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Title: Preparation and screening of crystalline inorganic materials

Abstract

Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc. Once prepared, these materials can be screened for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical, or other properties. Thus, the present invention provides methods for the parallel synthesis and analysis of novel materials having useful properties.

Inventors:
 [1];  [2];  [3];  [4];  [5];  [6]
  1. La Jolla, CA
  2. Danville, CA
  3. Palo Alto, CA
  4. {hacek over (n)}o, Gabriel (Baldwin Park, CA)
  5. Fremont, CA
  6. Cupertino, CA
Issue Date:
Research Org.:
Univ. of California (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
985172
Patent Number(s):
7442665
Application Number:
10/772,894
Assignee:
The Regents of the University of California (Oakland, CA); myx Technologies, Inc. (Santa Clara, CA)
Patent Classifications (CPCs):
B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01J - CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
B - PERFORMING OPERATIONS B82 - NANOTECHNOLOGY B82Y - SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
DOE Contract Number:  
AC03-76SF00098
Resource Type:
Patent
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE

Citation Formats

Schultz, Peter G, Xiang, Xiaodong, Goldwasser, Isy, Brice, Sun, Xiao-Dong, and Wang, Kai-An. Preparation and screening of crystalline inorganic materials. United States: N. p., 2008. Web.
Schultz, Peter G, Xiang, Xiaodong, Goldwasser, Isy, Brice, Sun, Xiao-Dong, & Wang, Kai-An. Preparation and screening of crystalline inorganic materials. United States.
Schultz, Peter G, Xiang, Xiaodong, Goldwasser, Isy, Brice, Sun, Xiao-Dong, and Wang, Kai-An. Tue . "Preparation and screening of crystalline inorganic materials". United States. https://www.osti.gov/servlets/purl/985172.
@article{osti_985172,
title = {Preparation and screening of crystalline inorganic materials},
author = {Schultz, Peter G and Xiang, Xiaodong and Goldwasser, Isy and Brice and Sun, Xiao-Dong and Wang, Kai-An},
abstractNote = {Methods and apparatus for the preparation and use of a substrate having an array of diverse materials in predefined regions thereon. A substrate having an array of diverse materials thereon is generally prepared by delivering components of materials to predefined regions on a substrate, and simultaneously reacting the components to form at least two materials. Materials which can be prepared using the methods and apparatus of the present invention include, for example, covalent network solids, ionic solids and molecular solids. More particularly, materials which can be prepared using the methods and apparatus of the present invention include, for example, inorganic materials, intermetallic materials, metal alloys, ceramic materials, organic materials, organometallic materials, non-biological organic polymers, composite materials (e.g., inorganic composites, organic composites, or combinations thereof), etc. Once prepared, these materials can be screened for useful properties including, for example, electrical, thermal, mechanical, morphological, optical, magnetic, chemical, or other properties. Thus, the present invention provides methods for the parallel synthesis and analysis of novel materials having useful properties.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Oct 28 00:00:00 EDT 2008},
month = {Tue Oct 28 00:00:00 EDT 2008}
}

Works referenced in this record:

Generation and screening of an oligonucleotide-encoded synthetic peptide library.
journal, November 1993


A fully programmable system for the study of catalytic gas reactions
journal, October 1985


Low temperature linear magnetic field sensor based on magnetoresistance of the perovskite oxide La–Sr–Co–O
journal, April 1995


Isomerization of Meta-Xylene Over Pentasil-Type Microporous Gallosilicates
journal, April 1992


Applications of raman spectroscopy to heterogeneous catalysis
book, May 1993


DTA apparatus as a catalytic microreactor with on-line analysis of the products
journal, June 1989


Isomerization and hydrolysis reactions of important disaccharides over inorganic heterogeneous catalysts
journal, November 1985


High-Fidelity Raman Imaging Spectrometry: A Rapid Method Using an Acousto-Optic Tunable Filter
journal, August 1992


Compositional Determination of rf Co-Sputtered Multicomponent Systems
journal, January 1971


Applications of Combinatorial Technologies to Drug Discovery. 1. Background and Peptide Combinatorial Libraries
journal, April 1994


At the crossroads of chemistry and immunology: catalytic antibodies
journal, May 1991


Crystallization of ribozymes and small RNA motifs by a sparse matrix approach.
journal, August 1993


Solid-State Chemistry: A A Rediscovered Chemical Frontier
journal, February 1990


Light-directed, spatially addressable parallel chemical synthesis
journal, February 1991


Purification and crystallization of components of the protein-synthesizing system from Thermus thermophilus
journal, March 1991


An automated system for micro-batch protein crystallization and screening
journal, August 1990


Influence of the Synthesis Procedure and Chemical Composition on the Activity of Titanium in Ti-Beta Catalysts
book, January 1994


In-situ Fourier transform infrared studies of reaction mechanisms in heterogeneous catalysis
conference, November 1990


Magnetoresistance in Metallic Crystals of La 1- x Sr x CoO 3
journal, June 1995


Effect of the Reaction Medium on the Metal Microstructure of Nickel-Zeolite Catalysts
book, January 1982


Four-reactor apparatus for chromatographic studies of catalysts and sorbents
journal, July 1982


Applications of Combinatorial Technologies to Drug Discovery. 2. Combinatorial Organic Synthesis, Library Screening Strategies, and Future Directions
journal, May 1994


Lateral-Chain Methylation of Toluene over Boron and/or Zinc Modified Cesium-X Zeolite
book, January 1993


In vitro selection of RNA molecules that bind specific ligands
journal, August 1990


The design and construction of a multichannel microreactor for catalyst evaluation
journal, January 1986


The thermal behavior of crystalline aluminosilicate catalysts
journal, January 1968


High-pressure study of the new Y-Ba-Cu-O superconducting compound system
journal, March 1987


Statistical design of experiments for protein crystal growth and the use of a precrystallization assay
journal, July 1988


Silver, sodium halosodalites: class A sodalites
journal, June 1992


Complex synthetic chemical libraries indexed with molecular tags
journal, December 1993


Electroluminescence in ZnS: Mn x : Cu y rf–Sputtered Films
journal, January 1974


Catalytic antibodies
journal, December 1986


Chemistry of High-Temperature Superconductors
journal, December 1988


Surface Analysis with FT-IR Emission Spectroscopy
journal, May 1992


Selective chemical catalysis by an antibody
journal, December 1986


H- and Cu- Forms of MFI Boralites with Enhanced Number of Skeletal Boron Atoms. Synthesis and Properties
book, January 1994


Integrated enzyme reactor/detector for the determination of multiple substrates by image analysis
journal, September 1993


The effect of grain size on the superconducting transition temperature of the transition metals
journal, October 1969


Preparation of Bifunctional Catalysts by Solid-State ION Exchange in Zeolites and Catalytic Tests
book, January 1993


Searching for peptide ligands with an epitope library
journal, July 1990


Acid-base properties of silica-aluminas: use of 1-butanol dehydration as a test reaction
journal, January 1991


A Combinatorial Method for Generating New Zeolite Frameworks
book, January 1993


Standing temperature waves on electrically heated catalytic ribbons
journal, January 1989


Automated protein crystallization and a new crystal form of a subtilisin:eglin complex
journal, January 1987


An investigation of protein crystallization parameters using successive automated grid searches (SAGS)
journal, July 1988


Ethanol to gasoline process: effect of variables, mechanism, and kinetics
journal, April 1985


Strategies for epitope analysis using peptide synthesis
journal, September 1987


Quantitative structural comparisons of heme protein crystals and solutions using resonance Raman spectroscopy
journal, October 1993


Studies on the Modified Claus Reaction Over Alkaline Faujasites by Simultaneous Infrared, Kinetics, and esr Measurements
book, January 1984


Assembly of combinatorial antibody libraries on phage surfaces: the gene III site.
journal, September 1991


Possible highT c superconductivity in the Ba?La?Cu?O system
journal, June 1986


Calculation of composition of dilute cosputtered multicomponent films
journal, November 1973


Carbon monoxide hydrogenation over Fe/HZSM-5 catalysts. Effect of SiO2/Al2O3 zeolite ratio
journal, March 1993


Vapor Phase Synthesis of Pyridine Bases from Aldehydes and Ammonia Over Pentasil Zeolites
book, January 1994


IR Emission Analysis of Temperature Profiles in Pt/SiO2 Catalysts during Exothermic Reactions
journal, October 1987


Peptides on phage: a vast library of peptides for identifying ligands
journal, August 1990


Magnetic compounds wtth perovskite structure III. ferromagnetic compounds of cobalt
journal, January 1953


Characterization of highly dealuminated faujasite-type zeolites: ultrastable zeolite Y and ZSM-20
journal, September 1993


Rationalizers and inventors in the drive for technical progress
journal, July 1969


Synthesis, Characterization, and Catalytic Properties of Metallo-Titanium Silicate Molecular Sieves with MEL Topology
journal, January 1994


Crystallization and preliminary characterization of mitogillin, a ribosomal ribonuclease from Aspergillus restrictus
journal, April 1991


Two approaches to the rapid screening of crystallization conditions
journal, August 1992


Evaluation of peptide libraries: An iterative strategy to analyze the reactivity of peptide mixtures with antibodies
journal, November 1992


Microstructural Study of an Iron Silicate Catalyst by Electron Microscopy
book, October 1989


Selectivity over unifunctional multicomponent catalysts with non-uniform distribution of components
journal, February 1985


Time-Resolved and Two-Dimensional NIR FT-Raman Spectroscopy
journal, September 1993


Rapid Scanning Raman Spectroscopy
journal, January 1968


In situ infrared measurements during hot filament CVD of diamond in a rotating substrate reactor
journal, April 1996


Unattended, robotic drug-release testing of enterically coated aspirin
journal, August 1986


The combinatorial synthesis and chemical and biological evaluation of a 1,4-benzodiazepine library.
journal, May 1994


Two-dimensional crystallization of a bacterial surface protein on lipid vesicles under controlled conditions
journal, January 1992


Thousandfold Change in Resistivity in Magnetoresistive La-Ca-Mn-O Films
journal, April 1994


Random peptide libraries: a source of specific protein binding molecules
journal, July 1990


Superconductivity at 93 K in a new mixed-phase Y-Ba-Cu-O compound system at ambient pressure
journal, March 1987


Infrared Thermographic Screening of Combinatorial Libraries of Heterogeneous Catalysts
journal, January 1996


A new type of synthetic peptide library for identifying ligand-binding activity
journal, November 1991


Comparison of protein structure in crystals and in solution by laser Raman scattering
journal, June 1973


Radio‐Frequency‐Sputtered Films of β‐Tungsten Structure Compounds
journal, November 1970


Generation and use of synthetic peptide combinatorial libraries for basic research and drug discovery
journal, November 1991


Characterization and deactivation of NiOThO2 catalysts
journal, March 1989


A Class of Cobalt Oxide Magnetoresistance Materials Discovered with Combinatorial Synthesis
journal, October 1995


Photochemical Preparation of a Film-Based Catalyst with Spatial Control
journal, March 1994