Photothermal method for in situ microanalysis of the chemical composition of coal samples
Abstract
Successive minute regions along a scan path on a coal sample are individually analyzed, at a series of different depths if desired, to determine chemical composition including the locations, sizes and distributions of different maceral inclusions. A sequence of infrared light pulses of progressively changing wavelengths is directed into each minute region and a probe light beam is directed along the sample surface adjacent the region. Infrared wavelengths at which strong absorption occurs in the region are identified by detecting the resulting deflections of the probe beam caused by thermally induced index of refraction changes in the air or other medium adjacent the region. The detected peak absorption wavelengths are correlated with known characteristic peak absorption wavelengths of specific coal constituents to identify the composition of each such minute region of the sample. The method enables rapid, convenient and non-destructive analyses of coal specimens to facilitate mining, processing and utilization of coals. 2 figures.
- Inventors:
- Issue Date:
- OSTI Identifier:
- 6867935
- Application Number:
- ON: DE84014497
- Assignee:
- Dept. of Energy
- DOE Contract Number:
- W-7405-ENG-48; AC03-76SF00098
- Resource Type:
- Patent
- Resource Relation:
- Other Information: Portions are illegible in microfiche products
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 01 COAL, LIGNITE, AND PEAT; COAL; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; MACERALS; INFRARED SPECTRA; NONDESTRUCTIVE ANALYSIS; PROBES; CARBONACEOUS MATERIALS; ENERGY SOURCES; FOSSIL FUELS; FUELS; MATERIALS; SPECTRA; 010600* - Coal, Lignite, & Peat- Properties & Composition
Citation Formats
Amer, N M. Photothermal method for in situ microanalysis of the chemical composition of coal samples. United States: N. p., 1983.
Web.
Amer, N M. Photothermal method for in situ microanalysis of the chemical composition of coal samples. United States.
Amer, N M. Tue .
"Photothermal method for in situ microanalysis of the chemical composition of coal samples". United States.
@article{osti_6867935,
title = {Photothermal method for in situ microanalysis of the chemical composition of coal samples},
author = {Amer, N M},
abstractNote = {Successive minute regions along a scan path on a coal sample are individually analyzed, at a series of different depths if desired, to determine chemical composition including the locations, sizes and distributions of different maceral inclusions. A sequence of infrared light pulses of progressively changing wavelengths is directed into each minute region and a probe light beam is directed along the sample surface adjacent the region. Infrared wavelengths at which strong absorption occurs in the region are identified by detecting the resulting deflections of the probe beam caused by thermally induced index of refraction changes in the air or other medium adjacent the region. The detected peak absorption wavelengths are correlated with known characteristic peak absorption wavelengths of specific coal constituents to identify the composition of each such minute region of the sample. The method enables rapid, convenient and non-destructive analyses of coal specimens to facilitate mining, processing and utilization of coals. 2 figures.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Oct 25 00:00:00 EDT 1983},
month = {Tue Oct 25 00:00:00 EDT 1983}
}