomilier; J. Tarbes; D. Guerard

1988-01-01T23:59:59.000Z

265

Quasi-zero dimensional CuB2O4: a resonant inelastic X-ray scattering case study  

SciTech Connect (OSTI)

We explore the general phenomenology of resonant inelastic scattering (RIXS) using CuB{sub 2}O{sub 4}, a network of CuO{sub 4} plaquettes electronically isolated by B{sup +3} ions. Spectra show a small number of well-separated features, and we exploit the simple electronic structure to explore RIXS phenomenology by developing a calculation which allows for intermediate-state effects ignored in standard approaches. These effects are found to be non-negligible and good correspondence between our model and experiment leads to a simple picture of such phenomenology as the genesis of d {yields} d excitations at the K edge and intermediate-state interference effects.

Hancock, J.N.

2010-04-29T23:59:59.000Z

266

Chest x-Rays  

Broader source: Energy.gov [DOE]

The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica.

267

X-ray beamsplitter  

DOE Patents [OSTI]

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5--50 pairs of alternate Mo/Si layers with a period of 20--250 A. The support membrane is 10--200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window. 6 figs.

Ceglio, N.M.; Stearns, D.G.; Hawryluk, A.M.; Barbee, T.W. Jr.

1987-08-07T23:59:59.000Z

268

X-ray beamsplitter  

DOE Patents [OSTI]

An x-ray beamsplitter which splits an x-ray beam into two coherent parts by reflecting and transmitting some fraction of an incident beam has applications for x-ray interferometry, x-ray holography, x-ray beam manipulation, and x-ray laser cavity output couplers. The beamsplitter is formed of a wavelength selective multilayer thin film supported by a very thin x-ray transparent membrane. The beamsplitter resonantly transmits and reflects x-rays through thin film interference effects. A thin film is formed of 5-50 pairs of alternate Mo/Si layers with a period of 20-250 A. The support membrane is 10-200 nm of silicon nitride or boron nitride. The multilayer/support membrane structure is formed across a window in a substrate by first forming the structure on a solid substrate and then forming a window in the substrate to leave a free-standing structure over the window.

Ceglio, Natale M. (Livermore, CA); Stearns, Daniel S. (Mountain View, CA); Hawryluk, Andrew M. (Modesto, CA); Barbee, Jr., Troy W. (Palo Alto, CA)

1989-01-01T23:59:59.000Z

269

X-ray binaries  

E-Print Network [OSTI]

We review the nuclear astrophysics aspects of accreting neutron stars in X-ray binaries. We summarize open astrophysical questions in light of recent observations and their relation to the underlying nuclear physics. Recent progress in the understanding of the nuclear physics, especially of X-ray bursts, is also discussed.

H. Schatz; K. E. Rehm

2006-08-01T23:59:59.000Z

270

Cryogenic x-ray diffraction microscopy utilizing high-pressure cryopreservation  

Science Journals Connector (OSTI)

We present cryo x-ray diffraction microscopy of high-pressure-cryofixed bacteria and report high-convergence imaging with multiple image reconstructions. Hydrated D. radiodurans cells were cryofixed at 200 MPa pressure into ?10??m-thick water layers and their unstained, hydrated cellular environments were imaged by phasing diffraction patterns, reaching sub-30-nm resolutions with hard x-rays. Comparisons were made with conventional ambient-pressure-cryofixed samples, with respect to both coherent small-angle x-ray scattering and the image reconstruction. The results show a correlation between the level of background ice signal and phasing convergence, suggesting that phasing difficulties with frozen-hydrated specimens may be caused by high-background ice scattering.

Enju Lima; Yuriy Chushkin; Peter van der Linden; Chae Un Kim; Federico Zontone; Philippe Carpentier; Sol M. Gruner; Petra Pernot

2014-10-15T23:59:59.000Z

271

hal-00154048,version1-12Jun2007 The new very small angle neutron scattering  

E-Print Network [OSTI]

hal-00154048,version1-12Jun2007 The new very small angle neutron scattering spectrometer The design and characteristics of the new very small angle neutron scattering spectrometer under construction in order to fill the gap between light scattering and classical small angle neutron scattering (SANS

Boyer, Edmond

272

Doppler shift anisotropy in small angle neutron scattering  

Science Journals Connector (OSTI)

The two-dimensional patterns in our small angle neutron scattering (SANS) experiments from rapidly moving aerosols are anisotropic. To test the kinematic theory of two-body scattering that describes the anisotropy, we conducted SANS experiments using a constant source of D2O aerosol with droplets moving at ?440 m/s, and varied the neutron velocity from 267 to 800 m/s. The theoretically predicted anisotropy of the laboratory scattering intensities agrees well with the experimental results. Based on an analysis of the scattering intensity in the Guinier region, we also determined the particle velocity. The results are in very good agreement with independent velocity estimates based on supersonic flow measurements.

B. E. Wyslouzil; G. Wilemski; J. L. Cheung; R. Strey; J. Barker

1999-10-01T23:59:59.000Z

273

Theory of low energy excitations in resonant inelastic x-ray scattering for rare-earth systems: Yb compounds as typical examples  

Science Journals Connector (OSTI)

Theoretical predictions are given for low energy excitations, such as crystal field excitations and Kondo resonance excitations, to be detected by high-resolution measurements of resonant inelastic x-ray scattering (RIXS) of rare-earth materials with Yb compounds as typical examples. Crystal field excitations in the Yb 3d RIXS of a Yb3+ ion in the cubic crystal field are formulated, and the calculation of RIXS spectra for YbN is done. Kondo resonance excitations revealed in the Yb 3d RIXS spectra are calculated for mixed-valence Yb compounds, Yb1-xLuxAl3, in the leading term approximation of the 1/Nf expansion method with a single impurity Anderson model. It is emphasized that the high-resolution RIXS with polarization dependence is a powerful tool to study the crystal field levels together with their symmetry and also the Kondo bound state in rare-earth compounds. Some in-depth discussions are given on the polarization effects of RIXS, including 4d and 2p RIXS spectra, the coherence effect of the Kondo bound states, and the importance of the high-resolution RIXS spectra for condensed matter physics under extreme conditions.

A. Kotani

2011-04-25T23:59:59.000Z

274

Probing of bonding changes in B[subscript 2]O[subscript 3] glasses at high pressure with inelastic X-ray scattering  

SciTech Connect (OSTI)

Full understanding of atomic arrangement in amorphous oxides both at ambient and high pressure is an ongoing fundamental puzzle. Whereas the structures of archetypal oxide glasses such as v-B{sub 2}O{sub 3} at high pressure are essential to elucidate origins of anomalous macroscopic properties of more complex melts, knowledge of the high-pressure structure and pressure-induced coordination changes of these glasses has remained elusive due to lack of suitable in situ experimental probes. Here, we report synchrotron inelastic X-ray scattering results for v-{sub 2}O{sub 3} at pressures up to 22.5 GPa, revealing the nature of pressure-induced bonding changes and the structure. Direct in situ measurements show a continuous transformation from tri-coordinated to tetra-coordinated boron beginning at 4-7 GPa with most of the boron tetra-coordinated above 20 GPa, forming dense tetrahedral v-B{sub 2}O{sub 3}. After decompression from high pressure the bonding reverts back to tri-coordinated boron but with the data suggesting a permanent densification.

Lee, Sung Kuen; Eng, Peter J.; Mao, Ho-Kwang; Meng, Yue; Newville, Matthew; Hu, Michael Y.; Shu, Jinfu (Seoul); (CIW); (UC)

2010-07-19T23:59:59.000Z

275

Investigations of the R5(SixGe1-x)4 Intermetallic Compounds by X-Ray Resonant Magnetic Scattering  

SciTech Connect (OSTI)

The XRMS experiment on the Gd{sub 5}Ge{sub 4} system has shown that, below the Neel temperature, T{sub N} = 127 K, the magnetic unit cells is the same as the chemical unit cell. From azimuth scans and the Q dependence of the magnetic scattering, all three Gd sites in the structure were determined to be in the same magnetic space group Pnma. The magnetic moments are aligned along the c-axis and the c-components of the magnetic moments at the three different sites are equal. The ferromagnetic slabs are stacked antiferromagnetically along the b-direction. They found an unusual order parameter curve in Gd{sub 5}Ge{sub 4}. A spin-reorientation transition is a possibility in Gd{sub 5}Ge{sub 4}, which is similar to the Tb{sub 5}Ge{sub 4} case. Tb{sub 5}Ge{sub 4} possesses the same Sm{sub 5}Ge{sub 4}-type crystallographic structure and the same magnetic space group as Gd{sub 5}Ge{sub 4} does. The difference in magnetic structure is that Tb{sub 5}Ge{sub 4} has a canted one but Gd{sub 5}Ge{sub 4} has nearly a collinear one in the low temperature antiferromagnetic phase. The competition between the magneto-crystalline anisotropy and the nearest-neighbor magnetic exchange interactions may allow a 3-dimensional canted antiferromagnetic structure in Tb{sub 5}Ge{sub 4}. The spin-reorientation transition in both Gd{sub 5}Ge{sub 4} and Tb{sub 5}Ge{sub 4} may arise from the competition between the magnetic anisotropy from the spin-orbit coupling of the conduction electrons and the dipolar interactions anisotropy.

Lizhi Tan

2008-08-18T23:59:59.000Z

276

Pitch-angle scattering of energetic particles with adiabatic focusing  

E-Print Network [OSTI]

Understanding turbulent transport of charged particles in magnetized plasmas often requires a model for the description of random variations in the particle's pitch angle. The Fokker-Planck coefficient of pitch-angle scattering, which is used to describe scattering parallel to the mean magnetic field, is therefore of central importance. Whereas quasi-linear theory assumes a homogeneous mean magnetic field, such a condition is often not fulfilled, especially for high-energy particles. Here, a new derivation of the quasi-linear approach is given that is based on the unperturbed orbit found for an adiabatically focused mean magnetic field. The results show that, depending on the ratio of the focusing length and the particle's Larmor radius, the Fokker-Planck coefficient is significantly modified but agrees with the classical expression in the limit of a homogeneous mean magnetic field.

Tautz, R C; Dosch, A

2014-01-01T23:59:59.000Z

277

E-Print Network 3.0 - angle neutron scattering Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

neutron scattering Search Powered by Explorit Topic List Advanced Search Sample search results for: angle neutron scattering Page: << < 1 2 3 4 5 > >> 1 Exceptional tools for...

278

X-ray laser  

DOE Patents [OSTI]

An X-ray laser (10) that lases between the K edges of carbon and oxygen, i.e. between 44 and 23 Angstroms, is provided. The laser comprises a silicon (12) and dysprosium (14) foil combination (16) that is driven by two beams (18, 20) of intense line focused (22, 24) optical laser radiation. Ground state nickel-like dysprosium ions (34) are resonantly photo-pumped to their upper X-ray laser state by line emission from hydrogen-like silicon ions (32). The novel X-ray laser should prove especially useful for the microscopy of biological specimens.

Nilsen, Joseph (Livermore, CA)

1991-01-01T23:59:59.000Z

279

Monitoring simultaneously the growth of nanoparticles and aggregates by in situ ultra-small-angle x-ray scattering  

E-Print Network [OSTI]

, silica volume fraction, number concentration, radius of gyration of the aggregate, and number of primary powders for a wide range of industrial and research uses. The particle size is controlled mainly through, a detailed quantitative comparison between the average primary-particle diameters obtained from nitrogen

Beaucage, Gregory

280

Small-Angle X-Ray Scattering for Imaging of Surface Layers on Intact Bacteria in the Native Environment  

Science Journals Connector (OSTI)

...primary particles or not? J. Colloid. Interface Sci. 194 :311-318. 25. Sinko K...of crystalline catalase as an internal standard of length in electron microscopy. J...Wu, and RM Glaeser. 1986. Three-dimensional structure of the surface layer protein...

Gerhard Sekot; David Schuster; Paul Messner; Dietmar Pum; Herwig Peterlik; Christina Schffer

2013-03-15T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


281

A structural model for unfolded proteins from residual dipolar couplings and small-angle x-ray scattering  

Science Journals Connector (OSTI)

...Burmeister, W. P., Ruigrok, R. W. H. & Marion, D. ( 2004 ) Virology...Tarbouriech, N., Curran, J. Ruigrok, R. W. H. & Burmeister, W. P. ( 2000...Chain Molecules (Wiley, New York). 33 Pappu, R. V., Srinivasan, R. & Rose, G...

Pau Bernad; Laurence Blanchard; Peter Timmins; Dominique Marion; Rob W. H. Ruigrok; Martin Blackledge

2005-01-01T23:59:59.000Z

282

X-ray absorption spectroscopy  

E-Print Network [OSTI]

009-9473-8 REVIEW X-ray absorption spectroscopy Junko Yano and application of X-ray absorption spectroscopy, bothX-ray absorption near-edge structure (XANES) and extended X-

Yano, Junko; Yachandra, Vittal K.

2009-01-01T23:59:59.000Z

283

X-ray Absorption Spectroscopy  

E-Print Network [OSTI]

type: Review X-ray Absorption Spectroscopy Junko Yano andPhotosystem II; XAS, X-ray absorption spectroscopy; EXAFS,X-ray absorption fine structure; EPR, electron paramagnetic

Yano, Junko

2010-01-01T23:59:59.000Z

284

The BioCAT undulator beamline 18ID: A facility for biological non-crystalline diffraction and x-ray absorption spectroscopy at the APS  

SciTech Connect (OSTI)

The 18ID undulator beamline of the Biophysics Collaborative Access Team at the Advanced Photon Source, Argonne, IL, USA, is a high-performance instrument designed for, and dedicated to, the study of partially ordered and disordered biological materials using the techniques of small-angle X-ray scattering, fiber diffraction, and X-ray absorption spectroscopy. The beamline and associated instrumentation are described in detail and examples of the representative experimental results are presented.

Fischetti, R.; Stepanov, S.; Rosenbaum, G.; Barrea, R.; Black, E.; Gore, D.; Heurich, R.; Kondrashkina, E.; Kropf, A.J.; Wang, S.; Zhang, K.; Irving, T.C.; Bunker, G.B. (IIT); (Georgia)

2008-07-02T23:59:59.000Z

285

X-Ray Generators  

Science Journals Connector (OSTI)

There are many types of X-ray generators sold commercially. The following are some of ... that should be considered when selecting a particular generator for a particular purpose. All the companies listed below s...

Reuben Rudman

1972-01-01T23:59:59.000Z

286

Pitch angle scattering and synchrotron radiation of relativistic runaway electrons in tokamak stochastic magnetic fields  

E-Print Network [OSTI]

Pitch angle scattering and synchrotron radiation of relativistic runaway electrons in tokamak is of a very different nature leading to a pitch angle scattering process which, under proper conditions, may

Martín-Solís, José Ramón

287

Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Scattering Print Scattering Print When a crystalline sample is illuminated with x-rays, the x-rays are scattered (diffracted) into very specific directions with various intensities. Detectors are used to measure this "diffraction pattern," which is then processed by computers to deduce the arrangement of atoms within the crystal. Hard x-rays have wavelengths comparable to the distance between atoms. Essentially everything we know about the atomic structure of materials is based on results from x-ray and neutron diffraction. From advanced ceramics to catalysts, from semiconductor technology to the frontiers of medicine, and from new magnetic materials and devices to framework compounds used to sequester radioactive waste, crystallography using hard x-ray diffraction techniques at synchrotron radiation facilities plays a crucial role in our ability to understand and control the world in which we live.

288

Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Scattering Print Scattering Print When a crystalline sample is illuminated with x-rays, the x-rays are scattered (diffracted) into very specific directions with various intensities. Detectors are used to measure this "diffraction pattern," which is then processed by computers to deduce the arrangement of atoms within the crystal. Hard x-rays have wavelengths comparable to the distance between atoms. Essentially everything we know about the atomic structure of materials is based on results from x-ray and neutron diffraction. From advanced ceramics to catalysts, from semiconductor technology to the frontiers of medicine, and from new magnetic materials and devices to framework compounds used to sequester radioactive waste, crystallography using hard x-ray diffraction techniques at synchrotron radiation facilities plays a crucial role in our ability to understand and control the world in which we live.

289

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

290

E-Print Network 3.0 - angle scattering techniques Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

angle ... Source: Ecole Polytechnique, Centre de mathmatiques Collection: Mathematics 2 Neutron Scattering in Polymer Micelle Characterization Summary: - Nondestructive technique...

291

X-ray Microscopy and Imaging: 2-BM  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

BM BM Introduction The 2-BM beamline offers measurement capabilities for x-ray microtomography, x-ray topography and x-ray microdiffraction. X-ray microtomography and x-ray diffraction instruments are installed on separate optical tables for independent operation with fast switch over time. Optically-coupled high-resolution CCD system is used for microtomography and topography with up to 1 micron spatial resolution. X-ray microdiffraction setup consists of KB microfocussing mirrors (~3 micron minimum spot), four-circle Huber diffractometer, high-precision translation sample stage, two orthogonally-mounted video cameras for viewing sample, fluorescence detector (Si-drift diode) and diffraction detector (a scintillation detector or a CCD). Three different levels of monochromaticity are available. Conventional monochromatic x-rays from a double-bounced Si (111) crystal monochromator (DCM, D E/E=1E-4), wide band-pass monochromatic x-rays from a double multilayer monochromator (DMM, D E/E=1~4E-2) and pink beam. The available x-ray range is from 5 keV to 30 keV. The lower limit is due to the x-ray windows and the upper limit is due to the critical angle of the x-ray mirror. Two different coatings (Cr and Pt) for the x-ray mirror allow either 20 keV or 30 keV energy cutoff.

292

X-ray Diffraction / MSE 603 Spring 2002 Qun Shen / CHESS qs11@cornell.edu  

E-Print Network [OSTI]

X-ray Diffraction / MSE 603 Spring 2002 Qun Shen / CHESS qs11@cornell.edu 1. X-ray production & basic properties ­ common sources for diffraction experiments ­ synchrotron radiation ­ response to x-rays by an electron ­ refraction index ­ total external reflection & evanescent wave, TXRF 2. X-ray scattering basics

Shen, Qun

293

Apparatus for generating x-ray holograms  

DOE Patents [OSTI]

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced.

Rhodes, Charles K. (Chicago, IL); Boyer, Keith (Los Alamos, NM); Solem, Johndale C. (Los Alamos, NM); Haddad, Waleed S. (Chicago, IL)

1990-01-01T23:59:59.000Z

294

Apparatus for generating x-ray holograms  

DOE Patents [OSTI]

Apparatus for x-ray microholography of living biological materials. A Fourier transform holographic configuration is described as being most suitable for the 3-dimensional recording of the physical characteristics of biological specimens. The use of a spherical scatterer as a reference and a charge-coupled device two-dimensional detector array placed in the forward direction relative to the incident x-radiation for viewing electromagnetic radiation simultaneously scattered from both the specimen and the reference scatterer permits the ready reconstruction of the details of the specimen from the fringe pattern detected by the charge-coupled device. For example, by using a nickel reference scatter at 4.5 nm, sufficient reference illumination is provided over a wide enough angle to allow similar resolution in both transverse and longitudinal directions. Both laser and synchrotron radiation sources are feasible for generating microholographs. Operation in the water window (2.4 to 4.5 nm) should provide maximum contrast for features of the specimen and spatial resolution on the order of the wavelength of x-radiation should be possible in all three dimensions, which is sufficient for the visualization of many biological features. It is anticipated that the present apparatus will find utility in other areas as well where microscopic physical details of a specimen are important. A computational procedure which enables the holographic data collected by the detector to be used to correct for misalignments introduced by inexact knowledge of the relative positions of the spherical reference scatterer and the sample under investigation has been developed. If the correction is performed prior to reconstruction, full compensation can be achieved and a faithfully reconstructed image produced. 7 figs.

Rhodes, C.K.; Boyer, K.; Solem, J.C.; Haddad, W.S.

1990-09-11T23:59:59.000Z

295

Contrast variation in spin-echo small angle neutron scattering  

Science Journals Connector (OSTI)

The use of contrast variation in spin-echo small angle neutron scattering (SESANS) experiments is discussed for the case of colloidal structural investigation. On the basis of calculations for several model systems, we find that the contrast variation SESANS technique, in terms of the measured SESANS correlation function G(z), is not sensitive to the structural characteristics of colloidal suspensions consisting of particles with uniform scattering length density profiles. However, its ability to resolve structural heterogeneity, at both intra-colloidal and inter-colloidal length scales, is clearly demonstrated. The prospect of using this new technique to investigate structural information that is difficult to probe in other ways is also explored.

Xin Li; Bin Wu; Yun Liu; Roger Pynn; Chwen-Yang Shew; Gregory S Smith; Kenneth W Herwig; J Lee Robertson; Wei-Ren Chen; Li Liu

2012-01-01T23:59:59.000Z

296

X-ray imaging crystal spectrometer for extended X-ray sources  

DOE Patents [OSTI]

Spherically or toroidally curved, double focusing crystals are used in a spectrometer for X-ray diagnostics of an extended X-ray source such as a hot plasma produced in a tokomak fusion experiment to provide spatially and temporally resolved data on plasma parameters using the imaging properties for Bragg angles near 45. For a Bragg angle of 45.degree., the spherical crystal focuses a bundle of near parallel X-rays (the cross section of which is determined by the cross section of the crystal) from the plasma to a point on a detector, with parallel rays inclined to the main plain of diffraction focused to different points on the detector. Thus, it is possible to radially image the plasma X-ray emission in different wavelengths simultaneously with a single crystal.

Bitter, Manfred L. (Princeton, NJ); Fraenkel, Ben (Jerusalem, IL); Gorman, James L. (Bordentown, NJ); Hill, Kenneth W. (Lawrenceville, NJ); Roquemore, A. Lane (Cranbury, NJ); Stodiek, Wolfgang (Princeton, NJ); von Goeler, Schweickhard E. (Princeton, NJ)

2001-01-01T23:59:59.000Z

297

X-ray Emission Processes in Radio Jets  

E-Print Network [OSTI]

The emission processes responsible for the observed X-rays from radio jets are commonly believed to be non-thermal, but in any particular case, it is unclear if synchrotron emission or one or more varieties of inverse Compton emission predominates. We present a formulation of inverse Compton emission from a relativistically moving jet (``IC/beaming'') which relies on radio emitting synchrotron sources for which the energy densities in particles and fields are comparable. We include the non-isotropic nature of inverse Compton scattering of the relativistic electrons on photons of the cosmic microwave background (CMB) and provide beaming parameters for a number of jets. A list of X-ray emitting jets is given and the jets are classified on the basis of their morphology and spectral energy distribution to determine their likely emission process. We conclude that these jets have significant bulk relativistic velocities on kpc scales; that higher redshift sources require less beaming because the energy density of the CMB is significantly greater than locally; and that for some nearby sources, synchrotron X-ray emission predominates because the jet makes a large angle to the line of sight.

D. E. Harris; H. Krawczynski

2001-09-27T23:59:59.000Z

298

X-ray beam finder  

DOE Patents [OSTI]

An X-ray beam finder for locating a focal spot of an X-ray tube includes a mass of X-ray opaque material having first and second axially-aligned, parallel-opposed faces connected by a plurality of substantially identical parallel holes perpendicular to the faces and a film holder for holding X-ray sensitive film tightly against one face while the other face is placed in contact with the window of an X-ray head.

Gilbert, H.W.

1983-06-16T23:59:59.000Z

299

Electronic Structure of the Mn(4)Ca Cluster in the Oxygen-Evolving Complex of Photosystem Ii Studied By Resonant Inelastic X-Ray Scattering  

SciTech Connect (OSTI)

Oxygen-evolving complex (Mn{sub 4}Ca cluster) of Photosystem II cycles through five intermediate states (S{sub i}-states, i=0--4) before a molecule of dioxygen is released. During the S-state transitions, electrons are extracted from the OEC, either from Mn or alternatively from a Mn ligand. The oxidation state of Mn is widely accepted as Mn{sub 4}(III{sub 2},IV{sub 2}) and Mn{sub 4}(III,IV{sub 3}) for S{sub 1} and S{sub 2} states, while it is still controversial for the S{sub 0} and S{sub 3} states. We used resonant inelastic X-ray scattering (RIXS) to study the electronic structure of Mn{sub 4}Ca complex in the OEC. The RIXS data yield two-dimensional plots that provide a significant advantage by obtaining both K-edge pre-edge and L-edge-like spectra simultaneously. The second energy dimension separates the pre-edge (1s to 3d) transitions from the main K-edge (1s to 4p), and thus more precise analysis is possible. The 1s2p RIXS final state electron configuration along the energy transfer axis is identical to conventional L-edge absorption spectroscopy and the RIXS spectra are therefore sensitive to the metal spin state. We have collected data from PS II samples in the each of the S-states and compared them with data from various inorganic Mn complexes. The spectral changes in the Mn 1s2p{sub 3/2} RIXS spectra between the S-states are small compared to those of the oxides of Mn and coordination complexes. The results indicate strong covalency for the electronic configuration in the OEC, and we conclude that the electron is transferred from a strongly delocalized orbital, compared to those in Mn oxides or coordination complexes. The magnitude for the S{sub 0} to S{sub 1}, and S{sub 1} to S{sub 2} transitions is twice as large as that during the S{sub 2} to S{sub 3} transition, indicating that the electron for this transition is extracted from a highly delocalized orbital with little change in charge density at the Mn atoms. The RIXS spectra of S{sub 0} and S{sub 3} states also showed characteristic features which were not clear from the K-edge spectroscopy.

Yano, J.; Pushkar, Y.; Messinger, J.; Bergmann, U.; Glatzel, P.; Yachandra, V.K.

2009-06-04T23:59:59.000Z

300

APS 7-BM Beamline: X-Ray Resources  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Useful Websites Useful Websites X-Ray Interactions with Matter from CRXO at LBNL. Intuitive interface for x-ray transmission and reflectivity for a wide range of materials. X-Ray Data Booklet from LBNL. Slightly outdated in places, but many useful tables of edge energies, fluorescence lines, and crystal lattice spacings. NIST XCOM Database. Powerful database of photoelectric absorption, elastic scattering, and Compton scattering cross-sections for a wide range of materials. X-Ray Server. Maintained by Sergey Stepanov at GMCA at the APS, this website has several powerful calculators for simulating x-ray reflection and diffraction. Software X-Ray Oriented Programs (XOP). This program, written by scientists at the ESRF and APS, is widely used in the synchrotron research community.

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


301

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

302

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

303

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

304

Compton backscattered collimated x-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source is disclosed for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications. 4 figs.

Ruth, R.D.; Huang, Z.

1998-10-20T23:59:59.000Z

305

Compton backscattered collmated X-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

2000-01-01T23:59:59.000Z

306

Compton backscattered collimated x-ray source  

DOE Patents [OSTI]

A high-intensity, inexpensive and collimated x-ray source for applications such as x-ray lithography is disclosed. An intense pulse from a high power laser, stored in a high-finesse resonator, repetitively collides nearly head-on with and Compton backscatters off a bunched electron beam, having relatively low energy and circulating in a compact storage ring. Both the laser and the electron beams are tightly focused and matched at the interaction region inside the optical resonator. The laser-electron interaction not only gives rise to x-rays at the desired wavelength, but also cools and stabilizes the electrons against intrabeam scattering and Coulomb repulsion with each other in the storage ring. This cooling provides a compact, intense bunch of electrons suitable for many applications. In particular, a sufficient amount of x-rays can be generated by this device to make it an excellent and flexible Compton backscattered x-ray (CBX) source for high throughput x-ray lithography and many other applications.

Ruth, Ronald D. (Woodside, CA); Huang, Zhirong (Stanford, CA)

1998-01-01T23:59:59.000Z

307

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Reflection Print Lensless X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs combine the advantages of sychrotron light sources (high brightness and x-ray wavelengths relevant to atomic and molecular phenomena) with the advantages of visible-light lasers (highly coherent beams). All of these characteristics are important for coherent x-ray diffraction imaging-lensless imaging techniques that are proving to be integral to single-shot, high-resolution imaging of both complex materials and biological samples. Existing techniques are typically designed for transmission geometry, however, and use isolated objects, requiring special sample fabrication and restricting the type of samples under investigation. Recently, researchers from the ALS and the University of Oregon have shown at ALS Beamline 12.0.2 that it is possible to form x-ray holograms in reflection geometry by using the light scattered from a sample, opening the door to lensless imaging of a wealth of new material samples.

308

X-ray Spectrometry  

Science Journals Connector (OSTI)

These provide excellent energy resolution for a wide range of X-ray energies, from the optical range up to several kiloelectronvolts. ... The Astro-E2 launched in 2005 was the first mission that contained a low-temperature microcalorimeter-based observatory, and three more low-temperature detector-based observatories are being developed (NeXT, Constellation-X, ZEUS). ...

Imre Szalki; Jnos Osn; Ren E. Van Grieken

2006-05-10T23:59:59.000Z

309

Pitch angle scattering of an energetic magnetized particle by a circularly polarized electromagnetic wave  

E-Print Network [OSTI]

Pitch angle scattering of an energetic magnetized particle by a circularly polarized://pop.aip.org/features/most_downloaded Information for Authors: http://pop.aip.org/authors #12;Pitch angle scattering of an energetic magnetized valley, but for finite mismatch, there can be two valleys separated by a hill. A large pitch angle

Bellan, Paul M.

310

Direct Detection of Resonant Electron Pitch Angle Scattering by Whistler Waves in a Laboratory Plasma  

E-Print Network [OSTI]

Direct Detection of Resonant Electron Pitch Angle Scattering by Whistler Waves in a Laboratory on the first laboratory experiment to directly detect resonant pitch angle scattering of energetic (ke or less, making it difficult to detect changes in electron pitch angle. A review of observations

California at Los Angles, University of

311

Solvent Entrainment in and Flocculation of Asphaltenic Aggregates Probed by Small-Angle Neutron Scattering  

E-Print Network [OSTI]

-Angle Neutron Scattering Keith L. Gawrys, George A. Blankenship, and Peter K. Kilpatrick* Department of ChemicalVed September 14, 2005. In Final Form: January 30, 2006 While small-angle neutron scattering (SANS) has proven to the scattering intensity curves were performed using the Guinier approximation, the Ornstein- Zernike (or Zimm

Kilpatrick, Peter K.

312

Small angle neutron scattering on periodically deformed polymers A. R. Rennie  

E-Print Network [OSTI]

765 Small angle neutron scattering on periodically deformed polymers A. R. Rennie Institut für Phys-768 SEPTEMBRE 1984, 1. Introduction. Neutron scattering has proved a useful tool for the investigation of a wide time for a small angle neutron scattering spectrum is several minutes. Obser- vation on rapidly

Boyer, Edmond

313

High temperature furnaces for small and large angle neutron scattering of disordered materials  

E-Print Network [OSTI]

725 High temperature furnaces for small and large angle neutron scattering of disordered materials and small angle neutron scattering (SANS) experiments respectively. They are vacuum furnaces with a thin maintained in a tantalum box. In a neutron beam, the furnaces produce a very low scattering level (without

Boyer, Edmond

314

Using multi-angle scattered sound to size fish swimbladders Jules S. Jaffe  

E-Print Network [OSTI]

Using multi-angle scattered sound to size fish swimbladders Jules S. Jaffe Jaffe, J. S. 2006. Using multi-angle scattered sound to size fish swimbladders. e ICES Journal of Marine Science, 63: 1397e1404 a simple one-dimensional model of scatter from a fish swimbladder, an expression is derived that predicts

Jaffe, Jules

315

X-ray Science Division: Groups  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Division: Groups Division: Groups Atomic, Molecular and Optical Physics (AMO) Primary Contact: Stephen Southworth Work focuses on understanding how strong optical and x-ray fields interact with matter, with an emphasis on photonic control of electronic, atomic and molecular motion. Chemical and Materials Science (CMS) Primary Contact: Randy Winans Research Disciplines: Chemistry, Materials Science Detectors (DET) Primary Contact: Antonino Miceli GMCA Structural Biology Facility (MX) Primary Contact: Robert Fischetti Research Disciplines: Biology, Life Sciences Imaging (IMG) Primary Contact: Francesco DeCarlo Research Disciplines: Materials Science, Biology, Physics, Life Sciences Inelastic X-ray & Nuclear Resonant Scattering (IXN) Primary Contact: Thomas Gog Research Disciplines: Condensed Matter Physics, Geophysics, Materials

316

X-ray spectra transmitted through Compton-thick absorbers  

E-Print Network [OSTI]

X-ray spectra transmitted through matter which is optically thick to Compton scattering are computed by means of Monte Carlo simulations. Applications to the BeppoSAX data of the Seyfert 2 galaxy in Circinus, and to the spectral modeling of the Cosmic X-ray Background, are discussed.

Giorgio Matt; Fulvio Pompilio; Fabio La Franca

1999-04-24T23:59:59.000Z

317

Synchrotron x-ray reflectivity study of oxidation/passivation of copper and silicon.  

SciTech Connect (OSTI)

Synchrotron x-ray-scattering technique studies of copper and silicon electrochemical interfaces are reported. These two examples illustrate the application of synchrotron x-ray techniques for oxidation, passivation, and dissolution of metals and semiconductors.

Chu, Y.; Nagy, Z.; Parkhutik, V.; You, H.

1999-07-21T23:59:59.000Z

318

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

319

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

320

X-Ray Diffraction Microscopy of Magnetic Structures  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Diffraction Microscopy of Magnetic Structures Print X-Ray Diffraction Microscopy of Magnetic Structures Print science brief icon Scientists working at ALS Beamline 12.0.2.2 have demonstrated a new x-ray technique for producing short-exposure nanoscale images of the magnetic structure of materials. The new method combines aspects of coherent x-ray diffraction, which can determine 3-D charge distributions, and resonant magnetic scattering, which is sensitive to magnetic structures. Physicists have used coherent x-ray diffraction to measure the electron density of complicated molecules. The formula used to make these calculations contains terms that relate to the electron spin of magnetic atoms, but these terms are traditionally ignored since coherent x-ray diffraction has not been used to retrieve magnetic information. Using the full formula allows for the determination of not only the electron density, but also the magnetic spin distribution and its orientation.

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


321

X-ray Pinhole Camera Measurements  

SciTech Connect (OSTI)

The development of the rod pinch diode [1] has led to high-resolution radiography for dynamic events such as explosive tests. Rod pinch diodes use a small diameter anode rod, which extends through the aperture of a cathode plate. Electrons borne off the aperture surface can self-insulate and pinch onto the tip of the rod, creating an intense, small x-ray source (Primary Pinch). This source has been utilized as the main diagnostic on numerous experiments that include high-value, single-shot events. In such applications there is an emphasis on machine reliability, x-ray reproducibility, and x-ray quality [2]. In tests with the baseline rod pinch diode, we have observed that an additional pinch (Secondary Pinch) occurs at the interface near the anode rod and the rod holder. This suggests that stray electrons exist that are not associated with the Primary Pinch. In this paper we present measurements on both pinches using an x-ray pinhole camera. The camera is placed downstream of the Primary Pinch at an angle of 60 with respect to the diode centerline. This diagnostic will be employed to diagnose x-ray reproducibility and quality. In addition, we will investigate the performance of hybrid diodes relating to the formation of the Primary and Secondary Pinches.

Nelson, D. S. [NSTec; Berninger, M. J. [NSTec; Flores, P. A. [NSTec; Good, D. E. [NSTec; Henderson, D. J. [NSTec; Hogge, K. W. [NSTec; Huber, S. R. [NSTec; Lutz, S. S. [NSTec; Mitchell, S. E. [NSTec; Howe, R. A. [NSTec; Mitton, C. V. [NSTec; Molina, I. [NSTec; Bozman, D. R. [SNL; Cordova, S. R. [SNL; Mitchell, D. R. [SNL; Oliver, B. V. [SNL; Ormond, E. C. [SNL

2013-07-01T23:59:59.000Z

322

X-ray lithography using holographic images  

DOE Patents [OSTI]

Methods for forming X-ray images having 0.25 {micro}m minimum line widths on X-ray sensitive material are presented. A holographic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required. 15 figs.

Howells, M.S.; Jacobsen, C.

1997-03-18T23:59:59.000Z

323

X-ray lithography using holographic images  

DOE Patents [OSTI]

Methods for forming X-ray images having 0.25 .mu.m minimum line widths on X-ray sensitive material are presented. A holgraphic image of a desired circuit pattern is projected onto a wafer or other image-receiving substrate to allow recording of the desired image in photoresist material. In one embodiment, the method uses on-axis transmission and provides a high flux X-ray source having modest monochromaticity and coherence requirements. A layer of light-sensitive photoresist material on a wafer with a selected surface is provided to receive the image(s). The hologram has variable optical thickness and variable associated optical phase angle and amplitude attenuation for transmission of the X-rays. A second embodiment uses off-axis holography. The wafer receives the holographic image by grazing incidence reflection from a hologram printed on a flat metal or other highly reflecting surface or substrate. In this second embodiment, an X-ray beam with a high degree of monochromaticity and spatial coherence is required.

Howells, Malcolm S. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1997-01-01T23:59:59.000Z

324

E-Print Network 3.0 - angle elastic scattering Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Force Academy, University of New South Wales Collection: Physics ; Materials Science 2 Neutron Scattering in Polymer Micelle Characterization Summary: is changed 12;Small Angle...

325

Regge trajectory of the ?(J) particles and pp elastic scattering at large angles  

Science Journals Connector (OSTI)

It is shown that the proton-proton elastic scattering data at large angles can be described by a trajectory with the same shape as the ?(J) trajectory.

M. Arik; D. D. Coon; S. Yu

1976-02-01T23:59:59.000Z

326

E-Print Network 3.0 - angle scattering revision Sample Search...  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

and scattering, effective index, surface autocovariance, and correlation... . The phenomenology is complex, including specular and diffuse reflection, high-angle forward...

327

Conformational Changes in Sindbis Virus Induced by Decreased pH Are Revealed by Small-Angle Neutron Scattering  

Science Journals Connector (OSTI)

...Are Revealed by Small-Angle Neutron Scattering Lilin He a b Amanda Piper c...Oak Ridge, Tennessee, USA b Neutron Scattering Sciences Division, Oak Ridge...we employed small-angle neutron scattering with contrast variation to...

Lilin He; Amanda Piper; Flora Meilleur; Raquel Hernandez; William T. Heller; Dennis T. Brown

2011-12-07T23:59:59.000Z

328

The Structure of Sindbis Virus Produced from Vertebrate and Invertebrate Hosts as Determined by Small-Angle Neutron Scattering  

Science Journals Connector (OSTI)

...Determined by Small-Angle Neutron Scattering Published ahead of print on...Raleigh, North Carolina 27695 3 Neutron Scattering Sciences Division, Oak Ridge...determined by small-angle neutron scattering (SANS), a nondestructive...

Lilin He; Amanda Piper; Flora Meilleur; Dean A. A. Myles; Raquel Hernandez; Dennis T. Brown; William T. Heller

2010-03-10T23:59:59.000Z

329

Dynamical Studies Using Coherent X-rays: A Short Review and Prospects for the Future  

SciTech Connect (OSTI)

The use of coherent x-ray beams for studying the structure and dynamics of both surfaces and bulk materials is rapidly increasing due to the advent of new high-brilliance x-ray sources. The field of x-ray photon correlation spectroscopy (XPCS) has steadily grown from demonstration experiments carried out some 15 years ago, to studies addressing real problems at the forefront of condensed matter and has attracted increasing numbers of users. the principal applications have been in the fields of soft condensed matter and nanoscience, but extension to the study of slow fluctuations in magnetic systems will undoubtedly grow. This talk will attempt to survey some of the recent applications at the limits of currently existing instruments, and present a wish list for XPCS-capable beamlines of the future for attacking certain important problems in condensed matter and materials science. This talk will also present a new formulation of the scattering of partially coherent radiation by condensed matter, which will enable us to go beyond the simple, kinematic approximation that is usually made, but which breaks down for grazing incidence small-angle x-ray scattering geometry.

Sinha, Sunil K. [University of California, San Diego

2010-07-07T23:59:59.000Z

330

Polarization Entangled Photons at X-Ray Energies  

E-Print Network [OSTI]

We show that polarization entangled photons at x-ray energies can be generated via spontaneous parametric down conversion. Each of the four Bell states can be generated by choosing the angle of incidence and polarization of the pumping beam.

S. Shwartz; S. E. Harris

2010-12-16T23:59:59.000Z

331

X-ray Spectrometry  

Science Journals Connector (OSTI)

The segmented STJ operated at total count rates of above 105 counts/s, and the best-achieved energy resolution of their single STJ was found to be 10 eV for X-ray energies below 1 keV. ... The Mo?Au TES, with an operating temperature of 230 mK, was developed for the Constellation-X mission and the energy resolution of the spectrometer is ?28 eV at 3.3 keV. ...

Imre Szalki; Szabina B. Trk; Jasna Injuk; Ren E. Van Grieken

2002-05-18T23:59:59.000Z

332

X-Ray Source Based on the Parametric X-Rays  

E-Print Network [OSTI]

Prospects of parametric x-rays (PXR) application for the development of a tuneable quasi-monochromatic x-ray source for medical imaging are discussed. Analysis of basic requirements for electron accelerator shows that it must be relatively low-energy and high-current linac. In comparison with known ultra-relativistic cases, at low energies PXR properties will be modified to a great extent by multiple scattering of the electrons. PXR intensity dependence on target thickness and beam energy are calculated taking multiple scattering into account. It is concluded that PXR source based on real medical accelerators is feasible and can provide x-ray flux needful for obtaining high quality medical images.

Alexander Lobko; Olga Lugovskaya

2005-09-02T23:59:59.000Z

333

Time-Resolved Small-Angle Neutron Scattering Study of Polyethylene Crystallization from Solution  

E-Print Network [OSTI]

Time-Resolved Small-Angle Neutron Scattering Study of Polyethylene Crystallization from Solution-resolved small-angle neutron scattering (TR-SANS), the crystal- lization kinetics of polyethylene from deuterated of polyethylene crystallization from xylene solutions. One unique feature of this experimentation is that both

Wang, Howard "Hao"

334

Small angle neutron scattering from single-wall carbon nanotube suspensions: evidence for isolated  

E-Print Network [OSTI]

Small angle neutron scattering from single-wall carbon nanotube suspensions: evidence for isolated online: Abstract We report small angle neutron scattering (SANS) from dilute suspensions of purified University, Houghton, MI 49931, USA e NIST Center for Neutron Research, National Institute of Standards

Wang, Howard "Hao"

335

Small angle neutron scattering (SANS) under non-equilibrium conditions R. C. Oberthr  

E-Print Network [OSTI]

663 Small angle neutron scattering (SANS) under non-equilibrium conditions R. C. Oberthür Institut with the times obtained from quasi- elastic neutron and light scattering, which yield information about neutrons aux petits angles (DNPA) pour l'étude des systèmes hors d'équi- libre thermodynamique est

Boyer, Edmond

336

Salt-Dependent Compaction of Di-and Trinucleosomes Studied by Small-Angle Neutron Scattering  

E-Print Network [OSTI]

Salt-Dependent Compaction of Di- and Trinucleosomes Studied by Small-Angle Neutron Scattering, Germany, and Institut Laue-Langevin Grenoble, F-38042 Grenoble, France ABSTRACT Using small-angle neutron scattering (SANS), we have measured the salt-dependent static structure factor of di- and trinucleosomes from

Langowski, Jörg

337

X-ray and neutron scattering studies of the Rb?MnF? and Cu???xMgx̳GeO? in an external magnetic field  

E-Print Network [OSTI]

This thesis presents results of two scattering studies of low dimensional magnetic materials. The first is a neutron scattering study of Rb2MnF4, a nearly ideal two-dimensional square lattice Heisenberg antiferromagnet ...

Christianson, Rebecca J. (Rebecca Jean), 1973-

2001-01-01T23:59:59.000Z

338

Directional fine structure in absorption of white x rays: A tomographic interpretation P. Korecki,1,  

E-Print Network [OSTI]

structure in absorption of white x rays can be interpreted as real-space projections of atomic structure from neigh- boring atoms.1 A straightforward analysis of the extended x-ray absorption fine structure of the absorbing atoms. Thus, the absorption cross section is effectively modulated by the x-ray scattering

Korecki, Pawe³

339

X-ray Absorption Spectroscopy  

SciTech Connect (OSTI)

This review gives a brief description of the theory and application of X-ray absorption spectroscopy, both X-ray absorption near edge structure (XANES) and extended X-ray absorption fine structure (EXAFS), especially, pertaining to photosynthesis. The advantages and limitations of the methods are discussed. Recent advances in extended EXAFS and polarized EXAFS using oriented membranes and single crystals are explained. Developments in theory in understanding the XANES spectra are described. The application of X-ray absorption spectroscopy to the study of the Mn4Ca cluster in Photosystem II is presented.

Yano, Junko; Yachandra, Vittal K.

2009-07-09T23:59:59.000Z

340

X-ray fluorescence mapping  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

biololgical cells, over the measurement of impurities in solar cells, to the rare earth content of geological materials. A somewhat 'typical' layout for a X-ray fluorescence...

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


341

Sharper Focusing of Hard X-rays  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Sharper Focusing of Hard X-rays FROM: Physics News Update Number 773 #1, April 12, 2006, by Phil Schewe and Ben Stein Note: This text has been slightly modified from the original. Sharper focusing of hard x-rays has been achieved with a device developed at Argonne National Lab. Because of their high energy, x-rays are hard to focus: they can be reflected from a surface but only at a glancing angle (less than a tenth of a degree); they can be refracted but the index of refraction is very close to 1, so that making efficient lenses becomes a problem; and they can be diffracted, but the relatively thick, variable pitch grating required for focusing is tricky to achieve. The Argonne device is of the diffraction type, and it consists of a stack of alternating layers of metal and silicon, made by depositing progressively thicker layers. When the x-rays fall on such a structure, nearly edge-on, what they see is a grating (called a linear zone plate) consisting of a sort of bar-code pattern.

342

Multiple wavelength X-ray monochromators  

DOE Patents [OSTI]

An improved apparatus and method is provided for separating input x-ray radiation containing first and second x-ray wavelengths into spatially separate first and second output radiation which contain the first and second x-ray wavelengths, respectively. The apparatus includes a crystalline diffractor which includes a first set of parallel crystal planes, where each of the planes is spaced a predetermined first distance from one another. The crystalline diffractor also includes a second set of parallel crystal planes inclined at an angle with respect to the first set of crystal planes where each of the planes of the second set of parallel crystal planes is spaced a predetermined second distance from one another. In one embodiment, the crystalline diffractor is comprised of a single crystal. In a second embodiment, the crystalline diffractor is comprised of a stack of two crystals. In a third embodiment, the crystalline diffractor includes a single crystal that is bent for focusing the separate first and second output x-ray radiation wavelengths into separate focal points. 3 figs.

Steinmeyer, P.A.

1992-11-17T23:59:59.000Z

343

Diffraction with a coherent X-ray beam: dynamics and imaging  

Science Journals Connector (OSTI)

Techniques for coherent X-ray scattering measurements are detailed. Applications in the study of the dynamics of fluctuations and in lensless high-resolution imaging are described.

Livet, F.

2007-02-15T23:59:59.000Z

344

Your access to the Oak Ridge National Laboratory (ORNL) is approved beginning Sunday, June 20, 2010, for the second week of the Neutron X-ray Scattering School.  

E-Print Network [OSTI]

Your access to the Oak Ridge National Laboratory (ORNL) is approved beginning Sunday, June 20, 2010, Neutron Scattering Science User Office Oak Ridge National Laboratory ORNL Neutron Scattering School June 20-25, 2010 Oak Ridge National Laboratory Oak Ridge, Tennessee #12;

Pennycook, Steve

345

Reverse Monte Carlo analysis of the local order in liquid Ge{sub 0.15}Te{sub 0.85} alloys combining neutron scattering and x-ray absorption spectroscopy  

SciTech Connect (OSTI)

The structure of liquid Ge{sub 0.15}Te{sub 0.85} alloys that exhibit a density anomaly between 633 K and 733 K at ambient pressure was investigated using x-ray absorption spectroscopy at the Ge K edge. Using a reverse Monte Carlo method to combine the present results with neutron scattering data, we show that the volume contraction is associated with an increase of the first neighbor coordination number around both Ge and Te by about one atom. The coordination number of Ge increases from 3{+-}0.3 to 4.1{+-}0.3. These results support an interpretation of the density anomaly in terms of the same Peierls-like distortion mechanism acting in the liquid state and in the neighboring (pure Te and GeTe compound) phases.

Coulet, Marie-Vanessa; Testemale, Denis; Hazemann, Jean-Louis; Gaspard, Jean-Pierre; Bichara, Christophe [Laboratoire TECSEN, UMR 6122, CNRS-Universite Paul Cezanne, Campus de St Jerome, 13397 Marseille Cedex 20 (France); SNBL/ESRF, 6 rue Jules Horowitz, Boite Postale 220, 38043, Grenoble (France); Laboratoire de Cristallographie, 25 Avenue des Martyrs, Boite Postale 166, 38043 Grenoble (France) and European Synchroton Radiation Facility, 6 rue Jules Horowitz, Boite Postale 220, 38043 Grenoble (France); Physique de la Matiere Condensee, B5, Universite de Liege, B4000 Sart-Tilman (Belgium); Centre de Recherches en Matiere Condensee et Nanosciences-CNRS, Campus de Luminy, Case 913, F13288 Marseille (France)

2005-11-01T23:59:59.000Z

346

A highly modular beamline electrostatic levitation facility, optimized for in situ high-energy x-ray scattering studies of equilibrium and supercooled liquids  

SciTech Connect (OSTI)

High-energy x-ray diffraction studies of metallic liquids provide valuable information about structural evolution on the atomic length scale, leading to insights into the origin of the nucleation barrier and the processes of supercooling and glass formation. The containerless processing of the beamline electrostatic levitation (BESL) facility allows coordinated thermophysical and structural studies of equilibrium and supercooled liquids to be made in a contamination-free, high-vacuum ({approx}10{sup -8} Torr) environment. To date, the incorporation of electrostatic levitation facilities into synchrotron beamlines has been difficult due to the large footprint of the apparatus and the difficulties associated with its transportation and implementation. Here, we describe a modular levitation facility that is optimized for diffraction studies of high-temperature liquids at high-energy synchrotron beamlines. The modular approach used in the apparatus design allows it to be easily transported and quickly setup. Unlike most previous electrostatic levitation facilities, BESL can be operated by a single user instead of a user team.

Mauro, N.A.; Kelton, K.F. (WU)

2011-10-27T23:59:59.000Z

347

X-ray shearing interferometer  

DOE Patents [OSTI]

An x-ray interferometer for analyzing high density plasmas and optically opaque materials includes a point-like x-ray source for providing a broadband x-ray source. The x-rays are directed through a target material and then are reflected by a high-quality ellipsoidally-bent imaging crystal to a diffraction grating disposed at 1.times. magnification. A spherically-bent imaging crystal is employed when the x-rays that are incident on the crystal surface are normal to that surface. The diffraction grating produces multiple beams which interfere with one another to produce an interference pattern which contains information about the target. A detector is disposed at the position of the image of the target produced by the interfering beams.

Koch, Jeffrey A. (Livermore, CA)

2003-07-08T23:59:59.000Z

348

Static light scattering and small-angle neutron scattering study on aggregated recombinant gelatin in aqueous solution  

E-Print Network [OSTI]

Static Light Scattering and Small-Angle Neutron Scattering Study on Aggregated Recombinant Gelatin in Aqueous Solution A. Ramzi 1, M. Sutter 2, W.E. Hennink 1, W. Jiskoot 1,2 1 Department of Pharmaceutics, UIPS, Utrecht University, The Netherlands...-angle neutron scattering (SANS) for detecting aggregation of recombinant gelatin in aqueous solution and to obtain structural information about the aggregates. Recombinant Gelatin: RG-15-His 5.6Ser 25.2Pro 1.9Lys 3.7His 34.2Gly 15.5Gln 5.2Glu 11.8Asn 1.2Ala...

Sutter, Marc

2006-10-25T23:59:59.000Z

349

Small angle neutron scattering study of deuterated sodium dodecylsulfate micellization in dilute poly((2edimethylamino)ethyl methacrylate) solutions  

E-Print Network [OSTI]

Small angle neutron scattering study of deuterated sodium dodecylsulfate micellization in dilute 2010 Keywords: Poly((2edimethylamino)ethyl methacrylate) Micelle Small angle neutron scattering a b angle neutron scattering. We found three transitions of the poly ((2edimethylamino)ethyl methacrylate

Kofinas, Peter

350

Dynamic model of anisotropic x-ray refraction  

Science Journals Connector (OSTI)

General mechanisms of anisotropic x-ray refraction at the resonance energy are investigated on the basis of dynamic-scattering theory. The deductions show that x rays within the crystals that have anisotropic susceptibility are completely polarized and have two elliptical polarization states. Analytical expressions of the elliptical axes, refractive indices, and absorption coefficients for these two types of polarized waves are obtained in terms of the anisotropic components of the susceptibility tensor. Anisotropic birefringence and dichroism effects associated with the polarization properties of the x-ray waves are also illustrated theoretically.

X. R. Huang, Yong Li, W. J. Liu, and S. S. Jiang

1997-11-01T23:59:59.000Z

351

X-ray radiography for container inspection  

DOE Patents [OSTI]

Arrangements of X-ray inspection systems are described for inspecting high-z materials in voluminous objects such as containers. Inspection methods may involve generating a radiographic image based on detected attenuation corresponding to a pulsed beams of radiation transmitted through a voluminous object. The pulsed beams of radiation are generated by a high-energy source and transmitted substantially downward along an incident angle, of approximately 1.degree. to 30.degree., to a vertical axis extending through the voluminous object. The generated radiographic image may be analyzed to detect on localized high attenuation representative of high-z materials and to discriminate high-z materials from lower and intermediate-z materials on the basis of the high density and greater attenuation of high-z material for higher energy (3-10 MeV) X-rays, and the compact nature of threatening masses of fissionable materials.

Katz, Jonathan I. (Clayton, MO); Morris, Christopher L. (Los Alamos, NM)

2011-06-07T23:59:59.000Z

352

CHANDRA X-RAY OBSERVATIONS OF 12 MILLISECOND PULSARS IN THE GLOBULAR CLUSTER M28  

SciTech Connect (OSTI)

We present a Chandra X-ray Observatory investigation of the millisecond pulsars in the globular cluster M28 (NGC 6626). In what is one of the deepest X-ray observations of a globular cluster, we firmly detect seven and possibly detect two of the 12 known M28 pulsars. With the exception of PSRs B1821-24 and J1824-2452H, the detected pulsars have relatively soft spectra, with X-ray luminosities 10{sup 30}-10{sup 31} erg s{sup -1} (0.3-8 keV), similar to most 'recycled' pulsars in 47 Tucanae and the field of the Galaxy, implying thermal emission from the pulsar magnetic polar caps. We present the most detailed X-ray spectrum to date of the energetic PSR B1821-24. It is well described by a purely non-thermal spectrum with spectral photon index {Gamma} = 1.23 and luminosity 1.4 x 10{sup 33}{Theta}(D/5.5 kpc){sup 2} erg s{sup -1} (0.3-8 keV), where {Theta} is the fraction of the sky covered by the X-ray emission beam(s). We find no evidence for the previously reported line emission feature around 3.3 keV, most likely as a consequence of improvements in instrument calibration. The X-ray spectrum and pulse profile of PSR B1821-24 suggest that the bulk of unpulsed emission from this pulsar is not of thermal origin, and is likely due to low-level non-thermal magnetospheric radiation, an unresolved pulsar wind nebula, and/or small-angle scattering of the pulsed X-rays by interstellar dust grains. The peculiar binary PSR J1824-2452H shows a relatively hard X-ray spectrum and possible variability at the binary period, indicative of an intrabinary shock formed by interaction between the relativistic pulsar wind and matter from its non-degenerate companion star.

Bogdanov, Slavko [Department of Physics, McGill University, 3600 University Street, Montreal, QC H3A 2T8 (Canada); Van den Berg, Maureen; Servillat, Mathieu; Grindlay, Jonathan E. [Harvard-Smithsonian Center for Astrophysics, 60 Garden Street, Cambridge, MA 02138 (United States); Heinke, Craig O. [Department of Physics, University of Alberta, 11322 89 Avenue, Edmonton, AB T6G 2G7 (Canada); Stairs, Ingrid H.; Begin, Steve [Department of Physics, University of British Columbia, 6224 Agricultural Road Vancouver, BC V6T 1Z1 (Canada); Ransom, Scott M. [National Radio Astronomy Observatory, 520 Edgemont Road, Charlottesville, VA 22901 (United States); Freire, Paulo C. C. [Max-Planck-Institut fuer Radio Astronomie, Auf dem Huegel 69, D-53121 Bonn (Germany); Becker, Werner, E-mail: bogdanov@physics.mcgill.ca [Max-Planck-Institut fuer Extraterrestrische Physik, D-85740 Garching bei Muenchen (Germany)

2011-04-01T23:59:59.000Z

353

Small-angle scattering gives direct structural information about a membrane protein inside a lipid environment  

Science Journals Connector (OSTI)

A hybrid approach to the analysis of small-angle scattering data is presented, allowing determination of the orientation of bacteriorhodopsin reconstituted into a phopholipid nanodisc. The method is applicable to similar systems.

Kynde, S.A.R.

2014-01-29T23:59:59.000Z

354

Demonstration of a novel focusing small-angle neutron scattering instrument equipped with axisymmetric mirrors  

E-Print Network [OSTI]

Small-angle neutron scattering (SANS) is the most significant neutron technique in terms of impact on science and engineering. However, the basic design of SANS facilities has not changed since the techniques inception ...

Liu, Dazhi

355

Analysis of randomly oriented structures by grazing-incidence small-angle neutron scattering  

Science Journals Connector (OSTI)

A formalism is presented which allows the quantitative evaluation of grazing-incidence small-angle neutron scattering patterns from randomly oriented one-dimensional paracrystal domains with lamellar structure.

Korolkov, D.

2012-03-15T23:59:59.000Z

356

Small Angle Neutron Scattering Characterization of the Porous Structure of Carbons Prepared Using Inorganic Templates  

Science Journals Connector (OSTI)

Small angle neutron scattering (SANS) was used for the characterization of the microstructure of carbons derived from organic-loaded inorganic template materials that are used as anodes in lithium ion cells. Pillared clays (PILC), layered silicates whose ...

Giselle Sand; P. Thiyagarajan; Kathleen A. Carrado; Randall E. Winans

1999-01-20T23:59:59.000Z

357

The X-ray background and the evolution of AGN  

E-Print Network [OSTI]

We discuss the constraints on the AGN evolution from the cosmic X-ray background and source counts. A synthesis model to fit the X-ray background is presented. In the model, the spectrum of type 2 AGN has been modeled including Compton down--scattering within the absorbing material. Besides, we introduced a dependence on redshift of the relative number of obscured sources and found a decrease of the fraction of type 2 AGN at redshifts larger than 2.

Fulvio Pompilio; Fabio La Franca; Giorgio Matt

1999-09-23T23:59:59.000Z

358

Sapphire analyzers for high-resolution x-ray spectroscopy.  

SciTech Connect (OSTI)

We present a sapphire (Al{sub 2}O{sub 3}) analyzer for high-resolution X-ray spectroscopy with 31-meV energy resolution. The analyzer is designed for resonant inelastic X-ray scattering (RIXS) measurements at the CuK{sub a} absorption edge near 8990 eV. The performance of the analyzer is demonstrated by measuring phonon excitations in beryllium because of its known dynamical structure and high counting rates.

Yavas, H.; Alp, E.; Sinn, H.; Alatas, A.; Said, A.; Shvydko, Y.; Toellner, T.; Khachatryan, R.; Billinge, S.; Hasan, Z.; Sturhahn, W.; Michigan State Univ.; Princeton Univ.; DESY

2007-11-11T23:59:59.000Z

359

Development of a high-resolution soft x-ray (30--1500 eV) beamline at the Advanced Light Source and its use for the study of angle-resolved photoemission extended fine structure  

SciTech Connect (OSTI)

ALS Bending magnet beamline 9.3.2 is for high resolution spectroscopy, with circularly polarized light. Fixed included-angle SGM uses three gratings for 30--1500 eV photons; circular polarization is produced by an aperture for selecting the beam above or below the horizontal plane. Photocurrent from upper and lower jaws of entrance slit sets a piezoelectric drive feedback loop on the vertically deflecting mirror for stable beam. End station has a movable platform. With photomeission data from Stanford, structure of c(2{times}2)P/Fe(100) was determined using angle-resolved photoemission extended fine structure (ARPEFS). Multiple-scattering spherical-wave (MSSW) calculations indicate that P atoms adsorb in fourfold hollow sites 1.02A above the first Fe layer. Self-consistent-field X{alpha} scattered wave calculation confirm that the Fe{sub 1}-Fe{sub 2} space is contracted for S/Fe but not for P/Fe; comparison is made to atomic N and O on Fe(100). Final-state effects on ARPEFS curves used literature data from the S 1s and 2p core levels of c(2{times}2)S/Ni(001); a generalized Ramsauer-Townsend splitting is present in the 1s but not 2p data. An approximate method for analyzing ARPEFS data from a non-s initial state using only the higher-{ell} partial wave was tested successfully. ARPEFS data from clean surfaces were collected normal to Ni(111) (3p core levels) and 5{degree} off-normal from Cu(111)(3s, 3p). Fourier transforms (FT) resemble adsorbate systems, showing backscattering signals from atoms up to 4 layers below emitters. 3p FTs show scattering from 6 nearest neighbors in the same crystal layer as the emitters. MSSW calulation indicate that Cu 3p photoemission is mostly d-wave. FTs also indicate double-scattering and single-scattering from laterally distant atoms; calculations indicate that the signal is dominated by photoemission from the first 2 crystal layers.

Huff, W.R.A. [California Univ., Berkeley, CA (United States). Dept. of Chemistry]|[Lawrence Berkeley National Lab., CA (United States)

1996-02-01T23:59:59.000Z

360

Optics for X-Ray Laser and Laser Plasma Soft X-Ray Radiation  

Science Journals Connector (OSTI)

Focusing X-ray grazing incidence optics for X-ray laser and laser plasma soft X-ray radiation has been studied. ... computer code. Parabolic axisymmetric mirror for focusing Princeton X-ray laser beam and ellipso...

L. Pina; A. Inneman; R. Hudec

1996-01-01T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


361

Elastic Scattering of O16 on O18 Including Backward Angles  

Science Journals Connector (OSTI)

The elastic scattering of O16 on O18 has been measured for incident beam energies of Elab=24,28,and32 MeV at center-of-mass angles up to 150. The angular distributions exhibit pronounced oscillations at backward angles which may be interpreted as due to the occurrence of an elastic transfer.

C. K. Gelbke; R. Bock; P. Braun-Munzinger; D. Fick; K. D. Hildenbrand; A. Richter; W. Weiss

1972-12-18T23:59:59.000Z

362

Study, by neutron small angle scattering, of addition of an electrolyte to reversed micellar solution  

E-Print Network [OSTI]

L-455 Study, by neutron small angle scattering, of addition of an electrolyte to reversed micellar the size of reversed micelles of the ternary system Aerosol OT-n-heptane-water by small angle neutron, highly soluble in hydro- carbon substances, which may give reversed micelles in the presence of water

Paris-Sud XI, Université de

363

Small-Angle Scattering from Polymeric Mass Fractals of Arbitrary Mass-Fractal Dimension  

Science Journals Connector (OSTI)

A scattering function is obtained that describes mass-fractal scattering over a wide range of angle in terms of the radius of gyration, contrast factor and fractal dimension. Applications to organic polymer blends as well as low-density ceramics and organic materials are also discussed.

Beaucage, G.

1996-04-01T23:59:59.000Z

364

SMB, X-Ray Spectroscopy & Imaging  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Home X-Ray Spectroscopy & Imaging X-Ray Spectroscopy & Imaging SSRL has five hard X-ray Spectroscopy beamlines and three Microfocus Imaging beamlines dedicated to Biological and...

365

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Lensless X-Ray Imaging in Reflection Lensless X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has...

366

Miniature x-ray source  

DOE Patents [OSTI]

A miniature x-ray source utilizing a hot filament cathode. The source has a millimeter scale size and is capable of producing broad spectrum x-ray emission over a wide range of x-ray energies. The miniature source consists of a compact vacuum tube assembly containing the hot filament cathode, an anode, a high voltage feedthru for delivering high voltage to the cathode, a getter for maintaining high vacuum, a connector for initial vacuum pump down and crimp-off, and a high voltage connection for attaching a compact high voltage cable to the high voltage feedthru. At least a portion of the vacuum tube wall is fabricated from highly x-ray transparent materials, such as sapphire, diamond, or boron nitride.

Trebes, James E. (Livermore, CA); Bell, Perry M. (Tracy, CA); Robinson, Ronald B. (Modesto, CA)

2000-01-01T23:59:59.000Z

367

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking  

E-Print Network [OSTI]

X-ray Stacking 2008-Apr-22 Astrostats X-ray Stacking Tom Aldcroft SAO/CXC #12;X-ray Stacking 2008 analysis for a sample Stacking ­ mean properties of sample Chandra X-ray data (faint point sources) are photon-limited with low background => stacking in X-rays is very effective #12;X-ray Stacking 2008-Apr-22

Wolfe, Patrick J.

368

Refinement of the crystal structure of the high-temperature phase G0 in (NH4)2WO2F4 (powder, x-ray, and neutron scattering)  

SciTech Connect (OSTI)

The (NH4)2WO2F4 compound undergoes a series of phase transitions: G0 -> 201 K -> G1 -> 160 K -> G2, with a significant change in entropy ( S1 ~ Rln10 at the G0 -> G1 transition), which indicates significant orientational disordering in the G0 phase and the order disorder type of the phase transition. X-ray diffraction is used to identify the crystal structure of the G0 phase as rhombohedral (sp. gr. Cmcm, Z = 4), determine the lattice parameters and the positions of all atoms (except hydrogen), and show that [WO2F4]2 ions can form a superposition of dynamic and static orientational disorders in the anionic sublattice. A determination of the orientational position of [NH4]+ ions calls for the combined method of elastic and inelastic neutron scattering. Inelastic neutron scattering is used to determine the state of hindered rotation for ammonium ions in the G0 phase. Powder neutron diffraction shows that the orientational disorder of NH4 ions can adequately be described within the free rotation approximation.

Novak, D. M. [Joint Institute for Nuclear Research, Dubna, Russia; Smirnov, Lev S [Alikhanov Institute for Theoretical and Experimental Physics, Moscow, Russia; Kolesnikov, Alexander I [ORNL; Voronin, Vladimir [Institute of Metal Physics, Russia; Berger, I. F. [Institute of Metal Physics, Russia; Laptash, N. M. [Institute of Chemistry, Vladivostok, Russia; Vasil'ev, N. M. [Kirensky Institute of Physics, Krasnoyarsk, Russia; Flerov, I. N. [Kirensky Institute of Physics, Krasnoyarsk, Russia

2013-01-01T23:59:59.000Z

369

Refinement of the crystal structure of the high-temperature phase G{sub 0} in (NH{sub 4}){sub 2}WO{sub 2}F{sub 4} (powder, X-ray, and neutron scattering)  

SciTech Connect (OSTI)

The (NH{sub 4}){sub 2}WO{sub 2}F{sub 4} compound undergoes a series of phase transitions: G{sub 0} {yields} 201, K {yields} G{sub 1} {yields} 160, and K {yields} G{sub 2}, with a significant change in entropy ({Delta}S{sub 1} {approx} Rln10 at the G{sub 0} {yields} G{sub 1} transition), which indicates significant orientational disordering in the G{sub 0} phase and the order-disorder type of the phase transition. X-ray diffraction is used to identify the crystal structure of the G{sub 0} phase as rhombohedral (sp. gr. Cmcm, Z = 4), determine the lattice parameters and the positions of all atoms (except hydrogen), and show that [WO{sub 2}F{sub 4}]{sup 2-} ions can form a superposition of dynamic and static orientational disorders in the anionic sublattice. A determination of the orientational position of [NH{sub 4}]{sup +} ions calls for the combined method of elastic and inelastic neutron scattering. Inelastic neutron scattering is used to determine the state of hindered rotation for ammonium ions in the G{sub 0} phase. Powder neutron diffraction shows that the orientational disorder of NH{sub 4} ions can adequately be described within the free-rotation approximation.

Novak, D. M., E-mail: dmn@nf.jinr.ru; Smirnov, L. S. [Joint Institute for Nuclear Research, Frank Neutron Physics Laboratory (Russian Federation)] [Joint Institute for Nuclear Research, Frank Neutron Physics Laboratory (Russian Federation); Kolesnikov, A. I. [Oak Ridge National Laboratory, Neutron Scattering Sciences Division (United States)] [Oak Ridge National Laboratory, Neutron Scattering Sciences Division (United States); Voronin, V. I.; Berger, I. F. [Russian Academy of Sciences, Institute of Metal Physics, Ural Branch (Russian Federation)] [Russian Academy of Sciences, Institute of Metal Physics, Ural Branch (Russian Federation); Laptash, N. M. [Russian Academy of Sciences, Institute of Chemistry, Far Eastern Branch (Russian Federation)] [Russian Academy of Sciences, Institute of Chemistry, Far Eastern Branch (Russian Federation); Vasil'ev, A. D.; Flerov, I. N. [Russian Academy of Sciences, Kirensky Institute of Physics, Siberian Branch (Russian Federation)] [Russian Academy of Sciences, Kirensky Institute of Physics, Siberian Branch (Russian Federation)

2013-01-15T23:59:59.000Z

370

Resonant inelastic soft-x-ray scattering spectra at the N1s and C1s edges of poly(pyridine-2,5-diyl)  

E-Print Network [OSTI]

Resonant inelastic scattering measurements of poly(pyridine-2,5-diyl) have been performed at the N1s and C1s edges using synchrotron radiation. For comparison, molecular orbital calculations of the spectra have been carried out with the repeat unit as a model molecule of the polymer chain. The resonant emission spectra show depletion of the p electron bands which is consistent with symmetry selection and momentum conservation rules. The depletion is most obvious in the resonant inelastic scattering spectra of carbon while the nitrogen spectra are dominated by lone pair n orbital emission of s symmetry and are less excitation energy dependent. By comparing the measurements to calculations an isomeric dependence of the resonant spectra is found giving preference to two of the four possible isomers in the polymer.

Magnuson, M; Guo, J - H; Sthe, C; Agui, A; Nordgren, J; Luo, Y; gren, H; Johansson, N; Salaneck, W R; Horsburgh, L E; Monkman, A P; 10.1016/S0368-2048(98)00354-5

2012-01-01T23:59:59.000Z

371

Femtosecond Time-Delay X-ray Holography  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Time-Delay X-ray Holography Time-Delay X-ray Holography X-ray free-electron lasers (XFELs) will produce photon pulses with a unique and desirable combination of properties. Their short X-ray wavelengths allow penetration into materials and the ability to probe structure at and below the nanometer scale. Their ultra-short duration gives information about this structure at the fundamental time-scales of atoms and molecules. The extreme intensity of the pulses will allow this information to be acquired in a single shot, so that these studies can be carried out on non-repeatable processes or on weakly-scattering objects that will be modified by the pulse. A fourth property of XFEL pulses is their high transverse coherence, which brings the promise of decades of innovation in visible optics to the X-ray regime, such as holography, interferometry, and laser-based imaging. Making an effective use of XFEL pulses, however, will benefit from innovations that are new to both X-ray science and coherent optics. One such innovation is the new method of time-delay X-ray holography [i], recently demonstrated at the FLASH FEL at DESY in Hamburg, to measure the evolution of objects irradiated by intense pulses.

372

Center for X-Ray Optics, 1991  

SciTech Connect (OSTI)

This report discusses: Soft-X-Ray imaging with zone-plate lenses; multilayer reflective optics; and spectroscopy with x-rays.

Not Available

1992-03-01T23:59:59.000Z

373

SMB, X-ray Absorption Spectroscopy  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Absorption Spectroscopy X-ray Absorption Spectroscopy X-ray absorption spectroscopy (XAS) is a well-established technique for simultaneous local geometric and electronic structure...

374

Tokamak x ray diagnostic instrumentation  

SciTech Connect (OSTI)

Three classes of x-ray diagnostic instruments enable measurement of a variety of tokamak physics parameters from different features of the x-ray emission spectrum. (1) The soft x-ray (1 to 50 keV) pulse-height-analysis (PHA) diagnostic measures impurity concentrations from characteristic line intensities and the continuum enhancement, and measures the electron temperature from the continuum slope. (2) The Bragg x-ray crystal spectrometer (XCS) measures the ion temperature and neutral-beam-induced toroidal rotation velocity from the Doppler broadening and wavelength shift, respectively, of spectral lines of medium-Z impurity ions. Impurity charge state distributions, precise wavelengths, and inner-shell excitation and recombination rates can also be studied. X rays are diffracted and focused by a bent crystal onto a position-sensitive detector. The spectral resolving power E/..delta..E is greater than 10/sup 4/ and time resolution is 10 ms. (3) The x-ray imaging system (XIS) measures the spatial structure of rapid fluctuations (0.1 to 100 kHZ) providing information on MHD phenomena, impurity transport rates, toroidal rotation velocity, plasma position, and the electron temperature profile. It uses an array of silicon surface-barrier diodes which view different chords of the plasma through a common slot aperture and operate in current (as opposed to counting) mode. The effectiveness of shields to protect detectors from fusion-neutron radiation effects has been studied both theoretically and experimentally.

Hill, K.W.; Beiersdorfer, P.; Bitter, M.; Fredrickson, E.; Von Goeler, S.; Hsuan, H.; Johnson, L.C.; Liew, S.L.; McGuire, K.; Pare, V.

1987-01-01T23:59:59.000Z

375

Diffracted X-ray tracking for monitoring intramolecular motion in individual protein molecules using broad band X-ray  

SciTech Connect (OSTI)

Diffracted X-ray tracking (DXT) enables the tilting and twisting motions of single protein molecules to be monitored with micro- to milliradian resolution using a highly brilliant X-ray source with a wide energy bandwidth. We have developed a technique to monitor single molecules using gold nanocrystals attached to individual protein molecules using the BL28B2 beamline at SPring-8. In this paper we present the installation of a single toroidal X-ray mirror at BL28B2 to focus X-rays in an energy range of 1020 keV (?E/E = 82% for an X-ray with a wide energy bandwidth). With this beamline we tracked diffraction spots from gold nanocrystals over a wide angle range than that using quasi-monochromatic X-rays. Application of the wide angle DXT technique to biological systems enabled us to observe the on-site motions of single protein molecules that have been functionalized in vivo. We further extend the capability of DXT by observing the fractional tilting and twisting motions of inner proteins under various conditions. As a proof of this methodology and to determine instrumental performance the intramolecular motions of a human serum albumin complex with 2-anthracenecarboxylic acid was investigated using the BL28B2 beamline. The random tilting and twisting intramolecular motions are shown to be directly linked to the movement of individual protein molecules in the buffer solution.

Ichiyanagi, Kouhei; Sasaki, Yuji C. [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan) [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan); Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan); Sekiguchi, Hiroshi; Hoshino, Masato; Kajiwara, Kentaro; Senba, Yasunori; Ohashi, Haruhiko; Ohta, Noboru [Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)] [Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan); Hoshisashi, Kentaro; Jae-won, Chang; Tokue, Maki; Matsushita, Yufuku [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan)] [Department of Advanced Materials Science, Graduate School of Frontier Sciences, The University of Tokyo, 609 Kiban Building 5-1-5 Kashiwanoha, Kahiwashi, Chiba 277-8561 (Japan); Nishijima, Masaki; Inoue, Yoshihisa [Department of Applied Chemistry and Office for University-Industry Collaboration, Osaka University, 2-1 Yamadaoka, Suita, Osaka 565-0871 (Japan)] [Department of Applied Chemistry and Office for University-Industry Collaboration, Osaka University, 2-1 Yamadaoka, Suita, Osaka 565-0871 (Japan); Yagi, Naoto [Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan) [Japan Science and Technology Agency, CREST, CREST, Sasaki-Team, 609 Kiban Building, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8561 (Japan); Japan Synchrotron Radiation Research Institute, SPring-8, 1-1-1 Kouto, Sayo, Hyogo 679-5198 (Japan)

2013-10-15T23:59:59.000Z

376

The pore structure of the Argonne coals as interpreted from contrast matching small angle neutron scattering  

Science Journals Connector (OSTI)

Contrast matching small angle neutron scattering has been performed on a series of Argonne coals using H2O/D2O mixtures using short contact times between the coal and liquid. Calculations of the neutron scattering densities of the coals based on their formulae and helium densities are discussed. The results of the CM-SANS are given and it is shown that the scattering from the scattering from the non-contrast-matched samples is unreliable. It is shown that porosity in coals is effectively determined by the presence of water and that porosity levels decrease with increasing rank.

P.J. Hall; S.D. Brown; J.M. Calo

2000-01-01T23:59:59.000Z

377

Apparatus for the investigation of liquid systems in a shear gradient by small angle neutron scattering (SANS)  

E-Print Network [OSTI]

of small angle neutron scattering from fluids in a constant shear gradient. Typical systems which can angle neutron scattering experiments with liquids have given information about structural pro- perties759 Apparatus for the investigation of liquid systems in a shear gradient by small angle neutron

Boyer, Edmond

378

Salt-Dependent DNA Superhelix Diameter Studied by Small Angle Neutron Scattering Measurements and Monte Carlo Simulations  

E-Print Network [OSTI]

Salt-Dependent DNA Superhelix Diameter Studied by Small Angle Neutron Scattering Measurements-38042 Grenoble Cedex 9, France ABSTRACT Using small angle neutron scattering we have measured the static the same behavior between 10 and 100 mM salt concentration: An undulation in the scattering curve

Langowski, Jörg

379

X-ray Emission from Massive Stars  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore be related to the production of X-rays on massive stars. If so, massive stars' X-rays are much different than those found our own Sun and other cooler stars like the Sun that produce X-rays via magnetic activity

Cohen, David

380

X-ray Emission from Massive Stars  

E-Print Network [OSTI]

X-ray Emission from Massive Stars David Cohen Department of Physics and Astronomy Swarthmore #12;What is the mechanism by which massive stars produce x-rays? New results from the Chandra X-ray Observatory ­ high-resolution x-ray spectroscopy: measuring Doppler broadening in emission lines Testing

Cohen, David

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


381

From Nuclei to Micro-structure: investigating intermediate length scales by small angle laser light scattering  

E-Print Network [OSTI]

Hard spheres are a well recognized model system of statistical physics and soft condensed matter. Their crystallization behaviour has been intensively studied at the structural length scale by Bragg light scattering and/or high resolution microscopy. We here present an improved light scattering apparatus capable to perform simultaneous measurements in the Bragg scattering regime and in the small angle regime. We give an account of its construction and demonstrate its performance for several examples of hard sphere and attractive hard sphere suspensions. Comparison of small angle to Bragg data allows a calibration of the sequence of events in time. We show how important complementary information can be gained from the small angle studies e.g. on the immediate environment of the growing crystals or the global scale crystallite distribution. We further demonstrate that processes occurring on larger length scales have a significant influence on the crystallization kinetics and the final micro-structure.

Richard Beyer; Markus Franke; Hans Joachim Schpe; Eckhard Bartsch; Thomas Palberg

2014-12-02T23:59:59.000Z

382

CMOS Imaging Detectors as X-ray Detectors for Synchrotron Radiation Experiments  

SciTech Connect (OSTI)

CMOS imagers are matrix-addressed photodiode arrays, which have been utilized in devices such as commercially available digital cameras. The pixel size of CMOS imagers is usually larger than that of CCD and smaller than that of TFT, giving them a unique position. Although CMOS x-ray imaging devices have already become commercially available, they have not been used as an x-ray area detector in synchrotron radiation experiments. We tested performance of a CMOS detector from Rad-icon (Shad-o-Box1024) in medical imaging, small-angle scattering, and protein crystallography experiments. It has pixels of 0.048 mm square, read-out time of 0.45 sec, 12-bit ADC, and requires a frame grabber for image acquisition. The detection area is 5-cm square. It uses a Kodak Min-R scintillator screen as a phosphor. The sensitivity to x-rays with an energy less than 15 keV was low because of the thick window materials. Since the readout noise is high, the dynamic range is limited to 2000. The biggest advantages of this detector are cost-effectiveness (about 10,000 US dollars) and compactness (thickness < 3 cm, weight < 2 kg)

Yagi, Naoto; Uesugi, Kentaro; Inoue, Katsuaki [SPring-8/JASRI, Mikazuki, Sayo, Hyogo, 679-5198 (Japan); Yamamoto, Masaki [SPring-8/RIKEN, Mikazuki, Sayo, Hyogo, 679-5198 (Japan)

2004-05-12T23:59:59.000Z

383

The new very small angle neutron scattering spectrometer at Laboratoire Leon Brillouin  

E-Print Network [OSTI]

The design and characteristics of the new very small angle neutron scattering spectrometer under construction at the Laboratoire Leon Brillouin is described. Its goal is to extend the range of scattering vectors magnitudes towards 2x10{-4} /A. The unique feature of this new spectrometer is a high resolution two dimensional image plate detector sensitive to neutrons. The wavelength selection is achieved by a double reflection supermirror monochromator and the collimator uses a novel multibeam design.

Sylvain Desert; Vincent Thevenot; Julian Oberdisse; Annie Brulet

2007-06-12T23:59:59.000Z

384

Effect of the concentration of inhomogeneities on the multiple small-angle neutron scattering  

SciTech Connect (OSTI)

The interference effects manifested during multiple small-angle neutron scattering (MSANS) on a chaotically arranged close-packed ensemble of scatterers have been studied. MSANS measurements have been performed for mixtures of Al and Ti-Zr alloy powders. It is shown that the results can be satisfactorily described based on a theory that takes into account spatial correlations in the arrangement of powder grains.

Abov, Yu. G.; Dzheparov, F. S.; Elyutin, N. O.; Lvov, D. V., E-mail: lvov@itep.ru; Tyulyusov, A. N. [Institute for Theoretical and Experimental Physics (Russian Federation)] [Institute for Theoretical and Experimental Physics (Russian Federation)

2013-03-15T23:59:59.000Z

385

Compact x-ray source and panel  

DOE Patents [OSTI]

A compact, self-contained x-ray source, and a compact x-ray source panel having a plurality of such x-ray sources arranged in a preferably broad-area pixelized array. Each x-ray source includes an electron source for producing an electron beam, an x-ray conversion target, and a multilayer insulator separating the electron source and the x-ray conversion target from each other. The multi-layer insulator preferably has a cylindrical configuration with a plurality of alternating insulator and conductor layers surrounding an acceleration channel leading from the electron source to the x-ray conversion target. A power source is connected to each x-ray source of the array to produce an accelerating gradient between the electron source and x-ray conversion target in any one or more of the x-ray sources independent of other x-ray sources in the array, so as to accelerate an electron beam towards the x-ray conversion target. The multilayer insulator enables relatively short separation distances between the electron source and the x-ray conversion target so that a thin panel is possible for compactness. This is due to the ability of the plurality of alternating insulator and conductor layers of the multilayer insulators to resist surface flashover when sufficiently high acceleration energies necessary for x-ray generation are supplied by the power source to the x-ray sources.

Sampayon, Stephen E. (Manteca, CA)

2008-02-12T23:59:59.000Z

386

Theory of angular dispersive imaging hard x-ray spectrographs  

E-Print Network [OSTI]

A spectrograph is an optical instrument that disperses photons of different energies into distinct directions and space locations, and images photon spectra on a position-sensitive detector. Spectrographs consist of collimating, angular dispersive, and focusing optical elements. Bragg reflecting crystals arranged in an asymmetric scattering geometry are used as the dispersing elements. A ray-transfer matrix technique is applied to propagate x-rays through the optical elements. Several optical designs of hard x-ray spectrographs are proposed and their performance is analyzed. Spectrographs with an energy resolution of 0.1 meV and a spectral window of imaging up to a few tens of meVs are shown to be feasible for inelastic x-ray scattering (IXS) spectroscopy applications. In another example, a spectrograph with a 1-meV spectral resolution and 85-meV spectral window of imaging is considered for Cu K-edge resonant IXS (RIXS).

Shvyd'ko, Yuri

2015-01-01T23:59:59.000Z

387

Ultrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS)  

E-Print Network [OSTI]

: ultrafast x-rays, x-ray absorption spectroscopy, terawatt lasers, ultrafast reaction dynamics, atomic motion atomic motion by scrutinizing the changes in x- ray absorption spectra during reactions. FirstUltrafast X-ray Absorption Spectroscopy using Laser-Driven Electron X-ray Sources (LEXS) Guangjun

Guo, Ting

388

Small-Angle Neutron Scattering Studies of the Conformation of Myeloma Protein MOPC315 and its Fab Fragment, and the Interaction with a Monovalent Dinitrophenyl Hapten  

Science Journals Connector (OSTI)

...research-article Small-Angle Neutron Scattering Studies of the Conformation...fixation. Small-angle neutron scattering studies of the conformation...Fragments Myeloma Proteins Neutrons Protein Conformation Scattering, Radiation The Royal Society...

1981-01-01T23:59:59.000Z

389

Focused X-ray source  

DOE Patents [OSTI]

Disclosed is an intense, relatively inexpensive X-ray source (as compared to a synchrotron emitter) for technological, scientific, and spectroscopic purposes. A conical radiation pattern produced by a single foil or stack of foils is focused by optics to increase the intensity of the radiation at a distance from the conical radiator. 8 figs.

Piestrup, M.A.; Boyers, D.G.; Pincus, C.I.; Maccagno, P.

1990-08-21T23:59:59.000Z

390

Short-Range Order and Collective Dynamics of DMPC Bilayers: A Comparison between Molecular Dynamics Simulations, X-Ray,  

E-Print Network [OSTI]

Simulations, X-Ray, and Neutron Scattering Experiments Jochen S. Hub,* Tim Salditt,y Maikel C. Rheinsta derived by molecular dynamics simulations, elastic x-ray, and inelastic neutron scattering experiments dynamics obtained from the simulations and from inelastic neutron scattering are analyzed and compared

de Groot, Bert

391

A modified Ising model for the thermodynamic properties of local and global protein folding-unfolding observed by circular dichroism and small-angle X-ray scattering  

Science Journals Connector (OSTI)

The application of a modified Ising model for the thermodynamic properties of local and global protein folding-unfolding is described.

Shiu, Y.-J.

2007-02-17T23:59:59.000Z

392

Small-Angle X-ray Scattering from Blends of PE and SBS. Observation of a Novel Kind of Deviation from Porod's Law  

Science Journals Connector (OSTI)

In the SAXS of modified poly(ethylene) (blends) a peculiar and reproducible deviation from Porod's law is found. The strength of this effect is a function of blend composition.

Stribeck, N.

1997-10-01T23:59:59.000Z

393

Small-Angle X-Ray Scattering- and Nuclear Magnetic Resonance-Derived Conformational Ensemble of the Highly Flexible Antitoxin PaaA2  

Science Journals Connector (OSTI)

Summary Antitoxins from prokaryotic type II toxin-antitoxin modules are characterized by a high degree of intrinsic disorder. The description of such highly flexible proteins is challenging because they cannot be represented by a single structure. Here, we present a combination of SAXS and NMR data to describe the conformational ensemble of the PaaA2 antitoxin from the human pathogen E.coli O157. The method encompasses the use of SAXS data to filter ensembles out of a pool of conformers generated by a custom NMR structure calculation protocol and the subsequent refinement by a block jackknife procedure. The final ensemble obtained through the method is validated by an established residual dipolar coupling analysis. We show that the conformational ensemble of PaaA2 is highly compact and that the protein exists in solution as two preformed helices, connected by a flexible linker, that probably act as molecular recognition elements for toxin inhibition.

YannG.J. Sterckx; AlexanderN. Volkov; WimF. Vranken; Jaka Kragelj; MaleneRingkjbing Jensen; Lieven Buts; Abel Garcia-Pino; Thomas Jov; Laurence VanMelderen; Martin Blackledge; NicoA.J. vanNuland; Remy Loris

2014-01-01T23:59:59.000Z

394

Domain mobility as probed by small-angle X-ray scattering may account for substrate access to the active site of two copper-dependent amine oxidases  

Science Journals Connector (OSTI)

SAXS analysis suggests that in solution CAOs homodimers could undergo a conformational change. The D3 domain seems to move with respect to the rest of the protein, increasing the accessibility of the active site.

Dainese, E.

2014-07-25T23:59:59.000Z

395

Studies of structure and dynamics of biological macro-molecular assemblies by low angle neutron diffraction and inelastic X-ray scattering  

E-Print Network [OSTI]

This thesis is organized into two parts which focus on the studies of the dynamic structure factor and static inter-particle structure factor respectively. In the first part, we have measured and analyzed the dynamic ...

Liu, Yun, 1973-

2005-01-01T23:59:59.000Z

396

Structured water in polyelectrolyte dendrimers: Understanding small angle neutron scattering results through atomistic simulation  

SciTech Connect (OSTI)

Based on atomistic molecular dynamics (MD) simulations, the small angle neutron scattering (SANS) intensity behavior of a single generation-4 (G4) polyelectrolyte polyamidoamine (PAMAM) starburst dendrimer is investigated at different levels of molecular protonation. The SANS form factor, P(Q), and Debye autocorrelation function, (r), are calculated from the equilibrium MD trajectory based on a mathematical approach proposed in this work which provides a link between the neutron scattering experiment and MD computation. The simulations enable scattering calculations of not only the hydrocarbons, but also the contribution to the scattering length density fluctuations caused by structured, confined water within the dendrimer. Based on our computational results, we question the validity of using radius of gyration RG for microstructure characterization of a polyelectrolyte dendrimer from the scattering perspective.

Chen, Wei-Ren [ORNL; Do, Changwoo [ORNL; Hong, Kunlun [ORNL; Liu, Emily [Rensselaer Polytechnic Institute (RPI); Liu, Yun [National Institute of Standards and Technology (NIST); Porcar, L. [National Institute of Standards and Technology (NIST); Smith, Gregory Scott [ORNL; Wu, Bin [ORNL; Egami, T [University of Tennessee, Knoxville (UTK); Smith, Sean C [ORNL

2012-01-01T23:59:59.000Z

397

A focusing-geometry small-angle neutron scattering instrument with a magnetic neutron lens  

Science Journals Connector (OSTI)

A focusing-geometry small-angle neutron scattering (FSANS) instrument with a magnetic neutron lens based on an extended Halbach-type sextupole magnet has been constructed and tested. A minimum value of the measurable range, , of ?-1 could be achieved by the FSANS instrument using a neutron wavelength ? with for the full width at half maximum.

Oku, T.

2007-02-23T23:59:59.000Z

398

Light propagation in tissues with forward-peaked and large-angle scattering  

E-Print Network [OSTI]

-angle scattering makes it difficult to solve the radiative transport equation, we present a method to construct to inhomogene- ities. The radiative transport equation is a partial differential-integral equation. Analytical of the sev- eral independent variables in the radiative transport equation. Biological tissues tend

Kim, Arnold D.

399

The use of multiple-scattering data to enhance small-angle neutron scattering experiments  

Science Journals Connector (OSTI)

It is shown that SANS patterns from specimens of different thicknesses but otherwise identical not only provide information on the shape and size of the scattering entity but also give absolute values of the scattering contrast between particles responsible for SANS and the matrix. No separate calibration of the incident beam is required.

Sabine, T.M.

1999-05-01T23:59:59.000Z

400

EQ-SANS: the Extended Q-Range Small-Angle Neutron Scattering Diffractometer  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

The Extended Q-Range Small-Angle Neutron Scattering Diffractometer at SNS The Extended Q-Range Small-Angle Neutron Scattering Diffractometer at SNS Extended Q-Range Small Angle Diffractometer EQ-SANS detector array The EQ-SANS Diffractometer is designed to study non-crystalline, nano-sized materials in solid, liquid, or gas forms such as polymers, micelles, proteins, and other large biological molecular complexes in solution. It offers high neutron flux, high wavelength resolution (precision), and wide Q-coverage. EQSANS is located on beam line 6, viewing the top-downstream, coupled supercritical hydrogen moderator. It has a curved multichannel beam bender to avoid the direct line of sight of the moderator, which cleans out the background from the prompt neutron pulse quite effectively. The cutoff wavelength of the optics is ~1.5 Å. Above this minimum wavelength, the

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


401

Measurements of the hard-x-ray reflectivity of iridium  

SciTech Connect (OSTI)

In connection with the design of a hard-x-ray telescope for the Constellation X-Ray Observatory we measured the reflectivity of an iridium-coated zerodur substrate as a function of angle at 55, 60, 70, and 80 keV at the National Synchrotron Light Source of Brookhaven National Laboratory. The optical constants were derived from the reflectivity data. The real component of the index of refraction is in excellent agreement with theoretical values at all four energies. However, the imaginary component, which is related to the mass attenuation coefficient, is 50% to 70% larger at 55, 60, and 70 keV than theoretical values.

Romaine, S.; Bruni, R.; Gorenstein, P.; Zhong, Z

2007-01-10T23:59:59.000Z

402

RYLLA. [X-ray transport code  

SciTech Connect (OSTI)

This paper describes a computer code, RYLLA, which models the deposition of x-rays into thin metal slabs, and transports the resulting photoelectrons, finding the distribution of electrons leaving the slab from both the front and back surfaces. The slab must be homogeneous, but can contain a mixture of up to 5 different elements. Due to the short electron mean free path at low electron energies, RYLLA should be used only for studying thin slabs, roughly < 100 mg/cm/sup 2/ for low Z metals, and < 10 mg/cm/sup 2/ for high Z metals. X-ray energies should be in the range of 1 to 150 keV, as they are deposited only via photoionization and Compton scattering processes. Following photoionization, a hole exists in the electron cloud of the absorbing atom. This fills either by Auger or fluoresence, resulting in lower energy holes which are also filled. Fluoresence photons are transported and absorbed in the same manner as the primary photons, except that they are isotropically produced. Once all photons have been transported and absorbed, and all holes have been filled, a space- and energy-dependent electron source spectrum has been obtained. This is used in a discrete ordinate expansion solution of the 1-D transport equation, which gives the output electron spectra at the two slab surfaces. This paper discusses both the physics and coding of RYLLA. Examples of user input are given, as are some comparisons with other codes.

Hyde, R.A.

1983-06-08T23:59:59.000Z

403

In Situ X-ray Study of the Solid Electrolyte Interphase (SEI) Formation on Graphene as a Model Li-ion Battery Anode  

Science Journals Connector (OSTI)

In Situ X-ray Study of the Solid Electrolyte Interphase (SEI) Formation on Graphene as a Model Li-ion Battery Anode ... Li-ion batteries; solid electrolyte interphase; graphene; graphite; X-ray scattering ...

Sudeshna Chattopadhyay; Albert L. Lipson; Hunter J. Karmel; Jonathan D. Emery; Timothy T. Fister; Paul A. Fenter; Mark C. Hersam; Michael J. Bedzyk

2012-07-23T23:59:59.000Z

404

Microgap x-ray detector  

DOE Patents [OSTI]

An x-ray detector which provides for the conversion of x-ray photons into photoelectrons and subsequent amplification of these photoelectrons through the generation of electron avalanches in a thin gas-filled region subject to a high electric potential. The detector comprises a cathode (photocathode) and an anode separated by the thin, gas-filled region. The cathode may comprise a substrate, such a beryllium, coated with a layer of high atomic number material, such as gold, while the anode can be a single conducting plane of material, such as gold, or a plane of resistive material, such as chromium/silicon monoxide, or multiple areas of conductive or resistive material, mounted on a substrate composed of glass, plastic or ceramic. The charge collected from each electron avalanche by the anode is passed through processing electronics to a point of use, such as an oscilloscope.

Wuest, Craig R. (Danville, CA); Bionta, Richard M. (Livermore, CA); Ables, Elden (Livermore, CA)

1994-01-01T23:59:59.000Z

405

Chest x-Rays | Department of Energy  

Broader source: Energy.gov (indexed) [DOE]

Chest x-Rays Chest x-Rays Chest x-Rays Chest X-ray B-Reading The B-reading is a special reading of a standard chest x-ray film performed by a physician certified by the National Institute for Occupational Safety and Health (NIOSH). The reading looks for changes on the chest x-ray that may indicate exposure and disease caused by agents such as asbestos or silica. The B-reading is considered a special reading because doctors who are certified by NIOSH to perform B-readings use a specific protocol to read and record the findings as developed by the International Labour Organization (ILO). The ILO's protocol provides rules for systematically examining the x-ray in a step-by-step method and recording certain abnormalities or changes on the chest x-ray that can be attributable to

406

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities in the field of lensless imaging. XFELs...

407

Lensless X-Ray Imaging in Reflection  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Imaging in Reflection Print Wednesday, 26 October 2011 00:00 The advent of x-ray free-electron laser (XFEL) light sources has led to an outburst of research activities...

408

Producing X-rays at the APS  

ScienceCinema (OSTI)

An introduction and overview of the Advanced Photon Source at Argonne National Laboratory, the technology that produces the brightest X-ray beams in the Western Hemisphere, and the research carried out by scientists using those X-rays.

None

2013-04-19T23:59:59.000Z

409

SMB, X-ray Fluorescence Imaging  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Fluorescence Imaging X-ray Fluorescence Imaging X-ray fluorescence imaging utilizes the high brightness of SPEAR3 and focused beam generated by the uses of K-B optics, capillaries...

410

Synchrotron radiation sources and condensers for projection x-ray lithography  

SciTech Connect (OSTI)

The design requirements for a compact electron storage ring that could be used as a soft x-ray source for projection lithography are discussed. The design concepts of the x-ray optics that are required to collect and condition the radiation in divergence, uniformity and direction to properly illuminate the mask and the particular x-ray projection camera used are discussed. Preliminary designs for an entire soft x-ray projection lithography system using an electron storage ring as a soft X-ray source are presented. It is shown that by combining the existing technology of storage rings with large collection angle condensers, a powerful and reliable source of 130[Angstrom] photons for production line projection x-ray lithography is possible.

Murphy, J.B.; MacDowell, A.A. (Brookhaven National Lab., Upton, NY (United States)); White, D.L. (AT and T Bell Labs., Murray Hill, NJ (United States)); Wood, O.R. II (AT and T Bell Labs., Holmdel, NJ (United States))

1992-01-01T23:59:59.000Z

411

Synchrotron radiation sources and condensers for projection x-ray lithography  

SciTech Connect (OSTI)

The design requirements for a compact electron storage ring that could be used as a soft x-ray source for projection lithography are discussed. The design concepts of the x-ray optics that are required to collect and condition the radiation in divergence, uniformity and direction to properly illuminate the mask and the particular x-ray projection camera used are discussed. Preliminary designs for an entire soft x-ray projection lithography system using an electron storage ring as a soft X-ray source are presented. It is shown that by combining the existing technology of storage rings with large collection angle condensers, a powerful and reliable source of 130{Angstrom} photons for production line projection x-ray lithography is possible.

Murphy, J.B.; MacDowell, A.A. [Brookhaven National Lab., Upton, NY (United States); White, D.L. [AT and T Bell Labs., Murray Hill, NJ (United States); Wood, O.R. II [AT and T Bell Labs., Holmdel, NJ (United States)

1992-11-01T23:59:59.000Z

412

Portable X-Ray, K-Edge Heavy Metal Detector  

SciTech Connect (OSTI)

The X-Ray, K-Edge Heavy Metal Detection System was designed and built by Ames Laboratory and the Center for Nondestructive Evaluation at Iowa State University. The system uses a C-frame inspection head with an X-ray tube mounted on one side of the frame and an imaging unit and a high purity germanium detector on the other side. the inspection head is portable and can be easily positioned around ventilation ducts and pipes up to 36 inches in diameter. Wide angle and narrow beam X-ray shots are used to identify the type of holdup material and the amount of the contaminant. Precise assay data can be obtained within minutes of the interrogation. A profile of the containerized holdup material and a permanent record of the measurement are immediately available.

Fricke, V.

1999-10-25T23:59:59.000Z

413

The impact of accretion disk winds on the X-ray spectrum of AGN: Part 2 - XSCORT + Hydrodynamic Simulations  

E-Print Network [OSTI]

abridged: We use XSCORT, together with the hydrodynamic accretion disc wind simulation from Proga & Kallman (2004), to calculate the impact that the accretion disk wind has on the X-ray spectrum from a 1E8 solar mass black hole Active Galactic Nuclei (AGN) accreting at 0.5 L/L_Edd. The properties of the resulting spectra depend on viewing angle and clearly reflect the distinct regions apparent in the original hydrodynamic simulation. Very equatorial lines-of-sight (l.o.s) are dominated by Compton scattering and nearly-neutral absorption. Polar l.o.s result in largely featureless spectra. Finally, l.o.s that intersect the transition region between these extremes have a wide range of absorption features imprinted on the spectrum. Both polar and transition region l.o.s produce spectra that show highly-ionized, blue-shifted, Fe absorption features that are qualitatively similar to features observed in the X-ray spectra of a growing number of AGN. The spectra presented here clearly demonstrate that current simulations of line driven AGN accretion disk winds cannot reproduce the smooth soft X-ray excess. Furthermore, they predict that high accretion rate (L/L_Edd) AGN are likely to be strongly affected by obscuration, in sharp contrast to the clean picture that is generally assumed, based on the observed relation between the opening angle of the molecular torus and AGN luminosity.

N. J. Schurch; C. Done; D. Proga

2008-10-06T23:59:59.000Z

414

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St in hot gas about 250 million light years from Earth. (Credit: X-ray: NASA/CXC/SAO/E.Bulbul, et al-Newton has revealed a mysterious X-ray signal in the data. This signal is represented in the circled data

415

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network [OSTI]

2/9/07 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 9, 07] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

416

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St million light years from Earth. (Credit: X-ray: NASA/CXC/Wesleyan Univ./R.Kilgard, et al; Optical: NASA with optical data from the Hubble Space Telescope (red, green, and blue). The X-ray data reveal hundreds

417

X-ray Spectroscopy of Cool Stars  

E-Print Network [OSTI]

High-resolution X-ray spectroscopy has addressed not only various topics in coronal physics of stars, but has also uncovered important features relevant for our understanding of stellar evolution and the stellar environment. I summarize recent progress in coronal X-ray spectroscopy and in particular also discuss new results from studies of X-rays from pre-main sequence stars.

M. Guedel

2006-09-11T23:59:59.000Z

418

X-Ray Physics Evan Berkowitz  

E-Print Network [OSTI]

X-Ray Physics Evan Berkowitz Junior, MIT Department of Physics (Dated: October 25, 2006) We measure a variety of phenomena related to X-Ray absorption and production. We present data which conforms within, as are 22 Na electron-positron annhilation lines. The importance of understanding x-rays is demonstrated

419

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St 200 million light years from Earth. (Credit: X-ray: NASA/CXC/UAH/M.Sun et al; Optical: NASA, ESA, & the Hubble Heritage Team (STScI/AURA) Caption: This composite image from the Chandra X-ray Observatory (blue

420

X-Ray Absorption Spectroscopy of Metallobiomolecules  

E-Print Network [OSTI]

9/6/09 1 X-Ray Absorption Spectroscopy of Metallobiomolecules The Outskirts of Structural Biology 6, 09] This is a tutorial about the use of X-ray Absorption Spectroscopy (XAS) in biology, RG; Eisenberger, P; Kincaid, BM "X-ray Absorption Spectroscopy of Biological Molecules" Annu. Rev

Scott, Robert A.

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


421

Chandra X-ray Observatory Center  

E-Print Network [OSTI]

Chandra X-ray Observatory Center Harvard-Smithsonian Center for Astrophysics 60 Garden St. Cambridge, MA 02138 USA http://chandra.harvard.edu Four Supernova Remnants: NASA's Chandra X-ray Observatory's Chandra X-ray Observatory, four newly processed images of supernova remnants dramatically illustrate

422

Small-angle neutron scattering analysis of a water-based magnetic fluid with charge stabilization: contrast variation and scattering of polarized neutrons  

Science Journals Connector (OSTI)

The nuclear and magnetic scattering contributions in small-angle scattering experiments on a diluted water-based magnetic fluid are separated by the contrast variation technique and scattering of polarized neutrons. The significant difference found in the nuclear and magnetic apparent particle sizes is related to different nuclear and magnetic correlation lengths in the system.

Avdeev, M.V.

2009-10-30T23:59:59.000Z

423

Small Angle Polarization in High Energy P--P Scattering Through Nonperturbative Chiral Symmetry Breaking  

E-Print Network [OSTI]

We show that a large anomalous contribution due to nonperturbative instanton-like gluonic field configurations to the axial charge of the proton implies high-energy spin effects in $p-p$ elastic scattering. This is the same mechanism which is responsible for anomalous baryon number violation at high energy in the standard model. We compute the proton polarization due to these effects and we show that it is proportional to the center-of-mass scattering angle with a universal (energy-independent) slope of order unity.

Mauro Anselmino; Stefano Forte

1992-11-06T23:59:59.000Z

424

Neutron reflectivity and small angle neutron scattering: An introduction and perspective on recent progress  

Science Journals Connector (OSTI)

Abstract In recent years both neutron reflectivity, NR, and small angle neutron scattering, SANS, have been applied to the study of increasingly complex surface and interfacial properties. The methodology and advantages of using these neutron scattering techniques to probe surfaces and interfaces will be briefly outlined. Some recent examples of surfactant, polymer and polymersurfactant adsorption at the airwater, liquidsolid, and liquidliquid planar interfaces are highlighted. These are contrasted by some examples of the nature of adsorption on colloidal sol particles and emulsion droplets.

Jeffrey Penfold; Robert K. Thomas

2014-01-01T23:59:59.000Z

425

Using Light to Control How X Rays Interact with Matter  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

ultrafast x-ray spectroscopy. ALS femtosecond spectroscopy beamline layout. Femtosecond x-ray and laser pulses derive from a single 800-nm laser oscillator. Femtosecond x rays...

426

Fabrication and performance of blazed transmission gratings for x-ray astronomy  

E-Print Network [OSTI]

We have developed a new type of soft x-ray diffraction grating. This critical-angle transmission (CAT) grating combines the advantages of traditional transmission gratings (low mass, extremely relaxed alignment and flatness ...

Schattenburg, Mark Lee

427

X-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336342  

E-Print Network [OSTI]

X-RAY SPECTROMETRY X-Ray Spectrom. 2007; 36: 336­342 Published online in Wiley InterScience (www.interscience.wiley.com) DOI: 10.1002/xrs.980 Fish otolith trace element maps: new approaches with synchrotron microbeam x-ray of elements as they accrete through a fish's life. We apply synchrotron microbeam x-ray fluorescence methods

Limburg, Karin E.

428

X-ray Pulsations in the Supersoft X-ray Binary CAL 83  

E-Print Network [OSTI]

X-ray data reveal that the supersoft X-ray binary CAL 83 exhibits 38.4 minute pulsations at some epochs. These X-ray variations are similar to those found in some novae and are likely to be caused by nonradial pulsations the white dwarf. This is the first detection of pulsations in a classical supersoft X-ray binary.

P. C. Schmidtke; A. P. Cowley

2005-09-28T23:59:59.000Z

429

X-ray Spectroscopy of Cooling Cluster  

SciTech Connect (OSTI)

We review the X-ray spectra of the cores of clusters of galaxies. Recent high resolution X-ray spectroscopic observations have demonstrated a severe deficit of emission at the lowest X-ray temperatures as compared to that expected from simple radiative cooling models. The same observations have provided compelling evidence that the gas in the cores is cooling below half the maximum temperature. We review these results, discuss physical models of cooling clusters, and describe the X-ray instrumentation and analysis techniques used to make these observations. We discuss several viable mechanisms designed to cancel or distort the expected process of X-ray cluster cooling.

Peterson, J.R.; /SLAC; Fabian, A.C.; /Cambridge U., Inst. of Astron.

2006-01-17T23:59:59.000Z

430

X-ray transmissive debris shield  

DOE Patents [OSTI]

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, R.B.

1996-05-21T23:59:59.000Z

431

X-ray Spectroscopy of Cooling Clusters  

E-Print Network [OSTI]

We review the X-ray spectra of the cores of clusters of galaxies. Recent high resolution X-ray spectroscopic observations have demonstrated a severe deficit of emission at the lowest X-ray temperatures as compared to that expected from simple radiative cooling models. The same observations have provided compelling evidence that the gas in the cores is cooling below half the maximum temperature. We review these results, discuss physical models of cooling clusters, and describe the X-ray instrumentation and analysis techniques used to make these observations. We discuss several viable mechanisms designed to cancel or distort the expected process of X-ray cluster cooling.

J. R. Peterson; A. C. Fabian

2005-12-21T23:59:59.000Z

432

X-ray transmissive debris shield  

DOE Patents [OSTI]

An X-ray debris shield for use in X-ray lithography that is comprised of an X-ray window having a layer of low density foam exhibits increased longevity without a substantial increase in exposure time. The low density foam layer serves to absorb the debris emitted from the X-ray source and attenuate the shock to the window so as to reduce the chance of breakage. Because the foam is low density, the X-rays are hardly attenuated by the foam and thus the exposure time is not substantially increased.

Spielman, Rick B. (Albuquerque, NM)

1996-01-01T23:59:59.000Z

433

X-ray lithography using holographic images  

DOE Patents [OSTI]

A non-contact X-ray projection lithography method for producing a desired X-ray image on a selected surface of an X-ray-sensitive material, such as photoresist material on a wafer, the desired X-ray image having image minimum linewidths as small as 0.063 .mu.m, or even smaller. A hologram and its position are determined that will produce the desired image on the selected surface when the hologram is irradiated with X-rays from a suitably monochromatic X-ray source of a selected wavelength .lambda.. On-axis X-ray transmission through, or off-axis X-ray reflection from, a hologram may be used here, with very different requirements for monochromaticity, flux and brightness of the X-ray source. For reasonable penetration of photoresist materials by X-rays produced by the X-ray source, the wavelength X, is preferably chosen to be no more than 13.5 nm in one embodiment and more preferably is chosen in the range 1-5 nm in the other embodiment. A lower limit on linewidth is set by the linewidth of available microstructure writing devices, such as an electron beam.

Howells, Malcolm R. (Berkeley, CA); Jacobsen, Chris (Sound Beach, NY)

1995-01-01T23:59:59.000Z

434

The General-Purpose Small-Angle Neutron Scattering Diffractometer at HFIR -  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

General-Purpose Small-Angle Neutron Scattering Diffractometer at HFIR General-Purpose Small-Angle Neutron Scattering Diffractometer at HFIR Instrument scientist Ken Littrell at GP-SANS. Instrument scientist Ken Littrell at GP-SANS. The General-Purpose Small-Angle Neutron Scattering Diffractometer (GP-SANS) instrument is optimized for providing information about structure and interactions in materials in the size range of 0.5 - 200 nm. It has a cold neutron flux on sample and capabilities comparable to those of the best SANS instruments worldwide, including a wide range of neutron wavelengths λ 5 - 30 Å, resolution Δλ ⁄ λ 9=45%, and a 1m2 area detector with 5 × 5mm2 pixel resolution with a maximum counting capability of up to 2.5 kHz. The sample-to-detector distance can be varied from 1 to 20 m, and the detector can be offset horizontally by up to 45 cm, allowing

435

Note: Application of a pixel-array area detector to simultaneous single crystal x-ray diffraction and x-ray absorption spectroscopy measurements  

SciTech Connect (OSTI)

X-ray diffraction (XRD) and X-ray absorption spectroscopy (XAS) are two main x-ray techniques in synchrotron radiation facilities. In this Note, we present an experimental setup capable of performing simultaneous XRD and XAS measurements by the application of a pixel-array area detector. For XRD, the momentum transfer in specular diffraction was measured by scanning the X-ray energy with fixed incoming and outgoing x-ray angles. By selecting a small fixed region of the detector to collect the XRD signal, the rest of the area was available for collecting the x-ray fluorescence for XAS measurements. The simultaneous measurement of XRD and X-ray absorption near edge structure for Pr{sub 0.67}Sr{sub 0.33}MnO{sub 3} film was demonstrated as a proof of principle for future time-resolved pump-probe measurements. A static sample makes it easy to maintain an accurate overlap of the X-ray spot and laser pump beam.

Sun, Cheng-Jun, E-mail: cjsun@aps.anl.gov; Brewe, Dale L.; Heald, Steve M. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)] [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Zhang, Bangmin [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States) [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States); Department of Materials Science and Engineering, National University of Singapore, 117575 Singapore (Singapore); NUSNNI-Nanocore, National University of Singapore, 117411 Singapore (Singapore); Chen, Jing-Sheng; Chow, G. M. [Department of Materials Science and Engineering, National University of Singapore, 117575 Singapore (Singapore)] [Department of Materials Science and Engineering, National University of Singapore, 117575 Singapore (Singapore); Venkatesan, T. [NUSNNI-Nanocore, National University of Singapore, 117411 Singapore (Singapore) [NUSNNI-Nanocore, National University of Singapore, 117411 Singapore (Singapore); Department of Physics, National University of Singapore, 117542 Singapore (Singapore); Department of Electrical and Computer Engineering, National University of Singapore, 117575 Singapore (Singapore)

2014-04-15T23:59:59.000Z

436

SANS (small-angle neutron scattering) from tetradecylpyridinium bromide based microemulsions  

SciTech Connect (OSTI)

Small-angle neutron scattering is used to investigate tetradecylpyridinium bromide/pentanol/heptane/heavy water microemulsions in the water-in-oil (W/O) microemulsion phase diagram region. The heavy water content is increased while the other components (surfacant, cosurfactant, hydrocarbon) are kept constant. With use of a simple model assuming spherical micelles interacting with a hard-sphere potential (Percus-Yevick model), aggregate sizes and packing fractions have been extracted and found to agree with values determined from the mixing conditions. These experiments clearly show the transition from the single-particle (heavy water + Stern layer droplet) scattering regime at low water concentration to the mixed single/interdroplet scattering regime when the intermicellar distance becomes comparable to the size of the micelles.

Lindemuth, P.M.; Venable, R.L. (Univ. of Missouri, Rolla (USA)); Hammouda, B. (Univ. of Missouri, Columbia (USA))

1990-10-18T23:59:59.000Z

437

Resonant Soft X-Ray Contrast Variation Methods as Composition-Specific Probes of Thin Polymer Film Structure  

SciTech Connect (OSTI)

We have developed complementary soft x-ray scattering and reflectometry techniques that allow for the morphological analysis of thin polymer films without resorting to chemical modification or isotopic 2 labeling. With these techniques, we achieve significant, x-ray energy-dependent contrast between carbon atoms in different chemical environments using soft x-ray resonance at the carbon edge. Because carbon-containing samples absorb strongly in this region, the scattering length density depends on both the real and imaginary parts of the atomic scattering factors. Using a model polymer film of poly(styrene-b-methyl methacrylate), we show that the soft x-ray reflectivity data is much more sensitive to these atomic scattering factors than the soft x-ray scattering data. Nevertheless, fits to both types of data yield useful morphological details on the polymer?slamellar structure that are consistent with each other and with literature values.

Welch, Cynthia; Welch, Cynthia F.; Hjelm, Rex P.; Mang, Joseph T.; Hawley, Marilyn E.; Wrobleski, Debra A.; Orler, E. Bruce; Kortright, Jeffrey B

2008-04-04T23:59:59.000Z

438

X-ray Observations of Mrk 231  

E-Print Network [OSTI]

This paper presents new X-ray observations of Mrk 231, an active galaxy of particular interest due to its large infrared luminosity and the presence of several blueshifted broad absorption line (BAL) systems, a phenomenon observed in a small fraction of QSOs. A ROSAT HRI image of Mrk 231 is presented, this shows an extended region of soft X-ray emission, covering several tens of kpc, consistent with the extent of the host galaxy. An ASCA observation of Mrk 231 is also presented. Hard X-rays are detected but the data show no significant variability in X-ray flux. The hard X-ray continuum is heavily attenuated and X-ray column estimates range from ~ 2 x 10^{22} - 10^{23} cm^{-2} depending on whether the material is assumed to be neutral or ionized, and on the model assumed for the extended X-ray component. These ASCA data provide only the second hard X-ray spectrum of a BAL AGN presented to date. The broad-band spectral-energy-distribution of the source is discussed. While Mrk 231 is X-ray weak compared to Seyfert 1 galaxies, it has an optical-to-X-ray spectrum typical of a QSO.

T. J. Turner

1998-08-10T23:59:59.000Z

439

Diffuse Scattering  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Diffuse Scattering Diffuse Scattering * Anticipatory (trick) question: If you have an x-ray or neutron detector looking at a small sample volume, which will scatter more x- rays or neutrons into the detector 1 atom 100 atoms or 1000 atoms? X-ray or neutron beam Answer: Depends! Diffuse Scattering Gene E. Ice Materials Science and Technology Division Oak Ridge National Laboratory, USA National School on Neutron and X-ray Scattering ORNL/SNS June 2011 Presentation concentrates year graduate-level course into 1 hour * Skip mathematical complexities * Expose to range of applications * Develop intuition for length scales * Talk like x-ray/neutron scattering guru - Reciprocal space - Debye Temperature - Laue monotonic - Krivoglaz defects of 1st/2nd kinds! Great for cocktail parties or impressing attractive strangers-

440

An experimental measurement of metal multilayer x-ray reflectivity degradation due to intense x-ray flux  

SciTech Connect (OSTI)

The degradation of the x-ray reflection characteristics of metal multilayer Bragg diffractors due to intense x-ray flux was investigated. The Z-pinch plasma produced by PROTO II of Sandia National Laboratories, Albuquerque, New Mexico, was used as the source. The plasma generated total x-ray yields of as much as 40 kJ with up to 15 kJ in the neon hydrogen- and helium-like resonance lines in nominal 20-ns pulses. Molybdenum-carbon, palladium-carbon, and tungsten-carbon metal multilayers were placed at 15 and 150 cm from the plasma center. The multilayers were at nominal angles of 5/sup 0/ and 10/sup 0/ to diffract the neon resonance lines. The time-integrated x-ray reflection of the metal multilayers was monitored by x-ray film. A fluorescer-fiber optic-visible streak camera detector system was then used to monitor the time-resolved x-ray reflection characteristics of 135 A- 2d tungsten-carbon multilayers. A large specular component in the reflectivity prevented determination of the rocking curve of the multilayer. For a neon implosion onto a vanadium-doped polyacrylic acid foam target shot, detailed modeling was attempted. The spectral flux was determined with data from 5 XRD channels and deconvolved using the code SHAZAM. The observed decay in reflectivity was assumed to correspond to the melting of the first tungsten layer. A ''conduction factor'' of 82 was required to manipulate the heat loading of the first tungsten layer such that the time of melting corresponded to the observed decay. The power at destruction was 141 MW/cm/sup 2/ and the integrated energy at destruction was 2.0 J/cm/sup 2/. 82 refs., 66 figs., 10 tabs.

Hockaday, M.Y.P.

1987-06-01T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


441

Small Angle Neutron Scattering for the Structural Study of Intrinsically Disordered Proteins in Solution: A Practical Guide  

Science Journals Connector (OSTI)

Small angle neutron scattering (SANS) allows studying bio-macromolecular structures and interactions in solution. It is particularly well-suited to study structural properties of intrinsically disordered proteins

Frank Gabel

2012-01-01T23:59:59.000Z

442

TheK-shell ionization induced by protons: Projectile scattering angle and electronic relativistic effects in the SCA calculations  

Science Journals Connector (OSTI)

The behaviour ofK-shell ionization probabilities for heavy charged projectiles scattered at large angles is investigated in the SCA with hyperbolic trajectories and both relativistic and nonrelativistic functions...

O. Aashamar; L. Kocbach

1976-01-01T23:59:59.000Z

443

Hard x-ray imaging from explorer  

SciTech Connect (OSTI)

Coded aperture X-ray detectors were applied to obtain large increases in sensitivity as well as angular resolution. A hard X-ray coded aperture detector concept is described which enables very high sensitivity studies persistent hard X-ray sources and gamma ray bursts. Coded aperture imaging is employed so that approx. 2 min source locations can be derived within a 3 deg field of view. Gamma bursts were located initially to within approx. 2 deg and X-ray/hard X-ray spectra and timing, as well as precise locations, derived for possible burst afterglow emission. It is suggested that hard X-ray imaging should be conducted from an Explorer mission where long exposure times are possible.

Grindlay, J.E.; Murray, S.S.

1981-11-01T23:59:59.000Z

444

Development of x-ray photoelectron microscope with an x-ray laser source  

Science Journals Connector (OSTI)

We have constructed an x-ray photoelectron microscopic system with an x-ray laser as an x-ray source. The lasing line is the Li-like Al 3d-4f transition at 15.47 nm where the recombining Al plasma is used as the x-ray laser medium. The beam from the x-ray laser cavity was then focused by using a Schwarzschild mirror coated with Mo/Si multilayers. The x-ray beam size with a diameter less than 0.5 ?m and the estimated photon number of about 210 6 ? photons/shot into the spot were achieved.

Tadayuki Ohchi; Naohiro Yamaguchi; Chiemi Fujikawa; Tamio Hara; Katsumi Watanabe; Ibuki Tanaka; Masami Taguchi

2000-01-01T23:59:59.000Z

445

On the variation of solar flare coronal x-ray source sizes with energy  

E-Print Network [OSTI]

Observations with {\\em RHESSI} have enabled the detailed study of the structure of dense hard X-ray coronal sources in solar flares. The variation of source extent with electron energy has been discussed in the context of streaming of non-thermal particles in a one-dimensional cold-target model, and the results used to constrain both the physical extent of, and density within, the electron acceleration region. Here we extend this investigation to a more physically realistic model of electron transport that takes into account the finite temperature of the ambient plasma, the initial pitch-angle distribution of the accelerated electrons, and the effects of collisional pitch-angle scattering. The finite temperature results in the thermal diffusion of electrons, that leads to the observationally-inferred value of the acceleration region volume being an overestimate of its true value. The different directions of the electron trajectories, a consequence of both the non-zero injection pitch-angle and scattering with...

Jeffrey, Natasha L S; Bian, Nicolas H; Emslie, A Gordon

2014-01-01T23:59:59.000Z

446

Xray and neutron diffraction studies and MD simulation of atomic configurations in polyamorphic Y2O3-Al2O3 systems  

Science Journals Connector (OSTI)

...McMillan and David C. Clary X-ray and neutron diffraction studies and MD simulation...new results of structural studies using neutron and high-energy X-ray diffraction...pair-correlation functions obtained from X-ray and neutron scattering data. Unexpectedly large density...

2005-01-01T23:59:59.000Z

447

Polarization Dependent High Energy Resolution X-ray Absorption Study of Dicesium Uranyl Tetrachloride  

Science Journals Connector (OSTI)

Tonya Vitova *, Jennifer C. Green , Robert G. Denning , Matthias Lble , Kristina Kvashnina , Joshua J. Kas ?, Kevin Jorissen ?, John J. Rehr ?, Thomas Malcherek ?, and Melissa A. Denecke ... This study confirms theoretically predicted electronic transitions to U 6dxy (6d?) orbital and measures relative energies of U 5f?, 5f?, 5f?, and 5f? orbitals of oriented uranyl (UVIO22+) in the same spectrum with remarkable energy resolution. ... We have obtained angle-resolved electronic structure information for oriented Cs2UO2Cl4 crystal, specifically relative energies of 5f and 6d valence orbitals probed with extraordinary energy resolution by polarization dependent high energy resolution X-ray absorption near edge structure (PD-HR-XANES) and compare these with predictions from quantum chemical Amsterdam density functional theory (ADF) and ab initio real space multiple-scattering Greens function based FEFF codes. ...

Tonya Vitova; Jennifer C. Green; Robert G. Denning; Matthias Lble; Kristina Kvashnina; Joshua J. Kas; Kevin Jorissen; John J. Rehr; Thomas Malcherek; Melissa A. Denecke

2014-12-08T23:59:59.000Z

448

Solar Hard X-ray Source Sizes in a Beam-Heated and Ionised Chromosphere  

E-Print Network [OSTI]

Solar flare hard X-rays (HXRs) are produced as bremsstrahlung when an accelerated population of electrons interacts with the dense chromospheric plasma. HXR observations presented by using the Ramaty High-Energy Solar Spectroscopic Imager (RHESSI) have shown that HXR source sizes are 3-6 times more extended in height than those predicted by the standard collisional thick target model (CTTM). Several possible explanations have been put forward including the multi-threaded nature of flare loops, pitch-angle scattering, and magnetic mirroring. However, the nonuniform ionisation (NUI) structure along the path of the electron beam has not been fully explored as a solution to this problem. Ionised plasma is known to be less effective at producing nonthermal bremsstrahlung HXRs when compared to neutral plasma. If the peak HXR emission was produced in a locally ionised region within the chromosphere, the intensity of emission will be preferentially reduced around this peak, resulting in a more extended source. Due to...

O'Flannagain, A; Gallagher, P T

2014-01-01T23:59:59.000Z

449

Applications of soft x-ray lasers  

SciTech Connect (OSTI)

The high brightness and short pulse duration of soft x-ray lasers provide unique advantages for novel applications. Imaging of biological specimens using x-ray lasers has been demonstrated by several groups. Other applications to fields such as chemistry, material science, plasma diagnostics, and lithography are beginning to emerge. We review the current status of soft x-ray lasers from the perspective of applications, and present an overview of the applications currently being developed.

Skinner, C.H.

1993-08-01T23:59:59.000Z

450

High speed x-ray beam chopper  

DOE Patents [OSTI]

A fast, economical, and compact x-ray beam chopper with a small mass and a small moment of inertia whose rotation can be synchronized and phase locked to an electronic signal from an x-ray source and be monitored by a light beam is disclosed. X-ray bursts shorter than 2.5 microseconds have been produced with a jitter time of less than 3 ns.

McPherson, Armon (Oswego, IL); Mills, Dennis M. (Naperville, IL)

2002-01-01T23:59:59.000Z

451

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma  

E-Print Network [OSTI]

X-ray laser frequency near-doubling and generation of tunable coherent x rays in plasma P. L plasmas in which efficient x-ray laser frequency near-doubling is expected for a number of available x-ray of coherent x rays and tunable optical radiation may result in tunable coherent x-ray radiation powerful

Kaplan, Alexander

452

Direct proof of a "more-than-single-layered" peptidoglycan architecture of Escherichia coli W7: a neutron small-angle scattering study.  

Science Journals Connector (OSTI)

...sacculus obtained by using a small-angle neutron scattering technique. A comparison of the hydrogenated...used as a measurement for background in the neutron scattering studies. Neutron scattering data collection and evaluation. Small...

H Labischinski; E W Goodell; A Goodell; M L Hochberg

1991-01-01T23:59:59.000Z

453

Colloid Coalescence with Focused X Rays  

SciTech Connect (OSTI)

We show direct evidence that focused x rays enable us to merge polymer colloidal particles at room temperature. This phenomenon is ascribed to the photochemical scission of colloids with x rays, reducing the molecular weight, glass transition temperature, surface tension, and viscosity of colloids. The observation of the neck bridge growth with time shows that the x-ray-induced colloid coalescence is analogous to viscoelastic coalescence. This finding suggests a feasible protocol of photonic nanofabrication by sintering or welding of polymers, without thermal damage, using x-ray photonics.

Weon, B. M.; Kim, J. T.; Je, J. H. [X-ray Imaging Center, Department of Materials Science and Engineering, Pohang University of Science and Technology, Pohang, 790-784 (Korea, Republic of); Yi, J. M. [Samsung Advanced Institute of Technology, Yongin, Gyeonggi, 446-712 (Korea, Republic of); Wang, S.; Lee, W.-K. [Advanced Photon Source, Argonne National Laboratory, Argonne, Illinois 60439 (United States)

2011-07-01T23:59:59.000Z

454

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE  

E-Print Network [OSTI]

X-RAY MICROBEAM SPEECH PRODUCTION DATABASE USER'S HANDBOOK Version 1.0 (June 1994) prepared by John . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Chapter Two: XRMB History

455

X-ray laser microscope apparatus  

DOE Patents [OSTI]

A microscope consisting of an x-ray contact microscope and an optical microscope. The optical, phase contrast, microscope is used to align a target with respect to a source of soft x-rays. The source of soft x-rays preferably comprises an x-ray laser but could comprise a synchrotron or other pulse source of x-rays. Transparent resist material is used to support the target. The optical microscope is located on the opposite side of the transparent resist material from the target and is employed to align the target with respect to the anticipated soft x-ray laser beam. After alignment with the use of the optical microscope, the target is exposed to the soft x-ray laser beam. The x-ray sensitive transparent resist material whose chemical bonds are altered by the x-ray beam passing through the target mater GOVERNMENT LICENSE RIGHTS This invention was made with government support under Contract No. De-FG02-86ER13609 awarded by the Department of Energy. The Government has certain rights in this invention.

Suckewer, Szymon (Princeton, NJ); DiCicco, Darrell S. (Plainsboro, NJ); Hirschberg, Joseph G. (Coral Gables, FL); Meixler, Lewis D. (East Windsor, NJ); Sathre, Robert (Princeton, NJ); Skinner, Charles H. (Lawrenceville, NJ)

1990-01-01T23:59:59.000Z

456

Automation in X-Ray Crystallography  

Science Journals Connector (OSTI)

Automation in X-Ray Crystallography ... But in the past few years, automation procedures have been applied to intrinsically superior experimental methods. ...

S.C. ABRAHAMS

1963-06-03T23:59:59.000Z

457

X-Ray Laser Sources for Microscopy  

Science Journals Connector (OSTI)

Progress and prospects in soft X-ray laser development at Princeton are presented. A comparison to plasma and synchrotron sources is made with a...

C. H. Skinner; D. E. Kim; A. Wouters; D. Voorhees; S. Suckewer

1988-01-01T23:59:59.000Z

458

Compound refractive X-ray lens  

DOE Patents [OSTI]

An apparatus and method for focusing X-rays. In one embodiment, his invention is a commercial-grade compound refractive X-ray lens. The commercial-grade compound refractive X-ray lens includes a volume of low-Z material. The volume of low-Z material has a first surface which is adapted to receive X-rays of commercially-applicable power emitted from a commercial-grade X-ray source. The volume of low-Z material also has a second surface from which emerge the X-rays of commercially-applicable power which were received at the first surface. Additionally, the commercial-grade compound refractive X-ray lens includes a plurality of openings which are disposed between the first surface and the second surface. The plurality of openings are oriented such that the X-rays of commercially-applicable power which are received at the first surface, pass through the volume of low-Z material and through the plurality openings. In so doing, the X-rays which emerge from the second surface are refracted to a focal point.

Nygren, David R. (Berkeley, CA); Cahn, Robert (Walnut Creek, CA); Cederstrom, Bjorn (Traellborg, SE); Danielsson, Mats (Stocksund, SE); Vestlund, Jonas (Stockholm, SE)

2000-01-01T23:59:59.000Z

459

X-Ray Science Division (XSD)  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

X-Ray Science Division (XSD) Search Button About Welcome Overview Visiting the APS Mission & Goals Find People Organization Charts Committees Job Openings User Information...

460

CHANDRA PHASE-RESOLVED X-RAY SPECTROSCOPY OF THE CRAB PULSAR  

SciTech Connect (OSTI)

We present a new study of the X-ray spectral properties of the Crab Pulsar. The superb angular resolution of the Chandra X-Ray Observatory enables distinguishing the pulsar from the surrounding nebulosity. Analysis of the spectrum as a function of pulse phase allows the least-biased measure of interstellar X-ray extinction due primarily to photoelectric absorption and secondarily to scattering by dust grains in the direction of the Crab Nebula. We modify previous findings that the line of sight to the Crab is underabundant in oxygen and provide measurements with improved accuracy and less bias. Using the abundances and cross sections from Wilms et al. we find [O/H] = (5.28 {+-} 0.28) Multiplication-Sign 10{sup -4} (4.9 Multiplication-Sign 10{sup -4} is solar abundance). We also measure for the first time the impact of scattering of flux out of the image by interstellar grains. We find {tau}{sub scat} = 0.147 {+-} 0.043. Analysis of the spectrum as a function of pulse phase also measures the X-ray spectral index even at pulse minimum-albeit with increasing statistical uncertainty. The spectral variations are, by and large, consistent with a sinusoidal variation. The only significant variation from the sinusoid occurs over the same phase range as some rather abrupt behavior in the optical polarization magnitude and position angle. We also compare these spectral variations to those observed in gamma-rays and conclude that our measurements are both a challenge and a guide to future modeling and will thus eventually help us understand pair cascade processes in pulsar magnetospheres. The data are also used to set new, and less biased, upper limits to the surface temperature of the neutron star for different models of the neutron star atmosphere. We discuss how such data are best connected to theoretical models of neutron star cooling and neutron star interiors. The data restrict the neutrino emission rate in the pulsar core and the amount of light elements in the heat-blanketing envelope. The observations allow the pulsar, irrespective of the composition of its envelope, to have a neutrino emission rate higher than {approx}0.2 of the standard rate of a non-superfluid star cooling via the modified Urca process. The observations also allow the rate to be lower but now with a limited amount of accreted matter in the envelope.

Weisskopf, Martin C.; Tennant, Allyn F.; O'Dell, Stephen L.; Elsner, Ronald F. [Space Sciences Department, NASA Marshall Space Flight Center, VP62, Huntsville, AL 35812 (United States); Yakovlev, Dmitry G. [Ioffe Physical Technical Institute, Politechnischeskaya 26, 194021 St. Petersburg (Russian Federation); Harding, Alice [NASA Goddard Space Flight Center, 8800, College Park, MD 20771 (United States); Zavlin, Vyacheslav E. [NASA Marshall Space Flight Center, Universities Space Research Association, VP62, Huntsville, AL 35812 (United States); Becker, Werner [Max-Planck-Institut fuer Extraterrestrische Physik, 85740 Garching bei Muenchen (Germany)

2011-12-20T23:59:59.000Z

Note: This page contains sample records for the topic "angle x-ray scattering" from the National Library of EnergyBeta (NLEBeta).
While these samples are representative of the content of NLEBeta,
they are not comprehensive nor are they the most current set.
We encourage you to perform a real-time search of NLEBeta
to obtain the most current and comprehensive results.


461

Measurement of the analysing power in proton-proton elastic scattering at small angles  

E-Print Network [OSTI]

The proton analysing power in $\\vec{p}p$ elastic scattering has been measured at small angles at COSY-ANKE at 796 MeV and five other beam energies between 1.6 and 2.4 GeV using a polarised proton beam. The asymmetries obtained by detecting the fast proton in the ANKE forward detector or the slow recoil proton in a silicon tracking telescope are completely consistent. Although the analysing power results agree well with the many published data at 796 MeV, and also with the most recent partial wave solution at this energy, the ANKE data at the higher energies lie well above the predictions of this solution at small angles. An updated phase shift analysis that uses the ANKE results together with the World data leads to a much better description of these new measurements.

Z. Bagdasarian; D. Chiladze; S. Dymov; A. Kacharava; G. Macharashvili; S. Barsov; R. Gebel; B. Gou; M. Hartmann; I. Keshelashvili; A. Khoukaz; P. Kulessa; A. Kulikov; A. Lehrach; N. Lomidze; B. Lorentz; R. Maier; D. Mchedlishvili; S. Merzliakov; S. Mikirtychyants; M. Nioradze; H. Ohm; M. Papenbrock; D. Prasuhn; F. Rathmann; V. Serdyuk; V. Shmakova; R. Stassen; H. Stockhorst; I. I. Strakovsky; H. Strher; M. Tabidze; A. Tschner; S. Trusov; D. Tsirkov; Yu. Uzikov; Yu. Valdau; C. Wilkin; R. L. Workman

2014-09-30T23:59:59.000Z

462

X-ray photon correlation spectroscopy under flow  

E-Print Network [OSTI]

X-ray photon correlation spectroscopy was used to probe the diffusive dynamics of colloidal particles in a shear flow. Combining X-ray techniques with microfluidics is an experimental strategy that reduces the risk of x-ray induced beam damage and also allows time-resolved studies of processes taking place in flowcells. The experimental results and theoretical predictions presented here, show that in the low shear limit, for a ``transverse flow'' scattering geometry (scattering wave vector q perpendicular to the direction of flow) the measured relaxation times are independent of the flow rate and determined only by the diffusive motion of the particles. This is not generally valid and in particular, for a ``longitudinal flow'' (q || flow) scattering geometry, the relaxation times are strongly affected by the flow-induced motion of the particles. Our results show that the Brownian diffusion of colloidal particles can be measured in a flowing sample and that, up to flux limitations, the experimental conditions under which this is possible are easier to achieve at higher values of q.

Andrei Fluerasu; Abdellatif Moussaid; Henri Gleyzolle; Peter Falus; Anders Madsen

2008-03-10T23:59:59.000Z

463

Patchy worm-like micelles: solution structure studied by small-angle neutron scattering  

E-Print Network [OSTI]

Triblock terpolymers exhibit a rich self-organization behavior including the formation of fascinating cylindrical core-shell structures with a phase separated corona. After crystallization-induced self-assembly of polystryrene-(block)-polyethylene-(block)-poly(methyl methacrylate) triblock terpolymers (abbreviated as SEMs = Styrene-Ethylene-Methacrylates) from solution, worm-like core-shell micelles with a patchy corona of polystryrene and poly(methyl methacrylate) were observed by transmission electron microscopy. However, the solution structure is still a matter of debate. Here, we present a method to distinguish in-situ between a Janus-type (two faced) and a patchy (multiple compartments) configuration of the corona. To discriminate between both models the scattering intensity must be determined mainly by one corona compartment. Contrast variation in small-angle neutron scattering enables us to focus on one compartment of the SEMs. The results validate the existence of the patchy structure also in solution.

S. Rosenfeldt; F. Luedel; C. Schulreich; T. Hellweg; A. Radulescu; J. Schmelz; H. Schmalz; L. Harnau

2012-09-20T23:59:59.000Z

464

On the analysis of small?angle scattering with elliptical azimuthal symmetry  

Science Journals Connector (OSTI)

Inhomogeneities which have azimuthal symmetry around some unique axis exhibit small?angle neutron scattering with elliptical symmetry. It is not necessary that these inhomogeneities have an ellipsoidal shape. The model of Debye e t a l. has been generalized to incorporate an anisotropic correlation length having this symmetry. A method is given for fitting two?dimensional intensity data to this model. This is illustrated by data taken for sections of slate and shale rock cut normal to the direction of the bedding planes and which exhibit both large? and small?pore anisotropies.

Peter L. Hall; D. F. R. Mildner

1983-01-01T23:59:59.000Z

465

Determination of Interbilayer and Transbilayer Lipid Transfers by Time-Resolved Small-Angle Neutron Scattering  

SciTech Connect (OSTI)

We applied a time-resolved small-angle neutron scattering technique to the vesicle system of dimyristoylphosphatidylcholine for the first time to determine lipid kinetics. The observed kinetics could be explicitly represented by a simple model that includes two independent kinetic parameters, i.e., the rates of transbilayer and interbilayer exchange. This technique is perfectly suited for the determination of lipid exchange kinetics in equilibrium and applicable to evaluation of the activity of the factors relevant to lipid migration, such as translocase and lipid transfer proteins.

Nakano, Minoru; Fukuda, Masakazu; Kudo, Takayuki; Handa, Tetsurou [Graduate School of Pharmaceutical Sciences, Kyoto University, Kyoto 606-8501 (Japan); Endo, Hitoshi [Institute for Solid State Physics, The University of Tokyo, Tokai, 319-1106 (Japan)

2007-06-08T23:59:59.000Z

466

An imaging-plate detector for small-angle neutron scattering  

Science Journals Connector (OSTI)

Small-angle neutron scattering (SANS) measurements have been performed on long-flight-path pinhole-collimation SANS instruments using, as a two-dimensional position-sensitive detector, both a neutron imaging plate, incorporating gadolinium, and a two-step transfer method, with dysprosium foil as the image transfer medium. The reduced pixel size of the imaging plates provides definite advantages over a conventional position-sensitive gas proportional counter in certain specific situations, namely when limited space necessitates a short sample-to-detector distance, when only small samples (comparable in size to the detector pixels) are available, or when used in conjunction with focusing beam optics.

Cheng, Y.T.

2000-10-01T23:59:59.000Z

467

X-ray spectroscopy of neutron star low-mass X-ray binaries  

E-Print Network [OSTI]

In this thesis, I present work spanning a variety of topics relating to neutron star lowmass X-ray binaries (LMXBs) and utilize spectral information from X-ray observations to further our understanding of these sources. ...

Krauss, Miriam Ilana

2007-01-01T23:59:59.000Z

468

Ultraluminous X-ray Sources: The most extreme X-ray binaries  

E-Print Network [OSTI]

1 Ultraluminous X-ray Sources: The most extreme X-ray binaries Luca Zampieri INAF ULXs ­ Lubiana ­ May 11, 2012- LZ #12;6 · X-ray observations of nearby galaxies show a population of pointlike, off-nuclear sources with L >> Ledd for 1 Msun (L>1.0e39 erg/s) UltraLuminous X-ray Sources (e

?umer, Slobodan

469

Aneta Siemiginowska Chandra X-ray Center  

E-Print Network [OSTI]

-ray and gamma-ray · High Energy Sky · Chandra X-ray Observatory · examples of typical X-ray data, · an example of a data analysis process · statistical challenges · what do we learn from the data? #12;What is Astronomy and phenomena do we study and how? Solar System: Sun and sollar wind, planets, moons, asteroids, comets Our

Wolfe, Patrick J.

470

Watershed in X-ray Astronomy  

Science Journals Connector (OSTI)

... extent the article on page 96 of this issue of Nature from the X-ray astronomy group at the Massachusetts Institute of Technology is a record of disappointments. That is ... near the galactic centre. Now that the first satellite to be devoted to X-ray astronomy has been launched, and is apparently working successfully, the MIT article and another from ...

1971-01-08T23:59:59.000Z

471

X-Ray Identification of Element 104  

Science Journals Connector (OSTI)

The daughter x-ray identification technique has been applied to the identification of element 104. The characteristic K-series x rays from the ?-decay daughter isotope, nobelium (Z=102), have been observed in coincidence with ? particles from the decay of 4.5-sec 104257, thus providing an unequivocal determination of the parent atomic number, Z=104.

C. E. Bemis; Jr.; R. J. Silva; D. C. Hensley; O. L. Keller; Jr.; J. R. Tarrant; L. D. Hunt; P. F. Dittner; R. L. Hahn; C. D. Goodman

1973-09-03T23:59:59.000Z

472

Quantitative Measurements of X-ray Intensity  

SciTech Connect (OSTI)

This chapter describes the characterization of several X-ray sources and their use in calibrating different types of X-ray cameras at National Security Technologies, LLC (NSTec). The cameras are employed in experimental plasma studies at Lawrence Livermore National Laboratory (LLNL), including the National Ignition Facility (NIF). The sources provide X-rays in the energy range from several hundred eV to 110 keV. The key to this effort is measuring the X-ray beam intensity accurately and traceable to international standards. This is accomplished using photodiodes of several types that are calibrated using radioactive sources and a synchrotron source using methods and materials that are traceable to the U.S. National Institute of Standards and Technology (NIST). The accreditation procedures are described. The chapter begins with an introduction to the fundamental concepts of X-ray physics. The types of X-ray sources that are used for device calibration are described. The next section describes the photodiode types that are used for measuring X-ray intensity: power measuring photodiodes, energy dispersive photodiodes, and cameras comprising photodiodes as pixel elements. Following their description, the methods used to calibrate the primary detectors, the power measuring photodiodes and the energy dispersive photodiodes, as well as the method used to get traceability to international standards are described. The X-ray source beams can then be measured using the primary detectors. The final section then describes the use of the calibrated X-ray beams to calibrate X-ray cameras. Many of the references are web sites that provide databases, explanations of the data and how it was generated, and data calculations for specific cases. Several general reference books related to the major topics are included. Papers expanding some subjects are cited.

Haugh, M. J., Schneider, M.

2011-09-01T23:59:59.000Z

473

Nondestructive Evaluation on Hydrided LWR Fuel Cladding by Small Angle Incoherent Neutron Scattering of Hydrogen  

SciTech Connect (OSTI)

A non-destructive neutron scattering method was developed to precisely measure the uptake of total hydrogen in nuclear grade Ziraloy-4 cladding. The hydriding apparatus consists of a closed stainless steel vessel that contains Zr alloy specimens and H gas. By controlling the initial H gas pressure in the vessel and the temperature profile, target H concentrations from tens of ppm to a few thousands of wppm have been successfully achieved. Following H charging, the H content of the hydrided specimens was measured using the vacuum hot extraction method (VHE), by which the samples with desired H concentration were selected for the neutron study. Small angle neutron incoherent scattering (SANIS) were performed in the High Flux Isotope Reactor at Oak Ridge national Laboratory (ORNL). Our study indicates that a very small amount ( 20 ppm) H in commercial Zr cladding can be measured very accurately in minutes for a wide range of H concentration by a nondestructive method. The H distribution in a tube sample was obtained by scaling the neutron scattering rate with a factor, which is determined by calibration process with direct chemical analysis method on the specimen. This scale factor can be used for future test with unknown H concentration, thus provide a nondestructive method for absolute H concentration determination.

Yan, Yong [ORNL; Qian, Shuo [ORNL; Littrell, Ken [ORNL; Parish, Chad M [ORNL; Bell, Gary L [ORNL; Plummer, Lee K [ORNL

2013-01-01T23:59:59.000Z

474

Neutron Scattering Tutorials | Neutron Science | ORNL  

Broader source: All U.S. Department of Energy (DOE) Office Webpages (Extended Search)

Neutron Scattering Tutorials SHARE Neutron Scattering Tutorials The following lectures were presented at the 2011 and 2010 National School on Neutron & X-Ray Scattering. This...

475

Potential of a beryllium x-ray lens  

SciTech Connect (OSTI)

The use of refractive lenses for focusing x-ray beams has been the subject of publications since the early 1980s. Detailed calculations have been made for different shapes for the refractive lens: cylindrical, spherical, parabolic, and for a Fresnel-type refractive lens. The main drawback to the use of a single refractive lens to focus x-rays is that the index of refraction (n = 1 {minus} {delta}) is very close to 1, which results in a lens with a very long focal length. Recently Snigerov and others have suggested and experimentally demonstrated, using cylindrical-shaped lenses, that this problem of long focal lengths can be overcome by using many lenses in series. Each lens refracts the photon through a small angle, but the sum of these sequential changes in direction can be moderately larger. This increase in effective refraction angle reduces the focal length of the lens to a few meters or less and makes the multi-element lens a much more useful instrument for focusing x-rays. This paper, annualizes the expected performance of a lens consisting of a series of aligned hollow spheres in a beryllium substrate. The use of hollow spheres rather than hollow cylinders produces focusing of the x rays into a small focal spot in contrast to the single-directional focusing of the hollow cylinders, which produces a line focus. Two multi-element lenses have been constructed: one with 20 1-mm-diameter hollow spheres in an aluminum substrate, and one with 50 hollow spheres, 1 mm in diameter, in a beryllium substrate. Some construction details and calculations of the expected performance, are given for these two multi-element lenses.

Smither, R.K.; Khounsary, A.M.; Xu, S. [Argonne National Lab., IL (United States). Advanced Photon Source

1997-09-01T23:59:59.000Z

476

X-ray Practicals Series 1 Advanced Data Reduction  

E-Print Network [OSTI]

X-ray Practicals Series 1 Advanced Data Reduction Instructor J. Reibenspies, Ph. D. Nattamai Bhuvanesh, Ph.D. Version 1.0.0 #12;X-ray Practicals Series 2 #12;X-ray Practicals Series 3 #12;X-ray is good. The y direction is shifting the most, but the shift is ok #12;X-ray Practicals Series 5 Other

Meagher, Mary

477

Fiber fed x-ray/gamma ray imaging apparatus  

DOE Patents [OSTI]

X-ray/gamma ray imaging apparatus is disclosed for detecting the position, energy, and intensity of x-ray/gamma ray radiation comprising scintillation means disposed in the path of such radiation and capable of generating photons in response to such radiation; first photodetection means optically bonded to the scintillation means and capable of generating an electrical signal indicative of the intensity, and energy of the radiation detected by the scintillation means; second photodetection means capable of generating an electrical signal indicative of the position of the radiation in the radiation pattern; and means for optically coupling the scintillation means to the second photodetection means. The photodetection means are electrically connected to control and storage means which may also be used to screen out noise by rejecting a signal from one photodetection means not synchronized to a signal from the other photodetection means; and also to screen out signals from scattered radiation.

Hailey, Charles J. (San Francisco, CA); Ziock, Klaus-Peter (Livermore, CA)

1992-01-01T23:59:59.000Z

478

X-ray absorption spectroscopy of the cubic and hexagonal polytypes of zinc sulfide B. Gilbert,1,  

E-Print Network [OSTI]

X-ray absorption spectroscopy of the cubic and hexagonal polytypes of zinc sulfide B. Gilbert,1 Received 18 June 2002; published 26 December 2002 We investigate the sensitivity of x-ray absorption. Experimental spectra and multiple-scattering calculations are reported at the major absorption edges

Haskel, Daniel

479

X-ray sources in globular clusters  

E-Print Network [OSTI]

The twelve bright (Lx>10(36) erg/s) X-ray sources in the globular clusters have lower luminosities than the brightest sources in the bulge of our galaxy. The dim (Lx<10(35) erg/s) X-ray sources in globular clusters reach higher luminosities than the cataclysmic variables in the disk of our galaxy. The first difference is a statistical fluke, as comparison with M31 indicates. The second difference is explained because the brightest of the dim sources are not cataclysmic variables, but soft X-ray transients in quiescence. This article describes the BeppoSAX, ROSAT and first Chandra observations leading to these conclusions.

Frank Verbunt

2001-11-22T23:59:59.000Z

480

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art  

E-Print Network [OSTI]

X-Ray Diffraction The X-Ray Diffraction facility is equipped with state-of-the-art diffractometers offering both single crystal and powder X-Ray diffraction. Powder X-Ray Diffraction High resolution data For more details on powder X-Ray analysis contact Dr J Hriljac on 0121 414 4458 or email: j

Birmingham, University of

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481

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray Source  

E-Print Network [OSTI]

Novel X-Ray Imaging Opportunities for the RPI Linear Accelerator's Tunable, Quasi-monochromatic X-ray of an intense, tunable, polarized, and quasi-monochromatic X-ray source has been ongoing at Rensselaer Polytechnic Institute since 2001 [1, 2, 3, 4, 5, 6]. This X-ray source, known as Parametric X-rays (PXR

Danon, Yaron

482

X-Ray Data Booklet X-RAY DATA BOOKLET  

E-Print Network [OSTI]

Electromagnetic Relations Radioactivity and Radiation Protection Useful Formulas CXRO Home | ALS Home | LBL Home Radiation Arthur L. Robinson 2-17 2.3 Operating and Planned Facilities Herman Winick 2-24 #12;3. Scattering of the Elements 5-4 5.3 Electromagnetic Relations 5-11 5.4 Radioactivity and Radiation Protection 5-14 5.5 Useful

Meagher, Mary

483

Towards weighing individual atoms by high-angle scattering of electrons  

E-Print Network [OSTI]

We consider theoretically the energy loss of electrons scattered to high angles when assuming that the primary beam can be limited to a single atom. We discuss the possibility of identifying the isotopes of light elements and of extracting information about phonons in this signal. The energy loss is related to the mass of the much heavier nucleus, and is spread out due to atomic vibrations. Importantly, while the width of the broadening is much larger than the energy separation of isotopes, only the sh