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Title: Method of detecting defects in ion exchange membranes of electrochemical cells by chemochromic sensors

Abstract

A method of detecting defects in membranes such as ion exchange membranes of electrochemical cells. The electrochemical cell includes an assembly having an anode side and a cathode side with the ion exchange membrane in between. In a configuration step a chemochromic sensor is placed above the cathode and flow isolation hardware lateral to the ion exchange membrane which prevents a flow of hydrogen (H.sub.2) between the cathode and anode side. The anode side is exposed to a first reactant fluid including hydrogen. The chemochromic sensor is examined after the exposing for a color change. A color change evidences the ion exchange membrane has at least one defect that permits H.sub.2 transmission therethrough.

Inventors:
;
Issue Date:
Research Org.:
University of Central Florida Research Foundation, Inc., Orlando, FL (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1234688
Patent Number(s):
9228954
Application Number:
13/594,163
Assignee:
University of Central Florida Research Foundation, Inc. (Orlando, FL)
Patent Classifications (CPCs):
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
H - ELECTRICITY H01 - BASIC ELECTRIC ELEMENTS H01M - PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
DOE Contract Number:  
FC36-04GO14225
Resource Type:
Patent
Resource Relation:
Patent File Date: 2012 Aug 24
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 30 DIRECT ENERGY CONVERSION

Citation Formats

Brooker, Robert Paul, and Mohajeri, Nahid. Method of detecting defects in ion exchange membranes of electrochemical cells by chemochromic sensors. United States: N. p., 2016. Web.
Brooker, Robert Paul, & Mohajeri, Nahid. Method of detecting defects in ion exchange membranes of electrochemical cells by chemochromic sensors. United States.
Brooker, Robert Paul, and Mohajeri, Nahid. Tue . "Method of detecting defects in ion exchange membranes of electrochemical cells by chemochromic sensors". United States. https://www.osti.gov/servlets/purl/1234688.
@article{osti_1234688,
title = {Method of detecting defects in ion exchange membranes of electrochemical cells by chemochromic sensors},
author = {Brooker, Robert Paul and Mohajeri, Nahid},
abstractNote = {A method of detecting defects in membranes such as ion exchange membranes of electrochemical cells. The electrochemical cell includes an assembly having an anode side and a cathode side with the ion exchange membrane in between. In a configuration step a chemochromic sensor is placed above the cathode and flow isolation hardware lateral to the ion exchange membrane which prevents a flow of hydrogen (H.sub.2) between the cathode and anode side. The anode side is exposed to a first reactant fluid including hydrogen. The chemochromic sensor is examined after the exposing for a color change. A color change evidences the ion exchange membrane has at least one defect that permits H.sub.2 transmission therethrough.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Jan 05 00:00:00 EST 2016},
month = {Tue Jan 05 00:00:00 EST 2016}
}

Works referenced in this record:

Method and apparatus for detecting transfer leaks in fuel cells
patent, November 2002


Hydrogen gas indicator system
patent, May 2005


Photo-oxidation catalysts
patent, July 2009


Gas permeable chemochromic compositions for hydrogen sensing
patent-application, September 2007


Precious Metal Oxide Catalyst for Water Electrolysis
patent-application, October 2014