Method for removing oxide contamination from titanium diboride powder
Abstract
A method for removing oxide contamination from titanium diboride powder involves the direct chemical treatment of TiB.sub.2 powders with a gaseous boron halide, such as BCl.sub.3, at temperatures in the range of 500.degree.-800.degree. C. The BCl.sub.3 reacts with the oxides to form volatile species which are removed by the BCl.sub.3 exit stream.
- Inventors:
-
- Oak Ridge, TN
- Issue Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- OSTI Identifier:
- 865032
- Patent Number(s):
- 4452767
- Assignee:
- United States of America as represented by United States (Washington, DC)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01B - NON-METALLIC ELEMENTS
- DOE Contract Number:
- W-7405-ENG-26
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- method; removing; oxide; contamination; titanium; diboride; powder; involves; direct; chemical; treatment; tib; powders; gaseous; boron; halide; bcl; temperatures; range; 500; degree; -800; reacts; oxides; form; volatile; species; removed; exit; stream; form volatile; titanium diboride; chemical treatment; oxide contamination; removing oxide; direct chemical; diboride powder; gaseous boron; /423/501/
Citation Formats
Brynestad, Jorulf, and Bamberger, Carlos E. Method for removing oxide contamination from titanium diboride powder. United States: N. p., 1984.
Web.
Brynestad, Jorulf, & Bamberger, Carlos E. Method for removing oxide contamination from titanium diboride powder. United States.
Brynestad, Jorulf, and Bamberger, Carlos E. Sun .
"Method for removing oxide contamination from titanium diboride powder". United States. https://www.osti.gov/servlets/purl/865032.
@article{osti_865032,
title = {Method for removing oxide contamination from titanium diboride powder},
author = {Brynestad, Jorulf and Bamberger, Carlos E},
abstractNote = {A method for removing oxide contamination from titanium diboride powder involves the direct chemical treatment of TiB.sub.2 powders with a gaseous boron halide, such as BCl.sub.3, at temperatures in the range of 500.degree.-800.degree. C. The BCl.sub.3 reacts with the oxides to form volatile species which are removed by the BCl.sub.3 exit stream.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Sun Jan 01 00:00:00 EST 1984},
month = {Sun Jan 01 00:00:00 EST 1984}
}