Method and apparatus for simultaneous spectroelectrochemical analysis
Abstract
An apparatus and method of simultaneous spectroelectrochemical analysis is disclosed. A transparent surface is provided. An analyte solution on the transparent surface is contacted with a working electrode and at least one other electrode. Light from a light source is focused on either a surface of the working electrode or the analyte solution. The light reflected from either the surface of the working electrode or the analyte solution is detected. The potential of the working electrode is adjusted, and spectroscopic changes of the analyte solution that occur with changes in thermodynamic potentials are monitored.
- Inventors:
- Issue Date:
- Research Org.:
- Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1108960
- Patent Number(s):
- 8585880
- Application Number:
- 13/246,090
- Assignee:
- Battelle Memorial Institute (Richland, WA)
- Patent Classifications (CPCs):
-
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- DOE Contract Number:
- AC05-76RL01830
- Resource Type:
- Patent
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION
Citation Formats
Chatterjee, Sayandev, Bryan, Samuel A, Schroll, Cynthia A, and Heineman, William R. Method and apparatus for simultaneous spectroelectrochemical analysis. United States: N. p., 2013.
Web.
Chatterjee, Sayandev, Bryan, Samuel A, Schroll, Cynthia A, & Heineman, William R. Method and apparatus for simultaneous spectroelectrochemical analysis. United States.
Chatterjee, Sayandev, Bryan, Samuel A, Schroll, Cynthia A, and Heineman, William R. Tue .
"Method and apparatus for simultaneous spectroelectrochemical analysis". United States. https://www.osti.gov/servlets/purl/1108960.
@article{osti_1108960,
title = {Method and apparatus for simultaneous spectroelectrochemical analysis},
author = {Chatterjee, Sayandev and Bryan, Samuel A and Schroll, Cynthia A and Heineman, William R},
abstractNote = {An apparatus and method of simultaneous spectroelectrochemical analysis is disclosed. A transparent surface is provided. An analyte solution on the transparent surface is contacted with a working electrode and at least one other electrode. Light from a light source is focused on either a surface of the working electrode or the analyte solution. The light reflected from either the surface of the working electrode or the analyte solution is detected. The potential of the working electrode is adjusted, and spectroscopic changes of the analyte solution that occur with changes in thermodynamic potentials are monitored.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Nov 19 00:00:00 EST 2013},
month = {Tue Nov 19 00:00:00 EST 2013}
}
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
Some examples of the use of thin layer spectroelectrochemistry in the study of electron transfer between metals and enzymes
journal, January 1994
- Comtat, Maurice; Durliat, Hélène
- Biosensors and Bioelectronics, Vol. 9, Issue 9-10
Spectroelectrochemical cell with adjustable solution layer thickness
journal, October 1984
- Porter, Marc D.; Dong, Shaojung.; Gui, Yupeng.
- Analytical Chemistry, Vol. 56, Issue 12
Thin-layer spectroelectrochemical cell
patent, January 2000
- Boss, Pamela A.; Boss, Roger D.
- US Patent Document 6,015,479
A comparison of the specificities of xanthine oxidase and aldehyde oxidase
journal, June 1972
- Krenitsky, Thomas A.; Neil, Shannon M.; Elion, Gertrude B.
- Archives of Biochemistry and Biophysics, Vol. 150, Issue 2
Spectroelectrochemical studies of metal deposition and stripping and of specific adsorption on mercury-platinum optically transparent electrodes
journal, October 1972
- Heineman, William R.; Kuwana, Theodore.
- Analytical Chemistry, Vol. 44, Issue 12
A small-volume thin-layer spectroelectrochemical cell for the study of biological components
journal, January 1979
- Anderson, C. William; Brian Halsall, H.; Heineman, William R.
- Analytical Biochemistry, Vol. 93
Spectroelectrochemistry. Combination of optical and electrochemical techniques for studies of redox chemistry
journal, March 1978
- Heineman, William R.
- Analytical Chemistry, Vol. 50, Issue 3
Micro volume rotating disk electrode (RDE) amperometric detection for a bead-based immunoassay
journal, November 1999
- Wijayawardhana, C. Ajith; Halsall, H. Brian; Heineman, William R.
- Analytica Chimica Acta, Vol. 399, Issue 1-2
Measurement of enzyme E.deg.' values by optically transparent thin layer electrochemical cells
journal, January 1975
- Heineman, William R.; Norris, Barbara J.; Goelz, John F.
- Analytical Chemistry, Vol. 47, Issue 1
High sensitivity internal reflection spectroelectrochemistry for direct monitoring of diffusing species using signal averaging
journal, February 1971
- Winograd, Nicholas.; Kuwana, Theodore.
- Analytical Chemistry, Vol. 43, Issue 2