Method of making a fuel cell polymer electrolyte membrane comprising manganese oxide

Frey, Matthew H.; Hamrock, Steven J.; Haugen, Gregory M.; Pham, Phat T.

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Title: Method of making a fuel cell polymer electrolyte membrane comprising manganese oxide

Abstract

Fuel cell membrane electrode assemblies and fuel cell polymer electrolyte membranes are provided comprising manganese oxides which demonstrate increased durability. Methods of making same are provided.

Inventors:: Frey, Matthew H.; Hamrock, Steven J.; Haugen, Gregory M.; Pham, Phat T.

Issue Date:: Tue Jan 10 00:00:00 EST 2012

Research Org.:: 3M Innovative Properties Company

Sponsoring Org.:: USDOE

OSTI Identifier:: 1531713

Patent Number(s):: 8092954

Application Number:: 12/621,795

Assignee:: 3M Innovative Properties Company (St. Paul, MN)

Patent Classifications (CPCs):: B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY

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B - PERFORMING OPERATIONS B01 - PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL B01D - SEPARATION
B01D2323/12 - Specific ratios of components used
B01D67/0079 - {Formation of membranes comprising organic and inorganic components}
B01D69/141 - {Heterogeneous membranes, e.g. containing dispersed material
B01D71/32 - containing fluorine atoms

H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
H01M8/1023 - having only carbon, e.g. polyarylenes, polystyrenes or polybutadiene-styrenes
H01M8/1039 - halogenated, e.g. sulfonated polyvinylidene fluorides
H01M8/1051 - Non-ion-conducting additives, e.g. stabilisers, SiO2 or ZrO2
H01M8/1081 - starting from solutions, dispersions or slurries exclusively of polymers

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02E - REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
Y02E60/50 - Fuel cells

Y - NEW / CROSS SECTIONAL TECHNOLOGIES Y02 - TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE Y02P - CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
Y02P70/50 - Manufacturing or production processes characterised by the final manufactured product

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DOE Contract Number:: FC36-02AL67621

Resource Type:: Patent

Resource Relation:: Patent File Date: 2009-11-19

Country of Publication:: United States

Language:: English

Subject:: 30 DIRECT ENERGY CONVERSION

Citation Formats


                    Frey, Matthew H., Hamrock, Steven J., Haugen, Gregory M., and Pham, Phat T. Method of making a fuel cell polymer electrolyte membrane comprising manganese oxide.  United States: N. p., 2012. 
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                    Frey, Matthew H., Hamrock, Steven J., Haugen, Gregory M., & Pham, Phat T. Method of making a fuel cell polymer electrolyte membrane comprising manganese oxide.  United States.

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                    Frey, Matthew H., Hamrock, Steven J., Haugen, Gregory M., and Pham, Phat T. Tue .  
        "Method of making a fuel cell polymer electrolyte membrane comprising manganese oxide".  United States.  https://www.osti.gov/servlets/purl/1531713.

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@article{osti_1531713,

  title        = {Method of making a fuel cell polymer electrolyte membrane comprising manganese oxide},

  author       = {Frey, Matthew H. and Hamrock, Steven J. and Haugen, Gregory M. and Pham, Phat T.},

  abstractNote = {Fuel cell membrane electrode assemblies and fuel cell polymer electrolyte membranes are provided comprising manganese oxides which demonstrate increased durability. Methods of making same are provided.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Jan 10 00:00:00 EST 2012},

  month        = {Tue Jan 10 00:00:00 EST 2012}

}

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Works referencing / citing this record:

High durability fuel cell components with cerium salt additives
patent, August 2016

Frey, Matthew H.; Pierpont, Daniel M.; Hamrock, Steven J.
US Patent Document 9,431,670
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/9431670

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Phosphonated polymers, and methods of production thereof, for use as polymer electrolyte membranes (PEMs) and/or catalyst ionomeric binders for electrodes in PEM fuel cells

Patent Park, Eun Joo; Kim, Yu Seung

The present disclosure provides phosphonated polymers that can be used, for example, as polymer electrolyte membranes (PEMs) and/or catalyst ionomeric binders for electrodes in PEM fuel cells, and more particularly for high-temperature PEM fuel cells. High-temperature PEM fuel cells that use phosphonated polymers of the present disclosure suffer from reduced or no acid leaching because, in at least some examples, phosphonic acid moieties are covalently bound to the backbone of the polymers. A phosphonated polymer include a backbone having one or more aromatic monomers, with each aromatic monomer having one or more phosphonic acid groups. A phosphonic acid group maymore » « less
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Method of making chalcogen catalysts for polymer electrolyte fuel cells

Patent Choi, Jong-Ho [Los Alamos, NM]; Zelenay, Piotr [Los Alamos, NM]; Wieckowski, Andrzej [Champaign, IL]; ...

A method of making an electrode catalyst material using aqueous solutions. The electrode catalyst material includes a support comprising at least one transition metal and at least one chalcogen disposed on a surface of the transition metal. The method includes reducing a metal powder, mixing the metal powder with an aqueous solution containing at least one inorganic compound of the chalcogen to form a mixture, and providing a reducing agent to the mixture to form nanoparticles of the electrode catalyst. The electrode catalyst may be used in a membrane electrode assembly for a fuel cell.
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Methods for using novel cathode and electrolyte materials for solid oxide fuel cells and ion transport membranes

Patent Jacobson, Allan J.; Wang, Shuangyan; Kim, Gun Tae

Methods using novel cathode, electrolyte and oxygen separation materials operating at intermediate temperatures for use in solid oxide fuel cells and ion transport membranes include oxides with perovskite related structures and an ordered arrangement of A site cations. The materials have significantly faster oxygen kinetics than in corresponding disordered perovskites.
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Title: Method of making a fuel cell polymer electrolyte membrane comprising manganese oxide

Abstract

Citation Formats

Article having surface layer of uniformly oriented, crystalline, organic microstructures patent, March 1989

Catalyst for membrane electrode assembly and method of making patent, March 2000

Molecule-Substrate Vibration of CO on Ni(100) Studied by Infrared-Emission Spectroscopy journal, February 1984

Proton-conducting ceramic/polymer composite membrane for the temperature range up to 300 degree C patent-application, December 2004

Role of ion-exchange membrane morphology and sorption properties in facilitated transport di-olefin/mono-olefin separations journal, June 1998

High durability fuel cell components with cerium oxide additives patent-application, May 2007

Fuel cell patent-application, January 2003

Method of producing a microstructured surface and the article produced thereby patent, July 1982

Membrane patent, September 1989

Durable fuel cell patent-application, March 2006

Electrochemical cell with improved energy efficiency patent, June 1988

Solid polymer electrolyte membrane electrode assembly and solid polymer electrolyte fuel cell using same patent-application, May 2006

Membrane electrode assembly having annealed polymer electrolyte membrane patent, November 2003

Membrane electrode assembly patent, March 1999

Catalyst for membrane electrode assembly and method of making patent, March 1999

Polymeric membrane electrochemical cell operating at temperatures above 100.degree. C. patent, December 2000

Performance Evaluation of Platinum Dispersed Self-humidifying Polymer Electrolyte Membrane Prepared by Using RF Magnetron Sputter journal, February 2003

Single-film membrane, process for obtaining it and use thereof patent, November 1998

Proton-conducting membrane, method for producing the same, and fuel cell using the same patent, January 2004

Hydrated metal ionomer membranes for gas separation patent, May 1988

Composites and composite membranes patent-application, October 2006

Method of Producing a Membrane Electrode Assembly, and Membrane Electrode Assembly Produced Using this Method, as Well as Associated Fuel Cell Battery patent-application, May 2002

Electrocatalyst for anode patent, July 1993

Toluic acid patent, November 1983

Effect of gravity on copper phthalocyanine thin films III: Microstructure comparisons of copper phthalocyanine thin films grown in microgravity and unit gravity journal, May 1990

Organic thin film controlled molecular epitaxy patent, January 1993

Fabrication of biologically based microstructure composites for vacuum field emission journal, October 1992

Liquid composition, process for its production and process for producing membrane-electrode assembly for polymer electrolyte fuel cells patent-application, January 2006

Process of preparing electrode for fuel cell patent, February 1993

Membrane electrode assemblies with hydrogen peroxide decomposition catalyst patent-application, March 2004

Incorporation and characterisation of oxides of manganese, cobalt and lithium into Nafion 117 membranes journal, January 2001

Constituents and methods for protecting fuel cell components, including PEMS patent-application, March 2006

Solid electrolyte composite for electrochemical reaction apparatus patent, June 2001

Summary Abstract: Dramatic variation of the physical microstructure of a vapor deposited organic thin film journal, July 1987

Solid polymer electrolyte fuel cell patent, December 1995

Fuel cell cathode catalyst patent-application, March 2005

Selective reaction of hexafluoropropylene oxide with perfluoroacyl fluorides patent-application, June 2004

Suboxide Fuel Cell Catalyst for Enhanced Reformate Tolerance patent-application, January 2002

Ion-exchanged transition metal catalysts for the direct oxidation of olefins to epoxyalcohols patent, May 1977

Sulfonic acid electrolytic cell having flourinated polymer membrane with hydration product less than 22,000 patent, November 1982

Constituents and methods for protecting fuel cell components, including PEMs patent, May 2007

Hydrogenation process patent, August 1981

Solid electrolyte composite for electrochemical reaction apparatus patent, October 2003

Polymer solid-electrolyte composition and electrochemical cell using the composition patent, June 1996

Fuel cell durability patent-application, March 2006

Method and Apparatus for Forming High Surface Area Material Films and Membranes patent-application, March 2004

Article with reduced friction polymer sheet support patent, February 1986

Effects of morphology on NO2 detection in air at room temperature with phthalocyanine thin films journal, December 1990

Process for making liquid composition of perfluorinated ion exchange polymer, and product thereof patent, February 1984

Preparation, characterization and catalytic properties of perfluorosulfonated ion-exchange membranes containing surface-concentrated, hydrated ruthenium oxide particles journal, December 1986

Process of preparing solid polymer electrolyte type fuel cell patent, March 1994

Composite article comprising oriented microstructures patent, August 1994

Bipolar membrane and method for its production patent, June 1993

Reinforced composite ionic conductive polymer membrane and fuel cell adopting the same patent-application, February 2002

Isoquinolinedione derivatives, pharmaceutical compositions and methods of use patent, April 1989

Preparation of perfluorinated vinyl ethers having a sulfonyl fluoride end-group patent, September 2003

Reduced degradation of ion-exchange membranes in electrochemical fuel cells patent-application, June 2003

Active solid polymer electrolyte membrane for solid polymer electrolyte fuel cell patent-application, June 2002

Fuel cell patent-application, January 2003

High durability fuel cell components with cerium salt additives patent-application, May 2007

Modified fluorosulfonic acids patent, September 1999

Ternary nanocatalyst and method of making patent-application, April 2007

Nanostructured electrode membranes patent, August 1994

Method for preparing an article having surface layer of uniformly oriented, crystalline, organic microstructures patent, August 1991

Polymer electrolyte membrane patent-application, June 2004

High dispersion and electrocatalytic properties of platinum on well-aligned carbon nanotube arrays journal, January 2004

Fuel cell systems and methods patent, October 2003

Solid polymer electrolyte fuel cell patent, January 2002

Vacuum vapor deposited thin films of a perylene dicarboximide derivative: Microstructure versus deposition parameters journal, May 1988

Composite membrane suitable for use in electrochemical devices patent, May 2000

Solid polymer electrolyte composition patent, June 1998

Electrochemical cell patent-application, March 2004

Electrode composition material for polymer electrolyte fuel cell and process of preparing same patent, June 1998

Membrane electrode assembly patent, November 2001

Proton-conducting ceramic/polymer composite membrane for the temperature range up to 300.degree.C patent-application, July 2002

Proton-conducting membrane, method for producing the same, and fuel cell using the same patent, March 2005

Development of novel self-humidifying composite membranes for fuel cells journal, October 2003

Article having surface layer of uniformly oriented, crystalline, organic microstructures
patent, March 1989

Catalyst for membrane electrode assembly and method of making
patent, March 2000

Molecule-Substrate Vibration of CO on Ni(100) Studied by Infrared-Emission Spectroscopy
journal, February 1984

Proton-conducting ceramic/polymer composite membrane for the temperature range up to 300 degree C
patent-application, December 2004

Role of ion-exchange membrane morphology and sorption properties in facilitated transport di-olefin/mono-olefin separations
journal, June 1998

High durability fuel cell components with cerium oxide additives
patent-application, May 2007

Fuel cell
patent-application, January 2003

Method of producing a microstructured surface and the article produced thereby
patent, July 1982

Membrane
patent, September 1989

Durable fuel cell
patent-application, March 2006

Electrochemical cell with improved energy efficiency
patent, June 1988

Solid polymer electrolyte membrane electrode assembly and solid polymer electrolyte fuel cell using same
patent-application, May 2006

Membrane electrode assembly having annealed polymer electrolyte membrane
patent, November 2003

Membrane electrode assembly
patent, March 1999

Catalyst for membrane electrode assembly and method of making
patent, March 1999

Polymeric membrane electrochemical cell operating at temperatures above 100.degree. C.
patent, December 2000

Performance Evaluation of Platinum Dispersed Self-humidifying Polymer Electrolyte Membrane Prepared by Using RF Magnetron Sputter
journal, February 2003

Single-film membrane, process for obtaining it and use thereof
patent, November 1998

Proton-conducting membrane, method for producing the same, and fuel cell using the same
patent, January 2004

Hydrated metal ionomer membranes for gas separation
patent, May 1988

Composites and composite membranes
patent-application, October 2006

Method of Producing a Membrane Electrode Assembly, and Membrane Electrode Assembly Produced Using this Method, as Well as Associated Fuel Cell Battery
patent-application, May 2002

Electrocatalyst for anode
patent, July 1993

Toluic acid
patent, November 1983

Effect of gravity on copper phthalocyanine thin films III: Microstructure comparisons of copper phthalocyanine thin films grown in microgravity and unit gravity
journal, May 1990

Organic thin film controlled molecular epitaxy
patent, January 1993

Fabrication of biologically based microstructure composites for vacuum field emission
journal, October 1992

Liquid composition, process for its production and process for producing membrane-electrode assembly for polymer electrolyte fuel cells
patent-application, January 2006

Process of preparing electrode for fuel cell
patent, February 1993

Membrane electrode assemblies with hydrogen peroxide decomposition catalyst
patent-application, March 2004

Incorporation and characterisation of oxides of manganese, cobalt and lithium into Nafion 117 membranes
journal, January 2001

Constituents and methods for protecting fuel cell components, including PEMS
patent-application, March 2006

Solid electrolyte composite for electrochemical reaction apparatus
patent, June 2001

Summary Abstract: Dramatic variation of the physical microstructure of a vapor deposited organic thin film
journal, July 1987

Solid polymer electrolyte fuel cell
patent, December 1995

Fuel cell cathode catalyst
patent-application, March 2005

Selective reaction of hexafluoropropylene oxide with perfluoroacyl fluorides
patent-application, June 2004

Suboxide Fuel Cell Catalyst for Enhanced Reformate Tolerance
patent-application, January 2002

Ion-exchanged transition metal catalysts for the direct oxidation of olefins to epoxyalcohols
patent, May 1977

Sulfonic acid electrolytic cell having flourinated polymer membrane with hydration product less than 22,000
patent, November 1982

Constituents and methods for protecting fuel cell components, including PEMs
patent, May 2007

Hydrogenation process
patent, August 1981

Solid electrolyte composite for electrochemical reaction apparatus
patent, October 2003

Polymer solid-electrolyte composition and electrochemical cell using the composition
patent, June 1996

Fuel cell durability
patent-application, March 2006

Method and Apparatus for Forming High Surface Area Material Films and Membranes
patent-application, March 2004

Article with reduced friction polymer sheet support
patent, February 1986

Effects of morphology on NO2 detection in air at room temperature with phthalocyanine thin films
journal, December 1990

Process for making liquid composition of perfluorinated ion exchange polymer, and product thereof
patent, February 1984

Preparation, characterization and catalytic properties of perfluorosulfonated ion-exchange membranes containing surface-concentrated, hydrated ruthenium oxide particles
journal, December 1986

Process of preparing solid polymer electrolyte type fuel cell
patent, March 1994

Composite article comprising oriented microstructures
patent, August 1994

Bipolar membrane and method for its production
patent, June 1993

Reinforced composite ionic conductive polymer membrane and fuel cell adopting the same
patent-application, February 2002

Isoquinolinedione derivatives, pharmaceutical compositions and methods of use
patent, April 1989

Preparation of perfluorinated vinyl ethers having a sulfonyl fluoride end-group
patent, September 2003

Reduced degradation of ion-exchange membranes in electrochemical fuel cells
patent-application, June 2003

Active solid polymer electrolyte membrane for solid polymer electrolyte fuel cell
patent-application, June 2002

Fuel cell
patent-application, January 2003

High durability fuel cell components with cerium salt additives
patent-application, May 2007

Modified fluorosulfonic acids
patent, September 1999

Ternary nanocatalyst and method of making
patent-application, April 2007

Nanostructured electrode membranes
patent, August 1994

Method for preparing an article having surface layer of uniformly oriented, crystalline, organic microstructures
patent, August 1991

Polymer electrolyte membrane
patent-application, June 2004

High dispersion and electrocatalytic properties of platinum on well-aligned carbon nanotube arrays
journal, January 2004

Fuel cell systems and methods
patent, October 2003

Solid polymer electrolyte fuel cell
patent, January 2002

Vacuum vapor deposited thin films of a perylene dicarboximide derivative: Microstructure versus deposition parameters
journal, May 1988

Composite membrane suitable for use in electrochemical devices
patent, May 2000

Solid polymer electrolyte composition
patent, June 1998

Electrochemical cell
patent-application, March 2004

Electrode composition material for polymer electrolyte fuel cell and process of preparing same
patent, June 1998

Membrane electrode assembly
patent, November 2001

Proton-conducting ceramic/polymer composite membrane for the temperature range up to 300.degree.C
patent-application, July 2002

Proton-conducting membrane, method for producing the same, and fuel cell using the same
patent, March 2005

Development of novel self-humidifying composite membranes for fuel cells
journal, October 2003

Class of Electrocatalysts and a Gas Diffusion Electrode Based Thereon for Fuel Cells
patent-application, September 2002

Composite polymer electrolytes for proton exchange membrane fuel cells
patent-application, March 2004

High durability fuel cell components with cerium salt additives
patent, August 2016