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DOI 10.1016/j.actamat.2004.08.033
Title Nanoparticles of the superconductor MgB{sub 2}: structural characterization and in situ study of synthesis kinetics
Creator/Author Cui Chunxiang [School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130 (China)]. E-mail: cxcui2000@yahoo.com ; Liu Debao [School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130 (China)] ; Shen Yutian [School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130 (China)] ; Sun Jinbin [School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130 (China)] ; Meng Fanbin [School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130 (China)] ; Wang Ru [School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130 (China)] ; Liu Shuangjin [School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130 (China)] ; Greer, A.L. [Department of Materials Science and Metallurgy, University of Cambridge, Cambridge CB2 3QZ (United Kingdom)] ; Chen, S.K. [Department of Materials Science and Metallurgy, University of Cambridge, Cambridge CB2 3QZ (United Kingdom)] ; Glowacki, B.A. [Department of Materials Science and Metallurgy, University of Cambridge, Cambridge CB2 3QZ (United Kingdom)]
Publication Date2004 Dec 01
OSTI IdentifierOSTI ID: 20634814
Other Number(s)Journal ID: ISSN 1359-6454; ACMAFD; TRN: US05R1356078042
Resource TypeJournal Article
Resource RelationJournal Name: Acta Materialia; Journal Volume: 52; Journal Issue: 20; Other Information: DOI: 10.1016/j.actamat.2004.08.033; PII: S1359-6454(04)00503-8; Copyright (c) 2004 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA)
Subject36 MATERIALS SCIENCE; CRYSTAL GROWTH; MAGNESIUM BORIDES; MICROSTRUCTURE; MONOCRYSTALS; NANOSTRUCTURES; REACTION KINETICS; SUPERCONDUCTORS; SYNTHESIS; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION; X-RAY DIFFRACTOMETERS
Description/AbstractSingle-crystal MgB{sub 2} nanoparticles, with diameters in the range 20-100 nm, have been synthesized in situ in the sample chamber of an X-ray diffractometer. The reaction kinetics are analyzed and related to the atomic-level structure of the particles as observed by high-resolution electron microscopy. Synthesis conditions may have a significant influence on microstructure and superconducting properties.
Country of PublicationUnited States
LanguageEnglish
FormatMedium: X; Size: page(s) 5757-5760
System Entry Date2010 Jun 03

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